WQ0035720_Residual Annual Report 2019_20200211

3308 Bernice Avenue
Russellville, AR 72802
PO Box 3036 - Russellville, AR 72811
Phone: [phone]
February 3, 2020
G�FQIQ�R
North Carolina Department of Environment and Natural Resources
p
Division of Water Quality
Information Processing Unit
1617 Mail Service Center Nor ti�r�9 ut��'t
Raleigh, NC 27699-1617 Perm
Subject: 2019 Annual Report - Distribution of Class A Residuals: Denali Water
Solutions (Lake Kilby Water Treatment Plant) Permit No. WQ0035720
To Whom it May Concern:
Denali Water Solutions is submitting the required 2019 Annual Report for Permit No.
WQ0035720. This permit is associated with the distribution
of water treatment residuals
produced at the City of Portsmouth - Lake Kilby Water Treatment
Plant located in Suffolk,
Virginia, with distribution in Gates County, North Carolina.
R
' prx:11/F_�
This Annual Report contains the following information:
• Form DMSDF
FEP
• Form RSSF
1 t ?�20
Form
' ORMA"OMP'OCESSINGUNIT
• Form SFLSF
• Lab Reports
If you have any questions, or need any additional information, please do not hesitate to
contact me at [phone] or via email at jeff.retzkeCcdenaliwater.com.
Sincerely,
Digitally signed by Jeff Retzke
DN: cn=Jeff Retzke, o=Denali
Water
nmSolutions, al ManaSenior,
Environmental Manager,
email=jeff.retzke@denali waters
om,--US
Date: 2020.02 0410:34:1 S-06'00'
Jeff Retzke
Senior Environmental Manager, East Region
cc: Nathan Litteral (Water Plant Manager, City of Portsmouth, Virginia)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0035720 FACILITY NAME: Lake Kilby Water Treatment Plant
PHONE: [phone] COUNTY: Suffolk, VA OPERATOR: Nathan Litteral (Water Plant Manager)
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
® Distribution and Marketing (complete Parts A, B, and C)
Nas the facility in operation during the past calendar year? Yes 0 No ❑ —► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
fanuary
February
larch
April
day
Tune
fuly
kugust
;eptember
Lake Kilby WTP
0
351.81
351.81
See FSF
351.81
Soil Amendment
)ctober
Lake Kilby WTP
0
1,028.67
1,028.67
See FSF
1028.67
Soil Amendment
Jovember
Lake Kilby WTP
0
701.03
701.03
See FSF
701.03
Soil Amendment
)ecember
Lake Kilby WTP
1 0
66.93
1 66.93
See FSF
66.93
Soil Amendment
Total from FORM DMSDF (sup)
rotals:
Annual (dry tons):1
0
2148.44
1 2'148.44
2148.44
Amendments used:
I
Bulking Agent(s) used:
(supp)): Total Number of Form DMSDF (Supp)
If more space is required, attach additional information sheets (FORM DMSDF
'art C:
+acility was compliant during the past calendar year with all conditions of the land application permit ® Yes
including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No No If No, Explain in Narritive
All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
;. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
'I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
ienalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Digitally signed by Jeff fletzke
tN ronmcn=Jeff RetM-gDenali
.: Water Solutions, u=Senio
#nvi ental Manager,
[e-mail]
05
Date: 2020.02.04 10W:" -0 00'
lignature of Permittee Date Signature of Preparer**
(if different from Permittee)
"Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0035720
Laboratory: 1) Waypoint Analytical, Richmond, VA
Facility Name: Lake Kilby WTP 2)
Residual Source WQ # or 3)
NPDES #: 4)
WWTP Name: 5)
Residual Analysis Data
Parameter
aramet)
Conc.
Limit
mg/kg )a
Sample or Composite Date
10/7/19
10/7/19
10/17/19
10/17/19
11/2/19
11/13/19
Max
Percent Solids (%)
NA
15.6
14.9
14
14.4
16.7
17.6
17.6
Arsenic
75
32.1
33.6
13.9
11.2
13.4
10.6
33.6
Cadmium
85
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
4,300
64.1
68.5
54.5
51.3
194
52.6
194
Chromium
NA
121
123
131
124
138
107
138
Lead
840
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
57
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molybdenum
75
16
16.8
2.6
2.4
2.8
2
16.8
Nickel
420
16
16.8
15.4
14.4
12.1
14.1
16.8
Selenium
100
32.1
33.6
3.6
3.5
3
2.8
33.6
Zinc
7,500
180
237
186
174
160
131
237
Total Phosphorus
NA
1240
1300
1330
1.260
1650
1130
1650
TKN
NA
17100
15800
19200
16500
19200
15500
19200
Ammonia -Nitrogen
NA
640
670
929
840
796
847
1
929
Nitrate and Nitrite
NA
30.2
33.6
33.9
32.6
27.7
27.8
1
33.9
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penal'' ' mittajug abe4m& oration, including the possibility of fines and imprisonment for knowing violations."
_- ter
Solutions,ou=Senior Environmental
Manager,
email=[e-mail], -US
Date: 2020.02.0410.33:32-06'00'
Signaluic ui r><CpaiCr * Date
*Prepares is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

rvi,qi,N utiL ivir, t 2xu3 r iL' L1) 3uivuvu,%m Y r "Kivi
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Lake Kilby WTP Total Dry Tons Applied (Annual): 50.45
Permit #: WQ0035720 Cation Exchange Capacity (non 503 only): 73,000 mg/kg
Operator: Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: NoA
Acres Used: 6.5 Acres Permitted: 6.5 Site #: NC-GT-03 Field #: 2A
Residual Analysis Data (Heavy Metals and Total Phosphorus use m2/k2, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
L1j
10/7/19
2
t0/7/19
3
10/17/19
41
10/17/19
5
11/2/19
6
11/13/19
7
8j
9
10
11
12
Max
% Solids
15.6
14.9
14
14.4
16.7
17.6
17.6
Arsenic
32.1
33.6
13.9
11.2
13.4
10.6
33.6
Cadmium
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
64.1
68.5
54.5
51.3
194
52.6
194
ChromiLini
121
123
131
124
138
107
138
Lead
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molyb-
denLlm
16
16.8
2.6
2.4
2.8
2
16.8
Nickel
16
16.8
15.4
14.4
12.1
14.1
16.8
Selenium
32.1
33.6
3.6
3.5
3
2.8
33.6
Zinc
180
237
186
174
160
131
237
Total
Phos-
horns
1240
1300
1330
1260
1650
1130
1650
Annual Heavv Metal Field Loadings (Calculated in Ibs/acre):
Total
L 1
2
3
4
5
6
7
8
9
10
111
12
DT/Ac./
o
App.
Event
7.76
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.522
0.522
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.104
0.104
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.012
3.012
ChromiLIM
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.142
2.142
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.312
0.312
Mercury
0.000
0.000
0 000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
0.002
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.261
0.261
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.261
0.261
Selenium
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.522
0.522
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
3.679
3.679
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
25.615
25.615
horus
1 certny, under penalty of iaw, tnat tms document was preparea under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility, of fines and
imprisonment for knowing violations".
�,ta.ry F.ada»taattw.
aM�,e 0.oena,wne.
o,MI- 2j.1.3���.a
ae.Y=iMl amdenaliwat..cam.
Signature of Land Applier
Date
nCniI-) Enonn nnci CC /4'W)00G\

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOY WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
Land Owner: Edwin Miller, etal
Operator: Ed Miller Farms
Crop 1 Name: Wheat
WQ Permit #: WQ0035720 Field #: 2A
Annual Dry Tons Applied: 50.4505 Site #: NC-GT-03
Predominant Soil Series: NoA
Crop I Max. PAN:
125
Crop 2 Name:
Acres Utilized: 6.5
Acres Permitted: 6.5
Cation Exchange Capacity (non 503): 73,000 mg/kg
N/A Crop 2 Max. PAN: N/A
p
V =
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
o
�o
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, W #,
Q
Fert., Animal
Waste, etc)
Soil
Cond.
D
( ry'
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
>
F° _
� o.
o
*
o
w
� �
-
*
o'
� �
�•
c'
TKN
mg/kg
Z Y
3
o 3
aq o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
Nov
340.37
17.6
7.762
WQ0035720
M
0
S
0.5
0.4
19200
929
33.9
121.187
NA
Wheat
0
0.000
0.000
0000'
0.000
0.000
0.000
0.000 -
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0:000
0.000
0.000
0.000
0,000
0.000
0.000
0,000-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
'OTALS:
340.37
o
As
Cd
Cu
Cr
Pb
Hg
Mo
I Ni
Se
Zn
P
121.1871
0.000
Lime Applied
Uinual lbs/acre
0.522
0.299
0.821
36.49
0.104 :
0.052
0.156 `
34.71
3.012
3.279
6.291
1335
2.142
3.331
5.473
N/A
0.312
0.198
0.510
267
0.002 -
0.01
0.012
1 1.5.13
0.261
0.131
0.392
N/A
0.261
0.443
0.704
373.8
0.522
0.131
0.653
1 89
3,679
5.902
9.581
1 2492
25.615
Date
lbs/ac
'rior Years Cumulative lbs/ac
:urrent Cumulative lbs/ac
'ermitted C. P. L. R.****
'ermit PAN Limit 1 st/2nd Crop
125 N/A
'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
aformation, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
/ **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

t%114111 UTAJU 1V1L' IIALO rlr L1J U"IIXL1111qV •7U1V11ViLiAi rVrI1Vl'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Lake Kilby WTP Total Dry Tons Applied (Annual): 84.72
Permit #: WQ0035720 Cation Exchange Capacity (non 503 only): 73,000 mg/kg
Operator: Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: NoA
Acres Used: 11.5 Acres Permitted: 11.5 Site #: NC-GT-03 Field #:
2B
Residual Analvsis Data (Heavv Metals and Total Phosphorus use miA2. % Solids use Raw Percent ft
Sample or
Com-
posite
Date
L1J
10/7/19
2
10/7/19
3
10/17/19
4
10/17/19
51
11/2/19
6
11/13/19
71
8
L2J
1101
Ill 1
12
Max
% Solids
15.6
1 14.9
14
14.4
1 16.7
17.6
17.6
Arsenic
32.1
33.6
13.9
11.2
13.4
10.6
33.6
Cadmium
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
64.1
68.5
54.5
51.3
194
52.6
194
Chromium
121
123
131
124
138
107
138
Lead
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molyb-
denum
16
16.8
2.6
2.4
2.8
2
16.8
Nickel
16
1 16.8
15.4
14.4
12.1
14.1
16.8
Selenium
32.1
33.6
3.6
3.5
3
2.8
33.6
Zinc
180
237
186
174
160
131
237
Total
Phos-
horus
1240
1300
1330
1260
1650
1130
1650
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
11
L2J3
4 J
1 5
161
7
8
9
10
11
12
DT/Ac./
App.
"oyr
Event
7.37
Arsenic
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.495 1
0.495
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.099
0.099
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.858
2.858
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.033
2.033
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.296
0.296
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Q.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.248
0.248
enum denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.248
0.248
Selenium
1 0.000
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.495
0.495
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.492
3.492
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
24.311
24.311
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
.{J +M+9repP�kW hX¢emtw
Signature of Land Applier
Date
nFNR F(-1RAA rum CG

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP WQ Permit #: WQ0035720 Field #: 2B Acres Utilized: 11.5
Land Owner: Edwin Miller, etal Annual Dry Tons Applied: 84.7225 Site #: NC-GT-03 Acres Permitted: 11.5
Operator: Ed Miller Farms Predominant Soil Series: NoA Cation Exchange Capacity (non 503): 73,000 mg/kg
Crop 1 Name: Wheat Crop 1 Max. PAN: 125 Crop 2 Name: N/A Crop 2 Max. PAN: N/A
y
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
�/o
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
D
4Ve '
Moist)
Precip
Past 24
Hrs.
inches
>
a
�•
o�
o
°
_
I
?
*
c
TKN
mg/kg
Z Ei
o
aD o
mg/kg
Nihate
and
Nitrite
mg/kg
PAN Applied
(]bs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
Nov
571.59
17.6
7.367
WQ0035720
M
0
S
0.5
1 0.4
19200
929
33.9
115.028
NA
Wheat
0
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
'OTALs:
571.59
0
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
115,028
0.000
Lime Applied
�nnuallbs/acre
0.495-
0.099
2.858
2.033
0.296
0.002
0.248
0.248
0.495
3,492
24.311
Date
1
'rior Years Cumulative lbs/ac
0.304
0.053
3.333
3.386
0.201
0.011
0.133
0.451
0.133
5.999
'urrent Cumulative lbs/ac
0.799
0.152
6.191-
5.419
0.497
0.013
0.381
0.699
0.628
9.491
'ermitted C. P. L. R.****
36.49
34.71
1335
N/A
1 267
15.13
N/A
373.8
89
2492
'ermit PAN Limit 1st/2nd Crop
125 N/A
'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
,/ac

Ivilil UL-1L 1V1L' 12AUa r1n1," LlJL1Vlil" 3UIVIiV1EiR1 rlJnivi,
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Lake Kilby WTP Total Dry Tons Applied (Annual):
113.24
WQ0035720 Cation Exchange Capacity (non 503 only): 73,000 nig/kg
Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: NoA
14.5 Acres Permitted: 14.5 Site #: NC-GT-03 Field #: 2C
Residual Analysis Data (Heavy Metals and Total Phosphorus use m2/k2, % Solids use Raw Percent #l:
Sample or
Com-
posite
Date
1
10/7/19
2
10/7/19
3
10/17/19
4
10/17/19
5
11/2/19
6
11/13/19
7
81
9
10
11
12
Max
% Solids 1
15.6
14.9
14
1 14.4
16.7
17.6
17.6
Arsenic
32.1
33.6
13.9
11.2
13.4
10.6
33.6
Cadmium
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
64.1
68.5
54.5
51.3
194
52.6
194
Chromiun
121
123
131
124
138
107
138
Lead
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molyb-
dcnum
16
16.8
2.6
2.4
2.8
2
16.8
Nickel
16
16.8
15.4
14.4
12.1
14.1
16.8
Selenium
32.1
33.6
3.6
3.5
3
2.8
33.6
Zinc
180
237
186
174
160
131
237
Total
Phos-
horus
1240
1300
1330
1260
1650
1130
1650
Annual tieavv )Metal Field Loadings (Calculated in lbs/acre):
Total
1
?
3;
4 j
5 j
6�
7
8
9
10
11
12
DT/Ac./
o
App.
Event
7.81
Arsenic
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.525
1 0.525
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.105
0.105
Copper
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.030
3.030
Chroiniurn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
2.155
2.155
Lead
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.314
0.314
Mercury 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.002
0,002
Molyb- 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.262
0.262
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.262
0.262
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.525
0.525
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
3.701
1 3.701
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
25.770
25.77
horus
"i certny, under penalty of taw, that ttiis document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Diq.raiIy yierr Rr:ke
,� {{{ DN: in=)efl Relzke, o=Denali Water
f fj Soluuons, ou=Senior Envlronmmral
(fVjy.+i�//)/ Manager,
L-�ef(retzkevntlenaliweter.com.
D-US
Dare: mzo.oz.oa iganav oeea
Signature of Land Applier
Date
nGnio cnDnn KAM cE7 /-II)/I)nnc\

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOY WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP WQ Permit #: WQ0035720 Field #: 2C Acres Utilized: 14.5
Land Owner: Edwin Miller, etal Annual Dry Tons Applied: 113.2360 Site #: NC-GT-03 Acres Permitted: 14.5
Operator: Ed Miller Farms Predominant Soil Series: NoA Cation Exchange Capacity (non 503): 73,000 mg/kg
Crop 1 Name: Wheat Crop 1 Max. PAN: 125 Crop 2 Name: N/A Crop 2 Max. PAN: N/A
s~
[�
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
PP � P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, W #,
Q
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet,
Moist)
Pirecip.
2
Past _4
Hrs.
inches
o
�° -
w
* c'
o
�; _
--
*
� �
N•
* P
c
TKN
mg/kg
z >
o �
ac o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
('lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
Nov
763.96
17.6
7.809
WQ0035720
M
1 0
S
1 0.5
0.4
19200
929
33.9
121.933
NA
Wheat
0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 _
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
'OTALs:
763.961
0
As
Cd
-Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
121.933
0.000
Lime Applied
1imuallbs/acre
0.525
0.309
0.834
36.49
0.105
0.054
0.159
34.71
3.030
3.387
6.417
1335
2.155
3.441
5.596
N/A
0.314
0.205
0.519
267
0,002
0.011
0.013
15.13
0.262
0.135
0.397
N/A
0.262
0.458
0.720
373.8
0.525
0.135
0.660 _
1 89
3.701
6.097
9.798
1 2492
25.770
Date
lbs/a
'rior Years Cumulative lbs/ac
.urrent Cumulative lbs/ac
'ermitted C. P. L. R.****
'ermit PAN Limit 1 st/2nd Crop
I
r 125 1 N/A
'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation, including the possibility of fines and imprisonment for knowing violations."
/ *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

A1rlr UAL 1V1L' 1 ALJ r 1r.L1J LVAlJllrkr IUIV11VIAKY 11 VKAIl
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Lake Kilby WTP Total Dry Tons Applied (Annual): 275.50
Permit #: WQ0035720 Cation Exchange Capacity (non 503 only): 73,000 mg/kg
Operator: Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: BoB
Acres Used: 43.7 Acres Permitted: 43.7 Site #: NC-GT-03 Field #: 8
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
10/7/19
21
10/7/19
1 31
10/17/19
41
10/17/19
51
11/2/19
61
11/13/19
L_Zj
81
9 j
110111
1
12
Max
% Solids
15.6
14.9
14
14.4
16.7
17.6 1
1
17.6
Arsenic
32.1
33.6
13.9
11.2
13.4
10.6
33.6
Cadmium
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
64.1
68.5
54.5
51.3
194
52.6
194
Chromiurr
121
123
131
124
138
107
138
Lead
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molyb-
denum
16
16.8
2.6
2.4
2.8
2
16.8
Nickel
16
16.8
15.4
14.4
12.1
14.1
16.8
Selenium
32.1
33.6
3.6
1 3.5
3
2.8
33.6
Zinc
180
237
186
174
160
131
237
Total
Phos-
horus
1240
1300
1330
1260
1650
1130
1650
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
o
©
D
-
N=nun
Nunn
NOWNWO
Event
• 1
1 lel
1 111
t I11
1 !11
1 Ilt
1 eil
1 111
i 111
1 ill
i 111
1 111
1.
e..
i 111
1 111
1 111
1 111
1 lit
1 111
1 lel
1 ill
1 111
1 111
1 ill
1 i:�
1 1:�
.•
! 111
1 ill
1 ill
! tll
! 11!
i 111
! tll
1 etl
ffITIT,e
1 1t1
!ill
•,•
IF, ,••
e 11!
1 111
1 111
1 1!1
t il!
1 ill
t !11
1 etl
i 111
1 111
i 111
-e
�1
i 111
1 111
1 lil
1 1!1
i 101
1 1!i
1 Ile
1 lil
1 111
1 111
1 111
��
• �
e ele
eee!
I Ili
! !rl
i !It
a ell
a ttt
i 1!e
I !el
i e!r
1 !el
��'
®
1111
1111
i111
1111
1111
lirl
lell
lell
1111
1111
e111
r
®
r 111
i 111
1 111
!ill
! tll
r tll
! iii
! tll
1 ili
1 lee
1 111
! ,
! . ,
Total
•
.•
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
V, ��
Signature of Land Applier
Date
rII=NR PnPKA KAM CG 117/7nnCZ\

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOY WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
Land Owner: Edwin Miller, eta]
Operator: Ed Miller Farms
Crop 1 Name: Wheat
WQ Permit #: WQ0035720 Field #: 8
Annual Dry Tons Applied: 275.4996 Site #: NC-GT-03
Predominant Soil Series: BoB
Crop 1 Max. PAN:
102
Crop 2 Name:
Acres Utilized: 43.7
Acres Permitted: 43.7
Cation Exchange Capacity (non 503): 73,000 mg/kg
N/A
Crop 2 Max. PAN:
N/A
o y
Volume applied
(enter one) Solids/
Liquid
1
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
D
(Dry,
Wet,
Moist)
Precip.
past 24
Hrs.
inches
a
a
*
o
'pb.
-
o'
��,
c
N
c
TKN
mg/kg
z D
B
o
0:, 0
�•
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
Nov
1858.69
17.6
6.304
W00035720
M
0
S
0.5
0.4
19200
929
33.9
98.433
NA
Wheat
0
0.000
0.000
0000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0,000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
'OTALS4
1858.691
o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
98.433
0,000
Lime Applied
%nnuallbs/acre
0.424
0
0.424
36.49
0,084
0
0.084
34.71
2.446
0
2.446
1 1335
1.740
0
1.740
1 N/A
0.253
0
0.253
1 267
0.001
0
0.001
1 15.13
0.212
0
0.212
NIA
0.212
0
0.212
373.8
0.424
0
0.424
89
2988
0
2.988
2492
20.803
Date
lbs/ac
'rior Years Cumulative lbs/ac
urrent Cumulative lbs/ac
3ermitted C. P. L. R.****
'ermit PAN Limit 1 st/2nd Crop
t
102 N/A
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation. includin
Digila sit the possibility of fines and imprisonment for knowing violations."
GYl�TMetske
• 1 DN: rn-JeHo„IA-ke, o=De hWatei
*Application Method: S -Surface, IN -Injection, INC -Incorporation
Manager,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
** Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

tii� utvi. ivir,tAu,5 riEt u uuALPii,4" 3uivuviHnr rvnivi
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Lake Kilby WTP Total Dry Tons Applied (Annual):
103.97
WQ0035720 Cation Exchange Capacity (non 503 only): 73,000 mg/kg
Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: BoB
59 Acres Permitted: 59 Site #: NC-GT-03 Field #: 9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mWki!, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
_1j
10/7/19
2
10/7/19
3!
10/17/19
4
10/17/19
5
11/2/19
61
11/13/19
7
8
9
10
11
12 I
Max
% Solids
15.6
14.9
14
14.4 1
16.7
17.6
17.6
Arsenic
32.1
33.6
13.9
11.2
13.4
10.6
33.6
Cadmium
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
64.1
68.5
54.5
51.3
194
52.6
194
Chromiun
121
123
131
124
138
107
138
Lead
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molyb-
denum
16
16.8
2.6
2.4
2.8
2
16.8
Nickel
16
16.8
15.4
14.4
12.1
14.1
16.8
Selenium
32.1
33.6
3.6
3.5
3
2.8
33.6
Zinc
180
237
186
174
160
131
237
Total
Phos-
horus
1240
1300
1330
1260
1650
1130
1650
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
11
2
3 '.
4
5
7;
81
9
10
11 i
12
DT/Ac./
a
APP•
Event
1.76
Arsenic
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.118
1 0.118
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
0.024
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.684
0.684
Chromiun
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.486
0.486
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.071
0.071
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0 000
0.000
0.000
0.000
Molybdenum
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
0.059
enum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
0.059
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.118
0.118
"Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.835
0.835
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.815
5.815
horus
"7 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
raiy.�edk Jett 0.etrke
p )'n_leH 0.ehke. o--Dewli Water
;d`ftvms, ocSeNx F.nvnmmenlal
✓✓ kfaiv9er,
ma�iyerceaxewenar.ae.u,n. <-us
Signature of Land Applier
Date
n1=KID cnonn nnGi cG

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
Land Owner: Edwin Miller, etal
Operator: Ed Miller Farms
Crop 1 Name: Wheat
WQ Permit #: WQ0035720 Field #: 9 Acres Utilized: 59
Annual Dry Tons Applied: 103.9707 Site #: NC-GT-03 Acres Permitted: 59
Predominant Soil Series: BoB Cation Exchange Capacity (non 503): 73,000 mg/kg
Crop 1 Max. PAN: 102 Crop 2 Name: N/A Crop 2 Max. PAN: N/A
°
°
A °
Volume applied
PP
enter one Solids/
( )
Liquid
Cu. Yds Gallons
/o
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
r ,
Moist
Precip.
Past 24
Hrs.
inches
Y
�° b
a W
* °
e
„
*
o
* �•
o'
TKN
mg/kg
z a
o
aD o
a
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
p yp
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
Nov
249.88
17.6
0.628
WQ003 320
M
0
S
0.5
0.4
19200
929
33.9
9.802
NA
Wheat
0
Dec
451.57
17.6
1.134
WQ0035720
M
0
S
0.5
0.4
19200
929
33.9
17.713
NA
Wheat
0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
'oTALS:
701.45
o
As
Cd
Cu
Cr
Pb
11 r
Mo
Ni
Se
Zn
P
27.515
0.000
Lillie Applied
knnuallbs/acre
0.118
0.335
0.453
36.49
0.024
0.086
0.110
34.71
0.684
0.207
6.891
1335 1
0.486
3.019
3.505
N/A
0.071
0.806
0.877
267
0.000
0.008
0.008
15.13
0.059
0.166
0.225
1 N/A 1
0.059
0.501
0.560
373.8
0.118
0.451
0.569
89 1
0.835
9.292
10.127
2492
5.815
Date
lbs/a
'rior Years Cumulative lbs/ac
,urrent Cumulative Ibs/ac
'ermitted C. P. L. R.****
'ermit PAN Limit 1 st/2nd Crop
102 N/A
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation. including the possibility of fines and imprisonment for knowing violations."
*Application Method: S -Surface, IN -Injection, INC - Incorporation
**Volatilization Rate• Surface - 0 5 Injection/Incor oration - 1 0
Signature of Land Applier Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

t11VPrUAL 1VMIAUJ r1L'UIJ UVALUNU JU1V11V1AKY rk-MM''
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Lake Kilby WTP Total Dry Tons Applied (Annual): 37.39
Permit #: WQ0035720 Cation Exchange Capacity (non 503 only): 73,000 mg/kg
Operator: Ed Mitler Farms Owner: Edwin Miller, etal Predominant Soil Series: PnA
Acres Used: 5.1 Acres Permitted: 5.1 Site #: NC-GT-03 Field #: 19
Residual Analysis Data (Heavy Metals and Total Phosphorus use m2/k2, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
10/7/19
�
10/7/19
3
10/17/19
4
10/17/19
5
11/2/19
6
11/13/19
7
8
9
10
11
12
Max
% Solids
15.6
14.9
14 1
14.4
16.7
17.6
17.6
Arsenic
32.1
33.6
13.9
11.2
13.4
10.6
33.6
Cadmium
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
64.1
68.5
54.5
51.3
194
52.6
194
Chromiur
121
123
131
124
138
107
138
Lead
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molyb-
dermn
16
16.8
2.6
2.4
2.8
2
16.8
Nickel
16
16.8
15.4
14.4
1 12.1
14.1
16.8
Selenium
32.1
33.6
3.6
3.5
3
2.8
33.6
Zinc
180
237
186
174
160
131
237
Total
Phos-
horns
1240
1300
1330
1260
1650
1130
1650
Annual Heavy Metal rield Loadings ((-alculated in lbs/acre):
Total
1
1 21
3
4
5
7
8
9
10
11
12�
DT/Ac./
o
App.
W.
Event
7.33
Arsenic
0.000
1 0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.493
1 0.493
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.098
0.098
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.844
2.844
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.023
2.023
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.295
0.295
Mercury
0.000
1 0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
0.002
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.246
0.246
denum
enum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.246
0.246
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.493
0.493
Zinc
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.475
3.475
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
24.192
24.192
horuS
r cernty, unaer penalty of iaw, tnat this clocument was preparea unaer my alrection or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
nC:niD r-:rnonn RACI cc 1-1010nnaN

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
Land Owner: Edwin Miller, etal
Operator: Ed Miller Farms
Crop 1 Name: Wheat
WQ Permit #: WQ0035720 Field #: 19
Annual Dry Tons Applied: 37.3906 Site #: NC-GT-03 Acres Permitted: 5.1
Predominant Soil Series: PnA Cation Exchange Capacity (non 503): 73,000 mg/kg
Acres Utilized: 5.1
Crop I Max. PAN: 121 Crop 2 Name: N/A Crop 2 Max. PAN:
N/A
$.
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry'
Moist)
Precip.
Past 24
Hrs.
inches
Y
Ts
'�
°a T
* °
c
*
d
*
o
TKN
mg/kg
Z
Mo c
Z.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop l
Crop 2
Nov
252.26
17.0
7.331
WQ0035720
M
0
S
0.5
0.4
19200
929
33.9
114.471
NA
Wheat
0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
'OTALS:
2E60
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
I P
114.471
r 0.000
Lime Applied
kimuallbs/acre
0.493
0
0.493
36.49
0.098
0
0.098
34.71
2.844
0
2.844
1335
2.023
0
2.023
N/A
0.295
0
0.295
267
0.002
0
0.002
15.13
0.246
0
0.246
N/A
0.246
0
0.246
373.8
0.493
0
0.493
89
3.475
0
5
2
E24
124.192 1
Date
lbs/a
'rior Years Cumulative lbs/ac
'urrent Cumulative lbs/ac
3ermitted C. P. L. R.****
'ermit PAN Limit 1 st/2nd Crop
1 121 1 N/A
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation, ippIop
ildincy the possibility of fines and imprisonment for knowing violations."
o.9�viMundW�ra.<
W-�1�•,((/ °"-°^_""'"<•°_°<"'"'""� *Application Method: S - Surface, IN -Injection, INC -Incorporation
muii.pit,<ct.�e.,,.r.w4.Goo.=5 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Hlrlr UHL 1vir t Au3 r Ir.Ltl LuAuir%h nuivtivtAn x r"rtivv
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Lake Kilby WTP Total Dry Tons Applied (Annual): 346.55
WQ0035720 Cation Exchange Capacity (non 503 only): 73,000 mg/kg
Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: NoA
44.5 Acres Permitted: 44.5 Site #: NC-GT-03 Field #: 20
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
10/7/19
2
10/7/19
_3j
10/17/19
41
10/17/19
5
11/2/19
61
11/13/19
7
81
9
101
11 1
12
Max
% Solids 1
15.6
14.9
14
14.4
16.7
17.6
17.6
Arsenic
32.1
33.6
13.9 1
11.2
13.4
10.6
33.6
Cadmium
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
64.1
68.5
54.5
51.3
194
52.6
194
ChrorniL1111.
121
123
131
124
138
107
138
Lead
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molyb-
denum
16
16.8
2.6
2.4
2.8
2
16.8
Nickel
16
16.8
15.4
14.4
12.1
14.1
16.8
Selenium
32.1
33.6
3.6
3.5
3
2.8
33.6
Zinc
180
237
186
174
160
131
237
Total
Phos-
horus
1240
1300
1330
1260
1650
1130
1650
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total0
©
©
©MEM
D
-
•
1111
1111
1111
1111
i111
1111
i111
till
1111
1111
1lli
��
1 111
i tll
ffITIT,t
1 111
1 111
my,
1 111
1 illKIT,11
1 111
t 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
��
1 111
1 111
1 111
1 111
1 111
1 111
Kim
ff1 my, MI
! 111
KIT, i!
,•
.•
i 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
��
®
1 111
1 111
1 111
i 111
1 !11
1 111
1 111
1 Iil
1 111
i 111
KINt
� �
1111
1111
1111
1111
i111
1111
1111
1111
1111
1111
1l11
1 .
! •
®
1111
1111
111!
1111
1111
1111
1111
1111
1111
1111
i111
1 •
1 •
®
1 111
1 111
1 111
1 111
1 111ffITITIMINM
111
1 11 !
1 111
1 111
1 111
��
®
1 111
1 111
1 Ili
1 111
1 ill
1 Ili
1 111
1 ill
1 111
1 111
1 ill
.'
•'
Total
Phos-
phorus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
�� YS Ui9italM s5red by le(f NeVke
�`(`j/a,',ITI(al{rrnl(v,_J, DNm=Wf nerzke. s=Denab Walei
Sdumns, a=Senwr Enviorxnental
ertiaMgdlrerzkcpdmaNwaMtsn, r_I15
Dam }(1}n.0}.Iq 10.}5.19116'W'
Signature of Land Applier
Date
nFNR rnann KAPI cP 110100nAl

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP WQ Permit #: WQ0035720 Field #: 20
Land Owner: Edwin Miller, etal Annual Dry Tons Applied: 346.5471 Site #: NC-GT-03
Operator: Ed Miller Farms
Crop 1 Name: Wheat
Predominant Soil Series: NoA
Crop 1 Max. PAN:
125
Crop 2 Name:
Acres Utilized: 44.5
Acres Permitted: 44.5
Cation Exchange Capacity (non 503): 73,000 mg/kg
N/A
Crop 2 Max. PAN
N/A
0 o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet'
Moist)
precip.
Past 24
Hrs.
inches
4 '°
!» 'S?
o w
a
ts
o
N
o'
°�
* N'
* o
TKN
m9mg
Z a
-
oOro B
„
mg/kg
Nitratc
and
Nitrite
mg/kg
PAN Applied
(]bs/acre)
Name of Crop Type
Receiving Residual
Application
pp
Crop 1
Crop 2
Crop 1
Crop 2
Oct
1646.51
17.6
5.484
WQ0035720
M
0
S
0.5
0.4
19200
929
33.9
85.629
NA
Wheat
0
Nov
691.51
17.6
2.303
WQ0035720
M
0
S
0.5
0A
19200
929
33.9
35.963
NA
Wheat
0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
'OTALS:
r38.02
0
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
121.5921
0.000
Lime Applied
knnuallbs/acre
0.523
0.971
1.494
36.49
0.104
0.178
0.282
1 34.71
3.021
12.347
15.368
1 1335
2.149
13.728
15.877
1 N/A
0.313
1.252
1.565
1 267
0.002
0.039
0.041
1 15.13
0.262
0.442
0.704
1 N/A
0.262
1.366
1.628
1 373.8
0.523
1.588
2.111
1 89
3.691
23.133
26.824
2492
25.697 1
Date
lbs/ac
'rior Years Cumulative lbs/ac
.urrent Cumulative lbs/ac
'ermitted C. P. L. R.****
'ermit PAN Limit 1 st/2nd Crop
I
F-1257N/A
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation_ lincindit,thepossibility of fines and imprisonment for knowing violations."
��°°x�-F°°°° • *Application Method: S -Surface, IN -Injection, INC -Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Yu,N rN V t1L lvin l t1LJ r 1GL1J u",AL11\ V a U1v11vuAix I r "Rlvl "
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Lake Kilby WTP Total Dry Tons Applied (Annual):
276.86
WQ0035720 Cation Exchange Capacity (non 503 only): 73,000 mg/kg
Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: BoB
43.6 Acres Permitted: 43.6 Site #: NC-GT-03 Field #: 21
Residual Analvsis Data (Heavv Metals and Total Phosphorus use m2/ki!, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
10/7/19
2
10/7/19
3
10/17/19
4
10/17/19
_5j
11/2/19
6j
11/13/19
7
8
9
10
11
12
Max
'% Solids
15.6
14.9
14
14.4
16.7
17.6
17.6
Arsenic
32.1
33.6
13.9
11.2
13.4
10.6
33.6
Cadmium
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
64.1
68.5
54.5
51.3
194
52.6
194
ChromiLu
121
123
131
124
138
107
138
Lead
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molyb-
denum
16
16.8
2.6
2.4
2.8
2
16.8
Nickel 1
16
16.8
15.4
14.4
12.1
14.1
16.8
Selenium
32.1
33.6
3.6
3.5
3
2.8
33.6
Zinc
180
237
186
174
160
131
237
Total
Phos-
horus
1240
1300
1330
1260
1650
1130
1650
Annual Heavv Metal Field Loadines (Calculated in lbs/acre):
Total
o©©
0
o
D
-
App.
Nunn
n
NONE
Event
i 111
1 tll
! 111
1 111
1 111
1 111
1 til
1 111
1 111
1 Itl
1 111
1 � •
1 � •
MIL"M
Kor, u1
1:
•••
1111
1111
1111
lilt
1111
Itll
i111
1111
1111
1111
1111
�®
1 !11
1 111
1 111
1 111
1 ill
1 111
1 111
1 ill
1 111
1 111
1 111
'1
'1
i Itl
1 111
1 111
t Itl
1 111
1 111
1 111
1 111
1 111
1,
1 tll
1•
1
®
! 111
1 ill
1 111
1 111
1 111
1 111
1 111
1 iil
1 111
1 111
1 111
1 11
1 11
�
1111
1111
1111
Itll
1111
illl
1i11
1111
1111
1111
1111
1
1
��
®
1 111
1 111
1 111
1 111
1 111
1 iil
1 !11
1 111
1 111
i !11
1 111
1
1
®
illl
1111
1111
Iill
1111
1111
1111
1111
1111
1111
1111
1Y•
1� •
®
1111
1111
t111
1111
1111
lill
1111
1111
1111
1111
1111
��
Total
Phos-
-phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
lI wauaiy%,9-d by ieff 9e¢ke
/� DN. rn-:1+ff Retzke. u-'mwmcom,
iy'r/tlj//)( '/R/l L umni, ow Ae Envy dal
Mann, e,
emWFja(fr ak.zM.nakwa
=US
Date. M]ooE o4 t0343]0600
Signature of Land Applier Date
np:niR Pnann KAM cG

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOY WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP WQ Permit #: WQ0035720 Field #: 21 Acres Utilized: 43.6
Land Owner: Edwin Miller, etal Annual Dry Tons Applied: 2768603 Site #: NC-GT-03 Acres Permitted: 43.6
Operator: Ed Miller Farms Predominant Soil Series: BoB Cation Exchange Capacity (non 503): 73,000 mg/kg
Crop 1 Name: Wheat Crop l Max. PAN: 102 Crop 2 Name: N/A Crop 2 Max. PAN: N/A
y =
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc
_)
Soil
Cond.
D
( ry'
Wet,'
Moist)
Precip
Past 24
Hrs.
inches
L'
'a
°a w
o
, -
F :=,
N
o.
I
N•
w
c
TKN
mg/kg
Z D
-3
o B
oa o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
Oct
1867.87
17.6
6.350
WQ0035720
M
0
S
0.5
0.4
19200
929
33.9
99.146
NA
Wheat
0
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0:000
0.000
0.000
0.000
0.000
0000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
'OTALS:
7867.871
o
As
Cd
Cu
Cr
Pb
Hg
Mo
I Ni
Se
Zn
P
99146
0.000
Lime Applied
knnuallbs/acre
0,436
0.624
1.060
0.087
0.116
0.203
34.71
2.516
7.896
10,412
1335
1.790
8.662
10.452
N/A
0.261
0.712
0.973
267
0.001
0.026
0.027
15.13
0,218
0.289
0.507
N/A
0.218
0.938
1.156 '
373.8
0,436
1.225
1.661
89
3.073 .
14.972
18.045
2492
20.955 1
Date
lbs/ac
'rior Years Cumulative lbs/ac
.urrent Cumulative lbs/ac
'ermitted C. P. L. R.****
'ermit PAN Limit 1 st/2nd Crop1
+--36.49
102 1 N/A
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation, including the possibility of fines and imprisonment for knowing violations."
Dy -Ilyvgdtyl (tk k
DN kk k De w s *Application Method: S - Surface, IN - Injection, INC - Incorporation
�1 e(fx dcv,alwae orr. c US
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Hl�ll�l UAL 1V111. 1 ALJ 1' 1L' LU LVALLr Vr .�U1V11V1HK Y C VK1VC'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Lake Kilby WTP Total Dry Tons Applied (Annual):
WQ0035720 Cation Exchange Capacity (non 503 only):
Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series:
353.83
73,000 mg/kg
GoA
42.7 Acres Permitted: 42.7 Site #: NC-GT-03 Field #: 25
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
10/7/19
2
10/7/19
3
10/17/19
4
10/17/19
5
11/2/19
6
11/13/19
__7j
8j
9
10
11
12
Max
% Solids 1
15.6
14.9
14 1
14.4
16.7
17.6
17.6
Arsenic
32.1
33.6
13.9
11.2
13.4
10.6
33.6
Cadmium
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
64.1
68.5
54.5
51.3
194
52.6
194
CbroniiUrr
121
123
131
124
138
107
138
Lead
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molyb-
denum
16
16.8
2.6
2.4
2.8
2
16.8
Nickel
16
16.8
15.4
14.4
12.1
14.1
16.8
Selenium
32.1
33.6
3.6
3.5
3
2.8
33.6
Zinc
180
237
186
174
160
131
237
Total
Phos-
horns
1240
1300
1330
1260
1650
1130
1650
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
31
4,
51
6'
7
8j
9
10
11 I
12
DT/Ac./
c
App.
Event
8.29
'
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.557
0.557
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.111
0.111
Copper
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
3.215
3.215
Chrominin
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.287
2.287
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.333
0.333
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
0.002
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.278
0.278
denum
Nickel
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.278
0.278
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.557
0.557
Zinc
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.928
3.928
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
27.344
27.344
horns
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
impricnnmPnt fnr knowinp, violations".
D Ig Ia111y signe yJef Retzke
DN' =Jeff Retzke, o=Den111 Water
So _ger,, ou=Senlor Environmental
Y Manager,
if mai4=jeff retzke:adenaliwatercom,c=US
Date2020,02.04 10 24'.30-06'00'
Signature of Land Applier
Date
rWKiQ GODKA KACI cc 11010nna\

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
Land Owner: Edwin Miller, etal
Operator: Ed Miller Farms
Crop 1 Name: Wheat
WQ Permit #: WQ0035720 Field #: 25
Acres Utilized: 42.7
Annual Dry Tons Applied: 353.8293 Site #: NC-GT-03 Acres Permitted: 42.7
Predominant Soil Series: GoA Cation Exchange Capacity (non 503): 73,000 mg/kg
Crop 1 Max. PAN:
136
Crop 2 Name:
N/A
Crop 2 Max. PAN: N/A
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
°
/°
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
We '
Moist)
Precip.
Past 24
Hrs.
inches
a
4
co
a W
*
o
w
*
°Z
5
w
* w
o
TKN
mg/kg
Z
o
oq o
CD
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop I
Crop 2
Oct
2387.15
17.6
8.286
WQ0035720
M
0
S
0.5
0.4
19200
929
33.9
129.381
NA
Wheat
0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp (o this form):
'OTALS:
2387.15
ol
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
129.381
0.000
Lime Applied
knnuallbs/acre
0.557
0
0.557
36.49
0.111
0
0.111
34.71
3.215
0
3.215
1 1335
2.287
0
2.287
1 N/A 1
0.333
0
0.333
267
0.002
0
0.002
1 15.13 1
0.278
0
0.278
N/A 1
0.278
0
0.278
373.8 1
0.557
0
0.557
89 1
3.928
0
3.929
2492
27.344
Date
lbs/ac
'rior Years Cumulative Ibs/ac
'.urrent Cumulative lbs/ac
'ermitted C. P. L. R.****
'ermit PAN Limit I st/2nd Crop
136 N/A
'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation_ inrinding the possibility of fines and imprisonment for knowing violations."
(' /J ° *Application Method: S - Surface, IN - Injection, INC - Incorporation
�t Solutions, ou=3enlw Environmental
IMugrr.
em Il.lehtexEeQMe^a'",°.,.°°m,a°5 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

A1r1NUAL MEIALJ 1:11L' LV LVAMIN" JU1V11V1AKY t'lJK1Vt -
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Lake Kilby WTP Total Dry Tons Applied (Annual):
505.67
Permit #: WQ0035720 Cation Exchange Capacity (non 503 only): 73,000 rng/kg
Operator: Stewart Askew Owner: Reginald Askew Predominant Soil Series: CrA
Acres Used: 74.4 Acres Permitted: 74.4 Site #: NC-GT-07 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mu/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
10/7/19
2�
10/7/19
3
10/17/19
4
10/17/19
5 E
11/2/19
61
11/13/19
7
8
_9j
10 1
Ill 1
12 1
Max
% Solids
15.6
14.9
14
14.4
16.7
17.6
17.6
Arsenic
32.1
1 33.6
13.9
11.2
1 13.4
10.6
1
33.6
Cadmium
6.4
6.7
0.7
0.7
0.6
0.6
6.7
Copper
64.1
68.5
54.5
51.3
194
52.6
194
ChromiLlIn
121
123
131
124
138
107
138
Lead
19.2
20.1
3.6
4.1
13
5.7
20.1
Mercury
0.096
0.099
0.104
0.103
0.091
0.086
0.104
Molyb-
denum
16
16.8
2.6
2.4
2.8
2
16.8
Nickel
16
16.8
15.4
14.4
12.1
14.1
16.8
Selenium
32.1
33.6
3.6
3.5
3
2.8
33.6
Zinc
180
237
186
174
160
131
237
Total
Phos-
horns
1240
1300
1330
1260
1650
1130
1650
Annual Heavy Metal Field Loadings Walculated in lbs/acre):
Total
1
2
3'
4
5
6
7
8
9
10
11 1
12
DT/Ac./
o
App.
Event
6.80
Arsenic
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
1 0.000
0.457
1 0.457
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.091
0.091
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
2.637
2.637
Chi-0111iLlIT1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.876
1.876
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.273
0.273
Mercury
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001,
0.001
Molyb-
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.228
0.228
denum
Nickel
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0,228
0.228
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.457
0.457
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.222
3.222
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
22.427
22.427
horns
"1 cernty, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
/t j) "" 'sr '"left`e
((VJ''�?`j/I(// -�Ielf Peukq mDenali Wa[ei 5olutlun�,
a=Senior Ennronmental Manager,
emaiLyeRrvrzke+.,�tlenaliwale.ccvn,r=US
D te: 30M02W Ih�9.Ov-tt�m
Signature of Land Applicr
Date
IiCnlo c/lnnn nnrl OC 14 n11)nnC\

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
Land Owner: Reginald Askew
Operator: Stewart Askew
WQ Permit #: WQ0035720
Annual Dry Tons Applied: 505.6714
Predominant Soil Series: CrA
Field #: I Acres Utilized: 74.4
Site #: NC-GT-07 Acres Permitted: 74.4
Crop 1 Name: Wheat Crop 1 Max. PAN: 112 Crop 2 Name:
Cation Exchange Capacity (non 503): 73,000 mg/kg
N/A Crop 2 Max. PAN: N/A
'~ ,�
0
Ca
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#
Fert., Animal
Waste, etc)
Soil
Cond.
D
(Dry,
e '
Moist
Precip.
Past 24
Hrs.
inches
Y
'b
:» 'd
r �•
°a a;
c
*
�
4
7° �;
N•
o
TKN
mg/kg
Z
o
o0 0
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Cro17
Crop 2
Crop 1
Crop 2
Sept
2373.31
17.6
4.728
WQ0035720
M
0
S
0.5
0.4
19200
929
33.9
73.824
NA
Wheat
0
Oct
1038.26
17.6
2.068
WQ0035720
M
0
S
0.5
0.4
19200
929
33.9
32.296
NA
Wheat
0
0:000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
i
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
'OTALS:
3411.571
01
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
106.1201
0.000
Lime Applied
knnuallbs/acre
0.457
0.091
2.637
1.876
0.273
0.001
0.228
0.228
0.457
3.222 22.427
9.292
12.514
2492
Date
lbs/ac
'rior Years Cumulative lbs/ac
0.335
0.086
6.207
3.019
0.806
0.008
0.166
0.501
0.451
.urrent Cumulative lbs/ac
0.792
0.177
8.844
4.895
1.079
0.009
0.394
0.729
0.908
'ermitted C. P. L. R.****
36.49
34.71
1335
N/A
267
15.13
1 N/A
373.8
89
'ermit PAN Limit Ist/2nd Crop
1 112 N/A
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation, including the possibility of fines and imprisonment for knowing violations."
IX9�rsryleMRecY�.,JReb4e u
Application Method: S -Surface, IN -Injection, INC -Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Wayt *r�pto
ANALYTICAL
10/16/2019
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 19-281-0004
Project Description: Lake Kilby WTP 2019 3 of 6
7621 Whitepine Road, Richmond, VA 23237
Main 804.743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/8/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Paae 1 of 8

Way po*l to
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Denali Water CASE NARRATIVE
Project: Lake Kilby WTP 2019 3 of 6
Lab Report Number: 19-281-0004
Date: 10/17/2019
Metals Analysis Method 6010D
Sample 68529
Analyte: Aluminum
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Calcium
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Potassium
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Lead
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Sulfur
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: L458430
PaQe 2 of 8

Waypoi t
4
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Paae 3 of 8

0 0 Ao"L
Waypoint,
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-281-0004
Client Project Description: Lake Kilby WTP 2019 3 of 6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
68528
3/6
Solids
10/07/2019
11:30
10/08/2019
68528
3/6
Solids
10/07/2019
11:30
10/08/2019
SM-2540G
WTN
68528
3/6
Solids
10/07/2019
11:30
10/08/2019
SW-7471B
WTN
68528
3/6
Solids
10/07/2019
11:30
10/08/2019
SM-4500-NH3C-TKN
WTN
68528
3/6
Solids
10/07/2019
11:30
10/08/2019
4500NO3F-2011
WTN
68528
3/6
Solids
10/07/2019
11:30
10/08/2019
6010D
WTN
68528
3/6
Solids
10/07/2019
11:30
10/08/2019
SM-4500-NH3C
WTN
68528
3/6
Solids
10/07/2019
11:30
10/08/2019
9045D
WTN
68528
3/6
Solids
10/07/2019
11:30
10/08/2019
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia
Pane 4 of 8

Waypointo
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 19-281-0004
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Lake Kilby WTP 2019 3 of 6
Information :
REPORT OFANALYSIS
Report Date : 10/17/2019
Received : 10/08/2019
Pam« Gowl"
44
Pauric McGroary
Agronomist
Lab No : 68528 Matrix: Solids
Sample ID: 3/6 Sampled: 30/7/2019 11:30
Moisture 84.4 H % 0.010 1 10/15/19 16:30 ADM SM-2540G
Selenium <32.1 mg/Kg - dry 32.1 10 10/10/19 23:10 BKN 6010D
Total Solids
15.6 H
%
0.010
1
10/15/19 16:30
ADM
SM-2540G
Total Kjeldahl Nitrogen
1.71
% - dry
0.160
1
10/15/19 09:00
JPJ >M-4500-NH3C-TKP
Phosphorus
1240
mg/Kg - dry
321
10
10/10/19 23:10
BKN
6010D
Potassium
<321
mg/Kg - dry
321
10
10/10/19 23:10
BKN
6010D
Sulfur
13600
mg/Kg - dry
321
10
10/10/19 23:10
BKN
6010D
Calcium
1700
mg/Kg - dry
1600
10
10/10/19 23:10
BKN
6010D
Magnesium
641
mg/Kg - dry
321
10
10/10/19 23:10
BKN
6010D
Iron
22100
mg/Kg - dry
321
10
10/10/19 23:10
BKN
6010D
Manganese
4180
mg/Kg - dry
32.1
10
10/10/19 23:10
BKN
6010D
Copper
64.1
mg/Kg - dry
16.0
10
10/10/19 23:10
BKN
6010D
Organic N
1.71
% - dry
0.160
1
10/15/19 09:00
DH
CALICULATION
Nitrate+Nitrite-N
<30.2
mg/Kg - dry
30.2
1
10/11/19 15:31
ZBD
4500NO3F-2011
Nickel
<16.0
mg/Kg - dry
16.0
10
10/10/19 23:10
BKN
6010D
Mercury
<0.0961
mg/Kg - dry
0.0961
1
10/11/19 12:23
TJS
SW-7471B
pH
6.3
S.U.
1
10/14/19 09:55
JSL
9045D
Calcium Carbonate Equivalent
7.3
%
0.1
1
10/15/19 14:55
DXT
AOAC 955.01
Total Volatile Solids
46.7 H
%
0.010
1
10/15/19 16:30
ADM
SM-2540G
Qualifiers/ *
Outside QC Limit
B
Analyte detected in blank
Definitions C
GCMS Confirmation Analysis
E
Result above cal range
9
GGA Outside QC Limits
H
Beyond holding time
J
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
Refer to cover letter.
Page 5 of 8

i
Waypoint,
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
07274
Denali Water
Jeff Retzke
Project
Lake Kilby
WTP 2019 3 of 6 Report Date : 10/17/2019
1001 Fraser Ave
Information :
Received : 10/08/2019
Huntsville , AL 35801
pwi4 imC 6ewr
Pauric McGroary
Report Number :19-281-0004
REPORT OF ANALYSIS
Agronomist
Lab No : 68528
Matrix: Solids
Sample ID: 3/6
Sampled: 10/7/2019 11:30
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
<0.064
% -dry
0.064
1 10/15/19 13:00 JPJ SM-4500-NH3C
Aluminum 176000
mg/Kg - dry
321
10 10/10/19 23:10 BKN 6010D
Arsenic
<32.1
mg/Kg - dry
32.1
10 10/10/19 23:10 BKN 6010D
Cadmium
<6.41
mg/Kg - dry
6.41
10 10/10/19 23:10 BKN 6010D
Chromium
121
mg/Kg - dry
16.0
10 10/10/19 23:10 BKN 6010D
Lead
<19.2
mg/Kg - dry
19.2
10 10/10/19 23:10 BKN 6010D
Molybdenum
<16.0
mg/Kg - dry
16.0
10 10/10/19 23:10 BKN 6010D
Sodium Absorption Ratio
3.31
1 CALCULATION
Sodium <1600 mg/Kg - dry 1600 10 10/10/19 23:10 BKN 6010D
Zinc 180 mg/Kg - dry 80.1 10 10/10/19 23:10 BKN 6010D
Qualifiers/ B Analyte detected in blank H Beyond holding time
Definitions
Paste 6 of 8

WayPAo�nt,..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 19-281-0004
Shipping Method
Fed Ex US Postal Lab
+� UPS Client Courier
Other : I
Thermometer ID:
Shipping container/cooler uncompromised?
Yes
No
Number of coolers received
F 1
Custody seals intact on shipping container/cooler?
Yes
No
Not Required
Custody seals intact on sample bottles?
Yes
No
0 Not Required
Chain of Custody (COC) present?
r Yes
No
COC agrees with sample label(s)?
0 Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
• Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
Yes
No
r N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with VOAs
Yes
No
0 N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions
Comments:
or instructions included?
I�
Yes
0 No
III
Signature: 'Brandi Watson Date & Time: 10/08/2019 14:44:03
Paae 7 of 8

@OIL SAMPLE TRH
PO 7621 Whitepine Road Richmond VA 2323
19-281-0004
07274
Denali water 14:42:56
Lake Kiibv WTP 2019 1 of 6
)DY
[e-mail]
Account #
Submitted By
unarge I o
Copy To
Jeff Retzke/Denali Water P0: DEW
jeff.retzkeedenaliwater.com
35 Refreshment Place
Jeff's Cell: 256.503.4300
Decatur, AL 35601
Project Lake Kilby WTP 2019 1&2 0 6
Sample Information
Lab Number
Collection infatuation
Container Information
Please Check Desired Teats
Type
Date
Time
Number
of Bottles
Type
Volume
SO
SL2
503
Metals
Nitrogen
Series
pH
CCE
Ag
CI
Volatile
Solids
Others
Sample ID
(Lab Use
Only)
Grab
i
Glass
X Plastic
oz
pint
Standard Compas
w/Aluminum, CCE
Composite
0 I
I//
—_
and S.A.R.
/
x Grab
1
X Plastic
x oz
--p flt
same as above
Can
d f
I( r
—Glass
at
Grab
Glass
— oz
_
Plastic
--pint
Com e
_
Grob
-- oz
icomp
—Glass
Plastic
—pint
i at
I
f
Rell uis nature
Date
Time
Received (Signature)
Date
Time
/O •
2 j0
Test Package Details
Special Instructions or Remarks
SLt: Total Solids (Moiswre) Total Kieldahi Nitrogen, Phosphorus and Potassium
SL2: Basic Test SLI plus Sulfur, Calcium, Magnmsium,Sodium, Iran, Alumintan, Manganese, Copper And Zinc
603 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc induded In SL2)
'
Nitrogen Series Total KieWahl, Ammonium, Nitrate dt Organic Nitrogen
CCE: Caldum Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
r

0 (D
Waypoint
ANALYTICAL
10/16/2019
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 19-281-0005
Project Description: Lake Kilby WTP 2019 4 of 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/8/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
i',• Or 0-7'
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Pane 1 of 8

Way po0l to
ANALYTICAL
Client: Denali Water
Project: Lake Kilby WTP 2019 4 of 6
Lab Report Number: 19-281-0005
Date: 10/17/2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 68529 (4/6)
Analyte: Aluminum
QC Batch No: L458430/L458055
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: L458430/L458055
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Calcium
QC Batch No: L458430/L458055
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Potassium
QC Batch No: L458430/L458055
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: L458430/1-458055
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Lead
QC Batch No: L458430/L458055
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Sulfur
QC Batch No: L458430/L458055
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: L4584301458055
PaQe 2 of 8

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 8

Waypoint(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-281-0005
Client Project Description: Lake Kilby WTP 2019 4 of 6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
68529
4/6
Solids
10/07/2019 11:45
10/08/2019
68529
4/6
Solids
10/07/2019 11:45
10/08/2019
SM-2540G
WTN
68529
4/6
Solids
10/07/2019 11:45
10/08/2019
SW-7471B
WTN
68529
4/6
Solids
10/07/2019 11:45
10/08/2019
SM-4500-NH3C-TKN
WTN
68529
4/6
Solids
10/07/2019 11:45
10/08/2019
4500NO3F-2011
WTN
68529
4/6
Solids
10/07/2019 11:45
10/08/2019
6010D
WTN
68529
4/6
Solids
10/07/2019 11:45
10/08/2019
SM-4500-NH3C
WTN
68529
4/6
Solids
10/07/2019 11:45
10/08/2019
9045D
WTN
68529
4/6
Solids
10/07/2019 11:45
10/08/2019
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia
Paae 4 of 8

Waypointo
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 19-281-0005
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Lake Kilby WTP 2019 4 of 6
Information :
REPORT OF ANALYSIS
Report Date : 10/17/2019
Received : 10/08/2019
Pam« OF 6ewr
Pauric McGroary
Agronomist
Lab No : 68529 Matrix: Solids
Sample ID: 4/6 Sampled: 10/7/2019 11:45
Moisture 85.1 H % 0.010 1 10/15/19 16:30 ADM SM-2540G
Selenium <33.6 mg/Kg - dry 33.6 10 10/10/19 23:15 BKN 6010D
Total Solids
14.9 H
%
0.010
1 10/15/19 16:30
ADM
SM-254OG
Total Kjeldahl Nitrogen
1.58
% - dry
0.167
1 10/15/19 09:00
JPJ ')M-4500-NH3C-TKP
Phosphorus
1300
mg/Kg - dry
336
10 10/10/19 23:15
BKN
6010D
Potassium
<336
mg/Kg - dry
336
10 10/10/19 23:15
BKN
6010D
Sulfur
14200
mg/Kg - dry
336
10 10/10/19 23:15
BKN
6010D
Calcium
3700
mg/Kg - dry
1680
10 10/10/19 23:15
BKN
6010D
Magnesium
671
mg/Kg - dry
336
10 10/10/19 23:15
BKN
6010D
Iron
22600
mg/Kg - dry
336
10 10/10/19 23:15
BKN
6010D
Manganese
4260
mg/Kg - dry
33.6
10 10/10/19 23:15
BKN
6010D
Copper
68.5
mg/Kg - dry
16.8
10 10/10/19 23:15
BKN
60I10D
Organic N
1.58
Igo - dry
0.167
1 10/15/19 09:00
DH
CALCULATION
Nitrate+Nitrite-N
<33.6
mg/Kg - dry
33.6
1 10/11/19 15:32
ZBD
4500NO3F-2011
Nickel
<16.8
mg/Kg - dry
16.8
10 10/10/19 23:15
BKN
6010D
Mercury
<0.0993
mg/Kg - dry
0.0993
1 10/11/19 12:24
TJS
SW-7471B
pH
6.6
s.u.
1 10/14/19 09:55
JSL
9045D
Calcium Carbonate Equivalent
6.8
%
0.1
1 10/15/19 14:55
DXT
AOAC 955.01
Total Volatile Solids
46.7 H
%
0.010
1 10/15/19 16:30
ADM
SM-2540G
Qualifiers/
*
Outside QC Limit
B
Analyte detected in blank
Definitions
C
GCMS Confirmation Analysis
E
Result above cal range
9
GGA Outside QC Limits
H
Beyond holding time
J
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
Refer to cover letter.
Pane 5 of 8

Waypoi nt,.
7621 Whitepine Road,
Richmond, VA 23237
Main 804-743-9401
° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
07274
Denali Water
Jeff Retzke
Project
Lake Kilby
WTP 2019 4 of 6
Report Date : 10/17/2019
1001 Fraser Ave
Information :
Received : 10/08/2019
Huntsville , AL 35801
Pam« or Gewr
Pauric McGroary
Report Number : 19-281-0005
REPORT OF ANALYSIS
Agronomist
Lab No : 68529
Matrix: Solids
Sample ID: 4/6
Sampled: 30/7/2019 11:45
Test
Results
Units
MQL
DF
Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
<0.067
% - dry
0.067
1
10/15/19 13:00 JPJ SM-4500-NH3C
Aluminum 183000
mg/Kg - dry
336
10
10/10/19 23:15 BKN 6010D
Arsenic
<33.6
mg/Kg - dry
33.6
10
10/10/19 23:15 BKN 6010D
Cadmium
<6.71
mg/Kg - dry
6.71
10
10/10/19 23:15 BKN 6010D
Chromium
123
mg/Kg - dry
16.8
10
10/10/19 23:15 BKN 6010D
Lead
<20.1
mg/Kg - dry
20.1
10
10/10/19 23:15 BKN 6010D
Molybdenum
<16.8
mg/Kg - dry
16.8
10
10/10/19 23:15 BKN 6010D
Sodium Absorption Ratio
2.56
1
CALCULATION
Sodium
<1680
mg/Kg - dry
1680
10
10/10/19 23:15 BKN 6010D
Zinc
237
mg/Kg - dry
83.9
10
10/10/19 23:15 BKN 6010D
Qualifiers/ B Analyte detected in blank
Definitions
H Beyond holding time
Paqe 6 of 8

WayPAo�nt.i
..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 19-281-0005
Shipping Method
Fed Ex US Postal Lab
UPS Client Courier
Other : l
Thermometer ID:
�—
Shipping container/cooler uncompromised?
Yes
No
Number of coolers received
�1
Custody seals intact on shipping container/cooler?
Yes
No
Not Required
Custody seals intact on sample bottles?
Yes
No
Not Required
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
0 Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
No
Water - Sample containers properly preserved
Yes
No
0 N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with VOAs
Yes
No
0 N/A
Sol VOA method 5035 — compliance criteria met
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Special precautions or instructions included?
Comments:
Yes No r N/A
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Yes • No
Signature: !Brandi Watson
Date & Time: 110/08/2019 15:04.29
Paqe 7 of 8

SAMPLE TRANSMITTAL Account it
ftuA&L Easte I� �� �� � 07274 9
7621 Whnepine Road Richmond VA 23'_37 Tel" 804-743-9401 Denali water 15.O:i.2
Lake Kill-- WTG N I0 2 of a
Customer infom _
Submitted By �• •-• s- " -
Jeff Retzke/Denali Water P0: DEW
jeff.retzke0denaliwater.com
35 Refreshment: --Place
Jeff's Cel=: 256.503.4300
Decatur, AL 35601
Project Lake Ki lby WTP 2019 1 &2 O 6
Sample Information
Lab Number
Collection Information
Container Information
Please Check Desired Tests
Type
Date
Time
Number
Type
Volume
SL1
SL2
$03
Metals
Nitrogen
Series
pH
CCE
Ag
Cl
Volatile
Solids
Others
Sample ID
(Lab Use
Only)
of Bottles
Grab
1
Glass
X plM
Standard campoa t
ajAlumirum, CCE
L
Composite
f
f f�
, *1�.�.
/ / J •0�
—LP' 83EIC
qt
and S.A.R.
2 1
Grab
x
Com osite
O 7
% f `
t
j
_ Glass
x Plastic
_ oz
x pint
t
Same as above
Grab
Glass
oz
_
Plastic
�nt
Com site
Grab
Glass
— oz
site
_
Plastic
pint
at
Reti uishe (Signature)
Date
Time
Received By: (Signature)
Date
Time
Gb S
Test Package Details
Special Instructions or Remarks
SLI: Total Solids (Moisture) Total Kleldehl Nitrogen, Phosphorus and Potassium
SL2: Basle Test SL 1 plus Sulfur, Calcium. Magnesium,Sodium, Iron, Aluminum. Manganese, Copper And Zinc
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc included in SL2)
Nitrogen Series: Total Kieldahl, Ammonium, Nitrate & Organic Nitrogen
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)

Waypoi s
ANALYTICAL
10/29/2019
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 19-291-0008
Project Description: Lake Kilby WTP 2019 5 of 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/18/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Paqe 1 of 6

Waypoint, 7621 (2) Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-291-0008
Client Project Description: Lake Kilby WTP 2019 5 of 6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
68724
5 of 6
Solids
68724
5 of 6
Solids
68724
5 of 6
Solids
68724
5 of 6
Solids
68724
5 of 6
Solids
68724
5 of 6
Solids
68724
5 of 6
Solids
68724
5 of 6
Solids
68724
5 of 6
Solids
10/17/2019
15:15
10/18/2019
10/17/2019
15:15
10/18/2019
10/17/2019
15:15
10/18/2019
10/17/2019
15:15
10/18/2019
10/17/2019
15:15
10/18/2019
10/17/2019
15:15
10/18/2019
10/17/2019
15:15
10/18/2019
10/17/2019
15:15
10/18/2019
10/17/2019
15:15
10/18/2019
SM-254OG
WTN
SW-7471 B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia
Paqe 2 of 6

Waypoint(l)
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 19-291-0008
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Lake Kilby WTP 2019 5 of 6
Information :
REPORT OPANALYSIS
Report Date : 10/29/2019
Received : 10/18/2019
Pit. OF 69wr
Pauric McGroary
Agronomist
Lab No : 68724 Matrix: Solids
Sample ID : 5 of 6 Sampled: 10/17/2019 15:15
Moisture 86.0 H % 0.010 1 10/26/19 13:00 CJR SM-254OG
Selenium <3.57 mg/Kg - dry 3.57 1 10/24/19 18:39 JTR 6010D
Total Solids
14.0 H
%
0.010
1 10/26/19 13:00
CJR
SM-2540G
Total Kjeldahl Nitrogen
19200
mg/Kg - dry
1790
1 10/25/19 10:00
JPJ ')M-4500-NH3C-TKP
Phosphorus
1330
mg/Kg - dry
35.7
1 10/24/19 18:39
JTR
6010D
Potassium
169
mg/Kg - dry
35.7
1 10/24/19 18:39
JTR
6010D
Sulfur
16100
mg/Kg - dry
35.7
1 10/24/19 18:39
JTR
6010D
Calcium
1500
mg/Kg - dry
179
1 10/24/19 18:39
JTR
6010D
Magnesium
647
mg/Kg - dry
35.7
1 10/24/19 18:39
JTR
6010D
Iron
22600
mg/Kg - dry
35.7
1 10/24/19 18:39
JTR
6010D
Manganese
4260
mg/Kg - dry
35.7
10 10/25/19 21:25
JTR
6010D
Copper
54.5
mg/Kg - dry
1.79
1 10/24/19 18:39
JTR
6010D
Organic N
18300
mg/Kg - dry
1790
1 10/25/19 10:00
DH
CA11CULATION
Nitrate+Nitrite-N
<33.9
mg/Kg - dry
33.9
1 10/24/19 14:36
ZBD
4500NO3F-2011
Nickel
15.4
mg/Kg - dry
1.79
1 10/24/19 18:39
JTR
6010D
Mercury
<0.104
mg/Kg - dry
0.104
1 10/23/19 14:18
TJS
SW-7471B
pH
7.1
S.U.
1 10/23/19 07:07
JSL
9045D
Calcium Carbonate Equivalent
10.7
% - dry
0.1
1 10/24/19 15:30
DXT
AOAC 955.01
Total Volatile Solids
47.5 H
%
0.010
1 10/26/19 13:00
CJR
SM-2540G
Qualifiers/
*
Outside QC Limit
B
Analyte detected in blank
Definitions
C
GCMS Confirmation Analysis
E
Result above cal range
9
GGA Outside QC Limits
H
Beyond holding time
J
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
Refer to cover letter.
Page 3 of 6

•
Waypo
i
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
07274
Denali Water
Jeff Retzke
Project
Lake Kilby
WTP 2019 5 of 6 Report Date : 10/29/2019
1001 Fraser Ave
Information :
Received : 10/18/2019
Huntsville , AL 35801i
y� , /
i Apia Ir (few
Pauric McGroary
Report Number : 19-291-0008
REPORT OFANAL YSIS
Agronomist
Lab No : 68724
Matrix: Solids
Sample ID : 5 of 6
Sampled: 10/17/2019 15:15
Test
Results
Units
MQL
DF Date I Time By Analytical
Analyzed Method
Ammonia Nitrogen
929
mg/Kg - dry
714
1 10/25/19 14:00 JPJ SM-4500-NH3C
Aluminum
209000
mg/Kg - dry
357
10 10/25/19 21:25 JTR 6010D
Arsenic
13.9
mg/Kg - dry
3.57
1 10/24/19 18:39 JTR 6010D
Cadmium
<0.714
mg/Kg - dry
0.714
1 10/24/19 18:39 JTR 6010D
Chromium
131
mg/Kg - dry
1.79
1 10/24/19 18:39 JTR 6010D
Lead
3.57
mg/Kg - dry
2.14
1 10/24/19 18:39 JTR 6010D
Molybdenum
2.57
mg/Kg - dry
1.79
1 10/24/19 18:39 JTR 6010D
Sodium Absorption Ratio
0.58
1 CALCULATION
Sodium
286
mg/Kg - dry
179
1
10/24/19 18:39
JTR
6010D
Zinc
186
mg/Kg - dry
8.93
1
10/24/19 18:39
JTR
6010D
Qualifiers/ B Analyte detected in blank
Definitions
H Beyond holding time
Paqe 4 of 6

(DW•
ayPa�nt..
7621 Wh 804-7 Road, Richmond,
27 -6446
Main 804-743-94U1 0Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 19-291-0008
Shipping Method
Fed Ex US Postal Lab
Other
UPS Client Courier
Thermometer ID:
Shipping container/cooler uncompromised?
+, Yes
No
Number of coolers received
F 1
Custody seals intact on shipping container/cooler?
Yes
No 0 Not Required
Custody seals intact on sample bottles?
Yes
No Not Required
Chain of Custody (COC) present?
! Yes
No
COC agrees with sample label(s)?
• Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
• Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Yes
No 0 N/A
Water - VOA vials free of headspace
Yes
No • N/A
Trip Blanks received with VOAs
Yes
No 0 N/A
$oil VOA method 5035 — compliance criteria met
Yes
No 0 N/A
High concentration container (48 hr)
Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
0 No
Comments:
--
Signature: lBrandi Watson
Date & Time: 10/18/2019 14:43:21
Page 5 of 6

7621 Whitepine Road Richmond VA 23237
is-291-0008
07214
10.18-2019
Denali Water 14:0324
C1 Lake KON VY I p zu in
Subm#W By
W114119" IV
Copy TO
Jeff Retzke/Denali Water PO: DEW
jeff.retzkeedenaliwater.com
35 Refreshment Place
Jeff's Cell 256.503.4300
Decatur, AL 35601
Project Lake Kilby WTP 2018 1&2 of 6
Sample Information
Lab Number
Collection Information
Container irdomtation
Plow Check Desired
Tests
Sem;* ID
(Lab Use
Only)
Type
Data
Time
N
Type
I
Volume
SLI
SL2
603
N*oW
pH
CCE
I
Ag
Cl
Vowft
Others
Of saw"
Mobil
Safi"
soft
Grob
")s
Glass
--r Plastic
1
— oz
X pint
St
W/Aluminum, CCZ
Composite
-3
-Qt
1.
and S.A. R.
Grob
,
Glass
oz
Int
Z—�at
7
x Plastic
Same an above
Grab
Gins
Plastic
oz
Int
Grab
Glass
Oz
Plastic
___jlnl
/R6$hquMk By:
Date
Time
Received By* (Signature)
Date
Time
—
Z
7
tQ
Test Packaw Details
Special Instructions or Remarks
SLI: Total Solids (Moisan) Total Kjoidshl Nitropti, Phosphorus and Potassium
SL2., Basic Test SL I plus Sulfur, Calcium lAwmium.Sodium lm% Aluminum, Manganese, CoppW And Zinc
50 11111stals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Load, Nickel, Selenium,
(Copper & Zinc included In SL2)
Nitrow Series. Total Yjeldahl, Aromonium Nitrate & Organic Nitropm
CCE.- Calclurn Carbonate Equivalent or Total neutralization Value (For Urne Treated Sludge)
D- a of F

Waypdint.,(D
ANALYTICAL
10/29/2019
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 19-291-0009
Project Description: Lake Kilby WTP 2019 6 of 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/18/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Paqe 1 of 6

f
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-291-0009
Client Project Description: Lake Kilby WTP 2019 6 of 6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
68725
6 of 6
Solids
68725
6 of 6
Solids
68725
6 of 6
Solids
68725
6 of 6
Solids
68725
6 of 6
Solids
68725
6 of 6
Solids
68725
6 of 6
Solids
68725
6 of 6
Solids
68725
6 of 6
Solids
10/17/2019
15:30
10/18/2019
10/17/2019
15:30
10/18/2019
10/17/2019
15:30
10/18/2019
10/17/2019
15:30
10/18/2019
10/17/2019
15:30
10/18/2019
10/17/2019
15:30
10/18/2019
10/17/2019
15:30
10/18/2019
10/17/2019
15:30
10/18/2019
10/17/2019
15:30
10/18/2019
SM-2540G
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia
Paqe 2 of 6

7621
Wa �s
�,. Whitepine Road, Richmond, VA 23237
yp Main 804-743-9401 ° fax [phone]
ANALYTICAL www.waypointanalytical.com
07274
Denali Water
Jeff Retzke Project Lake Kilby WTP 2019 6 of 6 Report Date : 10/29/2019
1001 Fraser Ave Information : Received : 10/18/2019
Huntsville , AL 35801
Report Number : 19-291-0009
REPORT OPANALYSIS
Pauric McGroary
Agronomist
Lab No : 68725 Matrix: Solids
Sample ID : 6 of 6 Sampled: 10/17/2019 15:30
Moisture 85.6 H % 0.010 1 10/26/19 13:00 CJR SM-2540G
Selenium <3.47 mg/Kg - dry 3.47 1 10/24/19 18:44 JTR 6010D
Total Solids
14.4 H
%
0.010
1 10/26/19 13:00
CJR
SM-254OG
Total Kjeldahl Nitrogen
16500
mg/Kg - dry
1740
1 10/25/19 10:00
JPJ
;M-4500-NH3C-TKP
Phosphorus
1260
mg/Kg - dry
34.7
1 10/24/19 18:44
JTR
6010D
Potassium
163
mg/Kg - dry
34.7
1 10/24/19 18:44
JTR
6010D
Sulfur
15300
mg/Kg - dry
34.7
1 10/24/19 18:44
JTR
6010D
Calcium
1430
mg/Kg - dry
174
1 10/24/19 18:44
JTR
6010D
Magnesium
619
mg/Kg - dry
34.7
1 10/24/19 18:44
JTR
6010D
Iron
21400
mg/Kg - dry
34.7
1 10/24/19 18:44
JTR
6010D
Manganese
4030
mg/Kg - dry
34.7
10 10/25/19 21:30
JTR
6010D
Copper
51.3
mg/Kg - dry
1.74
1 10/24/19 18:44
JTR
6010D
Organic N
15600
mg/Kg - dry
1740
1 10/25/19 10:00
DH
CALCULATION
Nitrate+Nitrite-N
<32.6
mg/Kg - dry
32.6
1 10/24/19 14:36
ZBD
4500NO3F-2011
Nickel
14.4
mg/Kg - dry
1.74
1 10/24/19 18:44
JTR
6010D
Mercury
<0.103
mg/Kg - dry
0.103
1 10/23/19 14:19
TJS
SW-7471B
pH
6.9
S.U.
1 10/23/19 07:07
JSL
9045D
Calcium Carbonate Equivalent
8.5
% - dry
0.1
1 10/24/19 15:30
DXT
AOAC 955.01
Total Volatile Solids
47.7 H
%
0.010
1 10/26/19 13:00
CJR
SM-254OG
Qualifiers/
*
Outside QC Limit
B
Analyte detected in blank
Definitions
C
GCMS Confirmation Analysis
E
Result above cal range
g
GGA Outside QC Limits
H
Beyond holding time
J
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
Refer to cover letter.
Paqe 3 of 6

Waypoint, 7621 (2) Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
07274
Denali Water
Jeff Retzke Project Lake Kilby WTP 2019 6 of 6 Report Date : 10/29/2019
1001 Fraser Ave Information : Received : 10/18/2019
Huntsville , AL 35801
Pam« imp Ga°"�
Report Number :19-291-0009 REPORT OFANALYSIS Pauric McGroary
Agronomist
Lab No : 68725 Matrix: Solids
Sample ID : 6 of 6 Sampled: 10/17/2019 15:30
Test Results Units MQL DF Date I Time By Analytical
Analyzed Method
Ammonia Nitrogen
840
mg/Kg - dry
694
1
10/25/19 14:00
JPJ
SM-4500-NH3C
Aluminum
203000
mg/Kg - dry
347
10
10/25/19 21:30
JTR
6010D
Arsenic
11.2
mg/Kg - dry
3.47
1
10/24/19 18:44
JTR
6010D
Cadmium
<0.694
mg/Kg - dry
0.694
1
10/24/19 18:44
JTR
6010D
Chromium
124
mg/Kg - dry
1.74
1
10/24/19 18:44
JTR
6010D
Lead
4.12
mg/Kg - dry
2.08
1
10/24/19 18:44
JTR
6010D
Molybdenum
2.35
mg/Kg - dry
1.74
1
10/24/19 18:44
JTR
6010D
Sodium Absorption Ratio
0.61
1
CALCULATION
Sodium
290
mg/Kg - dry
174
1
10/24/19 18:44
JTR
6010D
Zinc
174
mg/Kg - dry
8.68
1
10/24/19 18:44
JTR
6010D
Qualifiers/ B Analyte detected in blank H Beyond holding time
Definitions
Paqe 4 of 6

WayPAnt, r
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 19-291-0009
Shipping Method
Fed Ex US Postal Lab
UPS Client Courier
Other :
Thermometer ID:
�r
.
Shipping container/cooler uncompromised?
Yes
No
Number of coolers received
F
Custody seals intact on shipping container/cooler?
Yes
No
Not Required
Custody seals intact on sample bottles?
Yes
No
I* Not Required
Chain of Custody (COC) present?
Yes
No
COC agrees with sample label(s)?
Yes
No
COC properly completed
Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
i No
Water - Sample containers properly preserved
Yes
No
I* N/A
Water - VOA vials free of headspace
Yes
No
N/A
Trip Blanks received with VOAs
Yes
No
N/A
Soil VOA method 5035 — compliance criteria) met
Yes
No
I* N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
Yes 0 No
Signature: Brandl Watson _I Date & Time: 10/18/2019 14:59 06
Paqe 5 of 6

A&L Eastern Labor
7621 Whitepine Road Richmond VA 23237 Tel_$04-743.9401 Fax: $
Customer Information
Submitted By Charge .,
Jeff Retzke/Denali Water PO: DEW
35 Refreshment Place
Decatur, AL 35601
Lake Kilby WTP 2018 1&2 of 6
ffllf��l(I(�Illll(If(IIIIN1111111(INifl1111l(> 1107 g1--00009
Denali Water
Like Kiltry W TP 2019 6 of 6 14:58:52
jeff.retzkeedenaliwater.com
Jeff's Cell: 256.503.4300
E
ccount #
Sam le Information
Lab Number Collection Information Container intorma€lon
Sample ID (Lab Use Please Check Desired Tests
Only)
Type
Date
Time
Number
of Bottles
yp
Type
Volume
SL1
SL2
503
Nitrogen
CCE
Ag
Volatile
Metals
Series
pH
Cl
Solids
Others
S
Grab
Standard CQmpoe
rr/Aluminum, CCE
_
Composite
�1— jr
f j
1
_ Glass
x Plastic
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,
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t
Received B Sl nature Date Time
d
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Date
Time
f,+
� �•
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to
Test Package Details
SLI: Total Solids (Moisture) Total Kjcldahl Nitrogen, Phosphorus and Potassium
SL2: Basic Test SLI plus Sulfur, Calcium, Magnesium,Sodium, Iron, Aluminum, Manganese, Copper And Zinc
603 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc included in SL2)
;Nitrogen Series: Total Kjeidahl, Ammonium, Nitrate & Organic Nitrogen.
CCE: Calcium Carbonate Equivalenl or Total neutralization Value (For Lime Treated Sludge)
n
or Remarks
n--- r- -r r

Waypoint(D
ANALYTICAL
11/12/2019
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 19-308-0006
Project Description: Lake Kilby WTP 2019 1 of 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/4/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
e. Ir 6—r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Paqe 1 of 7

Waypdiant(D
ANALYTICAL
Client: Denali Water
Project: Lake Kilby WTP 2019 1 of 6
Lab Report Number: 19-308-0006
Date: 11 /12/2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 69509
Analyte: Aluminum
QC Batch No: L463362
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L463096
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Iron
QC Batch No: L463096
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Manganese
QC Batch No: L463362
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L463096
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 2 of 7

0
Waypoint. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-308-0006
Client Project Description: Lake Kilby WTP 2019 1 of 6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
69508
1 of 6
Solids
69508
1 of 6
Solids
69508
1 of 6
Solids
69508
1 of 6
Solids
69508
1 of 6
Solids
69508
1 of 6
Solids
69508
1 of 6
Solids
69508
1 of 6
Solids
69508
1 of 6
Solids
11/02/2019
10:00
11/04/2019
11/02/2019
10:00
11/04/2019
11/02/2019
10:00
11/04/2019
11/02/2019
10:00
11/04/2019
11/02/2019
10:00
11/04/2019
11/02/2019
10:00
11/04/2019
11/02/2019
10:00
11/04/2019
11/02/2019
10:00
11/04/2019
11/02/2019
10:00
11/04/2019
SM-2540G
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN
Paqe 3 of 7

Waypointo
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 19-308-0006
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Lake Kilby WTP 2019 1 of 6
Information :
REPORT OFANALYSIS
Report Date : 11/12/2019
Received : 11/04/2019
Pw« or 64w
Pauric McGroary
Agronomist
Lab No : 69508 Matrix: Solids
Sample ID : 1 of 6 Sampled: 31/2/2019 10:00
Moisture 83.3 % 0.010 1 11/06/19 17:12 ADM SM-2540G
Selenium <2.99 mg/Kg - dry 2.99 1 11/07/19 04:55 BKN 6010D
Total Solids
16.7
%
0.010
1 11/06/19 17:12
ADM
SM-2540G
Total Kjeldahl Nitrogen
19200
mg/Kg - dry
1500
1 11/11/19 09:00
JPJ >M-4500-NH3C-TKP
Phosphorus
1650
mg/Kg - dry
29.9
1 11/07/19 04:55
BKN
6010D
Potassium
272
mg/Kg - dry
29.9
1 11/07/19 04:55
BKN
6010D
Sulfur
15300
mg/Kg - dry
29.9
1 11/07/19 04:55
BKN
6010D
Calcium
1870
mg/Kg - dry
150
1 11/07/19 04:55
BKN
6010D
Magnesium
599
mg/Kg - dry
29.9
1 11/07/19 04:55
BKN
6010D
Iron
22600
mg/Kg - dry
29.9
1 11/07/19 04:55
BKN
6010D
Manganese
4960
mg/Kg - dry
29.9
10 11/08/19 10:52
BKN
6010D
Copper
194
mg/Kg - dry
1.50
1 11/07/19 04:55
BKN
6010D
Organic N
1�400
mg/Kg - dry
1500
1 11/11/19 09:00
DH
CALCULATION
Nitrate+Nitrite-N
<27.7
mg/Kg - dry
27.7
1 11/06/19 14:23
ZBD
4500NO3F-2011
Nickel
12.1
mg/Kg - dry
1.50
1 11/07/19 04:55
BKN
6010D
Mercury
<0.0910
mg/Kg - dry
0.0910
1 11/07/19 12:10
TJS
SW-7471B
pH
6.8
S.U.
1 11/08/19 05:47
JSL
9045D
Calcium Carbonate Equivalent
14.7
% - dry
0.1
1 11/08/19 13:43
DXT
AOAC 955.01
Total Volatile Solids
45.8
%
0.010
1 11/06/19 17:12
ADM
SM-2540G
Qualifiers/
*
Outside QC Limit
B
Analyte detected in blank
Definitions
C
GCMS Confirmation Analysis
E
Result above cal range
9
GGA Outside QC Limits
H
Beyond holding time
J
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
Refer to cover letter.
Paqe 4 of 7

•
Wavpoint7621
•
Whitepine
Road, Richmond,
VA 23237
Aw
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
07274
Denali Water
Jeff Retzke
Project
Lake Kilby
WTP 2019 1
of 6
Report Date : 11/12/2019
1001 Fraser Ave
Information :
Received : 11/04/2019
Huntsville , AL 35801
�p
Twia me 60°"'t/
Pauric McGroary
Report Number : 19-308-0006
REPORT OFANAL YSIS
Agronomist
Lab No : 69508
Matrix: Solids
Sample ID : 1 of 6
Sampled: 11/2/2019 10:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
796
mg/Kg - dry
599
1
11/11/19 14:30
JPJ SM-4500-NH3C
Aluminum
166000
mg/Kg - dry
299
10
11/08/19 10:52
BKN 6010D
Arsenic
13.4
mg/Kg - dry
2.99
1
11/07/19 04:55
BKN 6010D
Cadmium
<0.599
mg/Kg - dry
0.599
1
11/07/19 04:55
BKN 6010D
Chromium
138
mg/Kg - dry
1.50
1
11/07/19 04:55
BKN 6010D
Lead
13.0
mg/Kg - dry
1.80
1
11/07/19 04:55
BKN 6010D
Molybdenum
2.80
mg/Kg - dry
1.50
1
11/07/19 04:55
BKN 6010D
Sodium Absorption Ratio
0.74
1
CALCULATION
Sodium
354
mg/Kg - dry
150
1
11/07/19 04:55
BKN 6010D
Zinc
160
mg/Kg - dry
7.49
1
11/07/19 04:55
BKN 6010D
Qualifiers/ B Analyte detected in blank
Definitions
H Beyond holding time
Paste 5 of 7

WayPAaInts
..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 19-308-0006
Shipping Method
Fed Ex US Postal Lab
UPS Client Courier
Other : r
Thermometer ID:
�—
Shipping container/cooler uncompromised?
0 Yes
No
Number of coolers received
r 1
Custody seals intact on shipping container/cooler?
Yes
No
Not Required
Custody seals intact on sample bottles?
Yes
No
Not Required
Chain of Custody (COC) present?
Yes
No
COC agrees with sample label(s)?
• Yes
No
COC properly completed
Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
• No
Water - Sample containers properly preserved
Yes
No
N/A
Water - VOA vials free of headspace
Yes
No
N/A
Trip Blanks received with VOAs
Soil VOA method 5035 — compliance criteria met
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Special precautions or instructions included?
Comments: I
Yes No N/A
Yes No N/A
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Yes No
Signature: Brandi Watson Date & Time: 11/04/2019 14:32:25
Pane 6 of 7

NfttSAMPLE TRA
7621 W'hitepine Road Richmond VA 23237
�rrrrrrrrrrrr072
Denali water
Lake Kiibv WTP 2019 t of 6
►DY
. jalesswtlxom
Account #
Submitted By Charge To
Copy To
Jeff Retzke/Denali Water PC: DEW
jeff.retzkeadenaliwater.com
35 Refreshment Place
Jeff's Cell: 256.503.4300
Decatur, AL 35601
Project Lake Kilby WTP 2019 la&2a of 6
Sample Information
Lab Number
Collection Information
Container Information
Please Check Desired Tests
Type
Date
Time
Number
Type
Volume
SL1
SL2
503
Nitrogen
pH
CCE
Ag
Cl
Volatile
Others
Sample ID
(Lab Use
Only)
of Bottles
Metals
Series
Solids
Grab
_ oz
Standard Compoa.
13
81
1E
1
_Glass
Plastic
X int
—qt
rr/A:uminum, CCE
C Its
Otnp08
Q
and S.A.R.
2a
x Grab
—
Q
1
_ Glass
x Plastic
x oz
—p
Same as above
composite
('.S'��
'
at
Grab
Glass
Qz
Plastic
t
---nt
Com site
—
at
_ Grab
Guns
_ oz
_
Plastic
—pint
nature
Date
Time
ReceWed BY: re
Date
Time
Test Package De its
Special Instructions or Remarks
Lf: Total Solids (Moisture) Total K)cidahl Nitrogen, Phosphorus and Potassium
M, Basic Test SLI plus Sulfur, Calcium. Magrmum,Sodium, Iron, Aluminum, Manganese, Copper And Zinc
503 Yaws: Arsenic. Cadmium. Chromium, Mercury. Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc Included In SL2)
Nitrogen Series: Total Kieidahl, Ammonium. Nitrate & Organic Nitrogen
CCE; Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
Dana 7 of 7

Waypointo
ANALYTICAL
11 /25/2019
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 19-318-0004
Project Description: Lake Kilby WTP 2019 2b of 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/14/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Paqe 1 of 7

Waypoint(l)
aff ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-318-0004
Client Project Description: Lake Kilby WTP 2019 2b of 6
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
69591
2b
Solids
11/13/2019 15:00
11/14/2019
69591
2b
Solids
11/13/2019 15:00
11/14/2019
SM-2540G
WTN
69591
2b
Solids
11/13/2019 15:00
11/14/2019
SW-7471B
WTN
69591
2b
Solids
11/13/2019 15:00
11/14/2019
SM-4500-NH3C-TKN
WTN
69591
2b
Solids
11/13/2019 15:00
11/14/2019
4500NO3F-2011
WTN
69591
2b
Solids
11/13/2019 15:00
11/14/2019
6010D
WTN
69591
2b
Solids
11/13/2019 15:00
11/14/2019
SM-4500-NH3C
WTN
69591
2b
Solids
11/13/2019 15:00
11/14/2019
9045D
WTN
69591
2b
Solids
11/13/2019 15:00
11/14/2019
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN
Paae 2 of 7

a
Waypoint
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° fax [phone]
ANALYTICAL www.waypointanalyticall.com
07274
Denali Water Jeff Retzke
Jeff Retzke Project Lake Kilby WTP 2019 2b of 6 Report Date : 11/25/2019
1001 Fraser Ave Information : Received : 11/14/2019
Huntsville , AL 35801
Submitted By : Jeff Retzke
Report Number : 19-318-0004
REPORT OFANALYSIS
Pauric McGroary
Agronomist
Lab No : 69591
Matrix: Solids
Sample ID : 2b
Sampled:
11/13/2019
15:00
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
847
mg/Kg - dry
568
1
11/21/19 13:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<27.8
mg/Kg - dry
27.8
1
11/20/19 14:31
ZBD
4500NO3F-2011
Organic N
14600
mg/Kg - dry
1420
1
11/21/19 10:00
DH
CALCULATION
pH
6.9
S.U.
1
11/19/19 05:49
JSL
9045D
Total Solids
17.6
%
0.010
1
11/19/19 16:08
ADM
SM-2540G
Total Volatile Solids
48.3
%
0.010
1
11/19/19 16:08
ADM
SM-254OG
Total Kjeldahl Nitrogen
15500
mg/Kg - dry
1420
1
11/21/19 10:00
JPJ >M-4500-NH3C-TKP
Phosphorus
1130
mg/Kg - dry
28.4
1
11/19/19 17:47
BKN
6010D
Arsenic
10.6
mg/Kg - dry
2.84
1
11/19/19 17:47
BKN
6010D
Calcium
1890
mg/Kg - dry
142
1
11/19/19 17:47
BKN
6010D
Cadmium
<0.568
mg/Kg - dry
0.568
1
11/19/19 17:47
BKN
6010D
Chromium
107
mg/Kg - dry
1.42
1
11/19/19 17:47
BKN
6010D
Copper
52.6
mg/Kg - dry
1.42
1
11/19/19 17:47
BKN
6010D
Iron
20500
mg/Kg - dry
28.4
1
11/19/19 17:47
KKM
6010D
Lead
5.74
mg/Kg - dry
1.70
1
11/19/19 17:47
BKN
6010D
Magnesium
585
mg/Kg - dry
28.4
1
11/19/19 17:47
BKN
6010D
Manganese
4770
mg/Kg - dry
14.2
5
11/20/19 15:18
KKM
6010D
Mercury
<0.0857
mg/Kg - dry
0.0857
1
11/20/19 13:54
TJS
SW-7471B
Molybdenum
2.01
mg/Kg - dry
1.42
1
11/19/19 17:47
BKN
6010D
Nickel
14.1
mg/Kg - dry
1.42
1
11/19/19 17:47
BKN
6010D
Potassium
161
mg/Kg - dry
28.4
1
11/19/19 17:47
BKN
6010D
Selenium
<2.84
mg/Kg - dry
2.84
1
11/19/19 17:47
BKN
6010D
Sodium
311
mg/Kg - dry
142
1
11/19/19 17:47
BKN
6010D
Qualifiers/ OF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Paqe 3 of 7

(2)
•
Waypoint,
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
07274
Denali Water
Jeff Retzke
Jeff Retzke
Project
Lake Kilby WTP 2019 2b of 6 Report Date : 11/25/2019
1001 Fraser Ave
Information : Received : 11/14/2019
Huntsville , AL 35801
Submitted By : Jeff Retzke
Report Number :19-318-0004
REPORT OFANALYSlS Pauric McGroary
Agronomist
Lab No : 69591
Matrix: Solids
Sample ID: 2b
Sampled: 11/13/2019 15:00
Test
Results
Units MQL DF Date / Time By Analytical
Analyzed Method
Zinc
131
mg/Kg - dry 7.10 1 11/22/19 15:35 BKN 6010D
Sulfur
12300
mg/Kg - dry 28.4 1 11/19/19 17:47 BKN 6010D
Sodium Absorption Ratio
0.67
1 CALCULATION
Moisture
82.4
0.010 1 11/19/1916:08 ADM SM-2540G
Calcium Carbonate Equivalent
5.3
% - dry 0.1 1 11/19/19 14:20 DXT AOAC 955.01
Qualifiers/ B Analyte detected in blank
Definitions
H Beyond holding time
Paae 4 of 7

Waypoient(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Client: Denali Water CASE NARRATIVE
Project: Lake Kilby WTP 2019 2b of 6
Lab Report Number: 19-318-0004
Date: 11/25/2019
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 69591 (2b)
QC Batch No: 1-465257/1-465039
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Pa4e 5 of 7

Waypoint(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]"6
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 19-318-0004
Shipping Method
Fed Ex US Postal Lab
0 UPS Client Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
No
Number of coolers received
F1
Custody seals intact on shipping container/cooler?
Yes
No
Not Required
Custody seals intact on sample bottles?
Yes
No
• Not Required
Chain of Custody (COC) present?
* Yes
No
COC agrees with sample label(s)?
Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
• Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
No
Water - Sample containers properly preserved
Yes
No
N/A
Water - VOA vials free of headspace
Yes
No
N/A
Trip Blanks received with VOAs
Yes
No
I* N/A
Soil VOA method 5035 — compliance criteria) met
Yes
No
I* N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
-------------
Comments:
Yes
No
Signature Brandi Watson Date & Time: `11/14/2019 12.29:40
Paae 6 of 7

SAMPLE TRAM 191 800D4 Account #
D � -3-
0274
Denali Water 117-14-2019
12:2823
7621 Whitepine Road Richmond VA 23237 - I Lake Kilbv WTP 2019 2b of 6 leastem corn
C
Submitted By
Charge To
Copy To
Jeff Retzke/Denali Water PO: DEW
jeff.retzkeedenaliwater.com
35 Refreshment Place
Jeff's Cell: 256.503.4300
Decatur, AL 35601
Project Lake Kilby WTP 2019 2b of
Sample Information
Lab Number
Collection Information
Container Information
Please Check Desired Tests
Sample 10
(Lab Use
Only)
Type
Date
Time
Number
Type
Volume
SLI
SL2
503
Nitrogen
pH
CCE
Ag
Cl
V01111111111
Others
Of Bottles
Mallets
Sod"
sows
_ Carat)
Glass
st
Standard Compost
2b
/I -
'�5 *
x Plastic
wjAlluminum. CCR
—qt
and S A. R.
Grab
Glass
of
Plastic
---pomposite ,t
C
j.1
t
Grab
Glass
oz
Commisite
Plastic
at
— Grab
Glass
oat?
lCoMtle I
plastic
— pint
I I
I
R##nQvQpdByASlgnature)
Date
Time
Received BY: Ls&!L"J
Data
Time
Z14 -Vol'
ji-is -j?
lot
Test Package Details
gp2qW I2jMgg§n or Romeft
SLI: ToW Solids (Moisture) Total Kjoldalit Nitrogen. Phosphorus and Potassium
SLI: Basic Tea SL I plus Sulfur, Calcium. Magrwsium,Sodium, from Aluminum. Manganese. CopM And Zinc
$03 Motels: Arsenic, Cadmium, Chromium, Mercury, MoMxllenum, Lead, Nickel, Selenium.
(Copper & Zinc Included in SII)
Nitrogen Series: Total Kleldahl, Ammonium, Nitrate & Organic Nitrogen.
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
D- '7 of 7