WQ0012980_Residual Annual Report 2019_20200204

For Better Results. -., . w _.. ,, _. :, .
Milorganite r r
January 30, 2020
Information Processing Unit
Division of Water Quality
Department of Environment and Natural Resources
1617 Mail Service Center
Raleigh, North Carolina 27699 - 1617
Subject: Milorganite® Fertilizer Annual Report
Good day:
RFr;=1N/1=_D
FED? 0 4 2020
DWR SECTION
111,1TORMATION PROCESSING UNIT
To demonstrate the quality of the Milorganite° fertilizer sold in North Carolina during 2019, a report is enclosed. The
report shows that Milorganite° fertilizer continues to be an exceptional quality biosolids product, according to the
applicable regulations (40 CFR 503 and 15A NCAC 2T.1106 and 2T.1107). The report includes the following sample
results.
Parameter
Frequency
As, Cd, Cu, Fe, Pb, Mo, Ni, P, K, Se, Zn
Daily
Al, B, Cr
Monthly
Hg
Weekly
Fecal Coliform
Weekly
PCB Aroclors
Daily
Toxic Equivalents: Dioxins, Furans, and PCBs
Monthly
Priority Pollutants
Semi-annually
Moisture
Daily
The Residual Report Form, a report showing distributors and sales, and a report showing an example of product
temperatures at the dryer exit are enclosed.
The North Carolina Department of Agriculture continues to register Milorganite° fertilizer.
If you have questions, please contact me at 414-225-2243 or [e-mail]. If you have no interest in continuing
to receive this report, then please notify me. Thanks for your cooperation.
Sincerely yours,
Thomas A. Nowicki
Staff Attorney
Enclosures
Milorganite - MMSD 260 W. Seeboth Street Milwaukee, WI 53204 1 �,..'
Phone: [phone] [phone] Fax: [phone] "'
[e-mail] www.milorganite.com Sustaainininin
g Turfgrass Research
gs�wM
�� 9MFMG
CCSPP

For Better Results.
Naturally.
Milorganite
Milorganite° Fertilizer
North Carolina Exceptional Quality Biosolids Certification
Permit for Distribution of Class A Residuals WQ0012980
We, Steven J. Unger, Contract Compliance Administrator, Milwaukee Metropolitan Sewerage District, and
Brett Kelly, Operations Manager, Veolia Water Milwaukee LLC, certify we have personally examined and are
familiar with the submitted information. Based upon our inquiry of those individuals immediately responsible
collecting the information, we believe the information is true, accurate, and complete.
We certify Milorganite® fertilizer:
(1) complied with the limits of 40 CFR § 503.13(b)(3);
(2) was dried to achieve a pellet temperature exceeding 176°F/80°C and no more than 10% moisture, as
required for Class A pathogen destruction, according to 40 CFR § 503.32, Appendix B, B.2, and 15A NCAC
2T.1106(b)(3)(F); and
(3) was dried to achieve greater than 75% solids, as required for vector attraction reduction, according to
40 CFR § 503.33(b)(7) and 15A NCAC 2T.1107(a)(7).
We made this determination based upon an environmental management system in which qualified personnel
properly gather and evaluate information regarding pollutant concentrations, pathogen reduction, and vector
attraction reduction. We are aware of the significant penalties for submitting false information, including the
possibility of fine and imprisonment.
Certified January 1+, 2020:
Steven J. Unger, C ntract Compliance Administrator
Certified January /0 , 2020
Brett Kelly, Operations Manager
Milorganite - MMSD 260 W. Seeboth Street Milwaukee, WI 53204
Phone: [phone] [phone] Fax: [phone] s
[e-mail] www.milorganite.com SustainingTurfgrarsRerearrh tcuNuwnoN
a

North Carolina Department of Environment and Natural Resources
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ 00 12980 No Discharge
Facility Name: Milwaukee Metro Sewerage District
Residual Source WQ # or NPDES
WWTP Name:
Residual Analysis Data
WPDES WI 0036820
Jones Island
Laboratory: 1) Milwaukee Metro Sewerage District
2)
3)
4)
5)
aramet)
Parameter
Limit
m
Sample or Composite Date (monthly average)
January
February
March
April
May
June
July
August
September
October
November
December
Percent Solids (%)
NA
92
94
94
94
95
94
93
93
94
94
93
92
Arsenic
41
<6.3
<6.2
<6.2
<6.2
<3.0
<3.0
<17
<17
<16
<16
<17
<17
Cadmium
39
0.49
0.43
0.54
0.48
<0.9
<0.91
<0.91
<0.91
<0.89
<0.90
<0.92
<0.92
Chromium
NA
180
230
230
180
190
150
150
320
210
170
180
190
Copper
1,500
220
220
220
210
210
200
220
220
240
220
230
220
Lead
300
28
28
31
27
37
35
35
34
42
46
37
31
Mercury
17
0.17
0.13
0.045
0.090
0.11
0.081
0.15
0.12
0.19
0.12
0.25
0.28
Molybdenum
75
9.9
9.7
10.0
9.4
9.4
8.8
8.6
9.6
9.8
8.9
9.4
9.2
Nickel
420
27
26
27
27
27
24
23
23
23
22
27
23
Selenium
100
<6.7
<6.6
<6.7
<6.5
5.0
5.1
<4.1
<4.1
<4.0
<4.0
<4.1
4.1
Zinc
2,800
420
430
460
380
410
380
420
440
460
400
440
430
Total Phosphorus
NA
24,000
24,000
24,000
24,000
24,000
22,000
23,000
25,000
24,000
23,000
24,000
24,000
Total Nitrogen(%)
NA
6.4
6.2
6.4
6.9
6.5
6.2
5.9
6.1
5.8
6.0
5.8
6.1
Ammonia -Nitrogen(%)
NA
0.20
0.22
0.14
0.17
0.14
0.15
0.13
0.13
0.11
0.15
0.20
0.18
Nitrate Nitrogen(%)
NA
0.85
0.72
<0.5
0.80
0.78
0.96
1.5
1.3
0.71
0.93
0.95
1.0
Sampling frequency: Arsenic, cadmium, copper, lead, molybdenum, nickel, selenium, and zinc are daily; Mercury is weekly; Ammonia, chromium, nitrate, and nitrogen are monthly
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting
false information, including .the possibility of fines and imprisonment for knowing violations.
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
7 aov
(9!L ate

NC
Buncombe
NC Bunc # 03/12/19 INV20714 50PRO 50#
ombe 5 MILORGANITE
Buncombe.....,....._ .... ..,.
Edgecombe
NC Edge 03/26/19 INV20728 32PD 32# Bags
comb 0
Henderson
Watauga
Edgecombe
1 SITEONELAND SITEONE SITEONE ARDEN
SCAP LANDSCA LANDSCAPE
1.00
21.17 BWI BWI ALLEN'S ROCKY
Companie NURSERY MOUNT
21.17
NC
Hend
02/14/19INV20701 50PRO
50# 21 SOUTHERNAG
Southern Southern
HENDERSON
erson
1
MILORGANITE '
INS
Agricultural Agricultural
VILLE
NC
Hend
01/21/19 INV20688 50PRO
50#
21 SOUTHERNAG
Southern Southern
HENDERSON
erson
4
MILORGANITE
INS
Agricultural Agricultural
_ VILLE
NC
Hend
09/13/19 INV20844 50PRO
50#
21 SOUTHERNAG
Southern Southern
HENDERSON
erson
15
MILORGANITE
INS
Agricultural Agricultural
VILLE
NC
Hend
09/13/4-INV20843 50PRO
50#
21 SOUTHERNAG
Southern Southern
HENDERSON
erson
5
MILORGANITE `
INS
Agricultural Agricultural
VILLE
Henderson
84.00
NC
Wata `'
09/20/19 INV20849 50PRO
50#
21 SOUTHERNAG
Southern Southern
BOONE
uga
1
MILORGANITE
INS
Agricultural Agricultural
NC
Wata
09/16/19 INV20845 50PRO
50#
21 SOUTHERNAG
Southern Southern
BOONE
uga
0
MILORGANITE
INS
Agricultural Agricultural
_ »»%
NC
Wata
02/27/19 INV20705 50PRO
50#
21 SOUTHERNAG
Southern Southern
BOONE
uga
1
MILORGANITE ',
INS
Agricultural Agricultural
NC
Wata
04/10/19INV20741 50PRO
50#
21 SOUTHERNAG
Southern Southern
BOONE
uga
6
MILORGANITE
INS
Agricultural Agricultural
NC
Wata
06/12/19 INV20790 50PRO
50#
21 SOUTHERNAG
Southern Southern
BOONE
uga
2
MILORGANITE
INS
Agricultural Agricultural
NC
Wata
06/11/19 INV20788 50PRO
50#
21 SOUTHERNAG
Southern Southern
BOONE
uga
9
MILORGANITE
INS
Agricultural Agricultural
Watauga Total:
126.00
NC Total:
T
232.17;
�Vv4
1
Page 1 of 1 MKT600

Graph #1- Dryer Discharge Product Temperatures - South Dryers
O Dryer #1 O Dryer #2 a Dryer #3 o Dryer #4 O Dryer #5 O Dryer #6
275
50 -
25
0 -
rn M M a1 M 0 0+ 0 a+ rn m M a+ a1 Cl a, a M rn o+ a1 01 rn a) m m ON (n Ch a, m
.-1 N
N fn O to tD n
•-1 .-1 •-1 PI rl N N N N N N N N N N N N M M
Ln Ln Ln 1A Ln Ln Ln Ln VI VI 91 t`A 1`n Ln 1 f u`l in Ln Ln Ln LA L u\1 Ln Ln Ln t 1 l! U c` In

Graph #2 - Dryer Discharge Product Temperatures - North Dryers
300
275
250
225
200
100
75
so
25
0
o Dryer #7 c Dryer #8 L Dryer u9 o Dryer q10 Q Dryer Mil O Dryer #12
T 01 01 0) 01 C) 01 M 01 01 01 01 01 M O1 MM M O1 � 61 rn O\ 01 On Q% 01 (M O1 M 01
N � ', 1-4 � ti H , ., �
\i N m v v\i wO n Goo a% o N m c Ln rl 0000 m o N m v Ln 110 n 000 m
\ \ \ \ \ \ �. N N N N N N N N N N fn m
V1 V1 V1 V1 LA VI Ln Vf V1 \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ ^� \ \ \
Ln%n V1 Ln VI LnVl V1 LA InV1 V) V1 Vl V1 V1 V1 V1 Vi LnV7 Ul

tINNSD
PARTNERS FOR A CLEANER ENVIRONMENT
March 29, 2019
TO: Tom Nowicki
FROM: Zach Vogel
iI : 11 ' • !t
COPY: A. Sotomayor, S. Mertens, S. Unger, J. Spence, Lab File
SUBJECT: Milorganite TCLP Analyses to Meet Special State Requirements of North Carolina
Attached is the analytical report for the Milorganite sample collected in 2019 to meet the special
requirements of North Carolina. The sample analyses were performed by Pace Analytical Services, Inc. in
Green Bay, Wisconsin and Pace Analytical in Mt. Juliet, Tennessee.
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data/Report Review By:
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI S3204

aceAnalytical
www.pacelabs.com
Pace Analytical Services, L6C
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
March 27, 2019
Sharon Mertens
Milwaukee Metropolitan Sewerage
250 W. Seeboth Street
P.O. Box 3049
Milwaukee, WI 532041446
RE: Project: PACMIPP_19107
Pace Project No.: 40184019
Dear Sharon Mertens:
Enclosed are the analytical results for sample(s) received by the laboratory on March 11, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brian Basten
[e-mail]
[phone]
Project Manager
Enclosures
cc: Jessica Nanes, MMSD
Alfredo Sotomayor, MMSD
Zach Vogel, Milwaukee Metropolitan Sewerage District
Kim Walden, MMSD
A
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
6
Page 1 of 45

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
CERTIFICATIONS
Project: PACMIPP_19107
Pace Project No.: 40184019
Green Bay Certification IDs
1241 Bellevue Street, Green Bay, WI 54302
Virginia VELAP ID: 460263
Florida/NELAP Certification #: E87948
South Carolina Certification #: 83006001
Illinois Certification #: 200050
Texas Certification #: T104704529-14-1
Kentucky UST Certification #: 82
Wisconsin Certification #: 405132750
Louisiana Certification #: 04168
Wisconsin DATCP Certification #: 105-444
Minnesota Certification #: 055-999-334
USDA Soil Permit #: P330-16-00157
New York Certification #: 12064
Federal Fish & Wildlife Permit #: LE51774A-0
North Dakota Certification #: R-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 45

WCeAnalytical
www.pacelabs.com
Pace Analytical Services, LL.0
1241 Bellevue Street - Suite 9
Green Bay, WI 54302 ,
[phone]
SAMPLE SUMMARY
Project: PACMIPP_19107
Pace Project No.: 40184019
Lab ID Sample ID Matrix Date Collected Date Received
40184019001 19002892/964 Solid 03/09/19 05:00 03/11/19 15:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 45

4aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
SAMPLE ANALYTE COUNT
Project: PACMIPP_19107
Pace Project No.: 40184019
Lab ID Sample ID Method
Analysts
Analytes
Reported
40184019001 19002892/964 EPA 8081
DMH
9
EPA 6010
TXW
7
EPA 7470
AJT
1
EPA 8270
RJN
17
EPA 8260
LAP
13
ASTM D2974-87
PCG
1
EPA 9045
ALY
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 45

laceAnalXical-
www.pacelabs.com
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
PROJECT NARRATIVE
Project: PACMIPP_19107
Pace Project No.: 40184019
Method: EPA 8081
Description: 8081 GCS Pesticides, TCLP
Client: MILWAUKEE METROPOLITAN SEWERAGE DISTRICT
Date: March 27. 2019
General Information:
1 sample was analyzed for EPA 8081. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3510 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: 315787
CH: The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased high.
• 19002892/964 (Lab ID: 40184019001)
• Chlordane (Technical)
• Endrin
•Toxaphene
• BLANK (Lab ID: 1836921)
• Chlordane (Technical)
• Endrin
•Toxaphene
• LB (Lab ID: 1834551)
• Chlordane (Technical)
• Endrin
•Toxaphene
• LCS (Lab ID: 1836922)
• Chlordane (Technical)
• Endrin
•Toxaphene
• MS (Lab ID: 1836923)
• Chlordane (Technical)
• Endrin
•Toxaphene
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 45

aceAnalytical
i
wwwpaceiabs.com
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
PROJECT NARRATIVE
Project: PACMIPP_19107
Pace Project No.: 40184019
Method: EPA 8081
Description: 8081 GCS Pesticides, TCLP
Client: MILWAUKEE METROPOLITAN SEWERAGE DISTRICT
Date: March 27, 2019
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 45

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LUC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
PROJECT NARRATIVE
Project: PACMIPP_19107
Pace Project No.: 40184019
Method: EPA 6010
Description: 6010 MET ICP, TCLP
Client: MILWAUKEE METROPOLITAN SEWERAGE DISTRICT
Date: March 27, 2019
General Information:
1 sample was analyzed for EPA 6010. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3010 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: 315523
1 q: Analyte was detected in the associated leach blank at a concentration of 0.042 mg/L.
• 19002892/964 (Lab ID: 40184019001)
• Arsenic
2q: Analyte was detected in the associated method blank at a concentration of 0.012 mg/L.
•19002892/964 (Lab ID:40184019001)
• Arsenic
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 45

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
PROJECT NARRATIVE
Project: PACMIPP_19107
Pace Project No.: 40184019
Method: EPA 7470
Description: 7470 Mercury, TCLP
Client: MILWAUKEE METROPOLITAN SEWERAGE DISTRICT
Date: March 27, 2019
General Information:
1 sample was analyzed for EPA 7470. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 7470 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 45

acmnalytical
www-pacelabs.com
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
PROJECT NARRATIVE
Project: PACMIPP_19107
Pace Project No.: 40184019
Method: EPA 8270
Description: 8270 MSSV TCLP Sep Funnel
Client: MILWAUKEE METROPOLITAN SEWERAGE DISTRICT
Date: March 27. 2019
General Information:
1 sample was analyzed for EPA 8270. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3510 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 45

aceAnalXical
www.pacelabs.com
PROJECT NARRATIVE
Project: PACMIPP_19107
Pace Project No.: 40184019
Method: EPA 8260
Description: 8260 MSV TCLP
Client: MILWAUKEE METROPOLITAN SEWERAGE DISTRICT
Date: March 27, 2019
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, N 54302
[phone]
General Information:
1 sample was analyzed for EPA 8260. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 45

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LUC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
PROJECT NARRATIVE
Project: PACMIPP 19107
Pace Project No.: 40184019
Method: EPA 9045
Description: 9045 pH Soil
Client: MILWAUKEE METROPOLITAN SEWERAGE DISTRICT
Date: March 27. 2019
General Information:
1 sample was analyzed for EPA 9045. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H6: Analysis initiated outside of the 15 minute EPA required holding time.
• 19002892/964 (Lab ID: 40184019001)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 11 of 45

(���a'ceAnalyficalo
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
Project: PACMIPP_19107
Pace Project No.: 40184019
Sample: 19002892/964 Lab ID: 40184019001 Collected: 03/09/19 05:00 Received: 03/11/19 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Phenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
2,4,6-Tribromophenol (S)
Date: 03/27/2019 08:00 AM
Results Units LOQ LOD DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 03/13/19 12:58
<0.13
ug/L
0.42
0.13
1
03/19/19 07:30
03/21/19 01:43
58-89-9
<4.4
ug/L
14.5
4.4
1
03/19/19 07:30
03/21/19 01:43
57-74-9
<0.31
ug/L
1.0
0.31
1
03/19/19 07:30
03/21/19 01:43
72-20-8
<0.13
ug/L
0.44
0.13
1
03/19/19 07:30
03/21/19 01:43
76-44-8
<0.26
ug/L
0.87
0.26
1
03/19/19 07:30
03/21/19 01:43
1024-57-3
<1.6
ug/L
5.4
1.6
1
03/19/19 07:30
03/21/19 01:43
72-43-5
<30.0
ug/L
60.0
30.0
1
03/19/19 07:30
03/21/19 01:43
8001-35-2
51
%
10-108
1
03/19/19 07:30
03/21/19 01:43
2051-24-3
90
%
45-112
1
03/19/19 07:30
03/21/19 01:43
877-09-8
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 03/13/19 12:58
0.11J
mg/L
0.12
0.042
1
03/14/1914:24
03/15/1911:30
7440-38-2
0.47
mg/L
0.075
0.025
1
03/14/1914:24
03/15/1911:30
7440-39-3
<0.0066
mg/L
0.025
0.0066
1
03/14/1914:24
03/15/1911:30
7440-43-9
0.10
mg/L
0.050
0.013
1
03/14/1914:24
03/15/1911:30
7440-47-3
<0.030
mg/L
0.098
0.030
1
03/14/1914:24
03/15/1911:30
7439-92-1
<0.061
mg/L
0.25
0.061
1
03/14/1914:24
03/15/1911:30
7782-49-2
<0.017
mg/L
0.050
0.017
1
03/14/1914:24
03/15/1911:30
7440-22-4
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 03/13119 12:58
1.3 ug/L 0.56 0.17 1 03/20/19 13:15 03/21/19 09:14 7439-97-6
CH
CH
141"1
19,29
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date:
EPA 1311; 03/13/19
12:58
<37.5
ug/L
125
37.5
1 03/14/19 08:08
03/14/19 19:34
106-46-7
<15.8
ug/L
52.8
15.8
1 03/14/19 08:08
03/14/19 19:34
121-14-2
<49.2
ug/L
164
49.2
1 03/14/19 08:08
03/14/19 19:34
87-68-3
<33.9
ug/L
113
33.9
1 03/14/19 08:08
03/14/19 19:34
118-74-1
<53.2
ug/L
177
53.2
1 03/14/19 08:08
03/14/19 19:34
67-72-1
<17.4
ug/L
57.8
17.4
1 03/14/19 08:08
03/14/19 19:34
95-48-7
<31.2
ug/L
104
31.2
1 03/14/19 08:08
03/14/19 19:34
<29.0
ug/L
96.6
29.0
1 03/14/19 08:08
03/14/19 19:34
98-95-3
<28.7
ug/L
95.6
28.7
1 03/14/19 08:08
03/14/19 19:34
87-86-5
<12.0
ug/L
40.0
12.0
1 03/14/19 08:08
03/14/19 19:34
108-95-2
<35.8
ug/L
119
35.8
1 03/14/19 08:08
03/14/19 19:34
110-86-1
<16.8
ug/L
56.0
16.8
1 03/14/19 08:08
03/14/19 19:34
95-95-4
<42.3
ug/L
141
42.3
1 03/14/19 08:08
03/14/19 19:34
88-06-2
86
%
51-108
1 03/14/19 08:08
03/14/19 19:34
4165-60-0
83
%
47-105
1 03/14/19 08:08
03/14/19 19:34
321-60-8
124
%
57-131
1 03/14/19 08:08
03/14/19 19:34
118-79-6
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written
consent of Pace Analytical Services,
LLC.
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ANALYTICAL RESULTS
Project: PACMIPP_19107
Pace Project No.: 40184019
Pace Analytical Services, LL-C
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
Sample: 19002892/964 Lab ID: 40184019001 Collected: 03/09/19 05:00 Received: 03/11/19 15:00 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units LOQ LOD DF Prepared Analyzed CAS No. Qual
8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 03/13/19 12:58
Surrogates
Phenol-d6 (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Date: 03/27/2019 08:00 AM
34
%
18-120
1
03/14/19 08:08 03/14/19 19:34
13127-88-3
Analytical
Method: EPA
8260 Leachate
Method/Date: EPA 1311; 03/18/19 12:24
<5.0
ug/L
10.0
5.0
10
03/19/1910:37
71-43-2
146J
ug/L
200
29.8
10
03/19/1910:37
78-93-3
<5.0
ug/L
10.0
5.0
10
03/19/1910:37
56-23-5
<5.0
ug/L
10.0
5.0
10
03/19/1910:37
108-90-7
<25.0
ug/L
50.0
25.0
10
03/19/1910:37
67-66-3
<1.7
ug/L
10.0
1.7
10
03/19/1910:37
107-06-2
<4.1
ug/L
10.0
4.1
10
03/19/1910:37
75-35-4
<5.0
ug/L
10.0
5.0
10
03/19/1910:37
127-18-4
<3.3
ug/L
10.0
3.3
10
03/19/1910:37
79-01-6
<1.8
ug/L
10.0
1.8
10
03/19/1910:37
75-01-4
103
%
70-130
10
03/19/1910:37
2037-26-5
89
%
70-130
10
03/19/1910:37
460-00-4
93
%
70-130
10
03/19/1910:37
1868-53-7
Analytical
Method: ASTM D2974-87
5.4
%
0.10
0.10
1
03/12/1916:52
Analytical
Method: EPA 9045
6.24
Std. Units
0.100
0.0100
1
03/13/19 09:47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H6
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Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
QC Batch: 315965 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 40184019001
METHOD BLANK: 1837730 Matrix: Water
Associated Lab Samples: 40184019001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L <0.084 0.28 03/21/19 08:53
METHOD BLANK: 1834549
Matrix:
Water
Associated Lab Samples: 40184019001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
ug/L
<0.084
0.28
03/21/19 09:11
METHOD BLANK: 1837176
Matrix:
Water
Associated Lab Samples: 40184019001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
ug/L
<0.084
0.28
03/21/19 09:04
LABORATORY CONTROL SAMPLE: 1837731
Spike
LCS
LCS
% Rec
Parameter Units
Conc.
Result
% Rec
Limits Qualifiers
Mercury ug/L
5
4.6
92
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1837732
1837733
MS
MSD
40184156001
Spike
Spike MS
MSD
MS MSD % Rec Max
Parameter Units Result
Conc.
Conc. Result
Result
% Rec % Rec Limits RPD RPD Qual
Mercury ug/L <0.000084
5
5 5.7
5.7
115 115 85-115 0 20
mg/L
MATRIX SPIKE SAMPLE: 1837734
40184145001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Mercury ug/L <0.084 5 5.7 114 85-115
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 45

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Pace Analytical Services, LUC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
QC Batch: 315523 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 40184019001
METHOD BLANK: 1835473
Matrix:
Water
Associated Lab Samples: 40184019001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Arsenic
mg/L
0.012J
0.025
03/15/1911:15
Barium
mg/L
<0.0050
0.015
03/15/1911:15
Cadmium
mg/L
<0.0013
0.0050
03/15/1911:15
Chromium
mg/L
<0.0025
0.010
03/15/1911:15
Lead
mg/L
0.0066.1
0.020
03/15/1911:15
Selenium
mg/L
<0.012
0.050
03/15/1911:15
Silver
mg/L
<0.0033
0.010
03/15/1911:15
METHOD BLANK: 1834545
Matrix:
Solid
Associated Lab Samples: 40184019001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Arsenic
mg/L
<0.042
0.12
03/15/1911:27
Barium
mg/L
<0.025
0.075
03/15/1911:27
Cadmium
mg/L
<0.0066
0.025
03/15/1911:27
Chromium
mg/L
<0.013
0.050
03/15/1911:27
Lead
mg/L
<0.030
0.098
03/15/1911:27
Selenium
mg/L
<0.061
0.25
03/15/1911:27
Silver
mg/L
<0.017
0.050
03/15/1911:27
METHOD BLANK: 1834546
Matrix:
Solid
Associated Lab Samples: 40184019001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Arsenic
mg/L
<0.0083
0.025
03/15/1911:45
Barium
mg/L
<0.0050
0.015
03/15/1911:45
Cadmium
mg/L
<0.0013
0.0050
03/15/1911:45
Chromium
mg/L
<0.0025
0.010
03/15/1911:45
Lead
mg/L
<0.0059
0.020
03/15/1911:45
Selenium
mg/L
0.018J
0.050
03/15/1911:45
Silver
mg/L
<0.0033
0.010
03/15/1911:45
Qualifiers
Qualifiers
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
METHOD BLANK: 1834547
Matrix:
Solid
Associated Lab Samples: 40184019001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Arsenic
mg/L
0.042J
0.12
03/15/1911:32
Barium
mg/L
<0.025
0.075
03/15/1911:32
Cadmium
mg/L
<0.0066
0.025
03/15/1911:32
Chromium
mg/L
<0.013
0.050
03/15/1911:32
Lead
mg/L
<0.030
0.098
03/15/1911:32
Selenium
mg/L
0.070J
0.25
03/15/1911:32
Silver
mg/L
<0.017
0.050
03/15/1911:32
METHOD BLANK: 1834577
Matrix:
Solid
Associated Lab Samples: 40184019001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Arsenic
mg/L
0.021J
0.025
03/15/1911:50
Barium
mg/L
<0.0050
0.015
03/15/1911:50
Cadmium
mg/L
<0.0013
0.0050
03/15/1911:50
Chromium
mg/L
<0.0025
0.010
03/15/1911:50
Lead
mg/L
<0.0059
0.020
03/15/1911:50
Selenium
mg/L
<0.012
0.050
03/15/1911:50
Silver
mg/L
<0.0033
0.010
03/15/1911:50
LABORATORY CONTROL SAMPLE:
1835474
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Qualifiers
Qualifiers
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
0.5
0.47
95
80-120
0.5
0.49
99
80-120
0.5
0.50
100
80-120
0.5
0.50
100
80-120
0.5
0.49
99
80-120
0.5
0.52
103
80-120
0.25
0.25
99
80-120
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1835475
1835476
MS
MSD
40183650001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
mg/L
0.079J
2.5
2.5
2.4
2.4
92
91
75-125
1
20
Barium
mg/L
0.46
2.5
2.5
2.8
2.9
95
97
75-125
2
20
Cadmium
mg/L
<0.0066
2.5
2.5
2.4
2.4
98
98
75-125
0
20
Chromium
mg/L
<0.013
2.5
2.5
2.4
2.5
98
100
75-125
2
20
Lead
mg/L
0.18
2.5
2.5
2.5
2.6
94
96
75-125
2
20
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC.
Page 16 of 45

aceAnalytical
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Pace Analytical Services, LLrC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1835475
1835476
MS
MSD
40183650001 Spike
Spike
MS MSD
MS MSD % Rec
Max
Parameter Units
Result Conc.
Conc.
Result Result
% Rec % Rec Limits
RPD RPD Qual
Selenium mg/L
<0.061 2.5
2.5
2.5 2.5
97 99 75-125
3 20
Silver mg/L
<0.017 1.2
1.2
1.3 1.3
100 101 75-125
1 20
MATRIX SPIKE SAMPLE:
1835477
40183727002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
0.067J
2.5
2.4
91
75-125
Barium
mg/L
<0.025
2.5
2.5
99
75-125
Cadmium
mg/L
<0.0066
2.5
2.5
98
75-125
Chromium
mg/L
6.0
2.5
8.6
106
75-125
Lead
mg/L
0.13
2.5
2.6
97
75-125
Selenium
mg/L
<0.061
2.5
2.7
105
75-125
Silver
mg/L
<0.017
1.2
1.2
99
75-125
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 45

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QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
QC Batch: 315776 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV TCLP
Associated Lab Samples: 40184019001
METHOD BLANK: 1836880
Associated Lab Samples: 40184019001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1-Dichloroethene
ug/L
<0.41
1.0
03/19/19 07:18
1,2-Dichloroethane
ug/L
<0.17
1.0
03/19/19 07:18
2-Butanone (MEK)
ug/L
<3.0
20.0
03/19/19 07:18
Benzene
ug/L
<0.50
1.0
03/19/19 07:18
Carbon tetrachloride
ug/L
<0.50
1.0
03/19/19 07:18
Chlorobenzene
ug/L
<0.50
1.0
03/19/19 07:18
Chloroform
ug/L
<2.5
5.0
03/19/19 07:18
Tetrachloroethene
ug/L
<0.50
1.0
03/19/19 07:18
Trichloroethene
ug/L
<0.33
1.0
03/19/19 07:18
Vinyl chloride
ug/L
<0.18
1.0
03/19/19 07:18
4-Bromofluorobenzene (S)
%
90
70-130
03/19/19 07:18
Dibromofluoromethane (S)
%
91
70-130
03/19/19 07:18
Toluene-d8 (S)
%
105
70-130
03/19/19 07:18
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
METHOD BLANK: 1836718
Matrix:
Solid
Associated Lab Samples: 40184019001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1-Dichloroethene
ug/L
<4.1
10.0
03/19/19 07:40
1,2-Dichloroethane
ug/L
<1.7
10.0
03/19/19 07:40
2-Butanone (MEK)
ug/L
<29.8
200
03/19/19 07:40
Benzene
ug/L
<5.0
10.0
03/19/19 07:40
Carbon tetrachloride
ug/L
<5.0
10.0
03/19/19 07:40
Chlorobenzene
ug/L
<5.0
10.0
03/19/19 07:40
Chloroform
ug/L
<25.0
50.0
03/19/19 07:40
Tetrachloroethene
ug/L
<5.0
10.0
03/19/19 07:40
Trichloroethene
ug/L
<3.3
10.0
03/19/19 07:40
Vinyl chloride
ug/L
<1.8
10.0
03/19/19 07:40
4-Bromofluorobe nzene (S)
%
91
70-130
03/19/19 07:40
Dibromofluoromethane (S)
%
92
70-130
03/19/19 07:40
Toluene-d8 (S)
%
102
70-130
03/19/19 07:40
LABORATORY CONTROL SAMPLE: 1836881
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
1,1-Dichloroethene
ug/L
50
44.6
89 75-132
1,2-Dichloroethane
ug/L
50
55.9
112 73-134
Benzene
ug/L
50
56.2
112 69-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 45

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
LABORATORY CONTROL SAMPLE: 1836881
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Carbon tetrachloride
ug/L
50
55.8
112
73-142
Chlorobenzene
ug/L
50
55.0
110
70-130
Chloroform
ug/L
50
48.0
96
80-129
Tetrachloroethene
ug/L
50
52.1
104
70-130
Trichloroethene
ug/L
50
53.8
108
70-130
Vinyl chloride
ug/L
50
37.5
75
48-134
4-Bromofluorobenzene (S)
%
102
70-130
Dibromofluoromethane (S)
%
95
70-130
Toluene-d8 (S)
%
102
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1836896
1836897
MS
MSD
40184034001
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result % Rec % Rec
Limits RPD
RPD Qual
1,1-Dichloroethene
ug/L
<0.0041
500
500
439
449
88 90
72-137
2 20
mg/L
1,2-Dichloroethane
ug/L
<0.0017
500
500
558
573
112 115
71-137
3 20
mg/L
Benzene
ug/L
<0.0050
500
500
567
574
113 115
66-143
1 20
mg/L
Carbon tetrachloride
ug/L
<0.0050
500
500
567
561
113 112
73-142
1 20
mg/L
Chlorobenzene
ug/L
<0.0050
500
500
555
551
111 110
70-130
1 20
mg/L
Chloroform
ug/L
<0.025
500
500
487
488
97 97
80-131
0 20
mg/L
Tetrachloroethene
ug/L
<0.0050
500
500
520
516
104 103
70-132
1 20
mg/L
Trichloroethene
ug/L
<0.0033
500
500
542
546
108 109
70-131
1 20
mg/L
Vinyl chloride
ug/L
<0.0018
500
500
357
370
71 74
46-134
4 20
mg/L
4-Bromofluorobenzene(S)
%
103 101
70-130
Dibromofluoromethane (S)
%
95 94
70-130
Toluene-d8 (S)
%
102 101
70-130
MATRIX SPIKE SAMPLE:
1836898
40184145001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits
Qualifiers
1,1-Dichloroethene
ug/L
<4.1
500
442
88
72-137
1,2-Dichloroethane
ug/L
<1.7
500
565
113
71-137
Benzene
ug/L
<5.0
500
571
114
66-143
Carbon tetrachloride
ug/L
<5.0
500
576
115
73-142
Chlorobenzene
ug/L
<5.0
500
566
113
70-130
Chloroform
ug/L
<25.0
500
461
92
80-131
Tetrachloroethene
ug/L
<5.0
500
531
106
70-132
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC.
Page 19 of 45

aceAnalX cal
www.pacelabs.com
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
MATRIX SPIKE SAMPLE:
1836898
40184145001 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Trichloroethene
ug/L
<3.3 500
545 109
70-131
Vinyl chloride
ug/L
<1.8 500
362 72
46-134
4-Bromofluorobenzene (S)
%
104
70-130
Dibromofluoromethane (S)
%
94
70-130
Toluene-d8 (S)
%
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 45

Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
,1-�1acieAnallj4ical
www.pacelabs.com
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
QC Batch: 315787 Analysis Method: EPA 8081
QC Batch Method: EPA 3510 Analysis Description: 8081 GCS TCLP Pesticides
Associated Lab Samples: 40184019001
METHOD BLANK: 1836921
Matrix:
Water
Associated Lab Samples: 40184019001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chlordane (Technical)
ug/L
<0.44
1.5
03/20/19 21:13 CH
Endrin
ug/L
<0.031
0.10
03/20/19 21:13 CH
gamma-BHC (Lindane)
ug/L
<0.013
0.042
03/20/19 21:13
Heptachlor
ug/L
<0.013
0.044
03/20/19 21:13
Heptachlor epoxide
ug/L
<0.026
0,087
03/20/19 21:13
Methoxychlor
ug/L
<0.16
0.54
03/20/19 21:13
Toxaphene
ug/L
<3.0
6.0
03/20/19 21:13 CH
Decachlorobiphenyl (S)
%
74
10-108
03/20/19 21:13
Tetrachloro-m-xylene (S)
%
91
45-112
03/20/19 21:13
METHOD BLANK: 1834551
Matrix:
Water
Associated Lab Samples: 40184019001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chlordane (Technical)
ug/L
<2.2
7.3
03/21/19 01:25 CH
Endrin
ug/L
<0.16
0.52
03/21/19 01:25 CH
gamma-BHC (Lindane)
ug/L
<0.063
0.21
03/21/19 01:25
Heptachlor
ug/L
<0.065
0.22
03/21/19 01:25
Heptachlor epoxide
ug/L
<0.13
0.43
03/21/19 01:25
Methoxychlor
ug/L
<0.81
2.7
03/21/19 01:25
Toxaphene
ug/L
<15.0
30.0
03/21/19 01:25 CH
Decachlorobiphenyl (S)
%
95
10-108
03/21/19 01:25
Tetrachloro-m-xylene (S)
%
96
45-112
03/21/19 01:25
LABORATORY CONTROL SAMPLE:
Parameter
1836922
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chlordane (Technical)
ug/L
<0.44
CH
Endrin
ug/L
0.8
0.88
111
72-125 CH
gamma-BHC (Lindane)
ug/L
0.4
0.46
115
79-119
Heptachlor
ug/L
0.4
0.42
105
69-122
Heptachlor epoxide
ug/L
0.4
0.45
113
76-118
Methoxychlor
ug/L
4
4.9
122
73-130
Toxaphene
ug/L
<3.0
CH
Decachlorobiphenyl (S)
%
83
10-108
Tetrachloro-m-xylene (S)
%
96
45-112
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 45

aUuAnalytical
www.pacelabs.00m
rn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
Project: PACMIPP_19107
Pace Project No.: 40184019
MATRIX SPIKE SAMPLE:
1836923
40184019001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Chlordane (Technical)
ug/L
<4.4
<4.4
CH
Endrin
ug/L
<0.31
8
9.5
119
72-125 CH
gamma-BHC (Lindane)
ug/L
<0.13
4
4.3
108
79-119
Heptachlor
ug/L
<0.13
4
3.8
96
69-122
Heptachlor epoxide
ug/L
<0.26
4
3.8
96
76-118
Methoxychlor
ug/L
<1.6
40
48.4
121
73-130
Toxaphene
ug/L
<30.0
<30.0
CH
Decachlorobiphenyl (S)
%
38
10-108
Tetrachloro-m-xylene (S)
%
87
45-112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC.
Page 22 of 45

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LL.0
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
QC Batch: 315450 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: 8270 TCLP MSSV
Associated Lab Samples: 40184019001
METHOD BLANK: 1835264
Associated Lab Samples: 40184019001
Matrix: Water
Parameter
Units
Blank
Result
1,4-Dichlorobenzene
ug/L
<3.8
2,4,5-Trichlorophenol
ug/L
<1.7
2,4,6-Trichlorophenol
ug/L
<4.2
2,4-Dinitrotoluene
ug/L
<1.6
2-Methylphenol(o-Cresol)
ug/L
<1.7
3&4-Methylphenol(m&p Cresol)
ug/L
<3.1
Hexachloro-1,3-butadiene
ug/L
<4.9
Hexachlorobenzene
ug/L
<3.4
Hexachloroethane
ug/L
<5.3
Nitrobenzene
ug/L
<2.9
Pentachlorophenol
ug/L
<2.9
Phenol
ug/L
<1.2
Pyridine
ug/L
<3.6
2,4,6-Tribromophenol (S)
%
106
2-Fluorobiphenyl (S)
%
68
Nitrobenzene-d5 (S)
%
68
Phenol-d6 (S)
%
31
METHOD BLANK: 1834548
Associated Lab Samples: 40184019001
Reporting
Limit Analyzed
12.5
03/14/19 12:56
5.6
03/14/19 12:56
14.1
03/14/19 12:56
5.3
03/14/19 12:56
5.8
03/14/19 12:56
10.4
03/14/19 12:56
16.4
03/14/19 12:56
11.3
03/14/19 12:56
17.7
03/14/19 12:56
9.7
03/14/19 12:56
9.6
03/14/19 12:56
4.0
03/14/19 12:56
11.9
03/14/19 12:56
57-131
03/14/19 12:56
47-105
03/14/19 12:56
51-108
03/14/19 12:56
18-120
03/14/19 12:56
Matrix: Water
Parameter
Units
Blank
Result
1,4-Dichlorobenzene
ug/L
<18.8
2,4,5-Trichlorophen ol
ug/L
<8.4
2,4,6-Trichlorophen ol
ug/L
<21.1
2,4-Dinitrotoluene
ug/L
<7.9
2-Methylphenol(o-Cresol)
ug/L
<8.7
3&4-Methylphenol(m&p Cresol)
ug/L
<15.6
Hexachloro-1,3-butadiene
ug/L
<24.6
Hexachlorobenzene
ug/L
<16.9
Hexachloroethane
ug/L
<26.6
Nitrobenzene
ug/L
<14.5
Pentachlorophenol
ug/L
<14.3
Phenol
ug/L
<6.0
Pyridine
ug/L
<17.9
2,4,6-Tribromophenol (S)
%
116
2-Fluorobiphenyl (S)
%
79
Nitrobenzene-d5 (S)
%
85
Phenol-d6 (S)
%
31
Reporting
Limit
Analyzed
62.5
03/14/19 20:18
28.0
03/14/19 20:18
70.4
03/14/19 20:18
26.4
03/14/19 20:18
28.9
03/14/19 20:18
52.0
03/14/19 20:18
82.0
03/14/19 20:18
56.4
03/14/19 20:18
88.6
03/14/19 20:18
48.3
03/14/19 20:18
47.8
03/14/19 20:18
20.0
03/14/19 20:18
59.6
03/14/19 20:18
57-131
03/14/19 20:18
47-105
03/14/19 20:18
51-108
03/14/19 20:18
18-120
03/14/19 20:18
Qualifiers
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LI.C. Page 23 of 45

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
METHOD BLANK: 1834747
Associated Lab Samples: 40184019001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,4-Dichlorobe nzene
ug/L
<18.8
62.5
03/14/19 20:40
2,4,5-Trichlorophenol
ug/L
<8.4
28.0
03/14/19 20:40
2,4,6-Trichlorophenol
ug/L
<21.1
70.4
03/14/19 20:40
2,4-Dinitrotoluene
ug/L
<7.9
26.4
03/14/19 20:40
2-Methylphenol(o-Cresol)
ug/L
<8.7
28.9
03/14/19 20:40
3&4-Methylphenol(m&p Cresol)
ug/L
<15.6
52.0
03/14/19 20:40
Hexachloro-1,3-butadiene
ug/L
<24.6
82.0
03/14/19 20:40
Hexachlorobe nzene
ug/L
<16.9
56.4
03/14/19 20:40
Hexachloroethane
ug/L
<26.6
88.6
03/14/19 20:40
Nitrobenzene
ug/L
<14.5
48.3
03/14/19 20:40
Pentachlorophenol
ug/L
<14.3
47.8
03/14/19 20:40
Phenol
ug/L
<6.0
20.0
03/14/19 20:40
Pyridine
ug/L
<17.9
59.6
03/14/19 20:40
2,4,6-Tribromophenol (S)
%
116
57-131
03/14/19 20:40
2-Fluorobiphenyl (S)
%
82
47-105
03/14/19 20:40
Nitrobenzene-d5 (S)
%
89
51-108
03/14/19 20:40
Phenol-d6 (S)
%
29
18-120
03/14/19 20:40
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1835265
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,4-Dichlorobenzene
ug/L
50
37.6
75
57-120
2,4,5-Trichlorophenol
ug/L
50
42.5
85
59-124
2,4,6-Trichlorophenol
ug/L
50
42.1
84
64-125
2,4-Dinitrotoluene
ug/L
50
50.7
101
70-132
2-Methylphenol(o-Cresol)
ug/L
50
39.8
80
45-107
3&4-Methylphenoi(m&p Cresol)
ug/L
50
34.9
70
39-130
Hexachloro-1,3-butadiene
ug/L
50
43.5
87
63-107
Hexachlorobenzene
ug/L
50
54.5
109
70-124
Hexachloroethane
ug/L
50
32.8
66
50-130
Nitrobenzene
ug/L
50
42.6
85
70-130
Pentachlorophenol
ug/L
50
42.9
86
61-113
Phenol
ug/L
50
17.4
35
25-120
Pyridine
ug/L
50
24.0
48
10-78
2,4,6-Tribromophenol (S)
%
115
57-131
2-Fluorobiphenyl (S)
%
73
47-105
Nitrobenzene-d5 (S)
%
85
51-108
Phenol-d6 (S)
%
32
18-120
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, W 54302
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 45

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LkC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
MATRIX SPIKE SAMPLE:
1835266
40183991002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
<18.8
250
195
78
55-120
2,4,5-Trichlorophenol
ug/L
<8.4
250
240
96
26-124
2,4,6-Trichlorophenol
ug/L
<21.1
250
248
99
29-125
2,4-Dinitrotoluene
ug/L
<7.9
250
250
100
32-143
2-Methylphenol(o-Cresol)
ug/L
<8.7
250
205
82
25-107
3&4-Methylphenol(m&p Cresol)
ug/L
<15.6
250
175
70
21-130
Hexachloro-1,3-butadiene
ug/L
<24.6
250
215
86
63-109
Hexachlorobenzene
ug/L
<16.9
250
268
107
57-124
Hexachloroethane
ug/L
<26.6
250
174
70
50-130
Nitrobenzene
ug/L
<14.5
250
227
91
23-147
Pentachlorophenol
ug/L
<14.3
250
233
93
10-200
Phenol
ug/L
<6.0
250
94.5
37
20-120
Pyridine
ug/L
<17.9
250
103
41
10-78
2,4,6-Tribromophenol (S)
%
114
57-131
2-Fluorobiphenyl (S)
%
79
47-105
Nitrobenzene-d5 (S)
%
85
51-108
Phenol-d6 (S)
%
34
18-120
MATRIX SPIKE SAMPLE:
Parameter
1835267
Units
40183991007
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
<18.8
250
193
77
55-120
2,4,5-Trichlorophenol
ug/L
<8.4
250
228
91
26-124
2,4,6-Trichlorophenol
ug/L
<21.1
250
240
96
29-125
2,4-Dinitrotoluene
ug/L
<7.9
250
256
102
32-143
2-Methylphenol(o-Cresol)
ug/L
<8.7
250
206
82
25-107
3&4-Methylphenol(m&p Cresol)
ug/L
<15.6
250
184
74
21-130
Hexachloro-1,3-butadiene
ug/L
<24.6
250
218
87
63-109
Hexachlorobenzene
ug/L
<16.9
250
259
104
57-124
Hexachloroethane
ug/L
<26.6
250
178
71
50-130
Nitrobenzene
ug/L
<14.5
250
189
76
23-147
Pentachlorophenol
ug/L
<14.3
250
228
91
10-200
Phenol
ug/L
<6.0
250
90.6
35
20-120
Pyridine
ug/L
<17.9
250
146
59
10-78
2,4,6-Tribromophenol(S)
%
116
57-131
2-Fluorobiphenyl (S)
%
83
47-105
Nitrobenzene-d5 (S)
%
80
51-108
Phenol-d6 (S)
%
34
18-120
MATRIX SPIKE SAMPLE: 1835268
40184034001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
1,4-Dichlorobenzene ug/L <0.019 mg/L 250 202 81 55-120
2,4,5-Trichlorophenol ug/L <0.0084 mg/L 250 246 98 26-124
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 45

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
MATRIX SPIKE SAMPLE:
1835268
40184034001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2,4,6-Trichlorophenol
ug/L
<0.021 mg/L
250
250
100
29-125
2,4-Dinitrotoluene
ug/L
<0.0079 mg/L
250
253
101
32-143
2-Methylphenol(o-Cresol)
ug/L
<0.0087 mg/L
250
219
88
25-107
3&4-Methylphenol(m&p Cresol)
ug/L
<0.016 mg/L
250
192
77
21-130
Hexachloro-1,3-butadiene
ug/L
<0.025 mg/L
250
221
89
63-109
Hexachlorobenzene
ug/L
<0.017 mg/L
250
264
105
57-124
Hexachloroethane
ug/L
<0.027 mg/L
250
187
75
50-130
Nitrobenzene
ug/L
<0.015 mg/L
250
224
89
23-147
Pentachlorophenol
ug/L
<0.014 mg/L
250
214
86
10-200
Phenol
ug/L
<6.0
250
82.8
33
20-120
Pyridine
ug/L
<0.018 mg/L
250
95.9
38
10-78
2,4,6-Tribromophenol (S)
%
115
57-131
2-Fluorobiphenyl (S)
%
87
47-105
Nitrobenzene-d5(S)
%
92
51-108
Phenol-d6 (S)
%
33
18-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC.
Page 26 of 45

acmnalXical
www.pacelabs.com
Pace Analytical Services, LL-C
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
QUALITY CONTROL DATA
Project: PACMIPP_19107
Pace Project No.: 40184019
QC Batch: 315332 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 40184019001
SAMPLE DUPLICATE: 1834528
40184019001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 5.4 5.5 1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 45

aceAnalytical
www.pacelabs.com
Project: PACMIPP_19107
Pace Project No.: 40184019
QC Batch: 315361
QC Batch Method: EPA 9045
Associated Lab Samples: 40184019001
SAMPLE DUPLICATE: 1834624
Parameter Units
pH at 25 Degrees C Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9045
Analysis Description: 9045 pH
40184033002 Dup
Result Result RPD
8.28 8.24 0
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
Max
RPD Qualifiers
5 H6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 45

11�;alceAnalyfical"
www.pacelabs.com
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
QUALIFIERS
Project: PACMIPP_19107
Pace Project No.: 40184019
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above LOD.
J - Estimated concentration at or above the LOD and below the LOQ.
LOD - Limit of Detection adjusted for dilution factor, percent moisture, initial weight and final volume.
LOQ - Limit of Quantitation adjusted for dilution factor, percent moisture, initial weight and final volume.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected at or above the adjusted LOD.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
1 q Analyte was detected in the associated leach blank at a concentration of 0.042 mg/L.
2q Analyte was detected in the associated method blank at a concentration of 0.012 mg/L.
CH The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2019 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 45

aceAnalXical
www pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: PACMIPP_19107
Pace Project No.: 40184019
Pace Analytical Services, LLC
1241 Bellevue Street - Suite 9
Green Bay, WI 54302
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
40184019001
19002892/964
EPA 3510
315787
EPA 8081
315866
40184019001
19002892/964
EPA 3010
315523
EPA 6010
315639
40184019001
19002892/964
EPA 7470
315965
EPA 7470
316024
40184019001
19002892/964
EPA 3510
315450
EPA 8270
315528
40184019001
19002892/964
EPA 8260
315776
40184019001
19002892/964
ASTM D2974-87
315332
40184019001
19002892/964
EPA 9045
315361
Date: 03/27/2019 08:00 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 30 of 45

��aceAnalj4ical'
ww Patetabs tom
CHAIN -OF -CUSTODY / Analytical Request Document
The Cham-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
4o(8t4 0 19
Section A Section B
Section C m
Required Client information: Required Project Information
q q 1
Page: of ll
Invoice Information:
Attention: Zach Vogel
Company: Milwaukee Metro. Sewerage District Report
To: Zach Vogel
Address: 260 W Seeboth St. Copy
To: Alfredo Sotomayor, Neal Rehse, waIden
Company Name: MMSD
REGULObRYAGENCY ; ,• . .
Milwaukee, WI 53204
V
Address: 260 W Seeboth St. 53204
l— NPDES I— GROUND WATER (' DRINKING WATER
r UST I—RCRA E✓ OTHER
Email To: [e-mail] Purchase
Order No.:
Pace Quota
Reference
Phone: [phone]
Fax [phone] Project
Name:
Pace Pro/ect Brian Basten
LOCatiOp
Manager.
-;Site
" STATE:
Requested Due DatefTAT: 2 WEEK Project
Number. PACmlpp_19107
Pace Profile #:
";:
•' Requested
Anaysiis
Filfered
(Y/N)
'
.,
:::s.:...E..:.i..........-..:::::;:::;:::::::::::::::::::'
Section D Valid MatrixCodCes
Re uired Client information MATRIX ODE
o
2
COLLECTED
Preservatives
N
N
N
N
N
N
N
DRINKMGWATER DW
WATER WT
WASTEWATER WW
s
m
v
0
if
U
z
O
COMPOSITE
COMPOSITE
J
_
PRODUCT P
START
END/GRAB
U
uJ
Z
SOIUSOLID SL
OIL OL
«
JO
CO
2�
,G
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SAMPLE ID WIPE WP
(�
C.)UU
y
)
;
C
AIR AR
(A-Z. 0-9 IF,-) OTHER OT
Lll
Q
W
z
W
0
Sample IDS MUST BE UNIQUE TISSUE Ts
C)14—
H
:9
N
CLJ
X
W
W
0
N
C
'Jys
ti
0
=�
Co
#
W
Q
0-
a
<
<>
m
O
Z
2
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fn
rec
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=
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C
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J
D_
J
d
J
D-
J
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J
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rn
4
t=
c
U
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GI
U
U
c�
�
DATE
TIME
DATE
TIME
r¢n
at
O
2
=
2
Z
Z
2
O
y
LL
Pace Project No./ Lab I.D.
19002892/964
SL
C
3/3/19
6:00
03/09/19
5:00
1
x
X
X
x
x
X1
X
X
3
a
S
\ao
ADD1710NAG COMMENDS';'
RELINQUISHED BYhA C1AT]ON .: _
DATE ''
`" TIME
ACC D BYIAEFILIATION.'- '. "'.;,;
'• _,DATE' ;'
; ;TIME
SAMPLE CONDITIONS
Full panel of TCLP analysis to be performed on this biosollds
�f
Sample
/
SAMPLER NAME AND SIGNATURE
v
c
ro
c
m i
o U z
c z_
PRINT Name of SAMPLER:
E
d
f
0
eu o
� m
v
d
E
SIGNATURE of SAMPLER:
DATE Signed
(MM/DD/YY):
rn
'Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5 % per month for any invoices not paid wthin 30 days. F-ALL-Q-020rev.08, 12-Oct-2007

Milwaukee Metropolitan
Sewerage District
yo/No/ ?
Contract Lab Request Report
Pace -GB
Date samples sent:
3/11/19
Filename: PACmipp_19107.mdb
Original Sample
19002892 964
3/9/19
34
1208
TCLP 6010 Metals (Milo)
SW846: 6010
19002892
0
19002892
964
3/9/19
36
1211
TCLP Pesticides by m.8081 (Milo)
SW846: 8081
Pol
19002892
964
3/9/19
37
1212
TCLP Herbicides by m.8151 (Milo)
SW846: 8151
19002892
964
3/9/19
38
1209
TCLP VOC by m.8260 (Milo)
SW846: 8260
19002892
964
3/9/19
39
1210
TCLP BNA by m.8270 (Milo)
SW846: 8270
W
19002892
964
3/9/19
33
1170
Mercury, TCLP
SW846: 7470
19002892
964
319/19
35
1178
Final pH (2:1 vol/wt), TCLP
EPA 150.1
19002892
964
319/19
40
1192
Solids for dry weight determination (Pace)
ASTM D2974-87
19002892
964
3/9/19
49
1137
chlordane, TCLP
SW846: 8081
19002892
964
319119
50
1138
endrin, TCLP
SW846: 8081
19002892
964
3/9/19
51
1139
g-BHC, TCLP
SW846: 8081
19002892
964
3/9/19
52
1140
heptachlor epoxide, TCLP
SW846: 8081
19002892
964
3/9/19
53
1141
heptachlor, TCLP
SW846: 8081
19002892
964
3/9/19
54
1142
Methoxychlor, TCLP
SW846: 8081
19002892
964
3/9/19
55
1143
toxaphene, TCLP
SW846: 8081
El
19002892
964
3/9/19
56
1144
2,4,5-TP, TCLP
SW846: 8260
El
19002892
964
3/9/19
57
1145
2,4-D, TCLP
SW846: 8260
19002892
964
3/9/19
58
1146
1, 1 -dichloroethylene, TCLP
SW846: 8260
19002892
964
3/9/19
59
1147
1,2-dichloroethane, TCLP
SW846: 8260
19002892
964
3/9119
60
1148
1,4-dichlorobenzene, TCLP
SW846: 8260
19002892
964
3/9/19
61
1149
benzene, TCLP
SW846: 8260
El
19002892
964
3/9/19
62
1150
Carbon Tetrachloride, TCLP
SW846: 8260
El
19002892
964
3/9/19
63
1151
Chlorobenzene, TCLP
SW846: 8260
11
19002892
964
3/9/19
64
1152
Chloroform, TCLP
SW846: 8260
El
19002892
964
3/9/19
65
1153
Methyl Ethyl Ketone, TCLP
SW846: 8260
19002892
964
3/9/19
66
1154
tetrachloroethylene, TCLP
SW846: 8260
El
19002892
964
3/9/19
67
1155
trichloroethylene, TCLP
SW846: 8260
El
19002892
964
3/9119
68
1156
Vinyl Chloride, TCLP
SW846: 8260
El
19002892
964
3/9119
69
1157
2,45-Trichlorophenol, TCLP
SW846: 8270
El
19002892
964
3/9/19
70
1158
2,4,6-Trichlorophenol, TCLP
SW846: 8270
El
19002892
964
3/9/19
71
1159
2,4-Dinitrotoluene, TCLP
SW846: 8270
El
19002892
964
3/9/19
72
1160
hexachlorobenzene, TCLP
SW846: 8270
19002892
964
3/9/19
73
1161
hexachlorobutadiene, TCLP
SW846: 8270
El
19002892
964
3/9/19
74
1162
hexachloroethane, TCLP
SW846: 8270
El
19002892
964
3/9/19
75
1163
m & p-Cresol, TCLP (3 & 4-Methylphenol)
SW846: 8270
19002892
964
3/9/19
76
1164
nitrobenzene, TCLP
SW846: 8270
El
GU/rptContractLab &8/170
Page 1 of 2
Printed: 2/27/1909:51
Page 32 of 45

C(o /P (
Milwaukee Metropolitan
Contract Lab Request Report
Sewerage District
Pace -GB
Date samples sent:
3/11/19
Filename: PACmipp 19107 mdb
Original Sample
19002892
19002892 964 3/9/19
77
1165
o-Cresol, TCLP (2-Methylphenol)
SW846: 8270
19002892 964 3/9/19
78
1166
pentachlorophenol, TCLP
SW846: 8270
❑
19002892 964 3/9/19
79
1167
phenol, TCLP
SW846: 8270
❑
19002892 964 3/9/19
80
1168
Pyridine, TCLP
SW846: 8270
0
19002892 964 3/9/19
81
1169
Total Cresol, TCLP
SW846: 8270
❑
19002892 964 3/9/19
82
1171
Arsenic, TCLP
SW846: 6010
❑
19002892 964 3/9/19
83
1172
Barium, TCLP
SW846: 6010
11
19002892 964 3/9/19
84
1173
Cadmium, TCLP
SW846: 6010
❑
19002892 964 3/9/19
85
1174
Chromium, TCLP
SW846: 6010
El-
19002892 964 3/9/19
86
1175
Lead, TCLP
SW846: 6010
❑
19002892 964 3/9/19
87
1176
Selenium, TCLP
SW846: 6010
❑
19002892 964 3/9/19
88
1177
Silver, TCLP
SW846: 6010
❑
NOTE: A check mark in the Group field indicates that this item is the billable test name. This item will appear in the electronic data file, but does
not need data recorded. MMSD LIMS must identify that this test has been completed on upload. The associated analytes for the group will not
have a check mark, but will have the same method.
GU/rptContractLab &WI7 tj Page 2 of 2
Printed: 2 7/Pa9A3 of 45

Sample Preservation Receipt Form
Client Name: Mmm Project#
All containers needing preservation have been checked and noted below: ❑Yes ❑No fi/A
Lab Lot# of pH paper: Lab Std #ID of preservation (if pH adiusted)
Pace Analytical Services,LLC
1241 Bellevue Street, Su(b 9
Green Bay, WI 54102
a
Initial when Date/
completed: Time:
Plastic
General
J:
Volume
P
•
.
u
u CO u CO u u u
• •
•
■.-©--■--O
..............-�
■.-.
--
1 1
Exceptions to preservation check: VOA, Coliform, TOC, TOX, TOH, O&G, WI DRO, Phenolics, Other: Headspace in VOA Vials (>6mm) : oYes oNo */A *If yes look in headspace column
AGlU
AG1H
AG45 `
AG4U
1 liter amber glass
1 liter amber glass HCL
125 mL amber glass H2504
120 mL amber glass unpres
BPSU
BPZN
BP2Z
BP3U
1 liter plastic unpres
500 mL plastic HNO3
500 mL plastic NaOH, Znact
250 mL plastic unpres
DG9A
DG9T
VG9U
VG9H
40 mL amber ascorbic
40 ml. amber Na Thio
40 mL clear vial unpres
40 mL clear vial HCL
JGFU
WGFU
WPFU
4 oz amber jar unpres
4 oz clear jar unpres
4 oz plastic jar unpres
AGSU
AG2S
BG3U
100 mL amber glass unpres
500 mL amber glass H2SO4
250 mL clear glass unpres
BP3C
BP3N
BP35
250 mL plastic NaOH
250 mL plastic HNO3
250 mL plastic H2SO4
VG9M
VG91)
40 mL clear vial McOH
40 mL clear vial DI
SP5T
ZPLC
GN:
120 mL plastic Na Thiosulfate
ziploc bag
Page 1 of 2-
F-GB-C-046-Rev.02 (29Mar2018) Sample Preservation Receipt Form

aceAnalyiica/'"J54302
Document Name:
Sample Condition Upon Receipt (SCUR)
Document Revised: 25Apr2018
1241 Bellevue Street, Green Bay, WI
Document No.:
F-GB-C-031-Rev.07
Issuing Authority:
Pace Green Bay Quality Office
Sample Condition Upon Receipt Form (SCUR)
Proiect #
Client Name: �1 m� D
Courier: r- CS Logistics j" Fed Ex r- Speedee r- UPS
i— Client Pace Other:
Tracking #:
Custody Seal on Cooler/Box Present: I< yes r, no Seals intact: K yes r°' no
Custody Seal on Samples Present: r- yes K no Seals intact: r-, yes r no
Packing Material: r Bubble Wrap 0( Bubble Bags r None r Other
Thermometer Used _SR - �JA Type of Ice: & Blue Dry None
Cooler Temperature Uncorr: U. /Corr:
r7l! Waltco
WO#:40184019
40184019
iX Samples on ice, cooling process has begun
i emp tsianx I -resent: F yes rlkno
Biological Tissue is Frozen: r" yes no
Person a mi ing contents:
Temp should be above freezing to 6°C.
Date: it
Biota Samples may be received at s 0°C.
Initials:
Chain of Custody Present:
Yes
❑No
❑N/A
1.
Chain of Custody Filled Out:
❑Yes
o
❑N/A
2. Q
ain of Custody Relinquished:
IlYes
❑No
❑N/A
3,
�amplerName ignatu n COC:
❑Yes
19No
❑N/A
4,
Samples Arrived within Hold Time:
OYes
❑No
5.
- VOA Samples frozen upon receipt
❑Yes
❑No
Date/Time:
Short Hold Time Analysis (<72hr):
❑Yes
No
6.
Rush Turn Around Time Requested:
❑Yes
KNo
7.
Sufficient Volume:
8
For Analysis: es ❑No MS/MSD: Dyes
4No
❑N/A
Correct Containers Used:
Oyes
❑No
g,
-Pace Containers Used:
❑Yes
[�No
❑N/A
-Pace IR Containers Used:
❑Yes
Go
❑N/A
Containers Intact:
Yes
El No
10.
Filtered volume received for Dissolved tests
❑Yes
[%No
❑N/A
11.
Sample Labels match COC:
MYes
❑No
❑N/A
12. NlV VVLL ?31 It (l 1
-Includes date/time/ID/Analysis Matrix:
Trip Blank Present:
❑Yes
❑No
, 3N/A
13.
Trip Blank Custody Seals Present
❑Yes
❑No
ZN/A
Pace Trip Blank Lot # (if purchased):
Client Nntifiratinn/
Person Contacted:
Comments/ Resolution:
M6
iT cnecKea, see attached form for additional comments
Date/Time:
3
Project Manager Review: Date:
Page 2 Pf�35 of 45

I
eAnalytical" AIllALYTICAL REPORT
Center for Testing & Innovation March 26, 2019
Pace Analytical - Green Bay, WI
Sample Delivery Group: L1080230
Samples Received: 03/19/2019
Project Number: 40184019
Description: PACMIPP_19107
Report To: Brian Basten
1241 Bellvue Street, Suite 9
Green Bay, WI 54302
Entire Report Reviewed By
wV�w� AA .. l � `t, Lo'�
� �-
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
0

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
Fs
19002892/964 L1080230-01
5
Qc: Quality Control Summary
6
Fn
Chlorinated Acid Herbicides (GC) by Method 8151A
6
F
GI: Glossary of Terms
7
Al: Accreditations & Locations
8
QC
Sc: Sample Chain of Custody
9
F
E
E
Page 37 of 45
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:

SAMPLE SUMMARY
ONE LAB. NATIONWIDE.
Collected by
Collected date/time
Received date/time
19002892/964 L1080230-01 Waste
03/09/19 05:00
03/19/19 08:30
Method
Batch Dilution Preparation
Analysis
Analyst Location
date/time
date/time
Preparation by Method 1311
WG1253413 1 03/21/1914:51
03/21/1914:51
CGD Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1254854 1 03/25/19 07:03
03/25/19 20:44
MTJ Mt. Juliet, TN
Page 38 of 45
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

CASE NARRATIVE
ONE LAB. NATIONWIDE. .
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
&/Vv(A� � 4t La4�'_
Nancy McLain
Project Manager
ACCOUNT: PROJECT: SDG:
DATE/TIME:
Page 39 of 45
PAGE:

SAMPLE RESULTS - 01
L1080230
ONE LAB. NATIONWIDE.
19002892/964
Collected date/time: 03/09/19 05:00
Preparation by Method 1311
Result Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction
- 3/21/2019 2:51:13 PM
WG1253413
Fluid
1 3/21/2019 2:51:13 PM
WG1253413
Initial pH
6.36 3/21/2019 2:51:13 PM
WG1253413
Final pH
5.29 3/21/2019 2:51:13 PM
WG1253413
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date / time
2,4,5-TP (Silvex)
ND
0.00200
1
1 03/25/2019 20:44
WG1254854
2,4-D
ND
0.00200
10
1 03/25/2019 20:44
WG1254854
(S)2,4-DichlorophenylAcetic Acid
121
14.0-158
031251201920:44
WG1254854
Page 40 of 45
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

WG1254854
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1080230-01
(MB) R3395113-1 03/25/1916:58
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S) 2,4-Dichlorophenyl Acetic 56.6
Acid
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
0.000667
0.00200
0.000667
0.00200
14.0-158
Laboratory Control Sample (LCS)
(LCS) R3395113-2 03/25/1917:13
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg)]
mg/I
%
%
2,4-D 0.0500
0.0390
78.0
50.0-120
2,4,5-TP (Silvex) 0.0500
0.0421
84.2
50.0-125
(S) 2,4-Dichlorophenyl Acetic
74.2
14.0-158
Acid
L1079918-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1079918-01 03/25/1917:27 • (MS) R3395113-3 03/25/1917:41 • (MSD) R3395113-4 03/25/1917:55
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
2,4-D
0.0500
ND
0.0395
0.0387
79.0
77.4
1 50.0-120
2,4,5-TP (Silvex)
0.0500
ND
0.0425
0.0419
85.0
83.8
1 50.0-125
(S) 2,4-Dichlorophenyl Acetic
73.0
75.6
14.0-158
Acid
ACCOUNT: PROJECT: SDG:
Pace Analytical - Green Bay, WI 40184019 L1080230
MS Qualifier MSD Qualifier R
5
2
1.
DATE/TIN
03/26/191,

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not E
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG
ACCOUNT: PROJECT: SDG:
Page 42 of 45
DATE/TIME: PAGE:

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. ' ,*
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
"Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
State Accreditations
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico'
n/a
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky "
90010
South Carolina
84004
Kentucky'
16
South Dakota
n/a
Louisiana
A130792
Tennessee' "
2006
Louisiana'
LA180010
Texas
T104704245-18-15
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
TN00003
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
460132
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
Wyoming
A2LA
Third Party Federal Accreditations
A2LA— ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA — ISO 17025' 1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Crypto TN00003
' Drinking Water ' Underground Storage Tanks 'Aquatic Toxicity `Chemical/Microbiological 'Mold 'Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
Page 43 of 45
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

V
Chaim of Custody
40184019 s i'
r : 9 • }
Brian Basten
Pace Analytical Green Bay
1241 Bellevue Street
Suite 9
Green Bay, WI 54302
Phone [phone]
Email: [e-mail]
State of Sample Origin. Wl LODfLOQ
item Sample ID
19002892l954
2
3
4
5
Transfers Released By
�3 s
Cooler Temperature on
Monday, March 11. 2019 3:49'26 Plot
PACMIPP_19107
mtract To
P.O.
Face National
collect
DatefTime Lab ID LSolid
5
31912019 05:00 40184019001
RequestedResults By: 3/25j
rWUM
DaterTime Repived By Daterrime Wit. iC� e T'XCr
31.
cLLa B212
°C Custody Seal F or N Received on Ice or N
R110 C^^LEN: <0.5 mi
FMT-ALL-C-002rev.00 24M

Pace Analytical National Center for Testing & Innovation
Cooler Receipt
a w` r} 4 ljJ
Client: TRA��-
D(;#:Cooler
Received/Opened On: 3 I / 29 Temperature;
Received By: Kristin Willis
Signature:
Receipt Check list NP
Yes
COC Seal Present / Intact?
COC Signed / Accurate?
Bottles arrive intact?
f
Correct bottles used?
Sufficient volume sent?
'
If Applicable
VOA Zero headspace?
Preservation Correct / Checked?

For Better Results.
Milorganite
PW
Milorganite® Fertilizer
Exceptional Quality Biosolids Certification
We, Steven J. Unger, Contract Compliance Administrator, Milwaukee Metropolitan Sewerage District, and
Brett Kelly, Operations Manager, Veolia Water Milwaukee LLC, certify we have personally examined and are
familiar with the submitted information. Based upon our inquiry of those individuals immediately responsible
for obtaining the information, we believe the submitted information is true, accurate, and complete.
We certify Milorganite® fertilizer:
(1) complied with the limits of 40 CFR § 503.13(b)(3) and Wis. Adm. Code, sec. NR 204.07(5)(c) Table 3;
(2) was dried to achieve a pellet temperature exceeding 176 'F/80 'C and no more than 10% moisture, as
required for Class A pathogen destruction, according to 40 CFR § 503.32, Appendix B, sec. B.2, and Wis.
Adm. Code, sec. NR 204.07(6)(a)(2)c; and
(3) was dried to achieve greater than 75% solids, as required for vector attraction reduction by
40 CFR § 503.33(b)(7) and Wis. Adm. Code, sec. NR 204.07(7)(g).
We made this determination based upon an environmental management system in which qualified personnel
properly gather and evaluate information regarding pollutant concentrations, pathogen reduction, and vector
attraction reduction. We are aware of the significant penalties for submitting false information, including the
possibility of fine and imprisonment.
Certified January ILL, 2020: 1'
Steven J. Unger, &ntrad Compliance Administrator
Certified January _L0, 2020: z4z—"
Brett Kelly, Operations Manager
Milorganite - MMSD 260 W. Seeboth Street Milwaukee, WI 53204 0'
Phone: [phone] [phone] Fax: [phone]
Sustaining Turfgrass Research roan,— n�jv [e-mail] www.milorganite.com

hhh,11 SLOW -RELEASE
M'Ilorganimteo
NITROGEN FERTILIZER
Summary of Sample Results
2019
Parameter
Units
Highest
Day
Annual
Average
Federal
Limit
Arsenic
mg/kg
6.8
<3.91
41
Cadmium
mg/kg
2.2
0.92
39
Chromium
mg/kg
320
200
Copper
mg/kg
260
220
1,500
Lead
mg/kg
57
34
300
Mercury
mg/kg
0.37
0.14
17
Molybdenum
mg/kg
13
9.4
75
Nickel
mg/kg
41
25
420
Selenium
mg/kg
12
<4.11
100
Zinc
mg/kg
540
420
2,800
PCB Aroclors (total)
mg/kg
0.18
<0.0551
Dioxin TEQ2
pg/g
25
11
1. These annual averages were below the level of detection
2. Dioxin TEQ is the sum of the concentrations of various dioxins,
furans, and polychlorinated biphenyls multiplied by individual toxic
equivalency factors, as established by the U.S. Environmental
Protection Agency

MMSD
PARTNERS FOR A CLEANER ENVIRONMENT
January 17, 2020
TO: Brett Kelly, Todd Schwingle, Dion Doege, Jacob Holbert, Sam Lieven
FROM: Zach Vogel
COPY: S. Unger, T. Nowicki, J. Spence, J. Staufenbeil, B. Stroik, A. Sotomayor, R. Vincent,
Lab File
SUBJECT: Annual Milorganite Report-2019
Attached is the Annual Milorganite report for the year 2019. The boron and mercury analyses were performed
by CT Laboratories, in Baraboo, Wisconsin (Wisconsin Certification IN 157066030) and Pace Analytical
Services, Inc. in Green Bay, Wisconsin (Wisconsin Certification #: 405132750). All other analyses were
performed by Milwaukee Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #:
241325920, Florida NELAP Certification #: E571010).
There was no Milorganite production on the following dates:
• January 20, 2019;
• October 2 through October 12, 2019.
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Data Review By: Report Review By:
1/
Richard Vincent Date Zach Vogel Date
Laboratory Supervisor
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

SMMSD
PARTNERS FOR A CLEANER ENVIRONMENT
February 13, 2019
Memorandum
TO: Todd Schwingle, Dion Doege, Jacob Holbert, Brett Kelly, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Jaime Staufenbeil, Tom Nowicki, Beth Stroik, Kori
Kenney, Lab File
SUBJECT: Milorganite Monthly Data —January 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of January
2019. The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin
(Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
The following comment is associated with this report:
• There were no daily production samples on January 20, 2019.
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
Richard Vincent Date
Laboratory Team Supervisor
Report Review By:
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

I kN
ALUMINUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ QA Flags
Monthly Milorganite Report
January 2019
Analytical Method Lab
01/12/19
WMCO2/19000708
5400 mg/kg D.W.
87
240 B8.
SW846: 6010C
MMSD
Avg Result: 5400 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Sample Date Sample ID
Min LOD: 87 mg/kg D.W.
Result LOD LOQ .• Flags
Analytical Method
Lab
01/12/19 WMCO2/19000708
Avg Result: 0.2 %
ARSENIC ICP METHOD
Sample Date Sample ID
0.2 % 0.11
Min LOD: 0.11 "/o
Result LOD
LOQ •. Flags
AOAC (13) 2.065
Analytical Method__
MMSD
Lab
01/01/19
DMO101/19000023
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/02/19
DMO102/19000063
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/03/19
DMO103/19000237
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
01/04/19
DMO104/19000253
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
01/05/19
DMO105/19000264
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
01/06/19
DMO106/19000284
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
01/07/19
DMO107/19000298
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
01/08/19
DMO108/19000324
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
01/09/19
DMO109/19000353
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
01/10/19
DMO110/19000588
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
01/11/19
DMO111/19000608
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/12/19
DM0112/19000619
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
01/13/19
DM0113/19000639
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/14/19
DM0114/19000706
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/15/19
DM0115/19000742
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/16/19
DM0116/19000771
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
01/17/19
DM0117/19000792
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/18/19
DMO118/19000812
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/19/19
DM0119/19000823
< 6.5 mg/kg D.W.
6.5
19
SW846: 6010C
MMSD
01/21/19
DMO121/19000858
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
01/22/19
DMO122/19000920
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
01/23/19
DMO123/19000949
< 6.5 mg/kg D.W.
6..5
20
SW846: 6010C
MMSD
01/24/19
DMO124/19000970
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/25/19
DMO125/19000986
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/26/19
DMO126/19001042
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
01/27/19
DMO127/19001062
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
01/28/19
DMO128/19001109
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
01/29/19
DMO129/19001179
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
01/30/19
DMO130/19001246
< 6.5 mg/kg D.W.
6.5
19
SW846: 6010C
MMSD
01/31/19
DMO131/19001267
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
BORON ICP Dry wt.
'Sample Date Sample ID
Min LOD: 6.3 mg/kg D.W.
Result LOD LOQ QA Flags
Analytical Method
Lab
01/12/19
WMCO2/19000708
19 mg/kg D.W.
1.1
3.4
SW846: 6010C
CT Lab
Avg Result: 19 mg/kg D.W.
SY51WIM110Month/y 1110113 tj
Min LOD:
1.1 mg/kg D.W.
Page I of 1j
Printed: 211311910:56

�►�15 �t a Ct
CADMIUM ICP METHOD
Date Sample ID
01/01/19 DMO101/19000023
Result
0.6 mg/kg D.W.
LOD
0.31
LOQ
1.4
J.
Monthly Milorganite Report
January 2019
SW846: 6010C MMSD
01/02/19
DMO102/19000063
0.52 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/03/19
DMO103/19000237
0.51 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/04/19
DMO104/19000253
0.38 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/05/19
DMO105/19000264
0.77 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/06/19
DMO106/19000284
0.54 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/07/19
DMO107/19000298
0.69 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/08/19
DMO108/19000324
0.34 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/09/19
01/10/19
DMO109/19000353
DMO110/19000588
< 0.3 mg/kg D.W.
0.41 mg/kg D.W.
0.3
0.3
1.4
1.4
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/11/19
DMO111/19000608
0.58 mg/kg D.W.
0.31
1.4
J.
SW846: 6010C
MMSD
01/12/19
DM0112/19000619
0.58 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/13/19
DM0113/19000639
0.5 mg/kg D.W.
0.31
1.4
J.
SW846: 6010C
MMSD
01/14/19
DM0114/19000706
0.41 mg/kg D.W.
0.31
1.4
J.
SW846: 6010C
MMSD
01/15/19
DM0115/19000742
0.55 mg/kg D.W.
0.31
1.4
J.
SW846: 6010C
MMSD
01/16/19
DM0116/19000771
0.49 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/17/19
01/18/19
DM0117/19000792
DM0118/19000812
< 0.31 mg/kg D.W.
0.55 mg/kg D.W.
0.31
0.31
1.4
1.4
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/19/19
DM0119/19000823
0.48 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/21/19
DMO121/19000858
0.4 mg/kg D.W.
0.29
1.4
J.
SW846: 6010C
MMSD
01/22/19
DMO122/19000920
< 0.3 mg/kg D.W.
0.3
1.4
SW846: 6010C
MMSD
01/23/19
01/24/19
DMO123/19000949
DMO124/19000970
0.66 mg/kg D.W.
< 0.31 mg/kg D.W.
0.3
0.31
1.4
1.4
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/25/19
DMO125119000986
1.2 mg/kg D.W.
0.31
1.4
J.
SW846: 6010C
MMSD
01/26/19
DMO126/19001042
0.73 mg/kg D.W.
0.31
1.4
J.
SW846: 6010C
MMSD
01/27/19
DMO127/19001062
0.64 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/28/19
DMO128/19001109
0.48 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/29/19
DMO129/19001179
0.45 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/30/19
DMO130/19001246
0.52 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
01/31/19
DMO131/19001267
0.62 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
Avg Result: 0.49 mg/kg D.W.
CHROMIUM ICP Dry wt.
Sample Date
01/12/19 WMCO2/19000708
Avg Result: 180 mg/kg D.W.
COBALT ICP Dry wt.
Sample Date Sample ID
Min LOD: 0.29 mg/kg D.W.
Result LOD LOQ QA
180 mg/kg D.W. 1.4 4.3
Min LOD: 1.4 mg/kg D.W.
Result LOD LOQ QA
Flags
Flags
Max Result: 1.2 mg/kg D.W.
Analytical Method
SW846: 6010C
Analytical Method
Lab
MMSD
Lab
01/12/19
WMCO2/19000708
Avg Result: 3.8 mg/kg D.W.
3.8 mg/kg D.W. 1.2 3.5
Min LOD: 1.2 mg/kg D.W.
B8.
SW846: 6010C
MMSD
Page 2 of 13
SYSIWIMMoMonthly 1110113 tj Printed., 211311910:56

NSD
R1RtAEi'S ip � CLE4� HIfNCilll�l
COPPER ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ QA Flags
Monthly Milorganite Report
January 2019
NL==
Analytical Method
01/01/19
DMO101/19000023
210 mg/kg D.W.
7.9
24
SW846: 6010C
Lab
MMSD
01/02/19
DMO102/19000063
210 mg/kg D.W.
7.9
24
SW846: 6010C
MMSD
01/03/19
DMO103/19000237
210 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
01/04/19
DMO104/19000253
220 mg/kg D.W.
7.7
23
SW846: 6010C
MMSD
01/05/19
DMO105/19000264
210 mg/kg D.W.
7.7
23
SW846: 6010C
MMSD
01/06/19
DMO106/19000284
210 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
01/07/19
DMO107/19000298
220 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
01/08/19
DMO108/19000324
220 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
01/09/19
DMO109/19000353
220 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
01/10/19
DM0110/19000588
220 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
01/11/19
DM0111/19000608
220 mg/kg D.W.
7.9
24
SW846: 6010C
MMSD
01/12/19
DM0112/19000619
230 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
01/13/19
DMO113/19000639
230 mg/kg D.W.
7.9
24
SW846: 6010C
MMSD
01/14/19
DMO114/19000706
220 mg/kg D.W.
7.9
24
SW846: 6010C
MMSD
01/15/19
DM0115/19000742
220 mg/kg D.W.
8
24
SW846: 6010C
MMSD
01/16/19
DM0116/19000771
220 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
01/17/19
DM0117/19000792
220 mg/kg D.W.
7.9
24
SW846: 6010C
MMSD
01/18/19
DM0118119000812
220 mg/kg D.W.
7.9
24
SW846: 6010C
MMSD
01/19/19
DM0119/19000823
230 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
01/21/19
DMO121/19000858
230 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
01/22/19
DMO122/19000920
240 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
01/23/19
01/24/19
DMO123/19000949
DMO124/19000970
220 mg/kg D.W.
230 mg/kg D.W.
7.8
7.9
24
24
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/25/19
DMO125119000986
230 mg/kg D.W.
8
24
SW846: 6010C
MMSD
01/26/19
DMO126/19001042
230 mg/kg D.W.
7.9
24
SW846: 6010C
MMSD
01/27/19
DMO127/19001062
220 mg/kg D.W.
7.7
24
SW846: 6010C
MMSD
01/28/19
DMO128/19001109
220 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
01/29/19 DMO129/19001179
01/30/19 DMO130/19001246
01/31/19 DMO131/19001267
Avg Result: 220 mg/kg D.W.
FECAL COLIFORM SLUDGE
:Sample Date Sample ID
220 mg/kg D.W. 7.6 23
230 mg/kg D.W. 7.8 24
220 mg/kg D.W. 7.8 24
Min LOD: 7.6 mg/kg D.W.
Result LOD LOQ QA Flags
SW846: 6010C
SW846: 6010C
SW846: 6010C
Max Result:240 mg/kg D.W.
AnI�ethd
MMSD
MMSD
MMSD
Lab
01/02/19
MF/19000217
< 0.2 MPN/g TS
0.2
EPA 1680
MMSD
01/08/19
MF/19000895
< 0.2 MPN/g TS
0.2
EPA 1680
MMSD
01/15/19
MFI19001357
< 0.2 MPN/g TS
0.2
EPA 1680
MMSD
01/22/19
MF/19001707
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
Min LOD: 0.19 MPN/g TS
Page 3 of I.i
SY51rptlMi/oMonth/y 1110113 tj NOW: 211311910:56

MMSD
PAtTM, l01 A CUOU Ntiw9N(Mz
IRON ICP METHOD
Sample Date Sample ID
01/01/19 DMO101/19000023
Result
46000 mg/kg D.W.
LOD
260
LOQ frRi'gs
760
Monthly Milorganite Report
January 2019
`�—�--"A—nalqggrMW
SW846: 6010C MMSD
01/02/19
DMO102/19000063
48000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
01/03/19
DMO103119000237
50000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
01/04/19
DMO104/19000253
49000 mg/kg D.W.
260
740
SW846: 6010C
MMSD
01/05/19
DMO105/19000264
44000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
01/06/19
DMO106/19000284
43000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
01/07/19
DM0107/19000298
44000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
01/08/19
DMO108/19000324
42000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
01/09/19
01/10/19
DMO109/19000353
DMO110/19000588
43000 mg/kg D.W.
42000 mg/kg D.W.
260
260
760
760
SW846: 6010C _
SW846: 6010C
MMSD
MMSD
01/11/19
DMO111/19000608
42000 mg/kg D.W.
260
770
SW846: 6010C
MMSD
01/12/19
DM0112/19000619
44000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
01/13/19
DM0113/19000639
42000 mg/kg D.W.
260
770
SW846: 6010C
MMSD
01/14/19
DM0114/19000706
43000 mg/kg D.W.
260
770
SW846: 6010C
MMSD
01/15/19
DM0115/19000742
41000 mg/kg D.W.
270
780
SW846: 6010C
MMSD
01/16/19
DM0116/19000771
45000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
01/17/19
01/18/19
DM0117/19000792
DM0118/19000812
45000 mg/kg D.W.
46000 mg/kg D.W.
260
260
770
760
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/19/19
DM0119/19000823
48000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
01/21/19
DMO121/19000858
48000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
01/22/19
DMO122119000920
48000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
01/23/19
01/24/19
DMO123/19000949
DMO124/19000970
52000 mg/kg D.W.
45000 mg/kg D.W.
260
260
760
770
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/25/19
DMO125/19000986
42000 mg/kg D.W.
260
770
SW846: 6010C
MMSD
01/26/19
DMO126/19001042
44000 mg/kg D.W.
260
770
SW846: 6010C
MMSD
01/27/19
DMO127/19001062
43000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
01/28/19
DMO128/19001109
43000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
01/29/19
DMO129/19001179
43000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
01/30/19
DMO130/19001246
42000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
01/31/19
DMO131/19001267
Avg Result: 45000 mg/kg D.W.
42000 mg/kg D.W. 260
Min LOD: 250 mg/kg
760
D.W.
SW846: 6010C
Max Result: 52000 mg/kg D.W.
MMSD
Page 4 or1j
5Wrpt1Mi1bMonth1y 1/10/13 fj Pnnted: 211311910.56

'tiiNSD
LEAD ICP METHOD
..S ample ID
Result
LOD
LOQ .• Flags
Monthly Milorganite Report
January 2019
Analytical Method Lab
01/01/19
DMO101/19000023
33 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/02/19
DMO102/19000063
32 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/03/19
DMO103/19000237
31 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/04/19
DMO104/19000253
29 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
01/05/19
DMO105/19000264
27 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
01/06/19
DMO106/19000284
26 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
01/07/19
DMO107/19000298
27 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
01/08/19
DMO108/19000324
28 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/09/19
DMO109/19000353
27 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/10/19
DM0110/19000588
30 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/11/19
DMO111/19000608
30 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/12/19
DM0112/19000619
30 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/13/19
DM0113/19000639
29 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/14/19
DM0114/19000706
29 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/15/19
DM0115/19000742
29 mg/kg D.W.
4.9
14
SW846: 6010C
MMSD
01/16/19
DM0116/19000771
29 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/17/19
01/18/19
DM0117/19000792
DM0118/19000812
30 mg/kg D.W.
29 mg/kg D.W.
4.8
4.8
14
14
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/19/19
DM0119/19000823
28 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/21/19
DMO121/19000858
28 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/22/19
DMO122/19000920
27 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
01/23/19
01/24/19
DMO123/19000949
DMO124/19000970
30 mg/kg D.W.
27 mg/kg D.W.
4.8
4.8
14
14
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/25/19
DMO125/19000986
25 mg/kg D.W.
4.9
14
SW846: 6010C
MMSD
01/26/19
DMO126/19001042
26 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/27/19
DMO127/19001062
26 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
01/28/19
DMO128/19001109
25 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/29/19
DMO129/19001179
26 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/30/19
DMO130/19001246
25 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
01/31/19
DMO131/19001267
27 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
Avg Result: 28 mg/kg D.W.
MERCURY by M. 7471 (sludge)
Sample Date Sample ID
Min LOD: 4.6 mg/kg D.W.
Result LOD LOQ .• Flags
Max Result: 33 mg/kg D.W.
Analytical Method
Lab
01/05/19
01/12/19
WMC01/19000300
WMCO2/19000708
0.16 mg/kg D.W.
0.11 mg/kg D.W.
0.0056
0.012
0.019 AX.
0.039
EPA 7471B
EPA 7471E
Cr Lab
CT Lab
01/19/19
WMC03/19000860
0.27 mg/kg D.W.
0.0059
0.02 AX.
EPA 7471E
Cr Lab
01/26/19
WMC04/19001111
0.13 mg/kg D.W.
0.0054
0.018
EPA 7471E
CT Lab
Avg Result: 0.17 mg/kg D.W.
Min LOD:
0.0054 mg/kg D.W.
Max Result: 0.27 mg/kg D.W.
Page 5 of 1j
SwrptlMi/om-ffily 1110113 h Printed: 2113/1910:56

'?ifflSD
wtAM#
MOLYBDENUM ICP METHOD
01/01/19 DMO101/19000023
11 mg/kg D.W.
1.3
5.7
Monthly Milorganite Report
January 2019
SW846: 6010C MMSD
01/02/19
OM0102/19000063
10 mg/kg D.W.
1.3
5.7
SW846: 6010C
MMSD
01/03/19
DMO103/19000237
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
01/04/19
DMO104/19000253
9.5 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
01/05/19
DMO105/19000264
9.8 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
01/06/19
DMO106/19000284
9.4 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
01/07/19
DMO107/19000298
9.8 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
01/08/19
DMO108/19000324
10 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
01/09/19
01/10/19
DMO109/19000353
DM0110/19000588
9.7 mg/kg D.W.
9.4 mg/kg D.W.
1.3
1.3
5.6
5.7
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/11/19
DMO111/19000608
9.5 mg/kg D.W.
1.3
5.7
SW846: 6010C
MMSD
01/12/19
DM0112/19000619
9.7 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
01/13/19
DM0113/19000639
9.4 mg/kg D.W.
1.3
5.7
SW846: 6010C
MMSD
01/14/19
DM0114/19000706
9.8 mg/kg D.W.
1.3
5.7
SW846: 6010C
MMSD
01/15/19
DMO115/19000742
9.4 mg/kg D.W.
1.3
5.8
SW846: 6010C
MMSD
01/16/19
DM0116/19000771
11 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
01/17/19
01/18/19
DM0117/19000792
DM0118/19000812
9.5 mg/kg D.W.
9.5 mg/kg D.W.
1.3
1.3
5.7
5.7
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/19/19
DMO119/19000823
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
01/21/19
DMO121/19000858
11 mg/kg D.W.
1.3
5.5 D2.
SW846: 6010C
MMSD
01/22/19
DMO122/19000920
10 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
01/23/19
01/24/19
DMO123/19000949
DMO124/19000970
12 mg/kg D.W.
10 mg/kg D.W.
1.3
1.3
5.6
5.7
SW846: 6010C
SW846: 6010C
- MMSD
MMSD
01/25/19
DMO125/19000986
9.5 mg/kg D.W.
1.3
5.8
SW846: 6010C
MMSD
01/26/19
DMO126/19001042
9.9 mg/kg D.W.
1.3
5.7
SW846: 6010C
MMSD
01/27/19
DMO127/19001062
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
01/28/19
DMO128/19001109
9.4 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
01/29/19
DMO129/19001179
8.8 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
01/30/19
DMO130119001246
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
01/31/19
DMO131/19001267
Avg Result: 9.9 mg/kg D.W.
10 mg/kg D.W. 1.3 5.6
Min LOD: 1.3 mg/kg D.W.
SW846: 6010C
Max Result: 12 mg/kg D.W.
MMSD
Page 6 of I.i
SY5/rpti iloMonthly 1110113 q Printed: 211311910:56

NNSD
PMW FRAMANN MINM
NICKEL ICP METHOD
Sample Date Sample ID
01/01/19 DM0101/19000023
Result
29 mg/kg D.W.
LOD
4.6
L07 A ag's'
14
Monthly Milorganite Report
January 2019
Wjja- "7'77
SW846: 6010C MMSD
01/02/19 DMO102/19000063
30 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/03/19 DMO103/19000237
30 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/04/19 DMO104/19000253
28 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
01/05/19 DMO105/19000264
26 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
01/06/19 DMO106/19000284
25 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
01/07/19 DMO107/19000298
26 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
01/08/19 DMO108/19000324
26 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
01/09/19 DMO109/19000353
24 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/10/19 DMO110/19000588
24 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/11/19 DMO111/19000608
25 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/12/19 DMO112/19000619
24 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/13/19 DM0113/19000639
25 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/14/19 DM0114/19000706
25 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/15/19 DM0115/19000742
25 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/16/19 DM0116/19000771
27 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/17/19 DM0117/19000792
01/18/19 DMO118/19000812
26 mg/kg D.W.
26 mg/kg D.W.
4.6
4.6
14
14
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/19/19 DM0119/19000823
30 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
01/21/19 DMO121/19000858
31 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
01/22/19 DMO122/19000920
26 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
01/23/19 DMO123/19000949
32 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/24/19 DMO124/19000970
28 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/25/19 DMO125/19000986
26 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/26/19 DMO126/19001042
28 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
01/27/19 DMO127/19001662
27 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
01/28/19 DMO128/19001109
26 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
01/29/19 DMO129/19001179
26 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
01/30/19 DMO130/19001246
26 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
01/31/19 DMO131/19001267
Avg Result: 27 mg/kg D.W.
NITRATE NITROGEN
Sample Date Sample ID
26 mg/kg D.W. 4.6 14
Min LOD: 4.4 mg/kg D.W.
Result LOD LOQ QA Flags
SW846: 6010C
Max Result: 32 mg/kg D.W.
Analytical Method
MMSD
Lab
01/12/19 WMCO2/19000708
Avg Result: 0.85 °/u
NITROGEN -Total (Manua[)
Sample Date Sample ID
0.85 % 0.5
Min LOD: 0.5
Result LOD
LOQ QA Flags
AOAC (16) 930.01
Analytical Method
MMSD
Lab
01/12/19 WMCO2/19000708
Avg Result: 6.4 %
NITROGEN -Water Insoluble
Sample Date Sample ID
6.4 % 0.11
Min LOD: 0.11
Result LOD
LOQ .. Flags
AOAC (16) 955.04
Analytical Method
MMSD
Lab
01/12/19 WMCO2/19000708
4.6 %
0.5
AOAC (16) 945.01
MMSD
Avg Result: 4.6 %
SYS/rptlMi/oMontlr/y 1110113 tj
Min LOD:
0.5 %
Page 7 of l.i
Printed., 211311910:56

Monthly Milorganite Report
fkNSD January 2019
I'1R kf13 f0f A CLOW f
pH -Solids
Sample
Date Sample ID Result LOD LOQ .. Flags Method -( �-Lab
01/05/19 WMC01/19000300 6.3 Stnd. Units 0.1 SW846: 9045D MMSD
01/12/19 WMCO2/19000708 6.36 Stnd. Units 0.1 SW846-.9045D MMSD
01/19/19
WMC03/19000860
6.37 Stnd. Units
0.1
SW846: 9045D
MMSD
01/26/19 WMC04/19001111
Avg Result: 6.3 Stnd. Units
PHOSPHORUS ICP METHOD
ID
01/01/19 DMO101/19000023
6.23 Stnd. Units 0.1
Min LOD: 0.1 Stnd. Units
.• LOQ
26000 mg/kg D.W. 19 85
SW846: 9045D
Max Result: 6.37 Stnd. Units
•• Flags Analytical Method
SW846: 6010C
MMSD
Lab
MMSD
01/02/19
DMO102/19000063
26000 mg/kg D.W.
18
85
SW846: 6010C
MMSD
01/03/19
DMO103/19000237
26000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
01/04/19
DMO104/19000253
24000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
01/05/19
01/06/19
DMO105/19000264
DMO106/19000284
24000 mg/kg D.W.
23000 mg/kg D.W.
18
18
83
83
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/07/19
DMO107/19000298
24000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
01/08/19
DMO108/19000324
24000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
01/09/19
DMO109/19000353
24000 mg/kg D.W.
18
85
SW846: 6010C
MMSD
01/10/19
DMO110/19000588
23000 mg/kg D.W.
18
85
SW846: 6010C
MMSD
01/11/19
DMO111/19000608
24000 mg/kg D.W.
19
86
SW846: 6010C
MMSD
01/12/19
01/13/19
DMO112/19000619
DM0113/19000639
23000 mg/kg D.W.
23000 mg/kg D.W.
18
19
85
86
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/14/19
DM0114/19000706
23000 mg/kg D.W.
19
85
SW846: 6010C
MMSD
01/15/19
DM0115/19000742
22000 mg/kg D.W.
19
86
SW846: 6010C
MMSD
01/16/19
DM0116/19000771
23000 mg/kg D.W.
18
85
SW846: 6010C
MMSD
01/17/19
DM0117/19000792
23000 mg/kg D.W.
19
86
SW846: 6010C
MMSD
01/18/19
DM0118/19000812
23000 mg/kg D.W.
18
85
SW846: 6010C
MMSD
01/19/19
DM0119/19000823
25000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
01/21/19
DMO121/19000858
25000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
01/22/19
DMO122/19000920
24000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
01/23/19
DMO123/19000949
27000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
01/24/19
DMO124/19000970
25000 mg/kg D.W.
19
86
SW846: 6010C
MMSD
01/25/19
DMO125/19000986
24000 mg/kg D.W.
19
86
Q2. SW846: 6010C
MMSD
01/26/19
DMO126/19001042
24000 mg/kg D.W.
19
86
SW846: 6010C
MMSD
01/27/19
DMO127/19001062
24000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
01/28/19
01/29/19
DMO128/19001109
DMO129/19001179
24000 mg/kg D.W.
23000 mg/kg D.W.
18
18
82
82
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/30/19
DMO130/19001246
25000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
01/31/19
DMO131/19001267
24000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
Avg Result: 24000 mg/kg D.W.
Min LOD: 18 mg/kg D.W.
Max Result: 27000 mg/kg D.W.
Page 8 of 13
SYSIrptI iloMonthly 1110113 tj Printed.- 211311910:56

414SD
fqt A tiFA1B1 NM�9ANtk"
POTASSIUM ICP METHOD
��aniiiiebaite- —Sa—mpleiliii
Result
LOD
LOQ
QA Flags
Monthly Milorganite Report
January 2019
Analytical Method Lab
01/01/19
DMO101/19000023
4100 mg/kg D.W.
140
740
SW846: 6010C
MMSD
01/02/19
DMO102/19000063
3800 mg/kg D.W.
140
740
SW846: 6010C
MMSD
01/03/19
DMO103/19000237
3800 mg/kg D.W.
140
740
B8.
SW846: 6010C
MMSD
01/04/19
DMO104/19000253
3700 mg/kg D.W.
140
720
B8.
SW846: 6010C
MMSD
01/05/19
DMO105/19000264
4400 mg/kg D.W.
140
730
AO, B8.
SW846: 6010C
MMSD
01/06/19
DMO106/19000284
4100 mg/kg D.W.
140
720
AO, B8.
SW846: 6010C
MMSD
01/07/19
DMO107/19000298
4200 mg/kg D.W.
140
720
AO, B8, Q3.
SW846: 6010C
MMSD
01/08/19
DMO108/19000324
4500 mg/kg D.W.
140
720
AO.
SW846: 6010C
MMSD
01/09/19
DMO109/19000353
4400 mg/kg D.W.
140
740
B8.
SW846: 6010C
MMSD
01/10/19
DM0110/19000588
4200 mg/kg D.W.
140
740
B8, B9.
SW846: 6010C
MMSD
01/11/19
DM0111/19000608
4400 mg/kg D.W.
140
740
B8, B9, Q3.
SW846: 6010C
MMSD
01/12/19
DM0112/19000619
4200 mg/kg D.W.
140
740
B8.
SW846: 6010C
MMSD
01/13/19
DMO113/19000639
4200 mg/kg D.W.
140
750
B8.
SW846: 6010C
MMSD
01/14/19
DM0114/19000706
4400 mg/kg D.W.
140
740
B8.
SW846: 6010C
MMSD
01/15/19
DM0115/19000742
4200 mg/kg D.W.
140
750
B8.
SW846: 6010C
MMSD
01/16/19
DM0116/19000771
4200 mg/kg D.W.
140
740
B8.
SW846: 6010C
MMSD
01/17/19
DMO117/19000792
4500 mg/kg D.W.
140
750
AO, B8, B9.
SW846: 6010C
MMSD
01/18/19
DM0118/19000812
4400 mg/kg D.W.
140
740
AO, B8.
SW846: 6010C
MMSD
01/19/19
DM0119/19000823
4200 mg/kg D.W.
140
740
AO, B8.
SW846: 6010C
MMSD
01/21/19
DMO121/19000858
4000 mg/kg D.W.
140
720
AO, B8.
SW846: 6010C
MMSD
01/22/19
DMO122/19000920
4100 mg/kg D.W.
140
720
B8.
SW846: 6010C
MMSD
01/23/19
DMO123/19000949
4000 mg/kg D.W.
140
740
SW846: 6010C
MMSD
01/24/19
DMO124/19000970
4400 mg/kg D.W.
140
740
SW846: 6010C
MMSD
01/25/19
DM0125/19000986
4300 mg/kg D.W.
140
750
SW846: 6010C
MMSD
01/26/19
DMO126119001042
4500 mg/kg D.W.
140
750
SW846: 6010C
MMSD
01/27/19
DMO127/19001062
4800 mg/kg D.W.
140
730
SW846: 6010C
MMSD
01/28/19
DMO128/19001109
4900 mg/kg D.W.
140
720
SW846: 6010C
MMSD
01/29/19
DMO129/19001179
4900 mg/kg D.W.
140
720
Q2.
SW846: 6010C
MMSD
01/30/19
DMO130/19001246
5300 mg/kg D.W.
140
730
AO, B9.
SW846: 6010C
MMSD
01/31/19
DMO131/19001267
Avg Result: 4300 mg/kg D.W.
5200 mg/kg D.W.
Min LOD:
140 740
140 mg/kg D.W.
AO, B9. SW846: 6010C
Max Result: 5300 mg/kg D.W.
MMSD
Page 9 of 1j
SYS/rptI iloMonthly 1110113 tj Printed: 211311910:56

t
NSD
w x Cl[W �?
SELENIUM ICP METHOD
Sample Date Sample ID
01/01/19 DMO101/19000023
Result
11 mg/kg D.W.
LOD
7
LOQ
21
J.
Monthly Milorganite Report
January 2019
SW846: 6010C MMSD
01/02/19
DMO102/19000063
11 mg/kg D.W.
7
21
J.
SW846: 6010C
MMSD
01/03/19
DMO103/19000237
12 mg/kg D.W.
6.9
21
J.
SW846: 6010C
MMSD
01/04/19
DMO104/19000253
7.5 mg/kg D.W.
6.8
20
J.
SW846: 6010C
MMSD
01/05/19
DMO105/19000264
7.9 mg/kg D.W.
6.8
20
J.
SW846: 6010C
MMSD
01/06/19
DMO106/19000284
8.4 mg/kg D.W.
6.8
20
J.
SW846: 6010C
MMSD
01/07/19
DMO107/19000298
< 6.8 mg/kg D.W.
6.8
20
Q2.
SW846: 6010C
MMSD
01/08/19
DMO108/19000324
8.8 mg/kg D.W.
6.8
20
J.
SW846: 6010C
MMSD
01/09/19
01/10/19
DMO109/19000353
DM0110/19000588
< 7 mg/kg D.W.
< 7 mg/kg D.W.
7
7
21
21
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/11/19
DMO111/19000608
7.4 mg/kg D.W.
7
21
J.
SW846: 6010C
MMSD
01/12/19
DM0112/19000619
< 7 mg/kg D.W.
7
21
SW846: 6010C
MMSD
01/13/19
DM0113/19000639
8.5 mg/kg D.W.
7
21
J.
SW846: 6010C
MMSD
01/14/19
DM0114119000706
< 7 mg/kg D.W.
7
21
Q2.
SW846: 6010C
MMSD
01/15/19
DMO115/19000742
< 7.1 mg/kg D.W.
7.1
21
Q2.
SW846: 6010C
MMSD
01/16/19
DM0116/19000771
< 7 mg/kg D.W.
7
21
SW846: 6010C
MMSD
01/17/19
01/18/19
DM0117/19000792
DM0118/19000812
< 7 mg/kg D.W.
7.4 mg/kg D.W.
7
7
21
21
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/19/19
DM0119/19000823
< 6.9 mg/kg D.W.
6.9
20
SW846: 6010C
MMSD
01/21/19
DMO121/19000858
< 6.7 mg/kg D.W.
6.7
20
SW846: 6010C
MMSD
01/22/19
DMO122/19000920
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
01/23/19
01/24/19
DMO123/19000949
DMO124119000970
< 6.9 mg/kg D.W.
7.4 mg/kg D.W.
6.9
7
20
21
Q2.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/25/19
DMO125/19000986
8.5 mg/kg D.W.
7.1
21
J.
SW846: 6010C
MMSD
01/26/19
DMO126/19001042
< 7 mg/kg D.W.
7
21
SW846: 6010C
MMSD
01/27/19
DMO127/19001062
< 6.9 mg/kg D.W.
6.9
20
SW846: 6010C
MMSD
01/28/19
DMO128/19001109
9.4 mg/kg D.W.
6.8
20
J.
SW846: 6010C
MMSD
01/29/19
DMO129/19001179
< 6.8 mg/kg D.W.
6.8
20
Q2.
SW846: 6010C
MMSD
01/30/19
DMO130/19001246
< 6.9 mg/kg D.W.
6.9
20
SW846: 6010C
MMSD
01/31/19
DMO131/19001267
< 6.9 mg/kg D.W.
6.9
20
D2, Q2.
SW846: 6010C
MMSD
Avg Result: 3.8 mg/kg D.W.
Min LOD: 6.7 mg/kg D.W.
Max Result: 12 mg/kg D.W.
Page 10 o/ n
SYS/rptlMiloMonthly 1110113 t/ Printed: 211311910.56

kNSD
AIIIIIIISNAMAKIIIIIIIIII00
Solids (% Moisture)
Sample •.
.. LOQ .• Flags
Monthly Milorganite Report
January 2019
Analytical Method Lab
Daily Composite
01/01/19 DMO101/19000023
8.6 %
0.1
SM 2540 G (1997)
MMSD
01/02/19 DMO102/19000063
8.4 %
0.1
SM 2540 G (1997)
MMSD
01/03/19 DMO103/19000237
7.8 %
0.1
SM 2540 G (1997)
MMSD
01/04/19 DMO104/19000253
6 %
0.1
SM 2540 G (1997)
MMSD
01/05/19 DM0105/19000264
6.3 %
0.1
SM 2540 G (1997)
MMSD
01/06/19 DMO106/19000284
5.8 %
0.1
SM 2540 G (1997)
MMSD
01/07/19 DMO107/19000298
5.9 %
0.1
SM 2540 G (1997)
MMSD
01/08/19 DM0108/19000324
5.2 %
0.1
SM 2540 G (1997)
MMSD
01/09/19 DMO109/19000353
8.1 %
0.1
SM 2540 G (1997)
MMSD
01/10/19 DMO110/19000588
8.3 %
0.1
SM 2540 G (1997)
MMSD
01/11/19 DMO111/19000608
8.8 %
0.1
SM 2540 G (1997)
MMSD
01/12/19 DM0112/19000619
8.1 %
0.1
SM 2540 G (1997)
MMSD
01/13/19 DMO113/19000639
9.3 %
0.1
SM 2540 G (1997)
MMSD
01/14/19 DM0114/19000706
8.7 %
0.1
SM 2540 G (1997)
MMSD
01/15/19 DM0115/19000742
9.8 %
0.1
SM 2540 G (1997)
MMSD
01/16/19 DM0116/19000771
7.9 %
0.1
SM 2540 G (1997)
MMSD
01/17/19 DM0117/19000792
9.2 %
0.1
SM 2540 G (1997)
MMSD
01/18/19 DM0118/19000812
8.6 %
0.1
SM 2540 G (1997)
MMSD
01/19/19 DM0119/19000823
7.6 %
0.1
SM 2540 G (1997)
MMSD
01/21/19 DMO121/19000858
5 %
0.1
SM 2540 G (1997)
MMSD
01/22/19 DMO122/19000920
5.8 %
0.1
SM 2540 G (1997)
MMSD
01/23/19 DMO123/19000949
7.7 %
0.1
SM 2540 G (1997)
MMSD
01/24/19 DMO124/19000970
8.8 %
0.1
SM 2540 G (1997)
MMSD
01/25/19 DMO125/19000986
9.6 %
0.1
SM 2540 G (1997)
MMSD
01/26/19 DMO126/19001042
9 %
0.1
SM 2540 G (1997)
MMSD
01/27/19 DMO127/19001062
6.8 %
0.1
SM 2540 G (1997)
MMSD
01/28/19 DMO128/19001109
5.3 %
0.1
SM 2540 G (1997)
MMSD
01/29/19 DMO129/19001179
5.5 %
0.1
SM 2540 G (1997)
MMSD
01/30/19 DMO130/19001246
7.5 %
0.1
SM 2540 G (1997)
MMSD
01/31/19 DMO131/19001267
7.7 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 7.6 %
Weekly Composite
01/05/19 WMC01/19000300
Min LOD:
6.8 %
0.1 %
0.1
Max Result: 9.8 %
SM 2540 G (1997)
MMSD
01/12/19 WMCO2/19000708
7.8 %
0.1
SM 2540 G (1997)
MMSD
01/19/19 WMC03/19000860
8.5 %
0.1
SM 2540 G (1997)
MMSD
01/26/19 WMC04/19001111
8.2 %
0.1
SM 2540 G (1997)
MMSD
Solids (% Volatile)
iSample Date Sample ID
Min LOD: 0.1 a/o
Result LOD LOQ .• Flags
Analytical Method
Lab
01/12/19 WMCO2/19000708
72 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 72 %
5Y5/rptlMiloMonthly 1110113 tj
Min LOD:
0.1 a/o
Page 11 of IJ
Printed: 211311910:56

Monthly Milorganite Report
January 2019
si�excwe�a
ZINC ICP METHOD
a pie.. •. ..
01/01/19 DMO101/19000023 460 mg/kg D.W. 16 48 SW846: 6010C MMSD
01/02/19
DMO102/19000063
450 mg/kg D.W.
16
48
SW846: 6010C
MMSD
01/03/19
DMO103/19000237
450 mg/kg D.W.
16
48
SW846: 6010C
MMSD
01/04/19
DMO104119000253
430 mg/kg D.W.
16
47
SW846: 6010C
MMSD
01/05/19
DMO105/19000264
410 mg/kg D.W.
16
47
SW846: 6010C
MMSD
01/06/19
DMO106/19000284
410 mg/kg D.W.
16
47
SW846: 6010C
MMSD
01/07/19
DMO107/19000298
420 mg/kg D.W.
16
47
SW846: 6010C
MMSD
01/08/19
DMO108/19000324
420 mg/kg D.W.
16
46
SW846: 6010C
MMSD
01/09/19
01/10/19
DMO109/19000353
DM0110/19000588
420 mg/kg D.W.
410 mg/kg D.W.
16
16
48
48
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/11/19
DMO111/19000608
430 mg/kg D.W.
16
48
SW846: 6010C
MMSD
01/12/19
DM0112/19000619
430 mg/kg D.W.
16
48
SW846: 6010C
MMSD
01/13/19
DM0113/19000639
430 mg/kg D.W.
16
48
SW846: 6010C
MMSD
01/14/19
DM0114/19000706
420 mg/kg D.W.
16
48
SW846: 6010C
MMSD
01/15/19
DMO115/19000742
420 mg/kg D.W.
17
49
SW846: 6010C
MMSD
01/16/19
DMO116/19000771
430 mg/kg D.W.
16
48
SW846: 6010C
MMSD
01/17/19
01/18/19
DM0117119000792
DM0118/19000812
410 mg/kg D.W.
410 mg/kg D.W.
16
16
48
48
SW846: 6010C
SW846: 6010C
MMSD
MMSD
01/19/19
DM0119/19000823
430 mg/kg D.W.
16
48
SW846: 6010C
MMSD
01/21/19
DMO121/19000858
420 mg/kg D.W.
16
46
SW846: 6010C
MMSD
01/22/19
DMO122/19000920
400 mg/kg D.W.
16
47
SW846: 6010C
MMSD
01/23/19
01/24/19
01/25/19
DMO123/19000949
DMO124/19000970
DMO125/19000986
450 mg/kg D.W.
420 mg/kg D.W.
410 mg/kg D.W.
16
16
16
48
48
49
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
01/26/19
01/27/19
01/28/19
DMO126/19001042
DMO127/19001062
DMO128/19001109
410 mg/kg D.W.
400 mg/kg D.W.
390 mg/kg D.W.
16
16
16
48
47
46
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
01/29/19
DMO129/19001179
380 mg/kg D.W.
16
46
SW846: 6010C
MMSD
01/30/19
DMO130/19001246
410 mg/kg D.W.
16
48
SW846: 6010C
MMSD
01/31/19
DMO131/19001267
Avg Result: 420 mg/kg D.W.
410 mg/kg D.W.
Min LOD:
16 48
16 mg/kg D.W.
SW846: 6010C
Max Result: 460 mg/kg D.W.
MMSD
Page 12 of 13
5Y5/rptlMiloMonthly 1110113 tj Printed: 211311910:56

fTlt;ti itN s4 tlZutl�
Flag Descriptions
AO Other -- Flag requires additional explanation
AX Qualified data - see contract lab report
63 Target analyte detected in method blank > 10% of sample
concentration.
87 LCS recovery was above control limits.
68 LCS recovery was below control limits.
89 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
D1 Duplicate precision control limit was exceeded.
02 Matrix spike precision control limit was exceeded.
03 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
H1 Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
Monthly Milorganite Report
January 2019
IS Insufficient sample volume for analysis.
] Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
LA Not analyzed - lab accident.
M1 Too numerous to count.
142 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
M5 Incubator/water bath temperature was outside method
requirements.
M7 Micro sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
SS Reading was not confirmed by a constant weight measurement
SD Supplemental details provided.(Water Quality only.)
T3 The dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample exceeded prescribed method temperature range.
Page 13 of 15
5Y51rpt1MWbMonth/y 1110113 tlPrinted. 211311910.56

SNNSD
PARTNERS FOR A CLEANER ENVIRONMENT
March 12, 2019
Memorandum
TO: Todd Schwingle, Dion Doege, Jacob Holbert, Brett Kelly, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Jaime Staufenbeil, Tom Nowicki, Beth Stroik, Kori
Kenney, Lab File
SUBJECT: Milorganite Monthly Data — February 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of February
2019. The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin
(Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
i�f11/�rri?.Rof� //9
Richard Vincent Date
Laboratory Team Supervisor
Report Review By:
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

r
I fANSD
ALUMINUM ICP Dry wt.
Is
ample Date Sample ID
02/09/19 WMC06/19002209
Result
4900 mg/kg D.W.
86
QA Flags
240 B8.
Monthly Milorganite Report
February 2019
Analytical Method Lab
SW846: 6010C MMSD
Avg Result: 4900 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Date Sample ID
Min LOD: 86 mg/kg D.W.
Result LOD LOQ QA Flags
Analytical Method
Lab
'Sample
02/09/19 WMC06/19002209
0.22 %
0.11
AOAC (13) 2.065
MMSD
Avg Result: 0.22 O/o
ARSENIC ICP METHOD
Date Sample ID
Min LOD: 0.110/6
Result LOD
LOQ QA Flags
Analytical Method
Lab
02/01/19 DM0201/19001283
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
02/02/19 DM0202/19001320
< 6.2 mg/kg D.W.
6.2
19
SW846: 6010C
MMSD
02/03/19 DM0203/19001774
< 6.2 mg/kg D.W.
6.2
19
SW846: 6010C
MMSD
02/04/19 DM0204/19001791
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
02/05/19 DM0205/19001816
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
02/06/19 DM0206/19001845
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/07/19 DM0207/19001867
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
02/08/19 DM0208/19001883
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/09/19 DM0209/19001894
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
02/10/19 DM0210/19002088
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
02/11/19 DM0211/19002207
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/12/19 DM0212/19002232
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
02/13/19 DM0213/19002261
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
02/14/19 DM0214/19002348
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
02/15/19 DM0215/19002364
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/16/19 DM0216/19002447
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
02/17/19 DM0217/19002467
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/18/19 DM0218/19002490
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/19/19 DM0219/19002563
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/20/19 DM0220/19002596
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/21/19 DM0221/19002617
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/22/19 DM0222/19002632
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/23/19 DM0223/19002643
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
02/24/19 DM0224/19002662
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
02/25/19 DM0225/19002675
02/26/19 DM0226/19002702
< 6.3 mg/kg D.W.
< 6.3 mg/kg D.W.
6.3
6.3
19 Q3.
19
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/27/19 DM0227/19002767
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
02/28/19 DM0228/19002788
Avg Result: 0 mg/kg D.W.
BORON ICP Dry wt.
Sample Date Sample ID
< 6.4 mg/kg D.W. 6.4 19
Min LOD: 6.2 mg/kg D.W.
Result LOD LOQ QA Flags
SW846: 6010C
Analytical Method
MMSD
Lab
02/09/19 WMC06/19002209
18 mg/kg D.W.
1.1
3.5
SW846: 6010C
CT Lab
Avg Result: 18 mg/kg D.W.
Min LOD:
1.1 mg/kg D.W.
SYS/rp"Milom- ly 1110113 U
Page I of 13
Printed: 311211910:1j

If'kIMSD
NAlIBS N! �I pf�
CADMIUM ICP METHOD
Sample Date S I ample ID
Result
LOD
LOQ QA
Flags
Monthly Milorganite Report
February 2019
Analytic
02/01/19
DM0201/19001283
0.65 mg/kg D.W.
0.29
1.4
J.
SW846: 6010C
MMSD
02/02/19
DM0202/19001320
0.53 mg/kg D.W.
0.29
1.4
J.
SW846: 6010C
MMSD
02/03/19
DM0203/19001774
0.57 mg/kg D.W.
0.29
1.4
J.
SW846: 6010C
MMSD
02/04/19
DM0204119001791
0.52 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
02/05/19
DM0205/19001816
< 0.3 mg/kg D.W.
0.3
1.4
SW846: 6010C
MMSD
02/06/19
DM0206/19001845
< 0.3 mg/kg D.W.
0.3
1.4
SW846: 6010C
MMSD
02/07/19
DM0207/19001867
< 0.3 mg/kg D.W.
0.3
1.4
SW846: 6010C
MMSD
02/08/19
DM0208/19001883
0.46 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
02/09/19
02/10/19
DM0209/19001894
DM0210/19002088
< 0.3 mg/kg D.W.
0.42 mg/kg D.W.
0.3
0.3
1.4
1.4
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/11/19
DM0211/19002207
< 0.3 mg/kg D.W.
0.3
1.4
SW846: 6010C
MMSD
02/12/19
DM0212/19002232
0.45 mg/kg D.W.
0.31
1.4
J.
SW846: 6010C
MMSD
02/13/19
DM0213/19002261
0.32 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
02/14/19
DM0214/19002348
0.65 mg/kg D.W.
0.3
1.4
1.
SW846: 6010C
MMSD
02/15/19
DM0215/19002364
0.49 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
02/16/19
DM0216/19002447
0.52 mg/kg D.W.
0.31
1.4
J.
SW846: 6010C
MMSD
02/17/19
02/18/19
DM0217/19002467
DM0218/19002490
0.64 mg/kg D.W.
0.57 mg/kg D.W.
0.3
0.3
1.4
1.4
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/19/19
DM0219/19002563
0.5 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
02/20/19
DM0220/19002596
0.46 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
02/21/19
DM0221/19002617
0.55 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
02/22/19
02/23/19
DM0222/19002632
DM0223/19002643
0.58 mg/kg D.W.
0.58 mg/kg D.W.
0.3
0.3
1.4
1.4
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/24/19
DM0224/19002662
0.56 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
02/25/19
DM0225/19002675
0.5 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
02/26/19
DM0226/19002702
0.53 mg/kg D.W.
0.29
1.4
1.
SW846: 6010C
MMSD
02/27/19
DM0227/19002767
0.58 mg/kg D.W.
0.29
1.4
1
SW846: 6010C
MMSD
02/28/19
DM0228/19002788
0.53 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
Avg Result: 0.43 mg/kg D.W.
CHROMIUM ICP Dry wt.
Sample Date Sample ID
Min LOD: 0.29 mg/kg D.W.
Result LOD LOQ QA
Flags
Max Result: 0.65 mg/kg D.W.
Analytical Method
Lab
02/09/19
WMC06/19002209
230 mg/kg D.W.
1.4
4.3
SW846: 6010C
MMSD
Avg Result: 230 mg/kg D.W.
COBALT ICP Dry wt.
Sample Date Sample ID
Min LOD: 1.4 mg/kg D.W.
Result LOD L•• .•A�gs
Analytical Method
Lab
02/09/19
WMC06/19002209
3.8 mg/kg D.W.
1.2
3.4
B8.
SW846: 6010C
MMSD
Avg Result: 3.8 mg/kg D.W.
Min LOD: 1.2 mg/kg D.W.
Page 1 of 13
5Y51rpt1M116Month/y 1110113 tj Printed.• 311211910:23

' fkNSD
tilt A CtW
COPPER ICP METHOD
�Sample Date Sample ID
Result
LOD
LOQ
QA Flags
Monthly Milorganite Report
February 2019
Analytical MethGd Lab
02/01/19
DM0201/19001283
240 mg/kg D.W.
7.5
23
SW846: 6010C
MMSD
02/02/19
DM0202/19001320
230 mg/kg D.W.
7.5
23
SW846: 6010C
MMSD
02/03/19
DM0203/19001774
220 mg/kg D.W.
7.5
23
SW846: 6010C
MMSD
02/04/19
DM0204/19001791
230 mg/kg D.W.
7.9
24
SW846: 6010C
MMSD
02/05/19
DM0205/19001816
240 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
02/06/19
DM0206/19001845
240 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
02/07/19
DM0207/19001867
230 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
02/08/19
DM0208/19001883
220 mg/kg D.W.
7.7
24
SW846: 6010C
MMSD
02/09/19
DM0209/19001894
220 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
02/10/19
DM0210/19002088
220 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
02/11/19
DM0211/19002207
220 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
02/12/19
DM0212/19002232
220 mg/kg D.W.
7.9
24
SW846: 6010C
MMSD
02/13/19
DM0213/19002261
220 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
02/14/19
DM0214/19002348
210 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
02/15/19
DM0215/19002364
210 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
02/16/19
DM0216/19002447
240 mg/kg D.W.
7.9
24
SW846: 6010C
MMSD
02/17/19
DM0217/19002467
240 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
02/18/19
DM0218/19002490
240 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
02/19/19
DM0219/19002563
220 mg/kg D.W.
7.7
23
SW846: 6010C
MMSD
02/20/19
DM0220/19002596
210 mg/kg D.W.
7.7
23
SW846: 6010C
MMSD
02/21/19
DM0221/19002617
200 mg/kg D.W.
7.7
23
SW846: 6010C
MMSD
02/22/19
DM0222/19002632
200 mg/kg D.W.
7.7
24
SW846: 6010C
MMSD
02/23/19
DM0223119002643
180 mg/kg D.W.
7.6
23
B8.
SW846: 6010C
MMSD
02/24/19
DM0224/19002662
180 mg/kg D.W.
7.8
24
B8.
SW846: 6010C
MMSD
02/25/19
DM0225/19002675
180 mg/kg D.W.
7.6
23
B8.
SW846: 6010C
MMSD
02/26/19
DM0226/19002702
200 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
02/27/19
DM0227/19002767
200 mg/kg D.W.
7.6
23
B8.
SW846: 6010C
MMSD
02/28/19
DM0228/19002788
210 mg/kg D.W.
7.7
24
SW846: 6010C
MMSD
Avg Result: 220 mg/kg D.W.
FECAL COLIFORM SLUDGE
Date Sample ID
Min LOD: 7.5 mg/kg D.W.
Result LOD LOQ
..
Max Result: 240 mg/kg D.W.
02/05/19
MF/19002288
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
02/12/19
MF/19002742
< 0.2 MPN/g TS
0.2
EPA 1680
MMSD
02/19/19
02/26/19
MF/19003247
MF/19003732
< 0.19 MPN/g TS
< 0.19 MPN/g TS
0.19
0.19
D2.
EPA 1680
EPA 1680
MMSD
MMSD
Min LOD:
0.19 MPN/g TS
Page 3 of 1j
SYS/rytlMiloMonthly 1/10/13 f% Printed: 311211910:2i

Monthly Milorganite Report
IMSD February 2019
Au111i9t4 IOt A tltAi61
IRON ICP METHOD
Sample bate Sample ID
Result
LOD
LOQ •
02/01/19
DM0201/19001283
46000 mg/kg D.W.
250
730
SW846: 6010C
MMSD
02/02/19
DM0202/19001320
47000 mg/kg D.W.
250
730
SW846-.6010C
MMSD
02/03/19
DM0203/19001774
45000 mg/kg D.W.
250
730
SW846: 6010C
MMSD
02/04/19
DM0204/19001791
44000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
02/05/19
DM0205/19001816
44000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
02/06/19
DM0206/19001845
46000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
02/07/19
DM0207/19001867
44000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
02/08/19
DM0208/19001883
39000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
02/09/19
02/10/19
DM0209/19001894
DM0210/19002088
40000 mg/kg D.W.
40000 mg/kg D.W.
260
250
760
740
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/11/19
DM0211/19002207
36000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
02/12/19
DM0212/19002232
39000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
02/13/19
DM0213/19002261
39000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
02/14/19
DM0214/19002348
46000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
02/15/19
DM0215/19002364
52000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
02/16/19
DM0216/19002447
47000 mg/kg D.W.
260
770
SW846: 6010C
MMSD
02/17/19
02/18/19
DM0217/19002467
DM0218/19002490
46000 mg/kg D.W.
44000 mg/kg D.W.
250
250
740
740
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/19/19
DM0219/19002563
39000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
02/20/19
DM0220/19002596
37000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
02/21/19
DM0221/19002617
41000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
02/22/19
02/23/19
DM0222/19002632
DM0223/19002643
41000 mg/kg D.W.
36000 mg/kg D.W.
260
260
750
740
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/24/19
02/25/19
DM0224/19002662
DM0225/19002675
36000 mg/kg D.W.
36000 mg/kg D.W.
260
250
760
740
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/26/19
DM0226/19002702
33000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
02/27/19
DM0227/19002767
30000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
02/28/19
DM0228/19002788
27000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
Avg Result: 41000 mg/kg D.W.
Min LOD:
250 mg/kg
D.W.
Max Result: 52000 mg/kg D.W.
Page 4 of 13
SY5/rptlMiloMonth/y 1110113 tj Pnnted.• 311211910.23

i!Itt�S F6t � pl:+ua
LEAD ICP METHOD
Date Sample ID
Result
LOD
LOQ QA Flags
Monthly Milorganite Report
February 2019
Analytical Method Lab
02/01/19
DM0201/19001283
27 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/02/19
DM0202/19001320
28 mg/kg D.W.
4.6
14
SW846-.6010C
MMSD
02/03/19
DM0203/19001774
24 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/04/19
DM0204/19001791
23 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
02/05/19
DM0205/19001816
24 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/06/19
DM0206/19001845
25 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/07/19
DM0207/19001867
32 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
02/08/19
DM0208/19001883
27 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
02/09/19
DM0209/19001894
33 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
02/10/19
DM0210/19002088
31 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/11/19
DM0211/19002207
32 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/12/19
DM0212/19002232
30 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
02/13/19
DM0213/19002261
28 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
02/14/19
DM0214/19002348
29 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
02/15/19
DM0215/19002364
30 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
02/16/19
DM0216119002447
28 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
02/17/19
DM0217/19002467
30 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
02/18/19
DM0218/19002490
30 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
02/19/19
DM0219/19002563
27 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
02/20/19
DM0220119002596
29 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
02/21/19
DM0221/19002617
28 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
02/22/19
DM0222/19002632
28 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
02/23/19
DM0223/19002643
28 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
02/24/19
DM0224/19002662
27 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
02/25/19
DM0225/19002675
29 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/26/19
DM0226119002702
32 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/27/19
DM0227/19002767
30 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/28/19 DM0228/19002788
Avg Result: 28 mg/kg D.W.
MERCURY by M. 7471 (sludge)
Sample ..
30 mg/kg D.W. 4.7 14
Min LOD: 4.6 mg/kg D.W.
.. .. .. Flags
SW846: 6010C
Max Result: 33 mg/kg D.W.
A lytical Method
MMSD
Lab
02/02/19
WMC05/19001793
0.12 mg/kg D.W.
0.0058
0.02 AX.
EPA 7471E
CT Lab
02/09/19
WMC06/19002209
0.29 mg/kg D.W.
0.0058
0.02
EPA 7471E
CT Lab
02/16/19
WMC07/19002492
0.031 mg/kg D.W.
0.0056
0.019
EPA 7471B
CT Lab
02/23/19
WMC08/19002679
0.09 mg/kg D.W.
0.0058
0.02
EPA 7471B
CT Lab
Avg Result: 0.13 mg/kg D.W. Min LOD: 0.0056 mg/kg D.W. Max Result: 0.29 mg/kg D.W.
Page S of I3
SYS1rptlM11oMonth/y 1/10/13 tj Pdnted: 311211910:2i

kNSD
i1R311{RS Rw a CRW FV KIIWIV'
MOLYBDENUM ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ .•
Monthly Milorganite Report
February 2019
02/01/19
DM0201119001283
11 mg/kg D.W.
1.2
5.4
SW846: 6010C
MMSD
02/02/19
DM0202/19001320
11 mg/kg D.W.
1.2
5.4
SW846: 6010C
MMSD
02/03/19
DM0203/19001774
10 mg/kg D.W.
1.2
5.4
SW846: 6010C
MMSD
02/04/19
DM0204/19001791
11 mg/kg D.W.
1.3
5.7
SW846: 6010C
MMSD
02/05/19
DM0205/19001816
10 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
02/06/19
DM0206/19001845
10 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
02/07/19
DM0207/19001867
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
02/08/19
DM0208119001883
9.6 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
02/09/19
02/10/19
DM0209/19001894
DM0210119002088
9.4 mg/kg D.W.
9.7 mg/kg D.W.
1.3
1.3
5.6
5.5
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/11/19
DM0211/19002207
9.4 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
02/12/19
DM0212/19002232
9.3 mg/kg D.W.
1.3
5.7
SW846: 6010C
MMSD
02/13/19
DM0213/19002261
9.6 mg/kg D.W.
1.3
5.7
SW846: 6010C
MMSD
02/14/19
DM0214/19002348
9.9 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
02/15/19
DM0215/19002364
9.7 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
02/16/19
DM0216/19002447
11 mg/kg D.W.
1.3
5.7
SW846: 6010C
MMSD
02/17/19
02/18/19
DM0217/19002467
DM0218119002490
11 mg/kg D.W.
10 mg/kg D.W.
1.3
1.3
5.5
5.5
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/19/19
DM0219/19002563
9.8 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
02/20/19
DM0220/19002596
9.2 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
02/21/19
DM0221/19002617
9.2 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
02/22/19
02/23/19
DM0222/19002632
DM0223/19002643
9.2 mg/kg D.W.
8.3 mg/kg D.W.
1.3
1.3
5.6
5.5
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/24/19
DM0224/19002662
8.4 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
02/25/19
DM0225/19002675
8.6 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
02/26/19
DM0226/19002702
9.2 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
02/27/19
DM0227/19002767
8.6 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
02/28/19
DM0228/19002788
8.6 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
Avg Result: 9.7 mg/kg O.W.
Min LOD: 1.2 mg/kg D.W.
Max Result: it mg/kg D.W.
Page 6 of 13
SYS/rotlMiloMonthly 1110113 tj Printed., 3112119 10:7J

k11SD
IstalAa€�letno
NICKEL ICP METHOD
Date Sample ID
Result
LOD
LOQ QA Flags
Monthly Milorganite Report
February 2019
Analytical Method Lab
02/01/19
DM0201/19001283
27 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/02/19
DM0202119001320
28 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/03/19
DM0203/19001774
26 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/04/19
DM0204/19001791
27 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/05/19
DM0205/19001816
27 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/06/19
DM0206/19001845
26 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/07/19
DM0207/19001867
27 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/08/19
DM0208/19001883
25 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
02/09/19
DM0209/19001894
24 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/10/19
DM0210/19002088
26 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/11/19
DM0211119002207
26 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/12/19
DM0212/19002232
25 mg/kg D.W.
4.6
14
5W846: 6010C
MMSD
02/13/19
DM0213/19002261
25 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/14/19
DM0214/19002348
28 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/15/19
DM0215/19002364
30 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
02/16/19
DM0216/19002447
26 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/17/19
DM0217/19002467
27 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
02/18/19
DM0218/19002490
28 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/19/19
DM0219/19002563
28 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
02/20/19
DM0220/19002596
26 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
02/21/19
DM0221/19002617
29 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
02/22/19
02/23/19
DM0222/19002632
DM0223/19002643
28 mg/kg D.W.
25 mg/kg D.W.
4.5
4.5
14
14
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/24/19
DM0224/19002662
25 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
02/25/19
DM0225/19002675
25 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/26/19
DM0226119002702
26 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/27/19
DM0227/19002767
23 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
02/28/19
DM0228/19002788
23 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
Avg Result: 26 mg/kg D.W.
Min LOD: 4.4 mg/kg D.W.
Max Result: 30 mg/kg D.W.
NITRATE NITROGEN
Date Sani 113,
Result
ample
02/09/19 WMC06/19002209
LOD LOQ QA Flags
0.72 % 0.5
Analytical Method Lab
AOAC (16) 930.01 MMSD
Avg Result: 0.72 %
Min LOD: 0.5
NITROGEN-Total(Manual)
Sample Date Sample ID
Result LOD LGQ Flags
Analytical Method Lab
02/09/19 WMC06/19002209
QA
6.2 % 0.11
AOAC (16) 955.04 MMSD
Avg Result: 6.2 "/o
Min LOD: 0.11 "/o
NITROGEN -Water Insoluble
Sample Date Sample ID
Result LOD LOQ Q
Analytical Method Lab
02/09/19 WMC06/19002209
4.7 % 0.5
AOAC (16) 945.01 MMSD
Avg Result: 4.7 % Min LOD: 0.5 0/6
Page7ofli
SYS/rpt1Mi1bMonfhh 1/10/13 t% Printed: 311211910:23

�t'IkNSD
IfM R A Ci At6E
pH -Solids
Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report
February 2019
QA Flags Analytical Method La
02/02/19
WMC05/19001793
6.25 Stnd. Units
0.1
SW846: 9045D
MMSD
02/09/19
WMC06/19002209
6.24 Stnd. Units
0.1
SW846: 9045D
MMSD
02/16/19
WMC07/19002492
6.2 Stnd. Units
0.1
SW846: 9045D
MMSD
02/23/19
WMC08/19002679
6.24 Stnd. Units
0.1
SW846: 9045D
MMSD
Avg Result: 6.2 Stnd. Units
PHOSPHORUS ICP METHOD
Sample Date Sample ID
Min LOD: 0.1 Stnd. Units
Result LOD LOQ
Max Result: 6.25 Stnd. Units
.. Flags Analytical Method
Lab
02/01/19
DM0201/19001283
26000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
02/02/19
DM0202/19001320
26000 mg/kg D.W.
18
81
SW846: 6010C
MMSD
02/03/19
DM0203/19001774
25000 mg/kg D.W.
18
81
SW846: 6010C
MMSD
02/04/19
DM0204/19001791
24000 mg/kg D.W.
18
85
SW846: 6010C
MMSD
02/05/19
02/06/19
DM0205/19001816
DM0206/19001845
25000 mg/kg D.W.
24000 mg/kg D.W.
18
18
82
82
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/07/19
DM0207/19001867
25000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
02/08/19
DM0208/19001883
24000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
02/09/19
DM0209/19001894
22000 mg/kg D.W.
18
85
SW846: 6010C
MMSD
02/10/19
DM0210/19002088
22000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
02/11/19
DM0211/19002207
22000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
02/12/19
02/13/19
DM0212/19002232
DM0213/19002261
22000 mg/kg D.W.
22000 mg/kg D.W.
18
18
85
85
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/14/19
DM0214/19002348
24000 mg/kg D.W.
18
85
SW846: 6010C
MMSD
02/15/19
DM0215119002364
24000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
02/16/19
DM0216/19002447
25000 mg/kg D.W.
19
86
SW846: 6010C
MMSD
02/17/19
DM0217/19002467
26000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
02/18/19
DM0218/19002490
26000 mg/kg D.W.
18
83
Q2. SW846: 6010C
MMSD
02/19/19
DM0219/19002563
24000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
02/20/19
DM0220/19002596
24000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
02/21/19
DM0221/19002617
23000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
02/22/19
DM0222/19002632
23000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
02/23/19
DM0223/19002643
22000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
02/24/19
DM0224/19002662
22000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
02/25/19
DM0225/19002675
21000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
02/26/19
DM0226/19002702
23000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
02/27/19
02/28/19
DM0227119002767
DM0228/19002788
22000 mg/kg D.W.
22000 mg/kg D.W.
18
18
82
84
SW846: 6010C
SW846: 6010C
MMSD
MMSD
Avg Result: 24000 mg/kg D.W.
Min LOD:
18 mg/kg D.W.
Max Result: 26000 mg/kg D.W.
Page 8ofl3
SYSlipUN11oMonihly 1110113 ti Printed. 3112/1910.23

i
! NOOD
Pull" FRI I LUUR Rf"WN'
POTASSIUM ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ
QA Flags
Monthly Milorganite Report
February 2019
Analytical MethGd Lab
02/01/19
DM0201/19001283
4000 mg/kg D.W.
140
710
AO.
SW846: 6010C
MMSD
02/02/19
DM0202/19001320
3800 mg/kg D.W.
140
710
B8, B9.
SW846: 6010C
MMSD
02/03/19
DM0203/19001774
4000 mg/kg D.W.
140
710
B8, B9.
SW846: 6010C
MMSD
02/04/19
DM0204/19001791
4100 mg/kg D.W.
140
740
B8, B9, Q3.
SW846: 6010C
MMSD
02/05/19
DM0205/19001816
4000 mg/kg D.W.
140
720
88.
SW846: 6010C
MMSD
02/06/19
DM0206/19001845
4400 mg/kg D.W.
140
720
SW846: 6010C
MMSD
02/07/19
DM0207/19001867
4300 mg/kg D.W.
140
740
AO, B9.
SW846: 6010C
MMSD
02/08/19
DM0208/19001883
3700 mg/kg D.W.
140
730
B8, Q3.
SW846: 6010C
MMSD
02/09/19
DM0209119001894
4600 mg/kg D.W.
140
740
AO, BB, B9.
SW846: 6010C
MMSD
02/10/19
DM0210/19002088
4400 mg/kg D.W.
140
720
AD, B8, B9.
SW846: 6010C
MMSD
02/11/19
DM0211/19002207
4500 mg/kg D.W.
140
720 AO, B8, B9, Q3. SW846: 6010C
MMSD
02/12/19
DM0212/19002232
4600 mg/kg D.W.
140
740
B8.
SW846: 6010C
MMSD
02/13/19
DM0213/19002261
4400 mg/kg D.W.
140
740
B8.
SW846: 6010C
MMSD
02/14/19
DM0214/19002348
4200 mg/kg D.W.
140
740
B8.
SW846: 6010C
MMSD
02/15/19
DM0215/19002364
4300 mg/kg D.W.
140
730
SW846: 6010C
MMSD
02/16/19
DM0216/19002447
5000 mg/kg D.W.
140
750
AO.
SW846: 6010C
MMSD
02/17/19
02/18/19
DM0217/19002467
DM0218/19002490
4800 mg/kg D.W.
4900 mg/kg D.W.
140
140
720
720
AO.
AO.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/19/19
DM0219/19002563
5400 mg/kg D.W.
140
720
AO, B9, Q3.
SW846: 6010C
MMSD
02/20/19
DM0220/19002596
5100 mg/kg D.W.
140
720
AO, B9.
SW846: 6010C
MMSD
02/21/19
02/22/19
02/23/19
02/24/19
02/25/19
DM0221/19002617
DM0222/19002632
DM0223/19002643
DM0224/19002662
DM0225/19002675
4500 mg/kg D.W.
4700 mg/kg D.W.
4500 mg/kg D.W.
4600 mg/kg D.W.
4600 mg/kg D.W.
140
140
140
140
140
720
730
720
740
720
B8.
88.
88.
B8, Q3.
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
MMSD
02/26/19
02/27/19
02/28/19
DM0226/19002702
DM0227/19002767
DM0228/19002788
Avg Result: 4500 mg/kg D.W.
5300 mg/kg D.W. 140 720
5200 mg/kg D.W. 140 720
5000 mg/kg D.W. 140 730
Min LOD: 140 mg/kg D.W.
AO, B8. SW846: 6010C
AO, B8. SW846: 6010C
AO, B8. SW846: 6010C
Max Result: 5400 mg/kg D.W.
MMSD
MMSD
MMSD
SY5/rptl MiloMonthly V10/13 tj
Page 9 orlj
Printed. 311211910:2i

°'tiNSD
Ptlti1lels a A MAN BiAIONiBit
SELENIUM ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ
QA Flags
Monthly Milorganite Report
February 2019
Analytical Method Lab
02/01/19
DM0201/19001283
< 6.7 mg/kg D.W.
6.7
20
Q2.
SW846: 6010C
MMSD
02/02/19
DM0202/19001320
7.7 mg/kg D.W.
6.6
20
].
SW846: 6010C
MMSD
02/03/19
DM0203/19001774
< 6.6 mg/kg D.W.
6.6
20
SW846: 6010C
MMSD
02/04/19
DM0204/19001791
7.3 mg/kg D.W.
7
21
J.
SW846: 6010C
MMSD
02/05/19
DM0205/19001816
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
02/06/19
DM0206/19001845
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
02/07/19
DM0207/19001867
< 6.9 mg/kg D.W.
6.9
21
SW846: 6010C
MMSD
02/08/19
DM0208/19001883
8.2 mg/kg D.W.
6.9
20
J.
SW846: 6010C
MMSD
02/09/19
02/10/19
DM0209/19001894
DM0210/19002088
< 7 mg/kg D.W.
< 6.7 mg/kg D.W.
7
6.7
21
20
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/11/19
DM0211/19002207
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
02/12/19
DM0212/19002232
< 7 mg/kg D.W.
7
21
SW846: 6010C
MMSD
02/13/19
DM0213/19002261
< 7 mg/kg D.W.
7
21
SW846: 6010C
MMSD
02/14/19
DM0214/19002348
< 7 mg/kg D.W.
7
21
SW846: 6010C
MMSD
02/15/19
DM0215/19002364
10 mg/kg D.W.
6.9
20
J.
SW846: 6010C
MMSD
02/16/19
DM0216/19002447
< 7 mg/kg D.W.
7
21
SW846: 6010C
MMSD
02/17/19
02/18/19
DM0217/19002467
DM0218/19002490
< 6.8 mg/kg D.W.
< 6.8 mg/kg D.W.
6.8
6.8
20
20
Q2.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/19/19
DM0219/19002563
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
02/20/19
DM0220/19002596
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
02/21/19
02/22/19
02/23/19
02/24/19
DM0221/19002617
DM0222/19002632
DM0223/19002643
DM0224/19002662
10 mg/kg D.W.
7.4 mg/kg D.W.
< 6.8 mg/kg D.W.
< 6.9 mg/kg D.W.
6.8
6.8
6.8
6.9
20
20
20
20
J.
J.
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
02/25/19
DM0225/19002675
8.2 mg/kg D.W.
6.7
20
J.
SW846: 6010C
MMSD
02/26/19
DM0226/19002702
< 6.7 mg/kg D.W.
6.7
20
SW846: 6010C
MMSD
02/27/19
DM0227119002767
< 6.7 mg/kg D.W.
6.7
20
SW846: 6010C
MMSD
02/28/19
DM0228/19002788
< 6.9 mg/kg D.W.
6.9
20
SW846: 6010C
MMSD
Avg Result: 2.1 mg/kg D.W. Min LOD: 6.6 mg/kg D.W. Max Result: 10 mg/kg D.W.
Page 10 of 15
SYS/rptJH&Monthty 1/10/13 tj Printed.• 311211910:13

"IfkNSD
IM A MAN
Solids (% Moisture)
Sample Date "e
Result
LOD
Monthly Milorganite Report
February 2019
LOQ QA Flags Analytical Method Lab
Daily Composite
02/01/19 DM0201/19001283
4.6 %
0.1
SM 2540 G (1997)
MMSD
02/02/19 DM0202/19001320
3.8 %
0.1
SM 2540 G (1997)
MMSD
02/03/19 DM0203/19001774
3.7 %
0.1
SM 2540 G (1997)
MMSD
02/04/19 DM0204/19001791
8.4 %
0.1
SM 2540 G (1997)
MMSD
02/05/19 DM0205/19001816
5.2 %
0.1
SM 2540 G (1997)
MMSD
02/06/19 DM0206/19001845
02/07/19 DM0207/19001867
5.5 %
7.8 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
02/08/19 DM0208/19001883
7 %
0.1
SM 2540 G (1997)
MMSD
02/09/19 DM0209/19001894
8 %
0.1
SM 2540 G (1997)
MMSD
02/10/19 DM0210/19002088
5.1 %
0.1
SM 2540 G (1997)
MMSD
02/11/19 DM0211/19002207
5.5 %
0.1
SM 2540 G (1997)
MMSD
02/12/19 DM0212/19002232
8.6 %
0.1
DI. SM 2540 G (1997)
MMSD
02/13/19 DM0213/19002261
8.2 %
0.1
SM 2540 G (1997)
MMSD
02/14/19 DM0214/19002348
8 %
0.1
SM 2540 G (1997)
MMSD
02/15/19 DM0215/19002364
7.1 %
0.1
SM 2540 G (1997)
MMSD
02/16/19 DM0216/19002447
8.9 %
0.1
SM 2540 G (1997)
MMSD
02/17/19 DM0217/19002467
5.8 %
0.1
SM 2540 G (1997)
MMSD
02/18/19 DM0218/19002490
S.8 %
0.1
SM 2540 G (1997)
MMSD
02/19/19 DM0219/19002563
6.3 %
0.1
SM 2540 G (1997)
MMSD
02/20/19 DM0220/19002596
6.3 %
0.1
SM 2540 G (1997)
MMSD
02/21/19 DM0221/19002617
6.3 %
0.1
SM 2540 G (1997)
MMSD
02/22/19 DM0222119002632
6.7 %
0.1
SM 2540 G (1997)
MMSD
02/23/19 DM0223/19002643
5.9 %
0.1
SM 2540 G (1997)
MMSD
02/24/19 DM0224/19002662
7.8 %
0.1
SM 2540 G (1997)
MMSD
02/25/19 DM0225/19002675
5.1 %
0.1
SM 2540 G (1997)
MMSD
02/26/19 DM0226/19002702
4.9 %
0.1
SM 2540 G (1997)
MMSD
02/27/19 DM0227/19002767
4.9 % 0.1
SM 2540 G (1997) MMSD
02/28/19 DM0228/19002788
6.8 % 0.1
SM 2540 G (1997) MMSD
Avg Result: 6.4 %
Min LOD: 0.1 %
Max Result: 8.9
Weekly Composite
02/02/19 WMC05/19001793
5.6 % 0.1
SM 2540 G (1997) MMSD
02/09/19 WMC06/19002209
02/16/19 WMC07/19002492
7 % 0.1
7.3 % 0.1
SM 2540 G (1997) MMSD
SM 2540 G (1997) MMSD
02/23/19 WMC08/19002679 6.4 % 0.1 SM 2540 G (1997) MMSD
Min LOD: 0.1 %
Solids (a/o Volatile)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
02/09/19 WMC06/19002209 73 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 73 % Min LOD: 0.1
Page I or 13
SYS/rptlMMoMonthly 1110113 tl Printed.• 3/11/1910:13

f
i
i kNSD
�t�cuidlelaw�rl
ZINC ICP METHOD
Sample17
Date Sample ID
Result
LOD
LOQ QA Flags
Monthly Milorganite Report
February 2019
Analytical Methcd La
02/01/19
DM0201/19001283
440 mg/kg D.W.
16
46
SW846: 6010C
MMSD
02/02/19
DM0202/19001320
410 mg/kg D.W.
16
46
SW846: 6010C
MMSD
02/03/19
DM0203/19001774
390 mg/kg D.W.
16
46
SW846: 6010C
MMSD
02/04/19
DM0204/19001791
410 mg/kg D.W.
16
48
SW846: 6010C
MMSD
02/05/19
DM0205/19001816
430 mg/kg D.W.
16
46
SW846: 6010C
MMSD
02/06/19
DM0206/19001845
430 mg/kg D.W.
16
46
SW846: 6010C
MMSD
02/07/19
DM0207/19001867
450 mg/kg D.W.
16
48
SW846: 6010C
MMSD
02/08/19
DM0208/19001883
430 mg/kg D.W.
16
47
SW846: 6010C
MMSD
02/09/19
02/10/19
DM0209/19001894
DM0210119002088
430 mg/kg D.W.
440 mg/kg D.W.
16
16
48
46
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/11/19
DM0211/19002207
420 mg/kg D.W.
16
46
SW846: 6010C
MMSD
02/12/19
DM0212/19002232
420 mg/kg D.W.
16
48
SW846: 6010C
MMSD
02/13/19
DM0213/19002261
420 mg/kg D.W.
16
48
SW846: 6010C
MMSD
02/14/19
DM0214/19002348
450 mg/kg D.W.
16
48
SW846: 6010C
MMSD
02/15/19
DM0215/19002364
470 mg/kg D.W.
16
47
SW846: 6010C
MMSD
02/16/19
DM0216/19002447
450 mg/kg D.W.
16
48
SW846: 6010C
MMSD
02/17/19
02/18/19
DM0217/19002467
DM0218/19002490
470 mg/kg D.W.
460 mg/kg D.W.
16
16
47
47
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/19/19
DM0219/19002563
420 mg/kg D.W.
16
47
SW846: 6010C
MMSD
02/20/19
DM0220/19002596
430 mg/kg D.W.
16
47
SW846: 6010C
MMSD
02/21/19
DM0221/19002617
430 mg/kg D.W.
16
47
SW846: 6010C
MMSD
02/22/19
02/23/19
DM0222/19002632
DM0223/19002643
430 mg/kg D.W.
400 mg/kg D.W.
16
16
47
47
SW846: 6010C
SW846: 6010C
MMSD
MMSD
02/24/19
DM0224/19002662
400 mg/kg D.W.
16
48
SW846: 6010C
MMSD
02/25/19
DM0225/19002675
400 mg/kg D.W.
16
46
SW846: 6010C
MMSD
02/26/19
DM0226/19002702
420 mg/kg D.W.
16
46
SW846: 6010C
MMSD
02/27/19
DM0227/19002767
420 mg/kg D.W.
16
46
SW846: 6010C
MMSD
02/28/19
DM0228/19002788
420 mg/kg D.W.
16
47
SW846: 6010C
MMSD
Avg Result: 430 mg/kg D.W.
Min LOD:
16 mg/kg D.W.
Max Result: 470 mg/kg D.W.
Page 11 of Ij
SYSIrptlMiloMonthly 1110113 U Printed, 311211910.0

r.
r f
NNSD
I IRAGtAB81 W
Fiag Descriptions
AO Other -- Flag requires additional explanation
AX Qualified data - see contract lab report
83 Target analyte detected in method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits. _
88 LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
D3 Duplicate precision control limit was exceeded.
D2 Matra spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
D5 The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
Hi Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
Monthly Milorganite Report
February 2019
IS Insufficient sample volume for analysis.
3 Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
LA Not analyzed - lab accident.
M3 Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
M5 Incubator/water bath temperature was outside method
requirements.
M7 Micro sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
02 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
S5 Reading was not confirmed by a constant weight measurement
SD Supplemental details provided.(Water Quality only.)
T3 The dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample exceeded prescribed method temperature range.
Page 13 of 13
SYSIMUM116Month/y V10113 tJ Printed: 311211910.2i

-4�
CiNNSD
PARTNERS FOR A CLEANER ENVIRONMENT
April 15, 2019
Memorandum
TO: Todd Schwingle, Dion Doege, Jacob Holbert, Brett Kelly, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Jaime Staufenbeil, Tom Nowicki, Beth Stroik, Kori
Kenney, Lab File
SUBJECT: Milorganite Monthly Data — March 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of March 2019.
The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin
(Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
Richard Vincent Date
Laboratory Team Supervisor
Report Review By:
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

►l1NEit3 iR A
ALUMINUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ .• Flags
Monthly Mllorganite Report
March 2019
Analytical Method Lab
03/09/19
WMC10/19003333
5600 mg/kg D.W.
85
230 68.
SW846: 6010C
MMSD
Avg Result: 5600 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Date Sample ID
Min LOD: 85 mg/kg D.W.
Result LOD LOQ .. Flags
Analytical Method
Lab
03/09/19
WMC10/19003333
0.14 %
0.11
AOAC (13) 2.065
MMSD
Avg Result: 0.14 "/o
ARSENIC ICP METHOD
Date Sample ID
Min LOD: 0.11 0/0
Result LOD
LOQ QA Flags
Analytical Method
Lab
,Sample
03/01/19
DM0301/19002803
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/02/19
DM0302/19002834
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/03/19
DM0303/19002869
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/04/19
DM0304/19002882
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
< 6.5 mg/kg D.W.
6.5
20
SW846: 6010C
MMSD
03/06/19
DM0306/19002979
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/07/19
DM0307/19003273
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/08/19
DM0308/19003288
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
03/09/19
DM0309/19003299
< 6.2 mg/kg D.W.
6.2
19
SW846: 6010C
MMSD
03/10/19
DM0310/19003318
< 6.5 mg/kg D.W.
6.5
19
SW846: 6010C
MMSD
03/11/19
DM0311/19003331
< 6.5 mg/kg D.W.
6.5
19
SW846: 6010C
MMSD
03/12/19
DM0312/19003356
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
03/13/19
DM0313/19003481
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/15/19
DM0315/19003517
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/16/19
DM0316/19003528
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
03/17/19
DM0317/19003547
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
03/18/19
DM0318/19003625
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
03/19/19
DM0319/19003649
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
03/20/19
DM0320/19003677
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/21/19
DM0321/19003926
< 6.3 mg/kg D.W.
6.3
19
SW846: 6010C
MMSD
03/22/19
DM0322119003941
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/23/19
DM0323/19003952
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/24/19
DM0324119003971
< 6.5 mg/kg D.W.
6.5
19
SW846: 6010C
MMSD
03/25/19
DM0325/19003984
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/26/19
DM0326/19004136
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/27/19
DM0327/19004166
< 6.5 mg/kg D.W.
6.5
19
SW846: 6010C
MMSD
03/28/19
DM0328/19004187
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/29/19
DM0329/19004202
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
03/30/19
03/31/19
DM0330/19004221
DM0331/19004310
< 6.3 mg/kg D.W.
< 6.4 mg/kg D.W.
6.3
6.4
19
19
SW846: 6010C
SW846: 6010C
MMSD
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
6.2 mg/kg D.W.
Page 1 of 1.3
SWrptlMi/oMonthty 1110113 tj Printed.- 41151191436

1,fkNSD
41111113FRACILWYMW
BORON ICP Dry wt.
Sample Date Sample ID
Result
QA
Flags
Monthly Milorganite Report
March 2019
Analytical Method Lab i
03/09/19 WMC10/19003333
Avg Result: 20 mg/kg D.W.
CADMIUM ICP METHOD
Sample Date Sample ID
20 mg/kg D.W. 1.1 3.4
Min LOD: 1.1 mg/kg D.W.
Result LOD LOQ .•
Flags
SW846: 6010C
Analytical Method
CT Lab
Lab
03/01/19
DM0301/19002803
0.59 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/02/19
DM0302/19002834
0.48 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/03/19
DM0303/19002869
0.56 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/04/19
DM0304/19002882
0.59 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
0.5 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/06/19
DM0306/19002979
0.79 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/07/19
DM0307/19003273
0.62 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/08/19
03/09/19
DM0308/19003288
DM0309/19003299
0.57 mg/kg D.W.
0.52 mg/kg D.W.
0.3
0.29
1.4
1.4
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/10/19
DM0310/19003318
0.6 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/11/19
DM0311/19003331
0.56 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/12/19
DM0312/19003356
0.65 mg/kg D.W.
0.29
1.4
J.
SW846: 6010C
MMSD
03/13/19
DM0313/19003481
0.59 mg/kg D.W.
0.29
1.4
J.
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
0.42 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/15/19
03/16/19
DM0315/19003517
DM0316/19003528
0.35 mg/kg D.W.
0.56 mg/kg D.W.
0.3
0.29
1.4
1.4
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/17/19
DM0317/19003547
0.62 mg/kg D.W.
0.29
1.4
J.
SW846: 6010C
MMSD
03/18/19
DM0318/19003625
0.5 mg/kg D.W.
0.29
1.4
J.
SW846: 6010C
MMSD
03/19/19
DM0319/19003649
0.45 mg/kg D.W.
0.29
1.4
J.
SW846: 6010C
MMSD
03/20/19
DM0320/19003677
0.47 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/21/19
DM0321/19003926
0.43 mg/kg D.W.
0.29
1.4
J.
SW846: 6010C
MMSD
03/22/19
DM0322/19003941
0.46 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/23/19
DM0323/19003952
0.65 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/24/19
DM0324/19003971
0.59 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/25/19
DM0325119003984
0.62 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/26/19
DM0326/19004136
0.51 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/27/19
DM0327/19004166
0.54 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/28/19
DM0328/19004187
0.53 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/29/19
DM0329/19004202
0.57 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
03/30/19
03/31/19
DM0330/19004221
DM0331/19004310
0.53 mg/kg D.W.
0.44 mg/kg D.W.
0.3
0.3
1.4
1.4
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
Avg Result: 0.54 mg/kg O.W.
CHROMIUM ICP Dry wt.
Sample Date Sample ID
Min LOD: 0.29 mg/kg D.W.
Result LOD LOQ QA
Flags
Max Result: 0.79 mg/kg D.W.
Analytical Method
Lab
03/09/19
WMC10/19003333
230 mg/kg D.W.
1.4
4.2
SW846: 6010C
MMSD
Avg Result: 230 mg/kg D.W.
Min LOD:
1.4 mg/kg D.W.
Page 2of15
SYS/rpt1MiloM-thiy 1110113 tj Printed.• 411511914:36

I AD
r»ets rgt� taaei art
COBALT ICP Dry wt.
Date Sample ID
Result
LOD
LOQ QA Flags
Monthly Milorganite Report
March 2019
Analytical Method Lab
03/09/19
WMC10/19003333
4 mg/kg D.W.
1.1
3.4 138.
SW846: 6010C
MMSD
Avg Result: 4 mg/kg D.W.
COPPER ICP METHOD
:Sample Date Sample ID
Min LOD: 1.1 mg/kg D.W.
Result LOD LOQ QA Flags
Analytical Method
Lab
03/01/19
DM0301/19002803
220 mg/kg D.W.
7.7
23
SW846: 6010C
MMSD
03/02/19
DM0302/19002834
220 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
03/03/19
DM0303119002869
230 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
03/04/19
DM0304119002882
220 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
220 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
03/06/19
DM0306/19002979
230 mg/kg D.W.
7.7
24
SW846: 6010C
MMSD
03/07/19
DM0307/19003273
220 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
03/08/19
03/09/19
DM0308/19003288
DM0309/19003299
210 mg/kg D.W.
230 mg/kg D.W.
7.6
7.5
23
23
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/10/19
DM0310/19003318
220 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
03/11/19
DM0311/19003331
220 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
03/12/19
DM0312/19003356
220 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
03/13/19
DM0313/19003481
210 mg/kg D.W.
7.5
23
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
210 mg/kg D.W.
7.7
24
SW846: 6010C
MMSD
03/15/19
03/16/19
DM0316/19003517
DM0316/19003528
230 mg/kg D.W.
230 mg/kg D.W.
7.6
7.6
23
23
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/17/19
DM0317/19003547
240 mg/kg D.W.
7.5
23
SW846: 6010C
MMSD
03/18/19
DM0318/19003625
220 mg/kg D.W.
7.5
23
SW846: 6010C
MMSD
03/19/19
DM0319/19003649
220 mg/kg D.W.
7.5
23
SW846: 6010C
MMSD
03/20/19
DM0320/19003677
230 mg/kg D.W.
7.7
24
SW846: 6010C
MMSD
03/21/19
DM0321/19003926
220 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
03/22/19
DM0322/19003941
220 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
03/23/19
DM0323/19003952
230 mg/kg D.W.
7.7
24
SW846: 6010C
MMSD
03/24/19
DM0324/19003971
220 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
03/25/19
DM0325/19003984
230 mg/kg D.W.
7.7
24
SW846: 6010C
MMSD
03/26/19
DM0326/19004136
220 mg/kg D.W.
7.7
23
SW846: 6010C
MMSD
03/27/19
DM0327/19004166
230 mg/kg D.W.
7.8
24
SW846: 6010C
MMSD
03/28/19
DM0328/19004187
230 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
03/29/19
DM0329/19004202
230 mg/kg D.W.
7.7
24
SW846: 6010C
MMSD
03/30/19
DM0330/19004221
230 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
03/31/19
DM0331/19004310
230 mg/kg D.W.
7.6
23
SW846: 6010C
MMSD
Avg Result 220 mg/kg D.W.
FECAL COLIFORM SLUDGE
Date Sample ID
Min LOD: 7.5 mg/kg D.W.
Result LOD LOQ .• Flags
Max Result: 240 mg/kg D.W.
Analytical Method
Lab
03/05/19
MF/19004238
< 0.2 MPN/g TS
0.2
EPA 1680
MMSD
03/12/19
MF/19004476
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
03/19/19
MF/19005023
< 0.2 MPN/g TS
0.2
EPA 1680
MMSD
03/26/19
MF/19005730
< 0.2 MPN/g TS
0.2
EPA 1680
MMSD
SY5/rptJM11bMonth1y 1110113 tJ
Min LOD:
0.19 MPN/g TS
Page 3 of IS
Printed: 41151191436

Monthly Milorganite Report
f`NNSD
March 2019
IRON ICP METHOD
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Ua -b'
03/01/19 DM0301/19002803 33000 mg/kg D.W. 260 750 SW846: 6010C MMSD
03/02/19
DM0302/19002834
35000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
03/03/19
DM0303/19002869
37000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
03/04/19
DM0304/19002882
39000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
35000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
03/06/19
03/07/19
DM0306/19002979
DM0307/19003273
35000 mg/kg D.W.
35000 mg/kg D.W.
260
250
750
740
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/08/19
DM0308/19003288
31000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
03/09/19
03/10/19
DM0309/19003299
DM0310/19003318
35000 mg/kg D.W.
36000 mg/kg D.W.
250
260
730
760
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/11/19
DM0311/19003331
39000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
03/12/19
DM0312/19003356
37000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
03/13/19
DM0313/19003481
37000 mg/kg D.W.
250
730
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
35000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
03/15/19
DM0315/19003517
40000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
03/16/19
DM0316/19003528
44000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
03/17/19
03/18/19
DM0317/19003547
DM0318/19003625
44000 mg/kg D.W.
44000 mg/kg D.W.
250
250
730
730
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/19/19
DM0319/19003649
44000 mg/kg D.W.
250
730
SW846: 6010C
MMSD
03/20/19
DM0320/19003677
45000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
03/21/19
DM0321/19003926
44000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
03/22/19
03/23/19
DM0322/19003941
DM0323119003952
45000 mg/kg D.W.
40000 mg/kg D.W.
260
260
740
750
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/24/19
DM0324/19003971
38000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
03/25/19
DM0325/19003984
38000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
03/26/19
DM0326/19004136
38000 mg/kg D.W.
260
740
SW846: 6010C
MMSD
03/27/19
DM0327/19004166
40000 mg/kg D.W.
260
760
SW846: 6010C
MMSD
03/28/19
DM0328/19004187
40000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
03/29/19
DM0329/19004202
42000 mg/kg D.W.
260
750
SW846: 6010C
MMSD
03/30/19
DM0330/19004221
42000 mg/kg D.W.
250
740
SW846: 6010C
MMSD
03/31/19
DM0331/19004310
Avg Result: 39000 mg/kg D.W.
41000 mg/kg D.W. 250 740
Min LOD: 250 mg/kg D.W.
SW846: 6010C
Max Result: 45000 mg/kg D.W.
MMSD
Page 4 of 19
SYS/rptlMiloMonthly 1110113 tj Printed.• 41151191436

�
itSD
leu�
LEAD ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ QA Flags
Monthly Milorganite Report
March 2019
Analytical Method Lab
03/01/19
DM0301/19002803
31 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/02/19
DM0302/19002834
31 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/03/19
DM0303119002869
32 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/04/19
DM0304/19002882
33 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
33 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
03/06/19
DM0306/19002979
33 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/07/19
DM0307119003273
32 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/08/19
DM0308/19003288
30 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/09/19
DM0309/19003299
32 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/10/19
DM0310/19003318
34 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
03/11/19
DM0311/19003331
32 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/12/19
DM0312/19003356
33 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/13/19
DMO313/19003481
34 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
31 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/15/19
DM0315/19003517
33 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/16/19
DM0316/19003528
33 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/17/19
03/18/19
DM0317/19003547
DM0318/19003625
34 mg/kg D.W.
30 mg/kg D.W.
4.6
4.6
14
14
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/19/19
DM0319/19003649
31 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/20/19
DM0320/19003677
30 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/21/19
DM0321/19003926
29 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/22/19
03/23/19
DM0322/19003941
DM0323/19003952
26 mg/kg D.W.
32 mg/kg D.W.
4.7
4.7
14
14
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/24/19
DM0324/19003971
28 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
03/25/19
DM0325/19003984
27 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/26/19
DM0326/19004136
28 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/27/19
DM0327/19004166
28 mg/kg D.W.
4.8
14
SW846: 6010C
MMSD
03/28/19
DM0328/19004187
30 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/29/19
DM0329/19004202
30 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
03/30/19
DM0330/19004221
27 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/31/19
DM0331/19004310
26 mg/kg D.W.
4.7
14
SW846: 6010C
MMSD
Avg Result: 31 mg/kg D.W.
MERCURY by M. 7471 (sludge)
Sample Date Sample ID
Min LOD: 4.6 mg/kg D.W.
Result LOD LOQ QA Flags
Max Result: 34 mg/kg D.W.
Analytical Method
Lab
03/02/19
WMC09/19002884
0.068 mg/kg D.W.
0.0053
0.018 AX.
EPA 74718
Cr Lab
03/09/19
WMC10119003333
0.013 mg/kg D.W.
0.0006
0.0019
EPA 7471B
CT Lab
03/16/19
WMC11/19003986 <
0.0056 mg/kg D.W.
0.0056
0.019 AX.
EPA 7471B
Cr Lab
03/23/19
WMC12119003987
0.025 mg/kg D.W.
0.0055
0.019
EPA 7471B
Cr Lab
03/30/19
WMC13/19004553
0.12 mg/kg D.W.
0.0056
0.019
EPA 7471B
Cr Lab
Avg Result: 0.045 mg/kg D.W.
Min LOD: 0.00055 mg/kg D.W.
Max Result: 0.12 mg/kg D.W.
Page 5 of IS
5Y51rptlM116Month/y 1110113 U Printed.' 411511914.36

r1fNN$D
/� iRA �I(A� t11�IBR
MOLYBDENUM ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ QA Flags
Monthly Milorganite Report
March 2019
Analytical Method Lab
03/01/19
DM0301/19002803
9.6 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/02/19
DM0302119002834
9.9 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
03/03/19
DM0303/19002869
10 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/04/19
DM0304/19002882
11 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
03/06/19
DM0306/19002979
11 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
03/07/19
DM0307/19003273
11 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/08/19
DM0308/19003288
10 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/09/19
03/10/19
DM0309/19003299
DM0310/19003318
10 mg/kg D.W.
10 mg/kg D.W.
1.2
1.3
5.4
5.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/11/19
DM0311/19003331
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
03/12/19
DM0312/19003356
10 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/13/19
DM0313119003481
9.9 mg/kg D.W.
1.2
5.4
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
9.5 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
03/15/19
DM0315/19003517
10 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/16/19
DM0316/19003528
11 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/17/19
03/18/19
DM0317/19003547
DM0318/19003625
11 mg/kg D.W.
11 mg/kg D.W.
1.2
1.2
5.4
5.4
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/19/19
DM0319/19003649
10 mg/kg D.W.
1.2
5.4
SW846: 6010C
MMSD
03/20/19
DM0320/19003677
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
03/21/19
DM0321/19003926
10 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/22/19
03/23/19
DM0322119003941
DM0323/19003952
10 mg/kg D.W.
10 mg/kg D.W.
1.3
1.3
5.5
5.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/24/19
DM0324/19003971
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
03/25/19
DM0325/19003984
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
03/26/19
DM0326/19004136
10 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/27/19
DM0327/19004166
11 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
03/28/19
DM0328/19004187
11 mg/kg D.W.
1.3
5.5
SW846: 6010C
MMSD
03/29/19
DM0329/19004202
10 mg/kg D.W.
1.3
5.6
SW846: 6010C
MMSD
03/30/19
03/31/19
DM0330/19004221
DM0331/19004310
Avg Result: 10 mg/kg D.W.
11 mg/kg D.W. 1.3 5.5
11 mg/kg D.W. 1.3 5.5
Min LOD: 1.2 mg/kg D.W.
SW846: 6010C
SW846: 6010C
Max Result: 11 mg/kg D.W.
MMSD
MMSD
Page 6 o/1j
SVS/rptl MiloMonthly 1110113 h Printed.- 411511914:36

Monthly Milorganite Report
iNSD March 2019
POTIM iM 1 C1149 iYIHIINMIn
NICKEL ICP METHOD
Sample Date Sample ID Result LOD LOQ .. Flags Analytical Method Lab
03/01/19 DM0301/19002803 25 mg/kg D.W. 4.5 14 SW846: 6010C MMSD
03/02/19 DM0302/19002834 26 mg/kg D.W. 4.5 14 SW846: 6010C MMSD
03/03/19
DM0303/19002869
27 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/04/19
DM0304119002882
27 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
26 mg/kg D.W.
4.6
14
SW846: 6010C
MMSD
03/06/19
DM0306/19002979
28 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
03/07/19
DM0307/19003273
30 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/08/19
DM0308/19003288
26 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/09/19
DM0309/19003299
27 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/10/19
DM0310/19003318
27 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
03/11/19
DM0311119003331
26 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
03/12/19
DM0312/19003356
26 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/13/19
DM0313/19003481
27 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
26 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
03/15/19
DM0315/19003517
27 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/16/19
DM0316/19003528
30 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/17/19
03/18/19
DM0317/19003547
DM0318/19003625
30 mg/kg D.W.
29 mg/kg D.W.
4.4
4.4
14
14
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/19/19
DM0319/19003649
28 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/20/19
DM0320/19003677
25 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
03/21/19
DM0321/19003926
25 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/22/19
03/23/19
DM0322119003941
DM0323/19003952
24 mg/kg D.W.
25 mg/kg D.W.
4.5
4.5
14
14
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/24/19
DM0324/19003971
26 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
03/25/19
DM0325/19003984
27 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
03/26/19
DM0326/19004136
28 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
03/27/19
DM0327/19004166
31 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
03/28/19
DM0328/19004187
28 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/29/19
DM0329/19004202
31 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
03/30/19
DM0330/19004221
31 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
03/31/19
DM0331/19004310
32 mg/kg D.W.
4.4
14
SW846: 6010C
MMSD
Avg Result: 27 mg/kg D.W.
NITRATE NITROGEN
Sample ►.
Min LOD: 4.4 mg/kg D.W.
•► LOQ QA Flags
Max Result: 32 mg/kg D.W.
Analytical Method
Lab
03/09/19
WMC10/19003333
< 0.5 %
0.5
AOAC (16) 930.01
MMSD
Avg Result: 0 %
NITROGEN-Total(Manual)
Sample Date Sample ID
Min LOD: 0.3 0/6
Result LOD
LOQ QA Flags
Analytical Method
Lab
03/09/19
WMC10/19003333
6.4 %
0.11
AOAC (16) 955.04
MMSD
Avg Result: 6.4 %
Min LOD: 0.11 0/6
Page 7 of 1.i
SY5/ipt1Mi1bM0nth1y 1110113 ty Printed: 41151191436

rJ`t Monthly Milorganite Report
March 2019
M111EI'S lot A Mix? a
NITROGEN -Water Insoluble
Sample Date Sample ID
Result
LOD
LOQ
QA Flags Analytical Method
Lab
03/09/19
WMC10/19003333
5.4 %
0.5
AOAC (16) 945.01
MMSD
pH -Solids
Sample Date
03/02/19
Avg Result: 5.4 %
Sample ID
WMC09/19002884
Min LOD: 0.5
Result -LOD -4
6.22 Stnd. Units 0.1
i�OQ
QA Flags Analytical Method
SW846: 9045D
Lab
MMSD
03/09/19
WMC10/19003333
6.18 Stnd. Units
0.1
SW846: 9045D
MMSD
03/16/19
WMC11/19003986
6.05 Stnd. Units
0.1
SW846: 9045D
MMSD
03/23/19
WMC12119003987
6.15 Stnd. Units
0.1
SW846: 9045D
MMSD
03/30/19
WMC13/19004553
6.11 Stnd. Units
0.1
SW846: 9045D
MMSD
Avg Result: 6.1 Stnd. Units
PHOSPHORUS ICP METHOD
Date Sample ID
Min LOD: 0.1 Stnd. Units
Result LOD LOQ
Max Result: 6.22 Stnd. Units
QA Flags Analytical Method
Lab
03/01/19
DM0301/19002803
22000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
03/02/19
DM0302/19002834
23000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
03/03/19
DM0303/19002869
24000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
03/04/19
DM0304/19002882
24000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
24000 mg/kg D.W.
18
85
SW846: 6010C
MMSD
03/06/19
DM0306/19002979
24000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
03/07/19
DM0307/19003273
24000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
03/08/19
DM0308/19003288
22000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
03/09/19
DM0309/19003299
24000 mg/kg D.W.
18
81
SW846: 6010C
MMSD
03/10/19
DM0310/19003318
25000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
03/11/19
DM0311/19003331
24000 mg/kg D.W.
18
84
Q2. SW846: 6010C
MMSD
03/12/19
DM0312/19003356
24000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
03/13/19
DM0313/19003481
23000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
22000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
03/15/19
DM0315/19003517
23000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
03/16/19
DM0316/19003528
23000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
03/17/19
DM0317/19003547
23000 mg/kg D.W.
18
81
SW846: 6010C
MMSD
03/18/19
03/19/19
DM0318/19003625
DM0319/19003649
22000 mg/kg D.W.
24000 mg/kg D.W.
18
18
82
82
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/20/19
DM0320/19003677
24000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
03/21/19
03/22/19
DM0321/19003926
DM0322/19003941
23000 mg/kg D.W.
23000 mg/kg D.W.
18
18
82
83
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/23/19
DM0323/19003952
24000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
03/24/19
DM0324/19003971
23000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
03/25/19
DM0325/19003984
23000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
03/26/19
03/27/19
DM0326/19004136
DM0327/19004166
23000 mg/kg D.W.
25000 mg/kg D.W.
18
18
83
84
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/28/19
DM0328/19004187
25000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
03/29/19
DM0329/19004202
25000 mg/kg D.W.
18
84
SW846: 6010C
MMSD
03/30/19
DM0330/19004221
25000 mg/kg D.W.
18
82
SW846: 6010C
MMSD
03/31/19
DM0331/19004310
25000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
Avg Result: 24000 mg/kg D.W.
SYS/rptimmoMonthly 1110113 tj
Min LOD: 18 mg/kg D.W.
Max Result: 25000 mg/kg D.W.
Page 8 of 1j
Printed: 4115119 1436

IfNNSD
ow
POTASSIUM ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ„
.• Flags
Monthly Milorganite Report
March 2019
Analytical Method Lab
03/01/19
DM0301/19002803
5400 mg/kg D.W.
140
720
AO.
SW846: 6010C
MMSD
03/02/19
DM0302/19002834
5300 mg/kg D.W.
140
730
AC.
SW846: 6010C
MMSD
03/03/19
DM0303/19002869
5200 mg/kg D.W.
140
720
AO.
SW846: 6010C
MMSD
03/04/19
DM0304/19002882
5400 mg/kg D.W.
140
720
AO.
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
5600 mg/kg D.W.
140
740
AO, B8.
SW846: 6010C
MMSD
03/06/19
DM0306/19002979
5300 mg/kg D.W.
140
730
AO.
SW846: 6010C
MMSD
03/07/19
DM0307/19003273
5600 mg/kg D.W.
140
720
AO, Q3.
SW846: 6010C
MMSD
03/08/19
DM0308/19003288
5100 mg/kg D.W.
140
720
AO, B8.
SW846: 6010C
MMSD
03/09/19
DM0309/19003299
5100 mg/kg D.W.
140
710
AO.
SW846: 6010C
MMSD
03/10/19
DM0310/19003318
5300 mg/kg D.W.
140
740
AO.
SW846: 6010C
MMSD
03/11/19
DM0311/19003331
5100 mg/kg D.W.
140
730
AO.
SW846: 6010C
MMSD
03/12/19
DM0312/19003356
4600 mg/kg D.W.
140
710
AO, B8.
SW846: 6010C
MMSD
03/13/19
DM0313/19003481
4700 mg/kg D.W.
140
710
AO.
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
4800 mg/kg D.W.
140
730
AO, B8.
SW846: 6010C
MMSD
03/15/19
DM0315/19003517
4600 mg/kg D.W.
140
720
SW846: 6010C
MMSD
03/16/19
DM0316/19003528
4400 mg/kg D.W.
140
720
AO.
SW846: 6010C
MMSD
03/17/19
DM0317/19003547
4200 mg/kg D.W.
140
710
AO.
SW846: 6010C
MMSD
03/18/19
DM0318/19003625
4000 mg/kg D.W.
140
710
AO.
SW846: 6010C
MMSD
03/19/19
DM0319/19003649
3700 mg/kg D.W.
140
710
AO, B8.
SW846: 6010C
MMSD
03/20/19
DM0320/19003677
4100 mg/kg D.W.
140
730
AO, B8.
SW846: 6010C
MMSD
03/21/19
DM0321/19003926
4300 mg/kg D.W.
140
710
AO, B8.
SW846: 6010C
MMSD
03/22/19
DM0322/19003941
4700 mg/kg D.W.
140
720
AO, 88, Q3.
SW846: 6010C
MMSD
03/23/19
DM0323/19003952
4600 mg/kg D.W.
140
730
SW846: 6010C
MMSD
03/24/19
DM0324119003971
4600 mg/kg D.W.
140
740
SW846: 6010C
MMSD
03/25/19
DM0325/19003984
4400 mg/kg D.W.
140
730
SW846: 6010C
MMSD
03/26/19
DM0326/19004136
4600 mg/kg D.W.
140
720
AO, B8.
SW846: 6010C
MMSD
03/27/19
DM0327/19004166
4600 mg/kg D.W.
140
730
AO.
SW846: 6010C
MMSD
03/28/19
DM0328/19004187
5000 mg/kg D.W.
140
720
AO.
SW846: 6010C
MMSD
03/29/19
DM0329/19004202
4900 mg/kg D.W.
140
730
AO.
SW846: 6010C
MMSD
03/30/19
DM0330/19004221
5000 mg/kg D.W.
140
720
SW846: 6010C
MMSD
03/31/19
DM0331119004310
5200 mg/kg D.W.
140
720
SW846: 6010C
MMSD
Avg Result: 4800 mg/kg D.W.
Min LOD:
140 mg/kg D.W.
Max Result: 5600 mg/kg D.W.
Page 9 of 13
SY5/1ptlM110Manth/y 1110113 4 Printed: 411511914:36

� NSD
,i
f
rta�Ntttaet'
SELENIUM ICP METHOD
Date Sample ID
Result
LOD
LOQ QA Flags
Monthly Milorganite Report
March 2019
Analytical Method Lab
03/01/19
DM0301/19002803
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
03/02/19
DM0302/19002834
< 6.9 mg/kg D.W.
6.9
20
SW846: 6010C
MMSD
03/03/19
DM0303/19002869
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
03/04/19
DM0304/19002882
< 6.8 mg/kg D.W.
6.8
20 Q2.
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
< 7 mg/kg D.W.
7
21
SW846: 6010C
MMSD
03/06/19
DM0306/19002979
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
03/07/19
DM0307/19003273
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
03/08/19
DM0308/19003288
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
03/09/19
03/10/19
DM0309/19003299
DM0310/19003318
< 6.7 mg/kg D.W.
< 6.9 mg/kg D.W.
6.7
6.9
20
20
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/11/19
DM0311/19003331
< 6.9 mg/kg D.W.
6.9
20
SW846: 6010C
MMSD
03/12/19
DM0312/19003356
< 6.7 mg/kg D.W.
6.7
20
SW846: 6010C
MMSD
03/13/19
DM0313119003481
< 6.7 mg/kg D.W.
6.7
20
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
03/15/19
DM0315/19003517
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
03/16/19
DM0316/19003528
< 6.7 mg/kg D.W.
6.7
20
SW846: 6010C
MMSD
03/17/19
03/18/19
DM0317/19003547
DMQ318/19003625
< 6.7 mg/kg D.W.
< 6.7 mg/kg D.W.
6.7
6.7
20
20
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/19/19
DM0319/19003649
< 6.7 mg/kg D.W.
6.7
20
SW846: 6010C
MMSD
03/20/19
DM0320/19003677
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
03/21/19
DM0321/19003926
< 6.7 mg/kg D.W.
6.7
20
SW846: 6010C
MMSD
03/22/19
03/23/19
DM0322/19003941
DM0323/19003952
< 6.8 mg/kg D.W.
< 6.9 mg/kg D.W.
6.8
6.9
20
20
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/24/19
DM0324/19003971
< 6.9 mg/kg D.W.
6.9
20
SW846: 6010C
MMSD
03/25/19
DM0325/19003984
< 6.9 mg/kg D.W.
6.9
20
SW846: 6010C
MMSD
03/26/19
DM0326/19004136
< 6.8 mg/kg D.W.
6.8
20
SW846: 6010C
MMSD
03/27/19
DM0327/19004166
< 6.9 mg/kg D.W.
6.9
20
SW846: 6010C
MMSD
03/28/19
03/29/19
03/30/19
03/31/19
DM0328/19004187
DM0329/19004202
DM0330/19004221
DM0331/19004310
< 6.8 mg/kg D.W.
< 6.9 mg/kg D.W.
7.4 mg/kg D.W.
6.9 mg/kg D.W.
6.8
6.9
6.8
6.8
20
20
20 J.
20 1
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
Avg Result: 0.46 mg/kg D.W.
Min LOD:
6.7 mg/kg D.W.
Max Result: 7.4 mg/kg D.W.
Page 10 of I3
SYS/rptJMiioMonthiy 1/10/13 h Printed.41151191436

Monthly Mllorganite Report
ft4NSD
March 2019
�RIIIltS Epl1 tIEkEA EIlIl�itFy'
Solids (% Moisture)
..
.• •• .
-
Daily Composite
03/01/19 DM0301/19002803
6.2 %
0.1
SM 2540 G (1997) MMSD
03/02/19 DM0302/19002834
7.1 %
0.1
SM 2540 G (1997) MMSD
03/03/19 DM0303119002869
5.8 %
0.1
SM 2540 G (1997) MMSD
03/04/19 DM0304/19002882
5.5 %
0.1
SM 2S40 G (1997) MMSD
03/05/19 DM0305/19002951
8 %
0.1
SM 2540 G (1997) MMSD
03/06/19
03/07/19
DM0306/19002979
DM0307/19003273
6.5 %
5.6 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
03/08/19
DM0308/19003288
5.2 %
0.1
SM 2540 G (1997)
MMSD
03/09/19
DM0309/19003299
4.1 %
0.1
SM 2540 G (1997)
MMSD
03/10/19
DM0310119003318
7.7 %
0.1
SM 2540 G (1997)
MMSD
03/11/19
DM0311/19003331
7.3 %
0.1
SM 2540 G (1997)
MMSD
03/12/19
DM0312/19003356
4.8 %
0.1
SM 2540 G (1997)
MMSD
03/13/19
DM0313/19003481
4.6 %
0.1
SM 2540 G (1997)
MMSD
03/14/19
DM0314/19003502
6.4 %
0.1
SM 2540 G (1997)
MMSD
03/15/19
DM0315/19003517
5.6 %
0.1
SM 2540 G (1997)
MMSD
03/16/19
DM0316/19003528
5.1 %
0.1
SM 2540 G (1997)
MMSD
03/17/19
DM0317/19003547
4.2 %
0.1
SM 2540 G (1997)
MMSD
03/18/19
DM0318119003625
4.4 %
0.1
SM 2540 G (1997)
MMSD
03/19/19
DM0319/19003649
4.6 %
0.1
SM 2540 G (1997)
MMSD
03/20/19
DM0320/19003677
6.4 %
0.1
SM 2540 G (1997)
MMSD
03/21/19
03/22/19
DM0321/19003926
DM0322/19003941
4.8 %
6 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
03/23/19
DM0323/19003952
6.8 %
0.1
SM 2540 G (1997)
MMSD
03/24/19
DM0324/19003971
7.5 %
0.1
SM 2540 G (1997)
MMSD
03/25/19
DM0325/19003984
6.8 %
0.1
SM 2540 G (1997)
MMSD
03/26/19
DM0326/19004136
6.2 %
0.1
SM 2540 G (1997)
MMSD
03/27/19
DM0327/19004166
7.4 %
0.1
SM 2540 G (1997)
MMSD
03/28/19
DM0328/19004187
5.6 %
0.1
SM 2540 G (1997)
MMSD
03/29/19
DM0329/19004202
6.8 %
0.1
SM 2540 G (1997)
MMSD
03/30/19
DMO330/19004221
5.5 %
0.1
SM 2540 G (1997)
MMSD
03/31/19
DM0331/19004310
5.7 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 5.9 "/o
Weekly Composite
03/02/19 WMC09/19002884
Min LOD: 0.1 %
6.1 % 0.1
Max Result: 8 %
SM 2540 G (1997)
MMSD
03/09/19
WMC10/19003333
5.7 %
0.1
SM 2540 G (1997)
MMSD
03/16/19
WMC11/19003986
6.4 %
0.1
SM 2540 G (1997)
MMSD
03/23/19
WMC12/19003987
5.4 %
0.1
SM 2540 G (1997)
MMSD
03/30/19
WMC13/19004553
6.5 %
0.1
SM 2540 G (1997)
MMSD
Solids (% Volatile)
Sample Date Sample ID
Min LOD: 0.1 0/6
Result LOD LOQ QA Flags
Analytical Method
Lab
03/09/19
WMC10/19003333
73 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 73 %
SYS1rptlMi10M017th1y V10113 tl
Min LOD:
0.1
Page 11 o/ I.i
PAnted.• 41151191436

MMSD
ART"ti 01 Cl Erl�9AlIB1f
ZINC ICP METHOD
Sample Date Sample ID
03/01/19 DM0301/19002803
Result
450 mg/kg D.W.
LOD
16
LOQ QA Flags
47
Monthly Milorganite Report
March 2019
Analytical Method
SW846: 6010C MMSD
03/02/19
DM0302/19002834
460 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/03/19
DM0303/19002869
470 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/04/19
DM0304/19002882
460 mg/kg D.W.
16
46
SW846: 6010C
MMSD
03/05/19
DM0305/19002951
440 mg/kg D.W.
16
48
SW846: 6010C
MMSD
03/06/19
DM0306119002979
480 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/07/19
DM0307/19003273
460 mg/kg D.W.
16
46
SW846: 6010C
MMSD
03/08/19
DM0308/19003288
430 mg/kg D.W.
16
46
SW846: 6010C
MMSD
03/09/19
03/10/19
DM0309/19003299
DM0310/19003318
460 mg/kg D.W.
450 mg/kg D.W.
16
16
46
48
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/11/19
DM0311/19003331
440 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/12/19
DM0312/19003356
450 mg/kg D.W.
16
46
SW846: 6010C
MMSD
03/13/19
DM0313/19003481
440 mg/kg D.W.
16
46
SW846: 6010C
MMSD
03/14/19
DM0314/19003502
440 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/15/19
DM0315/19003517
480 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/16/19
DM0316/19003528
500 mg/kg D.W.
16
46
SW846: 6010C
MMSD
03/17/19
03/18/19
DM0317/19003547
DM0318/19003625
510 mg/kg D.W.
480 mg/kg D.W.
16
16
46
46
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/19/19
DM0319/19003649
470 mg/kg D.W.
16
46
SW846: 6010C
MMSD
03/20/19
DM0320/19003677
460 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/21/19
DM0321/19003926
440 mg/kg D.W.
16
46
SW846: 6010C
MMSD
03/22/19
03/23/19
DM0322/19003941
DM0323/19003952
440 mg/kg D.W.
460 mg/kg D.W.
16
16
47
47
SW846: 6010C
SW846: 6010C
MMSD
MMSD
03/24/19
DM0324/19003971
460 mg/kg D.W.
16
48
SW846: 6010C
MMSD
03/25/19
DM0325/19003984
450 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/26/19
DM0326/19004136
450 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/27/19
DM0327/19004166
470 mg/kg D.W.
16
48
SW846: 6010C
MMSD
03/28/19
DM0328/19004187
470 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/29/19
DM0329/19004202
450 mg/kg D.W.
16
47
SW846: 6010C
MMSD
03/30/19
DM0330/19004221
440 mg/kg D.W.
16
46
SW846: 6010C
MMSD
03/31/19
DM0331/19004310
430 mg/kg D.W.
16
47
SW846: 6010C
MMSD
Avg Result: 460 mg/kg D.W.
Min LOD:
16 mg/kg D.W.
Max Result: 510 mg/kg D.W.
Page 12 of 13
SY51rpt1H11bHontb1y 1/10/13 tj Printed.• 41151191436

iNSD
NIABS t1t t ttulel eH7W
Monthly Milorganite Report
March 2019
Flag Descriptions
AO Other -- Flag requires additional explanation
AX Qualified data - see contract lab report
B3 Target analyte detected in method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits.
B8 LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
Di Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
Hi Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
IS Insufficient sample volume for analysis.
3 Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
LA Not analyzed - lab accident.
M1 Too numerous to count. _
M2 Sample incubation period outside method requirement
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
MS Incubator/water bath temperature was outside method
requirements.
M7 Micro sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
SS Reading was not confirmed by a constant weight measurement
SD Supplemental details provided.(Water Quality only,)
T3 The dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The dilution water D.O. increase was > 0.2 mg/L.
TS Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample exceeded prescribed method temperature range.
Page 13 0/13
SYS1rpt1Mi1oM-th1y 1110113 tJ Printed: 411511914:36

NNSD
PARTNERS FOR A CLEANER ENVIRONMENT
May 15, 2019
Memorandum
TO: Todd Schwingle, Dion Doege, Jacob Holbert, Brett Kelly, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom Nowicki, Beth
Stroik, Kori Kenney, Lab File
SUBJECT: Milorganite Monthly Data —April 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of April 2019.
The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin
(Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
Richard Vincent Date
Laboratory Team Supervisor
Report Review By:
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

IfNIISD
►rIM PRA
ALUMINUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report
April 2019
La _J1
04/13/19
WMC15119005749
4400 mg/kg D.W.
23
74
B8. SW846: 6010C
MMSD
Avg Result: 4400 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Date Sample ID
Min LOD: 23 mg/kg D.W.
Result LOD LOQ ..
Flags Analytical Method
Lab
iSample
04/13/19
WMC15/19005749
0.17 %
0.11
0.37
AOAC (13) 2.065
MMSD
Avg Result 0.17 "/o
ARSENIC ICP METHOD
Sample Date Sample ID
Min LOD: 0.11
Result LOD
LOQ QA
Flags Analytical Method
Lab
04/01/19
DM0401/19004551
< 6.4 mg/kg D.W.
6.4
19
SW846: 6010C
MMSD
04/02/19
DM0402/19004576
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/03/19
DM0403/19004770
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/04/19
DM0404/19004791
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/05/19
DM0405/19004806
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/06/19
DM0406/19004817
< 6.3 mg/kg D.W.
6.3
25
SW846: 6010C
MMSD
04/07/19
DM0407/19004836
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/08/19
DM0408/19004849
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/09/19
DM0409/19005069
< 6.3 mg/kg D.W.
6.3
25
SW846: 6010C
MMSD
04/10/19
DMO410/19005097
< 6.2 mg/kg D.W.
6.2
25
SW846: 6010C
MMSD
04/11/19
DMO411/19005650
< 6.3 mg/kg D.W.
6.3
25
SW846: 6010C
MMSD
04/12/19
DM0412/19005665
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/13/19
DM0413/19005676
< 6.3 mg/kg D.W.
6.3
25
SW846: 6010C
MMSD
04/14/19
DMO414/19005695
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/15/19
DM0415/19005747
< 6.5 mg/kg D.W.
6.5
26
SW846: 6010C
MMSD
04/16/19
DM0416/19005837
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/17/19
DM0417/19005865
< 6.4 mg/kg D.W.
6.4
25
SW846: 6010C
MMSD
04/18/19
DM0418/19005886
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/19/19
DM0419/19005901
< 6.3 mg/kg D.W.
6.3
25
SW846: 6010C
MMSD
04/20/19
DM0420/19005912
< 6.4 mg/kg D.W.
6.4
26
SW846: 6010C
MMSD
04/21/19
DMO421/19006054
< 6.5 mg/kg D.W.
6.5
26
SW846: 6010C
MMSD
04/22/19
04/23/19
DM0422/19006067
DMO423/19006092
< 6A mg/kg D.W.
< 6.4 mg/kg D.W.
6.4
6.4
26
25
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/24/19
DMO424/19006120
< 6.3 mg/kg D.W.
6.3
25
SW846: 6010C
MMSD
04/25/19
04/26/19
DM0425/19006245
DM0426/19006496
6.5 mg/kg D.W.
< 6.5 mg/kg D.W.
6.5
6.5
26
26
]. SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/27/19
DM0427/19006507
< 6.3 mg/kg D.W.
6.3
25
SW846: 6010C
MMSD
04/28/19
DM0428/19006526
< 6.3 mg/kg D.W.
6.3
25
SW846: 6010C
MMSD
04/29/19 DM0429/19006539
04/30/19 DMO430/19006564
Avg Result: 0.22 mg/kg D.W.
BORON ICP Dry wt.
iSample Date Sample ID
04/13/19 WMC15/19005749
< 6.4 mg/kg D.W. 6.4 25
< 6.4 mg/kg D.W. 6.4 26
Min LOD: 6.2 mg/kg D.W.
Result LOD LOQ .•
18 mg/kg D.W. 1.1 3.4
SW846: 6010C
SW846: 6010C
Max Result: 6.5 mg/kg D.W.
Flags Analytical Method
SW846: 6010C
MMSD
MMSD
Lab
CT Lab
Avg Result: 18 mg/kg D.W.
SYS/rptlMibMonth/y 1/10/13 tj
Min LOD:
1.1 mg/kg D.W.
Page 1 o/13
Printed: 5/15/19 09:45

CADMIUM ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ
QA Flags
Monthly Milorganite Report
April 2019
Analytical Method Lab
04/01/19
DM0401/19004551
0.5 mg/kg D.W.
0.3
1.4
J.
SW846: 6010C
MMSD
04/02/19
DM0402/19004576
0.49 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/03/19
DM0403/19004770
0.55 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/04/19
DM0404/19004791
0.54 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/05/19
DM0405/19004806
0.44 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/06/19
DM0406/19004817
0.48 mg/kg D.W.
0.27
1
J.
SW846: 6010C
MMSD
04/07/19
DM0407/19004836
0.44 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/08/19
DM0408/19004849
0.52 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/09/19
- --
04/10/19
DM0409/19005069
_-
DM0410/19005097
0.42 mg/kg D.W.
--- ---- ----
0.46 mg/kg D.W.
0.27
---
0.27
1
-
1
1
---
J.
SW846: 6010C
-- ---- -- --
SW846: 6010C
MMSD
- - -- -
MMSD
04/11/19
DM0411/19005650
0.44 mg/kg D.W.
0.27
1
J.
SW846: 6010C
MMSD
04/12/19
DM0412/19005665
0.35 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/13/19
DM0413/19005676
0.46 mg/kg D.W.
0.27
1
J.
SW846: 6010C
MMSD
04/14/19
DM0414/19005695
0.5 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/15/19
DM0415/19005747
0.64 mg/kg D.W.
0.28
1.1
J.
SW846: 6010C
MMSD
04/16/19
DM0416/19005837
0.54 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/17/19
04/18/19
DM0417/19005865
DM0418/19005886
0.48 mg/kg D.W.
0.34 mg/kg D.W.
0.28
0.28
1
1
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/19/19
DM0419/19005901
0.57 mg/kg D.W.
0.27
1
J.
SW846: 6010C
MMSD
04/20/19
DM0420/19005912
0.48 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/21/19
DM0421/19006054
0.46 mg/kg D.W.
0.28
1.1
J.
SW846: 6010C
MMSD
04/22/19
04/23/19
DM0422/19006067
DM0423/19006092
0.48 mg/kg D.W.
0.38 mg/kg D.W.
0.28
0.28
1
1
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/24/19
DM0424/19006120
0.49 mg/kg D.W.
0.27
1
J.
SW846: 6010C
MMSD
04/25/19
DM0425/19006245
0.47 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/26/19
DM0426/19006496
0.47 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/27/19
DM0427/19006507
0.5 mg/kg D.W.
0.27
1
J.
SW846: 6010C
MMSD
04/28/19
DM0428119006526
0.41 mg/kg D.W.
0.27
1
J.
SW846: 6010C
MMSD
04/29/19
DM0429/19006539
0.48 mg/kg D.W.
0.28
1
J.
SW846: 6010C
MMSD
04/30/19
DM0430/19006564
0.48 mg/kg D.W.
0.28
1
1
SW846: 6010C
MMSD
Avg Result: 0.48 mg/kg D.W.
CHROMIUM ICP Dry wt.
Sample Date Sample ID
Min LOD: 0.27 mg/kg D.W.
Result LOD LOQ
., Flags
Max Result: 0.64 mg/kg D.W.
Analytical Method
Lab
04/13/19 WMC15/19005749
Avg Result: 180 mg/kg D.W.
COBALT ICP Dry wt.
pie Date Sample TO
04/13/19 WMC15/19005749
Avg Result: 4.3 mg/kg D.W.
180 mg/kg D.W. 1.7 17
Min LOD: 1.7 mg/kg D.W.
Result LOD LOQ
4.3 mg/kg D.W. 1.2 4.5
Min LOD: 1.2 mg/kg D.W.
.. Flags
88, J.
SW846: 6010C
Analytical Method
SW846: 6010C
MMSD
Lab
MMSD
Page 1 of 1j
SYS/MtIMiloMonthly 1110113 H Printed: 5115119 09:46

f
kNSD
PARAFRS IINS CI.FuR i11Y617Alliy'
COPPER ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ .. Flags
Monthly Milorganite Report
April 2019
Analytical Method Lab
04/01/19
DM0401/19004551
220 mg/kg D.W.
7.7
23
SW846: 6010C
MMSD
04/02/19
DMO402/19004576
220 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/03/19
DM0403/19004770
230 mg/kg D.W.
7
70 Q2.
SW846: 6010C
MMSD
04/04/19
DM0404/19004791
220 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/05/19
DM0405/19004806
220 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/06/19
DM0406/19004817
210 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/07/19
DM0407/19004836
200 mg/kg D.W.
7.1
71
SW846: 6010C
MMSD
04/08/19
DM0408/19004849
200 mg/kg D.W.
7.1
71
SW846: 6010C
MMSD
04/09/19
DM0409/19005069
200 mg/kg D.W.
6.9
69
SW846: 6010C
MMSD
04/10/19
DMO410/19005097
200 mg/kg D.W.
6.9
69
SW846: 6010C
MMSD
04/11/19
DM0411/19005650
200 mg/kg D.W.
6.9
69
SW846: 6010C
MMSD
04/12/19
DMO412/19005665
200 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/13/19
DM0413/19005676
200 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/14/19
DM0414/19005695
200 mg/kg D.W.
7.1
71
SW846: 6010C
MMSD
04/15/19
DM0415/19005747
220 mg/kg D.W.
7.2
72
SW846: 6010C
MMSD
04/16/19
DM0416/19005837
210 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/17/19
04/18/19
DMO417/19005865
DMO418/19005886
200 mg/kg D.W.
220 mg/kg D.W.
7
7
70
70
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/19/19
DM0419/19005901
210 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/20/19
DM0420/19005912
210 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/21/19
DM0421/19006054
200 mg/kg D.W.
7.2
72
SW846: 6010C
MMSD
04/22/19
04/23/19
DM0422/19006067
DMO423/19006092
210 mg/kg D.W.
200 mg/kg D.W.
7
7
70
70
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/24/19
DM0424/19006120
210 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/25/19
DM0425/19006245
200 mg/kg D.W.
7.1
71
SW846: 6010C
MMSD
04/26/19
DMO426/19006496
210 mg/kg D.W.
7.1
71
SW846: 6010C
MMSD
04/27/19
DM0427/19006507
200 mg/kg D.W.
6.9
69
SW846: 6010C
MMSD
04/28/19
DM0428/19006526
200 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/29/19
DM0429/19006539
190 mg/kg D.W.
7
70
SW846: 6010C
MMSD
04/30/19
DM0430/19006564
200 mg/kg D.W.
7
70
SW846: 6010C
MMSD
Avg Result: 210 mg/kg D.W.
FECAL COLIFORM SLUDGE
Date Sample ID
Min LOD: 6.9 mg/kg D.W.
Result LOD LOQ .• Flags
Max Result: 230 mg/kg D.W.
AnatyticalMe"46&i
04/02/19
04/09/19
/19006156
/19006787
< 0.19 MPN/g TS
< 0.19 MPN/g TS
0.19
0.19
EPA 1680
EPA 1680
MMSD
MMSD
04/16/19
/19007266
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
04/23/19
/19007656
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
04/30/19
/19008152
0.21 MPN/g TS
0.19
D2.
EPA 1680
MMSD
Min LOD: 0.19 MPN/g TS
Page 3 o/ 19
SYS/rptiMilbNonth/y 1110113 tj Printed.' 5115119 09:45

''i
1'
NNSD
�11f1�5 i5t 1 tQ11Bl f11MADIHI►
IRON ICP METHOD
Sample Date Sample ID Result LOD LOQ
04/01/19 DM0401/19004551 41000 mg/kg D.W. 260 740
Monthly Milorganite Report
April 2019
SW846: 6010C MMSD
04/02/19
DM0402/19004576
39000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
04/03/19
DM0403/19004770
40000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
04/04/19
DM0404/19004791
40000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
04/05/19
DM0405/19004806
40000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
04/06/19
DM0406/19004817
38000 mg/kg D.W.
57
210
SW846: 6010C
MMSD
04/07/19
DM0407/19004836
36000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
04/08/19
DM0408/19004849
35000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
04/09/19
04/10/19
DM0409/19005069
DM0410/19005097
38000 mg/kg D.W.
36000 mg/kg D.W.
57
56
210
210
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/11/19
DM0411/19005650
38000 mg/kg D.W.
57
210
SW846: 6010C
MMSD
04/12/19
DM0412/19005665
37000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
04/13/19
DM0413/19005676
34000 mg/kg D.W.
57
210
SW846: 6010C
MMSD
04/14/19
DM0414/19005695
32000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
04/15/19
DM0416/19005747
32000 mg/kg D.W.
59
220
SW846: 6010C
MMSD
04/16/19
DM0416/19005837
34000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
04/17/19
04/18/19
DM0417/19005865
DM0418/19005886
33000 mg/kg D.W.
35000 mg/kg D.W.
57
57
210
210
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/19/19
DM0419/19005901
39000 mg/kg D.W.
57
210
SW846: 6010C
MMSD
04/20/19
DM0420/19005912
33000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
04/21/19
DM0421/19006054
33000 mg/kg D.W.
59
220
SW846: 6010C
MMSD
04/22/19
04/23/19
DM0422/19006067
DM0423/19006092
35000 mg/kg D.W.
37000 mg/kg D.W.
57
57
210
210
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/24/19
DM0424/19006120
36000 mg/kg D.W.
57
210
SW846: 6010C
MMSD
04/25/19
DM0425/19006245
36000 mg/kg D.W.
58
220
SW846: 6010C
MMSD
04/26/19
DM0426/19006496
35000 mg/kg D.W.
58
220
SW846: 6010C
MMSD
04/27/19
DM0427/19006507
37000 mg/kg D.W.
57
210
SW846: 6010C
MMSD
04/28/19
DM0428/19006526
34000 mg/kg D.W.
57
210
SW846: 6010C
MMSD
04/29/19
DM0429/19006539
33000 mg/kg D.W.
57
210
SW846: 6010C
MMSD
04/30/19
DM0430/19006564
33000 mg/kg D.W.
58
210
SW846: 6010C
MMSD
Avg Result: 36000 mg/kg D.W.
Min LOD: 56 mg/kg D.W.
Max Result: 41000 mg/kg D.W.
Page 4 of 15
SWMt1MibMonth1y 4110113 t/ Printed.• 5115119 09.45

( fkNSD
s tet � ntuel �gla+eA
LEAD ICP METHOD
Date Sample ID
04/01/19 DMO401/19004551
Result
27 mg/kg D.W.
LOD
4.7
..Analytical
14
Monthly Milorganite Report
April 2019
Method Lab
SW846: 6010C MMSD
04/02/19
DMO402/19004576
28 mg/kg D.W.
3.8
38
3.
SW846: 6010C
MMSD
04/03/19
DM0403/19004770
25 mg/kg D.W.
3.8
38
D2, 3, Q2.
SW846: 6010C
MMSD
04/04/19
DM0404/19004791
24 mg/kg D.W.
3.8
38
3.
SW846: 6010C
MMSD
04/05/19
DM0405/19004806
26 mg/kg D.W.
3.8
38
1
SW846: 6010C
MMSD
04/06/19
DM0406/19004817
39 mg/kg D.W.
3.8
38
SW846: 6010C
MMSD
04/07/19
DM0407/19004836
23 mg/kg D.W.
3.8
38
3.
SW846: 6010C
MMSD
04/08/19
DM0408/19004849
23 mg/kg D.W.
3.8
38
1
SW846: 6010C
MMSD
04/09/19
DM0409/19005069
23 mg/kg D.W.
3.8
38
1
SW846: 6010C
MMSD
04/10/19
DMO410/19005097
24 mg/kg D.W.
3.8
38
1
SW846: 6010C
MMSD
04/11/19
DM0411/19005650
25 mg/kg D.W.
3.8
38
1
SW846: 6010C
MMSD
04/12/19
DM0412/19005665
24 mg/kg D.W.
3.8
38
1
SW846: 6010C
MMSD
04/13/19
DMO413/19005676
25 mg/kg D.W.
3.8
38
3.
SW846: 6010C
MMSD
04/14/19
DM0414/19005695
28 mg/kg D.W.
3.9
39
1
SW846: 6010C
MMSD
04/15/19
DM0415/19005747
31 mg/kg D.W.
3.9
39
1
SW846: 6010C
MMSD
04/16/19
DM0416/19005837
30 mg/kg D.W.
3.8
38
1
SW846: 6010C
MMSD
04/17/19
04/18/19
DM0417/19005865
DM0418/19005886
28 mg/kg D.W.
29 mg/kg D.W.
3.8
3.8
38
38
1
3.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/19/19
DM0419/19005901
30 mg/kg D.W.
3.8
38
3.
SW846: 6010C
MMSD
04/20/19
DM0420/19005912
28 mg/kg D.W.
3.8
38
3.
SW846: 6010C
MMSD
04/21/19
DM0421/19006054
27 mg/kg D.W.
3.9
39
1
SW846: 6010C
MMSD
04/22/19
04/23/19
DM0422/19006067
DM0423/19006092
28 mg/kg D.W.
25 mg/kg O.W.
3.8
3.8
38
38
1.
3.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/24/19
DM0424/19006120
25 mg/kg D.W.
3.8
38
D2, I
SW846: 6010C
MMSD
04/25/19
DM0425/19006245
27 mg/kg D.W.
3.9
39
3.
SW846: 6010C
MMSD
04/26/19
DMO426/19006496
26 mg/kg D.W.
3.9
39
1
SW846: 6010C
MMSD
04/27/19
DM0427/19006507
27 mg/kg D.W.
3.8
38
3.
SW846: 6010C
MMSD
04/28/19
DM0428/19006526
28 mg/kg D.W.
3.8
38
3.
SW846: 6010C
MMSD
04/29/19
DM0429/19006539
29 mg/kg D.W.
3.8
38
3.
SW846: 6010C
MMSD
04/30/19
DM0430/19006564
30 mg/kg D.W.
3.8
38
3.
SW846: 6010C
MMSD
Avg Result: 27 mg/kg D.W.
MERCURY by M. 7471 (sludge)
Date Sample ID
Min LOD: 3.8 mg/kg D.W.
Result LOD LOQ
QA Flags
Max Result: 39 mg/kg D.W.
Analytical Method
Lab
04/06/19
WMC14/19004851
0.14 mg/kg D.W.
0.0054
0.018
EPA 7471B
CT Lab
04/13/19
WMC15/19005749
0.17 mg/kg D.W.
0.0054
0.018
EPA 7471E
Cr Lab
04/20/19
04/27/19
WMC16/19006069
WMC17/19006541
Avg Result: 0.09 mg/kg D.W.
< 0.0058 mg/kg D.W. 0.0058 0.02
0.048 mg/kg D.W. 0.0055 0.019 AX.
Min LOD: 0.0054 mg/kg D.W.
EPA 7471B
EPA 7471E
Max Result: 0.17 mg/kg D.W.
CT Lab
Cr Lab
Page 5 o/ 1j
SYVrptIHj1bMonth/y 1110113 U Printed. • 5115119 09.45

fANSD
1AM lRA tIUa i . .
MOLYBDENUM ICP METHOD
Sample Date Sample ID
04/01/19 DM0401/19004551
Monthly Milorganite Report
April 2019
Result LOD LOQ QA Fla Analytical Method Lab
010
04/02/19
DM0402/19004576
10 mg/kg D.W.
2
8.8
SW846: 6010C
MMSD
04/03/19
DM0403/19004770
10 mg/kg D.W.
2
8.8
SW846: 6010C
MMSD
04/04/19
DM0404/19004791
10 mg/kg D.W.
2
8.8
SW846: 6010C
MMSD
04/05/19
DM0405/19004806
9.9 mg/kg D.W.
2
8.7
SW846: 6010C
MMSD
04/06/19
DM0406/19004817
9.4 mg/kg D.W.
2
8.7
SW846: 6010C
MMSD
04/07/19
DM0407/19004836
8.8 mg/kg D.W.
2
8.8
SW846: 6010C
MMSD
04/08/19
DM0408/19004849
8.9 mg/kg D.W.
2
8.8
SW846: 6010C
MMSD
04/09/19
04/10/19
DM0409/19005069
DM0410/19005097
9 mg/kg D.W.
9.4 mg/kg D.W.
2
2
8.6
8.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/11/19
DM0411/19005650
9 mg/kg D.W.
2
8.6
SW846: 6010C
MMSD
04/12/19
DM0412/19005665
8.8 mg/kg D.W.
2
8.7
SW846: 6010C
MMSD
04/13/19
DM0413/19005676
9.5 mg/kg D.W.
2
8.6
SW846: 6010C
MMSD
04/14/19
DM0414/19005695
9.8 mg/kg D.W.
2
8.8
SW846: 6010C
MMSD
04/15/19
DM0415/19005747
10 mg/kg D.W.
2.1
8.9
SW846: 6010C
MMSD
04/16/19
DM0416/19005837
9.6 mg/kg D.W.
2
8.8
SW846: 6010C
MMSD
04/17/19
04/18/19
DMO417/19005865
DM0418/19005886
9.7 mg/kg D.W.
9.6 mg/kg D.W.
2
2
8.7
8.7
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/19/19
DM0419/19005901
9.9 mg/kg D.W.
2
8.6
SW846: 6010C
MMSD
04/20/19
DM0420/19005912
9.3 mg/kg D.W.
2
8.7
SW846: 6010C
MMSD
04/21/19
DM0421/19006054
9.3 mg/kg D.W.
2.1
8.9
SW846: 6010C
MMSD
04/22/19
04/23/19
DM0422/19006067
DM0423/19006092
9.3 mg/kg D.W.
9.3 mg/kg D.W.
2
2
8.7
8.7
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/24/19
DM0424/19006120
9.3 mg/kg D.W.
2
8.6
SW846: 6010C
MMSD
04/25/19
DM0425/19006245
8.7 mg/kg D.W.
2
8.9
1. SW846: 6010C
MMSD
04/26/19
DM0426/19006496
9 mg/kg D.W.
2
8.8
SW846: 6010C
MMSD
04/27/19
DM0427/19006507
8.9 mg/kg D.W.
2
8.6
SW846: 6010C
MMSD
04/28/19
DM0428/19006526
8.7 mg/kg D.W.
2
8.7
SW846: 6010C
MMSD
04/29/19
DM0429/19006539
8.5 mg/kg D.W.
2
8.7
1. SW846: 6010C
MMSD
04/30/19
DM0430/19006564
9 mg/kg D.W.
2
8.8
SW846: 6010C
MMSD
Avg Result: 9.4 mg/kg D.W.
Min LOD:
1.3 mg/kg D.W.
Max Result: 11 mg/kg D.W.
Page 6 o/13
SYS1MtIHikM&ydW 4110113 0 Printed.5115119 09.45

-
1414SD
�, iat, uiu�t 11HltC#ii1y
NICKEL ICP METHOD
�Sample Date Sample ID
Result
LOD
LOQ
QA Flags
Monthly Milorganite Report
April 2019
Analytical Method Lab
04/01/19 DM0401/19004551
30 mg/kg D.W.
4.5
14
SW846: 6010C
MMSD
04/02/19 DM0402/19004576
27 mg/kg D.W.
9.2
38
J.
SW846: 6010C
MMSD
04/03/19 DM0403/19004770
28 mg/kg D.W.
9.2
38
J.
SW846: 6010C
MMSD
04/04/19 DM0404/19004791
29 mg/kg D.W.
9.2
38
J.
SW846: 6010C
MMSD
04/05/19 DM0405/19004806
25 mg/kg D.W.
9.2
38
J.
SW846: 6010C
MMSD
04/06/19 DMO406/19004817
23 mg/kg O.W.
9.1
38
J.
SW846: 6010C
MMSD
04/07/19 DM0407/19004836
22 mg/kg D.W.
9.2
38
J.
SW846: 6010C
MMSD
04/08/19 DM0408/19004849
22 mg/kg D.W.
9.2
38
J.
SW846: 6010C
MMSD
04/09/19 DM0409/19005069
22 mg/kg D.W.
9
38
J.
SW846: 6010C
MMSD
04/10/19 DM0410/19005097
23 mg/kg D.W.
9
38
J.
SW846: 6010C
MMSD
04/11/19 DM0411/19005650
23 mg/kg D.W.
9
38
J.
SW846: 6010C
MMSD
04/12/19 DM0412/19005665
24 mg/kg D.W.
9.2
38
J.
SW846: 6010C
MMSD
04/13/19 DM0413/19005676
23 mg/kg D.W.
9.1
38
J.
SW846: 6010C
MMSD
04/14/19 DM0414/19005695
24 mg/kg D.W.
9.2
39
J.
SW846: 6010C
MMSD
04/15/19 DM0415/19005747
24 mg/kg D.W.
9.4
39
J.
SW846: 6010C
MMSD
04/16/19 DM0416/19005837
24 mg/kg D.W.
9.2
38
J.
SW846: 6010C
MMSD
04/17/19 DM0417/19005865
04/18/19 DMO418/19005886
24 mg/kg D.W.
41 mg/kg D.W.
9.1
9.1
38
38
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/19/19 DM0419/19005901
35 mg/kg D.W.
9.1
38
J.
SW846: 6010C
MMSD
04/20/19 DM0420/19005912
33 mg/kg D.W.
9.2
38
1.
SW846: 6010C
MMSD
04/21/19 DM0421/19006054
31 mg/kg D.W.
9.4
39
1.
SW846: 6010C
MMSD
04/22/19 DM0422/19006067
04/23/19 DM0423/19006092
31 mg/kg O.W.
30 mg/kg D.W.
9.1
9.1
38
38
J.
1.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/24/19 DM0424/19006120
28 mg/kg D.W.
9.1
38
J.
SW846: 6010C
MMSD
04/25/19 DM0425/19006245
28 mg/kg D.W.
9.3
39
J.
SW846: 6010C
MMSD
04/26/19 DM0426/19006496
27 mg/kg D.W.
9.3
39
J.
SW846: 6010C
MMSD
04/27/19 DM0427/19006507
26 mg/kg D.W.
9
38
J.
SW846: 6010C
MMSD
04/28/19 DM0428/19006526
25 mg/kg D.W.
9.1
38
J.
SW846: 6010C
MMSD
04/29/19 DM0429/19006539
26 mg/kg D.W.
9.1
38
J.
SW846: 6010C
MMSD
04/30/19 DM0430/19006564
29 mg/kg D.W.
9.2
38
J.
SW846: 6010C
MMSD
Avg Result: 27 mg/kg D.W.
NITRATE NITROGEN
Sample Date Sample ID
Min LOD: 4.5 mg/kg D.W.
Result LOD LOQ
QA Flags
Max Result: 41 mg/kg D.W.
Analytical Method
Lab
04/13/19 WMC15/19005749
0.8 %
0.5
AOAC (16) 930.01
MMSD
Avg Result: 0.8 %
NITROGEN-Total(Manual)
Sample Date Sample ID
Min LOD: 0.5 %
Result LOD
LOQ
QA Flags
Analytical Method
Lab
04/13/19 WMC15/19005749
6.9 %
0.11
AOAC (16) 955.04
MMSD
Avg Result: 6.9 %
NITROGEN -Water Insoluble
Sample Date Sample TO
Min LOD: 0.11 %
Result LOD
LOQ
•. Flags
Analytical Method
Lab
04/13/19 WMC15/19005749
5.7 %
0.5
AOAC (16) 945.01
MMSD
Avg Result: 5.7 %
SYS/rptlMitoMonthty 1/10/13 lj
Min LOD: 0.5 °/n
Page 7 of 13
Printed.- 5115119 09.45

tHMSD
PU TIRS FIX ► Q11011MI i1MENt
pH -Solids
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report
April 2019
.• Flags Analytical Method Lab
04/06/19
WMC14/19004851
6.03 Stnd. Units
0.1
SW846: 9045D
MMSD
04/13/19
WMC15/19005749
5.94 Stnd. Units
0.1
SW846: 9045D
MMSD
04/20/19
WMC16/19006069
6.01 Stnd. Units
0.1
SW846: 9045D
MMSD
04/27/19
WMC17/19006541
6.06 Stnd. Units
0.1
SW846: 9045D
MMSD
Avg Result: 6 Stnd. Units
PHOSPHORUS ICP METHOD
Sample Date Sample ID
Min LOD: 0.1 Stnd. Units
Result LOD LOQ
Max Result: 6.06 Stnd. Units
QA Flags Analytical Method
Lab
04/01/19
DM0401/19004551
25000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
04/02/19
DM0402/19004576
24000 mg/kg D.W.
18
83
SW846: 6010C
MMSD
04/03/19
DM0403/19004770
25000 mg/kg D.W.
10
41
Q2. SW846: 6010C
MMSD
04/04/19
DM0404/19004791
26000 mg/kg D.W.
10
41
SW846: 6010C
MMSD
04/05/19
04/06/19
DM0405/19004806
DM0406/19004817
25000 mg/kg D.W.
24000 mg/kg D.W.
10
10
40
40
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/07/19
DM0407/19004836
24000 mg/kg D.W.
10
41
SW846: 6010C
MMSD
04/08/19
DM0408/19004849
24000 mg/kg D.W.
10
41
SW846: 6010C
MMSD
04/09/19
DM0409/19005069
24000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/10/19
DM0410/19005097
25000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/11/19
DM0411/19005650
25000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/12/19
04/13/19
DM0412/19005665
DM0413/19005676
24000 mg/kg D.W.
23000 mg/kg D.W.
10
10
40
40
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/14/19
DM0414/19005695
23000 mg/kg D.W.
10
41
SW846: 6010C
MMSD
04/15/19
04/16/19
DM0415/19005747
DM0416/19005837
23000 mg/kg D.W.
23000 mg/kg D.W.
11
10
41
41
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/17/19
DM0417/19005865
23000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/18/19
DM0418/19005886
24000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/19/19
DM0419119005901
23000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/20/19
DM0420/19005912
23000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/21/19
DM0421/19006054
24000 mg/kg D.W.
11
41
SW846: 6010C
MMSD
04/22/19
DM0422/19006067
24000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/23/19
DM0423/19006092
24000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/24/19
DM0424/19006120
24000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/25/19
DM0425/19006245
23000 mg/kg D.W.
10
41
SW846: 6010C
MMSD
04/26/19
DM0426/19006496
24000 mg/kg D.W.
10
41
SW846: 6010C
MMSD
04/27/19
04/28/19
DM0427/19006507
DM0428/19006526
24000 mg/kg D.W.
23000 mg/kg D.W.
10
10
40
40
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/29/19
DM0429/19006539
23000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
04/30/19
DM0430/19006564
24000 mg/kg D.W.
10
40
SW846: 6010C
MMSD
Avg Result: 24000 mg/kg D.W.
Min LOD:
10 mg/kg D.W.
Max Result: 26000 mg/kg D.W.
Page 8 of 15
SY5/iptlM11bMonth/y 1/10/1311 Printed: 5115119 09:45

1.,
'I" MMSD
P11111Rti F� A QEUER FIl1
POTASSIUM ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ
QA Flags
Monthly Milorganite Report
April 2019
Analytical Method Lab
04/01/19
DM0401/19004551
5300 mg/kg D.W.
140
720
SW846: 6010C
MMSD
04/02/19
DMD402/19004576
5100 mg/kg D.W.
140
470
AO.
SW846: 6010C
MMSD
04/03/19
DM0403/19004770
4800 mg/kg D.W.
140
470
AO.
SW846: 6010C
MMSD
04/04/19
DM0404/19004791
5600 mg/kg D.W.
140
470
AO.
SW846: 6010C
MMSD
04/05/19
DM0405/19004806
5300 mgAg D.W.
140
470
AO.
SW846: 6010C
MMSD
04/06/19
DM0406/19004817
5200 mg/kg D.W.
140
460
AO.
SW846: 6010C
MMSD
04/07/19
DM0407/19004836
5900 mg/kg D.W.
140
470
AO.
SW846-.6010C
MMSD
04/08/19
DM0408/19004849
5900 mg/kg D.W.
140
470
AO.
SW846: 6010C
MMSD
04/09/19
DM0409/19005069
5600 mg/kg D.W.
140
460
AO.
SW846: 6010C
MMSD
04/10/19
DM0410/19005097
4900 mg/kg D.W.
140
460
AO, B8.
SW846: 6010C
MMSD
04/11/19
DM0411/19005650
5100 mg/kg D.W.
140
460
AO.
SW846: 6010C
MMSD
04/12/19
DM0412/19005665
4800 mg/kg D.W.
140
470
AO, B8.
SW846: 6010C
MMSD
04/13/19
DM0413/19005676
5100 mg/kg D.W.
140
460
AO, B8.
SW846: 6010C
MMSD
04/14/19
DM0414/19005695
5200 mg/kg D.W.
140
470
AO, B8.
SW846: 6010C
MMSD
04/15/19
DM0415/19005747
5000 mg/kg D.W.
140
480
AO, B8.
SW846: 6010C
MMSD
04/16/19
DM0416/19006837
5000 mg/kg D.W.
140
470
AO.
SW846: 6010C
MMSD
04/17/19
DMO417/19005865
5100 mg/kg D.W.
140
470
AO.
SW846: 6010C
MMSD
04/18/19
DM0418/19005886
5400 mg/kg D.W.
140
470
AO.
SW846: 6010C
MMSD
04/19/19
DM0419/19005901
5400 mg/kg D.W.
140
460
AO.
SW846: 6010C
MMSD
04/20/19
DM0420/19005912
5200 mg/kg D.W.
140
470
AO, B8.
SW846: 6010C
MMSD
04/21/19
DM0421/19006054
5200 mg/kg D.W.
140
480
AO, B8.
SW846: 6010C
MMSD
04/22/19
04/23/19
DM0422119006067
DM0423/19006092
4700 mg/kg D.W.
4800 mg/kg D.W.
140
140
470
470
AO, B8.
AO, B8.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/24/19
DM0424/19006120
4800 mg/kg D.W.
140
460
AO.
SW846: 6010C
MMSD
04/25/19
DM0425/19006245
4700 mg/kg D.W.
140
480
AO, B8.
SW846: 6010C
MMSD
04/26/19
DM0426/19006496
4700 mg/kg D.W.
140
470
SW846: 6010C
MMSD
04/27/19
DM0427/19006507
4900 mg/kg D.W.
140
460
AO.
SW846: 6010C
MMSD
04/28/19
DM0428/19006526
5400 mg/kg D.W.
140
460
AO.
SW846: 6010C
MMSD
04/29/19
DM0429/19006539
5400 mg/kg D.W.
140
470
AO.
SW846: 6010C
MMSD
04/30/19
DM0430/19006564
5000 mg/kg D.W.
140
470
AO, B8.
SW846: 6010C
MMSD
Avg Result: 5200 mg/kg D.W.
Min LOD:
140 mg/kg D.W.
Max Result: 5900 mg/kg D.W.
Page 9 of 15
SY51rptlMiloMonthly 1110113 tj Pdnted:5115119 09.45

NNSD
P91111 F Fat A WA1B18tAlA1gF811
SELENIUM ICP METHOD
Sample Date Sample ID
Result
LOD
LOQ
QA Flags
Monthly Milorganite Report
April 2019
Analytic I Method Lab
04/01/19
DM0401/19004551
7.1 mg/kg D.W.
6.8
20
J.
SW846: 6010C
MMSD
04/02/19
DM0402/19004576
< 6.6 mg/kg D.W.
6.6
66
SW846: 6010C
MMSD
04/03/19
DM0403/19004770
< 6.6 mg/kg D.W.
6.6
66
Q2.
SW846: 6010C
MMSD
04/04/19
DM0404/19004791
< 6.6 mg/kg D.W.
6.6
66
Q2.
SW846: 6010C
MMSD
04/05/19
DM0405/19004806
< 6.6 mg/kg D.W.
6.6
66
Q2.
SW846: 6010C
MMSD
04/06/19
04/07/19
DM0406/19004817
DM0407/19004836
< 6.6 mg/kg D.W.
< 6.6 mg/kg D.W.
6.6
6.6
66
66
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/08/19
DM0408/19004849
< 6.6 mg/kg D.W.
6.6
66
Q2.
SW846: 6010C
MMSD
04/09/19
04/10/19
DM0409/19005069
DM0410/19005097
< 6.5 mg/kg D.W.
< 6.5 mg/kg D.W.
6.5
6.5
65
65
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/11/19
DM0411/19005650
< 6.5 mg/kg D.W.
6.5
65
Q2.
SW846: 6010C
MMSD
04/12/19
DM0412/19005665
< 6.6 mg/kg D.W.
6.6
66
SW846: 6010C
MMSD
04/13/19
DM0413/19005676
< 6.5 mg/kg D.W.
6.5
65
SW846: 6010C
MMSD
04/14/19
DM0414/19005695
< 6.6 mg/kg D.W.
6.6
66
SW846: 6010C
MMSD
04/15/19
DM0415/19005747
< 6.8 mg/kg D.W.
6.8
68
SW846: 6010C
MMSD
04/16/19
DM0416/19005837
< 6.6 mg/kg D.W.
6.6
66
SW846: 6010C
MMSD
04/17/19
04/18/19
DM0417/19005865
DM0418/19005886
< 6.6 mg/kg D.W.
< 6.6 mg/kg D.W.
6.6
6.6
66
66
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/19/19
DM0419/19005901
< 6.5 mg/kg D.W.
6.5
65
SW846: 6010C
MMSD
04/20/19
DM0420/19005912
< 6.6 mg/kg D.W.
6.6
66
SW846: 6010C
MMSD
04/21/19
DM0421/19006054
< 6.8 mg/kg D.W.
6.8
68
SW846: 6010C
MMSD
04/22/19
04/23/19
DM0422/19006067
DM0423/19006092
< 6.6 mg/kg D.W.
< 6.6 mg/kg D.W.
6.6
6.6
66
66
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/24/19
DM0424/19006120
< 6.5 mg/kg D.W.
6.5
65
SW846: 6010C
MMSD
04/25/19
DM0425/19006245
< 6.7 mg/kg D.W.
6.7
67
SW846: 6010C
MMSD
04/26/19
DM0426/19006496
< 6.7 mg/kg D.W.
6.7
67
SW846: 6010C
MMSD
04/27/19
DM0427/19006507
< 6.5 mg/kg D.W.
6.5
65
SW846: 6010C
MMSD
04/28/19
DM0428/19006526
< 6.5 mg/kg D.W.
6.5
65
SW846: 6010C
MMSD
04/29/19
DM0429/19006539
< 6.6 mg/kg D.W.
6.6
66
SW846: 6010C
MMSD
04/30/19
DM0430/19006564
< 6.6 mg/kg D.W.
6.6
66
SW846: 6010C
MMSD
Avg Result: 0.24 mg/kg D.W.
Min LOD: 6.5 mg/kg D.W.
Max Result: 7.1 mg/kg D.W.
Page 10 of 1j
5Y51rptlM110Month/y 1110113 tj Printed.' 5115119 09:45

fkNSD
Monthly Milorganite Report
April 2019
F111114#S w 1 CHUM E7<lIMAlIHO
Solids (% Moisture)
bampie .. •. •• •Flags -,W Analytical hethod Lab
Daily Composite
04/01/19 DM0401/19004551 6.1 % 0.1 SM 2540 G (1997) MMSD
04/02/19 DM0402/19004576 6.4 % 0.1 SM 2540 G (1997) MMSD
04/03/19
DM0403/19004770
6.5 %
0.1
SM 2540 G (1997)
MMSD
04/04/19
DMO404/19004791
6.4 %
0.1
SM 2540 G (1997)
MMSD
04/05/19
DM0405/19004806
6.2 %
0.1
SM 2540 G (1997)
MMSD
04/06/19
04/07/19
DM0406/19004817
DMO407/19004836
5.3 %
6.6 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
04/08/19
DM0408119004849
6.7 %
0.1 DI.
SM 2540 G (1997)
MMSD
04/09/19
DMO409/19005069
5 %
0.1
SM 2540 G (1997)
MMSD
04/10/19
DM0410/19005097
4.2 %
0.1
SM 2540 G (1997)
MMSD
04/11/19
DMO411/19005650
5 %
0.1
SM 2540 G (1997)
MMSD
04/12/19
DM0412/19005665
6.2 %
0.1
SM 2540 G (1997)
MMSD
04/13/19
DM0413/19005676
5.2 %
0.1
SM 2540 G (1997)
MMSD
04/14/19
DM0414/19005695
6.8 %
0.1
SM 2540 G (1997)
MMSD
04/15/19
DM0415/19005747
8.3 %
0.1
SM 2540 G (1997)
MMSD
04/16/19
DM0416/19005837
6.5 %
0.1
SM 2540 G (1997)
MMSD
04/17/19
DM0417/19005865
5.6 %
0.1
SM 2540 G (1997)
MMSD
04/18/19
DM0418/19005886
6 %
0.1
SM 2540 G (1997)
MMSD
04/19/19
DMO419/19005901
5.2 %
0.1
SM 2540 G (1997)
MMSD
04/20/19
DM0420/19005912
6.2 %
0.1
SM 2540 G (1997)
MMSD
04/21/19
04/22/19
DM0421119006054
DM0422/19006067
8.3 %
5.9 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
04/23/19
DM0423/19006092
5.6 %
0.1
SM 2540 G (1997)
MMSD
04/24/19
DM0424/19006120
5.2 %
0.1
SM 2540 G (1997)
MMSD
04/25/19
DM0425/19006245
7.5 %
0.1
SM 2540 G (1997)
MMSD
04/26/19
DM0426/19006496
7.2 %
0.1
SM 2540 G (1997)
MMSD
04/27/19
DMO427/19006507
4.7 %
0.1
SM 2540 G (1997)
MMSD
04/28/19
DM0428/19006526
5.3 %
0.1
04/29/19
DM0429/19006539
5.8 %
0.1
04/30/19
DM0430/19006564
6.3 %
0.1
Avg Result: 6.1 %
Min LOD:
0.1
Weekly Composite
04/06/19
WMC14/19004851
6 %
0.1
04/13/19 WMC15/19005749
6 % 0.1
04/20/19 WMC16/19006069 6.3 % 0.1
04/27/19 WMC17119006541 6.3 % 0.1
Min LOD: 0.1 °/u
Solids (% Volatile)
Sample Date Sample ID Result LOD
04/13/19 WMC15/19005749 76 % 0.1
Avg Result: 76 "/o Min LOD: 0.1 0/6
SWrptIANOM-thly 1110113 U
SM 2540 G (1997) MMSD
SM 2540 G (1997) MMSD
SM 2540 G (1997) MMSD
Max Result: 8.3
SM 2540 G (1997) MMSD
SM 2540 G (1997) MMSD
SM 2540 G (1997) MMSD
SM 2540 G (1997) MMSD
Methodlytical Lab
SM 2540 G (1997) MMSD
Page 11 of l3
Printed.- 5115119 09:45

�J P.
males
MMSD
wt a CitlABl ern�xlen
ZINC ICP METHOD
Sample Date Sample ID Result LOD LOQ
04/01/19 DM0401/19004551 420 mg/kg D.W. 16 47
Monthly Milorganite Report
April 2019
SW846: 6010C MMSD
04/02/19
DM0402119004576
430 mg/kg D.W.
8.5
85
SW846: 6010C
MMSD
04/03/19
DM0403/19004770
420 mg/kg D.W.
8.6
86
D2, Q2. SW846: 6010C
MMSD
04/04/19
DM0404/19004791
420 mg/kg D.W.
8.5
85
SW846: 6010C
MMSD
04/05/19
DM0405/19004806
400 mg/kg D.W.
8.5
85
SW846: 6010C
MMSD
04/06/19
DM0406/19004817
380 mg/kg D.W.
8.4
84
SW846: 6010C
MMSD
04/07/19
DM0407/19004836
360 mg/kg D.W.
8.6
86
SW846: 6010C
MMSD
04/08/19
DM0408/19004849
360 mg/kg D.W.
8.6
86
SW846: 6010C
MMSD
04/09/19
04/10/19
DM0409/19005069
DM0410/19005097
360 mg/kg D.W.
380 mg/kg D.W.
8.4
8.3
84
83
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/11/19
DM0411/19005650
370 mg/kg D.W.
8.4
84
SW846: 6010C
MMSD
04/12/19
DM0412/19005665
370 mg/kg D.W.
8.5
85
SW846: 6010C
MMSD
04/13/19
DM0413/19005676
380 mg/kg D.W.
8.4
84
SW846: 6010C
MMSD
04/14/19
DM0414/19005695
390 mg/kg D.W.
8.6
86
SW846: 6010C
MMSD
04/15/19
DM0415/19005747
410 mg/kg D.W.
8.7
87
SW846: 6010C
MMSD
04/16/19
DM0416/19005837
400 mg/kg D.W.
8.6
86
SW846: 6010C
MMSD
04/17/19
04/18/19
DM0417/19005865
DM0418/19005886
400 mg/kg D.W.
410 mg/kg D.W.
8.5
8.5
85
85
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/19/19
DM0419/19005901
380 mg/kg D.W.
8.4
84
SW846: 6010C
MMSD
04/20/19
DM0420/19005912
380 mg/kg D.W.
8.S
85
SW846: 6010C
MMSD
04/21/19
DM0421/19006054
380 mg/kg D.W.
8.7
87
SW846: 6010C
MMSD
04/22/19
04/23/19
DM0422/19006067
DM0423/19006092
380 mg/kg D.W.
380 mg/kg D.W.
8.5
8.5
85
85
SW846: 6010C
SW846: 6010C
MMSD
MMSD
04/24/19
DM0424/19006120
370 mg/kg D.W.
8.4
84
SW846: 6010C
MMSD
04/25/19
DM0425/19006245
360 mg/kg D.W.
8.6
86
SW846: 6010C
MMSD
04/26/19
DM0426/19006496
370 mg/kg D.W.
8.6
86
SW846: 6010C
MMSD
04/27/19
DM0427/19006507
370 mg/kg D.W.
8.4
84
SW846: 6010C
MMSD
04/28/19
DM0428/19006526
360 mg/kg D.W.
8.4
84
SW846: 6010C
MMSD
04/29/19
DM0429/19006539
370 mg/kg D.W.
8.5
85
SW846: 6010C
MMSD
04/30/19
DM0430/19006564
380 mg/kg D.W.
8.5
85
SW846: 6010C
MMSD
Avg Result: 380 mg/kg D.W.
Min LOD: 8.3 mg/kg D.W.
Max Result: 430 mg/kg D.W.
Page 12 of IS
SwrptImIlom-mly 1110113 U Printed.• 5115119 09:43

Monthly Milorganite Report
kl4SD April 2019
I Pot � nu,�l
Bagging Milorganite (Outfall 009) BAGGING
FECAL COLIFORM SLUDGE 48".-
..
4/2/19 190061583utfall 009 Bagging < 0.19 MPN/g TS 0.19 N.A. 4/5/19 EPA 1680 MMSD
Solids (% Total) 13>
Date LIMS # Cust ID Site Reported Value MDL .. Flags Analysis Date Method
4/2/19 190061583utfall 009 Bagging 95 % *** 4/3/19 SM 2540 G (1997) MMSD
Shippin
4/2/19 19006157)utfall 008 Shippin < 0.19 MPN/g TS 0.19 N.A.
4/2/19 19006157)utfall008 Shippin 95 %
.SU
Date LIMS # Cust ID Site Reported Value MDL LOQ
4/2/19 19006156 SU < 0.19 MPN/g TS 0.19 N.A.
4/9/19 19006787 SU < 0.19 MPN/g TS 0.19 N.A.
Milorganite (Outfall 008) SHIPPING
FECAL COLIFORM SLUDGE
lethod
jags Analysis Date Iv
4/5/19 EPA 1680 MMSD 3
Solids (% Total) 137
---
lysis '.
te Method
mn
4/3/19 SM 2540 G (1997) MMSD
Milorganite (Outfall 006) PRODUCTION
FECAL COLIFORM SLUDGE 482
.ags Analysis Date Method
4/5/19 EPA 1680 MMSD
4/12/19 EPA 1680 MMSD 3
4/16/19
19007266
SU
< 0.19 MPN/g TS
0.19 N.A.
4/19/19
EPA 1680 MMSD
3
4/23/19
19007656
SU
< 0.19 MPN/g TS
0.19 N.A.
4/26/19
EPA 1680 MMSD
3
4/30/19
19008152
SU
0.21 MPN/g TS
0.19 N.A. D2.
5/3/19
EPA 1680 MMSD
3
Date
LIMS # Cust ID
Site
Reported Value
MDL LOQ Flags
Analysis Date
Solids (% Total)
Method Lab
137
S
4/2/19
19006156
SU
93 %
"'
4/3/19
SM 2540 G (1997) MMSD
3
4/9/19
19006787
SU
94 %
" "'
4/10/19
SM 2540 G (1997) MMSD
3
4/16/19
19007266
SU
94 %
" **'
4/17/19
SM 2540 G (1997) MMSD
3
4/23/19
19007656
SU
95 %
*' **'
4/24/19
SM 2540 G (1997) MMSD
3
4/30/19
19008152
SU
95 %
'*'
5/1/19
SM 2540 G (1997) MMSD
3
Page 1 of 2
SYS1rpt5Genenc4 411 V14 tj Printed: Y15119 12.55

' l"
PIRiNfti f0i 1 ClIL1ER fWliCllMfR?
** The MDL for this test is the lowest level of precision shown, example: 4.1 would be "0.1".
*** The LOQ for this testis the lowest level of precision shown, example: 4.1 would be "0.1".
N.A. The MDL/LOQ is Not Available or Not Applicable for this test.
Column S: Test Status. Not Started=8, Intermediate=7, Final=3, Analyst Approved=12, Not Reportable=15.
Flag Descriptions
AO_ Other -- Flag requires additional explanation
AX Qualified data - see contract lab report
B3 Target analyte detected in method blank > 10% of sample
concentration.
87 LCS recovery was above control limits.
B8 LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
D1 Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
H1 Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
H5 Analysis performed beyond holding time.
Monthly Milorganite Report
April 2019
IS Insufficient sample volume for ana
] Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
LA Not analyzed - lab accident.
M1 Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
M5 Incubator/water bath temperature was outside method
requirements.
M7 Micro sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
SS Reading was not confirmed by a constant weight measurement
SD Supplemental details provided.(Water Quality only.)
T3 The dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA_ BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample exceeded prescribed method temperature range.
Page 2 of 2
SYSIfpOGenedO 4111114 fj Printed 5115119 12 55

MMMSD
PARTNERS FOR A CLEANER ENVIRONMENT
June 14, 2019
O Y&T, T iuffil
�
TO: Todd Schwingle, Dion Doege, Jacob Holbert, Brett Kelly, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom Nowicki, Beth
Stroik, Kori Kenney, Lab File
SUBJECT: Milorganite Monthly Data — May 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of May 2019.
The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin
(Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
Richard Vincent Date
Laboratory Team Supervisor
Report Review By:
6. /4/ /9
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

�j
0 14SD
PidlawAlUmf
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
May 2019
Milorganite Daily Composite
.• Flags Analytical Meth od Lab
05/01/19
DMO501/19006620
6.8 mg/kg D.W.
3
12
J.
SW846: 6010C
MMSD
05/02/19
DM0502/19006641
< 3 mg/kg D.W.
3
12
SW846: 6010C
MMSD
05/03/19
DM0503/19006656
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
05/04/19
DMO504/19006904
< 3 mg/kg D.W.
3
11
SW846: 6010C
MMSD
05/05/19
DM0505/19006923
< 3 mg/kg D.W.
3
11
SW846: 6010C
MMSD
05/06/19
DM0506/19006936
< 3 mg/kg D.W.
3
12
SW846: 6010C
MMSD
05/07/19
DM0507/19007221
3.5 mg/kg D.W.
3
12
J.
SW846: 6010C
MMSD
05/08/19
DM0508/19007289
< 3 mg/kg D.W.
3
11
SW846: 6010C
MMSD
05/09/19
DM0509/19007310
< 3 mg/kg D.W.
3
12
SW846: 6010C
MMSD
05/10/19
DM0510/19007325
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
05/11/19
DMO511/19007336
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
05/12/19
DM0512/19007355
< 3.2 mg/kg D.W.
3.2
12
SW846: 6010C
MMSD
05/13/19
05/14/19
DM0513/19007404
DMO514/19007429
< 3.1 mg/kg D.W.
< 3.1 mg/kg D.W.
3.1
3.1
12
12
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/15/19
05/16/19
DM0515/19007511
DM0516/19007573
3.2 mg/kg D.W.
< 3.1 mg/kg D.W.
3
3.1
11
12
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/17/19
DM0517/19007686
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
05/18/19
DM0518/19007697
< 3 mg/kg D.W.
3
12
Q3.
SW846: 6010C
MMSD
05/19/19
DM0519/19007716
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
05/20/19
DM0520/19008185
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
05/21/19
DM0521/19008212
< 3.1 mg/kg D.W.
3.1
12
Q3.
SW846: 6010C
MMSD
05/22/19
DM0522/19008240
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
05/23/19
DM0523/19008270
< 3.1 mg/kg D.W.
3.1
12
Q3.
SW846: 6010C
MMSD
05/24/19
DM0524/19008285
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
05/25/19
DM0525/19008316
4.3 mg/kg D.W.
3.1
12
J.
SW846: 6010C
MMSD
05/26/19
DM0526/19008335
5.1 mg/kg D.W.
3.1
12
J.
SW846: 6010C
MMSD
05/27/19
05/28/19
DM0527/19008348
DM0528/19008373
4.5 mg/kg D.W.
5.1 mg/kg D.W.
3
3
12
12
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/29/19
DMO529/19008430
4.8 mg/kg D.W.
3.1
12
J.
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
< 3 mg/kg D.W.
3
11
Q3.
SW846: 6010C
MMSD
05/31/19
0100531/19008495
5.2 mg/kg D.W.
3
11
J.
SW846: 6010C
MMSD
Avg Result: 1.4 mg/kg D.W.
Min LOD:
3 mg/kg
D.W.
Max Result: 6.8 mg/kg D.W.
Page 1 of 16
5Y5/rpt1M11oMonth1yDW 4126119 t/ Printed. 611311914:33

SH145D
POW tgt A Cl k
CADMIUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
May 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
05/01/19
DM0501/19006620
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
05/02/19
DMO502/19006641
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
05/03/19
DM0503/19006656
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
05/04/19
DM0504/19006904
< 0.9 mg/kg D.W.
0.9
3.4
SW846: 6010C
MMSD
05/05/19
DMO505/19006923
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
05/06/19
DM0506/19006936
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
05/07/19
DM0507/19007221
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
05/08/19
DM0508/19007289
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
05/09/19
DMO509/19007310
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
05/10/19
DM0510/19007325
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
05/11/19
DM0511/19007336
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
05/12/19
DMO512/19007355
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
05/13/19
DMO513/19007404
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
05/14/19
DMO514/19007429
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
05/15/19
DMO515/19007511
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
05/16/19
DMO516/19007573
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
05/17/19
DM0517/19007686
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
05/18/19
DMO518/19007697
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
05/19/19
DMO519/19007716
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
05/20/19
05/21/19
DMO520/19008185
DM0521/19008212
< 0.92 mg/kg D.W.
< 0.93 mg/kg D.W.
0.92
0.93
3.5
3.5
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/22/19
DM0522/19008240
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
05/23/19
DM0523/19008270
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
05/24/19
DM0524/19008285
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
05/25/19
DMO525/19008316
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
05/26/19
DMO526/19008335
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
05/27/19
DMO527/19008348
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
05/28/19
DM0528/19008373
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
05/29/19
DM0529/19008430
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
< 0.9 mg/kg D.W.
0.9
3.4
SW846: 6010C
MMSD
05/31/19
DMO531/19008495
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
0.9 mg/kg D.W.
Page 2 of 16
5Y5/rpt1Mi/oMonth/yDW 4126119 tj Printed: 611311914:33

Monthly Milorganite Report DW
14SD May 2019 14
PO NEIiISACI
Milorganite Daily Composite
COPPER ICP Dry wt.
barnpie
05/O1/19
DM0501/19006620
210 mg/kg D.W.
6.6
25
- vi
SW846: 6010C
r
MMSD
05/02/19
DM0502/19006641
210 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
05/03/19
DM0503/19006656
210 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
OS/04/19
DM0504/19006904
210 mg/kg D.W.
6.5
25
SW846: 6010C
MMSD
05/05/19
DM0505/19006923
210 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
05/06/19
DM0506/19006936
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
05/07/19
DM0507/19007221
200 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
05/08/19
DM0508/19007289
200 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
O5/09/19
05/10/19
DM0509/19007310
DM0510119007325
200 mg/kg D.W.
200 mg/kg D.W.
6.6
6.6
25
25
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/11/19
DM0511/19007336
200 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
05/12/19
DM0512/19007355
210 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
05/13/19
DM0513/19007404
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
05/14/19
DM0514/19007429
210 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
05/15/19
O5/16/19
DM0515/19007511
DM0516/19007573
210 mg/kg D.W.
200 mg/kg D.W.
6.6
6.7
25
26
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/17/19
DM0517/19007686
210 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
05/18/19
DM0518/19007697
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
05/19/19
DM0519119007716
220 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
05/20/19
05/21/19
DM0520/19008185
DM0521/19008212
220 mg/kg D.W.
220 mg/kg D.W.
6.6
6.7
25
26
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/22/19
DM0522119008240
230 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
05/23/19
DM0523119008270
220 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
05/24/19
DM0524/19008285
200 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
05/25/19
DM0525/19008316
230 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
05/26/19
DM0526/19008335
230 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
05/27/19
DM0527/19008348
230 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
05/28/19
DM0528/19008373
240 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
05/29/19
DM0529/19008430
230 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
05/31/19
DM0531/19008495
Avg Result: 210 mg/kg D.W.
210 mg/kg D.W. 6.6 25
Min LOD: 6.5 mg/kg D.W.
SW846: 6010C
Max Result: 240 mg/kg D.W.
MMSD
Page 3 of 16
SY51rptlMi1o1Vonth1yDW 4126119 tj Printed: 611311914:33

j
k14SD
i9tA ct�t6tlat
IRON ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ QA
Monthly Milorganite Report DW
May 2019
Milorganite Daily Composite
Flags Analytical Method Lab
05/01/19
DM0501/19006620
33000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/02/19
DM0502119006641
38000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/03/19
DMO503/19006656
37000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/04/19
DM0504119006904
36000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/05/19
DM0505/19006923
38000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/06/19
DM0506/19006936
39000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/07/19
DMO507/19007221
34000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/08/19
DMO508/19007289
34000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/09/19
DMO509/19007310
35000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/10/19
DMO510/19007325
34000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/11/19
DMO511/19007336
35000 mg/kg D.W.
250
2500
SW846: 6010C
MMSD
05/12/19
DM0512/19007355
35000 mg/kg D.W.
250
2500
SW846: 6010C
MMSD
05/13/19
DM0513/19007404
36000 mg/kg D.W.
250
2500
SW846: 6010C
MMSD
05/14/19
DM0514/19007429
36000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/15/19
05/16/19
DMO515/19007511
DM0516/19007573
34000 mg/kg D.W.
34000 mg/kg D.W.
240
240
2400
2400
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/17/19
DMO517119007686
37000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/18/19
DM0518/19007697
37000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/19/19
DM0519/19007716
35000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/20/19
DMO520/19008185
36000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/21/19
DMO521/19008212
35000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/22/19
DM0522/19008240
42000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/23/19
DM0523/19008270
35000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/24/19
DM0524/19008285
40000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/25/19
DM0525119008316
42000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/26/19
DMO526/19008335
41000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/27/19
DM0527/19008348
42000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/28/19
DM0528/19008373
44000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/29/19
DM0529/19008430
37000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
40000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
05/31/19
DMO531/19008495
35000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
Avg Result: 37000 mg/kg D.W.
Min LOD:
240 mg/kg
D.W.
Max Result: 44000 mg/kg D.W.
Page 4 of 16
SY5/rptlMiloMonthlyDW 4126119 tj Printed. 611311914.33

�j
NSD
eu11� tot � tlEtitet �
LEAD ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
May 2019
Milorganite Daily Composite
QA Flags An I a 11 1 11 y , tica I I I M I e6l od
05/01/19
DM0501/19006620
32 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/02/19
DM0502/19006641
31 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/03/19
DM0503/19006666
32 mg/kg D.W.
2.9
11
SW846: 6010C
MMSD
05/04/19
DM0504/19006904
32 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/05/19
DMO505/19006923
33 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/06/19
DM0506/19006936
35 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/07/19
DM0507/19007221
37 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/08/19
DM0508/19007289
32 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/09/19
DM0509/19007310
34 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/10/19
DM0510/19007325
34 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/11/19
DMO511/19007336
34 mg/kg D.W.
2.9
11
SW846: 6010C
MMSD
05/12/19
DMO512/19007355
37 mg/kg D.W.
2.9
11
SW846: 6010C
MMSD
05/13/19
DMO513/19007404
36 mg/kg D.W.
2.9
11
SW846: 6010C
MMSD
05/14/19
DMO514/19007429
36 mg/kg D.W.
2.9
11
SW846: 6010C
MMSD
05/15/19
05/16/19
DM0515/19007511
DM0516/19007573
36 mg/kg D.W.
35 mg/kg D.W.
2.8
2.9
10
11
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/17/19
DMO517/19007686
35 mg/kg D.W.
2.9
11
SW846: 6010C
MMSD
05/18/19
DMO518/19007697
43 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/19/19
DM0519/19007716
35 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/20/19
05/21/19
DMO520/19008185
DM0521/19008212
35 mg/kg D.W.
34 mg/kg D.W.
2.8
2.9
10
11
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/22/19
05/23/19
05/24/19
05/25/19
DM0522/19008240
DMO523/19008270
DM0524/19008285
DMO525/19008316
36 mg/kg D.W.
35 mg/kg D.W.
38 mg/kg D.W.
38 mg/kg D.W.
2.9
2.9
2.9
2.9
11
11
11
11
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
05/26/19
DM0526/19008335
42 mg/kg D.W.
2.9
11
SW846: 6010C
MMSD
05/27/19
DMO527/19008348
44 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/28/19
DMO528/19008373
43 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/29/19
DM0529/19008430
46 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
46 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
05/31/19
DMO531/19008495
47 mg/kg D.W.
2.8
10
SW846: 6010C
MMSD
Avg Result: 37 mg/kg D.W.
Min LOD:
2.8 mg/kg D.W.
Max Result: 47 mg/kg D.W.
Page 5 of 16
5Y5/rptlM11oM0nth1Y0W 4126119 tj Printed. • 611311914:33

MOLYBDENUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Mllorganite Report DW
May 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
05/01/19
DM0501/19006620
9.5 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/02/19
DM0502/19006641
8.9 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/03/19
DM0503119006656
9 mg/kg D.W.
2
7.6
SW846: 6010C
MMSD
05/04/19
DMO504/19006904
9 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/05/19
DMO505/19006923
9.7 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/06/19
DM0506/19006936
9.7 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/07/19
DM0507/19007221
9.3 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
05/08/19
DMOS08/19007289
9.2 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/09/19
DMO509/19007310
8.6 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/10/19
DMO510/19007325
8.6 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
05/11/19
DM0511/19007336
8.9 mg/kg D.W.
2
7.6
SW846: 6010C
MMSD
05/12/19
DMO512/19007355
9.5 mg/kg D.W.
2.1
7.7
SW846: 6010C
MMSD
05/13/19
DM0513/19007404
9.8 mg/kg D.W.
2
7.7
SW846: 6010C
MMSD
05/14/19
DM0514/19007429
9.5 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
05/15/19
DM0515/19007511
9.3 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/16/19
DM0516/19007573
9.2 mg/kg D.W.
2
7.6
SW846: 6010C
MMSD
05/17/19
DMO517/19007686
9.1 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
05/18/19
DM0518/19007697 '
10 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/19/19
DMO519/19007716
9.7 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
05/20/19
05/21/19
DM0520/19008185
DMO521/19008212
9.9 mg/kg D.W.
9.7 mg/kg D.W.
2
2
7.5
7.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/22/19
DMO522/19008240
9.5 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
05/23/19
DM0523/19008270
9.6 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
05/24/19
DM0524/19008285
9.1 mg/kg D.W.
2
7.6
SW846: 6010C
MMSD
05/25/19
DM0525/19008316
9.5 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
05/26/19
DM0526/19008335
9.3 mg/kg D.W.
2
7.6
SW846: 6010C
MMSD
05/27/19
DM0527/19008348
9 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/28/19
DMO528/19008373
9.3 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
05/29/19
DMO529/19008430
9.7 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
9.8 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
05/31/19
DM0531/19008495
9.4 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
Avg Result: 9.4 mg/kg D.W.
Min LOD:
2 mg/kg
D.W.
Max Result: 10 mg/kg D.W.
Page 6 of 16
5Y51rptlM11oMonth1yDW 4126119 h Printed.- 611311914:33

SN14SD
pip 3(15101 Act
NICKEL ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
May 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
05/01/19
DM0501/19006620
28 mg/kg D.W.
3.1
30
3.
SW846: 6010C
MMSD
05/02/19
DM0502/19006641
28 mg/kg D.W.
3.1
30
3.
SW846: 6010C
MMSD
05/03/19
DMO503119006656
26 mg/kg D.W.
3.2
31
3.
SW846: 6010C
MMSD
05/04/19
DMO504/19006904
26 mg/kg D.W.
3.1
30
3.
SW846: 6010C
MMSD
05/05/19
DMO505/19006923
28 mg/kg D.W.
3.1
30
1
SW846: 6010C
MMSD
05/06/19
DMO506/19006936
29 mg/kg D.W.
3.1
30
3.
SW846: 6010C
MMSD
05/07/19
DM0507/19007221
30 mg/kg D.W.
3.2
30
3.
SW846: 6010C
MMSD
05/08/19
DM0508/19007289
26 mg/kg D.W.
3.1
30
3.
SW846: 6010C
MMSD
05/09/19
DM0509/19007310
26 mg/kg D.W.
3.1
30
3.
SW846: 6010C
MMSD
05/10/19
DM0510/19007325
25 mg/kg D.W.
3.2
31
3.
SW846: 6010C
MMSD
05/11/19
DM0511/19007336
25 mg/kg D.W.
3.2
31
3.
SW846: 6010C
MMSD
05/12/19
05/13/19
05/14/19
05/15/19
05/16/19
DM0512/19007355
DM0513/19007404
DM0514/19007429
DM0515/19007511
DM0516/19007573
27 mg/kg D.W.
26 mg/kg D.W.
25 mg/kg D.W.
25 mg/kg D.W.
26 mg/kg D.W.
3.3
3.2
3.2
3.1
3.2
32
31
31
30
31
3.
3.
3.
3.
3.
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
MMSD
05/17/19
DMO517/19007686
26 mg/kg D.W.
3.2
31
3.
SW846: 6010C
MMSD
05/18/19
DM0518/19007697
27 mg/kg D.W.
3.1
30
3.
SW846: 6010C
MMSD
05/19/19
DM0519/19007716
26 mg/kg D.W.
3.2
31
3.
SW846: 6010C
MMSD
05/20/19
05/21/19
DM0520/19008185
DM0521/19008212
25 mg/kg D.W.
25 mg/kg D.W.
3.2
3.2
31
31
3.
3.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/22/19
DMO522/19008240
29 mg/kg D.W.
3.2
31
3.
SW846: 6010C
MMSD
05/23/19
DMO523/19008270
26 mg/kg D.W.
3.2
31
3.
SW846: 6010C
MMSD
05/24/19
DMO524/19008285
31 mg/kg D.W.
3.2
31
SW846: 6010C
MMSD
05/25/19
DM0525/19008316
29 mg/kg D.W.
3.2
31
3.
SW846: 6010C
MMSD
05/26/19
05/27/19
DM0526/19008335
DM0527/19008348
29 mg/kg D.W.
29 mg/kg D.W.
3.2
3.1
31
30
3.
3.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/28/19
DMO528/19008373
29 mg/kg D.W.
3.2
30
3.
SW846: 6010C
MMSD
05/29/19
05/30/19
DMO529/19008430
DMO530/19008480
27 mg/kg D.W.
26 mg/kg D.W.
3.2
3.1
31
30
3.
3.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/31/19
DM0531/19008495
Avg Result: 27 mg/kg D.W.
25 mg/kg D.W.
Min LOD:
3.1 30
3.1 mg/kg D.W.
3.
SW846: 6010C
Max Result: 31 mg/kg D.W.
MMSD
Page 7 of 16
SYS1rpt1Ni1aMonth/yDW 4126119 tj Printed: 6113119 14:3j

i ku
PHOSPHORUS ICP Dry wt.
sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
May 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
05/01/19
DM0501/19006620
24000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
05/02/19
DMO502/19006641
24000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
05/03/19
DMO503/19006656
24000 mg/kg D.W.
9.2
92
SW846: 6010C
MMSD
05/04/19
DMO504/19006904
23000 mg/kg D.W.
8.9
89
SW846: 6010C
MMSD
05/05/19
DMO505/19006923
23000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
05/06/19
DMO506/19006936
24000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
05/07/19
DM0507/19007221
23000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
05/08/19
DM0508/19007289
23000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
05/09/19
DM0509/19007310
23000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
05/10/19
DMO510/19007325
24000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
05/11/19
DM0511/19007336
23000 mg/kg D.W.
9.2
92
SW846: 6010C
MMSD
05/12/19
DMO512/19007355
23000 mg/kg D.W.
9.4
94
SW846: 6010C
MMSD
05/13/19
DM0513/19007404
23000 mg/kg D.W.
9.3
93
SW846: 6010C
MMSD
05/14/19
DM0514/19007429
23000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
05/15/19
DM0515/19007511
23000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
05/16/19
DM0516/19007573
23000 mg/kg D.W.
9.2
92
SW846: 6010C
MMSD
05/17/19
DM0517/19007686
24000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
05/18/19
DM0518/19007697
24000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
05/19/19
DM0519119007716
24000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
05/20/19
DM0520/19008185
24000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
05/21/19
DM0521/19008212
24000 mg/kg D.W.
9.2
92
SW846: 6010C
MMSD
05/22/19
DMO522/19008240
25000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
05/23/19
DMO523/19008270
24000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
05/24/19
DMO524/19008285
25000 mg/kg D.W.
9.2
92
SW846: 6010C
MMSD
05/25/19
OM0525/19008316
25000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
05/26/19
DM0526/19008335
24000 mg/kg D.W.
9.2
92
SW846: 6010C
MMSD
05/27/19
DMO527/19008348
24000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
05/28/19
DMO528/19008373
24000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
05/29/19
DM0529/19008430
23000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
23000 mg/kg D.W.
8.9
89
SW846: 6010C
MMSD
05/31/19
DM0531/19008495
23000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
Avg Result: 24000 mg/kg D.W.
Min LOD:
8.9 mg/kg D.W.
Max Result: 25000 mg/kg D.W.
Page 8 aF16
5Y51rptlM1/oMonth/yDW 4126119 Y Printed: 6113119 14.33

Monthly Milorganite Report DW
1 M14SD May 2019
1:u" FK A Q
Milorganite Daily Composite
POTASSIUM ICP Dry wt.
sample Date
05/01/19
sample ID
DMO501/19006620
Result
4800 mg/kg D.W.
LOD
280
Log
2800
AO, B8.
SW846: 6010C
MMSD
05/02/19
DM0502/19006641
5000 mg/kg D.W.
280
2800
AO.
SW846: 6010C
MMSD
05/03/19
DM0503/19006656
4800 mg/kg D.W.
290
2900
AO.
SW846: 6010C
MMSD
05/04/19
DM0504/19006904
5200 mg/kg D.W.
280
2800
AO.
SW846: 6010C
MMSD
05/05/19
DM0505/19006923
4800 mg/kg D.W.
280
2800
AO.
SW846: 6010C
MMSD
05/06/19
DM0506/19006936
4800 mg/kg D.W.
280
2800
AO.
SW846: 6010C
MMSD
05/07/19
DM0507/19007221
5200 mg/kg D.W.
280
2800
AO.
SW846: 6010C
MMSD
05/08/19
DM0508/19007289
4700 mg/kg D.W.
280
2800
AO, B8.
SW846: 6010C
MMSD
05/09/19
DMO509/19007310
5000 mg/kg D.W.
280
2800
AO, B8.
SW846: 6010C
MMSD
05/10/19
DM0510/19007325
5800 mg/kg D.W.
280
2800
AO.
SW846: 6010C
MMSD
05/11/19
DM0511/19007336
5400 mg/kg D.W.
290
2900
AO.
SW846: 6010C
MMSD
05/12/19
DM0512/19007355
5200 mg/kg D.W.
290
2900
AO.
SW846: 6010C
MMSD
05/13/19
DMO513/19007404
5100 mg/kg D.W.
290
2900
AO.
SW846: 6010C
MMSD
05/14/19
DMO514/19007429
5300 mg/kg D.W.
290
2900
AO.
SW846: 6010C
MMSD
05/15/19
05/16/19
DMO515/19007511
DM0516/19007573
5200 mg/kg D.W.
5300 mg/kg D.W.
280
290
2800
2900
AO, B8.
AO.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/17/19
DM0517/19007686
5700 mg/kg D.W.
290
2900
AO, Q3.
SW846: 6010C
MMSD
05/18/19
05/19/19
05/20/19
05/21/19
05/22/19
DM0518/19007697
DM0519/19007716
DM0520/19008185
DM0521/19008212
DM0522/19008240
5100 mg/kg D.W.
4800 mg/kg D.W.
4800 mg/kg D.W.
4800 mg/kg D.W.
4900 mg/kg D.W.
280
280
280
290
290
2800
2800
2800
2900
2900
AO.
AO.
AO.
AO.
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
MMSD
05/23/19
DM0523/19008270
4500 mg/kg D.W.
290
2900
AO.
SW846: 6010C
MMSD
05/24/19
DMO524/19008285
4500 mg/kg D.W.
290
2900
SW846: 6010C
MMSD
05/25/19
DM0525/19008316
5000 mg/kg D.W.
290
2900
SW846: 6010C
MMSD
05/26/19
DMO526/19008335
5000 mg/kg D.W.
290
2900
SW846: 6010C
MMSD
05/27/19
DM0527/19008348
4900 mg/kg D.W.
280
2800
SW846: 6010C
MMSD
05/28/19
DMO528119008373
4900 mg/kg D.W.
280
2800
SW846: 6010C
MMSD
05/29/19
DMO529119008430
4600 mg/kg D.W.
280
2800
AO.
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
4400 mg/kg D.W.
280
2800
AO.
SWB46: 6010C
MMSD
05/31/19
DM0531/19008495
4600 mg/kg D.W.
280
2800
AO, B8.
SW846: 6010C
MMSD
Avg Result: 5000 mg/kg D.W.
Min LOD:
280 mg/kg D.W.
Max Result: 5800 mg/kg D.W.
Page 9 o/16
5Y5/rpt1MiloMonth/yDW 4126119 tj Printed: 611311914:33

kNSD
W"F6tA ciiu0
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Mllorganite Report DW
May 2019
Milorganite Daily Composite
.. Flags Analytical Method Lab
05/01/19
DM0501/19006620
5.7 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/02/19
DMO502/19006641
4.7 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/03/19
DM0503/19006656
5.3 mg/kg D.W.
4.2
42
J.
SW846: 6010C
MMSD
05/04/19
DM0504/19006904
5.5 mg/kg D.W.
4
40
J.
SW846: 6010C
MMSD
05/05/19
DM0505/19006923
6.2 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/06/19
DM0506/19006936
5 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/07/19
DMO507/19007221
7.1 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/08/19
DMO508/19007289
4.6 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/09/19
DM0509/19007310
4.6 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/10/19
DM0510/19007325
5.8 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/11/19
DM0511/19007336
5 mg/kg D.W.
4.2
42
J, Q2.
SW846: 6010C
MMSD
05/12/19
DMO512/19007355
4.8 mg/kg D.W.
4.2
42
J.
SW846: 6010C
MMSD
05/13/19
DM0513/19007404
6.6 mg/kg D.W.
4.2
42
J.
SW846: 6010C
MMSD
05/14/19
DM0514119007429
6.8 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/15/19
DM0515/19007511
6.5 mg/kg D.W.
4.1
41
1
SW846: 6010C
MMSD
OS/16/19
DM0516/19007573
6.2 mg/kg D.W.
4.2
42
J.
SW846: 6010C
MMSD
05/17/19
DMO517/19007686
6.4 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/18/19
DM0518/19007697
7.3 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/19/19
DMO519/19007716
S.6 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/20/19
05/21/19
DM0520/19008185
DMO521/19008212
5.3 mg/kg D.W.
7.3 mg/kg D.W.
4.1
4.2
41
42
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/22/19
DM0522/19008240
4.8 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/23/19
DM0523/19008270
< 4.1 mg/kg D.W.
4.1
41
SW846: 6010C
MMSD
05/24/19
DM0524/19008285
7.7 mg/kg D.W.
4.2
42
J.
SW846: 6010C
MMSD
05/25/19
DMO525/19008316
< 4.1 mg/kg D.W.
4.1
41
SW846: 6010C
MMSD
05/26/19
DM0526/19008335
< 4.2 mg/kg D.W.
4.2
42
SW846: 6010C
MMSD
05/27/19
DM0527/19008348
<4.1 mg/kg D.W.
4.1
41
SW846: 6010C
MMSD
05/28/19
DM0528/19008373
< 4.1 mg/kg D.W.
4.1
41
SW846: 6010C
MMSD
05/29/19
DMO529/19008430
7.4 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
6.4 mg/kg D.W.
4
40
J.
SW846: 6010C
MMSD
05/31/19
DM0531/19008495
6.6 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
Avg Result: 5 mg/kg D.W.
Min LOD: 4 mg/kg
D.W.
Max Result: 7.7 mg/kg D.W.
Page 10 of 16
5Y5/rpt1Mi16Nonth/yDW 4126119 tj Printed. 6113119 1433

j
ONSD
PAiltlS IN A t!#iiAt
Solids (% Moisture)
'iarnpl. Date Sarnple ID
Result
LOD
Monthly Milorganite Report DW
May 2019
Milorganite Daily Composite
LOQ QA Flags A aijilcal Method
05/01/19
DMO501/19006620
4.7 %
0.1
SM 2540 G (1997)
MMSD
05/02/19
DM0502/19006641
4.6 %
0.1
SM 2540 G (1997)
MMSD
05/03/19
DMO503/19006656
6.4 %
0.1
SM 2540 G (1997)
MMSD
05/04/19
DMO504/19006904
3.6 %
0.1
SM 2540 G (1997)
MMSD
05/05/19
DM0505/19006923
4 %
0.1
SM 2540 G (1997)
MMSD
05/06/19
OM0506/19006936
4.5 %
0.1
SM 2540 G (1997)
MMSD
05/07/19
DMO507/19007221
5 %
0.1
SM 2540 G (1997)
MMSD
05/08/19
DMO508/19007289
4.2 %
0.1
SM 2540 G (1997)
MMSD
05/09/19
DM0509/19007310
4.4 %
0.1
SM 2540 G (1997)
MMSD
05/10/19
DMO510/19007325
5.3 %
0.1
SM 2540 G (1997)
MMSD
05/11/19
DM0511/19007336
6.6 %
0.1
SM 2540 G (1997)
MMSD
OS/12/19
DM0512/19007355
8.2 %
0.1
SM 2540 G (1997)
MMSD
05/13/19
DM0513/19007404
7.6 %
0.1
SM 2540 G (1997)
MMSD
05/14/19
DMO514/19007429
5.9 %
0.1
SM 2540 G (1997)
MMSD
05/15/19
05/16/19
DM0515/19007511
DMO516/19007573
4.2 %
6.3 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
05/17/19
DM0517/19007686
5.8 %
0.1
SM 2540 G (1997)
MMSD
05/18/19
DM0518/19007697
4.7 %
0.1
SM 2540 G (1997)
MMSD
05/19/19
DM0519/19007716
5.4 %
0.1
SM 2540 G (1997)
MMSD
05/20/19
05/21/19
DM0520/19008185
DM0521/19008212
5.4 %
6.2 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
05/22/19
DM0522/19008240
5.8 %
0.1
SM 2540 G (1997)
MMSD
05/23/19
DM0523/19008270
5.8 %
0.1
SM 2540 G (1997)
MMSD
05/24/19
DMO524/19008285
6.1 %
0.1
SM 2540 G (1997)
MMSD
05/25/19
DM0525/19008316
5.8 %
0.1
SM 2540 G (1997)
MMSD
05/26/19
DM0526/19008335
6.2 %
0.1
SM 2540 G (1997)
MMSD
05/27/19
DMO527/19008348
4.4 %
0.1
SM 2540 G (1997)
MMSD
05/28/19
DM0528/19008373
5.2 %
0.1
SM 2540 G (1997)
MMSD
05/29/19
DM0529/19008430
5.6 %
0.1
SM 2540 G (1997)
MMSD
05/30/19
DMO530/19008480
3.8 %
0.1
SM 2540 G (1997)
MMSD
05/31/19
DM0531/19008495
Avg Result: 5.4 %
4.2 %
Min LOD:
0.1
0.1 %
SM 2540 G (1997)
Max Result: 8.2 %
MMSD
Page 11 of 16
SY5/rptJHi1bMonth1yDW 4126119 tj Printed.- 611311914:33

ANSD
I'#1i[�S �t 1 CIEAiI�
ZINC ICP Dry wt.
'Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
May 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab MMI
05/01/19
DM0501/19006620
400 mg/kg D.W.
18
180
SW846: 6010C
j
MMSD
05/02/19
DM0502/19006641
380 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/03/19
DM0503/19006656
390 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/04/19
DM0504/19006904
390 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/05/19
DM0505/19006923
400 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/06/19
DM0506119006936
410 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/07/19
DM0507/19007221
390 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/08/19
DM0508/19007289
380 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/09/19
DM0509/19007310
370 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/10/19
DM0510/19007325
370 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/11/19
DM0511/19007336
390 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/12/19
DM0512/19007355
410 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/13/19
DM0513119007404
410 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/14/19
DM0514/19007429
400 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/15/19
05/16/19
DM0515/19007511
DMO516/19007573
400 mg/kg D.W.
400 mg/kg D.W.
18
18
180
180
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/17/19
DM0517/19007686
410 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/18/19
DMO518/19007697
430 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/19/19
DM0519/19007716
420 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/20/19
DM0520/19008185
420 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/21/19
DMO521/19008212
420 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/22/19
DM0522/19008240
450 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/23/19
DMO523/19008270
420 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/24/19
DMO524/19008285
440 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/25/19
DM0525/19008316
450 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/26/19
DM0526/19008335
450 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/27/19
DM0527/19008348
460 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/28/19
DMO528/19008373
470 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/29/19
DMOS29/19008430
440 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
420 mg/kg D.W.
18
180
SW846: 6010C
MMSD
05/31/19
DM0531/19008495
420 mg/kg D.W.
18
180
SW846: 6010C
MMSD
Avg Result: 410 mg/kg D.W.
Min LOD: 18 mg/kg D.W.
Max Result: 470 mg/kg D.W.
Page 11 of 16
5Y51rptlM1/oM6nth/yDW 4126119 tj Printed. 611311914:3j

PAR11105raIcum
Phosphorus - Total % DW (Calc.)
Sample Date Sample To
Result
LOD..
Monthly Milorganite Report DW
May 2019
Milorganite Daily Composite
.: Flags Anaiji6i Method 661
05/01/19
DMO501/19006620
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/02/19
DMO502/19006641
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/03/19
DM0503/19006656
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/04/19
DMO504/19006904
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/05/19
DMO505/19006923
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/06/19
DM0506/19006936
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/07/19
DM0507/19007221
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/08/19
DM0508/19007289
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/09/19
DM0509/19007310
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/10/19
DM0510/19007325
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/11/19
DM0511/19007336
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/12/19
DM0512/19007355
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/13/19
DM0513/19007404
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/14/19
DMO514/19007429
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/15/19
05/16/19
DM0515/19007511
DMO516/19007573
2.3 % D.W.
2.3 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/17/19
DMO517/19007686
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/18/19
DM0518/19007697
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/19/19
DM0519/19007716
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/20/19
05/21/19
DM0520/19008185
DM0521/19008212
2.4 % D.W.
2.4 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
05/22/19
DM0522/19008240
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/23/19
DM0523/19008270
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/24/19
DM0524/19008285
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/25/19
DM0525/19008316
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/26/19
DMO526/19008335
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/27/19
DM0527/19008348
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/28/19
DM0528/19008373
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/29/19
DM0529/19008430
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/30/19
DM0530/19008480
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/31/19
DM0531/19008495
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
Avg Result: 2.4 % D.W.
ALUMINUM ICP Dry wt.
U - mple 10 -
05/11/19 WMC19/19007406
Min LOD: 0.1 % D.W.
Result LOD LOQ
4500 mg/kg D.W. 57
200
Max Result: 2.5 % D.W.
Milorganite Weekly Composite
QA Flags Analytical Method Lab
B8. SW846-.6010C MMSD
Avg Result: 4500 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Min LOD: 57 mg/kg D.W.
Result LOD LOQ
QA Flags Analytical Method
Lab
05/11/19
WMC19/19007406
0.14 %
0.11
AOAC (13) 2.065
MMSD
Avg Result: 0.14 "/o
SY5/rpt1MiloMonthlyDW 4126119 tj
Min LOD:
0.11 %
Page 13 0/16
Printed.- 6/13/1914:3i

NSD
r F9ttt1�
Monthly Milorganite Report DW
May 2019
Milorganite Weekly Composite
BORON ICP Dry wt.
Sa pi� Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
05/11/19 WMC19/19007406 9.6 mg/kg D.W. 0.58 1.8 SW846: 6010C Cr Lab
Avg Result: 9.6 mg/kg D.W. Min LOD: 0.58 mg/kg D.W.
CHROMIUM ICP Dry wt.
05/11/19 WMC19/19007406
190 mg/kg D.W. 1.6
16
SW846: 6010C
MMSD
Avg Result: 190 mg/kg D.W.
COBALT ICP Dry wt.
��rnple Date Sample ID
Min LOD: 1.6 mg/kg D.W.
Result LOD LOQ
QA Flags
Analytkal Method
Lab
05/11/19 WMC19/19007406
3.7 mg/kg D.W. 1.1
4.3
B8, 3.
SW846: 6010C
MMSD
Avg Result: 3.7 mg/kg D.W.
MERCURY by M. 7471 (sludge)
iSample Date Sample ID
Min LOD: 1.1 mg/kg D.W.
Result LOD LOQ
QA Flags
Analytical Method
Lab
05/04/19 WMC18/19006938
0.093 mg/kg D.W. 0.0056
0.019
EPA 7471E
CT Lab
05/11/19 WMC19/19007406
0.17 mg/kg D.W. 0.0055
0.019
EPA 7471E
CT Lab
05/18/19 WMC20/19008187
0.063 mg/kg D.W. 0.0054
0.018
EPA 7471E
CT Lab
05/25/19 WMC21/19008350
0.12 mg/kg D.W. 0.0057
0.019
EPA 7471B
CT Lab
Avg Result: 0.11 mg/kg D.W.
NITRATE NITROGEN
Date Sample ID
Min LOD: 0.0054 mg/kg D.W.
Result LOD LOQ QA Flags
Max Result: 0.17 mg/kg D.W.
Analytical Method
Lab
05/11/19 WMC19/19007406
0.78 % 0.5
AOAC (16) 930.01
MMSD
Avg Result: 0.78 %
NITROGEN-Total(Manual)
Sample Date Sample ID
Min LOD: 0.5 %
Result LOD
LOQ
QA Flags
Analytical Method
Lab
05/11/19 WMC19/19007406
6.5 % 0.11
AOAC (16) 955.04
MMSD
Avg Result: 6.5 %
NITROGEN -Water Insoluble
Sample Date Sample ID
Min LOD: 0.11 0/0
Result LOD
LOQ
QA Flags
Analytical Method
Lab
05/11/19 WMC19/19007406
5.4 % 0.5
AOAC (16) 945.01
MMSD
Avg Result: 5.4 %
pH -Solids
Date Sample ID
Min LOD: 0.5 0/6
Result LOD
LOQ
QA Flags
Analytical Method
Lab
05/04/19 WMC18/19006938
6 Stnd. Units 0.1
SW846: 9045D
MMSD
05/11/19 WMC19/19007406
6.03 Stnd. Units 0.1
SW846: 9045D
MMSD
05/18/19 WMC20/19008187
6.07 Stnd. Units 0.1
SW846: 9045D
MMSD
05/25/19 WMC21/19008350
6.18 Stnd. Units 0.1
SW846: 9045D
MMSD
Avg Result: 6.1 Stnd. Units
Min LOD: 0.1 Stnd.
Units
Max Result: 6.18 Stnd. Units
Page 14 of 16
5Y5/rpl1M1/oMonth1yDW 4126119 tj Printed: 611311914:33

�(-
ND
PJA IRS i0k A Ctillr�
Monthly Milorganite Report DW
May 2019
Milorganite Weekly Composite
Solids (% Moisture)
Date Sample ID Resu t L.. .• •ags na ica,
05/04/19 WMC18/19006938 5.5 % 0.1 SM 2540 G (1997) MMSD
05/11/19 WMC19/19007406 5 % 0.1 SM 2540 G (1997) MMSD
05/18/19 WMC20/19008187 6.4 % 0.1 SM 2540 G (1997) MMSD
05/25/19 WMC21/19008350 6 % 0.1 SM 2540 G (1997) MMSD
Min LOD: 0.1 0/6
Solids (% Volatile)
Sample Date Sample ID Result .. LOQ .• Flags Analytical Method Lab
05/11/19 WMC19/19007406 73 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 73 % Min LOD: 0.1
Solids (a/o Total)
sm Samp Result LOD LOQ QA Flags Analytical Method Lab
ple Date
05/11/19 WMC19/19007406 95 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 95 % Min LOD: 0.1
Milorganite (Outfall 006) PRODUCTION
FECAL COLIFORM SLUDGE
Sample Date
Sample ID
Result,;
LOD LOQ
QA Flags Analytical Method
Lab
05/07/19
19008755
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
05/14/19
19009172
0.21 MPN/g TS
0.19
EPA 1680
MMSD
05/21/19
19009763
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
05/28/19
19010322
< 0.19 MPN/g TS
0.19
AO, Q3. EPA 1680
MMSD
Min LOD:
0.19 MPN/g TS
Solids (% Total)
Sample Date
Sample ID
Result
LOD LOQ
QA Flags Analytical Method
Lab
05/07/19
19008755
95 %
0.1
SM 2540 G (1997)
MMSD
05/14/19
19009172
96 %
0.1
SM 2540 G (1997)
MMSD
05/21/19
19009763
93 %
0.1
SM 2540 G (1997)
MMSD
05/28/19
19010322
94 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 94 %
Min LOD:
0.1 %
Max Result: 96 %
Milorganite (Outfall 009)
BAGGING
FECAL COLIFORM SLUDGE
Sample Date Sample ID
Result
LOD LOQ
., Flags Analytical Method
Lab
05/07/19
19008756
< 0.2 MPN/g TS
0.2
EPA 1680
MMSD
Min LOD: 0.2 MPN/g TS
Solids (% Total)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
05/07/19 19008756 92 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 92 % Min LOD: 0.1 %
Page 15 of 16
SYS/rpt1M11bMonth1yOW 4126119 tj Printed. • 611311914:33

Monthly Milorganite Report DW
May 2019
Milorganite (Outfall 009) BAGGING
Milorganite (Outfall 008) SHIPPING
FECAL COLIFORM SLUDGE
..te bampie ix, aesun: LIV L111t
05/14/19 19009173 0.21 MPN/g TS 0.19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
Solids (% Total)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
05/14/19 19009173 94 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 94 % Min LOD: 0.1 °/u
DescriptionsFlag
AO Other -- Flag requires additional explanation IS Insufficient sample volume for analysis.
AX Qualified data - see contract lab report ] Estimated concentration above the adjusted method detection limit
83 Target analyte detected in method blank > 10% of sample and below the adjusted reporting limit
concentration. LA Not analyzed - lab accident.
87 LCS recovery was above control limits.
58 LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
D1 Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
Hi Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
SYS1rpt1Mi1oMonth1yDW 4/16/19 rJ
M3 Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
MS Incubator/water bath temperature was outside method
requirements.
M7 Micro sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
SS Reading was not confirmed by a constant weight measurement
SO Supplemental details provided.(Water Quality only.)
T3 The dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The dilution water D.O. Increase was > 0.2 mg/L.
TS Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample exceeded prescribed method temperature range.
Page 16 of 16
Printed: 6113119 1433

if
ELMMMAM
s-
NF45D
PARTNERS FOR A CLEANER ENVIRONMENT
July 15, 2019
Memorandum
TO: Todd Schwingle, Dion Doege, Jacob Holbert, Brett Kelly, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom Nowicki, Beth
Stroik, Kori Kenney, Lab File
SUBJECT: Milorganite Monthly Data —June 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of June 2019.
The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin
(Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
�.4p
Richard Vincent Date
Laboratory Team Supervisor
Report Review By:
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

NSD
rS tit �
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
06/01/19
DMO601/19008681
< 3.1 mg/kg D.W.
3.1
12
Q3.
SW846: 6010C
MMSD
06/02/19
DM0602/19008700
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
3.4 mg/kg D.W.
3.1
12
1.
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
4.4 mg/kg D.W.
3
12
3, Q3.
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
5.5 mg/kg D.W.
3.1
12
1.
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
< 3 mg/kg D.W.
3
12
SW846: 6010C
MMSD
06/07/19
DM0607/19009357
< 3 mg/kg D.W.
3
12
SW846: 6010C
MMSD
06/08/19
DM0608/19009368
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
< 3 mg/kg D.W.
3
12
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
06/11/19
DMO611/19009796
< 3 mg/kg D.W.
3
12
SW846: 6010C
MMSD
06/12/19
DMO612/19009824
< 3 mg/kg D.W.
3
12
SW846: 6010C
MMSD
06/13/19
DM0613/19009845
5.3 mg/kg D.W.
3
12
].
SW846: 6010C
MMSD
06/14/19
DMO614/19009860
4.9 mg/kg D.W.
3
12
J.
SW846: 6010C
MMSD
06/15/19
DM0615/19009871
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
06/16/19
DM0616/19009890
< 3 mg/kg D.W.
3
12
SW846: 6010C
MMSD
06/17/19
DM0617/19010042
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
06/18/19
DM0618/19010453
< 3.1 mg/kg D.W.
3.1
12
SW846: 6010C
MMSD
06/19/19
DM0619/19010481
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
06/20/19
DM0620/19010504
< 17 mg/kg D.W.
17
70
Q3.
SW846: 6010C
MMSD
06/21/19
DM0621119010520
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
06/22/19
DM0622/19010531
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
06/23/19
DM0623/19010550
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
06/24/19
DM0624/19010563
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
06/25/19
DM0625/19011037
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
06/26/19
DM0626/19011065
< 17 mg/kg D.W.
17
68
Q2. SW846: 6010C
MMSD
06/27/19
DMO627/19011086
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
06/28/19
DM0628/19011158
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
06/29/19
DM0629/19011169
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
06/30/19
DM0630/19011189
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
Avg Result: 0.78 mg/kg D.W.
Min LOD: 3 mg/kg D.W.
Max Result: 5.5 mg/kg D.W.
Page 1 of 16
5Y5/rpt1M1/oMonth/yDW 4126119 q Printed: 7115119 09:13

�-j"
i D
i'lltii� tot A
CADMIUM ICP Dry wt.
T..ple -Dat. I Sample ID
Result
LOD
LOQ QA
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
Flags Analytical Method Lab
06/01/19
DM0601/19008681
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/02/19
DM0602/19008700
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
06/07/19
DM0607/19009357
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/08/19
DM0608/19009368
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
< 0.93 mg/kg D.W.
0.93
3.5
SWB46: 6010C
MMSD
06/11/19
DM0611/19009796
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
06/12/19
DM0612/19009824
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/13/19
DM0613/19009845
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/14/19
DM0614/19009860
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
06/15/19
06/16/19
DM0615/19009871
DM0616/19009890
< 0.93 mg/kg D.W.
< 0.91 mg/kg D.W.
0.93
0.91
3.5
3.4
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/17/19
DM0617/19010042
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/18/19
DM0618/19010453
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/19/19
DM0619/19010481
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
06/20/19
06/21/19
DM0620/19010504
DM0621/19010520
< 0.95 mg/kg D.W.
< 0.93 mg/kg D.W.
0.95
0.93
3.6
3.5
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/22/19
DM0622/19010531
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/23/19
DM0623/19010550
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
06/24/19
DM0624/19010563
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
06/25/19
DM0625/19011037
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
06/26/19
06/27/19
DM0626/19011065
DM0627/19011086
< 0.92 mg/kg D.W.
< 0.94 mg/kg D.W.
0.92
0.94
3.5
3.6
SW846: 6010C
SWB46: 6010C
MMSD
MMSD
06/28/19
DMO628/19011158
< 0.94 mg/kg D.W.
0.94
3.5
SW846: 6010C
MMSD
06/29/19
DM0629/19011169
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
06/30/19
DM0630/19011189
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
0.91 mg/kg D.W.
Page 1 of 16
5Y51rptJMAbMon[h/yOW 4126119 tj Printed: 7115119 09:13

14SD
� F1� A t1l�AHt
COPPER ICP Dry wt.
ample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report
June 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
06/01/19
DM0601/19008681
210 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
06/02/19
DM0602/19008700
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
210 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
210 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
06/07/19
DM0607119009357
210 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
06/08/19
DM0608/19009368
200 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
200 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
190 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
06/11/19
DM0611/19009796
200 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
06/12/19
DM0612/19009824
200 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
06/13/19
DM0613/19009845
180 mg/kg D.W.
6.6
25
B8. SW846: 6010C
MMSD
06/14/19
DM0614/19009860
190 mg/kg D.W.
6.6
25
Q3. SW846: 6010C
MMSD
06/15/19
06/16/19
DM0615/19009871
DM0616/19009890
200 mg/kg D.W.
200 mg/kg D.W.
6.7
6.6
26
25
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/17/19
DM0617/19010042
190 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
06/18/19
DM0618/19010453
210 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
06/19/19
DM0619/19010481
190 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
06/20/19
06/21/19
DM0620/19010504
DM0621/19010520
200 mg/kg D.W.
200 mg/kg D.W.
6.9
6.7
26
26
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/22/19
DM0622/19010531
200 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
06/23/19
DM0623/19010550
200 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
06/24/19
DM0624/19010563
200 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
06/25/19
DM0625/19011037
210 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
06/26/19
DM0626/19011065
210 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
06/27/19
DM0627/19011086
200 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
06/28/19
DM0628/19011158
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
06/29/19
DM0629/19011169
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
06/30/19
DM0630/19011189
210 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
Avg Result: 200 mg/kg D.W.
Min LOD:
6.6 mg/kg D.W.
Max Result: 220 mg/kg D.W.
Page 3 of 16
5Y5/rptlMi1oMonth1yDW 4126119 tj Printed.- 7115119 09:13

�'N
ND
PA910113 to A CUMH 191 07
IRON ICP Dry wt.
iaiWple Date Sample ID Result LOD LOQ
06/01/19 DM0601/19008681 39000 mg/kg D.W. 240 2400
06/02/19 DM0602/19008700 39000 mg/kg D.W. 250 2500
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
lags Analytical Meth6d La 6'-
SW846:6010C MMSD
SW846: 6010C MMSD
06/03/19
DM0603/19008713
41000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
40000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
38000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
41000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/07/19
DM0607/19009357
36000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/08/19
DM0608/19009368
34000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
34000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
33000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/11/19
DM0611/19009796
37000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/12/19
DM0612/19009824
36000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/13/19
DM0613/19009845
41000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/14/19
DM0614/19009860
42000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/15/19
06/16/19
DM0615/19009871
DMO616/19009890
34000 mg/kg D.W.
34000 mg/kg D.W.
240
240
2400
2400
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/17/19
DM0617/19010042
33000 mg/kg D.W.
240
2400
SW846: 6010C
MMSD
06/18/19
06/19/19
06/20/19
06/21/19
DM0618/19010453
DM0619/19010481
DM0620/19010504
DM0621/19010520
39000 mg/kg D.W.
39000 mg/kg D.W.
32000 mg/kg D.W.
36000 mg/kg D.W.
240
530
550
530
2400
1900
2000
1900
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
06/22/19
DM0622/19010531
33000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
06/23/19
DM0623/19010550
33000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
06/24/19
DM0624/19010563
34000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
06/25/19
DM0625/19011037
42000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
06/26/19
06/27/19
DM0626/19011065
DM0627/19011086
39000 mg/kg D.W.
33000 mg/kg D.W.
530
540
1900
1900
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/28/19
DM0628/19011158
34000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
06/29/19
06/30/19
DM0629/19011169
DM0630/19011189
34000 mg/kg D.W.
33000 mg/kg D.W.
540
540
2000
2000
SW846: 6010C
SW846: 6010C
MMSD
MMSD
Avg Result: 36000 mg/kg D.W.
Min LOD: 240 mg/kg D.W.
Max Result: 42000 mg/kg D.W.
SY5/rpt1M1/6Month1yDW 4126119 Y
Page 4 of 16
Printed: 7115119 09:13

R
11416D
WINI iot tt#tApt ta►r
LEAD ICP Dry wt.
!Sample Date .
Result
LOD
LOQ
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
06/01/19
DM0601/19008681
43 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
06/02/19
DM0602/19008700
40 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
39 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
39 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
38 mg/kg D.W.
2.8
8.6
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
38 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/07/19
DM0607/19009357
40 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/08/19
DM0608119009368
38 mg/kg D.W.
2.8
8.6
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
35 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
34 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
06/11/19
DM0611/19009796
33 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/12/19
DM0612/19009824
34 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/13/19
DMO613/19009845
33 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/14/19
DM0614/19009860
40 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/15/19
DM0615/19009871
37 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
06/16/19
DM0616/19009890
36 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/17/19
DM0617/19010042
35 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
06/18/19
DM0618/19010453
35 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
06/19/19
DM0619/19010481
35 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
06/20/19
06/21/19
DM0620/19010504
DM0621/19010520
32 mg/kg D.W.
34 mg/kg D.W.
3
2.9
8.8
8.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/22/19
DM0622/19010531
33 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
06/23/19
DM0623/19010550
33 mg/kg D.W.
3
8.8
SW846: 6010C
MMSD
06/24/19
DM0624/19010563
32 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
06/25/19
DM0625/19011037
33 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/26/19
DM0626/19011065
32 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
06/27/19
DM0627/19011086
33 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
06/28/19
DM0628/19011158
31 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
06/29/19
DM0629/19011169
31 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
06/30/19
DM0630/19011189
33 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
Avg Result: 35 mg/kg D.W.
Min LOD:
2.8 mg/kg D.W.
Max Result: 43 mg/kg D.W.
Page 5 of 16
5Y5/rptlM1/oMonth/yDW 4126119 t/ Printed: 7115119 09:13

14SD
Pig"Iffs a A CIM
MOLYBDENUM ICP Dry wt.
Sample ..
•D
LOQ
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
QA Flags Anaiy4ic'afketbo� Lab
06/01/19
DM0601/19008681
9.5 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
06/02/19
DM0602/19008700
9.1 mg/kg D.W.
2
7.6
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
9.2 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
9.4 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
9.4 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
9.4 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
06/07/19
DM0607/19009357
9 mg/kg D.W.
2
7.5
SWB46: 6010C
MMSD
06/08/19
DM0608/19009368
9 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
8.6 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
8.4 mg/kg D.W.
2
7.6
SW846: 6010C
MMSD
06/11/19
DM0611/19009796
8.9 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
06/12/19
DM0612/19009824
8.6 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
06/13/19
DM0613/19009845
8 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
06/14/19
DM0614/19009860
7.9 mg/kg D.W.
2
7.4
SW846: 6010C
MMSD
06/15/19
06/16/19
DMO615/19009871
DM0616/19009890
8.6 mg/kg D.W.
9 mg/kg D.W.
2
2
7.6
7.4
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/17/19
DM0617/19010042
8.7 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
06/18/19
DM0618/19010453
9.4 mg/kg D.W.
2
7.5
SW846: 6010C
MMSD
06/19/19
DM0619/19010481
8.8 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
06/20/19
06/21/19
DM0620/19010504
DM0621/19010520
8.4 mg/kg D.W.
8.7 mg/kg D.W.
4.6
4.5
17
17
1.
1.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/22/19
DM0622/19010531
8.8 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
06/23/19
DM0623/19010550
8.7 mg/kg D.W.
4.6
17
J.
SW846: 6010C
MMSD
06/24/19
DM0624/19010563
9 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
06/25/19
DM0625/19011037
9.3 mg/kg D.W.
4.4
17
1.
SW846: 6010C
MMSD
06/26/19
DM0626/19011065
8.7 mg/kg D.W.
4.4
17
1.
SW846: 6010C
MMSD
06/27/19
DM0627119011086
8.4 mg/kg D.W.
4.5
17
].
SW846: 6010C
MMSD
06/28/19
DM0628/19011158
8.7 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
06/29/19
DM0629119011169
8.6 mg/kg D.W.
4.6
17
1
SW846: 6010C
MMSD
06/30/19
DM0630/19011189
8.4 mg/kg D.W.
4.6
17
1
SW846: 6010C
MMSD
Avg Result: 8.8 mg/kg D.W.
Min LOD:
2 mg/kg
D.W.
Max Result: 9.5 mg/kg D.W.
Page 6 o/ 16
SY5/rp[IMiloMonthlyDW 4126119 U Printed: 7115119 09:13

pig 103 tol A CLIMB fit fll'
NICKEL ICP Dry wt.
sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
06/01/19
DM0601/19008681
25 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
06/02/19
DMO602/19008700
24 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
24 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
24 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
24 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
24 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
06/07/19
DM0607/19009357
23 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
06/08/19
DM0608/19009368
22 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
22 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
22 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
06/11/19
DM0611/19009796
22 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
06/12/19
DM0612/19009824
25 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
06/13/19
DM0613/19009845
25 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
06/14/19
DM0614/19009860
27 mg/kg D.W.
3.2
9.4
SW846: 6010C
MMSD
06/15/19
DM0615/19009871
22 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
06/16/19
DM0616/19009890
26 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
06/17/19
DM0617/19010042
22 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
06/18/19
DM0618/19010453
24 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
06/19/19
DM0619/19010481
25 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
06/20/19
DM0620/19010504
22 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
06/21/19
DM0621/19010520
22 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
06/22/19
DM0622/19010531
23 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
06/23/19
DM0623/19010550
23 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
06/24/19
DM0624/19010563
24 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
06/25/19
DM0625/19011037
27 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
06/26/19
DM0626/19011065
26 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
06/27/19
DM0627/19011086
21 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
06/28/19
DM0628/19011158
22 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
06/29/19
DM0629/19011169
22 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
06/30/19
DM0630/19011189
22 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
Avg Result: 24 mg/kg D.W.
Min LOD:
3.1 mg/kg D.W.
Max Result: 27 mg/kg D.W.
Page 7 of 16
5Y5/rpt1 Mi/aMonth/yDW 4126119 q Printed: 7115119 09:13

SHNSD
PHOSPHORUS ICP Dry wt.
•. •• LOQ
06/01/19 DM0601/19008681 22000 mg/kg D.W. 9.1 91
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
lags Analytkal kk6d' Lab
SW846: 6010C MMSD
06/02/19
DM0602/19008700
22000 mg/kg D.W.
9.2
92
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
22000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
22000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
22000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
22000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
06/07/19
DM0607/19009357
22000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
06/08/19
DM0608119009368
21000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
21000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
21000 mg/kg D.W.
9.2
92
SW846: 6010C
MMSD
06/11/19
DM0611/19009796
22000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
06/12/19
DM0612/19009824
22000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
06/13/19
DM0613/19009845
23000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
06/14/19
DM0614/19009860
23000 mg/kg D.W.
9
90
SW846: 6010C
MMSD
06/15/19
06/16/19
DM0615/19009871
DM0616/19009890
22000 mg/kg D.W.
22000 mg/kg D.W.
9.2
9
92
90
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/17/19
DM0617/19010042
22000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
06/18/19
DM0618/19010453
23000 mg/kg D.W.
9.1
91
SW846: 6010C
MMSD
06/19/19
DMO619/19010481
22000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
06/20/19
06/21/19
DM0620/19010504
DM0621/19010520
22000 mg/kg D.W.
22000 mg/kg D.W.
24
23
92
90
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/22/19
DM0622/19010531
22000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
06/23/19
06/24/19
DM0623/19010550
DM0624/19010563
23000 mg/kg D.W.
23000 mg/kg D.W.
24
24
92
90
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/25/19
DM0625/19011037
24000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
06/26/19
DM0626/19011065
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
06/27/19
DM0627/19011086
22000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
06/28/19
DM0628/19011158
23000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
06/29/19
06/30/19
DM0629119011169
DM0630/19011189
23000 mg/kg D.W.
22000 mg/kg D.W.
24
24
92
91
SW846: 6010C
SW846: 6010C
MMSD
MMSD
Avg Result: 22000 mg/kg D.W.
Min LOD:
9 mg/kg D.W.
Max Result: 24000 mg/kg D.W.
SWrpt1MI10M0nth1yDW 4126119 Of
Page 8 of 16
Printed., 7115119 09. IJ

mroD
b»t1�R5 t6t d Ct�
POTASSIUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
06/01/19
DM0601/19008681
4800 mg/kg D.W.
290
2900
AO.
SW846: 6010C
MMSD
06/02/19
DMO602119008700
4800 mg/kg D.W.
290
2900
AO.
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
4400 mg/kg D.W.
290
2900
AO.
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
4000 mg/kg D.W.
280
2800
AO, B8.
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
4200 mg/kg D.W.
280
2800
AO, B8.
SW846: 6010C
MMSD
06/06/19
DMO606/19008960
4300 mg/kg D.W.
280
2800
AO, B8, Q3. SW846: 6010C
MMSD
06/07/19
DM0607/19009357
4300 mg/kg D.W.
280
2800
B8.
SW846: 6010C
MMSD
06/08/19
DM0608/19009368
4200 mg/kg D.W.
280
2800
AO, B8.
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
4100 mg/kg D.W.
280
2800
AO, B8.
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
4200 mg/kg D.W.
290
2900
AO, B8.
SW846: 6010C
MMSD
06/11/19
DM0611/19009796
4500 mg/kg D.W.
280
2800
AO.
SW846: 6010C
MMSD
06/12/19
DM0612/19009824
4400 mg/kg D.W.
280
2800
AO.
SW846: 6010C
MMSD
06/13/19
DMO613/19009845
4300 mg/kg D.W.
280
2800
SW846: 6010C
MMSD
06/14/19
DMO614/19009860
4500 mg/kg D.W.
280
2800
SW846: 6010C
MMSD
06/15/19
DM0615/19009871
4600 mg/kg D.W.
290
2900
SW846: 6010C
MMSD
06/16/19
DM0616/19009890
4500 mg/kg D.W.
280
2800
SW846: 6010C
MMSD
06/17/19
DMO617/19010042
4500 mg/kg D.W.
290
2900
SW846: 6010C
MMSD
06/18/19
DM0618/19010453
4500 mg/kg D.W.
290
2900
AO.
SW846: 6010C
MMSD
06/19/19
DM0619/19010481
4100 mg/kg D.W.
290
860
B8.
SW846: 6010C
MMSD
06/20/19
DM0620/19010504
4400 mg/kg D.W.
300
880
SW846: 6010C
MMSD
06/21/19
DM0621/19010520
4300 mg/kg D.W.
290
860
SW846: 6010C
MMSD
06/22/19
DM0622/19010531
4300 mg/kg D.W.
290
860
SW846: 6010C
MMSD
06/23/19
DM0623/19010550
4300 mg/kg D.W.
300
880
SW846: 6010C
MMSD
06/24/19
DM0624/19010563
4300 mg/kg D.W.
290
870
SW846: 6010C
MMSD
06/25/19
DM0625/19011037
3800 mg/kg D.W.
280
850
SW846: 6010C
MMSD
06/26/19
DM0626/19011065
3800 mg/kg D.W.
280
850
B8.
SW846: 6010C
MMSD
06/27/19
DM0627/19011086
4400 mg/kg D.W.
290
870
AO.
SW846: 6010C
MMSD
06/28/19
DM0628/19011158
4200 mg/kg D.W.
290
870
AO.
SW846: 6010C
MMSD
06/29/19
DM0629/19011169
4200 mg/kg D.W.
290
880
AO.
SW846: 6010C
MMSD
06/30/19
DM0630/19011189
4300 mg/kg D.W.
290
880
AO.
SW846: 6010C
MMSD
Avg Result: 4300 mg/kg D.W.
Min LOD:
280 mg/kg D.W.
Max Result: 4800 mg/kg D.W.
Page 9 of 16
SY5/rpt1M1loMonth/yDW 4126119 fj Printed 7115119 09:1J

a
NSD
PI�RYlIklS F6t � ttER �°
SELENIUM ICP Dry wt.
Sample Oat eSample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
QA Flags Analyt . Ic al La
06/01/19
DM0601/19008681
7.4 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/02/19
DM0602/19008700
7.4 mg/kg D.W.
4.2
42
J.
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
7.5 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
5.6 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
5.6 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
6.2 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/07/19
DM0607119009357
5.8 mg/kg D.W.
4.1
41
J, Q2.
SW846: 6010C
MMSD
06/08/19
DM0608/19009368
5.9 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
6.3 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
5.7 mg/kg D.W.
4.2
42
J.
SW846: 6010C
MMSD
06/11/19
DM0611/19009796
6.8 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/12/19
DM0612/19009824
5.2 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/13/19
DM0613/19009845
< 4.1 mg/kg D.W.
4.1
41
SW846: 6010C
MMSD
06/14/19
DM0614119009860
4.6 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/15/19
06/16/19
DM0615/19009871
DM0616/19009890
< 4.2 mg/kg D.W.
4.5 mg/kg D.W.
4.2
4.1
42
41
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/17/19
DM0617/19010042
6.1 mg/kg D.W.
4.1
41
J, Q2.
SW846: 6010C
MMSD
06/18/19
DM0618/19010463
5.9 mg/kg D.W.
4.1
41
J.
SW846: 6010C
MMSD
06/19/19
DM0619/19010481
4.4 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
06/20/19
06/21/19
DM0620/19010504
DM0621119010520
5.8 mg/kg D.W.
6.6 mg/kg D.W.
4.3
4.2
13
13
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/22/19
DM0622119010531
4.4 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
06/23/19
DM0623/19010550
4.7 mg/kg D.W.
4.3
13
J.
SW846: 6010C
MMSD
06/24/19
DM0624/19010563
5.9 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
06/25/19
DM0625/19011037
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
06/26/19
DM0626/19011065
4.8 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
06/27/19
DM0627/19011086
5 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
06/28/19
DM0628/19011158
5.6 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
06/29/19
DM0629/19011169
4.5 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
06/30/19
DM0630/19011189
4.9 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
Avg Result: 5.1 mg/kg D.W.
Min LOD:
4.1 mg/kg D.W.
Max Result: 7.5 mg/kg D.W.
Page 10 of 16
SY5/rptl Mi/oNonth/yDW 4126119 tj Printed: 7115119 09:13

f
HNSD
IDf A ttikle� E "If
Solids (% Moisture)
Sample Date Sample ID
Result
LOD
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
LOQ QA Flags Analytical Method Lab
O6/01/19
DM0601/19008681
5.8 %
0.1
SM 2540 G (1997)
MMSD
06/02/19
DM0602/19008700
6.8 %
0.1
SM 2540 G (1997)
MMSD
06/03/19
DM0603/19008713
5.6 %
0.1
SM 2540 G (1997)
MMSD
06/04/19
DM0604/19008815
4.7 %
0.1
SM 2540 G (1997)
MMSD
06/05/19
DMO605/19008904
5.3 %
0.1
SM 2540 G (1997)
MMSD
06/06/19
DM0606/19008960
4.4 %
0.1
SM 2540 G (1997)
MMSD
06/07/19
DMO607/19009357
5 %
0.1
SM 2S40 G (1997)
MMSD
06/08/19
DM0608/19009368
5.4 %
0.1
SM 2540 G (1997)
MMSD
06/09/19
DM0609/19009388
4.8 %
0.1
SM 2540 G (1997)
MMSD
06/10/19
DM0610/19009402
6.3 %
0.1
SM 2540 G (1997)
MMSD
06/11/19
DMO611/19009796
4.4 %
0.1
SM 2540 G (1997)
MMSD
06/12/19
DM0612/19009824
4.9 %
0.1
SM 2540 G (1997)
MMSD
06/13/19
DM0613/19009845
5 %
0.1
SM 2540 G (1997)
MMSD
06/14/19
DM0614/19009860
4.8 %
0.1
SM 2540 G (1997)
MMSD
06/15/19
06/16/19
DM0615/19009871
DMO616/19009890
6.3 0/6
4.5 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
06/17/19
DM0617/19010042
5.8 %
0.1
SM 2540 G (1997)
MMSD
06/18/19
DM0618/19010453
5.9 %
0.1
SM 2540 G (1997)
MMSD
06/19/19
DM0619/19010481
6.1 %
0.1
SM 2540 G (1997)
MMSD
06/20/19
06/21/19
DM0620/19010504
DM0621/19010520
8.6 %
6.3 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
06/22/19
DM0622/19010531
6 %
0.1
SM 2540 G (1997)
MMSD
06/23/19
DM0623/19010550
8.5 %
0.1
SM 2540 G (1997)
MMSD
06/24/19
DM0624/19010563
6.5 %
0.1
SM 2540 G (1997)
MMSD
06/25/19
DM0625/19011037
5.2 %
0.1
SM 2540 G (1997)
MMSD
06/26/19
DM0626/19011065
5.2 %
0.1
SM 2540 G (1997)
MMSD
06/27/19
DMO627/19011086
7.3 %
0.1
SM 2540 G (1997)
MMSD
06/28/19
DM0628/19011158
7 %
0.1
SM 2540 G (1997)
MMSD
06/29/19
06/30/19
DM0629/19011169
DM0630/19011189
Avg Result: 6 %
8.3 % 0.1
8.2 % 0.1
Min LOD: 0.1 %
SM 2540 G (1997)
SM 2540 G (1997)
Max Result: 8.6
MMSD
MMSD
Page 11 of 16
SYS/rptJMi1oMonth/yDW 4126119 of PrInted.• 7115119 09:13

�ul
TIHNSD
1AM tot A tltall6t
ZINC ICP Dry wt.
Sample Date Sample ID Result LOD LOQ
06/01/19 DM0601/19008681 400 mg/kg D.W. 18 180
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
lags Analytical Method Lab
SW846: 6010C MMSD
06/02/19
DM0602/19008700
390 mg/kg D.W.
18
180
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
380 mg/kg D.W.
18
180
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
380 mg/kg D.W.
18
180
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
380 mg/kg D.W.
18
180
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
380 mg/kg D.W.
18
180
SW846: 6010C
MMSD
06/07/19
DM0607/19009357
380 mg/kg D.W.
18
180
SW846: 6010C
MMSD
06/08/19
DM0608/19009368
360 mg/kg D.W.
18
180
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
360 mg/kg D.W.
18
180
SW846: 6010C
MMSD
06/10/19
DMO610/19009402
360 mg/kg D.W.
18
180
SW846: 6010C
MMSD
06/11/19
06/12/19
DM0611/19009796
DM0612/19009824
360 mg/kg D.W.
360 mg/kg D.W.
18
18
180
180
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/13/19
DM0613/19009845
390 mg/kg D.W.
18
180
SW846: 6010C
MMSD
06/14/19
06/15/19
06/16/19
DM0614/19009860
DM0615/19009871
DM0616/19009890
390 mg/kg D.W.
390 mg/kg D.W.
380 mg/kg D.W.
18
18
18
180
180
180
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
06/17/19
06/18/19
DM0617/19010042
DM0618/19010453
380 mg/kg D.W.
400 mg/kg D.W.
18
18
180
180
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/19/19
DM0619/19010481
390 mg/kg D.W.
18
54
SW846: 6010C
MMSD
06/20/19
06/21/19
DM0620/19010504
DM0621/19010520
380 mg/kg D.W.
390 mg/kg D.W.
18
18
56
54
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/22/19
06/23/19
06/24/19
DM0622/19010531
DM0623/19010550
DM0624/19010563
390 mg/kg D.W.
380 mg/kg D.W.
380 mg/kg D.W.
18
18
18
54
56
54
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
06/25/19
DMO625/19011037
410 mg/kg D.W.
18
54
SW846: 6010C
MMSD
06/26/19
DM0626/19011065
390 mg/kg D.W.
18
54
SW846: 6010C
MMSD
06/27/19
DM0627/19011086
380 mg/kg D.W.
18
55
SW846: 6010C
MMSD
06/28/19
06/29/19
06/30/19
DM0628/19011158
DMO629/19011169
DM0630/19011189
Avg Result: 380 mg/kg D.W.
390 mg/kg D.W. 18 55
400 mg/kg D.W. 18 56
400 mg/kg D.W. 18 56
Min LOD: 18 mg/kg D.W.
SW846: 6010C
SW846: 6010C
SW846: 6010C
Max Result: 410 mg/kg D.W.
MMSD
MMSD
MMSD
Page 11 of 16
5YS1rpt1M11oMonth1yDW 4126119 tj Minted: 7115119 09:13

r
?aA'I�S 1I�t A tl
Phosphorus - Total % DW (Calc.)
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
June 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
06/01/19
DM0601/19008681
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/02/19
DM0602/19008700
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/03/19
DM0603/19008713
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/04/19
DM0604/19008815
2.2%D.W.
0.1
0.1
SW846: 6010C
MMSD
06/05/19
DM0605/19008904
2.2%D.W.
0.1
0.1
SW846: 6010C
MMSD
06/06/19
DM0606/19008960
2.2%D.W.
0.1
0.1
SW846: 6010C
MMSD
06/07/19
DM0607/19009357
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/08/19
DM0608/19009368
2.1 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/09/19
DM0609/19009388
2.1 %D.W.
0.1
0.1
SW846: 6010C
MMSD
06/10/19
DM0610/19009402
2.1 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/11/19
DM0611/19009796
2.2%D.W.
0.1
0.1
SW846: 6010C
MMSD
06/12/19
DM0612/19009824
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/13/19
DM0613/19009845
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/14/19
DM0614/19009860
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/15/19
06/16/19
DM0615/19009871
DM0616/19009890
2.2 % D.W.
2.2 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/17/19
DM0617/19010042
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/18/19
DM0618/19010453
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/19/19
DM0619/19010481
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/20/19
06/21/19
DM0620/19010504
DM0621/19010520
2.2%D.W.
2.2 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/22/19
DM0622/19010531
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/23/19
DM0623/19010550
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/24/19
DM0624/19010563
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
06/25/19
DM0625/19011037
2.4 % D.W.
0.1
0.1
SWB46: 6010C
MMSD
06/26/19
06/27/19
DM0626/19011065
DM0627/19011086
2.3 % D.W.
2.2 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/28/19
06/29/19
DM0628/19011158
DM0629/19011169
2.3 % D.W.
2.3 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
06/30/19 DM0630/19011189
2.2 % D.W. 0.1
0.1
SW846: 6010C MMSD
Avg Result: 2.2 % D.W.
Min LOD: 0.1 % D.W.
Max Result: 2.4 % D.W.
Milorganite Weekly Composite
ALUMINUM ICP Dry wt.
Sample Date Sample ID
Result LOD
LOQ
QA Flags Analytical Method Lab
06/08/19 WMC23/19009404
7700 mg/kg D.W. 57
200
B8. SW846: 6010C MMSD
Avg Result: 7700 mg/kg D.W.
Min LOD: 57 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Date Sample ID
Result
LOQ
Flags Analytical Method
06/08/19 WMC23/19009404
LOD
0.15 % 0.11
0.37
QA Lab
AOAC (13) 2.065 MMSD
Avg Result: 0.15 % Min LOD: 0.11 %
Page 13 of 16
5Y5/rpt1M1/oMonth1yDW 4126119 tJ Printed:7115119 09:13

Monthly Milorganite Report DW
1114SD June 2019
�1t'ltikil9t►C!� �€N'
Milorganite Weekly Composite
BORON ICP Dry wt.
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
06/08/19 WMC23/19009404 170 mg/kg D.W. 1 3.3 SW846: 6010C CT Lab
Avg Result: 170 mg/kg D.W. Min LOD: 1 mg/kg D.W.
CHROMIUM ICP Dry wt.
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
06/08/19 WMC23/19009404 150 mg/kg D.W. 1.6 4.8 SW846: 6010C MMSD
Avg Result: 150 mg/kg D.W. Min LOD: 1.6 mg/kg D.W.
COBALT ICP Dry wt.
Sample Date Sample ID Result .. LOQ .. Flags Analytical Method Lab
06/08/19 WMC23/19009404 3.9 mg/kg D.W. 0.28 1.1 B8. SW846: 6010C MMSD
Avg Result: 3.9 mg/kg D.W.
Min LOD: 0.28 mg/kg D.W.
MERCURY by M. 7471 (sludge)
Sample Date Sample ID
Result
LOD
LOQ QA Flags
Analytical Method
Lab
06/01/19 WMC22/19008715
< 0.0055 mg/kg D.W.
0.0055
0.019 AX.
EPA 74718
CT Lab
06/08/19 WMC23/19009404
0.22 mg/kg D.W.
0.0055
0.019
EPA 7471E
Cr Lab
06/15/19 WMC24119010044
0.044 mg/kg D.W.
0.0056
0.019
EPA 7471E
CT Lab
06/22/19 WMC25119010565
< 0.0055 mg/kg D.W.
0.0055
0.019
EPA 7471E
CT Lab
06/29/19 WMC26/19011205
0.14 mg/kg D.W.
0.0058
0.02
EPA 7471E
CT Lab
Avg Result: 0.081 mg/kg D.W. Min LOD: 0.0055 mg/kg D.W.
Max Result: 0.22 mg/kg D.W.
NITRATE NITROGEN
Sample Date Sample ID
Result
LOD
LOQ .• Flags
Analytical Method
Lab
06/08/19 WMC23/19009404
0.96 %
0.5
AOAC (16) 930.01
MMSD
Avg Result: 0.96 %
Min LOD: 0.5
NITROGEN-Total(Manual)
Sample Date Sample ID
Result
LOD
LOQ .• Flags
Analytical Method
Lab
06/08/19 WMC23/19009404
6.2 %
0.11
AOAC (16) 955.04
MMSD
Avg Result: 6.2 %
Min LOD: 0.11
NITROGEN -Water Insoluble
Sam le ..
06/08/19 WMC23/19009404
4.4 %
0.5
AOAC (16) 945.01
MMSD
Avg Result: 4.4 %
Min LOD: 0.5 %
pH -Solids
Sample Date Sample ID
Result
LOD
LOQ QA Flags
Analytical Method
Lab
06/01/19 WMC22/19008715
6.28 Stnd. Units
0.1
SW846: 9045D
MMSD
06/08/19 WMC23/19009404
6.31 Stnd. Units
0.1
SW846: 9045D
MMSD
06/15/19 WMC24/19010044
6.31 Stnd. Units
0.1
SW846: 9045D
MMSD
06/22/19 WMC25/19010565
6.22 Stnd. Units
0.1
SW846: 9045D
MMSD
06/29/19 WMC26/19011205
6.26 Stnd. Units
0.1
SW846: 9045D
MMSD
Avg Result: 6.3 Stnd. Units
Min LOD: 0.1 Stnd. Units
Max Result: 6.31 Stnd. Units
Page 14 of 16
5Y5/rptimloMonthlyDW 4126119 y
Printed: 7115119 09:13

j
Monthly Milorganite Report DW
NNSD
June 2019
!l�11BS tilt A ttliaHR
Milorganite Weekly Composite
Solids (% Moisture)
Sample Date Sample ID
Result
LOD
LOQ QA Flags Analytical Method Lab
06/01/19 WMC22119008715
5.2 %
0.1
SM 2540 G (1997) MMSD
06/08/19 WMC23/19009404
5.2 %
0.1
SM 2540 G (1997) MMSD
06/15/19 WMC24/19010044
5.4 %
0.1
SM 2540 G (1997) MMSD
06/22/19 WMC25/19010565
6.6 %
0.1
SM 2540 G (1997) MMSD
06/29/19 WMC26119011205
7.3 %
0.1
SM 2540 G (1997) MMSD
Min LOD:
0.1 "/o
Solids (% Volatile)
Sample Date Sample to
Result
LOD
LOQ QA Flags Analytical Method Lab
06/15/19 WMC24/19010044
71 %
0.1
SM 2540 G (1997) MMSD
Avg Result: 71 % Min LOD: 0.1 %
Solids (% Total)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
06/15/19 WMC24/19010044 95 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 95 % Min LOD: 0.1
FECAL COLIFORM SLUDGE
Sample Date Sample ID
Result
LOD LOQ
Milorganite (Outfall 006) PRODUCTION
.• Flags Analytical Method Lab
06/04/19 19011000
< 0.2 MPN/g TS
0.2
EPA 1680
MMSD
06/11/19 19011856
< 0.19 MPN/g TS
0.19
Q3. EPA 1680
MMSD
06/18/19 19012328
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
06/25/19 19013311
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
Solids (% Total)
Sample Date Sample ID
Min LOD: 0.19 MPN/g TS
Result LOD LOQ
., Flags Analytical Method
Lab
06/04/19 19011000
92 %
0.1
SM 2540 G (1997)
MMSD
06/11/19 19011856
96 %
0.1
SM 2540 G (1997)
MMSD
06/18/19 19012328
95 %
0.1
SM 2540 G (1997)
MMSD
06/25/19 19013311 95 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 94 % Min LOD: 0.1 % Max Result: 96
Milorganite (Outfall 009) BAGGING
FECAL COLIFORM SLUDGE
Sample Date Sample ID Result LOD LOQ i*'ff s Analytical Method
06/04/19 19011002 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
SYS/ipt1Mi10Month1YDW 4126119 tj
Page 15 of 16
Printed: 7115119 09:13

Monthly Milorganite Report DW
June 2019
it'il*D
MI IM 0 A LL6t, R LyiPCAVIN"
Milorganite (Outfall 009) BAGGING
Solids (% Total)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
06/04/19 19011002 94 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 94 % Min LOD: 0.1 0/6
Milorganite (Outfall 008) SHIPPING
FECAL COLIFORM SLUDGE
Sample Date it
.. ..
06/04/19 19011001 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD
Solids (% Total)
06/04/19 19011001
Avg Result: 96 0/6
'
AO Other -- Flag requires additional explanation _
AX Qualified data - see contract lab report
63 Target analyte detected in method blank > 10% of sample
concentration.
Min LOD: 0.19 MPN/g TS
96 % 0.1
Min LOD: 0.1
87 LCS recovery was above control limits.
B8 LCS recovery was below control limits.
69 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
D1 Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
H1 Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
IS Insufficient sample volume for analysis.
SM 2540 G (1997) MMSD
] Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
LA Not analyzed - lab accident.
M1 Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
MS Incubator/water bath temperature was outside method
requirements.
M7 Micro sample received without adequate ea space.
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements,
SS Reading was not confirmed by a constant weight measurement
SO Supplemental details provided.(Water Quality only.)
T3 The dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample exceeded prescribed method temperature range.
Page 16 of 16
5Y51rpt1M11bMonth1yDW 4126119 tj Printed: 7115119 09:13

'CIMMSD
PARTNERS FOR A CLEANER ENVIRONMENT
August 15, 2019
Memorandum
TO: Todd Schwingle, Dion Doege, Jacob Halbert, Brett Kelly, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom Nowicki, Beth
Stroik, Kori Kenney, Lab File
SUBJECT: Milorganite Monthly Data —July 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of July 2019.
The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin
(Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
Richard Vincent Date
Laboratory Team Supervisor
Report Review By:
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

i iNSD
lMR11�S i8t t Wlli�Will
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQMethod
Monthly Milorganite Report DW
July 2019
Milorganite Daily Composite
Lab
07/01/19
DM0701/19011203
< 18 mg/kg D.W.
18
71
SW846: 6010C
MMSD
07/02/19
07/03/19
DM0702/19011300
DM0703/19011567
< 17 mg/kg D.W.
< 18 mg/kg D.W.
17
18
70
71
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/04/19
DM0704119011586
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
07/05/19
DM0705/19011601
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
< 17 mg/kg D.W.
17
67
Q3. SW846: 6010C
MMSD
07/07/19
DM0707/19012153
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
07/08/19
DM0708119012166
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
< 18 mg/kg D.W.
18
70
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
07/11/19
DM0711/19012362
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
07/13/19
07/14/19
DM0713/19012388
DM0714/19012517
< 18 mg/kg D.W.
< 18 mg/kg D.W.
18
18
70
70
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/15/19
07/16/19
DM0715/19012530
OM0716/19012837
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
70
69
SW846: 6010C
Q3. SW846: 6010C
MMSD
MMSD
07/17/19
DM0717/19013099
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
07/19/19
DM0719/19013133
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
07/20/19
DM0720/19013337
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
07/21/19
DM0721/19013356
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
07/22/19
DM0722/19013369
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
07/23/19
DM0723/19013411
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
07/24/19
DM0724/19013439
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
07/25/19
DM0725/19013556
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
07/26/19
DM0726/19013626
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
07/27/19
07/28/19
DM0727/19013912
DM0728/19013931
< 17 mg/kg D.W.
< 18 mg/kg D.W.
17
18
68
71
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/29/19
DM0729/19014090
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
07/30/19
DM0730/19014117
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
< 17 mg/kg D.W.
17
68
Q3. SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
17 mg/kg D.W.
Page 1 of 16
SY5/rpt1N11oMonth1yDW 4126119 tj Printed: 8115119 0735

t" �<NNSD
::
i1iR11kRS t9f A Ci�t
CADMIUM ICP Dry wt.
Sample Date Sample ID
Result
•.
LOQ QA
Monthly Mllorganite Report DW
July 2019
Milorganite Daily Composite
Flags Analytical Method Lab
07/01/19
DM0701119011203
< 0.96 mg/kg D.W.
0.96
3.6
SW846: 6010C
MMSD
07/02/19
DM0702119011300
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
07/03/19
DM0703/19011567
< 0.96 mg/kg D.W.
0.96
3.7
SW846: 6010C
MMSD
07/04/19
DM0704/19011586
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
07/05/19
DM0705119011601
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
07/07/19
DM0707/19012153
< 0.92 mg/kg D.W.
0.92
IS
SW846: 6010C
MMSD
07/08/19
DM0708/19012166
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
< 0.96 mg/kg D.W.
0.96
3.6
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
07/11/19
DM0711/19012362
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
07/13/19
DM0713/19012388
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
07/14/19
DM0714/19012517
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
07/15/19
07/16/19
DM0715/19012530
DM0716/19012837
< 0.9S mg/kg D.W.
< 0.93 mg/kg D.W.
0.95
0.93
3.6
3.5
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/17/19
DM0717/19013099
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
07/19/19
DM0719/19013133
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
07/20/19
DM0720/19013337
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
07/21/19
DM0721/19013356
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
07/22/19
DM0722/19013369
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
07/23/19
DM0723/19013411
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
07/24/19
DM0724119013439
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
07/25/19
DM0726/19013556
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
07/26/19
DM0726/19013626
< 0.92 mg/kg D.W.
0.92
3.5
B8. SW846: 6010C
MMSD
07/27/19
DM0727/19013912
< 0.92 mg/kg D.W.
0.92
IS
B8. SW846: 6010C
MMSD
07/28/19
DM0728/19013931
< 0.96 mg/kg D.W.
0.96
3.6
B8. SW846: 6010C
MMSD
07/29/19
DM0729/19014090
< 0.92 mg/kg D.W.
0.92
IS
B8. SW846: 6010C
MMSD
07/30/19
DM0730/19014117
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
0.91 mg/kg
O.W.
Page 1 of 16
5Y51rpt1M1/oMonth/yDW 4126119 tj Printed.- 8115/19 07:35

4NSD
�ut1r�SFOtAttt;�l
COPPER ICP Dry wt.
.. .. LOQ
07/01/19 DM0701/19011203 210 mg/kg D.W. 6.9 26
Monthly Milorganite Report DW
July 2019
Milorganite Daily Composite
SW846: 6010C MMSD
07/02/19
DM0702/19011300
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
07/03/19
DM0703/19011567
220 mg/kg D.W.
7
27
SW846: 6010C
MMSD
07/04/19
DM0704/19011586
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
07/05/19
DM0705/19011601
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
07/07/19
DM0707/19012153
220 mg/kg D.W.
6.6
25
SWB46: 6010C
MMSD
07/08/19
DM0708/19012166
220 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
230 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
07/11/19
DM0711/19012362
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
07/13/19
DM0713/19012388
190 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
07/14/19
DM0714/19012517
190 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
07/15/19
07/16/19
DM0715/19012530
DM0716/19012837
190 mg/kg D.W.
220 mg/kg D.W.
6.9
6.8
26
26
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/17/19
DM0717/19013099
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
07/19/19
DM0719/19013133
240 mg/kg D.W.
6.8
26
QI SW846: 6010C
MMSD
07/20/19
07/21/19
DM0720/19013337
DM0721/19013356
230 mg/kg D.W.
220 mg/kg D.W.
6.6
6.7
25
25
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/22/19
DM0722/19013369
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
07/23/19
DM0723/19013411
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
07/24/19
DM0724/19013439
230 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
07/25/19
DM0725/19013556
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
07/26/19
DM0726/19013626
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
07/27/19
DM0727/19013912
210 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
07/28/19
DM0728/19013931
210 mg/kg D.W.
7
26
SW846: 6010C
MMSD
07/29/19
DM0729/19014090
200 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
07/30/19
DM0730/19014117
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
220 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
Avg Result: 220 mg/kg D.W.
Min LOD:
6.6 mg/kg D.W.
Max Result: 240 mg/kg D.W.
Page 3 of 16
5Y5/rptlM1f0M017h/yDW 4126119 t% Printed: 8115119 0735

iNNSDJuly
NIA1AN N A
IRON ICP Dry wt.
samp, bate Sample ID
Result
LOD
LOQ QA
Monthly Milorganite Report DW
2019
Milorganite Daily Composite
Flags Analytical Method Lab
07/01/19
DM0701/19011203
33000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
07/02/19
DM0702/19011300
36000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
07/03/19
DM0703119011567
35000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
07/04/19
DM0704/19011586
38000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
07/05/19
DM0705/19011601
37000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
42000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
07/07/19
DM0707/19012153
41000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
07/08/19
DM0708/19012166
38000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
36000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
38000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
07/11/19
DM0711/19012362
36000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
37000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/13/19
DM0713/19012388
32000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
07/14/19
DM0714/19012517
33000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
07/15/19
DM0715/19012530
33000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
07/16/19
DM0716/19012837
38000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/17/19
DM0717/19013099
38000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
37000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/19/19
DM0719/19013133
39000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/20/19
DM0720/19013337
37000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
07/21/19
DM0721/19013356
35000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
07/22/19
DM0722/19013369
34000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/23/19
DM0723/19013411
34000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/24/19
DM0724/19013439
35000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
07/25/19
DM0725/19013556
37000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/26/19
DM0726/19013626
38000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
07/27/19
DM0727/19013912
38000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
07/28/19
DM0728119013931
40000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
07/29/19
DM0729/19014090
38000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
07/30/19
DM0730119014117
42000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
46000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
Avg Result: 37000 mg/kg D.W.
Min LOD:
520 mg/kg
D.W.
Max Result: 46000 mg/kg D.W.
Page 4 o/ 16
5Y5/rpt1M11oMonth/yDW 4126119 tj Printed: 8115119 07.•35

NSD
PARIMfRS I'm A tiff
LEAD ICP Dry wt.
ampe ae Sample ID Result LOD LO.
07/01/19 DM0701/19011203 34 mg/kg D.W. 3 8.9
Monthly Milorganite Report DW
July 2019
Milorganite Daily Composite
SW846: 6010C MMSD
07/02/19
DM0702/19011300
32 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
07/03/19
DM0703/19011567
33 mg/kg D.W.
3
9
SW846: 6010C
MMSD
07/04/19
DM0704/19011586
36 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
07/05/19
DM0705/19011601
35 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
36 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
07/07/19
DM0707/19012153
39 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
07/08/19
DM0708/19012166
37 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
36 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
35 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
07/11/19
DM0711/19012362
34 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
36 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
07/13/19
DM0713/19012388
28 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
07/14/19
DM0714/19012517
28 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
07/15/19
07/16/19
DM0715/19012530
DM0716/19012837
27 mg/kg D.W.
34 mg/kg D.W.
2.9
2.9
8.8
8.7
SW846-.6010C
SW846: 6010C
MMSD
MMSD
07/17/19
DM0717/19013099
33 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
33 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
07/19/19
DM0719/19013133
34 mg/kg D.W.
2.9
8.8
D2, Q2. SW846: 6010C
MMSD
07/20/19
--- --
07/21/19
DM0720/19013337
-- -- -
DM0721/19013356
32 mg/kg D.W.
------- -
31 mg/kg D.W.
2.8
2.9
8.5
8.6
SW846: 6010C
--- ----
SW846: 6010C
MMSD
-- -
MMSD
07/22/19
DM0722/19013369
37 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
07/23/19
DM0723/19013411
43 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
07/24/19
DM0724/19013439
41 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
07/25/19
DM0725/19013556
40 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
07/26/19
DM0726/19013626
37 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
07/27/19
DM0727/19013912
36 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
07/28/19
DM0728/19013931
36 mg/kg D.W.
3
9
SW846: 6010C
MMSD
07/29/19
DM0729/19014090
36 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
07/30/19
DM0730/19014117
36 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
35 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
Avg Result: 35 mg/kg D.W.
Min LOD:
2.8 mg/kg D.W.
Max Result: 43 mg/kg D.W.
Page 5 016
5Y51rptlMi1oMonth1yDW 4126119 tj Printed: 8115119 07:35

1 iNSD
''t
+"1NEx4 M A CII]WI
MOLYBDENUM ICP Dry wt.
Sample Date Sample 16
Result
LOD
LOQ
Monthly Milorganite Report DW
July 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
07/01/19
DM0701/19011203
8.2 mg/kg D.W.
4.6
18
1
SW846: 6010C
MMSD
07/02/19
DM0702/19011300
9.1 mg/kg D.W.
4.6
17
J.
SW846: 6010C
MMSD
07/03/19
DM0703/19011567
8.9 mg/kg D.W.
4.7
18
1
SW846: 6010C
MMSD
07/04/19
DM0704/19011586
8.9 mg/kg D.W.
4.4
17
1
SW846: 6010C
MMSD
07/05/19
DM0705/19011601
8.8 mg/kg D.W.
4.4
17
1
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
8.9 mg/kg D.W.
4.4
17
1
SW846: 6010C
MMSD
07/07/19
DM0707/19012153
8.8 mg/kg D.W.
4.4
17
J.
SW846: 6010C
MMSD
07/08/19
DM0708/19012166
8.8 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
8.6 mg/kg D.W.
4.6
18
1
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
9.1 mg/kg D.W.
4.6
17
1
SW846: 6010C
MMSD
07/11/19
DM0711119012362
8.3 mg/kg D.W.
4.5
17
].
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
8.1 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
07/13/19
DM0713/19012388
7.1 mg/kg D.W.
4.6
18
1
SW846: 6010C
MMSD
07/14/19
DM0714/19012517
7.2 mg/kg D.W.
4.6
18
1.
SW846: 6010C
MMSD
07/15/19
DM0715/19012530
7 mg/kg D.W.
4.6
17
1.
SW846: 6010C
MMSD
07/16/19
DM0716/19012837
8.7 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
07/17/19
DM0717/19013099
8.8 mg/kg D.W.
4.5
17
J.
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
8.7 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
07/19/19
DM0719/19013133
9.4 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
07/20/19
07/21/19
DM0720/19013337
DM0721/19013356
8.8 mg/kg D.W.
8.5 mg/kg D.W.
4.4
4.4
17
17
1
1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/22/19
DM0722/19013369
8.8 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
07/23/19
DM0723119013411
8.8 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
07/24/19
DM0724/19013439
9.3 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
07/25/19
DM0725/19013556
9.4 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
07/26/19
DM0726/19013626
8.7 mg/kg D.W.
4.4
17
1
SW846: 6010C
MMSD
07/27/19
DM0727/19013912
8.6 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
07/28/19
DM0728/19013931
8.7 mg/kg D.W.
4.6
18
1
SW846: 6010C
MMSD
07/29/19
DM0729/19014090
8.4 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
07/30/19
DM0730/19014117
8.5 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
8.4 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
Avg Result: 8.6 mg/kg D.W.
Min LOD:
4.4 mg/kg D.W.
Max Result: 9.4 mg/kg D.W.
Page 6 of 16
5Y5/rptlM110M0nth1yDW 4126119 tj Printed: 8115119 07:35

thtIHNSD
�
3 ,
��A FDf A L1EI1�
NICKEL ICP Dry wt.
•.§amplelD Result LOD LOQ
07/01/19 DM0701/19011203 21 mg/kg D.W. 3.3 9.9
Monthly Milorganite Report DW
July 2019
Milorganite Daily Composite
SW846: 6010C MMSD
07/02/19
DM0702/19011300
22 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
07/03/19
DM0703/19011567
23 mg/kg D.W.
3.3
10
SW846: 6010C
MMSD
07/04/19
DM0704/19011586
23 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
07/05/19
DM0705/19011601
24 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
28 mg/kg D.W.
3.2
9.4
SW846: 6010C
MMSD
07/07/19
DM0707/19012153
28 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
07/08/19
DM0708/19012166
27 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
22 mg/kg D.W.
3.3
9.9
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
23 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
07/11/19
DM0711/19012362
22 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
22 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
07/13/19
DM0713/19012388
19 mg/kg D.W.
3.3
9.9
SW846: 6010C
MMSD
07/14/19
DM0714/19012517
19 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
07/15/19
07/16/19
DM0715/19012530
DM0716/19012837
18 mg/kg D.W.
25 mg/kg D.W.
3.3
3.2
9.8
9.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/17/19
DM0717/19013099
23 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
22 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
07/19/19
DM0719/19013133
23 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
07/20/19
07/21/19
DM0720/19013337
DM0721/19013356
21 mg/kg D.W.
21 mg/kg D.W.
3.2
3.2
9.5
9.5
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/22/19
DM0722/19013369
22 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
07/23/19
DM0723/19013411
25 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
07/24/19
DM0724/19013439
22 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
07/25/19
DM0725/19013556
26 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
07/26/19
DM0726/19013626
25 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
07/27/19
DM0727/19013912
26 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
07/28/19
DM0728/19013931
25 mg/kg D.W.
3.3
10
SW846: 6010C
MMSD
07/29/19
DM0729/19014090
24 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
07/30/19
DM0730/19014117
25 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
26 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
Avg Result: 23 mg/kg D.W.
Min LOD:
3.1 mg/kg D.W.
Max Result: 28 mg/kg D.W.
Page 7 of 16
5YS1rpt1MAbMonth/y0W 4126119 tj Printed.' 811511907:35

'tONSD
I"9;lf ►u ll cam eE
PHOSPHORUS ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
July 2019
Milorganite Daily Composite
.. Flags Analytical Method Lab
07/01/19
DM0701/19011203
22000 mg/kg D.W.
24
93
SW846: 6010C
MMSD
07/02/19
DM0702/19011300
22000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
07/03/19
DM0703/19011567
23000 mg/kg D.W.
24
93
SW846: 6010C
MMSD
07/04/19
DM0704/19011586
23000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
07/05/19
DM0705/19011601
23000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
24000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
07/07/19
DM0707/19012153
24000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
07/08/19
DM0708/19012166
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
23000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
23000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
07/11/19
DM0711/19012362
23000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
07/13/19
DM0713/19012388
21000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
07/14/19
DM0714/19012517
21000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
07/15/19
07/16/19
DM0715/19012530
DM0716/19012837
21000 mg/kg D.W.
25000 mg/kg D.W.
24
24
92
90
Q2.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/17/19
DM0717/19013099
25000 mg/kg D.W.
24
90
Q2.
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
26000 mg/kg D.W.
24
91
Q2.
SW846: 6010C
MMSD
07/19/19
DM0719/19013133
26000 mg/kg D.W.
24
91
Q2.
SW846: 6010C
MMSD
07/20/19
DM0720119013337
24000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
07/21/19
DM0721/19013356
24000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
07/22/19
DM0722/19013369
23000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
07/23/19
DM0723/19013411
23000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
07/24/19
DM0724/19013439
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
07/25/19
DM0725/19013556
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
07/26/19
DM0726/19013626
23000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
07/27/19
DM0727/19013912
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
07/28/19
DM0728/19013931
24000 mg/kg D.W.
24
93
SW846: 6010C
MMSD
07/29/19
DM0729/19014090
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
07/30/19
DM0730/19014117
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
24000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
Avg Result: 23000 mg/kg D.W.
Min LOD:
23 mg/kg D.W.
Max Result: 26000 mg/kg D.W.
Page 8 of 16
SYS/rptlM11oMonth1y0W 4126119 U Printed: 8115119 07:35

tIINSD
PJtNTOM 0 1 tlIM9 fVORCAk4N'
POTASSIUM ICP Dry wt.
Monthly Milorganite Report DW
July 2019
Milorganite Daily Composite
07/01/19
DM0701/19011203
4300 mg/kg D.W.
300
890
AO.
SW846: 6010C
MMSD
07/02/19
DM0702/19011300
3900 mg/kg D.W.
290
880
AO.
SW846: 6010C
MMSD
07/03/19
DM0703/19011567
3800 mg/kg D.W.
300
900
AO.
SW846: 6010C
MMSD
07/04/19
DM0704/19011586
4100 mg/kg D.W.
280
850
AO.
SW846: 6010C
MMSD
07/05/19
DM0705/19011601
4100 mg/kg D.W.
280
850
AO.
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
3500 mg/kg D.W.
280
850
B8.
SW846: 6010C
MMSD
07/07/19
DM0707/19012153
3600 mg/kg D.W.
280
850
B8.
SW846: 6010C
MMSD
07/08/19
DM0708/19012166
3700 mg/kg D.W.
290
870
B8.
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
4000 mg/kg D.W.
300
890
A0, B8.
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
4000 mg/kg D.W.
290
880
SW846: 6010C
MMSD
07/11/19
DM0711/19012362
3800 mg/kg D.W.
290
870
A0, B8.
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
3900 mg/kg D.W.
290
870
SW846: 6010C
MMSD
07/13/19
DM0713/19012388
3700 mg/kg D.W.
300
890
AO.
SW846: 6010C
MMSD
07/14/19
DM0714/19012517
4100 mg/kg D.W.
300
890
AO.
SW846: 6010C
MMSD
07/15/19
07/16/19
DM0715/19012530
DM0716119012837
3900 mg/kg D.W.
3500 mg/kg D.W.
290
290
880
870
AO.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/17/19
DM0717/19013099
4100 mg/kg D.W.
290
870
AO.
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
3800 mg/kg D.W.
290
880
AO.
SW846: 6010C
MMSD
07/19/19
DM0719/19013133
4100 mg/kg D.W.
290
880
AO.
SW846: 6010C
MMSD
07/20/19
07/21/19
DM0720/19013337
DM0721/19013356
3800 mg/kg D.W.
4200 mg/kg D.W.
280
290
850
860
AO.
AO.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/22/19
DM0722/19013369
4200 mg/kg D.W.
290
870
AO.
SW846: 6010C
MMSD
07/23/19
DM0723/19013411
3900 mg/kg D.W.
290
880
AO, B8.
SW846: 6010C
MMSD
07/24/19
DM0724/19013439
4000 mg/kg D.W.
290
860
AO.
SW846: 6010C
MMSD
07/25/19
DM0725/19013556
4000 mg/kg D.W.
290
870
A0, Q2.
SW846: 6010C
MMSD
07/26/19
07/27/19
DM0726/19013626
DM0727/19013912
3600 mg/kg D.W.
3500 mg/kg D.W.
280
290
850
860
B8.
B8.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/28/19
DM0728/19013931
3300 mg/kg D.W.
300
900
B8.
SW846: 6010C
MMSD
07/29/19
DM0729/19014090
3100 mg/kg D.W.
290
860
88.
SW846: 6010C
MMSD
07/30/19
DM0730/19014117
3100 mg/kg D.W.
290
870
B8.
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
2900 mg/kg D.W.
290
860
88.
SW846: 6010C
MMSD
Avg Result: 3800 mg/kg D.W.
Min LOD:
280 mg/kg D.W.
Max Result: 4300 mg/kg D.W.
Page 9 of 16
SY5/rpt1Mi1aMonth1yDW 4126119 tj Printed: 8115119 07:35

14NSD
w"WACam"WWO
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Mllorganite Report DW
July 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
07/01/19
DM0701/19011203
5.6 mg/kg D.W.
4.3
13
J.
SW846: 6010C
MMSD
07/02/19
DMO702119011300
6.5 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
07/03/19
DM0703/19011567
6 mg/kg D.W.
4.3
13
J.
SW846: 6010C
MMSD
07/04/19
DM0704/19011586
5.7 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
07/05/19
DM0705/19011601
5.2 mg/kg D.W.
4.1
12
J.
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
4.1 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
07/07/19
DM0707/19012153
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
07/08/19
DM0708/19012166
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
4.6 mg/kg D.W.
4.3
13
].
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
5.2 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
07/11/19
DM0711/19012362
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
7 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
07/13/19
DM0713/19012388
4.8 mg/kg D.W.
4.3
13
J.
SW846: 6010C
MMSD
07/14/19
DM0714/19012517
< 4.3 mg/kg D.W.
4.3
13
SW846: 6010C
MMSD
07/15/19
DM0715/19012530
< 4.3 mg/kg D.W.
4.3
13
SW846: 6010C
MMSD
07/16/19
DM0716/19012837
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
07/17/19
DM0717/19013099
7.5 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
6.7 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
07/19/19
DM0719/19013133
5 mg/kg D.W.
4.2
13
J, Q2.
SW846: 6010C
MMSD
07/20/19
07/21/19
DM0720/19013337
DM0721/19013356
5.7 mg/kg D.W.
5.4 mg/kg D.W.
4.1
4.1
13
13
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/22/19
DM0722/19013369
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
07/23/19
DM0723/19013411
6.1 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
07/24/19
DM0724/19013439
4.9 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
07/25/19
DM0725/19013556
5.4 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
07/26/19
DM0726/19013626
6.6 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
07/27/19
DM0727/19013912
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
07/28/19
DM0728/19013931
< 4.3 mg/kg D.W.
4.3
13
SW846: 6010C
MMSD
07/29/19
DM0729/19014090
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
07/30/19
DM0730/19014117
4.9 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
6.2 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
Avg Result: 3.8 mg/kg D.W.
Min LOD:
4.1 mg/kg D.W.
Max Result: 7.5 mg/kg D.W.
Page 10 of 16
SY5/rpt1M1/oMonth/yDW 4126119 tj Printed: 8115119 0735

NSD
[�t1�S t6f 1
Solids (% Moisture)
Sample Date Sample ID
07/01/19 DM0701/19011203
07/02/19 DM0702/19011300
Monthly Milorganite Report DW
July 2019
Milorganite Daily Composite
lit .. LOQ ••
9.3 % 0.1 SM 2540 G (1997) MMSD
8.3 % 0.1 SM 2540 G (1997) MMSD
07/03/19
DM0703/19011567
9.9 %
0.1
SM 2540 G (1997)
MMSD
07/04/19
DM0704119011586
4.9 %
0.1
SM 2540 G (1997)
MMSD
07/05/19
DM0705/19011601
4.4 %
0.1
SM 2540 G (1997)
MMSD
07/06/19
DM0706/19012134
4.8 %
0.1
SM 2540 G (1997)
MMSD
07/07/19
DM0707/19012153
5.2 %
0.1
SM 2540 G (1997)
MMSD
07/08/19
DM0708/19012166
6.7 %
0.1
SM 2540 G (1997)
MMSD
07/09/19
DM0709/19012193
9.2 %
0.1
SM 2540 G (1997)
MMSD
07/10/19
DM0710/19012221
7.9 %
0.1
SM 2540 G (1997)
MMSD
07/11/19
DM0711/19012362
7.2 %
0.1
SM 2540 G (1997)
MMSD
07/12/19
DM0712/19012377
7.1 %
0.1
SM 2540 G (1997)
MMSD
07/13/19
DM0713/19012388
8.9 %
0.1
SM 2540 G (1997)
MMSD
07/14/19
DM0714/19012517
8.7 %
0.1
SM 2540 G (1997)
MMSD
07/15/19
07/16/19
DM0715/19012530
DM0716/19012837
8.4 %
6.7 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
07/17/19
DM0717/19013099
7.1 %
0.1
SM 2540 G (1997)
MMSD
07/18/19
DM0718/19013118
7.7 %
0.1
SM 2540 G (1997)
MMSD
07/19/19
DM0719/19013133
7.4 %
0.1
SM 2540 G (1997)
MMSD
07/20/19
07/21/19
DM0720/19013337
DM0721/19013356
5.1 %
5.7 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
07/22/19
DM0722/19013369
7.1 %
0.1
SM 2540 G (1997)
MMSD
07/23/19
DM0723/19013411
7.6 %
0.1
SM 2540 G (1997)
MMSD
07/24/19
DM0724/19013439
5.8 %
0.1
SM 2540 G (1997)
MMSD
07/25/19
DM0725/19013556
6.8 %
0.1
SM 2540 G (1997)
MMSD
07/26/19
DM0726/19013626
5.2 %
0.1
SM 2540 G (1997)
MMSD
07/27/19
DM0727/19013912
5.8 %
0.1
SM 2540 G (1997)
MMSD
07/28/19
DM0728/19013931
9.6 %
0.1
SM 2540 G (1997)
MMSD
07/29/19
DM0729119014090
6 %
0.1
SM 2540 G (1997)
MMSD
07/30/19
DM0730/19014117
7.1 %
0.1
SM 2540 G (1997)
MMSD
07/31/19
DM0731/19014145
6.1 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 7 %
Min LOD: 0.1 %
Max Result: 9.9
Page 11 o/ 16
5Y5/rptlM1/oMonth/yDW 4/76119 q Printed: 8115119 0735

lltliNSD
ZINC ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Mllorganite Report DW
July 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
07/01/19
DM0701/19011203
390 mg/kg D.W.
19
56
SW846: 6010C
MMSD
07/02/19
DM0702/19011300
400 mg/kg D.W.
18
56
SW846: 6010C
MMSD
07/03/19
DM0703/19011567
410 mg/kg D.W.
19
56
SW846: 6010C
MMSD
07/04/19
DM0704/19011586
410 mg/kg D.W.
18
54
SW846: 6010C
MMSD
07/05/19
DM0705119011601
410 mg/kg D.W.
18
53
SW846: 6010C
MMSD
07/06/19
DM0706/19012134
440 mg/kg D.W.
18
54
SW846: 6010C
MMSD
07/07/19
DM0707119012153
440 mg/kg D.W.
18
54
SW846: 6010C
MMSD
07/08/19
DM0708/19012166
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
07/09/19
DM0709/19012193
420 mg/kg D.W.
19
56
SW846: 6010C
MMSD
07/10/19
DM0710/19012221
410 mg/kg D.W.
18
55
SW846: 6010C
MMSD
07/11/19
DM0711/19012362
410 mg/kg D.W.
18
55
SW846: 6010C
MMSD
07/12/19
DM0712/19012377
400 mg/kg D.W.
18
55
SW846: 6010C
MMSD
07/13/19
DM0713/19012388
340 mg/kg D.W.
19
56
SW846: 6010C
MMSD
07/14/19
DM0714/19012517
340 mg/kg D.W.
19
56
SW846: 6010C
MMSD
07/15/19
DM0715/19012530
350 mg/kg D.W.
18
56
SW846: 6010C
MMSD
07/16/19
DM0716/19012837
430 mg/kg D.W.
18
55
SW846: 6010C
MMSD
07/17/19
DM0717/19013099
420 mg/kg D.W.
18
S5
SW846: 6010C
MMSD
07/18/19
DM0718/19013118
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
07/19/19
DM0719119013133
450 mg/kg D.W.
18
55
D2, Q2. SW846: 6010C
MMSD
07/20/19
DM0720/19013337
420 mg/kg D.W.
18
54
SW846: 6010C
MMSD
07/21/19
DM0721/19013356
410 mg/kg D.W.
18
54
SW846: 6010C
MMSD
07/22/19
DM0722/19013369
420 mg/kg D.W.
18
55
SW846: 6010C
MMSD
07/23/19
DM0723/19013411
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
07/24/19
DM0724/19013439
450 mg/kg D.W.
18
54
SW846: 6010C
MMSD
07/25/19
DM0725/19013556
450 mg/kg D.W.
18
55
SW846: 6010C
MMSD
07/26/19
DM0726/19013626
440 mg/kg D.W.
18
54
SW846: 6010C
MMSD
07/27/19
DM0727/19013912
420 mg/kg D.W.
18
54
SW846: 6010C
MMSD
07/28/19
DM0728/19013931
420 mg/kg D.W.
19
56
SW846: 6010C
MMSD
07/29/19
DM0729/19014090
410 mg/kg D.W.
18
54
SW846: 6010C
MMSD
07/30/19
DM0730/19014117
430 mg/kg D.W.
18
55
SW846: 6010C
MMSD
07/31/19
DM0731/19014145
430 mg/kg D.W.
18
54
SW846: 6010C
MMSD
Avg Result: 420 mg/kg D.W.
Min LOD:
18 mg/kg D.W.
Max Result: 450 mg/kg D.W.
Page 12 of 16
5Y51rpt1M1/oMonth/yDW 4126119 tj Printed: 8115119 07•35

M14SD
16tA LiiAit
Phosphorus - Total % DW (Calc.)
Sample •.
07/01/19 DM0701/19011203
2.2 % D.W.
.D LOQ
0.1
0.1
Monthly Milorganite Report DW
July 2019
Milorganite Daily Composite
QA Flags
SW846: 6010C MMSD
07/02/19 DM0702/19011300
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/03/19 DM0703/19011567
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/04/19 DM0704/19011586
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/05/19 DM0705/19011601
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/06/19 DM0706/19012134
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/07/19 DM0707/19012153
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/08/19 DM0708/19012166
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/09/19 DM0709/19012193
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/10/19 DM0710/19012221
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/11/19 DM0711/19012362
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/12/19 DM0712/19012377
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/13/19 DM0713/19012388
2.1 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/14/19 DM0714/19012517
2.1 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/15/19 DM0715/19012530
07/16/19 DM0716/19012837
2.1 % D.W.
2.5 % D.W.
0.1
0.1
0.1
0.1
Q2.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/17/19 DM0717/19013099
2.5 % D.W.
0.1
0.1
Q2.
SW846: 6010C
MMSD
07/18/19 DM0718/19013118
2.6 % D.W.
0.1
0.1
Q2.
SW846: 6010C
MMSD
07/19/19 DM0719/19013133
2.6 % D.W.
0.1
0.1
Q2.
SW846: 6010C
MMSD
07/20/19 DM0720/19013337
07/21/19 DM0721/19013356
2.4 % D.W.
2.4 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
07/22/19 DM0722/19013369
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/23/19 DM0723/19013411
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/24/19 DM0724/19013439
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/25/19 DM0725/19013556
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/26/19 DM0726119013626
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/27/19 DM0727/19013912
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/28/19 DM0728/19013931
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/29/19 DM0729119014090
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/30/19 DM0730/19014117
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/31/19 DM0731/19014145
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
Avg Result: 2.3 0/6 D.W.
ALUMINUM ICP Dry wt.
Sample Date Sample ID
Min LOD: 0.1 % D.W.
Result LOD
LOQ
.• Flags
Max Result: 2.6 % D.W.
Milorganite Weekly Composite
Analytical Method Lab
07/13/19 WMC28/19012532
9600 mg/kg D.W.
57
200
B8.
SW846: 6010C
MMSD
Avg Result: 9600 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Sample Date Sample ID
Min LOD: 57 mg/kg D.W.
Result LOD LOQ
QA Flags
Analytical Method
Lab
07/13/19 WMC28/19012532
0.13 %
0.11
0.37
AOAC (13) 2.065
MMSD
Avg Result: 0.13 %
SY5/rpt1M11oMonfh1yDW 4126119 tj
Min LOD:
0.11
Page 13 o/ 16
Printed.• 8115119 07.-35

NSD
Ptilow fo licum
Monthly Milorganite Report DW
July 2019
Milorganite Weekly Composite
BORON ICP Dry wt.
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
07/13/19 WMC28/19012532 18 mg/kg D.W. 1.1 3.4 SW846: 6010C CT Lab
Avg Result: 18 mg/kg D.W. Min LOD: 1.1 mg/kg D.W.
CHROMIUM ICP Dry wt.
Date Sample ID Result LOD LOQ •• Flags Analytical Method Lab
07/13/19 WMC28/19012532 150 mg/kg D.W. 1.6 4.8 SW846: 6010C MMSD
Avg Result: 150 mg/kg D.W. Min LOD: 1.6 mg/kg D.W.
COBALT ICP Dry wt.
Sample Date ID Result LOD LOQ •• Flags Analytical Method Lab
07/13/19 WMC28/19012532 3.6 mg/kg D.W. 0.28 1.1 68. SW846: 6010C MMSD
Avg Result: 3.6 mg/kg D.W. Min LOD: 0.28 mg/kg D.W.
MERCURY by M. 7471 (sludge)
Date Sample ID Result LOD LOQ .• Flags Analytical Method Lab
07/06/19 WMC27/19012168 0.11 mg/kg D.W. 0.0055 0.019 EPA 7471E CT Lab
07/13/19 WMC28/19012532 0.14 mg/kg D.W. 0.012 0.04 EPA 74718 CT Lab
07/20/19 WMC29119013371 < 0.011 mg/kg D.W. 0.011 0.037 AX. EPA 7471E Cr Lab
07/27/19 WMC30/19014092 0.36 mg/kg D.W. 0.014 0.046 EPA 7471E CT Lab
Avg Result: 0.15 mg/kg D.W. Min LOD: 0.0055 mg/kg D.W. Max Result: 0.36 mg/kg D.W.
NITRATE NITROGEN
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
07/13/19 WMC28/19012532 1.5 % 0.5 AOAC (16) 930.01 MMSD
Avg Result: 1.5 % Min LOD: 0.5 "/o
NITROGEN-Total(Manual)
Date Sample ID Result .. LOQ QA Flags Analytical Method Lab
07/13/19 WMC28/19012532 5.9 % 0.11 AOAC (16) 955.04 MMSD
Avg Result: 5.9 "/o Min LOD: 0.11 "/o
NITROGEN -Water Insoluble
07/13/19
WMC28/19012532
4 % 0.5
AOAC (16) 945.01
MMSD
PH -Solids
Sample Date
Avg Result: 4 %
Sample ID
Min LOD: 0.5 "/o
Result LOD LOQ QA Flags
Analytical Method
Lab
07/06/19
WMC27/19012168
6.37Stnd. Units 0.1
SW846: 9045D
MMSD
07/13/19
WMC28/19012532
6.38 Stnd. Units 0.1
SW846: 9045D
MMSD
07/20/19
WMC29/19013371
6.33 Stnd. Units 0.1
SW846: 9045D
MMSD
07/27/19
WMC30/19014092
6.25 Stnd. Units 0.1
SW846: 9045D
MMSD
Avg Result: 6.3 Stnd. Units
Min LOD: 0.1 Stnd. Units
Max Result: 6.38 Stnd. Units
Page 14 of 16
5Y5/rpt1 Mi1dMonthlyDW 4126119 tj Printed: 8115119 07:35

Monthly Milorganite Report DW
i NSD
July 2019
Mllin n /I ttil smia eli
Milorganite Weekly Composite
Solids (% Moisture)
►.Sample ID
Result LOD
LOQ QA Flag s Analy tical Method
07/06/19 WMC27/19012168
8.2 % 0.1
SM 2540 G (1997) MMSD
07/13/19 WMC28/19012532
7.6 % 0.1
SM 2540 G (1997) MMSD
07/20/19 WMC29/19013371
7.3 % 0.1
SM 2540 G (1997) MMSD
07/27/19 WMC30/19014092
8.5 % 0.1
SM 2540 G (1997) MMSD
Min LOD: 0.1 a/o
Solids (% Volatile)
Sample Date Sample ID,
I.,
•.Analytical Method Lab
07/13/19 WMC28119012532
70 % 0.1
SM 2540 G (1997) MMSD
Avg Result: 70 %
Min LOD: 0.1 0/0
Solids (% Total)
Sample Date Sa"le ID
07/13/19 WMC28/19012532
oil
92 1
to 4"
SM 2540 G (1997) MMSD
Avg Result: 92 %
Min LOD: 0.1
Milorganite (Outfall 006) PRODUCTION
FECAL COLIFORM SLUDGE
..
Sample..
07/01/19
,-
19013889
< 0.19 MFN/g TS
..
0.19
QA Flags Analytical Method
EPA 1680
Lab
MMSD
07/09/19
19014352
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
07/16/19
19014903
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
07/23/19
19015672
0.21 MPN/g TS
0.19
AO. EPA 1680
MMSD
07/30/19
19016521
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
Min LOD:
0.19 MPN/g TS
Solids (%
Total)
,..
.. LOQ
QA Flags Analytical Method
Lab
07/01/19
19013889
92 %
0.1
SM 2540 G (1997)
MMSD
07/09/19
19014352
94 %
0.1
SM 2540 G (1997)
MMSD
07/16/19
19014903
94 %
0.1
SM 2540 G (1997)
MMSD
07/23/19 19015672 96 % 0.1 SM 2540 G (1997) MMSD
07/30/19 19016521 94 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 94 "/o Min LOD: 0.1 % Max Result: 96 %
Milorganite (Outfall 009) BAGGING
FECAL COLIFORM SLUDGE
Zample D mple ID Result LOD LOQ .• Flags Analytical Method Lab
07/09/19 19014354 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
Page IS of 16
SYS/rptI i/oMonth/yDW 4126119 tj Printed: 8115119 07.•35

I
14SD
Wo In A two soon
Monthly Milorganite Report DW
July 2019
Milorganite (Outfall 009) BAGGING
Solids (% Total)
Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
07/09/19 19014354 94 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 94 % Min LOD: 0.1
Milorganite (Outfall 008) SHIPPING
FECAL COLIFORM SLUDGE
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
0• •0. TS 0.19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
Solids (% Total)
Sample Date Sample To Result .. LOQ QA Flags Analytical Method Lab
07/09/19 19014353 93 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 93 0/6
Flag Descriptions
AO Other -- Flag requires additional explanation
AX Qualified data - see contract laboratory report
B3 Target analyte detected in method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits.
B8 LCS recovery was below control limits.
Min LOD: 0.1
B9 Low Level CCV recovery was outside of method acceptance limits
CO Data used for calculation of result was qualified
D3 Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
H1 Sample was received past holding time.
H3 . Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
IS Insufficient sample volume for analysis.
3 Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
LA Not analyzed - laboratory accident.
M1 Too numerous to count. _
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
MS Incubator/water bath temperature was outside method
requirements.
M7 Microbiology sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
SS Reading was not confirmed by a constant weight measurement
SD Supplemental details provided.(Water Quality only.)
T3 The BOD dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The BOD dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample is outside of the prescribed method temperature. range.
Page 16 o116
5Y5/rpt1Mi/oMonth/yDW 4126119 q Printed: 8115119 0735

TAW
S4, NNSD
PARTNERS FOR A CLEANER ENVIRONMENT
September 19, 2019
TO: Brett Kelly, Todd Schwingle, Dion Doege, Jacob Holbert, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom Nowicki, Beth
Stroik, Kori Kenney, Ethan Guyant, Lab File
SUBJECT: Milorganite Monthly Data — August 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of August 2019.
The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin
(Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
Richard Vincent Date
Laboratory Team Supervisor
Report Review By:
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

HSDAugust
tS t6t A C
ARSENIC ICP Dry wt.
�Sample Date Sample ID
ResultLOD
LOQ
Monthly Milorganite Report DW
2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
08/01/19
DMO801119014196
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
08/02/19
DM0802/19014211
< 18 mg/kg D.W.
18
70
SW846: 6010C
MMSD
08/03/19
DM0803/19014222
< 18 mg/kg D.W.
18
70
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
08/OS/19
DM0805/19014324
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
08/06/19
DMO806/19014383
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
08/07/19
DM0807/19015004
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
08/08/19
DM0808/19015023
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
08/09/19
DM0809/19015287
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
08/10/19
DM0810/19015298
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
08/11/19
DM0811/19015317
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
08/12/19
DM0812/19015332
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
08/13/19
08/14/19
DM0813/19015359
DM0814/19015387
< 18 mg/kg D.W.
< 17 mg/kg D.W.
18
17
70
69
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/15/19
08/16/19
DM0815/19015406
DM0816/19015623
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
69
68
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/17/19
DMO817/19015634
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
< 18 mg/kg D.W.
18
71
SW846: 6010C
MMSD
08/19/19
DM0819/19015709
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
08/20/19
DM0820/19015736
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
08/21/19
DM0821/19015769
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
08/22/19
DM0822/19015788
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
08/23/19
DMO823/19015803
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
08/24/19
DM0824/19015814
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
08/25/19
DM0825/19015833
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
08/26/19
DM0826/19015864
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
08/27/19
DMO827/19015890
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
08/28/19
DM0828/19015918
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
08/29/19
DM0829/19015937
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
08/30/19
DM0830119015952
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
08/31/19
DM0831/19015963
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
17 mg/kg D.W.
Page 1 of 16
5Y5/rpt1Mi1oMonth/y0W 4126119 tj Printed: 9119119 09:45

NNSD
t1 IMMACU
CADMIUM ICP Dry wt.
.. . Result LOD LOQ
08/01/19 DM0801/19014196 < 0.94 mg/kg D.W. 0.94 3.6
Monthly Milorganite Report DW
August 2019
Milorganite Daily Composite
lags Anali6k 4- 66-
SW846:6010C MMSD
08/02/19
DM0802/19014211
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
08/03/19
DM0803/19014222
< 0.95 mg/kg D.W.
0.95
3.6
B8.
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
< 0.93 mg/kg D.W.
0.93
3.5
B8.
SW846: 6010C
MMSD
08/05/19
DMO805/19014324
< 0.93 mg/kg D.W.
0.93
3.5
B8.
SW846: 6010C
MMSD
08/06/19
DM0806/19014383
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
08/07/19
DM0807/19015004
< 0.93 mg/kg D.W.
0.93
3.5
B8.
SW846: 6010C
MMSD
08/08/19
DM0808/19015023
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
08/09/19
DM0809/19015287
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
08/10/19
DM0810/19015298
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
08/11/19
DM0811/19015317
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
08/12/19
DM0812/19015332
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
08/13/19
DM0813/19015359
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
08/14/19
DM0814/19015387
< 0.93 mg/kg D.W.
0.93
3.5
B8.
SW846: 6010C
MMSD
08/15/19
08/16/19
DM0815/19015406
DM0816/19015623
< 0.93 mg/kg D.W.
< 0.92 mg/kg D.W.
0.93
0.92
3.5
3.5
B8.
B8.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/17/19
DM0817/19015634
< 0.95 mg/kg D.W.
0.95
3.6
B8.
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
< 0.96 mg/kg D.W.
0.96
3.6
B8.
SW846: 6010C
MMSD
08/19/19
DM0819/19015709
< 0.94 mg/kg D.W.
0.94
3.6
B8.
SW846: 6010C
MMSD
08/20/19
08/21/19
DM0820/19015736
DM0821/19015769
< 0.94 mg/kg D.W.
< 0.95 mg/kg D.W.
0.94
0.95
3.6
3.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/22/19
DM0822/19015788
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
08/23/19
DM0823/19015803
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
08/24/19
DMOB24/19015814
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
08/25/19
DM0825/19015833
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
08/26/19
DM0826/19015864
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
08/27/19
DM0827/19015890
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
08/28/19
DMOB28/19015918
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
08/29/19
DMO829/19015937
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
08/30/19
DM0830/19015952
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
08/31/19
DM0831/19015963
< 0.92 mg/kg D.W.
0.92
3.5
SW846-.6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
0.91 mg/kg D.W.
Page 1 of 16
5Y51rpt1MM0N0r?t171yDW 4126119 tj Printed., 9119119 09:45

SD
IMMINACUMMIlIff
COPPER ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
August 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
08/01/19
DM0801/19014196
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
08/02/19
DM0802/19014211
210 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
08/03/19
DM0803/19014222
210 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
210 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
08/05/19
DM0805/19014324
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
08/06/19
DM0806119014383
200 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
08/07/19
DM0807/19015004
200 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
08/08/19
DMO808/19015023
200 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
08/09/19
DMO809/19015287
210 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
08/10/19
DM0810/19015298
220 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
08/11/19
DM0811/19015317
220 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
08/12/19
DM0812/19015332
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
08/13/19
DM0813/19015359
210 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
08/14/19
DM0814/19015387
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
08/15/19
08/16/19
DMO815/19015406
DM0816/19015623
220 mg/kg D.W.
230 mg/kg D.W.
6.8
6.7
26
25
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/17/19
DMO817/19015634
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
220 mg/kg D.W.
7
26
SW846: 6010C
MMSD
08/19/19
DM0819/19015709
240 mg/kg D.W.
6.8
26
Q3. SW846: 6010C
MMSD
08/20/19
DM0820/19015736
240 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
08/21/19
DM0821/19015769
230 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
08/22/19
DM0822/19015788
230 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
08/23/19
DM0823/19015803
240 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
08/24/19
DMO824119015814
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
08/25/19
DMO825/19015833
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
08/26/19
DM0826/19015864
240 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
08/27/19
DM0827/19015890
240 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
08/28/19
DM0828/19015918
240 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
08/29/19
DM0829119015937
240 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
08/30/19
DM0830/19015952
240 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
08/31/19
DM0831/19015963
Avg Result: 220 mg/kg D.W.
220 mg/kg D.W.
Min LOD:
6.7 25
6.6 mg/kg D.W.
SW846: 6010C
Max Result: 240 mg/kg D.W.
MMSD
Page 3 of 16
SY5/rptl Mi/oMonth/yDW 4126119 0 Printed.• 9/19/19 09:45

f
014SD
r+ swtxe lr ano
IRON ICP Dry wt.
S iebate Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
August 2019
Milorganite Daily Composite
QA Flags Ana,lyt-kal Method b''
08/01/19
DM0801/19014196
47000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
08/02/19
DM0802/19014211
42000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
08/03/19
DMO803119014222
46000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
46000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
08/05/19
DM0805/19014324
47000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
08/06/19
DM0806/19014383
43000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
08/07/19
DM0807/19015004
44000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
08/08/19
DM0808/19015023
44000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
08/09/19
DM0809/19015287
47000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
08/10/19
DM0810/19015298
49000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
08/11/19
DM0811/19015317
49000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
08/12/19
DM0812/19015332
47000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
08/13/19
DM0813/19015359
51000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
08/14/19
DM0814/19015387
48000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
08/15/19
08/16/19
DM0815/19015406
DM0816/19015623
47000 mg/kg D.W.
44000 mg/kg D.W.
540
530
1900
1900
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/17/19
DM0817/19015634
43000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
45000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
08/19/19
DMO819119015709
47000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
08/20/19
08/21/19
DM0820/19015736
DM0821/19015769
50000 mg/kg D.W.
47000 mg/kg D.W.
540
540
1900
2000
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/22/19
DMO822/19015788
49000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
08/23/19
DMO823/19015803
51000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
08/24/19
DMO824/19015814
55000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
08/25/19
DMO825/19015833
58000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
08/26/19
08/27/19
DM0826/19015864
DM0827/19015890
61000 mg/kg D.W.
58000 mg/kg D.W.
530
520
1900
1900
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/28/19
DM0828/19015918
63000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
08/29/19
DM0829/19015937
55000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
08/30/19
DMO830/19015952
57000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
08/31/19
DM0831/19015963
55000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
Avg Result: 50000 mg/kg D.W.
Min LOD:
520 mg/kg D.W.
Max Result: 63000 mg/kg D.W.
Page 4 of 16
5Y5/rpt1M#oMonth1yDW 4126119 tj Printed.- 9119119 09:45

iNSD
LEAD ICP Dry wt.
SampCe Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
August 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
08/01/19
DM0801/19014196
34 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
08/02/19
DM0802/19014211
39 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
08/03/19
DM0803/19014222
34 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
34 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
08/05/19
DMO805/19014324
33 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
08/06/19
DM0806119014383
32 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
08/07/19
DMO807/19015004
32 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
08/08/19
DM0808/19015023
31 mg/kg D.W.
2.8
8.6
SW846: 6010C
MMSD
08/09/19
DMO809/19015287
32 mg/kg D.W.
2.8
8.6
SW846: 6010C
MMSD
08/10/19
DM0810/19015298
32 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
08/11/19
DM0811/19015317
31 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
08/12/19
DM0812/19015332
34 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
08/13/19
DM0813/19015359
36 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
08/14/19
DM0814/19015387
37 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
08/15/19
DMO815/19015406
36 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
08/16/19
DM0816/19015623
36 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
08/17/19
DM0817/19015634
35 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
35 mg/kg D.W.
3
9
SW846: 6010C
MMSD
08/19/19
DM0819/19015709
34 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
08/20/19
DM0820/19015736
34 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
08/21/19
DM0821/19015769
34 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
08/22/19
DM0822/19015788
34 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
08/23/19
DMO823/19015803
37 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
08/24/19
DM0824/19015814
34 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
08/25/19
DM0825/19015833
34 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
08/26/19
DMO826/19015864
32 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
08/27/19
DM0827/19015890
32 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
08/28/19
DMO828/19015918
33 mg/kg D.W.
2.8
8.4
SW846: 6010C
MMSD
08/29/19
DM0829/19015937
32 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
08/30/19
DM0830/19015952
32 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
08/31/19
DMO831/19015963
31 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
Avg Result: 34 mg/kg D.W.
Min LOD: 2.8 mg/kg D.W.
Max Result: 39 mg/kg D.W.
Page 5 of 16
5Y5/rotlMilaMonth/yDW 4126119 tJ Printed., 9119119 09:45

Monthly Milorganite Report DW
ltiNSD August 2019
�111�ttA!►ttf��
Milorganite Daily Composite
MOLYBDENUM ICP Dry wt.
Sample Date
08/01/19
I Sample TO
DM0801/19014196
Result
8.7 mg/kg D.W.
LOD
4.6
LOQ
17
i-
3.
SW846: 6010C
r..
MMSD
08/02/19
DM0802/19014211
9 mg/kg D.W.
4.6
18
1.
SW846: 6010C
MMSD
08/03/19
DM0803/19014222
9.6 mg/kg D.W.
4.6
18
3.
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
9.4 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
08/05/19
DM0805/19014324
9.6 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
08/06/19
DM0806/19014383
8.8 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
08/07/19
DMO807/19015004
8.8 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
08/08/19
DM0808/19015023
8.1 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
08/09/19
DM0809/19015287
8.3 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
08/10/19
DMO810/19015298
8.6 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
08/11/19
DM0811/19015317
8.5 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
08/12/19
DM0812/19015332
8.5 mg/kg D.W.
4.6
17
3.
SW846: 6010C
MMSD
08/13/19
OM0813/19015359
9.5 mg/kg D.W.
4.6
18
3.
SW846: 6010C
MMSD
08/14/19
DM0814/19015387
9 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
08/15/19
08/16/19
DM0815/19015406
DM0816/19015623
9.2 mg/kg D.W.
8.9 mg/kg D.W.
4.5
4.4
17
17
3.
3.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/17/19
DM0817/19015634
9.2 mg/kg D.W.
4.6
17
3.
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
9.8 mg/kg D.W.
4.6
18
3.
SW846: 6010C
MMSD
08/19/19
DM0819/19015709
9.7 mg/kg D.W.
4.6
17
3.
SW846: 6010C
MMSD
08/20/19
08/21/19
DM0820/19015736
DM0821/19015769
10 mg/kg D.W.
10 mg/kg D.W.
4.5
4.6
17
17
3.
1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/22/19
DM0822/19015788
9.5 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
08/23/19
DM0823/19015803
10 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
08/24/19
DM0824/19015814
11 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
08/25/19
DM0825/19015833
11 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
08/26/19
DM0826/19015864
12 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
08/27/19
DMO827/19015890
10 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
08/28/19
DM0828/19015918
12 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
08/29/19
DM0829/19015937
10 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
08/30/19
DM0830/19015952
11 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
08/31/19
DM0831/19015963
9.6 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
Avg Result: 9.6 mg/kg D.W.
Min LOD:
4.4 mg/kg D.W.
Max Result: 12 mg/kg D.W.
Page 6 of 16
5Y5/rptlMi1oMonth1yDW 4126119 tj Printed- 9119119 09:45

RA»�S t9! Id
NICKEL ICP Dry wt.
• Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
August 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
,Sam.
08/01/19
DM0801/19014196
27 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
08/02/19
DM0802/19014211
21 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
08/03/19
DM0803/19014222
22 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
22 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
08/05/19
DM0805/19014324
22 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
08/06/19
DM0806/19014383
21 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
08/07/19
DM0807/19015004
21 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
08/08/19
DM0808/19015023
22 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
08/09/19
DM0809/19015287
23 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
08/10/19
DMO810/19015298
22 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
08/11/19
DM0811/19015317
23 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
08/12/19
DM0812/19015332
23 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
08/13/19
DM0813/19015359
24 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
08/14/19
DM0814/19015387
21 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
08/15/19
DM0815/19015406
21 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
08/16/19
DM0816/19015623
22 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
08/17/19
DM0817/19015634
22 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
24 mg/kg D.W.
3.3
9.9
SW846: 6010C
MMSD
08/19/19
DM0819/19015709
22 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
08/20/19
08/21/19
DM0820/19015736
DM0821/19015769
22 mg/kg D.W.
22 mg/kg D.W.
3.2
3.3
9.7
9.8
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/22/19
DM0822/19015788
23 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
08/23/19
DM0823/19015803
22 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
08/24/19
DM0824/19015814
24 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
08/25/19
DM0825/19015833
23 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
08/26/19
DM0826/19015864
23 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
08/27/19
08/28/19
DM0827/19015890
DM0828/19015918
23 mg/kg D.W.
24 mg/kg D.W.
3.2
3.1
9.4
9.4
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/29/19
DM0829/19015937
24 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
08/30/19
DM0830/19015952
22 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
08/31/19
DM0831119015963
24 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
Avg Result: 23 mg/kg D.W.
Min LOD:
3.1 mg/kg D.W.
Max Result: 27 mg/kg D.W.
Page 7of16
5Y51rpt1M11oMonth1yDW 4126119 t/ Printed., 9119119 09:45

�ANSD
PAA4116
PHOSPHORUS ICP Dry wt.
.. .
..
LOQ
Monthly Milorganite Report DW
August 2019
Milorganite Daily Composite
QA Flags Analytical Meth ----Lab
08/01/19
DM0801/19014196
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
08/02/19
DMO802/19014211
24000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
08/03/19
DM0803/19014222
24000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
08/05/19
DM0805/19014324
25000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
08/06/19
DM0806/19014383
24000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
08/07/19
DMO807/19015004
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
08/08/19
DM0808/19015023
24000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
08/09/19
DM0809/19015287
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
08/10/19
DM0810/19015298
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
08/11/19
DM0811/19015317
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
08/12/19
DMO812119015332
24000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
08/13/19
DM0813/19015359
25000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
08/14/19
DMO814/19015387
25000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
08/15/19
08/16/19
DM0815/19015406
DM0816/19015623
25000 mg/kg D.W.
25000 mg/kg D.W.
24
23
90
89
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/17/19
DM0817/19015634
24000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
25000 mg/kg D.W.
24
93
SW846: 6010C
MMSD
08/19/19
DM0819/19015709
25000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
08/20/19
08/21/19
DM0820/19015736
DM0821/19015769
26000 mg/kg D.W.
25000 mg/kg D.W.
24
24
90
92
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/22/19
DMO822/19015788
25000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
08/23/19
DM0823/19015803
26000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
08/24/19
DM0824/19015814
26000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
08/25/19
DM0825/19015833
27000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
08/26/19
DM0826/19015864
27000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
08/27/19
DM0827/19015890
26000 mg/kg D.W. -
23
88
SW846: 6010C
MMSD
08/28/19
DM0828/19015918
27000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
08/29/19
DM0829/19015937
25000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
08/30/19
DM0830/19015952
26000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
08/31/19
DM0831/19015963
24000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
Avg Result: 25000 mg/kg D.W.
Min LOD: 23 mg/kg D.W.
Max Result: 27000 mg/kg D.W.
Page 8 of 16
SYS/rptlMi/oMonth/yDW 4126119 tj Printed.- 9119119 09:45

14SD
#:illm (fit A ttilm
POTASSIUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
August 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
08/01/19
DMO801/19014196
3000 mg/kg D.W.
290
880
B8.
SW846: 6010C
MMSD
08/02/19
DMO802/19014211
3500 mg/kg D.W.
300
890
SW846: 6010C
MMSD
08/03/19
DM0803/19014222
3500 mg/kg D.W.
300
890
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
3500 mg/kg D.W.
290
870
SW846: 6010C
MMSD
08/05/19
DM0805/19014324
3600 mg/kg D.W.
290
870
SW846: 6010C
MMSD
08/06/19
DM0806/19014383
3600 mg/kg D.W.
290
860
B8.
SW846: 6010C
MMSD
08/07/19
DMO807/19015004
3700 mg/kg D.W.
290
870
B8.
SW846: 6010C
MMSD
08/08/19
DM0808/19015023
3400 mg/kg D.W.
280
860
B8.
SW846: 6010C
MMSD
08/09/19
DMO809/19015287
3000 mg/kg D.W.
280
860
B8.
SW846: 6010C
MMSD
08/10/19
DM0810/19015298
2900 mg/kg D.W.
290
860
B8.
SW846: 6010C
MMSD
08/11/19
DMO811/19015317
3000 mg/kg D.W.
290
870
B8.
SW846: 6010C
MMSD
08/12/19
DM0812/19015332
3200 mg/kg D.W.
290
880
B8.
SW846: 6010C
MMSD
08/13/19
DM0813/19015359
3000 mg/kg D.W.
300
890
B8.
SW846: 6010C
MMSD
08/14/19
DM0814/19015387
3200 mg/kg D.W.
290
870
SW846: 6010C
MMSD
08/15/19
DM0815/19015406
3400 mg/kg D.W.
290
870
SW846: 6010C
MMSD
08/16/19
DM0816/19015623
3300 mg/kg D.W.
290
860
B8.
SW846: 6010C
MMSD
08/17/19
DM0817119015634
3500 mg/kg D.W.
290
880
B8.
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
3400 mg/kg D.W.
300
900
B8.
SW846: 6010C
MMSD
08/19/19
DM0819/19015709
3300 mg/kg D.W.
290
880
B8.
SW846: 6010C
MMSD
08/20/19
DMO820/19015736
3200 mg/kg D.W.
290
870
SW846: 6010C
MMSD
08/21/19
DM0821/19015769
3000 mg/kg D.W.
290
880
SW846: 6010C
MMSD
08/22/19
DM0822/19015788
3200 mg/kg D.W.
290
860
SW846: 6010C
MMSD
08/23/19
DM0823/19015803
3200 mg/kg D.W.
280
850
SW846: 6010C
MMSD
08/24/19
DM0824/19015814
3500 mg/kg D.W.
290
870
SW846: 6010C
MMSD
08/25/19
DM0825/19015833
3300 mg/kg D.W.
290
870
SW846: 6010C
MMSD
08/26/19
DM0826/19015864
2800 mg/kg D.W.
290
860
SW846: 6010C
MMSD
08/27/19
DM0827/19015890
2700 mg/kg D.W.
280
850
SW846: 6010C
MMSD
08/28/19
DMO828/19015918
2800 mg/kg D.W.
280
840
SW846: 6010C
MMSD
08/29/19
DM0829/19015937
2600 mg/kg D.W.
280
850
B8.
SW846: 6010C
MMSD
08/30/19
DMO830/19015952
2900 mg/kg D.W.
280
850
B8.
SW846: 6010C
MMSD
08/31/19
DMO831/19015963
2800 mg/kg D.W.
290
860
B8.
SW846: 6010C
MMSD
Avg Result: 3200 mg/kg D.W.
Min LOD:
280 mg/kg D.W.
Max Result: 3700 mg/kg D.W.
Page 9 of 16
5Y51rpt1M1/0M0nth/yDW 4126119 tj Printed.- 9119119 09.45

"?'ONSD
SELENIUM ICP Dry wt.
'§ample^ Date Safn�le ID
Result
LOD
LOQ
Monthly Milorganite Report DW
August 2019
Milorganite Daily Composite
QA Flags Analytical Meth6a La'6'
08/01/19
DM0801/19014196
7.3 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
08/02/19
DM0802/19014211
< 4.3 mg/kg D.W.
4.3
13
SW846: 6010C
MMSD
08/03/19
DM0803/19014222
< 4.3 mg/kg D.W.
4.3
13
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
08/05/19
DM0805/19014324
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
08/06/19
DM0806/19014383
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
08/07/19
DM0807/19015004
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
08/08/19
DM0808/19015023
5.4 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
08/09/19
DMO809/19015287
6.4 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
08/10/19
DM0810/19015298
4.5 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
08/11/19
DM0811/19015317
4.6 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
08/12/19
DM0812/19015332
4.8 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
08/13/19
DM0813/19015359
6.5 mg/kg D.W.
4.3
13
J.
SW846: 6010C
MMSD
08/14/19
DM0814/19015387
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
08/15/19
08/16/19
DM0815/19015406
DM0816/19015623
< 4.2 mg/kg D.W.
< 4.1 mg/kg D.W.
4.2
4.1
13
13
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/17/19
DM0817/19015634
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
< 4.3 mg/kg D.W.
4.3
13
SW846: 6010C
MMSD
08/19/19
DM0819/19015709
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
08/20/19
08/21/19
DM0820/19015736
DM0821/19015769
< 4.2 mg/kg D.W.
< 4.2 mg/kg D.W.
4.2
4.2
13
13
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/22/19
08/23/19
08/24/19
DM0822/19015788
DM0823/19015803
DM0824/19015814
< 4.1 mg/kg D.W.
< 4.1 mg/kg D.W.
< 4.2 mg/kg D.W.
4.1
4.1
4.2
13
13
13
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
08/25/19
DM0825/19015833
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
08/26/19
DM0826/19015864
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
08/27/19
DM0827/19015890
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
08/28/19
DM0828/19015918
< 4.1 mg/kg D.W.
4.1
12
SW846: 6010C
MMSD
OB/29/19
DM0829/19015937
< 4.1 mg/kg D.W.
4.1
12
SW846: 6010C
MMSD
08/30/19
DM0830/19015952
< 4.1 mg/kg D.W.
4.1
12
SW846: 6010C
MMSD
08/31/19
DM0831/19015963
4.5 mg/kg D.W.
4.1
13 J.
SW846: 6010C
MMSD
Avg Result: 1.4 mg/kg D.W.
Min LOD:
4.1 mg/kg D.W.
Max Result: 7.3 mg/kg D.W.
Page 10 of 16
SY51rpt1Mi1bMonth/yDW 4126119 tj Minted.- 9119119 09:45

Monthly Milorganite Report DW
fNI4SD August 2019
Nmlti� �t A UE��It
Solids (% Moisture)
Sample Date Sample ID
Result
LOD LOQ QA Flags
Milorganite Daily Composite
Analytical Method Lab
08/01/19
DMO801/19014196
8 %
0.1
SM 2540 G (1997)
MMSD
08/02/19
DM0802/19014211
8.6 %
0.1
SM 2540 G (1997)
MMSD
08/03/19
DM0803/19014222
8.6 %
0.1
SM 2540 G (1997)
MMSD
08/04/19
DMO804/19014283
6.6 %
0.1
SM 2540 G (1997)
MMSD
08/05/19
DM0805/19014324
6.8 %
0.1
SM 2540 G (1997)
MMSD
08/06/19
DMO806/19014383
6.1 %
0.1
SM 2540 G (1997)
MMSD
08/07/19
DMO807/19015004
6.7 %
0.1
SM 2540 G (1997)
MMSD
08/08/19
DM0808/19015023
5.3 %
0.1
SM 2540 G (1997)
MMSD
08/09/19
DM0809/19015287
5.6 %
0.1
SM 2540 G (1997)
MMSD
08/10/19
DM0810/19015298
5.7 %
0.1
SM 2540 G (1997)
MMSD
08/11/19
DM0811/19015317
6.5 %
0.1
SM 2540 G (1997)
MMSD
08/12/19
DM0812/19015332
8.4 %
0.1
SM 2540 G (1997)
MMSD
08/13/19
DM0813/19015359
8.7 %
0.1
SM 2540 G (1997)
MMSD
08/14/19
DM0814/19015387
6.8 %
0.1
SM 2540 G (1997)
MMSD
08/15/19
DM0815/19015406
6.9 %
0.1
SM 2540 G (1997)
MMSD
08/16/19
DM0816/19015623
5.7 %
0.1
SM 2540 G (1997)
MMSD
08/17/19
DM0817/19015634
8.3 %
0.1
SM 2540 G (1997)
MMSD
08/18/19
DM0818/19015653
9.5 %
0.1
SM 2540 G (1997)
MMSD
08/19/19
DMO819/19015709
7.9 %
0.1
SM 2540 G (1997)
MMSD
08/20/19
08/21/19
DM0820/19015736
DM0821/19015769
7.2 %
8.2 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
08/22/19
DMO822/19015788
5.9 %
0.1
SM 2540 G (1997)
MMSD
08/23/19
DM0823/19015803
5 %
0.1
SM 2540 G (1997)
MMSD
08/24/19
DM0824/19015814
7.1 %
0.1
SM 2540 G (1997)
MMSD
08/25/19
DM0825/19015833
6.9 %
0.1
SM 2540 G (1997)
MMSD
08/26/19
DMO826/19015864
5.8 %
0.1
SM 2540 G (1997)
MMSD
08/27/19
DM0827/19015890
4.8 %
0.1
SM 2540 G (1997)
MMSD
08/28/19
DM0828/19015918
4 %
0.1
SM 2540 G (1997)
MMSD
08/29/19
DM0829/19015937
4.4 %
0.1
SM 2540 G (1997)
MMSD
08/30/19
DMO830/19015952
4.6 %
0.1
SM 2540 G (1997)
MMSD
08/31/19
DM0831/19015963
5.8 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 6.6 %
Min LOD: 0.1 %
Max Result: 9.5 %
Page 11 of 16
SY51rptlMi1oMonth/y0W 4126119 tf Printed: 9119119 09:45

"t
iNSD
WM W A CI
ZINC ICP Dry wt.
§aW.. •. LOQ
58/01/19 DM0801/19014196 420 mg/kg D.W. 18 55
08/02/19 DMO802/19014211 420 mg/kg D.W. 19 56
Monthly Milorganite Report DW
August 2019
Milorganite Daily Composite
lags Analytical b
SW846: 6010C MMSD
SW846: 6010C MMSD
08/03/19
DM0803/19014222
420 mg/kg D.W.
19
56
SW846: 6010C
MMSD
08/04/19
DM0804/19014283
420 mg/kg D.W.
18
55
SW846: 6010C
MMSD
08/05/19
DM0805/19014324
420 mg/kg D.W.
18
55
SW846: 6010C
MMSD
08/06/19
DM0806/19014383
400 mg/kg D.W.
18
54
SW846: 6010C
MMSD
08/07/19
DM0807/19015004
400 mg/kg D.W.
18
55
SW846: 6010C
MMSD
08/08/19
DM0808/19015023
400 mg/kg D.W.
18
54
SW846: 6010C
MMSD
08/09/19
DM0809/19015287
420 mg/kg D.W.
18
54
SW846: 6010C
MMSD
08/10/19
DM0810/19015298
420 mg/kg D.W.
18
54
SW846: 6010C
MMSD
08/11/19
DMO811/19015317
420 mg/kg D.W.
18
54
SW846: 6010C
MMSD
08/12/19
DM0812/19015332
420 mg/kg D.W.
18
56
SW846: 6010C
MMSD
08/13/19
DM0813/19015359
460 mg/kg D.W.
19
56
SW846: 6010C
MMSD
08/14/19
DM0814/19015387
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
08/15/19
08/16/19
DMO815/19015406
DM0816/19015623
450 mg/kg D.W.
450 mg/kg D.W.
18
18
55
54
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/17/19
DM0817/19015634
450 mg/kg D.W.
18
56
SW846: 6010C
MMSD
08/18/19
DM0818/19015653
450 mg/kg D.W.
19
56
SW846: 6010C
MMSD
08/19/19
DM0819/19015709
460 mg/kg D.W.
18
55
SW846: 6010C
MMSD
08/20/19
08/21/19
DMO820/19015736
DM0821/19015769
470 mg/kg D.W.
460 mg/kg D.W.
18
18
55
56
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/22/19
DMO822/19015788
460 mg/kg D.W.
18
54
SW846: 6010C
MMSD
08/23/19
DM0823/19015803
470 mg/kg D.W.
18
54
SW846: 6010C
MMSD
08/24/19
DM0824/19015814
460 mg/kg D.W.
18
55
SW846: 6010C
MMSD
08/25/19
DM0825/19015833
460 mg/kg D.W.
18
55
SW846: 6010C
MMSD
08/26/19
DM0826/19015864
460 mg/kg D.W.
18
54
SW846: 6010C
MMSD
08/27/19
DM0827/19015890
440 mg/kg D.W.
18
54
SW846: 6010C
MMSD
08/28/19
DM0828/19015918
460 mg/kg D.W.
18
53
SW846: 6010C
MMSD
08/29/19
DMO829/19015937
440 mg/kg D.W.
18
53
SW846: 6010C
MMSD
08/30/19
DM0830/19015952
440 mg/kg D.W.
18
53
SW846: 6010C
MMSD
08/31/19
DM0831/19015963
420 mg/kg D.W.
18
54
SW846: 6010C
MMSD
Avg Result: 440 mg/kg D.W.
Min LOD: 18 mg/kg D.W.
Max Result: 470 mg/kg D.W.
Page 12 of 16
5Y51rpt1 MiloMonthly0W 4126119 tj Printed: 9119119 09:45

M14SDAugust
�1pf1�Ci � 1 CtE+.�ER EYPSI'G#�tEN°
Phosphorus - Total % DW (Calc.)
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
08/01/19 DMO801/19014196
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/02/19 DM0802/19014211
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/03/19 DMO803119014222
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/04/19 DM0804/19014283
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/05/19 DM0805/19014324
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/06/19 DM0806/19014383
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/07/19 DM0807/19015004
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/08/19 DMO808/19015023
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/09/19 DM0809/19015287
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/10/19 DM0810/19015298
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/11/19 DM0811/19015317
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/12/19 DMOB12/19015332
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/13/19 DM0813/19015359
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/14/19 DM0814/19015387
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/15/19 DM0815/19015406
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/16/19 DM0816119015623
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/17/19 DM0817/19015634
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/18/19 DM0818/19015653
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/19/19 DM0819/19015709
2.5 %D.W.
0.1
0.1
SW846: 6010C
MMSD
08/20/19 DM0820/19015736
08/21/19 DM0821119015769
2.6 % D.W.
2.5 %D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
08/22/19 DM0822/19015788
2.5 %D.W.
0.1
0.1
SW846: 6010C
MMSD
08/23/19 DM0823/19015803
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/24/19 DM0824/19015814
2.6%D.W.
0.1
0.1
SW846: 6010C
MMSD
08/25/19 DM0825/19015833
2.7 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/26/19 DM0826/19015864
2.7 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/27/19 DM0827/19015890
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/28/19 DM0828/19015918
2.7 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/29/19 DM0829/19015937
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/30/19 DM0830/19015952
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/31/19 DM0831/19015963
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
Avg Result: 2.5 % D.W.
ALUMINUM ICP Dry wt.
Sample Date Sample ID
Min LOD: 0.1 % D.W.
Result LOD
LOQ
Max Result: 2.7 °/u D.W.
Milorganite Weekly Composite
QA Flags Analytical Method
08/10/19 WMC32/19015334
5300 mg/kg D.W.
57
200
B8. SW846: 6010C
MMSD
Avg Result: 5300 mg/kg D.W.
(Milo) Ammonia in Fertilizer
•.
Min LOD: 57 mg/kg D.W.
.• LOQ
-
•Analytical Method
Lab
08/10/19 WMC32/19015334
0.13 %
0.11
0.37
AOAC (13) 2.065
MMSD
Avg Result: 0.13 %
SY51rotlMiloMonlhlyoW 41261191j
Min LOD:
0.11
Page 13 of 16
Printed: 9119119 09:45

Monthly Milorganite Report DW
August 2019
nlr�da �t� uwet �l�°
Milorganite Weekly Composite
BORON ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
QA Flags
Analytical Method
Lab
08/10/19 WMC32/19015334
12 mg/kg D.W.
1.1
3.4
SW846: 6010C
Cr Lab
Avg Result: 12 mg/kg D.W.
Min LOD:
1.1 mg/kg
D.W.
CHROMIUM ICP Dry wt.
Sample Date 5
Result
LOD
LOQ
QA Flags
Analytical Method
Lab
08/10/19 WMC32/19015334
320 mg/kg D.W.
1.6
4.8
B8.
SW846: 6010C
MMSD
Avg Result: 320 mg/kg D.W.
Min LOD:
1.6 mg/kg
D.W.
COBALT ICP Dry wt.
-D.te Sample ID
Result
LOD
LOQ
.• Flags
Analytical Method
Lab
08/10/19 WMC32/19015334
2.2 mg/kg D.W.
0.28
1.1
B8, Q3.
SW846: 6010C
MMSD
Avg Result: 2.2 mg/kg D.W.
Min LOD:
0.28 mg/kg
D.W.
MERCURY by M. 7471 (sludge)
Sample Date Sample ID
Result
LOD
LOQ
QA Flags
Analytical Method
Lab
08/03/19 WMC31/19014326
0.099 mg/kg D.W.
0.015
0.05
AX.
EPA 7471E
CT Lab
08/10/19 WMC32/19015334
0.16 mg/kg D.W.
0.014
0.047
EPA 7471B
CT Lab
08/17/19 WMC33/19015711
0.039 mg/kg D.W.
0.015
0.05
J
EPA 7471E
CT Lab
08/24/19 WMC34/19015968
< 0.015 mg/kg D.W.
0.015
0.05
AX.
EPA 7471E
CT Lab
08/31/19 WMC35/19017175
0.31 mg/kg D.W.
0.013
0.045
EPA 7471E
CT Lab
Avg Result: 0.12 mg/kg D.W.
Min LOD: 0.013 mg/kg D.W.
Max Result: 0.31 mg/kg D.W.
NITRATE NITROGEN
Sample Date Sample 10
08/10/19 WMC32/19015334
Result LOD LOQ QA Flags
1.3 % 0.5
Analytical Method
AOAC (16) 930.01
Lab
MMSD
Avg Result: 1.3 %
Min LOD: 0.5
NITROGEN-Total(Manual)
Sample Date Sample ID
LOD LOQ QA Flags
Analytical Method
Lab
08/10/19 WMC32/19015334
6.1 % 0.11
AOAC (16) 955.04
MMSD
Avg Result: 6.1 %
Min LOD: 0.11 0/6
NITROGEN -Water Insoluble
Sample Date Sample ID
Result LOD LOQ •• Flags
Analytical Method
Lab
08/10/19 WMC32/19015334
4.5 % 0.5
AOAC (16) 945.01
MMSD
Avg Result: 4.5 %
Min LOD: 0.5
pH -Solids
Sample Date Sample ID
Result LOD LOQ .. Flags
Analytical Method
Lab
08/03/19 WMC31/19014326
6.27 Stnd. Units 0.1
SW846: 9045D
MMSD
08/10/19 WMC32/19015334
6.21 Stnd. Units 0.1
SW846: 9045D
MMSD
08/17/19 WMC33/19015711
6.31 Stnd. Units 0.1
SW846: 9045D
MMSD
08/24/19 WMC34/19015968
6.4 Stnd. Units 0.1
SW846: 9045D
MMSD
08/31/19 WMC35/19017175
6.36 Stnd. Units 0.1
SW846: 9045D
MMSD
Avg Result: 6.3 Stnd. Units
Min LOD: 0.1 Stnd. Units
Max Result: 6.4 Stnd. Units
Page 14 of 16
5Y5/rpt1Mi/oMonth1yDW 4126119 tj Printed: 9119119 09:45

j
Monthly Milorganite Report DW
August 2019
!i!R"0 A time III;
Milorganite Weekly
Composite
Solids (% Moisture)
Sample Date Sample ID
Result
LOD LOQ
QA Flags Analytical Method
Lab
08/03/19 WMC31/19014326
8.2 %
0.1
SM 2540 G (1997)
MMSD
08/10/19 WMC32/19015334
6.2 %
0.1
SM 2540 G (1997)
MMSD
08/17/19 WMC33/19015711
7.3 %
0.1
SM 2540 G (1997)
MMSD
08/24/19 WMC34/19015968
7.6 %
0.1
SM 2540 G (1997)
MMSD
08/31/19 WMC35/19017175
5.6 %
0.1
SM 2540 G (1997)
MMSD
Min LOD:
0.1 a/o
Solids (% Volatile)
:Sample Date Sample ID
Result
LOD LOQ
QA Flags Analytical Method
Lab
08/10/19 WMC32/19015334
70 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 70 %
Min LOD:
0.1 "/o
Solids (% Total)
Sample Date Sample ID
Result
LOD LOQ
QA Flags Analytical Method
Lab
08/10/19 WMC32/19015334
94 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 94 %
Min LOD:
0.1 %
Milorganite (Outfall 006) PRODUCTION
FECAL COLIFORM SLUDGE
"ate Sample ID
Result
LOD LOQ
QA Flags Analytical Method
- - - Lab _7f
08/06/19 19017031
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
08/13/19 19017740
< 0.2 MPN/g TS
0.2
EPA 1680
MMSD
08/20/19 19018375
0.48 MPN/g TS
0.19
Q2. EPA 1680
MMSD
08/27/19 19018959
< 0.19 MPN/g TS
0.19
EPA 1680
MMSD
Min LOD:
0.19 MPN/g TS
Solids (% Total)
Sample Date Sample ID
Result
LOD LOQ
QA Flags Analytical Method
Lab
08/06/19 19017031
93 %
0.1
SM 2540 G (1997)
MMSD
08/13/19 19017740
92 %
0.1
SM 2540 G (1997)
MMSD
08/20/19 19018375
93 %
0.1
SM 2540 G (1997)
MMSD
08/27/19 19018959
96 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 94 %
Min LOD:
0.1 %
Max Result: 96 %
Milorganite (Outfall 009) BAGGING
FECAL COLIFORM SLUDGE
Sample Date Sample ID Result •. LOQ •• Flags Analytical Method Lab
08/13/19 19017742 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
Page 15 of 16
5Y5/rpt1M11dMonth/yDW 4126119 tj Printed: 9119119 09:45

Monthly Milorganite Report DW
� fkNSD August 2019
PgtI�Sl9tA t1;;JU�
Milorganite (Outfall 009) BAGGING
Solids (% Total)
Simple Date Sample ID Result LOD
08/13/19 19017742 93 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 93 % Min LOD: 0.1 %
Milorganite (Outfall 008) SHIPPING
FECAL COLIFORM SLUDGE
• • . ��� , .Lab
08/13/19 19017741 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
Solids (0/6 Total)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
0: •.
Avg Result: 94 %
AO Other -- Flag requires additional explanation
AX Qualified data - see contract laboratory report
Min LOD: 0.1 %
B3 Target analyte detected in method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits.
B8 LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
D3 Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
H3 Sample was received past holding time.
R3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
SY5/rpt1Nj1bMont17/yDW 4126119 h'
IS Insufficient sample volume for analysis.
Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
LA Not analyzed - laboratory accident.
M3 Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
MS Incubator/water bath temperature was outside method
M7 Microbiology sample received without adequate headspace. _
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
SS Reading was not confirmed by a constant weight measurement
SD Supplemental details_ provided.(Water Quality only.) _
T3 The BOD dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The BOD dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample is outside of the prescribed method temperature range.
Page 16 of 16
Printed: 91191.19 09:45

-CA&
�2NNSD
PARTNERS FOR A CLEANER ENVIRONMENT
October 18, 2019
Memorandum
TO: Brett Kelly, Todd Schwingle, Dion Doege, Jacob Holbert, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom Nowicki, Beth
Stroik, Kori Kenney, Ethan Guyant, Lab File
SUBJECT: Milorganite Monthly Data — September 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of September
2019. The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin
(Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
Richard Vincent Date
Laboratory Team Supervisor
Data/Report Review By:
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

NSD
POW WA M10
ARSENIC ICP Dry wt.
Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
September 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
09/01/19
DM0901/19017160
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
09/02/19
09/03/19
DM0902/19017173
DM0903/19017200
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
69
68
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/04/19
DM0904/19017215
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
09/05/19
DM0905/19017249
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
09/06/19
DM0906/19017389
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
09/07/19
DMO907/19017400
< 17 mg/kg D,W.
17
67
SW846: 6010C
MMSD
09/08/19
DMO908/19017792
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
09/09/19
DM0909/19017805
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
09/10/19
DM0910/19017832
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
09/11/19
DM0911/19017852
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
09/12/19
DM0912/19017873
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
09/13/19
09/14/19
DM0913/19017963
DM0914/19018457
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
67
67
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/15/19
09/16/19
DM0915/19018476
DM0916/19018489
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
67
66
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/17/19
09/18/19
09/19/19
DM0917/19018516
DM0918/19018540
DM0919/19018616
< 17 mg/kg D.W.
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
17
67
67
67
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
09/20/19
DM0920/19018631
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
09/21/19
DM0921/19019179
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
09/22/19
DM0922/19019198
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
09/23/19
DM0923/19019211
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
09/24/19
DM0924/19019343
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
09/25/19
DM0925/19019365
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
09/26/19
DM0926/19019401
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
09/27/19
09/28/19
DMO927/19019518
DM0928/19019529
< 16 mg/kg D.W.
< 17 mg/kg D.W.
16
17
66
67
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/29/19
DM0929/19019549
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
09/30/19
DM0930/19019563
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
16 mg/kg D.W.
Gage 1 of 16
5Y5/rpt1M11bMonth/yDW 4126119 tj printed: 1011811912 3i

'I
fiNSD
9914MINAWWWONUff
CADMIUM ICP Dry wt.
ample Date Sample ID
Result
LOD
LOQ QA
Monthly Milorganite Report DW
September 2019
Milorganite Daily Composite
Flags Analytical Method Lab
09/01/19
DM0901/19017160
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
09/02/19
DM0902/19017173
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
09/03/19
DM0903/19017200
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
09/04/19
DM0904/19017215
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
09/05/19
DM0905/19017249
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
09/06/19
DM0906/19017389
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
09/07/19
DM0907/19017400
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
09/08/19
DM0908/19017792
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
09/09/19
DM0909/19017805
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
09/10/19
DM0910/19017832
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
09/11/19
DM0911/19017852
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
09/12/19
DM0912/19017873
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
09/13/19
DM0913/19017963
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
09/14/19
DM0914/19018457
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
09/15/19
09/16/19
DM0915/19018476
DM0916/19018489
< 0.9 mg/kg D.W.
2.2 mg/kg D.W.
0.9
0.9
3.4
3.4
SW846: 6010C
3. SW846: 6010C
MMSD
MMSD
09/17/19
DM0917/19018516
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
09/18/19
DM0918/19018540
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
09/19/19
DM0919/19018616
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
09/20/19
DMO920/19018631
< 0.91 mg/kg D.W.
0.91
3.5
SW846: 6010C
MMSD
09/21/19
DM0921/19019179
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
09/22/19
DM0922/19019198
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
09/23/19
DMO923/19019211
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
09/24/19
DMO924/19019343
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
09/25/19
DMO925/19019365
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
09/26/19
DMO926/19019401
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
09/27/19
DM0927/19019518
< 0.89 mg/kg D.W.
0.89
3.4
SW846: 6010C
MMSD
09/28/19
DMO928/19019529
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
09/29/19
DM0929/19019549
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
09/30/19
DM0930/19019563
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
Avg Result: 0.073 mg/kg D.W.
Min LOD:
0.89 mg/kg
D.W.
Max Result: 2.2 mg/kg D.W.
Page 1 of 16
5Y5/rpt1MAoMonth/yDW 4126119 tj Printed: 10118119 1237

t
Monthly Milorganite Report DW
14SD
September 2019
PWO150Acam
Milorganite Daily Composite
COPPER ICP Dry wt.
Date Sample ID
Result LOD LOQ ifkffigs Lab
09/01/19 DMO901/19017160
230 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
09/02/19 DM0902119017173
220 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
09/03/19 DMO903/19017200
230 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
09/04/19
DM0904/19017215
220 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
09/05/19
DM0905/19017249
220 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
09/06/19
DM0906/19017389
220 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
09/07/19
DM0907/19017400
240 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
09/08/19
DMO908/19017792
240 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
09/09/19
DM0909/19017805
240 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
09/10/19
DM0910/19017832
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
09/11/19
DM0911/19017852
230 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
09/12/19
DM0912/19017873
250 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
09/13/19
DM0913119017963
250 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
09/14/19
DM0914/19018457
230 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
09/15/19
09/16/19
DM0915/19018476
DM0916/19018489
230 mg/kg D.W.
240 mg/kg D.W.
6.6
6.6
25
25
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/17/19
09/18/19
09/19/19
09/20/19
09/21/19
DM0917/19018516
DM0918/19018540
DM0919/19018616
DM0920/19018631
DM0921/19019179
260 mg/kg D.W.
260 mg/kg O.W.
260 mg/kg D.W.
250 mg/kg D.W.
240 mg/kg D.W.
6.6
6.6
6.6
6.6
6.6
25
25
25
25
25
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
MMSD
09/22/19
DM0922119019198
240 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
09/23/19
DM0923/19019211
250 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
09/24/19
DM0924/19019343
250 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
09/25/19
DM0925/19019365
250 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
09/26/19
DM0926/19019401
230 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
09/27/19
DM0927/19019518
230 mg/kg D.W.
6.5
25
SW846: 6010C
MMSD
09/28/19
DMO928/19019529
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
09/29/19
DM0929/19019549
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
09/30/19
DMO930/19019563
210 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
Avg Result: 240 mg/kg D.W.
Min LOD:
6.5 mg/kg D.W.
Max Result: 260 mg/kg D.W.
Page 3 of 16
SY5/rptI iloMonthlyDW 4126119 tj Printed: 1011811912.3i

iNSD
►A111�S Rt� ri
IRON ICP Dry wt.
Sample Date .
Result
LOD
LOQ
Monthly Milorganite Report DW
September 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
09/01/19
DMO901/19017160
55000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
09/02/19
DM0902/19017173
53000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
09/03/19
DM0903/19017200
52000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
09/04/19
DMO904/19017215
53000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
09/05/19
DM0905/19017249
51000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
09/06/19
DMO906/19017389
51000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
09/07/19
DM0907/19017400
50000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
09/08/19
DM0908/19017792
50000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
09/09/19
DM0909/19017805
49000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
09/10/19
DM0910/19017832
50000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
09/11/19
DMO911/19017852
47000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
09/12/19
DMO912/19017873
50000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
09/13/19
DM0913/19017963
49000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
09/14/19
DM0914/19018457
47000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
09/15/19
DMO915/19018476
45000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
09/16/19
DM0916/19018489
47000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
09/17/19
DMO917/19018516
48000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
09/18/19
DMO918/19018540
49000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
09/19/19
DMO919/19018616
49000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
09/20/19
09/21/19
DMO920/19018631
DMO921119019179
46000 mg/kg D.W.
45000 mg/kg D.W.
520
530
1900
1900
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/22/19
DM0922/19019198
46000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
09/23/19
DM0923/19019211
47000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
09/24/19
DM0924/19019343
52000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
09/25/19
DMO925/19019365
48000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
09/26/19
DMO926/19019401
48000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
09/27/19
DMO927/19019518
49000 mg/kg D.W.
510
1800
SW846: 6010C
MMSD
09/28/19
DM0928/19019529
49000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
09/29/19
DMO929/19019549
50000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
09/30/19 DM0930119019563 50000 mg/kg D.W. 530 1900
Avg Result: 49000 mg/kg D.W. Min LOD: 510 mg/kg D.W
SW846: 6010C MMSD
Max Result: 55000 mg/kg D.W.
Page 4 of 16
5Y5/rptlMi1oMonth1y0W 4126119 tj printed: 10118119 1237

14SD
W"WACUMBUNK
LEAD ICP Dry wt.
..SamplelD
Result
LOD
LOQ
Monthly Milorganite Report DW
September 2019
Milorganite Daily Composite
09/01/19 DMO901/19017160
32 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
09/02/19 DM0902/19017173
32 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
09/03/19 DM0903/19017200
34 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
09/04/19 DM0904/19017215
31 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
09/05/19 DM0905/19017249
30 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
09/06/19 DM0906/19017389
33 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
09/07/19 DM0907/19017400
37 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
09/08/19 DM0908/19017792
35 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
09/09/19 DM0909/19017805
34 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
09/10/19 DM0910/19017832
37 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
09/11/19 DM0911/19017852
35 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
09/12/19 DM0912/19017873
36 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
09/13/19 DM0913/19017963
38 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
09/14/19 DM0914/19018457
40 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
09/15/19 DM0915/19018476
09/16/19 DM0916/19018489
49 mg/kg D.W.
52 mg/kg D.W.
2.8
2.8
8.4
8.4
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/17/19 DM0917/19018516
57 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
09/18/19 DM0918/19018540
52 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
09/19/19
DM0919/19018616
49 mg/kg D.W.
2.8
8.5
09/20/19
DM0920/19018631
52 mg/kg D.W.
2.8
8.5
09/21/19
DM0921/19019179
47 mg/kg D.W.
2.8
8.5
09/22/19
DM0922/19019198
46 mg/kg D.W.
2.9
8.6
09/23/19
DM0923/19019211
46 mg/kg D.W.
2.9
8.7
09/24/19
DMO924/19019343
09/25/19
DM0925/19019365
09/26/19
DM0926/19019401
09/27/19
DMO927/19019518
09/28/19
DMO928/19019529
09/29/19
DMO929/19019549
09/30/19
DMO930/19019563
48 mg/kg D.W.
2.9
8.7
46 mg/kg D.W.
2.8
8.6
48 mg/kg D.W.
2.8
8.5
48 mg/kg D.W.
2.8
8.3
42 mg/kg D.W.
2.8
8.5
41 mg/kg D.W.
40 mg/kg D.W.
2.8
2.9
8.6
- 8.6
SW846: 6010C
MMSD
SW846: 6010C
-- --------
SW846:6010C
MMSD
MMSD
SW846: 6010C
MMSD
SW846: 6010C
MMSD
SW846: 6010C
MMSD
SW846: 6010C
MMSD
SW846: 6010C
MMSD
SW846: 6010C
MMSD
SW846: 6010C
MMSD
SW846: 6010C
MMSD
SW846: 6010C
MMSD
Avg Result: 42 mg/kg D.W. Min LOD: 2.8 mg/kg D.W. . Max Result: 57 mg/kg D.W.
5Y51rptlMi/oMonth1yDW 4126119 tj
Page 5 of 16
Printed.• 10116W1911:3i

-p
AND
II'?1"£I6 ! A CC#1f#R 11P71fC/1K1M'
MOLYBDENUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
September 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
09/01/19
DMO901/19017160
9.4 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
09/02/19
DMO902/19017173
9.4 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
09/03/19
DM0903/19017200
9.3 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/04/19
DMO904/19017215
9.4 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/05/19
DMO905/19017249
9 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/06/19
DM0906/19017389
9.4 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
09/07/19
DM0907119017400
10 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/08/19
DM0908/19017792
9.7 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
09/09/19
DM0909119017805
9.8 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
09/10/19
DM0910/19017832
10 mg/kg D.W.
4.6
17
1.
SW846: 6010C
MMSD
09/11/19
DM0911/19017852
9.8 mg/kg D.W.
4.6
17
1
SW846: 6010C
MMSD
09/12/19
DMO912/19017873
10 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
09/13/19
DMO913/19017963
10 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/14/19
DM0914/19018457
9.5 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/15/19
DMO915/19018476
9.5 mg/kg D.W.
4.4
17
1
SW846: 6010C
MMSD
09/16/19
DM0916119018489
9.9 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/17/19
DM0917/19018516
it mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/18/19
DM0918/19018540
11 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/19/19
DM0919/19018616
11 mg/kg D.W.
4.4
17
1
SW846: 6010C
MMSD
09/20/19
DM0920/19018631
30 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/21/19
DM0921/19019179
9.9 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/22/19
DMO922/19019198
10 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
09/23/19
DM0923119019211
10 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
09/24/19
DM0924/19019343
11 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
09/25/19
DM0925/19019365
10 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/26/19
DMO926/19019401
9.5 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/27/19
DMO927/19019518
10 mg/kg D.W.
4.3
16
3.
SW846: 6010C
MMSD
09/28/19
DMO928/19019529
8.6 mg/kg D.W.
4.4
17
1.
SW846: 6010C
MMSD
09/29/19
DM0929/19019549
8.3 mg/kg D.W.
4.4
17
3.
SW846: 6010C
MMSD
09/30/19
DM0930/19019563
8.4 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
Avg Result: 9.8 mg/kg D.W.
Min LOD: 4.3 mg/kg D.W.
Max Result: 11 mg/kg D.W.
Page 6 of 16
SYS/rptlMi/oMonth/yDW 4126119 tj Printed: 1011811911:37

'j A
NSDSeptember
WWWAMAORNAW
NICKEL ICP Dry wt.
- Date sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
2019
Milorganite Daily Composite
QA Flags Anaiytkal Method Lab
09/01/19
DM0901/19017160
23 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
09/02/19
DM0902/19017173
23 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
09/03/19
DM0903/19017200
23 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
09/04/19
DM0904/19017215
24 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
09/05/19
DM0905/19017249
23 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
09/06/19
DM0906/19017389
22 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
09/07/19
DM0907/19017400
24 mg/kg D.W.
3.2
9.4
SW846: 6010C
MMSD
09/08/19
DM0908/19017792
24 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
09/09/19
DM0909/19017805
24 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
09/10/19
DM0910/19017832
24 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
09/11/19
DM0911/19017852
24 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
09/12/19
DM0912/19017873
26 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
09/13/19
DM0913119017963
21 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
09/14/19
09/15/19
09/16/19
DM0914/19018457
DM0915/19018476
DM0916/19018489
20 mg/kg D.W.
21 mg/kg D.W.
24 mg/kg D.W.
3.1
3.1
3.1
9.4
9.4
9.4
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
09/17/19
09/18/19
DM0917/19018516
DM0918/19018540
25 mg/kg D.W.
25 mg/kg D.W.
3.2
3.1
9.5
9.4
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/19/19
DM0919/19018616
24 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
09/20/19
09/21/19
DM0920/19018631
DM0921/19019179
24 mg/kg D.W.
24 mg/kg D.W.
3.2
3.2
9.4
9.5
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/22/19
DMO922/19019198
24 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
09/23/19
09/24/19
DM0923/19019211
DM0924119019343
25 mg/kg D.W.
24 mg/kg D.W.
3.2
3.2
9.6
9.7
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/25/19
DM0925/19019365
24 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
09/26/19
DM0926/19019401
24 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
09/27/19
DM0927/19019518
23 mg/kg D.W.
3.1
9.2
SW846: 6010C
MMSD
09/28/19
DM0928/19019529
21 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
09/29/19
DM0929/19019549
21 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
09/30/19
DM0930/19019563
21 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
Avg Result: 23 mg/kg D.W.
Min LOD:
3.1 mg/kg D.W.
Max Result: 26 mg/kg D.W.
Page 7 of 16
5Y5/rptJMi/oMonth/yDW 4126119 q Printed.- 1011811912-3i

11 k 14 S D
t
Aso
PHOSPHORUS ICP Dry wt.
Date-
..
LOQ
Monthly Milorganite Report DW
September 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
09/01/19
DM0901119017160
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
09/02/19
DMO902119017173
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
09/03/19
DM0903/19017200
24000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
09/04/19
DM0904/19017215
25000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
09/05/19
DM0905119017249
24000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
09/06/19
DM0906/19017389
25000 mg/kg D.W.
23
90
SW846: 6010C
MMSD
09/07/19
DM0907/19017400
25000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
09/08/19
DM0908/19017792
25000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
09/09/19
DM0909/19017805
25000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
09/10/19
DM0910/19017832
26000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
09/11/19
DM0911/19017852
25000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
09/12/19
DM0912/19017873
26000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
09/13/19
DMO913/19017963
26000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
09/14/19
DM0914/19018457
24000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
09/15/19
DM0915/19018476
23000 mg/kg D.W.
23
87
SW846: 6010C
MMSD
09/16/19
DM0916/19018489
23000 mg/kg D.W.
23
87
SW846: 6010C
MMSD
09/17/19
DM0917/19018516
24000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
09/18/19
DMO918/19018540
24000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
09/19/19
DM0919/19018616
24000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
09/20/19
09/21/19
DM0920/19018631
DM0921/19019179
24000 mg/kg D.W.
23000 mg/kg D.W.
23
23
88
88
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/22/19
DM0922/19019198
24000 mg/kg D.W.
23
90
SW846: 6010C
MMSD
09/23/19
DM0923/19019211
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
09/24/19
DM0924/19019343
25000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
09/25/19
DM0925119019365
25000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
09/26/19
DM0926/19019401
24000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
09/27/19
09/28/19
DM0927/19019518
DM0928/19019529
24000 mg/kg D.W.
23000 mg/kg D.W.
22
23
86
88
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/29/19
DM0929/19019549
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
09/30/19
DM0930/19019563
Avg Result: 24000 mg/kg D.W.
23000 mg/kg D.W.
Min LOD:
23 89
22 mg/kg D.W.
SW846: 6010C
Max Result: 26000 mg/kg D.W.
MMSD
Page 8 of 16
SYS/rptlMiloMonth/yDW 4126119 0 Printed: 1011811912:37

a
� NSD
rhU" N A CUM MOq/Elr
POTASSIUM ICP Dry wt.
Sample Date Sample ID
09/01/19 DM0901/19017160
Result
3000 mg/kg D.W.
1.06777716q7-�V-
290
860
Monthly Milorganite Report DW
September 2019
Milorganite Daily Composite
777XAGAA �,4et i
B8. SW846: 6010C MMSD
09/02/19
DM0902/19017173
3000 mg/kg D.W.
290
870
B8.
SW846: 6010C
MMSD
09/03/19
DMO903/19017200
3200 mg/kg D.W.
290
860
B8.
SW846: 6010C
MMSD
09/04/19
DMO904/19017215
3200 mg/kg D.W.
290
860
B8.
SW846: 6010C
MMSD
09/05/19
DMO905/19017249
3300 mg/kg D.W.
290
860
SW846: 6010C
MMSD
09/06/19
DMO906/19017389
3200 mg/kg D.W.
290
860
B8.
SW846: 6010C
MMSD
09/07/19
DMO907/19017400
3300 mg/kg D.W.
280
850
B8.
SW846: 6010C
MMSD
09/08/19
DMO908/19017792
3200 mg/kg D.W.
290
860
B8.
SW846: 6010C
MMSD
09/09/19
DM0909/19017805
3200 mg/kg D.W.
290
860
B8.
SW846: 6010C
MMSD
09/10/19
DMO910/19017832
3500 mg/kg D.W.
290
880
SW846: 6010C
MMSD
09/11/19
DMO911/19017852
3300 mg/kg D.W.
290
880
SW846: 6010C
MMSD
09/12/19
DMO912/19017873
3400 mg/kg D.W.
290
870
SW846: 6010C
MMSD
09/13/19
DM0913/19017963
3400 mg/kg D.W.
280
850
SW846: 6010C
MMSD
09/14/19
DM0914/19018457
3700 mg/kg D.W.
280
850
SW846: 6010C
MMSD
09/15/19
09/16/19
DMO915/19018476
DM0916/19018489
3800 mg/kg D.W.
3900 mg/kg D.W.
280
280
840
840
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/17/19
DMO917119018516
3800 mg/kg D.W.
280
850
SW846: 6010C
MMSD
09/18/19
DM0918/19018540
3500 mg/kg D.W.
280
850
SW846: 6010C
MMSD
09/19/19
DMO919/19018616
3900 mg/kg D.W.
280
850
SW846: 6010C
MMSD
09/20/19
09/21/19
DMO920/19018631
DM0921119019179
4100 mg/kg D.W.
3800 mg/kg D.W.
280
280
850
850
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/22/19
DMO922/19019198
3800 mg/kg D.W.
290
860
SW846: 6010C
MMSD
09/23/19
DMO923/19019211
3800 mg/kg D.W.
290
870
SW846: 6010C
MMSD
09/24/19
DM0924/19019343
3800 mg/kg D.W.
290
870
SW846: 6010C
MMSD
09/25/19
DM0925/19019365
3700 mg/kg D.W.
280
860
SW846: 6010C
MMSD
09/26/19
DM0926/19019401
3800 mg/kg D.W.
280
850
AO.
SW846: 6010C
MMSD
09/27/19
DM0927/19019518
3700 mg/kg D.W.
280
830
SW846: 6010C
MMSD
09/28/19
DM0928119019529
3700 mg/kg D.W.
280
850
SW846: 6010C
MMSD
09/29/19
DM0929/19019549
3700 mg/kg D.W.
280
860
SW846: 6010C
MMSD
09/30/19
DM0930/19019563
3800 mg/kg D.W.
290
860
SW846: 6010C
MMSD
Avg Result: 3600 mg/kg D.W.
Min LOD:
280 mg/kg
D.W.
Max Result: 4100 mg/kg D.W.
Page 9 o/!6
SYS/rptlMMONonthlyDW 4126119 tj Printed: 1011811912:3i

3 kNSD
t1�tt1� t9e it C�
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
September 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
09/01/19
DM0901119017160
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
09/02/19
DM0902/19017173
5 mg/kg D.W.
4.2
13
1
SW846: 6010C
MMSD
09/03/19
DM0903/19017200
4.1 mg/kg D.W.
4.1
13
1
SW846: 6010C
MMSD
09/04/19
DM0904/19017215
7 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
09/05/19
DMO905/19017249
6.9 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
09/06/19
DM0906/19017389
5.2 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
09/07/19
DM0907/19017400
9.6 mg/kg D.W.
4.1
13
J.
SW846: 6010C
MMSD
09/08/19
DM0908/19017792
8.5 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
09/09/19
DM0909/19017805
8.2 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
09/10/19
DMO910/19017832
6.2 mg/kg D.W.
4.2
13
J, Q2.
SW846: 6010C
MMSD
09/11/19
DM0911/19017852
9 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
09/12/19
DM0912/19017873
8 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
09/13/19
DM0913/19017963
5.8 mg/kg D.W.
4.1
12
J.
SW846: 6010C
MMSD
09/14/19
DM0914/19018457
< 4.1 mg/kg D.W.
4.1
12
SW846: 6010C
MMSD
09/15/19
DM0915/19018476
< 4 mg/kg D.W.
4
12
SW846: 6010C
MMSD
09/16/19
DMO916/19018489
< 4 mg/kg D.W.
4
12
SW846: 6010C
MMSD
09/17/19
DM0917/19018516
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
09/18/19
DM0918/19018540
< 4.1 mg/kg D.W.
4.1
12
SW846: 6010C
MMSD
09/19/19
DMO919/19018616
< 4.1 mg/kg D.W.
4.1
12
SW846: 6010C
MMSD
09/20/19
DM0920/19018631
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
09/21/19
DM0921/19019179
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
09/22/19
DM0922/19019198
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
09/23/19
DM0923/19019211
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
09/24/19
DMO924/19019343
4.6 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
09/25/19
DM0925/19019365
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
09/26/19
DMO926119019401
< 4.1 mg/kg D.W.
4.1
12
SW846: 6010C
MMSD
09/27/19
DM0927119019518
< 4 mg/kg D.W.
4
12
SW846: 6010C
MMSD
09/28/19
DM0928/19019529
< 4.1 mg/kg D.W.
4.1
12
SW846: 6010C
MMSD
09/29/19
DMO929/19019549
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
09/30/19
DMO930/19019563
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
Avg Result: 2.9 mg/kg D.W.
Min LOD:
4 mg/kg
D.W.
Max Result: 9.6 mg/kg D.W.
Page 10 of 16
5Y51rpt1Mi1dMonth/y0W 4126119 tj P inted-1011811912.3;

# SD
14t5 �f A t1#1IiE>f
Solids (% Moisture)
Monthly Milorganite Report DW
September 2019
Milorganite Daily Composite
09/01/19
DMO901/19017160
6.5 %
0.1
SM 2540 G (1997)
MMSD
09/02/19
DMO902/19017173
6.7 %
0.1
SM 2540 G (1997)
MMSD
09/03/19
DM0903/19017200
5.7 %
0.1
SM 2540 G (1997)
MMSD
09/04/19
DMO904/19017215
5.7 %
0.1
SM 2540 G (1997)
MMSD
09/05/19
DMO905/19017249
5.7 %
0.1
SM 2540 G (1997)
MMSD
09/06/19
DMO906/19017389
6.3 %
0.1
SM 2540 G (1997)
MMSD
09/07/19
DMO907/19017400
4.8 %
0.1
SM 2540 G (1997)
MMSD
09/08/19
DM0908/19017792
6.1 %
0.1
SM 2540 G (1997)
MMSD
09/09/19
DM0909/19017805
6.1 %
0.1
SM 2540 G (1997)
MMSD
09/10/19
DMO910/19017832
7.8 %
0.1
SM 2540 G (1997)
MMSD
09/11/19
DM0911/19017852
8.2 %
0.1
SM 2540 G (1997)
MMSD
09/12/19
DMO912/19017873
7 %
0.1
SM 2540 G (1997)
MMSD
09/13/19
DMO913/19017963
4.6 %
0.1
SM 2540 G (1997)
MMSD
09/14/19
DMO914/19018457
4.8 %
0.1
SM 2540 G (1997)
MMSD
09/15/19
09/16/19
DMO915/19018476
DM0916/19018489
3.9 %
3.9 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
09/17/19
DMO917/19018516
4.9 %
0.1
SM 2540 G (1997)
MMSD
09/18/19
DMO918/19018540
4.7 %
0.1
SM 2540 G (1997)
MMSD
09/19/19
DM0919/19018616
4.4 %
0.1
SM 2540 G (1997)
MMSD
09/20/19
09/21/19
DM0920/19018631
DM0921/19019179
4.8 %
5 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
09/22/19
09/23/19
09/24/19
DM0922/19019198
DM0923119019211
DM0924/19019343
6.3 %
6.7 %
7.4 %
0.1
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
MMSD
09/25/19
DM0925/19019365
5.5 %
0.1
SM 2540 G (1997)
MMSD
09/26/19
09/27/19
DM0926/19019401
DM0927/19019518
4.4 %
2.5 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
09/28/19
09/29/19
09/30/19
DMO928/19019529
DM0929/19019549
DM0930/19019563
Avg Result: 5.5 °/a
4.3 % 0.1
5.4 % 0.1
6.1 % 0.1
Min LOD: 0.1 %
SM 2540 G (1997)
SM 2540 G (1997)
SM 2540 G (1997)
Max Result: 8.2
MMSD
MMSD
MMSD
Page 11 of 16
5Y5/rptlM11oMonth/yDW 4126119 tj Printed., 10118119 123i

i
i FINED
WWWACIUs"Allow
ZINC ICP Dry wt.
Sample Date Sample ID
09/01/19 DMO901/19017160
420 mg/kg D.W.
L D
18
OQ .
54
Monthly Milorganite Report DW
September 2019
Milorganite Daily Composite
a§s, Analytical Method La;W
SW846: 6010C MMSD
09/02/19
DM0902/19017173
420 mg/kg D.W.
18
55
SW846: 6010C
MMSD
09/03/19
DM0903/19017200
430 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/04/19
DM0904/19017215
440 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/05/19
DM0905/19017249
430 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/06/19
DM0906/19017389
440 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/07/19
DM0907/19017400
440 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/08/19
DM0908/19017792
450 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/09/19
DM0909119017805
450 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/10/19
DM0910/19017832
470 mg/kg D.W.
18
55
SW846: 6010C
MMSD
09/11/19
DMO911/19017852
440 mg/kg D.W.
18
56
SW846: 6010C
MMSD
09/12/19
DMO912/19017873
470 mg/kg D.W.
18
55
SW846: 6010C
MMSD
09/13/19
DM0913/19017963
480 mg/kg D.W.
18
53
SW846: 6010C
MMSD
09/14/19
DM0914/19018457
460 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/15/19
DM0915/19018476
480 mg/kg D.W.
18
53
SW846: 6010C
MMSD
09/16/19
DM0916/19018489
490 mg/kg D.W.
18
53
SW846: 6010C
MMSD
09/17/19
DM0917/19018516
540 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/18/19
DM0918/19018540
530 mg/kg D.W.
18
53
SW846: 6010C
MMSD
09/19/19
DM0919119018616
510 mg/kg D.W.
18
53
SW846: 6010C
MMSD
09/20/19
09/21/19
DM0920/19018631
DM0921/19019179
490 mg/kg D.W.
470 mg/kg D.W.
18
18
54
54
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/22/19
DM0922/19019198
470 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/23/19
DMO923/19019211
470 mg/kg D.W.
18
55
SW846: 6010C
MMSD
09/24/19
DM0924/19019343
480 mg/kg D.W.
18
55
SW846: 6010C
MMSD
09/25/19
DM0925/19019365
470 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/26/19
DM0926/19019401
460 mg/kg D.W.
18
53
SW846: 6010C
MMSD
09/27/19
DM0927/19019518
470 mg/kg D.W.
17
52
SW846: 6010C
MMSD
09/28/19
DM0928/19019529
430 mg/kg D.W.
18
53
SW846: 6010C
MMSD
09/29/19
DM0929/19019549
400 mg/kg D.W.
18
54
SW846: 6010C
MMSD
09/30/19
DM0930/19019563
400 mg/kg D.W.
18
54
SW846: 6010C
MMSD
Avg Result: 460 mg/kg D.W.
Min LOD:
17 mg/kg D.W.
Max Result: 540 mg/kg D.W.
Page 11 o/ 16
5Y5/rptlM11oMonth/yDW 4126119 of Printed. • 10/18/1911:3i

Monthly Milorganite Report DW
September 2019
vlulli�ls Not rN ttE�N9t
Milorganite Daily Composite
Phosphorus - Total % DW (Calc.)
Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
09/01/19 DMO901/19017160 2.4 % D.W. 0.1 0.1 SW846: 6010C MMSD
09/02/19
DM0902/19017173
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/03/19
DMO903/19017200
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/04/19
DM0904/19017215
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/05/19
DM0905/19017249
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/06/19
DM0906/19017389
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/07/19
DMO907/19017400
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/08/19
DMO908/19017792
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/09/19
DMO909/19017805
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/10/19
DM0910/19017832
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/11/19
DM0911/19017852
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/12/19
DMO912/19017873
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/13/19
DMO913/19017963
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/14/19
DM0914/19018457
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/15/19
09/16/19
DMO915/19018476
DMO916/19018489
2.3 % D.W.
2.3 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/17/19
09/18/19
DMO917/19018516
DM0918/19018540
2.4 % D.W.
2.4 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/19/19
DM0919/19018616
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/20/19
09/21/19
DM0920/19018631
DM0921/19019179
2.4 % D.W.
2.3 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
09/22/19
DM0922/19019198
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/23/19
DM0923/19019211
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/24/19
DM0924/19019343
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/25/19
DM0925/19019365
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/26/19
DM0926/19019401
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/27/19
DM0927/19019518
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/28/19
DM0928/19019529
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/29/19
DM0929/19019549
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
09/30/19
DM0930/19019563
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
Avg Result: 2.4 % D.W.
ALUMINUM ICP Dry wt.
Sample Date Sample ID
Min LOD: 0.1 % D.W.
Result LOD
LOQ
Max Result: 2.6 % D.W.
Milorganite Weekly Composite
QA Flags Analytical Method Lab
09/07/19
WMC36/19017807
4500 mg/kg D.W.
57
200
88. SW846: 6010C
MMSD
Avg Result: 4500 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Sample Date Sample ID
Min LOD: 57 mg/kg D.W.
Result LOD LOQ
QA Flags Analytical Method
Lab
09/07/19
WMC36/19017807
0.11 %
0.11
AOAC (13) 2.065
MMSD
Avg Result: 0.11 "/o
SYS/rptiMiloMonthlyDW 4126119 t/
Min LOD:
0.11
Page 13 of 16
Printed: 1011811912:3i

k14SD
Io ll
Monthly Milorganite Report DW
September 2019
Milorganite Weekly Composite
BORON ICP Dry wt.
Sample Da I te Sample ID Result LOD ­Lqq­',; QA Flags Analytical Method Lab
09/07/19 WMC36/19017807 21 mg/kg D.W. 1.1 3.7 SW846: 6010C Cr Lab
Avg Result: 21 mg/kg D.W. Min LOD: 1.1 mg/kg D.W.
CHROMIUM ICP Dry wt.
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
09/07/19 WMC36119017807 210 mg/kg O.W. 1.6 4.8 SW846: 6010C MMSD
Avg Result: 210 mg/kg D.W. Min LOD: 1.6 mg/kg D.W.
COBALT ICP Dry wt.
..Sample ID Result LOD LOQ �A Flags Analytical Method Lab
09/07/19 WMC36/19017807 2.7 mg/kg D.W. 0.28 1.1 B8, Q3. SW846: 6010C MMSD
Avg Result: 2.7 mg/kg D.W. Min LOD: 0.28 mg/kg D.W.
MERCURY by M. 7471 (sludge)
09/07/19
WMC36/19017807
0.26 mg/kg D.W.
0.014
0.046
EPA 7471B
CT Lab
09/14/19
WMC37/19018491
0.077 mg/kg D.W.
0.0029
0.01
EPA 7471E
CT Lab
09/21/19
WMC38/19019213
0.14 mg/kg D.W.
0.012
0.042
EPA 7471E
CT Lab
09/28/19
WMC39/19019565
0.28 mg/kg D.W.
0.014
0.049 AX.
EPA 7471B
CT Lab
Avg Result: 0.19 mg/kg D.W.
NITRATE NITROGEN
Sample Date Sample ID
Min LOD: 0.0029 mg/kg D.W.
Result LOD LOQ QA Flags
Max Result: 0.28 mg/kg D.W.
Analytical Method
Lab
09/07/19
WMC36/19017807
0.71 %
0.5
ADAC (16) 930.01
MMSD
Avg Result: 0.71 %
Min LOD: 0.5 %
NITROGEN-Total(Manual)
09/07/19 WMC36/19017807 5.8 % 0.11
Avg Result: 5.8 % Min LOD: 0.11
AOAC (16) 955.04
MMSD
NITROGEN -Water Insoluble
Date Sample TO Result LOD LOQ •, Flags Analytical Method Lab
09/07/19 WMC36/19017807 4.3 % 0.5 AOAC (16) 945.01 MMSD
Avg Result: 4.3 %
pH -Solids
Min LOD: 0.5 0/6
09/07/19 WMC36/19017807 6.36 Stnd. Units 0.1 SW846: 9045D' MMSD
09/14/19 WMC37/19018491 6.45 Stnd. Units 0.1 SW846: 9045D MMSD
09/21/19
WMC38/19019213
6.52 Stnd. Units 0.1
SW846: 9045D MMSD
09/28/19
WMC39/19019565
6.53 Stnd. Units 0.1
SW846: 9045D MMSD
Avg Result: 6.5 Stnd. Units
Min LOD: 0.1 Stnd. Units
Max Result: 6.53 Stnd. Units
5Y5/rpt1MVoMonth/yDW 412611917
Page 14 0/16
Printed- 1011811912:32

1-t}
P,tM WA f
Solids (% Moisture)
..
09/07/19 WMC36/19017807
09/14/19 WMC37/19018491
09/28/19 WMC39/19019565
Solids (% Volatile)
09/07/19
WMC36/19017807
Avg Result: 69 0/6
Solids (%
Total)
Sample ID
09/07/19
WMC36/19017807
Avg Result: 94
FECAL COLIFORM SLUDGE
Sample Date Sample 11
09/04/19 19019314
09/10/19 19020040
Monthly Milorganite Report DW
September 2019
Milorganite Weekly Composite
6.1 % 0.1
SM 2540 G (1997)
MMSD
6.2 % 0.1
SM 2540 G (1997)
MMSD
4.8 % 0.1
SM 2540 G (1997)
MMSD
5.6 % 0.1
SM 2540 G (1997)
MMSD
Min LOD: 0.1 a/o
.,< .. LOQ
QA Flags Analytical Method Lab
69 % 0.1 SM 2540 G (1997) MMSD
Min LOD: 0.1 "/o
suit .. ..
94 % 0.1 SM 2540 G (1997) MMSD
Min LOD: 0.1 0/6
Milorganite (Outfall 006) PRODUCTION
Result.. LO. Aflaq ica Met Lab
140 MPN/g TS 1.9 EPA 1680 MMSD
8.7 MPN/g TS 2 EPA 1680 MMSD
09/17/19 19020649
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
09/24/19 19021188
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
Min LOD: 0.19 MPN/g TS
Solids (% Total)
iSample Date Sample ID
Result LOD LOQ QA Flags
Analytical Method
Lab
09/04/19 19019314
95 % 0.1
SM 2540 G (1997)
MMSD
09/10/19 19020040
91 % 0.1
SM 2540 G (1997)
MMSD
09/17/19 19020649
96 % 0.1
SM 2540 G (1997)
MMSD
09/24/19 19021188
96 % 0.1
SM 2540 G (1997)
MMSD
Avg Result: 94 %
Min LOD: 0.1 "/o
Max Result: 96 0/6
Milorganite (Outfall 009)
BAGGING
FECAL COLIFORM SLUDGE
Sample Date
�sult COQ
"Me'
Sample ID
09/04/19 19019316
LOD QA Flags
< 0.19 MPN/g TS 0.19
Analyt4ca ethod
EPA 1680
Lab
MMSD m.
Min LOD: 0.19 MPN/g TS
Solids (% Total)
Sample Date Sample ID
Result LOD Ld QA Flags
Analytical Method
Lab
09/04/19 19019316
96 % 0.1
SM 2540 G (1997)
MMSD
Avg Result: 96 "/o
Min LOD: 0.1 0/0
Gage 15 of 16
SY5/rpt1M1/oMonth/yDW 4126119 tj
Minted.- 1011811912.•3i

Monthly Milorganite Report DW
NSD September 2019
lYA1NS F9l A piillRWW
Milorganite (Outfall 009) BAGGING
Milorganite (Outfall 008) SHIPPING
FECAL COLIFORM SLUDGE
09/04/19 19019315 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
Solids (% Total)
Sample Date Sample ID R .• Flags Analytical Method Lab
09/04/19 19019315 96 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 96 % Min LOD: 0.1
Flag Descriptions
AO Other -- Flag requires additional explanation IS Insufficient sample volume for analysis.
AX Qualified data - see contract laboratory report 7 Estimated concentration above the adjusted method detection limit
83 Target analyte detected in method blank > 10% of sample and below the adjusted reporting limit
concentration. LA Not analyzed - laboratory accident.
87 LCS recovery was above control limits.
B8 LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
Di Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
Hi Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
5Y5/rpt1Mi/oMonth1yDW 4126119 tj
M3 Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
M5 Incubator/water bath temperature was outside method
requirements.
M7 Microbiology sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
SS Reading was not confirmed by a constant weight measurement
SD Supplemental details provided.(Water Quality only.)
T3 The BOD dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The BOD dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample is outside of the prescribed method temperature range.
Page 16 of 16
Printed: 1011811911: 37

' INNSD
PARTNERS FOR A CLEANER ENVIRONMENT
November 18, 2019
Memorandum
TO: Brett Kelly, Todd Schwingle, Dion Doege, Jacob Holbert, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom Nowicki, Beth
Stroik, Kim Walden, Kori Kenney, Ethan Guyant, Lab File
SUBJECT: Milorganite Monthly Data — October 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of October
2019. The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin
(Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
The following comments are associated with this report:
• There were no daily production samples from October 2 —October 12, 2019
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
t
Kim Walden Date
Quality Assurance Specialist
Data/Report Review By:
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

-°
NNSD
9II;Tiiiti W A cum f
ARSENIC ICP Dry wt.
Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
October 2019
Milorganite Daily Composite
QA Flags Analytical method Lab
10/01/19
DM1001/19019630
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
10/13/19
DM1013/19020766
< 16 mg/kg D.W.
16
66
SW846: 6010C
MMSD
10/14/19
DM1014/19020779
< 16 mg/kg D.W.
16
66
SW846: 6010C
MMSD
10/15/19
DM1015/19021068
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
10/16/19
DM1016/19021083
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
10/17/19
DM1017/19021145
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
10/18/19
DM1018/19021208
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
10/19/19
DM1019/19021219
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
10/20/19
DM1020/19021238
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
10/21/19
DM1021/19021251
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
10/22/19
DM1022/19021290
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
10/23/19
10/24/19
DM1023/19021328
DM1024/19021495
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
69
68
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/25/19
DM1025/19021510
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
10/26/19
DM1026/19021694
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
10/27/19
DM1027/19021751
< 18 mg/kg D.W.
18
70
SW846: 6010C
MMSD
10/28/19
DM1028/19021764
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
10/29/19
DM1029/19021882
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
10/30/19 DM1030/19022136
10/31/19 DM1031/19022168
Avg Result: 0 mg/kg D.W.
CADMIUM ICP Dry wt.
Sample Date Sample ID
< 17 mg/kg D.W. 17 69
< 17 mg/kg D.W. 17 69
Min LOD: 16 mg/kg D.W.
Result LOD LOQ
SW846: 6010C
Q3. SW846: 6010C
QA Flags Analytical Method
MMSD
MMSD
Lab
10/01/19
DM1001/19019630
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
10/13/19
DM1013/19020766
< 0.9 mg/kg D.W.
0.9
3.4
SW846: 6010C
MMSD
10/14/19
DM1014/19020779
< 0.9 mg/kg D.W.
0.9
3.4
SW846: 6010C
MMSD
10/15/19
DM1015/19021068
< 0.91 mg/kg D.W.
0.91
3.4
SW846: 6010C
MMSD
10/16/19
10/17/19
DM1016/19021083
DM1017/19021145
< 0.92 mg/kg D.W.
< 0.91 mg/kg D.W.
0.92
0.91
3.5
3.5
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/18/19
DM1018/19021208
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
10/19/19
DM1019/19021219
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
10/20/19
DM1020/19021238
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
10/21/19
DM1021/19021251
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
10/22/19
DM1022/19021290
< 0.94 mg/kg D.W.
0.94
3.5
SW846: 6010C
MMSD
10/23/19
DM1023/19021328
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
10/24/19
DM1024/19021495
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
10/25/19
DM1025/19021510
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
10/26/19
DM1026/19021694
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
10/27/19
DM1027/19021751
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
10/28/19
DM1028/19021764
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
10/29/19
DM1029/19021882
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
10/30/19
DM1030/19022136
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
10/31/19
DM1031/19022168
1.2 mg/kg D.W.
0.94
3.6
J. SW846: 6010C
MMSD
Avg Result: 0.06 mg/kg D.W.
SYS/rptlMi/oMonthlyDW 4126119 tj
Min LOD:
0.9 mg/kg D.W.
Max Result: 1.2 mg/kg D.W.
Page 1 of 16
Printed: 11118119 08:06

I ND
COPPER ICP Dry wt.
Sample Date Sample ID
Result
LOD
Monthly Milorganite Report DW
October 2019
Milorganite Daily Composite
Flags Analytical Method Lab
10/01/19
DM1001/19019630
220 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
10/13/19
DM1013/19020766
210 mg/kg D.W.
6.5
25
SW846: 6010C
MMSD
10/14/19
DM1014/19020779
210 mg/kg D.W.
6.5
25
SW846: 6010C
MMSD
10/15/19
DM1015/19021068
210 mg/kg D.W.
6.6
25
Q3. SW846: 6010C
MMSD
10/16/19
OM1016/19021083
230 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
10/17/19
DM1017/19021145
230 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
10/18/19
DM1018/19021208
220 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
10/19/19
DM1019/19021219
210 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
10/20/19
DM1020/19021238
210 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
10/21/19
DM1021/19021251
210 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
10/22/19
10/23/19
DM1022/19021290
DM1023/19021328
210 mg/kg D.W.
220 mg/kg D.W.
6.8
6.8
26
26
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/24/19
DM1024/19021495
210 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
10/25/19
DM1025/19021510
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
10/26/19
DM1026/19021694
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
10/27/19
DM1027/19021751
210 mg/kg D.W.
6.9
26
SW846: 601OC
MMSD
10/28/19
DM1028/19021764
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
10/29/19 DM1029/19021882
10/30/19 DM1030/19022136
10/31/19 DM1031/19022168
Avg Result: 220 mg/kg D.W.
IRON ICP Dry wt.
►.Result
10/01/19 DM1001/19019630
220 mg/kg D.W. 6.7 26
220 mg/kg D.W. 6.8 26
220 mg/kg D.W. 6.8 26
Min LOD: 6.5 mg/kg D.W.
LOD LOQ
48000 mg/kg D.W. 530 1900
SW846: 6010C
SW846: 6010C
SW846: 6010C
Max Result: 230 mg/kg D.W.
QA Flags Analytical Method
SW846: 6010C
MMSD
MMSD
MMSD
Lab
MMSD
10/13/19
10/14/19
DM1013/19020766
DM1014/19020779
45000 mg/kg D.W.
46000 mg/kg D.W.
520
520
1900
1800
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/15/19
DM1015/19021068
48000 mg/kg D.W.
520
1900
Q3. SW846: 6010C
MMSD
10/16/19
OM1016/19021083
52000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
10/17/19
DM1017/19021145
49000 mg/kg D.W.
520
1900
SW846: 6010C
MMSD
10/18/19
10/19/19
DM1018/19021208
DM1019/19021219
51000 mg/kg D.W.
50000 mg/kg D.W.
530
540
1900
1900
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/20/19
DM1020/19021238
49000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
10/21/19
DM1021/19021251
49000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
10/22/19
DM1022/19021290
50000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
10/23/19
DM1023/19021328
48000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
10/24/19
DM1024/19021495
48000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
10/25/19
DM1025/19021510
46000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
10/26/19
DM1026/19021694
45000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
10/27/19
DM1027/19021751
44000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
10/28/19
DM1028/19021764
42000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
10/29/19
DM1029/19021882
41000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
10/30/19
DM1030/19022136
41000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
10/31/19
DM1031/19022168
42000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
Avg Result: 47000 mg/kg D.W.
5Y5/rpt1MdoM0nth1yDW 4126119 tj
Min LOD:
520 mg/kg D.W.
Max Result: 52000 mg/kg D.W.
Page 2 of 16
Printed; 11118119 08:06

w
kNSD
Monthly Milorganite Report DW
October 2019
IltA t�I.ElI/Bt
Milorganite Daily Composite
LEAD ICP Dry wt.
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
10/01/19 DM1001/19019630 48 mg/kg D.W. 2.9 8.6 SW846: 6010C MMSD
10/13/19 DM1013/19020766 48 mg/kg D.W. 2.8 8.4 SW846: 6010C MMSD
10/14/19 DM1014/19020779 44 mg/kg D.W. 2.8 8.4 SW846: 6010C MMSD
10/15/19 DM1015/19021068 44 mg/kg D.W. 2.8 8.5 SW846: 6010C MMSD
10/16/19 DM1016/19021083 48 mg/kg D.W. 2.8 8.5 SW846: 6010C MMSD
10/17/19 DM1017/19021145 48 mg/kg D.W. 2.8 8.5 SW846: 6010C MMSD
10/18/19 DM1018/19021208 44 mg/kg D.W. 2.9 8.6 SW846: 6010C MMSD
10/19/19 DM1019/19021219 46 mg/kg D.W. 2.9 8.7 SW846: 6010C MMSD
10/20/19 DM1020/19021238 44 mg/kg D.W. 2.9 8.6 SW846: 6010C MMSD
10/21/19 DM1021/19021251 45 mg/kg D.W. 2.9 8.8 SW846: 6010C MMSD
10/22/19 DM1022/19021290 45 mg/kg D.W. 2.9 8.7 SW846: 6010C MMSD
10/23/19 DM1023/19021328 43 mg/kg D.W. 2.9 8.8 SW846: 6010C MMSD
10/24/19 DM1024/19021495 40 mg/kg D.W. 2.9 8.7 SW846: 6010C MMSD
10/25/19 DM1025119021510 40 mg/kg D.W. 2.9 8.8 SW846: 6010C MMSD
10/26/19 DM1026/19021694 43 mg/kg D.W. 2.9 8.8 SW846: 6010C MMSD
10/27/19 DM1027119021751 46 mg/kg D.W. 3 8.9 SW846: 6010C MMSD
10/28/19 DM1028/19021764 47 mg/kg D.W. 2.9 8.8 SW846: 6010C MMSD
10/29/19 DM1029/19021882 48 mg/kg D.W. 2.9 8.6 SW846: 6010C MMSD
10/30/19 DM1030119022136 47 mg/kg D.W. 2.9 8.7 SW846: 6010C MMSD
10/31/19 DM1031/19022168 53 mg/kg D.W. 2.9 8.7 SW846: 6010C MMSD
Avg Result: 46 mg/kg D.W. Min LOD: 2.8 mg/kg D.W. Max Result: 53 mg/kg D.W.
MOLYBDENUM ICP Dry wt.
sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
10/01/19 DM1001/19019630 9 mg/kg D.W. 4.5 17 3. SW846: 6010C MMSD
10/13/19 DM1013/19020766 8.7 mg/kg D.W. 4.3 16 1 SW846: 6010C MMSD
10/14/19 DM1014/19020779 8.2 mg/kg D.W. 4.3 16 3. SW846: 6010C MMSD
10/15/19 DM1015/19021068 8 mg/kg D.W. 4.4 17 3, Q3. SW846: 6010C MMSD
10/16/19 DM1016/19021083 9.2 mg/kg D.W. 4.4 17 3. SW846: 6010C MMSD
10/17/19 DM1017/19021145 8.9 mg/kg D.W. 4.4 17 3. SW846: 6010C MMSD
10/18/19 DM1018/19021208 8.1 mg/kg D.W. 4.5 17 3. SW846: 6010C MMSD
10/19/19 DM1019/19021219 9.1 mg/kg D.W. 4.5 17 3. SW846: 6010C MMSD
10/20/19 DM1020/19021238 8.8 mg/kg D.W. 4.5 17 3. SW846: 6010C MMSD
10/21/19 DM1021/19021251 9.2 mg/kg D.W. 4.6 17 3. SW846: 6010C MMSD
10/22/19 DM1022/19021290 9.4 mg/kg D.W. 4.5 17 1 SW846: 6010C MMSD
10/23/19 DM1023/19021328 9.3 mg/kg D.W. 4.6 17 3. SW846: 6010C MMSD
10/24/19 DM1024/19021495 9.4 mg/kg D.W. 4.5 17 3. SW846: 6010C MMSD
10/25/19 DM1025/19021510 8.3 mg/kg D.W. 4.5 17 3. SW846: 6010C MMSD
10/26/19 DM1026/19021694 9 mg/kg D.W. 4.6 17 3. SW846: 6010C MMSD
10/27/19 DM1027/19021751 9.2 mg/kg D.W. 4.6 18 3. SW846: 6010C MMSD
10/28/19 DM1028/19021764 9.1 mg/kg D.W. 4.5 17 3. SW846: 6010C MMSD
10/29/19 DM1029/19021882 9 mg/kg D.W. 4.5 17 3. SW846: 6010C MMSD
10/30/19 DM1030/19022136 8.9 mg/kg D.W. 4.5 17 3. SW846: 6010C MMSD
10/31/19 DM1031/19022168 8.8 mg/kg D.W. 4.5 17 1. SW846: 6010C MMSD
Avg Result: 8.9 mg/kg D.W. Min LOD: 4.3 mg/kg D.W. Max Result: 9.4 mg/kg D.W.
Page 3 of 16
SKS/rptl MiloMonthlyDW 4126119 tj Printed.' 11118119 08:06

r'f
NNSD
t�t�w�let8W
NICKEL ICP Dry wt.
-Date Sample TO
Result
LOD
LOQ
Monthly Milorganite Report DW
October 2019
Milorganite Daily Composite
QA Flags Analytical Method
10/01/19
D101001/19019630
23 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
10/13/19
DM1013/19020766
22 mg/kg D.W.
3.1
9.3
SW846: 6010C
MMSD
10/14/19
DM1014/19020779
22 mg/kg D.W.
3.1
9.3
SW846: 6010C
MMSD
10/15/19
DM1015/19021068
22 mg/kg D.W.
3.1
9.4
Q3. SW846: 6010C
MMSD
10/16/19
DM1016/19021083
24 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
10/17/19
DM1017/19021145
23 mg/kg D.W.
3.1
9.4
SW846: 6010C
MMSD
10/18/19
DM1018/19021208
26 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
10/19/19
DM1019/19021219
22 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
10/20/19
DM1020/19021238
21 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
10/21/19
DM1021/19021251
21 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
30/22/19
10/23/19
DM1022/19021290
DM1023/19021328
22 mg/kg D.W.
21 mg/kg D.W.
3.2
3.2
9.7
9.8
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/24/19
DM1024/19021495
21 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
10/25/19
DM1025/19021510
19 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
10/26/19
DM1026/19021694
21 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
10/27/19
DM1027/19021751
22 mg/kg D.W.
3.3
9.9
SW846: 6010C
MMSD
10/28/19
DM1028119021764
24 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
10/29/19
DM1029/19021882
23 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
10/30/19
DM1030/19022136
23 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
10/31/19 DM1031/19022168
Avg Result: 22 mg/kg D.W.
PHOSPHORUS ICP Dry wt.
10/0(/19 DM1001/19019630
10/13/19 DM1013/19020766
10/14/19 DM1014/19020779
25 mg/kg D.W. 3.2 9.7
Min LOD: 3.1 mg/kg D.W.
Result •D LOQ
23000 mg/kg D.W. 23 89
22000 mg/kg D.W. 23 87
22000 mg/kg D.W. 23 87
SW846: 6010C
Max Result: 26 mg/kg D.W.
•• Flags Analytical Method
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
Lab
MMSD
MMSD
MMSD
10/15/19
DM1015/19021068
21000 mg/kg D.W.
23
88
Q3. SW846: 6010C
MMSD
10/16/19
DM1016/19021083
22000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
10/17/19
DM1017/19021145
23000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
10/18/19
10/19/19
DM1018/19021208
DM1019/19021219
22000 mg/kg D.W.
23000 mg/kg D.W.
23
24
89
90
SW846: 6010C .
SW846: 6010C
MMSD
MMSD
10/20/19
DM1020/19021238
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
10/21/19
DM1021/19021251
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
10/22/19
DM1022/19021290
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
10/23/19
DM1023/19021328
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
10/24/19
DM1024/19021495
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
10/25/19
DM1025/19021510
23000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
10/26/19
DM1026/19021694
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
10/27/19
DM1027/19021751
24000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
10/28/19
DM1028/19021764
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
10/29/19
DM1029/19021882
23000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
10/30/19
DM1030/19022136
22000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
10/31/19
DM1031/19022168
23000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
Avg Result: 23000 mg/kg D.W.
SYSIrptimomonthiyDW 4126119 tj
Min LOD: 23 mg/kg D.W.
Max Result: 24000 mg/kg D.W.
Page 4 OfIC
Printed.11118119 08:06

Monthly Milorganite Report DW
kNSD October 2019
POTASSIUM ICP Dry wt.
Date Sample ID
Result
LOD
LOQ QA
Flags
Milorganite Daily Composite
Analytical Method Lab
10/01/19
OM1001/19019630
3900 mg/kg D.W.
290
860
SW846: 6010C
MMSD
10/13/19
DM1013/19020766
3900 mg/kg D.W.
280
840
SW846: 6010C
MMSD
10/14/19
DM1014/19020779
3900 mg/kg D.W.
280
840
SW846: 6010C
MMSD
10/15/19
DM1015/19021068
4100 mg/kg D.W.
280
850
Q3.
SW846: 6010C
MMSD
10/16/19
DM1016/19021083
4300 mg/kg D.W.
280
850
SW846: 6010C
MMSD
10/17/19
DM1017/19021145
4200 mg/kg D.W.
280
850
SW846: 6010C
MMSD
10/18/19
DM1018/19021208
4500 mg/kg D.W.
290
860
SW846: 6010C
MMSD
10/19/19
DM1019/19021219
4800 mg/kg D.W.
290
870
SW846: 6010C
MMSD
10/20/19
DM1020/19021238
4700 mg/kg D.W.
290
860
SW846: 6010C
MMSD
10/21/19
DM1021/19021251
4800 mg/kg D.W.
290
880
SW846: 6010C
MMSD
10/22/19
10/23/19
DM1022/19021290
DM1023/19021328
4900 mg/kg D.W.
4000 mg/kg D.W.
290
290
870
880
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/24/19
DM1024/19021495
4100 mg/kg D.W.
290
870
SW846: 6010C
MMSD
10/25/19
DM1025/19021510
4200 mg/kg D.W.
290
880
SW846: 6010C
MMSD
10/26/19
DM1026/19021694
4800 mg/kg D.W.
290
880
SW846: 6010C
MMSD
10/27/19
DM1027/19021751
4900 mg/kg D.W.
300
890
SW846: 6010C
MMSD
10/28/19
DM1028/19021764
4800 mg/kg D.W.
290
880
SW846: 6010C
MMSD
10/29/19
DM1029/19021882
4400 mg/kg D.W.
290
860
SW846: 6010C
MMSD
10/30/19
DM1030/19022136
4600 mg/kg D.W.
290
870
SW846: 6010C
MMSD
10/31/19 DM1031/19022168
Avg Result: 4400 mg/kg D.W.
SELENIUM ICP Dry wt.
Sample Date Sample ID
4800 mg/kg D.W. 290 870
Min LOD: 280 mg/kg D.W.
Result LOD LOQ ••
Flags
SW846: 6010C
Max Result: 4900 mg/kg D.W.
Analytical Method
MMSD
Lab
10/01/19
DM1001/19019630
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
10/13/19
DM1013/19020766
<4 mg/kg D.W.
4
12
SW846: 6010C
MMSD
10/14/19
DM1014/19020779
<4 mg/kg D.W.
4
12
SW846: 6010C
MMSD
10/15/19
DM1015/19021068
< 4,1 mg/kg D.W.
4.1
12
SW846: 6010C
MMSD
10/16/19
DM1016/19021083
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
10/17/19
DM1017/19021145
5.1 mg/kg D.W.
4.1
12
3.
SW846: 6010C
MMSD
10/18/19
10/19/19
DM1018/19021208
DM1019/19021219
11 mg/kg D.W.
4.5 mg/kg D.W.
4.2
4.2
13
13
3.
3.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/20/19
DM1020/19021238
6.5 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
10/21/19
DM1021/19021251
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
10/22/19
DM1022/19021290
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
10/23/19
DM1023/19021328
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
10/24/19
DM1024/19021495
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
10/25/19
DM1025/19021510
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
10/26/19
DM1026/19021694
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
10/27/19
DM1027119021751
< 4.3 mg/kg D.W.
4.3
13
SW846: 6010C
MMSD
10/28/19
DM1028/19021764
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
10/29/19
DM1029/19021882
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
10/30/19
DM1030/19022136
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
10/31/19
DM1031/19022168
7.1 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
Avg Result: 1.7 mg/kg D.W.
SY51rpt1MVoM6nf 1YDW 4126119 fj
Min LOD:
4 mg/kg
D.W.
Max Result: 11 mg/kg D.W.
Page Sor16
Printed.• 11118119 08:06

t"
'e, NSD
PUT01M fa ACiii>
Solids (% Moisture)
10/01/19 DM1001119019630
Monthly Milorganite Report DW
October 2019
Milorganite Daily Composite
lit .. LOQ
6.1 % 0.1 SM 2540 G (1997) MMSD
10/13/19
DM1013/19020766
3.3 %
0.1
SM 2540 G (1997)
MMSD
10/14/19
DM1014/19020779
3.2 %
0.1
SM 2540 G (1997)
MMSD
10/15/19
DM1015/19021068
4.4 %
0.1
SM 2540 G (1997)
MMSD
10/16/19
DM1016/19021083
5.2 %
0.1
SM 2540 G (1997)
MMSD
10/17/19
DM1017/19021145
4.6 %
0.1
SM 2540 G (1997)
MMSD
10/18/19
DM1018/19021208
6 %
0.1
SM 2540 G (1997)
MMSD
10/19/19
DM1019/19021219
6.6 %
0.1
SM 2540 G (1997)
MMSD
10/20/19
DM1020/19021238
6.1 %
0.1
SM 2540 G (1997)
MMSD
10/21/19
DM1021/19021251
8.2 %
0.1
SM 2540 G (1997)
MMSD
10/22/19
10/23/19
DM1022/19021290
DM1023/19021328
7 %
7.8 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
10/24/19
DM1024/19021495
6.5 %
0.1
SM 2540 G (1997)
MMSD
10/25/19
DM1025/19021510
7.6 %
0.1
SM 2540 G (1997)
MMSD
10/26/19
DM1026/19021694
7.7 %
0.1
SM 2540 G (1997)
MMSD
10/27/19
DM1027/19021751
8.9 %
0.1
SM 2540 G (1997)
MMSD
10/28/19
DM1028/19021764
7.6 %
0.1
SM 2540 G (1997)
MMSD
10/29/19
DM1029/19021882
6.4 %
0.1
SM 2540 G (1997)
MMSD
10/30/19
DM1030/19022136
6.9 %
0.1
SM 2540 G (1997)
MMSD
10/31/19 DM1031/19022168
Avg Result: 6.4 %
ZINC ICP Dry wt.
Sample Date Sample ID
7.2 % 0.1
Min LOD: 0.1 %
Result LOD
LOQ .• Flags
SM 2540 G (1997)
Max Result: 8.9
Analytical Method
MMSD
Lab
10/01/19
DM1001/19019630
420 mg/kg D.W.
18
54
SW846: 6010C
MMSD
10/13/19
10/14/19
DM1013/19020766
DM1014/19020779
410 mg/kg D.W.
400 mg/kg D.W.
18
18
53
53
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/15/19
DM1015/19021068
380 mg/kg D.W.
18
53
SW846: 6010C
MMSD
10/16/19
DM1016/19021083
410 mg/kg D.W.
18
54
SW846: 6010C
MMSD
10/17/19
DM1017/19021145
400 mg/kg D.W.
18
53
SW846: 6010C
MMSD
10/18/19
10/19/19
DM1018/19021208
DM1019/19021219
390 mg/kg D.W.
390 mg/kg D.W.
18
18
54
54
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/20/19
DM1020/19021238
370 mg/kg D.W.
18
54
SW846: 6010C
MMSD
10/21/19
DM1021/19021251
380 mg/kg D.W.
18
56
SW846: 6010C
MMSD
10/22/19
DM1022/19021290
390 mg/kg D.W.
18
55
SW846: 6010C
MMSD
10/23/19
DM1023/19021328
390 mg/kg D.W.
18
55
SW846: 6010C
MMSD
10/24/19
DM1024/19021495
370 mg/kg D.W.
18
54
SW846: 6010C
MMSD
10/25/19
DM1025/19021510
360 mg/kg D.W.
18
55
SW846: 6010C
MMSD
10/26/19
DM1026/19021694
380 mg/kg D.W.
18
55
SW846: 6010C
MMSD
10/27/19
DM1027/19021751
390 mg/kg D.W.
19
56
SW846: 6010C
MMSD
10/28/19
DM1028/19021764
410 mg/kg D.W.
18
55
SW846: 6010C
MMSD
10/29/19
DM1029/19021882
410 mg/kg D.W.
18
54
SW846: 6010C
MMSD
10/30/19
DM1030/19022136
420 mg/kg D.W.
18
55
SW846: 6010C
MMSD
10/31/19
DM1031/19022168
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
Avg Result: 400 mg/kg D.W.
5Y5/rpt1M1/oMonth1yOW 4126119 tj
Min LOD:
18 mg/kg D.W.
Max Result: 440 mg/kg D.W.
Page 6 of IC
Printed., 11116119 08:06

k� i► �Ivlwl9t
Phosphorus - Total % DW (Calc.)
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
October 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
10/01/19 DM1001/19019630
2.3%D.W.
0.1
0.1
SW846: 6010C
MMSD
10/13/19 DM1013/19020766
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/14/19 DMID14/19020779
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/15/19 DM1015/19021068
2.1 % D.W.
0.1
0.1
Q3. SW846: 6010C
MMSD
10/16/19 DM1016/19021083
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/17/19 DM1017/19021145
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/18/19 DM1018/19021208
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/19/19 DM1019/19021219
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/20/19 DM1020/19021238
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/21/19 DM1021/19021251
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/22/19 DM1022/19021290
10/23/19 DM1023/19021328
2.4 9/6 D.W.
2.4 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
10/24/19 DM1024/19021495
2.4%D.W.
0.1
0.1
SW846: 6010C
MMSD
10/25/19 DM1025/19021510
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/26/19 DM1026/19021694
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/27/19 DM1027/19021751
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/28/19 DM1028/19021764
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/29/19 DM1029/19021882
2.3%D.W.
0.1
0.1
SW846: 6010C
MMSD
10/30/19 DM1030/19022136
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/31/19 DM1031/19022168
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
Avg Result: 2.3 "/o D.W.
ALUMINUM ICP Dry wt.
Sample Date Sample
Min LOD: 0.1 0% D.W.
Result LOD
LOQ
Max Result: 2.4 % D.W.
Milorganite Weekly Composite
QA Flags Analytical Method Lab
10/26/19 WMC43/19020781
4400 mg/kg D.W.
57
200
88. SW846: 6010C
MMSD
Avg Result: 4400 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Date Sample ID
Min LOD: 57 mg/kg D.W.
Result LOD LOQ
QA Flags Analytical Method
Lab
10/26/19 WMC43/19020781
0.15 %
0.11
0.37
AOAC (13) 2.065
MMSD
Avg Result: 0.15 %
BORON ICP Dry wt.
Sample Date Sample ID
Min LOD: 0.11 °/u
Result LOD
LOQ
+• Flags Analytical Method
Lab
10/26/19 WMC43/19020781
20 mg/kg D.W.
1.1
3.6
SW846: 6010C
CT Lab
Avg Result: 20 mg/kg D.W.
CHROMIUM ICP Dry wt.
Sample Date Sample ID
Min LOD: 1.1 mg/kg D.W.
Result LOD LOQ
QA Flags Analytical Method
Lab
10/26/19 WMC43/19020781
170 mg/kg D.W.
1.6
4.8
SW846: 6010C
MMSD
Avg Result: 170 mg/kg D.W.
Min LOD:
1.6 mg/kg
D.W.
Page 7 of 16
5Y51rpt1Hi/oM0nth1YDW 4126119 0 Pnnted.• 11118119 08:06

SD
i1tTMER3 t0# M CM [M�IlAllflr
Monthly Milorganite Report DW
October 2019
Milorganite Weekly Composite
COBALT ICP Dry wt.
-Date•. LOQ •.
Flags Analytical Method -Lab-
10/26/19 WMC43/19020781 1.8 mg/kg D.W. 0.28 1.1 B8. SW846: 6010C MMSD
Avg Result: 1.8 mg/kg D.W. Min LOD: 0.28 mg/kg D.W.
MERCURY by M. 7471 (sludge)
Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
10/05/19 WMC40/19019971 0.15 mg/kg D.W. 0.014 0.049 EPA 7471E Cr Lab
10/19/19 WMC42/19021253
0.041 mg/kg D.W. 0.014
0.048 3, AX.
EPA 7471E
CT Lab
10/26/19 WMC43/19020781
0.18 mg/kg D.W. 0.014
0.048
EPA 7471E
CT Lab
Avg Result: 0.12 mg/kg D.W.
Min LOD: 0.014 mg/kg D.W.
Max Result: 0.18 mg/kg D.W.
NITRATE NITROGEN
Lab
oil
10/26/19 WMC43/19020781
Result LOD
0.93 % 0.5
LOQ .. Flags
Analytical Method
AOAC (16) 930.01
MMSD
Avg Result: 0.93 %
Min LOD: 0.5
NITROGEN-Total(Manual)
,•..
.�
'7AnalyticalMethod
Lab
10/26/19 WMC43/19020781
6 % 0.11
AOAC (16) 955.04
MMSD
Avg Result: 6 %
Min LOD: 0.11 0/6
NITROGEN -Water Insoluble
V ..
Flags
Sample ..
10/26/19 WMC43/19020781
•.
4.7 % 0.5
.-
AOAC (16) 945.01
MMSD
Avg Result: 4.7 %
Min LOD: 0.5 %
pH -Solids
Sample ..
L.. .• Flags
Analytical Method
Lab
10/05/19 WMC40/19019971
6.42 Stnd. Units 0.1
SW846: 9045D
MMSD
10/19/19 WMC42/19021253
6.25 Stnd. Units 0.1
SW846: 9045D
MMSD
10/26/19 WMC43/19020781
6.2 Stnd. Units 0.1
SW846: 9045D
MMSD
Avg Result: 6.3 Stnd. Units Min LOD: 0.1 Stnd. Units Max Result: 6.42 Stnd. Units
Solids (% Moisture)
Sample Date Sample ID LOD LOQ QA Flags Analytical Method Lab
10/05/19 WMC40/19019971 6.2 % 0.1 SM 2540 G (1997) MMSD
10/19/19 WMC42/19021253 4.9 % 0.1 SM 2540 G (1997) MMSD
10/26/19 WMC43/19020781 7.1 % 0.1 SM 2540 G (1997) MMSD
Min LOD: 0.1 %
Solids (% Volatile)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
10/26/19 WMC43/19020781 70 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 70 % Min LOD: 0.1
Page 8 of 16
SYS/rptJMiioMonthiyDW 4126119 U Printed.• 11118119 08:05

tMonthly Milorganite Report DW
'iNSD October 2019
hRA R3 FIX A (11 9i) EIIIIIlmr,
Milorganite Weekly Composite
Solids (% Total)
Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
10/26/19 WMC43/19020781 93 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 93
Min LOD: 0.1
Milorganite (Outfall 006) PRODUCTION
FECAL COLIFORM SLUDGE
iSample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
10/15/19 19022900 1.8 MPN/g TS 0.19 EPA 1680 MMSD
10/22/19 19023411
< 0.2 MPN/g TS 0.2
EPA 1680
MMSD
10/29/19 19024055
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
Min LOD: 0.19 MPN/g TS
Solids (% Total)
Sample Date Sample ID
Result LOD LOQ QA Flags
Analytical Method
Lab
10/15/19 19022900
96 % 0.1
SM 2540 G (1997)
MMSD
10/22/19 19023411
92 % 0.1
SM 2540 G (1997)
MMSD
10/29/19 19024055
95 % 0.1
SM 2540 G (1997)
MMSD
Avg Result: 94 %
Min LOD: 0.1 %
Max Result: 96 0/6
Milorganite (Outfall 009)
BAGGING
FECAL COLIFORM SLUDGE
Sample Date Sample ID
Result LOD LOQ QA Flags
Analytical Method
Lab
10/01/19 19021904
4.8 MPN/g TS 1.9
EPA 1680
MMSD
Min LOD: 1.9 MPN/g TS
Solids (% Total)
iSample Date Sample ID
Result LOD LOQ •• Flags
Analytical Method
Lab
10/01/19 19021904
94 % 0.1
SM 2540 G (1997)
MMSD
Avg Result: 94 %
Min LOD: 0.1
Milorganite (Outfall 008) SHIPPING
FECAL COLIFORM SLUDGE
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
10/01/19 19021903 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
Solids (% Total)
Sample Date Sample ID Result .. LOQ •. Flags Analytical Method Lab
10/01/19 19021903 94 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 94 % Min LOD: 0.1
Page 9 of 16
5Y5/rpt1M1/oManth1YDW 4126119 tj Pnnted: 11118119 08.•06

P^
INNSD
IQA t1iA�so
Flag Descriptions
AO Other -- Flag requires additional explanation
AX Qualified data - see contract laboratory report
B3 Target analyte detected in method blank > 10% of sample
concentration.
87 LCS recovery was above control limits.
B8 LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
DI Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix Interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
H1 Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
Monthly Milorganite Report DW
October 2019
IS Insufficient sample volume for analysis.
7 Estimated concentration above the adjusted method detection limit
_ and below the adjusted reporting limit
LA Not analyzed - laboratory accident.
M11 Too numerous to count.
M12 Sample Incubation period outside method requirement.
M13 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
M15 Incubator/water bath temperature was outside method
requirements.
M7 Microbiology sample received without adequate headspace.
M19 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
S5 Reading was not confirmed by a constant weight measurement
SD Supplemental details provided.(Water Quality only.)
T3 The BOD dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
T5 GGA BOD was above method acceptance criteria.
T7 The BOD dilution water D.O. increase was > 0.2 mg/L.
TS Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample is outside of the prescribed method temperature range.
Page 10 of 16
SYS/rpflMi/oMonth/yDW 4126119 ti Printed.• 11/18/1908.M

NNSD
PARTNERS FOR A CLEANER ENVIRONMENT
December 13, 2019
Memorandum
TO: Brett Kelly, Todd Schwingle, Dion Doege, Jacob Holbert, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom Nowicki, Beth
Stroik, Kim Walden, Kori Kenney, Ethan Guyant, Lab File
SUBJECT: Milorganite Monthly Data — November 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of November
2019. The boron analysis was performed by CT Laboratories, in Baraboo, Wisconsin (Wisconsin
Certification ID# 157066030). The mercury analyses were performed by CT Laboratories, in Baraboo,
Wisconsin (Wisconsin Certification ID# 157066030) and by Pace Analytical Services, Inc. in Green Bay,
Wisconsin (Wisconsin Certification #: 405132750). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
Rich Vincent Date
Laboratory Supervisor
Data/Report Review By:
�✓%��/�/' 1d-) 3-1 q
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

14SD
PUMNAMMf
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
•. Flags AnalWcal Method Lab
11/01/19
DM1101/19022183
< 18 mg/kg D.W.
18
70
SW846: 6010C
MMSD
11/02/19
DM1102/19022194
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
11/03/19
DM1103/19022213
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
11/04/19
DM1104/19022226
< 18 mg/kg D.W.
18
70
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
11/06/19
DM1106/19022391
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
11/08/19
DM1108/19022948
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
11/10/19
DM1110/19022978
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
11/11/19
DM1111/19022991
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
11/12/19
11/13/19
DM1112/19023017
DM1113/19023033
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
70
68
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/14/19
DM1114/19023645
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
< 17 mg/kg D.W.
17
69
Q3.
SW846: 6010C
MMSD
11/16/19
DM1116/19023738
< 17 mg/kg D.W.
17
70
Q3.
SW846: 6010C
MMSD
11/17/19
DM1117/19023757
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
11/18/19
DM1118/19023770
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
11/19/19
11/20/19
DM1119/19023797
DM1120/19023964
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
69
70
Q3.
Q3.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/21/19
DM1121/19023996
< 17 mg/kg D.W.
17
69
Q3.
SW846: 6010C
MMSD
11/22/19
DM1122/19024012
< 17 mg/kg D.W.
17
69
Q3.
SW846: 6010C
MMSD
11/23/19
DM1123/19024023
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
11/24/19
DM1124/19024220
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
11/25/19
11/26/19
11/27/19
11/28/19
11/29/19
DM1125/19024233
DM1126/19024576
DM1127/19024593
DM1128/19024644
DM1129/19024659
< 17 mg/kg D.W.
< 17 mg/kg D.W.
< 17 mg/kg D.W.
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
17
17
17
69
68
68
69
69
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
MMSD
11/30/19
DM1130/19024670
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
17 mg/kg D.W.
Page 1 of 16
5Y5/rpt1MWoMonth1yDW 4126119 tj Printed: 12113/1914:31

I iNNSD
if,}
P,isiee�Ll#�i
CADMIUM ICP Dry wt.
Date Sample ID
Result
LOD
LOQ QA
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
Flags Analytical Method Lab
11/01/19
DM1101/19022183
<0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
11/02/19
DM1102/19022194
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
11/03/19
DM1103/19022213
<0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
11/04/19
DM1104/19022226
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/06/19
DM1106119022391
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
11/08/19
DM1108/19022948
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
11/10/19
DM1110/19022978
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/11/19
DM1111/19022991
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/12/19
DM1112/19023017
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
11/13/19
DM1113/19023033
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
11/14/19
DM1114/19023645
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
11/16/19
DM1116/19023738
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
11/17/19
DM1117/19023757
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
11/18/19
DM1118/19023770
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
11/19/19
DM1119/19023797
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/20/19
DM1120119023964
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/21/19
DM1121/19023996
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/22/19
DM1122/19024012
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/23/19
DM1123/19024023
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
11/24/19
DM1124/19024220
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/25/19
DM1125119024233
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/26/19
DM1126/19024576
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
11/27/19
DM1127/19024593
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
11/28/19
DM1128/19024644
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/29/19
DM1129/19024659
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
11/30/19
DM1130/19024670
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
0.92 mg/kg D.W.
Page 1 of 16
5Y5/rpt1Mi/oMonth1yDW 4126119 tj Printed.• 1211311914.31

14SD
P1R�i1f�3 iox A CIS
COPPER ICP Dry wt.
Uinj&b. .. LOQ
11/01/19 DM1101/19022183 220 mg/kg D.W. 6.9 26
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
.ags Analytical MetfiM La
SW846: 6010C MMSD
11/02/19
DM1102/19022194
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/03/19
DM1103/19022213
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/04/19
DM1104/19022226
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/06/19
DM1106/19022391
230 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
240 mg/kg D.W.
6.7
25
SW846: 6010C
MMSD
11/08/19
DM1108/19022948
240 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
250 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
11/10/19
OM1110/19022978
250 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/11/19
11/12/19
DM1111/19022991
DM1112/19023017
250 mg/kg D.W.
250 mg/kg D.W.
6.8
6.9
26
26
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/13/19
DM1113/19023033
240 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
11/14/19
DM1114/19023645
240 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/16/19
DM1116/19023738
240 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/17/19
DM1117/19023757
240 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/18/19
11/19/19
11/20/19
DM1118/19023770
DM1119/19023797
DM1120/19023964
240 mg/kg D.W.
220 mg/kg D.W.
240 mg/kg D.W.
6.8
6.8
6.8
26
26
26
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
11/21/19
DM1121/19023996
240 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/22/19
11/23/19
DM1122/19024012
DM1123/19024023
200 mg/kg D.W.
240 mg/kg D.W.
6.8
6.7
26
26
Q3. SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/24/19
DM1124/19024220
240 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/25/19
DM1125/19024233
240 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/26/19
DM1126/19024576
210 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
11/27/19
DM1127/19024593
240 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
11/28/19
DM1128/19024644
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/29/19
DM1129/19024659
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
11/30/19
DM1130/19024670
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
Avg Result: 230 mg/kg D.W.
Min LOD:
6.7 mg/kg D.W.
Max Result: 250 mg/kg D.W.
Page 3 of 16
5YS/rpflMiloMonfhlyOW 4126119 tj Printed: 12113119 14:31

IRON ICP Dry wt.
Sample Date Sample ID
11/01/19 DM1101/19022183
Result
44000 mg/kg D.W.
LOD
550
LOQ QA
2000
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
Flags 7, 1 MethGd Lab
SW846: 6010C MMSD
11/02/19
DM1102/19022194
45000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
11/03/19
DM1103/19022213
44000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
11/04/19
DM1104/19022226
47000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
43000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
11/06/19
DM1106/19022391
45000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
45000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
11/08/19
DM1108/19022948
45000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
45000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
11/10/19
DM1110/19022978
46000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
11/11/19
11/12/19
DM1111/19022991
DM1112/19023017
47000 mg/kg D.W.
47000 mg/kg D.W.
540
540
1900
2000
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/13/19
DM1113/19023033
51000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
11/14/19
DM1114119023645
59000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
52000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
11/16/19
DM1116/19023738
48000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
11/17/19
DM1117/19023757
48000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
11/18/19
DM1118119023770
48000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
11/19/19
DM1119/19023797
48000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
11/20/19
DM1120/19023964
51000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
11/21/19
DM1121/19023996
51000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
11/22/19
11/23/19
DM1122/19024012
DM1123/19024023
43000 mg/kg D.W.
50000 mg/kg D.W.
540
530
1900
1900
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/24/19
DM1124/19024220
48000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
11/25/19
DM1125/19024233
46000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
11/26/19
DM1126/19024576
45000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
11/27/19
DM1127/19024593
44000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
11/28/19
DM1128/19024644
45000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
11/29/19
11/30/19
DM1129/19024659
DM1130/19024670
46000 mg/kg D.W.
50000 mg/kg D.W.
540
540
1900
1900
SW846: 6010C
SW846: 6010C
MMSD
MMSD
Avg Result: 47000 mg/kg D.W.
Min LOD:
530 mg/kg D.W.
Max Result: 59000 mg/kg D.W.
Page 4 o/ 16
5Y5/rptlM11oMonth/YDW 4126119 0 Printed: 1211311914:31

� kl4SD
►AIMS IOt A CWAB B�NA[1tf
LEAD ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
.• Flags Analytical Method Lab
11/01/19
DMI101/19022183
51 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
11/02/19
DM1102/19022194
50 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
11/03/19
DM1103/19022213
45 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
11/04/19
DM1104/19022226
45 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
41 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
11/06/19
DM1106/19022391
40 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
39 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
11/08/19
DM1108/19022948
42 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
41 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
11/10/19
DM1110/19022978
41 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
11/11/19
11/12/19
DM1111/19022991
DM1112/19023017
40 mg/kg D.W.
39 mg/kg D.W.
2.9
2.9
8.8
8.8
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/13/19
DM1113/19023033
38 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
11/14/19
DM1114/19023645
39 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
35 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
11/16/19
DM1116/19023738
33 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
11/17/19
DM1117119023757
33 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
11/18/19
DM1118/19023770
33 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
11/19/19
DM1119/19023797
33 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
11/20/19
DM1120/19023964
44 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
11/21/19
DM1121/19023996
30 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
11/22/19
11/23/19
DM1122/19024012
DM1123/19024023
26 mg/kg D.W.
30 mg/kg D.W.
2.9
2.9
8.8
8.7
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/24/19
DM1124/19024220
31 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
11/25/19
DM1125/19024233
30 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
11/26/19
DM1126/19024576
35 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
11/27/19
DM1127/19024593
32 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
11/28/19
DM1128/19024644
36 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
11/29/19
11/30/19
DM1129/19024659
DM1130/19024670
33 mg/kg D.W.
33 mg/kg D.W.
2.9
2.9
8.7
8.8
SW846: 6010C
SW846: 6010C
MMSD
MMSD
Avg Result: 37 mg/kg D.W.
Min LOD: 2.9 mg/kg D.W.
Max Result: 51 mg/kg D.W.
Pane S o/1E
5YS1rptlM#oMonth1yDW 4126119 tj Printed: 121131191431

PIRVI ki f081 C11WR fvff iWY
MOLYBDENUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
11/01/19
DM1101/19022183
8.8 mg/kg D.W.
4.6
18
1.
SW846: 6010C
MMSD
11/02/19
DM1102/19022194
8.8 mg/kg D.W.
4.6
17
1
SW846: 6010C
MMSD
11/03/19
DM1103/19022213
9.4 mg/kg D.W.
4.6
17
1.
SW846: 6010C
MMSD
11/04/19
DM1104/19022226
9.5 mg/kg D.W.
4.6
18
1
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
8.6 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
11/06/19
DM1106119022391
8.8 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
8.4 mg/kg D.W.
4.4
17
1.
SW846: 6010C
MMSD
11/08/19
DM1108/19022948
9.3 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
9.6 mg/kg D.W.
4.5
17
1
SW846: 6010C
MMSD
11/10/19
DM1110/19022978
9.7 mg/kg D.W.
4.6
17
].
SW846: 6010C
MMSD
11/11/19
11/12/19
DM1111/19022991
DM1112/19023017
9.6 mg/kg D.W.
9.4 mg/kg D.W.
4.5
4.6
17
17
].
1.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/13/19
DM1113/19023033
9.8 mg/kg D.W.
4.5
17
J.
SW846: 6010C
MMSD
11/14/19
DM1114/19023645
9.9 mg/kg D.W.
4.5
17
3.
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
9.8 mg/kg D.W.
4.5
17
].
SW846: 6010C
MMSD
11/16/19
DM1116/19023738
9 mg/kg D.W.
4.6
17
1.
SW846: 6010C
MMSD
11/17/19
DM1117/19023757
9.4 mg/kg D.W.
4.5
17
].
SW846: 6010C
MMSD
11/18/19
DM1118/19023770
9.1 mg/kg D.W.
4.6
17
1.
SW846: 6010C
MMSD
11/19/19
DM1119/19023797
9.2 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
11/20/19
DM1120/19023964
10 mg/kg D.W.
4.6
17
1.
SW846: 6010C
MMSD
11/21/19
DM1121/19023996
13 mg/kg D.W.
4.5
17
1, Q3.
SW846: 6010C
MMSD
11/22/19
DM1122/19024012
8 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
11/23/19
DM1123/19024023
8.7 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
11/24/19
DM1124/19024220
8.6 mg/kg D.W.
4.5
17
J.
SW846: 6010C
MMSD
11/25/19
DM1125/19024233
8.8 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
11/26/19
DM1126/19024576
9.9 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
11/27/19
11/28/19
DM1127/19024593
DM1128/19024644
9.4 mg/kg D.W.
10 mg/kg D.W.
4.5
4.6
17
17
1.
1.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/29/19
DM1129/19024659
9.7 mg/kg D.W.
4.5
17
).
SW846: 6010C
MMSD
11/30/19
DM1130/19024670
9.7 mg/kg D.W.
4.5
17
1.
SW846: 6010C
MMSD
Avg Result: 9.4 mg/kg D.W.
Min LOD:
4.4 mg/kg D.W.
Max Result: 13 mg/kg D.W.
Page 6 of 16
5Y5/rptlM110M-th1YDW 4126119 U Printed.- 1211311914.31

F
NSD
swltau�ulet
NICKEL ICP Dry wt.
Sample Date Sample ID Result LOD LOQ
11/01/19 DM1101119022183 26 mg/kg D.W. 3.3 9.9
11/02/19 DM1102/19022194 26 mg/kg D.W. 3.3 9.8
11/03/19 DM1103/19022213 26 mg/kg D.W. 3.3 9.8
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
tags �nalyt!6�04k6
SW846: 6010C MMSD
SW846: 6010C MMSD
SW846: 6010C MMSD
11/04/19
DM1104/19022226
25 mg/kg D.W.
3.3
9.9
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
24 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
11/06/19
DM1106/19022391
24 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
24 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
11/08/19
DM1108119022948
26 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
26 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
11/10/19
DM1110/19022978
26 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
11/11/19
11/12/19
DM1111/19022991
DM1112/19023017
26 mg/kg D.W.
26 mg/kg D.W.
3.2
3.3
9.7
9.8
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/13/19
DM1113/19023033
26 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
11/14/19
DM1114/19023645
31 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
28 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
11/16/19
DM1116/19023738
26 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
11/17/19
DM1117/19023757
26 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
11/18/19
DM1118/19023770
27 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
11/19/19
DM1119/19023797
27 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
11/20/19
DM1120/19023964
28 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
11/21/19
DM1121/19023996
31 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
11/22/19
11/23/19
DM1122/19024012
DM1123/19024023
20 mg/kg D.W.
29 mg/kg D.W.
3.2
3.2
9.7
9.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/24/19
DM1124/19024220
28 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
11/25/19
DM1125/19024233
29 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
11/26/19
DM1126/19024576
28 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
11/27/19
DM1127/19024593
29 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
11/28/19
DM1128/19024644
29 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
11/29/19
DM1129/19024659
28 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
11/30/19
DM1130/19024670
28 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
Avg Result: 27 mg/kg D.W.
Min LOD:
3.2 mg/kg D.W.
Max Result: 31 mg/kg D.W.
Page 7 of 16
SYS/rptlMi/oMonth/yOW 4126119 tj Printed: 12113119 1431

f
kI4SD
01013WAMUR k,
PHOSPHORUS ICP Dry wt.
Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
.• Flags Analytical Method Lab
11/01/19
DM1101/19022183
23000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
11/02/19
DM1102/19022194
23000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/03/19
DM1103/19022213
23000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/04/19
DM1104/19022226
23000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
22000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/06/19
DM1106/19022391
23000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
11/08/19
DM1108/19022948
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
23000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/10/19
DM1110119022978
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/11/19
DM1111/19022991
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/12/19
DM1112/19023017
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/13/19
DM1113/19023033
25000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
11/14/19
DM1114/19023645
26000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
26000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/16/19
DM1116/19023738
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/17/19
DM1117/19023757
25000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/18/19
DM1118/19023770
25000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/19/19
DM1119/19023797
25000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/20/19
DM1120/19023964
26000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/21/19
DM1121119023996
25000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/22/19
DM1122/19024012
21000 mg/kg D.W.
24
91
Q2. SW846: 6010C
MMSD
11/23/19
DM1123/19024023
25000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/24/19
DM1124/19024220
25000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/25/19
DM1125/19024233
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/26/19
DM1126/19024576
24000 mg/kg D.W.
23
90
SW846: 6010C
MMSD
11/27/19
DM1127/19024593
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
11/28/19
DM1128/19024644
25000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/29/19
DM1129/19024659
25000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
11/30/19
DM1130/19024670
25000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
Avg Result: 24000 mg/kg D.W.
Min LOD:
23 mg/kg D.W.
Max Result: 26000 mg/kg D.W.
Page 8 of SE
SYS/iptlMAoMonth/yDW 4126119 tj Printed: 1211311914:31

Monthly Milorganite Report DW
NNSD
November 2019
�A CfUi� N'
Milorganite Daily Composite
POTASSIUM ICP Dry wt.
Date Sample ID Result LOD LOQ QA Flags Analytical Me hod Lab
11/01/19 DM1101/19022183 4700 mg/kg D.W. 300 890 SW846: 6010C MMSD
11/02/19 DM1102/19022194 5100 mg/kg D.W. 290 880 SW846: 6010C MMSD
11/03/19 DM1103/19022213 4800 mg/kg D.W. 290 880 SW846: 6010C MMSD
11/04/19
DM1104/19022226
4700 mg/kg D.W.
300
890
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
4400 mg/kg D.W.
290
880
SW846: 6010C
MMSD
11/06/19
DM1106/19022391
4100 mg/kg D.W.
290
870
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
4000 mg/kg D.W.
290
860
SW846: 6010C
MMSD
11/08/19
DM1108119022948
4100 mg/kg D.W.
290
870
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
3900 mg/kg D.W.
290
860
SW846: 6010C
MMSD
11/10/19
DM1110/19022978
3900 mg/kg D.W.
290
880
SW846: 6010C
MMSD
11/11/19
11/12/19
DM1111/19022991
DM1112119023017
3700 mg/kg D.W.
3800 mg/kg D.W.
290
290
880
880
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/13/19
DM1113/19023033
3500 mg/kg D.W.
290
860
SW846: 6010C
MMSD
11/14/19
DM1114119023645
3500 mg/kg D.W.
290
870
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
3800 mg/kg D.W.
290
870
SW846: 6010C
MMSD
11/16/19
DM1116/19023738
4000 mg/kg D.W.
290
880
Q2. SW846: 6010C
MMSD
11/17/19
DM1117/19023757
3700 mg/kg D.W.
290
870
SW846: 6010C
MMSD
11/18/19
DM1118/19023770
4000 mg/kg D.W.
290
880
SW846: 6010C
MMSD
11/19/19
DM1119/19023797
3700 mg/kg D.W.
290
870
SW846: 6010C
MMSD
11/20/19
DM1120/19023964
3600 mg/kg D.W.
290
880
SW846: 6010C
MMSD
11/21/19
DM1121/19023996
3300 mg/kg D.W.
290
870
SW846: 6010C
MMSD
11/22/19
11/23/19
DM1122/19024012
DM1123/19024023
3200 mg/kg D.W.
4900 mg/kg D.W.
290
290
880
870
Q2. SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/24/19
11/25/19
11/26/19
11/27/19
DM1124/19024220
DM1125/19024233
DM1126/19024576
DM1127/19024593
4800 mg/kg D.W.
5000 mg/kg D.W.
4400 mg/kg D.W.
4100 mg/kg D.W.
290
290
290
290
870
870
860
870
SW846: 6010C
Q2. SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
11/28/19
DM1128/19024644
4700 mg/kg D.W.
290
880
SW846: 6010C
MMSD
11/29/19
DM1129/19024659
4600 mg/kg D.W.
290
870
SW846: 6010C
MMSD
11/30/19
DM1130/19024670
4000 mg/kg D.W.
290
880
SW846: 6010C
MMSD
Avg Result: 4100 mg/kg D.W.
Min LOD:
290 mg/kg
D.W.
Max Result: 5100 mg/kg D.W.
Page 9 of le
SYS/rptlMiloMonthlyDW 4126119 tj Printed: 1211311914:31

r
1 k14$D
mmmiciflOmmm
SELENIUM ICP Dry wt.
�Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
11/01/19
DM1101/19022183
5 mg/kg D.W.
4.3
13
3.
SW846: 6010C
MMSD
11/02/19
DM1102/19022194
5.5 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
11/03/19
DM1103/19022213
5.2 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
11/04/19
DM1104/19022226
6.1 mg/kg D.W.
4.3
13
J.
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/06/19
DM1106119022391
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
11/08/19
DM1108/19022948
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/10/19
DM1110/19022978
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/11/19
11/12/19
DM1111/19022991
DM1112/19023017
< 4.2 mg/kg D.W.
< 4.2 mg/kg D.W.
4.2
4.2
13
13
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/13/19
DM1113119023033
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
11/14/19
DM1114/19023645
11 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/16/19
DM1116119023738
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/17/19
DM1117/19023757
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/18/19
DM1118/19023770
4.6 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
11/19/19
DM1119/19023797
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/20/19
DM1120/19023964
5.5 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
11/21/19
DM1121/19023996
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/22/19
DM1122/19024012
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/23/19
DM1123/19024023
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/24/19
DM1124/19024220
4.3 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
11/25/19
DM1125/19024233
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
11/26/19
DM1126/19024576
6.3 mg/kg D.W.
4.2
13
3, Q2.
SW846: 6010C
MMSD
11/27/19
DM1127/19024593
4.7 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
11/28/19
DM1128/19024644
11 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
11/29/19
DM1129119024659
9.8 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
11/30/19
DM1130/19024670
9.3 mg/kg D.W.
4.2
13
3.
SW846: 6010C
MMSD
Avg Result: 2.9 mg/kg D.W.
Min LOD:
4.1 mg/kg D.W.
Max Result: 11 mg/kg D.W.
Page 10 of 16
SY51rpt1MiloMonddyDW 4126119 h Prin[ed.-1211311914:31

i'%
i D
0tRttM ILIA / C1€ 1 MBIt
Solids (% Moisture)
1� Sample ID
11/01/19 DM1101/19022183
11/02/19 DM1102/19022194
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
►, LOQ QA Flags Analytical Method Lab
8.9 % 0.1 SM 2540 G (1997) MMSD
8.1 % 0.1 SM 2540 G (1997) MMSD
11/03/19
DM1103/19022213
8.2 %
0.1
SM 2540 G (1997)
MMSD
11/04/19
DM1104/19022226
8.9 %
0.1
SM 2540 G (1997)
MMSD
11/05/19
11/06/19
11/07/19
DM1105/19022376
DM1106/19022391
DM1107/19022933
7.6 %
6.5 %
5.7 %
0.1
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
MMSD
11/08/19
11/09/19
DM1108/19022948
DM1109/19022959
6.8 %
6.4 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
11/10/19
DM1110/19022978
7.9 %
0.1
SM 2540 G (1997)
MMSD
11/11/19
11/12/19
DM1111/19022991
DM1112/19023017
7.6 %
8.2 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
11/13/19
DM1113/19023033
6 %
0.1
SM 2540 G (1997)
MMSD
11/14/19
DM1114/19023645
6.6 %
0.1
SM 2540 G (1997)
MMSD
11/15/19
DM1115119023660
6.8 %
0.1
SM 2540 G (1997)
MMSD
11/16/19
DM1116/19023738
8.1 %
0.1
SM 2540 G (1997)
MMSD
11/17/19
DM1117/19023757
6.9 %
0.1
SM 2540 G (1997)
MMSD
11/18/19
11/19/19
DM1118/19023770
DM1119/19023797
8 %
7.3 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
11/20/19
DM1120/19023964
8 %
0.1
SM 2540 G (1997)
MMSD
11/21/19
DM1121/19023996
7.3 %
0.1
SM 2540 G (1997)
MMSD
11/22/19
11/23/19
DM1122/19024012
DM1123/19024023
7.6 %
6.5 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
11/24/19
DM1124/19024220
7.2 %
0.1
SM 2540 G (1997)
MMSD
11/25/19
DM1125/19024233
7.2 %
0.1
SM 2540 G (1997)
MMSD
11/26/19
DM1126/19024576
6.3 %
0.1
SM 2540 G (1997)
MMSD
11/27/19
DM1127/19024593
6.5 %
0.1
SM 2540 G (1997)
MMSD
11/28/19
DM1128/19024644
7.7 %
0.1
SM 2540 G (1997)
MMSD
11/29/19
DM1129/19024659
7.3 %
0.1
SM 2540 G (1997)
MMSD
11/30/19
DM1130/19024670
7.7 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 7.3 %
Min LOD:
0.1 °/n
Max Result: 8.9
Page 11 of 16
5Y5/rptl MiloMonthlyDW 4126119 tj Printed: 12113119 14:31

tkt4SD
POMINA M
ZINC ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
November 2019
Milorganite Daily Composite
.. Flags Analytical Method Lab
11/01/19
DM1101/19022183
450 mg/kg D.W.
19
56
SW846: 6010C
MMSD
11/02/19
DM1102/19022194
440 mg/kg D.W.
18
56
SW846: 6010C
MMSD
11/03/19
DM1103/19022213
430 mg/kg D.W.
18
56
SW846: 6010C
MMSD
11/04/19
DM1104/19022226
430 mg/kg D.W.
19
56
SW846: 6010C
MMSD
11/05/19
DM1105/19022376
400 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/06/19
DM1106/19022391
420 mg/kg D.W.
18
54
SW846: 6010C
MMSD
11/07/19
DM1107/19022933
420 mg/kg D.W.
18
54
SW846: 6010C
MMSD
11/08/19
DM1108/19022948
460 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
450 mg/kg D.W.
18
54
SW846: 6010C
MMSD
11/10/19
DM1110/19022978
460 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/11/19
11/12/19
DM1111/19022991
DM1112/19023017
460 mg/kg D.W.
440 mg/kg D.W.
18
18
55
56
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/13/19
DM1113/19023033
460 mg/kg D.W.
18
54
SW846: 6010C
MMSD
11/14/19
DM1114/19023645
480 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/15/19
DM1115/19023660
460 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/16/19
DM1116/19023738
430 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/17/19
DM1117/19023757
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/18/19
DM1118/19023770
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/19/19
DM1119/19023797
430 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/20/19
DM1120/19023964
470 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/21/19
DM1121/19023996
430 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/22/19
DM1122/19024012
350 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/23/19
DM1123/19024023
450 mg/kg D.W.
18
54
SW846: 6010C
MMSD
11/24/19
DM1124/19024220
450 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/25/19
DM1125/19024233
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/26/19
DM1126/19024576
450 mg/kg D.W.
18
54
SW846: 6010C
MMSD
11/27/19
DM1127/19024593
420 mg/kg D.W.
18
54
SW846: 6010C
MMSD
11/28/19
DM1128/19024644
430 mg/kg D.W.
18
55
SW846: 6010C
MMSD
11/29/19
11/30/19
DM1129/19024659
DM1130/19024670
430 mg/kg D.W.
440 mg/kg D.W.
18
18
55
55
SW846: 6010C
SW846: 6010C
MMSD
MMSD
Avg Result: 440 mg/kg D.W.
Min LOD:
18 mg/kg D.W.
Max Result: 480 mg/kg D.W.
Page 11 of 1E
SY51W1Mi1oMonth/yDW 41261190 Printed.1211311914:31

Monthly Milorganite Report DW
i ^
iNSD
November 2019
MA CIEM
Milorganite Daily Composite
Phosphorus - Total % DW (Calc.)
Date Sample ID
0
.�
,.
11/01/19 DM1101/19022183
2.3 % D.W.
0.1
0.1
SW846: 6010C MMSD
11/02/19 DM1102/19022194
2.3 % D.W.
0.1
0.1
SW846: 6010C MMSD
11/03/19 DM1103/19022213
2.3 % D.W.
0.1
0.1
SW846: 6010C MMSD
11/04/19 DM1104/19022226
2.3 % D.W.
0.1
0.1
SW846: 6010C MMSD
11/05/19 DM1105119022376
2.2 % D.W.
0.1
0.1
SW846: 6010C MMSD
11/06/19 DM1106/19022391
2.3%D.W.
0.1
0.1
SW846: 6010C MMSD
11/07/19 DM1107/19022933
2.3%D.W.
0.1
0.1
SW846: 6010C MMSD
11/08/19
DM1108/19022948
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/09/19
DM1109/19022959
2.3%D.W.
0.1
0.1
SW846: 6010C
MMSD
11/10/19
DM1110119022978
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/11/19
DM1111/19022991
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/12/19
DM1112/19023017
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/13/19
DM1113/19023033
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/14/19
11/15/19
DM1114/19023645
DM1115/19023660
2.6 % D.W.
2.6 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/16/19
DM1116/19023738
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/17/19
DM1117/19023757
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/18/19
DM1118/19023770
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/19/19
DM1119/19023797
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/20/19
DM1120/19023964
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/21/19
DM1121/19023996
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/22/19
11/23/19
DM1122/19024012
DM1123/19024023
2.1 % D.W.
2.5 % D.W.
0.1
0.1
0.1
0.1
Q2. SW846: 6010C
SW846: 6010C
MMSD
MMSD
11/24/19
DM1124/19024220
2.5%D.W.
0.1
0.1
SW846: 6010C
MMSD
11/25/19
DM1125/19024233
2.4%D.W.
0.1
0.1
SW846: 6010C
MMSD
11/26/19
DM1126/19024576
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/27/19
DM1127/19024593
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
11/28/19
DM1128/19024644
2.5%D.W.
0.1
0.1
SW846: 6010C
MMSD
11/29/19
DM1129/19024659
2.5%D.W.
0.1
0.1
SW846: 6010C
MMSD
11/30/19
DM1130/19024670
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
Avg Result: 2.4 0/a D.W.
ALUMINUM ICP Dry wt.
..
Min LOD: 0.1 % D.W.
.,
LOQ
Max Result: 2.6 % D.W.
Milorganite Weekly Composite
QA Flags Anaiiyilcaiketh6dLab
11/09/19
WMC45/19023019
5000 mg/kg D.W.
57
200
B8. SW846: 6010C
MMSD
Avg Result: 5000 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Date Sample ID
Min LOD: 57 mg/kg D.W.
Result LOD LOQ
QA Flags Analytical Method
Lab
11/09/19
WMC45/19023019
0.2 %
0.11
0.37
AOAC (13) 2.065
MMSD
Avg Result: 0.2 %
Min LOD: 0.11 %
page 13 of le
SYS/rpt1Mi1vMonth/y0W 4126119 tj Printed.• 12/13/1914.31

Monthly Mllorganite Report DW
14SD
November 2019
Fllt A tlf�
Milorganite Weekly Composite
BORON ICP Dry wt.
�.mple Date Sample ID
Result
LOD
LOQ QA
Flags Analytical Method
Lab i
11/09/19 WMC45119023019
20 mg/kg D.W.
1.2
3.8
SW846: 6010C
Cr Lab
Avg Result: 20 mg/kg D.W.
Min LOD:
1.2 mg/kg D.W.
CHROMIUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
Flaps Analytical Method
Lab
11/09/19 WMC45/19023019
180 mg/kg D.W.
1.6
4.8
SW846: 6010C
MMSD
Avg Result: 180 mg/kg D.W.
Min LOD:
1.6 mg/kg D.W.
COBALT ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ QA
Flags Analytical Method
Lab
11/09/19 WMC45/19023019
1.9 mg/kg D.W.
0.28
1.1
B8. SW846: 6010C
MMSD
Avg Result: 1.9 mg/kg D.W.
Min LOD:
0.28 mg/kg D.W.
MERCURY by M. 7471 (sludge)
Sample Date Sample ID
Result
LOD
LOQ ••
Flags Analytical Method
Lab
11/02/19 WMC44/19022228
0.14 mg/kg D.W.
0.014
0.049
EPA 7471E
Cr Lab
11/09/19 WMC45/19023019
0.31 mg/kg D.W.
0.015
0.05
EPA 7471E
Cr Lab
11/16/19 WMC46/19023799
0.28 mg/kg D.W.
0.014
0.047
EPA 7471B
CT Lab
11/23/19 WMC47/19024235
0.29 mg/kg O.W.
0.022
0.072
EPA 7471
Pace -GB
11/30/19 WMC48/19024704
0.21 mg/kg D.W.
0.024
0.079
EPA 7471
Pace -GB
Avg Result: 0.25 mg/kg D.W.
Min LOD:
0.014 mg/kg D.W.
Max Result: 0.31 mg/kg D.W.
NITRATE NITROGEN
Sample Date Sample ID
Result
LOD
LOQ ••
Flags Analytical Method
Lab
11/09/19 WMC45/19023019
0.95 %
0.5
AOAC (16) 930.01
MMSD
Avg Result: 0.95 "/o
Min LOD:
0.5 %
NITROGEN-Total(Manual)
Sample Date Sample ID
Result
LOD
LOQ QA
Flags Analytical Method
Lab
11/09/19 WMC45/19023019
5.8 %
0.11
AOAC (16) 955.04
MMSD
Avg Result: 5.8 "/o
Min LOD:
0.11
NITROGEN -Water Insoluble
Sample Date Sample ID
Result
LOD
LOQ .•
Flags Analyti al Method
Lab
11/09/19 WMC45/19023019
4.4 %
0.5
AOAC (16) 945.01
MMSD
Avg Result: 4.4 %
Min LOD:
0.5
pH -Solids
Sample Date Sample ID
Result
LOD
LOQ QA
Flags Analytical Method
Lab
11/02/19 WMC44/19022228
6.22 Stnd. Units
0.1
SW846: 9045D
MMSD
11/09/19 WMC45/19023019
6.4 Stnd. Units
0.1
SW846: 9045D
MMSD
11/16/19 WMC46/19023799
6.54 Stnd. Units
0.1
SW846: 9045D
MMSD
11/23/19 WMC47/19024235
6.45 Stnd. Units
0.1
SW846: 9045D
MMSD
11/30/19 WMC48/19024704
6.42 Stnd. Units
0.1
SW846: 9045D
MMSD
Avg Result: 6.4 Stnd. Units
Min LOD:
0.1 Stnd. Units
Max Result: 6.54 Stnd. Units
Page 14 of 1E
5Y5/rpt1MdoMonth/yDW 4126119 tj Vnnted: 1211311914:31

"
iffl$D
PUTMIRA111=10111111111iff
Monthly Milorganite Report DW
November 2019
Milorganite Weekly Composite
Solids (% Moisture)
Date Sample ID Result LOD LOQ
11/02/19 WMC44/19022228 7.4 % 0.1 SM 2540 G (1997) MMSD
11/09/19 WMC45/19023019 7.1 % 0.1 SM 2540 G (1997) MMSD
11/16/19 WMC46/19023799 7.2 % 0.1 SM 2540 G (1997) MMSD
11/23/19 WMC47/19024235 7.3 % 0.1 SM 2540 G (1997) MMSD
11/30/19 WMC48/19024704 7.3 % 0.1 SM 2540 G (1997) MMSD
Min LOD: 0.1 %
Solids (% Volatile)
'Sample Sample ID Result LOD LOQ QA Flags Analytical Method Lab
11/09/19 WMC45/19023019 70 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 70 % Min LOD: 0.1 %
Solids (% Total)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
11/09/19 WMC45/19023019 93 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 93 % Min LOD: 0.1 %
FECAL COLIFORM SLUDGE
Date Sample
mpl6
11/05/19
16
19024612
11/12/19
19025081
11/19/19
19025549
11/26/19
19025878
Solids (% Total)
Milorganite (Outfall 006) PRODUCTION
Result LOD LOQ QA Flags Analytical Method Lab
0.21 MPN/g TS 0.19
< 0.2 MPN/g TS 0.2 Q3.
0.99 MPN/g TS 0.19
Min LOD: 0.19 MPN/g TS
EPA 1680 MMSD
EPA 1680 MMSD
EPA 1680 MMSD
lawi
.. ..
11/05/19
19024612
92 %
0.1
SM 2540 G (1997)
MMSD
11/12/19
19025081
94 %
0.1
SM 2540 G (1997)
MMSD
11/19/19
19025549
91 %
0.1
SM 2540 G (1997)
MMSD
11/26/19
19025878
94 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 93 % Min LOD: 0.1 % Max Result: 94 %
Milorganite (Outfall 009) BAGGING
FECAL COLIFORM SLUDGE
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
11/12/19 19025083 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
Page 15 of 16
SYS/rptlMdoMonth/yOW 4126119 t% Primed.- LZ4311914:31

Monthly Milorganite Report DW
� ANSD November 2019
�ttiA�S �t I t1�t
Milorganite (Outfall 009) BAGGING
Solids (% Total)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
11/12/19 19025083 93 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 93 % Min LOD: 0.1
Milorganite (Outfall 008) SHIPPING
FECAL COLIFORM SLUDGE
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
11/12/19 19025082 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
Solids (% Total)
Sample Date Sample ID Result .► LOQ .• Flags
11/12/19 19025082 93 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 93 Wo Min LOD: 0.1
AO Other -- Flag requires additional explanation
AX Qualified data - see contract laboratory report
B3 Target analyte detected in method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits.
68 LCS recovery was below control limits.
89 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
Di Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
H1 Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
SYS1rpt1Mi/oMonth/yDW 4126119 tj
IS Insufficient sample volume for analysis.
7 Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
LA Not analyzed - laboratory accident.
M3 Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
MS Incubator/water bath temperature was outside method
M7 Microbiology sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
S5 Reading was not confirmed by a constant weight measurement
SD Supplemental details provided.(Water Quality only.)
T3 The Boo dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA Boo was below method acceptance criteria.
TS GGA Boo was above method acceptance criteria.
T7 The Boo dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample is outside of the prescribed method temperature range.
Page 16 of le
Printed: 12113/1914:31

S
PARTNERS FOR A CLEANER ENVIRONMENT
January 15, 2020
r
TO: Brett Kelly, Todd Schwingle, Dion Doege, Jacob Holbert, and Sam Lieven
FROM: Zach Vogel
Laboratory Project Manager
COPY: Richard Vincent, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom Nowicki, Beth
Stroik, Kim Walden, Kod Kenney, Ethan Guyant, Lab File
SUBJECT: Milorganite Monthly Data — December 2019
Attached is the MMSD Central Lab analytical report for Milorganite data for the month of December
2019. The boron and mercury analyses were performed by Pace Analytical Services, Inc. in Green Bay,
Wisconsin (Wisconsin Certification #: 405132750). All other analyses were performed by Milwaukee
Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP
Certification #: E571010).
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Thank you.
Data Review By:
Rich Vincent Date
Laboratory Supervisor
Data/Report Review By:
)- is- zc"-©
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

r
NDDecember
�uni�alsw��a�
ARSENIC ICP Dry wt.
:Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
12/01/19
DM1201/19024689
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
12/02/19
DM1202/19024702
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/03/19
DM1203/19024954
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/04/19
DM1204/19024993
< 18 mg/kg D.W.
18
70
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
< 18 mg/kg D.W.
18
70
SW846: 6010C
MMSD
12/06/19
DM1206/19025234
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/08/19
DM1208/19025264
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
12/09/19
DM1209/19025277
< 17 mg/kg D.W.
17
69
Q3.
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/11/19
DM1211/19025319
< 17 mg/kg D.W.
17
69
Q3.
SW846: 6010C
MMSD
12/12/19
12/13/19
DM1212/19025430
DM1213/19025517
< 17 mg/kg D.W.
< 17 mg/kg D.W.
17
17
70
70
D2, Q3.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/14/19
DM1214/19025528
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
12/15/19
DM1215/19025755
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/16/19
DM1216/19025768
< 17 mg/kg D.W.
17
68
SW846: 6010C
MMSD
12/17/19
DM1217/19025795
< 17 mg/kg D.W.
17
70
Q3.
SW846: 6010C
MMSD
12/18/19
DM1218/19026149
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/19/19
DM1219/19026252
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/20/19
DM1220/19026263
< 18 mg/kg D.W.
18
71
SW846: 6010C
MMSD
12/21/19
DM1221/19026282
< 18 mg/kg D.W.
18
70
SW846: 6010C
MMSD
12/22/19
DM1222/19026295
< 18 mg/kg D.W.
18
70
Q2.
SW846: 6010C
MMSD
12/23/19
DM1223/19026332
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
12/24/19
DM1224/19026436
< 18 mg/kg D.W.
18
70
SW846: 6010C
MMSD
12/25/19
DM1225/19026455
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/26/19
DM1226/19026470
< 17 mg/kg D.W.
17
70
Q3.
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
< 17 mg/kg D.W.
17
70
SW846: 6010C
MMSD
12/28/19
DM1228119026500
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/29/19
DM1229/19026513
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/30/19
DM1230/19026556
< 17 mg/kg D.W.
17
69
SW846: 6010C
MMSD
12/31/19 .
DM1231/19026567
< 17 mg/kg D.W.
17
67
SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
17 mg/kg D.W.
Page I of 16
5Y51rpt1MVoMonth/yOW 4124119 tj Printed.- 111512010.25

NSD
FRACI t
CADMIUM ICP Dry wt.
.. , • •• ••
12/01/19 DM1201/19024689 < 0.95 mg/kg D.W. 0.95 3.6
12/02/19 DM1202/19024702 < 0.94 mg/kg D.W. 0.94 3.6
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
SW846: 6010C MMSD
SW846: 6010C MMSD
12/03/19
DM1203/19024954
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
12/04/19
DM1204/19024993
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
12/06/19
DM1206/19025234
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
12/08/19
DM1208/19025264
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
12/09/19
DM1209/19025277
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
12/11/19
12/12/19
DM1211/19025319
DM1212/19025430
< 0.94 mg/kg D.W.
< 0.95 mg/kg D.W.
0.94
0.95
3.6
3.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/13/19
DM1213/19025517
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
12/14/19
DM1214/19025528
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
12/15/19
DM1215/19025755
< 0.94 mg/kg D.W.
0.94
3.5
SW846: 6010C
MMSD
12/16/19
DM1216/19025768
< 0.93 mg/kg D.W.
0.93
3.5
SW846: 6010C
MMSD
12/17/19
DM1217/19025795
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
12/18/19
DM1218/19026149
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
12/19/19
DM1219/19026252
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
12/20/19
12/21/19
DM1220/19026263
DM1221/19026282
< 0.96 mg/kg D.W.
< 0.95 mg/kg D.W.
0.96
0.95
3.6
3.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/22/19
12/23/19
DM1222/19026295
DM1223/19026332
< 0.95 mg/kg D.W.
< 0.94 mg/kg D.W.
0.95
0.94
3.6 Q2.
3.6
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/24/19
DM1224/19026436
< 0.96 mg/kg D.W.
0.96
3.6
SW846: 6010C
MMSD
12/25/19
DM1225/19026455
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
12/26/19
DM1226/19026470
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
< 0.95 mg/kg D.W.
0.95
3.6
SW846: 6010C
MMSD
12/28/19
DM1228/19026500
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
12/29/19
DM1229/19026513
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
12/30/19
DM1230/19026556
< 0.94 mg/kg D.W.
0.94
3.6
SW846: 6010C
MMSD
12/31/19
DM1231/19026567
< 0.92 mg/kg D.W.
0.92
3.5
SW846: 6010C
MMSD
Avg Result: 0 mg/kg D.W.
Min LOD:
0.92 mg/kg
D.W.
SYS1rpt1Mi16Month1yDW 4126119 tj
Page 2 of lE
Printed: 1/1512010:15

�tAtI316!/<Ct�iBt
COPPER ICP Dry wt.
Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
12/01/19
DM1201/19024689
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/02/19
DM1202/19024702
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/03/19
DM1203/19024954
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/04/19
DM1204119024993
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
12/06/19
DM1206119025234
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/08/19
DM1208/19025264
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
12/09/19
DM1209/19025277
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
240 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/11/19
12/12/19
DM1211119025319
DM1212/19025430
240 mg/kg D.W.
240 mg/kg D.W.
6.8
6.8
26
26
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/13/19
DM1213/19025517
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/14/19
DM1214/19025528
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/15/19
DM1215/19025755
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/16/19
DM1216/19025768
230 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
12/17/19
DM1217/19025795
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
12/18/19
DM1218/19026149
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/19/19
DM1219/19026252
210 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/20/19
DM1220/19026263
230 mg/kg D.W.
7
27
SW846: 6010C
MMSD
12/21/19
DM1221/19026282
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
12/22/19
DM1222/19026295
220 mg/kg D.W.
6.9
26
Q2. SW846: 6010C
MMSD
12/23/19
DM1223/19026332
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/24/19
DM1224/19026436
220 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
12/25/19
DM1225/19026455
220 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/26/19
DM1226/19026470
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
240 mg/kg D.W.
6.9
26
SW846: 6010C
MMSD
12/28/19
DM1228/19026500
240 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/29/19
DM1229/19026513
230 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/30/19
DM1230/19026556
240 mg/kg D.W.
6.8
26
SW846: 6010C
MMSD
12/31/19
DM1231/19026567
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
Avg Result: 220 mg/kg D.W.
Min LOD:
6.6 mg/kg D.W.
Max Result: 240 mg/kg D.W.
Page 3 of It
SYS1rptlM11aMonth/yDW 4126119 tj Pnnted.' 111512010:15

tiffl$D
NRtw wt d t1[M F 3 wfwl
IRON ICP Dry wt.
Sample Date Sample ID
12/01/19 DM1201/19024689
Result
51000 mg/kg D.W.
LOD
540
LOQ QA
2000
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
Flags I Method Lab
SW846: 6010C MMSD
12/02/19
DM1202/19024702
50000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
12/03/19
DM1203/19024954
50000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
12/04/19
DM1204/19024993
49000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
45000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
12/06/19
DM1206/19025234
47000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
46000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
12/08/19
DM1208/19025264
42000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
12/09/19
DM1209/19025277
45000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
45000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
12/11/19
12/12/19
DM1211/19025319
DM1212/19025430
46000 mg/kg D.W.
45000 mg/kg D.W.
540
540
1900
2000
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/13/19
DM1213119025517
47000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
12/14/19
DM1214/19025528
42000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
12/15/19
DM1215/19025755
44000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
12/16/19
DM1216/19025768
44000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
12/17/19
DM1217/19025795
42000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
12/18/19
DM1218/19026149
41000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
12/19/19
DM1219/19026252
40000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
12/20/19
DM1220119026263
45000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
12/21/19
DM1221/19026282
45000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
12/22/19
12/23/19
DM1222/19026295
DM1223/19026332
46000 mg/kg D.W.
43000 mg/kg D.W.
550
540
2000
2000
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/24/19
DM1224/19026436
41000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
12/25/19
DM1225/19026455
40000 mg/kg D.W.540
2000
SW846: 6010C
MMSD
12/26/19
DM1226/19026470
45000 mg/kg D.W.
540
2000
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
48000 mg/kg D.W.
550
2000
SW846: 6010C
MMSD
12/28/19
DM1228/19026500
48000 mg/kg D.W.
540
1900
SW846: 6010C
MMSD
12/29/19
12/30/19
DM1229119026513
DM1230/19026556
47000 mg/kg D.W.
44000 mg/kg D.W.
540
540
2000
1900
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/31/19
DM1231/19026567
43000 mg/kg D.W.
530
1900
SW846: 6010C
MMSD
Avg Result: 45000 mg/kg D.W.
Min LOD:
530 mg/kg D.W.
Max Result: 51000 mg/kg D.W.
Page 4 ofle
5Y51rptIM1/oMonth1yDW 4126119 tj Pnnted:111512010.25

kI4SD
15 f@t a rIgo
LEAD ICP Dry wt.
sa�fnpl�6ate- �--Sa-mwielm
Result
LOD
LOQ
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
12/01/19
DM1201/19024689
34 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/02/19
DM1202/19024702
34 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/03/19
DM1203/19024954
34 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/04/19
DM1204/19024993
37 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
32 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
12/06/19
DM1206/19025234
32 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
34 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
12/08/19
DM1208/19025264
34 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/09/19
DM1209/19025277
36 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
33 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
12/11/19
DM1211/19025319
34 mg/kg D.W.
2.9
8.7
MMSD
12/12/19
DM1212/19025430
33 mg/kg D.W.
2.9
8.8
_____________SW846-.6010C
SW846: 6010C
MMSD
12/13/19
DM1213/19025517
32 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/14/19
DM1214/19025528
29 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/15/19
DM1215/19025755
30 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
12/16/19
DM1216/19025768
30 mg/kg D.W.
2.9
8.6
SW846: 6010C
MMSD
12/17/19
DM1217/19025795
31 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/18/19
DM1218/19026149
33 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/19/19
DM1219/19026252
27 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
12/20/19
DM1220/19026263
26 mg/kg D.W.
3
9
SW846: 6010C
MMSD
12/21/19
DM1221/19026282
26 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
12/22/19
12/23/19
DM1222/19026295
DM1223/19026332
26 mg/kg D.W.
26 mg/kg D.W.
3
2.9
8.9
8.8
Q2. SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/24/19
DM1224/19026436
28 mg/kg D.W.
3
8.9
SW846: 6010C
MMSD
12/25/19
DM1225/19026455
27 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/26/19
DM1226/19026470
28 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
30 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/28/19
DM1228/19026500
28 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
12/29/19
DM1229/19026513
29 mg/kg D.W.
2.9
8.8
SW846: 6010C
MMSD
12/30/19
DM1230/19026556
30 mg/kg D.W.
2.9
8.7
SW846: 6010C
MMSD
12/31/19
DM1231/19026567
32 mg/kg D.W.
2.8
8.5
SW846: 6010C
MMSD
Avg Result: 31 mg/kg D.W.
Min LOD:
2.8 mg/kg D.W.
Max Result: 37 mg/kg D.W.
Page 5 of lE
5Y51rptlM11oMonth/yDW 4126119 tj Printed.- 111512010.25

SD
011W totA CILIM BMIAtM'
MOLYBDENUM ICP Dry wt.
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
12/01/19
DM1201/19024689
10 mg/kg D.W.
4.6
17
J.
SW846: 6010C
MMSD
12/02/19
DM1202/19024702
9.8 mg/kg D.W.
4.6
17
J.
SW846: 6010C
MMSD
12/03/19
DM1203/19024954
8.6 mg/kg D.W.
4.5
17
J.
SW846: 6010C
MMSD
12/04/19
DM1204/19024993
9.9 mg/kg D.W.
4.6
18
J.
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
9.2 mg/kg D.W.
4.6
18
J.
SW846: 6010C
MMSD
12/06/19
DM1206/19025234
9.5 mg/kg D.W.
4.5
17
J.
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
9.2 mg/kg D.W.
4.5
17
J.
SW846: 6010C
MMSD
12/08/19
DM1208/19025264
9 mg/kg D.W.
4.6
17
J.
SW846: 6010C
MMSD
12/09/19
DM1209/19025277
9.3 mg/kg D.W.
4.5
17
J.
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
8.8 mg/kg D.W.
4.5
17
J.
SW846: 6010C
MMSD
12/11/19
12/12/19
DM1211119025319
DM1212/19025430
9.1 mg/kg D.W.
9.2 mg/kg D.W.
4.5
4.6
17
17
J.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/13/19
DM1213/19025517
8.5 mg/kg D.W.
4.6
17
J.
SW846: 6010C
MMSD
12/14/19
12/15/19
12/16/19
DM1214/19025528
DM1215/19025755
DM1216/19025768
8 mg/kg D.W.
8.4 mg/kg D.W.
8.5 mg/kg D.W.
4.6
4.5
4.5
17
17
17
J.
J.
J.
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
12/17/19
12/18/19
12/19/19
12/20/19
OM1217119025795
DM1218/19026149
DM1219/19026252
DM1220/19026263
8.9 mg/kg D.W.
9.3 mg/kg D.W.
8.6 mg/kg D.W.
9.2 mg/kg D.W.
4.6
4.6
4.5
4.6
17
17
17
18
J.
J.
J.
J.
SW846: 6010C
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
MMSD
12/21/19
DM1221/19026282
9 mg/kg D.W.
4.6
18
J.
SW846: 6010C
MMSD
12/22/19
12/23/19
12/24/19
DM1222/19026295
DM1223/19026332
DM1224/19026436
9.4 mg/kg D.W.
9 mg/kg D.W.
9.1 mg/kg D.W.
4.6
4.6
4.6
18
17
18
J, Q2.
J.
J.
SW846: 6010C
SW846: 6010C
SW846: 6010C
MMSD
MMSD
MMSD
12/25/19
DM1225/19026455
9.1 mg/kg D.W.
4.6
17
J.
SW846: 6010C
MMSD
12/26/19
DM1226119026470
9.6 mg/kg D.W.
4.6
17
J.
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
9.6 mg/kg D.W.
4.6
17
J.
SW846: 6010C
MMSD
12/28/19
DM1228/19026500
9.8 mg/kg D.W.
4.5
17
J.
SW846: 6010C
MMSD
12/29/19
DM1229/19026513
9.7 mg/kg D.W.
4.6
17
J.
SW846: 6010C
MMSD
12/30/19
DM1230/19026556
9.6 mg/kg D.W.
4.5
17
J.
SW846: 6010C
MMSD
12/31/19
DM1231/19026567
9.4 mg/kg D.W.
4.4
17
J.
SW846: 6010C
MMSD
Avg Result: 9.2 mg/kg D.W.
Min LOD:
4.4 mg/kg D.W.
Max Result: 10 mg/kg D.W.
Page 6 of 16
SYS/rotlMiloMonth/yDW 4126119 tj Printed., 1115120 10:25

n
E
D
WWRIAMMMMM
NICKEL ICP Dry wt.
'Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
12/01/19
DM1201/19024689
28 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
12/02/19
DM1202/19024702
28 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
12/03/19
DM1203/19024954
27 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
12/04/19
DM1204/19024993
27 mg/kg D.W.
3.3
9.9
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
22 mg/kg D.W.
3.3
9.9
SW846: 6010C
MMSD
12/06/19
DM1206/19025234
22 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
24 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
12/08/19
DM1208/19025264
23 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
12/09/19
DM1209119025277
23 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
26 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
12/11/19
12/12/19
DM1211/19025319
DM1212119025430
22 mg/kg D.W.
22 mg/kg D.W.
3.2
3.3
9.7
9.8
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/13/19
DM1213119025517
27 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
12/14/19
DM1214/19025528
25 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
12/15/19
DM1215/19025755
26 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
12/16/19
DM1216/19025768
27 mg/kg D.W.
3.2
9.6
SW846: 6010C
MMSD
12/17/19
DM1217/19025795
22 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
12/18/19
DM1218/19026149
23 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
12/19/19
DM1219/19026252
21 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
12/20/19
DM1220119026263
21 mg/kg D.W.
3.3
10
SW846: 6010C
MMSD
12/21/19
DM1221/19026282
20 mg/kg D.W.
3.3
9.9
SW846: 6010C
MMSD
12/22/19
DM1222/19026295
21 mg/kg D.W.
3.3
9.9
Q2. SW846: 6010C
MMSD
12/23/19
DM1223/19026332
20 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
12/24/19
DM1224/19026436
21 mg/kg D.W.
3.3
9.9
SW846: 6010C
MMSD
12/25/19
DM1225/19026455
21 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
12/26/19
DM1226/19026470
22 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
23 mg/kg D.W.
3.3
9.8
SW846: 6010C
MMSD
12/28/19
DM1228119026500
23 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
12/29/19
DM1229/19026513
23 mg/kg D.W.
3.2
9.8
SW846: 6010C
MMSD
12/30/19
DM1230119026556
22 mg/kg D.W.
3.2
9.7
SW846: 6010C
MMSD
12/31/19
DM1231/19026567
22 mg/kg D.W.
3.2
9.5
SW846: 6010C
MMSD
Avg Result: 23 mg/kg D.W.
Min LOD: 3.2 mg/kg D.W.
Max Result: 28 mg/kg D.W.
Page 701E
SYS/rptlMiloMonth/yDW 4126119 tj Printed.• V1512010.25

ANSD
PARTIM in tiim
PHOSPHORUS ICP Dry wt.
Sample ►.
12/01/19 DM1201/19024689
26000 mg/kg D.W.
24
91
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
SW846: 6010C MMSD
12/02/19
OM1202/19024702
25000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
12/03/19
DM1203/19024954
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
12/04/19
DM1204/19024993
25000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
22000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
12/06/19
DM1206/19025234
22000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
12/08/19
DM1208/19025264
23000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
12/09/19
DM1209/19025277
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
24000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
12/11/19
12/12/19
DM1211/19025319
DM1212/19025430
24000 mg/kg D.W.
24000 mg/kg D.W.
24
24
91
91
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/13/19
DM1213/19025517
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
12/14/19
DM1214/19025528
23000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
12/15/19
12/16/19
DM1215/19025755
DM1216119025768
24000 mg/kg D.W.
24000 mg/kg D.W.
24
23
90
90
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/17/19
DM1217/19025795
24000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
12/18/19
DM1218/19026149
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
12/19/19
DM1219119026252
23000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
12/20/19
DM1220/19026263
24000 mg/kg D.W.
24
93
SW846: 6010C
MMSD
12/21/19
DM1221/19026282
24000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
12/22/19
12/23/19
DM1222/19026295
DM1223/19026332
24000 mg/kg D.W.
24000 mg/kg D.W.
24
24
92
91
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/24/19
DM1224/19026436
24000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
12/25/19
DM1225/19026455
24000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
12/26/19
DM1226/19026470
25000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
25000 mg/kg D.W.
24
92
SW846: 6010C
MMSD
12/28/19
DM1228/19026500
26000 mg/kg D.W.
24
90
SW846: 6010C
MMSD
12/29/19
DM1229/19026513
26000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
12/30/19
DM1230/19026556
25000 mg/kg D.W.
24
91
SW846: 6010C
MMSD
12/31/19
DM1231/19026567
24000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
Avg Result: 24000 mg/kg D.W.
Min LOD:
23 mg/kg D.W.
Max Result: 26000 mg/kg D.W.
Page 8 of 16
5Y51rptlMi1bMonth1yDW 4126119 tj Printed: 111512010:25

. i@R b UEk[it
POTASSIUM ICP Dry wt.
Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
12/01/19
DM1201/19024689
4000 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/02/19
DM1202/19024702
4100 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/03/19
DM1203/19024954
4400 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/04/19
DM1204/19024993
4600 mg/kg D.W.
300
890
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
4000 mg/kg D.W.
300
890
SW846: 6010C
MMSD
12/06/19
DM1206/19025234
3900 mg/kg D.W.
290
870
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
4300 mg/kg D.W.
290
870
SW846: 6010C
MMSD
12/08/19
DM1208/19025264
4400 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/09/19
DM1209/19025277
4500 mg/kg D.W.
290
870
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
3900 mg/kg D.W.
290
870
SW846: 6010C
MMSD
12/11/19
12/12/19
DM1211/19025319
DM1212/19025430
4200 mg/kg D.W.
4200 mg/kg D.W.
290
290
870
880
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/13/19
DM1213/19025517
4200 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/14/19
DM1214/19025528
4500 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/15/19
DM1215/19025755
4400 mg/kg D.W.
290
870
SW846: 6010C
MMSD
12/16/19
DM1216/19025768
4200 mg/kg D.W.
290
860
SW846: 6010C
MMSD
12/17/19
DM1217/19025795
4300 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/18/19
DM1218/19026149
4500 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/19/19
DM1219/19026252
4600 mg/kg D.W.
290
870
SW846: 6010C
MMSD
12/20/19
DM1220/19026263
4600 mg/kg D.W.
300
900
SW846: 6010C
MMSD
12/21/19
DM1221/19026282
4500 mg/kg D.W.
300
890
SW846: 6010C
MMSD
12/22/19
DM1222/19026295
4400 mg/kg D.W.
300
890
Q2. SW846: 6010C
MMSD
12/23/19
DM1223/19026332
4400 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/24/19
DM1224/19026436
4500 mg/kg D.W.
300
890
SW846: 6010C
MMSD
12/25/19
DM1225119026455
4500 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/26/19
DM1226/19026470
4400 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
4100 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/28/19
DM1228/19026500
4300 mg/kg D.W.
290
870
SW846: 6010C
MMSD
12/29/19
DM1229/19026513
4400 mg/kg D.W.
290
880
SW846: 6010C
MMSD
12/30/19
DM1230119026556
4100 mg/kg D.W.
290
870
SW846: 6010C
MMSD
12/31/19
DM1231/19026567
4100 mg/kg D.W.
280
850
SW846: 6010C
MMSD
Avg Result: 4300 mg/kg D.W.
Min LOD:
280 mg/kg D.W.
Max Result: 4600 mg/kg D.W.
Page 9 o/1E
SYS1rpt1Mi/0M017th/yDW 4126119 tj Primed.- V1512010.•15

v
Ps1AABS I� it p€ANBt N'
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
12/01/19
DM1201/19024689
8.7 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/02/19
DM1202/19024702
10 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/03/19
DM1203/19024954
5.6 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/04/19
DM1204/19024993
< 4.3 mg/kg D.W.
4.3
13
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
< 4.3 mg/kg D.W.
4.3
13
SW846: 6010C
MMSD
12/06/19
DM1206/19025234
4.4 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
12/08/19
OM1208/19025264
4.5 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/09/19
DM1209119025277
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
9.1 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/11/19
12/12/19
DM1211/19025319
DM1212/19025430
7 mg/kg D.W.
< 4.2 mg/kg D.W.
4.2
4.2
13
13
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/13/19
DM1213/19025517
10 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/14/19
DM1214/19025528
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
12/15/19
DM1215/19025755
6.6 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/16/19
DM1216/19025768
5.3 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/17/19
DM1217/19025795
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
12/18/19
DM1218/19026149
7.8 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/19/19
DM1219119026252
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
12/20/19
DM1220/19026263
6.2 mg/kg D.W.
4.3
13
B7, I
SW846: 6010C
MMSD
12/21/19
DM1221/19026282
6.2 mg/kg D.W.
4.3
13
B7, J.
SW846: 6010C
MMSD
12/22/19
12/23/19
DM1222/19026295
DM1223/19026332
4.6 mg/kg D.W.
4.4 mg/kg D.W.
4.3
4.2
13
13
B7, J, Q2.
J.
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/24/19
DM1224/19026436
4.9 mg/kg D.W.
4.3
13
J.
SW846: 6010C
MMSD
12/25/19
DM1225/19026455
5 mg/kg D.W.
4.2
13
J, Q2.
SW846: 6010C
MMSD
12/26/19
DM1226/19026470
7.2 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
12/28/19
DM1228/19026500
4.3 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/29/19
DM1229/19026513
4.7 mg/kg D.W.
4.2
13
J.
SW846: 6010C
MMSD
12/30/19
DM1230/19026556
< 4.2 mg/kg D.W.
4.2
13
SW846: 6010C
MMSD
12/31/19
DM1231/19026567
< 4.1 mg/kg D.W.
4.1
13
SW846: 6010C
MMSD
Avg Result: 4.1 mg/kg D.W.
Min LOD:
4.1 mg/kg D.W.
Max Result: 10 mg/kg D.W.
Page 10 of 1E
SYS1rpt1Mi/oMonth1yDW 4126119 0 Printed: 111512010:15

kNSD
Solids (% Moisture)
Sample Date Sample ID
Result
LOD
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
LOQ .. Flags Analytical Method Lab
12/01/19
DM1201/19024689
8 %
0.1
SM 2540 G (1997)
MMSD
12/02/19
DM1202/19024702
7.8 %
0.1
SM 2540 G (1997)
MMSD
12/03/19
DM1203/19024954
7.6 %
0.1
SM 2540 G (1997)
MMSD
12/04/19
DM1204/19024993
8.8 %
0.1
SM 2540 G (1997)
MMSD
12/05/19
DM1205/19025115
8.8 %
0.1
SM 2540 G (1997)
MMSD
12/06/19
DM1206/19025234
6.7 %
0.1
SM 2540 G (1997)
MMSD
12/07/19
DM1207/19025245
7.4 %
0.1
SM 2540 G (1997)
MMSD
12/08/19
DM1208/19025264
8.4 %
0.1
SM 2540 G (1997)
MMSD
12/09/19
DM1209/19025277
6.9 %
0.1
SM 2540 G (1997)
MMSD
12/10/19
DM1210/19025304
7.1 %
0.1
SM 2540 G (1997)
MMSD
12/11/19
12/12/19
DM1211/19025319
DM1212/19025430
7.4 %
8.1 %
0.1
0.1
SM 2540 G (1997)
SM 2540 G (1997)
MMSD
MMSD
12/13/19
DM1213119025517
8.1 %
0.1
SM 2540 G (1997)
MMSD
12/14/19
DM1214/19025528
8 %
0.1
SM 2540 G (1997)
MMSD
12/15/19
DM1215/19025755
7 %
0.1
SM 2540 G (1997)
MMSD
12/16/19
DM1216/19025768
6.4 %
0.1
SM 2540 G (1997)
MMSD
12/17/19
DM1217/19025795
8.4 %
0.1
SM 2540 G (1997)
MMSD
12/18/19
DM1218/19026149
7.8 %
0.1
SM 2540 G (1997)
MMSD
12/19/19
DM1219/19026252
7.2 %
0.1
SM 2540 G (1997)
MMSD
12/20/19
DM1220/19026263
9.8 %
0.1
SM 2540 G (1997)
MMSD
12/21/19
DM1221/19026282
8.7 %
0.1
SM 2540 G (1997)
MMSD
12/22/19
DM1222/19026295
8.7 %
0.1
SM 2540 G (1997)
MMSD
12/23/19
DM1223/19026332
8 %
0.1
SM 2540 G (1997)
MMSD
12/24/19
DM1224/19026436
9.2 %
0.1
SM 2540 G (1997)
MMSD
12/25/19
DM1225/19026455
7.9 %
0.1
SM 2540 G (1997)
MMSD
12/26/19
DM1226/19026470
8 %
0.1
SM 2540 G (1997)
MMSD
12/27/19
DM1227/19026481
8.4 %
0.1
SM 2540 G (1997)
MMSD
12/28/19
DM1228/19026500
7.1 %
0.1
SM 2540 G (1997)
MMSD
12/29/19
DM1229/19026513
7.9 %
0.1
SM 2540 G (1997)
MMSD
12/30/19
DM1230/19026556
7.3 %
0.1
SM 2540 G (1997)
MMSD
12/31/19
DM1231/19026567
5.1 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 7.8 %
Min LOD: 0.1 %
Max Result: 9.8 %
Page 11 of lE
SY5/rptlM11oMonth1yDW 4126119 tj Printed: 111512010:15

"'t
iNSD
119TWMACIFIARWAK,
ZINC ICP Dry wt.
..SarnplelD Result LOD LOQ
12/01/19 DM1201119024689 450 mg/kg D.W. 18 55
12/02/19 DM1202/19024702 440 mg/kg D.W. 18 55
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
SW846: 6010C MMSD
SW846:6010C MMSD
12/03/19
DM1203/19024954
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/04/19
DM1204/19024993
490 mg/kg D.W.
19
56
SW846: 6010C
MMSD
12/05/19
DM1205/19025115
440 mg/kg D.W.
19
56
SW846: 6010C
MMSD
12/06/19
DM1206/19025234
450 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/07/19
DM1207/19025245
450 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/08/19
DM1208/19025264
440 mg/kg D.W.
18
56
SW846: 6010C
MMSD
12/09/19
DM1209/19025277
460 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/10/19
DM1210/19025304
460 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/11/19
12/12/19
DM1211/19025319
DM1212119025430
460 mg/kg D.W.
450 mg/kg D.W.
18
18
55
55
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/13/19
DM1213/19025517
440 mg/kg D.W.
18
56
SW846: 6010C
MMSD
12/14/19
DM1214119025528
410 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/15/19
DM1215/19025755
420 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/16/19
DM1216/19025768
430 mg/kg D.W.
18
54
SW846: 6010C
MMSD
12/17/19
DM1217/19025795
410 mg/kg D.W.
18
56
SW846: 6010C
MMSD
12/18/19
DM1218/19026149
450 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/19/19
DM1219/19026262
370 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/20/19
DM1220/19026263
390 mg/kg D.W.
19
56
SW846: 6010C
MMSD
12/21/19
DM1221/19026282
390 mg/kg D.W.
19
56
SW846: 6010C
MMSD
12/22/19
12/23/19
DM1222119026295
DM1223/19026332
390 mg/kg D.W.
380 mg/kg D.W.
19
18
56
55
Q2. SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/24/19
DM1224/19026436
400 mg/kg D.W.
19
56
SW846: 6010C
MMSD
12/25/19
DM1225/19026455
400 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/26/19
DM1226/19026470
430 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/27/19
DM1227/19026481
450 mg/kg D.W.
18
56
SW846: 6010C
MMSD
12/28/19
DM1228/19026500
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/29/19
DM1229/19026513
430 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/30/19
DM1230/19026556
440 mg/kg D.W.
18
55
SW846: 6010C
MMSD
12/31/19
DM1231119026567
440 mg/kg D.W.
18
54
SW846: 6010C
MMSD
Avg Result: 430 mg/kg D.W.
Min LOD: 18 mg/kg D.W.
Max Result: 490 mg/kg D.W.
Page 11 of 16
SY51rpt1M11oMonth/yDW 4126119 tj Afted: 111512010:15

r
�f4
r�aa�
Phosphorus - Total % DW (Calc.)
rSample Date Sample ID
Result
LOD
LOQ
Monthly Milorganite Report DW
December 2019
Milorganite Daily Composite
QA Flags Analytical Method Lab
12/01/19 DM1201/19024689
2.6 %D.W.
0.1
0.1
SW846: 6010C
MMSD
12/02/19 DM1202119024702
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/03/19 DM1203/19024954
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/04/19 DM1204/19024993
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/05/19 DM1205/19025115
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/06/19 DM1206/19025234
2.2 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/07/19 DM1207/19025245
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/08/19 DM1208/19025264
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/09/19 DM1209/19025277
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/10/19 DM1210/19025304
2.4%D.W.
0.1
0.1
SW846: 6010C
MMSD
12/11/19 DM1211/19025319
12/12/19 DM1212/19025430
2.4%D.W.
2.4 % D.W.
0.1
0.1
0.1
0.1
SW846: 6010C
SW846: 6010C
MMSD
MMSD
12/13/19 DM1213/19025517
2.4 %D.W.
0.1
0.1
SW846: 6010C
MMSD
12/14/19 DM1214/19025528
2.3 %D.W.
0.1
0.1
SW846: 6010C
MMSD
12/15/19 DM1215/19025755
2.4%D.W.
0.1
0.1
SW846: 6010C
MMSD
12/16/19 DM1216/19025768
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/17/19 DM1217/19025795
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/18/19 DM1218/19026149
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/19/19 DM1219/19026252
2.3%D.W.
0.1
0.1
SW846: 6010C
MMSD
12/20/19 DM1220/19026263
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/21/19 DM1221/19026282
2.4%D.W.
0.1
0.1
SW846: 6010C
MMSD
12/22/19 DM1222/19026295
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/23/19 DM1223/19026332
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/24/19 DM1224/19026436
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/25/19 DM1225/19026455
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/26/19 DM1226/19026470
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/27/19 DM1227/19026481
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/28/19 DM1228119026500
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/29/19 DM1229119026513
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/30/19 DM1230/19026556
2.5 %D.W.
0.1
0.1
SW846: 6010C
MMSD
12/31/19 DM1231/19026567
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
Avg Result: 2.4 % D.W.
ALUMINUM ICP Dry wt.
• Date Sample ID
Min LOD: 0.1 % D.W.
Result LOD
LOQ
Max Result: 2.6 "/o D.W.
Milorganite Weekly Composite
QA Flags Analytical Method Lab
12/07/19 WMC49/19025279
5900 mg/kg D.W.
57
200
88. SW846-.6010C
MMSD
Avg Result: 5900 mg/kg D.W.
(Milo) Ammonia in Fertilizer
Sample Date Sample ID
Min LOD: 57 mg/kg D.W.
Result LOD LOQ
•. Flags Analytical Method
Lab
12/07/19 WMC49/19025279
0.18 %
0.11
0.37
AOAC (13) 2.065
MMSD
Avg Result: 0.18 %
SY51rpt1Mi1oMonth1yDW 4126119 tj
Min LOD:
0.110/6
Page 13 of 1E
Printed., 111512010:25

iNSD
i tOR a Lli#�i
Monthly Milorganite Report DW
December 2019
Milorganite Weekly Composite
BORON ICP Dry wt.
*imple Date Sample ID
Result LOD LOQ QA Flags
'Analytical method
12/07/19 WMC49/19025279
19 mg/kg D.W. 2.3 8.4
EPA 6010
Pace -GB
Avg Result: 19 mg/kg D.W.
Min LOD: 2.3 mg/kg D.W.
CHROMIUM ICP Dry wt.
12/07/19 WMC49/19025279
190 mg/kg D.W. 1.6 4.8 B8.
SW846: 6010C
MMSD
Avg Result: 190 mg/kg D.W.
Min LOD: 1.6 mg/kg D.W.
COBALT ICP Dry wt.
Sample ..
•. LOQ •• Flags
Analytical Method
Lab
12/07/19 WMC49/19025279
1.9 mg/kg D.W. 0.28 1.1
SWB46: 6010C
MMSD
Avg Result: 1.9 mg/kg D.W.
Min LOD: 0.28 mg/kg D.W.
MERCURY by M. 7471 (sludge)
• r. - ,
,. LOQ •• Flags
Analytical Method
Lab
12/07/19 WMC49/19025279
0.37 mg/kg D.W. 0.019 0.064
EPA 7471
Pace -GB
12/14/19 WMC50/19025770 0.32 mg/kg D.W. 0.023 0.076 EPA 7471 Pace -GB
12/21/19 WMC51/19026422
0.22 mg/kg D.W. 0.022 0.072
EPA 7471
Pace -GB
12/28/19 WMC52/19026515
0.2 mg/kg D.W. 0.022 0.073
EPA 7471
Pace -GB
Avg Result: 0.28 mg/kg D.W.
Min LOD: 0.019 mg/kg D.W.
Max Result: 0.37 mg/kg D.W.
NITRATE NITROGEN
I-Sam-p-le-1-D
Result LOD LOQ QA Flags
Analytical Method
Lab
12/07/19 WMC49/19025279
1 % 0.5
AOAC (16) 930.01
MMSD
Avg Result: 1 %
Min LOD: 0.5 %
NITROGEN-Total(Manual)
Sample Date Sample ID
Result LOD LOQ QA Flags
Analytical Method
Lab
12/07/19 WMC49/19025279
6.1 % 0.11
AOAC (16) 955.04
MMSD
Avg Result: 6.1 No
Min LOD: 0.11
NITROGEN -Water Insoluble
..Result
12/07/19
WMC49/19025279
LOD LOQ QA Flags
4.6 % 0.5
Analytical Method
AOAC (16) 945.01
Lab
MMSD
Avg Result: 4.6 %
Min LOD: 0.5 %
pH -Solids
Sample Date
Sample ID
Result LOD LOQ QA Flags
Analytical Method
Lab
12/07/19
WMC49/19025279
6.36 Stnd. Units 0.1
SW846: 9045D
MMSD
12/14/19
WMC50/19025770
6.37 Stnd. Units 0.1
SW846: 9045D
MMSD
12/21/19
WMC51/19026422
6.33 Stnd. Units 0.1
SW846: 9045D
MMSD
12/28/19
WMC52/19026515
6.32 Stnd. Units 0.1
SW846: 9045D
MMSD
Avg Result: 6.3 Stnd. Units
Min LOD: 0.1 Stnd. Units
Max Result: 6.37 Stnd. Units
Page 14 of 16
5Y51rpt1Mi/oMonth1yDW 4126119 tj Printed: 1115120 10:25

Monthly Milorganite Report DW
14DDecember
2019
P�
Milorganite Weekly Composite
Solids (% Moisture)
..
•. LOQ
QA Flags Analytical Method Lab
12/07/19 WMC49/19025279
7.9 % 0.1
SM 2540 G (1997) MMSD
12/14/19 WMC50/19025770
7.6 % 0.1
SM 2540 G (1997) MMSD
12/21/19 WMC51/19026422
7.5 % 0.1
SM 2540 G (1997) MMSD
12/28/19 WMC52/19026515
8.2 % 0.1
SM 2540 G (1997) MMSD
Min LOD: 0.1 %
Solids (% Volatile)
Date Sample ID
Result LOD LOQ
QA Flags Analytical Method Lab
12/07/19 WMC49/19025279
72 % 0.1
SM 2540 G (1997) MMSD
Avg Result: 72 1%
Min LOD: 0.1 %
Solids (% Total)
Date Sample ID
Result LOD LOQ
QA Flags Analytical Method Lab
12/07/19 WMC49/19025279
92 % 0.1
SM 2540 G (1997) MMSD
Avg Result: 92 "/o
Min LOD: 0.1 %
Milorganite (Outfall 006) PRODUCTION
FECAL COLIFORM SLUDGE
Sample Date Sample ID
Result LOD LOQ
• . Flags Analytical Method Lab
12/03/19 19026042
< 0.2 MPN/g TS 0.2
EPA 1680 MMSD
12/10/19 19026382
< 0.2 MPN/g TS 0.2
EPA 1680 MMSD
12/17/19 19026686
1.4 MPN/g TS 0.2
EPA 1680 MMSD
12/23/19 19026783
2.6 MPN/g TS 0.2
EPA 1680 MMSD
Min LOD: 0.2 MPN/g TS
Solids (% Total)
12/03/19
19026042
90 %
0.1
SM 2540 G (1997)
MMSD
12/10/19
19026382
91 %
0.1
SM 2540 G (1997)
MMSD
12/17/19
19026686
91 %
0:1
SM 2540 G (1997)
MMSD
12/23/19
19026783
92 %
0.1
SM 2540 G (1997)
MMSD
Avg Result: 91 % Min LOD: 0.1 % Max Result: 93
Milorganite (Outfall 009) BAGGING
FECAL COLIFORM SLUDGE
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
12/03/19 19026044 < 0.19 MPN/g TS 0-19 EPA 1680 MMSD
Min LOD: 0.19 MPN/g TS
Solids (% Total)
!ia--.ple-Date Sample ID Result LOD LOQ .. Flags Analytical Method Lab
12/03/19 19026044 93 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 93 % Min LOD: 0.1
Page 15 of 16
SYS/rptlMi/oMonth/yDW 4126119 tj Printed.• V1512010:1S

ItkN$D
WWWAUMMMM
FECAL COLIFORM SLUDGE
Monthly Milorganite Report DW
December 2019
Milorganite (Outfall 009) BAGGING
Milorganite (Outfall 008) SHIPPING
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
12/03/19 19026043 :0 MMSD
Min LOD: 0.2 MPN/g TS
Solids (% Total)
Sample DAW'�� le ID Result .. LOQ QA Flags Analytical Method Lab
12/03/19 19026043 92 % 0.1 SM 2540 G (1997) MMSD
Avg Result: 92 % Min LOD: 0.1
AO Other -- Flag requires additional explanation.
AX Qualified data - see contract laboratory report.
B3 Target analyte detected in method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits.
88 LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits.
CQ Data used for calculation of result was qualified.
D3 Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
04 Sample matrix interferences did not allow completing the analysis.
DS The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
H3 Sample was received past holding time. _
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
IS Insufficient sample volume for analysis.
7 Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit.
LA Not analyzed - laboratory accident.
M1 Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
MS Incubator/water bath temperature was outside method
requirements.
M7 Microbiology sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data (Water Quality only).
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
S5 Reading was not confirmed by a constant weight measurement.
SD Supplemental details provided (Water Quality only).
T3 The BOD dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The BOD dilution water D.O. increase was > 0.2 mg/L.
TS Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample is outside of the prescribed method temperature range.
Page 16 of 16
5Y5/rpt1M11oMonth1yDW 4126119 tj Printed: V1512010:25

11 HNSD
PARTNERS FOR A CLEANER ENVIRONMENT
January 9, 2020
TO: Tom Nowicki and Steve Unger
FROM: Zach Vogel
COPY: A. Sotomayor, Lab File
-MqI11617-ya�-`tt
SUBJECT: Annual PCB Milorganite Report — 2019
Attached is the Annual PCB Milorganite report for the year 2019. Daily Milorganite samples are 24-hour
composite samples, representative of a full day of production. All analyses were performed by Pace Analytical
Services, Inc. in Green Bay, WI (Wisconsin Certification #: 405132750). Full laboratory results are available upon
request.
There was no Milorganite production on the following dates:
• January 20, 2019;
• October 2 through October 12, 2019.
Please contact the Central Laboratory if there are any questions or comments regarding these data.
Data/Report Review By:
.''�✓''��,�/'� � � �• 20 z
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

2019 Milorganite Daily Production Samples
PCB Aroclors (ppb)'
COLLECTION ECTION HATE
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
Total PCB Aroclors
1/1/19
< 55
< 55
< 55
< 55
< 55
< 5S
< 55
< 55
1/2/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
1/3/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
1/4/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
1/5/19
< 54
< 54
< 54
< 54
< S4
< 54
< 54
< 54
1/6/19
< 53
< 53
< S3
< S3
< 53
< 53
< 53
< 53
1/7/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
1/8/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
1/9/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
1/10/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
1/11/19
< 55
< 55
< 55
< 55
< 55
< 55
< S5
< 55
1/12/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
1/13/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
1/14/19
< SS
< 55
< 55
< 55
< 55
< 55
< 55
< SS
1/15/19
< 56
< S6
< 56
< 56
< 56
< 56
< 56
< 56
1/16/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
1/17/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
1/18/19
< 55
< SS
< 55
< 55
< 55
< 55
< 55
< 55
1/19/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< S4
1/21/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
1/22/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
1/23/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
1/24/19
< 55
< 55
< 55
< 5S
< 55
< 55
< 55
< 55
1/25/19
< 56
< 56
< S6
< 56
< 56
< 56
< 56
< 56
1/26/19
< SS
< 55
< 55
< 55
< 55
< 55
< 55
< 55
1/27/19
< 54
< 54
< S4
< 54
< 54
< 54
< 54
< 54
1/28/19
< S3
< 53
< 53
< 53
< 53
< 53
< 53
< 53
1/29/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
1/30/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
1/31/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
2/1/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53

2019 Milorganite Daily Production Samples
PCB Aroclors (ppb)l
COLLECTION ECTION DATE
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
Total PCB Aroclors
2/2/19
< 52
< 52
< 52
< S2
< 52
< S2
< 52
< 52
2/3/19
< 52
< 52
< 52
< S2
< 52
< 52
< S2
< 52
2/4/19
< 55
< 55
< 55
< S5
< SS
< SS
< 55
< 55
2/5/19
< 53
< 53
< S3
< 53
< S3
< 53
< 53
< 53
2/6/19
< 53
< S3
< S3
< 53
< S3
< 53
< S3
< 53
2/7/19
< 54
< S4
< S4
< 54
< 54
< 54
< 54
< S4
2/8/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
2/9/19
< S4
< 54
< 54
< 54
< 54
< 54
< 54
< 54
2/10/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
2/11/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
2/12/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
2/13/19
< 55
< 55
< 55
< 55
< 55
< 55
< 5S
< 55
2/14/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
2/15/19
< S4
< 54
< 54
< 54
< 54
< 54
< 54
< 54
2/16/19
< 55
< 55
< 55
< 55
< 55
< 55
< S5
< 55
2/17/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
2/18/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
2/19/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
2/20/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
2/21/19
< SS
< 55
< 55
< 55
< 55
< 55
< 55
< 55
2/22/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
2/23/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
2/24/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
2/2S/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
2/26/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< S3
2/27/19
< S3
< 53
< 53
< 53
< 53
< S3
< 53
< 53
2/28/19
< S4
< S4
< 54
< S4
< 54
< 54
< S4
< 54
3/1/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
3/2/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
3/3/19
< 53
< 53
< 53
< 53
< 53
< S3
< S3
< S3
3/4/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53

2019 Milorganite Daily Production Samples
COLLECTION ECTION DATE
PCB Aroclors (ppb)l
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
Total PCB Aroclors
3/5/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
3/6/19
< 54
< 54
< 54
< 54
< 54
< 54
< S4
< 54
3/7/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/8/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/9/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/10/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
3/11/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
3/12/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/13/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
3/14/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
3/15/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/16/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/17/19
< 52
< 52
< 52
< S2
< 52
< 52
< 52
< 52
3/18/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< S2
3/19/19
< 52
SS
< 52
< 52
< 52
< 52
< S2
58
3/20/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
3/21/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/22/19
< S3
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/23/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/24/19
< 54
< 54
< 54
< S4
< 54
< 54
< 54
< 54
3/25/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
3/26/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/27/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
3/28/19
< 54
< 54
< 54
< 54
< 54
< 54
< S4
< 54
3/29/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
3/30/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
3/31/19
< 53
< S3
< 53
< 53
< 53
< 53
< 53
< 53
4/1/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
4/2/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
4/3/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
4/4/19
< 54
< 54
< S4
< 54
< 54
< 54
< 54
< 54

2019 Milorganite Daily Production Samples
COLLECTION ECTION Derr
PCB Aroclors (ppb)l
PCB-1242 PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
Total PCB Aroclors
4/5/19
< 54
< 54
< 54
< S4
< 54
< 54
< 54
< 54
4/6/19
< 54
< 54
< 54
< 54
< 54
< 54
< S4
< 54
4/7/19
< 54
< 54
< 54
< 54
< 54
< 54
< S4
< 54
4/8/19
< 54
< 54
< 54
< S4
< 54
< 54
< 54
< 54
4/9/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
4/10/19
< 53
< S3
< S3
< 53
< 53
< 53
< 53
< 53
4/11/19
< 53
< 53
< 53
< 53
< 53
< S3
< 53
< 53
4/12/19
< 53
< 53
< 53
< 53
< 53
< S3
< 53
< 53
4/13/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
4/14/19
< 54
< S4
< 54
< 54
< 54
< 54
< S4
< S4
4/15/19
< S4
< 54
< 54
< 54
< 54
< 54
< S4
< 54
4/16/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
4/17/19
< 54
< 54
< 54
< S4
< 54
< 54
< 54
< 54
4/18/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
4/19/19
< 53
< 53
< 53
< 53
< 53
< S3
< 53
< 53
4/20/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
4/21/19
< 55
< 55
< 55
< 55
< 55
< 5S
< 55
< 55
4/22/19
< S3
< 53
< 53
< 53
< S3
< 53
< S3
< 53
4/23/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
4/24/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
4/25/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
4/26/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
4/27/19
< 52
< 52
< 52
< 52
< 52
< S2
< 52
< 52
4/28/19
< 53
< 53
< S3
< 53
< 53
< 53
< 53
< 53
4/29/19
< 53
< 53
< 53
< 53
< 53
< 53
< S3
< 53
4/30/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
5/1/19
< 52
< 52
< 52
< 52
< 52
< 52
< S2
< 52
5/2/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
5/3/19
< 53
< 53
< 53
< 53
< 53
< S3
< 53
< 53
5/4/19
< S2
< 52
< 52
< 52
< 52
< 52
< 52
< 52
5/5/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52

2019
Milorganite Daily Production
Samples
PCB
Aroclors (ppb)l
COLLECTION ECTION 'DATE
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248 PCB-1260
PCB-1016
Total PCB Aroclors
5/6/19
< S3
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/7/19
< 53
< 53
< 53
< 53
< S3
< 53
< 53
< 53
5/8/19
< 53
< 53
< S3
< 53
< 53
< 53
< 53
< 53
5/9/19
< S2
< 52
< 52
< 52
< 52
< 52
< 52
< 52
5/10/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/11/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/12/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
5/13/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
5/14/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/15/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
5/16/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/17/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/18/19
< 52
< 52
< 52
< 52
< 52
< 52
< S2
< 52
5/19/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< S3
5/20/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/21/19
< 53
< 53
< S3
< 53
< 53
< 53
< 53
< 53
5/22/19
< 53
< 53
< S3
< 53
< 53
< 53
< 53
< 53
5/23/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
5/24/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
5/25/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/26/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
5/27/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/28/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/29/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
5/30/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
5/31/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
6/1/19
< S3
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/2/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
6/3/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/4/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/S/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53

2019 Milorganite Daily Production Samples
C LLECTION DATE
PCB Aroclors (ppb)'
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
Total PCB Aroclors
6/6/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/7/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/8/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/9/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
6/10/19
< S4
< 54
< 54
< 54
< 54
< 54
< 54
< 54
6/11/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/12/19
< 53
< 53
< S3
< 53
< 53
< 53
< 53
< 53
6/13/19
< 53
< 53
< 53
< 53
< 53
< S3
< 53
< 53
6/14/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/15/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/16/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
6/17/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/18/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/19/19
< 53
< 53
< 53
< 53
< 53
< 53
< S3
< 53
6/20/19
< 56
< 56
< 56
< 56
< 56
< 56
< 56
< 56
6/21/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/22/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
6/23/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
6/24/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
6/25/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/26/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
6/27/19
< 55
< 5S
< 55
< 55
< SS
< 55
< 55
< 55
6/28/19
< 54
< S4
< 54
< 54
< 54
< 54
< 54
< 54
6/29/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
6/30/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
7/1/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
7/2/19
< 54
< 54
< 54
< 54
< 54
< 54
< S4
< 54
7/3/19
< 56
< 56
< 56
< 56
< 56
< 56
< 56
< 56
7/4/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
7/5/19
< S2
< 52
< 52
< 52
< 52
< 52
< 52
< 52
7/6/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53

2019 Milorganite Daily Production Samples
co LEMON DATE
PCB Aroclors (ppb)i
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
Total PCB Aroclors
7/7/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
7/8/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
7/9/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
7/10/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
7/11/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
7/12/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
7/13/19
< SS
< 55
< 55
< 55
< 55
< 55
< S5
< 55
7/14/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
7/15/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
7/16/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
7/17/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
7/18/19
< 54
< 54
< 54
< 54
< 54
< 54
< S4
< 54
7/19/19
< 5S
< 55
< 55
< 55
< 55
< SS
< 55
< 55
7/20/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
7/21/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
7/22/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
7/23/19
< 54
< 54
< 54
< 54
< 54
< 54
< S4
< S4
7/24/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
7/25/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
7/26/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
7/27/19
< 54
< 54
< 54
< S4
< 54
< 54
< S4
< 54
7/28/19
< 55
< 55
< SS
< 55
< 55
< 55
< 55
< 55
7/29/19
< SS
< 55
< 55
< 55
< 55
< 55
< 55
< 55
7/30/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
7/31/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
8/1/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
8/2/19
< 56
< 56
< 56
< 56
< 56
< 56
< S6
< 56
8/3/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
8/4/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
8/5/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
8/6/19
< 53
< 53
< 53
< 53
< S3
< 53
< 53
< 53

2019 Milorganite Daily Production Samples
COLLECTION ECTION DATE
PCB Aroclors (ppb)l
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
Total PCB Aroclors
8/7/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
8/8/19
< 53
81
< 53
< 53
< 53
< 53
< 53
81
8/9/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
8/10/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
8/11/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
8/12/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
8/13/19
< 55
< SS
< SS
< 55
< 55
< 5S
< 55
< 55
8/14/19
< 54
< S4
< 54
< 54
< 54
< 54
< 54
< S4
8/15/19
< 54
58
< 54
< 54
< 54
< 54
< 54
S8
8/16/19
< 53
< 53
< 53
< 53
< S3
< 53
< S3
< 53
8/17/19
< 55
< 55
< 55
< 55
< SS
< 55
< SS
< S5
8/18/19
< SS
< 55
< 5S
< 55
< SS
< 55
< 55
< 55
8/19/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
8/20/19
< 54
< 54
< 54
< 54
< S4
< 54
< 54
< 54
8/21/19
< 55
< 55
< 55
< 55
< 55
< 55
< 55
< 55
8/22/19
< 54
< S4
< 54
< 54
< 54
< 54
< 54
< S4
8/23/19
< 53
58
< 53
< 53
< 53
< 53
< 53
58
8/24/19
< 54
< 54
< 54
< 54
< 54
< S4
< 54
< 54
8/2S/19
< 54
< S4
< 54
< 54
< 54
< S4
< 54
< 54
8/26/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
8/27/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
8/28/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
8/29/19
< S2
< 52
< 52
< 52
< 52
< S2
< 52
< 52
9/30/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
8/31/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
9/1/19
< 54
< 54
< 54
< 54
< 54
< 54
< S4
< 54
9/2/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
9/3/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
9/4/19
< 53
< 53
< 53
< 53
< 53
< S3
< 53
< 53
9/S/19
< S3
< 53
< 53
< 53
< 53
< 53
< S3
< S3
9/6/19
< 54
< S4
< 54
< 54
< 54
< 54
< 54
< 54

2019 Milorganite Daily Production Samples
COLLECTION E/'TION DATE
PCB Aroclors (ppb)l
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
Total PCB Aroclors
9/7/19
< 53
< S3
< 53
< 53
< 53
< 53
< 53
< 53
9/8/19
< S3
< S3
< 53
< 53
< 53
< 53
< 53
< 53
9/9/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< S3
9/10/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
9/11/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
9/12/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
9/13/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
9/14/19
54
SS
< 52
< 52
< 52
< 52
< 52
110
9/15/19
57
56
< 52
< 52
< 52
58
< 52
170
9/16/19
59
59
< 52
< 52
< 52
60
< 52
180
9/17/19
55
58
< 53
< 53
< 53
63
< 53
180
9/18/19
< 53
63
< 53
< 53
< S3
60
< 53
120
9/19/19
< 53
74
< 53
< S3
< 53
69
< 53
140
9/20/19
< 53
63
< 53
< 53
< 53
59
< 53
120
9/21/19
< 53
57
< 53
< 53
< 53
< 53
< 53
57
9/22/19
< 53
53
< 53
< 53
< 53
< 53
< 53
53
9/23/19
< 54
56
< 54
< 54
< 54
< 54
< 54
56
9/24/19
< 54
< 54
< 54
< 54
< 54
62
< 54
62
9/25/19
< 53
< 53
< 53
< 53
< 53
< S3
< 53
< 53
9/26/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
9/27/19
< 51
54
< 51
< 51
< 51
65
< 51
120
9/28/19
< 52
< 52
< 52
< 52
< 52
53
< 52
53
9/29/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
9/30/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
10/1/19
< 53
56
< 53
< S3
< S3
58
< 53
110
10/13/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
10/14/19
< 52
< 52
< 52
< 52
< 52
< 52
< S2
< 52
10/15/19
< 52
< 52
< 52
< 52
< 52
< 52
< 52
< 52
10/16/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
10/17/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
10/18/19
< 54
< 54
< S4
< 54
< 54
< 54
< S4
< 54

2019 Milorganite Daily Production Samples
COLLECTION ECTION DATE
PCB Aroclors (ppb)l
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
Total PCB Aroclors
10/19/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
10/20/19
< 54
< S4
< S4
< 54
< 54
< 54
< 54
< 54
10/21/19
< 54
< S4
< S4
< 54
< 54
< 54
< 54
< 54
10/22/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
10/23/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
10/24/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< S4
10/2S/19
< SS
< 55
< 55
< 55
< 55
< 55
< SS
< SS
10/26/19
< S4
< 54
< 54
< 54
< 54
< 54
< 54
< S4
10/27/19
< 5S
< 55
< 55
< 55
< 55
< 55
< 55
< 55
10/28/19
< S4
< 54
< 54
< 54
< 54
< 54
< 54
< 54
10/29/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
10/30/19
< 54
< 54
< 54
< S4
< 54
< 54
< 54
< 54
10/31/19
< 54
< 54
< 54
< S4
< 54
< 54
< 54
< 54
11/1/19
< S5
< 55
< 55
< SS
< 55
< 55
< 55
< S5
11/2/19
< 54
< 54
< 54
< 54
< S4
< 54
< 54
< S4
11/3/19
< S4
< 54
< 54
< 54
< 54
< 54
< S4
< 54
11/4/19
< 55
< 55
< 55
< 55
< 55
< 55
< 5S
< 5S
11/5/19
< S4
< 54
< 54
< 54
< 54
< 54
< 54
< 54
11/6/19
< S4
< 54
< 54
< 54
< 54
< S4
< S4
< 54
11/7/19
< S3
57
< 53
< 53
< 53
< 53
< S3
57
11/8/19
< 54
59
< 54
< 54
< 54
< S4
< S4
59
11/9/19
< S4
96
< 54
< 54
< S4
< 54
< S4
96
11/10/19
< SS
67
< 55
< 55
< 55
< 55
< 55
67
11/11/19
< 54
61
< 54
< 54
< 54
< 54
< 54
61
11/12/19
< 55
61
< 55
< S5
< 55
< 55
< 55
61
11/13/19
< 54
55
< S4
< 54
< 54
< 54
< 54
55
11/14/19
< 54
56
< 54
< 54
< 54
< 54
< 54
S6
11/15/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
11/16/19
< 54
< S4
< 54
< 54
< S4
< 54
< 54
< 54
11/17/19
< 54
58
< 54
< 54
< 54
< 54
< 54
58
11/18/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54

2019 Milorganite Daily Production Samples
PCB Aroclors (ppb)l
OLECTION DATE
COLLECTION
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
Total PCB Aroclors
11/19/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
11/20/19
< 55
< 55
< 55
< 55
< 55
< SS
< 55
< 55
11/21/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
11/22/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
11/23/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
11/24/19
< S4
< 54
< 54
< 54
< 54
< S4
< 54
< 54
11/25/19
< S4
< 54
< 54
< 54
< 54
< 54
< 54
< 54
11/26/19
< 54
< 54
< 54
< 54
< 54
< 54
< S4
< 54
11/27/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
11/28/19
< 54
< 54
< 54
< 54
< S4
< S4
< 54
< 54
11/29/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< S4
11/30/19
< 54
< S4
< S4
< 54
< 54
< S4
< 54
< 54
12/1/19
< 54
< 54
< 54
< 54
< S4
< S4
< 54
< 54
12/2/19
< S4
< S4
< 54
< 54
< 54
< S4
< 54
< 54
12/3/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
12/4/19
< 55
6S
< 5S
< 55
< 55
< 55
< SS
6S
12/5/19
< SS
< S5
< SS
< 55
< SS
< 55
< 55
< SS
12/6/19
< 54
< 54
< 54
< 54
< 54
< S4
< 54
< 54
12/7/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
12/8/19
< 55
< 55
< 55
< 55
< S5
< 5S
< 55
< 55
12/9/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
12/10/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
12/11/19
< S4
< 54
< 54
< 54
< S4
< S4
< 54
< 54
12/12/19
< 55
< 55
< 55
< 55
< 55
< SS
< SS
< 55
12/13/19
< 55
< 55
< 55
< SS
< 55
< 55
< 55
< 55
12/14/19
< 54
< 54
< 54
< 54
< S4
< 54
< 54
< 54
12/15/19
< 54
< 54
< 54
< 54
< 54
< 54
< 54
< 54
12/16/19
< 53
< 53
< 53
< 53
< 53
< 53
< 53
< 53
12/17/19
< 55
59
< 55
< 55
< 55
< 55
< 55
59
12/18/19
< 54
< 54
< S4
< S4
< 54
< 54
< 54
< 54
12/19/19
< 54
< S4
< 54
< 54
< 54
< 54
< 54
< S4

2019 Milorganite Daily Production Samples
COLLECTION ECTION DATE
1
PCB Aroclors (ppb)'
PCB-1242
PCB-1254
PCB-1221
PCB-1232 PCB-1248 PCB-1260
PCB-1016
Total PCB Aroclors
12/20/19
< 56
< 56
< 56
< 56 < 56 < 56
< 56
< 56
12/21/19
< 56
< 56
< 56
< 56 < 56 < S6
< 56
< 56
12/22/19
< 55
< 55
< SS
< S5 < 55 < SS
< 55
< 55
12/23/19
< 54
< 54
< 54
< 54 < 54 < S4
< 54
< 54
12/24/19
< SS
< 55
< 55
< 55 < 55 < S5
< 5S
< 55
12/25/19
< 54
< 54
< 54
< 54 < 54 < 54
< S4
< 54
12/26/19
< 54
< 54
< 54
< 54 < 54 < 54
< 54
< 54
12/27/19
< 55
< 55
< 55
< 55 < 55 < 55
< S5
< 55
12/29/19
< 54
< 54
< 54
< 54 < 54 < 54
< 54
< 54
12/29/19
< 55
< 55
< 55
< 55 < SS < 55
< 55
< 55
12/30/19
< 54
< 54
< 54
< 54 < 54 < 54
< 54
< 54
12/31/19
< 53
< 53
< 53
< 53 < S3 < 53
< 53
< 53
'Samples analyzed
by Pace Analytical Services, Green Bay, Wisconsin (WI Certification #405132750) by EPA 8082. All
results
reported on a dry weight basis.

Milorganite Dioxin Toxic Equivalent Concentrations 2019
Measured
Concentration (pgIg
or t
Factor
CAS
Congener
1/12/2019
2/9/2019
3/9/2019
4/13/2019
5/11/2019
6/8/2019
7/13/2019
8/10/2019
9/7/2019
10/26/2019
11/30/2019
1217/2019
EPA
Maine
1746-01-6
2,3,7,8- Tetrachlorodibenzo-p-dioxin
0
0
0
0
0
0
0
0
0
0
0
0
1.0
1.0
40321-76-4
1,2,3,7,8- Pentachlorodibenzo-p-dioxin
0
0
0
0
0
0
0
0
0
0
0
0
1.0
0.5
39227-28-6
1,2,3,4,7,8- Hexachlorodibenzo-p-dioxin
0
0
0
0
0
0
5
0.0
0
0
0
0
0.1
0.1
57653-85-7
1,2,3,6,7,8- Hexachlorodibenzo-p-dioxin
6.2
5
6.3
0
9.2
8.9
20
7.0
6.9
7.8
8.9
9.3
0.1
0.1
19408-74-3
1,2,3,7,8,9- Hexachlorodibenzo-p-dioxin
0
0
5.1
0.0
7.80
7.4
8.1
5.2
5.9
7.5
5.7
7.1
0.1
0.1
35822-46-9
1,2,3,4,6,7,8- Heptachlorodibenzo-p-dioxin
120
100
120
83
220
180
670
140
130
200
130
160
0.01
0.01
3268-87-9
1,2,3,4,6,7,8,9- Octachlorodibenzo-p-dioxin
1100
910
1100
790
1800
1700
3600
1400
1300
1900
1300
1500
0.0001
0.001
51207-31-9
2,3,7,8- Tetrachlorodibenzofuran
3.5
6
12.0
2.6
4.2
2.7
3.7
2
3.3
2.1
4.1
4.3
0.1
0.1
57117-41-6
1,2,3,7,8- Pentachlorodibenzofuran
0
0
0
0
0
0
0
0
0
0
0
0
0.05
0.05
57117-31-4
2,3,4,7,8- Pentachlorodibenzofu ran
8.5
18
37
7
6.9
6.8
7
0
7.5
0
7.9
8.2
0.5
0.5
70648-26-9
1,2,3,4,7,8- Hexachlorodibenzofuran
0
0
0
0
0
0
5.3
0
0
5.8
5.4
5.3
0.1
0.1
57117-44-9
1,2,3,6,7,8- Hexachlorodibenzofuran
0
0
0
0
5.6
0
6
0
0
0
7.9
8.4
0.1
0.1
72918-21-9
1,2,3,7,8,9- Hexachlorodibenzofuran
0
0
0
0
0
0
0
0
0
0
0
0
0.1
0.1
60851-34-5
2,3,4,6,7,8- Hexachlorodibenzofuran
0
0
0.0
0
6.6
5.3
6.5
0
0
0
0
0
0.1
0.1
67562-39-4
1,2,3,4,6,7,8- Heptachlorodi benzofu ran
53
35
50
34
93
100
110
68
65
120
65
76
0.01
0.01
55673-89-7
1,2,3,4,7,8,9- Heptachlorodibenzofu ran
0
0
0.0
0
0
0
5.2
0
0
0
0
0
0.01
0.01
39001-02-0
1,2,3,4,6,7,8,9-Octachlorodibenzofuran
100
71
87
65
150
160
140
150
110
190
0
150
0.0001
1 0.001
32598-13-3
3,3',4,4'- Tetrachlorobiphenyl
260
220
274
252
265
252
305
450
364
0
309
267
0.0001
0.0005
70362-50-4
3,4,4',5- Tetrachlorobiphenyl
0
0
0
0
0
0
0
0
0
0
0
0
0.0001
57465-28-8
3,3',4,4',5- Pentachlorobiphenyl
0
0
0
0
0
0
0
0
0
0
0
0
0.1
0.1
32598-14-4
2,3,3',4,4'- Pentachlorobiphenyl
1400
1170
3580
1160
1360
1760
1820
2670
2250
1830
1880
1700
0.0001
0.0001
31508-00-6
2,3',4,4',5- Pentachlorobiphenyl
3090
2650
7450
2830
3210
4130
3810
6060
4730
4210
4180
3990
0.0001
0.0001
65510-44-3
2',3,4,4',5- Pentachlorobiphenyl
0
0
145
0
0
0
0
151
102
0
0
0
0.0001
0.0001
74472-37-0
2,3,4,4',5- Pentachlorobiphenyl
0
0
191
0
0
115
106
171
131
115
0
0
0.0005
0.0005
32774-16-6
3,3',4,4',5,5'- Hexachlorobiphenyl
0
0
0
0
0
0
0
0
0
0
0
0
0.01
0.01
38380-08-4
2,3,3',4,4',5-Hexachlorobiphenyl
523
490
1670
501
622
704
680
1100
811
826
700
690
0.0005
0.0005
69782-90-7
2,3,3',4,4',5'- Hexachlorobiphenyl
0
0
0
0
0
0
0
0
0
0
0
0
0.0005
0.0005
52663-72-6
2,3',4,4',5,5'-Hexachlorobiphenyl
175
0
452
170
0
212
231
360
249
249
246
196
0.00001
0.00001
39635-31-9
2,3,3',4,4',5,5'- Heptachlorobiphenyl
0
0
155
0
0
0
0
0
0
0
0
0
0.0001
0.0001
35065-30-6
2,2',3,3',4,4',5-Heptachlorobiphenyl
1220
1010
2370
1240
1230
1220
1510
1900
1780
1700
1570
1500
0.0001
69782-91-8
2,2',3,4,4',5.5'-Heptachlorobiphenyl
3170
2200
5000
2900
2950
2720
3800
4680
4100
3710
3610
3230
0.0001
Total EPA Toxic Equivalent (TEQ)
7.8
12.2
24.8
5.7
10.9
9.8
18.2
5.2
8.7
6.8
10.2
11.0
Total Maine Toxic Equivalent (TEQ)
1 9.4
13.5
26.7
7.0
13.2
12.0
22.2
7.5
10.7
9.2
12.0
13.1
"0" means that the concentration was less than the level of detection

NSDSpring
aiM F9 # CtW8 Nti IMi#fi'
964
3/9/19 SU
Sample Date Site Code
�OpSID Test Name
WMC10
Customer ID
Reported Value
Milorganite Priority Pollunant and VOC Analysis
2019
Milo. Priority Pollutant Sample
19002892
LIMS Number
MDL•• Flags Analysis Date Method Lab
1253
1,2,4-Trichlorobenzene Dry wt.
< 360 ug/kg D.W.
360
4900
3/18/19
8270D
Test America B 3
1315
1,2-Diphenylhydrazine Dry wt.
< 280 ug/kg D.W.
280
4900
3/18/19
8270D
Test America B 3
1234
2,4,6-Trichlorophenol Dry wt.
< 510 ug/kg D.W.
510
2500
3/18/19
8270D
Test America B 3
1226
2,4-Dichlorophenol Dry wt.
< 270 ug/kg D.W.
270
2500
3/18/19
8270D
Test America B 3
1227
2,4-Dimethylphenol Dry wt.
< 610 ug/kg D.W.
610
2500
3/18/19
8270D
Test America B 3
1229
2,4-Dinitrophenol Dry wt.
< 12000 ug/kg D.W.
12000
25000
3/18/19
8270D
Test America B 3
1252
2,4-Dinitrotoluene Dry wt.
< 520 ug/kg D.W.
520
2500
3/18/19
8270D
Test America B 3
1317
2,6-Dinitrotoluene Dry wt.
< 300 ug/kg D.W.
300
2500
3/18/19
8270D
Test America B 3
1249
2-Chloronaphthalene Dry wt.
< 420 ug/kg D.W.
420
2500
3/18/19
8270D
Test America B 3
1225
2-Chlorophenol Dry wt.
< 460 ug/kg D.W.
460
2500
3/18/19
8270D
Test America B 3
1230
2-Nitrophenol Dry wt.
< 720 ug/kg D.W.
720
2500
3/18/19
8270D
Test America B 3
1324
3,3'-Dichlorobenzidine Dry wt.
< 3000 ug/kg D.W.
3000
4900
3/18/19
8270D
Test America B 3
1260
4,4-DDD Dry wt.
130 ug/kg D.W.
17
87
3/20/19
8081E
Test America B 3
1259
4,4-DDE Dry wt.
< 18 ug/kg D.W.
18
87
3/20/19
80818
Test America B 3
1258
4,4-DDT Dry wt.
< 20 ug/kg D.W.
20
87
3/20/19
8081E
Test America B 3
1228
4,6-Dinitro-o-Cresol Dry wt.
< 2500 ug/kg D.W.
2500
4900
3/18/19
8270D
Test America B 3
1247
4-Bromophenyl Phenyl Ether Dry wt. < 360 ug/kg D.W.
360
2500
3/18/19
8270D
Test America B 3
1250
4-Chloro-phenyl-phenyl ether Dry wt. < 310 ug/kg D.W.
310
2500
3/18/19
8270D
Test America B 3
1231
4-Nitrophenol Dry wt.
< 1800 ug/kg D.W.
1800
4900
3/18/19
8270D
Test America B 3
1254
A-BHC-Alpha Dry wt.
< 16 ug/kg D.W.
16
87
3/20/19
8081B
Test America B 3
1235
Acenaphthene Dry wt.
< 370 ug/kg D.W.
370
2500
3/18/19
8270D
Test America B 3
1318
Acenaphthylene Dry wt.
< 330 ug/kg D.W.
330
2500
3/18/19
8270D
Test America B 3
1304
Aldrin Dry wt.
< 21 ug/kg D.W.
21
87
3/20/19
8081B
Test America 8 3
524
ALUMINUM ICP Dry wt.
4200 mg/kg D.W.
4.6
10
3/18/19
6010C
Test America B 3
1236
Anthracene Dry wt.
< 630 ug/kg D.W.
630
2500
3/18/19
8270D
Test America B 3
545
ANTIMONY ICP Dry wt.
3.7 mg/kg D.W.
0.42
16 ]
3/18/19
6010C
Test America B 3
525
ARSENIC ICP Dry wt.
4.6 mg/kg D.W.
0.42
2.1
3/18/19
6010C
Test America B 3
1255
B-BHC-Beta Dry wt.
< 16 ug/kg D.W.
16
87
3/20/19
8081E
Test America B 3
1237
Benzidine Dry wt.
< 32000 ug/kg D.W.
32000
75000
3/18/19
8270D
Test America B 3
1238
Benzo(a)Anthracene Dry wt.
< 250 ug/kg D.W.
250
2500
3/18/19
8270D
Test America B 3
1239
Benzo(a)Pyrene Dry wt.
< 370 ug/kg D.W.
370
2500
3/18/19
8270D
Test America B 3
1240
Benzo(b)Fluoranthene Dry wt.
780 ug/kg D.W.
400
2500 1
3/18/19
8270D
Test America B 3
1241
Benzo(g,h,i)Perylene Dry wt.
< 270 ug/kg D.W.
270
2500
3/18/19
8270D
Test America B 3
1242
Benzo(k)Fluoranthene Dry wt.
< 330 ug/kg D.W.
330
2500
3/18/19
8270D
Test America B 3
528
BERYLLIUM ICP Dry wt.
0.067 mg/kg D.W.
0.029
0.21 1
3/18/19
6010C
Test America B 3
1256
BHC-Delta Dry wt.
< 16 ug/kg D.W.
16
87
3/20/19
8081E
Test America B 3
1243
Bis(2-Chloroethoicy)Methane Dry wt. < 540 ug/kg D.W.
540
2500
3/18/19
8270D
Test America B 3
1244
Bis(2-Chloroethyl)Ether Dry wt.
< 330 ug/kg D.W.
330
2500
3/18/19
8270D
Test America B 3
1245
Bis(2-Chloroisopropyl)Ether Dry wt.
< 510 ug/kg D.W.
510
2500
3/18/19
8270D
Test America B 3
1246
Bis(2-Ethy1hexy1)Phtha1ate Dry wt.
11000 ug/kg D.W.
870
2500
3/18/19
8270D
Test America B 3
526
BORON ICP Dry wt.
14 mg/kg D.W.
0.2
2.1
3/18/19
6010C
Test America B 3
1248
Butyl Benzyl Phthalate Dry wt.
< 420 ug/kg D.W.
420
2500
3/18/19
8270D
Test America B 3
530
CADMIUM ICP Dry wt.
0.67 mg/kg D.W.
0.031
0.21
3/18/19
6010C
Test America B 3
529
CALCIUM ICP Dry wt.
22000 mg/kg D.W.
3.5
52 AX.
3/18/19
6010C
Test America B 3
SYS/rpt5Genenc3 4111114 tj
Page 1 of 4
Printed: 4124119 08:39

1414SD
?allow 0 A CIIWR EYIIIQMMEIt
1305 Chlordane Dry wt.
< 190 ug/kg D.W.
Milorganite Priority Pollunant and VOC Analysis
Spring 2019
190 870 3/20/19 8081E Test America B 3
532
CHROMIUM ICP Dry wt.
210 mg/kg D.W.
0.21
0.52
3/18/19
6010C
Test America B
3
1251
Chrysene Dry wt.
670 ug/kg D.W.
570
2500 3
3/18/19
8270D
Test America B
3
531
COBALT ICP Dry wt.
4.2 mg/kg D.W.
0.052
0.52
3/18/19
6010C
Test America B
3
533
COPPER ICP Dry wt.
230 mg/kg D.W.
0.22
1
3/18/19
6010C
Test America B
3
263
Cyanide - Total (solids)
5 mg/kg D.W.
0.49
1 AX.
3/26/19
9012B
Test America B
3
1325
Dibenzo(a,h)Anthracene Dry wt.
< 450 ug/kg D.W.
450
2500
3/18/19
8270D
Test America B
3
1306
Dieldrin Dry wt.
< 21 ug/kg D.W.
21
87
3/20/19
8081E
Test America B
3
1314
1328
Diethyl Phthalate Dry wt.
Dimethyl Phthalate Dry wt.
< 330 ug/kg D.W.
< 300 ug/kg D.W.
330
300
2500
2500
3/18/19
3/18/19
8270D
8270D
Test America B
Test America B
3
3
1320
Di-n-Butylphthalate Dry wt.
< 430 ug/kg D.W.
430
2500
3/18/19
8270D
Test America B
3
1323
Dl-n-octyl phthalate Dry wt.
< 300 ug/kg D.W.
300
2500
3/18/19
8270D
Test America B
3
1261
Endosulfan alpha Dry wt.
< 17 ug/kg D.W.
17
87
3/20/19
8081B
Test America B
3
1262
Endosulfan beta Dry wt.
< 16 ug/kg D.W.
16
87
3/20/19
8081E
Test America B
3
1263
Endosulfan Sulfate Dry wt.
< 16 ug/kg D.W.
16
87
3/20/19
8081B
Test America B
3
1265
Endrin Aldehyde Dry wt.
< 22 ug/kg D.W.
22
87
3/20/19
8081B
Test America B
3
1264
Endrin Dry wt.
< 17 ug/kg D.W.
17
87
3/20/19
8081B
Test America B
3
1321
Fluoranthene Dry wt.
950 ug/kg D.W.
270
2500 3
3/18/19
8270D
Test America B
3
1316
Fluorene Dry wt.
< 300 ug/kg D.W.
300
2500
3/18/19
8270D
Test America B
3
1266
Heptachlor Dry wt.
< 19 ug/kg D.W.
19
87
3/20/19
8081E
Test America B
3
1267
Heptachlorepoxide Dry wt.
< 22 ug/kg D.W.
22
87
3/20/19
80818
Test America B
3
1330
1327
1308
1329
1326
534
Hexachlorobenzene Dry wt.
Hexachlorobutadiene Dry wt.
Hexachlorocyciopentadiene Dry wt.
Hexachloroethane Dry wt.
Indeno(1,2,3-cd)Pyrene Dry Wt.
IRON ICP Dry wt.
< 340 ug/kg D.W.
< 370 ug/kg D.W.
< 340 ug/kg D.W.
< 330 ug/kg D.W.
< 310 ug/kg D.W.
31000 mg/kg D.W.
340
370
340
330
310
3.7
2500
2500
2500
2500
2500
10 AX.
3/18/19
3/18/19
3/18/19
3/18/19
3/18/19
3/18/19
8270D
8270D
8270D
8270D
8270D
6010C
Test America B
Test America B
Test America B
Test America B
Test America B
Test America B
3
3
3
3
3
3
1311
Isophorone Dry wt.
< 540 ug/kg D.W.
540
2500
3/18/19
8270D
Test America B
3
544
LEAD ICP Dry wt.
35 mg/kg D.W.
0.25
1
3/18/19
6010C
Test America B
3
538
MAGNESIUM ICP Dry wt.
6400 mg/kg D.W.
0.97
21
3/18/19
6010C
Test America B
3
539
MANGANESE ICP Dry wt.
2100 mg/kg D.W.
0.034
0.21 AX.
3/18/19
6010C
Test America 8
3
428
MERCURY by M. 7471 (sludge)
0.28 mg/kg D.W.
0.0083
0.021
3/18/19
7471B
Test America B
3
540
1312
MOLYBDENUM ICP Dry wt.
Naphthalene Dry wt.
9.3 mg/kg D.W.
< 330 ug/kg D.W.
0.14
330
1
2500
3/18/19
3/18/19
6010C
8270D
Test America B
Test America B
3
3
542
NICKEL ICP Dry wt.
32 mg/kg D.W.
0.24
5.2
3/18/19
6010C
Test America B
3
1310
Nitrobenzene Dry wt.
< 280 ug/kg D.W.
280
2500
3/18/19
8270D
Test America B
3
1307
N-Nitrosodimethylamine Dry wt.
< 1100 ug/kg D.W.
1100
4900
3/18/19
8270D
Test America B
3
1309
N-Nitrosodi-n-propylamine Dry wt.
< 430 ug/kg D.W.
430
2500
3/18/19
8270D
Test America B
3
1313
N-Nitrosodiphenylamine Dry wt.
< 2100 ug/kg D.W.
2100
2500
3/18/19
8270D
Test America B
3
678
PCB-1016
< 0.041 mg/kg D.W.
0.041
0.21
3/17/19
8082A
Test America B 3
674
PCB-1221
< 0.041 mg/kg D.W.
0.041
0.21
3/17/19
8082A
Test America B 3
675
PCB-1232
< 0.041 mg/kg D.W:
0.041
0.21
3/17/19
8082A
Test America B 3
672
PCB-1242
< 0.041 mg/kg D.W.
0.041
0.21
3/17/19
8082A
Test America B 3
676
PCB-1248
< 0.041 mg/kg D.W.
0.041
0.21
3/17/19
8082A
Test America B 3
673
677
PCB-1254
PCB-1260
< 0.099 mg/kg D.W.
< 0.099 mg/kg D.W.
0.099
0.099
0.21
0.21
3/17/19
3/17/19
8082A
8082A
Test America B 3
Test America B 3
1224 p-Chloro-m-Cresol Dry wt. < 630 ug/kg D.W. 630 2500 3/18/19 8270D Test America B 3
1232 Pentachlorophenol Dry wt. < 2500 ug/kg D.W. 2500 4900 3/18/19 8270D Test America B 3
1319 Phenanthrene Dry wt. 390 ug/kg D.W. 370 2500 3 3/18/19 8270D Test America B 3
1233 Phenol Dry wt. < 390 ug/kg D.W. 390 2500 3/18/19 8270D Test America B 3
-- — -- -- - Page 2 0/ 4
SVS/rptWenenc3 4111114 tj Printed: 4124119 08:39

eiNSD
P1RTW3 01 WOR fWK11► O
543 PHOSPHORUS ICP Dry wt.
17000 mg/kg D.W.
Milorganite Priority Pollunant and VOC Analysis
Spring 2019
130 330 3/25/19 SM 4500 P E Test America B 3
1322
Pyrene Dry wt.
740 ug/kg D.W.
300
2500
3
3/18/19
8270D
Test America B 3
546
SELENIUM ICP Dry wt.
4.6 mg/kg D.W.
0.42
4.2
3/18/19
6010C
Test America B 3
523
SILVER ICP Dry wt.
2.3 mg/kg D.W.
0.21
0.63
3/18/19
6010C
Test America B 3
541
SODIUM ICP Dry wt.
1600 mg/kg D.W.
14
150
3/18t19
6010C
Test America B 3
1187
Solids for dry weight determination
(T 95 %
**
•••
3/18/19
Moisture
Test America B 3
1187
Solids for dry weight determination (T 96 %
"
••'
3/18119
Moisture
Test America B 3
1187
Solids for dry weight determination
(T 96 %
'•
'•'
3/18/19
Moisture
Test America B 3
550
THALLIUM ICP Dry wt.
< 0.31 mg/kg D.W.
0.31
6.3
3/18/19
6010C
Test America B 3
697
Total PCB Aroclors
< 0.099 mg/kg D.W.
0.099
0.21
3/17/19
8082A
Test America B 3
1268
Toxaphene Dry wt.
< 500 ug/kg D.W.
Soo
870
3/20/19
8081E
Test America B 3
1257
Y-BHC-Gamma(Lindane) Dry wt.
< 16 ug/kg D.W.
16
87
3/20/19
8081B
Test America 8 3
552
ZINC ICP Dry wt.
410 mg/kg D.W.
0.67
2.1
3/18/19
6010C
Test America B 3
3/11/19 SU
Sample Date Site Code
OpSID Test Name
WMC10
Customer ID
Reported Value
MDL
LOQ
Flags
Analysis Date
Method
19003869
LIMS Number
Lab S
1341
1,1,1-Trichloroethane Dry wt.
< 1.7 ug/kg D.W.
1.7
23
AX.
3/14/19
8260C
Test America B 3
1350
1,1,2,2-Tetrachloroethane Dry wt.
< 3.8 ug/kg D.W.
3.8
23
AX.
3/14/19
8260C
Test America B 3
1348
1,1,2-Trichloroethane Dry wt.
< 3 ug/kg D.W.
3
23
AX.
3/14/19
8260C
Test America B 3
1338
1,1-Dichloroethane Dry wt.
< 2.8 ug/kg D.W.
2.8
23
AX.
3/14/19
8260C
Test America B 3
1336
1,1-Dichloroethylene Dry wt.
< 2.8 ug/kg D.W.
2.8
23
AX.
3/14/19
8260C
Test America B 3
1355
1,2-Dichlorobenzene Dry Wt.
< 1.8 ug/kg D.W.
1.8
23
AX.
3/14/19
8260C
Test America B 3
1340
1,2-Dichloroethane Dry wt.
< 1.2 ug/kg D.W.
1.2
23
AX.
3/14/19
8260C
Test America B 3
1222
1,2-Dichloropropane Dry wt.
< 12 ug/kg D.W.
12
23
AX.
3/14/19
8260C
Test America B 3
1356
1,3-Dichlorobenzene Dry Wt.
< 1.2 ug/kg D.W.
1.2
23
AX.
3/14/19
8260C
Test America B 3
1357
1,4-Dichlorobenzene Dry Wt.
< 3.3 ug/kg D.W.
3.3
23
AX.
3/14/19
8260C
Test America B 3
1337
2-Chloroethylvinyl Ether Dry wt.
< 12 ug/kg D.W.
12
46
AX.
3/14/19
8260C
Test America B 3
1334
Acrolein Dry wt.
< 37 ug/kg D.W.
37
120
AX.
3/14/19
8260C
Test America B 3
1335
Acrylonitrile Dry wt.
< 21 ug/kg D.W.
21
120
AX.
3/14/19
8260C
Test America B 3
1346
Benzene Dry wt.
1.9 ug/kg D.W.
1.1
23
1 AX
3/14/19
8260C
Test America B 3
1343
Bromodichloromethane Dry wt.
< 3.1 ug/kg D.W.
3.1
23
AX.
3/14/19
8260C
Test America B 3
1219
Bromoform Dry wt.
< 12 ug/kg D.W.
12
23
AX.
3/14/19
8260C
Test America B 3
1342
Carbon Tetrachloride Dry wt.
< 2.2 ug/kg D.W.
2.2
23
AX.
3/14/19
8260C
Test America B 3
1352
Chlorobenzene Dry wt.
< 3.1 ug/kg D.W.
3.1
23
AX.
3/14/19
8260C
Test America B 3
1220
Chloroethane Dry wt.
< 5.2 ug/kg D.W.
5.2
23
AX.
3/14/19
8260C
Test America B 3
1339
Chloroform Dry wt.
1.4 ug/kg D.W.
1.4
23
1 AX
3/14/19
8260C
Test America B 3
1344
cis-1,3-Dichloropropene Dry wt.
< 3.3 ug/kg D.W.
3.3
23
AX.
3/14/19
8260C
Test America B 3
1347
Dibromochloromethane Dry wt.
< 3 ug/kg D.W.
3
23
AX.
3/14/19
8260C
Test America B 3
1353
Ethylbenzene Dry wt.
< 1.6 ug/kg D.W.
1.6
23
AX.
3/14/19
8260C
Test America B 3
1331
Methyl Bromide Dry wt.
< 2.1 ug/kg D.W.
2.1
23
AX.
3/14/19
8260C
Test America B 3
1354
Methyl Chloride dry wt.
< 1.4 ug/kg D.W.
1.4
23
AX.
3/14/19
8260C
Test America B 3
1333
Methylene Chloride Dry wt.
14 ug/kg D.W.
11
23
3 AX
3/14/19
8260C
Test America B 3
1187
Solids for dry weight determination
(T 94 %
••
- -
3/14/19
Moisture
Test America B 3
1349
Tetrachloroethylene Dry wt.
< 3.1 ug/kg D.W.
3.1
23
AX.
3/14/19
8260C
Test America B 3
1351
Toluene Dry wt.
4.9 ug/kg D.W.
1.8
23
1 AX
3/14/19
8260C
Test America B 3
1221
Trans-1,2-Dichloroethylene Dry wt.
< 2.4 ug/kg D.W.
2.4
23
AX.
3/14/19
8260C
Test America B 3
1223
Trans-1,3-Dichloropropene Dry wt.
< 10 ug/kg D.W.
10
23
AX.
3/14/19
8260C
Test America B 3
1345
Trichloroethylene Dry wt.
< 5.1 ug/kg D.W.
5.1
23
AX.
3/14/19
8260C
Test America B 3
SYS1rpt5Generic3 4111114 tj
Page 3 of 4
Printed: 4124119 08:39

)�NNSD
11111110
PilRIWIS M ,1 CAP €ih>"WIT
1332 Vinyl Chloride Dry wt.
Milorganite Priority Pollunant and VOC Analysis
Spring 2019
< 2.8 ug/kg D.W. 2.8 23 AX. 3/14/19 8260C Test America B 3
** The MDL for this test is the lowest level of precision shown, example: 4.1 would be "0.1".
*** The LOQ for this testis the lowest level of precision shown, example: 4.1 would be "0.1".
N.A. The MDL/LOQ is Not Available or Not Applicable for this test.
Column S: Test Status. Not Started=8, Intermediate=7, Final=3, Analyst Approved=12, Not Reportable=15.
Flag Descriptions
AO Other -- Flag requires additional explanation
AX Qualified data - see contract lab report
83 Target analyte detected in method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits.
BS LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
D1 Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
D5 The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
H1 Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
H5 Analysis performed beyond holding time.
140
IS Insufficient sample volume for analysis.
Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
LA Not analyzed - lab accident.
M1 Too numerous to count.
M2 Sample Incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
M5 Incubator/water bath temperature was outside method
requirements.
M7 Micro sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
SS Reading was not confirmed by a constant weight measurement
SD Supplemental details provided.(Water Quality only.)
T3 The dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
TS GGA BOD was above method acceptance criteria.
T7 The dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for SOD.
T9 Sample exceeded prescribed method temperature range.
SYS1rpt5Generic3 4111114 tj
Page 4 of 4
Printed: 4124119 08:39

r
• ak SD
18TIM" FOl A Ulm [O t owiv,
September
Monthly Milorganite:
Priority Pollutant and VOC Analysis
Fall 2019
1,2,4-Trichlorobenzene Dry wt.
9/20/19
< 2400 ug/kg D.W.
2400
Milo. Priority Pollutant Sample
19019216
8270D Test America Buffalo
1,2-Diphenylhydrazine Dry wt.
9/20/19
< 1900 ug/kg D.W.
1900
8270D
Test America Buffalo
2,4,6-Trichlorophenol Dry wt.
9/20/19
< 3400 ug/kg D.W.
3400
8270D
Test America Buffalo
2,4-Dichlorophenol Dry wt.
9/20/19
< 1800 ug/kg D.W.
1800
8270D
Test America Buffalo
2,4-Dimethylphenol Dry wt.
9/20/19
< 4100 ug/kg D.W.
4100
8270D
Test America Buffalo
2,4-Dinitrophenol Dry wt.
9/20/19
< 78000 ug/kg D.W.
78000
8270D
Test America Buffalo
2,4-Dinitrotoluene Dry wt.
9/20/19
< 3500 ug/kg D.W.
3500
8270D
Test America Buffalo
2,6-Dinitrotoluene Dry wt.
9/20/19
< 2000 ug/kg D.W.
2000
8270D
Test America Buffalo
2-Chloronaphthalene Dry wt.
9/20/19
< 2800 ug/kg D.W.
2800
8270D
Test America Buffalo
2-Chlorophenol Dry wt.
9/20/19
< 3100 ug/kg D.W.
3100
8270D
Test America Buffalo
2-Nitrophenol Dry wt.
9/20/19
< 4800 ug/kg D.W.
4800
8270D
Test America Buffalo
3,3'-Dichiorobenzidine Dry wt.
9/20/19
< 20000 ug/kg D.W.
20000
8270D
Test America Buffalo
4,4-DDD Dry wt.
9/20/19
< 3.3 ug/kg D.W.
3.3
8081B
Test America Buffalo
4,4-DDE Dry wt.
9/20/19
< 3.5 ug/kg D.W.
3.5
8081B
Test America Buffalo
4,4-DDT Dry wt.
9/20/19
< 3.9 ug/kg D.W.
3.9
8081B
Test America Buffalo
4,6-Dinitro-o-Cresol Dry wt.
9/20/19
< 17000 ug/kg D.W.
17000
8270D
Test America Buffalo
4-Bromophenyl Phenyl Ether Dry wt.
9/20/19
< 2400 ug/kg D.W.
2400
8270D
Test America Buffalo
4-Chloro-phenyl-phenyl ether Dry wt.
9/20/19
< 2100 ug/kg D.W.
2100
8270D
Test America Buffalo
4-Nitrophenol Dry wt.
9/20/19
< 12000 ug/kg D.W.
12000
8270D
Test America Buffalo
A-BHC-Alpha Dry wt.
9/20/19
4.7 ug/kg D.W.
3
3 AX
8081B
Test America Buffalo
Acenaphthene Dry wt.
9/20/19
< 2500 ug/kg D.W.
2500
8270D
Test America Buffalo
Acenaphthylene Dry wt.
9/20/19
< 2200 ug/kg D.W.
2200
8270D
Test America Buffalo
Aldrin Dry wt.
9/20/19
< 4.2 ug/kg D.W.
4.2
80818
Test America Buffalo
ALUMINUM ICP Dry wt.
9/17/19
4700 mg/kg D.W.
4.6
6010C
Test America Buffalo
Anthracene Dry wt.
9/20/19
< 4200 ug/kg D.W.
4200
8270D
Test America Buffalo
ANTIMONY ICP Dry wt.
9/16/19
3.9 mg/kg D.W.
0.42
3
6010C
Test America Buffalo
ARSENIC ICP Dry wt.
9/16/19
5.1 mg/kg D.W.
0.42
6010C
Test America Buffalo
B-BHC-Beta Dry wt.
9/20/19
< 3 ug/kg D.W.
3
80818
Test America Buffalo
Benzidine Dry wt.
9/20/19
< 210000 ug/kg D.W.
210000
8270D
Test America Buffalo
Benzo(a)Anthracene Dry wt.
9/20/19
< 1700 ug/kg D.W.
1700
8270D
Test America Buffalo
Benzo(a)Pyrene Dry wt.
9/20/19
< 2500 ug/kg D.W.
2500
8270D
Test America Buffalo
Benzo(b)Fluoranthene Dry wt.
9/20/19
< 2700 ug/kg D.W.
2700
8270D
Test America Buffalo
Benzo(g,h,I)Peryiene Dry wt.
9/20/19
< 1800 ug/kg D.W.
1800
8270D
Test America Buffalo
Benzo(k)Fluoranthene Dry wt.
9/20/19
< 2200 ug/kg D.W.
2200
8270D
Test America Buffalo
BERYLLIUM ICP Dry wt.
9/16/19
0.12 mg/kg D.W.
0.029
3
6010C
Test America Buffalo
BHC-Delta Dry wt.
9/20/19
4.5 ug/kg D.W.
3.1
3 AX
8081B
Test America Buffalo
Bis(2-Chloroethoxy)Methane Dry wt.
9/20/19
< 3600 ug/kg D.W.
3600
8270D
Test America Buffalo
Bis(2-Chloroethyl)Ether Dry wt.
9/20/19
< 2200 ug/kg D.W.
2200
8270D
Test America Buffalo
Sis(2-Chloroisopropyl)Ether Dry wt.
9/20/19
< 3400 ug/kg D.W.
3400
8270D
Test America Buffalo
Bis(2-Ethylhexyl)Phthalate Dry wt.
9/20/19
6300 ug/kg D.W.
5800
3
8270D
Test America Buffalo
BORON ICP Dry wt.
9/16/19
20 mg/kg D.W.
0.2
AX.
6010C
Test America Buffalo
Butyl Benzyl Phthalate Dry wt.
9/20/19
< 2800 ug/kg D.W.
2800
8270D
Test America Buffalo
CADMIUM ICP Dry wt.
9/16/19
0.33 mg/kg D.W.
0.031
6010C
Test America Buffalo
CALCIUM ICP Dry wt
9/16/19
24000 mg/kg D.W.
3.5
6010C
Test America Buffalo
SYS/rpt 1 MitoPP 1/10/13 tj
Page 1 of 5
Printed: 11120119 08:32

Monthly Milorganite: Priority Pollutant and VOC Analysis
Fall 2019
14MSD
P)p7AER's Fw d CLIM twit mom
September
Milo. Priority Pollutant Sample
9216
a
Chlordane Dry wt. 9/20/19 < 37 ug/kg D.W. 37 8081B Test America Buffalo
CHROMIUM ICP Dry wt. 9/16/19 190 mg/kg D.W. 0.21 6010C Test America Buffalo
Chrysene Dry wt.
COBALT ICP Dry wt.
9/20/19
9/16/19
< 3800 ug/kg D.W.
3.4 mg/kg D.W.
3800
0.052
8270D
6010C
Test America Buffalo
Test America Buffalo
COPPER ICP Dry wt.
9/16/19
220 mg/kg D.W.
0.22
6010C
Test America Buffalo
Cyanide - Total (solids)
9/26/19
4 mg/kg D.W.
0.48
AX.
9012B
Test America Buffalo
Dibenzo(a,h)Anthracene Dry wt.
9/20/19
< 3000 ug/kg D.W.
3000
8270D
Test America Buffalo
Dieldrin Dry wt.
9/20/19
< 4.1 ug/kg D.W.
4.1
80818
Test America Buffalo
Diethyl Phthalate Dry wt.
9/20/19
< 2200 ug/kg D.W.
2200
8270D
Test America Buffalo
Dimethyl Phthalate Dry wt.
9/20/19
< 2000 ug/kg D.W.
2000
8270D
Test America Buffalo
Di-n-Butylphthalate Dry wt.
9/20/19
< 2900 ug/kg D.W.
2900
8270D
Test America Buffalo
Dl-n-octyl phthalate Dry wt.
9/20/19
< 2000 ug/kg D.W.
2000
8270D
Test America Buffalo
Endosulfan alpha Dry wt.
9/20/19
< 3.2 ug/kg D.W.
3.2
8081B
Test America Buffalo
Endosulfan beta Dry wt.
9/20/19
< 3 ug/kg D.W.
3
8081B
Test America Buffalo
Endosulfan Sulfate Dry wt.
Endrin Aldehyde Dry wt.
9/20/19
9/20/19
6.6 ug/kg D.W.
5.1 ug/kg D.W.
3.1
4.3
J
J AX
8081B
8081B
Test America Buffalo
Test America Buffalo
Endrin Dry wt.
9/20/19
< 3.3 ug/kg D.W.
3.3
8081B
Test America Buffalo
Fluoranthene Dry wt.
9/20/19
< 1800 ug/kg D.W.
1800
8270D
Test America Buffalo
Fluorene Dry wt.
9/20/19
< 2000 ug/kg D.W.
2000
8270D
Test America Buffalo
Heptachlor Dry wt.
9/20/19
< 3.7 ug/kg D.W.
3.7
8081B
Test America Buffalo
Heptachlorepoxide Dry wt.
9/20/19
< 4.4 ug/kg D.W.
4.4
8081B
Test America Buffalo
Hexachlorobenzene Dry wt.
9/20/19
< 2300 ug/kg D.W.
2300
8270D
Test America Buffalo
Hexachtorobutadiene Dry wt.
9/20/19
< 2500 ug/kg D.W.
2500
8270D
Test America Buffalo
Hexachtorocyctopentadiene Dry wt.
Hexachloroethane Dry wt.
9/20/19
9/20/19
< 2300 ug/kg D.W.
< 2200 ug/kg D.W.
2300
2200
8270D
8270D
Test America Buffalo
Test America Buffalo
Indeno(1,2,3-cd)Pyrene Dry Wt.
9/20/19
< 2100 ug/kg D.W.
2100
8270D
Test America Buffalo
IRON ICP Dry wt.
9/16/19
42000 mg/kg D.W.
3.7
6010C
Test America Buffalo
Isophorone Dry wt.
LEAD ICP Dry wt.
9/20/19
9/16/19
< 3600 ug/kg D.W.
35 mg/kg D.W.
3600
0.25
8270D
6010C
Test America Buffalo
Test America Buffalo
MAGNESIUM ICP Dry wt.
9/16/19
7000 mg/kg D.W.
0.97
6010C
Test America Buffalo
MANGANESE ICP Dry wt.
9/16/19
1800 mg/kg D.W.
0.034
6010C
Test America Buffalo
MERCURY by M. 7471 (sludge)
9/17/19
0.25 mg/kg D.W.
0.0083
7471B
Test America Buffalo
MOLYBDENUM ICP Dry wt.
9/16/19
9.4 mg/kg D.W.
0.14
AX.
6010C
Test America Buffalo
Naphthalene Dry wt.
9/20/19
< 2200 ug/kg D.W.
2200
8270D
Test America Buffalo
NICKEL ICP Dry wt.
9/16/19
23 mg/kg D.W.
0.24
6010C
Test America Buffalo
Nitrobenzene Dry wt.
9/20/19
< 1900 ug/kg D.W.
1900
8270D
Test America Buffalo
N-Nitrosodimethylamine Dry wt.
9/20/19
< 7200 ug/kg D.W.
7200
8270D
Test America Buffalo
N-Nitrosodi-n-propylamine Dry wt.
9/20/19
< 2900 ug/kg D.W.
2900
8270D
Test America Buffalo
N-Nitrosodiphenylamine Dry wt.
PCB-1016
PCB-1221
9/20/19
9/17/19
9/17/19
< 14000 ug/kg D.W.
< 0.043 mg/kg D.W.
< 0.043 mg/kg D.W.
14000
0.043
0.043
8270D
8082A
8082A
Test America Buffalo
Test America Buffalo
Test America Buffalo
PCB-1232
9/17/19
< 0.043 mg/kg D.W.
0.043
8082A
Test America Buffalo
PCB-1242
9/17/19
< 0.043 mg/kg D.W.
0.043
8082A
Test America Buffalo
PCB-1248
9/17/19
< 0.043 mg/kg D.W.
0.043
8082A
Test America Buffalo
SYS/rptIWoPP 1/10/13 tj
Page 2 of 5
Printed: 11/20/19 08:32

f
M
Monthly Milorganite: Priority Pollutant and VOC Analysis
14MSD Fall 2019
?1F.TM, W A Cli lttt!IC01,11'
September
Milo. Priority Pollutant Sample
19019216
-",,Analyzed Result LOD..
PCB-1254 9/17/19 < 0.1 mg/kg D.W. 0.1 8082A Test America Buffalo
PCB-1260
9/17/19
< 0.1 mg/kg D.W.
0.1
8082A
Test America Buffalo
p-Chloro-m-Cresol Dry wt.
9/20/19
< 4200 ug/kg D.W.
4200
8270D
Test America Buffalo
Pentachlorophenol Dry wt.
9/20/19
< 17000 ug/kg D.W.
17000
8270D
Test America Buffalo
Phenanthrene Dry wt.
9/20/19
< 2500 ug/kg D.W.
2500
8270D
Test America Buffalo
Phenol Dry wt.
9/20/19
< 2600 ug/kg D.W.
2600
8270D
Test America Buffalo
PHOSPHORUS ICP Dry wt.
9/21/19
15000 mg/kg D.W.
140
SM 4500 P E
Test America Buffalo
POTASSIUM ICP Dry wt.
9/16/19
3000 mg/kg D.W.
21
6010C
Test America Buffalo
Pyrene Dry wt.
9/20/19
< 2000 ug/kg D.W.
2000
8270D
Test America Buffalo
SELENIUM ICP Dry wt.
9/16/19
2.6 mg/kg D.W.
0.42 3
6010C
Test America Buffalo
SILVER ICP Dry wt.
9/16/19
1.9 mg/kg D.W.
0.21
6010C
Test America Buffalo
SODIUM ICP Dry wt.
9/16/19
1400 mg/kg D.W.
14
6010C
Test America Buffalo
Solids for dry weight determination (Test America)
9/13/19
97 %
0.1
Moisture
Test America Buffalo
Solids for dry weight determination (Test America)
M %
N/A
Calculated value
DEFAULT
THALLIUM ICP Dry wt.
9/16/19
1.1 mg/kg D.W.
0.31 3
6010C
Test America Buffalo
Total PCB Arodors
9/17/19
< 0.1 mg/kg D.W.
0.1
8082A
Test America Buffalo
Toxaphene Dry wt.
9/20/19
< 98 ug/kg D.W.
98
8081B
Test America Buffalo
Y-BHC-Gamma(Lindane) Dry wt.
9/20/19
< 3.1 ug/kg D.W.
3.1
8081B
Test America Buffalo
ZINC ICP Dry wt.
9/16/19
370 mg/kg D.W.
0.67
6010C
Test America Buffalo
Page 3 o/ 5
SYS/rptIMiloPP 1/10/13 tj Printed. 11/20/19 08:32

NSD
?1>C;NE£; FI1i a Ctil34� fttiiRkliMCil'
September
Monthly Milorganite:
Priority Pollutant and VOC Analysis
Fall 2019
9/9/19
1,1,1-Trichloroethane Dry wt.
1,1,2,2-Tetrachloroethane Dry wt.
1,1,2-Trichloroethane Dry wt.
1,1-Dichloroethane Dry wt.
9/23/19
9/23/19
9/23/19
9/23/19
< 59 ug/kg D.W.
< 34 ug/kg D.W.
< 45 ug/kg D.W.
< 66 ug/kg D.W.
59
34
45
66
Milo. Priority Pollutant Sample
8260C Test America Buffalo
8260C Test America Buffalo
8260C Test America Buffalo
8260C Test America Buffalo
1,1-Dichloroethylene Dry wt.
1,2-Dichlorobenzene Dry Wt.
9/23/19
9/23/19
< 73 ug/kg D.W.
< 54 ug/kg D.W.
73
54
8260C
8260C
Test America Buffalo
Test America Buffalo
1,2-Dichloroethane Dry wt.
1,2-Dichioropropane Dry wt.
1,3-Dichlorobenzene Dry Wt.
1,4-Dichlorobenzene Dry Wt.
2-Chloroethylvinyl Ether Dry wt.
9/23/19
9/23/19
9/23/19
9/23/19
9/23/19
< 87 ug/kg D.W.
< 34 ug/kg D.W.
< 57 ug/kg D.W.
< 30 ug/kg D.W.
< 68 ug/kg D.W.
87
34
57
30
68
8260C
8260C
8260C
8260C
8260C
Test America Buffalo
Test America Buffalo
Test America Buffalo
Test America Buffalo
Test America Buffalo
Acrolein Dry wt.
9/23/19
< 430 ug/kg D.W.
430
8260C
Test America Buffalo
Acrylonitrile Dry wt.
9/23/19
< 530 ug/kg D.W.
530
8260C
Test America Buffalo
Benzene Dry wt.
9/23/19
< 40 ug/kg D.W.
40
8260C
Test America Buffalo
Bromodichloromethane Dry wt.
9/23/19
< 42 ug/kg D.W.
42
8260C
Test America Buffalo
Bromoform Dry wt.
9/23/19
< 110 ug/kg D.W.
110
8260C
Test America Buffalo
Carbon Tetrachloride Dry wt.
9/23/19
< 54 ug/kg D.W.
54
8260C
Test America Buffalo
Chlorobenzene Dry wt.
9/23/19
< 28 ug/kg D.W.
28
8260C
Test America Buffalo
Chloroethane Dry wt.
9/23/19
< 44 ug/kg D.W.
44
8260C
Test America Buffalo
Chloroform Dry wt.
9/23/19
< 150 ug/kg D.W.
150
8260C
Test America Buffalo
cis-1,3-Dichloropropene Dry wt.
9/23/19
< 51 ug/kg D.W.
51
8260C
Test America Buffalo
Dibromochloromethane Dry wt.
9/23/19
< 100 ug/kg D.W.
100
8260C
Test America Buffalo
Ethylbenzene Dry wt.
9/23/19
< 62 ug/kg D.W.
62
8260C
Test America Buffalo
Methyl Bromide Dry wt.
Methyl Chloride dry wt.
9/23/19
9/23/19
< 47 ug/kg D.W.
< 51 ug/kg D.W.
47
51
8260C
8260C
Test America Buffalo
Test America Buffalo
Methylene Chloride Dry wt.
9/23/19
< 42 ug/kg D.W.
42
8260C
Test America Buffalo
Solids for dry weight determination (Test America)
9/12/19
92 %
0.1
Moisture
Test America Buffalo
Tetrachloroethylene Dry wt.
Toluene Dry wt.
9/23/19
9/23/19
< 29 ug/kg D.W.
160 ug/kg D.W.
29
57 1
8260C
8260C
Test America Buffalo
Test America Buffalo
Trans-1,2-Dichloroethylene Dry wt.
9/23/19
< 50 ug/kg D.W.
50
8260C
Test America Buffalo
Trans-1,3-Dichloropropene Dry wt.
9/23/19
< 21 ug/kg D.W.
21
8260C
Test America Buffalo
Trichloroethylene Dry wt.
9/23/19
< 59 ug/kg D.W.
59
8260C
Test America Buffalo
Vinyl Chloride Dry wt.
9/23/19
< 71 ug/kg D.W.
71
8260C
Test America Buffalo
Page 4 of 5
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e-NIOD
PJAtl E foa i clue WOMEN!
Monthly Milorganite: Priority Pollutant and VOC Analysis
Fall 2019
140
00000
2
AO Other -- Flag requires additional explanation
AX Qualified data - see contract laboratory report
B3 Target analyte detected in method blank > 10% of sample
concentration.
87 LCS recovery was above control limits.
68 LCS recovery was below control limits.
89 Low Level CCV recovery was outside of method acceptance limits
CQ Data used for calculation of result was qualified
D1 Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix Interferences did not allow completing the analysis.
D5 The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
H1 Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
H5 Analysis performed beyond holding time.
IS Insufficient sample volume for analysis.
7 Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit
LA Not analyzed - laboratory accident.
M1 Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result. _
M4 Results are an approximation due to spreading colonies.
M5 Incubator/water bath temperature was outside method
requirements.
M7 Microbiology sample received without adequate headspace.
M9 Target organism detected In associated method blank.
NR Not usable data. (Water Quality only.)
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
S5 Reading was not confirmed by a constant weight measurement
SD Supplemental details provided.(Water Quality only.)
T3 The BOD dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
T5 GGA BOD was above method acceptance criteria.
T7 The BOD dilution water D.O. Increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample is outside of the prescribed method temperature range.
SYS/rpt 1 MiIoPP 1/10/13 tj
Page 5 of 5
Printed: 11120119 08:32