HomeMy WebLinkAboutWQ0000455_Residual Annual Report 2019_20200210Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submital an
application?*
r Yes r No
Annual Report 2019
Year*
Date Paper Copy 2/10/2020
Received:*
Project Number* WQ0000455
Email Notifications
...................................................................................................
Does this need O Yes
review by the a No
hydrogeologist? *
Regional Office
CO Reviewer
Admin Reviewer Kendall.Williams@ncdenr.gov
Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NJB Staff regarding electronic submittal, confirmation of receipt, and other issues.
....................................................................................................................................................................................................................................................................................................................................................................................................
Name * Martin Mabe
Email Address*
martin@willcoxmabesoil.com
Project Information
........................................................................................................................................................................
Submittal Type* f New Permit Application
r Renewal
r Annual Report
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0000455
Applicant\Permittee * Wesley Wooten
Facility Name * Lewis Farms and Liquid Waste, Inc.
Phone Number*
3363121396
r Modification (Major or Minor)
r Additional Information
r Other
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
One hardcopy is also being mailed to NCDEQ-DWR-NDCU
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
Lewis Farms'19 Annual Report (NCDEQ).pdf 24.56MB
Upload only 1 R7F document. K/Ultiple documents rust becombined into one RJF file.
For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contact the reviewer or Tessa Monday. If a paper application is required,
be advised, applications accepted for pre -review until both the paper and electronic copies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments (caIcs, sails report, specs, etc,}
o one full-size engineering plan set
0 one 11x17" engineering plan set
0 one extra set of specifications
o Fee (if required}
Mailine address:
Division of Water Resources Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
---- --- - --- - --- ------------ ------------------------------------i----------------------------------------------------------------------------
1617 Mail -service Center Att: Nathaniel Thornburg, 9"' Floor, Office #942W
---- -NC �-- - -------------------------------------------- ------------------------------------------------
Raleih, 7699-1617 512 N. SaVisbury St
For questions or problems contact Tessa Monday at tessa.monday@ncdenr.Qov or 919.707.3660.
* W By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/6/2020
2019 ANNUAL REPORT
LAND APPLICATION PROGRAM
LEWIS FARMS AND LIQUID WASTE, INC.
PERMIT #WQ0000455
Prepared For:
Lewis Farms and Liquid Waste, Inc.
8155 Malpass Corner Road
Currie, North Carolina 28435
Compiled By:
Willcox & Mahe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
February 2020
i
willcox&mabe
SOIL SOLUTIONS
February 6, 2020
NCDEQ-DWR Non -Discharge Compliance Unit
512 North Salisbury Street
9a` Floor, Office 942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Compliance Unit
Reference: 2019 LAND APPLICATION ANNUAL REPORT
Lewis Farms and Liquid Waste, Inc.
Permit No. WQ0000455
WMSS Project No. 15-20 Ph: 01
Non -Discharge Compliance Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Lewis Farms and Liquid
Waste, Inc. (Lewis Farms). WMSS compiled this report using data gathered during the
compliance year by Lewis Farms. This data includes: 1) certification form, 2) residuals
analyses and pathogen / vector data, 3) application summaries and field loading rate reports,
and 4) soil analyses.
If there is any finther information required or questions regarding this annual report please do
not hesitate to contact Lewis Farms or WMSS for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
A41A,k
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosures
Shamd\WMSS Proiects\2015\i 5-20 Lewis Farms\2019 Annual Reportt2019 ANNUAL REPORT.doc
Willcox & Mabe Soil Solutions, PLLC 17231 B Summerfield Road / Summerfield, NC 27358 / Rob336.339.9128 or
Martin 336.312.1396 /www.willcoxmabesoil.com
TABLE OF CONTENTS
SECTION NO. TITLE
Certification Form
H Residuals Analyses & Pathogen / Vector Attraction Data
III 2019 Application Summary and Field Loading Rate Reports
IV Soil Analysis
CERTIFICATION FORM
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00000455 County: Pender Year: 2019
Facility Name (as shown on permit): Lewis Farms and Liquid Waste, Inc.
Land Application Operator: Mr. Wesley Wooten Phone: 910-283-5444
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Annlication Summnrve
Total number of application fields in thepermit:
19
Total number of fields utilized for land application during the year:
11
Total amount of dry tons applied during the year for all application sites:
489.70
Total number of acres utilizes for land application during the year:
285.20
Part B - Annual Commiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Mr. Wesley Wooten, President 2/3/2020
Permittee Name and Title (type or print) Signature f Permittee Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)
RESIDUAL ANALYSES
TCLP ANALYSES IF REQUIRED
AND PATHOGEN AND VECTOR ATTRACTION REDUCTION
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LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type. Wastewater Treatment Plant
Date Sampled: February 12, 2019
Bald Head Island Permit No. WQ0000455
Mineralization Rate 0.30 3.92 % Solids
7.17 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
x 0.002)
Nitrogen (TKN)
3.840
38,400.000
76.800
Phosphorus
5.050
50,500.000
1O1.000
Potassium
0.339
3,390.000
6.780
PAN (injected)*
1.272
12 722.000
25.444
PAN (surface)*
1.199
11,987.000
23.974
Ammonia Nitrogen
0.147
1,470.000
2.940
Calcium
2.740
27,400.000
54.800
Calcium Carbonate E .
---
Magnesium
9,590.000
19.180
Sodium
2,130.000
4.260
Sulfur
Nitrate N / Nitrite N
---
173.000
0.346
Barium
___
___
SAR
Chloride
---
—
0.56
Iron
--
---
Ceiling Concen.
Aluminum
---
97,200.00
194.400
M
Arsenic
14.40
0.029
75
Cadmium
---
14.40
0.029
85
Chromium
--
30.600
--
-
Copper
594.00
L188
4,300
Lead
---
14.40
0.029
840
Mercury
0.510
0.001
57
Molybdenum
14.40
0.029
75
Nickel
42.30
0.085
420
Selenium
14.40
0.029
100
Zinc
---
1,440.00
2.880
7 500
Environmental Chemists, Inc. # 2019-02427
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
41',
�`pEnvi °onme���.1tal Chem sts, Inc®
E,�. p6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ^ 910.392.4424 Fax
710BowsertownRoad,Manteo,NC27954 • 252.473.5702Lab/Fax
" i '1 255-A WiLnington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.eom
Lewis Farms & Liquid Waste, INC. Date of Report: Feb 27, 2019
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-02427
Project ID: Bald Head WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-06137 Site: Sludge 2/12/2019 1:00 PM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA200.7
97200mg/kg
02/1812019
Arsenic
EPA 200.7
<14.4 mg/kg
02/18/2019
Cadmium
EPA 200.7
<14.4mg/kg
02/18/2019
Calcium
EPA 200.7
27400mg/kg
02/1512019
Chromium
EPA 200.7
30.6mg/kg
02/16/2019
Copper
EPA 200.7
594mg/kg
02118/2019
Lead
EPA 200.7
<14.4 mg/kg
02/1812019
Magnesium
EPA 200.7
9590mglkg
02/15/2019
Molybdenum
EPA 200.7
<14.4mg/kg
02/17/2019
Nickel
EPA 200.7
42.3mg/kg
02/18/2019
Potassium
EPA 200.7
3390mg/kg
02/15/2019
Selenium
EPA 200.7
<14.4mg/kg
02/18/2019
Sodium
EPA 200.7
2130mg/kg
02/15/2019
Zinc
EPA 200.7
1440mg/kg
02117/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
173mg/kg
02/21/2019
Total Solids (%)
SM 2540 B
3.92 %
02/14/2019
pH
SM 4500 H B
7.17 units
02/2012019
Ammonia Nitrogen
SM 4500 NH3 C
1470 mg/kg
02/20/2019
Total Kjeldahl Nitrogen (TKN)
SM45000rgB
38400mg/kg
02/20/2019
Total Phosphorus
SM 4500 P F
50500 mg/kg
02/24/2019
Mercury
Sw5467471B
<0.510mg/kg
02/23/2019
Ra rr s- 7io.n?A?,
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ^ 910.392,4424 Fax
710 Bowsertown load, Manteo, NC 27954 • 252.4735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.341.5843 Lab/Fax
in fo(ne nvi ron men to Ic hemist s. co m
Lewis Farms & Liquid Waste, INC. Date of Report: Feb 27, 2019
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-02427
Project ID: Bald Head WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-06138 Site: 1 2/12/2019 1:05 PM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 G
SM 9221C E MPN 24 hr 503
4.23 %
5674 MPN/g
02/13/2019
02/13/2019
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
19-06139 Site: 2
2/12/2019 1:06 PM
Solid/Sludge Client
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
4.27 %
02/13/2019
Fecal Density _
SM 9221C E MPN 24 hr 503
3982 MPN/g
02/13/2019
Lab ID
Sample ID:
Collect Date/Time
Matrix
Sampled by
19-06140
Site: 3
2/12/2019 1:07 PM
Solid/Sludge
Client
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
4.47 %
02/13/2019
Fecal Density
SM 9221C E MPN 24 hr 503
4922 MPN/g 02/13/2019
Lab ID
Sample ID:
Collect Date/Time
Matrix
Sampled by
19-06141
Site: 4
2/12/2019 1:08 PM
Solid/Sludge
Client
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
4.24 %
02/13/2019
Fecal Density
SM 9221C E MPN 24 hr 503
2595 MPN/g
02/13/2019
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
19-06142 Site: 5
2/12/2019 1:09 PM
Solid/Sludge Client
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
4.24 %
02/13/2019
Fecal Density
SM 9221C E MPN 24 hr 503
5661 MPN/g
02/13/2019
%1'
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inca
6602 windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertotvn lioad, ivlanteo, NC 27954 0 252.473.5702 Lab/Fax
255-A Wilmington Higluvay, Jacksonville, NC 28540 • 910.347.5843 Lab/Pax
in ro(u,environmen talchemi s'ts.cont
Lewis Farms & Liquid Waste, INC. Date of Report: Feb 27, 2019
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-02427
Project ID: Bald Head WWTP
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
19-06143 Site: 6 2/12/2019 1:10 PM Solid/Sludge Client
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-06144 Site:7
Test
Total Solids (%)
Fecal Density
Method
SM 2540 G
SM 9221C E MPN 24 hr 503
Collect Date/Time
2/12/2019 1:11 PM
Method
SM 2540 G
SM 9221C E MPN 24 hr 503
Results
4.31 %
1625 MPN/g
Matrix
Solid/Sludge
Results
Date Ana lyzec
02/13/2019
02/13/2019
Sampled by
Client
Date
4.29 % 02113/2019
3031 MPN/q 02/13/2019
Comment: `Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms & Liquid Waste, Inc.
WWTP Name: Bald Head Island
Monitoring Period: From 1/1/2019
WQ Permit Number: WQ0000455
NPDES Number: W00000193
To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indientp Ipvpl nehipvPA .,,,]
Class A:
Alt. A (time/temp) ❑
• - -.
Alt B (Alk Treatment) ❑
�v �„v ,,.ay. .au aa. ar rJYLV• IGY,
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
IIeatTreatment ❑ Thentlophdic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density El
I Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ I Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
Frequency
of Analysis
Sample
Type
na nca
y
Tech-
Minimu
Geo. Mean
Maximur
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
1,625
3,614
5,674
MPN/g
0
Annual
Grab
SM 922JCE
CFU
1000 mpn per gram
of total solid (dry
wei ht)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight
r a:YLVA huI "cuvu �ouucuuu tl3a9 119.1AI. U61 ,11U! 1 - Please Indicate alternative nerfnrmad-
JAIL (VS reduction) ❑
Alt. 2 (40-day bench) ❑
_____. _
Alt. 3 (30-day bench) ❑
r_______--_.
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
jAlt. 6 (Alk. Stabilization ❑
I Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) p
�nrlmrr. rr. a
jAlt. 10 (Incorporation) Rl
INo vector attraction reduction alternatives were performed ❑
� IIll 1.. it AMIN 01a1n1nr,ry l tpiease check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
has been made
with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David Suther, ORC Wesley Wooten, President
Preparer Name and Title print) Land Applier Name and Title (if applicable)(type or print)
- 2-10 "/i ! ♦ 3/6/19
Signature of Preparer* Date Signature of La Applier• (if applicable) Date
my atrection and
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
LEWIS FARMS
WQ0000455
Bald Head Island
Date
Fecal Coliform
MPN per gram
Log
02/12/19
5,674
3.7539
02/12/19
3,982
3.6001
02/12/19
4,922
3.6921
02/12/19
2,595
3.4141
02/12/19
1 5,661
3.7529
02/12/19
1 1,625
3.2109
02/12/19
1 3,031
3.4816
Total 24.9056
Average 3.5579
Geometric Mean Fecal Coliform MPN / gram
3,614
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen for Reduction
requirement.
LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 2, 2019
Beau Rivaee
2.80 % Solids
6.82 pH
Permit No. W00000455
Parameter
%
Mg/Kg Dry Weigh t
% x 10,000)
Pounds/DtyTon
(M x 0.002)
Nitrogen (TKN)
4.220
42,200.000
84.400
Phosphorus
2.230
22,300.000
44.600
Potassium
0.265
2,650.000
5.300
PAN (injected)*
2.015
20 145.000
40.290
PAN (surface)*
1.937
19 370.000
38.740
Ammonia Nitrogen
0.155
1,550.000
3.100
Calcium
3.850
38,500.000
77.000
Calcium Carbonate E .
---
---
---
Magnesium
1980.000
3.960
Sodium
3,370.000
6.740
Sulfur
Nitrate N / Nitrite N
-
6,400.000
12.800
Barium
Chloride
---
--_
---
Iron
Aluminum
---
7,000.00
14.000I
Arsenic
---
11.00
0.022
Cadmium
--
11.00
0.022
Chromium
---
17.900
Copper
-
364.00
0.728
Lead
---
17.20
0.034
Mere
1.860
0.004
Molybdenum
11.00
0.022
Nickel
11.50
0.023
Selenium
11.00
0.022
Zinc
--
4,140.00
8.280
1
Environmental Chemists, Inc. # 2019-05318
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
SAR
0.76
Ceiling Concert.
(Mg/Ka)
75
85
4,300
840
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
Environmental Chemists, Inc.
qiwcl��
6602 WindmillWay, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Apr 25, 2019
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2019-05318
Project ID: AquaNC-Beau Rivage
Lab ID Sample ID: Collect Daterrime Matrix Sampled by
19-13335 Site: Sludge 4/2/2019 1:00 PM Solid/Sludge wesley wooten
Test Method Results Date
Chlordane (TCLP)
SW 846 Method 8081813610
<0.02 mg1L
04/11/2019
Endrin(TCLP)
SW 846 Method 8081 B1351 0
<0.0005mg/L
04/11/2019
Heptachlor (TCLP)
SW 846 Method 808 1 B/351 0
<0.0005mg/L
04/11/2019
Heptachlor epoxide (TCLP)
SIN B46Method 8081B/3510
<0.0005mg/L
04/11/2019
Lindane(TCLP)
SW 846 Method 808 1 B/351 0
<0.0005mg/L
04/11/2019
Methoxychlor(TCLP)
SW 846 Method 8081 B/351 0
<0.0005mg/L
04111/2019
Toxaphene (TCLP)
SW 846 Method 8081BI3510
<0.05 mg/L
04/11/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
04/11/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 827013510
<0.050 mg/L
04/11/2019
2,4,6-Trlchlorophenol (TCLP)
SW 846 method 8270/3610
<0.050 mg/L
04/11/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
04/11/2019
Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
04/11/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 82701351 0
<0.050 mg/L
04/1112019
Hexachlorobenzene (TCLP)
SW 848 method 827013510
<0.050 mg/L
04/11/2019
Hexachloroethane (TCLP)
SW 846 method 827013510
<0.050 mg/L
04/11/2019
m + p-Cresol (TCLP)
SW 846 method 627MS10
<0.050 mg/L
04/11/2019
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050mg/L
04/1112019
o-Cresol(TCLP)
SW 846 method827013510
<0.050mg/L
04/11/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
04/11/2019
Pyridine (TCLP)
SW 846 method 827013510
<0.050 mg/L
04/11/2019
2,4,5-TP(TCLP)
SW846 Method8151A
<0.003mg/L
04/15/2019
2,4-D (TCLP)
SW846 Method 8151A
<0.003 mg/L
04/1512019
1,1-Dichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
04/10/2019
1,2-Dichloroethane (TCLP)
SW846 Method 826015030
<0.01 mg/L
04/10/2019
Benzene (TCLP)
SW848 Method 826015030
<0.01mg/L
0411012019
Carbon Tetrachloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
04/10/2019
Report#;: 2019-0531B
Pagel of
Environmental Chemists, Inc.
1 11111111IF 6602 Windmill VVay, Wilmington, NC 28405 e 910392.0223 Lab • 910.392.4424 Fax
7'10 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@emvironmentalchcmists.com
Lewis Farms & Liquid Waste, INC.
Date of Report: Apr 25, 2019
8155 Malpass Corner Road
Customer PO #:
Currie NC 28435
Customer ID: 14020008
Attention: Wesley Wooten
Report #: 2019-05318
Project ID: AquaNC-Beau Rivage
Chlorobenzene(TCLP)
SW846 Method 8260/5030
<0.01mg/L
04/10/2019
Chloroform (TCLP)
SW846 Method 826015030
<0.01 mg/L
04/1012019
Methyl ethyl ketone (TCLP)
SW846Method 626015030
<0.05mg/L
04/1012019
Tetrachloroethylene(TCLP)
SW846 Method 826015030
<0.01mg/L
04/10/2019
Trichlomethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
04/10/2019
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
04/10/2019
RCI
Cyanide
EPA335.4
0.159mg/kg
04/04/2019
Sulfide
Analyzed outside of hold time.
SM4500S0
0.38mg/kg
0411012019
Ignitability
SW 846 method 1010
>190OF
04/1012019
pH
SW 846 Method 90450
6.82 units
04/05/2019
Sludge Residuals
Aluminum
EPA200.7
7000mg/kg
04/10/2019
Arsenic
EPA200.7
<11.0 mg/kg
04/06/2019
Cadmium
EPA200.7
<11.0mg/kg
04/05/2019
Calcium
EPA200.7
38500mg/kg
04/06/2019
Chromium
EPA200.7
17.9mg/kg
04/05/2019
Copper
EPA 200.7
364 mg/kg
04/05/2019
Lead
EPA200.7
17.2mglkg
0410512019
Magnesium
EPA200.7
1980mg/kg
04/06/2019
Molybdenum
EPA200.7
<11.0mg/kg
04/10/2019
Nickel
EPA200.7
11.5mg/kg
04/0512019
Potassium
EPA200.7
2660mg/kg
04/06/2019
Selenium
EPA200.7
<11.0mg/kg
04/05/2019
Sodium
EPA200.7
3370mg/kg
04/06/2019
Zinc
EPA 2003
4140 mg/kg
04/0512019
N itrate+N itrite-N itrogen
EPA353.2
6400mg/kg
04/11/2019
Total Solids (%)
SM 2540 B
2.80 %
04/03/2019
Ammonia Nitrogen
SM4500NH3 C
1550mg/kg
0410812019
Report#: 2019.05318
Page 2 of 4
ANALYTICAL & CONSULTING CHEMISTS
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention: Wesley Wooten
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Minteo, NC 27954 � 252.473.5702 Lab/Fax
255-A Wilmington Highway, facksonville, NC 28540 a 910.347.S843 Lab; Pax
info@iiem ironmenLakhenlistscom
Date of Report: Apr 25, 2019
Customer PO #:
Customer ID: 14020008
Report #: 2019-05318
Project ID: AquaNC-Beau Rivage
Total Kjeldahl Nitrogen (TKN)
SM45000rgB
42200mg/kg
04/08/2019
Total Phosphorus
SM4500PF
22300mg/kg
04/15/2019
Mercury
SW0467471B
1.86mg/kg
04/12/2019
TCLP Metals
Arsenic
EPA200.7
<1.Omg/L
04/11/2019
Barium
EPA200.7
<1.0mg/L
04/11/2019
Cadmium
EPA200.7
<1.0mg/L
04/11/2019
Chromium
EPA200.7
<1.0mg/L
04/11/2019
Lead
EPA200.7
<1.0mg/L
04/11/2019
Selenium
EPA200.7
<1.0mg/L
04/11/2019
Silver
EPA200.8
<0.010mg/L
04/15/2019
Mercury
EPA245.1
<0.0002mg/L
04/12/2019
Lab ID Sample ID:
19-13336 Site:1
Test
Total Solids (%)
Fecal Density
Collect Date/Time
4/2/2019 1:05 PM
Method
SM 2540 G
SM 9221C EMPN 24 hr 503
Matrix Sampled by
Solid/Sludge wesley wooten
Results Date Analyzer
2.94 % 04/03/2019
54422 MPN/g 04/03/2019
Lab ID Sample ID:
Collect Date/Time
Matrix
Sampled by
19-13337 Site: 2
4/2/2019 1:07 PM
Solid/Sludge
wesley wooten
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
2.89 %
04/03/2019
Fecal Density
SM92210EMPN 24hr503
12111 MPN/g 04/0312019
Lab ID Sample ID:
Collect DatelTime
Matrix
Sampled by
19-13338 Site: 3
4/2/2019 1:08 PM
Solid/Sludge
wesley wooten
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
2.75 %
04/0312019
Fecal Density
SM92210EMPN 24hr5o3
6182MPN/g 04/03/2019
Report ,#- 2019-05316
Page 3 of 4
•51. 1^
i
ANALYTICAL & CONSULTING CHEMISTS
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention: Wesley Wooten
Environmental Chemists, Inc.
6602 Wuidmill 4Va f, Wilmington, NC 28405 > 9 t0.392.0223 Lab . 910392.4424 Fax
710 Bowsertown Road, Manteo, NC 279.94 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, tacks-onville NC 285-t0 . 910.3475843 Lab/Fax
in ro(Renvironmentalchenlists.com
Date of Report: Apr 25, 2019
Customer PO #:
Customer ID: 14020008
Report #: 2019-05318
Project ID: AquaNC-Beau Rivage
Lab ID
Sample ID:
Collect Date/Time Matrix
Sampled by
19-13339
Site:4
4/2/2019 1:09PM Solid/Sludge
wesley woolen
Test
Method Results
Date
Total Solids (%)
Fecal Density
SM 2540 G
SM 9221C E MPN 24 hr 503
3.05 % 04/03/2019
4591 MPN/g 04/0312019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-13340 Site: 5 4/2/2019 1:10 PM Solid/Sludge wesley wooten
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.79 % 04/0312019
Fecal Density SM 9221C E MPN 24 hr 503 6094 MPN/g 04103/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-13341 Site: 6 4/2/2019 1:11 PM Solid/Sludge wesley woolen
Test Method Results Date
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-13342 Site:7
Test
SM 2540 G
SM 9221C E MPN 24 hr 503
Collect Date/Time
4/2/2019 1:12 PM
Method
2.91 % 04/03/2019
12028MPN/g 04/03/2019
Matrix Sampled by
Solid/Sludge wesley wooten
Results Date Analyzed
Total Solids (%) SM 2540 G 2.76 % 04/03/2019
Fecal Density SM 9221C E MPN 24 hr 503 12682 MPN/g 04/03/2019
Comment: Results, except pH, reported on a dry weight basis, pH reported on an as received basis.
Reviewed by: �% A A ,�� �hQf.n AVJ
Report q'.' 2019-05318 Page 4 of
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_E
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: W00000455
WWTP Name: Beau Rivage NPDES Number; NCO065480
Monitoring Period; From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ❑
Alt.D (No Prior'fest) ❑ I Process to Further Reduce Pathogens ❑
If applicable to alternative crformed (Class A only) indicate "Process to Further Reduce Pathogens";
Compost ❑
Iicat Drying ❑
heat Treatment ❑
Themlophilic ❑
Beta Ra ❑
Gamma Ra ❑
Pasteurization
Class B:
Alt. (l) Fecal Density El
I All. (2) Process to SignificantlySignificandy
Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Dr ins ❑
Cut x�sliue ❑ jAcrobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
ilowing monitoring data:
Parameter
Allowable Level
in Sludge
PathogenDensity Densi
um er o
lixceo-
Frequency
of Analysis
Sample
Type
na yuca
•I'ech-
Minimun
Goo. MeanMaximut
Units
Fecal Colifornt
2x10tothe
Gih prover
per gram of
total solids
MPN
4,591
10,822
54,422
MPN/g
0
Annual
Grab
SMe221C
CPU
1000 mpn per gram
of Iota] solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colirorm)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction)
❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization ❑
I Alt 7 (Drying - Stable) ❑ JAR. 8 (Drying - Unstable)
❑
Alt. 9 (injection)
U
Alt. 10 (Incorporation) IJ
INo vector attraction reduction alternatives were pe formed
Ll
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
Ll "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T A 107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Eric Youngs, ORC Wesley Wooten, President
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
4/25/19
Signatu reparer* Date Signature of Lan Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and ISA NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
LEWIS FARMS AND LIQUID WASTE, INC.
WQ0000455
Beau Rivage WWTP
Date
Fecal Coliform
MPN per gram .
Log
04/02/19
54,422
4.7358
04/02/19
12,111
4.0832
04/02/19
6,182
3.7911
04/02/19
4,591
3.6619
04/02/19
6,094
3.7849
04/02/19
12,028
4.0802
04/02/19
12,682
4.1032
Total 28.2403
Average 4.0343
Geometric Mean F=--= Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.
LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 31, 2019
Carolina Plantation
2.98 % Solids
7.0 pH
Permit No. WQ0000455
Parameter
%
Mg/Kg Dry Weight
x 10,000
Pounds/Dry Ton
(M x 0.002)
Nitrogen (TKN)
2.300
23,000.000
46.000
Phosphorus
1.140
11,400.000
22.800
Potassium
0.261
2,610.000
5.220
PAN injected)*
1.186
11,862300
23.725
PAN (surface)*
0.836
8,357.300
16.715
Ammonia Nitrogen
0.701
7,010.000
14.020
Calcium
5.880
58,800.000
117.600
Calcium Carbonate E .
Magnesium
2,200.000
4.400
Sodium
2,440.000
4.880
Sulfur
- -
Nitrate N / Nitrite N
---
55.300
0.111
Barium
---
—
---
SAR
Chloride
---
--
--
0.46
Iron
---
--
---
Ceiling Concen.
Aluminum
---
3,830.00
7.660
(Mg/Kg)
Arsenic
---
16.00
0.032
75
Cadmium
---
16.00
0.032
85
Chromium
---
94.600
—
---
Copper
---
161.00
0.322
4,300
Lead
---
16.00
0.032
840
Mercury
---
0.805
0.002
57
Molybdenum
---
16.00
0.032
75
Nickel
---
60.10
0.120
420
Selenium
---
16.00
0.032
100
Zinc
---
2,530.00
5.060
7,500
Environmental Chemists, Inc. H 2O19-21859
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info�a,)environmentalchemists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Jan 14, 2020
8155 Malpass Corner Road Customer PO M
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2019-21859
Project ID: sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-55353 Site: Sludge 12/31/2019 4:OO.AM Solid/Sludge Wooten
Test �,rOli,,.�
Method Results Date Analyzed
Sludge Residuals
Aluminum
EPA200.7
3830mg/kg
01/03/2020
Arsenic
EPA200.7
<16.Omg/kg
O1/0312020
Cadmium
EPA200.7
<16.Omg/kg
01/03/2020
Calcium
EPA200.7
58800mg/kg
01/03/2020
Chromium
EPA200.7
94.6mg/kg
01/03/2020
Copper
EPA200.7
161mg/kg
01/03/2020
Lead
EPA200.7
<16.Omg/kg
01/03/2020
Magnesium
EPA200.7
2200mg/kg
01/03/2020
Molybdenum
EPA200.7
<16.0mg/kg
01/03/2020
Nickel
EPA200.7
60.1 mg/kg
01/03/2020
Potassium
EPA200.7
2610mg/kg
01/03/2020
Selenium
EPA200.7
<16.0mg/kg
01/03/2020
Sodium
EPA200.7
2440mg/kg
01/03/2020
Zinc
EPA200.7
2530mg/kg
01/03/2020
Total Kjeldahl Nitrogen (TKN)
EPA351.2
23000mg/kg
01/08/2020
Nitrate+ Nitrite-N itrogen
EPA353.2
55.3mg/kg
01/09/2020
Total Solids (%)
SM 2540 a
2.98 %
1213112019
pH
SM 4500 H 6
7.00 units
01/06/2020
Ammonia Nitrogen
SM 4500 NH3 C
7010 mg/kg
01/02/2020
Total Phosphorus
SM 4500 P F
11400 mg/kg
01/09/2020
Mercury
SW8467471B
0.8050mg/kg
01/05/2020
Report #:: 2019.21859
Paoe 1 of 3
Environmental Chemists, Inc.
® 1 6602 Windmill Wav, Wilmington, NC 28405 e 910.392.0223 tab • 910.392.4424 Fax
�srni 710 Bowsertown Road, Manteo, NC 27954 m 252.473.5702 Lab/Fax
255-A Wilmington Ftighway Jacksonvi Ile, NC 28540 • 910.347.5843 Lab /Fax
ANALYTICAL & CONSULTING CHEMISTS info(i;environmentitichemists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Jan 14, 2020
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-21859
Project ID: sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
19-55354 Site: 1 12/31/2019 4:05 AM Solid/Sludge Wooten
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-55355 Site:2
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-55356 Site:3
Test
Total Solids (%
Fecal Density
Lab ID Sample ID:
19-55357 Site:4
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-55358 Site:5
Test
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
Collect Date/Time
12/31/2019 4:06 AM
Method
SM 2540 B
SM 9221 C E MPN 24 hr 503
Method
2.95 % 12/31/2019
<611 MPN/g 12/31/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Date Analvzed
3.01 % 12/31/2019
<599MPN/q 12/31/2019
Collect DatelTime Matrix Sampled by
12/31/2019 4:07 AM Solid/Sludge Wooten
SM 2540 B
SM 9221C EMPN 24 hr 503
Collect Date/Time
12/31/2019 4:08 AM
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Collect Date/Time
12/31/2019 4:09 AM
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Results Date Analyzec
2.88 % 12/31/2019
<625MPN/g 12/31/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Date Analvzed
2.92% 12/31/2019
<617MPN/g 12/31/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Date Analyzec
2.95% 12/31/2019
<611 MPN/g 12/31/2019
Report #:: 2019-21859
Page 2 of 3
Environmental Chemists, Inc.
7envirohem 16602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab m 910.392.4424 Fax
710 I3owsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS into(a_)environmentalchemists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Jan 14, 2020
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-21859
Project ID: sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-55359 Site:6
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-55360 Site:7
Test
Total Solids (°h)
Fecal Density
12/31/2019 4:10 AM
Method
SM 2540 a
SM 9221C EMPN 24 hr 503
Collect Date/Time
12/31/2019 4:11 AM
Method
SM 2540 e
SM 9221C EMPN 24 hr 503
Solid/Sludge Wooten
Results
2.92 %
<617 MPN/n
Matrix
Solid/Sludge
Results
Date Analyzec
12131 /2019
17/41/9Mo
Sampled by
Wooten
Date
2.68 %
<672 MPN/n
12/31/2019
11)/111 lMn 10
comment: Sludge residuals and Fecal Density reported on a dry weight basis. pH reported on an as received
basis.
Reviewed by: _ V a A dl)
Report #:: 2019-21059
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❑
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms & Liquid Waste, Inc.
WWTP Name: Carolina Plantation
Monitoring Period:
From
1/1/2019
To
WQ Permit Number: W00000455
NPDES Number: WQ0033770
12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indirato IP.,P1 arh:PVPd a"a ile. .:..-..._e.
Class A:
Alt. A (time/temp) ❑
—--..._.
Alt B (Alk Tteatnrent) ❑
__ _........_........,. Yam .............
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thennophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ .
Class B:
Alt. (1) Fecal Densityp
Alt. (2) Process to Significantly Reduce Patho ens ❑
If applicable to alternative performed (Class B only) Indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Dryin ❑ Composting ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
Pathogen DensityNumber
g ty
Frequency
Sample
in Sludge
g
Minimu
Geo. Mean
aximu
Unitsenceq
Excee-o
of Analysis
Type
Tech-
niaue
2
2 x 10 to the
MPN
6th power
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
599
621
672
MPN/g
0
Annual
Grab
SM92210E
wei
Salmonella bacteria
3 MPN per 4ht)
grams
(in lieu of fecal
total solid (dry
coliform)
wei ht
VPnfnv AMtnwl:....
n.. a....a:.._ HG♦
➢r/.l
wu"4RV1J tXZY 11l.Al. V61 .111111 - 1'IeaRP. In, liars altarnafiVP nPrfnmm�d.
Alt.l (VS reduction) ❑
'
Alt. 2 (40-day bench) ❑
- - — ------ ----- . _ Y._............
Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Or uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying -Stable) ❑ Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) El
l'�L'b TYCYl+ • TYIILi nm . m
jAlt. 10 (Incorporation) p
lNo vector attraction reduction alternatives were performed ❑
11 V 11 a 1 t11 P.1vjmi I 1 tpiease eneck the appropriate statement)
O "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
i 1113 uc1c111111u111ou uas ueen maue unher my mrection and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Jeff Jarmon, ORC Wesley Wooten, President
Preparer Name and Title (type or print) Land Applier Name T� applicable)(type or print)
01 � � �O 1/23/2020
Signature U Kepdiler* Date Signature of Lag Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
LEWIS FARMS
WQ0000455
Carolina Plantation WWTP
1?ate
:Fecal Colt�ozm
MPZ+T et gram.
Log
12/31/19
611
2.7860
12/31/19
599
2.7774
12/31/19
625
2.7959
12/31/19
617
2.7903
12/31/19
611
2.7860
12/31/19
617
2.7903
�6�
12/31/19
672
2.8274
Total 19.5533
Average 2.7933
Geometric Mean I Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction
requirement.
LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 16, 2019
Castle Bav
2.55 % Solids
6.78 pill
Permit No. WQ0000455
Parameter
%*
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
x 0.002
Nitrogen(TKN)
6.910
69,100.000
138.200
Phosphorus
1.520
15,200.000
30.400
Potassium
0.490
4,900.000
9.800
PAN (injected)*
2.670
26,701.600
53.403
PAN surface)*
2.245
22,451.600
44.903
Ammonia Nitrogen
0.850
8,500.000
17.000
Calcium
0.017
171.000
0.342
Calcium Carbonate E .
---
--
Magnesium
-
2,540.000
5.O80
Sodium
---
7,250.000
14.500
Sulfur
Nitrate N / Nitrite N
---
21.600
0.043
Barium
Chloride
-
---
___
---
---
SAR
4.80
Iron
---
---
---
Ceiling Concen.
Aluminum
---
10,200.00
20.400
(M )
Arsenic
---
15.40
0.031
75
Cadmium
---
15.40
0.031
85
Chromium
---
15,400
---
---
Copper
---
243.00
0.486
4,300
Lead
---
15.40
0.031
840
Mercury
---
0.745
0.001
57
Molybdenum
---
15.40
0.031
75
Nickel
---
15.40
0.031
420
Selenium
--
15.40
0.031
100
Zinc
-•-
1,050.00
2.100
7,500
Environmental Chemists, Inc. # 2019-21108
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+ (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL &CONSULTING CHEMISTS infoO_enviromnentalcbemistxcom
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention: Wesley Wooten
Lab ID Sample ID:
19-53517 Site: Sludge
Test I,
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Total Kjeldahl Nitrogen (TKN)
Nitrate+N itrite-Nitrogen
Total Solids (%)
pH
Ammonia Nitrogen
Total Phosphorus
Date of Report: Jan 06, 2020
Customer PO #:
Customer ID: 14020008
Report #: 2019-21108
Project ID: sludge
Collect Date/Time Matrix Sampled by
12/16/2019 4:00 PM Solid/Sludge Wooten
Method Results Date Analv7ed
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 351.2
EPA 353.2
SM 2540 B
SM 4500 H B
SM 4500 NH3 C
SM 4500 P F
SW846 74718
10200 mg/kg
<15.4 mg/kg
<15.4 mg/kg
171 mg/kg
<15.4 mg/kg
243 mg/kg
<15.4 mg/kg
2540 mg/kg
<15.4 mg/kg
<15.4 mg/kg
4900 mg/kg
<15.4 mg/kg
7250 mg/kg
1050 mg/kg
69100 mg/kg
21.6 mg/kg
2.55%
6.78 units
8500 mg/kg
15200 mg/kg
<0.745 mg/kg
12/20/2019
12/20/2019
12/20/2019
12/20/2019
12/20/2019
12/20/2019
12/20/2019
12/20/2019
12/26/2019
12/20/2019
12/20/2019
12/20/2019
12/20/2019
12/20/2019
OIJ03/2020
01/02/2020
12/17/2019
12/17/2019
12/20/2019
01/03/2020
12/28/2019
ReporI M. 2019.21108
Pane i ors
Mik
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 29405 • 910.392.0223 Lab • 910.392A424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax
255-A Wilmingtoi Highway, Jacksonville, NC 29540 ° 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infotwenviromnentalchemists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Jan 06, 2020
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-21108
Project ID: sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-53518 Site: 1 12/16/2019 4:05 PM Solid/Sludge Wooten
Test Method Results Date Analvzed
Total Solids (%) SM 2540 B 2.43 % 12/17/2019
Fecal Density SM92210EMPN 24hr503 222223MPN/o 12/17/2n19
Lab ID Sample ID:
19-53519 Site:2
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-53520 Site:3
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-53521 Site:4
Test
Total Solids (%)
Fecal Density
Collect Date/Time
12/16/2019 4:06 PM
Method
SM 2540 B
SM 9221 C E MPN 24 hr 503
Collect Date/Time
12/16/2019 4:07 PM
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Collect Date/Time
12/16/2019 4:08 PM
Method
SM 2540 8
SM 9221C E MPN 24 hr 503
Matrix Sampled by
Solid/Sludge Wooten
Results Date Analyzec
2.51 % 12/17/2019
139443 MPN/g 12117/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Date Analvzed
2,48 % 12117/2019
217742MPN/g 12/17/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Date Analyzec
2.39 % 12/17/2019
146444MPN/a 12/17/2n19
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-53522 Site: 5 12/16/2019 4:09 PM Solid/Sludge Wooten
Test Method Results Date Analyzed
Total Solids (%) SM2540B 2.37% 12/17/2019
Fecal Density SM 9221C E MPN 24 hr 503 388186 MPN/g 12/17/2019
Report AP.: 2019-21108
PT 7 of 3
Fr- 19 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 I3owsertown Road, Manton, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS iufo(Tcnviromnentafchemists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Jan 06. 2020
8155 Malpass Corner Road Customer Po #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-21108
Project ID: sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-53523 Site:6
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-53524 Site:7
Test
Total Solids (%)
12/16/2019 4:10 PM
Method
SM 2540 8
SM 9221C EMPN 24 hr 503
Method
SM 2540 a
Collect Date/Time
12/16/2019 4:11 PM
Solid/Sludge Wooten
Results Date
2.53 %, 12/17/2019
213439MPN/g 12/1712019
Matrix Sampled by
Solid/Sludge Wooten
Results
Date Analyzed
12/17/2019
Fecal Density SM 9221C EMPN 24 hr503 102565 MPN/g 12/17/2019
Comment: Sludge residuals and Fecal Density reported on a dry weight basis. pH reported on an as received
basis.
Reviewed by: fl}� Ajs`nL t �pJ
2.34 %
Report #:: 2019-21108
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: W00000455
WWTP Name: Castle Bay NPDES Number: W00018755
Monitoring Period: From I/I/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative perforated:
Class A:
Alt. A (time/temp) 1:17
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Patho en s ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Dryin., ❑
Heat Treatment ❑
Thermo 9hilic ❑
Beta Ra ❑
Gatnma Ray ❑
Pasteurization ❑
Class B:
lAlt. (1) Fecal Density El
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization. ❑
Air D ing ❑
Coni ostin ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
............
...........
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
n Sludge
imaile
Pathogen Density
g ty
um er o
Excee-
Frequency
of Analysis
Sample
Tencaqype
Analytical
Tech-
Minimu
Ge0. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
102,565
188,310
388,186
MPN/g
0
Annual
Grab
SM 9221 CE
CFU
1000 man per gram
of total solid (dry
weight)
Salmonella bacterial
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight
Vector Attraction Reduction (15A NCAC UZ'1.11117) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
lAlt. 3 (30-day bench) ❑
lAlt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic)
lAlt. 6 (Alk. Stabilization ❑
lAlt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection)
lAlt. 10 (Incorporation) El
lNo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
CJ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .I106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note
if you check this statement attach an explanation why you have not met one or both of the
my
ce
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Charles Bryan, ORC Wesley Wooten, President
Preparer Name at Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .I 102 (26)
DENR FORM PVRF 02T (1212006)
LEWIS FARMS
WQ0000455
Castle Bay WWTP
Bate
Fecal CaliEorm
fag
12/16/19
222,223
5.3468
12/16/19
139,443
5.1444
12/16/19
217,742
5.3379
12/16/19
146,444
5.1657
12/16/19
388,186
5.5890
12/16/19
213,439
5,3293
12/16/19
102,565
5.0110
0 7d
Total 36.9241
Average 5.2749
Geometric Mean Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction
requirement.
LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant.
Date Sampled: January 10, 2019
Hampstead Pines
2.63 % Solids
6,_71 nH
Permit No. WQ0000455
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(M x 0.002)
Nitrogen (TKN)
3.690
36,900.000
73.800
Phosphorus
0.001
6.600
0.013
Potassium
0.127
1,270.000
2.540
PAN injected)*
1,324
13,242.510
26.485
PAN (surface)*
1.169
11,692.510
23.385
Ammonia Nitrogen
0.3I0
3,100.000
6.200
Calcium
2.370
23,700.000
47.400
Calcium Carbonate E .
--
Magnesium
1,220.000
2.440
Sodium
5,250.000
10.500
Sulfur
---
---
Nitrate N / Nitrite N
2.510
0.005
Barium
---
---
Chloride
---
---
___
Iron
—
Aluminum
---
1,340.00
2.680
Arsenic
20.10
0.040
Cadmium
20.10
0.040
Chromium
20.100
Copper
I79.00
0.358
Lead
20.10
0.040
Mercury
1.03
1 0.002
Molybdenum
12.10
0.024
Nickel
20.10
0.040
Selenium
20.10
0.040
Zinc
---
1,000.00
2.000
Environmental Chemists, Inc. # 2019-00602
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
SAR
Ceiling Concert.
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
840
57
75
420
100
Environmental Chemists, Inc.
4
0C.
6602 Windmill Way, Wilmington, NC 28405 0 910,392.0223 Lab 6 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoCa!eavironmentalchemists,com
Hampstead Pines Date of Report: Feb 07, 2019
1004 Bally Bunion Lane Customer PO M
Burgaw NC 28425 Customer ID: 09010034
Attention: J. Marty Fritz Report#: 2019-00602
Project ID: Sludge
Lab ID Sample ID:
19-01511 Site: Digester Sludge
Test
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Method
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 2007
EPA 200.7
EPA 2001
EPA 200.7
EPA 200.7
EPA 200.7
EPA 353.2
SM 2540 B
Collect Date/Time Matrix Sampled by
1/10/2019 8:10 AM Solid/Sludge J. Marty Fritz
Results
1340 mg/kg
<20.1 mg/kg
<20.1 mg/kg
23700 mg/kg
<20.1 mg/kg
179 mg/kg
<20.1 mg/kg
1220 mg/kg
<12.1 mg/kg
<20.1 mglkg
1270 mg/kg
<20.1 mg/kg
5250 mg/kg
1000 mg/kg
<2.51 mg/kg
2.63 %
pH SM 4500 H B 6.73 units
Ammonia Nitrogen SM4500NH3 C 3100 m/k
9 9
Total Kjeldahl Nitrogen (TKN) SM 4500 org B 36900 mg/kg
Total Phosphorus SM 4500 P F 6.60 mg/kg
Mercury SW8467471B <1.03m /k
9 9
Comment: Results. except pH, reported on a dry weight basis. pH reported on an as received basis
Reviewed by: Koa� Dw' ��jpjJ11
Date
01/22/2019
01/22/2019
01/22/2019
01/23/2019
01/22/2019
01/22/2019
01/22/2019
01/23/2019
01/25/2019
01/22/2019
01/23/2019
01/3012019
01/2412019
01/2212019
02/0412019
01/15/2019
D1/17/2019
01/22/2019
01/21/2019
01/25/2019
01 /26/2019
Report ik: 2019-00602 Page 1 of I
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
FacilityName: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: W00000455
WWTP Name: Hampstead Pines NPDES Number: W00022052
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) -Please indicate level achieved and alternative erformed
Class A:
I Alt. A (time/temp) ❑ I Alt B (Alk Treatment) ❑
P
Alt. C (Prior Testing) El
;&
A1t.D (No Prior Test) ❑
Process to Further Reduce Patho ens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01 Heat Drying ❑ Heat Treatment ❑ Thentio hilic ❑
Beta Ray ❑
Gainnia Ray ❑
Pasteurization ❑
Class B:
It. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative perdor•med (Glass B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El Air DryingElCoru ostin El Aerobic Digestion El
Anaerobic Digestion ❑
::::.:
If applicable to alternative performed (Class A or Class B) complete the follow' n monitoring data:
Parameter
Allowable Level
Pathogen DensityAnalytical
g ty
Frequency
Sample
in Sludge
g
Minim
Geo.
Units
Excee-o
of Analysis
Type
Tech-
2 x 10 to the
MPN
bth power
per gram of
Fecal Coliform
total solids
CFU
•
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
weight)
— -"Run IAoA r\l...L11. V61 .111111 - rIP.9Re inn irnrP nitnrn a tivo nnrl"n"m a
AIL I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ I
Alt. 4 (Spec.02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization p
JAR 7 (Drying - Stable) ❑ JAIL
8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
CE
JAR. 10 (Incorporation) ❑
jNo vector attraction reduction alternatives were performed ❑
RTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
- 1 uls uetermnarron nas Deen made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Wesley Wooten, President
Preparer Name and
/Title (type or print)
�N
Signature of P parer*
Land Applier Name and Title (if applicable)(type or print)
1/13/2020
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(1) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/20061
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LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled; February 25, 2019
House of Raeford Permit No. WQ0000455
Wallace Plant 3.36 % Solids
6.90 pH
Parameter
%
Mg/KgDryWeight
(%x 10,0001
Pounds/DryTon
1(M x 0.002
Nitrogen (TKN)
5.530
55,300.000
110.600
Phos horns
1.590
15,900.000
31.800
Potassium
0.310
3,100.000
6.200
PAN (injected)*
2.504
25,041.700
50.083
PAN (surface)*
2.268
22,681.700
45.363
Ammonia Nitrogen
0.472
4,720.000
9.440
Calcium
0.351
3,510.000
7.020
Calcium Carbonate E .
--Magnesium
628.000
1.256
Sodium
4,230.000
8.460
Sulfur
Nitrate N / Nitrite N
—
89.700
0,179
Barium
Chloride
---
--
--
Iron
---
---
---
Aluminum
---
1,810.00
3.620
Arsenic
15.10
0.030
Cadmium
---
15.10
0.030
Chromium
---
15.100
---
Copper
33.00
0.066
Lead
---
15.10
0.030
Mercury
0.66
0.001
Molybdenum
15.10
0.030
Nickel
15.10
0.030
Selenium
15.10
0.030
Zinc
---
35,10
0.070
Environmental Chemists H 2O19-03077
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
SAR
3.16
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
Environmental Clhernn-ts)ts9 Inc.
1 I 1 1 / 6602 Windmill Way, Wilmington, NC 28405 m 910.392.023 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ^ 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@envimnmentalchemists.com
House of Raeford -Wallace Facility Date of Report: Mar21, 2019
Post Office box 40 Customer PO #:
Rose Hill NC 28458 Customer ID: 13030026
Attention: Chris Murray Report#: 2019-03077
Project ID: Annual Sludge
Lab ID Sample ID: Collect Date[Time Matrix Sampled by
19-07776 Site: Sludge 2/25/2019 1:45 PM Solid/Sludge jay baker/envirochem
Test Method Results Date
Chlordane (TCLP)
SW 846 Method 8081B/3510
<0.02 mg/L
03/06/2019
Endrin(TCLP)
SW 846 Method8081B/3510
<0.0005mg/L
03/06/2019
Heptachlor (TCLP)
SW846 Method8081B/3510
<0.0005mg/L
03/06/2019
Heptachlor epoxide (TCLP)
SW 846 Method 8081313510
<0.0005 mg/L
03/06/2019
Lindane(TCLP)
SW 846 Method 0081 B/351 0
<0.0005mg/L
03/06/2019
Methoxychlor (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
03/06/2019
Toxaphene (TCLP)
SW 846 Method 8081BP3510
<0.05 mg/L
03/06/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 827013510
<0.050 mg/L
03/07/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 827013510
<0.050 mg/L
03/07/2019
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 827013510
<0.050 mg/L
03/07/2019
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
Hexachloroethane (TCLP)
SW 846 method B270/3510
<0.050 mg/L
03/07/2019
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
Nitrobenzene (TCLP)
SW 845 method 8270/3510
<0.050 mg/L
03/0712019
o-Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
03/07/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
03107/2019
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03107/2019
2,4,5-TP (TCLP)
SW846 Method 8151A
<0.003 mg/L
03106/2019
2,4-D (TCLP)
SW845 Method 8151A
<0.003 mg/L
03/06/2019
1,1-Dichloroethylene (TCLP)
SW846 Method B26015030
<0.01 mg/L
03/01/2019
1,2-Dichloroethane(TCLP)
SW846 Method826015030
<0.01mg/L
03/01/2019
Benzene (TCLP)
SW846 Method 826015030
<0,01 mg/L
03/01/2019
CarbonTetrachloride (TCLP)
SW845 Method 8260/5030
<0.01mg/L
03/01/2019
Report#:: 2019-03077
c_MaII 1=n ma,
n zat
Pagel of
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Mantec, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com
House of Raeford -Wallace Facility
Date of Report: Mar 21, 2019
Post Office box 40
Customer PO #:
Rose Hill NC
28458
Customer ID: 13030026
Attention: Chris Murray
Report #: 2019-03077
Project ID: Annual Sludge
Chlorobenzene(TCLP)
SW846 Method8260/5030
<0.01mg/L
03101/2019
Chloroform (TCLP)
SW846 Method826015030
<0.01 mg/L
03/01/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
03/01/2019
Tetrachloroethylene (TCLP)
SW846 Method 6260/5030
<0.01 mg/L
03/01/2019
Trichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
03/01/2019
Vinyl Chloride (TCLP)
SW846 Method826015030
<0.01 mg/L
03/0112019
TCLP - Extraction
TCLP-Extraction
DNR
RCI
Cyanide
EPA335.4
<0.05mg/kg
03/06/2019
Sulfide
SM 4500 s D
4.14 mg/kg
03/06/2019
Ignitability
SW846 method 1010
>190'F
03/05/2019
Sludge Residuals
Aluminum
EPA200.7
1810mg/kg
02/27/2019
Arsenic
EPA200.7
<15.1 mg/kg
02/27/2019
Cadmium
EPA200.7
<15.1 mg/kg
02127/2019
Calcium
EPA200.7
3510mg/kg
03/01/2019
Chromium
EPA200.7
<15.1 mg/kg
02/27/2019
Copper
EPA 2007.
33.0 mg/kg
02/27/2019
Lead
EPA 200.7
<15.1 mg/kg
02/27/2019
Magnesium
EPA200.7
628mg/kg
03/01/2019
Molybdenum
EPA200.7
<15.1 mg/kg
03/04/2019
Nickel
EPA200.7
<15.1 mg/kg
02/27/2019
Potassium
EPA200.7
3100mg/kg
03/01/2019
Selenium
EPA200.7
<15.1 mg/kg
02/27/2019
Sodium
EPA200.7
4230mg/kg
03101/2019
Zinc
EPA200.7
35.1 mg/kg
02127/2019
Total Kjeldahl Nitrogen (TKN)
EPA351.2
55300 mg/kg
03/06/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
89.7mglkg
03/07/2019
Total Solids (%)
SM25408
3.36%
02126/2019
PH
SM 4500 H B
6.90 units
03104/2019
Report#.: 2019-03077
Page 2 of 4
Environmental Chemists, Inc.
enviroehe�76602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ^ 252.470,5702 Lab/Fax
aM 255-A Wilmington Highway, Jacksonville, NC 28540 m 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com
House of Raeford -Wallace Facility
Date of Report: Mar 21, 2019
Post Office box 40
Customer PO #:
Rose Hill NC
28458
Customer ID: 13030026
Attention: Chris Murray
Report#: 2019-03077
Project ID: Annual Sludge
Ammonia Nitrogen
SM4500NH3 C
4720mg/kg
03/11/2019
Total Phosphorus
SM 4500 P F
15900 mg/kg
03/07/2019
Mercury
SW8467471B
<0.655mg/kg
03/03/2019
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg/L
03/08/2019
Barium
EPA200.7
<1.0mg/L
03/08/2019
Cadmium
EPA200.7
<1.0mg/L
03/08/2019
Chromium
EPA200.7
<1.0mg/L
03/08/2019
Lead
EPA200.7
<1.0mg/L
03/08/2019
Selenium
EPA200.7
<1.0mg/L
03/0812019
Silver
EPA200.7
<1.0mg/L
03108/2019
Mercury
EPA245.1
<0.0002mg/L
03/10/2019
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-07777 Site: 1
2/25/2019 1:46 PM Solid/Sludge jay baker/envirochem
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 G
2.50 %
02/26/2019
Fecal Density
SM92210EMPN 24hr503 216000MPN/g
02/25/2019
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-07778 Site: 2
2/25/2019 1:47 PM Solid/Sludge jay baker/envirochem
Test
Method
Results Date Analyzed
Total Solids (%) SM 2540 G 2.42 % 02/26/2019
Fecal Density SM 9221C E MPN 24 hr 503 145000 MPN/g 02/25/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-07779 Site: 3 2/25/2019 1:48 PM Solid/Sludge jay baker/envirochem
Test Method Results Date Analvzet
Total•Solids (%) SM 2540 G 2.38 % 02/26/2019
Fecal Density SM 9221C E MPN 24 hr 503 38700O MPN/g 02/25/2019
Report #:: 2019-03077 Page 3 of 4
(%I
^ F L n
R SM
ANALYTICAL & CONSULTING CHEMISTS
House of Raeford -Wallace Facility
Post Office box 40
Rose Hill NC 28458
Attention: Chris Murray
Envle I
ironmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
info@environmenWehemists.com
Date of Report: Mar 21, 2019
Customer PO M
Customer ID: 13030026
Report M 2019-03077
Project ID: Annual Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-07780 Site: 4 2/25/2019 1:49 PM Solid/Sludge jay baker/envirochem
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.53 % 02/26/2019
Fecal Density SM 9221C E MPN 24 hr 503 87000 MPN/g 02/25/2019
Lab ID
Sample ID:
Collect Daterrime
Matrix
Sampled by
19-07781
Site: 5
2/25/2019 1:50 PM
Solid/Sludge
jay baker/envirochem
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
2.50 %
02/26/2019
Fecal Density
SM 9221C E MPN 24 hr 503
140000 MPN/g 02/25/2019
Lab ID
Sample ID:
Collect Date/Time
Matrix
Sampled by
19-07782
Site: 6
2/25/2019 1:51 PM
Solid/Sludge
jay baker/envirochem
Test
Method
Results
Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-07783 Site:7
Test
SM 2540 G
SM 9221C E MPN 24 hr 503
Collect Daterrime
2125/2019 1:52 PM
Method
2.70 % 02/26/2019
130000MPN/g 02/2512019
Matrix Sampled by
Solid/Sludge jay baker/envirochem
Results Date Analvzec
Total Solids (%) SM 2540 G 2.47 % 02/26/2019
Fecal Density SM 9221 C E MPN 24 hr 503 219000MPN/g 02125/2019
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: ko l J o VYI j
Report #:: 2019-03077 Page 4 of 4
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms and Liquid Waste, Inc.
WWTP Name: Wallace Chicken Processing Plant
Monitoring Period: From 1/1/2019 To
WQ Permit Number: W00000455
NPDES Number: NC0003344
12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (timc/tcntp) ❑
Alt B (Alk Treatment) ❑
I Alt. C (Prior Tcsting)❑
AILD (No Prior Test) I Process to Further Reduce Pathoeengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
I Heat. Drying ❑
Heat Tretument ❑
Thennophilic EJ
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
I Alt. (1) Fecal Density E
Alt. (2) Process to Si<_ntilicantly Reduce Pathogens El
If applicable to alternative performed (('tars B only indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Com oslin g ❑
Acrobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
llowing monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
um er ot
Excee-
Frequency
of Analysis
Y
Sample
Type
natea
Tech-
Mittitnu
Geo. Meats
Maximitt
Unitsences
Fecal Coliform
2 x 10 tothe
6th power
per gram of
total solids
MPN
87,000
170,584
387,000
MPN/g
0
Annual
Grab
SM9221C
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
wet ht
Vector Attraction Reduction (15A NCAC 02T ,1107) -Please indicate alternative performed:
Alt.I (VS reduction) l ]
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
jAft. 4 (Spec. O> uptake) ❑
AIt. 5 (14-Day Aerobic) ❑
I Alt. 6 (Alk. Stabilization ❑
jAlt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Unstable) L
Alt. 9 (Injection) J
jAlt. 10 (Incorporation) S
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel property gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant peenna es for false certification including fine and imprisonment."
Y�hA
ORC Wesley Wooten, President
Preparer Name and tl pe or print) Land Applier Name and
TiTitle
e(if applicable)(type or print)
1��✓ll 4/3/2019
Sign toreo' reparer* Date Signature ofLao- Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .I 102 (26)
LEWIS FARMS
W00000455
House of Raeford - Wallace Plant
Date
Fecal Coli£orm
MPN per gram"
Log
02/25/19
216,000
5.3345
02/25/19
145,000
5.1614
02/25/19
387,000
5.5877
02/25/19
87,000
4.9395
02/25/19
140,000
5.1461
02/25/19
130,000
5.1139
02/25/19
219,000
5.3404
Total 36.6236
Average 5.2319
Geometric Mean 170,584 Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.
LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 26, 2019
Majestic Oaks WWTP Permit No. W00000455
1.31 % Solids
6.88 off
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
lMg/Kg x 0.002)
Nitrogen (TKN)
4.530
45,300.000
90.600
Phosphorus
2.070
20,700.000
41.400
Potassium
0.515
5,150.000
10.300
PAN injected)*
2.522
25,218.000
50.436
PAN surface)*
1.702
17,018,000
34.036
Ammonia Nitrogen
1.640
16,400.000
32.800
Calcium
4.920
49,200.000
98.400
Calcium Carbonate E .
---
---
_
Magnesium
---
3,240.000
6.480
Sodium
---
4,730.000
9.460
Sulfur
___
___
---
Nitrate N / Nitrite N
---
148.000
0,296
Barium
---
---
---
SAR
Chloride
---
---
---
0.64
Iron
---
---
---
Ceiling Concen.
Aluminum
---
5,380.00
10.760
M /K )
Arsenic
--
23.80
0.048
75
Cadmium
---
23.80
0.048
85
Chromium
---
109.000
---
—
Copper
--
153.00
0.306
4,300
Lead
---
23.80
0.048
840
Mercury
---
1.37
0.003
57
Molybdenum
---
23.80
0.048
75
Nickel
---
66.30
0.133
420
Selenium
---
23.80
0.048
100
Zinc
---
3,060.00
6.120
7,500
Environmental Chemists 2019-21716
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection Omits are listed as detection limits
for calculation purposes.
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 " 910.392.0223 Lab " 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 " 252.473-5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 " 910.'47.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchenlists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Jan 14, 2020
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-21716
Project ID: sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-55010 Site: -Sludge n 12/26/2019 3:30 PM Solid/Sludge Wooten
Test ' ""�Method
Results Date Analyzed
Total Kjeldahl Nitrogen (TKN)
SM45000rgB
45300mg/kg
01/08/2020
Sludge Residuals
Aluminum
EPA200.7
5380mg/kg
01/03/2020
Arsenic
EPA200.7
<23.8mg/kg
01/03/2020
Cadmium
EPA200.7
<23.8mg/kg
01/03/2020
Calcium
EPA200.7
49200mg/kg
01/03/2020
Chromium
EPA200.7
109mg/kg
01/03/2020
Copper
EPA200.7
153mg/kg
01/03/2020
Lead
EPA 200.7
<23.8 mg/kg
01/03/2020
Magnesium
EPA200.7
3240mg/kg
01/03/2020
Molybdenum
EPA200.7
<23.8mg/kg
01/03/2020
Nickel
EPA200.7
66.3mg/kg
01/03/2020
Potassium
EPA200.7
5150mg/kg
01/03/2020
Selenium .
EPA200.7
<23.8mg/kg
01/03/2020
Sodium
EPA200.7
4730mg/kg
01/03/2020
Zinc
EPA200.7
3060mg/kg
01/03/2020
Nitrate+Nitrite-Nitrogen
EPA3532
148mg/kg
01/08/2020
Total Solids (%)
SM 2540 B
1.31 %
12/27/2019
pH
SM 4500 H e
6.88 units
01/06/2020
Ammonia Nitrogen
SM 4500 NH3 C
16400 mg/kg
12/29/2019
Total Phosphorus
SM4500PF
20700mg/kg
01/09/2020
Mercury
SW8467471B
<1.37mglkg
1212812019
Report # 2019-21716 Page 1 of 3
Environmental Chemists, Inc.
® 6602 Windmill Way, Wilmington, NC 28405 ^ 9111.392.0223 Lab + 910.392.4424 Fax
l� 710 [lowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
�-- 255-A Wilmington Highway, Jacksonville, INC 26540 ^ 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS into(c cnvironnlentalchemists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Jan 14, 2020
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-21716
Project ID: sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
19-55011 Site: 1 12/26/2019 3:35 PM Solid/Sludge Wooten
Test Method Results Date Analvzed
Total Solids (%) SM 2540 B
Fecal Density SM 9221C EMPN 24 hr 503
Lab ID Sample ID:
19-55012 Site:2
Test
Total Solids (%)
Fecal Density
Lab ID
19-55013
Test
Sample ID:
Site: 3
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-55014 Site:4
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-55015 Site:5
Test
Total Solids (%)
Fecal Density
Collect Date/Time
12/26/2019 3:36 PM
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Collect DatelTime
12/26/2019 3:37 PM
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Collect DatelTime
12/26/2019 3:38 PM
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Collect Date/Time
12/26/2019 3:39 PM
Method
SM 2540 B
SM 9221 C E MPN 24 hr 503
1.24 % 12/27/2019
<1452 MPN/g 12/27/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Date Analyzec
1.58 % 12/27/2019
<1140 MPN/g 12/27/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Date Analvzed
1.61 % 12/27/2019
<1119 MPN/g 12/27/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Date Analyzed
1.67 % 12/27/2019
<1078 MPN/q 12/27/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Date Analvzed
1.08 % 12/27/2019
<1667 MPN/g 12127/2019
Report#r. 2019-21716 Paget of
Environmental Chemists, Inc.
7enviro hem 6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info Ogenvironmentalchemists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Jan 14, 2020
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-21716
Project ID: sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-55016 Site: 6 12/26/2019 3:40 PM Solid/Sludge Wooten
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 1.48 % 12/27/2019
Fecal Density SM 9221 C E MPN 24 hr 503 <1217MPN/g 12/27/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-55017 Site: 7 12/26/2019 3:41 PM Solid/Sludge Wooten
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 1.48 % 12/27/2019
Fecal Density SM 9221C E MPN 24 hr 503 <1217 MPN/g 12/27/2019
Comment: Sludge residuals and Fecal Density reported on a dry weight basis. pH reported on an as received
basis. o ,,
Reviewed by:
ReportU 2019-21716
Pane 3 of 3
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: W00000455
WWTP Name: Majestic Oaks NPDESNumber: W00030088
Monitoring Period: From 1/l/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T.1106) - Please ladlente hunt s.r.:e. A —A
Class A:
AIL A (time/temp) ❑ Alt B (Mk Treatment) ❑ Alt. C (Poor Tesfin ❑
Ji A1t.D (No Prior Test) ❑ Process to Further Reduce Patho gags ❑
ff applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Corn ost ❑ Heat Drying❑ Heat Treatment ❑ Thermo hilic ❑
Beta Ra ❑ Gamma Ra ❑ Pasteurization ❑
Class B: JAlt. (1) Fecal Densi ❑ Alt. (2) Process to significtintI7 Rednce Patho en7 ❑
ati
If applicable to alternve ettorated (Class B ouly) indicate "Process to Significantly Reduce
Pathogens.:
Lime Stabilization O Air in ❑ ostin ❑ Com
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative pertormed (Class A or Class B) complete the
followin monitoring data:
Allowable Level
in Sludge
en Density
Pathogen g
Nurnocrof
Ex"�
Frequency
of analysis
Sample
Type
na -
cai
Tech-
inim
Geo. Mean
aximu
Units
Fecal Colifonn
6th power
2 x 10 to thekCFU
per gram of
total solids
1000 mpn per gram
oftotalsolid (dry
weight)
1,078
1,256
1,667
MPNlg
0
Annual
Grab
SM9221CR
Salmonella bacteria
(in lieu of fecal
colifonn
V t
3 MPN per 4 grams
total solid (dry
weight)
ec or Attraction Reduction (15, NCAC 02T.11071- Please indiente akernafive ..e.r .",ed.
AR.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
AIt.3 (30-day bench) ❑ Alt. 4 (Spec. Or uptake) ❑
AIt.5(14-Day Aerobic) ❑
AIt 6(Alk Stabilization❑
JAk7(Drying -Stable) ❑AIL 8 (Drying- Unstable) ❑
AIL 9 (Injection) p
Alt. 10 (Into oration) El
We vector attraction reduction alternatives were performed ❑
o a n a GLr Mil a tpreuse cnecrr toe appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T 1107 have been met"
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my directioa and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Tony Baldwin, ORC Wesley Wooten, President
Preparer�Nammee and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Si a of Preparer' Date Signature of Lan Applier (if applicable) Date
•Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
LEWIS FARMS
WO0000455
Majestic Oaks WWTP
12/26/19
1,452
3.1620
12/26/19
1,140
3.0569
12/26/19
1,119
3.0488
12/26/19
1,078
3,0326
12/26/19
1,667
3.2219
12/26/19
1,217
3.0853
12/26/19
1,217
3.0853
Total 21.6928
Average 3.0990
Geometric Mean 1,Z$6 Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.
LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date. Sampled: October 24, 2019
North Topsail W WTF
3.04 % Solids
Permit No. W00000455
Parameter I % Mg/KgDry Weight Ponnds(Dry Ton
(% z 7,0.000) (N /Kg x 0.002)
Nitrogen (TKN) 4.840 48,400.000 1 96.800
1
1
u �wuuuaw c .
sium
t
N / Nitrite N ---
5.040
53.000
7,170.000 14.54(
45500 nm1
Barium
Chloride
---
- -
---
--
---
SAR
1 1.89
Iron
---
---
- -
Ceiling Concen.
Aluminum
---
17,200.00
34.400
(Mg/Kg)
Arsenic
10.40
0.021
75
Cadmium
---
8.49
0.017
85
Chromium
---
24.500
---
---
Copper
-
206.00
0.412
4,300
Lead
---
8.65
0,017
840
Mercury
0.526
0.001
57
Molybdenum
8.49
0.017
75
Nickel
10.70
0.021
420
Selenium
8.49
0.017
l00
Zinc
--
3,950.00 1
7.900
7,500
11 1 1 1 q
Environment 14 2019-18013
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
Environmental Chemists, Inca
i 6602 Windmill l4lav, Wilmington, NC 28405 910,392.0223 Lab • 910.392.4424 Pax
s� 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilnwigton E-fighivay, Jacksonvitle, NC 28540 , 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS i1il'oC�envimnmentalcbemists.com
Pluris LLC. Date of Report: Nov 01. 2019
P. 0. Box 856 Customer PO #:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Randy Hoffer Report #: 2019-18013
Project ID: North Topsail WWTP
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
19-45931 Site: Sludge 10/24/2019 11:24 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA200.7
17200mg/kg
10/28/2019
Arsenic
EPA200.7
10.4mg/kg
10/28/2019
Cadmium
EPA200.7
<8.49mg/kg
10/28/2019
Calcium
EPA200.7
26500mg/kg
10/2812019
Chromium
EPA200.7
24.5mg/kg
10/28/2019
Copper
EPA 200.7
206 mg/kg
10/28/2019
Lead
EPA200.7
8.65mg/kg
10/2812019
Magnesium
EPA200.7
4610mg/kg
10128/2019
Molybdenum
EPA200.7
<8.49mg/kg
10/2812019
Nickel
EPA200.7
10.7mg/kg
10/28/2019
Potassium
EPA200.7
3950mg/kg
10/28/2019
Selenium
EPA200.7
<8.49mg/kg
10/28/2019
Sodium
EPA200.7
7270mg/kg
10/2812019
Zinc
EPA200.7
3950mg/kg
10/28/2019
Nitrate+Nitrite-Nitrogen
EPA053.2
35.5mg/kg
10/29/2019
Total Solids (%)
SM 2540 B
3,04 %
10/24/2019
pH
SM 4500 H B
6.86 units
10/29/2019
Ammonia Nitrogen
SM4500NH3 C
2520mg/kg
10/27/2019
Total Kjeldahl Nitrogen (TKN)
SM 4500 Or9 a
48400 mg/kg
10/27/2019
Total Phosphorus
SM 4500 P F
40800 mg/kg
10/30/2019
Mercury
swe4B7471B
<0.526mg/kg
10/26/2019
Report #'.'. 2019-18013
Pace 1 of 3
Environmental Chemists, Inc.
Y 6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab • 910.392 4424 Fat
710 Bowsertown. Road, Manteo, NC 27954 • 252.473.5702 Lab/Fat
5m, 255-A Will" ington Highway, acksonvi Ile, NC 28540 n R } J� 970.347.5843 Lab/T'at
ANALYTICAL & CONSULTING CHEMISTS into(d!envirmunen(:dchcmists.com
Pluris LLC.
Date of Report: Nov 01, 2019
P. O. Box 856
Customer PO #:
Sneads Ferry NC
28460 Customer ID: 09110001
Attention: Randy Hoffer
Report #: 2019-18013
Project ID: North Topsail WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-45932 Site: 001
10/24/2019 11:25 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3.03 % 10/24/2019
Fecal Density
SM 9221C E MPN 24 hr 503 115512 MPN/g 1012512019
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-45933 Site: 002
10/24/2019 11:29 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3.09 % 10/24/2019
Fecal Density
SM 9221C E MPN 24 hr 503 113269 MPN/g 10/25/2019
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-45934 Site: 003
10/24/2019 11:33 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3.11 % 10/24/2019
Fecal Density
SM 9221 C E MPN 24 hr 503 77171MPN/g 10/25/2019
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-45935 Site: 004
10/24/2019 11:34 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 2.92 % 10/24/2019
Fecal Density
SM 9221C E MPN 24 hr 503 82192 MPN/g 10/25/2019
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-45936 Site: 005
10/24/2019 11:37 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 2.89 % 10/24/2019
Fecal Density
SM92210EMPN 24hr503 121108MPN/g 10/25/2019
Report M . 2019-18013
Paae 2 of 3
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910,392.4424 Fax
sM 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS iafo�a eavironmen[:flcllemisls.0om
Pluris LLC. Date of Report: Nov 01, 2019
P. O. Box 856 Customer PO #:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Randy Hoffer Report #: 2019-18013
Project ID: North Topsail WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-45937 Site: 006 10/24/2019 11:39 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.93 % 10124/2019
Fecal Density SM 9221C E MPN 24 hr 503 119454 MPN/g 10/25/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19 45938 Site: 007 10/24/2019 11:41 AM Solid/Sludge Client
Test Method Results Date Analyzer
Total Solids (%) SM 2540 B 2.94 % 10/24/2019
Fecal Density SM 9221 C E MPN 24 hr 503 119048MPN/g 10/25/2019
Comment: Sludge residual results, except pH, reported on a dry weight basis.
Reviewed by: AA �opjt(}A
RaPOn #:: 2019-18013
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
FacilityName: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: W00000455
W WTP Name: Pluris North Topsail NPDES Number: W00005849
Monitoring Period: From 1/1/2019 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106)- Please indieate teT,ni a a :o.,oa .,..a
Class A:
._. _. __.................+ueu+w+we F.+svuueu.
Alt. A (time/temp) ❑ Alt B (Alk Treatment) El I Alt. C (Prior Testing)❑
>'
AIt.D (No Prior Test) I Process to Further Reduce PathogenPathogengs ❑
If a plicable to alternative performed (Class A only) indiente "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo h tic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization
Class B:
Alt (1) Fecal Density El
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) Indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Ail' Dr rug ❑ Composting ❑ jAcrobic Digest -ion ❑
;;:,.:;.,..,:<..::.:::::..:::.>;; �:;;...............
Anaerobic Digestion ❑ s>«:,;:.,:;»s;•.;::;:;::;::;r:<:,,v:.;::<.:r::<;;;::.;:.....:::<.;:::•:::::
If applicable to alternative performed (Class A or Class B) com lete the following monitoring data:
Parameter
Allowable Level
Pathogen Densi
g ty
Frequency
Sample
in Slud e
g
Minim
Gen. Mean
aximu
Units
Excee
of Analysis
Type
Tech-m
26th0owehe
p
WN
77,171
105,235
121,108
MPN/g
0
Annual
Grab
SM92210E
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
oftotalsolid (dry
wei ht
Salmonella bacteria
3 MPN per4 grams
Ln lieu of fecal
(i
total solid (dry
colifibLn
wei ht
Vf A AAV / J - rlease maicare alternative ertormed:
AltI (VS reduction) ❑
JAIL 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ 1
P
Alt 4 (Spec. Oz uptake) ❑
Alt 5 (I4-Day Aerobic) ❑
JAIL 6 (Alk. Stabilization ❑
Alt 7 (Drying- Stable) ❑ JAIL
8 (Drying -Unstable) ❑
AIL 9 (Injection) El
1,T11 TTi.TTl.1 TT/lTT [T
I Alt 10 (Incorporation) El
JNo vector attraction reduction alternatives
were performed ❑
• L•••u=. r.��..�. o ro- 1r+rrrr ry r tprease cnecr(tne appropriate statement)
l7 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met "
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
A urs "e.er-muraaun Has Deen mane miner my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Randy Hoffer, ORC Wesley Wooten, President
Preparer Name and T' le or print) QLand Applieer Name
//and Title (if applicable)(type or print)
*De
/{N�12/5/19
n re o Pre *Signature of La d Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
DENR FORM PVRF 02T (12/2006)
LEWIS FARMS
WQ0000455
Pluris North Topsail WWTP
10/24/19
115,512
5.0626
10/24/19
113,269
5.0541
10/24/19
77,171
4.8875
10/24/19
82,192
4.9148
10/24/19
121,108
5.0832
10/24/19
119,454
5.0772
10/24/19
119,048
5.0757
Total 35.1551
Average 5.0222
Geometric Mean JL*,.-.10 5Ll j Fecal Coliform MPN / gram
... $_
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen for Reduction
requirement.
LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 17, 2019
River Bend
2.81 % Solids
7.48 pH
Permit No. W00000455
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002
Nitrogen (TKN)
5.830
58,300.000
116.600
Phosphorus
1.290
12,900.000
25.800
Potassium
0.356
3,560.000
7.120
PAN (injected)*
2.538
25,379.000
50.758
PAN (surface)*
2.104
21,044.000
42,088
Ammonia Nitrogen
0.867
8,670.000
17.340
Calcium
3.720
37,200M0
74.400
Calcium Carbonate E .
---
---
__
Magnesium
2,860.000
5.720
Sodium
4,660.000
9.320
Sulfur
___
_
Nitrate N / Nitrite N
---
1,820.000
3.640
Barium
---
---
---
SAR
Chloride
---
---
1.05
Iron
---
---
---
Ceiling Concen.
Aluminum
---
4,060.00
8.120(Mg/Kg)
Arsenic
---
9.82
0.020
75
Cadmium
---
9.82
0.020
85
Chromium
---
12.400
—
—
Copper
751.00
1.502
4,300
Lead
---
11.00
0.022
840
Mercury
---
0.71
0.001
57
Molybdenum
---
9.82
0.020
75
Nickel
---
10.60
0.021
420
Selenium
-
9.82
0.020
100
Zinc
---
765.00
1.530
71500
Environmental Chemists, Inc: 2019-21213
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 " 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchelnists.com
Town of River Bend
Date of Report: Jan 20. 2020
45 Shoreline Drive
Customer PO #:
New Bern NC 28562
Customer ID: 12110004
Attention: Brandon Mills
Report #• 2019-21213
Project ID: Wastewater
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-53738 Site: Sludge
12/17/2019
8:20 AM Solid/Sludge Tom Harper
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW846 Method 80818/3510
<0.02 mg/L
12123/2019
Endrin (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
12/23/2019
Heptachlor (TCLP)
SW 846 Method 60818/3510
<0.0005 mg/L
12/23/2019
Heptachlor epoxide (TCLP)
SW 846 Method 80818/3610
<0.0005 mg/L
12/23/2019
Llndane (TCLP)
SW 846 Method 80818/3510
<0.0005 mglL
12/23/2019
Methoxychlor(TCLP)
SW 846 Method8081B/3510
<0.0005mg/L
12/23/2019
Toxaphene (TCLP)
SW 846 Method 8081 B1351 0
<0.05 mg/L
12/2312019
1,4-Dichlorobenzene (TCLP)
SW 846 method a270/3510
<0.050 mg/L
12/1912019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
12/19/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 0270/3510
<0.050 mg/L
12/19/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
12/19/2019
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
12/19/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
12/19/2019
Hexachlorobenzene (TCLP)
SW 846 method 827013510
<0.050 mg/L
12/19/2019
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
12/19/2019
m + p-Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
12/1912019
Nitrobenzene (TCLP)
SW 846 method 827013510
<0.050 mg/L
12119/2019
o-Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
12/1912019
Pentachlorophenol (TCLP)
SW 846 method 827013510
<0.250 mg/L
12/19/2019
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
12/19/2019
2,4,5-TP(TCLP)
SW846method 8151A
<0.003mg/L
1212012019
2,4-D (TCLP)
SW848 Method 8151A
<0.003 mg/L
12/20/2019
1,1-Dichloroethylene(TCLP)
SW848 Method825015030
<0.01mg/L
12/21/2019
1,2-Dichloroethane (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
12/21/2019
Benzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
12/21/2019
Carbon Tetrachloride (TCLP)
SWB46 Method 8260/5030
<0.01 mg/L
12/21/2019
Report #:: 2019-21213
Page 2 of 5
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax
710 Sowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com
Town of River Bend
Date of Report: Jan 20, 2020
45 Shoreline Drive
Customer PO #:
New Bern NC
28562
Customer ID: 12110004
Attention: Brandon Mills
Report #: 2019-21213
Project ID: Wastewater
Chlorobenzene (TCLP)
SW846 Method8260/5030
<0.01 mg/L
12/21/2019
Chloroform (TCLP)
SW846 Method8260/5030
<0.01 mg/L
12/21/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
12/21/2019
Tetrachloroethylene(TCLP)
SW846 Method B260/5030
<0.01mg/L
12/21/2019
Trichloroethylene (TCLP)
SW846 Method 826015030
<0.01 mg/L
12/21/2019
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
12/21/2019
RCI
Cyanide
EPA335.4
<0.05mg/kg
12/27/2019
Sulfide
SM 4500 S o
0.56 mg/kg
12126/2019
Ignitablllty
SW 846 method 1010
>205 OF
01/10/2020
Sludge Residuals
Aluminum
EPA 200.7
4060mg1kg
12/30/2019
Arsenic
EPA 200.7
<9.82 mg/kg
12/30/2019
Cadmium
EPA 200.7
<9.82mg/kg
12130/2019
Calcium
EPA 200.7
37200mg/kg
12/30/2019
Chromium
EPA 200.7
12.4mg/kg
12/30/2019
Copper
EPA 200.7
751 mg/kg
12/30/2019
Lead
EPA 200.7
11.0mg/kg
12/3012019
Magnesium
EPA 200.7
2860mg/kg
12130/2019
Molybdenum
EPA 200.7
<9.82mg/kg
12/30/2019
Nickel
EPA 200.7
10.6mg/kg
12/30/2019
Potassium
EPA200.7
3560mg/kg
12/30/2019
Selenium
EPA 200.7
<9.82mg/kg
12130/2019
Sodium
EPA200.7
4660mg/kg
12/30/2019
Zinc
EPA 2001
765 mg/kg
12/30/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
1820mg/kg
01/04/2020
Total Solids (°fo)
SM 2540 B
2.81 %
12/18/2019
pH
SM 4500 H B
7.48units
12/23/2019
Ammonia Nitrogen
SM4500NH3 C
8670mg/kg
12/20/2019
Total Kjeldahl Nitrogen (TKN)
SM45000rgB
58300mg/kg
12/19/2019
Report #.: 2019-21213
Pane 3 of 5
Environmental Chemists, Inc.
ocheochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com
Town of River Bend
45 Shoreline Drive
New Bern NC
Attention: Brandon Mills
28562
Date of Report: Jan 20, 2020
Customer PO #:
Customer ID: 12110004
Report #: 2019-21213
Project ID: Wastewater
Total Phosphorus
SM 4500 P F
12900 mg/kg
01/03/2020
Mercury
SW84674718
<0.712mg/kg
12/28/2019
TCLP Metals
Arsenic
EPA200.7
<1.0mg/L
12/30/2019
Barium
EPA200.7
<1.Omg/L
12/26/2019
Cadmium
EPA200.7
<1.0mg/L
12/26/2019
Chromium
EPA200.7
<1.0mg/L
12/26/2019
Lead
EPA200.7
<1.0mg/L
12/26/2019
Selenium
EPA200.7
<1.Omg/L
12/30/2019
Silver
EPA200.7
<1.0mg/L
12/26/2019
Mercury
EPA245.1
<0,0002mg/L
12/28/2019
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-53756 Site: 1
12/17/2019 8:20 AM Solid/Sludge Tom Harper
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.70 %
12/18/2019
Fecal Density
SM92210EMPN 24hr503
1667MPN/g
12/18/2019
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
19-53757 Site: 2
12/17/2019 8:20 AM
Solid/Sludge Tom Harper
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.65 %
12/18/2019
Fecal Density
SM 9221C EMPN 24 hr5D3
2944 MPN/g
12/18/2019
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
19-53758 Site: 3
12/17/2019 8:20 AM
Solid/Sludge Tom Harper
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.70 %e
12118/2019
Fecal Density
SM92210EMPN 24hr503
741 MPN/g
12/18/2019
Report$t: 2019-21213
Page 4 of 5
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
sm 710 Sowsertown Road, Mantco, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@envitonmentalchemists.com
Town of River Bend
Date of Report:
Jan 20. 2020
45 Shoreline Drive
Customer PO #:
New Bern NC 28562
Customer ID:
12110004
Attention: Brandon Mills
Report#:
2019-21213
Project ID: Wastewater
Lab ID Sample ID:
Collect DatelTime Matrix
Sampled by
19-53759 Site: 4
12/17/2019 8:20 AM Solid/Sludge
Tom Harper
Test Method Results Date Analyzed
Total Solids (%) SM2540a 2.70% 12/1812019
Fecal Density SM92210EMPN 24hr503 <667MPN/g 12/18/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-53760 Site: 5 12/17/2019 8:20 AM Solid/Sludge Tom Harper
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.76 % 12/18/2019
Fecal Density SM92210EMPN 24hr503 725MPN/g 12/18/2019
Lab ID Sample ID:
19-53761 Site:6
Test
Total Solids (%)
Fecal Density
Collect Date/Time Matrix
12/17/2019 8:20 AM Solid/Sludge
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Results
Sampled by
Tom Harper
Date
2.55 % 12/18/2019
19216MPN/g 12/18/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-53762 Site: 7 12/17/2019 8:20 AM Solid/Sludge Tom Harper
Test Method Results Date
Total Solids (%) SM 2540 a 2.71 % 12/1812019
Fecal Density SM 9221 C E MPN 24 hr 503 251OMPN/g 12/18/2019
Comment. Sludge residual results, except pH, reported on a dry weight basis. pH reported on an as received
basis.
Reviewed by: � x Ivy, _ D-t-� S-�"
Report #:: 2019-21213
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: W00000455
WWTPName: River Bend NPDESNumber: NCO030406
Monitoring Period: From 1/l/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved And AunrnAw..n "e v . a.
Class A:
I Alt. A (time/tern) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) Indicate "Process to Further Reduce Pathogens":
Compost ❑
I Heat Drying ❑
Hent Treatment ❑ Thermo philic ❑
Beta Ray ❑
I Garmna RE ❑
Pasteurization ❑ < ;',;;`;;;;;
Class B:
jAlt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Dr in ❑ Coraposting ❑
Aerobic Digestion ❑
Anaerobic ' Dt r estion El
If applicable to alternative erf r o med Class ( A or Class B) complete the following monitoring data:
Parameter
Allowable Level
Pathogen Density
urn er °
Frequency
Sample
na yttca
in Sludge
Excee-
Rnr.Aqg
of Analysis
Type
Tech-
Minimu
Geo. Mean
aximu
Units
2 x 10 to the
6th power
MPN
667
1,886
19,216
MPN/g
0
Annual
Grab
SM92210E
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
oftotalsolid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
weight)
. c�.ga caua aurae ncuucu°n t1JA PILAU U61 .11u t - Nease mcneate alternative nerfnrmed•
Alt.l (VS reduction) ❑
•
Alt. 2 (40-day bench)' ❑
_ ___ __-_______. _
Alt. 3 (30-day bench) ❑
I---_-...__.
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
I Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El
jAlt. 10 (Incorporation) ❑
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC '02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Brandon Mills, ORC Wesley Wooten, President
iiinature
e ame a Title (type or pri Land Applier Name and Title (if applicable)(type or print)
2/4/20 � 1/29/20
of reparer* Date Signature of Lan Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)
LEWIS FARMS
W00000455
River Bend W WTP
I?ate
Fecal Cokifoxm
M1'1�T er gnariz
Log
12/17/19
1,667
3.2219
12/17/19
2,944
3.4689
12/17/19
741
2.8698
12/17/19
667
2.8241
12/17/19
725
2.8603
12/17/19
19,216
4.2837
12/17/19
2,510
3.3997
Total 22.9285
Average 3.2755
Geometric Mean I Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.
LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 28, 2019
Sherwood Mobile Home Park Permit No. WQ0000455
3.23 % Solids
7.24 off
Parameter
%
Mg/Kg Dry Weight
( o x 10,000)
Pounds/Dry Ton
Nitrogen (TKN)
5.650
56,500.000
113,000
Phosphorus
2.930
29,300.000
58.600
Potassium
0.204
2,040.000
4.080
PAN (injected)*
1.789
17,892.100
35.784
PAN (surface)*
1.722
17,222.100
34.444
Ammonia Nitrogen
0.134
1,340.000
1 2.680
Calcium
2.210
22,100.000
44.200
Calcium Carbonate E .
---
-__
---
Magnesium
---
4,020,000
8.040
Sodium
--
1,860.000
3.720
Sulfur
_
__
_--
Nitrate N / Nitrite N
4.100
0.008
Barium
Chloride
---
---
---
---
___
---
SpR
0.54
Iron
---
---
--
Ceiling Concen.
Aluminum
---
6,350.00
12.700
)
Arsenic
--
16.60
0.033
75
Cadmium
---
16.60
0.033
85
Chromium
---
22.600
—
—_
Copper
---
243.00
0.486K75500
Lead
---
16.60
0.033
Mercury---
0.619
0,001
Molybdenum
---
16.60
0.033
Nickel
---
16.60
0.033
Selenium
-
16.60
0.033
Zinc
---
3,280.00
6.560
Environmental Chemists, Inc. 2019-01456
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or<detection limits are listed as detection limits
for calculation purposes.
7n:Viro:hem
ANALYTICAL & CONSULTING CHEMISTS
Sherwood MHP (WWTP)
753 Tallman Circle
Midway Park NC
Attention: Mikel Seely
Lab ID Sample ID:
19-03722 Site: sludge
Test
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Total Kjeldahl Nitrogen (TKN)
Nitrate+N itrite-Nitrogen
Total Solids (%)
PH
Ammonia Nitrogen
Total Phosphorus
Mercury
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
info@environmentalchemists.com
Date of Report: Feb 23, 2019
Customer PO #:
28544 Customer ID: 11020011
Report M 2019-01456
Project ID: annual sludge
Collect Date/Time Matrix Sampled by
1/28/2019 6:05 AM Solid/Sludge M. Seely
Method Results Date
EPA 200.7
6350 mg/kg
0210612019
EPA 200.7
<16.6 mg/kg
02/09/2019
EPA 2003
<16.6 mg/kg
02/0912019
EPA 200.7
22100 mg/kg
02/03/2019
EPA 200.7
22.6 mg/kg
02/09/2019
EPA 200.7
243 mg/kg
02109/2019
EPA 200.7
<16.6 mg/kg
02/09/2019
EPA 200.7
4020 mg/kg
02/03/2019
EPA 2007
<16.6 mg/kg
02/03/2019
EPA 200.7
<16.6 mg/kg
02/09/2019
EPA 200.7
2040 mg/kg
02/03/2019
EPA 200.7
<16.6 mg/kg
02/09/2019
EPA 200.7
1860 mg/kg
02/02/2019
EPA 200.7
3280 mg/kg
02/04/2019
EPA351.2
56500mg/kg
02/06/2019
EPA 353.2
4.10 mg/kg
02/13/2019
SM 2540 B
323 %
01 /29/2019
SM 4500 H B
7.24 units
02/04/2019
SM 4500 NH3 C
1340 mg/kg
02/19/2019
SM 4500 P F
29300 mg/kg
02/0612019
SW8467471B
<0.619mg/kg
02/02/2019
Report #:: 2019-01450 Page 1 of 3
Environmental Chemists, Inc.
f 6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab a 910.392.4424 Fax
sM. 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com
Sherwood MHP (WWTP) Date of Report: Feb 23. 2019
753 Tallman Circle Customer PO M
Midway Park NC 28544 Customer ID: 11020011
Attention: Mike[ Seely Report #: 2019-01456
Project ID: annual sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-03728 Site: 1 1/28/2019 6:06 AM Solid/Sludge M. Seely
Test Method Results Date Analvzed
Total Solids (%)
SM 2540 c
3.33 % 01/29/2019
Fecal Density
SM 9221 C E MPN 24 hr 503
105106MPN/g 01/28/2019
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
19-03730 Site: 2
1/28/2019 6:07 AM
Solid/Sludge M. Seely
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 G
3.23 % 01/29/2019
Fecal Density
SM 9221 C E MPN 24 hr 503
108360MPN/g 01/28/2019
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
19-03731 Site: 3
1/28/2019 6:08 AM
Solid/Sludge M. Seely
Test
Method
Results Date Analyzed
Total Solids (%)
SM2540G
3.09% 01/29/2019
Fecal Density
SM 9221C E MPN 24 hr503
113269 MPN/g 01/28/2019
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
19-03732 Site: 4
1/28/2019 6:09 AM
Solid/Sludge M. Seely
Test
Method
Results Date Analyzed
Total Solids(%)
SM2540G
3.25% 01/29/2019
Fecal Density
SM92210EMPN24hr503
107693MPN/g 01/28/2019
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
19-03733 Site: 5
1/28/2019 6:10 AM
Solid/Sludge M. Seely
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 G
3.25 % 01/29/2019
Fecal Density
SM92210EMPN 24hr503
166154MPN/g 01/2812019
Report #:: 2019-01456
Page 2 of 3
Environmental Chemists, Inc.
la
mP,
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/ Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com
Sherwood MHP (WWTP) Date of Report: Feb 23, 2019
753 Tallman Circle Customer PO #:
Midway Park NC 28544 Customer ID: 11020011
Attention: Mikel Seely Report #: 2019-01456
Project ID: annual sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
19-03734 Site: 6 1/28/2019 6:11 AM Solid/Sludge M. Seely
Test Method Results Date Analyzed
Total Solids (%) SM2540G 3.31 % 01/29/2019
Fecal Density SM 9221C E MPN 24 hr 503 72508 MPN/g 01/28/2019
Lab ID Sample ID:
19-03735 Site:7
Test Method
Collect Date/Time Matrix
1/28/2019 6:13 AM Solid/Sludge
Results
Sampled by
M. Seely
Date Analyzed
Total Solids (%) SM 2540 c 3 12 %
Fecal Density SM 9221C E MPN 24 hr 503 54488 MPN/g
Comment: Results, excep pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: S A A A
01 /29/2019
01/28/2019
Report #:: 2019-01456 Page 3 or 3
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: W00000455
WWTP Name: Sherwood Mobile Home Park NPDES Number: NCO022462
Monitoring Period: From 1/I/2019 To 12/312019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and nitprnatiu. nprrnrmpd-
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing) ❑
A1t,D (No Prior Test) q
Process to Further Reduce Patlio en s ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermo hilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑ ..
Class B:
JAIL (1) Fecal Density El
I Alt. (2) Process to Significantly Reduce Pathogens ❑It
If applicable to alternative performed (Class B only) indicate "Process to Siooificantl Reduce Pntbagens":
Lime Stabilization ❑
AirDrying ❑
Composting ❑
jAembic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitorin data
Parameter
Allowable Level
in Sludge
g
Pathogen Density
um cr o
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech'-
Minimu
Geo. MeanMaximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
54,488
98,693
166,154
MPN/g
0
Annual
Grab
SM9221 CE
CFu
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
weight)
vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed•
AIL I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ JAR.
4 (Spec. 01 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
JAIt. 6 (Alk Stabilization ❑
JAR 7 (Drying - Stable) ❑ JAR.
8 (Drying - Unstable) ❑
Alt. 9 (Injection) El
Alt. 10 (Incorporation) rQ
INo vector attraction reduction alternatives were performed ❑
a..G1�11e 11.K 111j1V IIlA i r,lvir iN 1 tpiease cnectc the appropriate statement)
l7 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
_ vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
1 ",a uctcrIII natran nas oven mane unuer my airecuon ano supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike[ Seely, ORC Wesley Wooten, President
Preparer Na e and Title (type or print) Land Applie//r Name and Title (if applicable)(type or print)
1/13/20
Signature of Preparer* Date Signature oFLay(d Applier (ifapplicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
DENR FORM PVRF 02T (1 WOOS)
LEWIS FARMS
WQ0000455
Sherwood MHP WWTP
FQ 10
MPi�1 et grain
01/28/19
105,106
5.0216
01/28/19
108,360
5.0349.
01/28/19
113,269
5.0541
01/28/19
107,693
5.0322
01/28/19
166,154
5.2205
01/28/19
72,508
4.8604
01/28/19
54,488
4.7363
Total 34.9600
Average 4.9943
Geometric Mean ik!i I Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction
requirement.
LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 9, 2019
Sterling Farms WWTP Permit No. WQ0000455
2.29 % Solids
6.59 nH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(MgLKg x 0.0021
Nitrogen (TKN)
1.000
67,000.000
134.000
Phosphorus
2.020
21,800.000
43.600
Potassium
1.010
6,940.000
13.880
PAN (injected)*
0.323
3,232.200
6.464
PAN surface)*
0.307
3,071.700
6.143
Ammonia Nitrogen
0.032
10,200.000
20.400
Calcium
8.720
17,300.000
34.600
Calcium Carbonate E .
--
Magnesium
4280.000
8.560
Sodium
--
3,610.000
7.220
Sulfur
---
--
Nitrate N / Nitrite N
---
7.500
0.015
Barium
---
__
Chloride
Iron
---
---
Aluminum
---
1,830.00
j 3.660
Arsenic
---
14.10
0.028
Cadmium
---
14.10
0.028
Chromium
---
14.100
Copper
274.00
0,548
Lead
---
14.10
0.028
Mercury
---
0.873
0.002
Molybdenum
14.10
0,028
Nickel
---
14.10
0.028
Selenium
14.10
0.028
Zinc
---
2,510.00
5.020
Environmental Chemists, Inc. 2019-20621
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
SAR
Ceiling Concen.
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = %d PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
75
85
840
57
75
420
100
Environmental Chemists, Inc.
envirochem
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0923 Lab • 910.392.4424 Fax
- sa 710 Bowsertown Road, Manteo, NC 27954 1 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentEJchomists.coln
Lewis Farms & Liquid Waste, INC. Date of Report: Dec 23, 2019
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report #: 2019-20621
Project ID: sludge
Lab ID Sample ID: Collect Daterrime Matrix Sampled by
19-52263 Site: SludgQe 12/9/2019 3:00 PM Solid/Sludge Wooten
i% -K
Test ,)-T--s�%°Mfj
Method
Results
Date Analyzed
Total Kieldahl Nitrogen (TKN)
EPA 351.2
67000mg/kg
12/19/2019
Sludge Residuals
Aluminum
EPA 200.7
1830mg/kg
12113/2019
Arsenic
EPA 200.7
<14.1 mg/kg
12/13/2019
Cadmium
EPA 200.7
<14.1mg/kg
12/13/2019
Calcium
EPA200.7
17300mg/kg
12/13/2019
Chromium
EPA 200.7
<14.1 mg/kg
12/13/2019
Copper
EPA 200.7
274 mg/kg
12/13/2019
Lead
EPA 200.7
<14.1 mg/kg
12/13/2019
Magnesium
EPA 200.7
4280mg/kg
12/1312019
Molybdenum
EPA 200.7
<14.1 mg/kg
12/13/2019
Nickel
EPA 200.7
<14.1mg/kg
12/13/2019
Potassium
EPA 200.7
6940mg/kg
12113/2019
Selenium
EPA 200.7
<14.1mg/kg
12/13/2019
Sodium
EPA 200.7
3610mg/kg
12/18/2019
Zinc
EPA 200.7
2510 mg/kg
12/13/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
7.50mg/kg
12/16/2019
Total Solids (%)
SM 2540 a
2.29 %
12110/2019
pH
SM 4500 H B
6.59units
12/17/2019
Ammonia Nitrogen
SM4500NH3 C
10200mg/kg
12/1612019
Total Phosphorus
SM 4500 P F
21800 mg/kg
12/1812019
Mercury
sw5467471a
<0.673mq/kg
12/15/2019
epon #r. 2019-20521
Pano 1 nl a
Environmental Chemists, Inc.
irkvirochem 6602 Windmill Way, Wilmington, NC 28405 4 910.392.0223 Lab • 910.392.4424 Fax
igM710 6owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
295-A Wilmington Highway, Jacksonville, NC 28540 0 910.347-5843 Lab/Fax
ANALYTICAL & CONSULTING. CHEMISTS info@enviromnentalehemists eom
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention: Wesley Wooten
Lab ID Sample ID:
19-52264 Site:1
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-52265 Site:2
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-52266 Site:3
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-52267 Site:4
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-52268 Site:5
Test
Total Solids (%)
Fecal Density
Date of Report: Dec 23, 2019
Customer PO #:
Customer ID: 14020008
Report #: 2019-20621
Project ID: sludge
Collect Date/Time
12/9/2019 3:05 PM
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Matrix Sampled by
Solid/Sludge Wooten
Results Date
2.21 % 12/10/2019
244344MPN/g 12/10/2019
Collect Date/Time Matrix Sampled by
12/9/2019 3:06 PM Solid/Sludge Wooten
Method Results Date Analyzec
SM 2540 B 2.13 % 12/10/2019
SM 9221C E MPN 24 hr 503 431925 MPN/g 12/1012019
Collect Date/Time
12/9/2019 3:07 PM
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Collect Datefrime
12/9/2019 3:08 PM
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Collect Date/Time
12/9/2019 3:09 PM
Method
SM 2540 B
SM 9221C EMPN 24 hr 503
Matrix Sampled by
Solid/Sludge Wooten
Results Date
2.31 % 12/10/2019
692641 MPN/g 12110/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Data Annhrvuri
2.23 % 12/10/2019
_ 107624 MPN/g 12/10/2019
Matrix Sampled by
Solid/Sludge Wooten
Results Date AnaIV701i
2, 30 % 12/10/2019
152174MPN/g 12/10/2019
Report It:: 2019-20621--
Pane 2 of 3
Environmental Chemists, Inc.
envirocheiia 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424 Fax
[sM1 710 Bowsertown Road, Mateo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540. • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoCoenviromnentalchemists.com
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention: Wesley Wooten
Date of Report: Dec 23, 2019'
Customer PO #:
Customer ID: 14020008
Report#: 2019-20621
Project ID: sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
19-52269 Site: 6 12/9/2019 3:10 PM Solid/Sludge Wooten
Test Method Results Date Analyzed
Total Solids (%) SM 2540 5 2.12 % 12/10/2019
Fecal Density SM 9221C E MPN 24 hr 503 113208MPN/g 12/10/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-52270 Site:7 12/9/2019 3:11 PM Solid/Sludge Wooten
Test Method Results Date
Total Solids (%) SM 2640 a 2.07 % 12/10/2019
Fecal Density SM 9221C E MPN 24 hr 503 444445 MPN/g 12/1012019
Comment: Sludge residuals and Fecal Density reported on a dry weight basis. pH reported on an as received
basis.
Reviewed by:
Report #:: 2019-20521
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: W00000455
W WTP Name: Sterling Farms NPDES Number: W00029475
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tem) 07
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Patho ens ❑
If applicable to alternative performed (Class A only) Indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatmeat ❑ Thermo rhilic ❑
Beta Ray ❑
t Gatnn aR1 ❑
Pasteurization
Class B:
Alt. (1) Fecal Density El
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Dryin❑�
Composting ❑
jAerobicDi estion ❑
Anaerobic Digestion ❑
' ' :: > >: »:::; :•
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Numuer or
Excee-
Frequency
of Analysis
Sample
Type
na y wa
Tech-
Minimu
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
Gth power
per gram of
total solids
MPN
107,624
249,530
692,641
MPN/g
0
Annual
Grab
SM 9221 CE
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacterial
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight
Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed:
Alt.l (VS reduction) ❑
jAlt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
jAlt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
jAit. 6 (Alk. Stabilization ❑
jAlt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) El
I Alt. 10 (Incorporation) El
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
O
n
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation wiry you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Cowell, ORC
Preparer Name and Title (type or print)
Sig��of4rep Date
Wesley Wooten, President
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (t2/2006)
LEWIS FARMS
W00000455
Sterling Farms WWTP
I?aie
Fecal Colrfotin
�,stg ';€
12/09/19
244,344
5.3880
12/09/19
431,925
5.6354
12/09/19
692,641
5.8405
12/09/19
107,624
5.0319
12/09/19
152,174
5.1823
12/09/19
113,208
5.0539
12/09/19
444,445
5.6478
Total 37.7799
Average 5.3971
Geometric Mean 249,53Ui Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.
LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 18, 2019
Topsail Greens
2.31 % Solids
7.26 pH
Permit No. WQ0000455
Parameter
%
Mg/Kg Dry Weight
x 10,000
Pounds/Dry Too
(Mg/Kg(Mg/Kg x 0.002
Nitrogen (TKN)
3.400
34,000.000
68.000
Phosphorus
L960
19,600.000
39.200
Potassium
0.251
2,510.000
5.020
PAN (injected)*
1.093
10,925.400
21.851
PAN surface)*
1.046
10,455.900
20.912
Ammonia Nitrogen
0.094
939.000
1.878
Calcium
3.870
38,700.000
77.400
Calcium Carbonate E .
Magnesium
1,390.000
2.780
Sodium
14,900.000
29.800
Sulfur
---
---
Nitrate N / Nitrite N
---
68.100
0.136
Barium
---
---
---
Chloride
---
___
Iron
---
---
Aluminum
---
2,440.00
4.880
Arsenic
---
8.40
0.017
Cadmium
---
8.40
0.017
Chromium
---
8.400
Copper
---
168.00
0.336
Lead
---
8.40
0.017
Mercury
---
0.779
0.002
Molybdenum
--
8.40
0.017
Nickel
---
8.40
0.017
Selenium
---
9.35
0.019
Zinc
---
918.00
1.836
Environmental Chemists # 2019-21353
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN
SAR
3.07
Ceiling Concen.
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
■
840
EnvIrr onmental Chemists, Inc.
!�nviroehem J 6602 Windmill Way, Wilmington, NC 28405 ` 910.392.0223 Lab ° 910.392.4424 Fax
rsiu? 710 Bowsertown Road, Manteo, NC 27954 ° 252.473.9702 Lab/Fax
- 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.3475843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@ enviromnentalcbemists.com
SC Water Services
Date of Report: Jan 08. 2020
113 Bellowing Doe Road
Customer PO #:
Hampstead NC
28443
Customer ID: 17010010
Attention: Stephen Crews
Report#: 2019-21353
Project ID: Topsail Greens Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-54081 Site: Sludge
12/18/2019 6:32 AM Solid/Sludge client
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
2440mg/kg
12/30/2019
Arsenic
EPA 200.7
<8.40 mg/kg
12130/2019
Cadmium
EPA 200.7
<8.40mg/kg
12/30/2019
Calcium
EPA 200.7
38700mg/kg
12/30/2019
Chromium
EPA 200.7
<8.40mg/kg
12/30/2019
Copper
EPA 200.7
168mg/kg
12/3012019
Lead
EPA 200.7
<8.40 mg/kg
12/30/2019
Magnesium
EPA 200.7
1390mg/kg
12/30/2019
Molybdenum
EPA2DO-7
<8.40mg/kg
12/3012019
Nickel
EPA 200.7
<8.40 mg/kg
12/30/2019
Potassium
EPA 200.7
2510mg/kg
12/3012019
Selenium
EPA 200.7
9.35mg/kg
12/30/2019
Sodium
EPA 200.7
14900mg/kg
12/30/2019
Zinc
EPA 200.7
918mg/kg
12/30/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
68.1mg/kg
01/06/2020
Total Solids (%)
SM25408
2.31 %
12/19/2019
pH
SM 45110HB
7.26units
12/23/2019
Ammonia Nitrogen
SM4500NH3 C
939mg/kg
12/20/2019
Total Kjeldahl Nitrogen (TKN)
SM45000rg8
34000mg/kg
12/30/2019
Total Phosphorus
SM4500PF
19600mg/kg
01/06/2020
Mercury
SW8467471B
<0.779mg/kg
12/28/2019
Comment: Results, except
pH, reported on a dry
weight basis. pH reported on an as received basis.
Reviewed by:
Report #:: 2019-21353
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQD000455
WWTP Name: Topsail Greens NPDES Number: DEH / Local
Monitoring Period: From 1/1/2019 To 1213112019
Pathogen Reduction (15A NCAC 02T .1106) - Please indieota Ipvpl Ae6tpvpd ....a aue .:.. ...,.o.,.....-
Class A:
Alt, A (time/temp) ❑
Alt B Atk Treatment
Alt. C '
Alt.D (No Prior Test) ❑ Process to FuRber Reduce Patho en s ❑
1f appIten le to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
1 Heat Drying ❑
Heat Treatment ❑ Thermo hiGc ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
JAR. (1) Fecal Density ❑
I Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Patho eas
Lime Stabilization
Air Drying ❑
Composting ❑
Aerobic Di estion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data
Parameter
Allowable Level
in Sludge
Pathogen Density
unuierar
Excee-
Frequency
of Anal sis
y
Sample
Type
a ica
Tech-
Minimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
wei t
Salmonella bacteria
(in lieu of fecal
coliform)
V .. •. __ Au_- •
3 MPN per4 grams
total solid (dry
wei ht
. ceav, nu, ucauu 1 CuucuUrr t10A 11Il.AI. 021.11071 - Please indicate alternAtive nprfarmod-
Alt.l (VS reduction) ❑
JAIL 2 (40-day bench) ❑
JAIL 3 (30-day bench) ❑ JAR.
4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
JAIL 6 (Alk. Stabilization p
Alt 7 (Drying -Stable) ❑
Alt. 8 (Drying- Unstable) ❑
Alt. 9 (Injection) ❑
JAIL 10 (Into ration) ❑
INo vector attraction reduction alternatives were performed ❑
a-i'Ji�lll•,1.t111v1. 01A1r,lVML-11 i tpiense cnecK the appropriate statement)
O "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
1 r.0 ucrerimnanon nas oeen made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Darrell Covington, ORC
Preparer l e d l peor print)
Signature of Preparer*
Land Applier Name and Title (if applicable)(type or print)
2- s-2c)
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .I 102 (26)
DENR FORM PVRF 02T (12/2006)
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LEWIS FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 3, 2019
Pluris - Webb Creek Permit No. W00000455
3.42 % Solids
6.R2 nT4
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
1 (M x 0.002)
Nitrogen (TKN)
7.550
75,500.000
151.000
Phosphorus
2.950
29,500.000
59.000
Potassium
0.629
6,290.000
12.580
PAN (injected)*
2.666
26,655.000
53.310
PAN (surface)*
2.392
23,915.000
47.830
Ammonia Nitrogen
0.548
5,480.000
10.960
Calcium
2.130
21,300,000
42.600
Calcium Carbonate E .
---
Magnesium
-
6,050,000
12.100
Sodium
---
2,500.000
5.000
Sulfur
---
---
Nitrate N / Nitrite N
---
169.000
0.338
Barium
---
---
Chloride
---
---
Iron
---
---
Aluminum
---
2,610.00
5.220
Arsenic
--
M90
0.022
Cadmium
---
10.90
0.022
Chromium
---
10.900
---
Copper
348.00
0.696
Lead
---
10.90
0.022
Mercury
0.673
0.001
Molybdenum
10.90
0.022
Nickel
--
10.90
0.022
Selenium
---
10.90
0.022
Zinc
---
3,510.00
7.020
Environmental Chemists 2019-16745
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = a/o PAN
SAR
0.72
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7.500
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.022.3 Lab • 910.392,4424 Fax
spy 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmeutalchemists.com
Pluris LLC.
P. O. Box 856
Sneads Ferry NC
Attention: Randy Hoffer
28460
Date of Report: Oct 18. 2019
Customer PO #:
Customer ID: 09110001
Report #: 2019-16745
Project ID: Webb Creek Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-42886 Site: Sludge
10/3/2019 9:20 AM Solid/Sludge William Andrews
Test
Method
Results Date
Analyzed
Sludge Residuals
Aluminum
EPA 200.7
2610mg/kg
10/0712019
Arsenic
EPA 200.7
<10.9mg/kg
10/07/2019
Cadmium
EPA 200.7
<10.9mg/kg
10/07/2019
Calcium
EPA 200.7
21300mg/kg
10/07/2019
Chromium
EPA 200.7
<10.9mg/kg
10/07/2019
Copper
EPA 200.7
348mg/kg
10/07/2019
Lead
EPA200,7
<10.9mg/kg
10/07/2019
Magnesium
EPA 200.7
6050mg/kg
10/07/2019
Molybdenum
EPA200.7
<10.9mg/kg
10/07/2019
Nickel
EPA 200.7
<10.9 mg/kg
10107/2019
Potassium
EPA 200.7
6290mg/kg
10/09/2019
Selenium
EPA 200.7
<10.9mg/kg
10/07/2019
Sodium
EPA 200.7
2500mg/kg
10/09/2019
Zinc
EPA 200.7
3510 mg/kg
10/07/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
169mg/kg
10/09/2019
Total Solids (%)
SM 2540 B
3.42 %
10/04/2019
pH
SM 4500 H B
6.82 units
10/14/2019
Ammonia Nitrogen
SM 4500 NH3 C
5480 mg/kg
10/0812019
Total Kjeldahl Nitrogen (TKN)
SM 4500 org a
75500 mg/kg
10/08/2019
Total Phosphorus
SM 4500 P F
29500 mg/kg
10/09/2019
Mercury
SW8407471B
<0.673mg/kg
10/13/2019
Report#.; 2019.1674E
Page 1 of 3
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lewis Farms & Liquid Waste, Inc.
WWTP Name: Pluris - Webb Creek
Monitoring Period: From 1/1/2019
WQ Permit Number: W00000455
NPDES Number: NCO062642
12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed:
To
Class A:
Alt. A (time/temp) ❑
7Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treahnent ❑ Thennophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B. 7Alt.
(1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization p
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Num er o
Excee-
encesY
Frequency
of Analysis
Sample
Type
Analytical
Tech-
n one
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x I0 to the
6[h power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacterial
(in lieu of fecal
colif I
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction)
❑
Alt. 2 (40-day bench)
JAIL 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
lAlt. 6 (Alk. Stabilization Ej
lAlt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
lAlt. 10 (Incorporation) ❑
lNo vector attraction reduction alternatives were performed
❑
C'ER Dv!CATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
'"I ins determination nas been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Wesley Wooten, President
Preparer//Name and Title (type or print)
Gt/0-1-26--
Signature o reparer*
Land Applier Name and Title (if applicable)(type or print)
1/14/2020
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
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2019 APPLICATION SUMMARY
LEWIS FARMS
Permit # WQ 0000455
2019
RESIDUALS APPLICATIONS
APPLICATION SUMMARY
FIELD
NO.
ACRES
USED
TOTAL
GALLONS
TOTAL
WET TONS
TOTAL
DRY TONS
TOTAL PAN
Crop 1 Crop 2
L2
14.20
178,000
17.22
5.94
3.98
L3
18.60
271,000
40.66
25.82
36.80
L4
24.50
318,000
45.35
46.78
41,76
L5
23.30
289,500
40.29
82.14
0.00
L6
5.80
80,000
4.37
32.30
5.70
L8
31.20
612,000
76.05
36.47
21.36
L9
36.70
300,500
35.09
29.74
8.78
W 1
33.70
366,000
45.71
17.09
31.72
W2
36.70
540,000
75.66
103.25
0.00
W3
24.20
390,000
54.64
78.29
34.80
AW-F1
36.30
390,000
54.64
46.39
29.00
Totals
285.20
3,735,000
489.70
Metric Tons 444.16
FIELD LOADING RATE REPORTS
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SOIL ANALYSIS REPORTS
The current pH on these fields are not reflective of the liming amendments applied to the field in late
December of 2019 (1 ton/acre). Lewis Farms will continue to monitor these fields in the future and
make any necessary adjustments to pH as needed.
Martin Mahe
Agronomist
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