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HomeMy WebLinkAboutWQ0000702_Residual Annual Report 2019_20200210Initial Review INITIAL REVIEW Reviewer Williams, Kendall Is this submital an application?* r Yes r No Annual Report 2019 Year* Date Paper Copy 2/10/2020 Received:* Project Number* WQ0000702 Email Notifications ................................................................................................... Does this need O Yes review by the a No hydrogeologist? * Regional Office CO Reviewer Admin Reviewer Kendall.Williams@ncdenr.gov Submitted Form Project Contact Information Rease provide information on the person to be contacted by NUB Staff regarding electronic submittal, confirmation of receipt, and other issues. .................................................................................................................................................................................................................................................................................................................................................................................................... Name * Martin Mabe Email Address* martin@willcoxmabesoil.com Project Information ........................................................................................................................................................................ Submittal Type* f New Permit Application r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0000702 Applicant\Permittee * Frank Bottorff Facility Name * City of Havelock Phone Number* 3363121396 r Modification (Major or Minor) r Additional Information r Other r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. One hard copy is being mailed to NCDEW-DWR-NDCU Please attach all information required or requested for this submittal to be review here. Application Forrn Engineering Rans, Specifications, Calculations, Etc.) Havelock 2019 Annual Report NCDEQ.pdf 22.46MB Upload only 1 R7F document. I laltiple docurrents must be corrbined into one RJF file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contact the reviewer or Tessa Monday. If a paper application is required, be advised, applications accepted for pre -review until both the paper and electronic copies have been received. The paper copy shall include the following: o Application Form o All relevant attachments (caIcs, sails report, specs, etc. o one full-size engineering plan set 0 one 11x17" engineering plan set 0 one extra set of specifications o Fee (if required} Mailine address: Division of Water Resources Division of Water Resources Non -Discharge Branch I Non -Discharge Branch ---- --- - --- - --- ------------ ------------------------------------i---------------------------------------------------------------------------- 1617 Mail -service Center Att: Nathaniel Thornburg, 9"' Floor, Office #942W ---- -NC �-- - -------------------------------------------- ------------------------------------------------ Raleih, 7699-1617 512 N. SaVisbury St For questions or problems contact Tessa Monday at tessa.monday@ncdenr.Qov or 919.707.3660. * W By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 2/6/2020 2019 ANNUAL REPORT LAND APPLICATION PROGRAM CITY OF HAVELOCK PERMIT #WQ0000702 Prepared For: Bio-Nomic Services 530 Woodlawn Street Belmont, North Carolina 28012 Compiled By: Willcox & Mahe Soil Solutions, PLLC 7231B Summerfield Road Summerfield, North Carolina 27358 February 2020 willcox&mabe SOIL SOLUTIONS February 6, 2020 NCDEQ-DWR 512 North Salisbury Street, 9 h Floor, Room 942X Raleigh, North Carolina 27604 Attention: Non -Discharge Permitting Unit Reference: 2019 LAND APPLICATION ANNUAL REPORT City of Havelock Permit No. WQ0000702 WMSS Project No. 15-18 Ph: 02 Non -Discharge Permitting Unit: Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting requirements as specified in the above referenced permit on behalf of Bio-Nomic Services, Inc. (Bio-Nomics) for the City of Havelock. WMSS compiled this report using data gathered during the compliance year by Bio-Nomics and the City of Havelock. This data includes: 1) certification form, 2) residuals analyses and pathogen / vector data, 3) application summaries and field loading rate reports, and 4) soil analyses. If there is any further information required or questions regarding this annual report please do not hesitate to contact the City of Havelock for further assistance. Sincerely, WMSS Martin Mabe NC Land Application/Residuals Operator #22753 Enclosures Shared\WMSS Projects\2015\15-18 Bio-Nomics\Phase 02 - Havelock\2019 Annual Report\2019 ANNUAL REPORT.doc Willcox & Mabe Soil Solutions, PLLC /7231 B Summerfield Road / Summerfield, NC 27358 / Rob336.339.9128 or Martin 336.312.1396 / www.willcoxmabesoil.com Bio-Nomic Services, Inc. 530 Woodlawn Street Belmont, North Carolina 28012 704-529-0000 CITY OF HAVELOCK NPDES #NC0021253 NC PERMIT # WQ0000702 Mr. Frank Bottorff, City Manager City of Havelock Post Office Box 368 Havelock, NC 28532 LAND APPLIERS: Bio-Nomic Services, Inc. 530 Woodlawn Street Belmont, North Carolina 28012 704-529-0000 2019 City of Havelock WWTP Dry Tons to Land Application 153.81 2019 City of Havelock WWTP Dry Metric Tons to Land Application 139.51 Total Dry Metric Tons 139.51 TABLE OF CONTENTS SECTION NO. TITLE Certification Form II Residuals Analyses & Pathogen / Vector Attraction Data III 2019 Application Summary and Field Loading Rate Reports IV Soil Analysis CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit##: W00000702 County: Facility Name (as shown on permit): Land Application Operator: Craven Year: 2019 City of Havelock Bio-Nomic Services, Inc. Phone: 704-529-0000 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summarv: Total number of application fields in the permit: 61 Total number of fields utilized for land application during the year: 18 Total amount of dry tons applied during the year for all application sites: 153.81 Total number of acres utilizes for land application during the year: 68.9 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. El Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .l I I 1 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Frank Bottorff, City Manager Permittee Namond Title,('(ype or print) Signature of Permittee Date S ignature of Land Applier Date (if differe t rom�xmittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) RESIDUAL ANALYSES TCLP ANALYSES AND PATHOGEN AND VECTOR ATTRACTION REDUCTION Ew ►a Y c O c O W a N 0 n O O O O I N M 7 kn M N O O d E z PO F a OC> N p O O M M O O O � d• ,-- M � •r GJ cq Q m � O O O D O N O O O N M M V M O O O M C� Vt N Chi VMi O U 0 U Ll, E O CM N M O vt V1 M •� .-• N d' V Ozt D D M D 0 O O M D O p O M z z z z o rn y a� E o O `1 O •O P. ? F C x •O O `�' z _ z 'O \ bD y E a p m .. 'OO c� v 5 x ca E¢ N a F ¢ z 0 �+ y a Q �I-- — a 'y V 00 v G i.I E ° N Ln V�1 •ii O y •3 ro V L V O C � C3 y ra a+ O � V y lVQ V = L Cl C M O N � G ,a a y � L O � a o � i:+ y 4Vi C L O �y E E L F d � c o s a+ G � L � G m � C C �+ C3 C .fl d y E L C � u y o PC = a, r L � G = L� �+ G � V C wd 0 0 y �0 O G Gw'_ N R C O` C y w�' r L O V L u � y H R E 4� I a m 0 n 0 0 0 O I d M N 0 O I i i �u i ore■ fi CITY OF HAVELOCK LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 14, 2019 Havelock Permit No. NCO021253 Mineralization Rate 0.30 3.49 %Solids 6.3 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 4.930 49,300.000 98.600 Phosphorus 5.408 54,080.000 108.160 Potassium 0.424 4,244.000 8.488 PAN (injected)* 1.594 15,938.080 31.876 PAN (surface)* 1.512 15,121.580 30.243 AmmoniaNitrogen 0.163 1,633.000 3.266 Calcium 3.411 34,108.000 68.216 Calcium Carbonate Eq. - --- Magnesium --- 2,246.000 4.492 Sodium --- 3,413.000 6.826 Sulfur - Nitrate N / Nitrite N --- 4.980 0.010 Barium Chloride Iron --- --- --- ___ -- SA 0 Ceiling Concen. Aluminum --- 22,819.00 45.638 (M g) Arsenic --- 3.000 0.006 75 Cadmium 1.100 1 0.002 85 Chromium 17.000 0.034 -- Copper --- 708.00 1.416 4,300 Lead --- 21.00 0.042 840 Mere --- 0.390 0.001 57 Molybdenum --- 6.000 0.012 75 Nickel --- 11.00 0.022 420 Selenium --- 1 5.000 0.010 100 Zinc --- 1,800.00 3.600 7,500 Environmentl : 414 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Emworro�lo]i pM I D000rrPor Udo 114 OAKMONT DRIVE GREENVILL_E, N.C. 27858 CITY OF HAVELOCK(SLUDGE) MR. RODNEY GEORGE WASTEWATER TREATMENT PLANT 304 N. JACKSON DRIVE HAVELOCK ,NC 28532 PARAMETERS P11, Units Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt, basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt, basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/lig Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Sodium Adsorption Ratio (cahc) Total Solids, %. TIIN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/fig Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 6.3 01/18/19 JTH 4500HB-11 22819 01/17/19 LFJ EPA200.7 3.0 01/22/19 MTM 311313-04 34108 01/17/19 LFJ EPA200.7 1.1 01/17/19 MTM 3113B-04 708 01/17/19 LFJ EPA200.7 17 01/17/19 LFJ EPA200.7 21 01/18/19 MTM 3113E-04 2246 01/17/19 LFJ EPA200.7 0.39 02/07/19 MTM EPA7471B 11 01/17/19 LFJ EPA200.7 4244 01/17/19 LFJ EPA200.7 <5.0 01/28/19 MTM 3113E-04 3413 01/17/19 LFJ EPA200.7 1800 01/17/19 LFJ EPA200.7 4.8 3,49 01/14/19 RDS 2540G-11 c 49300 01/23/19 BLD 351.2 R2-93 c 1633 01/24/19 CLO 350.1 H2-93 c 54080 01/23/19 DTL 365.4.74 c 4.98 01/16/19 BLD 353.2 R2-93 15938 01/28/19 SEJ 6 01/17/19 LFJ EPA200.7 Drinking Water To, 17719 Waeteweter ID. 10 PHONE- (252) 756-6208 FAX (252) 756-0633 ID#: 414 DATE COLLECTED: 01/14/19 DATE REPORTED : 02/08/19 REVIEWED BY: 0 Dncertif Lod data. DWR doe. not offer non -aqueous certification for thin analytical procedure. C O2 ¢ p w U Q � ¢ p Z z ¢ Z O' C W Y W d Z 2 �2 a � � 51531/Sk1313Wtlkltld � r¢n a � � a s1OIOLII azal . 0 C sapp1q,13H dial U' d mwalMd d1ol 0 6 IOAS/[OA dial — QI �11AISO.IiOa — a @ 4111!ge11uEI 1L 6 ijlAllaEaZj Gi NVd w O a. .4 Pod W C '021IN Oluouruiy w @ NAS Q w C sPHOS IOIOI % Z' ZZ E1S <G -It SIRION a C Hd p SH3NIV1NO03011 U w s N0110311001V 0.,'3HmOdMi w N611O3TIOO ltl I1bO HO w w Lq 1/ W'3NIHOIHOltl101 Q Q w o Mw IE Z e 0aiE x ky7 0 m m m N�yj�j`S y �l 0o3c�0 a Sa z z z z ui v' P. `1 " El gs 3� w � E N N E a E � w CD 0 w z z t€yi 4 Q ¢ J F- cc Ur 2 N z > q t Z m J m ¢ o w u. c; 5 to j w m U El o� wa rn a U O S1S31JSU313V4VUVd a �s g 0 U F W z Z SH3NIVINOOHOIi M w o c� c� NOIlO311001V h u, x y O 0:'3un.LV83MR } a o a X, U 70. 110110311001v 116n u0 '3NIu0lHO O 0. [71 [71 w cwi ' p I16W lV101 w ¢ w N M o J w ¢� o � U O g (n . `-. �� .. oW aA Q S2 L9 Ou Zqw y r^i m m 6�DW.xx y s .9 0 Li '3 6' O fn ti a� o ti a 4-i VN�1 0. z v :c r l9 w u CITY OF HAVELOCK LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 15, 2019 Havelock Permit No. NC0021253 Mineralization Rate 0.30 3.44 % Solids 6.5 pH Parameter % Mg/Kg Dry Weight Pounds/Dry Ton (Mg/Kg x 0.002) (TKN) 4.793 47,930.000 95.860 horus 2.949 29,490.000 58.980 rNitrogen ium 0.428 4,283.000 8.566 (injected)* 1.700 17,002.280 34.005 PAN (surface)* 1.513 15,132.780 30.266 Ammonia Nitrogen 0.374 3,739.000 7.478 Calcium 2.951 29,512.000 59.024 Calcium Carbonate Eq. --- .-- __- Magnesium --- 2,165.000 4.330 Sodium --- 3,187.000 6.374 Sulfur ___ -__ --- Nitrate N / Nitrite N --• 5.980 0.012 Barium Chloride --- --- --- --- SAR 0.89 Iron --- --- --- Ceiling Concen. Aluminum 19,580.000 39.160 (Mg/Kg) Arsenic --- 2.500 0.005 75 Cadmium --- 1.200 0.002 85 Chromium -- 15.000 0.030 -- Copper --- 578.000 1.156 4,300 Lead --- 13.000 0.026 840 Mercury --- 0.220 0.000 57 Molybdenum --- 5.000 0.010 75 Nickel --- 11.000 0.022 420 Selenium 5.000 0.010 100 Zinc 1,508.000 3.016 7,500 Environment I, Inc. 414 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N+ Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. L�dorro��c�� Flo � �c�QpoQa �d Drinking Water 10. 17715 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OP HAVELOCK(SLUDGE) MR. RODNEY GEORGE WASTEWATER TREATMENT PLANT 304 N. JACKSON DRIVE HAVELOCK ,NC 28532 PARAMETERS PH, Units Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), fug/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/Icg Chromium, T.(dry wt, basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zhu (dry wt. basis), mg/kg Sodium Adsorption Ratio (cafe) Total Solids, % TKN (dry wt.), mg/lig Ammonia Nitrogen ((try wt.),mg/Icg Phosphorus, T. (dry wt.), mg/lig Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 6.5 04/17/19 JTH 4500HB-11 19580 04/24/19 LPJ EPA200.7 <2.5 04/23/19 MTM 3113E-04 29512 04/24/19 LPJ EPA200.7 1.2 04/25/19 MTM 3113B-04 578 04/24/19 LPJ EPA200.7 15 04/24/19 LPJ EPA200.7 13 04/24/19 MTM 3113B-04 2165 04/24/19 LPJ EPA200.7 0.22 05/10/19 MTM EPA7471B 11 04/24/19 LPJ EPA200.7 4293 04/24/19 LPJ EPA200.7 <5.0 04/30/19 bITM 3113B-04 3187 04/29/19 AKS 3111B-11 1508 04/24/19 LPJ EPA200.7 4.8 3.44 04/16/19 KDS 254OG-11 c 47930 04/18/19 TLH 351.2 R2.93 e 3739 04/18/19 BLD 350.1 112-93 c 29490 04/19/19 DTL 365.4.74 c 5.98 04/18/19 DTL 353.2 112-93 17002 04/22/19 SEJ <5.0 04/24/19 LPJ EPA200.7 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 414 DATE COLLECTED: 04/15/19 DATE REPORTED : 05/13/19 REVIEWED BY: -- c Uncertified data. ➢WR does not offer non-agueoue certification for this analytical procedure. 1-1 d'. 0 W 0 U < � 4 Z F G � w O ¢ j Fw- 4 Z N o Q S N Z Lu Q I- yi h W z Z m g ❑ w LL C7 � � �' � p w F � p Lai w CY w c ¢ Z ¢ U W ¢ ¢ U Q m U w¢ w IJ ¢ x O x a g S1931/Suli-INVIM cxi v a ''.'€ ~cW Ntld via 2 � w d el!al!N-a1xa1[hI �t� U a d 40d a - d .141IN ertLowwy — Z , : a d ARIL — a — a PROS 181oy b d Hys — a d Hd % Z j SN3NIU\100dOi!- 0 C7Lj7 N0110311001V C 0 z U O 0'3kifllVU34171 w o w w P!0110 �i IIV -_ — —..-- — ❑ NINOIH1100 OI I�6w'jNlti0lH'J lVi01 w w gCV)0 � M w � s �Q+ I`C O Vf O vl ry rl :L w (x� y=� a .40 zL) O Z Uo h u O �•oyw' w w V Z w u�3M� 0 CITY OF HAVELOCK LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: July 15, 2019 Havelock Mineralization Rate 0.30 Parameter Carbonate N / Nitrite N 4.39 %Solids 6.6 pH Y. Mg/Kg t% x 3.612 Permit No. NCO021253 D ry Weight Pounds/Dry Ton 10,000) (Mg/Kg x 0.002) 53,120.000 106.240 36,120.000 72.240 3,937.000 7.874 17,432.780 34.866 16,365.780 32.732 2,134.000 4.268 31,184.000 62.368 2.980 3.30 1.40 12.00 641.00 12.00 0.32 9.00 9.00 5.00 1.685.00 7.328 0.006 41.324 0.007 0.003 0.024 1.282 0.024 0.001 0.018 0.018 0.010 3.370 Environment 1, Inc. k 414 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. SAR 1.12 Ceiling Concert. (M /Kg) 75 85 4,300 840 57 75 420 100 7,500 2.980 3.30 1.40 12.00 641.00 12.00 0.32 9.00 9.00 5.00 1.685.00 7.328 0.006 41.324 0.007 0.003 0.024 1.282 0.024 0.001 0.018 0.018 0.010 3.370 Environment 1, Inc. k 414 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. SAR 1.12 Ceiling Concert. (M /Kg) 75 85 4,300 840 57 75 420 100 7,500 EmwoPomn@[N T, bw N.C. CITY OF HAVELOCK(SLUDGE) MR. RODNEY GEORGE WASTEWATER TREATMENT PLANT 304 N. JACK60N DRIVE RAVELOCK ,NC 28532 PARAMETERS PH, Units Aluminum, (dry wt. basis), mg/kg Arsenic ((fry wt. basis), mg/kg Calcium (dry wt, basis), mg/kg Cadmium (dry wt. basis), mk/kg Copper (dry wt. basis), mg/Icg Chromium, T.(dry wt. basis),mg/kg Lead (dry -weight basis),. mg/Icg Magnesium (dry wt, basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/Icg Sodium (dry wt. basis), mg/Icg. Zinc (dry wt. basis), mg/kg Sodium Adsorption Ratio (calc) Total. Solids, % TKN (dry wt.), mg/Icg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mglkg Nitrate-Nitri(e (dry wt.), mglkg Platt Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mglkg Sludge Analysis Method Sample Date Analyst Code 6.6 07/17/19 JTH 45001113-11 20662 08/06/19 LrJ EPA200.7 3.3 08107/19 MTM 3113B-04 31184 09/07/19 LFJ EPA200.7 1.4 08/06/19 MTM 3113B-04 641 08/07/19 LFJ EPA200.7 12. 08/07/19 LFJ EPA200.7 12 08/08119 MTM 3113B-04 2434 08/07/19 LFJ EPA200.7 0.32 07/26/19 MTM EPA7471B 9 08/07/19 LFJ EPA200.7 3937 08/07/19 LFJ EPA200.7 <5.0 08/07/19 MTM 3113B-04 3664 08/06/19 LFJ EPA200.7 1685 08/07/19 LFJ EPA200.7 5.4 4.39 07/16/19 IMS 2540G31 c 53120 07/18/19 TLH 351.2 R2-93 c 2134 07/19/19 AILS 350.1 R2-93 c 36120 07/18/19 BLD 365.4.74 c 2.98 07/19/19 TLH 353.2 R2.93 17433 07/25/19 SEJ 9 08/07/19 LFJ EPA200.7 ID#; 414 DATE COLLECTED; 07/15/19 DATE REPORTED : 08/13/19 REVIEWED BY: :� _ 0 Uncertified data. DWR does not oiler non -aqueous oartilicetlon for this -analytical procedure. 756-0. 03 I 0 a Q F y Z _ w F- O w ¢ Z O O a o tn� w g 3E w Q m � rlrlsa � s � � a S1S3JS8313WVHVd NVd w w d ��F11lN-alB�1FN a C Pod w C 'on�N oluowuiy � M � � w C NYZ w d SPHOS FIGIL % C Hvs OY w d SI�IaL1[ w C Rd w Za S83NIVBOOJON oz u `'' Z N0110311001tl 8 N011031loo IV I/6n HO 4 > A �'Cl[71 Aw'3NIHO]HO 1V101Is w o F �(w� N •Yi 0 i.j {I. Eo ac4o o ri U C4 in Ggi s� c�aoz m m m zk'Ogy_0 o m a a G0 *4 N 5a U CL N OI Z 1. 0 CITY OF HAVELOCK LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: October 8, 2019 Havelock Permit No. NCO021253 Mineralization Rate 0.30 5.09 % Solids 6.7 off Parameter %* Mg/Kg Dry Weight % x 19,0001 Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 4.745 47,450.000 94.900 Phosphorus 3.250 32;500.000 65.000 Potassium 0.261 2,606.000 5.212 PAN (injected)* 1.572 15,723.390 31.447 PAN (surface)* 1.466 14,662.390 29.325 Ammonia Nitrogen 0.212 2,122.000 4.244 Calcium 3.364 33,641.000 1 67.282 Calcium Carbonate Eq. --- -- Magnesium --- 1,907.000 3.814 Sodium --- 3,542.000 7.084 Sulfur --- --- --- Nitrate N / Nitrite N --- 2.990 0.006 Barium --- --- --- Chloride -- --- --- Iron --- --- --- Aluminum --- 22,524.00 45.048 Arsenic 3.000 0.006 Cadmium --- 1.300 0.003 Chromium --- 14.000 0.028 Copper --- 607.00 1.214 Lead --- 15.000 0.030 Mercury --- 0.300 0.001 Molybdenum --- 7.000 0.014 Nickel --- 8.00 0.016 Selenium --- 5.000 0.010 Zinc 2,417.00 4.834 Environment I, Inc. # 414 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits for calculation purposes. Ceiling Concen. 85 840 75 420 100 7.50i Environment 1t Inc GREENVILLE, N.C. 27858 CITY OF HAVELOCK(SLUDGE) MR. RODNEY GEORGE WASTEWATER TREATMENT PLANT 304 N. JACKSON DRIVE HAVELOCK ,NC 28532 PARAMETERS PH, Units Aluminum, (dry wt. basis), mg/Icg. Arsenic (dry wt. basis), rug/kg Calcium (dry wt. basis), mg/leg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt, basis),mgllcg Lead (dry weight basis), mg/kg Magnesium (dry wt, basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mglkg Sodium (dry wt. basis), mg/kg Zinc. (dry wt. basis), mg/kg Sodium Adsorption Ratio (cafe) Total Solids, %a TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/Icg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/lig Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/Icg Sludge Analysis Method Sample Date Analyst Code 6.7 10/10/19 GNB 4500HB-11 22524 11/22/19 LtJ EPA200.7 3.0 11114/19 MTM 3113)3.04 33641 11/22/19 LFJ EPA200.7 1.3 11/15/19 MTM 3113B-04 607 11/22/19 LFJ EPA200.7 14 11/22/19 LFJ EPA200.7 15 11/14/19 MTM 311313-04 1907 11/22119 LFJ EPA200.7 0.30 10/25/19 MTM EPA7471B 8 11/22/19 LFJ EPA200.7 2606 11/22/19 LFJ EPA200.7 <5.0 11/19/19 MTM 3113B-04 3542 11/22/19 LFJ EPA200.7 2417 11/22/19 LFJ EPA200.7 5.1 5.09 10/,10/19 ICDS 2540G-1l c 47540 10/16/19 AKS 351.2 R2-93 c 2122 10/10/19 BLD 350.1 R2.93 c 32500 10/16/19 TLH 365.4-74 c 2.99 10/15/19 BLD 353.2 112-93 15750 10/17/19 SEJ 7 11/22/19 LRJ EPA200,7 FAX ID#: 414 DATE COLLECTED-: 10/08/19 DATE REPORTED : 11/25/19 REVIEWED BY: c Uncertified data. DWa done not offer non-aquooun certification for thin analytical procedure.. 0 w ra i� F 7 R o w LL (7i 2 o a Pii La w � 0 ox } W y ¢ = U O U 2 Z j'0'� Q x S1S3llSH313WVHVd U1 Nvd w ¢ Pod °c3 a d 'oA!N encoumcyno m µES µFA r µES a 6 N311 Q Q M d SPROS MOIL % v d Nvs M d SIuIaw a d Hd p z SH3NIV1NOOdON '^ -- 0 N011O3TI0Oltl 0 z m m m W > o 0-'3HMVH3dVM A [D go �a V6W 3NIH01HOIltll001 c� o F c O w w \ w w w 0 EE a w ow SO 0e°$ z 0 0 cD 4.b CW7QU o e� y V � ¢ z O 3 O 0 N i . � ❑ � Y. F � N � rj� u� a M N. M :3 EE E E in L7 0 TCLP ANALYSIS —` h 0rlarfda; The reSLl1ts Set forth herei4 are provided by SGS North America Inc. T ' hn cal Report fat Environment 1, Inc City of Havelock WWTP; 304 N Jackson Dr, Havelock, NC 414 SGS Job Number: FA60954 Sampling Date: 01/14/19 Report to: ,ironment 1, Inc Box 7085 enville. NC 27835 Deedee Woolard Total number of pages in report: 14 e-Hardeopy 2.0 Anlorrrated Report V'pCf6 O etlinBZtMS. Test results contained within this data package meet Ike requirements of the National Environmental Laboratory Accreditation Program General Manager and/or stale specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Cal ti6callons: FL(E83510), LA(0305L), KS(E-10327), IL(200063), NC(573), NJ(FLOo2), NY(L2022), SC(96038000 DoD ELAP(ANAII L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, 1A, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV TIOs report shall not he reproduced, except in its enlirely, without (lie written approval of SGS. Tesl results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • lel; 407-425-0700 SGS is the sole au(hvi ily for authorizing edits or nmdifrca(ions to this document. please; shorn your ideas about Unliuthorized modification of (his report is strictly prohibiled. how wo onn serve you better at: Review standard terns at: blip:/hwvsysgs.comkn/Ictms-and-conditions EHSAJS.CuslmnarCare n sgs.com Fax: 407-425.0707 1 of 14 FA9e95A Table of Contents Section1: Sample Summary..........................................................................I....................... Section2: Summary of Hits ............................................................................................... Section3: Sample Results......................................................................................................, 3.1: FA60954-1: SLUDGE SAMPLE................................................................................. 3.2: FA60954-IL: SLUDGE SAMPLE............................................................................... Section4: Misc. Forms............................................................................................................ 4.1: Chain of Custody........................................................................................................... Sections: 3 4 p' 5 ^` 6 7 12 13 _ SGa''.. 2 of 14 rAGN54 SGS North America Inc. Sample Summary Environment 1, Inc City of Havelock WWTP; 304 N Jackson Dr, Havelock, NC Project No: 414 Job No: FAG0954 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA60954.1 01/14/19 13:25FW 01/19/19 AQ Water M6006474L401/14/19 13:25FW 01119119 AQ Water SLUDGEUMPLE SLUDGE8AMPLE I -SGS' 3 of 14 FAMU Summary of Hits Job Number: FAGO954 Account: Environment 1, Inc Project: City of Havelock WWTP; 304 N Jackson Dr, Havelock, NC Collected: 01/14/19 i e Page 1 of 1 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA60954-1 SLUDGE SAMPLE Corrosivity as pH kg Ignitability (Flashpoini) a > 200 FA60954-1L SLUDGE SAMPLE No hits reported in this sample. (a) Not ignitable. su SW846 CIIAP7 Deg. F SW8461010A 1 4of 14 _SG$. fAGU95d Sample Resplts Report of Analysis 5 of 99 _ SG5.. FAfi0951 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA60954-1 Date Sampled: 01/14/19 Matrix: AQ - Water Date Received: 01/19/19 Percent Solids: 1.2 Project: City of Havelock W WTP; 304 N Jackson Dr, Havelock, NC Page 1 of 1 General Chemistry Analyte Result RL Units DF Analyzed By Method Coirosivity as pH 6 0 so 1 01/29/1912:43 Bw SW846 CHAP7 Cyanide Reactivity <1,5 1.5 mg/I 1 01129/1918:27 JK SW046CHAP7 Ignitabilily (Flashpoint) a >'200 Deg. F 1 02/02/19 11:30 BW swe4c loioA Solids, Percent 1 01/23/19 14:46 BR SMI0254OG Sulfide Reactivity c5o 50 mg/1 1 01/29/19 14; 15 Bw sw64s cHAP7 (a) Not Ignitable. RL = Reporting Limit 6 of 14 i FA60964 SGS North America Inc. Report of Analysis Page 1 of I Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA60954-1L Date Sampled: O1114/19 Matrix: AQ - Water Date Received: 01/19/19 Method: SW846 8260B SW846 1311 Percent Solids: 1.2 Project: City of Havelock WWTP; 304 N Jackson Dr, Havelock, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run 41 Y39989.1) 10 01/25/19 15:30 SP O1/24/19 09:00 OP73531 VY1597 Run #2 Purge Volume #1 5.0 ml #2 VOA TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 71-43-2 Benzene ND D018 0.50 0.010 0.0031 mg/1 78-93.3 2-Butanone (MEK) ND D035 200 0.050 0.020 mg/I 56-23-5 Carban Tetrachloride ND DON 0.50 0.010 0.0036 mg/1 108-90-7 Chlorobenzene N..D D021 100 0.010 0.0020 mg/l 67-66-3 Cldorofonn ND D022 6.0 0,010 0.0030 mg/l 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.010 0.0026 mg/I 107-06-2 1,2-Dlchloroethane ND D028 0.50 0.010 0.0031 mg/1 75-35-4 1,1-Dichloroethylene ND '' D029 0.70 0.010 0.0032 mg/l 127-18-4 Tetrachloroethylene ND D039 0.70 0,010 0,0022 mg/l 79-01-6 Trichloroethylene 'ND D040 0.50 0.010 0.0035 mg/l 75-01-4 Vinyl Chloride ND D093 0.20 0.010 0.0041 mg/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromolluoromethane 111% 83-118% 17060-07-0 1,2-Dichloroelhane-D4 1.09% 79-125% 2037-26-5 Toluene-D8 93% 85-112% 460-00-4 4-Bromotluorobenzene 98So 83-118% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyle found In associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound AN i 7of 14 SG fAG0954 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA60954-1L Date Sampled: 01/14/19 Matrix: AQ - Water Date Received: Ol/19/19 Method: SW846 8270D SW846 3510C Percent Solids: 1.2 Project: City of Havelock W WTP; 304 N Jackson Dr, Havelock, NC File ID DF Analyzed By Prop Date Prep Batch Analytical Batch Run #1 X064918.1) 1 01/Z8/19 17:22 MV 01/26/19 09:30 OP73560 SX2675 Run #2 Initial Volume Final Volume Run #1 100 ml 1.0 ml Run #2 ABN TCLP List TCLP Leachato method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 95-48-7 2-Methylphenal ND D023 200 0.050 0.0056 mglf 3&4-Methylphenal ND D024 200 0.050 0.0098 mg/1 87.86.5 Pentachlorophenol ND D037 100 0.25 0.050 mg/1 95-95-4 2,45-Trichlorophenoi NI) D041 400 0.050 0.0074 mg/I 8846-2 2,9,6-Trichlorophenoi IVD D042 2.0 0,050 0.0075 mg/I 106-46-7 1,9-Dichlorabenzene ND D027 7.5 0.050 0.0050 mg/I 121-14-2 2,4-Dinitrotoluene ND _D030 0.13 0,050 0.0081 mg/l I18-74-1 Hexachlorobenzene ND D032 0.13 0.050 0.0069 mg/I 87-68-3 Hexachlorobutadiene ND D033 0.50 0.050 0.0050 mg/I 67-72.1 Hexacliloroethane ND D034 3.0 0.050 0.016 mg/1 98-95-3 Nitrobenzene Np s; D036 2.0 0.050 0.0093 mg/I 110.86-1 Pyridine ND D038 5.0 0.10 0.020 mg/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 41% 14-67% 4165-62-2 Phenol-d5 4U% 10-50% 118-79-6 2,4,6-Tribromophenol 33-118% 4165-60-0 Nitrobenzene-d5 7U°h 42-106% 321-60-8 Z-Fluorobiphenyl 6i3% 90-106°6 1718-51-0 Terphenyl-d14 7lp/o 39-121%' ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 2617/1111) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound EM 8 of 14 FAU°95.1 SGS North America Inc. Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA60954-1L Date Sampled: 01/14/19 x Matrix: AQ - Water Date Received: O1119/19 Method: SW846 8151A SW846 3510C Percent Solids: 1.2 Project: City of Havelock W WTP; 304 N Jackson Dr, Havelock, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC060886.D 1 01/28/19 18:12 RS 01/26/19 11:45 OP73562 GCC1403 Rut #2 Initial Volume Final Volume IRun #1 10.0 ml 5.0 Run #2 Herbicide TCLP Leachate CAS No. Compound 94-75-7 2,4-D 93-72-1 2,4,5-TP (SRvex) CAS No. Surrogate Recoveries I9719-28-9 2,4-DCAA ml Report of Analysis Result HW# MCL RL ND I . .'fi0016 10 0.050 ND D017 Run# 1 Run# 2 Limits 39-135% TCLP Leachate method SW846 1311 MDL Units Q 0,017 mg/1 0.0013 ntg/I ND = Not detected MDL = Method Defection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CPR 201 7/1/11) . B = Indicates analyle found in associated method blank E = Indicates value exceeds calibration range N = Indicates Presumptive evidence of a compound SG9 o114 FAGO964 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA60954-1L Date Sampled: 01/14/19 Matrix: AQ - Water Date Received: 01/19/19 Method: SW846 8081B SW846 3510C Percent Solids: 1.2 Project: City of Havelock W WTP; 304 N Jackson Dr, Havelock, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #I KK92795.D 1 01/29/19 01:46 WH O1/26/19 08:00 OP73561 GKK2949 6Run #2 Initial Volume Final Volume Zoo #1 100 ml 5.0 ml Zoo #2 Pesticide TCLP Leachate CAS No. Compound 58-89-9 gamma-BHC (Lindane) a 12789-03-6 Chlordane 72-20-8 Endrin a 76-44-8 Heplachlor a I024-57-3 heptachlor epoxide a 72-43-5 Methoxychlor 8001-35-2 Toxaphene CAS No. Surrogate Recoveries 877-09-8 Tetrachloro-m-xylene 2051-24-3 Decachlorobiphenyl TCLP Leachate method S W 846 1311 Result HW# MCL RL ..... ............. ND... _ ``: D013 0.40 0.00010 ND D020 0.030 0.0010 ND " D012 0.020 0.00020 ND._ D031 0100800.00010 ND ;:' D031 0,0080 0.00010 ND D014 10 0.00020 ND': .. D015 0.50 0.0050 Run# I Run# 2 Limits 99% 42-127% 27-127% (a) Associated CCV outside of control limits high, sample was ND. MDL Units Q 0.000022 mg/I 0.00038 mg/I 0.000021 mg/I 0.000026 mg/I 0.000020 mg/1 0.000050 mg/I 0.0021 mg/I ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 14 FAGO954 SGS North America Inc. Report of Analysis Client Sample ID; SLUDGE SAMPLE Lab Sample ID: FA60954-IL Date Sampled: 01/14/19 Matrix: AQ - Water Date Received: 01/19/19 Percent Solids: 1.2 Project: City of Havelock W WTP; 309 N Jackson Dr, havelock, NC Metals Analysis, TCLPLeachate SW8461311 Page 1 of t Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic <;p.10 ;+, D004 5.0 0.10 mg/1 1 01/28/19 01/28/19 LM SW846 60I0D 2 SW846 3010A 4 Barium <2 :0 D005 100 2.0 mg/1 1 01/28/19 01/28/19 LM SW846 6010D 3 SW846 3010A 4 Cadmium 2;0i050 ';.'' D906 1.0 0.050 mg/l 1 01/28/19 01/98/19 LM SW846 G610D 2 SW84G 3010A 1 Chromium D007 5.0 0.10 mg/l 1 01/28/19 01/28/19 LM SW846 6010D 2 SW840 3010A 4 Lead S 0 05.Vi :. D008 5.0 0.050 mg/l 1 01/28/19 01/28/19 LM SW846 6010D 2 SWE46 3010A 4 Mercury <0 0050 D009 0.20 0.0050 mg/l 1 01/25/19 01/25/19 1c SW846 7476A 1 SW046 7470A 3 Selenium <;010,`:.`:;i.y°DOW 1.0 0.10 mg/l 1 01/28/19 01/28/19 LM SW8466010D2 SW846 3010A4 Silver <' TV.;i'.:i' DOI l 5.0 0.10 mg/I 1 01/28/19 01/28/19 LM SWB46 Ga1OD 2 SW940 3010A 4 (1) Instrument QC Batch: MA15564 (2) Instrument QC Batch: MA15567 (3) Prep QC Batch: MP34974 (4) Prep QC Batch: MP34981 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) _ 11 of FAGOM Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody 14 _ S..12 of . FA50954 C A c 3 1 0 Grrvhnumenll,lne. CHAIN OFCT7STODYRECORD F jSq 1 s P.O. Box 7085.114 Oakmont Or. }�' ,�L7 Peee _.af_ rM. IISNC77&58 --'-- — - CLIENT.. 414 Mk. 6 �■MWMP ®mWULM UMI , www 5�/MiM i low. PLEASE BEM Instrucllons for complepnp Ibis form on the Inverse slde.l ...... "'�"°°°""""`"^"°'""'"""'°°""" N: H41" Fonu is Grub sample in 0e blocks above for each pammuler requested, FA60954: Chain of Custody Page 1 of 2 73 of 10. �� Faeobsa SGS Sample Receipt Summary Job Number: FA60954 Client: ENV. 1 Project: 414 Date ITlme Received: 1119/201910:00:OOAM Delivery Method: F% AIrblll#'s: 11101893382710003201100481211580901 Therm ID; IR 1; Thertn CF: -0.2; N of Coolers: 1 Cooler Temps (Raw Measured) °C: Cooler 1: (2.6); Cooler Temps (Corrected) IC: Gaoler 1: (2.4); 1. Custody Seals Present to ❑ 2. Custody Seals lnlect ® ❑ 3. Tomp called. achlawd ® ❑ 4. Cooler temp vadncalian IR Gun 5. Cooler media Ice regal Trip Blank Information 1. Trip Blank present/cooler 2. Trip Blank listed on COC 3. Type Of TB Received Y or N N/A ❑ ❑ ❑ ❑ W or 5 NIA ❑ ❑ 21 Sample Information 1. Sample labels present on bellies 2. Samples preserved properly 3. Sufficient volumerwnlelners raced for analysis: 4. Condienn of sample S. Sample recvd vAthln HT S. Datesfrimesfi0s on COC match Sample Label T. VOCs have headspace S. Bolllen received forumpecli ed testa 9. Compoallin9 Instructions dear 10. Von Soil WhIJare recolvad past 411hrs9 I i. % Sonds Jarracelved? 12. Residual Chlorine Present? I ? Y or N NIA El © ❑ Inlael ® ❑ ❑ 10 ❑ ❑ ❑ ❑ 21 ❑ ❑ Misc. Information Numberaf Enwres: 25-Gmm_ a -Gram Numberaf5035 Field Kits:_ Number of Lab Filtered Metals:_ Test Slip Lot Its: pH 0-3 230315 pH 10-12 219513A Other. (Specify) Residual Chlorine Test Ship Lot 0: Comments Technician: PETERH DOW 1/19201910:00:00A RaNawer: ow.] 0. 0lrs11fr Date: FA6O954: Chain of Custody Page 2 of 2 14 of 14 FAf0964 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Havelock WQ Permit Number: W00000702 WWTP Name: City of Havelock W WTP NPDES Number: NCO021253 Monitoring Period: From 1/1/2019 To 3/31/2019 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alterative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 El Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑I Air Drying ❑ Com ostius p � ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number o Excee- Frequency q i of Analysis Sample p Type na ica Tech- Minimu Geo. Mean Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry wei ht 11,218 25,461 50,794 MPN/g 0 Quarterly Grab SM9221E ella bacteria eu of fecal rliform) 3 MPNper 4 grams total solid (dry weight) . ccurr riuracuon rceuucaan k4u Cris 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ JAIL 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAIL 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) El jAlt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jams Carter, ORC Vaughn Stevenson, Land Application Manager Preparer Name nd Ti (type or print) Land /Applier Name and Title (if applicable)(type or print) G 3� oaf l/ a-Zy� � Signature of pa * � Signature of Land Applier (if applicable) Date *Preparer' d fine in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) CITY OF HAVELOCK WQ0000702 City of Havelock WWTP Date Fecal Coliform MPN per grain Log O1/14/19 17,308 4.2382 O1/14/19 17,035 4.2313 O1/14/19 49,080 4.6909 O1/14/19 16,770 4.2245 01/14/19 50,157 4.7003 O1/14/19 50,794 4.7058 O1/14/19 11,218 4.0499 Total 30.8411 Average 4.4059 Geometric Mean 25,461 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction requirement. I 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF HAVELOCK(SLUDGE) MR. RODNEY GEORGE WASTEWATER TREATMENT PLANT 304 N. TACKSON DRIVE HAVELOCK ,NC 28532 Drinking Water ID, 37735 Waatewatar ID, 10 PHONE (252) 756-6208 FA:: (252) 756.0633 ID#: 414 B DATE COLLECTED: 01/14/19 DATE REPORTED ; 01/18/19 REVIEWED BY: 4- Sample Sample Sample Sample Sample Analysis Method PARAMETERS #1 #2 #3 #4 #5 Date Analyst Cade Total Residue, mg/I 31240 31680 32600 32220 31900 01/15/19 JTH 2540B-11 Fecal Coliform WN), /gram Solids 17308 17035 49080 16770 50157 01/15/19 JTH 9221E-06 MAQm EM % hcwpo 0TM!'N 601 '114 OAKNIONT DRIVE GI?EENVILLE, N,C. 27858 CITY OF HAVELOCK(SLUDGE) MR. RODNEY GEORGE WASTEWATER TREATMENT PLANT 304 N. JACKSON DRIVE HAVELOCK ,NC 28532 Drinking Water IDi 37715 Waetawater Ioo 10 PHONE (252) 756-6206 FAX (252) 756-0633 ID#: 414 B DATE COLLECTED: 01/14/19 DATE REPORTED : 01/18/19 REVIEWED BY: Sample Sample Analysis Method PARAMGTCRS #6 #7 Date Analyst Code Total Residue, mg/1 31500 31240 01/15/19 JTH 2540B-11 Fecal Coliform (MPN), /grain Solids 50794 11218 01/15/19 JTH 9221E-06 0 O u•�� > _ Q � Z U 1�JIII r UU 1- <n w O Z z W W Ld w Q uq� a r a U w o. m ca w W EE x sls3usH313waavd 2 fn w +d8 W W W o m P. ¢' WBS 9/O3 k Q z SH3NIVWOOHOfI N N N N N N N u y m N0110311001V '— �^• a' N` > 0 0o'3H01VH3dW31 r'^ ^^ `�' 8 u ] z " � > w > ED Ea w E N0110311Op 1V Ilion yp \ \ q 1/6w'3�11HOlHO lV101 ¢ ¢ E w �n !p rJ n7 1�1 T .}` N T y W � ° m y U WO (VVNIJj� c7 c� c� Q W Q N qtr Q In VJ Oz a m m m y ` U V o W Ow 0 ., w J v a u a a a a d a O O a 21z e a _ zi vNi i cn I vl j m m W ¢ = ¢ a ¢ 0 z Y N ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Havelock WQ Permit Number: WQ0000702 W WTP Name: City of Havelock W WTP NPDES Number: NCO021253 Monitoring Period: From 4/1/2019 To 6/30/2019 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative nerfarmed- Class A: Alternative 1 ❑ Alternative 2 ❑ - . ---------- Altemative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray 01 Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 El Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying[] Compostin ❑ Aerobic Digestion O Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- Frequency �of`Analysis Sample Type na ica Tech - Minimu Geo. Mean Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry wei ht 2,687 5,882 52,288 MPN/g 0 Quarterly Grab SM 9221 CE Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) v Cctur arrraCH011 I-CUUCIIOn t4U C.UK nu'.SS) - Please indicate OW1011 Derformed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) [IAlt. 3 (30-day bench) El Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ I Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable). ❑ Alt. 9 (Injection) El Alt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." James Carter, ORC Vaughn Stevenson, Land Application Manager Preparer Na and Tit (type or print) Lannd7 A�pplier Name and Title (if applicable)(type or print) o dy 4Da � Signature f repa n to Signature of Land Applier (if applicable) *Preparedefined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) nrMD C(1DKA DXIDC cnc noronna� CITY OF HAVELOCK WQ0000702 City of Havelock W WTP Date Fecal Coliform MPN per'gram Log 04/15/19 2,687 3.4293 04/15/19 52,288 4.7184 04/15/19 3,846 3.5850 04/15/19 11,706 4.0684 04/15/19 1,591 3.2017 04/15/19 8,136 3.9104 04/15/19 2,974 3.4733 Total 26.3865 Average 3.7695 Geometric Mean 5,882 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. o�or��c��� Flo D��oQpo�a�c�c] 114 OAKMONT pRIVE GREENVILLE, qI.C.27858 CI Y OF HAVELOCK(SLUDGE) MR. RODNEY GEORGE WA TEWATER TREATMENT PLANT 30 N. JACKSON DRIVE HA, LOCK ,NC 28532 Total Residue, Fecal Colitorm Sample RAMETERS #1 mg/I 29360 (MEPN), /gram Solids 2687 Drinking Water ID, 37715 Weetemater ID, le PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 414 B DATE COLLECTED: 04/15/19 DATE REPORTED : 04/18/19 REVIEWED BY: Sample ample Sample Sample Analysis Method N2 N3 N4 k5 Date Analyst Code 30620 28600 29940 30800 04/16/19 KDS 254OB-11 52288 3846 11706 1591 04/16/19 KDS 9221&06 EflWUh*@fl1 �, WupwaW 114 0AKMONT ORRIVE GREENVILLE, G.27858 CI- OF RAVELOCK(SLUDGE) MR RODNEY GEORGE WASTEWATER TREATMENT PLANT 304 N. JACKSON DRIVE EWrELOCK ,NC 28532 Sample Sample #6 #7 Total Residue, g/l 29460 30100 Fecal Coliform N), /gram Solids 8136 2974 Dsiakiaa water IDt 17715 wastewater IDI 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 414 B DATE COLLECTED: 04/15/19 DATE REPORTED : 04/18/19 REVIEWED BY: Method Analyst Code KDS 254OB-11 KDS 9221E.06 \ \ a � § ) OD \ % ( LL , ) k } & » / / °�2§k Eoa»� u l=aE; u 0 - ) anp!saH m! p A +_NO3 z, § - ) 4 \i/cam d04 "/\§\ \ 0w NJ NJ .I , � / / \ �\ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Havelock WQ Permit Number: W00000702 WWTPName: City of Havelock WWTP NPDESNumber• NCO021253 Monitoring Period: From 7/1/2019 To 9/30/2019 . Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ " '' Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate 'Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 El Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Dryin ❑ Composting ❑ lAerobic Digestion 0 Anaerobic Digestion ❑ _.._ If applicable to alternative performed (Class A or Class B) complete the following monitoring data Parameter Allowable Level in Sludge g Pathogen Density Number o Excee- Frequency of Anal Analysis Sample Type na yttca Tech- Minimu Geo. Mean Maximu Units Fecal Coliform 2x10tothe 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) 968 2,030 3,790 MPN/g 0 Quarterly Grab SM 9221 CE Salmonella bacteria (in lieu of fecal coIiform 3 MPN per 4 grams total solid (dry weight) . ocur. auracuvu 1<eeuucnou 1,40 Crir, 30.5.33) - Please indicate option performed: Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ 1 Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ ITIt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) El jAlt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jagies Carter, OR C Vaughn Stevenson, Land Application Manager Preparer Nam and Ti e (type or print) Land/ A�pplier Name and Title (if applicable)(type or print) 240 Signature o P epa ate Signature of Land Applier (if applicable) Date *Preparer I" fine in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) CITY OF HAVELOCK WQ0000702 City of Havelock W WTP Mate;€ ..,...., .T. ....... ... riXJri et.. ram ......:....:..:...:.:.:.:.:.:.:.:.::::: og 07/15/19 1,508 3.1784 07/15/19 2,324 3.3662 07/15/19 1,503 3.1770 07/15/19 2,438 3.3870 07/15/19 968 2.9859 07/IS/19 3,790 3.5786 07/15/19 3,012 3.4789 Total 23.1520 Average 3.3074 Geometric Mean'Sl311`€€ Fecal Coliform MPN / ' .,. gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Nmwkoumm Flo 27858 CITY OF HAVELOCK(SLUDGE) MR. RODNEY GEORGE WASTEWATER TREATMENT PLANT 304 N. .JACKSON DRIVE HAVELOCK ,NC 28532 ' Sample PARAMETERS Nl Total Residue, mg/1 32540 Fecal Coliform (MPH /gram Solids 1508 Sample #2 34020 2324 Sample #3 32580 1503 Prl.king W.t.. My, 37715 FAX (252) 756-0.633 ID#: 414 B DATE COLLECTED: 07/15/19 DATE REPORTED : 07/17/19 REVIEWED BY: Sample Sample Analysis Method N4 #5 Date Analyst Cade 32360 34060 07/16/19 ICDS 2540D-11 2438 968 07/16/19 ICDS 9221E-06 EIMUnIOUM V % kwwl1 Mi Dsinkln9 Water ID1 I7715- utstvt PHONE (252) 756-6208 N.C. 27858 FAX (252) 756-06S3 ID#: 414 E CITY OF HAVELOCK (SLUDGE) MR. RODNEY GEORGE WASTEWATER TREATMENT PLANT DATE COLLECTED: 07/15/19 304- N. JACKSON DRIVE DATE REPORTED ; 07/17/19 HAVELOCK ,NC 28532 REVIEWED BY: Sample Sample Analysis Method PARAMETERS N6 #7 Date Analyst Code Total Residue, mg/l 34280 34660 OV16/19 ICDS 254OB-11. Petal. Coliform (MPH [gram Solids 3790 3012 07/16/19 KDS 9221E 06 0 o w y Z q= U Z S N Z O N O m F- ¢ v5F p o qq� w Z ¢ w W ¢ z O a Z 4 ¢ z :3 U 09 U tb z j�s� 0r.'Jv 171 DS V U n U S1S3llSH313WtlHUd ¢ n N Q anppH lelot ` rye ZO 7 Sf 3N[VINOD jp# N N N N N N N ^ fRG (d (7 [9 TT NOlO3l1OJltl > Oz Oe'3HfUVU3dW31 cy NOW O3 I/6a tlO W � \ A 0 � 173 3N[UOIHOIHOlNO lV1O1sq . b N cr ` w � � d a o�04 4 � .4-1 O z ¢ m m M w >0 °aJz a a V 0 OI Z ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Havelock WQ Permit Number: W00000702 W WTP Name: City of Havelock W WTP NPDES Number: NCO021253 Monitoring Period: From 10/1/2019 To 12/31/2019 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative nerfarmed- Class A: Alternative 1 ❑ Alterative 2 ❑ .----------- Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ I Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ I Gamma Ray ❑ L Pasteurization ❑ Class B: Alternative 1 O Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ I Air Drying[] Composting ❑ JAerobic Di estion C] Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data Parameter Allowable Level in Sludge Pathogen Density Number o Excee- Frequency 9 i Sample p Analytical Tech- ninnp Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) 59,533 188,929 399,002 MPN/g 0 Quarterly Grab SM 9221 CE Salmonella bacteria (in lieu of fecal coliforr I 3 MPN per 4 grams total solid (dry weight) vecwr attraction rteauctron (40 I.:FK JUS.33) -Please Indicate ontion performed- Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ JAIL 3 (30-day bench) ❑ Alt. 4 (Spec. 0, uptake) El Alt. 5 (14-Day Aerobic) ❑ I Alt. 6 (Alk. Stabilization ❑ jAlt 7 (Drying - Stable) ❑ jAlt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) El jAlt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ UER'1'WICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." James Cajiter, ORC Vaughn Stevenson, Land Application Manager Preparer N*definedin pe or print) Land Ap ier Name and Title (if applicable)(type or print) v aOoze) Signature ate Signatur of Land Applier (if applicable) Date *PreparerR Part 503.9(r) and 15A NCAC 2T .1102 (26) CITY OF HAVELOCK W00000702 City of Havelock W WTP 10/08/19 222,222 5.3468 10/08/19 134,328 5.1282 10/08/19 367,816 5.5656 10/08/19 59,553 4.7749 10/08/19 87,065 4.9398 10/08/19 378,251 5.5778 10/08/19 1 399,002 5.6010 Total 36.9341 Average 5.2763 Geometric Mean 18$49'_€ Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Environment 1, Inco GREENVILLE, N.C. 27858 MOO CITY OF HAVELOCK(SLUDGE) MR. RODNEY GEORGE WASTEWATER TREATMENT PLANT 304 N. JACKSON DRIVE HAVELOCK ,NC 28532 FAX ID#: 414 B DATE COLLECTED: 10/08/19 DATE REPORTED : 10/11/19 REVIEWED BY: Sample Sample Sample Sample Sample Analysis Method PARAMETERS #1 #2 #3 N4 #5 Date Analyst Code. Total Residue, mg1l 41433 40167 43467 40300 40233 10/08/19 JMS 2540B-11 Cecal Coliform (AlMP , /gram Solids 222222 134328 367816 59553 87065 10/08119 JMS 9221E-06 Environment 1, 114'.UAKMUN'1 DRIVE GREENVILLE, N.C. 27858 CITY OF HAVELOCK(SLUDGE) MR. RODNEY GEORGE WASTEWATER TREATMENT PLANT 304 N. JACKSON DRIVE HAVELOCK NC 28532 Sample PARAMETERS N6 Total Residue, mg/I 42267 Fecal Coliform (MPN), /gram Solids 378251 FAX (252) 756-0633 ID#: 414 B DATE COLLECTED: 10/06/19 DATE REPORTED : 10/11/19 REVIEWED BY: Sample Analysis Method N7 Date Analyst Code 40067 10/08/19 JMS 2540E-11 399002 10/08/19 JMS 9221E-06 9 Q o. a w d� � 0 F o 2 � w So J 0 Z Z ~ z 2Wa ¢ ¢� W~ (\ (0 C7 a ¢ ? = N Z o w LL co F ¢ F < V y Z h w m V cil w a V a m ti DG o¢ V = S.L53LS4f313Wtlkltld 8 w ' w w a o a Pk .4 allplsag jejoy a '=�,a; ' SH3NIV1NOOdOk N NON::// N N N N o D L9 S2 ?a o Nomonooltl 0-'3dIlltlN3dW31 c+i !„j (� z A [71 [7 NOLLo3-noo ltl 1/6n tjo IlBw'3NIdOlH0lV101 Q ¢ w � g Q w w fi N a 8 3 aws Q o a O D O :l t2 EO `l0, z O in m N g 6 0 �a �g w � 3 'Mti4 l��t gm dp d a pu � 8 E' i 2019 APPLICATION SUMMARY CITY OF HAVELOCK Permit #WQ0000702 2019 SUMMARY SITE NO. FIELD NO. SOURCE LAND APPLIED APPL. DATE ACRES USED TOTAL GALLONS TOTAL DRY TONS TOTALPAN Crop t Crop 2 NC-PA-2 6A Havelock Mar-19 5.21 66,000 9.61 58.77 NC-PA-2 6B Mar-19 6.48 84,000 12.22 60.14 NC-PA-2 6C Mar-19 6.16 78,000 11.35 58.74 NC-PA-2 6D Mar-19 6.26 84,000 12.22 62.25 NC-PA-2 6E Mar-19 3.90 30,000 4.37 35.68 Apr-19 1 18,000 2.62 21.41 NC-PA-2 6F Apr-19 3.59 48,000 6.99 62.03 NC-PA-2 Sep-19 12,000 2.20 21.33 NC-PA-2 6G Apr-19 3 84 30,000 4.37 36.24 NC-PA-2 Sep-19 48,000 8.79 79.78 NC-PA-2 7A Sep-19 2.18 30,000 5.49 87.83 NC-PA-2 7B Sep-19 2.57 30,000 5.49 74.50 NC-PA-2 7C Sep-19 3.32 42,000 7.69 80.74 NC-PA-2 7D Sep-19 3.32 42,000 7.69 80.74 NC-PA-2 7E Sep-19 3.26 42,000 7.69 82.23 NC-PA-2 7F Sep-19 3.03 42,000 7.69 88.47 NC-PA-2 7G Sep-19 3.53 48,000 8.79 86.79 NC-PA-2 7H Sep-19 3.28 42,000 7.69 81.73 NC-PA-2 71 Sep-19 3.25 42,000 7.69 82.48 NC-PA-2 W Sep-19 3.25 42,000 7.69 82.48 NC-PA-2 7K Sep-19 2.47 30,000 5.49 77.52 TOTALS 68.90 930,000 153.81 Dry Metric Tons 139.51 FIELD LOADING RATE REPORTS N vi a F t G y H G 6 E u Q o o E m z ce u " a Q d O O y o 0 0 0 0 0 0 0 0 0 0 0 X. M tl E Z Z E v w Ammonia Nitrogen c rn o F" E a M W on O o O 0 O 0 0 Mineralization o e e Rate*** c W z o s c o 0 A Volatilization Rate** c o 0 0 w Application Method* 0 0 0 O O O p 0 .W- V 0 r i 6 a a U o Q u d 9 W R$ U o o 0 c 0. o V d n E > 6 Q O' Ci � OO G OO OO 0 0 0 O OO C C C L Q 0 09 v e a h m u R A 4 U C o a v P4 .1. v c v N > y 0 0 U >v Uroz tl C Q gIUOYtI a 7 L y C' JO 012(j p o m v F a.Ua.a n f' M ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Permit #: WQ0000702 Total Dry Tons Applied (Annual): 9.61 Cation Exchange Capacity (non 503 only): 10.0 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Acres Used: 5.21 Acres Permitted: 5.21 Site #: NC-PA-2 Field #: Stockade 6A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): 111t t 111 1 1 1111 I I11 t 11t 1 Itl 1 Ilt I I11 1 Itl 1111 1111 1 1 •'® 1 111 1 111 1 11� 1 111 1 111 1 111 1 111 1 I11 ET, 11 1 111 1 111 1 111 1 11� ...- 1 111 1 111 1 1. 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1. '® 1 111 1 111 '® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 '® ®'' 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 11 I t 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 �� 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 1 : 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® 1 111 1 111 .. 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • . 1111 1111 ".1. 1111 1111 1111 1111 1111 1111 1111 1111 1111 "�1� '. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) 00 V M G Y U •p N '� N O FT G G � o U P d o o m z a U U a Ll v N o. O O 0 0 0 0 0 0 0 0 0 O E!o o z o 0 R 0 0 U o o c o 0 o c o 0 0 0 0 Q m 0 0 0 0 0 U G G� C O O O G C C O O � :' ' •••� `� E E Z ,^Z er w° $ Ammonia q a n v Nitrogen E e E N 00 c c rn o .o 2 M M !w/J fj o 0 0 E v G*w o c o a Mineralization M O Rate*"* o �Zoo� r o 0 0 W 2; Volatilization o N a e Rate** c o 0 0 m W Application 2. o o c o c Oc Method* x o o C U v a p, F b N U v 3 •� U N vMi ri �C ,' 0 3 a a V o 0 0 0 0 ai u E pa F O O ap 0 0 0 0 0 0 0 0 0 0 0 0 > Q O e a y O V � N o O u '� O O m N y •O a ti m w �^' CDis i .0i N vf�, > V ; U Ei i U p b z U gluow to aleQ M e< e ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tons Applied (Annual): 12.22 Permit #: Operator: Acres Used: WO0000702 Cation Exchange Capacity (non 503 only): Michael Spencer Owner: Spencer Farms, Inc. 6.48 Acres Permitted: 6.48 Site #: Predominant Soil Series: NC-PA-2 Field #: 10.3 Stockade 6B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . 0 © Annual Heavy eta ie oa ings ( alculated in lbs/acre): 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 •'® 1 111 1 111 1 11� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11� ,..- 1 111 1 111 1 1.� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1,� '® 1 111 1 111 '® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ®'' 1 111 1 111 1 1 • 1 111 1 111 1 111 EM 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 � 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1111 1 1� 1 111 1 111 1 1 ' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ' ® 1 111 1 111 . 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1111 1� 1�� 1111 1 111 1111 1111 1 111 1 I11 1 111 1 111 1111 1� 1�• •. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1 2_ 11-2-P Date DENR FORM MFLSF (12/2006) U e 7 W a L O U U 9 N [y = G W N O a � U m w c `o . E z� u U aq •o a 0 o Q o 0 0 0 0 0 0 0 0 0 :�: z 0 0 0 0 0 0 0 0 O .. . U 0 0 O O O O O O O O O G I U v y rn ^ R z 2 E w Ammonia N Nitrogen E lO c z rn o a Mineralization M O o Rate*** c W r Z o c o o .-: 0 R Volatilization o N N Vl Rate** a o 0 0 i; c. Application w o 0 0 Method* C O O 0 o a o 0 vv A o d d a o _ '�3'0 ❑ U o U ,�' 7'. N Ili e R ear.. =off 0-ig 3 E a U ri 2 0 o 0 0 VJ Q aON+ j gov3 x 9 d•ag�� [s. a V o o 0 c 0 o 0 v a O O O O O O O O CD O O U O •Md• y^ N IM+I Q � o � � e `T N M U y oo p U a y m Qi R y p �tl > a vea ��ay o r m U a y U U I]::::: p �U ll;uoNl p�¢ so a3eQ ° i U a a a` I N ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: of Havelock W00000702 Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Michael Spencer Owner: Spencer Farms, Inc. 6.16 Acres Permitted: 6.16 Site #: Predominant Soil Series: NC-PA-2 Field #: 11.35 9.9 Stockade 6C Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . . 0 © Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): one MEN00001010 • ,. 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 11� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11� ...- 1 111 1 111 1 1. 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1, '® 1 111 1 111 .1' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 .1' ®'' 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 �� � 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® 1 111 1 111 .. � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) E. N U UrZ a ' U v z U Cd q a rZ o 0 0 .' a � U o 0 0 6 0 0 6 0 6 0 6 0 6 0 6 6 c c :� R ,Z O O Oo C3 0 0 0 0 0 ~ U o � 6 0 0 6 6 c o u o rn b g ^ ': 2 Z E er E .� :....:.����:�:� m Ammonia M O b b Nitrogen E i N� p N o N � a rn Cl o M O M N ru E rw/J C/J O O O Mineralization M 0 Rate*** z .R. Volatilization o N M h Rate** c o o 0 0 o q w CS Application w o 0 0 Method* c c o O x v o ly o a y F v o 0 0 _C " ° ❑ e o ri �3'l0� .W U r, lV e? V n ,G C6 ICY 0 b❑ d3 d 71 x U o o 0 0 0 0 v a c O O O O O O O O O O O N N 2 g 0 0 vMt Ot O O O O O O O O O y ¢ 0 0 tq�l 0 O Q Q � 9 o � O m M p * o V .o .o c c $ a N N n a v U> m N h u U Z 0 U o Q IL TUOW ao alucl °¢aUaa ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tons Applied (Annual): 12.22 Permit #: WQ0000702 Cation Exchange Capacity (non 503 only): 8.2 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Yonges Acres Used: 6.26 Acres Permitted: 6.26 Site #: NC-PA-2 Field #: 6D Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 •'® 1 111 1 111 1 11� 1 111 1 111 1 111 1 111 MIT, 11 1 111 1 111 1 111 1 111 1 11� ...- 1 111 1 111 1 1,. 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1„ '® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ®'' 1 111 1 111 1 1: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1: 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 ' 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 ® 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ®I '. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier DENR FORM MFLSF (12/2006) nle�i ImIN Q u s E a N !] a v o Q a m U p U w c a d r zU a O U O U O R o 0 0 0 0 0 0 0 0 TITz 0 0 o c c o 0 0 0; d _ e ............. a U O O M N G C O O O C G G � W z Z E v w Ammonia Nitrogen E �o `O 8 N m ri o0 C o O Mineralization 0 Rate*** o c W o o rz000 z Volatilization Rate** o 0 0 a W Application 0 0 Method* 0 _ V V W s U In d N V o o N aQ v$ x 5 i0oe 0 0 0 0 0 0 0 ¢ 0 0 a 6 b j o o .: o 0 6 6 c o 6 0 6 0 0 6 0 Is6 0 0 Q o � y ] * FL O U v a O O t6 O O] .0 >v d 7U.a a r a ° u3uoLV N _ io aleQ ¢ o 'C d F d a U a w u R y � Q W O = y U a Z = m R u u 0 0 C R a+ G O C u U a C M1I _ u s. R T7 y U o o y y R •a O G m u 3a ° • d Y q ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tons Applied (Annual): 6.99 Permit #: WQ0000702 Cation Exchange Capacity (non 503 only): 8.7 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Yonges Acres Used: 3.9 Acres Permitted: 3.9 Site #: NC-PA-2 Field #: 6E Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in lbs/acre): • 1. 1 111 1 111 1 11 1 11� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 .'® 1 111 1 111 1 11 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11� ...- 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1. '® 1 111 1 111 � 1 ` 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ®' ®'' 1 111 1 111 1 1` 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 11 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 �� 1 111 1 111 1 1 1 11: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • 1 111 1 111 1 1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 1 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 . `�: 1 111 1 111 ®® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 '. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment knowing violations". v Signature of Land Applier Date DENR FORM MFLSF (12/2006) 'O 9 z b ai N a U 7 iE 9 « W � r. u Y w 3 m N y UCL a a U m 2 y a N 3 v o U z a a o 0 0 0 0 0 0 o Q o 0 o N a a o 0 0 0 0 0 0 z 0 0 0 0 .. 0 0 0 0 6 0 0 o o 0 0 :. u s0• � b e .b rn a •' �y b a •; :.:.;".;"':'';':` .:.:.:.:.:...: :.:.: Ammonia Nitrogen E N �•' N T N ^ c N c p O ^ yrAO 0 0 0 E" E a Mineralization Rate*** 0 o W s z o 0o c o A Volatilization _ v torte** G o o 0 0 0 0 = W Application a U w o 0 0 Method* ' �" o o o U v v O a O N y O O O s ti U q A A c v X. 3 U Iii. cba. R y h °o�N U 6 0 0 •'- Q m 3 x x `J v o ` cCR w aUo R o z� e o a ei v p a O O O O T O O O O b 0 0 0 Q' 0 0 0 F Q � e v a a rn n X.0 y y U 0 U y 9 9 C O O $ O u O •CL iF Q Ul t i6 V Y iF N ; Ki ^ 0.. E y }� U j C d 0. Tuow rn rn zo a;zQ ¢ N o �2 U H P. P. a N Q a ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Permit #: WQ0000702 Total Dry Tons Applied (Annual): 9.18 Cation Exchange Capacity (non 503 only): 7.8 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Yonges Acres Used: 3.59 Acres Permitted: 3.59 Site #: NC-PA-2 Field #: 6F Residual Analysis Data (Heavy Metals and Total Phosphorus use me/ke, % Solids use Raw Percent #): • Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 00000100001108 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 11� 1 111 1 111 1 111 1 1 • •'® 1 tll 1111 1 111 1 11� 1 111 1111 1111 1 111 111 1111 1111 1111 1 11• ••.- 1 111 1111 1 111 1 1•. 1 111 1111 1 111 1 111 11 1111 1111 1111 1 1� '® 1111 1111 1111 ® 1111 1111 1111 1111 1 :� 1111 1111 1111 �1 ®'' 1 111 1 111 t 111 1 1: 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1•• 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 •• 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 • 1 111 1 111 1 111 1 111 1 11 • 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 11 1 111 1 111 1 111 1 111 1. 1 111 1 111 1 111 ' 1. 1 1 1 1 1 1 1 1 1 11 1® 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 �� 1 1 11 1 1 1 1 1 1 1 1 1 �.. • •• "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". --�/+ zy Z0 Signature of Land Applier Date DENR FORM MFLSF (12/2006) U b W v a N tL ZZ La L V rA N — N p � \ o v o o n U U C fl 0=a z� u 3 z o, 2' � tj o 0 0 o 0 0 o o 0 0 `o M . Q � L a 0 0 0 o z rj o 0 o c o 0 0 o 0 0 `. R O Lt. N ' ........... Ammonia s ,M„ ❑ N Nitrogen E G G O k O O O N 0 0 0 Em Mineralization "' Rate*** z' o o — .c o 0 0 R Volatilization V o V M m Rate** c o 0 0 L- Application U w o 0 0 Method* x c c c O � U s m U O v 'o q q c h M O M Y G Cj � E 0 3 E V VJ yt' O O h is o 0 0 Q o Z S 04 G U o o 0 0 0 V u a Q > a Q O G C O O O G hl G O O O G O Q � o rn a. ti M v U R � o � E >v N�'a U U z m c Q 41uoW E d ao aIs4 ¢ o QcuCL •2 G y R y L N y w R � i a �W m ayi y a L w � v T y y R R y iG y •; G u O G R � a. L y O y V L• R R C L o •- y •� R i o y G � tL0 y 3 R L O R C c � O �'y R a, •E c a O � = o •p � w L E a R L y d w E L C C R r L a 3 a S w � G � R R p w i a a c E=� Y R O a � R W Ys y R � O � G w L L O y yam, a y c G o a�a a y v � R � w E u m o 7 c o I m ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tons Applied (Annual): 13.15 Permit #: WQ0000702 Cation Exchange Capacity (non 503 only): 8.9 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Argent Acres Used: 3.84 Acres Permitted: 3.84 Site #: NC-PA-2 Field #: 6G Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in lbs/acre): - 1 • 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 1• 1 111 1 111 1 111 1 1 .'® 1 111 1 111 1 111 1 11 WIT, 11 1 111 1 111 1 111 1 11. 1 111 1 111 1 111 1 11` 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1•• �� ������ 171'iiiiiWi' 1 111 1 111 1 111 1all 111 1 111 1 111 1 111 '® 1 111 1 111 1 111 1 111 1 111 1 111 1 1�: 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 •� 1 111 1 111 1 111 1 1 � 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1�� 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1' 1 111 1 111 1 111 1 111 ® 1 111 1 111 1 111 1 111 1111 1 111 ® 1111 1 111 1111 1 111 � 1 1111 1 111 1111 • , "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations". Signature of Land Applier 1-2A 2U Date DENR FORM MFLSF (12/2006) u d z 9 N PQ. U z d£ d6 of r m N U c U a y ro C F N O za U 3 �q G m Q � Z V u u w ..- a z E m :: Ammonia y q m N Nitrogen E N E N ,`t; N N c rn o m W U N •N4 b O .N. y p O O O E � Pko d o a Mineralization CI! O v m Rate*** o i z o 0 0 m 1: Volatilization o a v Rate** c o o 0 c 0 o h W Application U t`z1.-. o 0 0 Method* o c o OO M N v 3 d c d w O Q y O Q O O U N W u U o 0 0 Q u v W a U o 0 0 d o 0 u 0 0, Q O 9 Q ' A M y 9 > p N C C « N •°�• � � 0.i E o Q IDUOW a Q t 10 BjEQ F O U C. 0. V � o d O A L O O y O Y 'O ti o u A0 L fi ea 60 O U 7 a y L R C m O ezC o c_ Vl Y n N o C 'y y Cad rw u m m .e a c z o .a =� �3 '50 ai c o A u w G O G u o e o 14 t L v uL w y on ad+ m •= u� q�c�q' 9 °d iaa o Ct L u •R C p. m v ?t ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tans Applied (Annual): 5.49 Permit #: WQ0000702 Cation Exchange Capacity (non 503 only): 7.1 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Argent Acres Used: 2.18 Acres Permitted: 2.18 Site #: NC-PA-2 Field #: 7A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 0000000MENNING 1 111 1 111 1 111 WIT, 11 1 1 I i M, 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 .�.- 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1.1 1 111 1 111 1 111 1 1�1 '® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 � 1 111 1 111 1 111 ®1 ®'' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1.1 1 111 1 111 1 111 1 1�1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 • � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 tll 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 �'1 1 111 1 111 1 111 �`1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ® 1 111 1 111 1 111 • • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". W Signature of Land Applier Date DENR FORM MFLSF (12/2006) NINIInIOw N U z Q zz ad. d °•d ° as y u za u 3 aq a a o 0 0 0 0 0 0 o Q o O o o o d gyp, 0 0 0 0 0 0 0 0 0 z O O O O .' y u o o c o 0 0 0 o o 0 o c �° ZQ U b � :Z E s Ammonia Nitrogen E N 's N o a rn aC *� y o 0 0 E E M w UO o 0 0 i a Mineralization '^ 0 Rate*** Z o o .t6. Volatilization o ,°O� r,, Rate** _ c o 0 0 in w Application U Go o 0 0 Method* 4 X o 0 0 0 u p, 0 u a �� a c 0 = A Y Q U 03 v o 0 0 •o o� N �w •� =' � d 3 x •u 0 o a m a E a F c o 0 0 0 0 0 0 0 o 0 o M u o 0 0 0 0 0 0 0 0 0 0 0 y Q o n a O O G C O C C O N O 0 0 C O O Q � a a N � N y p O U N a v 2 o O o a v � id m fS`a c u i' '" ❑ 7 LL � U p �u 0LRUOFq Q o t to OTeQ ti o c C 91 Y Q ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tons Applied (Annual): 5.49 Permit #: WQ0000702 Cation Exchange Capacity (non 503 only): 7.9 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Argent Acres Used: 2.57 Acres Permitted: 2.57 Site #: NC-PA-2 Field #: 7B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 � 1 111 1 111 1 111 1 1 •'® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11. 1 111 1 111 1 111 1 11. ..,- 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 i 111 1 111 1 111 1 1 �� ►7ifi1il8t{W 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 � 1 1 111 1 111 1 111 ®'' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 � �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 . 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 � 1 111 1 111 1 111 MMMMMMMMMMMMMM 1 1 111M "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ,/A Signature of Land Applier 2,� LL0 Date DENR FORM MFLSF (12/2006) N M M M N1 N U z if iE � y y W 7h i d a i A N 5 c N > z ce u 3 a C] o 0 0 0 0 0 0 0 o z 0 0 0 0 0 0 06 0 :� a' W 0 0 0 0 0 0 0 0 0 0 0 O 0 0 6 0 0 o 0 0 t 2 i0 Z E . .......... Ammonia Nitrogen E 3 N r4 ni N ri d ^ d m o N y 0 0 0 O E E h y W in o 0 0 Mineralization Rate*** c V w Volatilization o Rate** _ a o o 0 0 0 W 0 Application U o 0 0 Method* ai a O v y a 0 N o 0 0 e y o g 3 -o A c a rn rn .0 u c � a �^ 3 Y y U? N 0 m n 0 O W 0 0 0 v 3 x v o N W C U o 0 0 0 0 0 U 0 0. 5 b C OO, U 0 0 0 0 0 0 0 0 0 0 0 min tN�l N O O O O O O O O O m 0 0 0 Q O O O Ga O O C C C 0 0 0 tV C O C C Cl 0 Q � a c o m � i A a� R i U a 9 .p C 5 O N v O o ,7, o w �v >v ; E U p U z WOW Y dau04 H ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Permit #: WQ0000702 Total Dry Tons Applied (Annual): 7.69 Cation Exchange Capacity (non 503 only): 9.0 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Argent Acres Used: 3.32 Acres Permitted: 3.32 Site #: NC-PA-2 Field #: 7C Residual Analysis Data (Heavy Metals and Total Phosphorus use me/ke. % Solids use Raw Percent M: a Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 .'® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11. 1 111 1 111 1 111 1 11. ...- 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 '.' 1 111 1 111 1 111 '.` 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 . 1 111 1 111 1 111 1 1 . 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 � � � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1, 1 111 1 111 1 111 1 1 1® 1® 1® 1® 1® 1® 1® 1®® 1® 1® 1®® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 111 1 111 1 111 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". __�4 i ,7.,t L�, Signature of Land Applier Date DENR FORM MFLSF (12/2006) 'O 9 'a a Zi r N Q z N yp. N U 0 ° 0 z, N 0 0 0 0 0 0 0 0 O O O O .. O ry o 0 0 0 0 0 0 0 0 0 0 0 o Ammonia Y ,�„ .z-. q c as Nitrogen E d e rn z m N 0 0 F E - �on W o o 0 0 Mineralization ,., O o M Rate*** o LL Z o O o O i W O Volatilization �', O N N o Rate** a 0 0 R es0 6 Application U w o 0 0 Method* OO O O V 4 ry� C V O O O R C Q O O V U b h y cc V c � o N d N3 y o 0 0 0 w 3 x a a V o 0 0 0 0 is a ¢ 0 0 0 0 0 0 0 0 o m ,yi voi ¢ F o 0 0 0 0 0 o M o 0 o d o 0 > c o 0 0 0 0 0 o Ni o 0 0 06 0 0 Q � M c y v o U A N OQ U TJ 9 C O N m ay o c 7 U 7 y E > y a U p U z d o. gluo I I to OJUG V ry R Q 0 0 N eNi LL 0 0 s Z ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tons Applied (Annual): 7.69 Permit #: WQ0000702 Cation Exchange Capacity (non 503 only): 6.5 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Argent Acres Used: 3.32 Acres Permitted: 3.32 Site #: NC-PA-2 Field #: 7D Residual Analysis Data (Heavy Metals and Total Phosphorus use rn&k¢, % Solids use Raw Percent M: Annual Heavy lyletal Field Loadings (Calculated in Ibs/acre): 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 1 $ 1 111 1 111 1 111 1 11. 1 111 1 111 1 111 1 11. 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 . 1 111 1 111 1 111 1 1 '® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 '.` 1 111 1 111 1 111 `.' ®'' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 . 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 Ili 1 11 1 111 1 111 1 111 1 11 � � � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 2®1 1 111 1 111 1 111 '®1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 111 1 111 1 111 1 ,. "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment(�ff or knowing violations". � 11- Signature of Land Applier 1/14/2-1.) Dat DENR FORM MFLSF (12/2006) M1I Nl I� I N Q 'z i! it W � 1R � u N F ,w •� p p c a I- U G P O pyp m N Q m 6 0 0 0 0 0 O O O O R O O O () O O O O O C O O W1 O C C C'i E w. ............ Ammonia Y ,d„ $ c a N N Nitrogen E N E N C o0 6 m o y E E N w o C C Mineralization Rate*** C s o C d uR Volatilization o Rate** a o C 0 0 0 m CD o Application Method* � CD 0 � 0a.y .- � v C C C Q L N a0 O U o b n c xi aA °o a �3Gv a yvCCC o 0 w 3 a wQ� V 0 6 C U u p c 0 0 0 0 0 0 0 0 0 0 0 b N V ya! U F O O O O O O O O Vf M O 0 0 y 0 0 0 Q¢ r G C 0 0 0 C O G N C C C Q O G G Q � arn v P U R o y o a ° y ; W E a U y O V on � U � 6 uo .10 QQ0.0 PO f� Y A ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tons Applied (Annual): 7.69 Permit #: WQ0000702 Cation Exchange Capacity (non 503 only): 7.5 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Argent Acres Used: 3.26 Acres Permitted: 3.26 Site #: NC-PA-2 Field #: 7E Residual Analysis Data (Heavy Metals and Total Phosphorus use me/Ict=. % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): •. 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 .'® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 ...� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 '® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1� 1 111 1 111 1 111 1 ®'' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 � � � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 � 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1111 1 111 � 1 111 1 111 1111 '�: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ® 1 111 1 111 1 111 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". �-V.4` 1Z9 20 Signature of Land Applier Date DENR FORM MFLSF (12/2006) WI6 U Z Zi N U O a U a w o 80 4.. C u Q E u 9 N 6 0 0 0 0 0 0 0 O 0 O 0 O 0 O 0 O Q O O O O O O O O I d O O O O O O O O O z O O O O _ p y o 0 0 0 a� Q � z. O O O O O O O O N O 0 0 N a00000000�000 � o ,Q,� (j 0 0 0 0 0 0 0 0 0 0 0 u u m c z"z E €° w Ammonia „a., $ ❑ ,;,� Nitrogen E d G rn `z x Ot O N ° L-i GJ Vt O] M O O O C Mineralization M O < v a Rate*** z o 0 0 V R Volatilization ' o Rate** _ c o 0 0 W Application UOf0 0 0 Method* a _ v o 0 0 y ° O ❑ y 0 0 � 0 O U N O M V c C �oA� 3 Y ¢UC oC! ti E 0 o = o M c Q u v v v 3 x iv 0. W a v o 0 0 z o a o V O 6 d V O O O O O O O O Vl O O O O O O F >Q aQ � O O O G G O 0 0 (V G C O ¢ G O O Q 0 9 ' e C M � m N o > N* V V >_J' N ^ O N C O_' o P G > ro U E U Z ..°u.- U � U R � >, C Q a uo ? ::: F< a V a a Y R 0 ?a ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Permit #: WQ0000702 Total Dry Tons Applied (Annual): 7.69 Cation Exchange Capacity (non 503 only): 8.5 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Argent Acres Used: 3.03 Acres Permitted: 3.03 Site #: NC-PA-2 Field #: 7F Residual Analysis Data (Heavy Metals and Total Phosphorus use ma/ke. % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): .'® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1. 1 111 1 111 1 111 1 1. �...- �7L'JL'IiiIL'iIL' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1. 1 111 1 111 1 111 1 1. 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 � � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1�. 1 111 1 111 1 111 1 1�. 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� . 1 111 1 111 1 111 1 1� . 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1' 1 111 1 111 1 111 1' ,. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) u 7k E a d z i N U a a U p w c a y is d z a u 3 a C] v a o 0 0 0 0 0 0 0 0 0 0 0 :.: N O O O O O O O O z () O O O C O 0 0 0 O O O O Q � V O C C G O O O O� C 6 O O :; •� Z z E E ......:::::.:::::::: w Ammonia \ y q c, e N Nitrogen c rn o n 0 0 0 E Mineralization Rate*** V O O O Volatilization O ry n Rate** c O d o o 0 d w Application U w o 0 0 Method* O o o c o O y W O O P' O O n o 0 0 R O `n U e.3 U mad a o00 v O 0. a U o 000 0 0 U 9 i' O O O O O O O O aQ0 0 0 0 N b a O O O O O O O O V O 0 0 ¢ 0 0 0 > d0 r 0 0 0 0 0 0 0 0 N 0 0 0 O O O .o e rn N * O V N c o O m � o 0 N '� C7 m tFtl d P4 .y PI > � � v E a u y Ci z o a Y U C 6 a MUM°� ¢ to ajeQ n o d U a P. a� u R i0. Y = R y w o 0 O y F W H O G y � 9 R C ti N �y O d e s cw z �- +' G F C u o o U e a F y Z y d cod+ ` m W � .� •ea 0 r_ 4 a x a , w o R o E .0 3 nl d aCi w °a Ca .0 C Y E d d w E F. •� o m y � e� d R R ;dd ° ° w Z• R O Y � y y «a a 00 d W Ls, G a o O G F 7 F C 7 c C b y as o C w fi u is *o ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tons Applied (Annual): 8.79 Permit #: WQ0000702 Cation Exchange Capacity (non 503 only): 9.9 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Argent Acres Used: 3.53 Acres Permitted: 3.53 Site #: NC-PA-2 Field #: 7G Residual Analysis Data (Heavy Metals and Total Phosphorus use me/ke, % Solids use Raw Percent #l: a Em N■■■■■■■■ • 1 ■■■ Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • 1 111 1 111 1 111 1 1 Im 111 EM 1 111 1 111 1 11 1 111 1 111 1 111 1 11 •..� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1.1 1 111 1 111 1 111 1 1.1 '® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ®' 1 111 1 111 1 111 ®' ®'' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1.1 1 111 1 111 1 111 1 1.1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 WM1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 :®:' 1 111 1 111 1 111 :®:' 1111 1111 1111 1111 1111 1111 1111 1111 ' 1 1111 1111 1111 • li • • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 2 Z;J Date DENR FORM MFLSF (12/2006) u MlMlgl� x a U ii d6 31tz ac d Y a z i O QcK m a� U .- Q c .5 a .� Q' a� z a a A N a O o O 0 O 0 O 0 O 0 O O O O O O O 0 a m U O G C o O C G O O C C .. Ammonia y n.... r o Nitrogen E G � m o E E n w o 0 0 Mineralization Rate*** o c o sq F o Volatilization �.. O V N Rate** c o 0 0 n w Application U wbfo 0 0 Method* Z M o 0 0 O u C H 0. O ci v c c o 0 " U 3 ' •W u_ G M ..i �c n any x auoo� of W Q5 N VJ N 9 PS U o 0 0 rL FS 0 0 0 V O O O O O O O O In V1 N A M Lam[.• y U O O 0 0 0 0 0 0 O O In O O O 0 O 0 ¢ 0 0 0 F > a¢ � O O O O G C C C N C O G O O C Q � a M c v N � U o U R O O O R N > .0 # C N a a v U a i '" U G U v¢ 0. qjuUW .q. X. Q y 70 a3Ea U a 0. Y R A a ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tons Applied (Annual): 7.69 Permit #: WQ0000702 Cation Exchange Capacity (non 503 only): 9.3 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Yonges Acres Used: 3.28 Acres Permitted: 3.28 Site #: NC-PA-2 Field #: 7H Residual Analysis Data (Heavy Metals and Total Phosphorus use me/kia. % Solids use Raw Percent #): Non Annual Heavy Metal P'ield Loadings (Calculated in Ibs/acre): 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 .'® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 �.�- 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 . 1 111 1 111 1 111 1 1 � '® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 11 1 111 1 111 1 111 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 . 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 � � � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ' 11 1 111 1 111 1 111 `11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 .' 1 111 1 111 1 111 �` ' '. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ail ri I.orl� °• m N a u 3 a Ca z o 0 0 0 0 0 0 0 0 0 0 y �j o 0 0 o c c o o� o 0 6 0 ? a Z z E 4 Ammonia Nitrogen EX. d ° o N w ? m 0 0 GO o E ,M W o 0 0 Mineralization ,., Rate*** o C C o O w Volatilization O a N b Rate** c/� C O o O c O d a w Application U WOfo o o Method* Z x o 0 0 O G G C t2 L _O vni m o m p o 0 _ P. y� � V CS c e o q "'o U 3 A a U o v M v u 3 E u Y d U o o; 0 ❑w � a U o 0 oc V L 6 O O O O O O O O b O O O b� •� � U O O O O O O O O O M O o O r/l ¢ O O M O G F lV G O O C C C Q � vrn a m � p♦ Q U c o o O0 o v a y r G 76 w E e c C4 ^ o U 7 d >v U U' p Ua¢ m MUM ¢ C ° G SO Q;EQ rn O Ua.a. . r-Q' R su F 0 C dE �� a� .Z. o s. 0 y y y O C u y p rr d R y r G z� a+ y C � u u o LQ o d k 7 eL�C u W p x s o cEa •a'. o-.i W L � E a 3 L _s1, C p .`l ! V C L W � d G 3 � s d s Pa Pa = ,WW odd r. W d PC W O ^ � G O y d NO A G C O p o p h C \ 0 C ^\ MO �y w E u id w c ._ ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Total Dry Tons Applied (Annual): 7.69 Permit #: WQ0000702 Cation Exchange Capacity (non 503 only): 10.1 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Yonges Acres Used: 3.25 Acres Permitted: 3.25 Site #: NC-PA-2 Field #: 7I Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #). nnua eavy Metal Field Loa togs a cu ated in lbs/acre): 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 . 1 111 1 111 1 111 1 1 . NOW 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 ...- 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 '® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1® 1 111 1 111 1 111 1® ®'' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 � �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1 1 111 1 111 mm1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 � 1 111 1 111 1 111 1 1 ® 1 111 lm1 111 1 111 1 111 1 111 '® 1 111 1 111 1 111 `® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 :`; 1 111 1 111 1 111 1 :': '. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for k owing violations". Signature of Land Applier 2 Date DENR FORM MFLSF (12/2006) N M N ri K v o a.w U N U co w za u 3 ^R U Q� 0 0 0 0 0 tjo o 0 0 0 0 6 0 0 6 U U 2 W ' 2 'z L e............. Ammonia Y a a Nitrogen E N E m v c a rn o y o 0 0 .4Z.' F E h pwj w rj o 0 0 Mineralization o00 R Volatilization v O ry b Rate** c Z o o 0 0 0 0 n w Application U cv'-, or o 0 0 Method* x o 0 0 0 o d A U U a O _ v W d o 0 s _ y V c C o 3 Y ¢ v o O N U y O O O a w 3 a U o 0 0 FS c o 0 U U y N o v. o 0 o 0 0 0 0 0 0 0 0 0 0 0 0 o o ro M 0 o o 0 c o o 0 2 o '-" a F as r c o 0 0 0 0 0 o ri o 0 0 Q o c 6 c a o 9 P o O M v v y a O U 9 9 C O O o N .a w (n o� r E �n c � C U a U n ? U z p �U•pa w v tguoW a flT ¢ .to OTEQ ti o a '0 ? Q ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Havelock Permit #: WQ0000702 Total Dry Tons Applied (Annual): 7.69 Cation Exchange Capacity (non 503 only): 9.4 Operator: Michael Spencer Owner: Spencer Farms, Inc. Predominant Soil Series: Yonges Acres Used: 3.25 Acres Permitted: 3.25 Site #: NC-PA-2 Field #: 7J Residual Analysis Data (Heavy Metals and Total Phosphorus use m0k¢. % Solids use Raw Percent #lc 0 Annual Heavy Metal k ield Loa m s a cu ate In lbs/acre : 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 . .'® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 �� �...�- �77:L•�iiiLYL 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1® 1 111 1 111 1 111 1® ®'' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 � � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� IREM 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 :': 1 111 1 111 1 111 1 :': '. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 24 '2_U Dae DENR FORM MFLSF (12/2006) N U E @ R a v o U w c Q E A m o r m za o a o 0 0 0 0 0 0 o Q o v o 0 0 0 0 0 0 0 0 z 0 0 R 0 0 0 0 e p, U O C G O O C Cl O G o O o a m d T., P. o 0 0 0 0 0 0 0 0 0 0 0 P V 0 0 0 0 0 0 0 0 0 0 0 i0 E E °' Z z w Ammonia Nitrogen E 1 E `v c of o y N C b F ^ E Mineralization O Rate*** M o W •z- o 0 0 r o 0 0 `R Volatilization v 0 Rate** _ c o 0 0 W Application Method* z x o 0 0 O v S a y V o c o R e o p `° c u 3 E 0 m U C u O h p o 0 0 N V1 d « ` b C 0 O W : m A U o 0 0 U N 6 Q O O O O O O O O N O O O F a d O O O O O O O O N O 0 0 O O O Q o v 'O a+ m M N O 3t 0 0 U C o O o .a oo y * o > C V V 3 A U U z qjuOw v ao a;aQ ° c o da`Uac`, [Ij ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Havelock W00000702 Michael Spencer Owner: Spencer Fanns, Inc. Predominant Soil Series: Yonges 2.47 Acres Permitted: 2.47 Site #: NC-PA-2 Field #: 7K Total Dry Tons Applied (Annual): 5.49 Cation Exchange Capacity (non 503 only): 10.0 Residual Analysis Data (Heavy Metals and Total Phosphorus use m2/k2, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 .'® ltll 1111 1111 1111 1111 1111 1111 1111 111. 1111 t111 1111 111. non, 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 '® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 :®1 1 111 1 111 1 111 :®1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 11 �� 1111 1111 1 111 1 111 1 111 1 111 1111 1 111 11�1 1 111 1 111 1111 11�1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 1 111 1 111 1 111 1 1� 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 �' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 .1 1 111 1 111 1 111 .1 . ' ,. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) SOIL ANALYSIS REPORTS Lime applications were performed by Spencer Farms during the 2019 calendar year to all fields with a pH below 6.0, however the 2019 soil sampling results do not reflect the lime amendments as the soil samples were collected prior to land application activities being performed. Additional sampling will be performed during the 2020 calendar year. 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