NCG550557_Effluent Sample Results_20171024

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
October 24, 2017
James Bain
Dr. James Bain
122 Archery Range Rd
Bahama, NC 27503
RE: Project: Waste Water
Pace Project No.: 92358462
Dear James Bain:
Enclosed are the analytical results for sample(s) received by the laboratory on October 10, 2017.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Clayton McCrickard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Raleigh One Time, Onetime -Raleigh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Waste Water
Pace Project No.: 92358462
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

aceAnalytical
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Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
SAMPLE SUMMARY
Project: Waste Water
Pace Project No.: 92358462
Lab ID Sample ID Matrix Date Collected Date Received
92358462001 WW01-WW04 Water 10/10/17 09:30 10/10/17 10:48
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
SAMPLE ANALYTE COUNT
Project: Waste Water
Pace Project No.: 92358462
Lab ID Sample ID Method
92358462001 WW01-WW04 SM 2540D
SM 5210B
SM 9222D
SM 4500-CI G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytes
Analysts
Reported
RAY
1
NMH
1
BWJ
1
NAL
1
Page 4 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
ANALYTICAL RESULTS
Project: Waste Water
Pace Project No.: 92358462
Sample: WW01-WW04
Lab ID: 92358462001 Collected:
10/10/17 09:30
Received: 10/10/17 10:48 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
4.4 mg/L
2.5
1
10/12/17 09:38
5210B BOD, 5 day EDN
Analytical Method: SM 5210B
BOD, 5 day
ND mg/L
2.0
1
10/11/17 17:09 10/16/17 11:41
MBIO 9222D Fecal Coliform RAL
Analytical Method: SM 9222D
Fecal Coliforms
36.0 CFU/100 mL
1.0
1
10/10/17 14:35
4500CL G Chlorine, Residual
Analytical Method: SM 4500-CI G
Chlorine, Total Residual
ND mg/L
0.024
1
10/23/17 22:36 7782-50-5 H1
Date: 10/24/2017 08:28 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QUALITY CONTROL DATA
Project: Waste Water
Pace Project No.: 92358462
QC Batch: 382037
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92358462001
METHOD BLANK: 2117021
Matrix:
Water
Associated Lab Samples: 92358462001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 10/12/17 09:35
LABORATORY CONTROL SAMPLE: 2117022
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
226
90 90-110
SAMPLE DUPLICATE: 2117023
92358582001
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Total Suspended Solids
mg/L
37.3
44.8 18 5 D6
SAMPLE DUPLICATE: 2117024
92358581001
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Total Suspended Solids
mg/L
5.4
6.0 11 5 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 08:28 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QUALITY CONTROL DATA
Project: Waste Water
Pace Project No.: 92358462
QC Batch: 381921
Analysis Method:
SM 5210B
QC Batch Method: SM 5210B
Analysis Description:
5210E BOD, 5 day EDN
Associated Lab Samples: 92358462001
METHOD BLANK: 2116415
Matrix: Water
Associated Lab Samples: 92358462001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
BOD, 5 day
mg/L
ND
2.0 10/16/17 11:41
LABORATORY CONTROL SAMPLE: 2116416
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
BOD, 5 day
mg/L
198 196
99 84.6-115.4
SAMPLE DUPLICATE: 2116417
92358550001 Dup
Max
Parameter
Units
Result Result
RPD RPD Qualifiers
BOD, 5 day
mg/L
186
186 0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 08:28 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QUALITY CONTROL DATA
Project: Waste Water
Pace Project No.: 92358462
QC Batch: 381820 Analysis Method: SM 9222D
QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL
Associated Lab Samples: 92358462001
METHOD BLANK: 2115848 Matrix: Water
Associated Lab Samples: 92358462001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 10/10/17 14:35
SAMPLE DUPLICATE: 2115849
92358462001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Fecal Coliforms CFU/100 mL 36.0 47.0 27 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 08:28 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QUALITY CONTROL DATA
Project: Waste Water
Pace Project No.: 92358462
QC Batch: 383640 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92358462001
METHOD BLANK: 2126144
Associated Lab Samples: 92358462001
Parameter Units
Chlorine, Total Residual mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.024 10/23/17 22:36
SAMPLE DUPLICATE: 2126145
92358462001 Dup
Parameter Units Result Result
Chlorine, Total Residual mg/L ND ND
Max
RPD RPD Qualifiers
10 H1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 08:28 AM without the written consent of Pace Analytical Services, LLC.
Page 9 of 15

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QUALIFIERS
Project: Waste Water
Pace Project No.: 92358462
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H1 Analysis conducted outside the EPA method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 08:28 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Waste Water
Pace Project No.: 92358462
Lab ID
Sample ID
QC Batch Method
QC Batch
92358462001
WW01-WW04
SM 2540D
382037
92358462001
WW01-WW04
SM 5210B
381921
92358462001
WW01-WW04
SM 9222D
381820
92358462001
WW01-WW04
SM 4500-CI G
383640
Date: 10/24/2017 08:28 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
SM 5210B
Analytical
Batch
381976
Page 11 of 15

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Page 14 of 15

October 10", 4017
Pace Analytical
6701 Conference Drive
Raleigh, NC 27607
Dear Pace Analytical:
Please perform these assays on effluent from my household sand -filter system:
• Biochemical oxygen demand.
• Total suspended solids.
• Total residual chlorine (water).
• Fecal coliforms (membrane filter).
Thank you for your help!
Best,
rJames R. Bain
122 Archery Range Road
Bahama, NC 27503
(414) 4514108 cell
Page 15 of 15