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NCG030447_DMR_20191031
^^ 4O CATERPILLAR Caterpillar,Inc. December 18, 2019 Building Construction Products Division RECEIVED 5000 Womack Road Sanford,North Carolina 27330 JAN 07 2020 DENR-LAND QUALITY Division of Water Resources(DWR) STORMWATER PERMITTING 1617 Mail Service Center Raleigh,North Carolina 27699-1617 To Whom It may Concern, Please find attached(COC Number NCG030447) our Semi-Annual Stormwater Discharge Monitoring Report for Caterpillar located at 5000 Womack Rd., Sanford,NC. Upon reviewing the report you will notice that our outfall location is above the benchmark range for total suspended solids, copper and zinc which requires us to perform a"Tier One"according to the permit. We have conducted a stormwater inspection of our facility since the sampling period and have potentially identified some possible causes of the exceedance of the established benchmark. We will implement some operational control measures for the parameter's of concern, with the anticipation of bringing the concentration's within regulatory limit. If you have any questions,please do not hesitate to call me. Best Regards, Kevin Staubus EHS Manager Caterpillar, Inc Sanford,NC Business Phone: 919-777-2375 Staubus_kevin@cat.com Caterpillar: Confidential Green STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year 2019 Individual NPDES Permit No. NCS❑❑❑❑❑❑ or Certificate of Coverage (COC) No. NCG030447 This monitoring report summary of the calendar year should be kept on file on-site with the facility SPPP. Facility Name: Caterpillar, Inc. County: Lee Phone Number: (919)777-2000 Total no. of SDOs monitored 1 Outfall No. 1 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No-Q If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No �sl Parameter, (units) Non-Polar Total Toxic Total Total pH Lead Zinc O&G/Total Organics Rainfall, Suspended Standard Units Copper Petroleum inches Solids Hydrocarbon Benchmark N/A 100 mg/L 6.0-9.0 0.007 mg/L 0.030 mg/L _ 0.067 mg/L 15 mg/L _ 1 mg/L Date Sample Collected, mm/dd/yy 10/30/2019 0.16 230 '6.3 <0.008 <0.0155 0.168 11.8 See Attached SWU-264-Generic-13Dec2012 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and im ' onment for ing violations." Signature _ Date (2,.-1 - <l_ For questions, contact your local Regional Office: DWQ Regional Office Contact Information: Winston-Sa(nm ri- I t" ,Vs::: ',,",:A �1( r '-'4 ,, e_s.., �`f i '' „.../ ------- , 1.„,,u14 .1, ---1--„,4--- ,. i -...,,, ,,,.. pp ASHEVILLE REGIONAL OFFICE ' FAYETTEVILLE REGIONAL OFFICE MOORESVILLE REGIONAL OFFICE 2090 US Highway 70 ! 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 (704) 663-1699 (910) 433-3300 RALEIGH REGIONAL OFFICE WASHINGTON REGIONAL OFFICE WILMINGTON REGIONAL OFFICE 3800 Barrett Drive 943 Washington Square Mall 127 Cardinal Drive Extension Raleigh, NC 27609 Washington,NC 27889 Wilmington, NC 28405-2845 (919) 791-4200 (252) 946-6481 (910) 796-7215 WINSTON-SALEM REGIONAL OFFICE CENTRAL OFFICE 585 Waughtown Street 1617 Mail Service Center - "To preserve.p rotect Winston-Salem, NC 27107 Raleigh,NC 27699-1617 and enhance (336) 771-5000 (919) 807-6300 North Carolina's water... SW U-264-Generic-13Dec2012 ( iEc )c) www.encolabs.com ANALYTICAL RESULTS Description: CAT Sanford Outfall 1 Lab Sample ID:CC18256-01 Received: 10/31/19 16:00 Matrix: Water Sampled:10/30/19 09:50 Work Order:CC18256 Project: Caterpillar(Sanford)Stormwater Sampled By:Mike Outlaw Volatile Organic Compounds by GCMS ^-ENCO Cary certified analyte[NC 591] Analvte 1CAS Number] Results Flaq Units DF MDL POL Batch Method Analyzed By Notes 1,1,1-Trichloroethane[71-55-6]^ <0.80 ug/L 1 0.80 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF 1,1,2,2-Tetrachloroethane[79-34-5]^ <0.54 ug/L 1 0.54 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF 1,1,2-Trichloroethane[79-00-5]^ <0.76 ug/L 1 0.76 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF 1,1-Dichloroethane[75-34-3]^ <0.62 ug/L 1 0.62 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF 1,1-Dichloroethene[75-35-4]^ <0.94 ug/L 1 0.94 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF 1,2-Dichlorobenzene[95-50-1]^ <0.73 ug/L 1 0.73 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF 1,2-Dichloroethane[107-06-2]^ <0.63 ug/L 1 0.63 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF 1,2-Dichloropropane[78-87-5]^ <0.80 ug/L 1 0.80 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF 1,3-Dichlorobenzene[541-73-1]^ <0.77 ug/L 1 0.77 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF 1,4-Dichlorobenzene[106-46-7]^ <0.76 ug/L 1 0.76 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Acrylonitrile[107-13-1] <3.2 ug/L 1 3.2 10 9K08021 EPA 624.1 11/09/19 05:29 REF Benzene[71-43-2]^ <0.71 ug/L 1 0.71 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Bromodichloromethane[75-27-4]^ <0.52 ug/L 1 0.52 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Bromoform[75-25-2]^ <0.75 ug/L 1 0.75 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Bromomethane[74-83-9]^ <0.95 ug/L 1 0.95 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Carbon Tetrachloride[56-23-5]^ <0.94 ug/L 1 0.94 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Chlorobenzene[108-90-7]^ <0.72 ug/L 1 0.72 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Chloroethane[75-00-3]^ <0.98 ug/L 1 0.98 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF QL-02 Chloroform[67-66-3]^ <0.80 ug/L 1 0.80 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Chloromethane[74-87-3]^ <0.82 ug/L 1 0.82 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF cis-1,3-Dichloropropene[10061-01-5]^ <0.59 ug/L 1 0.59 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Dibromochloromethane[124-48-1]^ <0.44 ug/L 1 0.44 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Ethylbenzene[100-41-4]^ <0.69 ug/L 1 0.69 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Methylene Chloride[75-09-2]^ <2.0 ug/L 1 2.0 5.0 9K08021 EPA 624.1 11/09/19 05:29 REF Tetrachloroethene[127-18-4]^ <0.76 ug/L 1 0.76 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Toluene[108-88-3]^ <0.72 ug/L 1 0.72 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF trans-1,2-Dichloroethene[156-60-5]^ <0.73 ug/L 1 0.73 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF trans-1,3-Dichloropropene[10061-02-6]^ <0.73 ug/L 1 0.73 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Trichloroethene[79-01-6]^ <0.89 ug/L 1 0.89 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Vinyl chloride[75-01-4]^ <0.71 ug/L 1 0.71 1.0 9K08021 EPA 624.1 11/09/19 05:29 REF Surrogates Results RE Spike Lvi %Rec Limits Batch Method Analyzed Ai Notes 4-Bromofluorobenzene 55 1 50.0 111% 41-142 9K08021 EPA 624.1 11/09/19 05:29 REF Dibromochoromethane 58 1 50.0 116% 53-146 9K08021 EPA 624.1 11/09/19 05:29 REF Toluene-d8 55 1 50.0 109% 41-146 9K08021 EPA 624.1 11/09/19 05:29 REF Semivolatile Organic Compounds by GCMSIII ^-ENCO Cary certified analyte INC 5911 gnalyte FCAS Number] Results Flaq Units Pf Ma PQL Batch Method Analyzed @y Notes 1,2,4-Trichlorobenzene[120-82-1]^ <3.3 ug/L 1 3.3 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 1,2-Dichlorobenzene[95-50-1] <3.2 ug/L 1 3.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 1,3-Dichlorobenzene[541-73-1] <3.4 ug/L 1 3.4 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 1,4-Dichlorobenzene[106-46-7] <3.2 ug/L 1 3.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 2,4,6-Trichlorophenol[88-06-2]^ <6.4 ug/L 1 6.4 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 2,4-Dichlorophenol[120-83-2]^ <6.5 ug/L 1 6.5 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 2,4-Dimethylphenol[105-67-9]^ <6.4 ug/L 1 6.4 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 2,4-Dinitrophenol[51-28-5]^ <7.7 ug/L 1 7.7 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 2,4-Dinitrotoluene[121-14-2]^ <3.2 ug/L 1 3.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 4 of 23 (eJSiEc') www.encolabs.com ANALYTICAL RESULTSIl Description: CAT Sanford Outfall 1 Lab Sample ID:CC18256-01 Received: 10/31/19 16:00 Matrix: Water Sampled:10/30/19 09:50 Work Order:CC18256 Project: Caterpillar(Sanford)Stormwater Sampled By:Mike Outlaw Semivolatile Organic Compounds by GCMS A-ENCO Cary certified analyte[NC 5911 Analvte FCAS Numberl Results Flaq Units DF MDL POL Batch Method Analyzed y Notes 2,6-Dinitrotoluene[606-20-2]^ <2.9 ug/L 1 2.9 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 2-Chloronaphthalene[91-58-7]^ <3.2 ug/L 1 3.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 2-Chlorophenol[95-57-8]^ <7.4 ug/L 1 7.4 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 2-Methyl-4,6-dinitrophenol[534-52-1]^ <6.0 ug/L 1 6.0 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 2-Nitrophenol[88-75-5]^ <5.2 ug/L 1 5.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 3,3'-Dichlorobenzidine[91-94-1]^ <3.3 ug/L 1 3.3 10 9K04016 EPA 625.1 11/07/19 07:27 DFM QV-01 4-Bromophenyl-phenylether[101-55-3]" <3.3 ug/L 1 3.3 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 4-Chloro-3-methylphenol[59-50-7]^ <7.3 ug/L 1 7.3 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 4-Chlorophenyl-phenylether[7005-72-3]^ <3.2 ug/L 1 3.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM 4-Nitrophenol[100-02-7]^ <7.9 ug/L 1 7.9 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Acenaphthene[83-32-9]^ <3.0 ug/L 1 3.0 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Acenaphthylene[208-96-8]^ <9.6 ug/L 1 9.6 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Anthracene[120-12-7]^ <3.0 ug/L 1 3.0 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Benzidine[92-87-5]^ <7.1 ug/L 1 7.1 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Benzo(a)anthracene[56-55-3]^ <3.2 ug/L 1 3.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Benzo(a)pyrene[50-32-8]^ <3.2 ug/L 1 3.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Benzo(b)fluoranthene[205-99-2]^ <3.4 ug/L 1 3.4 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Benzo(g,h,i)perylene[191-24-2]" <3.7 ug/L 1 3.7 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Benzo(k)fluoranthene[207-08-9]^ <3.8 ug/L 1 3.8 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Bis(2-chloroethoxy)methane[111-91-1]^ <3.3 ug/L 1 3.3 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Bis(2-chloroethyl)ether[111-44-4]^ <3.8 ug/L 1 3.8 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Bis(2-chloroisopropyl)ether[108-60-1]^ <3.5 ug/L 1 3.5 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Bis(2-ethylhexyl)phthalate[117-81-7]^ <3.5 ug/L 1 3.5 5.0 9K04016 EPA 625.1 11/07/19 07:27 DFM Butylbenzylphthalate[85-68-7]^ <5.1 ug/L 1 5.1 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Chrysene[218-01-9]^ <3.0 ug/L 1 3.0 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Dibenzo(a,h)anthracene[53-70-3]^ <3.8 ug/L 1 3.8 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Diethylphthalate[84-66-2]^ <3.0 ug/L 1 3.0 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Dimethylphthalate[131-11-3]^ <3.0 ug/L 1 3.0 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Di-n-butylphthalate[84-74-2]^ <3.2 ug/L 1 3.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Di-n-octylphthalate[117-84-0]^ <4.7 ug/L 1 4.7 10 9K04016 EPA 625.1 11/07/19 07:27 DFM DPH(as Azobenzene)[103-33-3] <3.1 ug/L 1 3.1 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Fluoranthene[206-44-0]^ <4.0 ug/L 1 4.0 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Fluorene[86-73-7]^ <2.9 ug/L 1 2.9 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Hexachlorobenzene[118-74-1]^ <3.0 ug/L 1 3.0 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Hexachlorobutadiene[87-68-3]^ <4.1 ug/L 1 4.1 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Hexachlorocyclopentadiene[77-47-4]^ <3.8 ug/L 1 3.8 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Hexachloroethane[67-72-1]^ <3.0 ug/L 1 3.0 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Indeno(1,2,3-cd)pyrene[193-39-5]^ <4.1 ug/L 1 4.1 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Isophorone[78-59-1]^ <4.5 ug/L 1 4.5 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Naphthalene[91-20-3]^ <3.6 ug/L 1 3.6 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Nitrobenzene[98-95-3]^ <3.2 ug/L 1 3.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM N-Nitrosodimethylamine[62-75-9]^ <3.8 ug/L 1 3.8 10 9K04016 EPA 625.1 11/07/19 07:27 DFM N-Nitroso-di-n-propylamine[621-64-7]^ <4.5 ug/L 1 4.5 10 9K04016 EPA 625.1 11/07/19 07:27 DFM N-nitrosodiphenylamine/Diphenylamine <5.4 ug/L 1 5.4 10 9K04016 EPA 625.1 11/07/19 07:27 DFM [86-30-6/122-39-4]^ Pentachlorophenol[87-86-5]^ <8.2 ug/L 1 8.2 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Phenanthrene[85-01-8]^ <2.8 ug/L 1 2.8 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Phenol[108-95-2]^ <5.6 ug/L 1 5.6 10 9K04016 EPA 625.1 11/07/19 07:27 DFM FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 5 of 23 EglINIIr '''- .-c::) www.encolabs.com ANALYTICAL RESULTS Description: CAT Sanford Outfall 1 Lab Sample ID:CC18256-01 Received: 10/31/19 16:00 Matrix: Water Sampled:10/30/19 09:50 Work Order:CC18256 Project: Caterpillar(Sanford)Stormwater Sampled By:Mike Outlaw 1 Semivolatile Organic Compounds by GCMSII ^-ENCO Cary certified analyte[NC 591] Analvte fCAS Numberl Results Flaq Units DF MDL PQL Batch Method Analyzed y Notes Pyrene[129-00-0]^ <4.1 ug/L 1 4.1 10 9K04016 EPA 625.1 11/07/19 07:27 DFM Surrogates Results OF Spike Lot %Rec %Rec Limits Batch Method Analyzed y Notes 2,4,6-Tribromophenol 89 1 100 89% 47-128 9K04016 EPA 625.1 11/07/19 07:27 DFM 2-F/uorobiphenyl 44 1 50.0 87% 44-102 9K04016 EPA 625.1 11/07/19 07:27 DFM 2-Fluorophenol 49 1 100 49% 25-79 9K04016 EPA 625.1 11/07/19 07.27 DFM Nitrobenzene-d5 36 1 50.0 73% 43-112 9K04016 EPA 625.1 11/07/19 07.27 DFM Phenol-d5 40 1 100 40% 14-54 9K04016 EPA 625.1 11/07/19 07:27 DFM Terphenyl-d14 51 1 50.0 101% 65-122 9K04016 EPA 625.1 11/07/19 07:27 DFM Semivolatile Organic Compounds by GC ^-ENCO Cary certified analyte[NC 591.1 Analvte ICAS Numberl Results Hag Units 12f !API PQL Itch Nelhol Analyzed BY Notes 4,4'-DDD[72-54-8]^ <0.018 ug/L 1 0.018 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK 4,4'-DDE[72-55-9]^ <0.036 ug/L 1 0.036 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK 4,4'-DDT[50-29-3]^ <0.025 ug/L 1 0.025 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK Aldrin[309-00-2]^ <0.032 ug/L 1 0.032 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK alpha-BHC[319-84-6]^ <0.026 ug/L 1 0.026 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK beta-BHC[319-85-7]^ <0.022 ug/L 1 0.022 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK Chlordane(n.o.s.)[57-74-9] <0.49 ug/L 1 0.49 0.50 9331021 EPA 608.3 11/04/19 09:00 LSK Chlordane(tech)[12789-03-6]^ <0.36 ug/L 1 0.36 0.50 9331021 EPA 608.3 11/04/19 09:00 LSK delta-BHC[319-86-8]^ <0.019 ug/L 1 0.019 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK Dieldrin[60-57-1]^ <0.017 ug/L 1 0.017 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK Endosulfan I[959-98-8]^ <0.016 ug/L 1 0.016 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK Endosulfan II[33213-65-9]^ <0.017 ug/L 1 0.017 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK Endosulfan sulfate[1031-07-8]^ <0.016 ug/L 1 0.016 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK Endrin[72-20-8]^ <0.014 ug/L 1 0.014 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK Endrin aldehyde[7421-93-4]^ <0.020 ug/L 1 0.020 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK gamma-BHC[58-89-9]^ <0.020 ug/L 1 0.020 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK Heptachlor[76-44-8]^ <0.018 ug/L 1 0.018 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK Heptachlor epoxide[1024-57-3]^ <0.018 ug/L 1 0.018 0.050 9331021 EPA 608.3 11/04/19 09:00 LSK PCB-1016/1242[12674-11-2/53469-21-9]^ <0.48 ug/L 1 0.48 0.50 9331022 EPA 608.3 11/04/19 09:00 LSK PCB-1221[11104-28-2]^ <0.43 ug/L 1 0.43 0.50 9331022 EPA 608.3 11/04/19 09:00 LSK PCB-1232[11141-16-5]^ <0.50 ug/L 1 0.50 0.50 9331022 EPA 608.3 11/04/19 09:00 LSK PCB-1248[12672-29-6]^ <0.45 ug/L 1 0.45 0.50 9331022 EPA 608.3 11/04/19 09:00 15K PCB-1254[11097-69-1]^ <0.43 ug/L 1 0.43 0.50 9331022 EPA 608.3 11/04/19 09:00 LSK PCB-1260[11096-82-5]^ <0.47 ug/L 1 0.47 0.50 9331022 EPA 608.3 11/04/19 09:00 LSK Toxaphene[8001-35-2]^ <0.48 ug/L 1 0.48 0.50 9331021 EPA 608.3 11/04/19 09:00 LSK Surrogates Results PE ,Spike L v/ 910 Rec %Rec Limits 6atc(/ Method Analyzed & notes 2,4,5,6-7Z7'IX 0.77 1 1.00 77 96 38-142 9131022 EPA 608.3 11/04/19 09:00 LSK 2,4,5,6-TCMX 0.83 1 1.00 83% 38-142 9131021 EPA 608.3 11/04/19 09:00 LSK Decachlorobiphenyl 0.50 1 1.00 50% 34-159 9131022 EPA 608.3 11/04/19 09:00 LSK Decachlorobiphenyl 0.63 1 1.00 63% 34-159 9131021 EPA 608.3 11/04/19 09:00 LSK FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 6 of 23 ICe.61011 —CD) www.encolabs.com ANALYTICAL RESULTS11 Description: CAT Sanford Outfall 1 Lab Sample ID:CC18256-01 Received: 10/31/19 16:00 Matrix: Water Sampled:10/30/19 09:50 Work Order:CC18256 Project: Caterpillar(Sanford)Stormwater Sampled By:Mike Outlaw Metals by EPA 200 Series MethodsII A-ENCO Cary certified analyte[NC 5911 Analvte ICAS Numberl Results Flaq Units DF MDL POL Batch Method Analyzed By Notes Copper[7440-50-8]^ <8.00 ug/L 5 8.00 50.0 9K06020 EPA 200.7 11/08/19 13:14 JDH Lead[7439-92-1]^ < 15.5 ug/L 5 15.5 50.0 9K06020 EPA 200.7 11/08/19 13:14 JDH Zinc[7440-66-6]^ 168 ug/L 5 22.0 50.0 9K06020 EPA 200.7 11/08/19 13:14 JDH Classical Chemistry ParametersII A-ENCO Cary certified analyte[NC 591.1 Analvte (CAS Numberl Results Flaq Units DF ]gyp` Batch Method Analyzed By Notes Total Suspended Solids^ 230 mg/L 12.5 31 31 9K01011 SM 2540D-2011 11/01/19 10:32 JAH [, Classical Chemistry Parameters I A-ENCO Jacksonville certified analyte[NC 442] Analvte (CAS Numberl Results Flaq Units DF MDL POL Batch Method Analyzed By Notes Oil&Grease(HEM-SGT)Non-Polar 11.8 mg/L 1 2.70 5.00 9K06014 EPA 1664E 11/07/19 15:50 SMA Material^ FINAL This report relates only to the sample as received by the laboratory,and may only be reproduced in full. Page 7 of 23 ( 1 — ---co ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN-OF-CUSTODY10775 Central Port Di 4810 Executive Patlt Court.Surt 111 : nv RECORD )1" --- A Woodwinds Industrial Ct. Orlando,FL 32824 Jacksonville,Ft.32216.6069 Car NC 27511 (407)820-5314 Fax(407)650-6945 (904)296-3007 Fax(904)296-6210 y, (919)46'7-3090 Fax(919)467-3515 www.encolabs.com Page of Chant Name Project Number Requested Analyses Requested Turnaround Atlantic Environmental Associates(ATO2S) [none] a Times Address Project Name/Desc Note.Rush requests sut4ect to 2483 Reliance Ave. Caterpillar(Sanford)Stammer acceptance by the facility CtlyiSTiZip PO Cl Billing into Apex, NC 27539 (.9 , CO Cl ...- Standard • Tat Fax Reporting Contact 0 0 eN (919)387-1269 Candice Moore CID ... Expedited Sampler(s) ay.Affiliab.on Ttin0 Billing Contact MIO0 A CO tie fil i Kt- ni 1 A til fiff) Debbie Behnke-Outlaw Lao tairq/Zt)ttO s 0 s nature Site Li9iitioniittne Ze COO CO vt to 0,4 ai YMTOrtft 2 2 le) (iD o a f.-) €106-a1-81zi-',/‘ Preservation(See Codes)(Combine as meet.,leery) Coilectic, Matrix Total*of item 4 Sample ID Field Identification) Geilerhon Dare Trn,-, Camp,Grab isee codes) Containers - ' Sample Comments ,.. ,CAT Saftrd°Wall r - 1 IX() G ma .9 x x x xx x x CAT Sanford Outran 1ALA 9 X X X X X X ..... X ......_ CAT Sanford Outran WA 9 X X X X X X_ X1 _ CAT Santod Outfail WA 9 X . X X X X X X CAT Sanford Outran WA 9 X X X_ _ X X X X . _ 4..... _ ..._ _ . . . ,.. I- -1,-, ..._. _a — ---i , , 1 ., I , 1 <--Total#of Containers Sample Kit Prepared By Batfime Ref Pile/Time Fle,-eivect By / DaterTime 17/091; c.„.. :Special Reporting Requirements saing• s DaterTime t--owed'iy Date/Time -,,V A 5 A) Relinquished By Data/Time R- ived By Datenirrie CO 6e r f y 1. v Cooler 4's&Temps on Receipt . Condition Upon Receipt C.-ZOO - C-1 472 )( Acceptable Unacceptable tA CO OW-Groundwater SO.-Soil OW-Drinking Water SE-Sediment SW-Surface Water Wei-Wastewater A-Air 0-Other(detail in comments) Preservation:I-Ice 14-110 N-HNO3 S-H2SO4 NO-NaOH 0-Other(detail in comments) Note Al samples submitted to ENCO Labs are in accordance with the terms arid conditions hated on the reverse of this form,unless prior written agreements exist Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form,please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-stormwater-gps Permit No.: N/C/6/0/3/0/0/0/0/ or Certificate of Coverage No.: N/C/G/0/d o/ /q/7/ Facility Name: Cev tYv i((�t� County: Lei Phone No. I i`f- Sao- I Inspector: �,-, -'taCN(..r Date of Inspection: 16,3 0 Time of Inspection: 1 `[S Q v� Total Event Precipitation(inches): Ot I - All permits require qualitative monitoring to be performed during a"measurable storm event." A"measurable storm event"is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period,and the permittee obtains approval from the local DEMLR Regional Office. —I By this signature, I certify that this report is accurate and complete to the best of my knowledge: t1 (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. 1 Structure(pipe, ditch, etc.): 61 i c 1 Receiving Stream: I I or CK-edC Describe the industrial activities tha occur within the outfall draiir ge area: Qc,✓' ,-k- Jo a A t1, 5 a o c „�� mom,--� 'r��t 14- Page 1 of 2 SWU-242,Last modified 06/01/2018 2. Color: Describe the color of the discharge using basic colors (red,brown,blue,etc.)and tint (light,medium, dark) as descriptors: C,\.e — 1 J 3. Odor: Describe any distinct odors that the discharge may have(i.e., smells strongly of oil,weak chlorine odor, etc.): p d\a 4. Clarity: Choose the number which best describes the clarity of the discharge,where 1 is clear and 5 is very cloudy: 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge,where 1 is no solids and 5 is the surface covered with floating solids: 1 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge,where 1 is no solids and 5 is extremely muddy: 1 0) 3 4 5 7. Is there any foam in the stormwater discharge? 0 Yes l► No. 8. Is there an oil sheen in the stormwater discharge? °Yes ?i► No. 9. Is there evidence of erosion or deposition at the outfall? Q Yes d No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe a ifvy� Note: Low clarity,high solids, and/or the presence of foam,oil sheen,or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242,Last modified 06/01/2018