WQ0001489_Residual Annual Report 2015_20160301

1 � ,
• 1
UNITED STATES MARINE CORPS
MARINE CORPS AIR STATION
POSTAL SERVICE CENTER BOX 8003
CHERRY POINT, NORTH CAROLINA 28533-0003
IN REPLY REFER
5090/07202
LN
February 25, 2016
North Carolina Department of Environment
and Natural Resources
Division of Water Resources 4ED
Information Processing Unit MAR 0
1617 Mail Service Center 201-
Raleigh, NC 21699 �� �Rt�1AT/0JV�� iU
SUBJECT: TREATMENT AND LAND APPLICATION OF RESIDUALS sl�U�jT
Marine Corps Air Station (MCAS) Cherry Point submits the,
enclosed original and two (2) copies of our 2015 Treatment and Land
Application of Residuals .Report for permit WQ0001489. RECEIVEDINCDEQIDWR
During the 2015 reporting year, 233.71 dry tons were 104 2 2016
applied on 90.31 acres on Sites 1 through 3 and 7 of our ten
permitted application sites that encompass 417 total acres Non -Discharge
Permitting Unit
For additional information, please contact Mr. Timothy Lawrence
of the Environmental Affairs Department at [phone].
Sincerely,
i G .' W . D ORD \
Enviro e to Affairs Officer
By direction of
the Commanding Officer
Enclosure: 1. 2015 Annual Land Application of Residuals Report
Copy to: EPA Region 7, Biosolids Center

2015 ANNUAL SLUDGE REPORT PACKAGE.ORDER
1.the ACF
2.the RSSF
3. the MFLSF
4.the FSF
5. Lab Report (3 copies)
a. the Residuals lab report (general chemistry)
b. the TCLP lab report
6. the PVRF
7. the PVRF.Supporting Documents (Lime Stabilization): Lab
"Analysis Bench Sheets
8. the Soils,test lab report (3 copies)
9. the Triennial Groundwater Monitoring (3 copies)

ANNUAL LAND APPLICATION CERTIFICATION FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit#: WQ0001489 County: Craven Year: 2015
Facility Name (as shown on permit): US Marine Corps -.Cherry Point
Land Application Operator: Patricia T. Davis Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the past calendar year?
X 'Yes No If No; skip Part A, and Part Band. proceed: to the certification. Also, if residuals were
generated but not land applied, please attach an explanation- on how the residuals were handled.
Part A:
Part B:.:
Facility was. compliant during calendar year 2015 with all conditions of the land application permit
(including but not limited to items 1.-12 below) issued by the. Division .of Water. Quality. X : Yes D No
If no please, provide a: written description why the facility :was not compliant,. the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites:
2: Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in:the permit.
3. Annual soils analysis. were performed on each site, receiving residuals during the.past calendar year and three
(3) copies of laboratory results, are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6.1he. facility. did not exceed any of the Pollutant Concentration Limits in Table l :of 40 CFR Part.503.13 or the
Pollutant. Loading Rates in Table 2 of 40 CFR part 503.13 (applicable. to 40 CFR Part 503.regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with'(' plicable to 40 CFR:Part 501regulated facilities).
8. All operations and maintenance requirements .in the permit were, complied .with or, in -the case. of a deviation,
prior authorization was received from the Division of Water Quality.
9.: No: contravention of Ground. Water Quality Standards occurred at a monitoring well or explanations, of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No. runoff of residuals from the application sites onto adjacent property .or. nearby surface waters has .occurred.. .
12. All buffer requirements as specified on the permit were maintained during each application:of residuals.
"I certify, under penalty of law, that the above information -is, to the best of my knowledge and belief,�irue,
accurate, and complete. -I am aware that.there are significant penalties for submitting false information, .
including the possibility of fines and imprisonment'for knowin violations.":.
G.W.Radford, Environmental_ Affairs Officer o�Q
Pe ttee Name and Title pe or print) Signature o Pftin
ee by Direction: Date
of the Comm Officer.:
Signature of Pr7Permittee)
r* Date Signature of Land Applier Date':
(if different fro (if different from Permittee: and Preparer)
*. Preparer is defined in 40 CFR:Part 503.0:(r)
DENR FORM.ACF (5/2003)

RESIDUAL SAMPLING SUMMARY FORMS

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001489 Laboratory: 1) PACE Analytical Services, Inc.
Facility Name: US Marine Corps - Cherry Point 2) .
NPDES # or
WQ#:
NC0003816
WWTP Name: USMCAS - Cherry Point WWTP
Residual Analysis Data
3)
4)
5)
Sample or
Composite Date
1/8/15
4/9/15
7/8/15
10/19/15
Percent Solids
2
2.4
1.6
0.09
Arsenic
0
ND
0
ND
0
ND
0
ND
Cadmium
0.012
0.017
0.016
0
ND
Chromium
0
ND
0
ND
0
ND
0
ND
Copper
860
961
750
1700
Lead
0
ND
0
ND
0
ND
0
ND
Mercury
0
ND
0
ND
0
ND
0
ND
tv
Molybdenum
0
ND
0
ND
0
ND
0
ND
Nickel.
43.2
99.6
35.8
0
ND
Selenium
0
ND
0
ND
0
ND
0
ND
Zinc
626
682
569
1930
Total Phosphorus
31100
39500
50600
142000
TKN
45200
75700
66300
217000
Ammonia -Nitrogen
680
12300
11000
135000
Nitrate and Nitrite
5190
0
ND
1 1300
30100
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
sig " ant penalties for su 'tting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Prepare Date
DENR FORM RSSF (5/2003)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001489 Laboratory: 1) PACE Analytical Services, Inc.
Facility Name: US Marine Corps - Cherry Point 2)
NPDES # or .NC0003816 3)
WQ#:
4)
WWTP Name: USMCAS - Cherry Point WWTP 5)
Residual Analysis Data
Sample or • o
®-
-----
-
••
omomomoo����
_EEff#T1TFW3=omo�omom����
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified !ersonnel properly gathered and evaluated the information submitted. I am aware that there are
Sig ' i ant penalties for sub mi g false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer Date
DENR FORM RSSF-B (5/2003)

METALS FIELD LOADING SUMMARY FORM

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 108.206496
Permit #: WQ0001489 Cation Exchange Capacity (non 503 only):
Operator: Patricia T. Davis Owner: - US Marine Corps - Cherry Point
Acres Used: 44.94 Acres Permitted: 44.94 Site #: 1 Field #:
Residual Analysis' Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1
4/9/15
2
4/9/15
3
4/9/15
_.4j
4/9/15
1516
4/9/15
7/8/15
7
7/8/15
8
7/8/15
9
7/8/15
10
10/19/15
11
12
% Solids
2.4
2.4
2.4
2.4
1 2.4.
1.6
1 1.6
1.6
1.6
0.09
Arsenic
0
0
0
0
0
0
0
0
0
0
Cadmium
0.017
0.017
0.017
0.017
0.017
0.016
0.016
0.016
0.016
0
Chromium
0
0
0
0
0
0
0
0
0
0
Copper
961
961
961
961
961
750
750
750
750
1700
Lead
0
0
0
0
0
0
0
0
0
0
Mercury
0
0
0.
0
0
0
0
0
0
0
Molyb-
denum
0
0
0
0
0
0
0
0
0
0
Nickel
99.6
99.6
99.6
99.6
99.6
35.8
35.8
35.8
35.8
0
Selenium
0
0
0
0
0
0
0
0
0
0
Zinc
682
682
682
682
682
569
569
569
569
1930
Total
Phos-
horus
39500
39500
39500
39500
39500
50600
50600
50600
50600
142000
Annual Heavy Metal Field Loadings (Calculated in.lbs/acre):
y
1
2-1
31
41
L.5]6
j
1 71
L.8j9
10
1 11
12
� o
CD '� d
o'
0.2806
0.2058
0.2325
0.2038
0.2332
0.2392
0.2532
0.2512
0,2392
0.2692
0
Arsenic
0
0
0
0
0
0
0
0.
0
0
0
0
0
Cadmium
1E-05
7E-06
8E-06
7E-06 •
8E-06
8E-06
8E-06
8E-06
8E-06
0
0
0
7E-05
Chromiurr
0
0
0
0
0
0
0
0
0
1 0
0
0
0
Copper
0.5393
0.3955
0.4469
0.3916
0.4481
0.3588
0.3798
0.3768
0.3588
0.9154
0
0
4.611
Lead
0
0
0
0
0
0
0
0
0
0
0
0
0
Mercury
0
0
0
0
0
0
0
0
0
0
0
0
0
Molyb-
0
0
0
0
0
0
0
0
0
0
0
0
0
denum
Nickel
0.05591
0.041
0.0463
0.0406
0.0464
0.0171
0.0181
0.018
0.0171
0
0
0
0.3006
Selenium
0
0.
0
0
0
0
0
0
0
0
0
0
0
Zinc '
0.3827
0.2807
0.3171
0.2779
0.318
0.2722
0.2881
0.2859
0.2722
1.0393
0
0
3.7342
Total
Phos-
22.167
16.256
18.367
16.098
18.42
24.205
25.624
25.422
24.205
76.464
0
0
267.23
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to, assure that qualified personnel properly gathered and evaluated the
information submitted. I am a re that there are significant penalties for submitting false information,
incl d' g he possibility of fi a and im isonment for knowing violations"
Signature of Land Appli r Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 59.627664
Permit #: WQ0001489 Cation Exchange Capacity (non 503 only):
Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point
Acres Used: 20.80 Acres Permitted: 23.40 Site #: 2 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
1
1/8/15
2
1/8/15
3
1/8/15
4
1/8/15
5
1/8/15
6
1/8/15
7
L.8J
9
16
11
12
% Solids
2
2
2
2
2
2
Arsenic
0
0
0
0
0
0
Cadmium
0.012
0.012
0.012.
0.012
0.012
0.012
Chromium
0
0
0
0
0
0
Copper
860
860
860
860
860
860
Lead
1 0
0
0
0
0
0
Mercury
0
0
0
0
0
0
Molyb-
denum
0
0
0
0
0
0
Nickel
43.2
43.2 .
43.2
43.2
43.2
43.2
Selenium
0
0
0
0
0
0
Zinc
626
626
626
626
626
626
Total
Phos-
horus
31100
31100
31100
31100
31100
31100
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
0
1
2
3
4
5
6
7
8
9
10
11
12
CD
a
o
0.5528
0.4374
0.5067
0.3002
0.55
0.5196
0
0
0
0
0
Arsenic
0
0
0
0"
0
0
0
0
0
0
0
0
0
Cadmium
1E-05
1E-05
1E-05
7E-06
1E-05
1E-05
0
0
0
0
0
0
7E-05
Chromitur
0
0
0
0
0.
0
0
0
0
0.
0
0
0
Copper
0.9509
0.7523
0.8714
0.5164
0.9459
0.8938
0
0
0
0
0
0
4.9307
Lead
0
0
0
0
0
0
0
0
0
0
0
0
0
Mercury
0
0
0
0
0
0
0
0
0
01
0
0
0
Molyb-
0
0
0
0
0
0
0
0
0
0
0
0
0
denum
Nickel
0.0478
0.0378
0.0438
0.0259
0.0475
0.0449
0
0
0
1 0
0
0
10.2477
Selenium
0
0
0
0
0
0
0
0
0
0
0
0
0
Zinc
1 0.6922
0.5476
0.6343
0.3759
0.6885
0.6506
0
0
0
0
0
0
3.5891
Total
Phos-
34.387
27.204
31.514
18.675
34.207
32.322
0
0
0
0
0
0
178.31
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure thatqualified personnel properly gathered and evaluated the
infor on submitted. I am aw a that there are significant penalties for submitting false information,
inr�#z&��J
g e possibility of fi s nd imprisonment for knowing violations"
"
Signature of Land Appli Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 55.124064
Permit #: WQ0001489 Cation Exchange Capacity (non 503 only):
Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point
Acres Used: 16.80 Acres Permitted: 16.80 Site #: 3 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
1
1/8/15
2
4/9/15
3
4/9/15
4
4/9/15
5
10/19/15
6
7
81
_af
11
12
% Solids
1 2
2.4
2.4
2.4
0.09
Arsenic
1 0
0
0
0
0
Cadmiuml
0.012
0.017
0.017
0.017
0
Chromiuml
0
0
0
0
0
Copper
860
961
961
961
1700
Lead
0
0
0
0
0
Mercury
0
0
0
0
0
Molyb-
denum
0
0
0
0
0
Nickel
43.2
99.6
99.6
99.6
0
Selenium
0
0
0
0
0
Zinc
626
682
682
682
1930
Total
Phos-
horus
31100
39500
39500
39500
142000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre): .
51
6
7
8
9
10
11
12
"a�
y
o'
0.6934
0.5987
0.5612
0.6612
0.7667
0
0
0
0
0
Arsenic
0
0
- 0
0
0
0
0
0
0
0
0
0
0
Cadmium
2E-05
2E-05
2E-05
2E-05
0
0
0
0
0
0
0
0
8E-05
Chromiurr
0
0
0
0
0
0
0
0-
0
0
0
0
0
Copper
1.1927
1.1507
1.0786
1.2709
2.6067
0
0
0
0
0
0
0
7.2995
Lead
0
0
0
0
0
0
0
0
0
0
0
0
0
Mercury
0
0
0
0
0
0
0
0
0
0
0
0
0
Molyb-
0
0
0
0
0
0
0
0
0
0
0
0
0
denum
Nickel
0.0599
0.1193
0.1118
0.1317
0
0
0
0
0
0
0
0
0.4227
Selenium
0
0
0
0
0
0
0
0
0
0
0
0
0
Zinc
0.8682
0.8166
0.7654
0.9019
2.9594
0
0
0
0
0
0
0
6.3115
Total
Phos-
43.13
47.297
44.332
' 52.238
217.74
0
0
0
0
0
0
0
404.74
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
infor on submitted: I am aw re that there are significant penalties for submitting false information,
incl ' g t e possibility of fi and imprisonment for knowing violations"
aj o - o?5 -/
Signature of Land App er Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0
Permit #: WQ0001489 Cation Exchange Capacity (non 503 only):
Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point
Acres Used: 0.00 Acres Permitted: 8.00 Site #: 4 ' Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
Phos-
phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
1
1
1
1
r"000�000000000
�0000000000000
• •
000000�000000
�Q0�0000000�00
�Q0��000000�00
�0�00000000000
�0000000000�00
®0000000000000
'•
1
1
1
1
1
1
1
1
1
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
g
tion submitted. I am aw athat there are significant penalties for submitting false information,
g he possibility of fin d imprisonment for knowing violations"
e of Land Appli r Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0
Permit #: WQ0001489 Cation Exchange Capacity (non 503 only):
Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point
Acres Used: 0.00 Acres Permitted: 24.00 Site #: 5 Field #:
Residual Analysis Data (Heavy Metals and Total.Phosphorus use mg/kg, % Solids use Raw Percent #):
N
'I
on,
MEMNON
a
U
i
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
E
l
w
n
o
n,
n,
11
1
I
N
�000�00000�000
�000000000�000
�0000000000000
. -
�0000000000�0
�0000000000000
�0000000000000
�000�000000�00
�00000000�0000
®0000000000000
Total
Phos-
phorusEEMENEEMENEEN
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered .and evaluated the
inform ion submitted. I am aware that there are significant penalties for submitting false information,
incl i gthe possibility of fines a imprisonment for knowing violations"
a �Sl6
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0
Permit #: WQ0001489 Cation Exchange Capacity (non 503 only):
Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point
Acres Used: 0.00 Acres. Permitted: 8.10 Site #: 6 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
NO
moo
Total
Phos-
phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
10
ON
0
113llU
mail
omen
�00000000�0000
�0000�0000000�
•
0�0000000000�
. •
000000000000�
�0000�0�00�00�
�000�0000�0000
�0000000000000
®0�00000000000
Total
Phos-
phorusEENEENEENEENE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance .with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
issibility of fines d imprisonment for knowing violations"
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 10.748592
WQ0001489 Cation Exchange Capacity (non 503 only):
Patricia T. Davis Owner: US Marine Corps - Cherry Point
7.77 Acres Permitted: 35.00 Site #: 7 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
' •M
..ENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
�0000000000000
�0000000000000
^a
0000000000000
.. • •
1
00000000000
1 '
�000000�000000
010000000000000
�00000000�0000
�000000000�000
®�00000�00000�
Total
'•
•
1
1
1
1
1
1
1
1
1
1
1
•
. •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
infor Flon submitted. I am awarepat at there are significant penalties for submitting false information,
incl • g Pe possibility of fines a imprisonment for knowing violations"
Signature of Land Applier Date
See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0
Permit #: WQ0001489 Cation Exchange Capacity (non 503 only):
Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point
Acres Used: 0.00 Acres Permitted: 110.00 Site #: 8 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids -use Raw Percent #):
on,
Total
' .M
•.ENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
logo
I,
I'm
�0000000000000
�0000000�0�000
�00�0000000000
• • • •
0000000�00000
�0000000000000
�000000000�00�
�000�0000�0000
�0000000000000
®000000000�000
Total
•
1
1
1
1
1
1
1
1
1
1
1
1
1
• •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware at there are significant penalties for submitting false information,
inclu t e possibility of fines,pfi impri onment for knowing violations"
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0
Permit #: WQ0001489 Cation Exchange Capacity (non 503 only):
Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point
Acres Used: 0.00 Acres Permitted: 28.00 Site #: 9 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
phorusENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
•
�0000000�00000
�000000000000�
000�0�00�000�
. • • -
000000�000000
�000000000000�
�00000000�0000
�0000�00000000
�0000�00000000
®0000000000000
Total
Phos-
_phorusEENEEMENEEMEN
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
inclu t possibility of fines imprisonment for knowing violations"
Signature of Land Applier 11'Date
* See bottom'of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0
Permit #: WQ0001489 Cation Exchange Capacity (non 503 only):
Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point
Acres Used: 0.00 Acres Permitted: 119.00 Site #: 10 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
_
II]
ME
MO,
VIM
•.
•M
phorusENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
193
-
IN.
�00000��00�000
�000000000�000
•
0000000�00000
. . •
0000000000000
�0000000000000
�0000000000000
�000000000�00�
�0000000000000
®00�0000��0000
Total
Phos-
i
o
�.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
in
cl i t possibility of fin nd imprisonment for knowing violations"
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003),

FIELD SUMMARY FORMS

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A _BLANK OR BOX WHEN NOT APPLICABLE. -
Facility Name: US Marine Corps - Cherry Point Permit #: WQ0001489- Annual Dry Tons Applied: 108.21
Owner: US Marine Corps-- Cherry Point Operator: Patricia T. Davis Cation Exchange Capacity (non 503):
Site #: 1 Field #: Acres Utilized: 44.94 Acres Permitted: 44.94
�1.
Specify
Totals
Per .
Acre
%
Solid
s
Dry Tons
Per Acre -
Residual
Sources
(Summarize)
tte
Cond.
. Dry,
Wet,
Inches
Precip.
Past 24
Hrs..
Appli-
cation
Meth-
od*
Vold-
tili-
zation
Rate**
Miner-
ali-
zation
.:Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and -
Nitrite
PAN 1
.
PAN 2
Must Select
Crop 1 or Crop
P - P
2
Cu.Yd.
Report
Totals
in Gal:
Crop 1
Crop 2
5/7/15
72000 •
1602.1
4.2
0.290598131
WWTP.
dry
0
S
0.5
0.2
75700
12300
0
10.5673
0
.Fescue
1
5/14/15
12000
1602.1
-3.08
0.205771963
WWTP
dry
0
S
0.5
0.2
75700
12300
'0.
7.74937
0
Fescue
2
5/28/15
72000 .
1602.1'
-"3.48
0.232495594
WWTP'
dry"
0 :.
S
0.5-.
0.2
75700
.12300
0
:8.75578
. 0
Fescue
3"
6/8/15
72000
1602.1
3.05
0.20376769
WWTP
dry
0
S
0:5
0.2
75700
..12300
0
7.67389.
0
Fescue.
4
6M/15 1
72000
1602.1
3.49
0.233163685
WWTP .."
dry
0
S
1 0.5
0.2
75700
1 12300
0
8.78094
0 ""
"Fescue
5
:7/27/15
72000
1602..1
3.58
0.239176502
WWTP.
dry
0
S.
0.5
0.2'.66300
11000
1300
8.54338
0
Fescue
6.
8/24/15
72000
1602.1
3.79
0.253206409
WWTP
dry
0
S
0.5
":0.2
66300"
1f000
1300
9.04453
0
Fescue-
7
9/21/15
72000
1602.1 1,336
0.251202136
WWTP
dry
0
S
0.5
0:2
66300
11000
1300..
"8.97294
0
Fescue
8,
10/14/15
72000
1602.1
3.58
0.2391765.02
WWTP
dry
0
S
0.5
6.2 ..
66300
11000
1300
18.54338
0 .. •
Fescue
9
10/26/15
72000.
1602.1
4.03
0.269240587
WWTP
dry
0
S
0.5.
0.2
1 217000
135000
30100
16.1.3869
0
Fescue
10
0
0
S
0:5
0.2
0.
p 0
11
0
0
S
0.5
0.2
0
0
12
TOTALS:-16021
` ` i
As
Cd
Cr
Cu.
Pb .
H
Mo
Ni
Se
Zn
P
PAN 1
: PAN 2
Lime "A
lied
Annual lbs/acre
0
7.1E-05
0
4.611
0
0
0
0.3006
0 .
3.73416
267.228
140.018
0
Date."
. lbs/ac
Current:Cumulative lbs/ac
2 7 4 7 4 7 14 7» 0.586338995 .855 8 0" 66.993 . 3228 0.2 071 0 6.98903 .0.6 8 . 3 6 > ......:;.:<.> :,::«:::,;:;...:".
0.586338995 2.85571 0 62:382 4.73228 0.24071 0 6.68843 0.67 77.7034 < <><> <` >> >< ...... : =>
6 34 /A 1 3 2 1 4 8 24 8
3 N 3 8 67 . 5 N/A 37 9 9
" .;:.::..;,<:> 2 .....
50
Prior Years Cumulative lbs/ac
Permitted C. P. L. R. ***
Permit PAN Limit 1 st/2nd Crop«':>`:;...;:
"I certify, under penalty of law, that this document was prepared under my direction or supervision -in accordance With -a system
designed to assure that qualified. personnel properly -gathered and evaluated the information submitted. I am aware that there are
sig c t penalties for muting false information, including the possibility of fines and. imprisonment for knowing violations"
*Application Method: S - Surface, IN .Injection, INC- Incorporation-
S' nature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - LO .
***.
C.P.L.R.: Cumulative Pollutant Loading Rate
The RSSF Data and the Dry Tons Per "Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie., FSF row # 1 to MFLSF column # 1.
„ DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Marine or - Cherry Point Permit #: WQ0001489 Annual Dry Tons Applied: 59.63
Owner: US Marine Corps - CherryPoint Operator: Patricia T. Davis Cation Exchange Capacity (non 503):
Site #: 2 Field #: Acres Utilized: 20.80 - Aerie's Permitted: 23.40
o
„ o
Q >?>
S ecif ..
Totals
Per
Acre
%
Solid
s
Dry: Tons,Crop
Per Acre
Residual,:C
Sources
(Summarize)
ite
Cond.
Dry;
Wet-'
Inches
Precip.
Past 24
; Appli-
cation
Meth =
od*
Vola-
_ tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen .
Ni-
trate
and .
Nitrite
PAN I.
PAN 2
Must Select
P 1 or. Crop
.: 2
Gal
Cu.Yd.
Report
Totals
in Gal.Hrs.
Crop I
Crop.2
1/16/15
72000
3461.5.
3.83
0.552845769
WWTP
dry.
0
S
0.5
0.2
45200
680
5190
15.9596
0
Fescue
1
1/21%15
_ 72000
3461.5
3.03
0.437368846
WWTP
dry
0
S
0.5
0.2
45200
680
5190.
12.626
0
Fescue
2
1/26/15
72000
3461.5
3.51
0.506655
WWTP
dry
0
S
0.5
0.2
45200-
680-.
5190
'14.6261
0
Fescue
3
2/4/15
12000
3461.5
2.08
0.30024
WWTP
dry
0.
S
0.5
0.2
45200
-680
5190
8.66733
0
Fescue
4
N9/.5,
72000
3461.5
3.81
0.549958846
WWTP
dry
1
S
0.5
0.2
45200
680
5190 :
15.8762
0
5
3/3/15
1_ 72000
3461.5
3.6
0.519646154-
WWTP
'dry
2
S
0.5
0.2
45200
680
5190-
:15.0011
0 -
6
0
0
S
0:5
02
5190
0
0
7
0
0
S
0.5
0:2
5190
0
0
8
0
0
S
0.5
6.2"
5190
0
0
9
0
0
S
0.5
0.2
5190
0
0
10
0
0
S
0.5.
0.2
5190
0.
A
11
p_.
...
0
S
0.5
0.2
5190
0
0
12
TOTALS:
20769
'::
As
Cd
Cr
Cu
Pb
Ii
Mo
Ni
Se
Zn
P
PAN 1.
PAN 2
Lime Applied
.
Annual lbs/acre
0
6.9E-05..
0
4.93075
0 -
0
0 :.
0.24768
0
3.58913
178.31
82.7563
0
Date
lbs/ac
Current.Cumulative lbs/ac:
0.963097176 : 5.04067 0 98.9334 1 .9907 0.29352. 0 9.87199 0.54 127.662 > <><> < '>>'<<<:
9
24 1 4 24 0.963097176 5.0406 0 94.0027 19.9907 0.293520 9 6 3 0.5 1 .073 '<>`">� `:<'><;<:>:.'
36 34 N/A 1338 267 15 N/A 374 89 2498
>::> » > >:::::.........:::.::::;;::.;;;>;;;:::::;;;;>;......:;;:.>;>;:;;;;;;;;,;;;;;:,:.; .:.;..,::.. ;:;;;;>;:.;:;<.;:;.:;;: . 250
Prior Years Cumulative lbs/ac
Permitted C. P. L R ***
Permit PAN Limit l sb nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified. personnel properly gathered and evaluated the information submitted. I am aware that there are
signiic nt penalties for sub 'ttmg false information, includingthe possibility of fines and. imprisonment for knowing violations. "
a6 A� *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signatur of Land Applier Date **Volatilization Rate: Surface-- 0.5, Iniection/Incorporation - LO
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The.FSF, and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered. on the identically numbered FSF row to properly complete the metals equations. ie. FSF, row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL LAND -APPLICATION FIELD SUMMARY FORM_
PLEASE_ MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. .. .
PLACE A "N/A" IN A..BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Marine Corps - Cherry Point Permit #s WQ0001480 . Annual Dry Tons Applied: - 55.12
Owner: US Marine Corps - Cherry Point Operator: Patricia T. Davis Cation Exchange Capacity (non 503):
Site #:: 3 Field #: Acres Utilized: 16.80 Acres Permitted: 16.80
o
„
Fill Specify
Totals
Per
Acre
%
Solid
s
Dry Tons
Per Acre
Residual
Sources
(Summarize)
site
Cond.
Dry,
Wet,
Inches
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
melon
Rate**
Miner-
ali-
zation
. Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and . .
Nitrite
PAN 1
PAN 2
Select
Crop 1 or Crop
p p
2
G�
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
4/6/15.
-72000
m 4285.7
3.88
0.693411429
WWTP
dry
0
S
0.5
0:2
45200
680
5190 .
20.0174
-0
Fescue
1
4/13/15
72000
4285.7
3.35
0.598692857
WWTP
dry
0
S
0.5
0.2
75700
12300
0 '
22.5468
0
Fescue
2
4/23115
72000
.4285.7
3.14
0.561162857
WWTP
dry
0
S
0.5
-0.2
75700 .
12300
0
21..1334
.0
Fescue
3
5/4/15
72000
4285.7
3.7
:0.661242857
WWTP
dry
.0
S
0.5
0,2
75700
.12300.
0
24.9024
, 0
Fescue
4
12/9/15
72000
4285.7
4,29 1
0.766684286
WWTP
dry
0
1 S.
-0.5
0.2
217000
135000
1 30100
174.804
0
Fescue
5
0.
0.
S ..
0.5
0.2
0
0
6'
0
0
S
0.5
0.2
0
0
7
0
0
S
0.5
0.2
0
0
8
0
0
S
0.5
0.2
0
0 -
9
0
'0
S
0.5
0.2
0
0
10
0
0
S
0.5
0.2
0
0
S
0.5
0.2
0
0
12
TOTALS:
21429
><>`>>
As.
Cd
Cr
Cu
Pb _
H
Mo
Ni
Se
Zn .
P
PAN 1
PAN 2
Lime A
lied
Annual lbs/acre
0
7.9E-05
0
7.29955
0
0
0 :
0.42267
0
6.31153
404.735
263.404
.0
Date
_ lbs/ac
Current: lbs/ac.
:
0.3243564870
3.623 7
0
89.6773
5.42948
.2 312
0 3
0.223
9 .59505
0.35:
• 1..
105 3
..<;:.::<:,,::`:;:><;»»'`>'>
250
Prior Years Cumulative'lbs/ac
0.324356487
3.62299
0
82.3778
5.42948
.23 12
0 33
0.223
9 .17238
0.35
98.9988
.
Permitted C. P. L.: R.
36
34
N A
/
1338
267
1 5
N/ A.
374
89
2 498
Permit PAN Limit 1 st/2nd Crop..........
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified: personnel properly gathered and evaluated the information submitted. I am aware that there are
signi n penalties for sub ' 'ng false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method:. S - Surface, IN - Injection, INC - Incorporation
Signature f Land Applier Date **Volatilization Rate: Surface:- 0.5, Iniection/Incorporation -1:0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** ,The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The:FSF and MFLSF are mathematically linked so this -information needs -to be entered into
the same numbered column on the MFLSF as is entered: on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column ##.1.
DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM:
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH. APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE:
Facility Name: US Marine Corps - Cherry Point Permit #: WQ0001489 Annual Dry Tons Applied: 0.00.
Owner: 'US Marine. Corps - Cherry Point.: Operator: Patricia T. Davis Cation Exchange Capacity (non 503):. .
Site t 4 Field #: Acres Utilized: ; 0.00 Acres, Permitted: 8'.00
r.
o _ .
Speciffy
Totals
Totals
Per
Acre
%
Solid
s
Dry Tons.
Per Acre
Residual
Sources ;
(Summarize)
Site .
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation.
Meth-
od *
Vola-
tili-
zation .:zation
Rate **
Miner-
ali-
Rate
-.
- TKN
Ammo
nia-
Ni-
trogen
Ni-
trate.
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
2
G�
Cu.Yd.
Report
Totals
in, Gal.
Crop 1[Crp
2
0
0
WWTP
dry
.0
S
0.5
0:2.
45200
680
5190
0
0
Fescue
1
0
0
S
0.5
0.2
5190
0
0
Fescue
2
0
0
S
.0.5-
0.2
5190
0
0
Fescue
3
0
0
S .:
0.5
0.2
=
5190'
0
0
Fescue
4
0
0.
S. ..
0.5
0:2:
5190
0
0.
5
0
0
_
S
0.5
..- 0.2
5190
.0.
0
6
0
0
S
0.5
0.2
5190
0
0
7
0.
0
S
0.5
0.2
5190
0
0
8
0
0
S
0.5
0.2
5190
0.
0
9
0
0
S
0.5
0.2
5190
1 0
0
10
0
0
S
0.5
0.2. _
5190
0
0_ _
11
0
0
S
0.5
0.2
5190
0
01
12
TOTALS:.
0:::::`:::::;
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se.
Zn
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre _.
0
0
0:
0
0
0;
0
0
0
0
0
0
0
Date
lbs/ac
Current Cumulative lbs/ac
0.339889659 3.31906 0 114.252 4.95525 :0:21454 1 0.223 11.4927 0.35 142.105
0.339889659 3.31906 0 114.252 4.95525 0.21454 1 0.223 11.4927 0.35 142.105
24 8
A 374 89 9 �2 15 N/
36 34N/A 1338 67
250
`
Prior Years Cumulative lbs/ac
C: P: L. ***
Permitted R.
P Limit 1 2tid Cro
Permit AN st/ P
"I -certify, under penalty of law, that this document was prepared: under my direction or supervision in accordance with asystem, -
designed to assure that qualified personnel properly, gathered and evaluated the information. submitted:. I am aware that there are.
sigm c t enalties for subn ng fal a information, including the possibility of fines and imprisonment for knowing violations:'
o�•/VI Application Method: S. - Surface, IN - Injection, INC - Incorporation
Signature df Land Applier . Date **Volatilization Rate: -Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.:. Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this: information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF-(5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN_ A BLANK OR BOX.WHEN NOT APPLICABLE.
Facility Name: US Marine Corps Cherry Point Permit #: WQ0001489 Annual Dry Tons Applied: 0.00
Owner: -US Marine Corps - Cherry Point Operator: Patricia T. Davis Cation Exchange Capacity (non 503):
Site #: 5 Field #: Acres Utilized: 0.00 Acres Permitted: - 24.00
o
(1) . �.
o
Q «>
Specify
Totals
-
Per .
Acre
%
Solid
s
Dry:Tons
Per Acre
Residual
Sources
(Summarize)
(Summarize)
ite
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation"
Meth-
od*
Vola-
tili-
� zation
Rate**
Miner-
ali- -"
zation
Rate
TKN
Ammo,
ma-
Ni-
trogen
Ni-
trate
and -
Nitrite
PAN 1
PAN 2
Must Select .
Crop 1 or Crop
p p
G�
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
.0.
0
WWTP
dry
0
S
0.5
0.2
45200
680
519.0
0
0
Fescue
1
0
0
S
0.5
0.2
0
0
Fescue
2
0
..0 .
S
0.5
0.2
0
0
Fescue
3
0
0
S
0.5..
0.2
0.
0
Fescue
4
0
01
S
0.5
0.2
0
0
Fescue
5
0:
0
S
0.5
0.2
-
0
0
Fescue
6
0
0
S
0.5
0.2
-0 -
0
7
.0
0.
S
0.5
0.2 -
0
0.
8
0
0
S
0.5
0.2
0
0
9
0
0
S
0.5
0.2
0
01
10
0
0
S
0.5 :
0.2
0
0
11
0 ..
0
S
0.5
0.2
0
0
12
TOTALS:.
0
< € '
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied .
Annuallbs/acre
0
0
0.
0
0
0
0-
0
0
0
0
0.
0
Date
lbs/ac::<:::.
Current: Cumulative lbs/ac
0.583796014 2.84326 0 53.8666 2.86497 0.22851 0.18 7.20884 0.33 61.7303 ;;',;;:
0.583796014 2.84326 0 53.9666 2.86497 0.22851 0.1 .2 4 1 8 7 088 0.33 6 .7303 »>>»»>«>>>'>»><>>
36 4 N 1 2 . 24
3 /A 338 67 15 N/A - 374 89 9 8
............
:........::::.... "' >
_;.
Prior Years Cumulative lbs/ac
Permitted- C. P. L. R. ***
Permit PAN Limit 1 st/2nd Crop
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
signi c :trn�lties for sub Ong false information, including the possibility of fines and imprisonment for knowing violations."
• 02 ' 075-/ *Application Method: S - Surface, IN - Injection, INC - Incorporation
ze,Signature Land Applier Date **Volatilization Rate: Surface- 0.5, Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
The RSSF Data, and, the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF_ and MFLSF are mathematically linked so this information needs -to be entered into
the same numbered column on: the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column #4.
OR FSF DENR FORM (/200 - 5 ) 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR=EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Marine Corps - Cherry Point Permit #: WQ0001489 Annual Dry Tons Applied: 0.00
Owner: US Marine Corps - Cherry Point Operator: Patricia T. Davis Cation Exchange Capacity (non 503):
Site #: 6 Field #: Acres Utilized: 0.00 Acres Permitted: 8.10
o
Q
Specifv
Per
Acre
Solid
s
Dry Tons
Per Acre
Residual
Sources
(Summarize)
SiteInches
Dry,
Wet,
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Crop 1 or Crop
P P
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
0
0
WWTP
S
0.5
0.2
45200
680
5190
0
0
Fescue
1
0
0
0
0
2
0
0
0
0
3
0
0
_.
0
0
4
0
0
0
0.
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
12
TOTALS:
0
>»
- As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
0
0
0
0
0
0
0
0
0
0
0
0
0
Date
lbs/k
»<
Current ent Cumulative lbs/ac
0 0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0
36 34 N/A1338 267 15 N/A 37424 89 98
250
'o Year Cumulative lbs/a Prior s v c
Permitted C. e P. L. R.***
Permit PAN Limit 1st/2 n d Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
signif a t p nalties for submit g false information, including the possibility of fines and imprisonment for knowing violations.
*Application Method: S -Surface, IN --Injection, INC -Incorporation
Signature of f2krdApplier Date **Volatilization Rate: Surface-- 0.5, Iniection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM_ .
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Marine Corps.- Cherry Point; Permit #: WQ0001489 . Annual Dry: Tons Applied: 10.75 .
Owner: US _Marine Corps - Cherry Point Operators Patricia T. Davis Cation Exchange Capacity (non 503):
Site.#:. 7 Field #: Acres Utilized: 7.77 Acres Permitted: 35.00
o �®
. o .
Q
Specify
Totals Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
lte
Cond.
Dry,
Wet,
.Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-.
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation .
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and .
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Cro
p p
2
Gala
Cu.yd.,
-_
Report
Totals
in Gal:
Crop 1
Crop 2
11/12/15
72000
9266.40927
3.58
1.383345174
WWTP
dry
0
S
0.5
0.2
217000.
435000
30100
315.403
0
Fescue
1
0
0
0
0
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0'
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0.
0
0
0
9
0
0..
0
0
0
0
ill,
0
0
:.
0
0,
12
TOTALS:
9266:409
'.' <:.-..
As '
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annual lbs/acre .
0
0
0
4.70337
.0.
0 .
0
0
0
5.33971
392.87
315.4031.
0
Date.
. lbs/ac
<:>:
Current Cumulative lbs/ac
4 2 447 4 1 2.73256 0.24012 0 1.43444 0.3 66.2665 >.` '>:::: ' <: <:>:>; % z:<:> ::>: > >
0.53048 .8 6 0 6.3 08
4 444. 0. 268 > : > :::;:';:'.z: ». .:: ;: >. ..... .
0.53048 2.84476 0 41.6074 2.73256 0.240120 7. 3 .0.3 6 9
36 34 N/A 1338 267 15 N/A 374 . 89 2498
. ...;::::::::<:;::::;::;;::;:::;:;:.::>:><;>:>:.:: > ......250
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***-
Permit PAN Limit lst/2ndCro P
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designe to assure that qualified personnel properly gathered and evaluated the information submitted. Tam aware that there are =
signif' t enalties for submit ' g false information, including the possibility of fines and imprisonment for knowing violations."
' 02 .Z5 *Application Method: S - Surface, :IN - Injection, INC - Incorporation
Signatu of Land Applies Date **Volatilization Rate: Surface -.0.5; Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK -FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. -
.Facility Name: US Marine Corps - Cherry Point Permit #: WQ0001489 Annual Dry Tons Applied: . 0.00
Owner: US Marine Corps - Cherry Point Operator: Patricia T. Davis Cation Exchange Capacity (non 503):
Site #: 8 Field #: Acres Utilized: 0.00 Acres Permitted: 110'.00
o
.0 C
o.
Q '
Specify
Totals
Per
Acre
%
Solid
s
Dry Tons
Per Acre.
Residual
Sources
(Summarize) •
ite
Cond.
Dry;.
Wet,
Inches
Precip.
Past 24
-Hrs.
Appli-
cation
Meth-
od*
Vola-
tili=
zation
Rate**
Miner-
ali-
zation
Rate
-TKN
Ammo;
ma-
Ni-
trogen
Ni-
trate .
and
Nitrite
PAN 1
PAN 2
Must Select:
Crop 1 or Crop
p p
2
Gal.
Cu.Yd.
Report
Totals
in Gal.:
Crop 1
Crop 2
0
0-
WWTP :
S
0.5
0.2 .
45200
680
5190
0
0
Fescue •
1
0
0
0
0
2
0
A
0
.0
3
0
0
0
0
4
0
0
0
0
5
0.
0
:.
0
0
6
0
0
0
0
7
0
0-
0
0
8
0.
0
0
0
9
0
0
0
01
10
0
0
0
0
11
0
0
0
0
12
TOTALS:
0
:` :_
As
Cd
Cr
Cu
Pb
gHR
Mo
Ni
Se
Zn .
-P
PAN 1
PAN 2
Lime A
liedAnnual
lbs/acre
0
0
0.
0
0
0
0
0
0
0
0
0
Date
lbs/ac
Current Cumulative lbs/ac
0 0 0:>:>:<::::..::.:::..:::.:.:.:.::::::.:..::.::.<...:::::::
0. 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0
36 34 N/A 1338 267 . 15 N / 374 89' 2498
A ..:..... :..:::::::........ .
...... .............................................._.............................................................. 250
PriorYears Cumulative
t ve lbs/ac z
Permitted_ C. P. L. °R. ***
Permit PAN Limit l st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a -system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. lam aware that there are
sign t penalties for sub ng false information, including the possibility of fines and, imprisonment for knowing violations:"
to *Application Method: S - Surface; IN - Injection,. INC - Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface:- 0.5, Iniection/Incorporation 1.0 .
***C.P.L.R.: Cumulative Pollutant Loadin' Rate
*** The RSSF Data: and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so. this information needs to be entered into
the same numbered column on the MFLSF as is -entered on the identically numbered FSF row to, properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF-
(5 /200 3)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Marine Corps - Cherry Point Permit #: WQ0001489 Annual Dry Tons Applied: 0.00
Owner: US Marine Corps - Cherry Point Operator: Patricia T. Davis Cation Exchange Capacity (non 503):
Site #:. 9 Field #: Acres Utilized: 0.00 Acres Permitted: 28-.00
o
+. o ..
cd
A
S eci
Totals
Per
Acre
%
Solid
s
Dry Tons
Per Acre
Residual
Sources
(Summarize)
ite
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo,
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 Crop
P or P
2
G�
Cu.Yd.
Report
- Totals
in Gal.
Crop 1
Crop 2
0
0
WWTP
S
0.5
0.2
45200
680
5190
0
0
Fescue
1
0
0
0
0
2
0
0
0
0
3
0.
0
0,
0
4
0
0
0
0
5
0
0
0
0-
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
9
0
1 0
0
10
0
- 0
0
-0
11
0
0
0
0
12
TOTALS:
0
<i>'<>'>>:
As
Cd
Cr
Cu
Pb
Hg
°Mo
Ni
Se
Zn
P
PAN 1
PAN 2.
Lime Applied
Annuallbs/acre
0
0
0
0
.0
0
0
0
0
D
0
0
-0.
Date
lbs/ac
Current Cumulative lbs/ac
0
0
0 0 0 0 0 0 1 0 0
0 0 0 0 0 0 0 0
N/A 1338 267 15 N/A 37 9
250
PriorYears Cumulative lbs/ac
0
0
Permitted C. P. L. R. ***
36
34
Permit PAN Limit 1st/ 2nd Cro P
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
signif a t p nalties for submitti alse infor ation, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of d Applier Date **Volatilization Rate: Surface - 0.5, Iniectionlncorporation - LO'
***C.P.L.R.: Cumulative Pollutant Loading Rate
****_ The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE- MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Marine Corps:- Cherry Point. Permit #: WQ0001489 - Annual Dry Tons Applied: 0.00
Owner: US Marine Corps - Cherry Point Operator: Patricia T. Davis Cation Exchange Capacity (non 503):
Site #: 10 Field #t- Acres Utilized: 0.00. Acres Permitted: 119.00
»
o
Z
o
Specify
Totals
Per
Acre
%
Solid
s
Dry Tons
Per Acre
Residual -
-
Sources
(Summarize)
ite
Cond.
Dry,
W et,
Inches
Precip.
Past 24
-Hrs.
Appli-
cation
Meth-.
' od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation-
- Rate
TKN
.
Ammo-
ma-
Ni-
tro,-en
Ni-
trate
and .
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
P .. P
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
0
0
WWTP
S
0.5
0.2
45200
680
5190
0
0
Fescue
1
0
0
0
0
2
0
0
0 ..
0
3
0
0
0
0
4
0
0
0
0
5
.0
0:
0
0.
6
0
..0
0 ..
0
7
0
0
-
0
0
8.
0
0
0
0
9
0
0
0
0
10
0
0
0 .::
0
11
0
0
0
0
1
12
TOTALS:
0
?<;;;
As
Cd
Cr
Cu
Pb
H
Mo _
Ni
Se
Zn-
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre.
0
0
01
0
R.
0
0
0 1
0
0
0
0
0
Date
lbs/ac
Current Cumulative lbs/ac
0 0 0 0 0 0. 0 0 0 0
0 0 0 0 0 0 0 0 0 0
36 34 N/A 1338 267 15 N/A 374 8 2498 : '>»>`>':'>::.:<_
9
250
Prior. Years Cumulative lbs/ac
Permitted C. R. ***
P. L.
Permit PAN Limit 1 st/2nd Crop
.1 certify, under penalty of law, that .this Aocument was prepared under my direction or supervision in accordance with a system
designell to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
signi C- t enalties for submittfalse information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S. Surface, IN Injection, INC - -Incorporation
Signature o , and Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 .
***C.P.L.R.: Cumulative Pollutant Loading Rate
The RSSF Data and the Dry Tons Perere are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into.
thesame numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column .# 1.
DENR FORM FSF (5/2003)

LABORATORY REPORT (3 COPIES)
1) RESIDUALS LABORATORY DRY WEIGHT TEST
2) TOXICITY CHARACTERISTIC LEACHING
PROCEDURE

` www.pacelabs.com
d
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SLUDGE
Pace Project No.: 92232729
Sample: MCAS 001 SLUDGE Lab ID: 92232729001 Collected: 01/08/15 11:30 Received: 01/09/15 11:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetra chloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 01/22/15 10:54
ND ug/L
0.50
1
01/22/1511:00
01/22/15 19:37
58-89-9
ND ug/L
3.0
1
01/22/1511:00
01/22/15 19:37
57-74-9
ND ug/L
0.50
1
01/22/1511:00
01/22/15 19:37
72-20-8
ND ug/L
0.50
1
01/22/1511:00
01/22/15 19:37
1024-57-3
ND ug/L
1000
1
01/22/1511:00
01/22/15 19:37
72-43-5
ND ug/L
3.0
1
01/22/1511:00
01/22/15 19:37
8001-35-2
46 %
10-138
1
01/22/1511:00
01/22/15 19:37
2051-24-3
56 %
10-110
1
01/22/1511:00
01/22/15 19:37
877-09-8
Analytical Method: EPA 8151
Preparation Method:
EPA 3510
ND mg/L
0.50
1
01/15/15 14:00
01/16/15 02:18
94-75-7
ND mg/L
0.50
1
01/15/15 14:00
01/16/15 02:18
93-72-1
88 %
42-142
1
01/15/15 14:00
01/16/15 02:18
19719-28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
18900 mg/kg
391
1
01/15/15 16:30
01/15/15 23:04
7429-90-5
ND mg/kg
39.1
1
01/15/15 16:30
01/16/1516:15
7440-38-2
10.7 mg/kg
3.9
1
01/15/15 16:30
01/15/15 23:04
7440-43-9
19800 mg/kg
391
1
01/15/15 16:30
01/15/15 23:04
7440-70-2
860 mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7440-50-8
ND mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7439-92-1
2190 mg/kg
391
1
01/15/15 16:30
01/15/15 23:04
7439-95-4
ND mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7439-98-7
43.2 mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7440-02-0
ND mg/kg
19500
1
01/15/15 16:30
01/15/15 23:04
7440-09-7
ND mg/kg
39.1
1
01/1511516:30
01/15/15 23:04
7782-49-2
ND mg/kg
19500
1
01/15/15 16:30
01/15/15 23:04
7440-23-5
626 mg/kg
39.1
1
01/15/15 16:30
01/15/15 23:04
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 01/15/15 18:00
Arsenic
ND mg/L 0.050 1 01/16/15 15:45
01/17/15 00:41
7440-38-2
Barium
0.34 mg/L 0.25 1 01/16/15 15:45
01/17/15 00:41
7440-39-3
Cadmium
0.012 mg/L 0.0050 1 01/16/15 15:45
01/17/15 00:41
7440-43-9
Chromium
ND mg/L 0.025 1 01/16/15 15:45
01/17/15 00:41
7440-47-3
Lead
ND mg/L 0.025 1 01/16/15 15:45
01/17/15 00:41
7439-92-1
Selenium
ND mg/L 0.10 1 01/16/15 15:45
01/17/15 00:41
7782-49-2
Silver
ND mg/L 0.025 1 01/16/15 15:45
01/17/15 00:41
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 01/15/15 18:00
Mercury
ND ug/L 0.20 1 01/16/1514:35
01/16/1517:28
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /27/2015 11:05 AM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 29

acice Analytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92232729
Sample: MCAS 001 SLUDGE Lab ID: 92232729001 Collected: 01/08/15 11:30 Received: 01/09/15 11:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.64 mg/kg 0.17 1 01/10/15 17:00 01/13/15 14:53 7439-97-6
8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 01/22/15 10:54
1,4-Dichlorobenzene
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
106-46-7
2,4-Dinitrotoluene
ND ug/L
500
1
01/22/15 12:20
01/23/15 13:30
121-14-2
Hexachloro-1,3-butadiene
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
87-68-3
Hexachlorobenzene
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
118-74-1
Hexachloroethane
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
67-72-1
2-Methylphenol(o-Cresol)
ND ug/L
50.0
1
01/22/15 12:20
01123/1513:30
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
Nitrobenzene
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
98-95-3
Pentachlorophenol
ND ug/L
100
1
01/22/15 12:20
01/23/15 13:30
87-86-5
Pyridine
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
110-86-1
2,4,5-Trichlorophenol
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
95-95-4
2,4,6-Trichlorophenol
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
88-06-2
Surrogates
Nitrobenzene-d5 (S)
60 %
12-102
1
01/22/15 12:20
01/23/15 13:30
4165-60-0
2-Fluorobiphenyl (S)
68 %
13-107
1
01/22/15 12:20
01/23/15 13:30
321-60-8
Terphenyl-d14 (S)
64 %
21-132
1
01/22/15 12:20
01/23/15 13:30
1718-51-0
Phenol-d6 (S)
21 %
10-110
1
01/22/15 12:20
01/23/15 13:30
13127-88-3
2-Fluorophenol (S)
33 %
10-110
1
01/22/15 12:20
01/23/15 13:30
367-12-4
2,4,6-Tribromophenol (S)
79 %
27-108
1
01/22/15 12:20
01/23/15 13:30
118-79-6
8260 MSV TCLP
Analytical Method: EPA 8260 Leachate Method/Date:
EPA 1311; 01/13/15 16:03
Benzene
ND ug/L
5.0
1
01/16/15 16:53
71-43-2
2-Butanone (MEK)
31.1 ug/L
10.0
1
01/16/15 16:53
78-93-3
Carbon tetrachloride
ND ug/L
5.0
1
01/16/15 16:53
56-23-5
Chlorobenzene
ND ug/L
5.0
1
01/16/15 16:53
108-90-7
Chloroform
ND ug/L
5.0
1
01/16/15 16:53
67-66-3
1,4-Dichlorobenzene
ND ug/L
5.0
1
01/16/15 16:53
106-46-7
1,2-Dichloroethane
ND ug/L
5.0
1
01/16/15 16:53
107-06-2
1,1-Dichloroethene
ND ug/L
5.0
1
01/16/15 16:53
75-35-4
Tetrachloroethene
ND ug/L
5.0
1
01/16/15 16:53
127-18-4
Trichloroethene
ND ug/L
5.0
1
01/16/15 16:53
79-01-6
Vinyl chloride
ND ug/L
5.0
1
01/16/15 16:53
75-01-4
Surrogates
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
01/16/15 16:53
17060-07-0 TP
Toluene-d8 (S)
95 %
67-135
1
01/16/15 16:53
2037-26-5
4-Bromofluorobenzene (S)
92 %
70-130
1
01/16/15 16:53
460-00-4
264OG Total Percent Solids
Analytical Method: SM 2540G
Total Solids
2.0 %
0.000010
1
01/13/15 15:30
Date: 01 /27/2015 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page 5 of 29

a06Anaiytica!
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92232729
Sample: MCAS 001 SLUDGE
Lab ID: 92232729001 Collected:
01/08/15 11:30
Received: 01/09/15 11:00 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.0 %
0.10
1
01/14/15 08:12
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
01/23/15 11:00
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
5.5 Std. Units
0.10
1
01/12/15 14:05
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
18900 mg/kg
0.12
1
01/23/15 14:08 N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
680 mg/kg
500
1
01/13/15 14:06 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total 45200 mg/kg 2130 20 01/13/15 15:05 7727-37-9 M6
353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2
Nitrogen, Nitrate 4860 mg/kg 498 5 01/21/15 20:32 M1
Nitrogen, Nitrite 330 mg/kg 249 5 01/21/15 20:32
Nitrogen, NO2 plus NO3 6190 mg/kg 498 5 01/21/15 20:32
366.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus 31100 mg/kg 1320 5 01/21/15 04:35 7723-14-0 M1,R1
733C S Reactive Cyanide Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive ND mg/kg 49.8 1 01/13/15 20:52
736S Reactive Sulfide Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive ND mg/kg 498 1 01/13/15 15:15
Sample: SAR Lab ID: 92232729002 Collected: 01/08/15 11:30 Received: 01/09/15 11:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Sodium 130000 ug/L 25000 5 01/15/15 15:10 01/15/15 20:38 7440-23-5
Sodium Adsorption Ratio, SAR Analytical Method: EPA 6010
Sodium Adsorption Ratio 1.8 meq/L 1 01/23/15 16:00 N2
Date: 01 /27/2015 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 29

acmnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE
Pace Project No.: 92244916
Sample: 001 SLUDGE Lab ID: 92244916001 Collected: 04/09/15 08:00 Received: 04/10/15 10:00 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
Analytical Method: EPA 8081
Preparation Method: EPA 3510
Leachate Method/Date:
EPA 1311; 04/22/15 09:30
gamma-BHC (Lindane)
ND
ug/L
10.0
20
04/27/15 08:30
04/27/15 20:28
58-89-9
Chlordane (Technical)
ND
ug/L
60.0
20
04/27/15 08:30
04/27/15 20:28
57-74-9
Endrin
ND
ug/L
10.0
20
04/27/15 08:30
04/27/15 20:28
72-20-8
Heptachlor epoxide
ND
ug/L
10.0
20
04/27/15 08:30
04/27/15 20:28
1024-57-3
Methoxychlor
ND
ug/L
20000
20
04/27/15 08:30
04/27/15 20:28
72-43-5
Toxaphene
ND
ug/L
60.0
20
04/27/15 08:30
04/27/15 20:28
8001-35-2
Surrogates
Decachlorobiphenyl (S)
0
%
10-138
20
04/27/15 08:30
04/27/15 20:28
2051-24-3 D3,S4
Tetrachloro-m-xylene (S)
0
%
10-110
20
04/27/15 08:30
04/27/15 20:28
877-09-8
8151 Chlorinate Herbicide TCLP Analytical Method: EPA 8151 Preparation Method: EPA 3510
2,4-D
ND
mg/L
0.010 1
04/21/15 07:30
04/21/15 12:51
94-75-7
2,4,5-TP (Silvex)
ND
mg/L
0.010 1
04/21/15 07:30
04/21/15 12:51
93-72-1
Surrogates
2,4-DCAA (S)
83
%
42-142 1
04/21/15 07:30
04/21/15 12:51
19719-28-9
6010 MET ICP
Analytical Method:
EPA 6010 Preparation Method: EPA 3050
Aluminum
29000
mg/kg
364 1
04/14/15 16:45
04/15/15 21:30
7429-90-5
Arsenic
44.3
mg/kg
36.4 1
04/14/15 16:45
04/15/15 21:30
7440-38-2
Cadmium
19.4
mg/kg
3.6 1
04/14/15 16:45
04/15/15 21:30
7440-43-9
Calcium
23100
mg/kg
364 1
04/14/15 16:45
04/15/15 21:30
7440-70-2
Copper
961
mg/kg
18.2 1
04/14/15 16:45
04/15/15 21:30
7440-50-8
Lead
20.3
mg/kg
18.2 1
04/14/15 16:45
04/15/15 21:30
7439-92-1
Magnesium
2420
mg/kg
364 1
04/14/15 16:45
04/15/15 21:30
7439-95-4
Molybdenum
ND
mg/kg
18.2 1
04/14/15 16:45
04/15/15 21:30
7439-98-7
Nickel
99.6
mg/kg
18.2 1
04/14/15 16:45
04/15/15 21:30
7440-02-0
Potassium
ND
mg/kg
18200 1
04/14/15 16:45
04/15/15 21:30
7440-09-7
Selenium
ND
mg/kg
36.4 1
04/14/15 16:45
04/15/15 21:30
7782-49-2
Sodium
ND
mg/kg
18200 1
04/14/15 16:45
04/15/15 21:30
7440-23-5
Zinc
682
mg/kg
36.4 1
04/14/15 16:45
04/15/15 21:30
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date:
EPA 1311; 04/14/15 00:55
Arsenic
ND
mg/L
0.050 1
04/15/15 21:35
04/16/15 15:41
7440-38-2
Barium
0.27
mg/L
0.25 1
04/15/15 21:35
04/16/15 15:41
7440-39-3
Cadmium
0.017
mg/L
0.0050 1
04/15/15 21:35
04/16/15 15:41
7440-43-9
Chromium
ND
mg/L
0.025 1
04/15/15 21:35
04/16/15 15:41
7440-47-3
Lead
ND
mg/L
0.025 1
04/15/15 21:35
04/16/15 15:41
7439-92-1
Selenium
ND
mg/L
0.10 1
04/15/15 21:35
04/16/15 15:41
7782-49-2
Silver
ND
mg/L
0.025 1
04/15/15 21:35
04/16/15 15:41
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 04/14/15 00:55
Mercury
ND
mg/L
0.00020 1
04/16/1511:10
04/16/1515:15
7439-97-6
REPORT
OF LABORATORY ANALYSIS
This report shall not
be reproduced, except
in full,
Date: 04/28/2015 05:15 PM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 30

;a'neAnalytical"
WWpacelabs.ccm
i
ANALYTICAL RESULTS
Project: 001 SLUDGE
Pace Project No.: 92244916
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 001 SLUDGE Lab ID: 92244916001 Collected: 04/09/15 08:00 Received: 04/10/15 10:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
254OG Total Percent Solids
Total Solids
Date: 04/28/2015 05:15 PM
Analytical Method: EPA 7471 Preparation Method: EPA 7471
0.50 mg/kg 0.13 1 04/11/1515:20 04/11/1519:13 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 04/22/15 09:30
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
106-46-7
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
121-14-2
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
87-68-3
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
118-74-1
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
67-72-1
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
95-48-7
683
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
L2
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
98-95-3
ND
ug/L
1000
10
04/23/15 08:20
04/24/15 10:01
87-86-5
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
110-86-1
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
95-95-4
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
88-06-2
0
%
12-102
10
04/23/15 08:20
04/24/15 10:01
4165-60-0
D3,S4
0
%
13-107
10
04/23/15 08:20
04/24/15 10:01
321-60-8
S4
0
%
21-132
10
04/23/15 08:20
04/24/15 10:01
1718-51-0
S4
0
%
10-110
10
04/23/15 08:20
04/24/15 10:01
13127-88-3
S4
0
%
10-110
10
04/23/15 08:20
04/24/15 10:01
367-12-4
S4
0
%
27-108
10
04/23/15 08:20
04/24/15 10:01
118-79-6
S4
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 04/20/15 10:47
ND
ug/L
100
20
04/28/1514:17
71-43-2
ND
ug/L
200
20
04/28/1514:17
78-93-3
ND
ug/L
100
20
04/28/1514:17
56-23-5
ND
ug/L
100
20
04/28/1514:17
108-90-7
ND
ug/L
100
20
04/28/1514:17
67-66-3
ND
ug/L
100
20
04/28/1514:17
106-46-7
ND
ug/L
100
20
04/28/1514:17
107-06-2
ND
ug/L
100
20
04/28/1514:17
75-35-4
ND
ug/L
100
20
04/28/1514:17
127-18-4
ND
ug/L
100
20
04/28/1514:17
79-01-6
ND
ug/L
100
20
04/28/1514:17
75-01-4
110
%
70-130
20
04/28/1514:17
17060-07-0
101
%
67-135
20
04/28/1514:17
2037-26-5
108
%
70-130
20
04/28/15 14:17
460-00-4
Analytical Method: SM 2540G
2.4 % 0.000010 1 04/16/1514:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 30

aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE
Pace Project No.: 92244916
Sample: 001 SLUDGE
Lab [D: 92244916001 Collected:
04/09/15 08:00
Received: 04/10/15 10:00 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qua]
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
97.6 %
0.10
1
04/17/15 11:09
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
04/16/15 14:00
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.6 Std. Units
0.10
1
04/13/15 13:30
H1
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
25200 mg/kg
0.12
1
04/27/15 15:36
N2
350.1 Ammonia
Analytical Method: EPA 350 1
Nitrogen, Ammonia
12300 mg/kg
423
1
04/16/1504:53
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
75700 mg/kg
1920
1
04/24/15 11:20
7727-37-9 M1
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA353.2
Nitrogen, Nitrate
ND mg/kg
83.7
1
04/23/15 19:05
Nitrogen, Nitrite
ND mg/kg
41.9
1
04/23/15 19:05
Nitrogen, NO2 plus NO3
ND mg/kg
83.7
1
04/23/15 19:05
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
39500 mg/kg
1690
10
04/21/1511:13
7723-14-0
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
42.2
1
04/16/15 19:34
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
422
1
04/16/15 16:00
Sample: SAR Lab ID: 92244916002 Collected: 04/09/15 08:00 Received: 04/10/15 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
200.7 MET ICP
Calcium
Magnesium
Sodium
Sodium Adsorption Ratio, SAR
Sodium Adsorption Ratio
Date: 04/28/2015 05:15 PM
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
483000 ug/L
1000 2
04/13/1514:30 04/27/1517:04 7440-70-2
47600 ug/L
1000 2
04/13/1514:30 04/27/1517:04 7439-95-4
144000 ug/L
25000 1
04/13/1514:30 04/15/1517:48 7440-23-5
Analytical Method: EPA 6010
1.7 meq/L
1
04/28/1512:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N2
Page 6 of 30

aceAnallXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE/CHLOROPHYLLA
Pace Project No.: 92257870
Sample: 001 SLUDGE Lab ID: 92257870001 Collected: 07/08/15 10:00 Received: 07/09/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl IS)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 07/21/15 09:00
ND
ug/L
0.50
1
07/22/1510:00
07/22/1515:40
58-89-9
ND
ug/L
3.0
1
07/22/1510:00
07/22/1515:40
57-74-9
ND
ug/L
0.50
1
07/22/1510:00
07/22/1515:40
72-20-8
ND
ug/L
0.50
1
07/22/1510-00
07/22/1515:40
1024-57-3
ND
ug/L
1000
1
07/22/1510:00
07/22/1515:40
72-43-5
ND
ug/L
3.0
1
07/22/1510:00
07/22/1515:40
8001-35-2
53
%
10-138
1
07/22/1510:00
07/22/1515:40
2051-24-3
60
%
10-110
1
07/22/1510:00
07/22/1515:40
877-09-8
Analytical Method:
EPA 8151
Preparation Method:
EPA 3510
ND
mg/L
0.64
1
07/17/15 08:00
07/18/15 04:39
94-75-7
ND
mg/L
0.64
1
07/17/15 08:00
07/18/15 04:39
93-72-1
107 % 42-142 1 07/17/15 08:00 07/18/15 04:39 19719-28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
9090
mg/kg
564
1
07/10/1518:15
07/14/1517:12
7429-90-5
ND
mg/kg
56.4
1
07/10/1518:15
07/14/1517:12
7440-38-2
31.3
mg/kg
5.6
1
07/10/1518:15
07/14/1517:12
7440-43-9
18800
mg/kg
564
1
07/10/1518:15
07/14/1517:12
7440-70-2
750
mg/kg
28.2
1
07/10/1518:15
07/14/1517:12
7440-50-8
ND
mg/kg
28.2
1
07/10/1518:15
07/14/1517:12
7439-92-1
1970
mg/kg
564
1
07/10/1518:15
07/14/1517:12
7439-95-4
ND
mg/kg
28.2
1
07/10/1518:15
07/14/1517:12
7439-98-7
35.8
mg/kg
28.2
1
07/10/1518:15
07/14/1517:12
7440-02-0
ND
mg/kg
28200
1
07/10/1518:15
07/14/1517:12
7440-09-7
ND
mg/kg
56.4
1
07/10/1518:15
07/14/1517:12
7782-49-2
ND
mg/kg
28200
1
07/10/1518:15
07/14/1517:12
7440-23-5
569
mg/kg
56.4
1
07/10/1518:15
07/14/1517:12
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 07/14/15 00:45
Arsenic
ND mg/L 0.050 1 07/15/15 03:00
07/16/15 13:45
7440-38-2
Barium
ND mg/L 0.25 1 07/15/15 03:00
07/16/15 13:45
7440-39-3
Cadmium
0.016 mg/L 0.0050 1 07/15/15 03:00
07/16/15 13:45
7440-43-9
Chromium
ND mg/L 0.025 1 07/15/15 03:00
07/16/15 13:45
7440-47-3
Lead
ND mg/L 0.025 1 07/15/15 03:00
07/16/15 13:45
7439-92-1
Selenium
ND mg/L 0.10 1 07/15/15 03:00
07/16/15 13:45
7782-49-2
Silver
ND mg/L 0.025 1 07/15/15 03:00
07/16/15 13:45
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 07/14/15 00:45
Mercury
ND mg/L 0.00020 1 07/15/1510:00
07/15/1514:11
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11 /2015 11:32 AM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 34

aceAnalXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE/CHLOROPHYLLA
Pace Project No.: 92257870
Sample: 001 SLUDGE Lab ID: 92257870001 Collected: 07/08/15 10:00 Received: 07/09/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1, 1 -Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
2540G Total Percent Solids
Total Solids
Date: 08/11 /2015 11:32 AM
Analytical Method: EPA 7471 Preparation Method: EPA 7471
0.72 mg/kg 0.31 1 07/17/1512:55 07/20/1515:46 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311, 07/21/15 09:00
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
106-46-7
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
121-14-2
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
87-68-3
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
118-74-1
10
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
67-72-1
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
95-48-7
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
98-95-3
ND
ug/L
100
1
07/22/1510:00
07/23/1512:30
87-86-5
10
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
110-86-1
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
95-95-4
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
88-06-2
15
%
12-102
1
07/22/1510:00
07/23/1512:30
4165-60-0
14
%
13-107
1
07/22/1510:00
07/23/1512:30
321-60-8
62
%
21-132
1
07/22/1510:00
07/23/1512:30
1718-51-0
7
%
10-110
1
07/22/1510:00
07/23/1512:30
13127-88-3
S5
9
%
10-110
1
07/22/1510:00
07/23/1512:30
367-12-4
S5
36
%
27-108
1
07/22/1510:00
07/23/1512:30
118-79-6
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 07/13/15 09:50
ND
ug/L
100
20
07/16/1517:33
71-43-2
ND
ug/L
200
20
07/16/1517:33
78-93-3
ND
ug/L
100
20
07/16/1517:33
56-23-5
ND
ug/L
100
20
07/16/1517:33
108-90-7
ND
ug/L
100
20
07/16/1517:33
67-66-3
ND
ug/L
100
20
07/16/1517:33
106-46-7
ND
ug/L
100
20
07/16/1517:33
107-06-2
ND
ug/L
100
20
07/16/1517:33
75-35-4
ND
ug/L
100
20
07/16/1517:33
127-18-4
ND
ug/L
100
20
07/16/1517:33
79-01-6
ND
ug/L
100
20
07/16/1517:33
75-01-4
99
%
70-130
20
07/16/1517:33
17060-07-0
101
%
67-135
20
07/16/1517:33
2037-26-5
82
%
70-130
20
07/16/1517:33
460-00-4
Analytical Method: SM 2540G
1.6 % 0.000010 1 07/11/15 02:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 34

5ceAna1Xica1
i
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE/CHLOROPHYLLA
Pace Project No.: 92257870
Sample: 001 SLUDGE
Lab ID: 92257870001 Collected:
07/08/15 10:00
Received: 07/09/15 09:30 Matrix: Solid
Results reported on a "dry weight'
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.4 %
0.10
1
07/13/15 14:30
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
07/14/15 12:20
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.0 Std. Units
0.10
1
07/10/15 12:00
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
23400 mg/kg
0.12
1
07/23/15 15:40
N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
11000 mg/kg
630
1
07/14/15 08:26
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
66300 mg/kg
2380
1
07/20/15 14:20
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
1300 mg/kg
128
1
07/15/15 11:39
Nitrogen, Nitrite
ND mg/kg
64.0
1
07/15/15 11:39
Nitrogen, NO2 plus NO3
1300 mg/kg
128
1
07/15/15 11:39
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
50600 mg/kg
1610
5
07/21/1512:15
7723-14-0
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
64.3
1
07/17/15 00:37
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
641
1
07/16/15 16:00
Sample: 001 SLUDGE SAR Lab ID: 92257870003 Collected: 07/08/15 10:00 Received: 07/09/15 09:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Calcium
Magnesium
Sodium
Sodium Adsorption Ratio, SAR
Sodium Adsorption Ratio
Date: 08/11/2015 11:32 AM
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
305000 ug/L
1000 10
07/23/1516:45 07/24/1517:03 7440-70-2
29300 ug/L
100 1
07/23/1516:45 07/24/1515:44 7439-95-4
99200 ug/L
50000 10
07/23/1516:45 07/24/1517:03 7440-23-5
Analytical Method: EPA 6010
1.4 meq/L
1
07/27/1513:05 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 34

aceAnaljftal
www.pacelabs.00w
Pace Analytical Services, Inc.
9800 KinceyAve Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: 001 SLUDGE Lab ID: 92272649001 Collected: 10/19/15 13:00 Received: 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
Analytical Method: EPA 8081
Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 10/30/15 00:00
gamma-BHC (Lindane)
ND ug/L
0.50 1
11/03/15 09:20
11/03/15 13:26
58-89-9
Chlordane (Technical)
ND ug/L
3.0 1
11/03/15 09:20
11/03/15 13:26
57-74-9
Endrin
ND ug/L
0.50 1
11/03/15 09:20
11/03/15 13:26
72-20-8
Heptachlor epoxide
ND ug/L
0.50 1
11/03/15 09:20
11/03/15 13:26
1024-57-3
Methoxychlor
ND ug/L
1000 1
11/03/15 09:20
11/03/15 13:26
72-43-5
Toxaphene
ND ug/L
3.0 1
11/03/15 09:20
11/03/15 13:26
8001-35-2
Surrogates
Decachlorobiphenyl (S)
40
%
10-138 '
1 11/03/15 09:20
11103/15 13:26
2051-24-3
Tetrachloro-m-xylene (S)
35
%
10-110
1 11/03/15 09:20
11/03/15 13:26
877-09-8
8151 Chlorinate Herbicide TCLP
Analytical Method: EPA 8151
Preparation Method:
EPA 3510
2,4-D
ND
mg/L
11.0
1 10/30/15 08:20
10/30/15 15:41
94-75-7
2,4,5-TP (Silvex)
ND
mg/L
11.0
1 10/30/15 08:20
10/30/15 15:41
93-72-1
Surrogates
2,4-DCAA (S)
102
%
42-142
1 10/30/15 08:20
10/30/15 15:41
19719-28-9
6010 MET ICP
Analytical Method: EPA 6010
Preparation Method:
EPA 3050
Aluminum
30400
mg/kg
9200
1 10/22/15 20:30
10/27/15 01:47
7429-90-5
Arsenic
ND
mg/kg
920
1 10/22/15 20:30
10/27/15 01:47
7440-38-2
Cadmium
ND
mg/kg
92.0
1 10/22/15 20:30
10/27/15 01:47
7440-43-9
Calcium
130000
mg/kg
9200
1 10/22/15 20:30
10/27/15 01:47
7440-70-2
Copper
1700
mg/kg
460
1 10/22/15 20:30
10/27/15 01:47
7440-50-8
Lead
ND
mg/kg
460
1 10/22/15 20:30
10/27/15 01:47
7439-92-1
Magnesium
19000
mg/kg
9200
1 10/22/15 20:30
10/27/15 01:47
7439-95-4
Molybdenum
ND
mg/kg
460
1 10/22/15 20:30
10/27/15 01:47
7439-98-7
Nickel
ND
mg/kg
460
1 10/22/15 20:30
10/27/15 01:47
7440-02-0
Potassium
ND
mg/kg
460000
1 10/22/15 20:30
10/27/15 01:47
7440-09-7
Selenium
ND
mg/kg
920
1 10/22/15 20:30
10/27/15 01:47
7782-49-2
Sodium
ND
mg/kg
460000
1 10/22/15 20:30
10/27/15 01:47
7440-23-5
Zinc
1930
mg/kg
920
1 10/22/15 20:30
10/27/15 01:47
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010
Preparation Method:
EPA 3010
Leachate Method/Date:
EPA 1311; 10/22/15 05:10
Arsenic
ND
mg/L
0.050
1 10/23/15 02:30
10/23/16 17:04
7440-38-2
Barium
ND
mg/L
0.25
1 10/23/15 02:30
10/23/15 17:04
7440-39-3
Cadmium
ND
mg/L
0.0050
1 10/23/15 02:30
10/23/15 17:04
7440-43-9
Chromium
ND
mg/L
0.025
1 10/23/15 02:30
10/23/15 17:04
7440-47-3
Lead
ND
mg/L
0.025
1 10/23/15 02:30
10/23/15 17:04
7439-92-1
Selenium
ND
mg/L
0.10
1 10/23/15 02:30
10/23/15 17:04
7782-49-2
Silver
ND
mg/L
0.025
1 10/23/15 02:30
10/23/15 17:04
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470
Preparation Method:
EPA 7470
Leachate Method/Date:
EPA 1311; 10/22/15 05:10
Mercury
ND
mg/L
0.00020
1 10/23/1510:00
10/23/1513:41
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2015 09:05.AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 40

aceAnalytical�
www.paceW&com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: 001 SLUDGE Lab ID: 92272649001 Collected: 10/19/15 13:00, Received: 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury
'Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trich loropheno I
2,4,6-Trich lorophen o I
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6- (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
254OG Total Percent Solids
Total Solids
Date: 11 /10/2015 09:05 AM
Analytical Method: EPA 7471 Preparation Method: EPA 7471 '
ND mg/kg 5.2 1 10/26/1513:20 10/27/1513:52 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 10/30/15 00:00
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
106-46-7.
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
121-14-2
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
87-68-3
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
118-74-1
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
67-72-1
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
95-48-7
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
ND
ug/L
50.0
1�
11/02/1510:00
11/03/1514:58
98-95-3
ND
ug/L
100
1
11/02/1510:00
11/03/1514:58
87-86-5
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
110-86-1
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
95-95-4
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
88-06-2
18
%
12-102
1
11 /02/15 10:00
11 /03/15 14:58
4165-60-0
22
%
13-107
1
11/02/1510:00
11/03/1514:58
321-60-8
56
%
21-132
1
11 /02/15 10:00
11 /03/15 14:58
1718-51-0
9
%
10-110
1
11/0211510:00
11/03/1514:58
13127-88-3 SO
12
%
10-110
1
11/0211510:00
11/03/1514:58
367-12-4
50
%
27-108
1
11/02/1510:00
11/03/1514:58
118-79-6
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 10/26/15 11:12
ND
ug/L
100
20
10/31/15 08:56
71-43-2
ND
ug/L
200
20
10/31/15 08:56
78-93-3
ND
ug/L
100
20
10/31/15 08:56
56-23-5
ND
ug/L
100
20
10/31/15 08:56
108-90-7
ND
ug/L
100
20
10/31/15 08:56
67-66-3
ND
ug/L
100
20
10/31/15 08:56
106-46-7
ND
ug/L
100
20
10/31/15 08:56
107-06-2
ND
ug/L
100
20
10/31/15 08:56
75-35-4
ND
ug/L'
100
20
10/31/15 08:56
127-18-4
ND
ug/L
100
20
10/31/15 08:56
79-01-6
ND
ug/L
100
20
10/31/15 08:56
75-01-4
124
%
70-130
20
10/31/15 08:56
17060-07-0
98
%
67-135
20
10/31/15 08:56
2037-26-5
105
%
70-130
20
10/31/15 08:56
460-00-4
Analytical Method:
SM 254OG
0.090
%
0.000010
1
10/21 /15 16:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 40

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[phone]
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: 001 SLUDGE
Lab ID: 92272649001 Collected:
10/19/15 13:00
Received: 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qua]
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
99.9 %
0.10
1
10/22/15 12:53
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
10/30/15 11:30
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.2 Std. Units
0.10
1
10/22/15 11:40
H1
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
122000 mg/kg
0.12
1
11/05/15 17:20
N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
135000 mg/kg
10200
1
10/26/15 01:31
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
217000 mg/kg
55200
1
11/03/15 02:36
7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
26000 mg/kg
2180
1
11/03/15 10:31
Nitrogen, Nitrite
4160 mg/kg
1090
1
11/03/15 10:31
Nitrogen, NO2 plus NO3
30100 mg/kg
2180
1
11/03/15 10:31
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
142000 mg/kg
4150
2
10/28/1512:19
7723-14-0
Sample: 001 SLUDGE Lab ID: 92272649002 Collected: 10/19/15 13:00 Received: 10/21/15 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Calcium
Magnesium
Sodium
Sodium Adsorption Ratio, SAR
Sodium Adsorption Ratio
733C Reactive Cyanide
Cyanide, Reactive
734S Reactive Sulfide
Sulfide, Reactive
Date: 11 /10/2015 09:05 AM
Analytical Method: EPA200.7 Preparation Method: EPA200.7
189000 ug/L
1000
1
11/05/1513:05 11/06/1515:41 7440-70-2
24200 ug/L
1000
1
11/05/1513:05 11/06/1515:41 7439-95-4
117000 ug/L
50000
1
11/05/1513:05 11/06/1515:41 7440-23-5
Analytical Method: EPA 6010
2.1 meq/L
1
11 /09/15 17:02 N2
Analytical Method: SW-846 7.3.3.2
ND mg/L
0.010
1
10/22/15 22:30
Analytical Method: SW-846 7.3.4.2
ND mg/L
1.0
1
10/22/1518:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 6 of 40

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ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92232729
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WAS 001 SLUDGE Lab ID: 92232729001 Collected: 01/08/15 11:30 Received: 01/09/15 11:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA IS)
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 01/22/15 10:54
ND ug/L
0.50
1
01/2211511:00
01/22/15 19:37
58-89-9
ND ug/L
3.0
1
01/22/15 11:00
01/22/15 19:37
57-74-9
ND ug/L
0.50
1
01/22/15 11:00
01/22/15 19:37
72-20-8
ND ug/L
0.50
1
01/22/15 11:00
01/22/15 19:37
1024-57-3
ND ug/L
1000
1
01/22/15 11:00
01/22/15 19:37
72-43-5
ND ug/L
3.0
1
01/22/15 11:00
01/22/15 19:37
8001-35-2
46 %
10-138
1
01/22/15 11:00
01/22/15 19:37
2051-24-3
56 %
10-110
1
01/22/15 11:00
01/22/15 19:37
877-09-8
Analytical Method: EPA 8151 Preparation Method: EPA 3510
ND mg/L
0.50 1
01/15/15 14:00
01/16/15 02:18
94-75-7
ND mg/L
0.50 1
01/15/15 14:00
01/16/15 02:18
93-72-1
88 %
42-142 1
01/15/15 14:00
01/16/15 02:18
19719-28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
18900 mg/kg
391
1
01/15/15 16:30
01/15/15 23:04
7429-90-5
ND mg/kg
39.1
1
01/15/15 16:30
01/16/1516:15
7440-38-2
10.7 mg/kg
3.9
1
01/15/15 16:30
01/15/15 23:04
7440-43-9
19800 mg/kg
391
1
01/15/15 16:30
01/15/15 23:04
7440-70-2
860 mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7440-50-8
ND mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7439-92-1
2190 mg/kg
391
1
01/15/15 16:30
01/15/15 23:04
7439-95-4
ND mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7439-98-7
43.2 mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7440-02-0
ND mg/kg
19500
1
01/15/15 16:30
01/15/15 23:04
7440-09-7
ND mg/kg
39.1
1
01/15/15 16:30
01/15/15 23:04
7782-49-2
ND mg/kg
19500
1
01/15/15 16:30
01/15/15 23:04
7440-23-5
626 mg/kg
39.1
1
01/15/15 16:30
01/15/15 23:04
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 01/15/15 18:00
Arsenic
ND mg/L 0.050 1 01/16/15 15:45
01/17/15 00:41
7440-38-2
Barium
0.34 mg/L 0.25 1 01/16/15 15:45
01/17/15 00:41
7440-39-3
Cadmium
0.012 mg/L 0.0050 1 01/16/15 15:45
01/17/15 00:41
7440-43-9
Chromium
ND mg/L 0.025 1 01/16/15 15:45
01/17/15 00:41
7440-47-3
Lead
ND mg/L 0.025 1 01/16/15 15:45
01/17/15 00:41
7439-92-1
Selenium
ND mg/L 0.10 1 01/16/15 15:45
01/17/15 00:41
7782-49-2
Silver
ND mg/L 0.025 1 01/16/15 15:45
01/17/15 00:41
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 01/15/15 18:00
Mercury
ND ug/L 0.20 1 01/16/1514:35
01/16/1517:28
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /27/2015 11:05 AM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 29

aceAnaly�ical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92232729
Sample: WAS 001 SLUDGE Lab ID: 92232729001 Collected: 01/08/15 11:30 Received: 01/09/15 11:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trich lorophe n o I
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
254OG Total Percent Solids
Total Solids
Date: 01 /27/2015 11:05 AM
Analytical Method: EPA 7471
Preparation Method: EPA 7471
0.64 mg/kg
0.17
1
01/10/1517:00
01/13/1514:53
7439-97-6
Analytical Method: EPA 8270
Preparation Method: EPA 3510
Leachate Method/Date: EPA
1311; 01/22/15 10:54
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
106-46-7
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
121-14-2
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
87-68-3
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
118-74-1
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
67-72-1
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
95-48-7
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
98-95-3
ND ug/L
100
1
01/22/15 12:20
01123/1513:30
87-86-5
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
110-86-1
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
95-95-4
ND ug/L
50.0
1
01/22/15 12:20
01/2311513:30
88-06-2
60 %
12-102
1
01/22/15 12:20
01/23/15 13:30
4165-60-0
68 %
13-107
1
01/22/15 12:20
01/23/15 13:30
321-60-8
64 %
21-132
1
01/22/15 12:20
01/23/15 13:30
1718-51-0
21 %
10-110
1
01/22/15 12:20
01123/1513:30
13127-88-3
33 %
10-110
1
01/22/15 12:20
01/23/15 13:30
367-12-4
79 %
27-108
1
01/22/15 12:20
01/23/15 13:30
118-79-6
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 01/13/15 16:03
ND ug/L
5.0
1
01/16/15 16:53
71-43-2
31.1 ug/L
10.0
1
01/16/15 16:53
78-93-3
ND ug/L
5.0
1
01/16/15 16:53
56-23-5
ND ug/L
5.0
1
01/1611516:53
108-90-7
ND ug/L
5.0
1
01/16/15 16:53
67-66-3
ND ug/L
5.0
1
01/16/15 16:53
106-46-7
ND ug/L
5.0
1
01/16/15 16:53
107-06-2
ND ug/L
5.0
1
01/16/15 16:53
75-35-4
ND ug/L
5.0
1
01/16/15 16:53
127-18-4
ND ug/L
5.0
1
01/16/15 16:53
79-01-6
ND ug/L
5.0
1
01/16/15 16:53
75-01-4
100 %
70-130 1
95 %
67-135 1
92 %
70-130 1
Analytical Method: SM 2540G
2.0 %
0.000010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/16/15 16:53 17060-07-0 TP
01116/1516:53 2037-26-5
01/16/15 16:53 460-00-4
01/13/15 15:30
Page 5 of 29

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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SLUDGE
Pace Project No.: 92232729
Sample: MCAS 001 SLUDGE
Lab ID: 92232729001 Collected:
01/08/15 11:30
Received: 01/09/15 11:00 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.0 %
0.10
1
01/14/15 08:12
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
01/23/15 11:00
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
5.6 Std. Units
0.10
1
01/12/15 14:05
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
18900 mg/kg
0.12
1
01/23/15 14:08 N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
680 mg/kg
500
1
01/13/15 14:06 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
45200 mg/kg
2130
20
01/13/15 15:05 7727-37-9 M6
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
4860 mg/kg
498
5
01/21/1520:32 M1
Nitrogen, Nitrite
330 mg/kg
249
5
01/21/1520:32
Nitrogen, NO2 plus NO3
5190 mg/kg
498
5
01/21/15 20:32
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
31100 mg/kg
1320 5
01/21/1504:35 7723-14-0 M1,R1
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
49.8 1
01/13/15 20:52
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
498 1
01/13/15 15:15
Sample: SAR
Lab ID: 92232729002 Collected:
01/08/15 11:30
Received: 01/09/15 11:00 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qua[
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Sodium 130000 ug/L 25000 5 01/15/15 15:10 01/15/15 20:38 7440-23-5
Sodium Adsorption Ratio, SAR Analytical Method: EPA 6010
Sodium Adsorption Ratio 1.8 meq/L 1 01/23/15 16:00 N2
Date: 01 /27/2015 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 29

�eMalxicalv
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Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE
Pace Project No.: 92244916
Sample: 001 SLUDGE Lab ID: 92244916001 Collected: 04/09/15 08:00 Received: 04/10/15 10:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 04/22/15 09:30
ND
ug/L
10.0
20
04/27/15 08:30
04/27/15 20:28
58-89-9
ND
ug/L
60.0
20
04/27/15 08:30
04/27/15 20:28
57-74-9
ND
ug/L
10.0
20
04/27/15 08:30
04/27/15 20:28
72-20-8
ND
ug/L
10.0
20
04/27/15 08:30
04/27/15 20:28
1024-57-3
ND
ug/L
20000
20
04/27/15 08:30
04/27/15 20:28
72-43-5
ND
ug/L
60.0
20
04/27/15 08:30
04/27/15 20:28
8001-35-2
0
%
10-138
20
04/27/15 08:30
04/27/15 20:28
2051-24-3 D3,S4
0
%
10-110
20
04/27/15 08:30
04/27/15 20:28
877-09-8
Analytical Method: EPA 8151
Preparation Method:
EPA 3510
ND
mg/L
0.010
1
04/21/15 07:30
04/21/15 12:51
94-75-7
ND
mg/L
0.010
1
04/21/15 07:30
04/21/15 12:51
93-72-1
83
%
42-142
1
04/21/15 07:30
04/21/15 12:51
19719-28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
29000
mg/kg
364
1
04/14/15 16:45
04/15/15 21:30
7429-90-5
44.3
mg/kg
36.4
1
04/14/15 16:45
04/15/15 21:30
7440-38-2
19.4
mg/kg
3.6
1
04/14/15 16:45
04/15/15 21:30
7440-43-9
23100
mg/kg
364
1
04/14/15 16:45
04/15/15 21:30
7440-70-2
961
mg/kg
18.2
1
04/14/15 16:45
04/15/15 21:30
7440-50-8
20.3
mg/kg
18.2
1
04/14/15 16:45
04/15/15 21:30
7439-92-1
2420
mg/kg
364
1
04/14/15 16:45
04/15/15 21:30
7439-95-4
ND
mg/kg
18.2
1
04/14/15 16:45
04/15/15 21:30
7439-98-7
99.6
mg/kg
18.2
1
04/14/15 16:45
04/15/15 21:30
7440-02-0
ND
mg/kg
18200
1
04/14/15 16:45
04/15/15 21:30
7440-09-7
ND
mg/kg
36.4
1
04/14/15 16:45
04/15/15 21:30
7782-49-2
ND
mg/kg
18200
1
04/14/15 16:45
04/15/15 21:30
7440-23-5
682
mg/kg
36.4
1
04/14/15 16:45
04/15/15 21:30
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 04/14/15 00:55
Arsenic
ND mg/L 0.050 1 04/15/15 21:35
04/16/15 15:41
7440-38-2
Barium
0.27 mg/L 0.25 1 04/15/15 21:35
04/16/15 15:41
7440-39-3
Cadmium
0.017 mg/L 0.0050 1 04/15/15 21:35
04/16/15 15:41
7440-43-9
Chromium
ND mg/L 0,025 1 04/15/15 21:35
04/16/15 15:41
7440-47-3
Lead
ND mg/L 0.025 1 04/15/15 21:35
04/16/15 15:41
7439-92-1
Selenium
ND mg/L 0.10 1 04/15/15 21:35
04/16/15 15:41
7782-49-2
Silver
ND mg/L 0.025 1 04/15/15 21:35
04/16/15 15:41
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 04/14/15 00:55
Mercury
ND mg/L 0.00020 1 04/16/1511:10
04/16/1515:15
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2015 05:15 PM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 30

lacoAnalyfical@
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE
Pace Project No.: 92244916
Sample: 001 SLUDGE Lab ID: 92244916001 Collected: 04/09/15 08:00 Received: 04/10/15 10:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.50 mg/kg 0.13 1 04/11/1515:20 04/11/1519:13 7439-97-6
8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 04/22/15 09:30
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
2540G Total Percent Solids
Total Solids
Date: 04/28/2015 05:15 PM
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
106-46-7
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
121-14-2
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
87-68-3
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
118-74-1
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
67-72-1
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
95-48-7
683
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
L2
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
98-95-3
ND
ug/L
1000
10
04/23/15 08:20
04/24/15 10:01
87-86-5
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
110-86-1
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
95-95-4
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
88-06-2
0
%
12-102
10
04/23/15 08:20
04/24/15 10:01
4165-60-0
D3,S4
0
%
13-107
10
04/23/15 08:20
04/24/15 10:01
321-60-8
S4
0
%
21-132
10
04/23/15 08:20
04/24/15 10:01
1718-51-0
S4
0
%
10-110
10
04/23/15 08:20
04/24/15 10:01
13127-88-3
S4
0
%
10-110
10
04/23/15 08:20
04/24/15 10:01
367-12-4
S4
0
%
27-108
10
04/23/15 08:20
04/24/15 10:01
118-79-6
S4
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 04/20/15 10:47
ND
ug/L
100
20
04/28/15 14:17
71-43-2
ND
ug/L
200
20
04/28/15 14:17
78-93-3
ND
ug/L
100
20
04/28/15 14:17
56-23-5
ND
ug/L
100
20
04/28/15 14:17
108-90-7
ND
ug/L
100
20
04/28/15 14:17
67-66-3
ND
ug/L
100
20
04/28/15 14:17
106-46-7
ND
ug/L
100
20
04/28/15 14:17
107-06-2
ND
ug/L
100
20
04/28/15 14:17
75-35-4
ND
ug/L
100
20
04/28/15 14:17
127-18-4
ND
ug/L
100
20
04/28/15 14:17
79-01-6
ND
ug/L
100
20
04/28/15 14:17
75-01-4
110
%
70-130
20
04/2811514:17
17060-07-0
101
%
67-135
20
04/28/15 14:17
2037-26-5
108
%
70-130
20
04/28/15 14:17
460-00-4
Analytical Method: SM 2540G
2.4
%
0.000010
1
04/16/1514:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 30

ace, Ma Oca I
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE
Pace Project No.: 92244916
Sample: 001 SLUDGE
Lab ID: 92244916001 Collected:
04/09/15 08:00
Received: 04/10/15 10:00 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
97.6 %
0.10
1
04/17/15 11:09
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
04/16/15 14:00
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.6 Std. Units
0.10
1
04/13/15 13:30 H1
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
25200 mg/kg
0.12
1
04/27/15 15:36 N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
12300 mg/kg
423
1
04/16/15 04:53 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
75700 mg/kg
1920
1
04/24/15 11:20 7727-37-9 M1
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA353.2
Nitrogen, Nitrate
ND mg/kg
83.7
1
04/23/15 19:05
Nitrogen, Nitrite
ND mg/kg
41.9
1
04/23/15 19:05
Nitrogen, NO2 plus NO3
ND mg/kg
83.7
1
04/23/15 19:05
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
39500 mg/kg
1690
10
04/21/1511:13 7723-14-0
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
42.2
1
04/16/15 19:34
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
422
1
04/16/15 16:00
Sample: SAR Lab ID: 92244916002 Collected: 04/09/15 08:00 Received: 04/10/15 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Calcium
Magnesium
Sodium
Sodium Adsorption Ratio, SAR
Sodium Adsorption Ratio
Date: 04/28/2015 05:15 PM
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
483000 ug/L
1000 2
04/13/1514:30 04/27/1517:04 7440-70-2
47600 ug/L
1000 2
04113/1514:30 04/27/15 17:04 7439-95-4
144000 ug/L
25000 1
04/13/1514:30 04/15/1517:48 7440-23-5
Analytical Method: EPA 6010
1.7 meq/L
1
04/28/1512:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
N2
Page 6 of 30

eAnalytical
www.pacelabs.com
I
ANALYTICAL RESULTS
Project: 001 SLUDGE/CHLOROPHYLLA
Pace Project No.: 92257870
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 001 SLUDGE Lab ID: 92257870001 Collected: 07/08/15 10:00 Received: 07/09/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 07/21/15 09:00
ND
ug/L
0.50
1
07/2211510:00
07/22/1515:40
58-89-9
ND
ug/L
3.0
1
07/22/1510:00
07/22/1515:40
57-74-9
ND
ug/L
0.50
1
07/22/1510:00
07122/1515:40
72-20-8
ND
ug/L
0.50
1
07/22/1510:00
07/22/1515:40
1024-57-3
ND
ug/L
1000
1
07/22/1510:00
07/22/1515:40
72-43-5
ND
ug/L
3.0
1
07/22/1510:00
07/22/1515:40
8001-35-2
53
%
10-138
1
07/22/1510:00
07/22/1515:40
2051-24-3
60
%
10-110
1
07/22/1510:00
07/22/1515:40
877-09-8
Analytical Method:
EPA 8151
Preparation Method:
EPA 3510
ND
mg/L
0.64
1
07/17/15 08:00
07/18/15 04:39
94-75-7
ND
mg/L
0.64
1
07/17/15 08:00
07/18/15 04:39
93-72-1
107
%
42-142
1
07/17/15 08:00
07/18/15 04:39
19719-28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
9090
mg/kg
564 1
07/10/1518:15
07/14/1517:12
7429-90-5
Arsenic
ND
mg/kg
56.4 1
07/10/1518:15
07/14/1517:12
7440-38-2
Cadmium
31.3
mg/kg
5.6 1
07/1011518:15
07/14/1517:12
7440-43-9
Calcium
18800
mg/kg
564 1
07/10/1518:15
07/14/1517:12
7440-70-2
Copper
750
mg/kg
28.2 1
07/10/1518:15
07/14/1517:12
7440-50-8
Lead
ND
mg/kg
28.2 1
07/1011518:15
07/14/1517:12
7439-92-1
Magnesium
1970
mg/kg
564 1
07/10/1518:15
07/14/1517:12
7439-95-4
Molybdenum
ND
mg/kg
28.2 1
07/10/1518:15
07/14/1517:12
7439-98-7
Nickel
35.8
mg/kg
28.2 1
07/10/1518:15
07/14/1517:12
7440-02-0
Potassium
ND
mg/kg
28200 1
07/10/1518:15
07/14/1517:12
7440-09-7
Selenium
ND
mg/kg
56.4 1
07/10/1518:15
07/14/1517:12
7782-49-2
Sodium
ND
mg/kg
28200 1
07/10/1518:15
07/14/1517:12
7440-23-5
Zinc
569
mg/kg
56.4 1
07/10/1518:15
07/14/1517:12
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 07/14/15 00:45
Arsenic
ND
mg/L
0.050 1
07/15/15 03:00
07/16/15 13:45
7440-38-2
Barium
ND
mg/L
0.25 1
07/15/15 03:00
07/16/15 13:45
7440-39-3
Cadmium
0.016
mg/L
0.0050 1
07/15/15 03:00
07/16/15 13:45
7440-43-9
Chromium
ND
mg/L
0.025 1
07/15/15 03:00
07/16/15 13:45
7440-47-3
Lead
ND
mg/L
0.025 1
07/15/15 03:00
07/16/15 13:45
7439-92-1
Selenium
ND
mg/L
0.10 1
07/15/15 03:00
07/16/15 13:45
7782-49-2
Silver
ND
mg/L
0.025 1
07/15/15 03:00
07/16/15 13:45
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA
7470
Leachate Method/Date: EPA 1311; 07/14/15 00:45
Mercury
ND
mg/L
0.00020 1
07/15/1510:00
07/15/1514:11
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
Date: 08/11 /2015 11:32 AM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 34

,��acqAnalyticale
www.pacelabs.com
I
ANALYTICAL RESULTS
race nnaryucai services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 001 SLUDGE/CHLOROPHYLLA
Pace Project No.: 92257870
Sample: 001 SLUDGE Lab ID: 92257870001 Collected: 07/08/15 10:00 Received: 07/09/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-dl4 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobe nzene (S)
254OG Total Percent Solids
Total Solids
Date: 08/11 /2015 11:32 AM
0.72 mg/kg 0.31 1 07/17/1512:55 07/20/1515:46 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 07/21/15 09:00
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
106-46-7
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
121-14-2
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
87-68-3
ND
ug/L
50.0
1
07/22/1510:00
07/2311512:30
118-74-1
10
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
67-72-1
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
95-48-7
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
98-95-3
ND
ug/L
100
1
07122/1510:00
07/23/1512:30
87-86-5
10
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
110-86-1
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
95-95-4
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
88-06-2
15
%
12-102
1
07/22/1510:00
07123/1512:30
4165-60-0
14
%
13-107
1
07/22/1510:00
07/23/1512:30
321-60-8
62
%
21-132
1
07/22/1510:00
07/23/1512:30
1718-51-0
7
%
10-110
1
07/22/1510:00
07/23/1512:30
13127-88-3
S5
9
%
10-110
1
07/22/1510:00
07/23/1512:30
367-12-4
S5
36
%
27-108
1
07/22/1510:00
07/23/1512:30
118-79-6
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 07/13/15 09:50
ND
ug/L
100
20
07/16/1517:33
71-43-2
ND
ug/L
200
20
07/16/1517:33
78-93-3
ND
ug/L
100
20
07/16/1517:33
56-23-5
ND
ug/L
100
20
07/16/1517:33
108-90-7
ND
ug/L
100
20
07/16/1517:33
67-66-3
ND
ug/L
100
20
07/16/1517:33
106-46-7
ND
ug/L
100
20
07/16/15 17:33
107-06-2
ND
ug/L
100
20
07/16/1517:33
75-35-4
ND
ug/L
100
20
07/16/1517:33
127-18-4
ND
ug/L
100
20
07116/1517:33
79-01-6
ND
ug/L
100
20
07/16/1517:33
75-01-4
99
%
70-130
20
07/16/1517:33
17060-07-0
101
%
67-135
20
07/16/1517:33
2037-26-5
82
%
70-130
20
07/16/1517:33
460-00-4
Analytical Method: SM 2540G
1.6 % 0.000010 1 07/11/15 02:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 34

u,�a.Analytical
www.pacelabs.com
ANALYTICAL RESULTS
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 001 SLUDGE/CHLOROPHYLLA
Pace Project No.: 92257870
Sample: 001 SLUDGE
Lab ID: 92257870001 Collected:
07/08/15 10:00
Received: 07/09/15 09:30 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.4 %
0.10
1
07/13/15 14:30
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
07/14/15 12:20
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.0 Std. Units
0.10
1
07/10/15 12:00
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
23400 mg/kg
0.12
1
07/23/15 15:40
N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
11000 mg/kg
630
1
07/14/15 08:26
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
66300 mg/kg
2380
1
07/20/15 14:20
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
1300 mg/kg
128
1
07/15/15 11:39
Nitrogen, Nitrite
ND mg/kg
64.0
1
07/15/15 11:39
Nitrogen, NO2 plus NO3
1300 mg/kg
128
1
07/15/15 11:39
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
50600 mg/kg
1610
5
07/2111512:15
7723-14-0
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
64.3
1
07/17/15 00:37
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
641
1
07/16/15 16:00
Sample: 001 SLUDGE SAR Lab ID: 92257870003 Collected: 07/08/15 10:00 Received: 07/09/15 09:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Calcium
Magnesium
Sodium
Sodium Adsorption Ratio, SAR
Sodium Adsorption Ratio
Date: 08/11 /2015 11:32 AM
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
305000 ug/L
1000 10
07/23/1516:45 07/24/1517:03 7440-70-2
29300 ug/L
100 1
07/23/15 16:45 07/24/15 15:44 7439-95-4
99200 ug/L
50000 10
07/23/1516:45 07/2411517:03 7440-23-5
Analytical Method: EPA6010
1.4 meq/L
1
07/27/1513:05 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 34

,�aceAnalytical@
. www.pecelabs.com
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: 001 SLUDGE Lab ID: 92272649001 Collected: 10/19/15 13:00 Received: 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 10/30/15 00:00
ND
ug/L
0.50
1
11/03/15 09:20
11/03/15 13:26
58-89-9
ND
ug/L
3.0
1
11/03/15 09:20
11/03/15 13:26
57-74-9
ND
ug/L
0.50
1
11/03/15 09:20
11/03/15 13:26
72-20-8
ND
ug/L
0.50
1
11/03/15 09:20
11/03/15 13:26
1024-57-3
ND
ug/L
1000
1
11/03/15 09:20
11/03/15 13:26
72-43-5
ND
ug/L
3.0
1
11/03/15 09:20
11/03/15 13:26
8001-35-2
40
%
10-138
1
11/03/15 09:20
11/03/15 13:26
2051-24-3
35
%
10-110
1
11/03/15 09:20
11/03/15 13:26
877-09-8
Analytical Method: EPA 8151 Preparation Method: EPA 3510
ND
mg/L
11.0 1
10/30/15 08:20
10/30/15 15:41
94-75-7
ND
mg/L
11.0 1
10/30/15 08:20
10/30/15 15:41
93-72-1
102
%
42-142 1
10/30/15 08:20
10/30/15 15:41
19719-28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
30400
mg/kg
9200
1
10/22/15 20:30
10/27/15 01:47
7429-90-5
ND
mg/kg
920
1
10/22/15 20:30
10/27/15 01:47
7440-38-2
ND
mg/kg
92.0
1
10/22/15 20:30
10/27/15 01:47
7440-43-9
130000
mg/kg
9200
1
10/22/15 20:30
10/27/15 01:47
7440-70-2
1700
mg/kg
460
1
10/22/15 20:30
10/27/15 01:47
7440-50-8
ND
mg/kg
460
1
10/22/15 20:30
10/27/15 01:47
7439-92-1
19000
mg/kg
9200
1
10/22/15 20:30
10/27/15 01:47
7439-95-4
ND
mg/kg
460
1
10/22/15 20:30
10/27/15 01:47
7439-98-7
ND
mg/kg
460
1
10/22/15 20:30
10/27/15 01:47
7440-02-0
ND
mg/kg
460000
1
10/22/15 20:30
10/27/15 01:47
7440-09-7
ND
mg/kg
920
1
10/22/15 20:30
10/27/15 01:47
7782-49-2
ND
mg/kg
460000
1
10/22/15 20:30
10/27/15 01:47
7440-23-5
1930
mg/kg
920
1
10/22/15 20:30
10/27/15 01:47
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/22115 05:10
Arsenic
ND mg/L 0.050 1 10/23/15 02:30
10/23/15 17:04
7440-38-2
Barium
ND mg/L 0.25 1 10/23/15 02:30
10/23/15 17:04
7440-39-3
Cadmium
ND mg/L 0.0050 1 10/23/15 02:30
10/23/15 17:04
7440-43-9
Chromium
ND mg/L 0.025 1 10/23/15 02:30
10/23/15 17:04
7440-47-3
Lead
ND mg/L 0.025 1 10/23/15 02:30
10/23/15 17:04
7439-92-1
Selenium
ND mg/L 0.10 1 10/23/15 02:30
10/23/15 17:04
7782-49-2
Silver
ND mg/L 0.025 1 10/23/15 02:30
10/23/15 17:04
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 10/22/15 05:10
Mercury
ND mg/L 0.00020 1 10/23/1510:00
10/23/1513:41
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/10/2015 09:05.AM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 40

ceAnalytical"
www.pWalabs.com
I
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: 001 SLUDGE Lab ID: 92272649001 Collected: 10/19/15 13:00 Received: 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methyl phenol (o-C reso I)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4, 5-Trich loropheno I
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobe nzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
2540G Total Percent Solids
Total Solids
Date: 11 /10/2015 09:05 AM
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg 5.2 1 10/26/1513:20 10/27/1513:52 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 10/30/15 00:00
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
106-46-7
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
121-14-2
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
87-68-3
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
118-74-1
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
67-72-1
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
95-48-7
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
ND
ug/L
50.0
1
11102/1510:00
11/03/1514:58
98-95-3
ND
ug/L
100
1
11/02/1510:00
11/03/1514:58
87-86-5
ND
ug/L
50.0
1
11/02/1510:00
11103/1514:58
110-86-1
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
95-95-4
ND
ug/L
50.0
1
11/02/1510:00
11/03/1514:58
88-06-2
18
%
12-102
1
11 /02/15 10:00
11 /03/15 14:58
4165-60-0
22
%
13-107
1
11/02/1510:00
11/03/1514:58
321-60-8
56
%
21-132
1
11/02/1510:00
11/03/1514:58
1718-51-0
9
%
10-110
1
11/02/1510:00
11/03/1514:58
13127-88-3 SO
12
%
10-110
1
11/02/1510:00
11/03/1514:58
367-12-4
50
%
27-108
1
11/02/1510:00
11/03/1514:58
118-79-6
Analytical Method:
EPA8260 Leachate Method/Date:
EPA 1311; 10/26/15 11:12
ND
ug/L
100
20
10/31/15 08:56
71-43-2
ND
ug/L
200
20
10/31/15 08:56
78-93-3
ND
ug/L
100
20
10/31/15 08:56
56-23-5
ND
ug/L
100
20
10/31/15 08:56
108-90-7
ND
ug/L
100
20
10/31/15 08:56
67-66-3
ND
ug/L
100
20
10/31/15 08:56
106-46-7
ND
ug/L
100
20
10/31/15 08:56
107-06-2
ND
ug/L
100
20
10/31/15 08:56
75-35-4
ND
ug/L
100
20
10/31/15 08:56
127-18-4
ND
ug/L
100
20
10/31/15 08:56
79-01-6
ND
ug/L
100
20
10/31/15 08:56
75-01-4
124
%
70-130
20
10/31/15 08:56
17060-07-0
98
%
67-135
20
10/31/15 08:56
2037-26-5
105
%
70-130
20
10/31/15 08:56
460-00-4
Analytical Method: SM 2540G
0.090
%
0.000010
1
10/21/15 16:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 40

ceAnalytical
mvpacWabac=
....... .. ....
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: 001 SLUDGE
Lab ID: 92272649001 Collected:
10/19/15 13:00
Received: 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
99.9 %
0.10
1
10/22/15 12:53
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
10/30/15 11:30
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.2 Std. Units
0.10
1
10/22/15 11:40
H1
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
122000 mg/kg
0.12
1
11/05/15 17:20
N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
135000 mg/kg
10200
1
10/26/15 01:31
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
217000 mg/kg
55200
1
11/03/15 02:36
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA353.2
Nitrogen, Nitrate
26000 mg/kg
2180
1
11/03/15 10:31
Nitrogen, Nitrite
4160 mg/kg
1090
1
11/03/15 10:31
Nitrogen, NO2 plus NO3
30100 mg/kg
2180
1
11/03/15 10:31
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
142000 mg/kg
4150
2
10/28/1512:19
7723-14-0
Sample: 001 SLUDGE
Lab ID: 92272649002 Collected:
10/19/15 13:00
Received: 10/21/15 08:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Calcium
189000 ug/L
1000
1
11/05/1513:05
11/06/1515:41
7440-70-2
Magnesium
24200 ug/L
1000
1
11105/1513:05
11/06/1515:41
7439-95-4
Sodium
117000 ug/L
50000
1
11/05/1513:05
11/06/1515:41
7440-23-5
Sodium Adsorption Ratio, SAR
Analytical Method: EPA 6010
Sodium Adsorption Ratio
2.1 meq/L
1
11/09/15 17:02
N2
733C Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/L
0.010
1
10/22/15 22:30
734S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/L
1.0
1
10/22/15 18:30
Date: 11/10/2015 09:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 40

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92232729
Sample: MCAS 001 SLUDGE Lab ID: 92232729001 Collected: 01/08/15 11:30 Received: 01/09/15 11:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 01/22/15 10:54
ND ug/L
0.50
1
01/22/15 11:00
01/22/15 19:37
58-89-9
ND ug/L
3.0
1
01/22/15 11:00
01/22/1519:37
57-74-9
ND ug/L
0.50
1
01/22/15 11:00
01/22/1519:37
72-20-8
ND ug/L
0.50
1
01/22/15 11:00
01/22/1519:37
1024-57-3
ND ug/L
1000
1
01/22/15 11:00
01/22/1519:37
72-43-5
ND ug/L
3.0
1
01122/1511:00
01/22/1519:37
8001-35-2
46 %
10-138
1
01/22/15 11:00
01/22/1519:37
2051-24-3
56 %
10-110
1
01/22/15 11:00
01/22/1519:37
877-09-8
Analytical Method: EPA 8151
Preparation Method:
EPA 3510
ND mg/L
0.50
1
01/15/15 14:00
01/16/15 02:18
94-75-7
ND mg/L
0.50
1
01/15/15 14:00
01/16/15 02:18
93-72-1
88 %
42-142
1
01/15/15 14:00
01/16/15 02:18
19719-28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
18900 mg/kg
391
1
01/15/15 16:30
01/15/15 23:04
7429-90-5
ND mg/kg
39.1
1
01/15/15 16:30
01/16/15 16:15
7440-38-2
10.7 mg/kg
3.9
1
01/15/15 16:30
01/15/15 23:04
7440-43-9
19800 mg/kg
391
1
01/15/15 16:30
01/15/15 23:04
7440-70-2
860 mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7440-50-8
ND mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7439-92-1
2190 mg/kg
391
1
01/15/15 16:30
01/15/15 23:04
7439-95-4
ND mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7439-98-7
43.2 mg/kg
19.5
1
01/15/15 16:30
01/15/15 23:04
7440-02-0
ND mg/kg
19500
1
01/15/15 16:30
01/15/15 23:04
7440-09-7
ND mg/kg
39.1
1
01/15/15 16:30
01/15/15 23:04
7782-49-2
ND mg/kg
19500
1
01/15/15 16:30
01/15/15 23:04
7440-23-5
626 mg/kg
39.1
1
01/15/15 16:30
01/15/15 23:04
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 01/15/15 18:00
Arsenic
ND mg/L 0.050 1 01/16/15 15:45
01/17/15 00:41
7440-38-2
Barium
0.34 mg/L 0.25 1 01/16/15 15:45
01/17/15 00:41
7440-39-3
Cadmium
0.012 mg/L 0.0050 1 01/16/15 15:45
01/17/15 00:41
7440-43-9
Chromium
ND mg/L 0.025 1 01/16/15 15:45
01/17/15 00:41
7440-47-3
Lead
ND mg/L 0.025 1 01/16/15 15:45
01/17/15 00:41
7439-92-1
Selenium
ND mg/L 0.10 1 01/16/15 15:45
01/17/15 00:41
7782-49-2
Silver
ND mg/L 0.025 1 01/16/15 15:45
01/17/15 00:41
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 01/15/15 18:00
Mercury
ND ug/L 0.20 1 01/16/1514:35
01/16/1517:28
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /27/2015 11:05 AM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 29

�amalXicale
wwwpacelabs,00m
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92232729
Sample: MCAS 001 SLUDGE Lab ID: 92232729001 Collected: 01/08/15 11:30 Received: 01/09/15 11:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared
7471 Mercury
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
254OG Total Percent Solids
Total Solids
Date: 01 /27/2015 11:05 AM
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Analyzed CAS No. Qual
0.64 mg/kg 0.17 1 01/10/15 17:00 01/13/15 14:53 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 01/22/15 10:54
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
106-46-7
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
121-14-2
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
87-68-3
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
118-74-1
ND ug/L
50.0
1
01122/1512:20
01/23/15 13:30
67-72-1
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
95-48-7
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
98-95-3
ND ug/L
100
1
01/22/15 12:20
01/23/15 13:30
87-86-5
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
110-86-1
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
95-95-4
ND ug/L
50.0
1
01/22/15 12:20
01/23/15 13:30
88-06-2
60 %
12-102
1
01/22/15 12:20
01/23/15 13:30
4165-60-0
68 %
13-107
1
01/22/15 12:20
01/23/15 13:30
321-60-8
64 %
21-132
1
01/22/15 12:20
01/23/15 13:30
1718-51-0
21 %
10-110
1
01/22/15 12:20
01/23/15 13:30
13127-88-3
33 %
10-110
1
01/22/15 12:20
01/23/15 13:30
367-12-4
79 %
27-108
1
01 /22115 12:20
01/23/15 13:30
118-79-6
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 01/13/15 16:03
ND ug/L
5.0
1
01/16/1516:53
71-43-2
31.1 ug/L
10.0
1
01/16/1516:53
78-93-3
ND ug/L
5.0
1
01/16/1516:53
56-23-5
ND ug/L
5.0
1
01/1611516:53
108-90-7
ND ug/L
5.0
1
01/16/1516:53
67-66-3
ND ug/L
5.0
1
01/16/15 16:53
106-46-7
ND ug/L
5.0
1
01/16/1516:53
107-06-2
ND ug/L
5.0
1
01/16/1516:53
75-35-4
ND ug/L
5.0
1
01/16/1516:53
127-18-4
ND ug/L
5.0
1
01/16/15 16:53
79-01-6
ND ug/L
5.0
1
01/16/1516:53
75-01-4
100 %
70-130 1
95 %
67-135 1
92 %
70-130 1
Analytical Method: SM 2540G
2.0 %
0.000010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/16/1516:53 17060-07-0 TP
01/16/1516:53 2037-26-5
01/16/1516:53 460-00-4
01/13/15 15:30
Page 5 of 29

,�aceAnalyticale
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SLUDGE
Pace Project No.: 92232729
Sample: MCAS 001 SLUDGE
Lab ID: 92232729001 Collected:
01/08/15 11:30
Received: 01/09/15 11:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.0 %
0.10
1
01/14/15 08:12
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
01/23/15 11:00
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
5.5 Std. Units
0.10
1
01/12/15 14:05
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
18900 mg/kg
0.12
1
01/23/15 14:08
N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
680 mg/kg
500
1
01/13/1514:06
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
45200 mg/kg
2130
20
01/13/15 15:05
7727-37-9 M6
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
4860 mg/kg
498
5
01/21/15 20:32
M1
Nitrogen, Nitrite
330 mg/kg
249
5
01/21/15 20:32
Nitrogen, NO2 plus NO3
5190 mg/kg
498
5
01/21/15 20:32
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
31100 mg/kg
1320
5
01/21/15 04:35
7723-14-0 M1,R1
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
49.8
1
01/13/15 20:52
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
498
1
01/13/15 15:15
Sample: SAR Lab ID: 92232729002 Collected: 01/08/15 11:30 Received: 01/09/15 11:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Sodium 130000 ug/L 25000 5 01/15/15 15:10 01/15/15 20:38 7440-23-5
Sodium Adsorption Ratio, SAR Analytical Method: EPA 6010
Sodium Adsorption Ratio 1.8 meq/L 1 01/23/1516:00 N2
Date: 01 /27/2015 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 29

eAnalytical
xtirw.peceiabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE
Pace Project No.: 92244916
Sample: 001 SLUDGE Lab ID: 92244916001 Collected: 04/09/15 08:00 Received: 04/10/15 10:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA IS)
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 04/22/15 09:30
ND
ug/L
10.0
20
04/27/15 08:30
04/27/15 20:28
58-89-9
ND
ug/L
60.0
20
04/27/15 08:30
04/27/15 20:28
57-74-9
ND
ug/L
10.0
20
04/27/15 08:30
04/27/15 20:28
72-20-8
ND
ug/L
10.0
20
04/27/15 08:30
04/27/15 20:28
1024-57-3
ND
ug/L
20000
20
04/27/15 08:30
04/27/15 20:28
72-43-5
ND
ug/L
60.0
20
04/27/15 08:30
04/27/15 20:28
8001-35-2
0
%
10-138
20
04/27/15 08:30
04/27/15 20:28
2051-24-3 D3,S4
0
%
10-110
20
04/27/15 08:30
04/27/15 20:28
877-09-8
Analytical Method: EPA 8151
Preparation Method: EPA 3510
ND
mg/L
0.010
1
04/21/15 07:30
04/21/15 12:51
94-75-7
ND
mg/L
0.010
1
04/21/15 07:30
04/21/15 12:51
93-72-1
83
%
42-142
1
04/21/15 07:30
04/21/15 12:51
19719-28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
29000
mg/kg
364
1
04/14/15 16:45
04/15/15 21:30
7429-90-5
44.3
mg/kg
36.4
1
04/14/15 16:45
04/15/15 21:30
7440-38-2
19.4
mg/kg
3.6
1
04/14/15 16:45
04/15/15 21:30
7440-43-9
23100
mg/kg
364
1
04/14/15 16:45
04/15/15 21:30
7440-70-2
961
mg/kg
18.2
1
04/14/15 16:45
04/15/15 21:30
7440-50-8
20.3
mg/kg
18.2
1
04/14/15 16:45
04/15/15 21:30
7439-92-1
2420
mg/kg
364
1
04/14/15 16:45
04/15/15 21:30
7439-95-4
ND
mg/kg
18.2
1
04/14/15 16:45
04/15/15 21:30
7439-98-7
99.6
mg/kg
18.2
1
04/14/15 16:45
04/15/15 21:30
7440-02-0
ND
mg/kg
18200
1
04/14/15 16:45
04/15/15 21:30
7440-09-7
ND
mg/kg
36.4
1
04/14/15 16:45
04/15/15 21:30
7782-49-2
ND
mg/kg
18200
1
04/14/15 16:45
04/15/15 21:30
7440-23-5
682
mg/kg
36.4
1
04/14/15 16:45
04/15/15 21:30
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 04/14/15 00:55
Arsenic
ND mg/L 0.050 1 04/15/15 21:35
04/16/15 15:41
7440-38-2
Barium
0.27 mg/L 0.25 1 04/15/15 21:35
04/16/15 15:41
7440-39-3
Cadmium
0.017 mg/L 0.0050 1 04/15/15 21:35
04/16/15 15:41
7440-43-9
Chromium
ND mg/L 0.025 1 04/15/15 21:35
04/16/15 15:41
7440-47-3
Lead
ND mg/L 0.025 1 04/15/15 21:35
04/16/15 15:41
7439-92-1
Selenium
ND mg/L 0.10 1 04/15/15 21:35
04/16/15 15:41
7782-49-2
Silver
ND mg/L 0.025 1 04/15/15 21:35
04/16/15 15:41
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 04/14/15 00:55
Mercury
ND mg/L 0.00020 1 04/16/1511:10
04/16/1515:15
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2015 05:15 PM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 30

aceMalXical
/ www.pacelabs.com
i
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 001 SLUDGE
Pace Project No.: 92244916
Sample: 001 SLUDGE Lab ID: 92244916001 Collected: 04/09/15 08:00 Received: 04/10/15 10:00 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
7471 Mercury
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
2540G Total Percent Solids
Total Solids
Date: 04/28/2015 05:15 PM
Analytical Method: EPA 7471 Preparation Method: EPA 7471
0.50 mg/kg 0.13 1 04/11/1515:20 04/11/1519:13 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 04/22/15 09:30
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
106-46-7
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
121-14-2
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
87-68-3
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
118-74-1
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
67-72-1
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
95-48-7
683
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
L2
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
98-95-3
ND
ug/L
1000
10
04/23/15 08:20
04/24/15 10:01
87-86-5
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
110-86-1
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
95-95-4
ND
ug/L
500
10
04/23/15 08:20
04/24/15 10:01
88-06-2
0
%
12-102
10
04/23/15 08:20
04/24/15 10:01
4165-60-0
D3,S4
0
%
13-107
10
04/23/15 08:20
04/24/15 10:01
321-60-8
S4
0
%
21-132
10
04/23/15 08:20
04/24/15 10:01
1718-51-0
S4
0
%
10-110
10
04/23/15 08:20
04/24/15 10:01
13127-88-3
S4
0
%
10-110
10
04/23/15 08:20
04/24/15 10:01
367-12-4
S4
0
%
27-108
10
04/23/15 08:20
04/24/15 10:01
118-79-6
S4
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 04/20/15 10:47
ND
ug/L
100
20
04/28/15 14:17
71-43-2
ND
ug/L
200
20
04/28/15 14:17
78-93-3
ND
ug/L
100
20
04/28/15 14:17
56-23-5
ND
ug/L
100
20
04/28/15 14:17
108-90-7
ND
ug/L
100
20
04/28/15 14:17
67-66-3
ND
ug/L
100
20
04/28/15 14:17
106-46-7
ND
ug/L
100
20
04/28/15 14:17
107-06-2
ND
ug/L
100
20
04/28/15 14:17
75-35-4
ND
ug/L
100
20
04/28/15 14:17
127-18-4
ND
ug/L
100
20
04/28/15 14:17
79-01-6
ND
ug/L
100
20
04/28/15 14:17
75-01-4
110
%
70-130
20
04/28/15 14:17
17060-07-0
101
%
67-135
20
04/28/15 14:17
2037-26-5
108
%
70-130
20
04/28/15 14:17
460-00-4
Analytical Method: SM 2540G
2.4
%
0.000010
1
04/16/1514:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 30

CieAnalyNoI
www.pacwabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE
Pace Project No.: 92244916
Sample: 001 SLUDGE
Lab ID: 92244916001 Collected:
04/09/15 08:00
Received: 04/10/15 10:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
97.6 %
0.10 1
04/17/15 11:09
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0 1
04/16/15 14:00
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.6 Std. Units
0.10 1
04/13/15 13:30 H1
Plant Available Nitrogen
Analytical Method: SM 271013
Plant Available Nitrogen
25200 mg/kg
0.12 1
04/27/15 15:36 N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
12300 mg/kg
423 1
04/16/15 04:53 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
75700 mg/kg
1920
1
04/24/15 11:20 7727-37-9 M1
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg
83.7
1
04/23/15 19:05
Nitrogen, Nitrite
ND mg/kg
41.9
1
04/23/15 19:05
Nitrogen, NO2 plus NO3
ND mg/kg
83.7
1
04/23/15 19:05
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
39500 mg/kg
1690
10
04/21/1511:13 7723-14-0
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
42.2
1
04/16/15 19:34
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
422
1
04/16/15 16:00
Sample: SAR Lab ID: 92244916002 Collected: 04/09/15 08:00 Received: 04/10/15 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Calcium
Magnesium
Sodium
Sodium Adsorption Ratio, SAR
Sodium Adsorption Ratio
Date: 04/28/2015 05:15 PM
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
483000 ug/L
1000 2
04113/1514:30 04127/1517:04 7440-70-2
47600 ug/L
1000 2
04/13/1514:30 04/27/1517:04 7439-95-4
144000 ug/L
25000 1
04/13/1514:30 04/15/1517:48 7440-23-5
Analytical Method: EPA6010
1.7 meq/L
1
04/28/1512:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
N2
Page 6 of 30

,�aceAnalyticalo
www.paceAsbs.corn
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 001 SLUDGE/CHLOROPHYLLA
Pace Project No.: 92257870
Sample: 001 SLUDGE Lab ID: 92257870001 Collected: 07/08/15 10:00 Received: 07/09/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
:%ir[rL51�111[y:
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
Date: 08/11/2015 11:32 AM
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 07/21/15 09:00
ND
ug/L
0.50
1
07/22/1510:00
07/22/1515:40
58-89-9
ND
ug/L
3.0
1
07/22/1510:00
07/22/1515:40
57-74-9
ND
ug/L
0.50
1
07/2211510:00
07/22/1515:40
72-20-8
ND
ug/L
0.50
1
07/22/1510:00
07/22/1515:40
1024-57-3
ND
ug/L
1000
1
07/22/1510:00
07/22/1515:40
72-43-5
ND
ug/L
3.0
1
07/22/1510:00
07/22/1515:40
8001-35-2
53
%
10-138
1
07/22/1510:00
07/22/1515:40
2051-24-3
60
%
10-110
1
07/22/1510:00
07/22/1515:40
877-09-8
Analytical Method:
EPA 8151
Preparation Method: EPA 3510
ND
mg/L
0.64
1
07/17/15 08:00
07/18/15 04:39
94-75-7
ND
mg/L
0.64
1
07/17/15 08:00
07/18/15 04:39
93-72-1
107
%
42-142
1
07/17/15 08:00
07/18/15 04:39
19719-28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
9090
mg/kg
564
1
07/10/1518:15
07/14/1517:12
7429-90-5
ND
mg/kg
56.4
1
07/10/1518:15
07/14/1517:12
7440-38-2
31.3
mg/kg
5.6
1
07/10/1518:15
07/1411517:12
7440-43-9
18800
mg/kg
564
1
07/10/1518:15
07/14/1517:12
7440-70-2
760
mg/kg
28.2
1
07/10/1518:15
07/14/1517:12
7440-50-8
ND
mg/kg
28.2
1
07/10/1518:15
07/14/1517:12
7439-92-1
1970
mg/kg
564
1
07/10/1518:15
07/14/1517:12
7439-95-4
ND
mg/kg
28.2
1
07/10/1518:15
07/14/1517:12
7439-98-7
35.8
mg/kg
28.2
1
07/10/1518:15
07/14/1517:12
7440-02-0
ND
mg/kg
28200
1
07/10/1518:15
07/14/1517:12
7440-09-7
ND
mg/kg
56.4
1
07/10/1518:15
07/14/1517:12
7782-49-2
ND
mg/kg
28200
1
07/10/1518:15
07/14/1517:12
7440-23-5
569
mg/kg
56.4
1
07/10/1518:15
07/14/1517:12
7440-66-6
Analytical Method: EPA 6010 Preparation Method: EPA3010
Leachate Method/Date: EPA 1311; 07/14/15 00:45
ND
mg/L
0.050
1
07/15/15 03:00
07/16/15 13:45
7440-38-2
ND
mg/L
0.25
1
07/15/15 03:00
07/16/15 13:45
7440-39-3
0.016
mg/L
0.0050
1
07/15/15 03:00
07/16/15 13:45
7440-43-9
ND
mg/L
0.025
1
07/15/15 03:00
07/16/15 13:45
7440-47-3
ND
mg/L
0.025
1
07/15/15 03:00
07/16/15 13:45
7439-92-1
ND
mg/L
0.10
1
07/15/15 03:00
07/16/15 13:45
7782-49-2
ND
mg/L
0.025
1
07/15/15 03:00
07/16/15 13:45
7440-22A
Analytical Method: EPA 7470 Preparation Method:
EPA
7470
Leachate Method/Date: EPA 1311; 07/14/15 00:45
ND
mg/L
0.00020
1
07/15/1510:00
07/15/1514:11
7439-97-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 34

�-aceAnalyficale
www.pacelabs.com
race nnaryucai aervice5, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE/CHLOROPHYLLA
Pace Project No.: 92257870
Sample: 001 SLUDGE Lab ID: 92257870001 Collected: 07/08/15 10:00 Received: 07/09/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobe nzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
::YZ�rLL69�iltd��
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
254OG Total Percent Solids
Total Solids
Date: 08/11 /2015 11:32 AM
0.72 mg/kg 0.31 1 07/17/1512:55 07/20/1515:46 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 07/21/15 09:00
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
106-46-7
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
121-14-2
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
87-68-3
ND
ug/L
50.0
1
07/22/1510:00
07/2311512:30
118-74-1
10
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
67-72-1
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
95-48-7
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
98-95-3
ND
ug/L
100
1
07/22/1510:00
07/23/1512:30
87-86-5
10
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
110-86-1
ND
ug/L
50.0
1
07/2211510:00
07/23/1512:30
95-95-4
ND
ug/L
50.0
1
07/22/1510:00
07/23/1512:30
88-06-2
15
%
12-102
1
07/22/1510:00
07/23/1512:30
4165-60-0
14
%
13-107
1
07/22/1510:00
07/23/1512:30
321-60-8
62
%
21-132
1
07/22/1510:00
07/23/1512:30
1718-51-0
7
%
10-110
1
07/22/1510:00
07/23/1512:30
13127-88-3
S5
9
%
10-110
1
07/22/1510:00
07/23/1512:30
367-12-4
S5
36
%
27-108
1
07/22/1510:00
07/23/1512:30
118-79-6
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 07/13/15 09:50
ND
ug/L
100
20
07/16/15 17:33
71-43-2
ND
ug/L
200
20
07/16/15 17:33
78-93-3
ND
ug/L
100
20
07/16/15 17:33
56-23-5
ND
ug/L
100
20
07/16/15 17:33
108-90-7
ND
ug/L
100
20
07/16/15 17:33
67-66-3
ND
ug/L
100
20
07/16/15 17:33
106-46-7
ND
ug/L
100
20
07/16/15 17:33
107-06-2
ND
ug/L
100
20
07/16/15 17:33
75-35-4
ND
ug/L
100
20
07/16/15 17:33
127-18-4
ND
ug/L
100
20
07/16/15 17:33
79-01-6
ND
ug/L
100
20
07/16/15 17:33
75-01-4
99
%
70-130
20
07/16/15 17:33
17060-07-0
101
%
67-135
20
07/16/15 17:33
2037-26-5
82
%
70-130
20
07/16/15 17:33
460-00-4
Analytical Method: SM 2540G
1.6 % 0.000010 1 07/11/15 02:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 34

coAnalytical
www.pacWabs.com
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 001 SLUDGE/CHLOROPHYLLA
Pace Project No.: 92257870
Sample: 001 SLUDGE
Lab ID: 92267870001 Collected:
07/08/15 10:00
Received: 07/09/15 09:30 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.4 %
0.10
1
07/13/15 14:30
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
07/14/15 12:20
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.0 Std. Units
0.10
1
07/10/15 12:00
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
23400 mg/kg
0.12
1
07/23/15 15:40
N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
11000 mg/kg
630
1
07/14/15 08:26
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
66300 mg/kg
2380
1
07/20/15 14:20
7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
1300 mg/kg
128
1
07/15/15 11:39
Nitrogen, Nitrite
ND mg/kg
64.0
1
07/15/15 11:39
Nitrogen, NO2 plus NO3
1300 mg/kg
128
1
07/15/15 11:39
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
50600 mg/kg
1610
5
07/21/1512:15
7723-14-0
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
64.3
1
07/17/15 00:37
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
641
1
07/16/15 16:00
Sample: 001 SLUDGE SAR Lab ID: 92257870003 Collected: 07/08/15 10:00 Received: 07/09/15 09:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Calcium 305000 ug/L 1000 10 07/23/1516:45 07/24/1517:03 7440-70-2
Magnesium 29300 ug/L 100 1 07/23/1516:45 07/24/1515:44 7439-95-4
Sodium 99200 ug/L 50000 10 07/23/1516:45 07/24/1517:03 7440-23-5
Sodium Adsorption Ratio, SAR Analytical Method: EPA 6010
Sodium Adsorption Ratio 1.4 meq/L 1 07/27/15 13:05 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11 /2015 11:32 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 34

�Analytical"
www.pacslabs.00m
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: 001 SLUDGE Lab ID: 92272649001 Collected: 10/19/15 13:00 Received: 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
Analytical Method: EPA 8081
Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 10/30/15 00:00
gamma-BHC (Lindane)
ND
ug/L
0.50 1
11/03/15 09:20
11/03/15 13:26
58-89-9
Chlordane (Technical)
ND
ug/L
3.0 1
11/03/15 09:20
11/03/15 13:26
57-74-9
Endrin
ND
ug/L
0.50 1
11/03/15 09:20
11/03/15 13:26
72-20-8
Heptachlor epoxide
ND
ug/L
0.50 1
11/03/15 09:20
11/03/15 13:26
1024-57-3
Methoxychlor
ND
ug/L
1000 1
11/03/15 09:20
11/03/15 13:26
72-43-5
Toxaphene
ND
ug/L
3.0 1
11/03/15 09:20
11/03/15 13:26
8001-35-2
Surrogates
Decachlorobiphenyl (S)
40
%
10-138 1
11/03/15 09:20
11/03/15 13:26
2051-24-3
Tetrachloro-m-xylene (S)
35
%
10-110 1
11/03/15 09:20
11/03/15 13:26
877-09-8
8151 Chlorinate Herbicide TCLP
Analytical Method; EPA 8151
Preparation Method: EPA 3510
2,4-D
ND
mg/L
11.0 1
10/30/15 08:20
10/30/15 15:41
94-75-7
2,4,5-TP (Silvex)
ND
mg/L
11.0 1
10/30/15 08:20
10/30/15 15:41
93-72-1
Surrogates
2,4-DCAA (S)
102
%
42-142 1
10/30/15 08:20
10/30/15 15:41
19719-28-9
6010 MET ICP
Analytical Method: EPA 6010
Preparation Method: EPA 3050
Aluminum
30400
mg/kg
9200 1
10/22/15 20:30
10/27/15 01:47
7429-90-5
Arsenic
ND
mg/kg
920 1
10/22/15 20:30
10/27/15 01:47
7440-38-2
Cadmium
ND
mg/kg
92.0 1
10/22/15 20:30
10/27/15 01:47
7440-43-9
Calcium
130000
mg/kg
9200 1
10/22/15 20:30
10/27/15 01:47
7440-70-2
Copper
1700
mg/kg
460 1
10/22/15 20:30
10/27/15 01:47
7440-50-8
Lead
ND
mg/kg
460 1
10/22/15 20:30
10/27/15 01:47
7439-92-1
Magnesium
19000
mg/kg
9200 1
10/22/15 20:30
10/27/15 01:47
7439-95-4
Molybdenum
ND
mg/kg
460 1
10/22/15 20:30
10/27/15 01:47
7439-98-7
Nickel
ND
mg/kg
460 1
10/22/15 20:30
10/27/15 01:47
7440-02-0
Potassium
ND
mg/kg
460000 1
10/22/15 20:30
10/27/15 01:47
7440-09-7
Selenium
ND
mg/kg
920 1
10/22/15 20:30
10/27/15 01:47
7782-49-2
Sodium
ND
mg/kg
460000 1
10/22/15 20:30
10/27/15 01:47
7440-23-5
Zinc
1930
mg/kg
920 1
10/22/15 20:30
10/27/15 01:47
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA
1311; 10/22/15 05:10
Arsenic
ND
mg/L
0.050 1
10/23/15 02:30
10/23/15 17:04
7440-38-2
Barium
ND
mg/L
0.25 1
10/23/15 02:30
10/23/15 17:04
7440-39-3
Cadmium
ND
mg/L
0.0050 1
10/23/15 02:30
10/23/15 17:04
7440-43-9
Chromium
ND
mg/L
0.025 1
10/23/15 02:30
10/23/15 17:04
7440-47-3
Lead
ND
mg/L
0.025 1
10/23/15 02:30
10/23/15 17:04
7439-92-1
Selenium
ND
mg/L
0.10 1
10/23/15 02:30
10/23/15 17:04
7782-49-2
Silver
ND
mg/L
0.025 1
10/23/15 02:30
10/23/15 17:04
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA
7470
Leachate Method/Date: EPA 1311; 10/22/15 05:10
Mercury
ND
mg/L
0.00020 1
10/23/1510:00
10/23/1513:41
7439-97-6
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/10/2015 09:05.AM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 40

agemaly�ical
wwwpaceeb&com
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: 001 SLUDGE
Lab ID: 92272649001
Collected: 10/19/15 13:00
Received: 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND
mg/kg
5.2
1
10/26/1513:20
10/27/1513:52
7439-97-6
8270 MSSV TCLP Sep Funnel
Analytical Method:
EPA 8270
Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 10/30/15 00:00
1,4-Dichlorobenzene
ND
ug/L
50.0
1
11/02/15 10:00
11/03/15 14:58
106-46-7
2,4-Dinitrotoluene
ND
ug/L
50.0
1
11/02/15 10:00
11/03/15 14:58
121-14-2
Hexachloro-1,3-butadiene
ND
ug/L
50.0
1
11/02/15 10:00
11103/1514:58
87-68-3
Hexachlorobenzene
ND
ug/L
50.0
1
11/02/15 10:00
11/03/15 14:58
118-74-1
Hexachloroethane
ND
ug/L
50.0
1
11/02/15 10:00
11/03/15 14:58
67-72-1
2-Methylphenol(o-Cresol)
ND
ug/L
50.0
1
11/02/15 10:00
11/03/15 14:58
95-48-7
3&4-Methylphenol(m&p Cresol)
ND
ug/L
50.0
1
11/02/15 10:00
11/03/15 14:58
Nitrobenzene
ND
ug/L
50.0
1
11/02/15 10:00
11/03/15 14:58
98-95-3
Pentachlorophenol
ND
ug/L
100
1
11/02/15 10:00
11/0311514:58
87-86-5
Pyridine
ND
ug/L
50.0
1
11/02/15 10:00
11/0311514:58
110-86-1
2,4,5-Trichlorophenol
ND
ug/L
50.0
1
11/02/15 10:00
11103/1514:58
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
50.0
1
11/02/15 10:00
11103/1514:58
88-06-2
Surrogates
Nitrobenzene-d5(S)
18
%
12-102
1
11/02/15 10:00
11103/1514:58
4165-60-0
2-Fluorobiphenyl(S)
22
%
13-107
1
11/02/15 10:00
11/03/15 14:58
321-60-8
Terphenyl-d14 (S)
56
%
21-132
1
11/02/15 10:00
11/03/15 14:58
1718-51-0
Phenol-d6 (S)
9
%
10-110
1
11/02/15 10:00
11/03/15 14:58
13127-88-3 SO
2-Fluorophenol (S)
12
%
10-110
1
11/02/15 10:00
11/03/15 14:58
367-12-4
2,4,6-Tribromophenol (S)
50
%
27-108
1
11/02/15 10:00
11/03/15 14:58
118-79-6
8260 MSV TCLP
Analytical Method: EPA8260 Leachate Method/Date:
EPA 1311; 10/26/15 11:12
Benzene
ND
ug/L
100
20
10/31/15 08:56
71-43-2
2-Butanone (MEK)
ND
ug/L
200
20
10/31/15 08:56
78-93-3
Carbon tetrachloride
ND
ug/L
100
20
10/31/15 08:56
56-23-5
Chlorobenzene
ND
ug/L
100
20
10/31/15 08:56
108-90-7
Chloroform
ND
ug/L
100
20
10/31/15 08:56
67-66-3
1,4-Dichlorobenzene
ND
ug/L
100
20
10/31/15 08:56
106-46-7
1,2-Dichloroethane
ND
ug/L
100
20
10/31/15 08:56
107-06-2
1,1-Dichloroethene
ND
ug/L
100
20
10/31/15 08:56
75-35-4
Tetrachloroethene
ND
ug/L
100
20
10/31/15 08:56
127-18-4
Trichloroethene
ND
ug/L
100
20
10/31/15 08:56
79-01-6
Vinyl chloride
ND
ug/L
100
20
10/31/15 08:56
75-01-4
Surrogates
1,2-Dichloroethane-d4 (S)
124
%
70-130
20
10/31/15 08:56
17060-07-0
Toluene-d8 (S)
98
%
67-135
20
10/31/15 08:56
2037-26-5
4-Bromofluorobenzene (S)
105
%
70-130
20
10/31/15 08:56
460-00-4
2540G Total Percent Solids
Analytical Method:
SM 2540G
Total Solids
0.090
%
0.000010
1
10/21/15 16:53
Date: 11 /10/2015 09:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 40

aceMaIXical
www.pmbbacom
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: 001 SLUDGE
Lab ID: 92272649001 Collected:
10/19/15 13:00
Received: 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
99.9 %
0.10
1
10/22/15 12:53
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
10/30/15 11:30
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.2 Std. Units
0.10
1
10/22/15 11:40
H1
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
122000 mg/kg
0.12
1
11/05/15 17:20
N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
135000 mg/kg
10200
1
10/26/15 01:31
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
217000 mg/kg
55200
1
11/03/15 02:36
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
26000 mg/kg
2180
1
11/03/15 10:31
Nitrogen, Nitrite
4160 mg/kg
1090
1
11/03/15 10:31
Nitrogen, NO2 plus NO3
30100 mg/kg
2180
1
11/03/15 10:31
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
142000 mg/kg
4150
2
10/28/1512:19
7723-14-0
Sample: 001 SLUDGE
Parameters
Lab ID: 92272649002 Collected: 10/19/15 13:00
Results Units Report Limit DF
Received: 10/21/15 08:00 Matrix: Water
Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Calcium
189000 ug/L
1000
1
11/05/1513:05
11/06/1515:41
7440-70-2
Magnesium
24200 ug/L
1000
1
11/05/1513:05
11/06/1515:41
7439-95-4
Sodium
117000 ug/L
50000
1
11/05/1513:05
11/0611515:41
7440-23-5
Sodium Adsorption Ratio, SAR
Analytical Method: EPA 6010
Sodium Adsorption Ratio
2.1 meq/L
1
11/09/1517:02
N2
733C Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/L
0.010
1
10/22/15 22:30
734S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/L
1.0
1
10/22/15 18:30
Date: 11 /10/2015 09:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 40

PATHOGEN/VECTOR ATTRACTION REDUCTION FORM

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: US Marine Corps - Cherry Point Permit Number: WQ0001489
WWTP Name: USMCAS - Cherry Point WWTP NPDES Number: NC0003816
Monitoring Period: From 1/1/2015 To 12/31/2015
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 101 .
Alternative.2 ®
Altemative:3 ❑
Alternative 4 ❑
Alternative 5
A1 ternative 6
If applicable to alternative performed (Class A only)'indicate "Process to'Further Reduce Pathogens":
Compost ❑:
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Be
Beta Ray
Y
Gamma Ray
Pasteurization
Past n ❑.
Class B:
Alternative 1 ❑
Alternative 2 x
Alternative -3 ❑
:.....................
If applicable to alternative performed (Class B only) .indicate "Process :to Significantly Reduce Pathogens":
Lime Stabilization X
Air Drying❑
Composting
❑
Aerobic Digestion ❑
Anaerobic Digestion[]
i es
g
If applicable to alternative performed (Class A or Class B) complete the
following monitorin data:
Allowable Level
Pathogen Density:: Number
of
Frequency
Sample
Analytical
Parameter
in Sludge
inimu
Geo. Mean
Maximurr
-Units
Excee-
dences.
of
Anal sis
_
Type
Tech -
nioue
2 x 10 to the 6th
power MPN per
gram of total
solids or 2 x 10 to
Fecal Coliform the 6th power
1000 mpn per
gram of total solid
ISalmonella bacterial 3 MPN per 4
(i.n,lieu of fecal grams total solid
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Dption 1 ❑ 1 Option 2 ❑ Option 3 ® Option 4. ❑ Option 5 ❑
Option Option 10 Dtion 6 X Option 7 Option 8 9 ❑ ❑
P P P P P
No vector attraction reduction options pe
rformed
CERTIFICATION STATEMENT (please check the appropriate statement)
X "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination. has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Patricia T. Davis - ORC
Pre r Name and Title (t or print)
Signature of Prepare Date
Land Applier Name and Title (if applicable)(type or print)
Signature of.Land Applier (if applicable) Date
DENR FORM RF (5/2003)

PATHOGEN/VECTOR ATTRACTION REDUCTION
SUPPORTING DOCUMENTATION
(LIME STABILIZATION):
LAB ANALYSIS BENCH SHEETS

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDEI 22
SOLIDS ANALYSIS BENCH SHEET
EVENT 7
ANALYST
BRIGMAN JDATE
1/5/2015
SAMPLE
HOLDING TANK TYPE
GRAB
TIME 1000 VOLUME
100
WO/LIME W/LIME
PERCENT -SOLIDS
3.16% 3.83%
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
"10-0412.471
10.95
90.20
PH MONITORING REPORT
SAMPLE DATE
TIME ANAI, PH TEMP C
'EMP CORI ACT PH
INITIALS
INITIAL PF 1/5/2015
1.020 5.38 20.7
-0.12 5.26
DB
1ST 1 /6/2015
1310 12.14 20.7
-0.12 12.02
DB
2ND 1/6/2015
1520 12.20 19.6
-0.15 12.05
DB
FINAL 1/7/2015
1325 11.87 17.8
-0.21 11.66
DB
FINAL CALIBRATION
RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00 SLOPE My/Ph % AGREEMENT
9.981 12.47
10.93
91.4
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
192.8702 grams
96.0389 grams
96.8313 grams
99.0964 grams
96.0389 grams
3.0575 grams
W/LIME
190.2357
99.6565
90.5792
103.1218
99.6565
3.4653
WEIGHT OF DRIED SAMPLE: 1 3.0575 igrams X 1001 3.4653
WEIGHT OF WET SAMPLE: 1 96.8313 lgrams 1 90.5792
3.1575531 3.8257131% TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST SHIMMEL JDATE
SAMPLE HOLDING TANK TYPE
TIME 1237 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS 2.45% 3.03%
EVENT
1/18/2015
GRAB
100
0
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK.
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
10.00 12.45
11.34
PH MONITORING REPORT
88.10
SAMPLE DATE
TIME ANAI.
PH TEMP C
EMP CORI,
ACT PH
INITIALS
INITIAL PF 1/18/2015
1ST 1 /19/2015
2ND 1/19/2015
FINAL 1/20/20151
1237
1300
1500
13001
5.91 16.5
12.37 16.9
12.41 16.9
11.981 19.9
-0.24
-0.24
-0.24
-0.151
5.67
FS
12.13
FS
12.17
FS
11.83
FS
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
10.001 12.461
10.92
90.2
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME W/LIME
179.8509 grams 182.1415
103.6295 grams 94.5541
76.2214 grams 87.5874
105.4983 grams 97.211
103.6295 grams 94.5541
1.8688 grams 2.6569
WEIGHT OF DRIED SAMPLE: 1 1.8688 grams X 1001 2.6569
WEIGHT OF WET SAMPLE: 1 76.2214 lqrams 1 87.5874
2.4518051 3.0334271% TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST BRIGMAN JDATE
SAMPLE HOLDING TANK TYPE
TIME 930 VOLUME
WO/LIME W/LIME
"PERCENTLIDS 2.787 3.51%
EVENT
1/22/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1
12.45
11.00 SLOPE My/Ph % AGREEMENT
9.99
12.471
10.90
PH MONITORING REPORT
93.10
SAMPLE
DATE
nME ANAI.
PH
TEMP C
EMP CORI
ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
1/22/2015
1400
1245
1445
12551
6.06
16.2
16.5
16.4
16.7
-0.27
-0.27
-0.27
-0.271
5.79
DB
1 /23/2015
12.27
12.00
DB
1/23/2015
1/24/20151
12.30
12.03
DB
12.011
11.741
JB
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00
1 12.45
11.00
SLOPE My/Ph % AGREEMENT
10.01
12.57
11.11
88.2
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME W/LIME
197.2029 grams 196.3473
102.2642 grams 103.7921
94.9387 grams 92.5552
104.9008 grams 107.0407
102.2642 grams 103.7921
2.6366 grams 3.2486
WEIGHT OF DRIED SAMPLE: 2.6366 grams X 100 3.2486
WEIGHT OF WET SAMPLE: 94.9387 grams 92.5552
2.77716 3.509905 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST ARMISTEAD JDATE
SAMPLE HOLDING TANK TYPE
TIME 1300 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS #DIV/0! 3.08%
EVENT
1/30/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00
SLOPE My/Ph % AGREEMENT
10.02 12.471
11.00
95.10
PH MONITORING REPORT
SAMPLE
I DATE
TIME ANA
PH
TEMP C
EMP CORI
ACT PH
INITIALS
INITIAL PH
1ST
2ND
FINAL
1325
1527
13501
16
16
16
-0.27
-0.27
-0.271
0.00
1 /30/2015
12.43
12.16
RA
1/30/2015
1/31/20151
12.37
12.10
RA
12.15
11.881
RA
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
9.98
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME W/LIME
grams 177.4087
grams 94.0909
0 grams 83.3178
grams 96.6589
0 grams 94.0909
0 grams 2.568
WEIGHT OF DRIED SAMPLE: 0 grams X 100 2.568
WEIGHT OF WET SAMPLE: 0 grams 83.3178
#DIV/0! 3.082175 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST BRIGMAN DATE
SAMPLE HOLDING TANK TYPE
TIME 1450 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS 2.95% 3.81%
EVENT
3/3/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
10.03 12.47
10.97
PH MONITORING REPORT
90.50
SAMPLE
DATE
TIME ANAI.
PH TEMP C
'EMP CORI
ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
3/1/2015
1450
1330
1530
1400
6.81 12.1
12.47 13.8
12.42 13.7
12.02 16
-0.34
-0.33
-0.33
-0.27
6.47
DLB
3/3/2015
12.14
DLB
3/3/2015
3/4/2015
12.09
DLB
11.75
DLB
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00
SLOPE My/Ph % AGREEMENT
10.051 12.47
10.96
90.5
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
196.9699 grams
103.7964 grams
93.1735 grams
106.5415 grams
103.7964 grams
2.7451 grams
W/LIME
189.8897
102.4686
87.4211
105.802
102.4686
3.3334
WEIGHT OF DRIED SAMPLE: 2.7451 grams X 100 3.3334
WEIGHT OF WET SAMPLE: 93.1735 grams 87.4211
2-9469941 3.813038 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST BRIGMAN DATE
SAMPLE HOLDING TANK TYPE
TIME 900 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS 2.74% 3.60%
EVENT
r 3/25/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00
SLOPE My/Ph % AGREEMENT
6il0.04 12.551
10.97
96.00
PH MONITORING REPORT
SAMPLE
DATE
rIME ANAI.
PH TEMP C
EMP CORI,
ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
3/25/2015
0905
1315
1515
13251
7.54 20.2
12.24 18.4
12.22 18.3
12.181 19.4
-0.15
-0.21
-0.21
-0.181
7.39
DLB
3/25/2015
12.03
DLB
3/25/2015
3/26/20151
12.01
DLB
12.001
DLB
FINAL CALIBRATION
RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
10.041 12.541
11.03
95.7
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
142.0848 grams
94.4843 grams
47.6005 grams
W/LIME
150.2573
103.7969
46.4604
95.7887 grams 105.4709
94.4843 grams 103.7969
1.3044 grams 1.674
WEIGHT OF DRIED SAMPLE: 1.3044 grams X 100 1.674
WEIGHT OF WET SAMPLE: 47.6005 grams 46.4604
2.7403071 3.603068 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST MARK JONES DATE
SAMPLE HOLDING TANK TYPE
TIME 2050 VOLUME
WO/LIME W/LIME
RCENT SOLIDS 3.05% 3.88%
i
EVENT
4/1/2015
r GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
10.03 12.521
11.30
88.20
PH MONITORING REPORT
SAMPLE
DATE
riME ANAI.
PH
TEMP C
'EMP CORI ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
3/30/2015
2050
1345
1555
1340
7.69
21.3
21.3
21.7
21.9
-0.12 7.57
-0.12 12.02
-0.09 12.10
-0.09 11.631
MJ
JEB
DLB
EW
4/1/2015
12.14
4/1/2015
4/2/2015
12.19
11.72
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
10.01 12.47
10.79
94.3
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WO/LIME W/LIME
WEIGHT OF DISH AND WET SAMPLE 166.4921 grams 191.6805
WEIGHT OF DISH 94.5561 grams 94.4858
WEIGHT OF WET SAMPLE 71.936 grams 97.1947
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
96.7474 grams
94.5561 grams
2.1913 grams
98.2525
94.4858
3.7667
WEIGHT OF DRIED SAMPLE: 2.1913 grams X 100 3.7667
WEIGHT OF WET SAMPLE: 71.936 grams 97.1947
3.046181 3.875417 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST ERVIN WADE JDATE
SAMPLE HOLDING TANK TYPE
TIME 1920 VOLUME
WO/LIME W/LIME
"PERCENTLIDS 2.55% 1 3.35%
EVENT
4/8/2015
F GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
10.04 12.571
11.05
PH MONITORING REPORT
93.40
SAMPLE
DATE
rIME ANAI
PH
TEMP C
'EMP CORI
ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
4/8/2015
1930
2100
2300
21001
7.34
22
22.7
22.7
23.3
-0.09
-0.06
-0.06
-0.061
7.25
EW
4/9/2015
12.30
12.24
EW
4/9/2015
4/10/20151
12.16
12.10
EW
11.951
11.891
EW
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
10.051 12.581
10.9
89.7
50LIDS WORKSHEET HOLDING TANK WITH LIME
WO/LIME W/LIME
WEIGHT OF DISH AND WET SAMPLE 192.9769 grams 198.8653
WEIGHT OF DISH 94.4856 grams 103.7975
WEIGHT OF WET SAMPLE 98.4913 grams 95.0678
WEIGHT OF DISH AND DRIED SAMPLE 96.9924 grams 106.9807
WEIGHT OF DISH 94.4856 grams 103.7975
WEIGHT OF DRIED SAMPLE 2.5068. grams 3.1832
WEIGHT OF DRIED SAMPLE: 2.5068 grams X 100 �18321
WEIGHT OF WET SAMPLE: 98.4913 grams
2.545199 3.348347 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST DAVID BRIGMAN JDATE
SAMPLE HOLDING TANK TYPE
TIME 1345 VOLUME
WO/LIME W/LIME
"PERCENTLIDS 2.36% 3.14%
EVENT
4/20/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00 SLOPE My/Ph % AGREEMENT
6il0.04 12.52
10.90
PH MONITORING REPORT
91.20
SAMPLE
DATE
TIME ANAL
PH TEMP C
EMP.CORI ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
4/20/2015
1350
0012
1435
12401
7.46 23
12.28 23.6
12.19 23.7
11.761 23.8
-0.06 7.40
-0.03 12.25
-0.03 12.16
-0.031 11.731
DLB
DLB
DLB
DLB
4/21/2015
4/21/2015
4/22/20151
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
10.051 12.46
10.94
197.6
SULIUg WUHKSHEET HULDING TANK WITH LIME
WO/LIME W/LIME
WEIGHT OF DISH AND WET SAMPLE 190.7695 grams 197.5587
WEIGHT OF DISH 94.4836 grams 103.7989
WEIGHT OF WET SAMPLE 96.2859 grams 93.7598
WEIGHT OF DISH AND DRIED SAMPLE 96.7526 grams 106.7474
WEIGHT OF DISH 94.4836 grams 103.7989
WEIGHT OF DRIED SAMPLE 2.269 grams 2.9485
WEIGHT OF DRIED SAMPLE: 2.269 grams X 100 aTOTAL
WEIGHT OF WET SAMPLE: 96.2859 grams 2.356524 .1.144738 %

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST DAVID BRIGMAN JDATE
SAMPLE HOLDING TANK TYPE
TIME 1330 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS 3.13% 3.70%
EVENT
4/27/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
6il0.03 12.461
10.97
PH MONITORING REPORT
92.30
SAMPLE
DATE
nME TN'Al PH
TEMP C
'EMP CORI ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
4/27/2015
1340 7.69
1225 12.06
1440 12.15
1240 11.83
23.7
22.7
25.1
22.8
-0.03 7.66
-0.06 12.00
0.00 12.15
1 -0.06 11.77
DLB
DLB
DLB
DLB
4/28/2015
4/28/2015
4/24/2015
FINAL CALIBRATION
RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
10.041 12.561
10.97
91.1
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
198.4199 grams
103.801 grams
94.6189 grams
106.7667 grams
103.801 grams
2.9657 grams
W/LIME
197.1674
103.4686
93.6988
106.9328
103.4686
3.4642
WEIGHT OF DRIED SAMPLE: 2.9657 grams X 100 3.4642
WEIGHT OF WET SAMPLE: 94.6189 grams 93.6988
3.134363 3.697156 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST ARMISTEAD/BRIGMAN JDATE
SAMPLE HOLDING TANK TYPE
TIME 640 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS 2.95% 4.20%
EVENT
5/5/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00
SLOPE My/Ph % AGREEMENT
10.04 12.54
10.93
91.40
PH MONITORING REPORT
SAMPLE
DATE
nME ANAI.
PH
TEMP C
EMP CORI ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
5/5/2015
0640
1155
1400
12201
7.66
24
26.9
25.7
25.91
-0.03 7.63
0.06 12.31
0.03 12.06
0.031 11.661
RA
DLB
DLB
DLB
5/5/2015
12.25
5/5/2015
5/6/20151
12.03
11.63
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
10.051 12.581
10.98
90.8
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
178.0979 grams
102.4703 grams
75.6276 grams
104.7023 grams
102.4703 grams
2.232 grams
W/LIME
192.8494
103.7979
89.0515
107.5348
103.7979
3.7369
WEIGHT OF DRIED SAMPLE: 2.232 grams X 100 3.7369
WEIGHT OF WET SAMPLE: 75.6276 grams 89.0515
2.9513031 4.196336 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST SHIMMEL JDATE
SAMPLE HOLDING TANK TYPE
TIME 1430 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS 2.17% 3.08%
EVENT
5/12/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00 SLOPE My/Ph %-AGREEMENT
"10-0312.5-41
10.97
PH MONITORING REPORT
92.00
SAMPLE
DATE
nME ANA
PH TEMP C
'EMP CORI
ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
5/11/2015
1430
1410
1610
14121
7.30 24.1
12.26 25.8
12.17 26.2
11.81 271
-0.03
0.03
0.03
0.061
7.27
FS
5/12/2015
12.29
DLB
5/12/2015
5/13/20151
12.20
RA
11.871
RA
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
10.011 12.511
10.97
93.3
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
196.818 grams
103.7973 grams
93.0207 grams
105.815 grams
103.7973 grams
2.0177 grams
W/LIME
191.3375
94.0883
97.2492
97.0864
94.0883
2.9981
WEIGHT OF DRIED SAMPLE: 1 2.0177 grams X 100 2.9981
WEIGHT OF WET SAMPLE: 93.0207 grams 97.2492
2.169087 3.082905 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST BOB ARMISTEAD JDATE
SAMPLE HOLDING TANK TYPE
TIME 1415 VOLUME
WO/LIME W/LIME
"PERCENTLIDS 2.56% 3.48%
EVENT
5/26/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
10.00 12.471
10.91
90.90
PH MONITORING REPORT
SAMPLE
DATE
TIME ANAi
PH TEMP C
'EMP CORI
ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
5/25/2015
1415
1250
1454
13101
7.46 28
12.06 28
12.12 28
11.69 281
0.09
0.09
0.09
0.091
7.55
RA
5/26/2015
12.15
RA
5/26/2015
5/27/20151
12.21
RA
11.781
RA
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 12.45
1 11.00.
SLOPE My/Ph % AGREEMENT
10.071 12.471
10.91
96.4
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME W/LIME
172.8939 grams 170.5544
103.6374 grams 94.4891
69.2565 grams 76.0653
105.4118 grams 97.1373
103.6374 grams 94.4891
1.7744 grams 2.6482
WEIGHT OF DRIED SAMPLE: 1.7744 grams X 100 2.6482
WEIGHT OF WET SAMPLE: 69.2565 grams 76.0653
2.562071 3.481482 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST DAVID BRIGMAN JDATE
SAMPLE HOLDING TANK TYPE
TIME 725 VOLUME
WO/LIME W/LIME
"PERCENTLIDS 2.06% 1 3.05%
EVENT
6/6/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45 1
11.00
SLOPE My/Ph % AGREEMENT
6il0.03 12.531
10.93 1
PH MONITORING REPORT
91.80
SAMPLE
DATE
EME TNAI
PH TEMP C I
'EMP CORI ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
6
6/2/2015
0730
1300
1500
1310
7.39 28.7
12.20 29.1
12.11 28.9
12.31 29.1
0.12 7.51
0.12 12.32
0.12 12.23
0.12 12.43
DLB
DLB
DLB
DLB
6/2/2015
6/2/2015
6/3/2015
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00
SLOPE My/Ph I % AGREEMENT
10.041 12.551
10.97
1
92.2
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
195.921 grams
103.6359 grams
92.2851 grams
105.538 grams
103.6359 grams
1.9021 grams
W/LIME
194.969
103.7985
91.1705
106.5803
103.7985
2.7818
WEIGHT OF DRIED SAMPLE: 1 1.9021 Igrams X 1001 2.78181
WEIGHT OF WET SAMPLE: 1 92.2851 larams 1 91.1705
2.0611131 3.0512061% TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST BRIGMAN DATE
SAMPLE HOLDING TANK TYPE
TIME 1300 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS 2.57% 3.49%
EVENT
F 6/23/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00 SLOPE My/Ph %, AGREEMENT
6010.02 12.471
10.98
93.20
PH MONITORING REPORT
SAMPLE
DATE
riME ANAL
PH
TEMP C
'EMP CORI
ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
6/22/2015
1425
1237
1440
12401
7.71
31.7
33
33
331
0.21
0.24
0.24
0.241
7.92
DLB
6/23/2015
12.10
12.34
RA
6/23/2015
6/24/2015
12.02
12.26
RA
12.151
12.391
DLB
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
10.021 12.511
10.98
92.7
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME W/LIME
196.447 grams 189.4925
103.4681 grams 94.5574
92.9789 grams 94.9351
105.8589 grams 97.8714
103.4681 grams 94.5574
2.3908 grams 3.314
WEIGHT OF DRIED SAMPLE: 2.3908 grams X 100 3.314
WEIGHT OF WET SAMPLE: 92.9789 grams 94.9351
2.571336 3.490806 % TOTAL

2015.
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST BRIGMAN IDATE
SAMPLE HOLDING TANK TYPE
TIME 755 VOLUME
WO/LIME W/LIME ,
"PERCENTLIDS 2.72% 3.58%
EVENT
7/21/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
6,ilO".0312.501
11.00
PH MONITORING REPORT
93.60
SAMPLE
DATE
riME ANAI. PH
TEMP C
'EMP CORI ACT PH
INITIALS
INITIAL PF
1 ST
2ND
FINAL
7/21/2015
0800 7.92
1215 12.31
1415 12.26
12501 12.131
29.3
30.6
30.9
31.31
0.12 8.04
0.18 12.49
0.18 12.44
0.181 12.31
DLB
DLB
DLB
DLB
7/21/2015
7/21/2015
7/22/20151
FINAL CALIBRATION
RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 12.45
11.00 SLOPE My/Ph % AGREEMENT
10.03 12.51
10.93
93.7
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
199.2963 grams
103.6385 grams
95.6578 grams
106.2375 grams
103.6385 grams
2.599 grams
W/LIME
194.1778
103.8018
90.376
107.0414
103.8018
3.2396
WEIGHT OF DRIED SAMPLE: 2.599 grams X 100 3.2396
WEIGHT OF WET SAMPLE: 95.6578 grams 90.376
2.716977 3.58458 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST ARMISTEAD/BRIGMAN DATE
SAMPLE HOLDING TANK TYPE
TIME 1034 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS 2.87% 3.79%
EVENT
8/18/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00 SLOPE My/Ph % AGREEMENT
10.03 12.50
11.00
PH MONITORING REPORT
93.90
SAMPLE
DATE
TIME ANAl
PH
TEMP C
EMP CORI
ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
8/17/2015
1034
1310
1515
14301
7.55
28
29.2
29.5
27.11
0.09
0.12
0.12
0.061
7.64
RLA
8/18/2015
12.30
12.42
DLB
8/18/2015
8/19/20151
12.27
12.39
DLB
12.331
12.391
DLB
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
10.031 12.51
10.991
93.9
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
OF DRIED SAMPLE:
WEIGHT OF WET SAMPLE:
WO/LIME W/LIME
173.3803 grams 194.548
103.8044 grams 103.471
69.5759 grams 91.077
105.8045 grams 106.9241
103.8044 grams 103.471
2.0001 grams 3.4531
2.0001 grams X. 100 3.4531
69.5759 grams 91.077
2.8747021 3.791407 % TOTAL

20115
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST BRIGMAN JDATE
SAMPLE HOLDING TANK TYPE
TIME 1250 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS 2.87% 3.76%
EVENT
9/13/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
11.00
SLOPE My/Ph % AGREEMENT
6j10".0512.461
11.11
PH MONITORING REPORT
96.30
SAMPLE
DATE
riME ANAI.
PH
TEMP C
'EMP COR ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
9/13/2015
1300
1255
1455
12551
7.78
27.4
27.8
27.4
28.21
0.06 7.84
0.09 12.56
0.06 12.49
0.091 12.331
DLB
DLB
DLB
DLB
9/14/2015
12.47
914/15
9/15/20151
12.43
12.241
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
10.051 12.531
11.1
96.1
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
190.8425 grams
103.6434 grams
87.1991 grams
106.1419 grams
103.6434 grams
2.4985 grams
W/LIME
196.023
103.4744
92.5486
106.9539
103.4744
3.4795
WEIGHT OF DRIED SAMPLE: 1 2.4985 lgrams X 1001 3.47951
WEIGHT OF WET SAMPLE: 1 87.1991 larams 1 92.5486
TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST ARMISTEAD/BRIGMAN/NOEL JDATE
SAMPLE HOLDING TANK TYPE
TIME 2030 VOLUME
WO/LIME W/LIME
"PERCENTLIDS 2.73% 3.58%
EVENT
F 10/7/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 12.45
11.00
SLOPE My/Ph % AGREEMENT
6ilO".0412.55f
10.91 194.80
PH MONITORING REPORT
SAMPLE
DATE
riME ANAt PH TEMP C
EMP CORI ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
10/7/2015
2030 7.63 23.3
1420 12.34 24.8
1620 12.27 25
14201 12.191 261
-0.06 7.57
0.00 12.34
0.00 12.27
0.031 12.221
BN
DLB
BN
RLA
10/8/2015
10/8/2015
10/9/20151
FINAL CALIBRATION
RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 1 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
9.96 ' 12.471
11.02
97
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
152.7366
grams
103.8051
grams
48.9315
grams
105.1415
grams
103.8051
grams
1.3364
grams
W/LIME
192.0049
94.4906
97.5143
97.9784
94.4906
3.4878
WEIGHT OF DRIED SAMPLE: 1.3364 grams X 1#%TOTAL
78
WEIGHT OF WET SAMPLE: 48.9315 grams 432.731165 3.5767

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST BRIGMAN JDATE 1
SAMPLE HOLDING TANK ITYPE
TIME 940 VOLUME
WO/LIME W/LIME
"PERCENTLIDS 2.60% 1 4.03%
EVENT
10/22/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 12.45
1 11.00 SLOPE My/Ph % AGREEMENT
609.94" 12.391
11.03
PH MONITORING REPORT
93.60
SAMPLE
DATE
riME ANAI.
PH
TEMP C
'EMP CORI
ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
10/22/2015
0950
1225
1430
1230
7.68 21.4
12.56 24
12.53 23.5
12.42 24.1
-0.12
-0.03
-0.03
-0.031
7.56
DLB
10/22/2015
12.53
DLB
10/22/2015
10/23/2015
12.50
DLB
12.391
DLB
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
9.93 12.47
11.02
94.3
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WO/LIME W/LIME
WEIGHT OF DISH AND WET SAMPLE 190.5855 grams 196.03
WEIGHT OF DISH 94.4899 grams 103.8043
WEIGHT OF WET SAMPLE 96.0956 grams 92.2257
WEIGHT OF DISH AND DRIED SAMPLE 96.9888 grams 107.5208
WEIGHT OF DISH 94.4899 grams 103.8043
WEIGHT OF DRIED SAMPLE 2.4989 grams 3.7165
WEIGHT OF DRIED SAMPLE: 1 2.4989 lgrams X 1001 3.7165
WEIGHT OF WET SAMPLE: 1 96.0956 Igrams 1 92.2257
2.6004311 4.0297881% TOTAL

2015
MARINE CORPS AIR STATION
CHERRY POINT NC
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST BRIGMAN JDATE
SAMPLE HOLDING TANK ITYPE
TIME 730 VOLUME
WO/LIME W/LIME
ENT SOLIDS 2.67% 3.58%
Q
EVENT
11/10/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 12.45 1
11.00 SLOPE My/Ph % AGREEMENT
10.08 12.541
11.05
PH MONITORING REPORT
96.30
SAMPLE
DATE
TIME ANAL
PH
TEMP C
'EMP CORI ACT PH
INITIALS
INITIAL P
1ST
2ND
FINAL
11/10/2015
0740
1230
1430
12551
7.19
22.8
24
23.7
23.2
-0.06 7.13
-0.03 12.54
-0.03 12.46
-0.061 12.471
DLB
DLB
DLB
DLB
11/10/2015
12.57
11/10/2015
11/11/20151
12.49
12.531
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 12.45
11.00
SLOPE My/Ph % AGREEMENT
10.09 12.53
11.08
95.8
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WEIGHT OF DISH AND WET SAMPLE
WEIGHT OF DISH
WEIGHT OF WET SAMPLE
WEIGHT OF DISH AND DRIED SAMPLE
WEIGHT OF DISH
WEIGHT OF DRIED SAMPLE
WO/LIME
191.9376 grams
94.4889 grams
97.4487 grams
97.0942 grams
94.4889 grams
2.6053 grams
W/LIME
196.6542
103.803
92.8512
107.1276
103.803
3.3246
WEIGHT OF DRIED SAMPLE: 2.6053 grams X 100 3.3246
WEIGHT OF WET SAMPLE: 97.4487 grams 92.8512
2.673509 3.580568 % TOTAL

2015
MARINE CORPS AIR STATION
CHERRY( POINT NC '
TASK ORDER SOLIDS ANALYSIS BENCH SHEET
ANALYST BRIGMAN JDATE
SAMPLE HOLDING TANK JTNYPE
TIME 945 VOLUME
WO/LIME W/LIME
PERCENT SOLIDS 3.04% 4.29%
EVENT
12/7/2015
GRAB
100
BEGINNING CALIBRATION RECORD
PH METER CALIBRATION ELECTRODE CHECK
BUFFER
INITIAL
10.00 12.45
11.00 SLOPE My/Ph % AGREEMENT
10.00 12.48
11.06
PH MONITORING REPORT
96.90
SAMPLE
DATE
riME ANAI.
PH
TEMP C
'EMP CORil ACT PH
INITIALS
INITIAL PF
1ST
2ND
FINAL
66"
12/7/2015
0950
1245
1445
1300
7.70
16.9
17.5
17.5
19.1
-0.24 7.46
-0.24 12.27
-0.24 12.20
-0.18 12.24
DLB
DLB
DLB
DLB
12/7/2015
12.51
12/7/2015
12/8/2015
12.44
12.42
FINAL
CALIBRATION
RECORD
PH METER CALIBRATION
ELECTRODE CHECK
BUFFER
INITIAL
10.00 12.45
1 11.00
SLOPE My/Ph % AGREEMENT
10.001 12.461
11.06
96.4
SOLIDS WORKSHEET HOLDING TANK WITH LIME
WO/LIME W/LIME
WEIGHT OF DISH AND WET SAMPLE 193.0642 grams 189.0158
WEIGHT OF DISH 103.8055 grams 94.4892
WEIGHT OF WET SAMPLE 89.2587 grams 94.5266
WEIGHT OF DISH AND DRIED SAMPLE 106.5158 grams 98.5435
WEIGHT OF DISH 103.8055 grams 94.4892
WEIGHT OF DRIED SAMPLE 2.7103 grams 4.0543
WEIGHT OF DRIED SAMPLE: 2.7103 grams X 100 4.0543
WEIGHT OF WET SAMPLE: 89.2587 grams 94.5266
3.0364551 4.289057 % TOTAL

STANDARD SOIL FERTILITY ANALYSIS
REPORT
(3 COPIES)

ceAnalXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: SOIL FERTILITY
Pace Project No.: 92255961
Lab ID Sample ID
92255961001 MCAS FIELD #1
92255961002 MCAS FIELD #2
92255961003 MCAS FIELD #3
92255961004 MCAS FIELD #4
92255961005 MCAS FIELD #5
92255961006 WAS FIELD #7
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 17

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL FERTILITY
Pace Project No.: 92255961
Sample: MCAS FIELD #1 Lab ID: 92255961001 Collected: 06/24/15 09:10 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
1660 mg/kg
10.2
1
06/29/1515:35
06/30/1518:17
7440-70-2
3.7 mg/kg
0.51
1
06/29/1515:35
06/30/1518:17
7440-50-8
166 mg/kg
10.2
1
06/29/1515:35
06/30/1518:17
7439-95-4
12.0 mg/kg
0.51
1
06/29/1515:35
06/30/1518:17
7439-96-5
ND mg/kg
511
1
06/29/1515:35
06/30/1518:17
7440-09-7
ND mg/kg
511
1
06/29/1515:35
06130/1518:17
7440-23-5
11.3 mg/kg
1.0
1
06/29/1515:35
06/30/1518:17
7440-66-6
Analytical Method: ASTM D2974-87
17.0 %
0.10
1
07/10/1513:09
Analytical Method: EPA 9045
5.7 Std. Units
0.10
1
07/02/15 15:55
Analytical Method: EPA 365.1
29.1 mg/kg
2.4
1
07/05/1516:47
7723-14-0
H1
Sample: MCAS FIELD #2 Lab ID: 92255961002 Collected: 06/24/15 09:20 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Date: 07/10/2015 04:04 PM
Analytical Method: EPA 6010 Preparation Method: EPA 3050
237 mg/kg
8.1
1
06/29/1515:35
06/30/1518:20
7440-70-2
1.0 mg/kg
0.41
1
06/29/1515:35
06/30/1518:20
7440-50-8
70.4 mg/kg
8.1
1
06/29/1515:35
06/30/1518:20
7439-95-4
9.5 mg/kg
0.41
1
06/29/1515:35
06/30/1518:20
7439-96-5
ND mg/kg
406
1
06/29/1515:35
06/30/1518:20
7440-09-7
ND mg/kg
406
1
06/29/1515:35
06/30/1518:20
7440-23-5
2.0 mg/kg
0.81
1
06/29/1515:35
06/30/1518:20
7440-66-6
Analytical Method: ASTM D2974-87
5.4 %
0.10
1
07/10/1513:07
Analytical Method: EPA 9045
5.6 Std. Units
0.10
1
07/02/15 15:55
H1
Analytical Method: EPA 365.1
26.5 mg/kg
2.0
1
07/05/1516:47
7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 17

lIIrl ytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL FERTILITY
Pace Project No.: 92255961
Sample: MCAS FIELD #3 Lab ID: 92255961003 Collected: 06/24/15 09:35 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
496 mg/kg
8.3
1
06/29/1515:35
06/30/1518:23
7440-70-2
1.6 mg/kg
0.42
1
06/29/1515:35
06/30/1518:23
7440-50-8
88.1 mg/kg
8.3
1
06/29/1515:35
06/30/1518:23
7439-95-4
10.1 mg/kg
0.42
1
06/29/1515:35
06/30/1518:23
7439-96-5
ND mg/kg
415
1
06/29/1515:35
06/30/1518:23
7440-09-7
ND mg/kg
415
1
06/29/1515:35
06/30/1518:23
7440-23-5
3.3 mg/kg
0.83
1
06/29/1515:35
06/30/1518:23
7440-66-6
Analytical Method: ASTM D2974-87
7.3 %
0.10
1
07/10/1513:07
Analytical Method: EPA 9045
5.5 Std. Units
0.10
1
07/02/15 15:55
Analytical Method: EPA 365.1
27.5 mg/kg
2.1
1
07/05/1516:48
7723-14-0
H1
Sample: WAS FIELD #4 Lab ID: 92255961004 Collected: 06/24/15 09:50 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Date: 07/10/2015 04:04 PM
Analytical Method: EPA 6010 Preparation Method: EPA 3050
991 mg/kg
7.1
1
06/29/1515:35
06/30/1518:26
7440-70-2
1.5 mg/kg
0.35
1
06/29/1515:35
06/30/1518:26
7440-50-8
123 mg/kg
7.1
1
06/29/1515:35
06/30/1518:26
7439-95-4
9.7 mg/kg
0.35
1
06/29/1515:35
06/30/1518:26
7439-96-5
ND mg/kg
353
1
06/29/1515:35
06/30/1518:26
7440-09-7
ND mg/kg
353
1
06/29/1515:35
06/30/1518:26
7440-23-5
14.7 mg/kg
0.71
1
06/29/1515:35
06/30/1518:26
7440-66-6
Analytical Method: ASTM D2974-87
3.0 %
0.10
1
07/10/1513:08
Analytical Method: EPA 9045
5.8 Std. Units
0.10
1
07/03/15 16:15
Analytical Method: EPA 365.1
93.1 mg/kg
1.9
1
07/05/1516:49
7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
H1
Page 5 of 17

acte"Analytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL FERTILITY
Pace Project No.: 92255961
Sample: MCAS FIELD #5 Lab ID: 92255961005 Collected: 06/24/15 10:15 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
6420 mg/kg
8.7
1
06/29/1515:35
06/30/1518:29
7440-70-2
26.9 mg/kg
0.44
1
06/29/1515:35
06/30/1518:29
7440-50-8
258 mg/kg
8.7
1
06/29/1515:35
06/30/1518:29
7439-95-4
23.7 mg/kg
0.44
1
06/29/1515:35
06/30/1518:29
7439-96-5
ND mg/kg
437
1
06/29/1515:35
06/30/1518:29
7440-09-7
ND mg/kg
437
1
06/29/1515:35
06/30/1518:29
7440-23-5
33.1 mg/kg
0.87
1
06/29/1515:35
06/30/1518:29
7440-66-6
Analytical Method: ASTM D2974-87
9.1 %
0.10
1
07/10/1513:08
Analytical Method: EPA 9045
6.2 Std. Units
0.10
1
07/03/15 16:15
Analytical Method: EPA 365.1
957 mg/kg
21.2
10
07/06/1511:13
7723-14-0
a
Sample: MCAS FIELD #7 Lab ID: 92255961006 Collected: 06/24/15 10:30 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Date: 07/10/2015 04:04 PM
Analytical Method: EPA 6010 Preparation Method: EPA 3050
1620 mg/kg
8.5
1
06/29/1515:35
06/30/1518:32
7440-70-2
3.1 mg/kg
0.42
1
06/29/1515:35
06/30/1518:32
7440-50-8
145 mg/kg
8.5
1
06/29/1515:35
06130/1518:32
7439-95-4
23.0 mg/kg
0.42
1
06/29/1515:35
06/30/1518:32
7439-96-5
ND mg/kg
424
1
06/29/1515:35
06/30/1518:32
7440-09-7
ND mg/kg
424
1
06/29/1515:35
06/30/1518:32
7440-23-5
7.1 mg/kg
0.85
1
06/29/1515:35
06/30/1518:32
7440-66-6
Analytical Method: ASTM D2974-87
10.7 %
0.10
1
07/10/1513:08
Analytical Method: EPA 9045
5.8 Std. Units
0.10
1
07/03/15 16:15
H1
Analytical Method: EPA 365.1
24.5 mg/kg
2.2
1
07/05/1516:50
7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 17

Page 1 of 2
Report Number: 15-180-0513
Account Number: 05755 F&A
99
www.aleastern.com
Send To: PACE ANALYTICAL CHARLOTTE (for Tat
TABITHA M DACAL
9800 KINCEY AVE - STE 100
HUNTERSVILLE NC 28078
Date Received: 06/29/2015 Date Of Analysis: 06/30/2015
A&L Eastern Laboratories
7621 Whdepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-W6
Grower:
MCAS FIELD/CHERRY POINT SA Farm ID:
92255961
SOIL ANALYSIS REPORT Analytical Method(s): "Every acre... Every year. TM
Mehlich 3
Date Of Report: 06/30/2015
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
% Rate ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm Rate
pH
Index
meq/100g
meq/100g
#1
7
VL
26 VL
33
VL
939
H
19868
4.9 M 139
5.7
6.80
1.3
6.4
NC=6
NC=13
#2
10
VL
32 VL
34
M
383
M
19869
1.7 L 80
5.8
6.88
0.5
2.8
NC=B
NC=16
#3
9
VL
24 VL
26
L
469
H
19870
2.7 M 99
5.7
6.86
0.7
3.3
NC=7
NC=12
#4
42
M
33 VL
45
L
672
H
19871
1.7 L 78
6.5
0.3
4.1
NC=35
NC=17
#5
131 VH
47 VL
90
VL
2322
VH
19873
2.6 M 84
7.1
0.0
12.5
NC=109
NC=24
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
Field ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mn
Fe
Cu
B
SS
Cl
Al
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm Rate
ppm Rate
ms/cm
Rate
ppm Rate
ppm
#1
1.0
4.3
73.4
21.0
#2
2.9
10.1
68.4
19.1
#3
1.9
6.6
71.1
21.2
#4
2.1
9.1
82.0
7.5
#5
1.0
6.0
92.9
0.0
v
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soi�j2ating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. /
H (bigh), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. by: Pwi. m G �"
C.E. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary

Page 2 of 2
Report Number: 15-180-0513 Account Number: 05755 At
9
ww
Send To: PACE ANALYTICAL CHARLOTTE (for TTa ealeastern.com
TABITHA M DACAL
9800 KINCEYAVE - STE 100
HUNTERSVILLE NC 28078
Date Received: 06/29/2015 Date Of Analysis: 06/30/2015
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-WG
Grower:
MICAS FIELD/CHERRY POINT SA Farm ID:
92255961
SOIL ANALYSIS REPORT Analytical Method(s): "Every acre ... Every year. TM"
Mehlich 3
Date Of Report: 06/30/2015
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
ENR
% Rate
Mehl ich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
#7
12 VL
26 VL
38 VL
1118 H
19874
3.2 M 104
6,3
0.7
6.7
NC=10
NC=13
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
Field ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mn
Fe
Cu
B
SS
CI
Al
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
#7
1.0
4.7
83.4
10.5
�
:7]
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
w
to
m
J
O
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by.
Salts ms/cm x 640 = ppm. Analysis prepared by: A8L Eastern Laboratories, Inc.
Pauric McGroary
t

aceAnalytical
www.pacelabs.com
I
i
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SOIL FERTILITY
92255961
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92255961001
MCAS FIELD #1
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
92255961002
MCAS FIELD #2
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
92255961003
MCAS FIELD #3
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
92255961004
WAS FIELD #4
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
92255961005
MCAS FIELD #5
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
92255961006
MCAS FIELD #7
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pnop 3 of 17

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: SOIL FERTILITY
Pace Project No.: 92255961
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MCAS FIELD #1 Lab ID: 92255961001 Collected: 06/24/15 09:10 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
1660 mg/kg
10.2
1
06/29/1515:35
06/30/1518:17
7440-70-2
3.7 mg/kg
0.51
1
06/29/1515:35
06/30/1518:17
7440-50-8
166 mg/kg
10.2
1
06/29/1515:35
06/30/1518:17
7439-95-4
12.0 mg/kg
0.51
1
06/29/1515:35
06/30/1518:17
7439-96-5
ND mg/kg
511
1
06/29/1515:35
06/30/1518:17
7440-09-7
ND mg/kg
511
1
06/29/1515:35
06/30/1518:17
7440-23-5
11.3 mg/kg
1.0
1
06/29/1515:35
06/30/1518:17
7440-66-6
Analytical Method: ASTM D2974-87
17.0 %
0.10
1
07/10/1513:09
Analytical Method: EPA 9045
5.7 Std. Units
0.10
1
07/02/15 15:55
Analytical Method: EPA 365.1
29.1 mg/kg
2.4
1
07/05/1516:47
7723-14-0
H1
Sample: WAS FIELD #2 Lab ID: 92255961002 Collected: 06/24/15 09:20 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
237 mg/kg
8.1
1
06/29/1515:35
06/30/1518:20
7440-70-2
1.0 mg/kg
0.41
1
06/29/1515:35
06/30/1518:20
7440-50-8
70.4 mg/kg
8.1
1
06/29/1515:35
06/30/1518:20
7439-95-4
9.5 mg/kg
0.41
1
06/29/1515:35
06/30/1518:20
7439-96-5
ND mg/kg
406
1
06/29/1515:35
06/30/1518:20
7440-09-7
ND mg/kg
406
1
06/29/1515:35
06/30/1518:20
7440-23-5
2.0 mg/kg
0.81
1
06/29/1515:35
06/30/1518:20
7440-66-6
Analytical Method: ASTM D2974-87
5.4 %
0.10
1
07/10/1513:07
Analytical Method: EPA 9045
5.6 Std. Units
0.10
1
07/02/15 15:55
Analytical Method: EPA 365.1
26.5 mg/kg
2.0
1
07/05/1516:47
7723-14-0
1E
Date: 07/10/2015 04:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 17

aceAnalytical
www.pacelabs.com
I
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SOIL FERTILITY
Pace Project No.: 92255961
Sample: MCAS FIELD #3
Lab ID: 92255961003 Collected: 06/24/15 09:35 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qua[
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Calcium
496 mg/kg 8.3 1 06/29/1515:35
06/30/1518:23
7440-70-2
Copper
1.6 mg/kg 0.42 1 06/29/1515:35
06/30/1518:23
7440-50-8
Magnesium
88.1 mg/kg 8.3 1 06/29/1515:35
06/30/1518:23
7439-95-4
Manganese
10.1 mg/kg 0.42 1 06/29/1515:35
06/30/1518:23
7439-96-5
Potassium
ND mg/kg 415 1 06/29/1515:35
06/30/1518:23
7440-09-7
Sodium
ND mg/kg 415 1 06/29/1515:35
06/30/1518:23
7440-23-5
Zinc
3.3 mg/kg 0.83 1 06/29/1515:35
06/30/1518:23
7440-66-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
7.3 % 0.10 1
07/10/15 13:07
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
5.5 Std. Units 0.10 1
07/02/15 15:55
H1
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
27.5 mg/kg 2.1 1
07/05/1516:48
7723-14-0
Sample: MCAS FIELD #4
Lab ID: 92255961004 Collected: 06/24/15 09:50 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Calcium
991 mg/kg 7.1 1 06/29/1515:35
06/30/1518:26
7440-70-2
Copper
1.5 mg/kg 0.35 1 06/29/1515:35
06/30/1518:26
7440-50-8
Magnesium
123 mg/kg 7.1 1 06/29/1515:35
06/30/1518:26
7439-95-4
Manganese
9.7 mg/kg 0.35 1 06/29/1515:35
06/30/1518:26
7439-96-5
Potassium
ND mg/kg 353 1 06/29/1515:35
06/30/1518:26
7440-09-7
Sodium
ND mg/kg 353 1 06/29/1515:35
06/30/1518:26
7440-23-5
Zinc
14.7 mg/kg 0.71 1 06/29/1515:35
06/30/1518:26
7440-66-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
3.0 % 0.10 1
07/10/15 13:08
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
5.8 Std. Units 0.10 1
07/03/15 16:15
H1
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
93.1 mg/kg 1.9 1
07/05/1516:49
7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2015 04:04 PM
without the written consent of Pace Analytical Services, Inc..
Page 5 of 17

aceAnalytical
www.pacelabs.00m
i
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SOIL FERTILITY
Pace Project No.: 92255961
Sample: MCAS FIELD #5 Lab ID: 92255961005 Collected: 06/24/15 10:15 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
6420 mg/kg
8.7
1
06/29/1515:35
06/30/1518:29
7440-70-2
26.9 mg/kg
0.44
1
06/29/1515:35
06/30/1518:29
7440-50-8
258 mg/kg
8.7
1
06/29/1515:35
06/30/1518:29
7439-95-4
23.7 mg/kg
0.44
1
06/29/1515:35
06/30/1518:29
7439-96-5
ND mg/kg
437
1
06/29/1515:35
06/30/1518:29
7440-09-7
ND mg/kg
437
1
06/29/1515:35
06/30/1518:29
7440-23-5
33.1 mg/kg
0.87
1
06/29/1515:35
06/30/1518:29
7440-66-6
Analytical Method: ASTM D2974-87
9.1 %
0.10
1
07/10/1513:08
Analytical Method: EPA 9045
6.2 Std. Units
0.10
1
07/03/15 16:15
Analytical Method: EPA 365.1
957 mg/kg
21.2
10
07/06/1511:13
7723-14-0
Sample: MCAS FIELD #7 Lab ID: 92255961006 Collected: 06/24/15 10:30 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
1620 mg/kg
8.5
1
06/29/1515:35
06/30/1518:32
7440-70-2
3.1 mg/kg
0.42
1
06/29/1515:35
06/30/1518:32
7440-50-8
145 mg/kg
8.5
1
06/29/1515:35
06/30/1518:32
7439-95-4
23.0 mg/kg
0.42
1
06/29/1515:35
06/30/1518:32
7439-96-5
ND mg/kg
424
1
06/29/1515:35
06/30/1518:32
7440-09-7
ND mg/kg
424
1
06/29/1515:35
06/30/1518:32
7440-23-5
7.1 mg/kg
0.85
1
06/29/1515:35
06/30/1518:32
7440-66-6
Analytical Method: ASTM D2974-87
10.7 %
0.10
1
07/10/1513:08
Analytical Method: EPA 9045
5.8 Std. Units
0.10
1
07/03/15 16:15
Analytical Method: EPA 365.1
24.5 mg/kg
2.2
1
07/05/1516:50
7723-14-0
H1
Date: 07/10/2015 04:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 17

Page 1 of 2
Report Number: 15-180-0513 ATLI
Account Number: 05755
www.aleastem.com
Send To: PACE ANALYTICAL CHARLOTTE (for Tat
TABITHA M DACAL
9800 KINCEY AVE - STE 100
HUNTERSVILLE NC 28078
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271.WG
Grower:
MICAS FIELD/CHERRY POINT SA Farm ID:
92255961
SOIL ANALYSIS REPORT Analytical Method(s)
Mehlich 3
natP t7f Rennrt, 06/30/2015
"Every acre... Every year. TA°"
yp`c "yy •yM vv
`V `V
V
Organic Matter'
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
% Rate
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm Rate
pH
Index
megl100g
meq/100g
#1
7
VL
26 VL
33
VL
939
H
5.7
6.80
1.3
6.4
19868
4.9 M 139
NC=6
NC=13
#2
10
VL
32 VL
34
M
383
M
5.8
6.88
0.5
2.8
19869
1.7 L 80
NC=8
NC=16
#3
9
VL
24 VL
26
L
469
H
5.7
6.86
0.7
3.3
19870
2.7 M 99
NC=7
NC=12
#4
42
M
33 VL
45
L
672
H
6.5
0.3
4.1
19871
1.7 L 78
NC=35
NC=17
#5
131 VH
47 VL
90
VL
2322
VH
71
0.0
12.5
19873
2.6 M 84
NC = 109
NC = 24
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
K
Mg
Ca
Na
H
NON
S
Zn
Mn
Fe
Cu
B
SS
CI
Al
Field ID
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm Rate
ppm Rate
ms/cm
Rate
ppm Rate
ppm
1l1
1.0
4.3
73.4
21.0
02
2.9
10.1
68.4
19.1
r#3
1.9
6.6
71.1
21.2
�4
2.1
9.1
82.0
7.5
�5
1.0
6.0
92.9
�00�
!aloes on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soiGFating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: ?XI:.
1 (bigh), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc
Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
J
Pauric McGroary

Page 2 of 2
Report Number: 15-180-0513
Account Number: 05755
www.aleastem.com
Send To: PACE ANALYTICAL CHARLOTTE (for Tat
TABITHA M DACAL
9800 KINCEY AVE - STE 100
HUNTERSVILLE NC 28078
ncioni�n�c
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-WG
Grower:
MICAS FIELD/CHERRY POINT SA Farm ID:
92255961
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
natp of Rpnnrt- 06/30/2015
"Every acre... Every year TIM11
LJOLU
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
% Rate Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
#7
12 VL
26 VL
38 VL
1118 H
6.3
0.7
6.7
19874
3.2 M 104
NC=10
NC=13
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
K
Mg
Ca
Na
H
NON
S
Zn
Mn
Fe
Cu
B
SS
Cl
AI
Field ID
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
ppm Rate
ppm Rate
ins/cm Rate
ppm Rate
ppm
#7
1.0
4.7
83.4
10.5
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium)
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
V
0
Explanation of symbols: % (percent), ppm (parts per minion), ms/m i nis report appi— to aaiupw a --w— a-- —......
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/1009 maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
Salts ms/cm x 640 = ppm.
by: per,, Iff 60-r
Pauric McGroary

aceAnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SOIL FERTILITY
92255961
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92255961001
MCAS FIELD #1
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
92255961002
MCAS FIELD #2
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
92255961003
WAS FIELD #3
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
92255961004
MCAS FIELD #4
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
92255961005
MCAS FIELD #5
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
92255961006
MCAS FIELD #7
EPA 6010
JMW
7
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
TEP
1
PASI-A
EPA 365.1
JDA
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Paae 3 of 17

!;a'ceAnalytical"
www.pacelabs.com
i
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
Project: SOIL FERTILITY
Pace Project No.: 92255961
Sample: MCAS FIELD #1 Lab ID: 92255961001 Collected: 06/24/15 09:10 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
1660 mg/kg
10.2
1
06/29/1515:35
06/30/1518:17
7440-70-2
3.7 mg/kg
0.51
1
06/29/1515:35
06/30/1518:17
7440-50-8
166 mg/kg
10.2
1
06/29/1515:35
06/30/1518:17
7439-95-4
12.0 mg/kg
0.51
1
06/29/1515:35
06/30/1518:17
7439-96-5
ND mg/kg
511
1
06/29/1515:35
06/30/1518:17
7440-09-7
ND mg/kg
511
1
06/29/1515:35
06/30/1518:17
7440-23-5
11.3 mg/kg
1.0
1
06/29/1515:35
06/30/1518:17
7440-66-6
Analytical Method: ASTM D2974-87
17.0 %
0.10
1
07/10/1513:09
Analytical Method: EPA 9045
5.7 Std. Units
0.10
1
07/02/15 15:55
Analytical Method: EPA 365.1
29.1 mg/kg
2.4
1
07/05/1516:47
7723-14-0
Sample: WAS FIELD #2 Lab ID: 92255961002 Collected: 06/24/15 09:20 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
237 mg/kg
8.1
1
06/29/1515:35
06/30/1518:20
7440-70-2
1.0 mg/kg
0.41
1
06/29/1515:35
06/30/1518:20
7440-50-8
70.4 mg/kg
8.1
1
06/29/1515:35
06/30/1518:20
7439-95-4
9.5 mg/kg
0.41
1
06/29/1515:35
06/30/1518:20
7439-96-5
ND mg/kg
406
1
06/29/1515:35
06/30/1518:20
7440-09-7
ND mg/kg
406
1
06/29/1515:35
06/30/1518:20
7440-23-5
2.0 mg/kg
0.81
1
06/29/1515:35
06/30/1518:20
7440-66-6
Analytical Method: ASTM D2974-87
5.4 %
0.10
1
07/10/1513:07
Analytical Method: EPA 9045
5.6 Std. Units
0.10
1
07/02/15 15:55
H1
Analytical Method: EPA 365.1
26.5 mg/kg
2.0
1
07/05/1516:47
7723-14-0
Date: 07/10/2015 04:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 17

1'�qceAnalyticale
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SOIL FERTILITY
Pace Project No.: 92255961
Sample: MCAS FIELD #3 Lab ID: 92255961003 Collected: 06/24/15 09:35 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
496 mg/kg
8.3
1
06/29/1515:35
06/30/1518:23
7440-70-2
1.6 mg/kg
0.42
1
06/29/1515:35
06/30/1518:23
7440-50-8
88.1 mg/kg
8.3
1
06/29/1515:35
06/30/1518:23
7439-95-4
10.1 mg/kg
0.42
1
06/29/1515:35
06/30/1518:23
7439-96-5
ND mg/kg
415
1
06/29/1515:35
06/30/1518:23
7440-09-7
ND mg/kg
415
1
06/29/1515:35
06/30/1518:23
7440-23-5
3.3 mg/kg
0.83
1
06/29/1515:35
06/30/1518:23
7440-66-6
Analytical Method: ASTM D2974-87
7.3 %
0.10
1
07/10/1513:07
Analytical Method: EPA 9045
5.5 Std. Units
0A0
1
07/02/15 15:55
Analytical Method: EPA 365.1
27.5 mg/kg
2.1
1
07/05/1516:48
7723-14-C
a
Sample: MCAS FIELD #4 Lab ID: 92255961004 Collected: 06/24/15 09:50 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
991 mg/kg
7.1
1
06/29/1515:35
06/30/1518:26
7440-70-2
1.5 mg/kg
0.35
1
06/29/1515:35
06/30/1518:26
7440-50-8
123 mg/kg
7.1
1
06/29/1515:35
06/30/1518:26
7439-95-4
9.7 mg/kg
0.35
1
06/29/1515:35
06/30/1518:26
7439-96-5
ND mg/kg
353
1
06/29/1515:35
06/30/1518:26
7440-09-7
ND mg/kg
353
1
06/29/1515:35
06/30/1518:26
7440-23-5
14.7 mg/kg
0.71
1
06/29/1515:35
06/30/1518:26
7440-66-6
Analytical Method: ASTM D2974-87
3.0 %
0.10
1
07/10/1513:08
Analytical Method: EPA 9045
5.8 Std. Units
0.10
1
07/03/15 16:15
H1
Analytical Method: EPA 365.1
93.1 mg/kg
1.9
1
07/05/1516:49
7723-14-0
Date: 07/10/2015 04:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 17

aceAnalytical
www.pacelabs.com
1
I
ANALYTICAL RESULTS
Project: SOIL FERTILITY
Pace Project No.: 92255961
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MCAS FIELD #5 Lab ID: 92255961005 Collected: 06/24/15 10:15 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
6420 mg/kg
8.7
1
06/29/1515:35
06/30/1518:29
7440-70-2
26.9 mg/kg
0.44
1
06/29/1515:35
06/30/1518:29
7440-50-8
258 mg/kg
8.7
1
06/29/1515:35
06/30/1518:29
7439-95-4
23.7 mg/kg
0.44
1
06/29/1515:35
06/30/1518:29
7439-96-5
ND mg/kg
437
1
06/29/1515:35
06/30/1518:29
7440-09-7
ND mg/kg
437
1
06/29/1515:35
06/30/1518:29
7440-23-5
33.1 mg/kg
0.87
1
06/29/1515:35
06/30/1518:29
7440-66-6
Analytical Method: ASTM D2974-87
9.1 %
0.10
1
07/10/1513:08
Analytical Method: EPA 9045
6.2 Std. Units
0.10
1
07/03/15 16:15
Analytical Method: EPA 365.1
957 mg/kg
21.2
10
07/06/1511:13
7723-14-0
H1
Sample: MCAS FIELD #7 Lab ID: 92255961006 Collected: 06/24/15 10:30 Received: 06/25/15 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Calcium
Copper
Magnesium
Manganese
Potassium
Sodium
Zinc
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010 Preparation Method: EPA 3050
1620 mg/kg
8.5
1
06/29/1515:35
06/30/1518:32
7440-70-2
3.1 mg/kg
0.42
1
06/29/1515:35
06/30/1518:32
7440-50-8
145 mg/kg
8.5
1
06/29/1515:35
06/30/1518:32
7439-95-4
23.0 mg/kg
0.42
1
06/29/1515:35
06/30/1518:32
7439-96-5
ND mg/kg
424
1
06/29/1515:35
06/30/1518:32
7440-09-7
ND mg/kg
424
1
06/29/1515:35
06/30/1518:32
7440-23-5
7.1 mg/kg
0.85
1
06/29/1515:35
06/30/1518:32
7440-66-6
Analytical Method: ASTM D2974-87
10.7 %
0.10
1
07/10/1513:08
Analytical Method: EPA 9045
5.8 Std. Units
0.10
1
07/03/15 16:15
Analytical Method: EPA 365.1
24.5 mg/kg
2.2
1
07/05/1516:50
7723-14-0
H1
Date: 07/10/2015 04:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 17

Page 1 of 2
Report Number: 15-180-0513
Account Number: 05755
www.aleastern.com
Send To: PACE ANALYTICAL CHARLOTTE (for Tat
TABITHA M DACAL
9800 KINCEYAVE - STE 100
HUNTERSVILLE NC 28078
.4. nall)WI MIA n.f. fif a-iya;a. r1R/3r1/9r15
A&L Eastern Laboratories
7621 Whitepine Road Richmond. Virginia 23237 [phone] Fax [phone]
Grower:
MCAS FIELD/CHERRY POINT SA Farm ID:
92255961
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
natP Of Renort: 06/30/2015
"Every acre... Every year. rm"
w-
Organic Matter'
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Sample ID
Lab
Field ID
Number
% Rate Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm- Rate
pH
Index
me /100
q g
meq/100 g
#1
7
VL
26 VL
33
VL
939
H
5.7
6.80
1.3
6.4
19868
4.9 M 139
NC=6
NC=13
#2
19869
1.7 L 80
10 VL
32 VL
34
M
383
M
5.8
6.88
0.5
2.8
NC=B
NC=16
#3
9
VL
24 VL
L
469
H
5.7
6.86
0.7
3.3
19870
2.7 M 99
126
NC=7
NC=12
#4
42
M
33 VL
45
L
672
H
6.5
0.3
4.1
19871
1.7 L 78
NC=35
NC=17
#5
VH
VL
90
VL
2322
VH
71
0.0
12.5
19873
2.6 M 84 1131
147
NC=109
NC=24
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mn
Fe
Cu
B
SS
Cl
Al
Field ID
,
/o
,
/o
%
%
%
pp m Rate
pp m Rate
PP m Rate
PP m
Rate
PP m
Rate
PP m Rate
PP m Rate
ms/cm Rate
PP m Rate
PPm
1
1.0
4.3
73.4
21.0
�2
2.9
10.1
68.4
19.1
/3
1.9
6.6
71.1
21.2
/4
2.1
9.1
82.0
7.5
'a~5
1.0
6.0
92.9
0.0
v
(aloes on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
,oiWating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
i (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: AaL Eastern Laboratories, Inc.
Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
by: paw'` mF 60wr
i
Pauric McGroary

Page 2 of 2
Report Number: 15-180-0513 j[
Account Number: 05755 @�!
www.aleastem.com
Send To: PACE ANALYTICAL CHARLOTTE (for Tat
TABITHA M DACAL
9800 KINCEYAVE - STE 100
HUNTERSVILLE NC 28078
i....:... ncnn10ni r
A &L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271.WG
Grower:
WAS FIELD/CHERRY POINT SA Farm ID:
92255961
SOIL ANALYSIS REPORT Analytical Method(s)
Mehlich 3
rinro r)f Rannrt• nR/3n/gn1.si
"Every acre... Every year. T°" "
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
% Rate Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
P H
Index
meq/100g
meq/100g
#7
12 VL
26 VL
38 VL
1118 H
763
0.7
6.7
19874
3.2 M 104
NC=10
NC=13
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
K
Mg
Ca
Na
H
NON
S
Zn
Mn
Fe
Cu
B
SS
Cl
Al
Field ID
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
#7
1.
44.7
83.4
10.5
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium)
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
w
n
m
0
Explanation of symbols: % (percent), ppm (parts per million), IDsia, I nis report appues to sampieis) resieu. ­iiiplr d�G �­ 11 a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
Salts ms/cm x 640 = ppm.
by: per;. or 6&-r
Pauric McGroary

TRIENNIAL GROUNDWATER MONITORING
REPORTS
(3 COPIES)

UNITED STATES MARINE CORPS
MARINE CORPS AIR STATION
POSTAL SERVICE CENTER 8003
CHERRY POINT, NORTH CAROLINA 28533-0003
IN REPLY REFER TO;
5090/07109
LN
April 13, 2015
North Carolina Department of Environment
and Natural Resources
Division of Water Quality
Information Processing Center
1617 Mail Service Center
Raleigh, NC 27699-1617
Subj: TRIENNIAL GROUNDWATER MONITORING
In accordance with the groundwater monitoring and reporting
requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for
Land Application of Wastewater Residuals, enclosed are the
original and one copy of the GW-59-A report and the four GW-59
reports (one each for monitoring wells 1, 2, 3, and 5) for the
triennial reporting for February 2015.
These reports are being submitted after the 31 March 2015
deadline as established in the permit due to an internal
administrative oversight.
Should you have any questions, please contact Mr. Timothy
Lawrence of the Environmental Affairs Department at your earliest
convenience at [phone].
Sincerely,
G. w. IRAD o ~
Environm nta Affairs Officer
By directs n of the
Commanding Officer
Enclosure: (1)
GW-59-A
(2)
GW-59
for
MW-1
(3)
GW-59
for
MW-2
(4)
GW-59
for
MW-3
(5)
GW-59
for
MW-5

GW-59A COMPLIANCE REPORT FORM Permit # WQ0001489
(Submit one each monitoring period with Gil =59 forms.)
Enter date monitoring results were due. (3/31/151 Will this monitoring report (GW-59 and GW-59A) be submitted after
l ES
NO
I
the established due date?
X
2
"'as any required information missing on the GNV-59 report forms?
YES
NO
X
IF the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems
encountered in obtaining the required information
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
l ES
NO
3
identification plate, area overgrown, etc.)? if the annreris "tes", contact the Regional Ofceforguidance
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
X
If the answer to question 4 is "NO", skip to section 8
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the
space provided below
MW-2 N113 1.73 mg/L
NIW-5 NI13 2.99 m L
For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s)
I ES
NO
5
in the same well(s) in the last two years?
X
If the answer to question 5 is "NO", skip to section 8
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentratwn(s)
reported, and sample collection date for each occurrence (for the last two years).
PINY-5: Feh. 2015 N113 2.68 Feb. 2014 N113 3.13; June 2013 N113 2.45; Feb. 2013 N113 2,25
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
1'ES
NO
X
Irthe answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY
FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office.
Is the permittee implementing previously approved actions required by the Division involving this groundwater quality
YES
NO
7
problem?
X
If the answer to question 7 is "YES", describe those actions in the space provided below
If the answer to question 7 is "NO", contact the Reeional Office N ithin 90 days; an evaluation may be required to determine the
impact the waste dism2al system is having at the review and compliance boundaries surrounding this facility. Failure to do sg may
subiecl the twrmitlee to a Noire or violation, fines, and/or Penalties.
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with
8
GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that.the above information was evaluated and the information submitted in this report (Comphanc e
Report GW-59A) is true and complete to the best of my knowledge.
Patricia T. Davis, Utility Systems Operator Supervisor
Signature of Permittee (or Authorized Agent) Date 4A3'20I5

SUBMIT FORM ON YELLOW PAPER ONLY
e
DEPARTMENT OF ENVIRONMENT 3 NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER -QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
a e e
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617 PHONE: [phone]
FACILITY INFORMATION
Please Pnnr Cteady or Type
PERMIT Ntmtber. Expiration Date: 7/3112019
Facility Name, MCAS Cherry Point
Non -Discharge UIC
Permit Name (if different):
NPDES W00001489 Other
Facility Address: MCAS Cherry Point, NC 28533-0006
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ moon Remediation: Infiltration Gallery
County
Craven
,c•y, ts;a.r
,zvr
D Spray Field Remedtation:
Contact Person: Patricia T. Davis
Telephone M 2524664599
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Site 21. MCAS Cherry Point
No of Wells to be Sampled: 1
,gym
❑ Water Source Heat Pump other:
SAMPLING INFORMATION
if WELL
WELL ID NUMBER (From Permit): MW-1
Date Sample Collected W912015 FIELD ANALYSIS.
WAS
DRY at
Well Depth 26.66 R.
Well Diameter 2
pH 00400 6.71 units Temp 00010 18 'C
time of
Depth to Water Level 82546: 1.5 tL below measuring point
Screened Interval -0.17
ft to -15.2 ft. Spec. Cond. 00094 71 µMhos
sampling,
Measuring Point is 1.33 ft. above land surface
Relative M.P. Elevation 10.78 Odor 00D85 NONE
check
Volume of water pumpedtbailed before sampling:
5 Gal.
Appearance. CLEAR
here:
Sam Res for metals were collected unfiltered
YES '
NO and field acidified W YES
NO
LABORATORY INFORMATION
Date sample analyzed: 2/9/2015
Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201 / 37706
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 µg/L
Colifonm: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620
<0,05 mg/L Zn -Zinc 01092 mg/L
Coliform: MF Total 31504
1100ml-
Phosphorus: Total as P 00665
mg/L
(Note Use MPN method ror flighty brbd wmptes)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):.
Dissolved Solids: Total 70300 60
mg/L
AI - Aluminum 01105
mg/L
pH (Lab) 00403 6.71
units
Ba - Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 6.5
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L ORGANICS (by GC, GC/MS, HPLC)
Phenol 32730
µg/L
Fe - Iron 01045
µg/L (Specify test and method M ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L Lab Report Attached? ❑ Yes(1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L Method#
Total Ammonia 00610 <1.0
mg/L
Mg - Magnesium 00927
mg/L Method#
(Ammon a Nidogen, NN, as N, Ammonia N&ogen, Total)
Mn - Manganese 01055
µg/L , Method#
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L Method#
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Remcival%
t ceMty that to the Cost cf my knowledge any bcEef, the mlormetion submaled m this re,^.en rs vue. accurate, and complete, and that the labore!ery anat,•lical data ryas produced using approceJ rnelhoJs of an !7ss by a
R:1Q•carufad laboralcry. I am mvare that there are mgnYicant penaPT5 fer submdltng false Information• tndud:ng the possib:l.ly of fines and imprisonment for kno•:,9ng violaRons.
Patricia T. •� r
Davis
15
GW-59 Rev.
2/2
r r

SUBMIT FORM ON YELLOW PAPER ONLY
a
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER CIUALITY4NFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER
RAL.EIGH. NC 27699-1617 PHONE: [phone]
FACILITY INFORMATION
Please Pnnt Clearfy or Type
PERMIT Number: Expiration Date: 7 31/2019
Facility Name: MCAS Cherry Point
Non -Discharge UIC
Permit Name (it different):
NPDES W00001489 Other
Facility Address: MCAS Cherry Point, NC 28533-0006
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
County
,,o,
Craven
❑ Spray Field [] Remediation:
,ce,l ,,,,
Contact Person: Patricia T. Davis
Telephone M 2524664599
❑ Rotary Distributor 0 Land Application of Sludge
Well Location/Site Name: Site 21, MCAS Cherry Point
No.of Welts to be Sampled: 1
(, Water source Heat Pump ?] Other:
hMn
SAMPLING INFORMATION
If WELL.
WAS
WELL ID NUMBER (From Permit): MW-2
Dale Sample Collected 2/9/2015 FIELD ANALYSIS:
DRY at
Well Depth 26.58 ft
Well Diameter 2
pH 00400 6.33 units Temp 00010 16 °C
time of
Depth to Water Level 82546 4.5 fL below measuring pant
Screened Interval -1 03
ft to -11 ft. Spec Cond. 00094 701 µMhos
sampling,
Measuring Point is 1.28 ft above land surface
Relative M P Elevation 14.8
Odor 00085 NONE
check
Volume of water pumped/ba led before sampi ng
5 Gal.
Appearance CLEAR
here: r
Samoles for metals were cotfected unfiltered
YES __]
NO and field acidified YES
NO
LABORATORY INFORMATION
Date sample analyzed: 2/9/2015
Laboratory Name: MCAS Cherry Point J Pace Analytical Certification Number: 201137706
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 µg/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note. Use MPNmetindWhgh)yttsbi "s 003)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total 70300 172
mg/L
At - Aluminum 0114S
mg/L
pH (Lab) 00403 6.33
units
Ba - Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 11.4
mg/L
Cd - Cadmium Total 01027
µgJL
Arsenic 01002
µg/L
Chromium: Total 01034
µgJL
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L ORGANICS (by GC, GC/MS, HPLC)
Phenol 32730
µg/L
Fe - lron 01045
µg/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L Lab Report Attached? ❑ Yes(1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L Method#
Total Ammonia 00610 1.65
mg/L
Mg - Magnesium 00927
mg/L Method#
(Ammo" N"en. NHj as N. Ammons Nstroyen, Total)
Mn - Manganese 01055
µgJL . Method#
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L Method#
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOU. Removal t.
Patricia T. Davis - Utility Systems Operator
Permiltee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev 2/2010
4/13/2015
Signature of Perm ittee (or Authorized Agent) (Date)

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
ATypeqPERMIT
1617 MAIL seRvlcE CENTER
RALEIGH, NC 27699-1617 PHONE: [phone]
FACILITY INFORMATION
Please Print Clearly or
Number: Expiration Date: 773172019
Facility Name: MCAS Cherry Point
Non -Discharge UIC
Permit Name (if different):
NPDES W00001489 Other
Facility Address: MCAS Cherry Point, NC 28533-0006
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedlation: infiltration Gallery
County:
ilFi
Craven
0 Spray Field ❑ Remediation:
;who ,st,.*t
Contact Person: Patricia T, Davis
Telephone M 252-466-4599
Rotary Distributor [) Land Application of Sludge
Well Location/Site Name Site 21 MCAS Cherry Point
No.of Wells to be Sampled: 1
jTpM
❑ Water Source Heat Pump ❑ Other
SAMPLING INFORMATION
If WELL
WAS
WELL ID NUMBER (From Permit): MW-3
Date Sample Collected 2/912015 FIELD ANALYSIS:
DRY at
Well Depth 25 58 ft.
Well Diameter 2
pH 00400 6.69 units Temp 00010: 18 aC
time of
Depth to Water Level 82546 0 ft. below measuring point
Screened Intervat -11.7
ft. to -21.7 ft. Spec. Cond. 00094- 240 µMhos
sampling,
Measuring Point is 1.46 ft. above land surface
Relative M.P. Elevation: 3.1
Odor 00085 NONE
check
Volume of water pumped/bailed before sampling
5 Gal.
Appearance; TURBID
here: ❑
Samples for metals were collected unfiltered
YES F ]
NO and field acidified YES
NO
LABORATORY INFORMATION
Date sample analyzed: 2/9/2015
Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201137706
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 µg/L
Coliform: MF Fecal 31616 <1
1100ml-
Nitrate (NO3) as N 00520 0.15 mg/L Zn - Zinc 01092 mg/L
Conform: MF Total 31504
1100ml-
Phosphorus: Total as P 00665
mg/L
(Note. Use MPN "Mod for "Iffy tw" samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 70300 104
mg/L
AI - Aluminum 01105
mg/L
pH (Lab) 00403 6.69
units
Ba - Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 5
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L ORGANICS (by GC, GC/MS, HPLC)
Phenol 32730
µg/L
Fe - iron 01045
µg/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L Lab Report Attached? ❑ Yes(l) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L Method#
Total Ammonia 00610 <1.0
mg/L
Mg - Magnesium 00927
mg/L Method#
(AffmWis Nnm9en; NHS as N: Ammorua Nmopen, Total)
Mn - Manganese 01055
µg/L . Method#
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L , Method#
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs:
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.2/2010
Effluent Total VOCs:
VQG Removal%a
4/13/2015
Signature of Permittee (or Authorized Agent) (Date)

SUBMIT FORM ON YELLOW PAPER ONLY
(GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Please Print Clearly or Type
Facility Name- MCAS Cherry Point
Permit Name (if different):
Facility Address: MCAS Cherry Point, NC 28533-0006
County Craven
act Person: Patricia T. Davis Telephone M 252466-4599
Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617 PHONE: [phone]
Non -Discharge UIC
NPDES WQ0001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
p Lagoon ❑ Remediation: infiltration Gallery
�] Spray Field ❑ Remediation:
Rotary Distributor 0 Land Application of Sludge
Water Source Heat Pump L] Other:
SAMPLING INFORMATION
If WELL
WELL to NUMBER (From Permit): MW-5
Date Sample Collected: 2/5/2015
FIELD ANALYSIS:
WAS
@RY at
Well Depth 13 fL
Well Diameter 2
pH 00400 6.05 units Temp 00010
15 °C
time of
Depth to Water level 82546: 5.2 it below measuring point
Screened Interval: 3 ft. to 13
tL Spec. Cond. 00094, 617
pMhos
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation 12
Odor 00085 NONE
check
Volume of water pumped/bailed before sampling: 5 Gal.
Appearance CLEAR
here-.--
Sarnoles for metals were collected unfiltered YES R NO
and field acidified YES NO
LABORATORY INFORMATION
Date sample analyzed: 2/5/2015 Laboratory Name MCAS Cherry Point / Pace Analytical Certification Number 201 137706
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COI) 00335
mg/L
Nitrite (NO2) as N 00615
mg1L
Cohform. MF Fecal 31616
<1
/100ml-
Nitrate (NO3) as N 00620 <0.05
mg1L
Coliform MF Total 31504
/100ml-
Phosphorus Total as P 00665
mg/L
(Note Use MPN meerod ror h-g* (wad samples)
Orthophosphate 70507
mg/L
Dissolved Solids. Total 70300
210
mg/L
AI - Aluminum 01105
mg/L
pH (Lab) 00403
6.05
units
Ba - Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
10A
mg/L
Cd - Cadmium. Total 01027
µg/L
Arsenic 01002
µg1L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg1L
Phenol 32730
µg/L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610
2.68
mg/L
Mg - Magnesium 00927
mg/L
(Ammon Netrogen. NH, as N, Amn roa N"en, Tatali
Mn - Manganese 01055
µg/L
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units)'
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method M ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(i) ❑ No (0)
Method#
Method#
Method#
Method#
For • - Only • •r. Z•.- *•• ••
i centy that to the test of my knovrled,7o and bel,cf, the inf rma!ion submilte9 o this report is true, accurate, and ccrri:!=!e, and Ihat the labcra:ary analy!ical d3!a +:as produced using approved methods of analysis by a
G':.'0-ceruted lnbcralury ! am aware ihol there are signr5cant pcnaL`ms for submi!ling fate information, including the possibil,ty of fines and imprisonment fer knoving v cla!icns.
DavisPatricia T. Operator
1
15
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev.
010212

UNITED STATES MARINE CORPS
MARINE CORPS AIR STATION
POSTAL SERVICE CENTER 8003
CHERRY POINT, NORTH CAROLINA I8533-0003
IN REPLY REFER TO
5090/07109
LN
April 13, 2015
North Carolina Department of Environment
and Natural Resources
Division of Water Quality
Information Processing Center
1617 Mail Service Center
Raleigh, NC 27699-1617
Subj: TRIENNIAL GROUNDWATER MONITORING
In accordance with the groundwater monitoring and reporting
requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for
Land Application of Wastewater Residuals, enclosed are the
original and one copy of the GW-59-A report and the four GW-59
reports (one each for monitoring wells 1, 2, 3, and 5) for the
triennial reporting for February 2015.
These reports are being submitted after the 31 March 2015
deadline as established in the permit due to an internal
administrative oversight.
Should you have any questions, please contact Mr. Timothy
Lawrence of the Environmental Affairs Department at your earliest
convenience at [phone].
Sincerely,
CR.AD O �'
Environm nta Affairs Officer
By directs n of the
Commanding Officer
Enclosure: (1)
GW-59-A
(2)
GW-59
for
MW-1
(3)
GW-59
for
MW-2
(4)
GW-59
for
MW-3
(5)
GW-59
for
MW-5

GW-59A COMPLIANCE REPORT FORM Permit # WQ0001489
(Submit one each monitoring period with Gtl -39 forms.)
Enter date monitoring results were Clue. (3/3^ 1/151 Will this monitoring report (GW-59 and GW-59A) be submitted after
YES
NO
I the
established due date?
X
2
Was any required information missing on the G1Y-59 report forms?
YES
NO
X
1F
the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems
encountered in obtaining the required mrormation
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
3
identification plate, area overgrown, etc.)? If the annreris" lei", contact the Regional Ofceforguidance
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
X
1f the answer to question 4 is "NO", skip to section 8
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards to the
space provided below
NIW-2 NIt3 1.73 mg/L
NIW-5 N113 2.99 mgJL
For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s)
YES
NO
5
in the same well(s) in the last two years?
X
If the answer to question 5 is "NO", skip to section 8
If the answer to question 5 is "YES", list in the space provided below, each well with constitumt(s) exceeding standards, concentration(s)
reported, and sample collection date for each occurrence (for the last two years).
Al\Y-5: Feb. 2015 N113 2.68 Feb. 2014 NI13 3.13; June 2013 N113 2.45; Feb. 2013 N113 2.25
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
X
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY
FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office.
Is the permittee implementing previously approved actions required by the Division involving this groundwater quality
VES
NO
7
problem?
If the answer to question 7 is "YES", describe those actions to the space provided below
if the answer to question 9 is "NO", contact the Regional-( ffice within 90 days: an evaluation may be required to determine the
impact the waste distiglal syslem is having at the review and compliance hounds ries surrounding this facility. Failure to do so may
subiect the permittee to a Notice of violation, fines, and/or penalties.
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with
8
GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submined in this repast (Compliance
Report GW-59A) is true and complete to the best of my knowledge.
Patricia T. Davis. Utility Systems Operator Supervisor
�����
Signature of Permittee (or Authorized Agent) Date 4?13/2015

SUBMIT FORM ON YELLOW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Please Print Clearly or Type
Name: MCAS Cherry Point
Name (if different):
Address: MCAS Cherry Point, NC 28533-0006
County: Craven
act Person: Patricia T. Davis Telephone #; 2524664599
Location/Site Name: Site 21. MCAS Cherry Point No.of Wells to be Sampled:
IPLING INFORMATION
L ID NUMBER (From Pennit):
Depth 26.66 ft.
MW-1
Depth to Water Level 82546: 1,5 ft. below measuring paint
Measuring Point is 1.33 ft. above land surface
',volume of water pumped/bailed before sampling: 5 Gal.
Samries for metals were collected unfiltered YES NO
34ON OF WATER.QUALITY-INFORMATION PROCESSING UNIT
MAIL SERVICE CENTER
OGH, NC 27699-1617 PHONE: [phone]
ber: kxptranon ware: rro
rge UIC
W00001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: infiltration Gallery
(� Spray Field Remediation:
Rotary Distributor [] Land Application of Sludge
Water Source Heat Pump other:
Date Sample Cottected 2/9/2015
Well Diameter 2
Screened Interval -0.17 ft to -15.2 t
Relative M.P. Elevation 1018
field
NO
if
FIELD ANALYSIS:
DRY at
pH 00400 6.71 units Temp 00010. 18 C time of
Spec. Cond. 00094 71 µMhos samplin(
Odor 00D85 NONE check
Appearance. CLEAR here:F1
LABORATORY INFORMATION
r. samle anal zed' 219/2015 Laboratory Name: MCAS CherryPoint / Pace Anal tical Certification Number. 201137706
e p y
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
m91L
Colifonn: MF Fecal 31616 <1
1100ml-
Nitrate (NO3) as N 00620 <0,05
mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Nola-. Use MPN method W highly WrW $-MPW$)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300 60
mg/L
Al - Aluminum 01105
mg/L
_
pH (Lab) 00403 6.71
units
Ba - Barium 01007
pg/L
TOC 00680
mg/L
Ca -Calcium 00916
mg1L
Chloride 00940 6,5
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
µg/L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
pg1L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610 <1.0
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia NmW on; NHS at N, Ammom N Jopen, TOW)
Mn - Manganese 01055
µg/L
TKN as N 00625
mg/L
Ni - Nickel 01067
pg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC. GCfMS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) 0 No (0)
Method#
Method#
Method#
Method#
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal%
• • S ._ t _,c=: =.•�_ 4/13/2015
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev.2/2010

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: MCAS
Permit Name (if different):
Facility Address: MCAS
Please Pnnt Clearly or Type
Point
Point, NC 28533-0006
County. Craven
act Person: Patricia T. Davis - Telephone * 252466A599
Location/Site Name. Site 21 MCAS Cherry Point No.of Wefts to be Sampled:
jl
DIVISION OF WATER -r, 1UAuTY4NFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH, NC 2769941617 PHONE: [phone]
PERMIT Number: Expiration Date: 7 31/201
Non -Discharge UIC
NPDES WQ0001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Q Remedlation: infiltration Gallery
Ej Spray Field Lr] Remedlation:
Rotary Distributor Land Application of Sludge
1EjWater Source Heat Pump r] other:
WELL
,MPLING INFORMATION
MW-2
Date Sample Collected,2/9/2015
FIELD ANALYSIS. p
C
WA5
DRY at
:LL ID NUMBER (From Permit):
Well Diameter 2
pH 00400 6.33 units Temp 00010 16
.time of
tti Depth 26,58 ft
to Water Level 8254& 4.5 fL below measuring point Screened Interval -1,03 It. to -11 fL
Spec. Cond. 00094. 701 µMhos
sampling,
check
pth
asunng Point Ric 1.28 it above land surface
Relative M. P, Elevation 14.8
Odor 00085 NONE
Appearance: CLEAR
here:
ume of water pumped/ba led before sampling:
5 Gal.
Triples for metals were collected unfiltered
YES �� Nt? and field acidified YES NO
,BORATORY INFORMATION
Name: MCAS Cher Point / Pace Anal tical
Certification Number: 201 / 37706
le anal zed' 21912015
Laboratory
... mp y
ZAMETERS NOTE: values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Caliform: MF Fecal 31616 <1
/100ml-
Nitrate (NO3) as N 00620 <0.05
mg/L
Coliform: MF Total 31504
Phosphorus: Total as P 00665
mg/L
-/100ml-
(Note.. use MPN maftd Tor hiehty tUrW campfes)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300 172
At - Aluminum 01105
mg/L
�mg/L
pH (Lab) 00403 6,33
units
Ba - Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 11.4
mg/L
Cd - Cadmium: Total 01027
µglL
Arsenic 01002
µg/L
Chromium: Total 01034
tag/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
Fe - Iron 01045
µg/L
,µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610 1.65
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Nd"en, NH, as N. Am"W" Nitrogen, Total)
Mn - Manganese 01055
µg/L
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) ❑ No (0)
Method#
Method#
Method#
Method#
Effluent Total VOCs: s
For Rernediation Systems Only (Attach Lab Reports): I nf luent Total VOCS:
cert,ty that to the Lest of my kriec9edle and belief, the mfcrmaGon submiCed to this report is true, aecurattf. and complete, and that the 13beratcry analy:ocal data Was produced using aFprcved methods cf analysis by a
p%*,', -(,n ned Saboratcry. 1 am avrare that tha: a arc slge.,ficanl ponaibes for submitting false intormatiom indudng the posc,b.i.ty of Lnes and lmpmonrnent for kno,; ng viola?ions.
15
Patricia T.�_ •. • (Date)
GW-59 Rev.
2/2
r r

— ma r snore nA1 vsr I nthf PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Please Print clearly or Type
Facility Name: MCAS Cherry Point
Permit Name (if different):
Facility Address: MCAS Cherry Point, NC 28533-0006
County: Craven
act Person: Patricia T. Davis Telephone M 252-466-4599
Location/Site Name: Site 21 MCAS Cherry Point No.of Welts to be Sampled:
SAMPLING_ INFORMATION
WELL ID NUMBER (From Permit): MW-3
Well Depth 25 58 ft.
Depth to Water Level 82546 0 ft. below measuring point
Measuring Point is 1,46 ft. above land surface
Volume of water pumped/bailed before sampling, 5 Gal.
,Samples for metals were collected unfiltered NO
I nt30RATORY INFORMATION
DIVISION OF WATER QUALITY -INFORMATION PROCE55INU urn 1`777
r 1617 MAIL SERVICE CENTER
RALEIGH NC 276994617 PHONE: [phone]t:
PERMIT Number: Expiration Date: 9
Non -Discharge UIC
NPDES W00001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon ❑ Remedlation: Infiltration Gallery
0 Spray Field Remedlation:
Rotary Distributor I] Land Application of Sludge
1 I-] Water Source Heat Pump ❑ Other,
Date Sample Collected: 2/9/2015
Well Diameter 2
Screened interval: -11.7 ft. to -21.7 ft.
Relative M.P. Elevation: 3.1
and field acidified itD YES ; I NO
WELL
FIELD ANALYSIS: u DRY at
PH 00400 6,69 units Temp 00010 18 c time of
Spec. Cond. 00094: 240 }iMhos samplinc
Odor 00085 NONE check
Appearance: TURBID here: r -I
e sam Inanalyzed: 2/9/2015 Laboratory Name: MCAS Cherry Point I Pace Anal tical Certification Number. 201 ! 37706
r
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg1L
Nitrite (NO2) as N 00615
mg/L
Coliform: MF Fecal 31616 <1
/100ml-
Nitrate (NO3) as N 00620 0.15
mg/L
Cotiform: MF Total 31504
/100ml-
Phosphorus: Total as P 00665
mg/L
(Note: use MPN method for hlghrytudnd samAles)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300 104
mg/L
AI - Aluminum 01105
mg/L
pH (Lab) 00403 6.69
units
Sa - Barium 01007 ^
ug/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 5 '
mg/L
Cd - Cadmium: Total 01027
t+9/L
Arsenic 01002
pg/L
Chromium: Total 01034 �
P9/1-
_
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
N9/L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
pg/L
Specific Conductance 00095
uMhos
K - Potassium 00937
mg/L
Total Ammonia 00610 71.0
mg/L
Mg - Magnesium 00927
mglL
(Ammonia Nrtrooen; NHS as N: AmmON A NNDQen. To"[)
Mn - Manganese 01055
P91L
TKN as N 00625
mg/L
Ni - Nickel 01067
pg/L
For Remedlation Systems Only (Attacn LaD Kepor15J: uupsc��s .
am*
Pb - Lead 01051 N9/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? CJ Yes(1) ❑ No (0)
Method#
Method#
Method#
Method#
TMA vnrc, VOC Removal%
f
4/13/2015
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please pent or type Signature of Permittee (or Authorized Agent} (pate)
GW-59 Rev.2/2010

ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Please Print Clearly or
Facility Name: MCAS Cherry Point
Permit Name (if different):
Facility Address: MCAS Cherry Point, NC 28533-0006
SUBMIT FORM ON YELLOW PAPER ONLY
County; Craven
3cl Person: Patricia T. Davis Telephone M 252-466-4599
Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled:
DIVISION ORWATER QUALITY4NFORMATION PROCESSING UNIT
1617 iWE- SERVICE CENTER
RALEIGH, INC 27699-1617 PHONE: [phone]
Non -Discharge UIC
NPDES WQ0001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon ❑ Remediation: infiltration Gallery
Spray Field Remediation:
J Rotary Distributor Land Application of Sludge
Water Source Heat Pump] Other:
SAMPLING INFORMATION
WELL ID NUMBER (From Permit): MW-5 Date Sample Collected: 2/5/2015 FIELD ANALYSIS:
Well Depth 13 fL Well Diameter 2 pH 0040o 6.05
Depth to Water Level 82546: 5.2 fL below measuring point Screened Interval: 3 ft, to 13 ft. Spec. Cond. 00094:
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: 12 Odor 00065:
Volume of water pumped/bailed before sampling: 5 Gal. Appearance
Samples for metals were collected unfiltered = YES R NO and field acidified � YES n NO
If WELL
units Temp 00010: 15 eC DRY at
time of
617 pMhos sampling,
NONE check
CLEAR here:
r..
LABORATORY INFORMATION
Date sam le analyzed 2/5/2015 Laboratory Name MCAS Cherry Point 1 Pace Analytical Certification Number 201
p
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COO 00335mglL
Nitrite (NO2) as N 00615
mgJL
Coliform: MF Fecal 31616 <1
1100mL
Nitrate (NO3) as N 00620 <0.05
mgJL
Coliform. MF Total 31504
1100mL
Phosphorus, Total as P 00665
mgJL
(Note Use PAPN mental for hgMy Wtbd samples)
Orthophosphate 70507
mgJL
Dissolved Solids:. Total 70300 210
mg/L
AI - Aluminum 01105
mgJL
pH (Lab) 00403 6.05
units
Ba - Barium 01007µg/L
TOC 00680
mg1L
Ca - Calcium 00916
mgJL
Chloride 00940 10.4
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium° Total 01034
µg1L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
µg/L
Fe - Iron 01045
µg/L
Sulfate 00945
mgJL
Hg - Mercury 71900
µg/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610 2,68
mgJL
Mg - Magnesium 00927
mg/L
(Ammom Nitrogen. NH, as. N. Ammonia N.VopeM TOW
Mn - Manganese 01055
uglL
TKN as N 00625
mg/L
Ni - Nickel 01067
pg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(i) ❑ No (0)
Method#
Method#
Method#
Method#
For Remediation Systems Only - • • •
P certify Ihal to the heel of my knot;led,je and hol cf, the infcrmation subm!lted in this report is true, accurate, acid complete, and that the Isbcratory analytical data +:,as produced us n3 arpro ed melhods of ana'ys s try a
Cr::O•certified hboralory I am ar;are ihat here are significant penalties for submitting false inforrnaLon mclad:na the pessib'il,ty of ones and lmprisonmenl for knoeing mefa+.rons.
4113/2015
DavisPatricia T. Operator
• s • '•• • • • •. . • • • a Agent)
4OV-59 Rev. 2/2
010

UNITED STATES MARINE CORPS
MARINE CORPS AIR STATION
POSTAL SERVICE CENTER $003
CHERRY POINT, NORTH CAROLINA 28S33-0003
IN REPLY REFER TO
5090/07109
LN
April 13, 2015
North Carolina Department of Environment
and Natural Resources
Division of Water Quality
Information Processing Center
1617 Mail Service Center
Raleigh, NC 27699-1617
Subj: TRIENNIAL GROUNDWATER MONITORING
In accordance with the groundwater monitoring and reporting
requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for
Land Application of Wastewater Residuals, enclosed are the
original and one copy of the GW-59-A report and the four GW-59
reports (one each for monitoring wells 1, 2, 3, and 5) for the
triennial reporting for February 2015.
These reports are being submitted after the 31 March 2015
deadline as established in the permit due to an internal
administrative oversight.
Should you have any questions, please contact Mr. Timothy
Lawrence of the Environmental Affairs Department at your earliest
convenience at [phone].
Sincerely,
G. W. �ZAD o
Environm nta Affairs Officer
By directs n of the
Commanding Officer
Enclosure: (1)
GW-59-A
(2)
GW-59
for
MW-1
(3)
GW-59
for
MW-2
(4)
GW-59
for
MW-3
(5)
GW-59
for
MW-5

C!V-59A COMPLIANCE REPORT FORM Permit # WQ0001489
(Submit one each monitoring period a-ith GIi 59 forms.)
Enter
slate monitoring results were Clue. (3/31/15) Will this monitoring report (GW-59 and GW-59A) be submitted after
YES
NO
I the
established due date?
Was
any required information missing on the GW-59 report forms?
YES
NO
2
IF
the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems
encountered
in obtaining the required information
Are
any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
3 identification
plate, area overgrown, etc.)? If the onsreris "les", contact the Regional Ofceforguidance
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If
the answer to question 4 is "NO", skip to section 8
If
the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentrauon(s) exceeding standards in the
space
provided below
AtW-2 NIB 1.73 mg/L
11Iw-5
NIi3 2.99 m L
For the constituents identified in question 4 above, have standards been exceeded previously for the some constituent(s)
YES
NO
5
in the same welts) in the last two years?
If the answer to question 5 is "NO", skip to section 8
If the answer to question 5 is "VFS", list in the space provided below, each well with constituent(s) exceeding standards, concentrations)
reported, and sample collection date for each occurrence (for the last two years).
biW-5: Feb. 2015 N113 2.68 Feb. 2014 N113 3.13; June 2013 N113 2.45; Feb, 2013 N113 2.25
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
6
if the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY
FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Once.
is the permittee implementing previously approved actions required by the Division involving this groundwater quality
VES
NO
7
problem?
t
If the answer to question 7 is "YES", describe those actions to the space provided below
If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be reauired to determine the
impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure tom so may
subiect the permittee to a Notice of violation, fines, and/or Penalties.
The person completing this portion (G%V-59A) of the monitoring report should sign below and submit this form with
8
GW-59 forms for required wells to the address provided at the top of the current GIV-59 farm.
I hereby acknowledge that. the above information was evaluated and the informadon submitted in this report (Compliance
Report GW-59A) is true and complete to the best of my knowledge.
Patricia T. Davis. Utility Systems Operator Supervisor
Signature of Permittee (or Authorized Agent) Date 4113,12015

ct IRMtT FnRM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM r 1617, GH. NERV 99-1610E TER
RALEJGH, NC 2Tti49-1fi1T PHONE:,[phone]
Name: MCAS
Name (if different):
Address: MCAS
Please Pant Clearly or Type
Point
Point, NC 28533-0006
County: Craven
act Person: Patricia T. Davis Telephone M _ 252466.4599
Location/Site Name: Site 21 MCAS Cherry Point No.of Wells to be Sampled
IPLING INFORMATION
L ID NUMBER (From Permit): MW-1
Depth 26.66 ft.
a to Water Level 82546: 1.5 tL below measuring point
luring Point is 1.33 ft. above land surface
ne of water pumpedlbailed before sampling: 5 Gal.
:les for metals were collected unfiltered YES 71 NO
ORATORY INFORMATION
Non -Discharge UIC
NPDES W00001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon ❑ Remediation: Infiltration Gallery
(� Spray Field Remediation:
Rotary Distributor Land Application of Sludge
rl Water Source Heat Pump other:
Date Sample Collected 2/9/2015
Well Diameter 2
Screened Interval -0.17 ft to -15.2 it.
Relative M.P. Elevation, 10.78
and field acidified
It WELL
FIELD ANALYSIS: WAS
e DRY at
pH 00400 6.71 units Temp 00010 18 C time of
Spec. Cond. 00094 71 µMhos sampling,
Odor 00085 NONE check
Appearance: CLEAR here:
e sample analyzed: 2/9/2015 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201137706
1AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg1L
Coliforn: MF Fecal 31616 <1
/100ml-
Nitrate (NO3) as N 00620 <0.05
mg1L
Coliform: MF Total 31504
1100ml-
Phosphorus: Total as P 00665
mg/L
(Nole: Use MPN mehod for highly lurbid sampled
Orthophosphate 70507 _
mglL
Dissolved Solids: Total 70300 60
mg/L
At - Aluminum 01105
m9/L
pH (Lab) 00403 6.71
units
ea - Barium 01007
µ9/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 6.5
mglL
Cd - Cadmium: Total 01027
119/L
Arsenic 01002
µg/L
Chromium: Total 01034
tigIL
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
µg/L
Fe - Iran 01045
µgIL
Sulfate 00945
mg/L
Hg - Mercury 71900µglL
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610 <1.0
mg/L
Mg - Magnesium 00927
mg/L
(AmmoNa NMW*n: NH, as N. Ammonia Nitrogen, Total)
Mn - Manganese 01055
µg/L
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L
For Remediation Systems Only (Attach Lab Reports): innuenr r oral vvt s:
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method M ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) ❑ No (0)
Method#
Method#
Method#
Method#
...... _.c _s,...,�_ 4/13/2015
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authonzed Agent) (Date)
GW-59 Rev.2/2010

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: MCAS Cherry Point
Permit Name (if different):
Facility Address: MCAS
Please Annt
Point, NC 28533-0006
SUBMIT FORM ON YELLOW PAPER ONLY
DIVISION OF WATER QUAUTY4NFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699!1617 PHONE: [phone]
or Type
Non -Discharge UIC
NPDES W00001489 Other
County: Craven
act Person: Patricia T. Davis Telephone # 252466-A599
Location/Site Name: Site 21, MCAS Cherry Point _No.of Wells to be Sampled:
IPLING INFORMATION
L ID NUMBER (From Permit): MW-2
Depth 26,58 ft
i to Water Level 8254& 4.5 fL below measuring pant
;unna Point r� 1.28 ft. above land surface
of water pumpedlba led before sampt.ng 5 Gal,
for metals were collected unfiltered j YES
PE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remedlation: infiltration Gallery
Spray Field Remedlation:
Rotary Distributor 0 Land Application of Sludge
Cl Water Source Heat Pump ;Other:
Date Sample Cnilected 2/9/2015
Well Diameter 2
Screened Interval -1.03 ft. to -11 It.
Relative M. P, Elevation 14.8
and
NO
WELL
4 DRY at
pH 00400 6.33 units Temp 00010 16 --time of
Spec. Cond. 00094: 701 µMhos samplin(
odor00085. NONE check
Appearance: CLEAR here:
FIELD ANALYSIS:
30RATORY INFORMATION
e sample analyzed 219/2015 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.05
mg/L
Coliform. MF Total 31504
/100mL
Phosphorus. Total as P 00665
mg/L
(Nate: Use MPN merhOd far highy turbid sampbs(
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300 172
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 6.33
units
Ba - Barium 01007
pg/L
TOG 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 11.4
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
pg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
µg/L
Fe - Iron 01045
pg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L
Specific Conductance 00095
pMhos
K - Potassium 00937
mg/L
Total Ammonia 00610 1.65
mg/L
Mg - Magnesium 00927
rngn-
(Ammutia Ntrogen, NHr as N. AmmoN Nitrogen, Total)
Mn - Manganese 01055
Pg/L
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) ❑ No (0)
Method#
Method#
Method#
Method#
•
For Remediation Systems •nly (Attach Lab Reports): Influent Total •.
I certrfy that to the brst of my 1k1ccded3e a.n.d be.i&rr, the information submrlted in this report is true, accurate, and complete, and that the Tabora±cry analytical data r:as produced us;ng approved methods 0 anat,sis by a
GC.'Q•camSed laboratory. I am ar;are Shot fh;e:e are s:nificartl pcnatttes fcr submill;ng fate informtion. indud:ng the possiw.ty of tines and impnsonment for kncving viola±ions.
Davis15
Patricia T. Operator 1
AuthorizedSignature of Permittee (or Authorized Agent) (Date)
Permiltee (or . or s
GW-59 Rev. 1 1

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Please Print Clearly or
Facility Name: MCAS Cherry Point
Name (if different):
Address: MCAS Cherry Point, NC 28533-0006
Contact Person:
Location/Site Name:
IPLING INFORMATION
SUBMIT FORM ON YELLOW PAPER ONLY
County: Craven
Patricia T. Davis Telephone #: 252—t66 4599
Site 21 MCAS Cherry Point No,of Welts to be Sampled:
L ID NUMBER (From Permit): MW-3
Depth 25.58 ft,
i to Water Level 82546: 0 ft, below measuring point
;unna Point is 1,46 ft. above land surface
of water pumpedlbailed before sampling 5 Gal.
s for metals were collected unfiltered j YES n NO
DEPARTMENTOFtryVIKUNmcn
6gSION OF WATER QUALITY -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH NC Z7699-161T PHONE: [phone]Z:
n-Discharge UIC
DES W00001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
Q Lagoon ❑ Remedlation: Infiltration Gallery
0 Spray Field ❑ Remedlation:
Rotary Distributor Land Application of Sludge
Water Source Heat Pump ❑ Other
Date Sample Collected: 2/9/2015
Well Diameter 2
Screened interval: -11.7 ft. to -21.7 ft
Relative M.P. Elevation: 3.1
field
FIELD ANALYSIS: o DRY at
pH 00400 6.69 units Temp 00010: i8 � time of
Spec. Cond. 00094: 240 liMhos sampling,
Odor 00085: NONE check
Appearance: TURBID here:l—I
F&MTORY INFORMATION
1 anal ed' 2/9/2015 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201 / 37706
e samp a Yz
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 __
^
mglL
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00520 0.15
mg/L
Coliform: MF Total 315041100mL
Phosphorus: Total as P 00565
m91L
mg/L
(Note. use MPN method for "hly tum-d samples)
Orthophosphate 70507
Dissolved Solids: Total 70300 104
mg/L
AI -Aluminum 01105
mg/L
pH (Lab) 00403 6.69
units
Ba -Barium 01007 ^�
µ4lL
TOG 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 5
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
pg/L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L
Specific Conductance 00095
µMhos
K - Potassium 00937 -
mg/L
Total Ammonia 00610 <1.0
mg/L
Mg - Magnesium 00927
mgfL
(Ammonm Ndfogen; NHI as N. Ammons NNopen, TOWS
Mn - Manganese 01055
tlgn-
TKN as N 00625
mg/L
Ni - Nickel 01067
µ9/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg1L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) ❑ No (0)
Method#
Method#
Method#
Method#
a �+e­ n. lu rAHarh Lah Reports): Influent Total VOCs: Effluent Total VOCS: VOC Removal%
. _ 4/13/2015
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type Signature ai Permittee (or Authorized Agent) (Date)
GW-59 Rev.2/2010

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Please Print Clearly or
Name: MCAS Cherry Point
Name (if different):
Address: MCAS Cherry Point, NC 28533-0006
SUBMIT FORM ON YELLOW PAPER ONLY
County Craven
act Person: Patricia T. Davis Telephone #: [phone]
Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER
RALEIGH. NC 27699-1617 PHONE: [phone]
Non -Discharge UIC
NPDES W00001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
n Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
1 ❑ Water Source Heat Pump ❑ Other
WELL
SAMPLING INFORMATION
WAS
WELL ID NUMBER (From Permit): MW-5
Date Sample Coifected: 2/5/2015
FIELD ANALYSIS:
15 C
DRY at
13 ft.
Well Diameter 2
pH 00400 6.05 units Temp 00010
time of
Well Depth
Depth to Water Level 82546: 5.2 ft. below measuring point Screened Interval 3 ft. to 13 ft.
Spec- Cond. 00094: 617 µMhos
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: 12
Odor 00085: NONE
check
here:
Volume of water pumped/bailed before sampling:
5 Gal.
Appearance CLEAR
a.
,Samples for metals were collected unfiltered
NO and field acidified YES NO
LABORATORY INFORMATION
Laboratory Name. MCAS Cherry Point I Pace Analytical
Certification Number 201137706
Date sample analyzed: 2/512015
PARAMETERS NOTE: values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mglL
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.05
mg/L
Coliform. MF Total 31504
/100mL
Phosphorus Total as P 00665
mg/L
jNote us. MPN matnad for hghfy kKW samples)
Orthophosphate 70507
mg1L
Dissolved Solids, Total 70300 210
mglL
AI - Aluminum 01105
mg/L
pH (Lab) 00403 6.05
units
Ba - Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium G0916
mg/L
Chloride 00940 10.4
mg/L
Cd - Cadmium: Total 01027
pg/L
Arsenic 01002
µg1L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mglL
Phenol 32730
µg/L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610 2.68
mg/L
Mg - Magnesium 00927
mg/L
(Ammorva NRropen. NHi as N, Ammon a Nmopen, Totaq
Mn, - Manganese 01055l,
µg/L
TKN as N 00625
mglL
Ni - Nickel 01067
µg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes0) ❑ No (0)
Method#
Method#
Method#
Method#
•
For Remedlation Systems • Reports): influent Total
I Certify Thal to the hest of my knorrlcd:7e and hv.Lcr, the intermotion submitted to Inms report is true, accurate, and complete. and [hot the uticratary analytical data v:as proda ed us'n3 approved methods of analysis by a
D'::O-certified laboratory 1 am avrare that there are signrficanl penalties torsubmitt ng false lntormafon inclad:ng the pcssib.l,ty et tines and imprisonment fer knoving welatrons.
Patricia15
Davis• a s 1
GW-59 Rev.
2/2
1 1

GW-59A COMPLIANCE REPORT:FORM: . , ''Permit #' WQ0001489
(Suiniii:one eaeh monitoring period iilith,GlY-59 fnraes.)
Enter date monitoring results were.due. 7 3(/ 11151' Will this -monitoring report (PW49 and GW=59A) be submitted niter ;:
_ YES
NO,:; ..
1
the established due data?: ' "
X.
any required, information. missing on the GW-59, report forms?. :<
YES
NO
IWOs
2
`•
X
IF the answer to question I or 2 is "YES", list in the space provided. below the %vItidentilication numbers) and explain the pniblems .. .
encountered in obtaining the required'information,
Arc any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
3
identification plate,; area overgrown, ete.)7 jthe armVer is: !'Yes_. +contact the Regional Opcefor,guidance,
Are.any monitored constituents equal to or:above the established standards'..
YES
: NO
if the answer to question.4 is "NO", skip to section 8.. .
If the answer to question 4•is "YES" listthe affected %+ells individually with constitueat(s) and concentration(s) exceeding standards in the
space provided below
For the constituents identified in question "4 Above, have standards been exceeded. previously for the saute constituents) ,
YES
NO
5
in,thesame well(s) in the last two years?"
X .
If the answcr to: question. S: is "NO", skip to section 8, . '
if the answer to question 5 is "YES"; list' in the space pto4ided below; such well W1 aoFlStituetit(s);ehceedmi; standards,, concentration(s).
reported.- and sample collection date far each -occurrence (for the,lasi two years).
Are the monitoring wells listed in section 5 located at or beyond: the review boundary?
YES
NO
ti
If the answer Is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL, OFFICE INIMEDIATELY '
FOR GUIDANCE. If the answer is "NO";:moultoring wells may be Improperly loeuted; contact the Reglom it Office.
Is: the.permitteeimplementing: previously, approved"actions required by the Division involving.this groundwater quality.
YES
NO
7
probiem7
If the answer to .question 7, is "YM. ; describe those:actions in,the;cpace provided below. .
If the answer to question 7 is "NO". Contact the Regional Ofiice within 90 devst an evaluation may he required 16 determine the .
Impact the waste disrro+al system is having rt the reviewand eomntiance beundraries aurronndine this facility: Failure to do so may
ssubieet the nermiltee to a Notice or Violation. finew and/or nendlllee:'
The person. completing this portion (G1V-59A) of the monitoring report should sign, below aad.submit this rorm.with .
$
GW-59 forms for required wells to the address provided at the top of the current GW-59 form. .
1 y, ac a e;thatth�e "abuVe information,wasgvaluated and e,tn atton s bi cdjn is t+epott ('Comphanca
✓^.Y ''w••x.fiN
+ n' W' 3=. # �.0 d � �ai+ a<1+�,.1k. "i ,fir a'-tr nay z V g � ,F h M tu�+C,'$�,'v'KMry
ReportGW 59A)lsuu andoompiete��Ct�ibebeesta�my towledge M a a F �
�k
:Patricia T. Davis, Utility Systems. Oia(or Supervisor
....
'
'
Si natnre:of Permittee for Authorized •:.
orized Agent) Date ..: 7f13i+2015
.

SUBMIT FORM ON YELLOW PAPER ONLY r ...• `: `
QUALITY MONITORING:
_ • .
tl INATU
� �xDEPA DF ENItiRONInt:Nld� RAL�RE
DIVISION oF. �M41JAtm-tNFORMAnoKPROc
GROUNDWATER
!n��++e,kbd^°aN
COMPLIANCE REPORT FORM
L 1s�70AISERVICEZENT ON,
`M�k, PHONE-(9t9}7333221.,;,�
„
RACEICIH,H,NCilZT899.161Tm•
FACILITY INFORMATION ° PlessePrintClesrlyorType
PERMIT Number •�'. Expiration Date:; 7/31/2019
Facility Name MCAS CherryPaint
Non -Discharge UIC .
Permit Name (if different);
NPDES W00001489 . _ Other _
Facility Address: MCAS CherryPoint, NC 28533-0006
TYPE OF PERMITTED OPERATION BEING MONITORED
O Lagoon ❑ Remediation: infiltration Gallefy°� :
County: Craven
'
❑ Spray Field ❑ Remedlatio*
ism"I
s
Contact Person: Patricia T. Davis, Telephone M.252-4 664599
-
❑ Rotary Distributor ❑ Land Application of Sludge, .
Well Location/Site Name:, Site 21, MCAS Cherry Point
No.of Wells to be Sampled: 1
❑ Water Source Heat Pump ❑ Other
ELL
SAMPLING INFORMATION
W S'_
Wes'
WELL ID NUMBER (From Permit)t MW-1;
Date Sample Collected: 6/23/2015 .. FIELD ANALYSIS:
°C
DRY at '
Well Depth 26,66 ft..
Wail Diameter 2 .
pH 004t>D 6.5 urrts Tempf}t}d10: 24;
time of
Depth to Water Level 82548: - 3.5 ft below measuring pant
Scieened Interval: -0.17:
ft. to ..15.2 - IL Spec. Cond. 00094 119 NMhos
sampling,
Measuring Point is' 1.33 ft° above land surface
Relative M.P. Elevation: 10.78 Odor 00085: None
`
check
here:
Volume of water pumped/bailed before sampling: 5 Get.
Appearance;... Clear.
o�
Sam 'tes for metals were collected unfiltered ❑ YES •
NO and field acidified .YES
_ NO
LABORATORY INFORMATION
Date sample analyzed: 6/231201S
Laboratory Name: MCAS Cherry Point Pace Analytical Certifca$on Number. 201 / 37706
PARAMETERS NOTE -Values should reflect dissolved andcolloidal
concentrations.
COD 00335^�mg/L
Nitrite (NO2) as N W615
mg1L Pb - Lead 01051. - µglL
Colifomtt` MF Fecal 31616 .- <i /1OOmL
Nitrate (NO3) as N 00620 <0.1 mg►L Zn -Zinc 01092 mg/L'
Coliform: MF Total 315u4 /100mL
tNoso: useMaNiiiatlwdtort+ Mwroiasama�ea)
- PhosphorusI.Total as P 00665
Orthophosphate 70507
mg/L
mgiL Other (Specify Compounds and Concentration Umts)�:,_,
Dissolved Solids: Total 70300-. 44 : _ . mg/L
AI : Aluminum 01105
pH (Cab) 00403 6.5 units
Be - Barium 01007
TOC 04680 mglL
Ca, Calcium 00916
mg
Chloride 00940 12 mgiL
Cd =Cadmium: Total 01027
µglL
Arsenic 01002 µg/L '
Chromium;, Total 01034
µ k.
Grease and Oils 00552 ' . .' mg/L
Cy - Copper 01042°�mg/L
. ORGANICS`(by GC, GC1MS,_ HPLC)
Pheno132730 µglL
Fe -Iron, 01045 '
• p (Specify test and`m®thad #: ATTACH LAB REPORT.)
''
Sulfate 00!)45. - mg1L _
Hg'-Mercury 71900
pglL Lab Report Attached? El Yes(1) . ❑ No'
Specific Conductance 00095 - µMhos
K - Potassium 00937
mglL :Method#,
Total Ammonia 00610; <1:0 mglL'
Mg a Magnesium 00927
IL ,Method#
(PUmiorra N{ nam NH3 as N; Ammdtia MrWn, TOO!) '
Mn - Manganese 01056
pg!L... ; Me thod#.,,
TKN as N 00625. mgll.
Ni - Nickel01067
pg1L Method#
For Remediation Systems Oniy (Attach Lab Reports):
Influent Total VOCs:
7—
Effluent Total VOCst VOC Remov al96;
'1777777777777=
.....: 7113l2015
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorised Agent) Name and Title -Please print or type - -.
Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev, 212010

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:.'
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or. Type
Facility Name: MCAS Chen Point
Permit Name (if different): .
Facility Address; MCAS Cherry Point, NC 28533.0006
IS
County: Craven
act Person: Patricia T. Davis Telephone #; 257-466-4599
LocationlSite Name: Site 21i MCAS Cherry Point No,of Wells to be Sampled: 1
("mom
.LL 10 NUMBER (From Permit): MW-2 =
4 Depth 26.58 fL
3th to Water Level 82546: 9.5 fL below measuring point
asuring Point is 1.26 fL above land surface
ume of water pumped/bailed before sampling.; 5 Gal,
nples for metals were collected unfiltered .. n, YES
BORATORY INFORMATION
Non -Discharge ' UIC
NPDES WQ0001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
[� Spray Fleld ❑ Remediatlon;
❑ ' Rotary Distributor 0 Land Application of Sludge
❑ Water Source Heat Pump ❑ Other.
Date Sample Collected: 6/2312016 FIELD ANALYSIS:
Well Diameter, 2 pH 00400 5.8 units Temp 00010: 25 °C
Screened Interval: 4.'03 ft. to -11 . ft. Spec. Conti. 00094: 740 µMhos
Relative M.R Elevation: 14.8 . - Odor 00085: None
Appearance: Clear
and field acidified n YES ❑ NO
Ile sample analyzed: 6/2312015 Laboratory Name: _ . MCAS Cherry Point / Pace Analytical,
AAMETERS NOTE.,, Values should reflect dissolved and colloidal concentrations;
Certification Number_ 201 /
COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L
Coliform: MF Fecal 31616 <1 1100mL Nitrate (NO3) as N 00620 <0.1 mg/L Zn - Zinc 01092 mg/L
at
of
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00565
mg/L
(Note, Use MPNmeOwdrm►,orayw W$amlmal
Orthophosphate 70507
mgiL
Other (Specify Compounds and,Concentration Units):
Dissolved Solids: Total 70300 152.
mg/L
Al'Aluminum 01105
mg/L
OH (Lab) 00403 5.8
units
Ba-, Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 8.9.
mg/L
Cd -Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg/L'
Cy - Copper 01042
mg/L
ORGANICS (by GC, GCIMS, HPLC)
Phenol 32730
µg/L
Fe - Iron 01045
µg/L
(Specify test and method M. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 719DO
µglL
Lab Report Attached? ❑ Yes(1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
; Method#.
Total Ammonia 00610 . 1.2
mg/L
Mg -. Magnesium 00927
mg1L
, Method#
(Ammonia Nkopen; NNI as N. Amor" Nbnen, rail
Mn - Manganese 01055
µg/L
, Method#
TKN,as N 00625
mg/L
Ni - Nickel 01061
µ91L
, Method#
c... a.,r—f—a rinlu rA#arh I ah Rannrtcl-' Influent Total
Effluent Total VOCs: VOC Removal°%
(cer'.,7!tta! !o !lie be.St of my kno •. eC.,e and Lef e!,!t„e 7.5101=1:loa sutl,m;,ed' is !ttisrep ort is !rue,.. acct rt:e:.•nnd earn, !e:e: and !hut :he !3xato: / an:.l;,icra _,.:a .1as ;t.odc:rc;! usin;; a, fro -en .�ctf;o..., o' .....�I}•sis L� a
e ,!.at there are s gad .:at pera res!or st:br ,tng !<a.!se r itorrnatio.i, iuudin g Me p oss hr.;:y a fines and ,!mp:isoflmest Tpr kno:, nq riol3lionS,
7113/2015
Patricia T. 1 .
-- , , ',- - - - - ,' c - , , -, - D-
te
1 1

SUBMIT FORM ON YELLOW PAPER ONLY
• � DEPAR iMEN3 OF ENNIRONMFIrT tL NATURAL RE90UM.
GROUNDWATER QUALITY MONITORING: - . DiV1310NOPWATERQUALITY41111FORMATIONVICENTER
PROCESSI KiU T �;fr3
COMPLIANCE REPORT FORM aRp 1sits
r��„,
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number. Expiration Date: 7131/2019
Facility Name: MCAS Che Point Non -Discharge UIC
Permit Name (if different): NPOES. " WQ0001489.. Other
Facility Address: MCAS Cherry Point, NC 28533-6066.` TYPE OF PERMITTED OPERATION BEING MONITORED
County: Craven ❑ Lr.agoon ElRemediation� Iniiitration Gallery.
(crl iswq iui. ❑. Spray Field ❑ Remediation:
Contact Person: Patricia T. Davis Telephone #: [phone] ❑ -Rotary Distributor 0 Land Application of Sludge
Well LocationlSite Name: Site 21 MCAS Chevy Point No.of Wells to:be Sampled: 1 0 Water Source Heat Pump []other
SAMPLING INFORMATION If WELL
WELL ID NUMBER (From Permit): MW-3 Date Sample Collected: 6123/2015 FIELD ANALYSIS: WAS
e DRY aE
Well Depth 25.58 fL Well Diameter. 2 pH OD400 .5.5, units_ Temp 00010:- . 25,.0 time of
Screened Interval: -11.7 fL to .-211 ft., . Spec Cond, 00094:v . - - µMhds sampling;
Depth to Water Level 82546: 0 IL below measuring pant 282
Measuring Point is 1.46 ft above land surface Relative M.P, Elevation: 3:1 Odor 00085: None. check.,.'.--
Volume of water pumpedib fled before sampling: 5 Gala Appearance Turbid here:
Sam les for metals were collected unfiltered ❑ yES El NO and field acidified YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/23/2016 Laboratory Name: - MCAS Cherry Point 1 Pace Analytical Certification Number,. 201137706
PARAMETERS: NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mglL . Nitrite (NO2) as N 00615 mg1L Pb - Lead 01051 ' .. µg1L
Coliform MF Fecal 31616 <1 1100mL Nitrate (NO3) as N 00620 0,3 . mg1L - Zn.- Zinc 01092, mglL
Coliform: , MF Total 31504 /100mL-. Phosphorus: Total as P 00665 ' : mg/L
iiwm'u.a MON inejwil1wrW.ra.b+awn > Orthophosphate 70507 mg1L Other (Specify Compounds and ConcentrationUnits}
Dissolved Solids: Total 70300.....152 mg1L Al m Aluminum 01105 mg/L '
pH (Lab) 00403 5,5 units Ba - Barium 010.07 µg/L .
TOG 00680 mg1L Ca - Calcium 00916 mg1L
Chloride 00940, : 5 : mg1L Cd - Cadmium: - Total 01027 µg(L
Arsenic 01002 pg1L - Chromium: Tota101M4 pg/L
Grease and Oils 00552 niglL Cy - Copper 01042 `mg1L ORGANICS (by GC; GC/MS, HPLC) '
Phenol 32730 µglL Fe -Iron 01045 µg/L . (Specify test and method #. ATTACH LAB REPORT.)
Sulfate D0945 mglL Hg - Mercury 71900 . µg1L Lab Report Attached? . ❑ Yes(7) ❑ No (0) : , '
Specific Conductance 00095, , µMhos K,- Potassium 00937 mg/L ; - k Methodf�
Total Ammonia 00610 <1A mgtL Mg - Magnesium 00927 mglL. Method#
(AMnoda Nitrogen: NH3 as N; Anwoonia NdMen, ToW.) _ Mn - Manganese 01058 - _ - µg1G « Method#
TKN as N 00625. mg/L N! = Nickel 01067 µg/L .Method#
For Remedia y ( ;.
lion Systems Only Attach Lab Reports): Influent Total VOCs: Effluent Total VOCS: VOC Removal96
Parla
T: Davis - UOrty Systems Operator-7/13/2015
Pe_rmittee (or Authonzed Agent) Name and Title -'Please Please print ortype -' Signature'of Permittee (or Authorized Agent) ": '.-' ` ,_" ° . (Date)'
GW-% Rev., 212010

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: MCA$ Cherry Point
Permit Name (if different):
Facility Address: MCAS Cherry Point, NC 28533-0006
SUBMIT FORM ON YELLOW PAPER ONLY
Fehr Clearly or Type
County:
act Person: Patricia T. Davis Telephone #: [phone]
Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1
in -Discharge UIC
DES WOOM1489 Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedlation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION
WAS
WELL ID NUM13ER (From Permit): MW-5
Date sample Collected: 6/22/2015
FIELD ANALYSIS:
27 °C
DRY at
Well Depth 13 it.
Well Diameter. 2
pH 00400 5.8
units Temp 00010:
time of
Depth to Water Level 82546: 8.5 ft. below measuring pant
Screened Interval: 3 ft. to 13
ft. Spec. Cond. 00094:.
496
pMhos
sampling,
Measuring Point is 3 it. above land surface
Relative M.P. Elevation, 12
Odor 00085:
Norte
check
Volume of water pumpedlbailed before sampling: 5 Gal.
Appearance:
Clear .
here;
C=mnlve fnr r.sPtwlc were rsAlecfecd unfiltered n YES n NO
and field acidified ❑ YES. ❑ NO
-
30RATORY INFORMATION
e sample analyzed: 6/22/2015 Laboratory Name: MCAS Cherry Point! Pace Analytical Certification Number.- 201137706
tAMETERS NOTE: Values should reflect dissolved and colloldal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 '
mg/L
Coliform: MF Fecal 31616
<i
1100mL
Nitrate (NO3) as N 00620 <0.I
mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN matlwd for hV* tumid samples)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300
208
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
5.8
units
Ba - Barium 01007
µg►L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
18
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
pg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Pheno132730
µg/L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
µglL
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610
<0.1
mg/L
Mg;. Magnesium 00927 _
mg1L
(Ammonia NhMen: NH3 as K Ammmia NmoQen, Totn!)
Mn - Manganese 01055
µg/L
TKN as N 00626
mg/L
NI - Nickel 01067
µg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.).
Lab Report Attached? • ❑ Yes(1) ❑ No (0)
Method#
Method#
Method#
Method#
For Remediation Systems Only (Attach Lab Reports): Influent Total Vvcs: rrnuem i orat vutos: resnnuvm io
a
, 7113/2015
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev.2/2010

UNITED STATES MARINE CORPS
MARINE CORPS AIR STATION
POSTAL SERVICE CENTER 8003
CHERRY POINT, NORTH CAROLINA 23533.OM
IN REPLY REFER TO'
5090/07109
LN
July 13, 2015
North Carolina Department of Environment
and Natural Resources
Division of Water Resources
Attn: Information Processing Center
1617 Mail Service Center
Raleigh, NC 27699-1617
Subj: TRIENNIAL GROUNDWATER MONITORING
In accordance with the groundwater monitoring and reporting
requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489-for
Land Application of Wastewater Residuals, enclosed are the
original and one copy -of the GW-59-A report and the four GW-59
reports (one each for monitoring wells 1, 2, 3, and 5) for the
triennial reporting for June 2015.
Should you have any questions, please contact Mr. Timothy -
Lawrence of the Environmental Affairs Department at your earliest
convenience at [phone].
Sincerely,
G. W. F
Environmen al ffairs Officer
By direction of the
Commanding Officer
Enclosure: (1) GW-59-A
(2)
GW-59
for
MW-1
(3)
GW-59
for
MW-2
(4)
GW-59
for
MW-3
(5)
GW-59
for
MW-5

GW-59A COMPLIANCE REPORT FORM Permit # WQQ001489
(Subnrll one each nronitnriirg period ts,ith GIV--59 forms.)
Enter date monitering'results were due. 7/{ 31/151 Will this monitoring report (GW-59 and GW-59A) be submitted after . YES NO
l the established due date?
2 Was any required information missing on the GIV-59 report forms? YES NO
a:.
IF the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems
encountered in obtaining the required information.
Are any of the monitor wells In need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES I NO'
3 identification plate, area overgrown, etc.)? lf(he aria=eris "Yes". epntactthe Regional Opceforguldance, \ .
4 Are nay monitored constituents equal to or above the established standards? YES NO
If the answer to question 4 is "NO", skip to section B.
1f the answer to question 4 is "YES" list the at%@ted wells individually with constituent(s) and corteentradWs) exceeding standards in the
space provided below.
For the constituents identified in question 4 above, have standards been exceeded previously for the some constituent(s) YES NO
5 in the same well(s) in the last two years? a
Irthe answer to question 5 is "NO", skip to section 8,
it the answer to question 5 Is "YES". list in the space ptovided below, each welt with com0tuent(s) exceeding standards, concentrations)
reported, and sample collection date for each occurrence (for the last two years).
6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? I YES I NO I
answer Is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY '
GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office.
II Is the permittee implementing previously approved actions required by the Division involving this groundwater quality YES I NO
7 problem?
If the answer to question 7 is "YES". describe those actions in the space provided below,
If the answer to question 7 Is "NO". contact the Regional Ottice within 90 days: an evaluation may be required to determine the
impact the waste disposal system Is having at the review and eomnliance boundaries surrounding this facility Failure to do so may
subject the nermittee to a Notice er Violation. finm and/or penalties.
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with
S
G%V-59 forms for required wells to the address provided at the top of the current GW-59 forth.
-- ems' M '-- (2^�'s '..*'pus, n,
I;hcreby°ackttowlt dge flint the ab vetiafotrnetIon was evaluated t nd:i formation sabtnttiedtiit'tiiis'tepo (Complitittec
lieliort OW-59A) is true and complete to,the bestofmyknowledge- # t Y
R m , a
Patricia T. Davis, Utility Systems Operator Supervisor
Y6.L1 f
Signature of Permittee (or Authorized Agent) Date 7,413120151

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
r A^11 rry 1mcf1DUATIAN Please Print
Facility Name: MCA$ cnerry volnr
Permit Name (if different):
Facility Address: MCAS Cherry Point, NC
SUBMIT FORM ON YELLOW PAPER ONLY
County: Craven
act Person: Patricia T. Davis Telephone #: [phone]
Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: �1
Nnn-fliarharne
UIC
DES W00001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
El Lagoon ❑ Remedlation: Infiltration Gallery
Spray Field Reinedlation:
Rotary Distributor Q Land Application of Sludge
Water Source Heat Pump ❑ Other.
IYi.IIYta IiYr'Vltmna,v,.
Permit): MW-1
LID NUMBER (From Pe rm
sam
Date Sample Collected: 6/23/2015
FIELD ANALYSIS: ,�C
6.5 Temp 00010, 24
DRY at
—
Depth 26 ft.
Well Diameter, 2
Screened Interval: -0.17 ft. to -15.2 IL
pH 00400 units
Spec. Cond. 00094: 119 µMhos
time of
sampling,
to Water Level 82546: 3.5 ft. below measuring pant
Relative M.P, Elevation: 10.76
Odor 00085: None
check
wring Point is 1.33 ft above land surface
Appearance: Clear
here:El ,
ne of water pumped/bailed before sampling: 5 Gal.
ales for metals were collected unfiltered YES
NO and field acidified YES NO
ORATORY INFORMATION
Name: MCAS Cherry Point / Pace Analytical
Certification Number. 201 1377
le anal zed 6/2312015
Laboratory
tAMETERS NoTE: Values should reflect dissolved and colloidal concentrations.
mg/L
COD 00335�,,m9/L
Nitrite ( as N 00615
Ni)
Coliform; MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0,1
mg/L
mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
m9/L
fyter
tNote: Use MPNmetladIWNO bidse 0")
Orthophosphate 70507 _
mg/L
Dissolved Solids: Total 70300 _ 44
mg/L
AI - Aluminum 01105
pH (Lab) 00403 6.5
units
Ba - Barium 01007
µg/L
mg/L
TOC 00680
mg1L
Ca - Calcium 00916
Chloride 00940 12
Cd -Cadmium: Total 01027
µg1L
,mg/L
Arsenic 01002��trg/L
Chromium: Total 01034µg/L
Grease and Oils 00552 _
mg/L
Cy - Copper 01042-
mg►L
Phenol 32730
µg/L
Fe - Iron 01045 _
µg/L
Sulfate 00945
H Mercury 71900µg/L
9 - �'m91L
mg/L
Specific Conductance 00095
µMhos
K - Potassium OD937
mg/I.
Total Ammonia 00610 41.0
mg/L
Mg - Magnesium 00927
Mn - Manganese 01055
µg/L
(AmmaraNitrogen:NH, asN,Affvpw Nitrogen.Temlx
Ni - Nickel 01067
TKN as N 00625
mg1L
_.^µg/L
For Remedlation Systems Only (Attach Lab Reports):
Influent Total VOCS:
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev, 212010
Pb- Lead 01051 µg/L
Zn - Zinc 01092�_-mg1L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #• ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) ❑ No (0)
Method#
Method#
Method# .
, Method#
Effluent Total VOCs:
VOC Removal%
7/13/2015
Signature of Permittee (or Authorized Agent) (Date)

OUNDWATER QUALITY MONITORING:
MPLIANCE REPORT FORM
Name: MCAS
Name (if different):
Address: MCAS
SUBMIT FORM ON YELLO PAPER ONLY
Please print c/eady or Type
Point -
Point, NC 28533.0006
County: Craven
act Person: Patricia T,, Davis Telephone M 252-4664599
Location/Site Name: Site 21 MCAS Chevy Point No,of Wells to be Sampled:
L ID NUMBER (From Permit): MW-2
Depth 26.58IL
h to Water Level 82546: 9.5 ft. below measuring point
wring Point is 1.28 fL above land surface
ne of water pumped/bailed before sampling; 5 Gal,
for metals were
YES
NO
Non -Discharge UIC
NPDES WOCOO1489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor Q Land Application of Sludge
11 Water Source Heat Pump ❑ Other. _
Date Sample Collected: 6/2312015
Well Diameter. 2
Screened Interval: -1.03 ft. to -11 ft.
Relative MP, Elevation: 14_8
WAS
FIELD ANALYSIS: eC DRY at
pH 00400 5.8 units Temp 00010: 25 • time of
Spec. Cond. 00094: . 740 (iMhos samplinc
Odor 00085: None_ check
Appearance: Clear here:❑
30RATORY INFORMATION
e sam le analyzed• 6/23/2015 Laboratory Name: MCAS Cherry Point /Pace Analytical Certification Number. 201
p
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
m9/L
e (NO2) as N 00615
mg/L
Coliform: MF Fecal 31616 <1
1100mL
Nitrate (NO3) as N 00620_<0.1
� mgtL
Coliforrm MF Total 31504
/100mL
Phosphorus: Total as P 00665�mg/L
mg1L
(Note, use MPN meows fa h4Wy WdAd samPas)
Orthophosphate 70507
Dissolved Solids: Total70300 152
mg/L
AI -Aluminum 01105mg/L
PH (Lab) 00403 5.8
units
Be.- Barium 01007µg1L
-
mg/
TOC 00660
mg/L
Ca Calcium 00916
-
Chloride 00940 8^ 9
mg/L
Cd -Cadmium: Total 01027 _
µ9/L
Arsenic 01002µg/L
Chromium: Total01034�_µg/L
Grease and Oils 00552-mg/L
Cy - Copper 01042�-mg/L
Phenol 32730!_pg/L
Fe- Iron 01045
Ng/L
Sulfate 00945mg/L
Hg - Mercury 719DO.PgfL
Specific Conductance 00095
K -Potassium 00937
mg/L
_�_PMhos
Total Ammonia 00610 1.2. _mg/L
Mg -Magnesium 00927_�
L
(Ammonia Nis wm; NH, es N; AmmcnW Ntmpe0. TOW
Mn - Manganese 01055
pg/L
µ91
TKN as N 00625
mg/L
NI - Nickel 01057Ng1L
Pb - Lead 01051 pg/L
Zn - Zinc 01092_-mg/L
Other (Specify Compounds and Concentration Units):.
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? - ❑ Yes(1) ❑ No (0)
Method#
Melhod#
Method#
Method#
Influent Total VOCs: Effluent Total VOCs: VOC Removal%
For Remedlation Systems Only (Attach Lab Reports):
7li312015-
Patricia T. Davis - Utility Systems O eraiar Signature of Permittee (or Authorized Agent) (Date)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.212010

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: MCAS
Permit Name (if different):
Facilitv Address: MCAS
Point
SUBMIT FORM ON YELL W PAPER ONLY
or
County: Craven
act Person: Patricia T. Davis Telephone M 252466-4599
Location/Site Name: Site 21 MCAS Cherry Point No.of Wells to be Sampled:1
n-Discharge UIC
DES WO0001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ lagoon ❑ Remedlation: infiltration Gallery
Spray Field Remedlation:
Rotary Distributor 0 Land Application of Sludge
❑ Water Source Heat Pump ❑ Other.
WILING INFORMATION
LID NUMBER (From Permit)- MW-3
sam
Date Sample Collected: 6123/2015
FIELD ANALYSIS:
o
25 C
WAS
DRY at
—
Well Diameter 2
pH 00400 5.5 units Temp 00010:
time of
Depth 25.58rM ft.
0 ft. below measuring pant
Screened Interval: -11.7 ft. to -21.7 ft.
Spea. Cond, 00094: 282
NMhos
sampllnt
h to Water Level 825411
wring Pant is 1.46 ft. above land surface
Relative M.P. Elevation: 3.1
—i�
Odor 00085: None
Appearance: Turbid
check
here:
ne of water pumped/bailed before sampling: 5 Gal,
YES ❑ NO
Dies for metals were collected unfiltered ❑ YES
Q NO and field acidified Q
ORATORY INFORMATION
Name: MCAS Cherry Point /Pace Analytical
Certification Number 201137706
to analyzed• 6/23/2015
Laboratory
� p
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg1L
Nitrite (NO2) as N 00615
mg1L
Cbliform: MIT Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0,3'
mg/L
Coliform: MFTotal 31504/100ml-
Phosphorus: Total as P 00665mg/L
(Note: UsaMPNMOW 10ft* rtubiA5-P*S)
Orthophosphate 70507mg/L
Dissolved Solids: Total 70300 .152 _
mg/L
AI - Aluminum 01105l,mg/L
pH (Lab) 00403 5.5 ^units
Ba - Barium 01007
_µg1L
TOC 00680rng/L
Ca- Calcium 00916mg/L
Chloride 00940 5
Cd - Cadmium: Total 01027
µg/L
_mg/L
Arsenic 01002µg/L
Chromium: Total 01034µg1L
Grease and Oils 00552
mg/L
Cy - Copper 01042mg/L
Phenol 32730
µg/L
Fe - Iron 01045µg1L
Sulfate D0945mg/L
Hg - Mercury 71goo _I1g/L
Specific Conductance 00095
PMhos
K - Potassium 00937
mg./L
Total Ammonia 00610 <1.0
TOW)
mg/L
Mg - Magnesium 00927mg/L
Mn - Manganese 01055µg/L
(Amnwda N&Ww, NNj as N; Amnw;;Ndmg. n
TKN as N 00625mg/L
NI - Nickel 01067
µg/L
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCS:l,
Patricia T. Davis - Utility Systems O erator
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev, 212010
Pb - Lead 01051 µg/L
Zn - Zinc 01092�img/L
Other (Specify Compounds and Concentration Units:
ORGANICS (by GC, GCIMS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) ❑ No (0)
Method#
Method#
Method#
Method#
Effluent Total VOCs:
VOC Removal%
Signature of Permittee (or Authorized Agent) (Date)

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Please Print Cleady or Type
Facility Name: MCAS Cherry Point
Permit Name (if different):
Facility Address: MCAS Cherry Point. NC 285334=
County: Craven
act Person: Patricia T. Davis Telephone #: - 2524664599
Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled:
IPLING INFORMATION
L ID NUMBER (From Permit): MW-5
Depth 13 ft,
h to Water Level 82546: 6.5 ft. below measuring point
suring Point is 3 ft. above land surface
ne of water pumpedlbailed before sampling: ____ 5 Gal.
for metals were
YES
�n-Discharge UIC
DES WQ0001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
Lagoon [] Remediation: Infiltration Gallery
Spray Field Remediation:
Rotary Distributor Land Application of Sludge
El Water Source Heat Pump ❑ Other.
Date Sample Collected: 6/22/2015
Well Diameter. 2
Screened Interval: 3 ft. to 13 ft.
Relative M.P. Elevation: 12 !e
NO and field
FIELD ANALYSIS: DRY at
pH 00400 5,8 . units Temp 00010: 27 °C time of
Spec Cond, 00094: 496 pMhos sampling,
Odor00085: None check
Appearance; Clear
30RATORY INFORMATION
I al zed• 6/22/2015 Laboratory Name: WAS Cherry Point /Pace Analytical Certification Number 201137706
e samp a an y
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg1L
Nitrite (NO2) as N 00615mgIL
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.1
m91L
Coliforrt: MF Total 31504
/100mL
Phosphorus: Total as P 00665 _
mg/L
mg/L
(Nora: us® MPN menrod roc 1*0* aroea "InPlHs)
Orthophosphate 70507
Dissolved Solids: Total 70300 208
mg/L
Al -Aluminum 01105mg/L
pH (Lab) 00403 5.8 _
units
Be - Barium 01007
µg/L
mg/L
TOC 00680
mg/L
Ca - Calcium 00916
_
Chloride 00940 18
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002µ91L
Chromium: Total01034a
pg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
µg/L
Fe - Iron 01045µg1L
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L
malt.
Specific Conductance 00095 �_
µMhos
K - Potassium 00937
Total Ammonia 00610 <0.1
TOW)
mg/L
Mg - Magnesium 00927�_m91L
Mn - Manganese 01055
Ng/L
(Anwnrxra N"en: NH3 as NS Amnorua N&O"n.
Ni- Nickel 01067µg/L
TKN as N 00525mg/L
For Remediatlon Systems Only (Attach Lab Reports):
Influent Total VOCs:
Patricia T.. Davis - UtilitV 5 stems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev, 2/2010
Pb - Lead 01051 µ9/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
Fak
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LA13 REPORT.)
Lab Report Attached? ❑ Yes(1) ® No (0)
Method#
Method#
Method#
Method#.
Effluent Total VOCs:o,
VOC Removal%
711312015
Signature of permittee (or Authorized Agent) (Date)

UNITED STATES MARINE CORPS,
MARINE CORPS AIR STATION
POSTAL SERVICE CENTER 5003 .
CHERRY POINT. NORTH CAROLINA 28533-0003
IN REPLY REFER TO,
5090/07109
LN
July 13, 2015
North Carolina Department of Environment
and Natural Resources
Division of Water Resources
Attn: Information Processing Center
1617 Mail Service Center'
Raleigh, NC 27699-1617
Subj: TRIENNIAL GROUNDWATER MONITORING
In accordance with the groundwater monitoring and reporting
requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for
Land Application of Wastewater Residuals, enclosed are the
original and one copy of the GW-59-A report and the four GW-59
reports (one each for monitoring wells.1, 2, 3, and 5) for the
triennial reporting for June 2015.
Should you have any questions, please contact Mr. Timothy
Lawrence of the Environmental Affairs Department at your earliest
convenience at (252).466-2754.
Sincerely,
G. V. Valffairs
EnvironmOfficer
By direction of the
Commanding Officer
Enclosure: (1) GW-59-A
(2)
GW-59
for
MW-1
(3)
GW-59
for
MW-2
(4)
GW-59
for
MW-3-
(5)
GW-59
for
MW-5

GW-59A COMPLIANCE REPORT FORM Permit # WQ0001489
(Subunit one each monitoring period ikth GIV--59 forms)
Enter date monitoring results were due. 7( /31/151 Will this monitoring report (GW-59 and GW-59A) be submitted after : YES NO
1 the established due date?
2 Was any required information missing on the GVV-59 report forms? YES NO .
X
IF the answer to question I or 2 is "YES", list in the space provided below the well idenlification number(s) and explain the problems
encountered in obtaining the required information,
3 1 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing I YES 1 NO
identification plate, area overgrown, etc.)? Irthe aum veris "Yes', contact the Regional QQiccejorguidance, II
h' Are any monitored constituents equal to or above the established standards? I YES I NO I
'X
If the answer to question 4 is NO", skip to section S.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the
space provided below,
For the constituents identified in question 4 above, have standards been exceeded previously for the some constituents) YES I NO
5 in the same well(s) in the last two years? I X
If the answer to question 5 is "NO", skip to section 8,
ir the answer to question 5 is "YES", list in the space provided below, each well with constituents) exceeding standards,, concentration(s)
reported, and sample collection date for each occurrence (for the last two years).
6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO
if the answer Is "YES", a groundwater quality problem may he occurring. CONTACT THE REGIONAL OFFICE 11MMEDIATELY
FOR GUIDANCE. If the answer is "NO", monitoring wells may, be Improperly located; contact the Regional Office.
Is the permittee implementing previously approved actions required by the Division involving this groundwater quality YES NO'
7 problem?
If the answer to question 7 is "YES", describe those actions in the space provided below,
If the answer to question 7 is "NO", contact the Regional Office within 90 dour, an evaluation may be required to determine the
impact the waste 41sposal stem Is vin at the review gad comnlianceboundaries ur un in ibis racility, Failure to do so may
suhiect the nermiltee to a Notice orViolation. fines. apolor penalties
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with
8
G%V 59 forms for required wells to the address provided at the top of the current GIV-59 form.
I+htxeby�ac��� taedkaoedehthebveioago� mpaoitance,
s
trepan GW-39A) is trite rttu! compkte to the bestofmy#knowledge,
-� 4 y� �t
Patricia T. Davis, Utility Systems Operator Supervisor
Signature of Permittee (or Authorized Agent) Date 711312015

ROUNDWATER (QUALITY MONITORING:
OMPLIANCE REPORT FORM
Please Print Cleady or
Name: _MCAS Cherry Point
Name (if different):
Address: MCAS Cherry Point, NC 28533-0006
SUBMIT FORM ON YELLOW PAPER ONLY
County: Craven
act Person: Patricia T. Davis Telephone IP 2524664599
LocafiontSite Name:Site 21, MCAS Cherryr Point - No.of Wells to be Sampled:
pre
L ID NUMBER (From Permit): MW-1
Depth 26.65 ft.
h to Water Level 82546: — 3.5 fL Wow measuring pant
Turing Point is 1.33 It above land surface
ne of water pumpedlbailed before sampling: ^ 5 Gal.
for metals were
v-Discharge UIC
DES W00001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
Lagoon ❑ Remedlation: infiltration Gallery
Spray Field Remediation:
Rotary Distributor 0 Land Application of Sludge
El Water Source Heat Pump ❑ Other:
Date Sample Collected: 6/23/2015
Well Diameter, 2
Screened Interval: -0.17 ft. to -15.2 k
Relative M.P. Elevation: 10.78
NO and
NO
FIELD ANALYSIS: PC DRY'at
pH 00400 6.5 units Temp 00l}10: 24 time of
Spec. Cond. 00094: 119 NMhos samplinc
Odor 00085: None check
Appearance: Clear here:
30RATORY INFORMATION
lanal e zed' 6/23/2015 Laboratory Name: MCAS Cherry Point I Pace Analytical Certification Number. 201` 137706
e samp y
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
mg/L
COD 00335n'►9/L
Nitrite ( as N 00615
)
Colifomt• MF Fecal 31616_<1
/100ml-
Nitrate (NO3) as N 00620 <0,1
mg/L
mg/L
Colifonn: MF Total 31504
/100ml-
Phosphorus: Total as P 00665
Orthophosphate 70507
mg/l
(Note: Use MPN medvd for f4* bxW samples)
mg/L
AI - Aluminum 01105
mg/L
Dissolved Solids: Total 70300 44
Ba - Barium 01007 _
u9/L
PH (Lab) 00403 6.5units
TOC 00680
mg/L
_
Ca - Calcium 00916
mg/L
Chloride 00940 12
mg/L
Cd - Cadmium: Total 01027
tig/L
_
Arsenic 01002µg/L
Chromium, Total 01034t19/L
Grease and Oils 00552 _
mg/L
Cy - Copper 01042mg/L
Pheno1327W
NglL
Fe- Iron 01045µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900R9/L
mg/L
Specific Conductance 00095
NMhos
K - Potassium 00937�
Mg - Magnesium 00927
mg/l.
Total Ammonia 00610 <1.0
(Amrtaroa Nit"Itn: NH. as N, Amimwda Nioopan. rout
mg/L
Mn - Manganese 01055+_
Ng/L
TKN as N 00625m9/L
NI - Nickel 01067_�_N9/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092mglL
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test"and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) ❑ No (0)
Method#
Method#
Method#
Method#
For Remediation Systems Only (Af3ach Lab Reports):
Influent Total VO- Effluent Total VOCs:_, VOC Removal%
7/13/2015
Patricia T. Davis - Utilft S stems Operator Perrnittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev, 212010

SUBMIT FORM ON YELLOW PAPER ONLY
DUNDWATER QUALITY MONITORING: oirL
alr>I"vt=eWA7CK�iNAG1TNnrvnnu�i�asnr�ww..,
MPLIANCE REPORT FORM RAt3FNC'27899=i8iT�'H t?FION�ts1s)733-322
LITY INFORMATION Please Print Clearly or Type EMIT Expiration Date: 7l3112 1
ty Name: MCAS Chegy Point Non -Discharge UIC
pit Name (if different): NPDES W00001489 Other
ty Address; MCAS CherryPoint, NC 28533.0006 TYPE OF PERMITTED OPERATION BEING MONITORED
County: Craven ❑ Lagoon ❑ Remediation: Infiltration Gallery
r izwg 0 Spray Ffeid ❑ Remediation:
Rotary Distributor Land Application of Sludge
act Person: Patricia T- Davis Telephone #: [phone] ❑ ❑
Location/Site Site 21. MCAS Cherry Point No,of Wells to be Sampled: 1 ❑ Water Source Heat Pump ❑ other.
LL ID NUMBER (From Permit): MW-2 _
Date Sample Collected: 6/23/2015
FIELD ANALYSIS: 0C,
00400 5.8 units Temp 00010: 25
DRY at
time
I Npth 26.58 ft
tlr to Water Level 82546: 9.5 ft below measuring print
Well Diameter. 2
Screened Interval: -1.03 ft. to -11
ft.
pH
Spec. Cond. 00094: 740 NMI
of,
sampinnt
isuring Pant is 1.28 fL above land surface
Relative M.P. Elevation: 14.8 -�_
Odor ran None
Appearance: Clear
check
here: ❑
Ime of water pumpedlbailed before sampling:.
5 Gal,
,pies for metals were collected unfiltered
YES ❑
NO and field addified ❑ YES NO
30RATORY INFORMATION
e sample analyied: 6/23/2015
Laboratory Name. MCAS Cherry Point! Pace Analytical
Certification Number. 201137706
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
mg/L
Pb -Lead 01051
COD 00335m9/L
Nitrite (NO2) as N 00615
Nitrate (NO3) as N 00620 <0.1 —mg/L
�rl►9n-
Zn - Zinc 01092mg/L
Coliform: MF Fecal 31616 <1 _1100ml
Coliforma MF Total 31504
1100mL
Phosphorus, Total as P 00865mg/L
Other (Specify Compounds and Concentration Units):
(Note. UseMPNRMOMfwhipNYWla 6MMIas)
Orthophosphate 70507��m9/L
Dissolved Solids: Total 70300 152
mglL
Al - Aluminum 01105_
mg/L
PH (Lab) 00403 5.8
units
Be - Barium 01007N9lL
TOC 00680_mg/L
Ca - Calcium 00916mg/t.
Chloride 00940 8.9_mg/L
Cd -Cadmium: Total 01027^�
µg/L
Arsenic 01002li9/L
Chromium: Total 01034p9/L
Cy -Copper 01042��mg/L
ORGANICS (by GC, GClMS, HPLC}
Grease and Oils 00552,_mg/L
Fe - Iron 01045
pglL
(Specify test and method #. ATTACH LAB REPORT.)
Phenol 32730pg/L
mg/L
Hg - Mercury 71900 _u9n-
Lab Report Attached? ❑ Yhod# ❑ No (0)
Sulfate 00945
Specific Conductance 00095
a
K - Potassium 00937
mglL
, Melhodrl
Method#
_^NMhos
Total Ammonia 00610 1.2 _mg/L
Mg - Magnesium 00927mg/L
,
,Method# .
(ArtmcrM ftoa-; NN3 u �+ N; Aor" Naoc@+. Tyr
Mn - Manganese 01055 _ _
Ng/L
Method#:
TKN as N 00625
mg/L
NI - Nickel 01057pg/L
,
For Re -mediation Systems Only (Attach Lab Reports):' Influent Total VOCs: Effluent Total VOCs: _
VOC Removal•%
7/13/2015
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev.212010

UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
Name: MCAS
Name (if different):
Address: MCAS
Point
SUBMIT FORM ON YELLOW PAPER ONLY
or
County: Craven
act Person: Patricia T. Davis Telephone #: [phone]
LocationlSile Name: Site 21 MCAS Cherry Point No.of Wells to be Sampled:
n-Discharge UIC
DES W00001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedlation: infiltration Gallery
❑ Spray Field 0 Remedlation:
❑ Rotary Distributor 0 Land Application of Sludge
❑ Water Source Heat Pump ❑ Other.
rrurvu mrvnwcn .�+••
L ID NUMBER (From Permit): MW-3
Date Sample Cotlected: 6/23/2015
FIELD ANALYSIS:
Temp 00010; 25
o C
DRY at
25 58 R
Well Diameter. 2
pH 0040o 5.5 units
time of.
Depth
i to Water Level 82546, 0 ft. below measuring point
Screened interval: -11.7 ft. to -21.7 R
Spea Cond. 00094, 282 pMhos
sampling
check
;udng Point is 1,46 fL above land surface
Relative M.P. Elevation: 3.1
Odor 00085: None
Appearance_ Turbid
here: i
no of water pumped/bailed before sampling: 5 Gal
YES ❑ NO
Aes for metals were collected unfiltered � YE5
NO and field addified Q
ORATORY INFORMATION
samp le analyzed• 6/23/2015
Laboratory Name: MCAS Cherry Point I Pace Analytical
Certification Number. 201137706
�
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615mg/L
Coliform; MF Fecal 31616 <1
1100mL
Nitrate (NO3) as N 00620 0,3mg1L
.
Coliform: MF Total 31504
/100ml-
Phosphorus: Total as P 00665_
mg/L
(Note use MPNmeundr«IMplrra.mas=pw)
Orthophosphate 70507mg/L
Dissolved Solids: Total 70300 .152
mg/L
AI - Aluminum 01105!_mg/L
pH (Lab) ONO3 5.5
units
Ba - Barium 01007
µg1L
TOC 00680mg/L
Ca- Calcium 00916m9/L
Chloride 00940 5
mg/L
Cd - Cadmium: Total 01027
pg/L
Arsenic 01002�^µg/L
Chromium: Total 01034µglL
Grease and Oils 00552
mg/L
Cy - Copper 01042mg/L
Phenol 32730
µg/L
Fe - Iron •01045µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900µg/L
Specific Conductance 00095µMhos
K - Potassium 00937mg/L
Total Ammonia 00610 <1,0
mg/L
Mg • Magnesium 00927mg/L
(Am rwoc" Nitropso: NN2 as N; AmrmZ N&OW. Toted
Mn - Manganese 01055
TKN as N 00625mg/L
NI - Nickel 01067
µglL
Pb - Lead 0105.1 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC1MS, HPLC)
(Specify test and method X ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) ❑ No (0)
Method#
Method#
Method#
Method#
:..
I .:en G'ltal !e,!;le !iCi! c(: '/ F ;o:.!cCre lac' L'r!iC!.'h^ r :ic^ cuali:::edit !hs re c : a !roe i wfra:e e❑t cot ,;c!0-,1r1'' !ha! the la5ora'ery a u ;ac as OdUCLd oc nc ap; w cc cne!!:o n! an: !rs s tty
o: c cena;ed ma;iora!ary !am ..r:c that !hc c am s ,n cant., en7!ies!or su[s,:u"1, !rse in!a:matior mch id:nq 9,,o , osSjbt!d/ o!i.aes and ent.for kr.o.�ia� •�{-ltcns
/ r
Patricia T. Davis - Utiry Systems O erator
Permitted (or Authorized Agent) Name and Title- Please print or type Signature of Permittee (or Authorized Agent) (Date)
)
GW-59 Rev, 212010

ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Name: MCAS Cherry Point
Name (if different):
Address: MCAS Cherry Point, NC 28533-M
County:
SUBMIT FORM ON YELLOW PAPER ONLY
or Type
act Person: Patricia T. Davis Telephone #: 252-4W,45W
Location/Site Name: Site 21 MCAS Cherry Point No -of Wells to be Sampled: 1
rt-Discharge UIC
DES WQ0001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
0 Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation: _
Rotary Distributor Land Application of Sludge
❑ Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION
MW-5
Date Sample Collected: 6/22/2015
FIELD ANALYSIS:
WAS
DRY at
WELL ID NUMBER (From Permit):
Diameter. 2
pH 00400 5.8 units Temp 00010: 27
time of
Well Depth 13 ft.Well
6.5 It. below measuring point
Screened Interval: 3 IL to 13 _ - ft.
Spec. Cond., 00094:. 496 µMhos
sampling,
Depth to Water Level 82646:
Relative M.P. Elevation: 12
Odort}0085: None
check
Measuring Point is 3 fL above land surface
���
Appearance; Clear
here:
Volume of water pumped/balled before sampling: 5 Gal.
.
samples for metals were collected unfiltered YES
NO and field acidified YES NO
LABORATORY INFORMATION
Name: MCAS Cherry Point i Pace Analytical
Certification Number. 201 137706
M�f m In anal zed• 6/22/2015
Laboratory
e sa p Y
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615+_mg/L
Coliform: MF Fecal 31616 <1
/100ml-
Nitrate (NO3) as N W620 <0.1
mglL
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665mg/L
mg/L
(Note: We MPH method (er hV0y urwd $=*')
Orthophosphate 70507
Dissolved Solids: Total 70300 208�mg/L
Al -Aluminum 011051,mg1L
pH (Lab) 00403 5.8
Ba - Barium 01007
pg/L
_units
TOC 00680
mg1L
Ca - Calcium 00916
mg/L
ipg/L
Chloride 00940 18
mg1L
Cd - Cadmium: Total 01027
Arsenic 01002pg1L
Chromium: Total 01034
pg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042mg/L
Phenol 32730-
pg1L
Fe- Iron 01045pg/L
Sulfate 00945mg/L
Hg - Mercury 71900
Pg/L
Specific Conductance00095
K - Potassium 00937µMhos �
— mg/L
Total Ammonia 00610 <0.1mg/L
W Toms)
Mg - Magnesium 00927rng/L
Mn - Manganese 0105.5
µg/L
(Ammonia Nitrogen: NH3 of Nl+AMM Nuo��t.
TKN as N 00625mg/L
N1- Nickel 01067µg/L
For Remediatlon Systems Only (Attach Lab Reports):
Influent Total VOCS:
Pb - Lead 01051 pg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) ❑ No (0)
Method#
Method#
Method#
Method#
Effluent Total VOCs:
VOC Removal%
Patricia T Davis - Utility Systems Operator - 5�
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev.2/2010

UNITED STATES MARINE CORPS
MARINE CORPS AIR STATION
POSTAL SERVICE CENTER 1100.7
CHERRY POINT, NORTH CAROLINA 2ES33-OM
IN REPLY REFER TO;
5090/07109
LN
November 16, 2015
North Carolina Department of Environment
and Natural Resources
Division of Water Quality
Information Processing Center
1617 Mail Service Center
Raleigh, NC 27699-1617
Subj: TRIENNIAL GROUNDWATER MONITORING
In accordance with the groundwater monitoring and reporting
requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for
Land Application of Wastewater Residuals, enclosed are the original
and one copy of the GW-59-A report and the four GW-59 reports (one
each for monitoring wells 1, 2, 3, and 5) for the triennial
reporting for October 2015.
Should you have any questions, please contact Mr. Timothy
Lawrence, PE of the Environmental Affairs Department at your
earliest convenience at [phone].
Sincerely,
G. i0
Envir4'Qntm1 Affairs Officer
By direcof the
Commanding Officer
Enclosure: (1)
GW-59-A
(2)
GW-59 for MW-1
(3)
GW-59 for MW-2
(4)
GW-59 for MW-3
(5)
GW-59 for MW-5
(6)
Lab Report

GW-59A COMPLIANCE REPORT FORM Permit # WQ0001489
(Submit one each monitoring period u th Gli -59 forms)
Enter date monitoring results were due. (11130115 Will this monitoring report (GW-59 and GW-59A) be submitted after
YES
NO
I
the established due date?
X
2
Was any required information missing on the GW-59 report forms?
YES
NO
X
IF the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems
encountered in obtaining the required information.
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
3
identification plate, area overgrown, etc.)? If the annrer is "Yes", contact the Regional Oflicejorguidance.
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
X
If the answer to question 4 is "NO", skip to section 8
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentmtion(s) exceeding standards in the
space provided below-
WV-2 TOTAL AMMONIA (NI13) 2.4 mg/L
NlW-5 TOTAL AhINIONIA (NI13) 2.1 mg/L
For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s)
YES
NO
5
in the same well(%) in the last two years?
X
If the answer to question 5 is "NO", skip to section 8
If The answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentrations)
reported, and sample collection date for each occurrence (for the last two years).
MIV-2: Oct. 2013 N113 3.0, Feb. 2014 N113 3.0, Oct. 2014 N113 1.7, Feb. 2015 N113 1.7
MW-5: Feb. 2014 N113 3Z, June 2014 NII3 2.7, Oct. 2014 NI13 3.0. Feb. 2015 NI13 2.7
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
X
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY
FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office.
Is the permittee implementing previously approved actions required by the Division involving this groundwater quality
YES
NO
7
problem?
X
If the answer to question 7 is "YES", describe those actions in the space provided below
If the answer to question 7 is "NO", contact the Regional Mee within 90 days: an evaluation may be rrouired to determine the
impact the wssle disnosal system Is having at the review and compliance boundaries surrounding this facility. Failure to do so may
subitet the nermittee to a Notice or Violation, andlor twinillic&
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with
S
GW-59 forms for required wells to the address provided at the lop of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance
Report GW-59A) is true and complete to the lest of my knowledge.
Patricia T. Davis, Utility Systems Operator Supervisor
t �"�
Signature of Permittee (or Authorized Agent) Dale 11/1612015

(GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Name MCAS
Name (if different){
Address. MCAS
SUBMIT FORM ON YELLOW PAPER ONLY
Please Print Clearly or Type
Pout
Point, NC 28533-0006
County- Craven
act Person: Patricia T. Davis Telephone * 2524564599
Location/Site Name: Site 21, MCAS Cherry Point No of Wells to be Sampled: 1
j"M perm
PERMIT Number: expiration uate: na ircv i U
Non -Discharge U1C
NPDES W00001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedlation: infiltration Gallery
Spray Field F1 Remediation:
Rotary Distributor Ej Land Application of Sludge
Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION
WAS
WELL ID NUMBER (From Permit): MW-1
Date Sample Collected: 10/1912015
FIELD ANALYSIS:
DRY at
Well Depth 26.66 it
Well Diameter. 2
pH ONW 6.1 units Temp olmlo:
21 °C
time of
Depth to Water Level 82546 1 ft. below measuring point
Screened Interval -0 17 It. to -15.2
R Spec. Coral. 00094: 190
uMhos
sampling,
Measuring Pant is 1.33 It. above land surface
Re!attve M P Elevation 10.78
Odor 00065- none
check
Volume of water ptimpedlbaiied before sampling 5 Gal
Appearance clear
here: ❑
Samples for metals were collected unfiltered YES [_,. NO
and field acidified ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/19/2015 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number 201 / 37706
1AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Coliforrm MF Fecal 31616
<1
1100mL
Nitrate (NO3) as N D0620 <0.1
mg/L
Coliform: MF Total 31504
/100ml-
Phosphorus- Total as P 00665
mg/L
(Noe Use MPN method tw hg* hffW sampks)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300
56
mg1l
Al - Aluminum 01105
mg/L
pH (Lab) 00403
6.1
units
Ba - Barium 01007
µg/L
TOC 00580
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
12
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium. Total 01034
µg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
µg1L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
pg/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610
<0.1
mgfL
Mg - Magnesium 00927
mg/L
{Ammma Nerogen, NH3 ae N. Arnmor" Nmogen, TOW
Mn - Manganese 01055
µg/L
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units)
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method A ATTACH LAB REPORT.)
Lab Report Attached? E] Yes(1) ❑ No (0)
VOC 78732 Method# 6200B
Method#
Method#
Method#
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: unuent rota{ vut;s: vuL. Kemovai Al
Patricia T. Davis - Utility Systems Operator 11/6/2015
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev 2/2010

SUBMIT FORM ON YELLOW PAPER ONLY
_whi"VENt Of IRONI AWff i NATURAL RE3OUftC i3
GROUNDWATER QUALITY MONITORING: WSTONi OF WATER QUALI Y-RWott MT11O 1 PROCE040 t
1617 CENTER
COMPLIANCE REPORT FORM RAMC li SERVICE 1617
RALDt3H, FIC 27B98-1617 PHONE: (9i917J3-3&t
FACILITY INFORMATION PfeasePrintCleadyo►Type PERMIT Number: Expiration Date:
Facility Name: MCAS Che Point Non -Discharge UIC
Permit Name (if different): NPOES W00001489 Other
Facility Address: MCAS Cherry Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED
County: Craven 0 Lagoon ❑ Remediation: Infiltration Gallery
(Cr,t ltw*) Rot ❑ Spray Field Remediation:
Contact Person: Patricia T. Davis Telephone M 252-4664599 ❑ Rotary Distributor 0 Land Application of Sludge
Well Location/Site Name: Site 21. MCAS Cherry Point No of Wells to be Sampled: 1 ❑ Water Source Heat Pump ❑ other.
than
If WELL
SAMPLING INFORMATION
WAS
WELL ID NUMBER (From Permit): MW-2
Date Sample Collected: 10119/2015
FIELD ANALYSIS:
aC
DRY .
DRY
Well Depth 26.58 ft.
Well Diameter 2
pH 00400 5.85
units Temp D0010: 19
Depth to Water Level 82546 7 ft below measuring point
Screened Interval -1 03 R to -11
ff. Spec. Cond 0- 94
897 µMhos
• „ p,, o
Measuring Point is 1-28 ft. above land surface
Relative M P Elevation 148
Odor D0085
none
Volume of water pumped/bailed before sampling. 5 Gal
Appearance
clear
^ •'
Samples for metals were aalected unfiltered ( } YES
NO and field acidified _ ID YES Lj NO
LABORATORY INFORMATION
Date sample analyzed: 1011912015
Laboratory Name: MCAS Cherry Point / Pace Analytical
Certification
Number. 201 / 37706
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Coliform: MF Fecal 31616
<1
/100mL
Nitrate (NO3) as N 00620 <01
mg/L
Coliform: MF Total 31504
/100mL
Phosphorus- Total as P 00665
mg/L
(Note use WN munod ror hg* eaoo ads)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300
308
mg1L
AI - Aluminum 01105
mglL
pH (Lab) 00403
585
units
Ba - Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
14
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and pits 00552
mg/L
Cy - Copper 01 D42
mg/L
Phenol 32730
µg/L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610
2.4
mg/L
Mg - Magnesium D0927
mg/L
(Ammonia Nitrogen: NFy at N; Ammoru Nitrogen, Tctaq
Mn - Manganese 01055
µg/L
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCS:
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.2/2010
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units)
ORGANICS (by GC. GCIMS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes(1) :j No (0)
VOC 78732 Method# 6200E
Method#
Method#
Method#
Effluent Total VOCs: VOC Removal°%
11/6/2015
Signature of Permittee (or Authorized Agent) (Date)

(GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Name' MCAS Cherry Point
Name (if different):
Address MCAS Cherry Point
SUBMIT FORM ON YELLOW PAPER ONLY
Clearly or
County: Craven
act Person. Patricia T. Davis Telephone #: 252.466AS99
Location/Site Name: Site 21 MCAS Cherry Point No of Wells to be Sampled:
it"
UIC
DES W00001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
[] Lagoon ❑ Remedlatlon: Infiltration Gallery
Spray Field 0 Remediation:
Rotary Distributor Q Land Application of Sludge
Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION
If WELL
WAS
WELL ID NUMBER (From Permit): MW-3
Date Sample Collected: 1011912015
FIELD ANALYSIS:
DRY
Well Depth 25.58 IL
Well Diameter 2
pH 00400 6.1 unis Temp t)0010 20 °C
..
Depth to Water Level e2546 0 fL below measuring point
Screened Intervat: -11.7 ft_ to -21.7 ft.
Spec. Cond. 00094 201 tiMhos
Measuring Point is 146 ft above land surface
Relative M P Elevation. 3.1
Odor 00085 none
.....
Volume of water pumped/bailed before sampling: 5 Gal
Appearance. turbid
"•
Samples for metals were collected unfiltered YES
NO and field acidified YES Q NO
LABORATORY INFORMATION
Date sample analyzed: 10/19/2015
Laboratory Name: MCAS Cherry Point / Pace Analytical
Certification Number. 201 / 37706
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Coliform: MF Fecal 31616
<1
/100ml-
Nitrate (NO3) as N 00620 2.5
mg/L
Coliform: MF Total 31504
/100ml-
Phosphorus: Total as P OW65
mg/L
(Nala- Use MPN merod for frpth Qsbd "ff4fts)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300
144
mg/L
AI - Aluminum 01105
mg/L
pH (Lab) 00403
6.1
units
Ba - Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
6.9
mg/L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and Oils 00552
~�mg/L
Cy - Copper 01042
mg/L
Phenol 32730
µg/L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
µglL
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610
<1 0
mg1L
Mg - Magnesium 00927
rng/L
(Anenana ta"an. NH3 as N. Anno" N*Wen. TOUR
Mn - Manganese 01055
µg/L
TKN as N 00625
mg/L
Ni - Nickel 01057
µg/L
Pb - Lead 01051 µg1L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units)?
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? Yes(1) ❑ No (0)
VOC 78732 Method# 62008
Method#
Method#
Method#
For Remediadon Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total vuus: vu%. memvvarn
a
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev.212010

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
ee
AL R.E,300,RCIES
D[VtSO OF WATER", �� TIONPftOCESSINGUNIT
COMPLIANCE REPORT FORM
a
1617MAIL SE"CECENTER
RALEIGK FCC 2709-1617 PHONE: [phone]
FACILITY INFORMATION
Please Pruit Clearly or Type
PERMIT Number: Explration Date: 7/31 1
Facility Name: MCAS Cherry Point
Non -Discharge UIC
Permit Name (if different):
NPDES W00001489 Other
Facility Address: MCAS Cherry Point, NC 5533-0006
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑Remediation: Infiltration Gallery
��„
County:
Craven
❑ Spray Field ❑ Remediation:
Contact Person: Patncia T. Davis
Telephone M 252-466-4599
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Site 21. MCAS Cherry Point
No of Wells to be Sampled:
1 Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (From Permit): MW-5
Date Sample Collected: 10119/2015 FIELD ANALYSIS:
WAS
DRY
Well Depth 13 it
Well Diameter 2
pH 00400 6.2 units Temp 00010: 24 "C
. t
tl en• eT
Depth to Water Level 82546 6.5 ft. below measuring point
Screened Interval 3
it to 13 ft. Spec. Cond. 00094 544 µMhos
Measuring Point is 3 ft above land surface
Relative M P Elevation: 12
Odor 00085 none
<. ...
Volume of water pumped/bailed before sampling
5 Gal
Appearance clear
^- ❑
Samoles for metals were collected unfiltered
YES NO and field acidifiedLj YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/19/2015
Laboratory Name: MCAS Cherry Point) Pace Analytical Certification Number 201137706
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 µg/L
Coliform: MF Fecal 31616 <1
/100ml-
Nitrate (NO3) as N 00620
<0.1 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00565
mglL
thofe: Use MPN method rw npnyft,fHd wngesl
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total 70300 192
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 6.2
units
Ba - Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 12
mg/L
Cd - Cadmium Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L ORGANICS (by GC, GC/MS, HPLC)
Phenol 32730
µg/L
Fe - Iron 01045
µg/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
µg/L Lab Report Attached? Yes(1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732 Method# 6200E
Total Ammonia 00610 2.1
mgfL
Mg - Magnesium 00927
mg/L Method#
(Amrwroe N&opn; NH3as N;Amfom N WwL Te;wl
Mn - Manganese 01055
µg/L , Method#
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L Method#
For Remediation Systems Only (Attach Lab Reports): influent Total VOCs: Effluent Total VOCs: you Removai A
ol
Patricia T. Davis - Utility Systems Operator 11/6/2015
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev 2/2010

aceAnaljdical s
aww.psceiabsoom
November 10, 2015
Mr. Stephen Reavis
MCAS Cherry Point
Facilities Maintenance Depart
PSC Box 8006, LCU
Cherry Point, NC 28533
RE: Project: Sampling 10/19/15
Pace Project No.: 92272649
Dear Mr. Reavis:
Pace AnsWal Services, Inc.
9800 Kincey Ave Suite 100
Huntersvrtle. NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Owe, yY1. � i aru
Angela Baioni
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page 1 of 40

aceAnalyh'cat'
Project: Sampling 10/19/15
Pace Project No.: 92272649
Pennsylvania Certification IDs
Georgia Certification #: C040
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
L-A-B DOD-ELAP Accreditation #: L2417
Alabama Certification #: 41590
Arizona Certification #: AZO734
Arkansas Certification
California Certification #: 04222CA
Colorado Certification
Connecticut Certification #: PH-0694
Delaware Certification
Florida/TNI Certification #: E87683
Georgia Certification #: C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification #: 391
KansasfTNI Certification #: E-10358
Kentucky Certification #: 90133
Louisiana DHH/TNI Certification #: LA140008
Louisiana DECrrNI Certification #: 4086
Maine Certification #: PA00091
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification
Missouri Certification #: 235
CERTIFICATIONS
Montana Certification * Cert 0062
Nebraska Certification #: NE-05-29-14
Nevada Certification #: PA014572015-1
New HampshirefrNi Certification #: 2976
New Jersey/TNI Certification M PA 051
New Mexico Certification #: PA01457
New York/TNI Certification #: 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
Oregon/TNI Certification #: PA200002
Pennsylvania/TNI Certification #: 65-00282
Puerto Rico Certification #: PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification #: TN2867
Texas/TNI Certification #d T104704188-14-8
Utah/TNI Certification #: PA014572015.5
USDA Soil Permit #: P330.14-00213
Vermont Dept. of Health: ID# VT 0282
Virgin Island/PADEP Certification
VrrginialVELAP Certification #: 460198
Washington Certification #: C868
West Virginia DEP Certification #: 143
West Virginia DHHR Certification #: 99MC
Wisconsin Certification
Wyoming Certification #: 8TMS-L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Nebraska Certification: NE-OS-28-14
Alabama Certification #: 41320
Nevada Certification: FL NELAC Reciprocity
Connecticut Certification* PH-0216
New Hampshire Certification #: 2958
Delaware Certification: FL NELAC; Reciprocity
New York Certification * 11608
Florida Certification #: E83079
North Carolina Environmental Certificate #: 667
Georgia Certification #: 955
North Carolina Certification #: 12710
Guam Certification: FL NELAC Reciprocity
North Dakota Certification # R-216
Hawaii Certification: FL NELAC Reciprocity
Oklahoma Certification #: D9947
Illinois Certification #: 200068
Pennsylvania Certification #: 68-00547
Indiana Certification: FL NELAC Reciprocity
Puerto Rico Certification #: FL01264
Kansas Certification #: E-10383
South Carolina Certification: #96042001
Kentucky Certification #: 90050
Tennessee Certification #: TN02974
Louisiana Certification #: FL NELAC Reciprocity
Texas Certification: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
US Virgin Islands Certification: FL NELAC Reciprocity
Maryland Certification: #346
Virginia Environmental Certification #- 460165
Michigan Certification #: 9911
West Mrginla Certification #: 9962C
Mississippi Certification: FL NELAC Reciprocity
Wisconsin Certification #: 399079670
Missouri Certification #: 236
Wyoming (EPA Region 8): FL NELAC Reciprocity
Montana Certification * Cert 0074
Charlotte Certification iDs
9800 Kincey Ave. Ste 100, Huntersvilie, NC 28078 Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #, 84
North Carolina Field Services Certification M 5342 West Virginia Certification M 357
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Asheville Certification IDs
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Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification M 37712 VirgiNaNELAP Certification * 460222
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Sampling 10/19/15
Paoe Project No.: 92272649
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Sample: MW 01
Parameters
Lab ID: 92272649003 Collected: 101191151300
Results Units Report Limit OF
Received. 10/21/15 08 00 Matrix: Water
Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Benzene
NO
ug/L
0.50
1
10125115 03:49 71-43-2
Bromobenzene
NO
ug/L
0.50
1
10/25/15 03:49 108-86-1
Bromochtoromethane
NO
ug/L
0.50
1
10/25/15 03:49 74-97-5
Bromodichloromethane
NO
ug/L
0.50
1
10/25W15 03:49 75-27-4
Bromoform
NO
ug/L
0.50
1
10125/15 03:49 75-25-2
Bromomethane
ND
ug/L
5 0
1
10/26/15 03419 74-83-9
n-Butylbenzene
ND
ug/L
0,50
1
10/25/15 03:49 104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
10/25/15 03 49 135-98-8
tert-Butylbenzene
ND
ug/L
0.50
1
10/25/15 03 49 98-06-6
Carbon tetrachloride
NO
ug/L
0.50
1
10/25/15 03 49 56-23-5
Chlorobenzene
NO
ug/L
0.50
1
10/25115 03 49 108-90-7
Chloroethane
NO
ug/L
1.0
1
10/25/15 0149 75.00-3
Chloroform
6.4
ug/L
0.50
1
10/25/15 03:49 67-66-3
Chloromethane
NO
ug/L
1.0
1
10/25/15 03,49 74-87.3
2-Chlorotoluene
NO
ug/L
0.50
1
10125115 0349 95-49-8
4-Chlorotoluene
NO
ug/L
0.50
1
10/25115 03:49 106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
1
10/25/15 03:49 96-12-8
Dibromochloro methane
NO
ug/L
0.50
1
10/25/15 03:49 124-48-1
1,2-Dibromoethane (EOB)
NO
ugfL
0.50
1
10/25/15 03:49 106-93-4
Dibromomethane
NO
ug/L
0,50
1
1012511603:49 74-95-3
1,2-Dichlombenzene
NO
ug/L
0.50
1
10125115 03:49 95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
10/25115 03:49 541-73.1
1,4-Dichlorobenzene
NO
ug/L
0.50
1
10125/1503:49 106-46-7
Dichlorodifluoromethane
ND
ugIL
0 50
1
10/25/15 03 49 75-71-8
1,1-Dichloroethane
ND
ugfL
0.50
1
10/25/15 03 49 75-34-3
1,2-Dichloroethane
NO
ug/L
0.50
1
10/25/15 03:49 107-06-2
11-Dichloroethene
ND
ug/L
0.50
1
10/25/15 03:49 75.35-4
cis-1,2-Dichloroethene
ND
ug/L
0,50
1
10/25115 03:49 166-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
10/25115 03:49 156-60-5
1,2-Dichloropropane
ND
ugll-
0.50
1
10125/15 03:49 78-87-5
1,3-Oichloropropane
NO
ugfL
0.50
1
10/25/15 03:49 142-28-9
2,2-Dichloropropane
NO
ug1L
0.50
1
10/25/15 03:49 594-20-7
1,1-Dichloropropene
ND
uglL
0.50
1
10/25/15 03:49 563-58.6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
10/25/15 03:49 10061-01.5
trans-1,3-Dichloropropene
ND
ug/L
0.50
1
10125115 03.49 10061-02-6
Dilsopropyl ether
ND
ug/L
0 50
1
10/25115 03*49 108-20-3
Ethylbenzene
NO
ug/L
0.60
1
10/25115 03:49 100.41-4
Hexachloro-1,3-butadiene
NO
ug/L
2.0
1
10/25/15 03:49 87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0 50
1
10/25/15 03:49 98-82-8
Methylene Chloride
ND
ug/L
2.0
1
10/25/15 03:49 75.09-2
Methyl-lert-butyl ether
NO
ug/L
0,50
1
10/25/15 03.49 1634.04-4
Naphthalene
NO
ug/L
2.0
1
10/25/15 03:49 91-20-3
n-Propylbenzene
NO
ugfL
0.50
1
10/25/15 03:49 103-65-1
Styrene
ND
ug/L
0.50
1
10/25/15 03:49 100-42-5
1,1,1,2•Tetrachloroethane
ND
ug/L
0,50
1
10/25/15 03:49 630-20-6
1,1,2.2-Tetrachlaroethane
ND
ug/L
0.50
1
10125/15 03,49 79-34-5
Tetrachloroethene
ND
ug/L
0 50
1
10/25/15 03 49 127.18-4
REPORT OF LABORATORY ANALYSIS
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Dale: 11/10/2015 09-05 AM without the written consent of Pace Analytical Services, Inc. Page 7 of 40

aeeAnalytical
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ANALYTICAL RESULTS
ProjectSampling 10/19115
Pace Project No.: 92272649
Pace Ana"cal Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvrlie. NC 28078
[phone]
Sample: MW 01 Lab ID: 92272649003 Collected: 10/19/15 13.00 Received 101211150800 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichiorobenzene
1,1,1-Trichloroethane
1,1,2-Trichtoroethane
Trichloroethene
Tdchlaro8uoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromotluorobenzene (S)
Toluene-d8 (S)
Analytical Method, SM 6200B
NO
uglL
0.50
1
10/25/15 03:49 108-88.3
ND
ug/L
2.0
1
10/25/15 03:49 87-61-6
ND
ug/L
2.0
1
10/25115 03:49 120-82-1
ND
ug1L
0.50
1
10/25/15 03;49 71-55-6
ND
ug1L
0.50
1
1012SMS 03:49 79-00-5
ND
ug/L
0,50
1
10/2511503,49 79-01-6
ND
ug/L
1.0
1
10/25/15 03 49 75.69-4
ND
ug/L
0,50
1
10/25115 03 49 96-18-4
NO
ug/L
0.50
1
10/25115 03 49 95-63-6
NO
ug1L
0,50
1
10/25/15 0149 108-67.8
ND
ug/L
1.0
1
10/25/15 0149 75-01-4
ND
ug/L
1.0
1
10/25/15 0149 179601-23-1
NO
ug/L
0.50
1
10/25/15 03:49 95-47-6
103
%
70-130
1
10/25/15 03:49 17060-07-0
97
%
70-130
1
10/25/15 03:49 460-DO-4
100
%
70-130
1
10/25115 03:49 2037-26-5
Sample: MW 02 Lab ID: 92272649004 Collected; 10119/1513:00 Received: 10/21/15 08:00 Matrix: Water
Parameters
Results Units Report Limit DF Prepared Analyzed
6200E MSV Analytical Method: SM 6200B
CAS No. Qual
Benzene
NO
ug1L
0.50
1
10/25115 04 06 71-43-2
Bromobenzene
ND
ug/L
0.50
1
10/25/15 04:06 108-86.1
Bromochloromethane
ND
ug/L
0.50
1
10/25/15 04:06 74.97-5
Bromodichloromethane
ND
ug/L
0.50
1
10125/15 04,06 75-27-4
Bromoform
ND
ug/L
0.50
1
10/25/15 04 06 75-25-2
Bromomelhane
ND
ug/L
&0
1
10/25/15 04,06 74-83-9
n-Butylbenzene
NO
ug/L
0.50
1
10/25/15 04:06 104-51-8
sec-Butyibenzene
ND
ug/L
050
1
10/25/15 04:06 135-98.8
tert-Butyibenzene
ND
ug/L
0.60
1
10/26/15 04:06 98.06-6
Carbon tetrachloride
NO
ug/L
0.50
1
10125/15 04 06 56-23-5
Chlorobenzene
NO
ugtL
0.50
1
10/25/15 04 06 108-90-7
Chloroethane
NO
ug/L
1.0
1
10/25/15 04 06 75-00-3
Chloroform
NO
ug/L
0.50
1
10125/15 04,06 67-66-3
Chloromethane
ND
ug/L
1.0
1
10/25/15 04:06 74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
10/25/15 04:06 9549-8
4-Chlorotoluene
ND
ug/L
0.50
1
10/25/15 04:06 106434
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
1
10/25/15 04:06 96-12-8
Dibromochloromethane
NO
ug/L
0.50
1
10/25/15 04�06 12448.1
1,2-Dibromoethane (EDB)
NO
ug1L
0.50
1
10/25/15 04 06 106-934
Dibromomethane
ND
ug/L
0.50
1
10/25/15 04:06 74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
10/25/15 04:06 95-50-1
1,3-Dichiorobenzene
NO
ug/L
0.50
1
10/25/15 04 06 541-73.1
1,4-Dichlorobenzene
ND
ug/L
050
1
10/25/15 04,06 106.46-7
REPORT OF LABORATORY ANALYSIS
This report chat not be reproduced, except in full,
Date. 11/10/2015 09 05 AM without the written consent of Pace Analytical Services, Inc. Page 8 of 40

aceAnalytical
im pec&W&cora
ANALYTICAL RESULTS
Project: Sampling 10119/15
Pace Project No.: 92272649
Pace Analytical Services, Inc.
98001(inceyAve Suite 100
Huntersville NC 20D78
[phone]
Sample: MW 02 Lab ID: 92272649004 Collected: 10/19/15 13:00 Received. 10/21/15 08 00 Matrix Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Quaff
6200E MSV Analytical Method: SM 6200B
Dichlorodi0uoromethane
NO
ug/L
0.50
1
10/25/15 04 06
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
10/25/15 04 06
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
10/25/15 04 06
107-06-2
1,1-Dichloroethane
NO
ug/L
0.50
1
10/25/15 04 06
75-35.4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
10/25/15 04 06
156-59.2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
10/25/15 04,06
156-60-5
1,2-Dichloropropane
NO
ug/L
0.50
1
10/25/15 04 06
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
10/251160406
142-28.9
2,2-Dichloropropane
ND
ug/L
0.50
1
10125115 04 06
594-20.7
1,1-Dichloropropene
NO
ug/L
0.50
1
10/25/15 04 06
553-58-6
cis-1,3-Dichloropropene
NO
ug/L
0.50
1
10/25/15 04 06
10061-01.5
tran5-1,3-Dichloropropene
NO
ug1L
0,50
1
10/25/15 04.06
10061.02-6
Diisopropyl ether
NO
ug1L
0.50
1
10/25/15 04,06
108-20-3
Ethylbenzene
ND
ugJL
0.50
1
10/25/15 04:06
1OD-41.4
Hexachloro-1,3-butadiene
ND
ug1L
2.0
1
10t25/1504:06
87-68-3
isopropylbenzene (Cumene)
ND
ug/L
0.50
1
10/25/15 04:06
98-82-8
Methylene Chloride
NO
ug1L
2,0
1
10t25/15 04:06
75-09-2
Methyl-tert-butyl ether
NO
ug/L
0.50
1
10/25/15 04:06
1634-044
Naphthalene
NO
ug/L
2.0
1
10/25115 04 06
91-20-3
n-Propylbenzene
ND
ugtL
010
1
10/25/15 04 06
103-65.1
Styrene
NO
uglL
0.50
1
10/25/15 04 06
100-42-5
1,1,1,2-Tetrachioroethane
ND
ug/L
0.60
1
10/25/15 04 06
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
10/25/15 04 06
79-34-5
Tetrachtoroethene
NO
ug/L
0.60
1
10t25/15 04 06
127.18-4
Toluene
ND
ugtL
0,50
1
10/25115 04 06
108-88-3
1,2,3-Tdchlorobenzene
ND
ug1L
2.0
1
10/25/15 04:06
87-61-6
1,2,4-Trichtorobenzene
NO
ug/L
2.0
1
10/25/15 04:06
120-82-1
1,1,1-Trichloroethane
NO
ug/L
0.50
1
10/25/15 04:06
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
10/26/15 04:06
79-00.5
Trichloroethene
ND
ug/L
0.50
1
10/25/15 04:06
79-01-6
Trichioro0uoromethane
ND
ug/L
1.0
1
10/25115 04-06
75-69-4
1,2,3-Tdchloropropane
NO
ug/L
0.50
1
10/25/15 04:06
96-18-4
1,2,4-Trimethylbenzene
NO
ug/L
0.50
1
10/25M504:06
95.63-6
1,3,5-Trimelhylbenzene
NO
ug/L
0.50
1
10/25115 04 06
108.67-8
Vinyl chloride
ND
ug/L
1.0
1
10125115 04 06
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
10/25115 04.06
179601-23-1
o-Xylene
NO
ug/L
0.50
1
10/25/15 04:06
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
10/25/15 04.06
17060-07.0
4-Bromonuorobenzene (S)
98
%
70-130
1
10/25/15 04.06
460-00-4
Toluene-d8 (S)
100
%
70-130
1
10/25/15 04:06
2037-26.5
REPORT OF LABORATORY ANALYSIS
This report shah not be reproduced, except in fu',
Date: 11/10/2015 09 05 AM without the written consent of Pace Analytical Services, Inc. Page 9 of 40

aceAnalytJcal e
► *WMcabbs cum
ANALYTICAL RESULTS
Project: Sampling 10/19115
Pace Project No,: 92272649
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW 03 Lab 10: 92272649005 Collected: 10/19/15 14:00 Received: 10/21/15 08 00 Matrix. Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No Qual
62008 MSV Analytical Method; SM 6200B
Benzene
NO
ug/L
0.50
1
10/25/15 04:22
7143-2
Bromobenzene
NO
ug/L
050
1
10/25/15 04:22
108-86-1
Bromochioromethane
NO
ug/L
0.50
1
10/25/15 04:22
74-97-5
Bromodichloromethane
NO
ug/L
0.50
1
10/25/15 04:22
75-274
Bromoform
NO
ug/L
0.50
1
10/25/15 04:22
75-25-2
Bromomethane
ND
ug/L
5.0
1
10/25/15 04:22
74-83-9
n-Butylbenzene
NO
ug/L
0.50
1
10125/15 04:22
104-51-8
sec-Butylbenzene
NO
ug/L
0,50
1
10/25115 04:22
135-98-8
tert-Butylbenzene
NO
ug/L
0.50
1
10/25/16 04,22
98-06-6
Carbon tetrachloride
NO
ug1L
0.50
1
10/25/15 0422
56-23.5
Chlorobenzene
NO
ug/L
0.50
1
10/25115 0422
108.90.7
Chloroethane
NO
ug/L
1.0
1
10/25/15 04.22
75-00-3
Chloroform
NO
ug/L
0.50
1
10125/15 0422
67-66-3
Chloromethane
NO
ug/L
1.0
1
10/25/15 04;22
74-87-3
2-Chiorotoluene
NO
ug/L
0.50
1
10/25/15 04:22
9549.8
4-Chlorotoluene
NO
ug/L
0,50
1
10/25/15 04:22
106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
1
10/25/15 04:22
96-12-8
Oibromochloromethane
NO
ug/L
050
1
10/25/15 04.22
124-48-1
1,2-Dibromoethane (EDB)
NO
ug/L
0.50
1
1012511504:22
106.934
Dibromomethane
NO
ug/L
0.50
1
10/25/15 04:22
74-95-3
1,2-Dichlorobenzene
NO
ug/L
0.50
1
10/25/15 04 22
95.50-1
1,3-Dichlorobenzene
NO
ug/L
0.50
1
10/25115 0422
541-73-1
1,4-Dichlorobenzene
ND
uglL
0.50
1
10/25115 04:22
10646-7
Dichlorodifluoromethane
NO
ug/L
0.50
1
10/25/15 04:22
75-71-8
1,1-Dichloroethane
NO
ug/L
0.50
1
10/25/15 04:22
75-34-3
1,2-Dichloroethene
ND
ug/L
0,60
1
10/25/15 04:22
107.06-2
1,1-Dichloroethene
NO
ug/L
0,50
1
10/25/15 04,22
75-35-4
cis-1,2-Dichloroethene
NO
ug/L
0.50
1
10/25/15 04.22
156-59-2
trans-1,2-Dichloroethene
NO
4L
050
1
10/25/150422
156-60.5
1,2-Dichloropropane
NO
ugiL
0.50
1
10/25115 04:22
78-87-5
1.,3-Dichloropropane
NO
ug/L
0.50
1
10/25/15 04:22
142-28-9
2,2-Dichloropropane
NO
ug/L
0.50
1
10/25115 04:22
594-20-7
1,1-Dichloropropene
NO
ug/L
0.50
1
10/26/15 D4 22
563-58-6
cis.1,3-Dichloropropene
NO
ug/L
0.50
1
10/25115 04 22
10061-01.5
trans-1,3-Dichloropropene
NO
ug/L
0.50
1
10/25/1504:22
10061-02-6
Dilsopropyl ether
NO
ug/L
0.50
1
10/25/15 04:22
108-20-3
Ethylbenzene
NO
ug1L
0.50
1
10/25115 04:22
100-41-4
Hexachtoro-1.3-butadiene
NO
ug/L
2.0
1
10125/15 04:22
87-68-3
Isopropylbenzene (Cumene)
NO
ug/L
0.50
1
10/25/15 04;22
98-82-8
Methylene Chloride
NO
uglL
2,0
1
10/25115 04:22
75-09-2
Methyl•tert-butyl ether
NO
ug/L
0.50
1
10125/15 04:22
1634-04.4
Naphthalene
NO
4L
20
1
10/25/15 04 22
91-20-3
rrPropylbenzene
NO
ug/L
0.50
1
10/25/15 04 22
103-65-1
Styrene
NO
ug/L
0,50
1
10125/15 04.22
100-42-5
1,1,1,2-Tetrachloroethane
NO
ug/L
0.50
1
1012511504:22
630-20-6
1,1,2,2-Tetrachloroethane
NO
ug/L
0.50
1
10125/15 04:22
79-34-5
Tetrachloroethene
NO
ugli.
0.50
1
10/25/15 04:22
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
Date: 11110/2015 09:05 AM without the written consent of Pace Analytical Services,. Inc Page 10 of 40

acmnalytical
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ANALYTICAL RESULTS
Project: Sampling 10119/15
Pace Project No.: 92272649
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 25078
[phone]
Sample: MW 03 Lab ID: 92272649005 Collected: 10119/15 14 00 Received. 10/21/15 08 00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method SM 6200B
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichloro benzene
1,1,11-Trichl o roeth a ne
1,1,2-Tdchloroethane
Trichloroethene
Trichlorotluorometh ane
1,2,3-Trichloropropane
1,2,4-Tdmethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylerle
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
ND
ug/L
0.50
1
10/25/15 0422
108-88-3
ND
ug/L
2.0
1
10/25/15 04:22
87-61.6
NO
ugfL
20
1
10/25/15 04:22
12M2-1
NO
ug/L
0.50
1
10/25/15 04:22
71-55-6
ND
ug/L
0.50
1
10/25/15 0422
79-00-5
ND
ug/L
050
1
10/25/15 04:22
79-01-6
NO
ug/L
10
1
10/25/15 04:22
75-69.4
NO
ug/L
050
1
10/25115 0422
96-18-4
NO
ug/L
0.50
1
10125/15 04:22
95-63.6
ND
4L
0.50
1
10125/15 04:22
108.67.8
NO
ug/L
1.0
1
10125/15 04 22
75-01-4
NO
ug/L
1.0
1
10125115 04 22
179601-23-1
NO
ug/L
0.50
1
10/25/15 0422
95-47.6
102
%
70-130
1
10/25/15 04:22
17060-07-0
99
%
70-130
1
10/25/15 04:22
460.00-4
101
%
70-130
1
10125/15 04:22
2037-26-5
Sample: MW 05 Lab ID: 92272649006 Collected. 10/19/15 14 30 Received 10/21/15 08:00 Matrix: Wafer
Parameters
Results
Units
Report Limit
OF
Prepared Analyzed CAS No. Quaff
6200B MSV
Analytical Method SM 62008
Benzene
NO
ug/L
0 50
1
10/25/15 04 39 71-43-2
Bromobenzene
ND
ug/L
0.50
1
10/25/15 04:39 108-86-1
Bromochioromethane
ND
ug/L
0.50
1
10/25/15 04:39 74-97-5
Bromodichloromethane
NO
ug/L
0.50
1
10/25/15 0419 75-27-4
Bromoform
NO
ug/L
0.50
1
10/25/15 04:39 75-25-2
Bromomethane
NO
ug/L
5.0
1
10/25/15 04 39 74-83-9
n-Butyibenzene
NO
ug/L
0.50
1
1012511504.39 104.51-8
sec-Butylbenzene
NO
ug/L
0.50
1
10125/1504,39 135-98-8
tert-Butylbenzene
NO
ug/L
0.50
1
10/25115 04:39 98-06-6
Carbon tetrachloride
NO
ug/L
0.50
1
10/25/15 04 39 56-23-5
Chlorobenzene
NO
ug1L
0.50
1
10/25/15 04 39 108-90-7
Chloroelhane
NO
ug/L
1.0
1
10125/15 04:39 75-00-3
Chloroform
NO
ug/L
0.50
1
10/25/15 04:39 67-68-3
Chloromethane
ND
ug/L
1.0
1
10/25115 04:39 74-87-3
2-Chlorotoluene
NO
ug/L
0.50
1
10/25115 04:39 95-49-8
4-Chlorotoluene
NO
ug/L
0.50
1
10125/15 04:39 106-43.4
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
1
10/25/1504:39 96-12-8
Dibromochloromethane
ND
ugtL
050
1
10/25/15 04:39 12448.1
1,2-Dibromoethane (EDB)
ND
ug/L
050
1
10125/15 04.39 106.93-4
Dibromomelhane
NO
ug/L
0.50
1
10125/15 04:39 74.95-3
1,2-Dichlorobenzene
NO
ug/L
0.50
1
10/25115 04-39 95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
1012511504:39 641-73-1
1,4-Dichtorobenzene
NO
ug/L
0.50
1
10125/15 04:39 10846-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fu-1,
Date: 11/10/2015 09:05 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 40

aceAnalyh'cal
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ANALYTICAL RESULTS
Project Sampling 10/19115
Pace Project No.: 92272649
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Sample: MW 05 Lab ID: 92272649006 Collected: 10119/15 1430 Received: 10/21/15 08,00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
62008 MSV Analytical Method: SM 6200B
Dichlorodifluoromethane
NO
ug1L
0.50
1
10/25/1504.39 75-71-8
1,1-Dichloroethane
NO
ug/L
0.50
1
10/25/15 04:39 75-34-3
1,2-Dichloroethane
NO
ug/L
0.50
1
102511504:39 107.06-2
1,1-Dichloroethene
NO
ug/L
0.50
1
10/25/15 04:39 75-35-4
Cis-1,2-Dichloroethene
NO
ug/L
0.50
1
10/25/15 04:39 156-59-2
trans-1,2-Dichloroethene
NO
ug/L
0.50
1
10/25/15 04:39 156.60.5
1,2-Dichloropropane
NO
ug/L
0.50
1
10/25/15 04.39 78-87-5
1,3-Dichloropropane
NO
ug/L
0.50
1
10/25/15 04:39 142.28-9
2,2-Dichloropropane
NO
ug/L
0,50
1
10125/15 04 39 594-20-7
1,1-Dichloropropene
NO
ug/L
0.50
1
10125115 0439 663-58-6
cis-1,3-Dichloropropene
NO
ug/L
0.50
1
10/25/15 04 39 10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
0.50
1
10/25/15 04:39 10061-02.6
Diisopropyl ether
NO
ug/L
0,50
1
10/25/15 04,39 108-20-3
Ethyibenzene
NO
ug/L
0.50
1
10/25/15 04:39 100-41-4
Hexachloro-1,3-butadiene
NO
ug/L
2,O
1
101251150439 87-W3
Isopropyibenzene (Cumene)
ND
ug/L
0.50
1
10/25/15 04:39 98-82-8
Methylene Chloride
ND
ug/L
2.0
1
10/25/15 04:39 75-09-2
Methyl-tert-butyl ether
NO
ug/L
0.50
1
10/25/15 04:39 1634.04-4
Naphthalene
NO
ug/L
2.0
1
10/25/15 04:39 91-20-3
n-Propylbenzene
NO
ug/L
050
1
10/25/15 04:39 103-65-1
Styrene
NO
ug/L
050
1
10/25/15 04:39 100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
1012511504:39 630-20-6
1,1,2,2-Tetrachloroethane
ND
uglL
0,50
1
10125/15 04 39 79-34.5
Tetrachloroethene
NO
ug/L
0.50
1
10/25/15 04 39 127-18-4
Toluene
NO
ug/L
0.50
1
1025/15 04 39 108-88.3
1,2,3-Tdchlorobenzene
NO
ug/L
2.0
1
10251150439 87-61-6
1,2,4-Tdchlorobenzene
ND
ug/L
2.0
1
10/2511504:39 120-82-1
1,1,1-Tdchioroethane
ND
ug/L
0,50
1
1025/15 D4:39 71-55-6
1,1,2-Tdchloroethane
ND
ug/L
0.50
1
1012511504:39 79-OD-5
Tdchloroethene
NO
ug/L
050
1
10/25/15 04:39 79-01-6
Trichlorofluoromethane
NO
ug/L
1.0
1
10/25/15 04.39 75-69-4
1,2,3-Tdchloropropane
NO
ug/L
0,50
1
10125/15 04 39 96-18-4
1,2,4-Tdmethylbenzene
NO
ug/L
0.50
1
10/25/1504:39 95-63-6
1,3,5-Tdrnethylbenzene
NO
ug/L
0.50
1
10/25/15 04 39 108-67.8
Vinyl chloride
ND
ug/L
1 D
1
1025115 04,39 75.01-4
m&p-Xylene
NO
ug/L
1,0
1
10/25/15 04 39 179601-23-1
o-Xylene
NO
ug/L
0.50
1
10/25/15 04.39 95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
102
%
70-130
1
1025115 D4:39 17060-07.0
4-Bromofluorobenzene (S)
99
70.130
1
1025115 04:39 460-DO-4
Toluene-d8(S)
100
%
70-130
1
10/25/15 04:39 2037-26-5
REPORT Of LABORATORY ANALYSIS
This report shall not be reproduced except in full,
Date: 11/1012015 09:05 AM without the written consent of Pace Analytical Services Inc. Page 12 of 40

/IceAnaljdicalo
� www!paeefabaoom
November 10, 2015
Mr. Stephen Reavis
MCAS Cherry Point
Facilities Maintenance Depart
PSG Box 8006, LCU
Cherry Point, NC 28533
RE: Project: Sampling 10/19/15
Pace Project No.: 92272649
Dear Mr. Reavis:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
IQ, qn .
Angela Baioni
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Project: Sampling 10/19/15
Pace Project No.: 92272649
Pennsylvania Certification IDs
Georgia Certification #: C040
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15501
L-A-B DOD-ELAP Accreditation #: L2417
Alabama Certification #: 41590
Arizona Certification #: AZ0734
Arkansas Certification
California Certification #: 04222CA
Colorado Certification
Connecticut Certification M PH-0694
Delaware Certification
FloridafTN1 Certification * E87683
Georgia Certification #: C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification #: 391
Kansas/TNI Certification #: E-10358
Kentucky Certification M 90133
Louisiana DHHrrNI Certification M LA140008
Louisiana DEO/TNI Certification #: 4086
Maine Certification #: PA00091
Maryland Certification* 308
Massachusetts Certification #: M-PA1457
MichiganfPADEP Certification
Missouri Certification #: 235
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #- 41320
Connecticut Certification #: PH-0216
Delaware Certification. FL NELAC Reciprocity
Florida Certification # E83079
Georgia Certification #: 955
Guam Certification FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification- FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification. #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #_ CeA 0074
Charlotte Certification IDs
9800 Kincey Ave Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification M 12
South Carolina Certification #; 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28NA
Ftorlda/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services, inc.
9800 Kincey Ave Suite 100
Huntersvilie, NC 28078
[phone]
CERTIFICATIONS
Montana Certification M Cert 0082
Nebraska Certification #: NE-05-29-14
Nevada Certification #: PA014572015-1
New Hampshire/TNi Certification * 2976
New JerseyfrN1 Certification * PA 051
New Mexico Certification * PA01457
New YorkrTNI Certification #: 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
OregonfrNI Certification #: PA200002
PennsylvaniafTNI Certification #: 65-00282
Puerto Rico Certification #: PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification M TN2867
TexasfTNI Certification M 7104704188-14-8
Utah1TNI Certification #: PA014572015.5
USDA Soil Permit #: P330-14-00213
Vermont Dept. of Health: ID# VT-0282
Virgin IsiandlPADEP Certification
Virginia/VELAP Certification #: 460198
Washington Certification #: C868
West Virginia DEP Certification* 143
West Virginia DHHR Certification #: 9964C
Wisconsin Certification
Wyoming Certification #: 8TMS-L
Nebraska Certification: NE-OS-28-14
Nevada Certification FL NELAC Reciprocity
New Hampshire Certification #: 2958
New York Certification #• 11608
North Carolina Environmental Certificate # 667
North Carolina Certification #: 12710
North Dakota Certification # R-216
Oklahoma Certification # D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification- #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification P 9962C
Wisconsin Certification* 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
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Virginia/VELAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Ana`ytical Services Inc
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SAMPLE ANALYTE COUNT
Project: Sampling 10/19/15
Pace Project No.: 92272649
Pace Analytical Services, Inc.
9BOO IGnceyAve Suite 100
Huntersville NC 28078
[phone]
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92272649001
001 SLUDGE
EPA 8081
SWB
8
PASI-C
EPA 8151
Lim
3
PASI-0
EPA 6010
CDF
13
PASI-A
EPA6010
CDF
7
PASI-A
EPA 7470
SH1
1
PASI-A
EPA 7471
SH1
1
PASI-A
EPA 8270
Bpi
18
PASI•C
EPA 8260
GAW
14
PASI-C
SM 254OG
KDF
1
PASI-C
ASTM D2974-87
CLW
1
PASI-C
EPA 1010
TEP
1
PASI-A
EPA 9045
MLS
1
PASI-A
SM 2710B
EWS
1
PASI-A
EPA 350.1
SER
1
PASI-A
EPA 351.2
SER
1
PASI-A
EPA 3532
DMN
3
PASI-A
EPA 3651
AES2
1
PASI-A
92272649002
001 SLUDGE
EPA 200.7
CDF
3
PASI-A
EPA6010
JMW
1
PASt-A
SW-846 7.3.3.2
BMS
1
PASI-PA
SW-846 7.3.4.2
PAS
1
PASI-PA
92272649003
MW 01
SM 6200B
CAH
63
PASI-C
92272649004
MW 02
SM 6200B
CAM
63
PASI-C
92272649005
MW 03
SM 6200B
CAH
63
PASI-C
92272649006
MW 05
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 3 of 40

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ANALYTICAL RESULTS
Project; Sampling 10/19/15
Pace Project No,, 92272649
Puce Analytical Services, Inc.
9800 KinceyAve, Suite 100
Huntersviile, NC 28078
[phone]
Sample: 001 SLUDGE Lab ID: 92272649001 Collected: 101191151100 Received: 10121115 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any ditutlons.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Clual
8081 GCS Pesticides, TCLP
Analytical Method., EPA 8081 Preparation Method, EPA 3510
Leachale Method/Date: EPA 1311;10130/15 00:00
gamma-BHC (Lindane)
NO uglL 0.50 1
11103/15 09,20
1110311513:26
58-89-9
Chlordane (Technical)
NO ug/L 3.0 1
11/03/15 09,20
11/0311513:26
57-74-9
Endrin
NO ug/L 0.50 1
11103/15 0920
1110311513;26
72-20-8
Heptachlor epoxide
NO ug1L 0.50 1
11103/15 09.20
1110311513:26
1024-57.3
Methoxychlor
NO ug1L 1000 1
11/03/15 09:20
11/03/15 13:26
72-43-5
Toxaphene
NO ug/L 3.0 1
11/03/15 09`20
11/03/15 13:26
8001-35-2
Surrogates
Decachtaroblphenyl(S)
40
%
10-138 1
1110311509:20
11/0311613.26 2051-24.3
Telrachtoro-m-xylene (S)
35
%
10-110 1
11/03115 09:20
11/03/1513;26 877-09.8
8151 Chlorinate Herbicide TCLP
Analytical Method: EPA 8151 Preparation Method: EPA 3510
2,4-D
NO
mg/L
11.0 1
10/30116 08:20
10/30/1515:41 94 75-7
2,4,5-TP (Silvex)
ND
mg1L
11.0 1
10/30/15 08:20
10130/1515:41 93-72-1
Surrogates
2,4-DCAA (S)
102
'%
42.142 1
10/30/15 0820
10/30/15 15A1 19719 28-9
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
30400
mglkg
9200 1
10/22/15 20:30
10127/15 01:47 7429-90.5
Arsenic
NO
mglkg
920 1
10/22/15 20:30
10/27115 01:47 7440.38-2
Cadmium
NO
mglkg
92.0 1
10/22115 20:30
10/27/15 01,47 7440-43-9
Calcium
130000
mglkg
9200 1
10/22/15 20:30
10/27115 01:47 7440-70-2
Copper
1700
mg/kg
460 1
10/22115 20:30
10/27/15 01:47 7440-50-8
Lead
NO
mglkg
460 1
10/22/15 2010
10/27/15 01A7 7439-92-1
Magnesium
19000
mg1kg
9200 1
10/22/15 20:30
10127115 01:47 7439.95-4
Molybdenum
NO
mglkg
460 1
10/22/15 20:30
10/27/15 01:47 7439.98-7
Nickel
ND
mglkg
460 1
10/22/15 20:30
10/27/15 01:47 7440.02-0
Potassium
ND
mglkg
460000 1
10/22115 20:30
10127/15 01A7 7440.09 7
Selenium
NO
mglkg
920 1
10122/15 20:30
10/27/15 01 A7 7782-49>2
Sodium
NO
mglkg
460000 1
10122/15 20:30
10/27/15 01.47 7440-23.5
Zinc
1930
mglkg
920 1
10122/15 20:30
10/27/15 01.47 7440-68.6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 131t 10122115 05:10
Arsenic
NO
mg1L
0.050 1
10123/15 02:30
10/23/1517,04 7440-38-2
Barium
NO
mg/L
0.25 1
10123116 02.30
10123/1517:04 7440.39.3
Cadmium
NO
mg/L
0.0050 1
10/23115 02:30
10/23/1517;04 7440-43.9
Chromium
NO
mg/L
0.025 1
10/23/15 02.'30
1012311517,04 7440-47-3
Lead
NO
mg/L
0.025 1
10123115 OZ30
10/23/1517:04 7439.92-1
Selenium
ND
mgiL
0,10 1
10/23/15 02-30
10/23/1517:04 7782-49 2
Silver
ND
mg/L
0.025 1
10/2311502.30
101231151T.04 7440-22.4
7470 Mercury, TCLP
Analytical Method: EPA7470 Preparation Method; EPA7470
Leachate Method/Date, EPA 1311,10122/15 05:10
Mercury
NO
mg/L
0,00020 1
1012311510:00
1012311513:41 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
In full,
Date: 11/1012015 09:05 AM
without the written consent of Pace Analytical Services, Inc..
Page 4 of 40

aceAnalyh'caJ'
mva:pacabbs oom
ANALYTICAL RESULTS
Project: Sampling 10119115
Pace Project No, 92272649
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntenvilie, NC 28078
[phone]
Sample: 001 SLUDGE Lab lD: 92272649001 Collected 10/19/15 13 00 Received: 10/21/15 08,00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
7471 Mercury
Mercury
8270 MSSV TCLP Sep Funnel
1.4-Dichlorobenzene
2,4-Dinitmtoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridfne
2,4,5-Trichlorophenol
2,4,6-Trich lorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenot (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachtoroethene
Tdchloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
254OG Total Percent Solids
Total Solids
Analytical Method EPA 7471 Preparation Method: EPA 7471
NO mg/kg 5.2 1 10126/15 13 20 10/27/15 13 52 7439-97-6
Analytical Method;. EPA 8270 Preparation Method EPA 3510
Leachate Method/Date: EPA 1311, 10130/15 00:00
NO
ug/L
50.0
1
11102/15 10 00
11/03/15 14.58
106.46-7
NO
ug/L
50,0
1
11/02M5 10 00
11/03/15 14 58
121-14-2
NO
ug/L
50.0
1
11/02/1510,00
1110311514;58
87-68.3
NO
ug1L
50.0
1
11102/1510,00
11/03/1514:58
118-74-1
NO
ug/L
50.0
1
11102/15 10 00
11103/15 14;58
67-72-1
ND
ug/L
500
1
11102/1510.DO
11/03/15 14'58
95-48-7
ND
ug/L
50.0
1
1110211510:00
11/03115 14 58
ND
ug/L
500
1
11102/15 10:00
11/03/15 14.58
98-95-3
NO
uglL
100
1
1110211510'00
11103/1514:58
87-86-5
NO
ug1L
50.0
1
1110211510:00
11103/1514:58
110-86-1
NO
ug/L
50.0
1
11/02/1510:00
1110311514:58
95.95.4
NO
ugfL
50.0
1
11/02/15 1010
11/03/15 14:58
88-06-2
18
%
12-102
1
11/0211510.00
11/0311514:58
4165.60-0
22
%
13-107
1
11102/1510:00
11/03/1514:58
321.60-8
56
%
21-132
1
11/02/1510:00
11/03/1514.58
1718-61-0
9
%
10.110
1
11/0211510:00
11103/1514:58
13127-88-3 SO
12
%
10-110
1
11102115 10 00
11/0311514:58
367-124
50
%
27-108
1
11102/15 10 00
11/03/15 14 58
118-79-6
Analytical Method EPA8260 Leachate MethodfDate: EPA 1311; 10/26/15 11'12
NO
ug/L
100
20
10/31115 08 56 71-43.2
NO
ug1L
200
20
10131115 08,56 78.93.3
ND
ug/L
100
20
10/31/15 08:56 56.23.5
NO
ug/L
100
20
10/31/15 08:56 108-90-7
NO
ug/L
100
20
10/31/15 08:56 67-66-3
NO
ug1L
100
20
10/31115 08:56 106-46-7
NO
ug/L
100
20
10131/16 08:56 107-06-2
NO
ug1L
100
20
10/31/15 08:56 75-354
ND
ug/L
100
20
10/31/15 08 56 127-18-4
NO
ug/L
100
20
10/31/15 08 56 79-01.6
NO
ug/L
100
20
10/31/15 08:56 75-01-4
124
%
70-130
20
10/31/15 08:56 17060-07-0
98
%
67A35
20
10131/1508:56 2037-26.5
105
%
70.130
20
10/31/15 08:56 460.00-4
Analytical Method: SM 254OG
0.090 % 0000010 1
REPORT OF LABORATORY ANALYSIS
10/21/15 16.53
This report sha`I not be reproduced, except in full,
Date: 11110/2015 09 05 AM without the written consent of Pace Analytical Services, Inc., Page 5 of 40

aceAnalytical s
w»w.P&C01 oora
ANALYTICAL RESULTS
Project. Sampling 10/19/15
Pace Project No.; 92272649
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersvlle, NC 2807E
(704)8754092
Sample: 001 SLUDGE
Lab ID: 92272649001 Collected:
10/19/15 13 00
Received: 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
99.9 %
0,10 1
10122/15 12,53
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0 1
10/30/15 11:30
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.2 Std. Units
0,10 1
10/22/15 11:40 H1
Plant Available Nitrogen
Analytical Method; SM 2710B
Plant Available Nitrogen
122000 mg/kg
0,12 1
11/05/15 17,20 N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
136000 mglkg
10200 1
10/26/15 01:31 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 3511
Nitrogen, Kjeldahl, Total
217000 mg/kg
55200 1
11/03/15 02 36 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method EPA 353.2
Nitrogen, Nitrate
26000 mg/kg
2180
1
11/03116 10 31
Nitrogen, Nitrite
4160 mg/kg
1090
1
11/03/15 10.31
Nitrogen, NO2 plus NO3
30100 mg/kg
2180
1
11/03/15 10:31
365.1 Phosphorus, Total
Analytical Method. EPA 365.1
Phosphorus
142000 mg/kg
4150
2
10/2811512:19 7723-14-0
Sample: 001 SLUDGE Lab ID: 92272649002 Collected 10/19115 13 00 Received: 10/21/15 08:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No
200.7 MET 1CP
Analytical Method: EPA 200.7 Preparation Method EPA 200.7
Calcium
189000 ug/L 1000
1
11/05/15 13 05
it/06115 15:41
7440-70-2
Magnesium
24200 ug1L 1000
1
11/05/15 13 05
11/06/15 15 41
7439-95-4
Sodium
117000 ug/L 50000
1
1110511513,05
1110611515,41
7440-23-5
Sodium Adsorption Ratio, SAR
Analytical Method. EPA 6010
Sodium Adsorption Ratio
2.1 meq/L
1
11/09/15 17 02
733C Reactive Cyanide
Analytical Method: SW-846 7.3 3.2
Cyanide, Reactive
ND mg/L 0,010
1
10/22/15 22 30
734S Reactive Sulfide
Analytical Method SW-846 7.3,4.E
Sulfide, Reactive
ND mg/L 1.0
1
10/22/15 18 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/10/2015 09'05 AM without the written consent of Pace Analytical Services :nc.
Qual
N2
Page 6 of 40

x
UNITED STATES MARINE CORPS
MARINE CORPS AIR STATION
POSTAL SERVICE CENTER BOW
CHERRY POINT, NORTH CAROUNA 2E6. 3aW
IN REPLY REFER TO:
5096/07109
LN
November 16, 2015
North Carolina Department of Environment
and Natural Resources
Division of Water Quality
Information Processing Center
1617 Mail Service Center
Raleigh, NC 27699-1611
Subj: TRIENNIAL GROUNDWATER MONITORING
In accordance with the groundwater monitoring and reporting
requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489.for
Land Application of Wastewater Residuals, enclosed are the original
and -one copy of the GW-59-A report and the four GW-59 reports (one
each for monitoring wells 1, 2, 3, and 5) for the triennial
reporting for October 2015.
Should you have any questions, please contact Mr. Timothy
Lawrence, PE of the Environmental Affairs Department at your
earliest convenience at [phone].
Enclosure: (1) GW-59-A
(2) GW-59 for MW-1
(3) GW-59 for MW-2
(4) GW-59 for MW-3
(5) -GW-59 for MW-5
(6) Lab Report
Sincerely,
G. U
Envm n
By direct
Commanding
1 Affairs Officer
n of the
Officer

GW-59A COMPLIANCE REPORT FORM,. Permit # ' WQ0001489
(Submit one each manitoring period with GIV-59 farms.)
Enter date monitoring results were due. l I130/15 Will this monitoring report (GW-59 and G1V S9A) be submitted after YES
NO
1 the
established due date?
X
2
Was any required information missing on the GIV-59 report forms? YES
NO
X
IF
the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems
encountered in obtaining the required information.
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES
'NO
3
identification plate, area overgrown, etc.)? ljthe answeris "Yes", contact the Regional C riceforguidance.
X
4
Are any monitored constituents equal to or above the established standards? YES
NO.
X .
If the answer to question 4 is "NO", skip to section 8:
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the 1
space provided below,
M%V-2 TOTAL AMMONIA (NI13) 2.4 mpjL
MW-5 TOTAL AMMONIA (NI13) 2.1 mg/L
For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s)' YES
NO
5
in the some well(s) in the last two years? X
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 Is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentrations)
reported, and sample collection date for each occurrence (for the last two years).
Mw-2: Oct. 2013 NI13 3.0, Feb. 2014 N113 3.0, Oct. 2014 Nil! 1.7, Feb. 2015 N1131.7
MW-5: 'Feb. 2014 NI13 3.2, June 2014 NIi3 2.7, Oct. 2014 N113 3.0, Feb. IOIS NI13 2.7
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES
NO
X
If the answer is "YES", a groundwater quality problem maybe occurring, CONTACT THE REGIONAL OFFICE IMMEDIATELY
FOR GUIDANCE. it the answer is "NO", monitoring wells maybe Improperly located; contact the Regional Office.
Is the permittee implementing previously approved actions required by the Division involving this groundwater quality YES
NO
7
problem?
X
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be renulred to determine the
Impact the waste disnosal system Is having of the review and comnllance boundaries surrounding this racility. Failure to do so may
subiect the permiltee to a Notice of Violstion, fines, and/or nenallics.
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with
8
GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
12
0 ertsby ac ~ledge: the yes utfotmaitanwra titttedAandtthe infarmagott sa u�mtbts caps CoIIsLttaee" y
Patricia T. Davis, Utility Systems Operator Su rvisor
t`f"v�
Signature of Permittee (or Authorized Agent) pate 1111612015

Si IRMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or
Facility Name: MCAS Cherry Point
Permit Name (if different),
Facilltv Address: MCAS Cherry Point NC 28533-0006_
County: Craven
act Person: Patricia T. Davis Telephone #: [phone]
Location/Site Name: Site 21, MCAS Cherry Point No.of Welts to be Sampled: m i
SAMPLING INFORMATION
WELL ID NUMBER (From Permit): MW 1
Well Depth 26.66 &
Depth to Water Level 82546: 1 ft. below measuring point
Measuring Pant is 1,33 fL above land surface
Volume of water pumpedlbailed before sampling. 5 Gal.
Samples for metals were collected unfiltered ) YES
LABORATORY INFORMATION
QI�A#.S[Y-ih1Fbf WT
16'1� 7� P"me 01>i)734^;721
Non -Discharge UIC
NPDES WQ0001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remedlation:
❑ Rotary Distributor 0 Land Application of Sludge
❑ Water Source Heat Pump ❑ Other.
Date Sample Collected: 10119/2015 FIELD ANALYSIS: nC DRY at
Well Diameter, 2 pH omo 6.1 units Temp 00010: 21 time of
Screened Interval: -0.17 ft to -15.2 ft. Spec. Cond. OW94: 190 liMhos samplinc
Relative M R Elevabon: 10.78 Odor 00085 none check
Appearance: clear here:
NO and field acidified U YES LJ NO
Date sample analyzed' 10119/2015 Laboratory Name: MCAS Cherry Point 1 Pace Analytical Certification Number. 20i 1
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg1L
Nitrite (NO2) as N 00615
mg/L
Coliform; MF Fecal 31616 <1
1100mL
Nitrate (NO3) as N 00620 <0,1
mg/L
Coliform: MF Total 31504
1100mL
Phosphorus: Total as P 00665
mg/L
(NoW Usa MPN mst $Od for NQ* hnbd samples)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300 56
mg/L
At -Aluminum 01105
mg/L
pH (Lab) 00403 6.1
units
Sa - Barium 01007
µgn-
TOC 00680
mg/L
Ca -Calcium 00916
mg/L
Chloride 00940 12
mg/L
Cd -Cadmium: Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg1L
Cy - Capper 01042
mg1L
Phenol 32730
pg1L
Fe - Iron 01045
µg/L
Sulfate 00945
mg1L
Hg - Mercury 71900
N91L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610 <0.1
mg1L
Mg - Magnesium 00927
mg1L
(Anwnom NMragen, NH3 as N. Anroor a Nitrogen, TOW
Mn - Manganese 01055
µg[-
TKN as N 00625
mg1L
NI - Nickel 01067
µg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units);
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? El Yes(1) ❑ No (0)
VOC 78732 Method# 6200B
Method#
Method#
Method#
e-.-- ��..-...J3..�1.... a„arF- rinlu lAttarh I ath RenertSt: innuent i uLdi vuLa.
VOC Removal%
11/612015
Patricia T. Davis - Utility Systems Operator
Pennittee (or Authorized Agent) Name and Title - Please print or type Signature of Permitiee (or Authorized Agent) (Date)
GW-59 Rev, 212010

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATI N Please Print Clearty or
Facility Name: MCAS Cherry Point
Permit Name (if different):
Facility Address: MCAS Cherry Point NC 28533-0006
County: C
act Person: Patricia T. Davis Telephone #: [phone]
Location/Site Name: Site 21. MCAS Cherry Point No of Wells to be Sampled
on
on -Discharge UIC
PDES WQ0001489 Other
YPE OF PERMITTED OPERATION BEING MONITORED
Lagoon ❑ Remediation: infiltration Gallery
Spray Field Remediation:
Rotary Distributor Q Land Application of Sludge —
Water Source Heat Pump ❑ Other.
MPLING INFORMATION
LL ID NUMBER (From Permit): MW-2 Date Sample C d: 10/19/2015
II Depth 26.58 ft.Well Diameter ^2
Screened Interval: -1 03 ft. to -11 It.
to Water Level 82546. 7 it below measunng point
asuring Point is 1,28 it- above land surface Relative M P. Elevation 14 8
ime of water pumped/bailed before sampling: 5 Gal_
nples for metals were mlected unfiltered f ) YES U NO and field acidified ❑ YES Lj NO
WAS
FIELD ANALYSIS: a DRY ..
pH oo40o 5.85 units _Temp 00010: 19 C M . a.
Spec. Cond. 00094 897 pMhos . ,„ p,; � o .
Odor00085 none^•�{
Appearance clear "'
90RATORY INFORMATION
am le anal zed' 10/19/2015 Laboratory Name: MCAS Cherry Point 1 Pace Analytical Certification Number.
es p y
;AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nilnte (NO2) as N 00615
mg/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0:1
mg/L
Coliform: MF Total 31504
1106mL
Phosphorus: Total as P 00665
mg/L
(Nola use MFN memod for K9* 1U`W sam0es)
Orthophosphate
mg/L
Dissolved Solids: Total 70300 308
mg/L
01107
Al -Aluminum 01107
L
pH (Lab) 00403 585
units
Ba -Barium Oi007
Ng1L
pg/
L
TOC 00680
mg/L
Ca -Calcium 00916
Chloride 00940 14
mg/L
Cd - Cadmium: Total 01027
µg/L
pg/
Arsenic 01002
pg/L
Chromium: Total 01034
µgn-
Greaseand Oils 00552
mg1L
Cy - Copper 01042
mg1L
Phenol 32730
pg/L
Fe - Iron 1
ugn-
Sulfate 00945
mg/L
7
Hg -Mercury 1900 00
Ngn
Specific Conductance 00095
NMhos
K - Potassium 00937
mg/L
mg/L
Total Ammonia 00610 2.4
mg/L
Mg - Magnesium 00927
(Amnwrw Ntrogan; NH2 as N; Amrnom NWOQon. Total)
Mn - Manganese 01055
Ng/L
TKN as N 00625
mg/L
Ni - Nickel 01067
µg/L
137706
Pb - Lead 01051 Ng/L
Zn - Zinc 01092 mgn
Other (Specify Compounds and Concentration Units)'
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? [ Yes(1) D No (0)
VOC 78732 Method# 6200B
Method#
Method#
Method#
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Effluent Total VOCs: VOC Removal°%
11/6/2015
Patricia T. Davis - Utility Systems Operator (Date)
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent)
GW-59 Rev.2/2010

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearty Of
Facility Name: MCAS Cherry Point
Permit Name (if different):
Facility Address: MCAS Cheer Point. NC 28533-0006
County: Craven
act Person. Patricia T. Davis Telephone #: [phone]
Location/Site Name: Site 21 MCAS Cherry Point No of Wells to be Sampled
T7Gti9 16i7, f'hMr W
um
on -Discharge UIC
PDES W00001489 Other
YPE OF PERMITTED OPERATION BEING MONITORED
0 Lagoon [] Remedlation: Infiltration Gallery
Spray Field (] Remediation:
Rotary Distributor Q Land Application of Sludge
E] Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION WAS
WELL ID NUMBER (From Permit): MW-3 rmDate Sample Collected: 10/19/2015 FIELD ANALYSIS: PC DRY
Well Depth 25.rm .,
fL Well Diameter. 2 pH 00400 6.1 un is Temp 00010: 20 - o
Depth to Water Level 82546 0 FL below measuring point Screened Interval: -11.7 ft. to -21,7 fL Spec. Cond. 00094 201 t . m, ...o
Relative M P Elevation: 3.1 Odor 00085: none
Measuring Paint is 1 46 ft above land surface Volume of water pumped/b sampling: ,,,,.
ailed before sam lin 5 Gal. Appearance: turbid El
Samples for metals were collected unfiltered YES NO and field acidified (� YES NO
LABORATORY INFORMATION
1-I=le sample analyzed 10/19/2015 Laboratory Name: MCAS Cherry Point /Pace Analytical Certification Number. 201 / 37706
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Coliform: MF Fecal 31616 <1
1100ml-
Nitrate (NO3) as N 00620 2.5
mglL
Coliform: MF Total 31504
1100mL
Phosphorus: Total as P 00665
mg/L
(Nate- We MPN merod for hn M bred samples)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300 144
mg/L
All - Aluminum 01105mg/L
pH (Lab) 00403 6.1
units
Ba - Barium 01007
µg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 6.9
mg/L
Cd - Cadmium: Total 01027
µ9/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
µg/L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
V9/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg1L
Total Ammonia 00610 <1 0
mg/L
Mg - Magnesium 00927
mg/L
tAm t-M Ntrogen. NH, as N. Ammaw Nr Ww. Touq
Mn - Manganese 01055
µg/L
TKN as N 00625
mg/L
Ni - Nickel 01067
pg/L
Pb - Lead 01051 µg1L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? [:—�j Yes(() ❑ No (0)
VOC 78732 Method# 6200E
Method#
Method#
Method#
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Effluent Total VOCs: VOC Removal%
11/6/2015
Patricia T. Davis - UtilitySystems Operator Date)
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent)
GW-59 Rev.212010

SUBMIT FORM ON YELLOW PAPER ONLY
UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
Please Pnnt Clearly or
Facility Name: MCAS Cherry Point
Permit Name (if different):
Facility Address: MCAS Cherry Point, NC
County: Craven
act Person: Patncia T. Davis Telephone M 252466.4599
Location/Site Name: Site 21 MCAS Cherry Paint No.of Wells to be Sampled
UOT
PHONE.
n-Discharge UIC
DES WQ0001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
Lagoon 0 Remediation: Infiltration Gallery
[� Spray Fleid Remedlation:
Rotary Distributor [ Land Application of Sludge
Li Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION
MW-5
Date Sample Collected.
10/19/2015
FIELD ANALYSIS:
WAS
DRY .�
WELL ID NUMBER (From Permit):
Well Diameter
2
pH 00 6.2 units Temp 00010: 24 C
040
m _ o
Well Depth 13 ft.
Depth to Water Level 82546. 6.5 ft below measuring point Screened Interval 3
ft. to 13 It,
Spec. Cond. 00094: 544 pMhos
Measuring Point is 3 It. above land surface
Relative M.P Elevation:
12
Odor 00085 none
clear
-
Volume of water pumped/bailed before sampling:
5 Gal.
Appearance
Sam es for metals were collected unfiltered
YES �. NO and field acidified r YES ❑ NO
LABORATORY INFORMATION
n=fe sam le analyzed: 10119/2015
Laboratory Name: MCAS Cherry
Point 1 Pace Analytical
Certification Number. 201137706
p
tAMETERS NOTE: Values should mnect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
m9n-
Coliform: MF Fecal 31616 <1
/100ml-
Nitrate (NO3) as N 00620 <0.1
mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00565
mg/L
(,Nola: use MPN medWd for hgt9y tubid sanOes)
Orthophosphate 70507 _
mg/L
Dissolved Solids: Total 70300 192
mg/L
Al - Aluminum 01105
mg[L
pH (Lab) 00403 62
units
Ba - Barium 01007
Irg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg1L
Chloride 00940 12
mg/L
Cd - Cadmium: Total 01027
p9/L
Arsenic 01002
Vg/L
Chromium: Total 01034
p9/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
pgtL
Fe - Iron 01045
p9/L
Sulfate D0945
mglL
Hg - Mercury 71900
pg/L
Specific Conductance 00095
pMhos
K - Potassium 00937
mg1L
Total Ammonia 00610 2.1
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Ntropan; NH3 as N; Armioni N wtgon. Tetwl
Mn - Manganese 01055
p9/L
TKN as N 00625
mg/L
N1- Nickel 01067
pg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? Yes(1) ❑ No (0)
VOC 78732 Method# 6200B
Method#
Method#
Method#
c—r....,r nMv rAtfarh I ah Renortsl: Influent Total VOCs: Effluent Total VOCs: VOC Removal%
11/6/2015
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev.2/2010

aceAnalyticala
wwwp�etabatnm
November 10, 2015
Mr. Stephen Reavis
MCAS Cherry Point
Facilities Maintenance Depart
PSC Box 8006, LCU
Cherry Point, NC 28533
RE:, Project: Sampling 10/19/15
Pace Project No.: 92272649
Dear Mr. Reavis:
Pace Analytical Services, Inc.
SB00 IQncey Ave. Suite 100
Hunter%Wla, NC 2807a-
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Angela Baioni
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 40

aceAnalyirca!'
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Project: Sampling 10/19/15
Pace Project No.: 92272649
Pennsylvania Certification IDs
Georgia Certification#: C040
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
L-A-B DOD -FLAP Accreditation #: L2417
Alabama Certification #: 41690
Arizona Certification #: AZ0734
Arkansas Certification
California Certification #: 04222CA
Colorado Certification
Connecticut Certification M PH-0694
Delaware Certification
Florida/rNI Certification * E87683
Georgia Certification #: C040
Guam Certification
Hawaii 'Cerlifica{Ion
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification M 391
KansasffNI Certification M E-10358
Kentucky Certification * 90133
Louisiana DHHrTNI Certification M LA140008
Louisiana DEOJTNI Certification #: 4086
Maine Certification #: PA00091
Maryland Certification #: 308
Massachusetts Certification M M-PA1467
Michlgan/PADEP Certification
Missouri Certification #: 235
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification # 41320 .
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification P E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification M 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification:#346
Michigan Certification * 9911
Mississippi Cerfification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification#: Carl 0074
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification M 12
South Carolina Certification #: 99008001
Asheville Certification IDs
Pace Analytical'Servlcea, Inc.
9800IUnceyAve. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Montana Certification M Cert 0082
Nebraska Certifcalon #: NE-05-29-14
Nevada Certification M PA014572015-1
New HampshirefTNI Certification #: 2976
New JerseyrrNI Certification#: PA051
New Mexico Certificatlon#: PA01457
New York[TNI Certification #:10888
North Carolina Certification #] 42706
North Dakota Certification #: R-190
Oregon/TNI Ceritfication #: PA200002
Pennsylvania/TNI Certification #: 65-00282
Puerto Rica Certification #: PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification #: TN2867
Texas/TNI Certification #: T104704188-14.-8
UlaWTNi Certification #: PA014572015.5
USDA Soli Permit V 13330-14-00213
Vermont Dept. of Health: ID# VT 0282
Virgin Island/PADEP Certification
Virginia/VELAP Certification #: 460198
Washington Certification #: C868
West Virginia DEP Certification * 143
West Virginia DHHR Certification #: 99MC
Wisconsin Certification
Wyoming Certification #: 8TMS-L
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification M 2958
New York Certification #:11608
North Carolina Environmental Certificate # 667
North Carolina Certification #:.12710
North Dakota Certification #: R 216
Oklahoma Certification #: D9947
Pennsylvania Certification M GM0547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification M TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Flodda/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaIVELAP Certification #. 460221
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Fladda/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in tug,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 40

aceAnaliftal�
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 I(Incey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: MW 01 Lab 1D: 92272649003 Collected: 10/19/15 13:00 Received: 10/21/15 08:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
62009 MSV Analytical Method: SM.6200B
Benzene
NO
ugfL
0.50
1
10/25115 03:49 71-43-2
Bromobenzene
NO
ug/L
0.50
1
10/25115 03,49 108-86.1
Bromochtoromethane
NO
ug/L
0.50
1
10/25/15 03:49 74-97-5
Bromodichloromethane .
NO
uglL
0.60
1
10/25115 03:49 75-27-4
Bromofomt
NO
ug/L
0.50
1
"10125115 03:49 75-25-2
Bromomethane
NO
ug1L
&0
1
10/25/15 03A9 74 83-9
n-Butylbenzene
NO
ug/L
0.50
1
10125/15 03A9 104-51-8
sec-Butylbenzene
NO
ug/L
0.50
1
1012511503.49 13.5-98-8
ter(-Butylbenzene
NO
ug/L
0.50
1
10/26115 0149 98-06-6
Carbon tetrachloride
NO
uglL
0.50
1
10/25/15 03:49 56-23.5
Chlorobenzene
NO
ug/L
0.50
1
10/25115 03A9 108-90-7
Chtoroethane
NO
ug1L
1.0
1
10/25/1503A9 75.00.3
Chloroform
6.4
ug1L
.0.50
1
10/25/15 03AS 67.66.3
Chioromethane
NO
ug/L
1.0
1
10125/15 03,49 74.87=3
2-Chlorotoluene
NO
ug1L
0.50
1
10125115 03A9 ' 95=49-8
4-Chlorotoluene
NO
ug/L
0.60
1
10/25/15 03,49 106-434
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
1
10/25115 03:49 96-12.8
Dibromochloromelhane
NO
ug/L
0.50
1
10/26/15 03:49 12448.1
1,2-Dibromoethane (EDB)
NO
uglL
0.50
1
10/25/15 03,49 106-934
Dibromomethane
NO
ug/L
0.50
1
10/2511503:49 74-95-3
1,2-Dichlorobenzene
NO
ug/L
0.50
1
10/25/15 03:49 95-50.1
1,3-Dichlor8benzene
NO
ug/L
0.50
1
10125/15 03:49 541-73-1
1,4-Dichtorobenzene
NO
ug/L
0.50
1
10/25115 03:49 106-46-7
Dichlorodifluoromethane
NO
ug/L
0,50
1
10/25/15 03.49 75-71-8
1,1-Dichloroethane
NO
ug/L
0.50
1
10/26115 03,49 75-34-3
1,2-Dlchtoroethane
ND
ug/L
0.50
1
10125/15 03A9 107-06-2
11-Dichloroethene
NO
uglL
M50
1
10125/15 03A9 75-36.4
cis-1,2-Dichloroethene
NO
ug/L
0,50
1
10125115 03:49 156-59-2
'156-60-5
trans-1,2-Dichioroelhene
NO
ugiL
0.50
1
10/25115 03:49
1,2-Dichloropropane
ND
uglL
0.50
1
10/2511503:49 78-87-5
1,3-Dichloropropane
NO
uglL
0.50
1
10125115 03:49 142-28-9
2,2-Dichloropropane
NO
uglL
0.50
1
10125/15 03A9 594-20-7
1,1-Dichtoropropene
NO
ug/L
0.50
1
10125/15 03A9 563-58.6
cis-1,3.Dichloropropene
NO
ug/L
0,50
1
10125115 03:49 10061-DI.5
trans-1,3-Dichtoropropene
NO
ug/L
0.50
1
10/25115 03,49 10061-02-6
DI)sopropyl ether
ND
ug1L
0,50
1
10125/15 03:49 108-20-3 •
Ethylbenzene
NO
ug/L
0.50
1
10125115 03:49 1OD 41-4
Hexachloro-1.3-butadiene
NO
uglL
2.0
1
10125/15 03,49 87-68-3
Isopropylbenzene (Cumene)
NO
ug/L
0.50
1
10125115 03:49 98.82-8
Methylene Chloride
NO
ug/L
2.0
1
10/25/15 03A9 75-09-2
Methyl -tent -butyl ether
NO
ug/L
0.50
1
10125115 03:49 1634.04.4
Naphthalene .
NO
ug/l.
2.0
1
10125/15 03:49 91-20.3
n-Propylbenzene
NO
uglL
0.50
1
10125115 03A9 103-65-1
Styrene
NO
ugfL
0.50
1
10/25/15 03A9 100-42-5
1,1,1,2-Teirachloroethane
NO
uglL
0,50
1
10/25115 03:49 630-20.6
1,1,2,2-Telrachloroethane
NO
u911-
0.50
1
10125/15 03:49 79-34-5
Tetrachloroethene
NO
ug1L
0.50
1
10125115 03:49 127-18.4
REPORT OF LABORATORY ANALYSIS
This report shall not be repmdumd, except in full,
Date: 11/10/2015 09:05 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 40

Pace Analytical Services; Inc.
te 100,
IeC,
Analytical 9e00I(incey Ave. H ntersva e, NCr 260766
[phone]
ANALYTICAL RESULTS
Project: Sampling 10/19115
Pace Project No.: 92272649
Sample: MW 01 Lab ID: 92272649003 Collected: 10/1911513:00 Received: 10121/15 08:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichiorobenzene
1,1,1-Trichioroethane
1,1,2-Trichtoroethane
Tdchioroethene
Tdchloro8uoromethane
1,2,3-Tdchloropropane
1,2,4-Tdmethylbenzene _
1,3,5-Tdmethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-BromoOuorobenzene (S)
Toluene -dB (S)
Analytical Method, SM 6200B
NO
ug/L
0.50
1
10/25115 03:49 108-88-3
ND
ug/L
2.0
1
10125/15 03:49 87-61-6
NO
ug1L
20
1
10/25115 03A9 120-82-1
ND
ug/L
0.50
1
10125115'03A9 71=55-6
NO
ug/L
0150
1
10/25/15 0149, 79.00-5
NO
ug1L
0.60
1
10/25/15 03.49 79-01.6
NO
ug/L
1.0
1
10/25/15 0149 75-69-4
NO
ug/L
0.50
1
10125115 03:49 96-18.4
NO
ug/L
0.50
1
10/25118 03:49 95-63.6
NO
ug/L
0.60
1
10125/16 03:49 108-67-8
ND
ugiL
110
1
10/25115 03:49 75-01.4
ND
ug/L
1.0
1
10/25/15 03:49 179601-23-1
NO
ug/L
0.50
1
10125/15 03:49 95-47-6
163
%
70-130
1
10/25/15 03:49 17060-07-0 ,
97
%
-10.130
1
10/25115 03A9 450.004
100
%
70-130
1
10/25/15 03:49 2037-26-5
Sample: MW 02 Lab ID: 92272649004 Collected: 10/19/151100 Received: 10/21/15 08,.00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
NO
ug/L
0.50
.1
10/25/15 04,06 7143-2 .
Bromobenzene
ND
ug1L
0.50
1
10/25115 04:06 108-86.1
Bromochloromethane
ND
ug/L
0.50
1
10125115 04:05 74.97-5
Bromodichloromethane
ND
ug/L
0.50
1
1012511504:06 75-274
Bromoform
ND
VL
0.5D
1
10125/15 04:06 75-25-2
Bromomelhane
NO
ug/L
5.0
1
10125115 04:06 74-83-9
n-Butylbenzene
NO
uglL
0.50
1
10/25115 04:08 104.51-8
sec-Butylbenzene
ND
uglL
0.50
1
10125/15 0446 135-98-8
tart-Butylbenzene
ND
ug/L
0.50
1
1D12511504,06 98.06-6
Carbon tetrachloride
ND
ug1L
0.50
1
10125/15 04:06 56-23-5
Chlorobenzene
NO "
ug/L
0.60
1
10125115 04:06 108-90 7
Chloroethane
NO
ug/L
1.0
1
10125115 04,06 75-00-3
Chloroform
NO
ug/L
0.60
1
10/25/15 04:06 67-66-3
Chloromethane
ND
ug/L
1.0
1
10125/1504,06 74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
10/26/16 ft06 9549-8
4-Chlorotoluene
ND
ug/L
0.60
1
10125/15 04:06 106.43.4
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
1
10125/15 04:06 96-12.8
Dibromochloromethene
NO
ug/L
0.50
'1
10125115 04:06 124-48-1
1,2-Dibromoethane (EDB)
NO
ug1L
0.5D
1
10125/15 04:06 106-93-4
Dibromomethane
ND
ug1L
0.50
1
10/25115 04,06 74-95-3
1,2-Dichlorobenzene
NO
ug/L
0.50
1
10/25/15 04,06 95-50-1
1,3-Dichlorobenzene
NO
ug/L
0.50
1
10125/15 04:06 541-73.1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
1012511504:06 106.46-7
REPORT OF LABORATORY ANALYSIS
This report shal not be reproduced, except In full,
Dale: 11/10/2016 09:05 AM without the written consent of Parse Analytical Services, Inca Page 8 of 40

aceAnalyt6ca!`
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ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Pace Analytical Services; Inc.
9800 Fin •ceyAve. Suite 100
Hunlersvillex NC'2ao7a
[phone]
Sample: MIN 02
Lab ID: 92272649004 Collected: 10/19/15 13:00
Received: 10/21115 08:00 Mabix:.Water
Parameters
Results
Units
Report Limit
OF
Prepared Analyzed CAS No. Qual
6200E MSV
Analytical Method: SM 6200B
Dichloroditluoromethane
'ND
ug/L
0.50
1
10125116 04±06 75 71.8
1;1-Dichloroethane
NO
ug/L
050
1
10/25/15 04106 75-34.3
1,2-Dichloroethane
NO
ug/L
0,50
1
10/25115 04:06 107-06.2
1,1-Dichloroethane
NO
ug/L
050
1
10/251150406 75.35.4
cis-1,2-Dichloroethene
NO
ug/L
0.60
1
10/25/15 04.06 156-59.2
trans-1,2-Dichloroethene
NO
ug/L
0.50
1
10/25/15 04:06 156-60.5
1,2-1316loropropane
NO
ug/L
0.50
1
10125/iSO4:06 78'-87-5
1;3-Dichloropropane
NO
ugiL
0.60
1
1012511504-'06 142-28.9
2,2-Dichloropropane,,
NO
ug/L
0.50
1
1012511504'.06 594-20.7
1,1-Dichloropropene
NO
ug/L
0,50
1
10/251,15 04:06 563-58-6
cis-1,3-Dichloropropene
NO
ug/L
0.50
1
10/25/15 04,06 10061.01.5
trans-1,3-Dichloropropene
NO
ug1L
0,60
1
10/2511504:06 10061.62.6
Diisopropyl ether
NO
ugiL
050
1
10125/15 04:06 10B-20.3
Ethylbenzene
NO
ug/L
0.50
1
10/2511504:06 100.41-4
Hexachloro-1,3-butediene
NO
ug/L
2.0
1
10/25/1504:06 87-68-3
Isopropylbenzene (Cumene)
NO
ug/L
0.50
1
10/25/15 04:06 98-82.8
Methylene Chloride
ND
ug/L
2,0
.1
10125M5 04:06 75-09-2
Methyl-tert-butyl ether
NO
ugiL
0.50
1
10/25/15 04,06 1634-04-4
Naphthalene
NO .
ug/L
2.0
1
10125/15 04,06 91411-3
n-Propylbenzene
NO
ug/L
0.50
1
10125H 5 04.06 103-65-1
Styrene
NO
ug/L
050
1
10/25/15 04,06 100-42-5
1,1,1,2-Tetrachloroethane
ND
ugiL
0.50
1
10125/1504:06 630-20-6
1,1,2,2-Teirachiamethane
ND
ug/L
0.50
1
10125115 04,06 79.34-5
Tetrachloroethene
NO
ugiL
0,50
1
10125/15 04=06 127-18-4
Toluene
NO
ug1L
050
1
10/25/15 0*06 108-88-3
1,2,3-Trichlorobenzene
NO
ugiL
2.0
1
10/2511504.06 87-61-6
1,2,4-Tdchlorobenzene
NO
ug/L
2,0
1
1012511504:06 120-82-1
1,1,1-Trichloroethane
NO
ugiL
0,50
1
1012611604,06 7145.6
1,1,2-Tdchloroethane
ND
ugiL
0.50
1
10/25115 04:06 79-00.5
Trichloroethene
NO
ltg/l.
0.50
1
10/25/15 04,,06 79-01-6
Trichloro8uoromethane
NO
ugiL
1.0
1
10125115 04:06 75.69-4
1,2,3-Tdchloropropane
ND
ug/L
0:50
1
1012511504:06 96-18-4
1,2,4-Tdmethylbenzene
NO
ug/L
0,50
1
1012511504�6 95.63.6
1,3,5-Trimethylbenzene
NO
ugiL
0.50
1
1012511504;06 108.67-8
Vinyl chloride
ND
ugiL
1.0
1
10125/15 04:06 75-01-4
m&p-Xylene
NO
ugiL
1.0
1
10/25115 04:06 179601.23-1
o-Xylene
NO
ug/L
0.50
1
10/25/15 04:06 95-47.6
Surrogates
1,2-Dichloroethane-d4 (S)
101
°%
70-130
1
10/25/15 04:08 17060-07.0
4-BromoOuorobenzene (S)
98
%
70-130
1
10/25/16 04:06 460.00-4
7oluene-d8 (S)
100
%
.70430
1
10/25/15 04!06 2037-26.5
Date: 11/1012015 09:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in W1,
without the written consent of Pace Analytical Services, hoc..
Page 9 of 40

aceAnaliftala
xwncpeeelebsosm
ANALYTICAL RESULTS
Paca AtiMytical S®rvices, Inc.
9860 Wncey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: Sampling 10/19/15
Pace Project No.., 92272649
Sample: MW 03 Lab ID: 92272649005 Collected: 1011911514:00 Received: 10/21/15 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
62008 MSV Analytical Method: SM 6200B
Benzene
NO
ug/L
0.50
1
10125/15 04:22 71-43-2
Bromobenzene
NO
ug/L
0150
1
10/25115 04:22 108-86-1
Bromochloromethane
NO
ug/L
0.50
1
10/25/15 04,22 74-97-5
Bromadichloromethane
NO
ug/L
0,50
1
10/25/15 0412 75.27-4
Bromoform
NO
ug/L
0,50
1
10/25/15 04:22 75-25-2
Bromomethane
ND
ug/L
5,0
1
10/25/15 04:22 74.63-9
n-Butylbenzene
NO
ug/L
0.50
1
1012511504.22 104-51-8
sec-Butylbenzene
NO
ug/L
0.50
1
10/25/15 64.22 135-SM
tert-Butyibenzene
NO
ug/L
0.50
1
10125/15 04:22 98-06-6
Carbon tetrachloride
NO
ug/L
0,50
1
10/25115 04:22 56-23-5
Chlorobenzene
NO
uglL
0.50
1
10125115 04:22 108-90.7
Chloroethane
NO
ug/L
1.0
1
16125/1504:22 75-06-3
Chloroform
NO
ug/L
0,50
1
10/26115 04:22 67-66-3
Chloromethane
NO
ug/L
1.0
1
10/25116 04:22 74-87-3
2-Chlorololuene
NO
ug/L
0.50
1
10/25/15 (14:22 9549.8
4-Chlorotoluene
NO
ug/L
0.50
1
10125115 04:22 106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
1
10)25115 04:22 96-12.8
Dibromochloromelhene
NO
ug/L
0.50
1
10/25/15 04:22 124-48-1
1,2-Dibromoethane (EDS)
NO
ug/L
0.50
1
10125/1504:22 106.93-4
.Dibromomethane
NO
ug/L
0,50
1
10/25115 04:22 74-95-3
1.2-Dichlorobenzene
NO
ug/L
0.50
1
10/25/15 04:22 95.50-1
1,3-Dichlorobenzene
NO
ug/L
0.50
1
10125115 04:22 541-73-1
1,4-Dichlorobenzene
ND
ug/L
0,50
1
10125116 04:22 106-46-7
Dichlarodifluaromethane
ND
ug/L
04o
1-
10125/15 04,22 75.71.8
1,1-Dichlorcethane
ND
ug/L
0.50
1
10/25/15 04:22 75-34.3
1,2-Dichlaroethane
NO
ug/L
0.60
1
10/25115 04:22 107-06-2
1,1-Dlchloroelhene
NO
ug/L
0.50
1
10/25/15 04:22 75«35-4
cis-1,2-Dichloroethene
NO
'ug/L
0.50
1
10/25/15 04:22 156-59-2
trans-1,2-Dichioroethene
NO
ug/L
0,50
1
1WWI 604:22 156-60.6
1,2-Dichtoropropane
NO
ug/L
Q50
1
10125h504:22 78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
10/25115 04:22 142-28.9
2,2-Dichloropropane
NO
ug/L
0.50
1
10125/15 04-22 594-20-7
1,1-Dichloropropene
NO
ug/L
0.50
1
101251150422 563-58-6
cis•1,3-Dichloropropene
NO
ug/L.
0.50
1
10/25115 04:22 10061-01.5
trans-1,"Ichloropropene
NO
ug/L
0.60
1
10/2511504:22 10061.02-6
Dlisopropyl ether
NO
ug1L
0.50
1
10125/15 04,22 108-20-3
Ethylbenzene
NO
ug1L
0.50
1
10125/15 04:22 100-41-4
Hexachloro-1.3-buladiene
NO
uglL
2.0
1
10/26115 04:22 87-68-3
Isopropylbenzene (Cumene)
NO
ug/L
0.50
1
10125115 04:22 98-82.8
Methylene Chloride
NO
ug/L
2,0
1
10125/15 04:22 75-08-2
Methyl•tert-butyl ether
NO
ug/L
0.50
1
10/25115 04:22 1634.04.4
Naphthalene
NO
ug/L
2.0
1
10125/15 04:22 91-20-3
n-Propyibenzene
NO
ug/L
0.50
1
10/25115 04:22 103.65-1
Styrene
NO
ug/L
0.50
1
10125/15 04,22 100-42-5
1,1,1,2 Tetrachioroethane
NO
ug/L
0,50
1
10/26/16 04:22 630-20-6
1,1,2,2-Teirachloroethene
NO
ug/L
0.50
1
10/25/15 04:22, 79-34-5
Tetrachloroelhene
NO
ug1L
0.50
1
10126115 04:22 127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/10/2015 09:05 AM without the written consent of Pace Analytical Services, Int, Page 10 of 40

aceftlytical*
W*Wp eabbicam
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Pace Analytical Services, Inc.
98001GncelrAve. Suite100
Huntersvale, NC 26076
(704)87S-9092.
Sample: MW 03 Lab ID: 9227264900E Collected; 1011911514:00 Received: 10121/15 08;00 Matrix: Water
Parameters Results Units Report Limit' DF ' Prepared Analyzed CAS No.. Qual
62009 MSV Analytical Method, SM 6200B
Toluene
1,2,3-Trichlorobenzene
1,2,4-Tdchlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichlomethane: ,
Tdchlaroethene
Trichlorofluoromethane
1,2,3-Trichioropropane
1,2,4-Trimethylbenzene
1,3, 5-Trimethylbe nzene
Vinyl chloride
mBp-Xylene
o-Xylene
Surrogates
1,2-Dichloroelhane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
ND
ug1L
0.50
1
10/25/15 04:22 108-88-3
ND
ug/L
2.0
1
10125/15 04,22 87-61.6
NO
ugll.
2,0
1
10125/15 04:22 120.82.1
NO
ug/L
0.50
f
10/25115 041,22 71-56-6
ND
uglL
0.50
1
10125/15 04:22 79-00-5
NO
fig/L
0,50
1
10125115 041.22 79-01-6
ND
ug/L
1a0
1
1012511504:22 75.69-4
NO
ug/L
0.60
1
10/29/15 04:22 96di8.4
NO
ug/L
0150
1
10125115 04:22 95-63.6
NO
ug1L
0.50
1
10125115 04.22 108.67-8
NO
ug/L •
110
1
' 1012$/i 5 04:22 75.01.4
NO
ugIL
1.0
1
10/25/1504:22 179601-23-1
ND
ug/L
040
1
10/25/15 04:22 95-47.6
102
%
70-130
1
10/25115 04,22 17060-07-0
99
%
70-130
1
10125/15 04:22 460=00-4
101
%
70-130
1
101251i504:22'2037-26-5
Sample: 'MW 05 Lab ID: 92272649006 Collected: 10119115141,30 Received: 10/21/15 08:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua[ -
62009 MSV Analytical Method: SM 6200B
Benzene
NO
ug/L
0,50 •
1
10l25l1504,39 71-43-2
Bromobenzene
NO
ug/L
0.50
1
10/25115 04,39 10&86-1
Bromochloromethane
ND
• ug1L
0.50
1
10125/15 04:39 74-97-5
Bromodichloromethane
NO
ugiL
0.50 .
1
10125/15 64:39 75-27-4
Bromoforril
NO
ug/L
0.50
.1
10/25115 04,39 75-25-2
Broniornethane
ND
ug/L
5.0
1
10/25/15 04,39 74.83-9
n-Butylbenzene
ND
ug/L
0.50
1
1o/25/1504:39 104.51-8
sec-Butylbenzene
ND
uglL
0.50
1
10/25/15 04:39 135-98-8
tart-Butylbenzene
ND
ug/L
0.50
1
10/25115 04:39 98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
10125/15 04.39 56-23-5
Chlorobenzene
NO
ug1L
0.50
1
10125115 04:39 108-96-7
Chloroethane
ND
ug/L
1.0
1
10125116 04:39 75-00-3
Chloroform
ND
ug/L
0.50
1
10125/15 04:39 67-66-3
Chlommethane
.ND
ugli-
1.0
1
10/25115 OC39 74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
1012511504,39 9549.8
4-Chlorotoluene
ND
ug/L
0.50
1
10/25/15 04:39 106-43-4
1,2-Dibromo-3-chloroprnpane
NO
ug/L
1.0
1
10/25115 04:39 96-12.8
Dibromochloromethane
NO
u91L
0,50
1
101251'15 04119 124-48.1
1,2-Dibromoethane (EDB)
ND
ug1L
0.50
1
10125/15 04:39 10B-93-4
Dibromomethane
ND
uglL
0.50
1
10125115 04,39 74.95-3
1,2-Dichlorobenzene
NO
ug1L
0.50
1
10125/15 04,39 95-50-1
1,3-01chlorobenzene
NO
ug/L
0.50
1
1012511504,39 64173-1
1,4-Dichlorotienzene
ND
ug1L
0.50
1
10/25115 04:39 10646-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 11/1012015 09:05 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 40

aceAnalyhcal
wwwPocni isewn
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
Project; Sampling 10/19115
7
Pace Project No.: 92272649
Sample: MW 05 Lab I0: 92272649006 Collected: 1011911514:30 Received; 10/21/15 08:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6200E IVISV Analytical Method; SM 6200B
Dichlorodifluoromethane
ND
uglL
0.50
1
10125115 04,39 75-71-8
1,1-Dichioraethane
ND
uglL
0.50
1
1012511504:39 75-34-3
1,2-Dichtoroethane
NO
ug/L
0.50
1
10125/15 04:39 107.06.2
1,1-Dichlorcethene
NO
ug/L
0.50 •
1
10125/15 04,39 75-35.4
cis-1,2-Dichicroethene
NO
ugll-
0:50
1
1d/25115 04:39 156-59.2
trans-1.2-Dichloroethene
NO
ug/L
0.50
1
10125115 04:39 156.60.5
1,2-Dichloropropene
ND
ug/L
0150
1
10/25/15 04,39 78.87.5
1,3-Dichloropropane
ND
uglL
0.50
1
10125115 04:39 142-28.9
2,2-Dichloropropane
NO
ug/L
0.50
1
10125115 04'39 594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
10125115 04:39 563-58.6
cis-1,3-Dichioropropene
ND
ug/L
0.50 .
1
10125115 04:39 10061.01.5
trans-1,3-Dichioropropene
ND
ug/L
0.50
1
10/25/15 04;39-10061-02-6
Dflsopropyl ether
ND
ug/L
0.50
1
10/25/15 0429 108-20-3
Ethylbenzene
NO
ug/L
0.50
1
10125/15 04:39 160-414
Hexachloro-1,3-buladiene
ND
ug1L
2.0
1
10/2511504:39 87-68-3
Isopropylbenzene (Cumene)
ND
uglL
0.50
1
10/26115 04,39 98-82-8
Methylene Chloride
ND
ug/L
2.0
1
1101251150439 75.09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
10125/15 04:39 163 -044
Naphthalene
ND
ug/L
2.0
1
10/25/15 04:39 91-20-3
n-Propylbenzene
ND
ug/L
0,50
1
10125/15 04:39 103-65-1
Styrene
NO
uglL
0.50
•1
10/25/15 04:39 100-42-5
1,1,1,2-Telrachloroethane
ND
ug/L
0.50
1
10/2511504,39 630-20-6
1,1,2,2Tetrachlorcethane
ND
ug/L
0,50
1
1012611604:39 79-34-5
Tetrachtoroelhene
ND
ug/L
0.50
1
10125115 DC39 127.18-4
Toluene
ND
ug/L
also
1
10125115 04:39 108.88-3
.1,2,3-Tdchlorobenzene
ND
ug/L
2.0
1
1012511504,39 87-61.6
1,2,4-Tdchtarobenzene
ND
ug1L
2.0
1
10125115 04:39 126-82-1
1,1,1-Tdchloroethane
ND
ug1L
0.50
1
10/26115 04:39 71-55-6
1,1,2-Tdchloroethane
ND
ug/L
0.50
1
10126/16 0439 19-00-5
Trichloroethene
ND
ug/L
0.50
1
10/25/15 04,,39 79-01-6
Tdchlorofluoromethane
ND
ug/L
1.0
1
10125/15 04,39 75-69-4
1,2,3-Trichlompropane
NO
ug/L
0.50
1
1012511504,39 96-18-4 .
1,2,4-Tdmethylbenzene
ND
uglL
0.50
1
10125115 04:39 95-63.6
1,3,5-Tdmethylbenzene
ND
uglL
0.50
1
10125115 04:39 108.67.8
Vinyl chloride
ND
ug/L
1.0
1
10/25115 ,04:39 75.01-4
m&p-Xylene
ND
uglL
1.0
1
10125115 04:39 179601-23-1
o-Xylene
ND
uglL
0,50
1
10125/15 04:39 95-47-6
Surrogates
1,2-Olchloroethane-d4 (S)
102
%
70-130
1
10125/15 04:39 17060=07.0
4-Bromofluorobenzene (S)
99
70-130'
1
10126/15 04,39 460.00.4
Toluene -dB (S)
100
%
70-130
1
10125115 04:39 2037-26.5
REPORT OF LABORATORY ANALYSIS
This report. shell not be reproduced, except in full,
Date: 1111012015 09:05 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 40

N
eAnalytica!'
November 10, 2015
Mr. Stephen Reavis
MCAS Cherry Point
Facilities Maintenance Depart
PSC Box 8006, LCU
Cherry Point, NC 28633
RE: Project: Sampling 10/19/15
Pace Project No.: 92272649
Dear Mr: Reavis:
Pace Analytical Services, Inc.
9900 1 lejncey Ave. Suita l0o
Huntersvale, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2015.
The results relate only to the,samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
C"'
Angela Baioni
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in toil,
without tiro written consent of Pace Analytical Services, In -
Pap 1 of 40

Pace Analytical Services, inc.
aceAnalyical a 9BQ0 Kinsey Ave: Suite 100
Hunt ersviUe,'NC 2807a
Nnax ptcefe� Co+rf t704)875-9092
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Project: Sampling 10/19/15
Pace Project No.: 92272649 '
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Wisconsin Certification*: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84•
West Virginia Certification #: 357
MrginiaNELAP Certification #: 460221
2225 Riverside, Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: ES7648 South Carolina Certification M 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Anatytical Services, Inc,. Page 2 or 40

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SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave..Suite 100
Huntensville, Nt6078
(7D4)675.9082
Project,
Sampling 10119115
i
Pace Project No.,
92272649
Analyses
Lab ID
Sample ID
Method
Analysts "
Reported
Laboratory,
92272649001
001 SLUDGE
EPA 8081
SIM
8
PAS14C
EPA 8151
LJM
3
PASI.O
EPA6010
CDF
13
PASt-A
EPA6010
CDF
7
PASI-A
EPA7470
SHi
1
PASI-A
EPA7471
SH1
.1
PASI-A
EPA 8270
BPJ
18
PASImC
'EPA826D
GAW
14
PASI-C
SM 254OG
KDF
1
PASI-C
ASTM D297"7
CLW
1
PASI-C
EPA 1010
TEP
1
PASI•A
EPA9045
MLS
1
PASI-A
SM 2710B
EWS
1
PASI-A
EPA 350,1
SER
1
PASI-A
EPA 351.2
SER
1
PASI•A
EPA 353.2
DMN
3
PASI•A
EPA 365.1
AES2
1
PASI•A
92272649002
001 SLUDGE
EPA200.7
CDF
3
PASI•A
EPA 601D
JMW
1
PASt•A .
SW-846 7.3.3.2
BMS
1
PASI-PA
SW 846 7.3A.2
PAS
1
PASWA
92272649003
MW 01
SM 6200E
CAH
63
PASI•C
92272649004
MW 02
SM 6200B
CAH
63
PASI•C
92272649005
MW 03
SM 6200B
CAH
63
PASI-C
92272649006
MW 05
SM 6200B
CAH
63
PASI•C
REPORT OF LABORATORY ANALYSIS
This report shall not.be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 40

aceAnalytical®
vdtw.pec Wh coel
ANALYTICAL RESULTS
Project; Sampling 10119/15
Pace Project No.: 92272649
Pace Analytical Services, Inc.
9aoo KinceyAve. Suite lo0
Huntersville, NC 28070
[phone]
Sample: 001 SLUDGE
Lab iD: 92272649001
Collected:' 10/1911513.00
- Received: 10121/15 08:00 Matrix; Solid
Results reported on a "dry weight" basis and are adjusted fdrpercent moisture, sample size and any dilutions.
Parameters
Results Units
Report Limit . OF
Prepared
-,Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
Analytical Method EPA 8081 Preparation Method; EPA 3510 -
Leachate Method/Date: EPA
1311;10/30/15 00:00
gamma-BHC (Undane)
NO Wit.
0.50 1
11/03115 09:20
1110311513:26 58.89-9
Chlordane (Technical)
NO ug/L
3.0 1
11/03/1509:20
1110311513:26 57-749
Endrin _
ND ug/L
0.50 1
111031150920
111031151326 72-20-8 .
Heptachlor epoxide
NO ug/L
0.50 1
11/03/15 09:20
1110311513:26 10247,57-3
Methoxychlor
ND ug/L
1000 1
11/03/15 09:20
11/03115 13:26 7243-5
Toxaphene
NO uglL
3.0 1
11/03/15 09,20
11/031151326 8001-352
Surrogates
Decachiorobiphenyl (S)
40 %
10-138 1
11/03115 0920
111031151326 2051-24.3 ,
Tstrachloro-m-xylene (S)
35 %
10-110 1
11/03115 09.20
1110311513.26 877-09-8
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
Date: 11110/2015 09:05 AM
Analytical Method: EPA 8151 Preparation Method: EPA 3510
NO mg/L 1110 1 10/30115 08:20 1013011615,41 94 75-7
ND mg/L 11.0 1 10/30/16 08:20 10130/1515:41 93 72-1
102 % 42.142 1 10130/15 01120 1013011515:41 19719 28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
30400
mglkg
9200
1
10/22115 20,30
10127/15 01:47 7429-90.5
NO
mglkg
920
1
1 Q/22115 20:30
10/27115 01,47 7440.38-2
ND
mglkg
92.0
1
10/22/15 20:30
10127/15 01,47 7440-4379 .
130000
mg/kg
9200
1
101=15 20:30
10/27116 01:47 7440.70-2
1700
mglkg
460
1
10QV15 20:30
10/27115 01:47 7440-50.8
NO
mglkg
460
1
10/22/15 20:30
10127/15 01 A7 7439.92-1
19000
mglkg
9200
1
10122/15 20.30
10127/15 01:47 7439.95-4
NO
mglkg
460
I
10/22115 20:30
10/27/15 01:47 7439.98.7
ND
mglkg
460
1
10122/15 20:30
10127/15 01:47 7440.02-0
ND
mglkg
460000
1
10122/15 20:30
10/27115 01:47 7440.09 7
ND
mglkg
920
1
101=15 20:30
10/27115 01A7 7782.49.2
ND
mglkg
460000
1
10122/15 20,30
10127/15 01:47 7440.23-5
1930
mgfkg
920
1
10122/15 20:30
10/27/15 01,47 7440.66-6
Analytical Method: EPA 6010 Preparation Method; EPA 3010
Leachate Method/Date: EPA 1311;10122115 05:10
ND
mg/L
0.050
1
10123115 02,30
10/23/1517:04 7440-38.2
ND
mgfL
0.25
1
10123115 02.30
10123/1517:04 7440.39.3
NO
mg/L
0,0050
1
10/23/15 02:30
1012311517,04 7440-43.9
NO
mg1L
0.025
1
10123/15 02.30
10123/1517:04 7440-47-3
NO
mgfL
0.025
1
10123115 02;30
1012311517.04 7439.92-1
NO
mg/L
0,10
1
10123115 0210
1012311517:04 7782-49-2
ND
mg/L
0,025
1
10123/15 62:30
1012311517.04 7440.22-4
Analytical Method: EPA7470 Preparation Method: EPA7470
Leachate Method/Date: EPA 1311,,10/22115 05:10
ND
mg/L
0.00020
1
1012311510:00
1012311513:41 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fulf,
without the written consent of Pace Analytical Services, inc-
Page 4 of 40

aceAnalyflcal
www.pece/abscarrr
ANALYTICAL RESULTS
Project: Sampling 10119/15
Pace Project No_: 92272649
Pace Analytical Services, Inc.
9800 Wncey Ave. Suite 100
Hunters_ ville. NC 28078
(704)8754092
Sample: 001 SLUDGE Lab 10: 92272649001 Collected; 1011911513:00 Received:.10121115 08:00 Matrix: Solid
Results reported one "dry we/ght" basis and are adjusted for percent moisture. sample size and any di►utlons.
Parameter's Results Units Report Limit DF 'Prepared Analyzed CAS No. 'dual
7471 Mercury Analytical Method: EPA 7471 Preparation Method, EPA 7471
Mercury
8270 MSSV TCLP Sep Funnel
1.4-Dichlorobenzene
2,4-Dinitrototuene
Hexachloro-1,3-butadiene
Hexactllorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachtorophenol
Pyridine
2,4,5-Tdchlorophenol
2,4,6-Trichiorophenol
surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyi-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenal (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1.4-Dlchlorobenzene
1,2-Dichloroethane
1,1-Dichlor6ethane
Tetrachloroethene
Tdchloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-BromoBuorobenzene (S)
254OG Total Percent Solids
Total Solids
ND mg/kg 5,2 1 10126/151120 101271151152 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311 ; 10130/15 00:00
ND
ug/L
50.0.
1
1110211610.00
11103/1514:58
10646-7
ND
uglL
solo
1
1110211510:06
1110311514.58
121-14-2
ND
ug/L
SOD
1
1110211510,00
1110311514.58
87-68-3
ND
uglL
50.0
1
1110211510:00
11/0311514:58
118-74-1
ND
ugfL
50.0
1
1110211510.00
1110311514;58
67 72-1
ND
uglL
50-0
1
11/02)1510:00
11103/1514,58
95-48-7
ND
ug/L
50.0
1
11/02/15 %00
11/03/15 14:58
ND
ug/L
50,0
1
11/0211510:00
11103/1514*58
98-95-3
ND
uglL
100
1
11102h510.00
11/0311514,58
87-86-5
ND
ug1L
50.0
1
1110211510:00
1110311614:58
110-86-1
ND
ug1L
50M
1
1110211510:00
11/0311514.58
95-954
ND
ugli-
50.0
1
11102/1516:00
11/0311514:58
88-OB-2
18
%
12-102
1
11/0211510:00
11/0311514,58
4185.60.0
22
%
13-107
1
1110211510.00
11 /03115 14:58
321.60.8
56
%
21-132
1
11102/15 10:00
11/03115 14:58
1718-51.0
9
%
10-110
1
1110211610:00
1110311514:58
13127-88-3 SO
12
%
10-110
1
11102115 1 D.00
11/0311514:58
367-12-4
50
%
27-108
1
11102/15 10,00
11103/15 14Z8
118-79-6
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311,,10/26115 11,12
ND
4L
°1O0
20
10/31115 08;56 7143.2
ND
uglL
200
20
10131h 5 08:56 78.93.3
ND
uglL
100
20
10/31/15 0B:56 55.23.5
ND
uglL
100
20
10/31115 08:56 108-96-7
ND
ug/L
100
20 .
10/31/15 08,56 67-66-3
ND
ug/L
100
20
10131115 08:56 10648-7
ND
ug1L
100
20
10131/1508:56 107-06-2
ND
u91L
100
20
10/31/15 08:56 75-354
ND
ug/L
100
20
10131/15 08:56 127-18.4
ND
ug/L
100
20
10131/15 08:56, 79-01-6
ND
ug/L
100
20
/0131/15 08:56 75-014
124
%
70-130
20
10/31/15 08,56 17060,07-0
98
56
67-135
20
10/31/15 08:56 2037-26.5
105
,ear
70-130
20
10131/15 08:56 460-00-4
Analytical Method, SM 254OG
0.090 % 0.000010 1
REPORT OF LABORATORY ANALYSIS
1012111516:53
This report shall not be•reproduced, except In full,
Date,,1111012015 09:05 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 40

acemal Cal e
www.pacasbaconr
ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Pace Analytical Services, Inc.
9800, Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-092
Sample: 001 SLUDGE
Lab ID: 92272649001 Collected. 10/19/151&00
Received: 10121/15 08M, Matrix, Solid
Results reported on a "dry weight" basis and ate adjusted forpereent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No, Qual
Percent Moisture
Analytical Method, ASTM 02974-87
Percent Moisture
99.9 96
0.10
1
10/2211512:53
1010 Flashpoint,Closed Cup
Analytical Method. EPA 1010
Flashpoint
>200 deg F
70.0
1
1013011511,30
9045 pH Solt
Analytical Method: EPA 9045
pH at 25 Degrees C
7.2 Sid, Units
0.10
1
10122/1511 AO H1
Plant Available Nitrogen
Analytical Method; SM 2710B
Plant Available Nitrogen
122000 mglkg
0.12
1
1110511517:20 N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
135000 m09
10200
1
10/26115 01,31 7664-41-7
361.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 3512
Nitrogen. Kjeldahl, Total
217000 mglkg
55200
1
11103/15 02:36 7727-37.9
353.2 Nitrogen, N021NO3
Analytical Method,, EPA 3512
Nitrogen, Nitrate
26000 mglkg
2180
1
11/03115 10-31
Nitrogen, Nitrite
4160 mgtkg
1090
1
1110311510:31
Nitrogen, NO2 plus NO3
30100 mglkg
2180
1
11103115. 10.31
365A Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
142000 mg/kg
' 4150
2
10128/1512:19 7723-14.0
Sample: 001 SLUDGE
Lab tD: 92272649002 Collected. 1011911513,00
Received; 10121115 08:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed .
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 2001
Calcium
189000 ug/L 1000
1
11/0511513,05
1110611516:41
7440.70.2
Magnesium
24200 ug1L 1000
1
1110511511,05
1110611515,41
7439-95-4
Sodium
117000 ug1L 50000
1
1110511513:05
1110611515:41
7440-23-6
Sodium Adsorption Ratio, SAR
Analytical Method: EPA 6010
Sodium Adsorption Ratio
2.1 meq/L
1
1110911517,02
N2
733C Reactive Cyanide
Analytical Method: SW 846 7.3.3.2
Cyanide, Reactive
ND mg/L 0.010
1
10/22/15 22:30
7345 Reactive Sulfide
Analytical_ Method: SW-846 7.3,42
Sulfide, Reactive
ND mgll - 1,0
1
1012211518,30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full;
Dale: 11/1012015 09:05 AM without the written consent of Pace Analytical Services, Inc..
Page 6 of 40

UNITED STATES MARINE CORPS
MARINE CORPS AIR STATION
POSTAL SERVICE CENTER E003
CHERRY POINT, NORTH CAROLINA 2ES33.OM
IN REPLY REFER TO:
5090/07109
LN
November 16, 2015
North Carolina Department of Environment
and Natural Resources
Division of Water Quality
Information Processing Center
1617 Mail Service Center
Raleigh, NC 27699-1617
Subj: TRIENNIAL GROUNDWATER MONITORING
In accordance with the groundwater monitoring and reporting
requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for
Land Application of Wastewater Residuals, enclosed are the original
and one copy of the GW-59-A report and the four GW-59 reports (one
each for monitoring wells 1, 2, 3, and 5) for the triennial
reporting for October 2015.
Should you have any questions, please contact Mr. Timothy
Lawrence, PE of the Environmental Affairs Department at your
earliest convenience at [phone].
Sincerely,
G. W. 0 \
Envir m nt 1 Affairs Officer
By direct n of the
Commanding Officer
Enclosure: (1)
GW-59-A
(2)
GW-59 for MW-1
(3)
GW-59 for MW-2
(4)
GW-59 for MW-3
(5)
GW-59 for MW-5
(6)
Lab Report

GW-59A COMPLIANCE REPORT FORM Permit # WQ0001489
(Submit one each monitoring period with Gli -59 jorms.)
Enter date monitoring results were due 11/( 30/151 Will this monitoring report (GW-59 and GW-59A) be submitted after
YES
NO
I the
established due dale?
X
2
Was any required information missing on the GW-59 report forms?
YES
NO
X
IF
the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems
encountered in obtaining the required information.
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
3
identification plate, area overgrown, etc.)? If the annreris "Yes", contact the Regional CrIcejorguidance.
N
4
Are any monitored constituents equal to or above the established standards?
YES
NO
t
If the answer to question 4 is "NO", skip to section 8
If the answer to question 4 is "YES" list the affected wells individually with constitucnt(s) and concentration(s) exceeding standards in the
space provided below•
MW-2 TOTAL AN1NiONiA (NI13) 2.4 mp/L
SIW-5 TOTAL AMMONIA (NI13) 2.1 mg/L
For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s)
YES
NO
5
in the same well(s) in the last two years?
a
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s)
reported, and sample collection date for each occurrence (for the last two years).
NIW-2: Oct. 2013 NI13 3.0, Feb. 2014 N113 3.0, Oct. 2014 NIB 1.7, Feb. 2015 N113 1.7
MW-5: Feb. 2014 N113 3.2, June 2014 NI13 2.7, Oct. 2014 NIM 3.0, Feb. 2015 N113 2.7
G
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
N
If the answer is "YES", a groundwater quality problem may be occurring, CONTACT THE REGIONAL OFFICE IMMEDIATELY
FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office.
Is the permiltee implementing previously approved actions required by the Division involving this groundwater quality
YES
NO
7
problem?
X
If the answer to question 7 is "YES", describe those actions in the space provided below
If the answer to question 7 is "NO", contact the Regional Mee within 90 days: no evaluation may be required to determine the
Impact the waste disposal system is having at the review and compliance boundaries surroundine this facility. Failure to do so may
subieef the nermitlee to a Notice of Violation- rines. and/or Penalties
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with
8
GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
rwwiedge that the tl o've inforn"on +ryas evaluated and the information submitted to this report {Complies
Thereby ackReport
GW-59A) is true and complete to the best of my knowledge. r.... ,. „ s
Patricia T. Davis, Utility Systems Operator Supervisor
Signature of Permittee (or Authorized Agent) Date 11IM20I5

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Name: MCAS Cherry Point
Name (if different),. _
Address: MCAS Chagy Point, NC
Please Print Clearly or Type
County -
act Person: Patricia T. Davis Telephone #: [phone]
Localion/Site Name: Site 21, MCAS Cheffy Point No.of Wells to be Sampled:
im
SAMPLING INFORMATION
WELL ID NUMBER (From Permit): MW-1
Well Depth 26.66 it
Depth to Water Level 82546: 1 fL bek w measuring point
Measuring Pant is 1.33 ft. above land surface
Volume of water pumped/bailed before sampling 5 Gal,
Samotes for metals were collected unfiltered i ) YES [,—j NO
61a,tn si%
R/►t.FiG iW2T889.48'17 PttOfdE:t91ti733.3221 ,
PERMIT Number: Expiration Date:
Non -Discharge UIC
NPDES WQ0001489 Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon 0 Remediation: infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor [I Land Application of Sludge
1 ❑ Water Source Heat Pump ❑ other. -
Date Sample Collected: 10119/2015 FIELD ANALYSIS:
Well Diameter. 2 pH D0400 6.1 units Temp 00010: 21 °C
Screened Interval: -0.17 It. to -15.2 fL Spec. Cond. DW94: 190 pMhos
Re,ative M, R Elevation, 10.78 Odor 00085- none
Appearance: clear
and field acidified n YES ❑ NO _ _
DL/RK 1 LR r �17rvRrne� wn
'e sample analyzed: 10119/2015 Laboratory Name: MCAS Cherry Point I Pace Analytical Certification Number. 2011
RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Coliform,' MF Fecal 31616 <1
1i00mL
Nitrate (NO3) as N 00620 <0.1
mg/L
Coliform: MF Total 31504
1100mL
Phosphorus: Total as P 00665
mg/L
(Now Use MPN meewd ro(Ng* Wrb4 samples)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300 56
mg/L
A) -Aluminum 01105
mglL
pH (Lab) 00403 6.1
units
Ba - Barium 01007
pg/L
TOC 00680
mg/L
Ca - Calcium 00916
mg[ -
Chloride 00940 12
mg/L
Cd -Cadmium: Total 01027
pg/L
Arsenic 01002
pg/L
Chromium: Total 01034
pg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mglL
Phenol 32730
pg/L
Fe - Iron 01045
Pg/L
Sulfate D0945
mg1L
Hg - Mercury 71900
pg/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg1L
Total Ammonia 00610 <0.1
mg1L
Mg - Magnesium 00927
mg/L
(Ammus N&Ktn, NHs as N; Annnor" NArvgen. Total)
Mn - Manganese 01055
p9/-
TKN as N 00625
mg/L
Ni - Nickel 01067
Pg/L
Pb - Lead 01051 pg/L
Zn - Zinc 01092 mg1L
P:I711111111
at
of
ding,
here: 1-1
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? F±] Yes(1) ❑ No (0)
VOC 78732 Method# 6200B
Method#
Method#
Method#
vnr- 13-1-11eL
For Remediation Systems Only (Attach Lab Reports): innuent total vu;ls: 1— •mow -- - - -
Patricia T. Davis - Utility Systems Operator 1116/2015
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev, 212010

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATI N Please Print Clearty or
Facility Name: MCAS Cherry Point
Permit Name (if different):
Facilitv Address: MCAS Cherry Point, NC 28533-0006
County: Craven
act Person: Patricia T. Davis Telephone M 252-466-4599
Location/Site Name: Site 21. MCAS Cherry Point No of Wells to be Sampled: 1
L ID NUMBER (From Permit): MW-2
Depth 26.58 fL ^
i to Water Level 82546. 7 ft below measuring point
wring Pant is 118 ft. above land surface
ne of water pumpedibailed before sampling: 5 Gal.
HONE; (li 903,41M .
n-Discharge UIC
DES W00001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
[] Lagoon ❑ Remediation: Infiltration Gallery
Spray Field Remediation:
Rotary Distributor Land Application of Sludge
Water Source Heat Pump ❑ Other.
Date Sample Collected: 10119/2015
Well Diameter. 2 _
Screened Interval: -1 03 ft, to -11 fi.
Relative M P. Elevation 148
and
FIELD ANALYSIS: s DRY.
pH 00400 5,85 units .Temp 00010: 19 C
Spec. Cond, 0 94: 897 pMhos
OdorOD085 none ^•�;
Appearance. clear
BORATORY INFORMATION
e sam le analyzed 10/1912015 Laboratory Name: MCAS Cherry Point 1 Pace Analytical Certification Number. 201 137706
P
: AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 0Qfi15mg1L
Coliform: MF Fecal 31616 <1
Nitrate (NO3) as N 00620 110:1
mg/L
�/100mL
Coliform: MF Total 31504
1100mL
Phosphorus: Total as P 00665m91L
mg/L
(Nola Use UPN mairod far hoohb k*W simples)
Orthophosphate 70507
Dissolved Solids: Total 70300 308
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 585
units
Sa - Barium 01007
pg1L
TOC 00680
mg1L
Ca - Calcium 00916
mg/6
Chloride 00940 14
mg/L
Cd - Cadmium: Total 01027
pg/L
Arsenic 01002
pg1L
Chromium: Total 01034pg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg1L
Phenol 32730tig/L
Fe - Iron 01045
ug1L
Sulfate 00945
mg/L
Hg - Mercury 71900
ug8-
Specific Conductance 00095
pMhos
K - Potassium 00937.
mg/L
mg/L
Total Ammonia 00610 2.4
mg1L
Mg - Magnesium 00927 _
(AffvTw4 N&ccon; NH, at N; Amn o u Nevgan, Total)
Mn - Manganese 01055
Ng/L
TKN as N 00625�
^mg1L
Ni - Nickel 01067_
µg1L
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
Pb - Lead 01051 Vg/L
Zn - Zinc 01092 mg1L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? {Q Yes(1) 0 No (0)
VOC 78732 Method# 6200B
Method#
Method#
Method#
Effluent Total VOCs: VOC Removale%
a xg,_, 11/6/2015
Patricia T. DaVis - Utility Systems Operator Permittee (or AUthorized Agent) Name and Title - Please print or type Signature of Pem}ittee (or Authorized Agent) (Date)
GW-59 Rev.2/2010

ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
r+u 1= rarcnnuATtnrj Please Print ClearlYtw
Facility Name: MCAS Cherri Point
Permit Name (if different)_
Facility Address: MCAS CheiTy Point. NC
County'
SUBMIT FORM ON YELLOW PAPER ONLY
act Person. Patricia T. Davis Telephone #: 252-466A599
Location/Site Name: Site 21 MCAS Cherry Point No of Wells to be Sampled
WELL 10 NUMBER (From Permit): MW-3
Well Depth 25.58 fL
Depth to Water Level 82546 0 fL below measuring point
Measuring Point is 1.46 R above land surface
Volume of water pumped/balled before sampling: 5 Gal:
Les for metal
in -Discharge UIC
DES WQ0001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field Remediation:
0 Rotary Distributor Q Land Application of Sludge
❑ Water Source !-Feat Pump ❑ Other.
Date Sample Collected: 10119/2015
Well Diameter. 2
Screened Interval: -111 ft. to -21,7 ft.
Relative M.P Elevation: 3.1
NO and field acidified � I YES L[ NO
FIELD ANALYSIS: �C DRY
—
PH pH 00400 6.1 us Temp 00010: 20
Spec. Cond. 00094' 201 UMW
Odor00085: none ^•�•
Appearance: turbid "•
ORATORY INFORMATION
sampIe analyzed 10/19/2015 Laboratory Name: MCAS CherryPoint / Pace Analytical
Certification Number. 201 / 37706
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Conform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 2.5
mgn-
Coliform: MF Total 31504
1100mL
Phosphorus: Total as P 00665
mg1L
{Nate- Use MPN merood for hq tvy art W samples}
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300 144
mg/L
At - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
µg/L
_6.1
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 6.9
mg1L
Cd - Cadmium: Total 01027
µg/L
Arsenic 01002µg'L
Chromium: Total 01034
µgn-
Grease and Oils 00552
mg/L
Cy - Copper 01042
mg/L
Phenol 32730
µg/L
Fe - Iron 01045
µg/L
Sulfate 00945
mg/L
Hg - Mercury 71900
Vg/L
Specific Conductance 00095
µMhos
K - Potassium 00937
UVIL
Total Ammonia 00610 <1 0
mg1L
Mg - Magnesium 00927
mg/L
jAmmarm NeWen. NH, as N, Amm xue NMwen, iota9
Mn - Manganese 01055
µg/L
TKN as N 00625
mg1L
Ni - Nickel 01067
µg/L
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC1MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ( Yes(1) ❑ No (0)
VOC 78732 Method# 6200E
Method#
Method#
Method#
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: EffluentTotal VOCS: VOC Removal----^—
a-; 11/6/2015
Patricia T, Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev.212010

SUBMIT FORM ON YELLOW PAPER ONLY
NDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
Name: MCAS
Name (if different};
Address: MCAS
Please Print Clearly or Type
NC 28533-0006
County: Craven
act Person. Patricia T. Davis Telephone M 2524664599
Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled:
NG UNIT
n-Discharge UIC
DES W00001489 Other
PE OF PERMITTED OPERATION BEING MONITORED
Lagoon ❑ Remedlation: Infiltration Gallery
Spray Field Remedlation:
Rotary Distributor E-] Land Application of Sludge
Water Source Heat Pump ❑ Other.
IPLING INFORMATION 10/19t2015 FIELD ANALYSIS: WAS
6.2
L ID NUMBER (From Permit): MW-5 Date Sample Collected: zC DRY
Depth 13 fL Well Diameter 2 pH 00400 6.2 units Temp 00010: 24 m o.
h to Water Level 82546. 6.5 it below measuring point Screened Interval, 3 it to 13 fL Spec. Cond. 00094: 544 NMhos M1 m pe<^ a
wring Point is 3 it above land surface Relative M.P Elevabon; 12 Odor 00085 none -�
ne of water pumped/bailed before sampling: 5 Gal.
Appearance- clear
:les for metals were collected unfiltered YES NO and field aGdfied YES NO
ORATORY INFORMATION
sample analyzed: 10/19/2015 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201 / 37706
tAMETERS NOTE: Values should mnect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
m9n-
Coliform: MF Fecal 31616 <1
Nitrate (NO3) as N 00620 <0.1
mg/L
Coliform: MF Total 31504
_/104mL
/100mL
Phosphorus: Total as P 00665mg/L
(Note: Use MPN method for NNW Y tAW WrOes)
Orthophosphate 70507
mg/L
Dissolved Solids: Total 70300 192
mglL
Al - Aluminum 01105
mg[ -
pH (Lab) 00403 6.2
units
Ba - Barium 01007
µg/L
TOC 00680
mglL
Ca - Calcium 00916
mg/L
Chloride00940 12
mg/L
Cd -Cadmium'. Total 01027
µg/L
Arsenic 01002
µg/L
Chromium: Total 01034
µg/L
Grease and Oils 00552
mg/L
Cy - Copper 01042
mgfL
Phenol 32730
µg/L
Fe - Iron 01045
µg/L
Sulfate D0945
mg/L
Hg - Mercury 71900µg/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610 2.1
mg/L
Mg - Magnesium 00927mg/L
(Anvronia wwQen; NH3 as N;Arwona N*tyon, T4rsa
Mn - Manganese 01055
µgn-
TKN as N 00625
mg/L
N1- Nickel 01067
u9n-
Pb - Lead 01051 µg/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? 0 Yes(1) ❑ No (0)
VOC 78732 Method# 6200B
Method#
Method# _
Method#
For RemediatIon Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal%
1116/2015
Patricia T. Davis - Utility Systems Operator
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59 Rev, 2/2010

aceAnaliftal.
NmrpacW%bic=
November 10, 2015
Mr. Stephen Reavis
MCAS Cherry Point
l=acilities-Maintenance Depart
PSC Box 8006, LCU -
Cherry Point, NC 28533
RE: Project: Sampling 10/19115,
Pace Project No.: 92272649
Pace Analytical Services, Inc.
9e0o lGricey Ave. Suite 100
Hunterawle, NC 28078
(704WS.9092
Dear -Mr. Reavis:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2015.
The results relate only to the samples included in this report. Results reported herein .conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baloni
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 40

aceAnalyilcal'
W#Wpabbm
Project: Sampling 10/19/15
Pace Project No.: 92272649
Pennsylvania Certification IDs
Georgia Certification W. C040
1638 Roseylown Rd Suites 2,3&4, Greensburg, PA 15601
L-A-B DOD-ELAP Accreditation #: L2417
Alabama Certification #: 41690
Arizona Certification #: AZO734
Arkansas Certification
California Certification V. 04222CA
Colorado Certification
Connecticut Certification#: PH-0694
Delaware Certification
Florida/TNI Certification #: E87683
Georgia Certification M C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification M 391
Kansas/TNI Certification #: E-10358
Kentucky Certification #: 90133
Louisiana DHHITNI Certification M LA140008
Louisiana DEQ/rNI Certification M 4086
Maine Certification #: PA00091
Maryland Certification #: 308
Massachusetts Certification M M-PA1467
Michtgan/PADEP Certification
Missouri Certification #: 236
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification P E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification M FL NELAC Reciprocity
Louisiana Environmental Certificate M 05007
Maryland Certification:#346
Michigan Certificallon #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Carl 0074
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification M 12
South Carolina Certification #: 99008001
Pace Analytical Services, Inc.•
9800 KinceyAve. Suite 100
Hunterriville. NC 28078
[phone]
CERTIFICATIONS
Montana Certification #: Cert.0082 .
Nebraska Certification #: NE;.05-29-14
Nevada Certification # PA014572015-1
New Hampshire/rNi Certification #. 2976
New Jersey/TNI Certification#: PA051
New Mexico Certification fk PA01457
New York/TNI Certification #:.10888
North Carolina Certification #. 42706
North Dakota Certification #. R-190
Oregon/TNI Certification #: PA200D02
PennsylvanialTNI Certification M 65-00282
Puerto Rico Certification M PA01457
.Rhode Island Certification #; 65-00282
South Dakota Certification
Tennessee Certification #: TN2867
Texas/TNI Certification #: T104704188-14.-8
UtahffNI Certification #: PA014572015.5
USDA Soil Permit #: P330-14.00213
Vermont Dept. of Health: ID# VT-0282
Virgin Island/PADEP Certification
VirginialVELAP Certification M 460198
Washington Certification #: C868
West Virginia DEP Certification M 143
West Virginia DHHR Certification #: 9964C
Wisconsin Certification
Wyoming Certification #: 8TMS-L
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification.#, 2958
New York Certification #:11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #:12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification M 6M0547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TNO2974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification M 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Flodda/NELAP Certification M E87627
Kentucky UST Certification #: 84
Wiest Virginia Certification #: 357
Virginia1VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification M 40
Flortda/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M•NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification M 37712 VirginiaNELAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in futi,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 40

aceAnalytical
xwwpacolshicam .
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9600 Kincey Ave, Suite 100
Huntersville, NC 28078
(704)B75-9092
Project: Sampling 10/19/15
Pace Project No: 92272649
Sample: MW 01 Lab ID: 92272649003 Collected: 10/1911513.00 Received: 10121/15 08:00 Matrix: Water
Parameters Results Units Report Limit Df Prepared Analyzed, , CAS No. Qual
6200E MSV Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
10125115 03:49 71-43-2
Brnmobenzene
ND
ug/L
0.51)
1
10/25/15 03:49 108-86-1
Bromachtoromethane
ND
ug/L
0.50
1
10/25/15 03,49 7"74 .
Bromodichloromethane
ND
ugfL
0.50
1
10125/15 03A9 75-27.4
Bromoform
ND
ug/L
0.50
1
10/25/15 03,49 75-25-2
Bromorhethane
ND
ug/L
5.0
1
10125/15 03A9 74-83.9
n-Butylbenzene
ND
ug/L
0.60'
1
10125/15 03.49 104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
10125/15 03A9 135-98-8
tert-Butylbeluene
ND
uglL
0.50
1
10/25/15 03A9 98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
10/25/15 03:49 56-23.5
Chlorobenzene
ND
ug1L
0.50
1
10/25115 0149 108-90.7
Chloroethane
ND
ug/L
1.0
1
1012511503,,49 75-00.3
Chloroform
6.4
ug/L
0.50
1
10125/15 03:49 67.66-3
Chloromethane
ND
ug/L
1.0
1
10/25/15 03.49 74o87.3
2-Chlorotoluene
ND
ug/L
0.50•
1
10/25/15 03A9 95-49-8
4-Chlorotoluene
ND
uglL
0.50
1
10/25/15 03:49 106=43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0 .
1
10125115 03:49 96-12.8
Dibromochloromethane
ND
ug1L
0.50
1
10125/15 03:49 124-48-1
1.2-Dibromoethane (EDB)
ND
ug/L
0.50
1
10/25115 03:49 106-93-4
Dibromomethane
ND
ug/L
0.50
1
10125115 03A9 74-95-3
1,2-Dichlorobenzene
ND
ug1L
0.50
1
10/25/15 03:49 95.50.1
1,3-Dlchlorobenzene
ND
ug/L
0.50
1
10/25115 03A9 541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
10125115 03:49 106-46-7
Dichlorodifluaromethane
ND
ugfL
0,50
1
10/25115 03.49 75-71-8
1,1-Dichto'roethane
ND
ug1L
0.50
1
10/2511503:49 75-34-3
1,2-Dichioroethane
ND
ug1L
0.50
1
10/2511503*49 107-06-2
1,1-Dichlomethene
ND
ug/L
U0
1
10/25/1503:49 75-36.4
cis-1,2-Dlchloroethene
ND
ug/L
0,50
1
16/25115 03A9 156 59-2
trans-1,2-Dichlomethene
ND
uglL
0.50
1
10/25115 03:49 156-60-5
1,2-Dichloropropane
ND
ug1L
0.50
1
10/26115 03:49 78-87-5
1;3-Dichloropropane
ND
ug/L
0.50
1
10125115 03A9 142-28-9
2,2-Dichloropropane
ND
uglL
0.50
1
10125/15 03:49 594-20.7
1,1-Dichtoropropene
ND
ug/L
0.50
1
10125115 03A9 563-58.6
cis-1,3-Dlchloropropene
ND
ug/L
0.50
1
10125/15 63:40 10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
1
10125115 03A9 10061-02-6
biisopropyl ether
ND
ug/l.
0,60
1
10/25115 03:49 108.26-3
Ethylbenzene
ND
ug/L
0.50
1
10/25115 03:49 100.41-4
Hexa6hloro-1.3-butadiene
ND
ug/L
2.0
1
10/25115 03.49 87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
10125115 03:49 98-82-8
Methylene Chloride
ND
ug/L
2.0
1
10125/15 03:49 75.09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
10125/15 03:49 1634.04.4
Naphthalene
ND
ttg1L
2.0
1
10/25/16 03,49 91-20.3
n-Propylbenzene
ND
ug/L
0.50
- 1
10125115 03:49 103-65-1
Styrene
ND
ug/L
0.50
1
10125/15 03:49 100-42-5
1,1,1,2-Teirachioroethane
ND
ug/L
0.50
1.
10125/15 03:49 630-20-6
1,1,2;2-Tetrachtoroethene
ND
ug/L
0.50
1
10125/15 03,49 79-34.5
Tetrachloroethene
ND
ug1L
0.50
1
10125/15 0149 127-18.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11110/2015 09:05 AM without the written consent of Pace Analytical Services, lnc.. Page 7 of 40

aceAnalytical*
wwrxpaoslabs.-
,ANALYTICAL RESULTS
Pace Analytical Services; Inc.
9800 KinceyAve_ Suite 100
Nuntersville, NC 28076
(704}a75-9092
-Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: MW 01 Lab ID: 92272649003 Collected: 1011911513:00 Received: 10121115 08:00 Matrix; Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No: Qua]
6200E MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
11,1-Trichl oroethane
1,1,2-Trichlomethane
Trichloroethene
Tdchioro0uoromethane
1,2,3-Tdchlo ropropane
1,2,4-Tdmethylhenzene
1,3,5-Tdmethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-BromoBuorobenzene (S)
Toluene-d6 (S)
Analytical Method: SM 6200B
NO
ug/L
0,50
1
10125/15 03.49 108-88-3
NO
uglL
2-0 •
1
10/25115 03:49 87-61-6
NO
ugiL
2.0
1
10/25/15 03:49 120-82-1
NO
uglL
0.50
1
104VI5 03A9 .71-55-6'
ND
ug/L
0150
1
10125/15 03.49 79.00-5
NO
ug/L
U0
1
10/25/15 03:49 79-01.6
NO
ug/L
to
1
10/25115 0149 75-69-4
NO
ug/L
0,50
1
10/25/15 03:49 96-18-4
NO
uglL
0.50
1
10125/15 03:49 95-63.6
NO
uglL
0.60
1
10125115 03,49 108-67-6
ND
ug/L
1,0
1
10125115 03:49 75-01-4
ND
ug/L
1,0
1
10125/1503:49 179601-23-1
NO
ug/L
0.50
1
10/25/15 03:49 95.47-6.
103
%
70-130
1
10125115 03,49 17060-07-0
97
9b
70-130
1
10/25115 03A9 460.00-4
100
%
70-130
1
10125/15 03:49 2037-26-5
Sample: MW 02 Lab ID: 92272649004 Collected: 10119/1513:00 Received: 10121/15 08:00 ' Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
6200E MSV Analytical Method: SM 6200B
Benzene
NO
ug/L
0.60
1
10/25/15 04:06 71-43-2
Bromobenzene
NO
ug/L
0.50
1
10/25115 04,06 108-86-1
Bromochloromethane
NO
ug/L
0.60
1
10/25/15 04:05 74-97 5
Bromodichloromeihane
NO
ug/L
0.50
'1
10/25115 04,06 75-27-4
Bromoform
ND
ug1L
0.50
1
10125/15 04:06 75-26-2
Bromomethene
NO
ug1L
5.0
1
10/25115 04,06 74-83-9
n-Butylbenzene
NO
ug/L
0.50
1
10125/15 04:06 104.51-8
sec-Butylbenzene
NO
uglL
0,50
1
10/25/15 006 135-98-8
tert-Butyibenzene
ND
uglL
0.50
1
10/25/16 04T5 98.06-6
Carbon tetrachloride
NO
ug/L
0.50
1
10125/15 04,06 56-23-5
Chlorobenzene
NO
ug/L
0.50
1
10/25/15 04:06 108-90 7
Chloroethane
NO
ug/I.
1.0
1
10/25/15 04,06 75-00-3
Chloroform
NO
uglL
0.50
1
10/25/15 04:06 67-66-3
Chloromethane
'ND
uglL
1.0
1
10/25/15 04,06 , 74-87.3
2-Chlorotoluene
ND
ug/L
0.50
1
10126/15 04:06 95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
10128/15 04;06 106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/L
1,0
1
10125/15 04:06 96-12-8
Dibromochloromethane
NO
ug/L
0.50
. 1
10125/15 04:06 124-48-1
1,2-Dibromoethane (EDB)
NO
uglL
0.50
1
10/25115 04:06 106-93-4
Dibromomethane
NO
ug/L
0.50
1
10/25115 04:06 74-95-3
1,2-Dichlorobenzene
NO
ug/L
0.50
1
1012511504:06 95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
10/25/15 04:06 541 73.1
1,4-Dichlorobenzene
NO
ug/L
0.50
1
10125/15 04,06 10646-7
REPORT OF LABORATORY ANALYSIS
This report shO not be reproduced, except in full;
Date; 1111012016 09,05 AM without the written consent of Pace Analytical Services, Inc... Page 8 of 40

lialooAnaljdcal'
rMMsptCahbs.conr .
'ANALYTICAL RESULTS
Project: Sampling 10/19/15
Pace Project No.: 92272649
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: MiN 02
Parameters
Lab ID: 92272649004 Collected. 1011911513:00 Received:
Results Units Report Limit DF Prepared
10/21/15 08:00 Matrix: Water
- Analyzed CAS No. Quaff
6200B MSV
Analytical Method: SM 6200B
Dichlorodifluoromethane
ND
ug/L
0.50
1
10/25/15 04:06 75+71.8
1,1-Dichloroethane
ND
ug/L'
also
1
10/25/15 04t06 75-34.3
1,2-Dichiomethane
ND
ug/L
0,50
1
10/25115 04:06 107-06-2
1,10chloroelhene
ND
ug/L
also
1
10/25/1504:06 75-35.4
cis-1,2-Dichloroethene
ND
ug/L
also
1
10125115 04:06 156.59.2
trans-1,2-Dichloroelhene
ND
ug/L
0.50
1
10125/15 04,06 156-613-5
1,2-Dichlompmpane
ND
ug/L
0.50
1
1012511504:06 78-87-5
1,3-Dichtoropropane
ND
ug/L
0.50
1
10/2511504,06 142-28.9
2,2-Dichloropropane
ND
ug/L
0.50
1
10/25115 04,06 594-20.7
1,1-Dichloropropene
ND
ug/L
0.50
1
10/25115 04:08 553-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
10126115 04:06 10061.01.5
trans-1,3-Dichlompropene
ND
ug/L
0,50
1
10125115 04:06 10061.02.6
Dilsopropyl ether
ND
ug/L
0.50
1
10125/15 04:06 108.20.3
Ethylbenzene
ND
ug/L
0,50
1
10125115 04:06 100.41.4
Hexachlora-1,3-butadiene
ND
ug/L
2.0
1
10125/15 04:06 87-68.3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
10/25/15 04:06 98-82.8
Methylene Chloride
ND
ug/L
2,0
1
10/25/15 04:06 75-09-2
Methyl-tert-butyl ether
ND
ug/L •
0.50
1
10125/15 04:06 1634-04-4
Naphthalene
ND
ug/L
2.0
1
10125115 04:06 91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
10125/15 04,06 103-65-1
Styrene
ND
ug1L
0.50
1
10125/15 04:06 100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
OM
1
10125/15 04,06 630-20-6
1,1,2,2 Tetrachlomethane
ND
ug/L
0.50
1
10125115 04:06 79-34-5
Tetrachloroethene
ND
ugiL
0.50
1
10/25115 04:06 127-18-4
Toluene
ND
ug1L
0;50
1
10125h5 04:06 108-88-3
1,2,3-Tdchlorobenzene
ND
ug1L
2.0
1
1012511504,06 87-61-6
1,2,4-Tdchtorobenzene
ND
ug/L
2,0
1
10125/15 04:06. 120-82.1
1,1,1-Trichloroethane
ND
uglL
0.50
1
1012611504,06 71-55-6
1,1,2-Tdchloroethane
ND
ug/L
0.50
1
10125115 04:06 79.00.5
Trichloroelhene
ND
ug/L
0.50
1
10/25/15 04:06 79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
1D/25115 04:06 75.69-4
1,2,3-Tdchloropropane
ND
ug/L
0;50
1
10125/1504:06 96-18-4
1,2,4-Tdmethylbenzene
ND
ug/L
0.50
1
1012511504,06 95.63.6
1,3,5-Tdmethylbenzene
ND
ug/L
0.50
1
10/25/1504,,06 108.67-8
Vinyl chloride
ND
ug/L
1.0
1
10125/15 04:06 75-01-4
m&p Xylene
ND
ugfL
1.0
1
10/25/15 04:D6 179601-23-1
o-Xylene
ND
ug/L
0.50
1
10/25/15 04:06 95-47.6
Surrogates
1,2-Dichlorcethane-d4 (S)
101
%
70-130
1
10125/15 04:06 17060-07.0
4-Bromotiuorobenzene (S)
98
%
70-130
1
10/25115 04:06 460.0D-4
Toluene-dS(S)
100
%
70-130
1
10/25115 04:06 2037-26.5
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced,
except in fug,
Date: 11110/2016 09:05 AM
without the written consent of Pace Analytical Services, Inn..
Page 9 of 40

aeUA17al Cal'
t»WWcpsoshbamnr
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 VJnceyAve, Suite 100
Huntersville, NC 28078
[phone]
Project: Sampling 10/19/15
Pace Project No.: 92272649
Sample: MW 03 Lab ID: 92272649006 Collected: 1011911514100 Received: 102111508,400 Matrix; Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
62008 MSV . Analytical Method, SM 6200B
Benzene
NO
ug/L
0.50
1
10/25115 04:22 7143-2
Bromobenzene
NO
ug►L
0150
1
10/25115 04:22 108-86-1
Bromochloromethane
ND
ug1L
0.50
1
10125/15 04:22 74-97-5
Bromodichiorometharte
ND
ug/L
0.50
1
10125/15 04:22 75.27-4
Bromoform
ND
ug/L
0.50
1
10125/1504:22 75.25-2
Bromomethane
ND
uglL
. 5.0
1
1012511504:22 -74.63-9
n-Butylberizene
ND
ug/L
0.50
1
1012511504,22 104-51-8
sec-Butylbenzene
NO
ug1L
0.50
1
10125115 0422 135-98.8
tert-Butylbenzene
ND
ug/L
0.5D
1
10125116 04.22 98-06-6
Carbon tetrachloride
NO
ug/L
0.50
1
10/25/15 04.22 56-23.5
Chlorobenzene
ND
ug/L
0.50
1
10126115 04:22 108-90-7
Chloroethane
ND
ug/L
1.0
1
10125/15 04:22 75-00-3
Chloroform
ND
ug/L
0,50
1
10125115 04:22 67-66-3
Chloromethane
ND
ug/L
1.0
1
10/25/15 04,22 74-87-3
2-Chlorotoluene
ND
ug/L
0.5D
1
10/25/15 04:22 95.49.8
4-Chlorotoluene
ND
ug1L
0.50
1
10/25115 04:22 106.43-4
1,2-Dibromo-3-chloropropene
NO
ug/L
110
1
10/25116 04,22 96-12-8
Oibromochloromethane
ND
ug/L
0.50
1
10/25/15 04:22 124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
1012511504:22 106.93-4
Dibromomethane
ND
ug/L
0,50
1
10125115 04,22 74-95-3
1.2-Dichlorobenzene
ND
ug/L
0.50
1
10/25/15 D4,22 95-60-1
1,3-Dichlorobenzene
ND
ug1L
0.50
1
10125115 0412 541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
10125115 04:22 10646-7
Dichlomdifluoromethane
ND
ug1L
0.50
1
10/25116 04,22 75-71.8
1,1-Dichlomethane
NO
ugfL
0.60
1
10/25/15 04:22 75-34-3
1,2-Dichloroethene
ND
ug/L
0.50
1
10/25115 04:22 107-06-2
1,1-Dichloroethene
NO
ug/L
0,50
1
10/25/15 04:22 7&35-4
ds-1,2-Dichloroethene
ND
ug1L
0.50
1
10/26115 04,22 156-59-2
trans-1,2-Dichloroethene
NO
ug/L
0.50
1
1012511604:22 156-60-5
1,2-Dichloropropane
NO
uglL
0.50
1
10/25/15 04:22 78-87.5
1,3-Dichloropropane
ND
ug/L
0.50
.1
10125115 04:22 142-28.9
2,2-Dichloropropane
ND
ug/L
0.50
1
10125115 04:22 694-20-7
1,1-Dichlorapropene
NO
uglL
0.50
1
10/25115 04:22 563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
10125115 04:22 10061-01.5
trans-1,34Dichloropropene
NO
uglL
0,60
1
1012511504:22 10061-02-6
Diisopropyl ether
ND
ug/L
0.60
1
10/25/15 04.22 108-20.3
Ethylbenzene
ND
ug/L
0.50
1
10/2511504:22 100-41-4
Hexachloro-1,3.butadiene
ND
ug/L
2.0
1
10/25115 04:22 87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
10125115 04:22 98-82.8
Methylene Chloride
NO
ug1L
2.0
1
10/25/15 04:22 75.09-2
Methyltert-butyl ether
NO
uglL
0.50
1
10/25/15 04:22 1634.044
Naphthalene
ND
ug/L
2.0
1
10125/15 04:22 91-20.3
ri-Propyibenzene
ND
ug/L
0.50
1
10125/16 04:22 103.65-1
Styrene
ND
ug/L
0.60
1
10125115 04,22 10042-5
1,1.1,2-Tetrachtoroethane
ND
ug/L
0.50
1
10/2511504:22 630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
1012511504.22.79-34-5
Tetrachlomethene
ND
ug/L
0.50
1
10126115 04:22 127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date, 11/1012015 09:05 AM without the written consent of Para Analytical Services, Ina. Page 10 of 40

"Analytical #
xwwoo kucarr
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
98001GnceyAve, Suite 100
Huntersvilie, NC 28078
(704)875.9t)92
Project: Sampling 10119115
Pace Project No.: 92272649
,Sample: MW 03 Lab ID: 92272649005 Collected: 1011911514.00 Received: 10121/16 08.00 Matrix: Water
Parameters Results Units Report Limit OF Prepared -Analyzed• CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trtchloroberizene
1,1,1-Trichlo methane
1,1,2-Trichlor6ethane .
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Tdmethylbenzene
1,3,5-Trimethytbenzene
Vinyl chloride
m8p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Analytical Method: SM 6200B
ND
uglL
0.50
1
10/25115 04:22 108.88-3
NO
ug/L
2.0
1
10126/15 04:22 87-61.6
NO
ugIL
2.0
1
10/25115 04:22.120.82.1/
ND
uglL
0.50
1
10125/15 04:22 71-55-6
NO
ug1L
0:50
1
101251150422'79-00-5
NO
6g/L
0,50
1
10/25115 0422 79-01-6
ND
ug/L
1.0
1
10/25/15 04:22 75.69.4
NO
u911-
0.50
1
10125/15 0422 96.18.4
ND
ug/L
0150
1
10/25115 04:22 95-63-6
NO
ug/L
0.50
1
10125115 04:22 168.67-8
ND
ug/L
1.0
1
10/25115 0422 75.014
NO
ug/L
1.0
1
10125115 04:22 179601-23-1
.ND
ug/L
0150
1
10126/15 0422 9547-6
102
%
70.130
1
10/25115 04.22 17060-07-0
99 .
%
70-13b
1
10/25115 04:22 460-00-4
101
%
70-130
1
10/25115 04:22 2037-26.5
Sample: MIN 05 Lab lD: 92272649006 Collected: 1011911514:30 Received: 10/21/15 08:00 Matrix: -Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method: SM 6200B
Benzene
NO
ug/L
0.50
1
1012511504:39 71-43-2
Bromobenzene
ND
uglL
0.50
1
10125115 04:39 108-86-1,
Bromochlommethane
ND
ug/L
0.50
1
10/25/16 04:39 74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
10/25/16 64:39 7547-4
Bromoform
ND
ug1L
0.50
1
1OW15 04:39 75-25-2
Broinomethane
ND
ug/L
5.0
1
10/25/16 04,39 74.83.9
n-Butylbenzehe
ND
ug/L
0.50
1
10125115 04:39 W4-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
10/25/15 04,39 135-98-8
tert-Butyibenzene
ND
ug/L
0.50
1
10125/15 04:39 98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
10/25/15 04s39 55-23-5
Chiorobenzene
NO
ug/L
0.50
1
10125/15 04:39 108-90-7
Chloroethane
ND
ug/L
1.0
1
10125/1504:39 75-06-3
Chloroform
NO
ug/L
0.50
1
10125/16 04:39 67-66-3
Chloromethane
ND
ug/L
1.0
1
10/25/15 04:39 74-87.3
2-Chlorotoluene
. ND
ugli-
0.50
1
10125115 04:39 9549-8
4-Chlorotoluene
ND
ug/L
0.50
1
10/25/15 04:39 106-43-4
1,2-Dibromo-3-chloropropane
ND
uglL
1.0
1
1012511504:39 96-12.8
Dibromochloromethane
ND
ug/t-
0,50
1
10125115 04:39 12448.1
1,2-Dibromoethane (EDB)
NO
ug/L
0,50
1
10125/15 04:39 106.93-4
Dibromornethane
NO
ug1L
0.50
1
10125115 04.39 74.95-3
1,2-Dichlorobenzene
ND
uglL
0.50
1
10125/15 04:39 95-50-1
1,3-Dichlorobenzene
NO
ug/L
0.50
1
10/25/15 04.39 541-73-1
1,4-Dichlorobenzene
ND
ug1L
0.50
1
'10125115 04:39 106-46 7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 1111012015 09.05 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 40

aceArtalyh'cal;
wMvr.DerokAtcom
ANALYTICAL RESULTS
Pace Analytical Servlces, Inc.
9800 IOnceyAve, Suite 100
Huntersvitle, NC 28078
(704)B75-9092
Project; Sampling'10/19115
Pace Project No.: 92272649
Sample: MW 05 Lab 10: 92272"9006 Collected: 1011911614,30 Received: 10/21/15 08:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method. SM 6200B
Dichlorodifluaromethane
ND
ugll.
0.60
1
10/25/15 04:39 75-71-8
1,1-Dichloroethane
ND
ug2
0.50
1
1012511504,39 75-34-3
1,2-Dichloroethane
ND
ug/L
0.60
1
10125/15 04:39 107.06.2
1,1-Dichloroethene
NO
ug/L
0.50
1
10125115 04:39 75-35-4
cis-1,2-Dichicroelhene
NO
ug/L
0.50 '
1
10125/15 04:39 156.59.2
trans-1,2-Dichloroethene
NO
ug/L
0.50
1
10/25115 04,39 156.60.5
1,2-Dichlaropropane
NO
ug/L
0.50
1
10125/15 04:39 78.87.5
1,3-Dichloropropane
NO
ug/L
0.50
1
1012511504,39 142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
10125/15 04,39 594-20-7
1,1-Dichloropropene
NO
ug/L
'0.50
1
10126115 04:39 563-58.6
cis-1,3-Dlchloropropene
ND
ug/L
0.50
1
10125115 04:39 10061-01-5
trans-1,3-01chloropropene
ND
ug/L-
0.50
1
10/25115 04:39 10061.02.6
DHsopropyl ether
ND
ug/L
D.50
1
10125115 04:39 108-20-3
Ethylbenzene
NO
ug/L
b.50
1
1012511504:39 160-41-4
Hexachtoro-1,3-butadiene
ND
ugll.
2.0
1
1012511504:39 87-68-3
Isopropyibenzene (Cumene)
ND
ug/L
0.50
1
10/26115 04,39 98-82-8
Methylene Chloride
ND
ug/L
2.0
1
10/25/15 0419 75-69.2
Methyl4ert-butyl ether
ND
ug/L
0.50
1
10/25115 04:39 1634.04.4
Naphthalene
ND
ug/L
2.0
1
10/25/15 D4:39 91-20.3
n-Propylbenzene
NO
ug/L
0,50
1
10/25/15 04:39 103-65-1
Styrene
ND
ug1L
0.50
1
1012511504:39 10042-5
1,1,1,2-Teirachloroethane
ND
ug/L
0.50
1
10125115 04:39 630-20-6
1,1,2,2Tetrachloroethane
ND
ug/L
0.50
1
1012511604:39 79-34-5
Tetrachtoroethene
ND
ug/L
0,50
1
10125/15 04:39 127-18-4
Toluene
ND
ug/L
0150
1
10125/15 04:39 108.88-3
.1,2,3-Tdchlorobenzene
ND
ug/L
2.0
1
10/25115 04:39 87-61.6
1,2,4-Trichtorobenzene
ND
ugll-
2.0
1
1012511504:39 126-82-1
1,1,1-Tdchtoroethane
ND
ug/L
0.50
1
10/25/15 04:39 71-55-6
1,1,2-Tdchloroelhane
ND
ug/L
0.50
1
10125115 04,39 79-OM
Trichloroethene
ND
ug/L
0.50
1
10125/15 04:39 79-01-6
Tdchlomfluoromethane
ND
ug/L
1.0
1
10125/1504,39 75-694
1,2,3-Tdchlompropane
ND
ug/L
0.50
1
1012611504:39 96-18-4
1,2,4 Tdmethylbenzene
ND
ug/L
0.50
1
1012611604:39 95-63.6
1,3,5-Tdmethylberizene
ND
uglL
0.50
1
10/25115 04:39 108-67.8
Vinyl chloride
ND
ug/L
1.0
1
10125115 04:39 75.01-4
m$p-Xylene
ND
uglL
1.0
1
10125115 04:39 179601.23-1
o-Xylene
ND
ug/L
0.50
1
10125/15 04:39 95-47-6
Surrogates
1,2-Dlchloroethane-d4 (S)
102
95
70-130
1
10/25/15 04:39 17060-07.0
4-Bromoftuorobenzene (S)
99
%
70-130
1
10/25115 04,39 460.OG-4
Toluene -dB (S)
100
%
70-130
. 1
10125116 04:39 2037-26.5
Date: 11/1012015 09:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inca
Page 12 of 40

I
oAnalytical"
www.pacewilow
November 10, 2015
Mr. Stephen Reavis
MCAS Cherry Point
Facilities Maintenance Depart
PSC Box 8006, LCU
Cherry Point, NC 28533
RE: Project: Sampling 10/19/15
Pace Project No.: 92272649
Pace Mialytleal Services; Inc.
9800 KlnceyAve. Suite 10D
Hunteravdle; NC 28078
[phone]
Dear Mr. Reavis:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
wo, ". %- an
Angela Baioni
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in Neil,
without the written Consent of Pace Analytical Services, Me -
Page 1 of 40

aceAnalytical
www.pecelabscM
Project: Sampling 10/19/16
Pace Project No.: 92272649
Pennsylvania Certification IDs
Georgia Certification #: C040
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
L-A-B DOD-ELAP Accreditation #: L2417
Alabama Certification P. 41590
Arizona Certification #: AZO734
Arkansas Certification
California Certification M 04222CA
Colorado Certification
Connecticut Certification #: PH-0694
Delaware Certification
FloridarTNI Certification #: E87683
Georgia Certification #: C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification M 391
Kansas/TNI Certification #: E-10358
Kentucky Certification M 90133
Louisiana DHH/TNI Certification M LA140008
Louisiana DEQrTNI Certification #: 4086
Maine Certification M PA00091
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification
Missouri Certification #: 235
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #:41320
Connecticut Certification M PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #. E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification M 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Cer ification: #346
Michigan Certification M 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification M. 236
Montana Certification #: Cert 0074
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification M 99006001
Asheville Certification IDs
Pace Analytical Service, inc.
9800 Kincey Ave. Suite 100
HuntemVille, NC 28078
[phone]
CERTIFICATIONS
Montana Certification M Cert 0082
Nebraska Certification #: NE-05-29-14
Nevada Certification#: PA014572015.1 .
New HampshirerTNi Certification #: 2976
New Jersey/ TNI Certification #: PA 051
New Mexico Certification M PA01457
New YorkrrNt Certification M 10888
North Carolina Certification * 42706
North Dakota Certification #: R-190
OregonrrNi Certification M PA200002
PennsylvanlaffNI Certification M 65-00282
Puerto Rico Certification * PA01457
Rhode Island Certification M 65.00282
South Dakota Certification
Tennessee Certification #. TH2867
Texas/TNI Certification M 7104704IM14-8
UtahrTNI Certification #: PA014572015-5
USDA Soil Permit #: P330.14-00213
Vermont Dept. of Health: ID# VT-0282
Virgin Island/PADEP Certification
Virginia/VELAP Certification M 460198
Washington Certification #: C868
West Virginia DEP Certification M 143
West Virginia DHHR Certification #: 9964C
Wisconsin Certification
Wyoming Certification #: BTMS-L
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification M 2958
New York Certification #,11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #:12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification M 460165
West Virginia Certification M 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Florida/NELAP Certification M E87627
Kentucky UST Certification M 84
West Virginia Certification #: 357
Virginla/VELAP Certification M 460221,
2225 Riverside Drive, Asheville, NC 28&M North Carolina Wastewater Certification #: 40
Fiorida/NELAP Certification M E87648 South Carolina Certification M 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc. Page 2 of 40

aceArraly#r'ca!'
WWW..jueerabsrnm
SAMPLE ANALYTE COUNT
Project, Sampling 10/19/15
Pace Project No_, 92272649
Pace Analytical Services. Inc.
9800 KinCeyAve, Suite 100
Huntersvilte, NC 29075
(704j875.9092
Analytea
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92272649001
001 SLUDGE
EPA 8081
SWB
8
PASI,C
EPA 8151
LJM
3
PASI-0
EPA6010
CDF
13
PASI-A
EPA6010
CDF
7
PASI-A
EPA7470
SHi
1
PASI-A
EPA7471
SH1
1
PASI-A
EPA 8270
Bpi
18
PA%C
EPA 8260
GAW
14
PASI-C
SM 254OG
KDF
1
PASI-C
ASTM D297"7
CLW
1
PASI-C
EPA1010
TEP
1
PASI,A
EPA 9045
MLS
1
PASI-A
SM 2710B
EWS
1
PASI-A
EP WOA
SER
1
PASI-A
EPA 351.2
SER
1
PASI•A
EPA 353.2
DMN
3
PASI•A
EPA 3651
AES2
1
PAS1-A
92272649002
001 SLUDGE
EPA 2001
CDF
3
PASI-A
EPA6010
JMW
1
PASLA
SW-846 7.3.3.2
BMS
1
PASI-PA
SW 846 7.3.4.2
PAS
1
PASWA
92272649003
MW 01
SM 6200B,
CAH
63
PASI-C
92272649004
MW 02
SM 6200B
CAH
63
PASI-C
92272549005
MW 03
SM 6200B
CAH
63
PASI-C
92272649006
MW 05
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except In full,
without the written consent of Pace Analytical Senrices, Inc..
Page 3 of 40

Pace Analytical Services, Inc.
aceAnalyiicad ® 980b IOneey Ave, Suite 100
Huntersville, NC 28078
www.pwakftcom
[phone]
ANALYTICAL RESULTS
Project; Sampling 10119/15
Pace Project No.: 92272649
Sample: 001 SLUDGE Lab ID: 92272649001 Collected: 10/1911513.00 Received: 10121/15 08:00 Matrix; Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit • DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
Analytical Method: EPA 8081 Preparation Method; EPA 3510
Leachale Method/Date: EPA 1311;10130115 00,00
gamma-BHC (Undane)
ND ugiL
0:50 1
11/031150920 11103115 13:26 58.89-9
Chlordane (Technical)
ND ug/L
3.0 1
11/03/15 09:20 111031i513:26 57-74-9
Enddn
ND ug1L
0.50 1
11/03/150920 1110311513:26 72-20-8.
Heptachlor epoxide
ND ug1L
0.50 1
11/03115 09:20 11103/1513:26 1024-57-3
Methoxychlor
ND uglL
1000 1.
11/03/15 09,20 11/03/15 13:26 72-43-5
Toxaphene
ND ug1L
3,0 1
11/03115 09:20 11/03/15 113:26 8001-35-2
Surrogates
Decachloroblphenyl (S)
40 %
10-138 1
11103115 0920 11/0311513:26 2051-24-3
Tetrachloro-m-xylene (S)
35 %
10-110 1
11/03115 09,20 1110311513,26 877-09-8 .
8151 Chlorinate Herbicide TCLP
Analytical Method: EPA 8151
Preparation Method; EPA 3510
2,4-1) ..
ND mg/L
11.0 1
10/34115 08:20 10/3011515AI 94 75-7
2,4,5-TP (Silvex)
ND mg1L
11.0 1
10/30/15 08:20 1 D/30115.15:41 93 72-1
Surrogates
2,4-DCAA (S)
102 %
42-142 1
10/30/15 0820 10/30/1515;41. 197i 9-28-9
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
30400 mglkg
9200 1
10/22115 20:30 10127/15 01:47' 7429-90-5
Arsenic
ND mglkg
920 1
10122115 20:30 1027115 01,47 7440.38-2
Cadmium
ND mglkg
92.0 1
10/22/15 20:30 10127115 01:47 7440-43-9 .
Calcium
130000 mg/kg
9200 1
10122/1520:30 10127115.01:47 744070-2
Copper
1700 mglkg
460 1
10122115 20:30 10/27/15 01:47 7440-50.8
Lead
ND mglkg
460 1
10/22/15 20:30 10127/15 01:47 7439-92-1
Magnesium
19000 mglkg
9200 1
10/22115'20,20 10/27/15 01:47 7439.95.4
Molybdenum
ND mgikg
460 1
10122115 20:30 10/27/15 01,47 ,7439.98-7
Nickel
ND mglkg
460 1
10122115 20:30 10127/15 01�47 7440.02-0
Potassium
ND mglkg
460000 1
10/22/15 20:30 16/27/15 01 A7 7440.09 7
Selenium
ND mg/kg
920 1
10/22115 20:30 10/27/15 01:47 7782-49.2
Sodium
ND mgikg
460000 1
10122/15 20.30 1027/15 01;47 7440.23-5
Zinc
1930 mglkg
920 1
10122/15 20:30 1627/15 01:47 7440.66#6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method:'EPA 3010
Leachate Method/Date: EPA 1311;10122/15 05:10
Arsenic
ND mg1L
0.050 1
1023115 0220 1012311517:04 7440-38-2
Barium
ND mg1L
0.25 1
1023115 02,30 10/2311517:04 7440.39-3
Cadmium
ND mg/L
0,0060 1
10/23115 02:30 102311517.04 7440-43.9
Chromium
ND mg1L
0,025 1
10123/15 02:30 102311517;04 7440-47-3
Lead
ND mg1L
0,025 1
10123/15 02:30 1023/1517:04 7439.92-1
Selenium
ND mg/L
DA0 1
10/23/16 02,30 10Q2 1115 17:04 7782-49-2
Silver
ND mg/L
0,025 , 1
10123/16 02.30 1012311517M4 7440.22.4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311;1022115 05:10
Mercury
ND mg/L
0.00020 1
1012311510:00 10/2311513:41 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report
shall not be reproduced, except
In full,
Date: 11/1012015 09:05 AM
without the written consent of Pace Anelylicat Senrkes, tnrA, Page 4 of 40

acemal Cale
WWWpaefibbicom
ANALYTICAL RESULTS
Project: Sampling 10119115
Pace Project No.: 92272649
Pace Analytical Services, Inc.
9806 Wncay Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 001 SLUDGE Lab ID: 92272649001 Collected: 1011911513:00 Received; 10/21/15 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
7471 Mercury
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2.4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresoq
3ti4-Methylphenol(mtip Cresol)
Nitrobenzene
Pentachtorophenol
Pyridine
2,4,5-Tdchiorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluomblphenyl (S)
Terphenyl-dl4 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichlorcethene
Tetrachtoroethene
Tdchloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromonuorobenzene (S)
2540G Total Percent Solids
Total Solids
Analytical Method: EPA7471 Preparation Method: EPA7471
ND mglkg 5.2 1 10126/1513:20 1012711513:52 7439-97-6
Analytical Method: EPA 8270 Preparation Method. EPA 3510
Leachate Method/Date., EPA 1311;10/30115 00,00
ND
ug/L
50.0
1
1110211510.00
11/03/1514:58
106.46.7
ND
ug1L
50,0
1
1110211510.00
11/0311514;58
121-14-2
ND
ug/L
50.0
1
1110211510.00
11/0311514,58
87-68-3
ND
ug/L
50,0
1
1110211510:00
11/0311614;58
118.74-1
ND
ug/L
50.D
1
11102/1510:00
11/0311514,66
67 72-1
ND
ug/L
50,0
1
11/02/1510.00
11/D3/1514:58
95.48.7
ND
ug/L
50.0
1
1110211510:00
11/0311514:58
ND
ug/L
50,0
1
11/02/15 WOO
11/03/15 14:58
98-95-3
ND
ug/L
100
1
11/02/1510:00
1110311514:58
87-86-5
ND
ug1L
50.0
1
1110211510:00
1110311514:58
110-86-1
ND
ug/L
50..0
1
11/02/1510:00
1110311514.58
95-95.4
ND
uglL
50.0 '
1
11102/1510:00
11/03/1514:58
88.0&2
18
%
12-102
1
11/0211510!00
11/03/1514:58
4165.60.0
22
%
13-107
1
11/0211510:00
11/0311514:58
321-60-8
56
%
21-132
1
11102/1510:00
11/0311514,58
1718-51.0
9
%
10-110
1
11/0211510:00
1110311514:58
13127-88-3 SO
12
%
1D-110
1
1110211510.00
1110811514:58
367-12-4
50
%
27-108
1
11/02/1510.00
11103/1514:58
118 79-6
Analytical Method:, EPA 8260 Leachate Method/Date: EPA 1311;10i26/15 11:12
ND
u91L
°100
20
10131115 08,56 7143.2
ND
ug/L
200
20
10/31/15 08,56 78-93.3
ND
ug/L
100
20
10131/1506,56 56.M-5
ND
uglL
100
20
10/31/15 08:56 106-90-7
NO
ug/L
100
20
10/31/15 08:56 67-66-3
ND
ug/L
100
20
10/31/16 08:56 106 46.7
ND
ug/L
100
20
10/31/15 08:56 107-06-2
ND
uglL
100
20
10131115 08:56 75-36 4
ND
ugli-
100
20 .
10131/15 08:56 127-18-4
ND
ug/L
100
20
10/31/15 08,66 79-01-6
ND
ug/L
100
20
10131/16 08:56 75-014
124
%
70-130
20
10/31115 08:56 17060,07-0
98
%
67-135
20
10/31/15 08.66 2037-26-5
105
%
70-130
20
10/31/15 08:56 46MO-4
Analytical Method: SM 254OG
0.090 tA 0.000010 1
REPORT OF LABORATORY ANALYSIS .
10/21/1516:53
This report shall not be reproduced, except In full,
Date, 11/10/2015 09:05 AM without the written consent of Pace Analytical Services, Inc- Page 5 of 40

t
aceAnalj cal
w►nrrp+cdebs mm
ANALYTICAL RESULTS
Project Sampling 10/19/15
Pace Project No.: 92272649
Pace Analytical Services, Inc.
9800 loncey Ave. Suite 100
HuntnrsWle. NC 28078
(704)8754092
Sample: 001 SLUDGE
Lab ID: 92272649001 Collected: 10/19/1513:00
Received: 10121115 08:00 Matrix;, Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No, Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
99.9 %
0.10
1
10122/1512:53
1010 Flashpoint,Closed Cup
Analytical Method; EPA 1010
Flashpoint
>200 deg F
70.0
1
1Q13011511:30
9045 pH Soil
Analytical Method_ EPA 9045
PH at 25 Degrees C
7.2 Sid. Units
0.10
1
10122/1511 A0 H1
Plant Available Nitrogen
Analytical Method., SM 2710B
Plant Available Nitrogen
122000 mg/kg
0.12
1
1110511517:20 N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
136000 mglkg
10200
1
10126/15 01:31 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
217000 mg/kg
55200
1
11/03/15 02:36 7727.37.9
353.2 Nitrogen, N021NO3
Analytical Method; EPA 353,2
Nitrogen, Nitrate
26000 mglkg,
2180
1
11103115 10:31
Nitrogen, Nitrite
4160 mg/kg
1090
1
11103/151011
Nitrogen, NO2 plus NO3
30100 mg/kg
2180
1
11/03/15. 10:31
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
142000 mglkg
' 4150
2
10/2811512:19 7723-14.0
Sample: 001 SLUDGE
LOW: 92272649002 Collected,
10/19/151100
Received: 10121/15 08,0D Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No.. Qual
200.7 MiET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Calcium
'189000 ug/L
1000
1
11105/1513:05
11106/151SAI
7440-70.2
Magnesium
24200 ug1L
1000
1
11/05/1513:05
11/06/1515A1
7439-954
Sodium
117000 uglL
50000
.1
1110511513:05
1110611515:41
7440-23-5
Sodium Adsorption Ratio, SAR
Analytical Method, EPA 6010
Sodium Adsorption Ratio
2.1 meq/L .
1
1110911517.02
N2
733C Reactive Cyanide
Analytical Method: SW-846 7,3,3.2
Cyanide, Reactive
ND mg/L
0.010
1
10/22/15 22:30
734S Reactive Sulfide
Analytical Method: SW-846 7,3,4,2
Sulfide, Reactive
ND mg/L -
1.0
1
1012211518,30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in tun.
Date: 11110/2015 09:05 AM without the written consent of Pace Analytical Services, Inc,
Page 6 of 40