WQ0006245_Residual Annual Report 2019_20200131

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submital an
application?*
r Yes r No
Annual Report 2019
Year*
Date Paper Copy 1/31/2020
Received:*
Project Number* WQ0006245
Email Notifications
............................................................................................
Does this need O Yes
review by the a No
hydrogeologist? *
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues.
.......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Ken Galloway
Email Address*
[e-mail]
Project Information
........................................................................................................................................................................
Submittal Type* r New Permit Application
r Renewal
IT Annual Report
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0006245
Applicant\Permittee * City of Statesville
Facility Name * City of Statesville
Phone Number*
7048783438
r Modification (Major or Minor)
r Additional Information
r Other
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Formt Engineering Rans, Specifications, Calculations, Etc.)
2019 Sta-Lime.pdf 21.15MB
Upload only 1 RJF docurrent. NiLRiple docurrents must be con bind into one RJF file.
For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contact the reviewer or Tessa Monday. If a paper application is required,
be advised, applications accepted for pre -review until both the paper and electronic copies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments (caIcs, sails report, specs, etc,}
0 one full-size engineering plan set
o One 11x17" engineering plan set
0 0ne extra set of specifications
o Fee (if required}
Mailing address:
By U.S. Postal Service
By Courier/Special Delivery;
Division of Water Resources
Division of Water Resources
------------ --------------
Non -Discharge Branch
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
----------------------------------------------------------------------------
Non -Discharge Branch
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
1617 Mail Service Center
--------------------------------------------------'
Att: Nathaniel Thornburg, 5" Floor, Office #942W
-------- ------------------------------------------------------------
Raleigh. NC 27699-1617
512 N. Salisbury St.
For questions or problems contact Tessa Monday [e-mail] or 919.707.3660.

* W By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 1/29/2020

taf e
NORTH CAROLINA
January 23, 2020
Attention: Troy Doby
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: Annual Report for 2019
Alkaline Stabilization (W00006245)
Dear Mr. Doby:
Enclosed, you will find a copy of the required fonns and lab data for the Alkaline Stabilization
program. Permit # W00006245.
There was zero Sta-Lime produced in the Third Quarter of 2019, therefor no lab results reported
for that time period.
Should you require more information, or if further action is required, please contact me at 704- 878-3438,
Sincere)
allow —
ay
W WTP Supervisor, Fourth Creek W WTP
PO Box 1111 Statesville, NC 28687 • ci.statesville.nc.us

GENERAL INFORMATION
ALKALINE STABLIZATION REPORT
CALENDER YEAR 2019
PERMIT NO. WQ0006245
FACILITY NAME: Fourth Creek WWTP NPDES NCO031836
LOCATION: 693 Bell Farm Road
MAILING ADDRESS: P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESPONSIBLE OFFICIAL: Andy Smith, Operations Manager
Water Resources
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Ken Galloway
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Ken Galloway
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
APPLICATION: Class A Exceptional Quality Product
Test Data and Summary Operations
Attached

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Fourth Creek W WTP Alkaline Stabilization
WWTPName: Fourth Creek WWTP
WQ Permit Number: W00006245
NPDES Number: NCO031836
Monitoring Period: From 1/1/2019
To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and altPrnativP
Class A:
I Alt. A (time/tem) ❑
Alt B (Alk Treatment) p
- - ---------_--
Alt. C (Prior Testing) U
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogen s i:-1
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Path ens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Themro hilic L1
Beta Ray ❑
Gamma Ra ❑
Pasteurization M
Class B:
Alt. (1) Fecal Densit ❑
Alt. (2) Process to Significantly
Reduce Pt ens U
If applicable to alternative performed Class B only) Indicate "Process to Significantly Reduce Pathogens",
Lime Stabilization ❑
AjrDrying ❑
Composting U
JAcrobicDigestion U
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
I Pathogen Density
Number
Frequency
9 y
Sample
P
na y tica
in Sludge
Excee-
deuces
of Analysis
Type
Tech-
jMinimuHGco.
Mean
Maxima
Units
ni ue
2 x 10 to the
6th power
MPN
<0.2
<0.3
m n/
p g
Quarterly
grab
sm9221 e
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
weight)
r ccwr a Macuun Keuucnon ttaA 1N4.Al. ULI .11U/) - Please indicate alternative nerformed-
Alt.l (VS reduction) ❑
AI[. 2 (40-day bench) ❑
Alt. 3 (30-day bench) [ )�
Alt 4 (Spec. Oz uptake) L�1
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization U
Alt 7 (Drying -Stable) U
Alt. 8 (Drying -Unstable) L1
Alt. 9 (Injection) ❑
JAR. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed Ll
Le,K11V1t-A11U1N J1Alr,1V1EIN 1 (please check the appropriate statement)
hd "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Preparer Name,9,v#Tit1e (type or pri
/23-ZC)
Land Applier Name and Title (if applicable)(type or print)
Signature of Prep"-* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
DENR FORM PVRF 02T (12/2006)

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Isetup Date: I- a s- I q
Removal From Bin Date: /-31. 17
Date
Time
pH >12.0 For 72 HrS.
TEMP: >52 Deg. C For 12 Hrs.
Operator
i-dS-19
O9%30
InitialpH: la,5q
1-de-19
93003.'ao
I-a9- 19
W&07;65
R4W
Corrected pH: 12,7E
I.31-17
10:.72
FinalpH: Ia,58
1-31-17
'7300Ilam
,q
R4W
Corrected pH: Id. 7d
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria
Been Met? Y N
BIN # a ,'3
Setup Date: I-2 q - 3 1
Removal From Bin Date: d- I -19
Date
Time
pH >12.0 For 72 Hrs.
TEMP.>52 Deg. C For 12 Hrs.
Operator
I-t9-19
11 om
initial pH: Id, 93
1-24-14
95"@IIA'
1-3o-19
Fr5'009;0o
14W
CorrectedpH:Id.6
1 1 19
n
1d Y5'�
Final pH: Id . 6N
R( W
Corrected pH: /1, ?q
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met? Y N
BIN # 7Z F
Setup Date:. 1-30 - 14
Removal From Bin Date: a- 4- 19
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1-30-Iq
o9;3q
InitialpH: Ia.59
I-30-19
q0 @ IA O`I
1031-19
86 (?011UI
RAW
Corrected pH: Id.79
a-4 I
q
10
to"Corrected
Final pH: l a. 5 q
a 4 19
°@ /o: is
(l(I✓)
pH: 1d.93&8
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met? Y N
BIN# 5
Setup Date: /-3/-!9
Removal From Bin Date: a-5-- Iq
Date
Time
pH >12.0 For.72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
l 31. 19
09. 30
Initial pH: 11, 1
1. 31-19
SO'& lV 36
Z(--1- 19
S6 @ 07,'5q
RAW
Corrected pH: 1a,7 g
d•�-19
i0:45M
FinalpH: I). 5a
2.9-1q
F3'C-' IO'15M
/?/,W
Corrected pH: 1a,6
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met? Y N
BIN # �
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
d-I-I9
InitialpH:
09,30
Ia,51
1-1-Iq
90 12Pn,
a-q-19
0@.07: 3y
R(
Corrected pH:12,71
A
"I
FinalpH: I d r 50
Corrected pH: 1d , d
Has 12 Hour Temp Criteria Been
Met? Y N
Has 72 Hour pH Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # ` e $
Setup Date: 1-r3-Iq
Removal From Bin Date: I- 11.1q
Date
Time
pH >12.0 For 72 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator
d-r8-Iq
q
1o:45'n
Initial pH: Id.go
2-18-1q
'eII;II�n
R-19-1 q.
09007%91
PUL:
Corrected pH: /,/,
21al-1q
11:30�
^�
Final 12.43
.1-21-I1
85°�09:40
.n*vs° T,
CGVCAVOONO
%24W
Corrected pH: /.7g/
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria
Been Met? Y N
BIN # bra
Setup Date:,4_/9_1 9
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
A'19- If
11 iU
Initial pH: 12. 58
Iq
fool? 11:40ti,
1-10-19
760 Sys—
RAW
CorrectedpH4: 1Z,75
R-U-19
12%50
FinalpH: 19.57
93-19
7F /015M
�1W
CorrectedpH: 12,73
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met? Y N
BIN # 34-S
Setup Date: _/ 9
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
2M-1q
// D
Initial pH: 11, 48
a-.11-19
90'&07:Ya
.i-22-I4
8S°"09:/5
RII`l
Corrected pH: /9.88
2-4S--19
12'50
Final pH: / 2. G y
2.15- 19
7s@(007%15
R1ti'
CorrectedpH: /2.79
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met? Y N
BIN # y i (
Setup Date: 2. 7/- 1 q
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
2-,tl• /9
0911/0
Initial pH: 12.5
R-v-Iq
90*& 09:40
1-ll•1q
80°C207;30
RAW
CorrectedpH: 12.71
1-QS-19
f2%.55
Final pH: 12. 6.:
2-ZS-lj
8SO
MOVED ry
7rYsler,15,_
kl.kAf
CorrectedpH: /2, S'�
Has 12 Hour Temp Criteria
Been Met? N
Has 72 Hour pH Criteria Been Met? Y
N
BIN # l e �2
Setup Date: 2- 2d_ )9
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
2-]z-19
1 Prn
InitialpH: 1.7.57
2-JA-Iq
90° �°l0�20
a-zs-ry
750
w
Corrected pH: /2,77
2-��1q
f PnI
Final pH:
Rjo,.
CorrectedpH: 1,7.73
Has 12 Hour Tennp Criteria
Been Met? N
Has 72 Hour pH CritBeen Met? N
eriayyy

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # / g'a
Setup Date: 5- $- 19
Removal From Bin Date: 5.13.19
Date
Time
pH >12.0 For 72 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator
5•8-19
1o;931n
Initial pH: /J.
10:43A q00
iQ, o
07:V7 90
.
RA
Corrected PH:l,1. 82
S. 13 - q
lo: 50 A
Final pH: id. 51
S-Q' 19
ro:Jd 900
� t'
Corrected pH: l d.7 g
Has 12 Hour Temp Criteria
Been Met? N
Has 72 Hour pH Criteria
Been Met? Y N
BIN # 3 e5
Setup Date: 5- 9- 1 q
Removal From Bin Date: S- 13 •19
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5.9- 1 q
Nt04 A
InitialpH: i.t. S7
5-9- iq
Il A 906
0'7.'30 900
Rtw
Corrected pH: la, '77
5-13-i9
//:ySA
Final pH: 0.e'/
5--r3--49
io:3t'A qO6
RAW
Corrected pH:/,7, 84
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN # 7 e$
Setup Date:.5.10- I q
Removal From Bin Date: 5-/3 - l q
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5 10-19
W 09 A
Initial pH: /,7, 55
S- l0- 19
W 10 A 90'
5-11-19
05.'oo 6 i '
R4 w
Corrected pH: 14, 75
S i3-19
1i *q
Final pH: /J. S
5-13'• 19
10.3d A 10'
Rd W
Corrected pH: 1.2,7d
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met? Y N
BIN # 14
Setup Date: 5-• 13-19
Removal From Bin Date: S-• 16 - 1 q
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5-13-Iq
io:3sA
Initial pH: /,ZS,j
3'-+3 19
10:3EA 900
5-14-19
07;3290'
RRW
Corrected pH: /.?,74
5- r[- l 9
11:ySA
Final pH: /,/, C q
Corrected pH: /J, 5,?
Has 12 Hour Temp Criteria
Been Met? N
Has 72 Hour pH Criteria Been
Met? Y N
BIN # 3 �5
Setup Date: 5-/y-Iq
Removal From Bin Date: s.17-1
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3-./y• 19
InitialpH:
I I :oo A
it.60
5 ly`r`I
/l A go*
5.1$..11
og; 00 65'
/�(q
Corrected pH:/ j, 77
S-17-iq
IZ: 15 P
Final pH: /.Z,q/.
S-/6-iq
0 7: /5 90 0
Corrected pH: /,./, 59
Has 12 Hour Temp Criteria Been
Met? N
Has 72 Hour pH Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # 7q P
Setup Date: S 1S--1 q
Removal From Bin Date: S• 20-1 q
Date
Time
pH >12.0 For 72 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator
5.15.19
id1a0P
Initial PH: /.1,5`7
S-7g•-14
11:30A 40° 07:15
3'-16-1q.
80°
RLW
Corrected PH:1,2.117
d0-19
0q:.4
Final pH: tbAo, jj,qj
R( In1
Corrected pH: 1, .5,r
Has 12 Hour Temp Criteria
Been Met? N
Has 72 Hour pH Criteria Been Met? Y N
BIN # I f' ?
Setup Date: 5-16-19
Removal From Bin Date: 6-2o-ill
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
S /6-14
II A
InitialpH: 1.7.56
3,4 -1q
09:30 qT 4 0
5-14_1q
7: 15 10°
R� W
Corrected pH: U. 76'
5 .?o -1 q
o 9: d 7
Final pH: / 2.413
� IJ
Corrected pH: 1.2.13
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met? Y N
BIN # VS
Setup Date:.3=P7-lq
Removal From Bin Date: 5-40- I
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5'-17 19
IOA
Initial PH: /d.53
5.17-i9
ov r5 95 °
6-Ao-1q
o4.'So 9o°
Rl,w
Corrected pH: 1a.73
3'-Jo-iq
09: 28
Final pH: 1.7,13
R
Corrected PH:1.4 3
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met?
Y N
BIN #3
Setup Date: S. Z 0 _ I q
Removal From Bin Date: 5- .13 . I
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5-to -19
09: 3 0
Initial pH: 1.1,63
-&-11
91 itj `fo'
.5- LI -Iq
id: `1,t
Corrected pH: /.1. 73
5- 23- Iq
IZ:4 3
Final pH: i.1,4 q
Corrected pH: 1.?.1 7
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # lie d
Setup Date: I1-19- I q
Removal From Bin Date: 11.2a _ i 9
Date
Time
I pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Yl•14-i9
A
11:3G.n
Initial pH: 1.1.53
11.19-19
70° 10:43 n
11.10-19
70 07:19
RCW
Corrected pH: 12, 6%
11-2A-19
11:40,i
Final
Rl.w
Corrected
tdPH:Id.EO
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN # 3 1.5
Setup Date: 11-,20 - 19
Removal From Bin Date: 11-J5• I9
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
,a
IP034
Initial pH: IJ.54
If•ao-w
774 11 03 y
it-a1-19
77 09:J7
21w
Corrected pH: l2.'10
u• 2 5-17
11130 »
Final pH: 1..4s
R l w
Corrected PH:11. 6 1
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria
Been Met? Y N
BIN # 7 {' 8
Setup Date: )I- a l -19
Removal From Bin Date: l l - :4 [ • j 9
Date
Time
I pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
I Operator
11-11-19
e
11:As�„
Initial pH: j1.53
U-41-19
° R
da 11:1i,n
11-4d-1a
°
6� oil; 10
I?kVj
Corrected j
H:
P .1. G4
11.15-19
A
163014
FinalpH: I„1.4y
RkW
Corrected pH:1.2.55
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met?
Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 Hour pH Criteria Been
Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial
pH:
Corrected pH:
Final pH:
Corrected pH:
Has 12 Hour Temp Criteria Been
Met? Y N
Has 72 Hour pH Criteria Been Met? Y N

NC Certification No. 402 Case Narrative
'P R I S M I Full -Service Analytical & NC Drinking Water Cart No. 37735 5/8/19 10 16
Environmental Solutions SC Certification No. 99012
-V'"AATOFHE3, M
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 01/03/2019
Prism Work Order: 9010010
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the revised laboratory report dated 2/ 11/19. PAN Equation has
been added to Case Narrative.
Analysis note for SAR:
SAR =iNa]/SQRT{((Ca]+ift)/2)
SAR = i 130/23.0 ] / SORT ((11300/20.01 + (0.025/12.21) / 2 )
SAR = 1,0
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SORT designates
taking the square root of the operand in parentheses.
PAN Equation = 0.3 * (TKN - Ammonia) + 0.5 * (Ammonia) +
Nitrate -Nitrite
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
PAN Equation = 0.3 * (1750 - 300) + 0.5 * (300) + 3.5
PAN = <1100 mg/kg
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone]
Page 1 of 17
j�
I

Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones'
President/Project Manager
Data Qualifiers Key Reference
Reviewed By RobbiA. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
DM Sample diluted and RL increased due to the matrix.
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0643
Phone: [phone]-Toll Free Number: l-8001529-6364- Fax: [phone] Page 2of17

I s n n I Full -Service Analytical 8
&Ak. ' V' Environmental Solutlona
Sample Receipt Summary
05/08/2019
Prism Work Order: 9010010
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
Stal-ime (and Fecal 1)
9010010-01
Solid
01/02/19
11:00
01/03/19
8:00
Fecal #2
9010010-02
Solid
01/02/19
11:00
01/03/19
8:00
Fecal #3
9010010-03
Solid
01/02/19
11:00
01/03/19
8:00
Fecal #4
9010010-04
Solid
01/02/19
11:00
01/03/19
8:00
Fecal #5
9010010-05
Solid
01/02/19
11:00
01/03/19
8:00
Fecal #6
9010010-06
Solid
01/02/19
11:00
01/03/19
8:00
Fecal #7
9010010-07
Solid
01/02/19
11:00
01/03/19
8:00
Samples were received at 22.3 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: t-8001629-6364- Fax: [phone]A409 Page 3of17

I S m I Fu6-Service Analytical a
r� 'v' Environmen[el Solutions
iwl41HG
Laboratory Report
05/08/2019
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: StaLime (and Fecal l)
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 9010010-01
P.O. Box 1111
Prism Work Order: 9010010
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter
Result Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor DateRme ID
General Chemistry Parameters
Plant Available Nitrogen
BRL
mg/kg dry
1100
310
5
'Calculation
1/7/19 10:48
CLB
[CALCI
% Solids
71.4
% by
0.100
0.100
1
'SM2640 G
118119 14:30
TJY
P9A0141
Weight
Ammonia as N
300
mg/kg dry
13
3.3
1
'SM4500-NH3 C 117119 10:48
BMS
P9A0089
Nitrate/Nitrite as N
BRL
mg/kg dry
7.0
1.9
1
'SM4500-NO3 F 1/3/19 11:17
CLB
PRA0038
Phosphorus -Total
2300
mg/kg dry
70
16
20
'SM4600-PF
117119 9:33
CLB
P9A0067
Total Kjeldahl Nitrogen
BRL
mg/kg dry
3500
1000
5
'351.2
1/4/19 9:01
CLB
P9A6037
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
'SM9221 E
1/3119 9:00
BMS
P9A0065
Total Metals
Mercury
0.060
mg/kg dry
0.028
0.0027
1
'7471B
11711912:37
MMR
PSA0078
SAR Soil Preparation
Complete
g
1
'2-78-054
1/7/19 8:30
MMR
P9A0046
SAR Percent Moisture
Complete
% by
0.100
0.100
1
'2-78-054
V7/19 8:30
MMR
POA0075
Weight
Arsenic
BRLDM
mg/kg dry
7.0
0.43
10
'6010D
177/19 10:37
JAB
P9A0055
Sodium Absorption Ratio
1.0
[blank]
0.30
0.016
1
'2-78-064
1/8119 10:69
JAB
P9A0056
Cadmium
BRLDM
mg/kg dry
3.5
0.094
10
'6010D
117/1916:37
JAB
P9A0055
Calcium, SAR
.1300
mg/L
10
1.0
100
'6010D
1/4119 17:16
JAB
PSA0066
Copper
33
mg/kg dry
7.0
0.63
10
'6010D
117/19 16:37
JAB
P9A0066
Lead
8.6
mg/kg dry
3.6
0.65
10
'6010D
1/7/19 16:37
JAB
P9A0055
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
'6010D
1/4/19 17:24
JAB
P9A0056
Nickel
9.6
mg/kg dry
7.0
0.26
10
'6010D
117119 16:37
JAB
PSA0065
Potassium
1900 BH
mg/kg dry
180
6.3
10
'6010D
1/7/19 16:37
JAB
P9A0065
Selenium
7.9
mg/kg dry
7.0
1.7
10
'6010D
117119 16:37
JAB
P9A0056
Sodium
1100
mg/kg dry
210
6.9
10
'6010D
1/7/19 16:37
JAB
P9A0055
Sodium, BAR
130 BH, B
mg/L
50
1.8
100
'6010D
118119 13:64
JAB
P9A0056
Zinc
49
mg/kg dry
35
1.3
10
'6010D
1/7/19 16:37
JAB
P9A0055
This report should not be reproduced, except in its entirety. without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]A409 Page of 17

&Aat'
Laboratory Report i I S l� n I Full -Service d Solutio a
'v' Environmental Solutions 05/08/2019
ran,ea me
City of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #2
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 9010010-02
P.O. Box 1111
Prism Work Order: 9010010
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
72.0 % by
0.100 0.100
1 'SM2540 G 118/19 14:30 TJY
P9A0141
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 `SM9221E 1/3/19 9:00 BMS
P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: l-8001629-6364-Fax: [phone] Page 5of 17

ISM
Full -Service Analytical&
Environmental Solutions
AAJMdba.area ixc
Laboratory Report
05/08/2019
City of Statesville, NC
Project: Stal-ime (Otrly, BiWeekly,
Client Sample ID: Fecal #3
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 9010010-03
P.O. Box 1111
Prism Work Order: 9010010
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Datefrme
ID
General Chemistry Parameters
Solids
70.2 % by
0.100 0.100
1 'SM2640 G 118/19 14:30 TJY
P9A0141
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 1/3/19 900 BMS
P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone],6364 - Toll Free Number: l-8001529-6364-Fax: [phone] Page 6 of 17

r I S m I Full-aeMee analytical s
V' Envlronmentel locona
�ueaarowv. we
Laboratory Report
05/08/2019
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #4
Prism Sample ID: 9010010-04
Prism Work Order: 9010010
Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch
Limit Factor DateRme ID
General Chemistry Parameters
Solids 72.0 % by 0.100 0.100 1 'SM2640 G 118/19 14:30 TJY P9A0141
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 1/3/19 9:00 BMS P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]- Toll Free Number: 1-8001629-6364- Fax: [phone] Page 7 of 17

AndR I S M I Full -Service Analytical &
Environmental Solutions
uwx..ua,�,ac
Laboratory Report
05/08/2019
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #5
Prism Sample ID: 9010010-05
Prism Work Order: 9010010
Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch
Limit Factor DateRme ID
General Chemistry Parameters
Solids 80.6 % by 0.100 0.100 1 'SM2640 G 118/19 14:30 TJY P9A0141
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 "SM9221 E 1/3/19 9:00 BMS P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NO 28224.0643
Phone: [phone] - Toll Free Number: 1-8001629-6364- Fax: [phone] Page 8of17

/IZ ISM
A I Full-mnmaeAnelyuoal3
'v1 F ll-S n ,lce A aolutlona
�uewurarea me
Laboratory Report
05/08/2019
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #6
Prism Sample ID: 9010010-06
Prism Work Order: 9010010
Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 71.7 % by 0.100 0.100 1 *SM2540 G 118/19 14:30 TJY P9A0141
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221E 1/3/19 9:00 BMS P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 282244543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone]
Page 9 of 17 —

�TJ In Full -Service Analytical&
ISM
r� Environmental Solutions
®wonnroava �xc
Laboratory Report
05/08/2019
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #7
Prism Sample ID: 9010010-07
Prism Work Order: 9010010
Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch
Limit Factor Daternme ID
General Chemistry Parameters
Solids 72.5 % by 0.100 0.100 1 •SM2540 G 1/8119 14:30 TJY P9A0141
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 1/3/19 9:00 BMS P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone]- Toll Free Number: l-8001629.6364-Fax: [phone] Page 10 of 17

Level It QC Report
APR ISM I FullIronmee al Solutions
&
Envlronmentel Solutions 5/8/19
iiaeomroeisx ixc
City of Statesville, NC Project: Stal-ime (Otrly, BiWeekly, 60Day Prism Work Order: 9010010
Attn: Andy Smith 7 Fecal) Time Submitted: 1/3/2019 8:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9A0046 - SAR 2.78.064
Blank (P9AO046-BLK1) Prepared: 01/03/19 Analyzed: 01/07/19
SAR Soil Preparation Complete g
Batch P9AO055 - 3060B
Blank (P9AO065-BLK1)
Prepared &Analyzed: 01/04/19
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P9A0055-BS1)
Prepared &Analyzed: 01/04/19
Arsenic
11.6
0.50
mg/kg wet
12.50 93
80-120
Cadmium
11.9
0.25
mg/kg wet
12.50 95
80-120
Copper
12.1
0.50
mg/kg wet
12.50 97
80-120
Lead
11.8
0.25
mg/kg wet
12.50 94
80-120
Nickel
12.0
0.50
mg/kg wet
12.50 96
80-120
Potassium
1230
12
mg/kg wet
1250 98
80-120
Selenium
11.2
0.50
mg/kg wet
12.50 90
80-120
Sodium
1380
15
mg/kg wet
1250 110
80-120
Zinc
10.5
2.5
mg/kg wet
12.50 84
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643
Phone: [phone]- Toll Free Number: 1.8001629-6364- Fax: [phone] Page 11 of 1] -

Level II QC Report
I S n /(I I Fuu-servroo al Solutions
a
1 V' EnU-Samientel aolunal & 5/8/19
IV' .awraei.. I.C.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: Stal-ime (Qtrly, BiWeekly, 60Day
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Prism Work Order: 9010010
Time Submitted: 1/3/2019 8:00:OOAM
%REC RPD
%REC Limits RPD Limit Notes
Batch P9AO056 - 301 OA
Blank (P9A0066-BLK1) Prepared &Analyzed: 01/04/19
Calcium, SAR BRL 0.10 mg/L
Magnesium, SAR
Sodium, SAR
BRL 0.10 mg/L
5.46 0.50 mg/L
Batch P9A0075 - NO PREP
Duplicate(P9A0075-DUP1) Source: 9010010-01 Prepared: 01/04/19 Analyzed: 01/07/19
SAR Percent Moisture Complete 0.100 % by Weight Complete 0.2 200
Batch P9AO078. 7471E
Blank (P9A0078-BLK1) Prepared &Analyzed: 01/07/19
Mercury BRL 0.020 mg/kg wet
LCS (P9A0078-BSI) Prepared &Analyzed: 01/07/19
Mercury 0.405 0.020 mg/kg wet 0.4167 97 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
BH
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone]- Toll Free Number: 1.800/629-6364 - Fax: [phone] Page 12 of 17

a.\
iR Funle I S M I Evironmental Solutions
7-uewurosregwc
Level II QC Report
518119
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, 6ODay
Attn: Andy Smith 7 Fecal)
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - quality Control
Reporting Spike Source
Analyte Result Limit Units Level Result
Batch P9AO037. 351.2
Prism Work Order: 9010010
Time Submitted: 1/3/2019 8:00:OOAM
%REC RPD
%REC Limits RPD Limit Notes
Blank (P9A0037-BLKI)
Prepared: 01/03/19 Analyzed: 01/04/19
Total Kjeldahl Nitrogen
BRL 50 mg/kg wet
LCS (P9A0037-BSI)
Prepared: 01/03/19 Analyzed: 01/04/19
Total Kjeldahl Nitrogen
127 50 mg/kg wet
125.0 102 90-110
Matrix Spike (P9A0037-MSI)
Source: 9010010.01
Prepared: 01/03/19 Analyzed: 01/04/19
Total Kjeldahl Nitrogen
10400 3500 mg/kg dry
7001 3390 101 90-110
Matrix Spike Cup (P9A0037-MSD1)
Source: 9010010.01
Prepared: 01/03/19 Analyzed: 01/04/19
Total Kjeldahl Nitrogen
10400 3500 mg/kg dry
7001 3390 101 90-110 0.03 20
Batch PRA0038 - NO PREP
Blank (P9A0038-BLK1)
Prepared &Analyzed: 01/03/19
Nitrate/Nitrite as N
BRL 5.0 mg/kg wet
LCS (P9A0038-BSI)
Prepared &Analyzed: 01/03/19
Nitrate/Nitrite as N
48.0 5.0 mg/kg wet
50.00 96 80-120
Matrix Spike (P9A0038-MS1)
Source: 9010010-01
Prepared &Analyzed: 01/03/19
Nitrate/Nitrite as N
71.6 7.0 mg/kg dry
70.01 2.52 99 80-120
Matrix Spike Dup (P9A0038-MSDI)
Source: 9010010.01
Prepared &Analyzed: 01/03/19
Nitrate/Nitrite as N
70.8 7.0 mg/kg dry
70.01 2.52 98 80-120 1 20
Batch P9AO057 - SM4500-PB5
Blank (PM0057-131_1<1) Prepared &Analyzed: 01/07/19
Phosphorus -Total BRL 2.5 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0643
Phone: [phone]- Tall Free Number: 1.8001629-6364- Fax: [phone] Page 13 of 17

FjISMFull -Service Analytical &
Environmental Solutions
uem�aoaaa we
Level II QC Report
5/8/19
City of Statesville, NC Project: Stal-ime (Otrly, BiWeekly, 60Day
Attn: Andy Smith 7 Fecal)
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source
Analyle Result Limit Units Level Result
Prism Work Order: 9010010
Time Submitted: 1/3/2019 8:00:00AM
%REC RPD
%RFC i imlm Pon I ImJ ._.
Batch P9A0057 - SM4500-PB5
LCS (P9A0067-BSI) Prepared &Analyzed: 01/07/19
Phosphorus -Total 91.6 2.5 mg/kg wet 100.0 92 90-110
Matrix Spike (P9A0057-MS1) Source: 9010010.01 Prepared &Analyzed: 01/07/19
Phosphorus -Total 2940 70 mg/kg dry 140.0 2320 438 80-120 MC
Matrix Spike DuP(P9A0B57-MSD1) Source: 9010010-01 Prepared&Analyzed: 01/07/19
Phosphorus -Total 2900 70 mg/kg dry 140.0 2320 411 80-120 1 20 Mc
Batch P9A0089 - SM4500-NH3 B
Blank (PSA0089-BLK1) Prepared &Analyzed: 01/07/19
Ammonia as N BRL 10 mg/kg wet
LCS (P9A0089-BSI) Prepared &Analyzed: 01/07/19
Ammonia as N 498 10 mg/kg wet 500.0 100 80-120
Matrix Spike(P9A(D089-MS1) _ Source: 9010010-01 Prepared&Analyzed: 01/07/19
Ammonia as N 761 14 mg/kg dry 686.4 303 67 80-120
Batch P9A0141 - NO PREP
Duplicate (P9A0141-DUP2) Source: 9010010-04 Prepared &Analyzed: 01/08/19
Solids 72.0 0.100 % by Weight 72.0 0.1 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 14 of 17

Level II QC Report
I S I� A I Full -Service envlronmental Analytical a
' V' Solclutlona 5/8/19
uwuronietiac
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 6ODay Prism Work Order: 9010010
Attn: Andy Smith 7 Fecal) Time Submitted: 1/3/2019 8:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
AnaMe Result Limit Units Level Result %REC Limits RPD Limit Nntee
Batch MOM. - NO PREP
Blank (PSA0065-BLK7) Prepared &Analyzed: 01/03/19
Fecal Coliforrns BRL 0.2 MPN/gwel
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Date/Time
9010010-01 P9A0037 0.05 g 25 mL 01/03/19 9:50
Prep Method: SM4500-NH3 B
Lab Number Batch Initial Final Date/Time
9010010-01
Prep Method: SM4500-PBS
Lab Number
P9A0089
Batch
1.06 9
Initial
50 mL
Final
01/07/19 10:48
Date/Time
9010010-01
P9A0057
1 g
50 mL
01/07/19 6:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
9010010-01
P9A0056
50 mL
50 mL
01/04/19 9:22
9010010-01
PRA0056
50 mL
50 mL
01/04/19 9:22
9010010-01
P9A0056
50 mL
50 mL
01/04/19 9:22
9010010-01
P9A0056
50 mL
50 mL
01/04/19 9:22
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Datemme
9010010-01
P9A0055 2 g
50 mL
01/04/19 7:50
Prep Method: 7471 B
Lab Number
Batch Initial
Final
Date/Time
9010010-01 P9A0078
Prep Method: SAR 2-78-054
Lab Number Batch
0.6 g 50 mL 01/07/19 8:35
Initial Final Date/Time
9010010-01 POA0046 250 g
250 g 01/03/19 14:45
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629.6364 - Fax: [phone]
Page 15 of 17
i

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16 of 17

Main Office:
449 Springbrook Road
PtiR I S M I Full SDTWI a Analytical and P.O. Box 240543
Environmonl Al Solutions Charlotte, NC 28224.0543
"V �O.TOf1E61Na Phone: [phone]
118001529-6364
Fax: [phone]
www.prismiabs.com
Sodium Absorption Ratio
The amount of exchangeable sodium ions versus the amount of exchangeable
calcium & magnesium ions in a given material.
Sample Numberl 9010010 1 Sample Name Sta-Lime
Na: Sodium (mg/L) Equivalent weight: 23
Ca : Calcium (mg/L) Equivalent weight: 20
Mg : Magnesium (mg/L) Equivalent weight: 12
Milli Equivalent (ME) = mg/L / Equivalent weight
Na12m8.0/L am0L m/L,
M
Na ME
Ca lME1
Mg (ME)
5.57
67.00
0.00
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent+ Mg Milli equivalent)]0.5 power
SAR = 1.0 (From mg/L entered above)
Calculated By:
Page 17 of 17

PRISM
L _ IABOFATOaIE$ INC
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cart No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime
Lab Submittal Date: 02/04/2019
Prism Work Order: 9020029
Case Narrative
5/8119 10:14
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are Flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the original laboratory report dated 2/13/19. PAN Equation has
been added to Case Narrative.
Analysls note for SAR;
BAR =[Naj/SORT (( (Cal +(Mgj)/2}
BAR - [224/23.01 / SORT ( (11640/20.01 + [0/12.21) / 2 }
SAR = 1.6
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SORT designates
taking the square root of the operand in parentheses.
PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) +
Nitrate —Nitrite
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
PAN Equation = 0.3 * (1900 — 240) + 0.5 * (240) + 9.6
PAN = <1200 mg/kg
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0643
Phone: [phone]- Toll Free Number: 1-8001629-6364- Fax: [phone] Page 1 of 10

Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a- 9-OV-1
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference
Reviewed By Robbi A. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
DM Sample diluted and RL increased due to the matrix.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone]- Toll Free Number: 1-800/529-6364-Fax: [phone] Paget of 10

9
&Gkk�
I S M I Full-Sarvlce Analytical 8
Environmental Solutions
7ineovaoeies ixc
Sample Receipt Summary
05/08/2019
Prism Work Order: 9020029
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
StaLime (and Fecal 1) 9020029-01 Solid 02/04/19 11:37 02/04/19 13:26
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224.0643
Phone: [phone] -Toll Free Number; 1-800/629-6364- Fax: [phone] Page 3of10 >

&k.? I S M I Fullrvlce AnalyticalEviroiro nmental 6olutlons
Wuwuroa,ra,ac
Laboratory Report
05/08/2019
City of Statesville, INC
Project: Stal-ime
Client Sample ID:
Stat-ime (and Fecal 1)
Attn: Ken Galloway
Prism Sample ID:
9020029-01
P.O. Box 1111
Prism Work Order: 9020029
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/04/19 11:37
Time Submitted: 02/04/19 13:26
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Tme
ID
General Chemistry Parameters
Plant Available Nitrogen
BRL
mg/kg dry
1200
340
5
'Calculation
2/7/19 16:02
CLB
[CAI -CI
Solids
66.4
% by
0.100
0.100
1
'SM2540 G
218/19 9:20
KBS
P980100
Weight
Ammonia as N
240
mg/kg dry
15
3.7
1
'SM4500-NHS C 217119 16:02
BMS
P980090
Nitrate/Nitrite as N
9.6
mg/kg dry
7.6
2.1
1
'SM4500-NO3
F 2f7/19 10:38
CLB
P9130084
Phosphorus -Total
3400
mg/kg dry
76
17
20
'SM4600-PF
218119 9:40
CLB
P9130038
Total Kjeldahl Nitrogen
BRL
mg/kg dry
3800
1100
5
'351.2
2/6/19 10:52
CLB
P980051
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
'SM9221E
214/1913:17
BMS
P9130061
Total Metals
Mercury
0.079
mg/kg dry
0.031
0.0029
1
'7471B
2/8119 12:16
ICP
P9130118
BAR Soil Preparation
Complete
g
1
'2-78-054
2/6/19 10:15
MMR
PRB0047
SAR Percent Moisture
Complete
%by
0,100
0.100
1
'2-78-054
217/19 10:15
MMR
P9130079
Weight
Arsenic
BRLDM
mg/kg dry
76
4.7
100
'6010D
2/11/19 19:58
JAB
P9130072
Sodium Absorption Ratio
1.6
[blank]
0.30
0.016
1
'2-78-064
218/19 9:31
JAB
P980078
Cadmium
BRLDM
mg/kg dry
38
1.0
100
•6010D
2/11/19 19:58
JAB
P9130072
Calcium, SAR
1600 all, B
mg/L
10
1.0
100
'6010D
218119 9:31
JAB
P9130078
Copper
BRLDM
mg/kg dry
76
6.9
100
'6010D
2/11/19 19:58
JAB
P980072
Lead
BRLDM
mg/kg dry
38
7.1
100
'6010D
2111119 19:58
JAB
P980072
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
'60100
2/8119 9:31
JAB
P9130078
Nickel
BRLDM
mg/kg dry
76
2.8
100
'6010D
2/11/19 19:58
JAB
P9B0072
Potassium
3900 DM
mg/kg dry
1900
69
100
'6010D
2111119 19:58
JAB
P9190072
Selenium
BRLDM
mg/kg dry
76
18
100
'6010D
2/11/19 19:58
JAB
P9130072
Sodium
BRLDM
mg/kg dry
2300
75
100
"6010D
2/11/19 19:58
JAB
P9B0072
Sodium, SAR
220 BB, a
mg/L
50
1.8
100
'6010D
218119 9:31
JAB
P980078
Zinc
BRLDM
mg/kg dry
380
14
100
'6010D
2/11/19 19:58
JAB
P960072
This report should not be reproduced, except in its entirety, without the written consent or Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone]
Page 4 of 10

® R4 Full-seme a Level II QC ReportI S M I Environmental Solutions 5/8/19
7 Mei64 iNG
City of Statesville, NC Project: Stal-ime Prism Work Order: 9020029
Attn: Ken Galloway Time Submitted: 2/4/2019 1:26:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals -Quality Control
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9B0047 - SAR 2-78-054
Blank (P9B0047-BLK1)
Prepared: 02/05/19 Analyzed: 02/06/19
SAR Soil Preparation
Complete
g
Batch P9B0072 - 3050B
Blank (P9B0072-BLKI)
Prepared: 02/06/19 Analyzed: 02/07/19
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
'
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P9B0072-BS1)
Prepared: 02/06/19 Analyzed: 02/07/19
Arsenic
11.7
0.50
mg/kg wet
12.50 94 80-120
Cadmium
11.7
0.25
mg/kg wet
12.50 94 80-120
Copper
12.0
0.50
mglkg wet
12.50 96 80-120
Lead
11.8
0.25
mg/kg wet
12.50 94 80-120
Nickel
11.8
0.50
mg/kg wet
12.50 94 80-120
Potassium
1210
12
mg/kg wet
1250 97 80-120
Selenium
11.1
0.50
mg/kg wet
12.50 89 80-120
Sodium
1180
15
mg/kg wet
1250 95 80-120
Zinc
11.1
2.5
mg/kg wet
12.50 89 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-D543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 5 of 10 1 V_

Level II QC Report
ISMFulk8ervice Analytical a
Environmental Solutions $/8/19
uwrvroaac iuc
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P9B0078 - 3010A
Project: Stal-ime
Reporting
Result Limit Units
Prism Work Order: 9020029
Time Submitted: 2/4/2019 1:26:00PM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9B0078-BLKI)
Prepared: 02/06/19 Analyzed: 02/08/19
Sodium Absorption Ratio
BRL
0.30
[blank]
Calcium, SAR
1.26
0.10
mg/L BH
Magnesium, SAR
BRL
0.10
mg/L
Sodium, SAR
2.46
0.50
mg/L BH
Batch P9B0079 - NO PREP
Duplicate(PSB0079-DUP1) Source: 9020029.01 Prepared: 02/06/19 Analyzed: 02/07/19
SAR Percent Moisture Complete 0.100 % by Weight Complete 8 200
Batch P900118 - 7471 B
Blank (P9B0118-BLKI) Prepared &Analyzed: 02/08/19
Mercury BRL 0.020 mg/kg wet
LCS (P9B0118-BSI) Prepared &Analyzed: 02/08/19
Mercury 0.428 0.020 mg/kg wet 0.4167 103 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone]- Toll Free Number: 1.8001629-6364 - Fax: [phone] Page of 10

vice
Anayncel8I V VI Environmental Solution.
u&auro&i&&ixc
Level II QC Report
518/19
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime
Prism Work Order: 9020029
Time Submitted: 2/4/2019 1:26:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9B0038 - SM4500-PBS
Blank (P9B0038-BLK1) Prepared &Analyzed: 02/05/19
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P9B0038-BS1) Prepared &Analyzed: 02/05/19
Phosphorus -Total 103 2.5 mg/kg wet 100.0 103 90-110
Batch PSB0051 - 351.2
Blank (PSB0051-BLK1)
Prepared: 02/05/19 Analyzed: 02/06/19
Total Kjeldahl Nitrogen
BRL 50 mg/kg wet
LCS (P9B0051-BSI)
Prepared: 02/05/19 Analyzed: 02/06/19
Total Kjeldahl Nitrogen
128 50 mg/kg wet
125.0 102 90-110
Matrix Spike (PSB0051-MS1)
Source: 9020029-01
Prepared: 02/05/19 Analyzed: 02/06/19
Total Kjeldahl Nitrogen
11800 3800 mg/kg dry
7642 3710 106 90-110
Matrix Spike Dup (P9B0051-MSD1)
Source: 9020029.01
Prepared: 02/05/19 Analyzed: 02/06/19
Total Kjeldahl Nitrogen
11300 3800 mg/kg dry
7642 3710 99 90-110 5 20
Batch P9B0084 - NO PREP
Blank (P9B0084-BLK1) Prepared &Analyzed: 02/07/19
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P9B0084-BSI) Prepared &Analyzed: 02/07/19
Nitrate/Nitrite. as 50.0 5.0 mg/kg wet 50.00 100 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 7 of 10

IJIVI I
�n Full -Service Anelyticel8 Level II QC Report
r� Environmental Solutions 5/8/19
uaauroa,aa ma
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - quality Control
Project: Stal-ime
Prism Work Order: 9020029
Time Submitted: 2/4/2019 1:26:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9B0084 - NO PREP
Matrix Spike(P980084WS1)
Source: 9020029.01
Prepared&Analyzed: 02/07/19
Nitrate/Nitrite as N
Matrix Spike Dup(P9B0084-MSD1)
83.1 7.6 mg/kg dry
Source: 9020029-01
76.42 9.63 96 80-120
Prepared&Analyzed: 02/07/19
Nitrate/Nitrite as N
Batch P9B0090 - SM4600-NH3 B
84.6 7.6 mg/kg dry
76.42 9.63 98 80-120 2 20
Blank (P980090-13LK7)
Prepared &Analyzed: 02/07/19
Ammonia as N
LCS (P960090-13151)
BRL 10 mg/kg wet
Prepared &Analyzed: 02/07/19
Ammonia as N
Matrix Spike (P9130090-MSt)
524 10 mg/k9 wet
Source: 9020029-01
500.0 105 80-120
Prepared &Analyzed: 02/07/19
Ammonia as N
Matrix Spike Dup (P9B0090-MSD1)
1020 15 mg/kg dry
Source: 9020029-01
764.2 237 103 80-120
Prepared &Analyzed: 02/07/19
Ammonia as N
1020 15 mg/kg dry
734.8 237 107 80-120 0.2 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224.0643
Phone: [phone]- Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8of 10

Level II QC Report
I S I� A I FM,.rMce Analyrlcel &
'v' Envlronmenlal Solutions
5/8/19
rooaa ixc
City of Statesville, NC
Project: Stal-ime
Prism Work Order: 9020029
Attn: Ken Galloway
Time Submitted: 2/4/2019 1:26:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters -Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P9130061 - NO PREP
Blank (P9B0061-BLKi)
Prepared &Analyzed: 02/04/19
Fecal Coliforms
BRL
0.2
MPN/gwet
Sample Extraction
Data
Prep Method: 351.2
Lab Number Batch
Initial
Final
DatoMme
9020029-01 P9B0051
0,05 g
25 mL
02/05/19 10:50 '
Prep Method: SM4600-NH3 B
Lab Number Batch
Initial
Final
Date/Time
9020029-01 P9B0090
1.03 g
50 mL
02/07/19 9:25
Prep Method: SM4600-PB6
Lab Number Batch
Initial
Final
Date/Time
9020029-01 P9130038
1 g
50 mL
02/05/19 6:15
Prep Method: 3010A
Lab Number Batch
Initial
Final
Date/Time
9020029-01 P980078
50 mL
50 mL
02/06/19 10:10
9020029-01 P9B0078
50 mL
50 mL
02/06/19 10:10
Prep Method: 3050B
Lab Number Batch
Initial
Final
Date/Time
9020029-01 P9B0072
2 g
50 mL
02/06/19 8:35
Prep Method: 7471E
Lab Number Batch
Initial
Final
Datemme
9020029-01 P980118
0.6 g
50 mL
02/08/19 9:05
Prep Method: BAR 2-78-064
Lab Number Batch
Initial
Final
Date/Time
9020029-01 P9130047
250 g
250 g
02/05/19 10:15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 Of 10

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NC Certification No. 402
Case Narrative
P R I S M I Full -Service Analytical & NC Drinking Water Can No. 37735 5/31/19 13 15
Environmental Solutions SC Certification No. 99012 ®/'IA90RAi0RIEA ING
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 05/22/2019
Prism Work Order: 9050402
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR =[Na)/SORT (([Cal+(Mg))/2}
SAR = [150123) / SORT { ( [2600/20] + [-0.034/12.21) / 2 }
SAR = 0.79
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SORT designates
taking the square root of the operand in parentheses.
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) +
Nitrate —Nitrite
PAN = 0.3 * (5000 — 210) + 0.5 * (210) + 2.9
PAN = 1500 mg/kg
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]- Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 17

Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference
Reviewed By Robbi A. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
Bld MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: l-800/529.6364- Fax: [phone] Page 2of17

.P R I S M I Full -Service Analytical S
Enviranmenlal Solutions
Sample Receipt Summary
05/31/2019
Prism Work Order: 9050402
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
Stal-ime (and Fecal 1)
9050402-01
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #2
9050402-02
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #3
9050402-03
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #4
9050402-04
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #5
9050402-05
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #6
9050402-06
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #7
9050402-07
Solid
05/22/19
9:00
05/22/19 14:15
Samples were received in good condition at 3.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0543
Phone: [phone]-Toll Free Number: 1-8001629-6364-Fax:[phone] Page3of17

SI RISM I Full-sereca Anatylyucatiol&
s
Environmental Solutions
.oas., nc
Laboratory Report
05/31/2019
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: StaLime (and Fecal 1)
Attn: Ken Galloway
60Day 7 Fecal)
Prism Sample ID: 9050402-01
P.O. Box 1111
Prism Work Order: 9050402
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor DateMme
ID
General Chemistry Parameters
Plant Available Nitrogen
1600
mg/kg dry
18
6.4
2 'Calculation 6129119 11:02
CLB
[CALC]
Solids
71.6
% by
0.100
0.100
1 •SM2640 G 6128/19 9:06
KBs
P9E0457
Weight
Ammonia as N
210
mg/kg dry
14
3.6
1 'SM4500-NH3 C 6123/19 15:04
BMS
P9E0427
Nitrate/Nitrite as N
BRL
mg/kg dry
7.0
1.9
1 'SM4500-NO3 F 5/24/19 8:42
CLB
P9E0441
Phosphorus -Total
3100
mg/kg dry
140
42
20 'SM4600-PF 6130/19 7:21
CLB
PSE0483
Total Kjeldahl Nitrogen
6000
mg/kg dry
28
13
2 '351.2 6/29119 11:02
CLB
P9E0475
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 'SM9221 E 5/22119 14:45
BMS
P9E0433
Total Metals
Mercury
BRL
mg/kg dry
0.070
0.024
1 '7471B 5/29/19 10:54
MMR
P9E0477
BAR Soil Preparation
Complete
g
1 '2-78-054 5/24/19 10:30
JAB
POE0426
SAR Percent Moisture
62.8
% by
0.100
0.100
1 '2-78-054 5128119 9:16
MMR
P9E0464
Weight
Arsenic
4.2
mg/kg dry
1.4
0.18
1 '6010D 6/29119 17:67
JAB
PSE0438
Sodium Absorption Ratio
0.79
[blank]
0.30
0.016
1 '2.78-054 6/30/19 8:46
JAB
P9E0453
Cadmium
BRL
mg/kg dry
0.70
0.047
1 '6010D 5/29/19 17:57
JAB
P9E0438
Calcium, SAR
2600
mg/L
5o
0.60
50 '6010D 5/30/19 8:46
JAB
P9E0463
Copper
300
mg/kg dry
170
24
50 '6010D 5/29119 17:49
JAB
P9E0438
Lead
BRL
mg/kg dry
1.4
0.23
1 `6010D 5/29119 17:57
JAB
P9E0438
Magnesium, SAR
BRL
mg/L
0.10
0.0088
1 '6010D 5/30/19 846
JAB
P9E0453
Nickel
37
mg/kg dry
1.4
0.42
1 '6010D 6/29119 17:67
JAB
P9E0438
Potassium
27000
mg/kg dry
7000
730
60 •6010D 5/29/19 17:49
JAB
P9E0438
Selenium
12
mg/kg dry
1.4
0.38
1 '6010D 6129119 17:57
JAB
PSE0438
Sodium
4800
mg/kg dry
140
19
1 '6010D 5/29/19 17:57
JAB
P9E0438
Sodium, SAR
160 s
mg/L
25
0.90
5o '6010D 6130119 8:46
JAB
PSE0453
Zinc
BRL
mg/kg dry
14
2.0
1 '6010D 5/29119 17:57
JAB
P9E0438
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0643
Phone: [phone]- Toil Free Number: 1-800/529-6364- Fax: [phone] Page 4of 17

R Fun -Service Analytical s
I S M I
Environmental Solutions
®ueo,vmect n,c
Laboratory Report
05/31 /2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #2
Prism Sample ID: 9050402-02
Prism Work Order: 9050402
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch
Limit Factor DateRme ID
General Chemistry Parameters
Solids 70.3 % by 0.100 0.100 1 'SM2640 G 6128/19 9:06 KBS P9E0467
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221E 5/22/1914:45 BMS P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 � Fax: [phone] Page 5 of 17

r
I V I V I I Full-fieMoe Ae u
Envlronm.n[al Solutions
figg..m.nosse 1.
Laboratory Report
05/31/2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #3
Prism Sample ID: 9050402-03
Prism Work Order: 9050402
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateRme ID
General Chemistry Parameters
Solids 68.2 % by 0.100 0.100 1 'SM2640 G 6128/19 9:05 KBS P9E0457
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 5/22/19 14:45 BMS P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/629-6364- Fax: [phone] Page 6of17
t

SIPi Full -Service Analytical&
R I S M I Environmental Solutions
a..eom.oaaa,sa
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/31/2019
Client Sample ID: Fecal #4
Prism Sample ID: 9050402-04
Prism Work Order: 9050402
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateRme ID
General Chemistry Parameters
Solids 71.2 % by 0.100 0.100 1 'SM2540 G 6128119 9:06 Kay PSE0457
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 5/22/19 14:45 BMS P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 7 of 17

i
JP I S M I Full-Servlce Analytical a
Environmental Solution.
r.aonna.ac sac
Laboratory Report
05/31/2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, INC 28687
Parameter
Result
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #5
Prism Sample ID: 9050402-05
Prism Work Order: 9050402
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Units Report MOIL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 68.9 % by 0.100 0.100 1 'SM2640 G 6/28119 9:05 KBS PSE0457
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221E 5122/1914:45 BIAS P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone]- Toll Free Number: l-800/529-6364-Fax: [phone] Page 8of 17

1 j
n� I Fun-Servlce Analytical &
V' Environmental Solution.
A5lavom'.
Laboratory Report
05/31/2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #6
Prism Sample ID: 9050402-06
Prism Work Order: 9050402
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch
Limit Factor Datemme ID
General Chemistry Parameters
Solids 69.0 % by 0.100 0.100 1 'SM2540 G 6128/19 9:06 KBS P9E0457
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221E 5/2211914:45 BMS P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone]- Toll Free Number: 1.8001529-6364- Fax: [phone] Page 9of 17 -

1��� I l� �t I Full-Servlce Analytical &
' V' Environmental Solutions
7w.auoeaa,uc
Laboratory Report
05/31/2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #7
Prism Sample ID: 9050402-07
Prism Work Order: 9050402
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
General Chemistry Parameters
Solids 70.2 % by 0.100 0.100 1 'SM2640 G 6/28119 9:06 KBS P9E0457
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 5/22/19 14:45 BMS P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone]-Toll Free Number: 1-8001529-6364- Fax: [phone] Page 10of 17

Level II QC Report
�P I S M I Full -Service Aneryllcal a
Envlronmentel Solutions 5/31/19
uoauroxrumc
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, 6ODay Prism Work Order: 9050402
Attn: Ken Galloway 7 Fecal) Time Submitted: 5/22/2019 2:15:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9EO426 - SAR 2.78.054
Blank (P9E0426-BLK1) Prepared: 05/23/19 Analyzed: 05/24/19
SAR Soil Preparation Complete g
Batch P9E0438 - 3060B
Blank (PSE0438-BLK1)
Prepared: 05/24/19 Analyzed: 05/28/19
Arsenic
BRL
1.0
mg/kg wet
Cadmium
BRL
0.50
mg/kg wet
Copper
BRL
2.5
mg/kg wet
Lead
BRL
1.0
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
100
mg/kg wet
Selenium
BRL
1.0
mg/kg wet
Sodium
BRL
100
mg/kg wet
Zinc
BRL
10
fill wet
LCS (P9E0438-BS1)
Prepared: 05/24/19 Analyzed: 05/28/19
Arsenic
12.1
1.0
mg/kg wet
12.50 97 80-120
Cadmium
12.1
0.50
mg/kg wet
12.50 97 80-120
Copper
12.9
2.5
mg/kg wet
12.50 103 80-120
Lead
12.2
1.0
mg/kg wet
12.50 98 80-120
Nickel
12.2
1.0
mg/kg wet
12.50 98 80-120
Potassium
1220
100
mg/kg wet
1250 97 80-120
Selenium
11.7
1.0
mg/kg wet
12.50 93 80-120
Sodium
1230
100
mg/kg wet
1250 98 80-120
Zinc
12.0
10
mg/kg wet
12.50 96 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543 -
Phone: [phone] - Toll Free Number: 1-800/629-6364- Fax: [phone] Page 11 Of 17 =-

I n A Full -Service Analytical &
r� ' V' I Environmental Solutions
m Ia%INC.
Level II QC Report
5/31/19
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P9E0453 - 3010A
Project: Stal-ime (Qtrly, Biweekly, 60Day
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Prism Work Order: 9050402
Time Submitted: 5/22/2019 2:15:OOPM
%REC RPD
%REC Limits RPD Limit Notes
Blank (P9E0453-BLK1) Prepared: 05/24/19 Analyzed: 05/30/19
Calcium, SAR BRL 1.0 mg/L
Magnesium, SAR BRL 0.10 mg/L
Sodium, SAR 2.00 0.50 mg/L BH
Batch P9E0464 - NO PREP
Duplicate (P9E0464-DUP1) Source: 9050402.01 Prepared: 05/24/19 Analyzed: 05/28/19
SAR Percent Moisture 53.1 0.100 % by Weight 52.8 0.6 200
Batch P9E0477.747181
Blank (P9E0477-BLK1) Prepared &Analyzed: 05/29/19
Mercury BRL 0.050 mg/kg wet
LCS (P9E0477-BS1) Prepared &Analyzed: 05/29/19
Mercury 0.411 0.050 mg/kg wet 0.4167 99 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 23224.0543
Phone: [phone] - Toll Free Number: 1-800/529-6364- Fax: 704/525A409 Page 12 of 17

i
Level II QC Report
IP R I S M I Environwlcemental
al Solution 8
2 Environmental Solutions & 5/31/19
.oxirsixa
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters -Quality Control
Analyte
Batch P9E0427 - SM4500-NH3 B
Project: Stal-ime (Qtrly, BiWeekly, 60Day Prism Work Order: 9050402
7 Fecal) Time Submitted: 5/22/2019 2:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9E0427-BLK1)
Prepared &Analyzed: 05/23/19
Ammonia as N
BRL 10 mg/kg wet
LCS (PSE0427-BSI)
Prepared &Analyzed: 05/23/19
Ammonia as N
507 10 mg/kg wet
500.0 101 80-120
Matrix Spike (PSE0427-MS1)
Source: 9050402-01
Prepared &Analyzed: 05/23/19
Ammonia as N
859 14 mg/kg dry
691.1 207 94 80-120
Matrix Spike Dup(P9E0427-MSD1)
Source: 9060402.01
Prepared &Analyzed: 05/23/19
Ammonia as N
866 14 mg/kg dry
684.3 207 96 80-120 0.8 200
Batch P9E0441 - NO PREP
Blank (P9E0441-BLK1)
Prepared &Analyzed: 05/24/19
Nitrate/Nitrite as N
BRL 5.0 mg/kg wet
LCS (P9E0441-BS1)
Prepared &Analyzed: 05/24/19
Nitrate/Nitrite as N
49.0 5.0 mg/kg wet
50.00 98 80-120
Matrix Spike (P9E0441-MS1)
Source: 9050402-01
Prepared &Analyzed: 05/24/19
Nitrate/Nitrite as N
73.0 7.0 mg/kg dry
69.80 5.79 96 80-120
Matrix Spike Dup (P9E0441-MSD1)
Source: 9050402-01
Prepared &Analyzed: 05/24/19
Nitrate/Nitrite as N
72.0 7.0 mg/kg dry
69.80 5.79 95 80-120 1 20
Batch P9E0457 - Solids, Dry Weight
Duplicate (P9E0457-DUP2) Source: 9050402-06 Prepared: 05/24/19 Analyzed: 05/28/19
Solids 69.5 0.100 % by Weight 69.0 0.6 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NO 28224-0643
Phone: [phone]- Toll Free Number: l-8001629-6364-Fax: [phone] Page 13 of 17

* 9 i Full-fieMee cal a Level II QC Report
®R I S M I Environmentalal Solutions 5131/19
*onirainc
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P9E0475 - 351.2
Project: StaLime (Qtrly, BiWeekly, 600ay
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Prism Work Order: 9050402
Time Submitted: 5/22/2019 2:15:OOPM
%REC RPD
%REC Limits RPD Limit Notes
Blank (129E0475-13LK1)
Prepared: 05/28/19 Analyzed: 05/29/19
Total Kjeldahl Nitrogen
BRL 1.0 mg/kg wet
LCS (P9E0475-BS1)
Prepared: 05/28/19 Analyzed: 05/29/19
Total Kjeldahl Nitrogen
124 1.0 mg/kg wet
125.0 100 90-110
Matrix Spike (P9E0475-MS1)
Source: 9060402-01
Prepared: 05/28/19 Analyzed: 05/29/19
Total Kjeldahl Nitrogen
10400 70 mg/kg dry
6980 4990 78 90-110
MI
Matrix Spike Dup (P9E0475.MSD1)
Source: 9050402.01
Prepared: 05/28/19 Analyzed: 05/29/19
Total Kjeldahl Nitrogen
11200 70 mg/kg dry
6980 4990 89 90-110 7
20 MI
Batch P9E0483 - SM4500-PBS
Blank (P9E0483-BLK1)
Prepared: 05/29/19 Analyzed: 05/30/19
Phosphorus -Total
BRL 5.0 mg/kg wet
LCS (1`9E0483-831)
Prepared: 05/29/19 Analyzed: 05/30/19
Phosphorus -Total
110 5.0 mg/kg wet
100.0 110 90-110
Matrix Spike (P9E0483-MS1)
Source: 9050402.01
Prepared: 05/29/19 Analyzed: 05/30/19
Phosphorus -Total
3030 140 mg/kg dry
139.6 3140 NR 80-120
MC
Matrix Spike Dup (P9E0483.MSD1)
Source: 9050402-01
Prepared: 05/29/19 Analyzed: 05/30/19
Phosphorus -Total
3050 140 mg/kg dry
139.6 3140 NR 80-120 0.5
20 MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone]-Toll Free Number: 1-8001629-6364- Fax: [phone] Page 14 of 17

kAGOR.
Full-Service Analytical&
ISM I Environmental Solutions
®u .'aawe
Level II QC Report
5/31/19
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters -Quality Control
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Prism Work Order: 9050402
Time Submitted: 5/22/2019 2:15:0013M
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9E0433 - NO PREP
Blank (P9E0433-BLKI) Prepared &Analyzed: 05/22/19
Fecal Coliforms BRL 0.2 MPN/gwet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15of17

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0475
0.05 g
25 mL
05/28/19 1L02
Prep Method: SM4500-NH3
B
Lab Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0427
1 g
50 mL
05/23/19 8,56
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Datemme
9050402-01
P9E0483
1 g
50 mL
05/29/19 10.00
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0457
30 g
30 il
05/24/19 16,10
9050402-02
P9E0457
30 g
30 g
05/24/19 16.10
9050402-03
P9E0457
30 g
30 g
05/24/19 16,10
9050402-04
P9E0457
30 g
30 g
05/24/19 16,10
9050402-05
PgE0457
30 g
30 g
05/24/19 16.10
9050402-06
P9E0457
30 g
30 g
05/24/19 16.10
9050402-07
P9E0457
30 g
30 g
05/24/19 16.10
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0453
50 mL
50 mL
05/24/19 11.00
9050402-01
P9E0453
50 mL
50 mL
05/24/19 11:00
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0438
2 g
50 mL
05/24/19 7:05
9050402-01
P9E0438
2 g
50 mL
05/24/19 7:05
Prep Method: 7471 B
Lab Number
Batch
Initial
Final
Date/Tme
9050402-01
P9E0477
0.6 g
50 mL
05/29/19 9:00
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/T ne
9050402-01
P9E0426
250 g
250 g
05/23/19 10.30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone]- Toll Free Number: l-800/629-6364-Fax: [phone] Page 16 Of 17 -

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17 of 17

NC Certification No. 402 Case Narrative
h�R I S M I Full -Service Analytical 8 NC Drinking Water Cart No. 37735 8/21/19 13:44
/Environmental Solutions SC Certification No. 99012
�%IAIlOMr0aIE8, INC
City of Statesville, NC Project: Sludge (Hazardous Testing)
Ken Galloway
P.O. Box 1111 Lab Submittal Date: 08/07/2019
Statesville, NC 28687 Prism Work Order: 9080093
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Herbicide analysis was subcontracted to AES. Reactivity analysis was subcontracted to GCAL,
Laboratory reports are attached.
Prism Summary of Detections does not include subcontracted data.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference
Reviewed By Robbi A. Jones
President/Project Manager
A Negative, Pass
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0543
Phone: [phone]-Toll Free Number: 1.8001629-6364 - Fax: [phone] Page 1of30

//' P R I S M I FWbSorvien al Solution s
environm&nlal Solutions
�.a�.on,ea,ua
Sample Receipt Summary
08/21/2019
Prism Work Order: 9080093
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
4th Creek Sludge 9080093-01 Solid 08/07/19 9:55 08/07/19 16:00
3rd Creek Sludge
Sta-Lime
9080093-02 Solid 08/07/19 9:45
9080093-03 Solid 08/07/19 9:30
Samples were received in good condition at 5.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
08/07/19 16:00
08/07/19 16:00
449 Springbrock Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Tall Free Number: 1-800/629-6364 - Fax: [phone] Page 2 of 30

ISM Laboratory Report
,r1i A� Full-SaMce Analyttios 08/21/2019
Environmental Solutions
rs INC
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Client Sample ID:
4th Creek Sludge
Attn: Ken Galloway
Prism Sample ID:
9080093-01
P.O. Box 1111
Prism Work Order: 9080093
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 08/07/19 09:55
Time Submitted: 08/07/19 16:00
Parameter
Result
Units
Report
MOIL
Dilution Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
14.7
% by
0.100
0.100
1 'SM2540 G
8/16/19 8:30
EDV
P9H0264
Weight
Corrosivity-pH
6.4
pH Units
1 '9046D
819119 13:40
BMS
P91-10161
Ignitability,
BRLA
mm/sec
0.10
1 '1030
8/9/19 825
BMS
P91-10143
Temperature
22
pH Units
1 '9045D
819119 13:40
BMS
P91-10161
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1 '1311 ZHE
8113119 7:30
TBL
P91-10174
TCLP Extraction
Complete
N/A
1 '1311
8/13/19 7:50
MMR
P91-10185
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000034
1 '7470A
8115/19 14:09
MMR
P91-10261
Arsenic
BRL
mg/L
0.10
0.030
1 '6010D
8/13119 17:06
JAB
P9H0203
Barium
8RL
mg/L
5.0
0.010
1 '6010D
8113/19 17:06
JAB
P91-10203
Cadmium
BRL
mg/L
0.025
0.0020
1 '6010D
8/13/19 17:06
JAB
P91-10203
Chromium
BRL
mg/L
0.25
0.015
1 '6010D
8/13119 1706
JAB
P91-10203
Lead
BRL
mg/L
0.050
0.020
1 '6010D
8/13/19 1706
JAB
P9H0203
Selenium
BRL
mg/L
0.15
0.063
1 '6010D
8/13119 17:06
JAB
P9H0203
Silver
BRL
mg/L
0.25
0,0045
1 '6010D
8113119 17:06
JAB
P91-10203
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00090
1 '8081B
8/14119 16:49
ZRC
P91-10227 _
Dieldrin
BRL
mg/L
0.00050
0.000068
1 '8081B
8/14/19 16:49
ZRC
P91-10227
Endrin
BRL
mg/L
0.00050
0.000068
1 '8081B
8/14119 16:49
ZRC
P91-10227 -
gamma-BHC
BRL
mg/L
0.00050
0.000030
1 '8081B
8/14/19 1649
ZRC
P91-10227
Heptachlor
BRL
mg/L
0.00050
0.000065
1 '8081B
8/14/19 1649
ZRC
P91-10227
Heptachlor Epoxide
BRL
mg/L
0.00050
0.00011
1 '8081B
8114/19 16:49
ZRC
PSH0227
Methoxychlor
BRL
mg/1-
0.00050
0.000090
1 '8081B
8/14119 1649
ZRC
1`91-10227
Toxaphene
BRL
mg/L
0.025
0.0018
1 '8081B
8/14/19 16:49
ZRC
P91-10227
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
82 %
13-186
Tetrachlorc-m-xylene
92 %
40-134
TCLP Semivolatile Organic Compounds by GCIMS
2,4,5-Tfichlorophenol
BRL
mg/L
0.25
0.0036
1 '8270E
8/13/19 1807
JMV
P91-10193
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0045
1 '8270E
8/13/19 1807
JMV
_
P91-10193
2,4-Dinitrotoluene
BRL
mg/L
0.012
0.0042
1 '8270E
8/13/19 1807
JMV
P91-10193
2-Methylphenol
BRL
mg/L
0.050
0.0024
1 '8270E
8/13/19 1807
JMV
P91-40193 -
3/4-Methylphenol
BRL
mg/L
0.050
0.0025
1 '8270E
8113/19 1807
JMV
P91-10193
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1 '8270E
8/13/19 18.07
JMV
P91-10193
Hexachlorobutadiene
BRL
mg/L
0.050
0.0045
1 '8270E
8/13/19 1807
JMV
POH0193
Hexachloroethane
BRL
mg/L
0.050
0.0037
1 '8270E
8/13119 18:07
JMV
POH0193 -
Nitrobenzene
BRL
mg/L
0.050
0.0038
1 '8270E
8/13/19 18:07
JMV
P9H0193 _
This report should not be reproduced, except in its entirety, without
the written consent of Prism Laboratories, Inc.
449 Springbrook
Road - P.O. Box 240543 - Charlotte,
NC
28224-0543
Phone: [phone]-Toll Free Number:
1-8001529-6364- Fax: [phone]
Page 3 Of 30

■ n Full -Service Analyticala
rP R I S M I Environmental fiolutiotlona
�MR
Laboratory Report
08/21/2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Client Sample ID: 4th Creek Sludge
Prism Sample ID: 9080093-01
Prism Work Order: 9080093
Time Collected: 08/07/19 09:55
Time Submitted: 08/07/19 16:00
Parameter Result units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateRme ID
Pentachlorophenol BRL mg/L 0.25 0.011 1 '8270E 8/13/19 18:07 JMV P9H0193
Pyridine BRL mg/L 0.25 0.0016 1 '8270E 8/13119 18:07 JMV P9110193
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
91 %
43-140
2-Fluorobiphenyl
97 %
44-119
2-Fluorophenol
65 %
19-119
Nitrobenzene-d5
90 %
44-120
Phenol-d5
42 %
11-52
Terphenyl-d14
98 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.0035
1
'8260D
8/13119 19:18
KDM
P91-10197
1,2-Dichloroethane
BRL
mg/L
0.025 0.0041
1
'8260D
8/13/19 19:18
KDM
P9110197
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.0042
1
'8260D
8113119 19:18
KDM
P9H0197
Benzene
BRL
mg/L
0.025 0.0034
1
-8260D
8/13/19 1918
KDM
P9H0197
Carbon Tetrachloride
BRL
mg/L
0.025 0.0055
1
'8260D
8/13119 19:18
KDM
P9H0197
Chlorobenzene
BRL
mg/L
5.0 0.0034
1
'8260D
8113/19 19:18
KDM
P91-0197
Chloroform
BRL
mg/L
0.30 0.0048
1
'8260D
8113/19 19:18
KDM
P9H0197
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/L
10 0.0078
1
'8260D
8/13119 19:18
KDM
P91-10197
Tetrachloroethylene
BRL
mg/L
0.035 0.0031
1
'8260D
8/13/19 19:18
KDM
P9110197
Trichloroethylene
BRL
mg/L
0.025 0.0046
1
'8260D
8/13/19 19:18
KDM
P9H0197
Vinyl chloride
BRL
mg/L
0.010 0.0041
1
-8260D
8/13/19 1918
KDM
P9110197
Surrogate
Recovery
Control Limits
4-BromoOuorobenzene 103 % 80-124
Dibromofluoromelhane 107 % 75-129
Toluene-d8 94 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 • Charlotte, NC 28224-0543
Phone: [phone]- Toll Free Number: 1-8001629-6364- Fax: [phone] Page 4 of 30

&WR.I S M I Fun -Service Analytical
Environmental 8oiutlons
7ueau.0aiec,ue
Laboratory Report
08/21 /2019
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Client Sample ID: 3rd Creek Sludge
Attn: Ken Galloway
Prism Sample ID: 9080093-02
P.O. Box 1111
Prism Work Order: 9080093
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 08/07/19 09:45
Time Submitted: 08/07/19 16:00
Parameter
Result Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor DateMme ID
General Chemistry Parameters
% Solids
18.6
% by 0.100
0.100 1 'SM2540 G
8116/19 8:30
EDV
P91-10264
Weight
Corrosivity-pH
4.4
pH Units
1 '904513
819119 13:40
BMS
PSH0161
Ignitability
BRLA
mm/sec 0.10
1 '1030
819/19 8:25
BMS
P91-10143
Temperature
22
pH Units
1 '904513
819/19 13:40
BMS
PSH0161
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
'1311 ZHE
8/13119 7:30
TBL
P9H0174
TCLP Extraction
Complete
N/A
1
'1311
8/13/19 7:50
MMR
P91-10185
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000034
1
'7470A
8/15/19 13:57
MMR
P9H0261
Arsenic
BRL
mg/L
0.10
0.030
1
'601 OD
8/13119 17:13
JAB
P91-10203
Barium
BRL
mg/L
5.0
0.010
1
'6010D
8/13119 17:13
JAB
P91-10203
Cadmium
BRL
mg/L
0.025
0.0020
1
'6010D
8/13/19 17:13
JAB
P9H0203
Chromium
BRL
mg/L
0.25
0.015
1
'6010D
8/13119 17:13
JAB
P91-10203
Lead
BRL
mg/L
0.050
0.020
1
'6010D
8/13/19 17:13
JAB
P9H0203
Selenium
BRL
mg/L
0.15
0.063
1
'6010D
8/13/19 17:13
JAB
P91-10203
Silver
BRL
mg/L
0.25
0.0045
1
'6010D
8/13/19 17:13
JAB
P9110203
TCLP Organochlorine Pesticides
by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00090
1
'80818
8/14119 1700
ZRC
P9110227
Dieldrin
BRL
mg/L
0.00050
0.000068
1
'8081B
8/14119 17:00
ZRC
P91-10227
Endrin
BRL
mg/L
0.00050
0.000068
1
'8081B
8114/19 17:00
ZRC
P9H0227
gamma-BHC
BRL
mg/L
0.00050
0.000030
1
'8081B
8/14119 17:00
ZRC
P9H0227
Heptachlor
BRL
mg/L
0.00050
0.000065
1
'8081B
8/14119 17:00
ZRC
P91-10227
Heptachlor Epoxide
BRL
mg/L
0.00050
0.00011
1
'80818
8114/19 17:00
ZRC
P9H0227
Methoxychlor
BRL
mg/L
0.00050
0.000090
1
'8081B
8/14119 17:00
ZRC
P91-10227
Toxaphene
BRL
mg/L
0.025
0.0018
1
'8081B
8/14/19 17:00
ZRC
P9H0227
Surrogate
Recovery
Control Limits
Decachlorobiphenyl 82 % 13-186
Tetrachloro-m-xylene 83 % 40-134
TCLP Semivolatile Organic Compounds by GCIMS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0036
1
'8270E
8/13/19 18:30
JMV
P9H0193
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0045
1
'8270E
8/13/19 18:30
JMV
P91-10193
2,4-Dinitrotoluene
BRL
mg/L
0.012
0.0042
1
'8270E
8/13119 18:30
JMV
PSH0193
2-Methylphenol
BRL
mg/L
0.050
0.0024
1
'8270E
8/13/19 18:30
JMV
P91-10193
3/4-Methylphenol
BRL
mg/L
0.050
0.0025
1
'8270E
8113/19 18:30
JMV
P9H0193
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1
'8270E
8113/19 18:30
JMV
P9110193
Hexachlorobutadiene
BRL
mg/L
0.050
0.0045
1
'8270E
8/13119 18:30
JMV
P91-10193
Hexachloroethane
BRL
mg/L
0.050
0.0037
1
'8270E
8113/19 18:30
JMV
P9110193
Nitrobenzene
BRL
mg/L
0.050
0.0038
1
'8270E
8/13/19 18:30
JMV
P91-10193
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1.8001629.6364 - Fax: [phone]
Page 5 of 30 -

I S n n I Full-earvlcs Analytloal a
' V' Environmental Solutions
ww..oarea iao
Laboratory Report
08121/2019
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Client Sample ID: 3rd Creek Sludge
Attn: Ken Galloway
Prism Sample ID: 9080093-02
P.O. Box 1111
Prism Work Order: 9080093
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 08/07/19 09:45
Time Submitted: 08/07/19 16:00
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Datemme ID
Peniachlorophenol
BRL mg/L
0.25 0.011
1 '8270E 8/13119 18:30 JMV P91-10193
Pyridine
BRL mg/L
0.25 0.0016
1 '8270E 8/13119 1830 JMV P91-10193
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
106 %
43-140
2-Fluorobiphenyl
IDS %
44-119
2-Fluorophenol
72%
19-119
Nitrobenzene-d5
94 %
44-12D
Phenol-d5
46 %
11-52
Terpheny1-d14
98%
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroelhylene
BRL
mg/L
0.035 0.0035
1
'8260D
8113/19 1952
KDM
P9110197
1,2-Dichloroethane
BRL
mg/L
0.025 0.0041
1
'8260D
8113119 1952
KDM
P9110197
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.0042
1
'8260D
8/13119 1952
KDM
P91-10197
Benzene
BRL
mg/L
0.025 0.0034
1
'8260D
8/13/19 19:52
KDM
P9H0197
Carbon Tetrachloride
BRL
mg/L
0.025 0.0055
1
'8260D
8/13119 19:52
KDM
POH0197
Chlorobenzene
BRL
mg/L
5.0 0.0034
1
'8260D
8/13/19 19:52
KDM
P91-10197
Chloroform
BRL
mg/L
0.30 0.0048
1
'8260D
8/13/19 19:52
KDM
P91-0197
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/1-
10 0.0078
1
'8260D
8/13/19 1952
KDM
P91-0197
Tetrachloroelhylene
BRL
mg/L
0.035 0.0031
1
'8260D
8113/191952
KDM
P91-10197
Trichloroethylene
BRL
mg/L
0.025 0.0046
1
'8260D
8113/19 19:52
KDM
P91-10197
Vinyl chloride
BRL
mg/L
0.010 0.0041
1
'8260D
8/13/19 19:52
KDM
P9H0197
Surrogate Recovery Control Limits
4-Bromofluorobenzene 104 % 80-124
Dibromoguoromethane 104 % 75-129
Toluene-d8 95 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 6 0f 30

J R I S M I Full -Service Analyticala
iOe Environmental Solutiodons
Laboratory Report
08/21/2019
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Client Sample ID: Sta-Lime
Attn: Ken Galloway
Prism Sample ID: 9080093-03
P.O. Box 1111
Prism Work Order: 9080093
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 08/07/19 09:30
Time Submitted: 08/07/19 16:00
Parameter
Result
Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor DateRme
ID
General Chemistry Parameters
% Solids
76.6
% by
0.100 0.100
1 `SM2640 G 8116/19 8:30
EDV
P91-10264
Weight
Corrosivity-pH
12
pH Units
1 '9046D 819/19 13:40
BMS
P91-40161
Ignitability
BRLA
mm/sec
0.10
1 '1030 8/9/19 8:25
BMS
P91-10143
Temperature
22
pH Units
1 '9045D 819119 13:40
BMS
P9H0161
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1 '1311 ZHE 8/13/19 7:30
TBL
P91-10174
TCLP Extraction
Complete
N/A
1 '1311 8/13/19 7:50
MMR
P91-40185
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000034
1
'7470A
8115/19 14:12
MMR
P9t10261
Arsenic
BRL
mg/L
0.10
0.030
1
'6010D
8/13119 17:21
JAB
P91-10203
Barium
BRL
mg/L
5.0
0.010
1
'6010D
8/13/19 17:21
JAB
P91-10203
Cadmium
BRL
mg/L
0.025
0.0020
1
'6010D
8113119 17:21
JAB
P91-10203
Chromium
BRL
mg/L
0.25
0.015
1
'6010D
8/13/19 17:21
JAB
P91-10203
Lead
BRL
mg/L
0.050
0.020
1
'6010D
8/13119 17:21
JAB
P91-10203
Selenium
BRL
mg/L
0.15
0.063
1
'6010D
8/13/19 1721
JAB
P91-10203
Silver
BRL
mg/L
0.25
0.0045
1
'6010D
8/13/19 1721
JAB
P91-10203
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00090
1
'8081B
8/14119 1712
ZRC
P91-10227
Dieldrin
BRL
mg/L
0.00050
0.000068
1
'8081B
8/14119 17:12
ZRC
P91-10227
Endrin
BRL
mg/L
0.00050
0.000068
1
'8081B
8/14/19 17:12
ZRC
P91-10227
gamma-BHC
BRL
mg/L
0.00050
0.000030
1
'8081B
8114/19 17:12
ZRC
P91-10227
Heptachlor
BRL
mg/L
0.00050
0.000065
1
'8081B
8114119 17:12
ZRC
P91-10227
Heptachlor Epoxide
BRL
mg/L
0.00050
0.00011
1
'8081B
8/14119 17:12
ZRC
P91-10227
Methoxychlor
BRL
mg/L
0,00050
0.000090
1
'8081B
8/14/19 17:12
ZRC
P91-10227
Toxaphene
BRL
mg/L
0.025
0.0018
1
'80818
8/14119 17:12
ZRC
P91-10227
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
75
%
13-186
Tetrachloro-m-xylene
97
%
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0036
1
'8270E
8/13/19 18:53
JMV
P91-10193
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0045
1
'8270E
8/13/19 18:53
JMV
P91-10193
2,4-Dinitrotoluene
BRL
mg/L
0.012
0.0042
1
'8270E
8/13/19 18:53
JMV
P91-10193
2-Methylphenol
BRL
mg/L
0.050
0.0024
1
'8270E
8/13/19 18:53
JMV
P91-10193
3/4-Methylphenol
BRL
mg/L
0.050
0.0025
1
'8270E
8/13/19 18:53
JMV
P91-10193
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1
'8270E
8113119 1853
JMV
P91-10183
Hexachlorobutadiene
BRL
mg/L
0.050
0.0045
1
'8270E
8/13/19 1853
JMV
P9H0193
Hexachloroethane
BRL
mg/L
0.050
0.0037
1
'8270E
8/13/19 1853
JMV
P91-10193
Nitrobenzene
BRL
mg/L
0.050
0.0038
1
'8270E
8/13/19 1853
JMV
P91-10193
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road • P.O. Box 240643 -Charlotte, NC 28224.0643
Phone: [phone]- Toll Free Number: 1-8001629-6364- Fax: [phone] Page 7of 30

/P R Fule Analytical sI S M I environmental Solutions
Toes% Iuc
Laboratory Report
08/21/2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Client Sample ID: Sta-Lime
Prism Sample ID: 9080093-03
Prism Work Order: 9080093
Time Collected: 08/07/19 09:30
Time Submitted: 08/07/19 16:00
Parameter
Result Units
Report MOIL Dilution
Limit Factor
Method Analysis Analyst Batch
Date/Time ID
Pentachlorophenol
BRL mg/L
0.25 0.011 1
`8270E 8/13/19 18:53 JMV P91-10193
Pyridine
BRL mg/L
0.25 0.0016 1
'8270E 8113119 18:53 JMV P91-10193
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
114 % 43-140
2-Fluorobiphenyl
104 % 44-119
2-Fluorophenol
73 % 19-119
Nitrobenzene-d5
92 % 44-120
Phenol-d5
46% 11-52
Terphenyl-d14
95 % 50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0,035
0.0035
1
'8260D
8/13/19 20:26
KOM
P9H0197
1,2-Dichloroethane
BRL
mg/L
0.025
0.0041
1
*82600
8/13119 20:26
KDM
P91-10197
1,4-Dichlorobenzene
BRL
mg/L
0.38
0.0042
1
'8260D
8/13/19 20:26
KDM
P91-10197
Benzene
BRL
mg/L
0.025
0.0034
1
'8260D
8/13119 20:26
KDM
P9H0197
Carbon Tetrachloride
BRL
mg/L
0.025
0.0055
1
•8260D
8/13119 20:26
KDM
P91-10197
Chlorobenzene
BRL
mg/L
5.0
0.0034
1
'8260D
8113119 20:26
KDM
P9H0197
Chloroform
BRL
mg/L
0.30
0.0048
1
'8260D
8/13/19 2026
KDM
P91-10197
Methyl Ethyl Ketone (2-Bulanone)
BRL
mg/L
10
0.0078
1
'8260D
8/13/19 2026
KDM
P9H0197
Tetrachloroethylene
BRL
mg/L
0.035
0.0031
1
'8260D
8/13/19 20:26
KDM
P91-10197
Trichloroethylene
BRL
mg/L
0.025
0.0046
1
'8260D
8/13/19 20:26
KDM
P91-10197
Vinyl chloride
BRL
mg/L
0.010
0.0041
1
'8260D
8/13119 20:26
KDM
P91-10197
Surrogate Recovery Control Limits
4-BromoBuorobenzene 101 % 80-124
Dibromofluoromethane 88% 75-129
Toluene-d8 96 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]- Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 30

Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P91-10264
30 g
30 g
08/15/19 15:05
9080093-02
P9H0264
30 g
30 g
08/15/19 15.05
9080093-03
P9H0264
30 g
30 g
08/15/19 1505
Prep Method: 1311
Lab Number
Batch
Initial
Final
DatelTime
9080093-01
P91-10185
100 g
2000 mL
08/12/19 15:45
9080093-01
P91-10174
12.5 g
250 mL
08/12/19 13,40
9080093-02
P91-10174
12.5 g
250 mL
08/12/19 13:40
9080093-02
P91-10185
100 g
2000 mL
08/12/19 15,45
9080093-03
P91-10185
100 g
2000 mL
08/12/19 15:45
9080093-03
P91-40174
12.5 g
250 mL
08/12/19 13:40
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P91-10203
10 mL
50 mL
08/13/19 10.43
9080093-02
P91-10203
10 mL
50 mL
08/13/19 1043
9080093-03
P91-10203
10 mL
50 mL
08/13/19 10:43
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P9H0261
20 mL
30 mL
08/15/19 10,30
9080093-02
P9H0261
20 mL
30 mL
08/15/19 1030
9080093-03
P9H0261
20 mL
30 mL
08/15/19 10,30
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P91-10227
200 mL
10 mL
08/14/19 9:08
9080093-02
1`91-10227
200 mL
10 mL
08/14/19 9:08
9080093-03
P91-10227
200 mL
10 mL
08/14/19 9:08
Prep Method: 3510C MS
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
1`91-10193
200 mL
1 mL
08/13/19 1030
9080093-02
P91-10193
200 mL
1 mL
08/13/19 10 30
9080093-03
P91-10193
200 mL
1 mL
08/13/19 10 30
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P9H0197
1 mL
10 mL
08/13/19 8:19
9080093-02
P91-10197
1 mL
10 mL
08/13/19 8:19
9080093-03
P91-10197
1 mL
10 mL
08/13/19 8,19
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643
Phone: [phone] - Toll Free Number: 1-800/529-6364- Fax: [phone] Page 9 of 30

Subcontracted Analyses
The following analyses were subcontracted to Analytical Environmental Services, Inc.
Lab.Number Analysis
9080093-01 Herbicides TCLP (Sub)
9080093-02 Herbicides TCLP (Sub)
9080093-03 Ilerbicidcs TCLP (Sub)
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab \'umber
Analysis
9090093-01
Reactivity, Cyanide (Sub)
9080093-01
Reactivity, Sulfide (Sub)
9080093-02
Reactivity, Cyanide (Sub)
9080093-02
Reactivity, Sulfide (Sub)
9080093-03
Reactivity, Cyanide (Sub)
9080093-03
Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone]- Toll Free Number: 1-800/529-6364- Fax: [phone] Page 10 of 30

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Paqe 11 of 30 ,

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
RobbiJones
PROJECTID
9080093
LABORATORY REPORT NUMBER
219081317
DATE
08/16/2019
Primary Data Review By Secondary Data Review By
Authorized Signature
PLEASE NOTE:
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820.
GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab If 618, GA certified lab # LA-01955,
NELAP certified laboratory # 01955
Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888. 315,4243
Lab Report#:219081317 Page 12 of 30

GCA
LELAP CERTIFICATE NUMBER: 01955
DOD -FLAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
PERFORMED BY
GCAL, LLC
7979Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 08/16/2019
ID��iIINI�'YIIIIIW
Project 9080093
Deliver To Additional Recipients
Robbi Jones NONE
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
800-529-6364
ISO
17025
PJLA
ieMIng
Dun MAP
-Q �CCR'p0-
ti (rT�11
9eORivoz
219081317 Pa e 2 of 12
Page 13 of 30

���� 1219081317
�� ,.,,, „ -, , ,;,,,,�_ ,_� Project ID: 9080093 Report Date: 08/16/2019
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations that may be Utilized In this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLO Indicates the analysis was performed in the Field
DL Defection Limit
LOD Limit of Defection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant OC Result (See Q Flag Application Report)
Indicates a non -compliant or not applicable QC recovery or RPD —see narrative
E Organics -The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis —when appended to Client Sample ID
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the Information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD OSM as specified in the contract if
applicable.
Authorized Signature
GCAL Report 219081317
Lab Report#: 219081317
Page 14 of 30

Q Gc14L
Report#: 219081317
Project ID: 9080093
Certifications
Report Date: 08/16/2019
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentuckv
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
06001
South Dakota
55
Tennessee
55
Texas
704178
F460215
Vermont
5
Virginia
Washin ton
9
USDA Sail Permit
P330-16-00234
Lab Report#: 219081317
Page 15 of 30

/� Report#: 219081317
Q 4 GC,&L Project ID: 9080093 Report Date: 08/16/2019
® Case Narrative
Client: Access Analytical Report: 219081317
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Lab Report#219081317
Page 16 of 30

I� GCAL
Report#: 219081317
Project ID: 9080093
Sample Summary
ReportDate: 08/16/2019
GOAL ID
Client ID
Matrix
Collect Date/Time
Receive Date/Time
21908131701
4th Creek Sludge
Solid
08/07/2019 09:55
08/13/2019 10:20
21908131702
3rd Creek Sludge
Solid
08/07/2019 09:45
08/13/2019 10:20
21908131703
Sta-Lime
Solid
08/07/2019 09:30
08/13/2019 10:20
Lab Report#: 219081317
Page 17 of 30

OW4 G SALL Report#: 219081317
&f , "Z 11 L. Project ID: 9080093 Report Date: 08/16/2019
Summary of Compounds Detected
No analytes were detected for analyses performed by GCAL.
Report#: 219081317 --
Page 18 of 30

�40 Report#: 908081317
,11 Project lD: 9080093 Report Date: 08/16/2019
Sample Results
14th Creek Sludge Collect Date 08107/201909:55 GCALID 21908131701
Receive Date 08/13/2019 10:20 Matrix Solid
E
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
OS/16/2019 08:00 665475 EPA 7.3.3.2 (1997) 1 081161201914:48 MOS 665678
CAS#
Parameter
Result
DL
LOQ
Units
57-12-5R
Reactivity Cyanide
248U
248
248
mg/kg
EPA 9034
Prep Date
Prep Batch Prep Method
Dilution Analysis Date
By
Analytical Batch
08/16/201908:00
665476 EPA 7.3.4.2(1997)
1 08/161201913:16
RYC
665676
CAS#
Parameter
Result
DL
LOQ
Units
18496-25-8R
Reactivity Sulfide
248U
248
248
mg/kg
Collect Date
08/071201909:45
GCALID
21908131702
3rd Creek Sludge
Receive Date
08/13/2019 10:20
Matrix
Solid
m
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/201908:00 665475 EPA 7.3.3.2(1997) 1 08/16/201914:50 MOS 665678
CAS#
Parameter
Result
OL
LOQ
Units
57-12-5R
Reactivity Cyanide
25OU
250
250
mg/kg
EPA 9034
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/201908:00 665476 EPA 7.3.4.2 (1997) 1 08/161201913:16 RYC 665676
CAS#
Parameter
Result
DL
LOQ
Units
18496-25-8R
Reactivity Sulfide
25OU
250
250
mg/kg
Lab Report#: 219081317 Pa e 8 of 12
Page 19 of 30

GC/�L Project ID: 908009317 Report Date: 08/16/2019
Sample Results
L ta-Lime Collect Date 08/07/2019 09:30 GCAL ID 21908131703
Receive Date 081131201910:20 Matrix Solid
E
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665475 EPA 7.3.3.2 (1997) 1 08/16/2019 14:53 MOS 665678
uAJe
Parameter
Result DL LOQ
Units
57-12-513
Reactivity Cyanide
248U 248 248
mg/kg
EPA 9034
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/1612019 08:00 665476 EPA 7.3.4.2 (1997) 1 08/16/2019 13:16 RYC 665676
CAS#
Parameter
Result
DL
LOQ
Units
18496-25-SR
Reactivity Sulfide
248U
248
248
mg/kg
219081317 --
Page 20 of 30

Q� GcIA4.
Report#: 219081317
Project ID: 9080093
General Chemistry QC Summary
Report Date: 08/16/2019
Analytical Batch Client ID
M6665476
LCS665476
665676 GOAL ID
1952122
1952123
Prep Batch Sample Type
MB
LCS
665476 Prep Dale
08/16/2019 08:00
08/16/2019 08:00
Prep Method Analysis Date
08/16/2019 13:16
08/16/2019 13:16
EPA 7.3,4.2 (1997) Matrix
Solid
Solid
EPA 9034
Units
mg
Spike
Result
%R
Control
Result
OL
Added
Limits%R
Reactivity Sulfide 18496-25-8R
250U
250
1000
1026
103
47 - 135
Analytical Batch Client ID
MB665475
475
665678 GCALID
1952119
Prep Batch Sample Type
MB
665475 Prep Date
08/16/2019 08:00
19 08:00
Prep Method Analysis Date
08/16/2019 14:39
1914:41
;Added
EPA 7.3.3.2 (1997 Matrix
Solid
EPA 9012B
Units
m9D9
ke
Result
% R
ntrol
Result
L mils % R
Reactivity Cyanide 57-12-5R
ND
250
29.4
12
1 - 25
Lab Report#: 219081317 Page 10 of 12
Page 21 of 30

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Sol �f 279061317
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SUBCONTRACT ORDER
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9080093 N1111
ILENDIM; 1.a110RnT0FI,
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➢Jsm Lab,..w, ics, Inc.
Gull Cunt Analysic0) Labs, Tor.
P. 0. Box 240543
107SI Cocrsc_Y Blvd
Chorlouq NC 23724-0543
Baton Rougc, LA 70916
Pgonc: 300-529-6364
Nmnc:(nS)769-490D
Fax: 7W.525-0409
F.: [phone]
N,p'. >.br.'+Sm: Robbi A. Jones
nmlitsis Due
Exphes Labs.,., ID Cnm,neno
SamP1e ID: 9080093-01 Solid
S.,Ie4: OW07/1909:55
Rcenie,, S016de(Sub)
W14A 909:55
Rcaclivitg Cyan de (Sab1
OS/21/1909:SS
S3mPIe ID: 909003-02 1+ Solid SamPW: 9aN711909:45 .5rJ Ge k JI��Pj f a
R e:niviry, SaiDJa (Sub) OY14;1909i5
iinai.iry, Cyanide (Sub) I MU1909:45
Cnna:uos Svpp Fr A.
1­,d. ID;911800Y3413 Solid SampIN:O&OM 09:39 Vk—
R c,uniry, S.M.&(Sub) 0SIM1909:30
Ronfeilq Cyanide(Sab) 03PIM909:30
0
a
sp
0
N
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Pap. 1 0l 1
Page 22 of 30

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Access
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbi A. Jones
PROJECTID
9080093
LABORATORY REPORT NUMBER
1908C31
DATE
August 19, 2019
Primate Data Review By Secondary Data Review By
Ashley Amick
Chris Pafford Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE:
Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab 9 EL-E87582,
NELAP certified laboratory # E87582
AIHA-LAP,LLC Laboratory ID:100671 for Indust) ial Hygiene samples (Organics, i\Icials, PCNI Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental \licrobiologp (Fungal)
Direct Examination.
Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative orAFS serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.791.4243 or toll fee at 883.315.4243
Pag Page 24 of 30

su h �o ��S a 1�o n 9I (2 1 E� S4�
r�w I g08C31
Full-S men Analytical S
j J Environmental Solutions
SUBCONTRACT ORDER
Ccnificalion. ELAC_ USAGE_
Prism Lahnratories�Inc. NC'_ SC_Other
9080093
SENDING LARORATORY:
RECEIVIN'G I ABORATOAV,
Prism Lobomtories, Inc.
Analytical Pnvimnmental Services; Mc.
P. 0. Be, 240543
30SO Presidential P.,kwny
Charla0c, NC 28224-0543
Atlanta, GA 30340
Phone: [phone]
Phone :(770)457-SI77
Pax: 704-525-0409
Fax: NA
Prdjccs h(onegcr. Rabbi A. 7oncs
V
.tnslysis
Dec
Expires
Lab(.,mery ID
((\'��Conimenls
� IU �y{/
Sample ID: 9080093-01
Solid
Sampled: 0810711909:55
- _-'•� _J
lla'nicldcs TC'LP (Snb)
031p4)19 09:55
1
G��E
3 ;d SlIJd
Sam90
Sample ID: R00'J]-03
Solid
Sampled: OS/07A9 U9:45
4�/
l lsbicidc. TCLP (Sob)
O8/3Al19 09:45
CmMnecobgpBed:
Rf
Sample ID: 908009MI Solid Sampled: 0Sl07/19 0930 � ^ ✓" r L'L�
Nni bict des TILP (SO) OR/ 4/19 09:30
�� �f 8 l2 •I � ��
15' / Unu: Reenri 3, G I]am
l,.:ei:<:: R,.
lb,
Page I of
Pao Page 25 of 30

Analytical Environmental Services, Inc
Date: 19-Aug-19
Client:
Prism Laboratories
Client Sample ID:
4th Creek Sludge
Lab Order
1908C31
Tag Number:
9080093-01
Project Name:
9080093
Collection Date:
8/7/2019 9:55:00 AM
Lab ID:
1908C31-001A
Matrix:
Solid
Analyses Result Reporting
Y Qua[ MDL Limit Units BatchlD DF DateAnalyzed Analyst
HERBICIDES, TCLP SW1311/8151A
2,4,5-TP (Silvex) BRL
2,4-D BRL
Sum: DCAA 69 1
Qnarreo. < va ---d, nra.nnnni nnmane mm to el
BRL \or Deicned ni%IDL
H HoIdi ny eme, for prep -.non onnall s,se,rcvaNN
N Anaklcoor KELAC cenduH
B Ar.h1o&rttud or iM rl,00alod nunLW blank
(SW3510C)
0.030 0,20 mg/L 283568
1 08/16201914:32 HB
0.051 0.20 mS)L 283568
1 08/16/201914:32 HB
0 49.4-120 %REC 283568
1 08116201914:32 HB
E Emmned wine aW,e quo ammo anye
S Spike R.00-, ow,ide limns dne iomarrn
> 0,.I,r NoRemli mruc
1 Eslimomd vlue&Ioocd belmv Reporurw Lvnv
< Lees rhvr Resuh, Ao
Page Page 26 of 30

Analytical Environmental Services, Inc
Date: 19-Aug-19
Client:
Prism Laboratories
Client Sample ID:
3rd Creek SLUDGE
Lab Order
1908C31
Tag Number:
9080093-02
Project Name:
9080093
Collection Date:
linl 19 9:45:00 AM
Lab ID:
1908C31-002A
Matrix:
Solid
Analyses
Result
Qual MDL
Reporting
Units
BatchlD
DF Date Analyzed Analyst
Limit
HERBICIDES,TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.030
0.20
-A
283568
1 08/162019 14:53 HB
2,4-D
BRL
0.051
0.20
-91
283568
1 08/16201914:53 HB
Surr: DCAA
65.6
0
49.4A20
%REC
283568
1 08116201914:53 HB
QualMers: . Wain e.eeeds ma..imum eommnrinom lawl
BRI. Not Deenedm NIDL
H Holding lima ror..... ration or analysis exceeded
N Aroly¢ nor NELAC m1&red
B Analyze delceled In die amwialN method blank
E ESIImalM value abo.e gwminnan rani,
S Spike Recovery onside I it, due rnmmris
> Grat then Rnull value
J Eniaved value dnened We. R,,.n.,y Limit
e Las thin Result value
Pag Page 27 of 30

Analytical Environmental Services, Inc
Date: 19-Aug-19
Client:
Prism Laboratories
Client Sample ID:
Sta-Lime
Lab Order
1908C31
Tag Number:
9080093-03
Project Name:
9080093
Collection Date:
8/7/2019 9:30:00 AM
Lab ID:
190SC31-003A
Matrix:
Solid
Analyses Result Reporting
y Qual MDL Limit Units BatchlD DF Date Analyzed Analyst
HERBICIDES,TCLP SW1311/8151A
2,4,5-TP (Silvex) BRL
2,4-D BRL
Surr: DCAA 662
Qunlaters: ValuaexceNsmxi m...n ee.,unrem level
BRL No De¢emd aiSIDL
H Holdlna lanes fo,p,v,ua,ion ar analysis e,,evdvH
N Analy,enm NEL\CeeuiGed
B ,lnakm de,n,ed in aM1e assoeiaaed me,Fad blan4
(SW3510C)
0.030 0.20
-A 283568
1 08/16/201915:14 HB
0.051 0.20
mA 283568
1 08116/201915:14 HB
0 49.4-120
%REC 283568
1 08/16201915:14 HB
E ESlinua,ed value aboae quarwalion range
S Spike Reeo ,side liugl duu,..ua, x
> G,c¢nhan Rcuh value
J E„immed value de,eacd bvlom Repomng Linul
< less aan Rnull value
Pa91 Page 28 of 30

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Page 30 of 30

NC Certification No. 402
Case Narrative
/ALR I S M Full -Service Analytical & INC Drinking Water Cert No. 37735 12/5/19 11:46
Environmental Solutions SC Certification No. 99012
®NBOFAiOPIE$ INC
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime
Lab Submittal Date: 11/2512019
Prism Work Order: 9110421
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR =[Na]/SQRT(([Ca)+[Mg])/2}
SAR - ( 180/23) / SQRT (( [2400/20] + (0.047/12.2]) / 2 }
SAR = 1.0
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) +
Nitrate —Nitrite
PAN = 0.3 * (4000 — 120) + 0.5 * (120) + 9.3
PAN = 1200 mg/kg
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0643
Phone: [phone] - Toll Free Number: l-800/629-6364-Fax: [phone] Page 1 of 17

Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Terri W. Cole
Project Manager
Data Qualifiers Key Reference
Reviewed By Terri W. Cole
Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0543
Phone: [phone]- Toll Free Number: 1-8001629-6364-Fax: [phone] Page 2of 17

1
�1 I S n n I Full-SeMca Analytical &
' V' Environmental Solutions
�axuaouua.'.'
Sample Receipt Summary
12/05/2019
Prism Work Order: 9110421
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
DatelTime Received
Stal-ime (and Fecal 1)
9110421-01
Solid
11/25/19 11:45
11/25/19 12:40
2
9110421-02
Solid
11/25/19 11:45
11/25/19 12:40
3
9110421-03
Solid
11/25/19 11:45
11/25/19 12:40
4
9110421-04
Solid
11/25/19 11:45
11/25/19 12:40
5
9110421-05
Solid
11/25/19 11:45
11/25/19 12:40
6
9110421-06
Solid
11/25/19 11:45
11/25/19 12:40
7
9110421-07
Solid
11/25/19 11:45
11/25/19 12:40
Samples were received in good condition at 2.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratones, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: 1-8001529-6364- Fax: [phone] Page 3of17
3I
1

Laboratory Report
12/05/2019
�P R I S M I Fell -Service Analytical a
7 ro Environmental Solutions
ni[4 ixc
City of Statesville, NC
Project: Stal-ime
Client Sample ID: Stal-ime (and Fecal l)
Attn: Ken Galloway
Prism Sample ID: 9110421-01
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor DateMme
ID
General Chemistry Parameters
Plant Available Nitrogen
1200
mg/kg dry
120
63
1 'Calculation 12/4119 9:05
CLB
[CALC]
Solids
66.3
% by
0.100
0.100
1 'SM2540 G 11/27/19 9:08
EDV
P9K0490
Weight
Ammonia as N
120
mg/kg dry
16
3.7
1 'SM4500.NH3 C 11/27/19 14:00
BMS
P9K0504
Nitrate/Nitrite as N
9.3
mg/kg dry
7.6
2.1
1 'SM4500-NO3 F 1212/19 10:32
CLB
P9L0009
Phosphorus -Total
4300
mg/kg dry
160
46
20 'SM4500-P F 12/3119 12:15
CLB
P91-0031
Total Kjeldahl Nitrogen
4000
mg/kg dry
380
200
1 '361.2 12/4/19 9:06
CLB
P91L0041
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 'SM9221 E 11/25/19 14:30
BMS
P91<0483
Total Metals
Mercury
0.095
mg/kg dry
0.076
0.026
1 '7471B 11/27/19 10:34
MMR
P91<0493
BAR Soil Preparation
Complete
g
1 '2-78-054 11/27/19 13:30
EDV
P91<0491
BAR Percent Moisture
61.5
% by
0.100
0.100
1 '2.78-054 1212119 8:10
EDV
P91<0510
Weight
Arsenic
13
mg/kg dry
1.6
0.20
1 '6010D 1212/19 20:13
JAB
P9K0494
Sodium Absorption Ratio
1.0
[blank]
0.30
0.016
1 '2.78-054 1213119 8:60
JAB
P91<0508
Cadmium
BRL
mg/kg dry
0.75
0.051
1 '60100 1212119 20:13
JAB
P9K0494
Calcium, BAR
2400
mg/L
200
2.0
200 '6010D 12/3119 8:50
JAB
P91(0508
Copper
54
nrl dry
3.8
0.61
1 '6010D 12/2/19 20:13
JAB
P91<0494
Lead
9.0
mg/kg dry
1.5
0.26
1 '6010D 1212119 20:13
JAB
P9K0494
Magnesium, BAR
BRL
mg/L
1.0
0.086
10 '6010D 12/3/19 850
JAB
P9K0$08
Nickel
16
mg/kg dry
1.6
0.46
1 '60101) 1212119 20:13
JAB
P9K0494
Potassium
4600
mg/kg dry
160
16
1 '6010D 12/2/19 20:13
JAB
P91<0494
Selenium
27
mg/kg dry
1.6
0.41
1 '6010D 1212/19 20:13
JAB
P9K0494
Sodium
1100
mg/kg dry
160
20
1 '6010D 12/2119 20:13
JAB
P9K0494
Sodium, BAR
1808
mg/L
5.0
0.18
10 '6010D 1213119 8:60
JAB
P91(0508
Zinc
100
mg/kg dry
15
2.1
1 '6010D 1212/19 20:13
JAB
P9K0494
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643
Phone: [phone]- Toll Free Number: 1-8001529-6364- Fax: [phone] Page of 17

,�P R iea aI S M I Environmental Solutions kwrueaunain ixc
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime
Sample Matrix: Solid
Laboratory Report
12/05/2019
Client Sample ID: 2
Prism Sample ID: 9110421-02
Prism Work Order: 9110421
Time Collected: 11/25/1911,45
Time Submitted: 11/25/19 12:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datemme ID
General Chemistry Parameters
Solids 66.3 % by 0.100 0.100 1 'SM2640 G 11/27/19 9:08 EDV P9K0490
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0543
Phone: [phone]- Toll Free Number: 1.800/629-6364 - Fax: [phone] Page 5of 17 —

Laboratory Report
AIR ISM /� I FUIbSmWental S ytical 6 12/05/2019
as .a Emiranmenlal SOWtlona
®uwuroarec ixc
City of Statesville, NC
Project: Stal-ime
Client Sample ID: 3
Attn: Ken Galloway
Prism Sample ID: 9110421-03
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter
Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor DateRme
ID
General Chemistry Parameters
Solids
63.9 % by
0.100
0.100 1 •SM2640 G 11/27/19 9:08 EDV
P9K0490
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 11/25/19 14:30 BMS
P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone]-Tall Free Number: i-8001629-6364- Fax: [phone] Page 6of17

IIP Full-SeMce lcal 8
Laboratory Report
Envirnmental Soluios SM I
12/05/2019
vsw..rawes, ixc
City of Statesville, NC
Project: Stal-ime
Client Sample ID: 4
Attn: Ken Galloway
Prism Sample ID: 9110421-04
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12,40
Parameter
Result Units
Report
MOIL Dilution Method Analysis Analyst
Batch
Limit
Factor DateRme
ID
General Chemistry Parameters
Solids
66.1 % by
0.100
0.100 1 'SM2640 G 11/27/19 9:08 EDV
P91(0490
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 11/25/19 14:30 BMS
P9K0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0643 -
Phone: [phone]- Toll Free Number: 1.8001529-6364- Fax: 704/626A409 Page 7 of 17 �—
I

�.
i R ISM I Fnll-Service al Solutions
S
Environmental Solutlona
q7� ewurax,ea me
Laboratory Report
12/05/2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime Client Sample ID: 5
Prism Sample ID: 9110421-05
Prism Work Order: 9110421
Sample Matrix: Solid Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch
Limit Factor DateRme ID
General Chemistry Parameters
Solids 66.4 % by 0.100 0.100 1 •SM2640 G 11/27/19 9:08 EDV P91<0490
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221E 11/25/1914:30 BMS P91(0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643 -
Phone: [phone]- Toll Free Number: 1-8001629-6364- Fax: [phone] Page 8of 1] —

PRISM I Laboratory Report
Full -Service Analytical &
Environmental Solutlone 12/05/2019
Jue ORP.s mn
City of Statesville, NC
Project: Stal-ime Client Sample ID: 6
Attn: Ken Galloway
Prism Sample ID: 9110421-06
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Daternme
ID
General Chemistry Parameters
Solids 64.0
% by
0.100
0.100 1
"SM2540 G 11/27/19 9:08 EDV
P9K0490
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
•SM9221 E 11/25/19 14:30 BMS
P91(0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 9 of 17

ISM I Fun-SaMce Analytical 8
Environmental Solutions
V.P4100R,641N4
Laboratory Report
12/05/2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime Client Sample ID: 7
Prism Sample ID: 9110421-07
Prism Work Order: 9110421
Sample Matrix: Solid Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateRme ID
General Chemistry Parameters
Solids 67.2 % by 0.100 0.100 1 'SM2640 G 11/27/19 9:08 EDV P91<0490
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224.0543
Phone: [phone] - Toll Free Number: l-800/629-6364- Fax: [phone] Page 10 of 17

1 �fii I S I� A I ErAn eaten Analytical &
' V' Environmental Solutions
®rnswumniaa iw
Level II QC Report
12/5119
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime
Reporting
Result Limit Units
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P91<0491 - SAR 2.78.064
Blank (P91<0491-BLKI) Prepared: 11/26/19 Analyzed: 11/27/19
SAR Soil Preparation Complete g
Batch P91<0493. 7471 B
Blank (1391<0493-BLKI) Prepared &Analyzed: 11/27/19
Mercury BRL 0.050 mg/kg wet
LCS (P9K0493-BS1) Prepared &Analyzed: 11/27/19
Mercury 0.421 0.050 mg/kg wet 0.4167 101 80-120
Batch P91<0494. 3050B
Blank (P9K0494-BLK1)
Prepared: 11/27/19 Analyzed: 12/02/19
Arsenic
BRL
1.0
mg/kg wet
Cadmium
BRL
0.50
mg/kg wet
Copper
BRL
2.5
mg/kg wet
Lead
BRL
1.0
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
100
mg/kg wet
Selenium
BRL
1.0
mg/kg wet
Sodium
BRL
100
mg/kg wet
Zinc
BRL
10
mg/kg wet
LCS (P9K0494-BSI)
Prepared: 11/27/19 Analyzed: 12/02/19
Arsenic
12.8
1.0
mg/kg wet
12.50 103 80-120
Cadmium
12.8
0.50
mg/kg wet
12.50 103 80-120
Copper
13.8
2.5
mg/kg wet
12.50 110 80-120
Lead
13.0
1.0
mg/kg wet
12.50 104 80-120
Nickel
13.1
1.0
mg/kg wet
12.50 105 80-120
Potassium
1200
100
mg/kg wet
1250 96 80-120
Selenium
12.2
1.0
mg/kg wet
12.50 98 80-120
Sodium
1210
100
mg/kg wet
1250 97 80-120
Zinc
12.7
10
mg/kg wet
12.50 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0543
Phone: [phone]- Toll Free Number: 1-800/629-6364- Fax: [phone] Page 11 of 17

Level II QC Report
/201,FR ISM I Full-SeMce Analytical s 12/5119
Environmental Solutioalytical &
/lp¢quTOP,µ ING
City of Statesville, NC Project: StaLime Prism Work Order: 9110421
Attn: Ken Galloway Time Submitted: 11/25/2019 12:40:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P91(0508. 3010A
Blank (P9K0508-BLK1) Prepared: 11/27/19 Analyzed: 12/03/19
Calcium, SAR BRL 1.0 mg/L
Magnesium, SAR BRL 0.10 mg/L
Sodium, SAR 1.73 0.50 mg/L BH
Batch P91(0510 - NO PREP
Duplicate(P9K0510-DUP1) Source: 9110421-01 Prepared: 11/27/19 Analyzed: 12/02/19
SAR Percent Moisture 51.0 0.100 % by Weight 51.5 1 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone]- Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 of 17

Fan-ServiceAnalynoal&
a R ISM I Environmental Solutions
roa�.a pan
Level II CC Report
12/5/19
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, INC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaLime
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P91<0490 - NO PREP
Duplicate (P9K0490-DUP2) Source: 9110421.01 Prepared: 11/26/19 Analyzed: 11/27/19
Solids 66.5 0.100 % by Weight 66.3 0.2 20
Batch P9K0504 - SM4500-NH3 B
Blank (PSK0504-BLK1) Prepared &Analyzed: 11/27/19
Ammonia as N BRL 10 mg/kg wet
LCS (P9K0504-BSI) Prepared &Analyzed: 11/27/19
Ammonia as N 454 10 mg/kg wet 500.0 91 80-120
Matrix Spike (P9K0504-MS1) Source: 9110421-01 Prepared &Analyzed: 11/27/19
Ammonia as N 791 14 mg/kg dry 724.7 121 92 80-120
Matrix Spike Dup (PSK0504-MSD1) Source: 9l10421.01 Prepared &Analyzed: 11/27/19
Ammonia as N 816 14 mg/kg dry 724.7 121 96 80-120 3 200
Batch P91-0009 - NO PREP
Blank (P9L0009-BLK7) Prepared &Analyzed: 12/02/19
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P9L0009-BS1) Prepared &Analyzed: 12/02/19
Nitrate/Nitrite as N 47.7 5.0 mg/kg wet 50.00 95 80-120
Matrix Spike (P9L0009-MS1) Source: 9110421-01 Prepared &Analyzed: 12/02/19
Nitrate/Nitrite as N W8 7.5 mg/kg dry 75.37 9.35 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 13 of 17

r�P I S M I Fu ,...ce Anelyticel a
Envlranmental ao tical &
�Ixx lea
Level II QC Report
12/5/19
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters -Quality Control
Analyte
Project: Stal-ime
Reporting
Result Limit Units
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P9L0009 - NO PREP
Matrix Spike Dup (PSL0009-MSDt) Source: 9110421.01 Prepared &Analyzed: 12/02/19
Nitrate/Nitrite as N 89.2 7.5 mg/kg dry 75.37 9.35 106 80-120 0.8 20
Batch P91L0031 - SM4500-PB6
Blank (PSL0031-BLK1) Prepared &Analyzed: 12/03/19
Phosphorus -Total BRL 5.0 mg/kg wet
LCS (P9L0031-BS1)
Prepared &Analyzed: 12/03/19
Phosphorus -Total
Matrix Spike (P91.0031-MS1)
97.6 5.0 mg/kg wet 100.0 98 90-110
Source: 9110421-01 Prepared &Analyzed: 12/03/19
Phosphorus -Total
Matrix Spike Dup(P9L0031-MSD1)
4790 150 mg/kg dry
Source: 9110421.01
150.7 4250 353 80-120 MC
Prepared & Analyzed: 12/03/19
Phosphorus -Total
Batch P91_0041 -351.2
4920 150 mg/kg dry
150.7 4250 445 80.120 3 20 MC
Blank (P91.0041-BLKt)
Prepared: 12/03/19 Analyzed: 12/04/19
Total Kjeldahl Nitrogen
LCS (P9L0041-SS1)
BRL 25 mg/kg wet
Prepared: 12/03/19 Analyzed: 12/04/19
Total Kjeldahl Nitrogen
Matrix Spike (P9L0041.MS7)
123 25 mg/kg wet
Source: 9110421.01
125.0 99 90-110
Prepared: 12/03/19 Analyzed: 12/04/19
Total Kjeldahl Nitrogen
6750 750 mg/kg dry
1884 3960 148 90-110 M
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 140f 17 —

�fP ' I S M Full -Service Anelyecal8
Level II QC Report
Environmental Sautions 12/5/19
mareaixc
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime
Reporting
Result Limit Units
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P90041.351.2
Matrix Spike Dup (P9L0041-MSD1) Source: 9110421.01 Prepared: 12/03/19 Analyzed: 12/04/19
Total Kaldahl Nitrogen 6490 750 mg/kg dry 1884 3960 134 90-110 4 20 M
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0543
Phone: [phone] - Toll Free Number: l-8001529-6364- Fax: [phone] Page 15of 17

u
Level II QC Report
A R I S M I Full -Service oei &
Environmental al SolSolutions
12/5/19
®uaauroairaixc
City of Statesville, NC
Project:
Stal-ime
Prism Work Order: 9110421
Attn: Ken Galloway
Time Submitted:
11/25/2019 12:40:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters -Quality Control
Reporting
Spike Source %REC
RPD
Analyte
Result
Limit
Units
Level Result %REC Limits
RPD Limit Notes
Batch P91<0483 - NO PREP
Blank (P9K0483-BLK1)
Prepared &Analyzed: 11/25/19
Fecal Coliforms
BRL
0.2
MPN/g wet
Sample
Extraction
Data
Prep Method: 361.2
Lab Number Batch
Initial
Final
Date/Time
9110421-01 P910041
0.05 g
25 mL
12/03/19 10:15
Prep Method: SM4500-NH3 B
Lab Number Batch
Initial
Final
Date/Time
9110421-01 P91<0504
1.01 g
50 mL
11/27/19 8:55
Prep Method: SM4500-PBS
Lab Number Batch
Initial
Final
Date/Time
9110421-01 P910031
1 g
50 mL
12/03/19 6:15
Prep Method: 3010A
Lab Number Batch
Initial
Final
DateFrIme
9110421-01 P91<0508
50 mL
50 mL
11/27/19 13:30
9110421-01 P91(0508
50 mL
50 mL
11/27/19 13:30
Prep Method: 30508
Lab Number Batch
Initial
Final
Date/Time
9110421-01 P9K0494
2 g
50 mL
11/27/19 8:05
Prep Method: 7471B
Lab Number Batch
Initial
Final
Date/Time
9110421-01 P91<0493
0.6 g
50 mL
11/27/19 8:14
Prep Method: SAR 2.78-054
Lab Number Batch
Initial
Final
Date/Time
9110421-01 P91<0491
250 g
250 g
11/26/19 13:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 16 of 17

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