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WQ0001346_Residual Annual Report 2015_20160218
M,FCFIVE FEB 18 2016 CITY OF MONROE heritage of progress RESIDUALS LAND APPLICATION CITY OF MONROE RECEIVEDINCDEO/DWR FEB 1 8 2016 Non -Discharge Permitting unit ANNUAL REPORT 2015 PERMIT NUMBER WQ0001346 CITY OF TARE a heritage of progress City of Monroe Water & Wastewater Residuals Land Application Program 2015 Annual Report Table of Contents l . Certification Form & Annual Operations Summary 2. Annual Residual Sampling Summary Forms & Biosolids Analysis 3. TCLP Analysis 4. Field Summary Forms 5. Pathogen Reduction & Vector Attraction Reduction 6. Soil Analysis OPERATION SUMMARY Permit # W00001346 FIELDS USED IN 2015 SITE NAME FIELD NO. DATE ACRES WWTP GALS WTP GALS WWTP YARDS WTP YARDS WWTP Dry Tons WTP Dry Tons PAN (lbs/ac) Calvin Morris 1 u y 0.8 250 40.21 79.49 -A -019 Harry 1 Dec 35.5 375 61.17 35.90 Myers 2 May 34.2 196 28.15 20.32 NC-UN-18 June 434 62.31 44.99 3 May 2.1 42 6.03 70.91 4 May 4.9 84 12.06 60.78 5 May 14.9 238 34.18 56.63 May 116,000 25.93 19.4 June 26,000 5.81 4.35 Sept 253,500 39.53 36.35 6 May 6.9 126 18.09 64.75 June 65,000 14.53 23.47 7 May 5.4 112 16.08 73.54 6 Dec 3 75 12.23 84.97 ayne 1 ec 6.5 5 2.23 39.22 McBride Dec 64 12.77 20.63 3 Dec 14.1 131 21.38 31.58 NC -UN ---Dec- 14 2.79 2.08 merson 1 Sept 15.4 75 14.2 7.54 McBride Sept 50 8.35 10.76 NC-UN-26 Oct 125 23.65 29.23 2 Sept 6.1 50 9.46 29.52 Sept 50 8.36 26.16 3 Oct 10.5 200 37.85 68.59 4A Oct 12.1 175 33.12 52.08 Oct 75 14.97 12.99 4B Oct 12.7 50 9.46 14.18 5 Aug 11.6 175 28.15 51.8 Aug 75 12.53 21.42 6 25.8 250 40.22 33.27 Wep 150 25.05 19.26 50 9.47 6.98 50 8.36 6.42 Leland May 13.4 280 40.21 74.09 Wolfe 2 July 17 175 28.15 35.35 NC-UN-27 July 50 8.35 9.74 Aug 100 16.08 20.20 Aug 7 2.53 14.62 William Griffin 3 April 7.4 182 31.31 115.22 - -29 4 May 1 7.2 54 22.11 15.84 Tom May 3.1 294 42.22 79.57 Appenzeller 4 April 15.2 182 31.31 56.09 NC-UN-30 May 84 12.07 19.59 5 April0.8 182 31.31 78.95 Totals WWTP- Metric Tons 711.51 WTP- Metric Tons 181.27 Total Metric Tons 892.79 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0001346 County: Union Year: 2015 Facility Name (as .shown on permit): Land Application Operator: City of Monroe Steve Holden, Land Residual Coordinator Phone: 704-282-4679 Land application of residuals as allowed by the permit occurred during the past calendar year? 21 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in thepermit: 1 44 Total number of fields utilized for land application during the year7F 25 Total amount of dry tons applied during the year for all application sites: 984 Total number of acres utilizes for land application during the year: 316.6 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2015 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. R] Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual. TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .l 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40, CFR Part 503 regulated facilities). - 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Russell Colbath, P.E., Water Res. Director 2 - %' Permittee Name and Title (type or print) Signature of Permittee , , Date 9-/� Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0001346 Laboratory: Facility Name: City of Monroe Residual Source WQ # or N NPDES #: - C0024333 WWTP Name:.... Monroe. WWTP (cake) Residual Analvsis Data 1) A&L Eastern Lab. Inc. 2) 3) 4) 5) ._- - Parameter (mpg) Ceiling Conc. Limit Sample or Composite Date 1-7-15 3-3-15 4-27-15 6-24-15 8-25-15 10-26-15 Percent Solids (%) NA 15.95 20.43 17.05 19.1 22.47 19.37 Arsenic 75 12 11 14 13 13 15 Cadmium 85 2 3 2• 3 2 2 Copper 4,300 302 313 326 382 398 358 Chromium NA 122 117 126 119 128 122 Lead 840 31 31 31 29- 23 33 Mercury 57 < 0.4 0.5 0.4 0.5 < 0.4 0.9 Molybdenum 75 24 21 27 31 31 37 _ Nickel 420 49 43 42 40 44 46 Selenium 100 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 Zinc 7,500 780 822 671 872 766 887 Total Phosphorus NA 14800 17000 13600 18200 17400 17600 TKN NA .42400 42600 37900 33100 29900 33100 Ammonia -Nitrogen NA 3130 4160 4870 3660 2710 2430 Nitrate and Nitrite NA 184 < 2.0 < 2.0 1 11.5 < 2.0 < 2.0 For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." O I dIli-lid - Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0001346 Facility Name: City of Monroe Residual Source NCO024333 NPDES # or WQ#: WWTP Name: Monroe WWTP (cake) RPeidnal Annlveie Dntn Laboratory: 1) 2) 3) 4) 5) A&L Eastern Lab. Inc. Parameter (mg/kg) Sample or Composite Date 1-7-15 3-3-15 4-27-15 6-24-15 8-25-15 10-26-15 Potassium 2050 1680 1910 1890 1710 1640 Sulfur 6690 7790 7220 9760 7570 7670 Calcium 13400 11900 11600 12500 14600 12000 Magnesium 1840 1700 1890 2470 2110 1790 Sodium 850 649 2110 1070 842 829 Iron 106000 110000 129000 140000 153000 124000 Aluminum 12200 11800 10400 10700 11500 9000 Manganese 1030 910 975 1230 1160 1250 Organic N 39270 38440 33030 29440 27190 30670 pH ( standard units) 6.47 6.54 7.44 6.21 6.3 5.96 Volitile Solids % 58.83 58 56.79 55.12 51.06 52.7 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signafure of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional .parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0001346 Laboratory: 1) Facility Name: City of Monroe 2) Residual Source WQ # or NCO024333 3) NPDES #: 4) WWTP Name: Monroe WTP (cake) 5) Residual Analvsis Data A & L Eastern Lab. Inc. Parameter (mg/kg) Ceiling Cone. Limit Sample or Composite Date 1-7-15 4-6-15 6-24-15 9-29-15 Percent Solids (%) NA 21.2 24.67 -19.84 23.69 Arsenic 75 22 20 16 25 Cadmium 85 < 2.0 3 < 2.0 < 2.0 Copper 4,300 417 409 471 524 Chromium NA 194 189 163 185 Lead 840 23 23 -25 21 Mercury 57 < 0.4 < 0.4 -"0.8 < 0.4 Molybdenum 75 47 44 43 57 Nickel 420 28 31 32 26 Selenium 100 < 5.0 < 5.0 < 5.0 < 5.0 Zinc 7,500 276 307 545 258 Total Phosphorus NA 4250 5830 11000 4920 TKN NA 16100 21400 24100 12700 Ammonia -Nitrogen NA 1230 1700 2720 1690 Nitrate and Nitrite NA 394 210 < 2.0 - < 2.0 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1�4 jallS�/��i Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (1212006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not.listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0001346 Laboratory: 1) Facility Name: City of Monroe 2) Residual Source NCO024333 3) NPDES # or WQ#: 4) WWTP Name: Monroe WTP (cake) 5) Residual Analvsis Data Parameter (mg/kg) Sample or Composite Date 1-7-15 4-6-15 6-24-15 9-2915 Potassium 672 846 1080 735 Sulfur 3090 3940 6760 3900 Calcium 6570 5920 7050 3860 Magnesium 837 1050 1490 776 Sodium 530 567 643 782 Iron 267000 245000 225000 305000 Aluminum 5100 6000 7200 5100 Manganese 793 791 872 773 Organic N 14870 19700 21380 11010 pH ( standard units) 6.19 6.31 5.79 6.68 Volitile Solids % 45.11 46.26 48.38 44.97 ., "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1 l Au'A signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and '15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B W-Q Permit Number: WQ0001346 Laboratory: 1) Facility Name: City of Monore 2) Residual Source WQ # or NCO024333 3) NPDES #: 4) WWTP Name: WTP Ferric Liquid 5) Recidnal Analvcic nntn A & L laboratories Parameter (mg/kg) Ceiling Conc. Limit Sample or Composite Date 4-6-15 6-24-15 9-29-15 Percent Solids (%) NA 5.36 3.74 5.22 Arsenic 75 23 21 28 Cadmium 85 3 < 2.0 < 2.0 Copper 4,300 462 530 544 Chromium NA 194 202 188 Lead 840 22 24 22 Mercury 57 < 0.4 < 0.4 < 0.4 Molybdenum 75 47 55 60 Nickel 420 21 23 28 Selenium 100 < 5.0 < 5.0 < 5.0 Zinc 7,500 173 186 212 Total Phosphorus NA ° 2580 3150 2950 TKN NA 11900 13400 12300 Ammonia -Nitrogen NA 373 1600 2870 Nitrate and Nitrite NA I 776 1330 < 2.0 - For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0001346 Laboratory: 1) Facility Name: City of Monroe 2) Residual Source NCO024333 3) NPDES # or WQ#: 4) WWTP Name: WTP Ferric Liquid 5) Residual Analvsis Data A & L Laboratories Parameter (mg/kg) Sample or Composite Date 4-6-15 6-24-15 9-29-15 Potassium 394 524 539 Sulfur 3090 3220 3400 Calcium 2150 2640 2960 Magnesium 630 710 735 Sodium 533 911 795 Iron 297000 312000 320000 Aluminum 4300 3500 4600 Manganese 747 699 817 Organic N 11527 11800 9430 pH (standard units) 4.74 4.65 6.29 Volitile Solids 42.53 43.06 44.27 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." /� Imo" Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) City of Monroe Reports of Lab Analysis 1 St 60 Days Page: 1 of 1 Report Number: 15-008-0210 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 59551 Sample Id: RAS s A&L Eastern Laboratories Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 u www.aleastern.com Project: RAS/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/7/2015 10:51:00 Date Received: 01/08/2015 00:00 Date Reported: 01/14/2015 Total Solids * 1.24 12400 100.0 CZ 01/09/2015 08:44 SM-254OG Moisture ` 98.76 100.0 CZ 01/09/2015 08:44 SM-2540G Total Volatile Solids 70.18 701800 100.0 CZ 01/09/2015 08:44 SM-2540G Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising. news release. or other public announcements without obtaining our prior mitten authorization. Debbie Holt NSMITTAL FORM/CHAIN OF CUSTODY 01 °�0,5 :L Eastern Laboratories, Inc. 13 46 35 I CITY OF MONROE itepine Road Riclunotid VA 23237 Tel: 804-743-940I IL r-- FLOSINC CERT#257 aunmitted By Charge To Copy To Proje Steve Holden City of Monroe customer Information -de� Acct # 46205 POB 69 Monroe NC 28111 Ema Lab Number (Lab Use Only) Sam le ID Container T e Sampled Date: / 17- 77 Date Recd:R�5 Glass (Yes or No) ( es or No) elirquisl a By: {Signature Datelastic Y I Ime Sam pled Time: Q.' - Time Recd: Sampled fay: J ,✓ Recd Py: Received By: (Signature) Date Please Place a 'W' by Desired Tests'--�' Internal Lab Code: $ci♦iiiisR, x T14N l" K- S Ca _ mg Na Te Ai tin Cu Zn ; N - s Cd Cr Ni Pb As Hg SO _ CaCO3 pH Eq, °t, 1olatile Solids % Orq-N ,Mo Ba 304 'SOL NA'���.�iC,t� Ag Sa „�.,IPt�� ; Co �T�S 5n 5iaue>;2g. Ti ,Sieve#s0 Sieve#100 8e ALK ,,ASH SS Avail P dot K Cond tIN SOL 6 ` t37N ° ' 7OC Env TOTAL P205 TONAL K20 TN TKNW NH4W NO3W ORGN-W PA CE-F2T AZ CERT ETU REACT PCBS CN FECAL TCLP ICR _ State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page: 1 of 2 Report Number: 15-008-0208 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 59549 Sample Id: WWTP CAKE A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.WG www.aleastern,com Project: WWTP CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/7/2015 10:45:00 Date Received: 01/08/2015 00:00 Date Reported: 01/14/2015 Total Solids " 15.95 159500 100.0 CZ 01/09/2015 08:44 SM-2540G Moisture " 84.05 100.0 CZ 01/09/2015 08:44 SM-2540G Total Kjeldahl Nitrogen 4.24 42400 10.0 JM 01/09/2015 08:19 SM-4500-NH3C-TKN Total Phosphorus 1.48 14800 100 KM 01/09/2015 13:36 SW 6010C Total Potassium 0.21 2050 100 KM 01/09/2015 13:36 SW 6010C Total Sulfur 0.67 6690 100 KM 01/09/2015 13:36 SW 6010C Total Calcium 1.34 13400 100 KM 01/09/2015 13:36 SW 6010C Total Magnesium 0.18 1840 100 KM 01/09/2015 13:36 SW 6010C Total Sodium 0.09 850 100 KM 01/09/2015 13:36 SW 6010C Total Iron 106000 100 KM 01/09/2015 13:36 SW 6010C Total Aluminum 12200 100 KM 01/09/2015 13:36 SW 6010C Total Manganese 1030 5 KM 01/09/2015 13:36 SW 6010C Total Copper 302 5 KM 01/09/2015 13:36 SW 6010C Total Zinc 780 5 KM 01/09/2015 13:36 SW 6010C Ammonia Nitrogen 0.31 3130 10.0 JM 01/12/2015 09:29 SM-4500-NH3C Organic N 3.93 39270 10.0 01/09/2015 08:19 CALCULATION Nitrate+Nitrite-N 184 2.00 JM 01/09/2015 08:20 SM-450ONO3F Total Cadmium 2.0 2.0 KM 01/09/2015 13:36 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part. nor may any reference be made (`�l to the work, the results, or the company in any advertising, news release. or other public announcements without obtaining our prior Written authorization. Debbie Holt Page: 2 of 2 Report Number: 15-008-0208 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 59549 Sample Id: WWTP CAKE A&L Eastern Laboratories Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 www.aleastern.com Project: WWTP CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/7/2015 10:45:00 Date Received: 01/08/2015 00:00 Date Reported: 01/14/2015 Total Chromium 122 5 KM 01/09/2015 13:36 SW 6010C Total Nickel 49 5 KM 01/09/2015 13:36 SW 6010C Total Lead 31 5 KM 01/09/2015 13:36 SW 6010C Total Arsenic 12.0 3.0 KM 01/09/2015 13:36 SW 6010C Total Mercury <0.4 0.4 KM 01/12/2015 10:50 SW-7471B Total Selenium <5.0 5.0 KM 01/09/2015 13:36 SW 6010C pH (Standard Units) 6.47 2.00 JM 01/09/2015 08:19 SW-9045D Total Volatile Solids 58.83 588300 100.0 CZ 01/09/2015 08:44 SM-2540G Total Molybdenum 24 5 KM 01/09/2015 13:36 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our r epohs and letters are for the exclusive and confidential use of our clients. and may no[ bo rap10duced it wrrole o% part. no, may any reference be made; to the work, the results. or the company in any advertising, news release. or other public announcements without obtaining our prior written authorization Debbie Holt SAMPLE TRANSMITTAL FORNUCHAIN OF CUSTODY A&L Eastern Laboratories, 7r!1 Ulh.'r.....:.... D....,7 b:-L.IA Y3 11i 'P 1. VA, Office Information _. ... _ ... .... .. ...,.., .1._ 208 15-W Customer Inf I`I�IIIIIiII�IIIIIIIIIII�I1Hill 11111III1Hill11111Hill 11111 01-08-zols ubmitted By Charge To CITY OFMONROE 13.4421 eve Holden City of Monroe wwrPCAKE POB 69 Monroe NC 28111 sholdcn(ct%monroene.gr ZSamplo Rept# Acct # 46205 Lab Number' (Lob Use Only) ID Container Type Sampled Data:, Date Recd: 'j_n WWTI? Cake Glass (Yes or No) Sampled Time: D.' V's- Time Recd: Plastic (Yes or No) Sampled By; *q 1710 Recd By-, R,elinquisf d By: (Signature) Date Time Received By; (Signature) Date Time Please Puce a "" " by Desired Tests Internal Lab Coder SLIVIONR Ca 9 ""Na Po , r11 � 7'r a Zn 611-I4 d Ni Ply As lig8�..' r 1i CaCO3 Eq;fL Volatile Solids °fo OrN Ito Cl B Bo ... .. 2. s . 11 web Ca Sn T6 v Be ACK` `T SS ii;ell l Sol l Gonci i VVIN� ,SOL B SLiL Nyi O&G SP.OR. TSS ScYveTtzo 8iovef. y sleve#,100 ., ASH cao CaCO3 M CO3 E !Vl� - Cll+l iC:C Env 4 TOTA.L P2C}5 TOTAL K20 TN TKNVV I NH4VV WAN DRG.N*VV, FA CEW.;QZ GERT 8TU PCBS REACT C14 FECAL TCLi� ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page: 1 of 2 Report Number: 15-008-0209 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 59550 Sample Id: WTP FERIC A&L Eastern_ Laboratories, Inc. _ ' 7621 Whitepine Road Richmond Virginia 23237 (804) 743.9401 Fax (804) 271-6446 www.aleastern.com Project : WTP FERIC NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/7/2015 10:40:00 Date Received: 01/08/2015 00:00 Date Reported: 01/14/2015 Total Solids 21.20 212000 100.0 CZ 01/09/2015 08:44 SM-254OG Moisture' 78.80 100.0 CZ 01/09/2015 08:44 SM-2540G Total Kjeldahl Nitrogen 1.61 16100 10.0 JM 01/09/2015 08:19 SM-4500-NH3C-TKN Total Phosphorus 0.43 4250 100 KM 01/09/2015 13:36 SW 6010C Total Potassium 0.07 672 100 KM 01/09/2015 13:36 SW 6010C Total Sulfur 0.31 3090 100 KM 01/09/2015 13:36 SW 6010C Total Calcium 0.66 6570 100 KM 01/09/2015 13:36 SW 6010C Total Magnesium 0.08 837 100 KM 01/09/2015 13:36 SW 6010C Total Sodium 0.05 530 100 KM 01/09/2015 13:36 SW 6010C Total Iron 267000 100 KM 01/09/2015 13:36 SW 6010C Total Aluminum 5100 100 KM 01/09/2015 13:36 SW 6010C Total Manganese 793 5 KM 01/09/2015 13:36 SW 6010C Total Copper 417 5 KM 01/09/2015 13:36 SW 6010C Total Zinc 276 5 KM 01/09/2015 13:36 SW 6010C Ammonia Nitrogen 0.12 1230 10.0 JM 01/12/2015 09:29 SM-4500-NH3C Organic N 1.49 14870 10.0 01/09/2015 08:19 CALCULATION Nitrate+Nitrite-N 394 2.00 JM 01/09/2015 08:20 SM-450ONO3F Total Cadmium <2.0 2.0 KM 01/09/2015 13:36 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. I'o reference f be m Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part. nor may any r a ad� to the work, the results, or the company in any advertising. news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 15-008-0209 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 59550 Sample Id: WTP FERIC A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446A h www.aleastern.com Project: WTP FERIC NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/7/2015 10:40:00 Date Received: 01/08/2015 00:00 Date Reported: 01/14/2015 Total Chromium 194 5 KM 01/09/2015 13:36 SW 6010C Total Nickel 28 5 KM 01/09/2015 13:36 SW 6010C Total Lead 23 5 KM 01/09/2015 13:36 SW 6010C Total Arsenic 22.0 3.0 KM 01/09/2015 13:36 SW 6010C Total Mercury <0.4 0.4 KM 01/12/2015 10:50 SW-7471B Total Selenium <5.0 5.0 KM 01/09/2015 13:36 SW 6010C pH (Standard Units) * 6.19 2.00 JM 01/09/2015 08:19 SW-9045D Total Volatile Solids 45.11 451100 100.0 CZ 01/09/2015 08:44 SM-2540G Total Molybdenum 47 5 KM 01/09/2015 13:36 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. nor may any reference be mado to the work, the results: or the company in any advertising. news release. or other public announcements without obtaining our prior written authorizatio, r Debbie Holt �����������111111111111111111 o 2 Q,sg RAN S M I I'TA L FUFtN1/C `HA IN Oh' C: U STUD ' cITYormoNROE 134523 r,&L Eastern Laboratories, Inc. WTP FERIC 1 While pine. Road Richmond VA 23237 Tcl: 804-743,9401 Customer Information Rept# Submitted By Charge To Copy To Project Steve Holden Cit of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sbolden(a7monrocnc.c�r� b Number (Lab Use Only) Sam le ID Container Tye Sem Ied'Date: - S Dgte Recd: WTP Feric Glass (Yes or No) Sampled Time; A: Time Recd; Plastic (Yes or No) Sam Ied,6 ,i Re ByB Ralin uis) d, y; Si nature' bate Tune __ Received By: Si' natur+a) Date Time and -»:-. State Certification Needed: I NORTH CAROLINA Special Instructions or Remarks City of Monroe Reports of Lab Analysis 2n' 60 Days Page: 1 of 1 Report Number: 15-063-0201 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 60491 Sample Id: RAS Y A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 www.aleastern.com Project: RAS NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 3/3/2015 11:25:00 Date Received: 03/04/2015 00:00 Date Reported: 03/06/2015 Total Solids 1.51 15100 100.0 JM 03/04/2015 14:10 SM-254OG Moisture * 98.49 100.0 JM 03/04/2015 14:10 SM-2540G Total Volatile Solids 72.64 726400 100.0 JM 03/04/2015 14:10 SM-2540G Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and tellers an: for the exclusive and confidential use of our clients, and may not bo reproduced in whoio or part. nor may any reference be made o the ovork, the resedts or the company in any advertising, news release or other public announcements Without obtaining our prior written authorization Debbie Holt c A-N4PT R TR ANSMITTAL FORM/CHAEN OF CUSTODY + II I15-063-0201 L Eastern Laboratories, Inc. CII�I�IIII��I�III��II���II�IItIII i Y OF bic�pJRUE IIIIIII��III�IIIIIIIIIII�IIlIII( 03--04-2015 wpine Road Richmond VA 23237 Tel: 804-143_9401 C RA; 1a"o5 Customer Inforrnation Charge To Copy To Project City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholden@)n1011r0enC.01-9 Lab Number (Lab Use Only) Sara le ID Container Type Isampled Date: - - j - Date Reed: �� ] ll1 / Glass (Aft or No) Sam led Time: ,. Time Recd: Plastic {Yes or i>i} Sampled By:df v Recd By: Relinquished : (Signature) Date Time Received By-. (Signature) Date Time Please Place a "X" by Desired Tests - Intemal Lab Code: Solids % TKN 'K S Cap MCI Na Fe Al - tVl,z f Cu Z0 NH4-N' 40-3-N x C1l Gr Ni Pb. As Hq So 1--pH CaCO3 Eq. % Volatile Solids % Erg-N IV C1 B Pa x SO4 Ag Sb 7C6, Sh , .. ht. V Be ALK SS Avail P "Sol K Cond WIN SOL B SOL NA O&G SP.GR. T'SS Sieve#20 Sieve#,O Slevell1t3tl ASH Cao CaCO3 MgCO3 MgO CIN TOG Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special instructions or Remarks Comments Page: 1 of 2 Report Number: 15-063-0200 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 60490 Sample Id: WWTP CAKE A&L Eastern Laboratories, Inc_. �T 7621 Whitepine Road Richmond, Virginia 23237 (904) 743-9401 Fax (804) 271-6446 www.aleastern.com Project: WWTP CAKE NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 3/3/2015 11:15:00 Date Received: 03/04/2015 00:00 Date Reported: 03/06/2015 Total Solids 20.43 204300 100.0 JM 03/04/2015 14:10 SM-2540G Moisture ` 79.57 100.0 JM 03/04/2015 14:10 SM-2540G Total Kjeldahl Nitrogen 4.26 42600 10.0 JM 03/05/2015 08:24 SM-4500-NH3C-TKN Total Phosphorus 1.70 17000 100 KM 03/05/2015 12:30 SW 6010C Total Potassium 0.17 1680 100 KM 03/05/2015 12:30 SW 6010C Total Sulfur 0.78 7790 100 KM 03/05/2015 12:30 SW 6010C Total Calcium 1.19 11900 100 KM 03/05/2015 12:30 SW 6010C Total Magnesium 0.17 1700 100 KM 03/05/2015 12:30 SW 6010C Total Sodium 0.06 649 100 KM 03/05/2015 12:30 SW 6010C Total Iron 110000 100 KM 03/05/2015 12:30 SW 6010C Total Aluminum 11800 100 KM 03/05/2015 12:30 SW 6010C Total Manganese 910 5 KM 03/05/2015 12:30 SW 6010C Total Copper 313 5 KM 03/05/2015 12:30 SW 6010C Total Zinc 822 5 KM 03/05/2015 12:30 SW 6010C Ammonia Nitrogen 0.42 4160 10.0 JM 03/05/2015 08:24 SM-4500-NI3C Organic N 3.84 38440 10.0 03/05/2015 08:24 CALCULATION Nitrate+ N itrite-N <2.00 2.00 JM 03/05/2015 08:25 SM-450ONO3F Total Cadmium 3.0 2.0 KM 03/05/2015 12:30 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9 Our reports and letters are for the exclusive and confidential use of ourclients, and may not be reproduced io whole orpart. nor may any reference be rnadr C�d�C�C-./L/J_ to the work, the results: or the company in any advertising news release. or other public announcements Without obtaining our prior ivatten authorization Debbie Holt Page: 2 of 2 Report Number: 15-063-0200 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 60490 Sample Id: WWTP CAKE A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (904) 271-6446 www.aleastern.com Project: WWTP CAKE NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 3/3/2015 11:15:00 Date Received: 03/04/2015 00:00 Date Reported: 03/06/2015 Total Chromium 117 5 KM 03/05/2015 12:30 SW 6010C Total Nickel 43 5 KM 03/05/2015 12:30 SW 6010C Total Lead 31 5 KM 03/05/2015 12:30 SW 6010C Total Arsenic 11.0 3.0 KM 03/05/2015 12:30 SW 6010C Total Mercury 0.5 0.4 KM 03/05/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 03/05/2015 12:30 SW 6010C pH (Standard Units) 6.54 2.00 JM 03/05/2015 08:24 SW-9045D Total Volatile Solids 58.00 580000 100.0 JM 03/04/2015 14:10 SM-254OG Total Molybdenum 21 5 KM 03/05/2015 12:30 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for- the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be male ?o the vvork, the results. or the company in any advertising. news release. or other public announcements without obtaining our prior watten authorization Debbie Holt 0 5-063-02oa IIII11111N11111NU111111181t111111111I1it»i��ti�i►►�Jill m1 3�06.17 VV\NTP CAKE ANSM ITTAL FORM/CHAIN OF CUSTODY n&L Eastern Laboratories, Inc;. Office Information Customer Information ate W Submitted By Charge To Steve Holden City of Monroe Copy To Project Acci # POB 69 Email �46205 Monroe NC 28111 sholden nmonroea�c.ar Lab Number bats Use Oni { )' Sam tt] ContalnQi`T s Sain ate; 3'3 - iS Date Recd: ` � Glass (Yes or No) V✓ WTP Cabe plastic Yes or No )arnpled'B., Sam �cTTir�ae: J :i5 _ TLtfi�:F3ecd: t►: i _ t :,( ,- natuna _ - . ', by e' Tttns. ' l�t#aai _ ' : (.Sighaturo} _ ift , `[rime 7a,, _ i ��r; I TSt - Ittkerltat lh"Ga�e. SLMO NR x X. x x x x X x x x x x x x x x x x x x x x _-N ME — a . Ell � , P'' State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page: 1 of 2 Report Number: 15-097-0200 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 61159 Sample Id : WTP FERRIC CAKE A&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 U www.aleastern.com Project: WTP FERRIC CAKE/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/6/2015 10:25:00 Date Received: 04/07/2015 00:00 Date Reported: 04/13/2015 Total Solids 24.67 246700 100.0 JM 04/07/2015 13:30 SM-2540G Moisture ' 75.33 100.0 JM 04/07/2015 13:30 SM-2540G Total Kjeldahl Nitrogen 2.14 21400 10.0 JM 04/08/2015 13:09 SM-4500-NH3C-TKN Total Phosphorus 0.58 5830 100 KM 04/08/2015 13:00 SW 6010C Total Potassium 0.08 846 100 KM 04/08/2015 13:00 SW 6010C Total Sulfur 0.39 3940 100 KM 04/08/2015 13:00 SW 6010C Total Calcium 0.59 5920 100 KM 04/08/2015 13:00 SW 6010C Total Magnesium 0.11 1050 100 KM 04/08/2015 13:00 SW 6010C Total Sodium 0.06 567 100 KM 04/08/2015 13:00 SW 6010C Total Iron 245000 100 KM 04/08/2015 13:00 SW 6010C Total Aluminum 6000 100 KM 04/08/2015 13:00 SW 6010C Total Manganese 791 5 KM 04/08/2015 13:00 SW 6010C Total Copper 409 5 KM 04/08/2015 13:00 SW 6010C Total Zinc 307 5 KM 04/08/2015 13:00 SW 6010C Ammonia Nitrogen 0.17 1700 10.0 jm 04/09/2015 10:00 SM-4500-NH3C Organic N 1.97 19700 10.0 04/08/2015 13:09 CALCULATION Nitrate+Nitrite-N 210 2.00 JM 04/08/2015 09:00 SM-450ONO3F Total Cadmium 3.0 2.0 KM 04/08/2015 13:00 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our repo r s and letters are ior,tie csdustr; and USEe 01 o�,rchants. ,nt ,t °l :;LT ui ueno w �)arf. ;Mr y , ;,er:,nre ,<. r, ro the work, the results: or the company in any advertising. news release. or other public announcements without obtaining our prio! ; rittetr authorizatioc Debbie Holt Page: 2 of 2 Report Number: 15-097-0200 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 61159 Sample Id : WTP FERRIC CAKE �x A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 r� www.aleastern,com Project: WTP FERRIC CAKE/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/6/2015 10:25:00 Date Received: 04/07/2015 00:00 Date Reported: 04/13/2015 Total Chromium 189 5 KM 04/08/2015 13:00 SW 6010C Total Nickel 31 5 KM 04/08/2015 13:00 SW 6010C Total Lead 23 5 KM 04/08/2015 13:00 SW 6010C Total Arsenic 20.0 3.0 KM 04/08/2015 13:00 SW 6010C Total Mercury <0.4 0.4 KM 04/09/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 04/08/2015 13:00 SW 6010C pH (Standard Units) ` 6.31 2.00 JM 04/08/2015 09:00 SW-9045D Total Volatile Solids 46.26 462600 100.0 JM 04/07/2015 13:30 SM-2540G Total Molybdenum 44 5 KM 04/08/2015 13:00 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Fe" AND "Se". THE MSD WAS OUT OF LIMITS FOR "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our repoas and ;;dcrs arms,, for 10, oxc.i.r i,c ia, j';o nliucntial use or cr�r s. anU r,ra, 1aIt b r ru >,;rulo orpad- nor rIa ..crence be rnade to the v^ ork, the results, or the company io any advertising. news release. or other public announcements Without obtaining our prior ,^;rirtea authorization Debbie Holt SAMPLE TRANSMITTAL FO IllililIN1111111I1hill 11111111111E11111111111111111111111 040 720`15 CITY OF t00NROE 1.3957 A&L Eastern Lab WTPFERRIC CAKENCCERT#257 i621 Whitepiitc Road Richmond V; Office Information Customer Information Rept# Submitted By Change To Copy To Steve Holden City of Monroe Acct # POB 69 46205 Monroe NC 28111 shop Lab Number (Lab Use Only) Satt'i le 1D Container Type Sampled Qate: - - Date Recd: -�1 } r 1 li Fet'ric � Glass or No) Sam led Timer /Q; Z,� Time Recd., Plastic (Yes or ) Sarn _!od B f Reed.B Relln uished B , i naw - Date ;' Tune - Received B :Signature) Date - • IS 1l: cac� -- I'll 147 r u - Pl"Se,. P��ice Y lrrtemaiLab Gc X X X X X X X o;4 , , State Certification Needed: NORTH CAROLINA Special Instructlons or Remarks Common, Page: 1 of 2 Report Number: 15-097-0201 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 61160 Sample Id: WTP FERIC A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 www.aleastern.com Project: WTP FERIC/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/6/2015 10:10:00 Date Received: 04/07/2015 00:00 Date Reported: 04/13/2015 Total Solids " 5.36 53600 100.0 JM 04/07/2015 13:30 SM-2540G Moisture * 94.64 100.0 JM 04/07/2015 13:30 SM-2540G Total Kjeldahl Nitrogen 1.19 11900 10.0 JM 04/08/2015 13:09 SM-4500-NH3C-TKN Total Phosphorus 0.26 2580 100 KM 04/08/2015 13:00 SW 6010C Total Potassium 0.04 394 100 KM 04/08/2015 13:00 SW 6010C Total Sulfur 0.31 3090 100 KM 04/08/2015 13:00 SW 6010C Total Calcium 0.22 2150 100 KM 04/08/2015 13:00 SW 6010C Total Magnesium 0.06 630 100 KM 04/08/2015 13:00 SW 6010C Total Sodium 0.05 533 100 KM 04/08/2015 13:00 SW 6010C Total Iron 297000 100 KM 04/08/2015 13:00 SW 6010C Total Aluminum 4300 100 KM 04/08/2015 13:00 SW 6010C Total Manganese 747 5 KM 04/08/2015 13:00 SW 6010C Total Copper 462 5 KM 04/08/2015 13:00 SW 6010C Total Zinc 173 5 KM 04/08/2015 13:00 SW 6010C Ammonia Nitrogen 0.04 373 10.0 jm 04/09/2015 10:00 SM-4500-NH3C Organic N 1.15 11527 10.0 04/08/2015 13:09 CALCULATION Nitrate+Nitrite-N 776 2.00 JM 04/08/2015 09:00 SM-450ONO3F Total Cadmium 3.0 2.0 KM 04/08/2015 13:00 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients. and ma not be ra reduced in whole or art. nor may any rofercnce he made Y p P to the work, the results or the cornpany in any advertising. news release. or other public announcements without obtaining our prior written authorization Debbie Holt Page: 2 of 2 Report Number: 15-097-0201 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 61160 Sample Id: WTP FERIC A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 m www.aleastern.com Project: WTP FERIC/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/6/2015 10:10:00 Date Received: 04/07/2015 00:00 Date Reported: 04/13/2015 Total Chromium 194 5 KM 04/08/2015 13:00 SW 6010C Total Nickel 21 5 KM 04/08/2015 13:00 SW 6010C Total Lead 22 5 KM 04/08/2015 13:00 SW 6010C Total Arsenic 23.0 3.0 KM 04/08/2015 13:00 SW 6010C Total Mercury <0.4 0.4 KM 04/09/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 04/08/2015 13:00 SW 6010C pH (Standard Units) " 4.74 2.00 JM 04/08/2015 09:00 SW-9045D Total Volatile Solids 42.53 425300 100.0 JM 04/07/2015 13:30 SM-2540G Total Molybdenum 47 5 KM 04/08/2015 13:00 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Fe" AND "Se". THE MSD WAS OUT OF LIMITS FOR "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in who/e or -part. nor may any reference be made to the work. the results or the company in any advertising, news release. or other public announcements without obtaining our prior written authorization. Debbie Holt ,a N/LP L.1 'I'IZA N S LIT' ������ ����� ��� ������ f���� ����� ���� ������ 1111111111 11111111 Jul &j. CITY OF MONROE Easi 06205 ,5 12: 7 2 LA L WTP FERIC'NC CERTK257 76_1 V1 i11lC lI0i; lltl;]tt Office Information Customer Information Rep,# Submitted B Charge To Co To PY Project Acct # Steve Holden City of Monroe 46205 POB 69 Entail .ab Number (Lab Use Oilly) Monroe NC 28111 Sarn .le Ill Container Type sampled Date: sholden c�monroenc oro -Recd., Date ems'i itkC% ass (� or No Saul led T1me: WTP Fens Glass 149110 Time Recd; Relin t1► h d'B Si iidtur ( Data'astic Yes 1f 61b Setif led I3 : Recs►ved By: (Signature) Date Time Please Place a-"X" b Desired Tests y - IntoMel Lab Code: SLMONR Ir x x x x X7 x x x x x X x x x x x x x x x x alwf A State Certification Needed: I NORTH CAROLINA' Special Instructlons•or Remarks . :J ' trip City of Monroe Reports of Lab Analysis 3r' 60 Days Page: 1 of 1 Report Number: 15-118-0209 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 61629 Sample Id: RAS A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 www.aleastern.com Project: RAS/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/27/2015 09:35:00 Date Received: 04/28/2015 00:00 Date Reported: 05/04/2015 Total Solids ; 0.82 8200 100.0 BW 04/28/2015 15:20 SM-2540G Moisture ` 99.18 100.0 BW 04/28/2015 15:20 SM-2540G Total Volatile Solids 89.40 894000 100.0 BW 04/28/2015 15:20 SM-2540G Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our repo.4s and letters are for the exclusive and confidential use of our clients. and nray not be reproduced in whole or part. nor may any reference be made. to the work, the rasults or the cowpany in any advertising. news release. or other public announcements without obtaining our prior written authorization. LNII Debbie Holt Q A NAr31 C "T`n A N10n Alm l.lL-Qp4'�1 V 111 t4'.t J J }}. II�,1 IIII II��II IIII IIIII IIII IIIIII �I�II IIIII I!I I� III) I'II 462 85 015y I A & L F, � l CITY OF MONRUE 131557 RASINC CERT#257 L iG2 1 i'v IuLe zinc Raau Office Information ~jvCapy Rcpt# By Charge To olden City of Monroe To Project Acct # 46205 POB 69 Monroe NC 28111 [;Sed Finail Shol�fenii4 )nroenc.org Lab Number (Lab Use Only) CQuIalner Type Sam led Date:Zg .5Date Reed;r l� (L Z Glass (Yes or No) -Sampled Time: Time Reed: Plastic (Yes or No) Sampte4 p `: f ti1 Rgcd;p :, Relfn_ ulsFteci; By: Sl rt>atvr2' Dole I Time Received By: Signature Date Time -2 7.1 — .2'o Pies q Plac rr nr y Desired Tests Internal Lab Code: I m .. — m x TKNW {.%fiW t r n" BTU 4i 4 : ALP +P dS x L7k�(E °RSII� f &:z, k2© C^, TN �ejV �, H NH4VV LBO �1a� .�s&`7'S�"...kQ a1""i"', �'. '' lr�i [' ', Cii2GWWI A .-_.••Y t «i s r PA,•l~ERT l%�. �' g� CERT .�*f � PCBs E.-CT GbI IN FECAL TtrLP State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page: 1 of 2 Report Number: 15-118-0208 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 61628 Sample Id: WWTP CAKE A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (604) 271-6446 www.aleastern.com Project: WWTP CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/27/2015 09:50:00 Date Received: 04/28/2015 00:00 Date Reported: 05/05/2015 Total Solids * 17.05 170500 100.0 BW 04/28/2015 15:20 SM-2540G Moisture " 82.95 100.0 BW 04/28/2015 15:20 SM-2540G Total Kjeldahl Nitrogen 3.79 37900 10.0 JM 04/29/2015 09:35 SM4500-NH3C-TKN Total Phosphorus 1.36 13600 100 KM 04/29/2015 14:25 SW 6010C Total Potassium 0.19 1910 100 KM 04/29/2015 14:25 SW 6010C Total Sulfur 0.72 7220 100 KM 04/29/2015 14:25 SW 6010C Total Calcium 1.16 11600 100 KM 04/29/2015 14:25 SW 6010C Total Magnesium 0.19 1890 100 KM 04/29/2015 14:25 SW 6010C Total Sodium 0.21 2110 100 KM 04/29/2015 14:25 SW 6010C Total Iron 129000 100 KM 04/29/2015 14:25 SW 6010C Total Aluminum 10400 100 KM 04/29/2015 14:25 SW 6010C Total Manganese 975 5 KM 04/29/2015 14:25 SW 6010C Total Copper 326 5 KM 04/29/2015 14:25 SW 6010C Total Zinc 671 5 KM 04/29/2015 14:25 SW 6010C Ammonia Nitrogen 0.49 4870 10.0 JM 04/29/2015 09:35 SM-4500-NI3C Organic N 3.30 33030 10.0 04/29/2015 09:35 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 04/29/2015 09:35 SM-450ONO3F Total Cadmium 2.0 2.0 KM 04/29/2015 14:25 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our chorus. _and may nrt be reptoduced in whole or part, not may any reference be made to the work. the results, or the company in any advertising. news release. or other public announcements -without obtaining our odor ;vritten authorization. Debbie Holt Page: 2 of 2 Report Number: 15-118-0208 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 61628 Sample Id: WWTP CAKE A&L Eastern Laboratories Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-WG www.aleastern,com Project: WWTP CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/27/2015 09:50:00 Date Received: 04/28/2015 00:00 Date Reported: 05/05/2015 Total Chromium 126 5 KM 04/29/2015 14:25 SW 6010C Total Nickel 42 5 KM 04/29/2015 14:25 SW 6010C Total Lead 31 5 KM 04/29/2015 14:25 SW 6010C Total Arsenic 14.0 3.0 KM 04/29/2015 14:25 SW 6010C Total Mercury 0.4 0.4 KM 04/29/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 04/29/2015 14:25 SW 6010C pH (Standard Units) 7.44 2.00 JM 04/29/2015 09:35 SW-9045D Total Volatile Solids 56.79 567900 100.0 BW 04/28/2015 15:20 SM-2540G Total Molybdenum 27 5 KM 04/29/2015 14:25 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reporls and letters are for the exclusive and confidential use of cur clients. and may not be reproduced in whole or part. nor may any reference bo ;lad: - to the work. the resuRs, or the rompany in any aciveaising. news tElease. or other public announcements vithOU! obtabnng our prior' Written atWIQJ-7atiur.. Debbie Holt SA rvi11LL Tlk AN SM F1 A&L La< 7021 Whitcpinc koi . IIIIIIIIIIIIiIIIIIIIiIiIIIIIIIIIIIIIIIIIIIINIIIilllllliliillllllCITY OF MONROE 4 g&o;08 W WTP CAKE 13.14:51 AtL Office Information Customer Information Rept# Subrnitted By Charge To Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholden momocnc.or� Lab Number (Lath Use 001y) Sarnpie IDContainel• Typo sgm W. Data. - 7-/,,S- Date Recd: (p I (# Z jGlass W WTP Cake (`des or No) Sampled The: : 5U T1�'ie Recd'. Plastic (Yes or M) Sain d Reed=6 R+elingpMe By. (S" nature pate;` ..+ T�I1 8 R iY ay i nature Qi The Please P'l 'c a %` De81red Test8 Internal Lab Cotlw SLINONR ' x x x x x x x x x x x x x x x. x x x x x x x x x M1 x x 1AT jJ�y/G�i'� -TK W-' .. ', ,17H � ;w '�iWx� �, IYe b I� `:t�iUR r' t4�i°-� ryry Ilt Y� e� �. �L�V A .,,l,,li' ,. F+.$Ji� State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments City of Monroe Reports of Lab Analysis 4' 60 Days Page: 1 of 1 Report Number: 15-176-0203 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 62634 Sample Id: RAS Total Solids " Moisture Total Volatile Solids Comments: ® A&L Eastern Laboratories, Inc. 7Y 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271&446 www.aleastern,com Project: RAS/NC CERT#257 REPORT OF ANALYSIS 0.76 7600 100.0 99.24 100.0 71.56 715600 100.0 Date Sampled: 6/24/2015 07:50:00 Date Received: 06/25/2015 00:00 Date Reported: 07/02/2015 JM 06/25/201516:00 SM-2540G JM 06/25/201516:00 SM-254OG JM 06/25/201516:00 SM-2540G All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reporis and letters art: for the exchiswe and confidential use of our clients. and may not be reproduced in whole or-parf. nor fray any reference be made to the woA. the results. or the company in any advertising. o,ews release. or other public announcements ndthout obtaining our prior wtitten authorization Debbie Holt SAMPLE 'TRANSMITT� A&L Easter 7621 Vdhitepiue Road Ric I II�II III �II>�I� IIIII IIIII llll llllil 11 IIIII oil IIII III 5_2131653 CITY OF MONROF 1145.11 RASINC CERT#257 AFL Office Information Rept# Submitted By Charge To Copy To Project Steve Holden City of Monroe Awl # POB 69 Email 46205 Monroe NC 28111 _ ,,S sholdepaxuuoenc.oxg Lab Number(Lab Use Only) _ Sampfe iD Container T : e Sang led Date: - - ! S Date Recta: "- r _ t-P RAS Glass for No arrt d Time: -c� Time Read: Plastic (Yes or I*) , i"t i B'.M c Recd By: R ttasht _ l l e - Date '<. G'z Tih1i ' " Ft+ a Wed Hy::S ghairrr) bete Time - y-s' fr 2 IC ill rr �a 1�f. 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Ir✓►Z State Certification Needed: NORTH CAROLINA Special Instructions or Rernarks Comments Page: 1 of 2 Report Number: 15-176-0200 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 62631 Sample Id: WWTP CAKE �Y A &L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446 www.aleastern.com Project: WWTP CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/24/2015 08:15:00 Date Received: 06/25/2015 00:00 Date Reported: 07/02/2015 Total Solids * 19.10 191000 100.0 JM 06/25/2015 16:00 SM-2540G Moisture " 80.90 100.0 JM 06/25/2015 16:00 SM-2540G Total Kjeldahl Nitrogen 3.31 33100 10.0 JM 06/26/2015 09:04 SM-4500-NH3C-TKN Total Phosphorus 1.82 18200 100 KM 06/26/2015 15:24 SW 6010C Total Potassium 0.19 1890 100 KM 06/26/2015 15:24 SW 6010C Total Sulfur 0.98 9760 100 KM 06/26/2015 15:24 SW 6010C Total Calcium 1.25 12500 100 KM 06/26/2015 15:24 SW 6010C Total Magnesium 0.25 2470 100 KM 06/26/2015 15:24 SW 6010C Total Sodium 0.11 1070 100 KM 06/26/2015 15:24 SW 6010C Total Iron 140000 100 KM 06/26/2015 15:24 SW 6010C Total Aluminum 10700 100 KM 06/26/2015 15:24 SW 6010C Total Manganese 1230 5 KM 06/26/2015 15:24 SW 6010C Total Copper 382 5 KM 06/26/2015 15:24 SW 6010C Total Zinc 872 5 KM 06/26/2015 15:24 SW 6010C Ammonia Nitrogen 0.37 3660 10.0 JM 06/26/2015 09:04 SM4500-NH3C Organic N 2.94 29440 10.0 06/26/2015 09:04 CALCULATION Nitrate+Nitrite-N 11.5 2.00 JM 06/26/2015 09:20 SM-450ONO3F Total Cadmium 3.0 2.0 KM 06/26/2015 15:24 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our t,eports and letters are for the axGusrvo and Got Ificientm! use of our clronts. end tnay r;oi he reproduced in vvho;c or part. not may any reference b= r iao=r :'o the work, the results. er the cornpany it any advertising news release, or other public announcements ntatitoul obtaining our prior written authorization Debbie Holt Page: 2 of 2 Report Number: 15-176-0200 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 62631 Sample Id: WWTP CAKE A&L Eastern Laboratories, Inc. @D,'7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 www,aleastern.com Project: WWTP CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/24/2015 08:15:00 Date Received: 06/25/2015 00:00 Date Reported: 07/02/2015 Total Chromium 119 5 KM 06/26/2015 15:24 SW 6010C Total Nickel 40 5 KM 06/26/2015 15:24 SW 6010C Total Lead 29 5 KM 06/26/2015 15:24 SW 6010C Total Arsenic 13.0 3.0 KM 06/26/2015 15:24 SW 6010C Total Mercury 0.5 0.4 KM 06/26/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 06/26/2015 15:24 SW 6010C pH (Standard Units) 6.21 2.00 JM 06/26/2015 09:20 SW-9045D Total Volatile Solids 55.12 551200 100.0 JM 06/25/2015 16:00 SM-2540G Total Molybdenum 31 5 KM 06/26/2015 15:24 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the c:clus»o and cooridcntial use Wow cbvn, s o^;, ,v r of 4:,c iop,c.diced in whole or par'. ;��, �auc� no made to the work, the results, or the company in any advertising. news release. or other public announcements without obtaining our prior rnitten authorization? Debbie Holt SAMPLE •lARANSNII'I'1 1s" &, L111111111111111111111111111111111101111111111111111�10�20 CI i Y OF MONROE 11 ag:48 7621 Wi111C111nc Road Ri. ,AA-r .WF IQ;L Office InforTation �� By inarge I q Copy To Project eve Holden Cityof Monroe Rept##ubmitted Aect # 46205 POB 69 Monroe NC 28111 Ema11 sholden(cr�monroenc.o� Lab Number (LOIJCe ID Cant inns T pe Sampled pate;bate Recd: ' Cake Glass (k or No} ?itPlastic (Yes or Ij Rell °," wished C3y• (Si ltaturP) Date Time Sum led Time: — Time Recd: Sampled By; f f� d By, (Signature) Recd By: Date Time Lkp> to 12S7 1 tS : �10 Please Place a ►'X" by desired T08ts Interval Lab Code: 5�IVIONR x 7�4()L X x x x 1 / 1 x x x :*"Cdo mat 03 Az G1.RT .:::B7U :FAl- ,,TN TKIW. NIH4vV 4 r�aaW. Sl6y'e#1CKz _ D.R.uN-W ASil ' PACERT g _ C11 1'ivfvv', pG8$ EA RCT r1V FECAL TCLP lr R State Certification Needed: NORTH CAROLINA i Special Instructions or Remarks Comments Page: 1 of 2 Report Number: 15-176-0201 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 62632 Sample Id: WTP FERRIC CAKE �Y A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 www.aleastern.com Project: WTP FERRIC CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/24/2015 08:25:00 Date Received: 06/25/2015 00:00 Date Reported: 07/02/2015 Total Solids * 19.84 198400 100.0 JM 06/25/2015 16:00 SM-2540G Moisture * 80.16 100.0 JM 06/25/2015 16:00 SM-254OG Total Kjeldahl Nitrogen 2.41 24100 10.0 JM 06/26/2015 09:04 SM-4500-NH3C-TKN Total Phosphorus 1.10 11000 100 KM 06/26/2015 15:24 SW 6010C Total Potassium 0.11 1080 100 KM 06/26/2015 15:24 SW 6010C Total Sulfur 0.68 6760 100 KM 06/26/2015 15:24 SW 6010C Total Calcium 0.71 7050 100 KM 06/26/2015 15:24 SW 6010C Total Magnesium 0.15 1490 100 KM 06/26/2015 15:24 SW 6010C Total Sodium 0.06 643 100 KM 06/26/2015 15:24 SW 6010C Total Iron 225000 100 KM 06/26/2015 15:24 SW 6010C Total Aluminum 7200 100 KM 06/26/2015 15:24 SW 6010C Total Manganese 872 5 KM 06/26/2015 15:24 SW 6010C Total Copper 471 5 KM 06/26/2015 15:24 SW 6010C Total Zinc 545 5 KM 06/26/2015 15:24 SW 6010C Ammonia Nitrogen 0.27 2720 10.0 JM 06/26/2015 09:04 SM-4500-NH3C Organic N 2.14 21380 10.0 06/26/2015 09:04 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 06/26/2015 09:20 SM-450ONO3F Total Cadmium <2.0 2.0 KM 06/26/2015 15:24 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. a trudc, Jurn�pnrf5arn/;at!ws are (•�rlh_ .c�usiva and cor(de^:,cl �,:>� ,, "i„ clieu,s. _,ld ,nay „o. ��e r;;produced:n wi7oL ni�parL r,_-n.ay a;ry reference b� .. to tha work, tl;e ,es!#ts or J:e ; ourpan y io any adve,tising ne s !&'ease. or otl;a, pwvic announcements :without oUtaining oui pr,ui iv;iffcn autho,irafiun. Debbie Holt Page: 2 of 2 Report Number: 15-176-0201 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 62632 Sample Id: WTP FERRIC CAKE A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 www.aleastern.com Project: WTP FERRIC CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/24/2015 08:25:00 Date Received: 06/25/2015 00:00 Date Reported: 07/02/2015 Total Chromium 163 5 KM 06/26/2015 15:24 SW 6010C Total Nickel 32 5 KM 06/26/2015 15:24 SW 6010C Total Lead 25 5 KM 06/26/2015 15:24 SW 6010C Total Arsenic 16.0 3.0 KM 06/26/2015 15:24 SW 6010C Total Mercury 0.8 0.4 KM 06/26/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 06/26/2015 15:24 SW 6010C pH (Standard Units) 5.79 2.00 JM 06/26/2015 09:20 SW-9045D Total Volatile Solids 48.38 483800 100.0 JM 06/25/2015 16:00 SM-2540G Total Molybdenum 43 5 KM 06/26/2015 15:24 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reporls and letiors are for tree exclusive and confidential use of our clients. and may not be reproduced in wliole or part. nor n:ay any reference be mad., 'o the work, the ;r;,.uNs or the company in any ad:ettising. nays release. or other public announcemenis without obtaining out ptior widlen authorization. Debbie Holt 'S A MP L E. TRA N S N/11 TTA IITrOF IINI�IVIININNIIIIIIIIINIIIIIIIIINIIIIII��NIII� 5ROE 52015' WTp ,A�'; L Easter FERRIC CAKE 11'4325 ?621 Wkitepine Roar! Ric:hniono Office Information ---� Customer Information ReAt# Submitted By Charge To Co To- Project Steve Holden Cit of Monroe Aect #� P0i 69 46205 Email Monroe NC 28111 sholdett((u�monrocnc.or? y Number (Lab-lJse Only) SaMple ID lCiontainafT pe Sampled =efn: _ Date Reed., �. Glass or No Sam ad.i rrle; ,•2,,- Time Recd., u TF' Ferric Cake Plastic (Yes or Imo) ' S ✓t s JRecdB P 0 6 'M M r i U",,1,c.._ i ® y = -- - - State Certification Needed: I NORTH CAROLINA Spe t instruCtIons or Remarks Page: 1 of 2 Report Number: 15-176-0202 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE . NC 28110 Lab Number: 62633 Sample Id: WTP FERIC ® A&L Eastern Laboratories, Inc. ■ ■Y 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 c� www,aleastern.com Project: WTP FERIC NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/24/2015 08:00:00 Date Received: 06/25/2015 00:00 Date Reported: 07/02/2015 Total Solids * 3.74 37400 100.0 JM 06/25/2015 16:00 SM-254OG Moisture * 96.26 100.0 JM 06/25/2015 16:00 SM-254OG Total Kjeldahl Nitrogen 1.34 13400 10.0 JM 06/26/2015 09:04 SM-4500-NH3C-TKN Total Phosphorus 0.32 3150 100 KM 06/26/2015 15:24 SW 6010C Total Potassium 0.05 524 100 KM 06/26/2015 15:24 SW 6010C Total Sulfur 0.32 3220 100 KM 06/26/2015 15:24 SW 6010C Total Calcium 0.26 2640 100 KM 06/26/2015 15:24 SW 6010C Total Magnesium 0.07 710 100 KM 06/26/2015 15:24 SW 6010C Total Sodium 0.09 911 100 KM 06/26/2015 15:24 SW 6010C Total Iron 312000 100 KM 06/26/2015 15:24 SW 6010C Total Aluminum 3500 100 KM 06/26/2015 15:24 SW 6010C Total Manganese 699 5 KM 06/26/2015 15:24 SW 6010C Total Copper 530 5 KM 06/26/2015 15:24 SW 6010C Total Zinc 186 5 KM 06/26/2015 15:24 SW 6010C Ammonia Nitrogen 0.16 1600 10.0 JM 06/26/2015 09:04 SM-4500-NH3C Organic N 1.18 11800 10.0 06/26/2015 09:04 CALCULATION Nitrate+ N itrite-N 1330 2.00 JM 06/26/2015 09:20 SM-450ONO3F Total Cadmium <2.0 2.0 KM 06/26/2015 15:24 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Durreporta and hrH?:ar; tirt for the axc�us;ve ana cca•rdo,:ba, i.>a or n:r. ;,I;�:rts. airru racy r%u; ra (er)rLC.uLou in „rr_iio cn par,. no, ma; .: ry r, cronc.. be r . :o the work. the r esull.s or the company in any advertising. oesys release. or other public announcements without obtaining our prior •mitten authorizatior! Debbie Holt Page: 2 of 2 Report Number: 15-176-0202 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 62633 Sample Id : WTP FERIC AY A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-W6 www.aleastern.com Project: WTP FERIC NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/24/2015 08:00:00 Date Received: 06/25/2015 00:00 Date Reported: 07/02/2015 Total Chromium 202 5 KM 06/26/2015 15:24 SW 6010C Total Nickel 23 5 KM 06/26/2015 15:24 SW 6010C Total Lead 24 5 KM 06/26/2015 15:24 SW 6010C Total Arsenic 21.0 3.0 KM 06/26/2015 15:24 SW 6010C Total Mercury <0.4 0.4 KM 06/26/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 06/26/2015 15:24 SW 6010C pH (Standard Units) ` 4.65 2.00 JM 06/26/2015 09:20 SW-9045D Total Volatile Solids 43.06 430600 100.0 JM 06/25/2015 16:00 SM-2540G Total Molybdenum 55 5 KM 06/26/2015 15:24 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 'Jur reports and lettC rs are rof irtu a:<clusrve and ca ii(!ent+a! use )i our �ii--Ws. and may oot br reproc oc d in wheie or part. nor may any reference be made bj the work, the results, or the company in any advertising. ri bvs release, or other public announcements without obtaining our prior written authorization Debbie Holt SAMPLl TRANSM] A&L E . IIIIIIII�I�llllllllQ�lllIlllilllllllll�IIIIIII�llllllillll o � o,�`A_ CrrY OF MONROE 1021 White ine 16 WTPFERIC 11.44.19 T� Office Information --*�--�—..— Re t# S.0mltted By Uttar a-i 9 __. Copy To ry Project Steve Holden CRY of Monroe AGpf # PUB 69 46205 Email Monroe NC 28111 Lab Number (Lab Use OnIY� _ . Sample 1D Containea Type, Sam lecM717te F >;liolden( nonrocnc.o� zf - Data Recd; LQ�iQ 3 WTP Feric Mass '.f or Igo) Sam ied Time. Time Deed; Plastic (Yes or hIZ4 Sampled By; Recd.'Dy; g!`-"uishad$y° i net ss ClatrS Time Receive _B 5i.nature) bate _-Time P1e�9e P1a0 r air '' by` Desired Tests � � Internal Lab Code, LMOMR � X x X x X X x x _. __.Y .. �xJ x Y /\ �P R x , Y Nam ' yet. l e11215 -- _ § fto ini'L {ii}' ,r' till a �.+c9411�3_. � ..fig l I! r .6 1�._._..........� .�...-._...»_ - _ _ _ w r%�C} _ - ..,, T W AID.: - _ -_.a.__.--._ s TN 7 OW � Ni.Y GRG . .. � A CERT ��Rl," 9TIJ S � � � ! `'` I' N . c J - ����� y , jfi State Certification Needed: NORTH CAROLINA Special Instruct ons or Remarks Comments City of Monroe Reports of Lab Analysis St" 60 Days Page: 1 of 1 Report Number: 15-238-0203 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 63720 Sample Id: RAS Waypoint-(D ANALYTICAL Project : RAS NC CERT#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 8/25/2015 07:25:00 Date Received: 08/26/2015 00:00 Date Reported: 09/01/2015 Total Solids 0.96 9600 100.0 BW 08/26/2015 14:35 SM-2540G Moisture * 99.04 100.0 BW 08/26/2015 14:35 SM-2540G Total Volatile Solids 82.92 829200 100.0 BW 08/26/2015 14:35 SM-254OG Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. nor may any reference be mace to the work, the results: or the company in any advertising. news release. or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLE TRANSMI' IIINIIIIIIIIIIIIIIIIIIIIniIINIIIIIIIIIIIIIIIIIIIINIIIIIIIIIN o& - L A&L Ea CITY of moNFZGE 1356:36 7621 Whitepine Ro RAS j Office Information SubmitteTCo To Project Submitted By *✓hang' e PY Steve Holden City of Monroe _ f�ect # P013 69 Email 462Q5 Monroe NC 28111 ;holden mYno roene.rJr ample ID_ rG,1,a=(Yes itaioer Type Sam Ied Date: - Z = iS' Date Recd, Lab Numberr (Lab Use QnIY) p Time Recd; or No) Sam led Timer �] ks stic (Yes or No) Sampled 8y: �J Reed By: Relirrqulsh' d 8 : (Si nature Date Time Received By (Signature)Date Time Desired t. T s Please Place a ,1�11 by IrtteYnai Lib �.�: X, . 9 11[ AMU WT—M- �� 1 1=CAL r �� TNWTNH4V11 - -- - - TCI P CR �= - State Certification Needed: NORTH CAROLINA - Rnprial Instructions or Remarks Comments Page: 1 of 2 Report Number: 15-238-0202 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 63719 Sample Id: WWTP CAKE Waypoint,.0 ANALYTICAL Project: WWTP CAKE NC CERT#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 8/25/2015 07:35:00 Date Received: 08/26/2015 00:00 Date Reported: 09/02/2015 Total Solids * 22.47 224700 100.0 BW 08/26/2015 14:35 SM-2540G Moisture " 77.53 100.0 BW 08/26/2015 14:35 SM-2540G Total Kjeldahl Nitrogen 2.99 29900 10.0 SB 09/01/2015 15:04 SM-4500-NH3C-TKN Total Phosphorus 1.74 17400 100 KM 08/27/2015 13:07 SW 6010C Total Potassium 0.17 1710 100 KM 08/27/2015 13:07 SW 6010C Total Sulfur 0.76 7570 100 KM 08/27/2015 13:07 SW 6010C Total Calcium 1.46 14600 100 KM 08/27/2015 13:07 SW 6010C Total Magnesium 0.21 2110 100 KM 08/27/2015 13:07 SW 6010C Total Sodium 0.08 842 100 KM 08/27/2015 13:07 SW 6010C Total Iron 153000 100 KM 08/27/2015 13:07 SW 6010C Total Aluminum 11500 100 KM 08/27/2015 13:07 SW 6010C Total Manganese 1160 5 KM 08/27/2015 13:07 SW 6010C Total Copper 398 5 KM 08/27/2015 13:07 SW 6010C Total Zinc 766 5 KM 08/27/2015 13:07 SW 6010C Ammonia Nitrogen 0.27 2710 10.0 SB 08/27/2015 08:15 SM-4500-NH3C Organic N 2.72 27190 10.0 08/27/2015 08:15 CALCULATION Nitrate+ N itrite-N <2,00 2.00 SB 08/27/2015 08:15 SM-450ONO3F Total Cadmium 2.0 2.0 KM 08/27/2015 13:07 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidentiat use of our clients. and may not be reproduced in whole or part, nor may Y an reference be made to the work, the results, or the company in any advertising, news release. crother public announcements without obtaining ourprior written authorization. Debbie Holt Page: 2 of 2 Report Number: 15-238-0202 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 63719 Sample Id: WWTP CAKE Waypoint, ANALYTICAL Project: WWTP CAKE NC CERT#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 8/25/2015 07:35:00 Date Received: 08/26/2015 00:00 Date Reported: 09/02/2015 Total Chromium 128 5 KM 08/27/2015 13:07 SW 6010C Total Nickel 44 5 KM 08/27/2015 13:07 SW 6010C Total Lead 23 5 KM 08/27/2015 13:07 SW 6010C Total Arsenic 13.0 3.0 KM 08/27/2015 13:07 SW 6010C Total Mercury <0.4 0.4 KM 08/28/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 08/27/2015 13:07 SW 6010C pH (Standard Units) " 6.30 2.00 SB 08/27/2015 08:15 SW-9045D Total Volatile Solids 51.06 510600 100.0 BW 08/26/2015 14:35 SM-2540G Total Molybdenum 31 5 KM 08/27/2015 13:07 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER:THE QCS WAS OUT OF LIMITS FOR "NO3/NO2-N". THE LRB WAS OUT OF LIMITS FOR "Na". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Ca", "K", "Mg", "P", "Se", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. not' may any reference be made to the work, the results. or -the company in any advertising. news release. or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLE TRANSMI1-1- A&L LaStc 7021 whitepine Rf-d 1 Illlllllllllllli1111111illlllllilllllllllllllllilllllilllllllllll4�2 0;5` CITY or, MONROE 1355.23 W W TP CAKE i YA Office Information Charge To Co To pY;Submitlo Project Kept# Cit of MonroeAcct # # POB 6@EmailAcct Monroe NC 28111 sholden wrnonmenc.orLabNumber (Lab Use Canly)tainer Type 5aM led Date: - / Date Recd: Recd: �` � ���tic s (Yes or No) Sampled Time:Time (Yes or No) Sampled B , Reed 13y: Ielinquishe B (Si nature) C�ate Time Receive�i_Sy:: (Signature) Date T -ne - r'f o Please Place a " X" by Desired Tests Internal Lab Code: sLMONR i KN Cu `< , NHd= Soilds_°�:, .�{ X► x x x C IC03 �totatlle _ — __ _._ — G}u Cr Ni Pb A l ig S off £' L ;, ' il1t ', CJrc1l MC? I C1 Ei t3rr x j xLx x x + 4 Ba ALIT ry " r so)-K > lad, lfliihl SO.L i3' S - 8i v�1 0., �S 13ve ffio ;Sieye#10Q /kSH .,. :.'- d .;, , Ca_C0 . M Ct?3:: r p235 TC�1T , L TKNA NH4 l ORGNW, PA CERT AZ e iU REAG r. F TCLP✓ _ JCR'PGBS State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page: 1 of 2 Report Number: 15-274-0201 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 64498 Sample Id: WTP FERRIC CAKE D Waypoin(t. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: WTP FERRIC CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 9/29/2015 10:10:00 Date Received: 09/30/2015 00:00 Date Reported: 10/05/2015 Total Solids * 23.69 236900 100.0 BW 09/30/2015 15:09 SM-2540G Moisture * 76.31 100.0 BW 09/30/2015 15:09 SM-254OG Total Kjeldahl Nitrogen 1.27 12700 10.0 JM 10/01/2015 08:35 SM-4500-NH3C-TKN Total Phosphorus 0.49 4920 100 KM 10/01/2015 10:38 SW 6010C Total Potassium 0.07 735 100 KM 10/01/2015 10:38 SW 6010C Total Sulfur 0.39 3900 100 KM 10/01/2015 10:38 SW 6010C Total Calcium 0.39 3860 100 KM 10/01/2015 10:38 SW 6010C Total Magnesium 0.08 776 100 KM 10/01/2015 10:38 SW 6010C Total Sodium 0.08 782 100 KM 10/01/2015 10:38 SW 6010C Total Iron 305000 100 KM 10/01/2015 10:38 SW 6010C Total Aluminum 5100 100 KM 10/01/2015 10:38 SW 6010C Total Manganese 773 5 KM 10/01/2015 10:38 SW 6010C Total Copper 524 5 KM 10/01/2015 10:38 SW 6010C Total Zinc 258 5 KM 10/01/2015 10:38 SW 6010C Ammonia Nitrogen 0.17 1690 10.0 JM 10/01/2015 08:35 SM-4500-NI3C Organic N 1.10 11010 10.0 10/01/2015 08:35 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 10/01/2015 08:35 SM-450ONO3F Total Cadmium <2.0 2.0 KM 10/01/2015 10:38 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9&UDur,aports and letters are for the exclusive andconfidential use of our clients, and ma nor be re roducedin whole or art. nor ma • any reference be made mez- toY p P y r the ivoric the results, or the company in any advertising. nevvs release, or other public announcements without obtaining our prior !written authorization. Debbie Holt Page: 2 of 2 Report Number: 15-274-0201 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 64498 Sample Id: WTP FERRIC CAKE Waypoint''- ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.corn Project: WTP FERRIC CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 9/29/2015 10:10:00 Date Received: 09/30/2015 00:00 Date Reported: 10/05/2015 Total Chromium 185 5 KM 10/01/2015 10:38 SW 6010C Total Nickel 26 5 KM 10/01/2015 10:38 SW 6010C Total Lead 21 5 KM 10/01/2015 10:38 SW 6010C Total Arsenic 25.0 3.0 KM 10/01/2015 10:38 SW 6010C Total Mercury <0.4 0.4 KM 10/02/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 10/01/2015 10:38 SW 6010C pH (Standard Units) 6.68 2.00 JM 10/01/2015 08:44 SW-9045D Total Volatile Solids 44.97 449700 100.0 BW 09/30/2015 15:09 SM-2540G Total Molybdenum 57 5 KM 10/01/2015 10:38 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "As" AND "TKN". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Dar reports at s nr a :,:..sa D1 urr ci _, . a; Ito 3e raprodur ,, ;it uvhole orpart. no, iie,—nce be made ro the 1vork, the results or the company in any advertising. news release, or other public announcements without obtaining our prior written authorization Debbie Holt SAMPLE TRANSMITTAL FO A&L Eastern Lai. 7h?I \l%h;Irnint Rnnd Richmond b IIIIII I IU I I) I IIII Illll II III IIII IIIII IIII IIIII I II IIII 09�4' 015 CITY OF MONROE 12.47 2] W T P FERRIC CAKE Ai Office Information Customer Information Rept# SubmittWB-y Charge To Copy To Project Steve Hoiden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholden(a.,monrocne.ork Lab Number(Lab-U5e Only) Sample ID 'Container Type ISampled Dafe: — Date Recd: �j , Il; VVTP Ferric Coke Glass (Yes or No) Sam led Time: ; / Time Recd: Plastic (Yes or No) ISampled By; ,,� Reed BY: ftin ui'shetl Si nat�7e `' Date Time Received 8y: Signature) Date Time Please Place a ' X" by Desired f esLS InIemal Lab 00de: SLMONR t uds °la T9 A P K S C l Mg Na i . Fe l Mn Cu -Zn NN'd=N:1:_1903_-_N- I ..,: I �'� � i d y EQ X i Fe E I it Mo = CI j1 S Ba 5S A�rail;F $al KCottd,SO.I 6 , I FrI , tb1 d. , C!N TOC Env a fZ0A �C85 ;^ CN FECAL ! 'TGL'w — ICR State Certification Needed: NORTH CAROLINA Special instructions or Remarks Comments Page: 1 of 2 Report Number: 15-274-0202 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 64499 Sample Id: WTP FERIC Waypoint(z) ANALYTICAL Project: WTP FERIC NC CERT#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 9/29/2015 10:30:00 Date Received: 09/30/2015 00:00 Date Reported: 10/05/2015 Total Solids ' 5.22 52200 100.0 BW 09/30/2015 15:09 SM-2540G Moisture * 94.78 100.0 BW 09/30/2015 15:09 SM-2540G Total Kjeldahl Nitrogen 1.23 12300 10.0 JM 10/01/2015 08:35 SM-4500-NH3C-TKN Total Phosphorus 0.30 2950 100 KM 10/01/2015 10:38 SW 6010C Total Potassium 0.05 539 100 KM 10/01/2015 10:38 SW 6010C Total Sulfur 0.34 3400 100 KM 10/01/2015 10:38 SW 6010C Total Calcium 0.30 2960 100 KM 10/01/2015 10:38 SW 6010C Total Magnesium 0.07 735 100 KM 10/01/2015 10:38 SW 6010C Total Sodium 0.08 795 100 KM 10/01/2015 10:38 SW 6010C Total Iron 320000 100 KM 10/01/2015 10:38 SW 6010C Total Aluminum 4600 100 KM 10/01/2015 10:38 SW 6010C Total Manganese 817 5 KM 10/01/2015 10:38 SW 6010C Total Copper 544 5 KM 10/01/2015 10:38 SW 6010C Total Zinc 212 5 KM 10/01/2015 10:38 SW 6010C Ammonia Nitrogen 0.29 2870 10.0 JM 10/01/2015 08:35 SM-4500-NI3C Organic N 0.94 9430 10.0 10/01/2015 08:35 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 10/01/2015 08:35 SM-450ONO3F Total Cadmium <2.0 2.0 KM 10/01/2015 10:38 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our repo; [s and tatters are r-c; the axCtUSP/e and cooltdotioa! us;: of our clients. and easy not be relerodrr. e i in whole or part. nor may any reference be mac?a to the work, fhe results or the cornpany m any advertising. views release. or other public announcements without obtaining our prior mitten authorization. Debbie Holt Page: 2 of 2 Report Number: 15-274-0202 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 64499 Sample Id : WTP FERIC Waypoint . . ANALYTICAL Project: WTP FERIC NC CERT#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 9/29/2015 10:30:00 Date Received: 09/30/2015 00:00 Date Reported: 10/05/2015 Total Chromium 188 5 KM 10/01/2015 10:38 SW 6010C Total Nickel 28 5 KM 10/01/2015 10:38 SW 6010C Total Lead 22 5 KM 10/01/2015 10:38 SW 6010C Total Arsenic 28.0 3.0 KM 10/01/2015 10:38 SW 6010C Total Mercury <0.4 0.4 KM 10/02/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 10/01/2015 10:38 SW 6010C pH (Standard Units) 6.29 2.00 JM 10/01/201508:44 SW-9045D Total Volatile Solids 44.27 442700 100.0 BW 09/30/2015 15:09 SM-2540G Total Molybdenum 60 5 KM 10/01/2015 10:38 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "As" AND "TKN". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters an; .ror iha o,�ciusive and irai use of our clients. ant ay rat oa reproduced ru „c:e organ. ,,o; may and ice -t� nre_�a to the work, the results or the company in any advertising. news release. or other public announcements without obtaining our prior written authorization Debbie Holt 15-22 SAMPLE TRAN SM ITTA ilia°a oi5� At CITY OF MONROE '12:48:52 ILI 9,2�— AL Easter WTPFERIC '' 7621 While inc Read Ricl �--� Customer Information Office Information Charge To Copy To project Reps Submitted Submitted By Steve Holden of Monroe Ernaii Acct � POB 69 51ioIderl a� yjc)nrocnC.01 Monroe NC 28111 46205 Lab Number (Lab Use Only) Sample JD Contein6r Type Sampled N16 Date Reed Time Recd: t _ WTP Feric Glass (Yes or No) Sampled TI.me, plastic (Yes or No) Sampled By. �Ed� ecd B. i rime ©ate T1MO �tocerreti 6y; Sinnatutt ©ate Rel 1*0 d .y.; (Sionature) _ . Please Place a by Desired Tests Internal Lab Code: SLIVIONR F � r _ ►9 !��. lVl n _ IT. H CaCO3 E . �/Q Wlatile Solid's `rMis CI qa -- Cat Ni_ Pb As x x x y j' V 6� ALK- Avail P„ Soi�K Gond �+,11A1" ' ,_ .i: - SOL NA U$�C SP.Gi�. TSS. slave#afl �lev_ 6G Sieve#100 A� . CaCa3 M CfJ3 Moo G1N TOG'n - REACT TOTAL TOTAL TN TJ�NW NH4W NQ 3W._._ '_QR�Iv�1N FA C6RT - Ai CLE T� BTU PCBS CN FECAL TCLP 1CR P205 K20 State Certification Needed: NORTH CAROLINA Comments -^,nr.rlal Instructions or Remarks City of Monroe Reports of Lab Analysis 6' 60 Days Page: 1 of 1 Report Number: 15-300-0202 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 64951 Sample Id: RAS Wayp2int..AYTICAL Project : RAS NC CERT#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 10/26/2015 07:00:00 Date Received: 10/27/2015 00:00 Date Reported: 10/30/2015 Total Solids " 0.74 7400 100.0 JM 10/27/2015 15:00 SM-2540G Moisture ` 99.26 100.0 JM 10/27/2015 15:00 SM-2540G Total Volatile Solids 68.98 689800 100.0 JM 10/27/2015 15:00 SM-2540G Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the e.xctusive at id confidential use of our clients. and may not be reproduced in whole or pan'. nor may any reference be made to the work, the results or the company in any advedising. news release. or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLE TRANSMITTAL l A&L Eastern I 7621 Whilenine Road Richnim Ifl ll IIIIII If IIII ll► IIII ill III! Il ill.11l lA IIII IIII '0.27 �,°z F, 4 3 21.52 Office Information Customer Information �B' Rept# Submitted By Charge To Copy l"o Project Steve Holden City of Monroe Acot # POB 69 Email 46205 Monroe NC 28111 sll:�1den(2( 1norg-ge�nexI-P, Lab Number (Lola Use Only) Sample ID Container Type - Safripled Date: Date Recd: II qq.� 1 RAS Glass (Yes or No) Sampled Time: vrD Time Recd: Plastic (Yes or No) Sampled By; ¢�,>f11,440 Recd 13y: Relin; uished fay- (Sig; iatwe) Date Time Received By: (Signature) Date Time Al" - e I <- : ,,10 r 121I,�- • r " -- Plecase Place a 'X' by Desired Tests Internal Lab code: S61 ds % TKN P K 5 a Mg it Al Mn Cu zn NH4-_N NO3.N +Cd Cr N1 Pb As . Ho Se pH CaCO3 Eg,1A Volatile Solids `b Org-N I h90 i_:I B Eta x SO4 Aq Sta Cis _. Sn 'fi V `' Bi. ALK ' SS Avail P Sol K Cond 1'ihi SO7~ E, SOL NA 0&G 7SP,I;R. TSS Sieve;020 Sieve#6U Sieve#100 ASH Carl CaCO3 MW CO3 MgO C/N TOO Env TOTAL P205 TOTAL K20 TN TKNW NH44W NO3W ORGN-W Ppj.CERT AZ CERT BTU PCBS REACT CN FECAL TCLP (CR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page: 1 of 2 Report Number: 15-300-0201 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 64950 Sample Id: WWTP CAKE Waypoint,. ANALYTICAL Project: WWTP CAKE NC CERT#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 10/26/2015 07:15:00 Date Received: 10/27/2015 00:00 Date Reported: 10/30/2015 Total Solids * 19.37 193700 100.0 JM 10/27/2015 15:00 SM-254OG Moisture * 80.63 100.0 JM 10/27/2015 15:00 SM-2540G Total Kjeldahl Nitrogen 3.31 33100 10.0 JM 10/28/2015 09:49 SM-4500-NH3C-TKN Total Phosphorus 1.76 17600 100 KM 10/28/2015 12:15 SW 6010C Total Potassium 0.16 1640 100 KM 10/28/2015 12:15 SW 6010C Total Sulfur 0.77 7670 100 KM 10/28/2015 12:15 SW 6010C Total Calcium 1.20 12000 100 KM 10/28/2015 12:15 SW 6010C Total Magnesium 0.18 1790 100 KM 10/28/2015 12:15 SW 6010C Total Sodium 0.08 829 100 KM 10/28/2015 12:15 SW 6010C Total Iron 124000 100 KM 10/28/2015 12:15 SW 6010C Total Aluminum 9000 100 KM 10/28/2015 12:15 SW 6010C Total Manganese 1250 5 KM 10/28/2015 12:15 SW 6010C Total Copper 358 5 KM 10/28/2015 12:15 SW 6010C Total Zinc 887 5 KM 10/28/2015 12:15 SW 6010C Ammonia Nitrogen 0.24 2430 10.0 JM 10/28/2015 09:49 SM-4500-NH3C Organic N 3.07 30670 10.0 10/28/2015 09:49 CALCULATION Nitrate+ N itrite-N <2.00 2.00 JM 10/28/2015 09:50 SM-450ONO3F Total Cadmium 2.0 2.0 KM 10/28/2015 12:15 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. / Our repor is and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part. nor may any reference be mad , to the work, the results. or the company in any advertising, news release. or other public .announcements without obtaining our prior written authorization Debbie Holt Page: 2 of 2 Report Number: 15-300-0201 Account Number: 46205 Submitted By: STEVE HOLDEN Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE , NC 28110 Lab Number: 64950 Sample Id: WWTP CAKE D Waypoint( ANALYTICAL Project: WWTP CAKE NC CERT#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 10/26/2015 07:15:00 Date Received: 10/27/2015 00:00 Date Reported: 10/30/2015 Total Chromium 122 5 KM 10/28/2015 12:15 SW 6010C Total Nickel 46 5 KM 10/28/2015 12:15 SW 6010C Total Lead 33 5 KM 10/28/2015 12:15 SW 6010C Total Arsenic 15.0 3.0 KM 10/28/2015 12:15 SW 6010C Total Mercury 0.9 0.4 KM 10/28/2015 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 10/28/2015 12:15 SW 6010C pH (Standard Units) 5.96 2.00 JM 10/28/2015 09:49 SW-9045D Total Volatile Solids 52.70 527000 100.0 JM 10/27/2015 15:00 SM-2540G Total Molybdenum 37 5 KM 10/28/2015 12:15 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or pad. nor may any reference be made to the work, the results, orthe company in any advertising. news release. or other public announcements wilhout obtaining our prior written authorization. Debbie Holt °615';0SAMPLr TRANSMITTALrol 2 CiW OF M1AKE � F (7 t Eastern i� 1228:52 AOCL 1�(�S1eI�I7 Lab WWTPCAKE vII i 1,t1,. n1 17;, 1......... I v A - .0 Office Information Rept y Customer Information Submitted By Charge To Copy To Project Acct # 46205 Stave Holden City of Monroe POB 69 Monroe NC 28111 Email shnJcleniU),monroenc.ork Lab Wmber.(Lab Use Qrtly) Sample ID Container Type Glass (Yes or No) t n14160 WWTP Fake ,Plastic (Yes or No) Relinquished Fay: (Sigii aturej Date . _ Time Sampled Date; Saniplod Time: Date Recd: Time Recd: Sampled By: _ `S " /ter Roceived By: (Signatore) Recd By: Date Tina 7 1 G j Please Pace a "XIby Desired Tests Internal Lab Code; SLMONR pv/ R T i(IJI?: ,,w . ,..K. er y A �v,+ h tla Fe �,/ — /� - Al +y� R Mn r,/ !1 Cu �/ 11 Ito y A Ali ( tl �/ h lf?.N; ra I ' Hg SQ i i C,-GO ; [q, % Volatile Sands 5� YJtg N > x Mo x. Cl B. 8e Co Sn Tr '" �� ' �/ ' , B ALK, avail P. � t K Can i Vint+ SOL l3 S17L NA Ofi Gr I GR; 1` ;S V, Y. 20< <:.Si vetiQD: S{�y�#1�4 ASH CaO CaCCl3 f4tgC.i33 , M O CJN T© Env TOTAL. P205 TOTAL'' K210 _; .. >JN TKNW NI-14W NO3W ORGN,W PA CER7 AZ CERT' BTU PGBS REACT ON FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions. or Remarks Comments SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis City of Monroe PO Box 69 Monroe, NC 28111 Attention: Steve Holden Project Name: Land Application Lot Number:Q130057 Date Completed:10/12/2015 Lucas Odom Project Manager This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, Inc. J Page: 7 of 10 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative City of Monroe Lot Number: Q130057 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc: ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time Shealy Environmental. Services, Inc. Page: 2 of 10 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Monroe Lot Number: Q130057 Sample Number Sample ID Matrix Date Sampled Date Received 001 WWTP CAKE Solid 09/30/2015 0705 09/30/2015 002 WTP CAKE Solid 09/30/2015 0655 09/30/2015 (2 samples) Shealy Environmental Services, Inc. Page: 3 of 10 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com i - SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary City of Monroe Lot Number: Q130057 I Sample Sample ID Matrix Parameter Method Result Q Units Page 001 VVVVTP CAKE Solid Ignitability (Pensky-Martens 1010A >140 ° F 5 001 VVVVTP CAKE Solid Paint Filter Test 9095B Pass pass/fail 5 001 VVVVTP CAKE Solid Chromium 6010C 0.11 mg/L 7 002 VVTP CAKE Solid Ignitability (Pensky-Martens 1010A >140 ° F 8 002 VVTP CAKE Solid Paint Filter Test 9095B Pass pass/fail 8 002 VVTP CAKE Solid Barium 6010C 0.29 mg/L 10 (6 detections) Shealy Environmental Services, Inc. Page: 4 of 10 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Client: City of Monroe Laboratory ID:Q130057-001 Description: WWTP CAKE Matrix: Solid Date Sampled:09/30/2015 0705 % Solids: 15.1 09/3012015 2127 Date Received:09/3012015 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ignitability) 1010A' 1 10/08/2015 1844 BLO 87100 1 (Paint Filter) 9095B 1 10/06/2015 2201 ECP 1 (pH) 9045D •1 10/01/2015 1530 AEH2 86341 1 (Reactive Cya) 7.3.3 1 10/07/2015 1823 HMA 10/06/2015 1249 1 (Reactive Sul) 7.3.4 1 10/06/2015 1945 ECP 10/06/2015 1249 CAS Analytical Parameter Number Method Result Q PQL Units Run Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 ° F 1 Paint Filter Test 9095B Pass pass/fail 1 pH 9045D 6.85 su 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 ND 50 mg/kg 1 TCLP Volatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 131115030B 8260B 10 10/06/2015 1229 PAP 86617 10/01/2015 2231 CAS Analytical Parameter Number Method Result Q PQL Units Run Benzene 71-43-2 8260B ND 0.050 mg/L 1 2-Butanone (MEK) 78-93-3 8260B ND 0.10 mg/L 1 Carbon tetrachloride 56-23-5 8260B ND 0.050 mg/L 1 Chlorobenzene 108-90-7 8260B ND 0.050 mg/L 1 Chloroform 67-66-3 8260B ND 0.050 mg/L 1 1,2-Dichloroethane 107-06-2 8260E ND 0.050 mg/L 1 1,1-Dichloroethene 75-35-4 8260B ND 0.050 mg/L 1 Tetrachloroethene 127-18-4 8260E ND 0.050 mg/L 1 Trichloroethene 79-01-6 8260B ND 0.050 mg/L 1 Vinyl chloride 75-01-4 8260B ND 0.010 - mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 108 70-130 - Bromofluorobenzene 113 70-130 Toluene-d8 109 70-130 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270D 1 10/05/2015 1752 JCG 10/03/2015 1500 86450 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run 1 T4-Dichlorobenzene 106-46-7 8270D ND 0.050 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270D ND 0.10 mg/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GO columns exceeds 40 % N = Recovery Is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Shealy Environmental Services, Inc. Page' 5 of 10 - 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Client: City of Monroe Laboratory I D: Q130057-001 Description: WWTP CAKE Matrix: Solid Date Sampled:09/30/2015 0705 % Solids: 15.1 09/30/2015 2127 Date Received:09/30/2015 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270D 1 10/05/2015 1752 JCG 10/03/2015 1500 86450 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run Hexachlorobenzene 118-74-1 8270D ND 0.050 mg/L 1 Hexachlorobutadiene 87-68-3 8270D ND 0.050 mg/L 1 Hexachloroethane 67-72-1 8270D ND 0.050 mg/L 1 2-Methylphenol 95-48-7 8270D ND 0.050 mg/L 1 3 & 4-Methylphenol 106-44-5 8270D ND 0.10 mg/L 1 Nitrobenzene 98-95-3 8270D ND 0.050 mg/L 1 Pentachlorophenol 87-86-5 8270D ND 0.25 mg/L 1 Pyridine 110-86-1 8270D ND 0.050 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270D ND 0.050 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270D ND 0.050 mg/L 1 Run 1 Acceptance Surrogate Q %, Recovery Limits 2,4,6-Tribromophenol 93 41-144 2-Fluorobiphenyl 88 37-129 2-Fluorophenol 79 24-127 Nitrobenzene-d5 109 38-127 Phenol-d5 89 28-128 Terphenyl-d14 66 10-148 TCLP Herbicides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 10/07/2015 1505 MEM 10/06/2015 1503 86600 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run 2,4-D 94-75-7 8151A ND 0.020 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q %, Recovery Limits DCAA 93 62-117 TCLP Pesticides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 10/06/20151557 MEM 10/02/20151705 86451 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run gamma-BHC (Lindane) 58-89-9 8081B ND 0.00050 mg/L 1 Chlordane 57-74-9 8081 B ND 0.0025 mg/L 1 Endrin 72-20-8 8081B ND 0.00050 mg/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time jNo = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 6 of 10 106 Vantage Point Drive West Columbia, SC 29172 '(803) 791-9700 Fax (803) 791-9111 www.shealylab.com I Client: City of Monroe Laboratory ID:Q130057-001 - Description: WWTP CAKE Matrix: Solid Date Sampled:09/30/2015 0705 % Solids: 15.1 09/30/2015 2127 Date Received:0913012015 TCLP Pesticides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 10/06/20151557 MEM 10/02120151705 86451 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run Heptachlor 76-44-8 8081B ND 0.00050 mg/L 1 Heptachlor epoxide 1024-57-3 8081B ND 0.00050 mg/L 1 Methoxychlor 72-43-5 8081 B ND 0.0020 mg/L 1 Toxaphene 8001-35-2 8081E ND 0.0050 mg/L 1 Surrogate Run 1 Acceptance Q % Recovery Limits Decachlorobiphenyl 64 20-131 Tetrachloro-m-xylene 79 26-132 TCLP Metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/7470A 7470A 1 10/03/2015 1516 KDB 10/03/2015 1212 86460 10/01/2015 2058 1 1311/3010A 6010C 10 10/05/2015 2304 RKT 10/02/2015 1932 86458 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run Arsenic 7440-38-2 6010C ND 0.10 mg/L 1 Barium 7440-39-3 6010C ND 0.25 mg/L 1 Cadmium 7440-43-9 6010C ND 0.020 mg/L 1 Chromium 7440-47-3 6010C 0.11 0.050 mg/L 1 Lead 7439-92-1 6010C ND 0.10 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010C ND 0.10 mg/L 1 Silver 7440-22-4 6010C ND 0.050 mg/L 1 Nun = vracucal quantitatlon limit B = Detected in the method blank E = Quantilation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Shealy Environmental Services, Inc. Page: 7 of 10 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Client: City of Monroe Laboratory ID:Q130057-002 Description: WTP CAKE Matrix: Solid Date Sampled:09/30/2015 0655 % Solids: 28.9 09/30/2015 2127 Date Received:09130/2015 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst, Prep Date Batch 1 (Ignitability) 1010A 1 10/08/2015 1859 BLO 87100 1 (Paint Filter) 9095B 1 10/06/2015 2201 ECP 1 (pH) 9045D 1 10/01/2015 1530 AEH2 86341 1 (Reactive Cya) 7.3.3 1 10/07/2016 1825 HMA 10/06/2015 1249 1 (Reactive Sul) 7.3.4 1 10/06/2015 1945 ECP 10/06/2015 1249 CAS Analytical Parameter Number Method Result Q PQL Units Run Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 ° F 1 Paint Filter Test 9095B Pass pass/fail 1 pH 9045D 6.00 su 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 ND 50 mg/kg 1 TCLP Volatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/5030B 8260B 10 10/06/2015 1251 PAP 86617 10/01/2015 2231 CAS Analytical Parameter Number Method Result Q PQL Units Run Benzene 71-43-2 8260B ND 0.050 mg/L 1 2-Butanone (MEK) 78-93-3 8260B ND 0.10 mg/L 1 Carbon tetrachloride 56-23-5 8260B ND 0.050 mg/L 1 Chlorobenzene 108-90-7 8260B ND 0.050 mg/L 1 Chloroform 67-66-3 8260B ND 0.050 mg/L 1 1,2-Dichloroethane 107-06-2 8260B ND 1 0.050 mg/L 1 1,1-Dichloroethene 75-35-4 8260B ND 0.050 mg/L 1 Tetrachloroethene 127-18-4 8260B ND 0.050 mg/L 1 Trichloroethene 79-01-6 8260B ND 0.050 mg/L 1 Vinyl chloride 75-01-4 8260E ND 0.010 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 102 70-130 Bromofluorobenzene 102 70-130 Toluene-d8 101 70-130 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270D 1 10/05/2015 1841 JCG 10/03/2015 1500 86450 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run 1,4-Dichlorobenzene 106-46-7 8270D ND 0.050 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270D ND 0.10 mg/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range . H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W" Shealy Environmental Services, Inc. Page: 8 of 10 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Client: City of Monroe Laboratory I D: Q130057-002 Description: WTP CAKE Matrix: Solid Date Sampled:09/30/2015 0655 % Solids: 28.9 09/30/2016 2127 Date Received:09/3012015 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270D 1 10/05/2015 1841 JCG 10/03/2015 1500 86450 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run Hexachlorobenzene 118-74-1 8270D ND 0.050 mg/L 1 Hexachlorobutadiene 87-68-3 8270D ND 0.050 mg/L 1 Hexachloroethane 67-72-1 8270D 'ND 0.050 mg/L 1 95-48-7 8270D ND 0.050 mg/L 1 '2-Methylphenol 3 & 4-Methylphenol 106-44-5 8270D ND 0.10 mg/L 1 Nitrobenzene 98-95-3 8270D ND 0.050 mg/L 1 Pentachlorophenol 87-86-5 8270D ND 0.25 mg/L 1 Pyridine 110-86-1 8270D ND 0.050 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270D ND 0.050 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270D ND 0.050 mg/L 1 I Run 1 Acceptance Surrogate Q % Recovery Limits 2,4,6-Tribromophenol 83 41-144 2-Fluorobiphenyl 87 37-129 2-Fluorophenol 79 24-127 Nitrobenzene-d5 110 38-127 Phenol-d5 89 28-128 Terphenyl-d14 85 10-148 TCLP Herbicides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 10/07/2015 1528 MEM 10/06/2015 1503 86600 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run 2,4-D 94-75-7 8151A ND 0.020 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits DCAA 94 62-117 TCLP Pesticides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 10/06/20151628 MEM 10/02/20151705 86451 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run gamma-BHC (Lindane) 58-89-9 8081E ND 0.00050 mg/L 1 Chlordane 57-74-9 8081B ND 0.0025 mg/L 1 Endrin 72-20-8 8081B ND 0.00050 mg/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of cdteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W' Shealy Environmental Services, Inc. Page: 9 of 10 - 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com I ' Client: City of Monroe Laboratory ID:Q130057-002 Description: WTP CAKE Matrix: Solid Date Sampled:09/30/2015 0655 % Solids: 28.9 09/30/2015 2127 Date Received:09/3012015 TCLP Pesticides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date !, 1 131113520C 8081E 1 10/06/20151628 MEM 10/02/20151705 86451 10/01/20152058 CAS Analytical Parameter Number Method Result Q PQL Units Run Heptachlor 76-44-8 8081B ND 0.00050 mg/L 1 Heptachlor epoxide 1024-57-3 8081 B ND 0.00050 mg/L 1 Methoxychlor 72-43-5 8081B ND 0.0020 mg/L 1 Toxaphene 8001-35-2 8081E ND 0.0050 mg/L 1 Surrogate Run 1 Acceptance Q % Recovery Limits Decachlorobiphenyl 64 20-131 Tetrachloro-m-xylene 66 26-132 TCLP Metals Run Prep Method 1 131117470A 1 1311/3010A Analytical Method Dilution Analysis Date Analyst 7470A 1 10/03/2015 1522 KDB 6010C 10 10/05/2015 2308 RKT Prep Date Batch Leachate Date 10/03/2015 1212 86460 10/01/2015 2058 10/02/2015 1932 86458 10/01/2015 2058 CAS Analytical Parameter Number Method Result Q PQL Units Run Arsenic 7440-38-2 6010C ND 0.10 mg/L 1 Barium 7440-39-3 6010C 0.29 0.25 mg/L 1 Cadmium 7440-43-9 6010C ND 0.020 mg/L 1 Chromium 7440-47-3 6010C ND 0.050 mg/L 1 Lead 7439-92-1 6010C ND 0.10 rng/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 -' Selenium 7782-49-2 6010C ND 0.10 mg/L 1 Silver 1 ' 7440-22-4 6010C ND 0.050 mg/L 1 PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 10 of 10 106 Vantage;Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com ,cn o� CD d� m m =1 m < m o o CD O10 < CDm m C-D. N N 0 7 O O C 3 o- m cp n N W V N O V W t0 V O O x O W v =S CD N `G O 3 Cl) m n 1r m z X 0 z ic m z r CA m /C m co z 0 0 i SHEALY ENVIRONMENTAL SERVICES, INC. Shealy Eavirenmental Semcea, rile, Page I of I ll:n:urner Minh v: MEGOfEC-01 Kepluces Dale, 69:73?tS k.ff'rritie Vuw- LW.'lt}ll $ Sample Receipt Checklist (SKQ Clicnt: =Cooler Inspected byJdate: ^�x�,,_ Lot 9: 1wean_s ofroceipt: 0SESI ❑ Client ❑ UPS ❑ FedEx ❑ Other Yes j�EEq-K-_1 1. Wero custody seals rreaent on the cooler? Yea ❑A2. Trcust seals were Ercsicat, were Ibey initact 1md tunbroken? pF1 Strip ILI: _ C 1 strip ila: l Cooler 11. iOriginal temperature upon reccipt/Derived (=Tected) telliperu t urc upr)n receipt: Method: 'T'cmpeaatur: Blank ❑ Against Bo[llcs 11C 4ian ID: "e IR Crun Correction Factar: b °C Method of coolant: Fi " e-t Trr 171 111— 1-- ri ram_. ..___ r-"I Yes ❑ Nu ❑ NA J� - L_j 3. If temperature of any cooler exceoded 6.0°C, was Pxuitxt Manager notified? PM notified by SRC, phone, note (circle one), other: , (For coolers received via commercial courier, P S are In by notified imrnediatGl •.) Ycs ❑ lvo ❑� NA4. Is the couuteereial couricris packing slip attached to this form? Yes No ` 5. Were proper cusrodY proceduros relin uished'm ivv42 followed? Yews No ❑ NA Sit Wcnsamples relinquished by client to wmmcrcial courier'? Yes No ❑ 6. Were sans le [Da listed on the CUC? Ycs 1Vo ❑ 7_ V4'wc sans le [Ds listed on till sample containers? Ycs No ❑ $. Was collccti on, date & tune listed on the COC? YC4 No 9. T143 collection date & time listed'on all sample containers? Ync No 10. Did all container label inl'orm,ation ffD, dates tiat<ae anree with the CQC? Ycs o 11, Were tests to be ormed iisted on the COC? I Yes o 12. Did all samples Arrive in the pner containers for each test? i c r h'rs ❑ [ 3. Did all soiawinc m arrive in good condition funbroken, flids on, elc. ? '+ No ❑ 14. Was adequate sample volnure available-? Ycs No ❑ 15. Were all sWmmpl —received within %a thn. balding time or 49 hour's, whicfiever runes first? Ycs ❑ No " lG. Wereany samples containers inimin ? Yes ❑ No 17. Wcrr there tut excess samples not listed on CDC? Ycs ❑ No NA 19. %),It= bubbles present>" -size"(%"or Crum in diameter) in any VOA vials? Yes Ta NA 19. Werc ail metalsiO&USEMP'nutrient sain les received at a pH of r,2'1 Yey No NA20. Were all cyanide anWor sulfide sam lee received at a pH >12? Ycs ❑ No ❑ NA 21. Were all alppliuubic NTi3,TKNicyaniiidphenol (<0_2mgel) samples free of residual chlorine? Ycs - No ❑ NA 32. Were collection tcml2oralures docaumeneed on the COC for NC sari lm? Yes ❑' No ❑ NA 23. Were client rermariss'Tcquests fi.a reyueslad dilutions, h4Sd47SD deni8matiorr:s, etc... correctly transcribed from the COC into the coinwenl station in LIMS? Yes ❑ No 24, Was the quote number used taken from the Container label? Sainple Preser'►•rrtinR f�eli95t bi' COSYIilICrfYt fnr aav ¢amr,t�c'i inenrr.?.�ritrr.r.•:,..r.,...1 nt.a�rl� ti�ar«�..a 7 l.amlTTC11TS: Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 10.8 Land Owner: Calvin Morris Annual Dry Tons Applied: 40.2138 Site #: NC-AN49 Acres Permitted: 10.8 Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity (non 503): N/A Crop 1 Name: , Fescue (past.) Crop 1 Max. PAN: 126 . Crop 2 Name: Fescue (past.) Crop 2 Max. PAN: 50 S. .� ° +� o Q Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources PDES # W # Q , Fert., Animal Waste, etc ) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Y � '� cc n 5 -0' a w * o o C o w * � 0 7� � p-' TKN mg/kg Z Y i;' � o °u w mg/kg Nitrate and Nitrite mg/kg PAN Applied pp (lbs/acre)" Name of CropType ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 July 15 250 19.1 3.723 WWTPC D 0 S 0.5 0.3 33,100 3,660 -11.5 79.485 1 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4--- Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ............... TOTALS: 250 0 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 79.485 0.000 Lime Applied Annuallbs/acre 0.097 1.027 1.124 36 0.022 0.155 0.177 34 2.844 7.945 10.789 1338 0.886 20.713 21.599 X 0.216 2.338 2.554 267 0.004 0.077 0.081 15 0.231 1.748 1.979 X 0.298 3.57 3.868 374 0.037 0.397 0.434 89 6.493 69.834 76.327 2498 135.517::::::::::::::::::::::::: :: Date lbs/ac Prior Years Cumulative lbs/ac April 2080 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop ... ............................ 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." g / *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Iucorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate 0 DENR FORM FSF (19/9f)nR) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe , Total Dry Tons Applied (Annual): 40.21 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Calvin Morris Owner: Same Predominant Soil Series: GOB-Goldston Acres Used: 10.8 Acres Permitted: 10.8 Site #: NC-AN-19 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Sample or 1 1 2 j 3j 4 _5j 6 7j 8 9 10 11 12 Com- posite Date 6/24/15 % Solids 19.1 Arsenic 13 Cadmium 3 Copper 382 Chromium 119 Lead 29 Mercury 0.5 denum31 Nickel 40 Selenium 5 Zinc 872 Total Phos- T_ 18200 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 4j 5j L6J7 81 9 LOJ 11 12 DT/Ac./ _3j 0 App. y Event 3.72 Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.097 1 0.000 0.000 0.000 0.000 0.000 0.097 Cadmium 0.000 0.000 0.000 0.000 0.000 0,.000 6.022 0.000 0.000 0.000 0.000 0.000 0.022 Copper 0.000 0.000 0.000 0.000 0.000 0.000 2.844 0.000 0.000 0.000 0.000 0.000 2.844 Chromium 0.000 0.000 '0.000 0.000 0.000 0.000 0.886 0.000 0.000 0.000 0.000 0.000 0.886 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.216 0.000 0.000 0.000 0.000 0.000 0.216 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.004 0.000 0.000 0.000. 0.000 0.000 0.004 Molyb- 0.000 0.000 0.000 0.000 0.000 0.000 0.231 0.000 0.000 0.000 0.000 0.000 0.231 denum Nickel 0.000 0.000 0.000 0.000 0.000 0.000 -0.298 0.000 0.000 0.000 0.000 0.000 0.298 Selenium 0.000 1 0.000 0.000 0.000 0.000 0.000 0.037 0.000 0.000 0.000 0.000 0.000 0.037 Zinc 0.000 0.000 0.000 1 0.000 0.000 0.000 6.493 0.000 0.000 0.000 0.000 0.000 6.493 Total Phos- 0.000 0.000 0.000 0.000 0.000 0.000 135.517 0.000 0.000 0.000 0.000 0.000 135.517 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance ;with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006 - r ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #.: WQ0001346 Field #: 1 Acres Utilized: 35.5 Land Owner: Harry Myers Annual Dry Tons Applied: 61.1734 Site #: NC-UN18 Acres Permitted: 35.5 Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max: PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 Y Ll Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist) precip. Past 24 Hrs. inches Y 4 b cY _. o a o c �, M. ?; x w, ?± - 0 TKN mg/kg z Y aq c cc a w mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Dec 15 375 19.37 1.723 WWTPC D 0 S 0.5 0.3 33,100 2,430 2 35.904, NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 375 0::,:::::::: As I Cd Cu Cr Pb Ha I Mo Ni Se Zn P 35.904 0.000 Lime Applied Annuallbs/acre 0.052 0.663 0.715 36 0.007 0.078 0.085 34 1.234 8.444 9.678 1338 0.420 12.823 13.243 X 0.114 1.379 1.493 267 0.003 0.022 0.025 15 0.128 0.227 0.355 X 0.159 1.711 1.870 374 0.017 0.04 0.057 89 3.057 35.522 38.579 2498 60.650 ::: :::::::::::::::::::::::::::::::: ........................... ....................... .... Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop P 122 50 ••I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Compost -0.1 -0.2 Signature of Land Applier Date x** Mineralization Rates: Com p y digested anaerobiall di g ' aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 61.17 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Harry Myers Owner: Same Predominant Soil Series: 1302-Badin Acres Used: 35.5 Acres Permitted: 35.5 Site #: NC-UN18 Field #: 1 Residual Analvsis Data (Heave Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Com- posite Total Phos- j__phorusEEEEEEEEEEME Annual Total DT/Ac./ APP• Event Arsenic Cadmium Copper Chromium Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- Heavy 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ivietai riela l.oaaings (calculated in lbs/acre): F1.72 0 14 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.052 0.000 0.052 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.000 0.007 0.000 0.000 0.000 0.000 0.0,00 0.000 0.000 0.000 0.000 1.234 0.000 1.234 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.420 0.000 0.420 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.114 0.000 0.114 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.128 0.000 0.128 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.159 0.000 0.159 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 0.000 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.057 0.000 3.057 0.000 1 0.000 1 0.000 1 0.000 1 0.000 1 0.000 1 0.000 1 0.000 10.000 160.6501 0.000 160.650 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". - -.,Signature of Land Applier Date '.I DENR FORM MFLSF r19i9nnFi ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 2 Acres Utilized: 34.2 Land Owner: Harry Myers Annual Dry Tons Applied: 90.4620 Site #: NC-UN18 Acres Permitted: 34.2 Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 135 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 S. = +� a3 0 A 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES # WQ# Fert., Animal Waste, etc) Soil Cond. (Dry,,CD Wet Moist) Precip. Past 24 Hrs. inches Y b �? c o o �., * po 0 w -, * w * = TKN mg/kg Z Y ff S o 5 w• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 15 196 17.05 0.823 WWTP cake D 0 S 0.5 0.3 37,900 4,870 2 20.319 NA Fescue June 15 434 17.05 1.822 WWTP cake D 0 S 0.5 0.3 37,900 4,870 2 44.993 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.00.0 0.000 0.000 0.000 .. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 J 0.000 0.060 0.000 0.000 0.600 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 630 0 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 65.313 0.000 Lime Applied Annual lbs/acre 0.074 4.208 4.282 36 0.011 0.321 0.332 34 1.725 15.239 16.964 1 1338 0.667 15.139 15.806 X 0.164 4.458 4.622 267 0.002 1.429 1.431 15 0.143 2.775 2.918 X 1 0.222 3.501 3.723 374 1 0.026 2.136 2.162 89 3.550 46.732 50.282 2498 71.944 ::::::::::::::::::::::::::::: ::::::::::::::::::::::::::::::::: .................... Date lbs/ac Prior Years Cumulative lbs/ac July 2150 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop p 135 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation -� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 xX Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* I Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Monroe WQ0001346 Harry Myers Owner: 34.2 Acres Permitted: Total Dry Tons Applied (Annual): 90.46 Cation Exchange Capacity (non 503 only): N/A Same Predominant Soil Series: GoB-Golston 34.2 Site #: NC-UN18 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 31 4 5 4/27/15 6 7 8 9 10 F 11 j 12 % Solids 17.05 Arsenic 14 Cadmium 2 Copper 326 Chromium 126 Lead 31 Mercury 0.4 Molyb- denum 27 Nickel 42 Selenium 5 Zinc 671 Total I Phos- horus 13600 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 11 2 3 4 5 2.65 _ 7 8 9 10 11 12 o rt in Arsenic 0.000 0.000 0.000 0.000.1 0.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.074 Cadmium 0.000 0.000 0.000 0.000 0.011 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.011 Copper 0.000 0.000 0.000 0.000 1.725 0.000 0.000 0.000 0.000 0.000 0.000 -0.000 1.725 Chromium 0.000 0.000 0.000 0.000 0.667 0.000 0.000 0.000 0.000 0.000 0.00.0 0.000 0.667 Lead 0.000 0.000 0.000 0.000 0.164 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.164 Mercury 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- denum 0.000 0.000 0.000 0.000 0.143 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.143 Nickel 0.000 0.000 0.000 0.000 0.222 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.222 Selenium 0.000 0.000 0.000 0.000 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Zinc 0.000 0.000 0.000 0.000 3.550 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.550 Total Phos- horus 0.000 0.000 0.000 0.000 71.944 0.000 0.000 0.000 0.000 0.000 0.000 0.000 71.94 "I certify, under penalty of law, that this document was Drenared under my direction or sunervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the, information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier c:,) -9-/ 4 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 3 Acres Utilized: 2.1 Land Owner: Harry Myers Annual Dry Tons Applied: 6.0308 Site #: NC-UN18 Acres Permitted: 2.1 Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop I Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 0 Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet Moist) Precip. past 24 Hrs. inches 7�Y CD 'S o w o .. # o w �• N' w o' 0 ? * N w o TKN mg/kg Z > o El as o w mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 15 42 17.05 2.872 WWTP cake D 0 S 0.5 0.3 37,900 4,870 2 70.911 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 421 As Cd Cu Cr Pb Hg Mo Ni Se Zn I P 70.911 0.000 Lime Applied Annual lbs/acre 0.080 0.011 1.873 0.724 0.178 0.002 0.155 0.241 0.029 3.854 1 78.118 :::::::::::::::::°:: ' ::::::;: 0.484 0.05 6.354 7.407 0.961 0.019 0.655 1.359 0.109 27.175::::::::::::::::::::::::::::::::::::: 0.564 0.061 8.227 8.131 1.139 0.021 0.810 1.600 0.138 31.029 36 34 1 1338 1 X 1 267 1 15 1 X 374 1 89 2498 2 12 50 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 s t/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation cl% 9�/�! **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Appliet• Date x** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach -this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 6.03 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Harry Myers Owner: Same Predominant Soil Series: BdB2-Badin Acres Used: 2.1 Acres Permitted: 2.1 Site #: NC-UN18 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 21 3j 4� 5 4/27/15 6 7 8 ' 9 ;10 2 % Solids 17.05 Arsenic 14 Cadmium 2 Copper 326 Chromium 126 Lead 31 Mercury 0.4 Molyb- denum 27 Nickel 42 Selenium 5 Zinc 671 Total I Phos- horus 13600 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ITotal DT/Ac./ App. Event 1 21 3 4 5 2.87 6 7 8 9 ,10 11 12 o Arsenic 0.000 1 0.000 0.000 0.000 1 0.080 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.080 Cadmium 0.000 0.000 0.000 0.000 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.000 0.000 0.000 0.000 1.873 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.873 Mromium 0.000 0.000 0.000 0.000 0.724 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.724 Lead 0.000 0.000 0.000 0.000 0.178 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.178 Mercury 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- denum 0.000 0.000 0.000 0.000 0.155 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.155 Nickel 0.000 0.000 0.000 0.000 0.241 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.241 Selenium 0.000 0.000 0.000 0.000 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Zinc 0.000 0.000 0.000 0.000 3.854 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.854 ITotal Phos- horus 0.000 0.000 0.000 0.000 78.118 0.000 0.000 0.000 0.000 0.000 0.000 0.000 78.12 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. it am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier -/4 Date ,DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 4 Acres Utilized: 4.9 Land Owner: Harry Myers Annual Dry Tons Applied: 12.0616 Site #: NC-UN18 Acres Permitted: 4.9 Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 o Q Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist) Precip. Past 24 Hrs. inches a 0 v o o' o w o ° C o w w« ; - ? N * 0 m o ?' 0 TKN mg/kg Z > o 3 �; o w• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of CropType yP Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 15 84 17.05 2.462 WWTP cake D 0 S 0.5 0.3 37,900 4,870 2 60.781 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 '0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.600 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ..... TOTALS: 84 0:::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 60.781 0.000 Lime Applied Annuallbs/acre 0.069 0.536 0.605 36 1 0.010 0.067 0.077 34 1.605 7.86 9.465 1 1338 0.620 8.417 9.037 X 0.153 1.122 1.275 267 0.002 0.022 0.024 15 0.133 0.794 0.927 X 0.207 1.608 1.815 374 0.025 0.129 0.154 89 3.304 33.131 36.435............ 2498 66.966 ::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2n d Crop 122 50 "I certify, under penalty of law, that this .document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." /� *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) - ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 12.06 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Harry Myers Owner: Same Predominant Soil Series: BdB2-Badin Acres Used: 4.9 Acres Permitted: 4.9 Site #: NC-UN18 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw. Percent #): Sample or 1 2 3 4 5 6 7 8 j 9 10 11 12 Com- posite Date 4/27/15 % Solids 17.05 Arsenic 14 Cadmium Total Phos- _phorus Total 1 2 3 4 5 6 7 8 9 L0 '11 12 DT/Ac./ o App. y Event 2.46 Arsenic 0.000 0.000 0.000 0.000 0.069 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.069 Cadmium 0.000 0.000 0.000 0.0.00 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Copper 0.000 0.000 0.000 0.000 1.605 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.605 Chromium 0.000 0.000 0.000 0.000 0.620 0.000' 0.000 0.000 0.000 0.000 0.600 0.000 0.620 Lead 0.000 0.000 0.000 0.000 0.153 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.153 Mercury 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- denum 0.000 0.000 0.000 0.000 0.133 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.133 Nickel 0.000 1 0.000 0.000. 0.000 0.207 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.207 Selenium 0.000 0.000 0.000 0.000 0.025 0.000 0.000 0.000 0.000 0.000 0.000 E0.000 0.025 -Zinc 0.000 0.000 0.000 0.000 3.304 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.304 Total Phos- 0.000 0.000 0.000 0.000 66.966 0.000 0.000 0.000 0.000 0.000 0.000 0.000 66.97 horus -I cel-Llly, uLLueL- NeualLy ui Law, gnat inls aocumeni was preparea unaer my alrectlon or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. ,I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 5 Acres Utilized: 14.9 Land Owner: Harry Myers Annual Dry Tons Applied: 105.4486 Site #: NC-UN18 Acres Permitted: 14.9 Operator: Same Predominant Soil Series: TbB2-Tatum Cation Exchange Capacity (non 503): N/A Cron 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 0 ..0 Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Moist) Precip. Past 24 Hrs. inches Y 4 '° o S w o w w P , * 0 w 0 TKN mg/kg Z �o o g w• mg/kg Nitrate and Nitrite mg/kg PAN Applied pp ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 15 238 17.05 2.294 WWTPC D 0 D 0.5 0.3 37,900 4,870 2 56.633 NA Fescue May 15 116,060 5.36 1.740 WTP Liquid D 0 S 0.5 0.4 11,900 373 776 19.396 NA Fescue June 15 26,000 5.36 0.390 WTP Liquid D 0 S 0.5 0.4 11,900 373 776 4.347 NA Fescue Sept 15 253500 3.74 2.653 WTPL D 0 S 0.5 0.4 13,400 1,600 1,330 Na 36.351 Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.00.0 0.000 0.006 0.000 0.00.0 .0.000 0.060 _ 0.000 0.000 0.006 6.600 0.000 0.000 0.000 0.000 0.000 0.000. Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 238 395500 :::::::::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 80.377 36.351 Lime Applied Annual lbs/acre 0.274 0.033 6.276 2.476 0.363 0.006 0.616 0.404 0.071 4.802 90.102 ::::;: ::::::::::::::::::::.':.':.':.':.m:M':.':.':.':.':.m:.':.'.'.m.*. :::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.815 0.1 8.653 16.851 1.535 0.036 1.222 0.936 0.2 40.097 Current Cumulative lbs/ac 1.089 0.133 14.929 19.327 1.898 0.042 1.838 1.340 0.271 44.899 Permitted C. P. L. R.**** 36 34 1338 1 X 1 267 1 15 1 X 374 89 1 2498 t Cro it PAN Limit 1st/ PermiP 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false ' information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation �� �-J�'✓� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 a' Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge 70.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate r DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Total Dry Tons Applied (Annual): 105.45 Cation Exchange Capacity (non 503 only): N/A Same Predominant Soil Series: TbT2-Tatum 14.9 Site #: NC-UN18 Field #: 5 Residual Analvsis Data (Heave Metals and Tntal Phnenlhnrne ,an rnerflr" o/ Q-].Ac , - D.,.., D...•..--J. ui. City of Monroe WQ0001346 Harry Myers Owner: 14.9 Acres Permitted: Sample or I L 2j L3 j4 5 6 7 8 9 10 11 12 Com- posite Date 4/6/15 4/27/15 6/24/15 % Solids 1 5.36 1 17.05 3.74 Arsenic 23 14 21 Cadmium 3 2 2 Copper 462 326 530 Chromium 194 126 202 Lead 22 31 24 Mercury 0.4 0.4 0.4 Molyb- denum 47 27 55 Nickel 21 42 23 Selenium 5 5 5 Zinc 173 671 186 Total Phos- 2580 13600 3150 horus A� �1 TT___-_AT_.__■ri• r■T aau _T ♦ xlx�&LL %.5\\l'\\1i\\V%l \\■ \\\\/•A ■•r•\+�• Total 1 2j L3J L4J 5 6 7 8j 9 Oj 1121 DT/Ac./ c App. Event 2.13 2.29 2.65 y Arsenic 0.000 0.000 0.000 0.098 0.064 0.000 0.111,.1 0.000 0.000 0.000 1 0.000 0.000 0.274 Cadmium f0.000 «, 0.000 0.000 0.013 0.009 0.000 0.011 0.000 0.000 0.000 0.000 0.000 0.033 Copper :M`, 0.000 0.000 0.000 1.968 1.496 0.000 2.812 0.000 0.000 0.000 0.000 0.000 6.276 Chromium 0.000 0.000 0.000 0.826 0.578 0.000 1.072 0.000 0.000 0.000 0.000 0.000 2.476 Lead 0.000 0.000 0.000 0.094 0.142 0.000:, 0.127,__ . ,0.000 0.000 0.000 0.000 0.000 0.363 Mercury 0.000 0.000 0.000 0.002 0.002 0.000, 0.002 0.000 0.000 0.000 O 000 0.000 0.006 Molyb- denum 0.000 0.000 0.000 0.200 0.124 0.000 0.292..__0.000 0:000 0.000 0.000 0.000 0.616 Nickel 0.000 0.000 0.000 0.089 0.193 0.000, A 122 0.000, 0.000 0.000 0.000 0.000 0.404 Selenium 0.000 0.000 0.000 0.021 0.023 0.000- . 0.027_ 0.000. 0.000 0.000 0.000 0.000 0.071 Zinc 0.000 0.000 0.000 0.737 3.079 0.000 .:0.987,1 0.000 0.000 1 0.000 0.000 0.000 4.802 Total Phos- 0.000 0.000 0.000 10.991 62.397 0.000 < ,.16.714_ .0.000. -.0:000 0.000 0.000 0.000 90.10 horus ��- --ja aa.., \ua\, iu10 uvMuulCui Was prureu unuer my airecilon or supervision in accordance - with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". C Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 6 Acres Utilized: 6.9 Land Owner: Harry Myers Annual Dry Tons Applied: 32.6207 Site #: NC-UN18 Acres Permitted: 6.9 Operator: Same Predominant Soil Series: ChA-Chewacla Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 149 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: pill � � � +� 0 Q � Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons ' % Solids Volume Applied per Acre D Tons/Ac (Dry ) Residual Sources (NPDES # WQ# Fert., Animal Waste, etc) Soil Cond. (Dry. Wet, Moist) Precip. Past 24 Hrs. inches � � N Zs R' �' o w a o o %' �'. � `CD N o � � w ., = * o' TKN mg/kg Z Y o c0°c n �• mg/kg Nitrate and Nitrite mg/kg PAN Applied pp Ibs/acre ) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 15 126 1 17.05 2.622 WWTPC D 0 S 0.5 0.3 37,900 4,870 2 64.745 NA Fescue June 15 65,000 5.36 2.106 WTP Liquid D 0 S 0.5- 0.4 11,900 373 776 23.470 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ......... ....... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): .................... TOTALS: 1261 65000 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 88.214 0.000 Lime Applied Annuallbs/acre 0.170 0.586 0.756 36 0.023 0.078 0.101 34 3.655 5.911 9.566 1 1338 1 1.478 12.324 13.802 X 1 0.255 1.284 1.539 267 1 0.004 0.029 0.033 15 1 0.340 0.858 1.198 X 0.309 1.8 2.109 374 1 0.047 0.15 0.197 89 4.247 40.04 44.287 2498 82.185 1: ::: Date Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop 4 1 9 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �+ *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Harry Myers Owner: Same Predominant Soil Series: Acres Used: 6.9 Acres Permitted: 6.9 Site #: NC-UN18 Field #: 32.62 N/A ChA-Chewacla 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mvYkg. % Solids use Raw Percent ft Wmrp Com- positeD. - , Total ' .. :� .Il Annual rieavv 1VJ.etal Yield Loadings Walculated in Ihs/acrel: Total 1 2 3 4 5 6 7 8 9 L01 iij 2 DT/Ac./ o App. Event 2.11 2.62 Arsenic 0.000 0.000 .0.000 0.097 1 0.073 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.170 Cadmium 0.000 0.000 0.000 0.013 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Copper 0.000 0.000 0.000 1.946 1.710 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.655 Chromium 0.000 0.000 0.000 0.817 0.661 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.478 Lead 0.000 0.000 0.000 0.093 0.163 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.255 Mercury 0.000 0.000 0.000 0.002 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.198 0.142 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.340 Nickel 0.000 0.000 0.000 0.088 0.220 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.309 Selenium 0.000 0.000 0.000 0.021 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.047 Zinc 0.000 0.000 '0.000 0.729 3.519 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.247 Total Phos- 0.000 0.000 0.000 10.867 71.318 0.000 0.000 0.000 0.000 0.000 0.000 0.000 82.185 horus I ceru,y, Ulmer peuauy ui ►aw, inat inis aocument was preparea unaer my mrection or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". �t _ Signature of Land Applier i Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 7 Acres Utilized: 5_4 Land Owner: Harry Myers Annual Dry Tons Applied: 16.0821 Site #: NC-UN18 Acres Permitted: 5.4 Operator: Same Predominant Soil Series: CmB-Cid Cation Exchange Capacity (non 503): N/A Cron 1 Name: Fescue (Past.) Cron 1 Max. PAN: 141 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 o Q Volume applied PP enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (D�' Wet Moist) Precip. Past 24 Hrs. inches Y K 'o co t? o w a ow' o c wrt _ N' :h w * N TKN mg/kg z o o0 0 mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 15 112 17.05 2.978 WWTP cake D 0 S 0.5 0.3 37,900 4,870 2 73.537 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 .. 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.0.00 0.000 - 0.000 0.000 . Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 112 0 :::::::::::::: AS Cd Cu Cr Pb Hg Mo Ni Se Zn P 73.537 0.000 Lime Applied14 Annual lbs/acre 0.083 0.111 0.194 36 0.012 0.018 0.030 1 34 1.942 3.27 5.212 1 1338 0.750 0.961 1.711 1 X 0.185 0.277 0.462 1 267 0.002 0.006 0.008 15 0.161 0.222 0.383 X 0.250 0.379 0.629 1 374 0.030 0.046 0.076 1 89 3.996 8.312 12.308 2498 81.002:::::::::::: . . Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Lim s Limit 1 t/2nd Crop P 141 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, i aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 16.08 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Harry Myers Owner: Same Predominant Soil Series: CmB-Cid Acres Used: 5.4 Acres Permitted: 5.4 Site #: NC-UN18 Field #: 7 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 11 21 3 4 , 5 4/27/15 6 7 8 _9j 10 LIJ 12 % Solids 17.05 Arsenic 14 Cadmium 2 Copper 326 Chromium 126 Lead 31 Mercury 0.4 Molyb- denum 27 Nickel 42 Selenium 5 Zinc 671 Total I Phos- horus 13600 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 2 3 4 5 2.98 6 7 8 9 10 11 12 y 0 Arsenic 0.000 0.000 0.000 0.000 1 0.083 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.083 Cadmium 0.000 0.000 0.000 0.000 1 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Copper 0.000 0.000 0.000 0.000 1.942 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.942 Chromium 0.000 0.000 0.000 0.000 0.750 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.750 Lead 0.000 0.000 0.000 0.000 0.185 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.185 Mercury 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.002 y' Molyb- denum 0.000 0.000 0.000 0.000 0.161 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.161 Nickel 0.000 0.000 0.000 0.000 0.250 0.000. 0.000. 0.000 0.000 0.000 0.000 0.000 0.250 A Selenium 0.000 0.000 0.000 0.000 0.030 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.030 Zinc 0.000 0.000 0.000 0.000 3.996 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 3.996 Total Phos- horus 0.000 0.000 0.000 0.000 81.002 0.000 0.000, 0.000 0.000 0.000 0.000 0.000 81.00 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance --with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 8 Acres Utilized: 3 Land Owner: Harry Myers Annual Dry Tons Applied: 12.2347 Site #: NC-UN18 Acres Permitted: 3 Operator: Same Predominant Soil Series: CmB-Cid Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 141 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 0 A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. Wet' Moist) Precip. Past 24 Hrs. inches �Y 8 'b r, a m, * ° c ;n �, * w' �. a g 9 w * w �. 0 TKN mglkg Z > -+ o g w' mg/kg Nitrate and Nitrite mg/kg PAN Applied lbs/acre ( ) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 Dec 15 75 19.37 4.078 WWTPC D 0 S 0.5 0.3 33,100 2,430 2 84.974 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 751 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 84.974 0.000 Lime Applied Annual lbs/acre 0.122 0.082 0.204 36 0.016 0.014 0.030 34 2.920 2.414 5.334 1338 0.995 0.709 1.704 X 0.269 0.205 0.474 267 0.007 0.004 0.011 15 0.302 0.164 0.466 X 0.375 0.28 0.655 374 0.041 0.034 0.075 89 7.234 6.138 13.372 2498 143.546 :::::::::::::::::::::::::::::: *: . .......................... Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1st/2nd Crop 141 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �*Application Method: S - Surface, IN - Injection, INC - Incorporation � c '/ 14. **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, t aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Monroe Total Dry Tons Applied (Annual): 12.23 WQ0001346 Cation Exchange Capacity (non 503 only): Harry Myers Owner: Same Predominant Soil Series: 3 Acres Permitted: 3 Site #: NC-UN18 Field #: N/A CmB-Cid 8 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 11 21 3 _4j 5j 6 7 8 9 10 11 10/26/15 12 % Solids 19.37 Arsenic 15 Cadmium 2 Copper 358 Chromium 122 Lead 33 Mercury 0.9 Molyb- denum 37 Nickel 46 Selenium 5 Zinc 887 Total Phos- horus 17600 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ITotal DT/Ac./ App. Event 1 2 3 4 5 6 7 8 9 �10 1112 4.08 o y Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.122 0.000 1 0.122 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 0.000 0.016 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.920 0.000 2.920 Ichromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.995 0.000 0.995 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.269 0.000 0.269 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.000 0.007 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.302 0.000 0.302 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.375 0.000 0.375 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.041 0.000 1 0.041 Zinc 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 1 0.000 7.234 0.000 7.234 rTotal Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 143.546 0.000 143.55 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance -with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 6.5 Land Owner: Wayne McBride Annual Dry Tons Applied: 25.0034 Site #: NC-UN25 Acres Permitted: 6.5 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 137 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 S. Y �; o Q Volume applied PP enter one Solids/ ( ) Liquid Cu. Yds Gallons u /o Solids Volume Applied per PP P Acre (Dry Tans/Ac) Residual Sources (NPDES #, W #, Q Fert. Animal , Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches a 4.0 co S o I a o' o w �• N' * •Q'•, 0 = � a� -, w - + 0 TKN mgikg z Y o own_ ° �' mg/kg Nitrate and Nitrite mg/kg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual g Application PP Crop 1 Crop 2 Crop 1 Crop 2 Dec 15 75 19.37 1.882 WWTPC D 0 S 0.5 0.3 33,100 2,430 2 39.219 NA Fescue Dec 15 64 23.69 1.964 WTPC D 0 S 0.5 0.4 12,700 1,690 2 20.630 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000� 0.000 ......... ....... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ...... . TOTALS: 139 0 ::::::;:... As Cd Cu Cr Pb H Mo Ni Se Zn P !L8491 0.000 Lime Applied Annuallbs/acre 0.155 0.015 3.406 1.186 0.207 0.005 0.363 0.275 0.038 4.352 85.572 :: :: 0.475 0.062 6.017 9.065 0.762 0.029 0.81 1.212 0.111 23.304 0.630 0.077 9.423 10.251 0.969 0.034 1.173 1.487 0.149 27.656 36 34 1338 X 267 15 X 374 89 2498 ................................ 137 50 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." _�,• *Application Method: S - Surface, IN - Injection, INC - Incorporation /��Lt **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date "** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 25.00 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Wayne McBride Owner: Same Predominant Soil Series: TaB-Tatum Acres Used: 6.5 Acres Permitted: 6.5 Site #: NC-UN25 Field #: 1 Residual Analvsis Data (Heave Metals and Total Phosuhorus use me/kLy. % Solids use Raw Percent #l: Com- posite Date Total ' I • Annuai Heavy ivietai v ieia Loadings (ualculated in lbs/acre): Total 11 21 3 4, 5 6 7 8 9 10 11 12 DT/Ac./ c App- Event 1.96 1.88 Arsenic 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.098 1 0.056 0.000 0.155 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 0.008 0.000 0.015 Copper '0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.058 1.348 0.000 3.406 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.727 0.459 0.000 1.186 Lead 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.082 0.124 0.000 0.207 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.003 0.000 0.005 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.224 0.139 0.000 0.363 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.102 0.173 0.000 0.275 Selenium 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.020 0.019 0.000 0.038 Zinc 0.000 0.000 0.000 .,0.000 0.000 0.000 0.000 0.000 0.000 1.013 3.339 0.000 4.352 Total Phos- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 19.326 66.246 0.000 85.572 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A.COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 3 Acres Utilized: 14.1 Land Owner: Wayne McBride Annual Dry Tons Applied: 24.1630 Site #: NC-UN25 Acres Permitted: 14.1 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 137 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 >~ Q Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons o/a Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES # WQ# Fert., Animal Waste, etc) Soil Cond. D (Dry, e ' Moist) Precip. past 24 Hrs. inches D b �• '. w * ° C o � .- �J 0 w w TKN mg/kg Z Y 9 o � oa o g R. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbslacre) Name of CropType YP Receiving Residual Application Crop 1 Crop 2 Crop I Crop 2 Dec 15 131 19.37 1.516 WWTPC D 0 S 0.5 0.3 33,100 2,430 2 31.579 NA Fescue Dec 15 14 23.69 0.198 WTPC D 0 S 0.5 0.4 12,700 1,690 2 2.080 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): ................... TOTALS: 1451 As Cd Cu Cr Pb Hg Mo Ni Se Zn I P 33.659 1 0.000 Lime ARplied Annuallbs/acre 0.055 0.007 1.293 0.443 0.108 0.003 0.135 0.150 0.017 2.792 55.312:::::::::::::::::::::::::::::::: ............ Date lbs/ac Prior Years Cumulative lbs/ac 0.665 0.1 8.101 11.316 0.84 0.027 1.101 1.46 0.129 27.44 Current Cumulative lbs/ac 0.720 0.107 9.394 11.759 0.948 0.030 1.236 1.610 0.146 0.232 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 ]2498 Permit PAN Limit 1st12nd Crop .P 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation !� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Wayne McBride Owner: Same Predominant Soil Series: Acres Used: 14.1 Acres Permitted: 14.1 Site #: NC-UN25 Field #: 24.17 N/A TaB-Tatum 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- Iposite Date 11 21 3 4 JJ 6 7 L 8 9 10 9/29/15 11 10/26/15 12 % Solids 23.69 19.37 Arsenic 25 15 Cadmium 2 2 Copper 524 358 Chromium 185 122 Lead 21 33 Mercury 0.4 0.9 Molyb- denum 57 37 Nickel 26 46 Selenium 5 5 Zinc 258 887 Total I Phos- horus 4920 17600 ;Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 21 5 6 7 8 9 10 0.20 11 1.52 h 2 o rt in " Arsenic 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.010 1 0.045 0.000 1 0.055 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.006 0.000 0.007 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.208 1.085 0.000 .1.293 .-Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.073 0.370 0.000 0.443 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 0.100 0.000 0.108 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 01 000 0.000 0.000 0.003 0.000 0.003 Molyb- . denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 0.112 0.000 0.135 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 0.139 0.000 0.150 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.015 0.000 0.017 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.102 2.689 0.000 2.792 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.948 53.363 0.000 55.312 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance Ath a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 15.4 Land Owner: Emerson McBride Annual Dry Tons Applied: 46.2016 Site #: NC-UN26 Acres Permitted: 15.4 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue Crop 1 Max. PAN: 137 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 ° o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES # , WQ# Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. past 24 Hrs. inches �Y o a M o c � - * w' K w `; u * N �'•. 0 TKN mg/kg Z > o � � w. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Sep 15 75 22.47 1 0.922 WWTPC D 0 S 1 0.5 6.3 29,900 2,710 2 17.536 NA Fescue Sep 15 50 19.84 0.542 WTPC D 0 S 0.5 0.4 24,100 2,720 2 10.757 NA Fescue Oct 15 125 22.47 1.536 WWTPC D 0 S 0.5 0.3 29,900 2,710 2 29.227 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 250 0 ::::::::... As Cd Cu Cr Pb Hg Mo Ni Se Zn P 57.520 0.000 Lime Applied Annuallbs/acre 0.081 0.489 0.570 36 1 0.012 0.089 .0.101 34 2.467 6.754 9.221 1 1338 0.806 8.679 9.485 X 0.140 0.973 1.113 267 0.003 0.018 0.021 15 0.199 0.782 0.981 X 1 0.251 1.345 1.596 374 1 0:030 0.086 0.116 89 4.356 28.37 32.726 1 2498 97.462 .Date ........................... lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Li 2nd Limit 1st/ Crop P 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *x* Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate f1FNR FnR,M FSF (19/9MR1 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 46.20 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Emerson Mcbride Owner: Same Predominant Soil Series: TaB-Tatum Acres Used: 15.4 Acres Permitted: 15.4 Site #: NC-UN26 Field #: 1 Residual Analvsis Data (Heave Metals and Total Phosnhorus use mu/ku_ %. Ralirla nee Raw Percent M. Com- posite Date; Total Phos- phorus cxuuuaa iicavy 1--al r-im ,uunumgs <<,aicuiazeu in iosiacre): Total 1 21 3 4 5 6 7 8 9 10 11 12 - DT/Ac./ o App. Event 0.54 2.46 Arsenic' 0.000 0.000 0.000 0.000 0.000 0.000 0.017 1 0.000 0.064 0.000 1 0.000 0.000 0.081 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.010 0.000 0.000 0.000 0.012 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.511 0.000 1.957 0.000 0.000 0.000 2.467 ,Chromi 0.000 0.000 0.000 0.000 0.000 0.000 0.177 0.000 0.629 0.000 0.000 0.000 0.806 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.027 0.000 0.113 0.000 0.000 0.000 0.140 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.002 0.000 0.000 0.000 0.003 Molyb- denum num 0.000 0.000 0.000 0.000 0.000 0.000 0.047 0.000 0.152 0.000 0.000 0.000 0.199 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 -0.035 0.000 0.216 1 0.000 0.000 0.000 0.251 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.005 0.000 0.025 0.000 0.000 0.000 0.030 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.591 0.000 3.766 0.000 0.000 0.000 4.356 ITotal Phos- 0.000 0.000 0.000 0.000 0.000 0.000 11.924 0.000 85.538 0.000 0.000 0.000 97.462 horus "I certify, under of law, that this document penalty was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". r Signature of Land Applier Date l DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 2 Acres Utilized: 6_1 Land Owner: Emerson McBride Annual Dry Tons Applied: 17.8162 Site #: NC-UN26 Acres Permitted: 6.1 Operator: Same Predominant Soil Series: TaB2-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue Crop 1 Max. PAN: 137 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 .c +� s~ Q 0 Volume applied Pp (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. D W Moist) Precip. Past 24 Hrs. inches Y 410 a '� 5 rs o * o ° c w �», � W �, w * TKN mg/kg Z E o E3 as c g w• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Sep 15 50 22.47 1.551 WWTPC D 0 S 0.5 0.3 29,900 2,710 2 29.515 NA Fescue Sep 15 50 19.84 1.370 WTPC D 0 S 0.5 1 0.4 24,100 2,720 2 27.156 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 1001 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 56.670 1 0.000 Lime Applied Annual lbs/acre 0.084 0.012 2.525 0.844 0.140 0.003 i 0.214 0.224 0.029 3.869 84.115 ::::::::::::::::::::::::::::: :::::::::::::::::::::::::::::::::::::: :: Date lbs/ac Prior Years Cumulative lbs/ac 0.404 0.07 6.37 7.443 1.105 0.018 0.652 1.382 0.079 30.216 Current Cumulative lbs/ac 0.488 0.082 8.895 8.287 1.245 0.021 0.866 1.606 0.108 34.085 Permitted C. P. L. R.**** 36 34 1338 X 1 267 1 15 X 374 89 2498 Permit PAN Limit 1 st/2nd Cro P 137 50 "I certify, under penalty of law, that this Vocument was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date x** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Emerson McBride Owner: Same Predominant Soil Series: Acres Used: 6.1 Acres Permitted: 6.1 Site #: NC-UN26 Field #: 17.82 N/A TaB2-Tatum 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5j 6 7 6/24/15 8 9 8/25/15 10 11 12 % Solids 19.84 22.47 Arsenic 16 13 Cadmium 2 2 Copper 471 398 Chromium 163 128 Lead 25 23 Mercury 0.8 0.4 Molyb- denum 43 31 Nickel 32 44 Selenium 5 5 Zinc 545 766 Total Phos- horus 11000 17400 [Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App• Event 1 2j 3] 4 5 _6j 7 1.37 8 9j 1.55 10 11 12 rt y Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.044 0.000 0.040 0.000 0.000 0.000 0.084 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.005 0.000 0.006 0.000 0.000 0.000 0.012 Copper 0.000 0.000 0.000 0.000 0:000 0.000 1.291 0.000 1.235 0.000 0.000 0.000 2.525 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.447 0.000 0.397 0.000 0.000 0.000 0.844 Lead 0.000 0.000 0.000 0.000 0:000 0.000 0.069 0.000 0.071 0.000 0.000 0.000 0.140 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.001 0.000 0.000 0.000 0.003 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.118 0.000 0.096 0.000 0.000 0.000 0.214 el 0.000 0.000 0.000 0.000 0.000 0.000 0.088- 0.000 0.136 0.000 0.000 0.000 0.224 um 0.000 0.000 0.000 0.000 0.000 0.000 0.014 0.000 0.016 0.000 0.000 0.000 0.029 c r 0.000 0.000 0.000 0.000 0.000 0.000 1.493 0.000 2.376 0.000 0.000 0.000 3.869 l Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 30.140 0.000 53.975 0.000 0.000 0.000 84.115 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Q�_ --�?-f -//, Signature of Land Applier Date DENR FORM MFLSF (12/2.006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 3 Acres Utilized: 10.5 Land Owner: Emerson McBride Annual Dry Tons Applied: 37.8473 Site #: NC-UN26 Acres Permitted: 10.5 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue Crop 1 Max. PAN: 137 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 $. = +- Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES # WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Moist) Precip. Past 24 Hrs. inches Y 1IC30 cro b a * o * w' ;* � w w * w' * 0 TKN mg/kg Z � o 0 as o M. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Oct 15 200 22.47 3.605 WWTPC D 0 S 0.5 0.3 29,900 2,710 2 68.586 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 200 0 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 68.586 0.000 Lime Applied Annual lbs/acre 0.094 0.014 2.870 0.923 0.166 0.003 0.224 0.317 0.036 5.523 125.454::::::::::::::::::::::::::::::::: ::: Date lbs/ac Prior Years Cumulative lbs/ac 0.641 0.101 9.551 14.065 1.228 0.024 1.09 1.705 0.114 33.565 Current Cumulative lbs/ac 0.735 0.115 12.421 14.988 1.394 0.027 1.314 2.022 0.150 39.088 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 1 374 89 1 2498 't A Limit 1st/ 2nd Crop Perms PAN 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 i Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* l Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report - Facility Name: Permit #: Operator: i Acres Used: City of Monroe Total Dry Tons Applied (Annual): 37.85 WQ0001346 - Cation Exchange Capacity (non 503 only): N/A Emerson McBride Owner: Same Predominant Soil Series: TaB-Tatum 10.5 Acres Permitted: 10.5 Site #: NC-UN26 Field #: 3 Residual Analvsis Data (Heave Metals and Total Phosphorus use m&ke. % Solids use Raw Percent ft Com- posite Date Total Phos- _phorusEENEENEEMENE Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total 1 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ __2j o App- Event 3.61 14 Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.094 0.000 0.000 0.000 0.094 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 0.000 0.000 0.000 0.014 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.870 0.000 0.000 0.000 2.870 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.923 0.000 0.000 0.000 0.923 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.166 0.000 0.000 0.000 0.166 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0.000 0.003 Molyb- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.224 0.000 0.000 0.000 0.224 denum Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.317 0.000 0.000 0.000 0.317 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 0.000 0.000 0.000 0.036 Zinc 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 5.523 0.000 0.000 0.000 5.523 Total Phos- 0.000 0.000 0.000 0.000 0.000 0.000 0.000... 0.000 125.454 0.000 0.000 0.000 125.454 horus "1 certily, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date . DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 4A Acres Utilized: 12.1 Land Owner: Emerson McBride Annual Dry Tons Applied: 48.0797 Site #: NC-UN26 Acres Permitted: 12.1 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue Crop 1 Max. PAN: 137 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 1. +� A Volume applied pp enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume A lied er pp p Acre o Tons/Ac (ry ) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D We ' Moist) Precip. Past 24 Hrs. inches > " b �s' o o� w * 0 c �' �, � ; -- * w a � .��, � * N * w c �3 TKN mg/kg Z Y o w mg/kg Nitrate and Nitrite mg/kg PAN Applied pp ( lbs/acre) Name of Crop Type Receiving Residual g Application Crop 1 Crop 2 Crop 1 Crop 2 Oct 15 175 1 22.47 2.737 WWTPC D 0 S 0.5 0.3 29,900 2,710 2 52.078 NA Fescue Oct 15 75 23.69 1.237 WTPC D 0 S 0.5 0.4 12,700 1,690 2 12.987 NA Fescue 0.000 0.000 0.000 0.000 0.000 j 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000, 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000- 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 250 0 :::::::::::::c As Cd Cu Cr Pb H Mo I Ni Se Zn P 65.0 55 0.000 Lime Applied Annual lbs/acre 0.133 0.549 0.682 36 0.016 0.086 0.102 34 3.475 7.842 11.317 1338 1.158 8.659 9.817 X 0.178 1.099 1.277 267 0.003 0.021 0.024 15 0.311 0.898 1.209 X 0.305 1.535 1.840 374 1 0.040 0.095 0.135 89 1 4.831 31.46 36.291 2498 107.420 ::::::::::::::::::::::::::::::: :: .:::""':*""::':'':-""".:.""*-:::*"'* ."""-:: Date lbs/ac Prior Years Cumulative lbs/ac July 1950 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1st/2nd Crop jiFT 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 x** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Emerson Mc Bride Owner: Same Predominant Soil Series: Acres Used: 12.1 Acres Permitted: 12.1 Site #: NC-UN26 Field #: 48.09 N/A TaB-Tatum 4A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/ke. % Solids use Raw Percent ft Sample or Com- posite Date 1 __2j 3j 4 L5J 1 6j Ljj_8 v vL 9 8/25/15 �0 9/29/15 11 12 % Solids 22.47 23.69 Arsenic 13 25 Cadmium 2 2 Copper 398 524 Chromium 128 185 Lead 23 21 Mercury 0.4 0.4 Molyb- denum 31 57 Nickel 44 26 Selenium 5 5 Zinc 766 258 Total Phos- horus ♦- _1 TT__ AR 17406 4920 Annuai neavy Metal r ieia Loaaings (Ualculated in lbs/acre): Total L 11 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ o App. Event 2.74 1.24 y Arsenic 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.071 0.062 1 0.000 0.000 0.133 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 0.005 0.000 0.000 0.016 Copper .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.179 1.296 0.000 0.000 3.475 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.701 0.458 0.000 0.000 1.158 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.126 0.052 0.000 0.000 0.178 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.001 0.000 0.000 0.003 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.170 0.141 0.000 0.000 0.311 Nickel 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.241 0.064 1 0.000 0.000 0.305 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 0.012 0.000 0.000 0.040 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.193 0.638 0.000 0.000 4.831 Total Phos- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 95.248 12.172 0.000 0.000 107.420 horus "I certify unde f 1 , r I pen" %T o aw, tat this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier o) Date DENR FORM MFLSF (19/2nnm ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 4B Acres Utilized: 12.7 Land Owner: Emerson McBride Annual Dry Tons Applied: 9.4618 Site #: NC-UN26 Acres Permitted: 12.7 Operator: Same Predominant Soil Series: CmB-CID Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue Crop 1 Max. PAN: 141 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 ° ° ° Q Volume applied enter one Solids/ ( ) Liquid 9 Cu. Yds Gallons /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. (DrY, Moist) Precip. Past 24 Hrs. inches > c� , = �' o ,P, a o 0 c qO P �, * N *w, w � 0 P_ * N ter. TKN mg/kg Z B o B °q ° ° �. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Oct 15 50 1 22.47 0.745 WWTPC D 0 S 0.5 0.3 29,900 2,710 1 2 14.176 NA Fescue 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 501 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 14.176 0.00o Lime Applied Annual lbs/acre 0.019 0.481 0.500 36 0.003 0.088 0.091 34 0.593 6.836 7.429 1338 0.191 8.636 8.827 X 0.034 1.053 1.087 267 0.001 0.02 0.021 15 0.046 0.759 0.805 X 1 0.066 1.467 1.533 374 1 0.007 0.085 0.092 89 1.141 30.867 32.008 2498 25.926 :::::::::::::::::::::::::::: .::::::::::::::::::::: :::: .......................... ::::::::::::::::::::::::::::::::::::::::::::::::::: ........................... Date lbs/ac Prior Years Cumulative lbs/ac July 1950 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop 141 50 "I certify, under penalty of law, that this document was prepared undermy direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 x** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate nr=niR GnRnn FCF ri�i9nnan ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 9.46 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Emerson McBride Owner: Same Predominant Soil Series: CmB-Cid Acres Used: 12.7 Acres Permitted: 12.7 Site #: NC-UN26 Field #: 413 Residual Analvsis Data (Heavy Metals and Total Phosnhorus use mu/lru_ %. ,qnlid.q nce Raw Pe.rrent #)- Com- .. Date Non googol .. P . . .EENEENEEM ENE tiuuda. ncavy .ivieiai rieia Loaainis (Caicuiatea in insiacre►_ Total 1 2j 3 4 5 6 7 8 9 10 11 12 DT/Ac./ *3 0 App. a_ Event 0.75 y Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.019 0.000 1 0.000 0.000 0.019 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0.000 0.003 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.593 0.000 0.000 0.000 0.593 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.191 0.000 0.000 0.000 0.191 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 0.000 0.000 0.000 0.034 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 " 0.000 0.001 0.000 0.000 0.000 0.001 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.046 0.000 0.000 0.000 0.046 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.066 0.000 0.000 1 0.000 0.066 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.000 0.000 0.000 0.007 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.141 0.000 0.000 0.000 1.141 Total Phos- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 25.926 0.000 0.000 0.000 25.926 horus 1 %.Wl L11J', LL11LLG1 NcualLy ui .aw, LdaL Lms document was ,prepares under my airection or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/20061 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 5 Acres Utilized: 11.6 Land Owner: Emerson McBride Annual Dry Tons Applied: 40.6812 Site #: NC-UN26 Acres Permitted: 11.6 Operator: Same Predominant Soil Series: TaB2-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (hay) Crop 1 Max. PAN: 137 Crop 2 Name: Fescue (hay) Crop 2 Max. PAN: 50 ° N ° Q Volume applied enter one Solids/ ( ) Li Liquid 9 Cu. Yds Gallons o /o Solids Volume A lied er PP P - Acre (Dry Tons/Ac) (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Past 24 Hrs. inches � b o S' ao. n �', N Z w * N 0 TKN mg/kg Z Y o D d° o mg/kg Nitrate and Nitrite mg/kg ( Ibs/acre) Name of CropType Receiving Residual p, Application Crop 1 Crop 2 Crop 1 Crop 2 Aug 15 175 19.1 2.427 WWTPC D 0 S 0.50 0.30 33,100 3,660 11.5 51.803 NA Fescue Aug 15 75 19.841 1.080 WTPC D 0 S 0.5 0.4 24,100 2,720 2 21.420 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.006 0.000 0.000 0.000 0.0.00 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 250 0 ....... :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 73.223 0.000 Lime ApElied Annuallbs/acre 0.098 0.739 0.837 36 0.019 0.099 0.118 34 2.872 10.41 13.282 1 1338 1 0.930 12.069 12.999 X 1 0.195 1.176 1.371 267 1 0.004 0.037 0.041 15 1 0.243 1.235 1.478 X 1 0.263 1.899 2.162 374 0.035 0.215 0.250 89 5.410 33.894 39.304 2498 112.103 :* :::' :::::::::::::::::::::'::::`::::::: ........................... Date lbs/ac Prior Years Cumulative lbs/ac July 15 1950 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop 37 1 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." r� *Application Method: S - Surface, IN - Injection, INC - Incorporation , ZZ **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 x** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate - DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Emerson McBride Owner: Same Predominant Soil Series: Acres Used: 11.6 Acres Permitted: 11.6 Site #: NC-UN-26 Field #: 40.68 N/A TaB2-Tatum 5 Residual Analysis Data (Heave Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): • .. Date 6/24/15 Total • Annual rieavv Metal Yield Loadings (Ualculated in lbs/acrel: Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ o App- Event 2.43 1.08 Arsenic 1 0.000 0.000 0.000 0.000 0.000 0.063 0.035 0.000 1 0.000 0.000 0.000 1 0.000 0.098 Cadmium 0.000 0.000 0.000 0.000 0.000 0.015 0.004 0.000 0.000 0.000 0.000 0.000 0.019 Copper 0.000 0.000 0.000 0.000 0.000 1.854 1.017 0.000 0.000 0.000 0.000 0.000 2.872 Chromium 0.000 0.000 0.000 0.000 0.000 0.578 0.352 0.000 0.000 0.000 0.000 0.000 0.930 Lead 0.000 0.000 0.000 0.000 0.000 0.141 0.054 0.000 0.000 0.000 0.000 0.000 0.195 Mercury 0.000 0.000 0.000 0.000 0.000 0.002 0.002 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.000 0.000 0.000 0.000 0.000 0.150 0.093 0.000 0.000 0.000 0.000 0.000 0.243 denum Nickel 0.000 0.000 0.000 0.000 0.000 0.194 0.069 0.000 0.000 0.000 0.000 0.000 0.263 Selenium 0.000 0.000 0.000 0.000 0.000 0.024 0.011 0.000 0.000 0.000 0.000 0.000 0.035 Zinc 0.000 0.000 0.000 0.000 0.000 4.233 1.177 0.000 0.000 0.000 0.000 0.000 5.410 Total Phos- 0.000 0.000 0.000 0.000 0.000 88.343 23.760 0.000 0.000 0.000 0.000 0.000 112.103 horus i certuy, unuer penatry of law, Mal tnis aocument was preparea unaer my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier -Y 1 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 6 Acres Utilized: 25.8 Land Owner: Emerson McBride Annual Dry Tons Applied: 83.0930 Site #: NC-UN26 Acres Permitted: 25.8 Operator: Same Predominant Soil Series: TaB2-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (hay) Crop 1 Max. PAN: 137 Crop 2 Name: Fescue (hay) Crop 2 Max. PAN: 50 ° ° ° ,_ ° Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume A lied per pp p Acre (Dry TonsiAc) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. past 24 Hrs. inches � �? � o a; -� o o %'� �' w ; 2 0 `; # N' * TKN mgtkg Z > o � 0 w mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Aug 15 250 19.1 1.559 WWTPC D 0 S 0.5 0.3 33,100 3,660 11.5 33.273 NA Fescue Aug 15 150 19.84 0.971 WTPC D 0 S 0.5 1 0.4 24,100 2,720 2 19.262 NA Fescue Sept 15 50 22.47 0.367 WWTPC D 0 S 0.5 0.3 29,900 2,710 2 6.978 NA Fescue Sept 15 50 .19.84 0.324 WTPC D 0 S 0.5 0.4 24,100 2,720 2 6.421 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.600 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000- 0.000 0.000 0.000 0.000 0.000 ......... ....... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ............... TOTALS:. 500 0 ::::::;::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn I P 65.933 1 0.000 Lime Applied Annuallbs/acre 0.092 0.016 2.703 0.887 0.172 0.004 0.231 0.240 0.032 4.693 98.009 :: :: :: .:::::::::::::::: ::::: :: ........................... Date lbs/ac Prior Years Cumulative lbs/ac 0.106 0.02 2.792 0.982 0.256 0.003 0.206 0.373 0.034 7.214 July 1950 Current Cumulative lbs/ac 0.198 0.036 5.495 1.869 0.428 0.007 0.437 0.613 0.066 11.907 Permitted C. P. L. R.**** 36 34 1338 1 X I 267 15 1 X 374 89 2498 Permit PAN Limit lst/2nd Cro p 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Monroe WQ0001346 Emerson McBride Owner: 11.6 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Same Predominant Soil Series: 11.6 Site #: NC-UN-26 Field #: 37.36 N/A TaB2-Tatum 5 Residual Analvsis Data (Heavv Metals and Total Phosphorus use in&ke. % Solids use Raw Percent ft Sample or Com- posite Date 1 2 3 4 5 6 6/24/15 7 6/24/15 8 9 8/25/15 10 11 12 % Solids 19.1 19.84 22.47 Arsenic 13 16 13 Cadmium 3 2 2 Copper 382 471 398 Chromium 119 163 128 Lead 29 25 23 Mercury 0.5 0.8 0.4 Molyb- denum 31 43 31 Nickel 40 32 44 Selenium 5 5 5 Zinc 872 545 766 Total Phos- horus '18200 11000 17400 Annual rieavv iuetal neld Loadln2s (ualculated in lbs/acrel: Total 11 2j 3 4 5 6 7 8j 1 91 10 11j 12 DT/Ac./ o App. Event 1.56 1.30 0.37 y " Arsenic 1 0.000 0.000 0.000 0.000 1 0.000 0.041 0.041 1 0.000 0.010 0.000 1 0.000 0.000 0.092 Cadmium 0.000 0.000 0.000 0.000 0.000 0.009 0.005 0.000 0.001 0.000 0.000 0.000 0.016 Copper 0.000 0.000 0.000 0.000 0.000 1.191 1.220 0.000 0.292 0.000 0.000 0.000 2.703 Chromium 0.000 0.000 0.000 0.000 0.000 0.371 0.422 0.000 0.094 0.000 0.000 0.000 0.887 Lead 0.000 0.000 0.000 0.000 0.000 0.090 0.065 0.000 0.017 0.000 0.000 0.000 0.172 Mercury 0.000 0.000 0.000 0.000 0.000 0.002 0.002 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.000 0.000 0.000 0.000 0.000 0.097 0.111 0.000 0.023' 0.000 0.000 0.000 0.231 denum Nickel 0.000 1 0.000 0.000 0.000 0.000 0.125 0.083 0.000 0.032 0.000 0.000 0.000 0.240 Selenium 0.000 0.000 0.000 0.000 0.000 0.016 0.013 0.000 0.004 1 0.000 0.000 1 0.000 0.032 Zinc 0.000 0.000 0.000 0.000 0.000 2.719 1.412 0.000 0.562 0.000 0.000 0.000 4.693 Total Phos- 0.000 0.000 0.000 0.000 0.000 56.748 28.490 0.000 12.772 0.000 0.000 0.000 98.009 horus i cernry, unuer penany of jaw, tnat tms document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Z-�-�-14 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field M 1 Acres Utilized: 13.4 Land Owner: Leland Wolfe Annual Dry Tons Applied: 40.2053 Site #: NC-UN27 Acres Permitted: 13.4 Operator: Same Predominant Soil Series: GsB-Goldston Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 135 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 .� ° +� Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, W #, Fert., Animal Waste, etc) Soil Cond. We , Moist) Precip. Past 24 Hrs. inches Y � '0 co ? 0 w ° o ?.' w• 7c w N' Z TKN mg/kg Z Y cq o S IR w mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 May 15 280 17.05 3.000 WWTP cake D 0 S 0.5 0.3 37,900 4,870 2 74.086 NA Fescue 0.000 - 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ......... ....... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 2801 0 .::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 74.086 0.000 Lime Applied Annuallbs/acre 0.084. 0.056 0.140 36 0.012 0.022 0.034 34 1.956 1.901 3.857 1338 0.756 0.627 1.383 X 0.186 0.18 0.366 267 0.002 0.002 0.004 15 0.162 0.114 0.276 X 0.252 0.248 0.500 374 0.030 0.028 0.058 89 4.026 5.002 9.028 2498 81.600 :::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 4/15 2182 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop P 35 5 1 0 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Ile **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date xx* Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Leland Wolfe Owner: Same Predominant Soil Series: Acres Used: 13.4 Acres Permitted: 13.4 Site #: NC-UN27 Field #: 40.20 N/A GsB-Golston 1 Residual Analvsis Data (Heave Metals and Total Phosphorus use mz/kLy. % Solids use Raw Percent #): Com- posite Date Total Phos- _phorus,00MEMENEEMEN Annual tleavv lvletal Yield Loadines (Calculated in lbs/acre): Total 1 3j 4 5 6j 7 8 9 10 11 12 DT/Ac./ _2j o App. rt Event 3.00 14 Arsenic 0.000 0.000 0.000 0.000 0.084 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.084 Cadmium 0.000 0.000 0.000 0.000 0.012 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.012 Copper 0.000 0.000 0.000 0.000 1.956 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.956 Chromium 0.000 0.000 0.000 0.000 0.756 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.756 Lead 0.000 1 0.000 0.000 0.000 0.186 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.186 Mercury 0.000 0.000 0.000 0.000- 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.000 0.000 0.000 0.000 0.162 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.162 denum Nickel 0.000 0.000 0.000 0.000 1 0.252 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.252 Selenium 0.000 1 0.000 0.000 0.000 0.030 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.030 Zinc 0.000 0.000 0.000 0.000 4.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.026 Total Phos- 0.000 0.000 0.000 0.000 81.600 0.000 0.000 0.000 0.000 0.000 0.000 0.000 81.600 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 2 Acres Utilized: 17 Land Owner: Leland Wolfe Annual Dry Tons Applied: 65.1210 Site #: NC-UN27 Acres Permitted: 17.0 Operator: Same Predominant Soil Series: GsB-Golston Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 135 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 ° y o Q Volume applied PP enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Preci P• past 24 Hrs. inches Y 4-0 o' 0 w o o C o � - . * �' M w K F * N ?; TKN mg/kg Z Y o �; w' mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type P YP Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 July 15 175 19.1 1.656 WWTPC D 0 S 0.5 0.3 33,100 3,660 11.5 35.348 NA Fescue July 15 50 19.84 0.491 WTPC D 0 S 0.5 0.4 24,100 2,720 2 9.744 NA Fescue Aug 15 100 19.1 0.946 WWTPC D 0 S 0.5 0.3 33,100 3,660 11.5 20.199 NA Fescue Aug 15 75 19.84 0.737 WTPC D 0 S 0.5 0.4 24,100 2,720 2 14.616 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ......... ....... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 4001 0 1::::::... As Cd Cu Cr Pb Hg Mo Ni Se Zn P 79.907 1 0.000 Lime Applied Annual lbs/acre 0.107 0.096 0.203 1 36 0.021 0.036 0.057 34 3.145 2.803 5.948 1338 1 1.020 0.977 1.997 X 0.212 0.237 0.449 267 0.005 0.003 0.008 15 0.267 0.186 0.453 X 0.287 0.311 - 0.598 374 0.038 0.038 0.076 -89 5.876 5.966 11.842 -2498 121.729 ::::::::::::::::::::::::::::: :: .::::::::::::::::::::::::::::::::::::::::::::::: : Date lbs/ac Prior Years Cumulative lbs/ac 4/15 2182 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop 135 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 xxx Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 65.11 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Leland Wolfe Owner: Same Predominant Soil Series: GsB-Golston Acres Used: 17 Acres Permitted: 17 Site #: NC-UN27 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use m2/kg, % Solids use Raw Percent #): 6MMV1,o Com- posite Date, © a EIi Total ' .� ; �� ��� Annual Heavy 1Vletal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 6 7 8 9 10 11 12 DT/Ac./ _5j o App. Event 2.60 1.23 14 Arsenic 0.000 0.000 0.000 0.000 0.000 0.068 1 0.039 0.000 0.000 0.000 0.000 0.000 0.107 Cadmium 0.000 0.000 0.000 0.000 0.000 0.016 0.005 0.000 0.000 0.000 0.000 0.000 0.021 Copper 0.000 0.000 0.000 0.000 0.000 1.988 1.157 0.000 0.000 0.000 0.000 0.000 3.145 Chromium 0.000 0.000 0.000 0.000 0.000 0.619 0.400 0.000 0.000 0.000 0.000 0.000 1.020 Lead 0.000 0.000 0.000 0.000 0.000 0.151 0.061 0.000 0.000 0.000 0.000 0.000 0.212 Mercury 0.000 0.000 0.000 0.000 0.000 0.003 0.002 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.000 0.000 0.000 0.000 0.000 0.161 0.106 0.000 0.000 0.000 0.000 0.000 0.267 denum Nickel 0.000 0.000 0.000 0.000 0.000 0:208 0.079 1 0.000 0.000 0.000 0.000 0.000 0.287 Selenium 0.000 0.000 0.000 0.000 0.000 0.026 0.012 0.000 0.000 0.000 0.000 0.000 0.038 Zinc 0.000 0.000 0.000 0.000 0.000 4.538 1.339 0.000 0.000 0.000 0.000 0.000 5.876 Total Phos- 0.000 0.000 0.000 0.000 0.000 94.713 27.016 0.000 0.000 0.000 0.000 0.000 121.729 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". J� a Signature of Land Applier .,)-i-4e, Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM . PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR -EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346. Field #: 3 Acres Utilized: 7.4 Land Owner: William Griffin Annual Dry Tons Applied: M.3142 Site #: NC-UN29 Acres Permitted: 7.4' Operator: •Same Predominant Soil -Series: BaB_Bitdini Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max.-PAN:.':'122. Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: - 50 ° + ° Q. Volume applied (enter one) Solids/ Liquid -Cu. Yds Gallons % Solids Volume Applied per PP. P , Acre (cry Tons/Ac) Residual Sources (NPDES #, W # Fert., Animal Waste, etc) Soil Cond. (DrS, . Wet;. Moist) Precip. Past 24 Hrs. inches Y . 4 '° cc. ,.r . o o w o %'� �' � - N o w i9. * N - TKN mg/kg Z Y o . �;._ o mg/kg' Nitrate and . Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual g. Application•- Crop 1 Crop 2 Crop 1 Crop 2 Apr 15 182 . 20.43 4.232 ,WWTPC D 0 - S - 0.5 .0.3. 42,600 .4,160 2 115.219 NA Fescue 0.000. _ 0.000 0.000 0.000' 0.000 0.000 0.000 0.000 . 0.000. 0.000 . .0.000 0.000 .0.000 0.000 0.000... . 0.000 -.0.000 . 0.000, 0.000 . 0.000 0.000- 0.000 0.000 0.000 0.000 0.000 0.000. 0.000, 0.000 0.000. 0.060 0.000 0.000 Residuals Applications totals -'on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 182 o ::::::::::: As Cd Cu Cr Pb H Mo . Ni Se- Zn P :. 115.219 .. uoo ' Lime Apolied Annual.lbs/acre . , 0.093 0.115 0.208 1 36 -0.025. .0.01 0.035 " 34 .°. 2.649 2.865 . 5.514 -1338 0.990 1.131 2.121 X '0.262 .0.141 0.403 267. 0.004 ; 0:002 .0.066. r5 0.178 0.21 0.388 X 0.364 •0.189 0.553 : 374 0.042 0.026- 0.068 89: 6.957 1:058 8.015 2498' .143.888::;:;:::::':::::::::::::`::::::;:;: .......................... ' Date lbs/ac Prior Years Cumulative.lbs/ac Current Cumulative lbs/ac Permitted-C. P. L:.R.**** Permit N PA Limit lst/2nd Crop P 22 1 50 "I certify, under, penalty of law, that this document'was preparedunder my direction or supervision in accordance with a system designed to'assure that qualified personnel properly gathered and.evaluated the information submitted..I am .aware 4hat there are significant penalties for submitting false information, including the possibility of fines and imprisonment.for.knowing violations. *Application Methodi S - Surface; IN - Injection,'INC.- Incorporation **Volatilization Rate: Surface : 0.5, Injection/Incorporation - 1.0 Signature of Land Applier. Date Mineralization. Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM- FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: William Griffin Owner: Same Predominant Soil Series: Acres Used: 7.4 Acres Permitted: 7.4 Site #: NC-UN29 Field #: 31.32 NIA BaB-Badin 3 Residual Analvsis Data (Heave Metals and Total Phosuhorus use mg/kg. % Solids use Raw Percent #): Com- posite Date Total Phos- _;�hor'USEEMEEEEEEEEE Annual tieaw lvletal Vield Loadings (Ualculated in lbs/acre): Total 1 �2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ o App. Event 4.23 y Arsenic 1 0.000 0.000 0.093 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.093 Cadmium 0.000 0.000 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Copper 0.000 0.000 2.649 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.649 Chromium 0.000 0.000 0.990 0.000 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.990 Lead 0.000 0.000 0.262 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.262 Mercury 0.000 0.000 0.004 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.000 0.000 0.178 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.178 denum Nickel 0.000 0.000 0.364 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.364 Selenium 0.000 .0.000 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 Zinc 0.000 0.000 6.957 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.957 Total Phos- 0.000 0.000 143.888 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 143.888 horus i certuy, under penaity of ►aw, inat tms document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier C Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 4 Acres Utilized: 7.2 Land Owner: William Griffin Annual Dry Tons Applied: 22.1129 Site #: NC-UN29 Acres Permitted: 7.2 Operator: Same Predominant Soil Series: BM-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 ° +� o y o A Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume A lied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (D�. Wet, Moist) Precip. Past 24 Hrs. inches Y ° b o o w cu 0 7y w ., TKN' mg/kg Z Y 0Q o C' � w• mg/kg Nitrate and Nitrite mg/kg PAN Applied lbs/acre ) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 15 154 17.05 3.071 WWTP cake D 0 S 0.5 0.3 37,900 4,870 2 75.835 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 154 0 ::;:;:;:;:;:;: AS Cd Cu Cr Pb H Mo Ni Se Zn P 75.835 0.000 Lime Applied Annuallbs/acre 0.086 0.078 0.164 36 0.012 0.007 0.019 34 2.002 1.928 3.930 1 1338 0.774 0.761 1.535 1 X 0.190 0.095 0.285 1 267 0.002 0.001 0.003 1 15 0.166 0.141 0.307 1 X 0.258 0.127 0.385 374 1 0.031 0.018 0.049 89 1 4.121 0.712 4.833 2498 83.531 :: ::: :: :: Date lbs/ac Prior Years Cumulative lbs/ac April 2080 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop122 50 "I certify; under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �s *Application Method: S - Surface, IN - Injection, INC_- Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, 'raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: William Griffin Owner: Same Predominant Soil Series: Acres Used: 7.2 Acres Permitted: 7.2 Site #: NC-UN29 Field #: 22.11 N/A BdB2-Badin 4 Residual Analvsis Data (Heavv Metals and Total Phosphorus use mg/kg. % Solids use Raw Percent #): Com- posite Date Total ' o '' .�� annual neavv ivletal rleia Loactinas (ualcutatea in ins/acre): Total 1 2 3 4 5 6 7j 8 9J 10 11 12 DT/Ac./ c App. Event 3.07 Arsenic 0.000 0.000 0.000 0.000 0.086 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.086 Cadmium 0.000 0.000 0.000 0.000 0.012 0.000 0.000 0.000 0.000 0.000-1 0.000 0.000 0.012 Copper 0.000 0.000 0.000 0.000 2.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.002 Chromium 0.000 0.000 0.000 0.000 0.774 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.774 Lead 0.000 0.000 0.000 0.000 0.190 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.190 Mercury 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.000 0.000 0.000 0.000 0.166 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.166 denum Nickel 0.000 0.000 0.000 0.000 0.258 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.258 Selenium 0.000 0.000 0.000 0.000 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.031 Zinc 0.000 0.000 0.000 0.000 4.121 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 4.121 Total Phos- 0.000 0.000 0.000 0.000 83.531 0.000 0.000 0.000 0.000 0.000 0.000 0.000 83.531 horus ' i certify, unaer penalty of law, tnat this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier C> -/-I Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 13.1 Land Owner: Tom Appenzeller Annual Dry Tons Applied: 42.2156 Site M UN-UN30 Acres Permitted: 13.1 Operator: William Griffin Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Cron 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 .� ,4 A Volume applied (enter one) Solids/ Liquid Q Cu. Yds Gallons ova Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES ##, WQ#, Fert. Animal Waste, etc) Soil Cond. D (Dry, e ' Moist) Precip. Past 24 Hrs. inches Y 4 'b a 'b o o o o w R ° * w 7y P -+ * # TKN mg/kg Z Y cr El o c °Q w• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 15 294 17.05 3.223 WWTP cake D 0 S 0.5 0.3 37,900 4,870 2 79.572 NA Fescue 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1,0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 294 0 ::;::::':::;::: As Cd Cu Cr Pb H Mo Ni_ Se Zn. P 79.572 0.000 Lime A lied Annual lbs/acre 0.090 0.013 2.101 0.812 0.200 0.003 0.174 0.271 0.032 4.325 87.666:::::::::::::::::::::::::::::'.:::::: ................._. .. :. Date lbs/ac . Prior Years Cumulative lbs/ac 0.192 0.03 4.737 1.787 0.391 0.005 0.385 0.539 0.057 9.287 April 2080 Current Cumulative lbs/ac 0.282 0.043 6.838 2.599 0.591 0.008 0.559 0.810 0.089 13.612 Permitted C.P. L. R.**** 36 34 1 1338 1 X 267 15 X 374 1 89 1 2498 i it 1 st/2n d Crop Permit PAN L m 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date x** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Tom Appenzeller Owner: William Griffin Predominant Soil Series: Acres Used: 13.1 Acres Permitted: 13.1 Site #: NC-UN30 Field #: 42.22 N/A BdB2-Badin Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 j 3 _jr 5j 4/27/15 6 7 8 9 10 11 j 12 % Solids 17.05 Arsenic 14 Cadmium 2 Copper 326 Chromium 126 Lead 31 Mercury 0.4 Molyb- denum 27 Nickel 42 Selenium 5 Zinc 671 Total Phos- horus 13600 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 2 3 4 5 3.22 6 7 8 9 10 11 12 .y ° 14 Arsenic 0.000 1 0.000 0.000 0.000 1 0.090 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.090 Cadmium 0.000 0.000 0.000 0.000 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Copper 0.000 0.000 0.000 0.000 2.101 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.101 Chromium 0.000 0.000 0.000 0.000 0.812 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.812 Lead 0.000 0.000 0.000 0.000 0.200 0.000 0.000 0.000 0.060 0.000 0.000 0.000 0.200 Mercury 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0'.000 0.000 0.000 1 0.000 0.000 0.003 Molyb- denum 0.000 0.000 0.000 0.000 0.174 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.174 Nickel 0.000 0.000 -0.000 0.000 0.271 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.271 Selenium 0.000 1 0.000 0.000 0.000 0.032 0:000 0.000 0.000 0.000 0.000 0.000 0..000 0.032 Zinc 0.000 1 0.000 0.000 0.000 1 4.325 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.325 Total Phos- horus 0.000 0.000 0.000 0.000 87.666 0.000 0.000 0.000 0.000 0.000 0.000 0.000 87.666 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". <Z i �; � ; 5 ��- 1r,14 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 4 Acres Utilized: 15.2 Land Owner: Tom Appenzeller Annual Dry Tons Applied: 43.3758 Site #: NC-UN30 Acres Permitted: 15.2 Operator: Same Predominant Soil Series: BaB-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: ' 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 S. O 'S >~ A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D (ry' Moist) Precip. Past 24 Hrs. inches Y 410 co b �• o0 w, * o o _ * w' 7y w -+ * N' TKN mg/kg X Y -- S o c ao w mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 April 15 182 20.43 2.060 WWTP cake D 0 S 0.5 0.3 42,600 4,160 2 56.094 NA Fescue May 15 84 17.05 0.794 WWTP cake D 0 S 0.5 0.3 37,900 4,870 2 19.594 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 2661 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 75.687 0.000 Lime Applied Annual lbs/acre 0.068 0.016 1.807 0.682 0.177 0.003 0.129 0.244 0.029 4.452 91.637::.::::::::::::::::::::::::::::::::: .................. :::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.132 0.02 3.226 1.228 0.262 0.004 0.265 0.358 0.038 6.049 April 2080 Current Cumulative lbs/ac 0.200 1 0.036 5.033 1.910 0.439 0.007 0.394 0.602 0.067 10.501 Permitted C. P. L. R.****1 36 34 1 1338 1 X 1 267 1 15 1 X 374 1 89 2498 Permit PAN Limit 1 s tl2nd Crop 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ' *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Tom Appenzeller Owner: Same Predominant Soil Series: Acres Used: 15.2 Acres Permitted: 15.2 Site #: NC-UN30 Field #: 43.38 N/A BaB-Badin Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Com- posite Date 0 ro •' t �_©_©_______ Total Phos- M M Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ ,oy, App. Event 2.06 0.79 Arsenic 0.000 0.000 0.045 0.000 1 0.022 0.000 0.000 1 0.000 0.000 0.000 0.000 1 0.000 0.068 Cadmium 0.000 0.000 0.012 0.000 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Copper 0.000 0.000 1.290 0.000 0.518 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.807 Chromium 0.000 0.000 0.482 0.000 0.200 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.682 Lead 0.000 0.000 0.128 0.000 1 0.049 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.177 Mercury 0.000 0.000 0.002 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.000 0.000 0.087 0.000 0.043 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.129 denum Nickel 0.000 0.000 0.177 0.000 0.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.244 Selenium 0.000 0.000 0.021 0.000 1 0.008 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.029 Zinc 0.000 0.000 3.387 0.600 1 1.066 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 4.452 Total Phos- 0.000 0.000 70.040 0.000 21.597 0.000 0.000 0.000' 0.000 0.000 0.000 0.000 91.637 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier -If'/4 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 5 Acres Utilized: 10.8 Land Owner: Tom Appenzeller Annual Dry Tons Applied: 31.3142 Site #: NC-UN30 Acres Permitted: 10.8 Operator: Same Predominant Soil Series: BaB-Badin - Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 '- o ' +' Q9 Volume applied pp enter one Solids/ ( ) Liquid Cu. Yds Gallons u /o Solids Volume Applied per PP P Acre (Dry Tons/AC) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist) Preci . p Past 24 Hrs. inches Y b 'b o w a �. * 0 o En w CD �' * w $ 70 0 w C, .* w * N' w TKN mg/kg z 3 o 0 as o � w' mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 April 15 - 182 20.43 2.899 WWTP cake D 0 S 0.5 0.3 42,600 4,160 2 78.947 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000, 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... . ......... TOTALS: 182 0 :::::::::::::: As Cd Cu Cr Pb Hg Mo I Ni Se Zn I P 78.947 0.000 Lime A _ lied Annuallbs/acre 0.064 0.017 1.815 0.678 0.180 0.003 0.122 0.249 0.029 4.766 98.566 :::::::::::::::::::::::::::: :. :: Date lbs/ac Prior Years Cumulative lbs/ac 0.132 0.02 3.243 1.234 0.264 0.004 0.267 0.36 0.039 6.082 April 2080 Current Cumulative lbs/ac 0.196 0.037 5.058 1.912 0.444 0.007 0.389 0.609 0.068 10.848 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X = 89 2498 Permit PAN Limit 1st/2n d Crop 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Monroe WQ0001346 Tom Appenzeller Owner: 10.8 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Same Predominant Soil Series: 10.8 Site #: NC-UN30 Field #: 31.31 N/A BaB-Badin 5 Residual Analvsis Data (Heave Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): N"ImMIN Com- posite Date Non Total Phos- phorus Annual Heave Metal Meld Loadings Walculated in lbs/acre): Total 1 2 3 4 5 6 7 8 ` 9 10 11 12 H DT/Ac./ 0 APP• Event 2.90 Arsenic 0.000 0.000 0.064 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.064 Cadmium 0.000 0.000 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 Copper 0.000 0.000 1.815 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.815 Chromium 0.000 0.000 0.678 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.678 Lead 0.000 0.000 0.180 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.180 Mercury 0.000 0.000- 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.000 0.000 0.122 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.006 0.000 0.122 denum Nickel 0.000 1 0.000 0.249 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.249 Selenium 0.000 0.000 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Zinc 0.000 0.000 4.766 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.766 Total 1 Phos- 0.000 .0.000 98.566 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 98.566 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ' Signature of Land Applier Date DENR FORM MFLSF (12/2006) Volatile Solids Reduction 2015 1st 60 days IN OUT 0.7018 0.5883 0.1135 Reduction IN- (IN -OUT) 1 39.28% 0.7018 0.412869 0.288931 2nd 60 days IN OUT 0.7264 0.5800 0.1464 lReduction IN- (IN -OUT) 1 47.99% 0.7264 0.421312 0.305088 3rd 60 days IN OUT 0.8940 0.5679 0.3261 lReduction IN- (IN -OUT) 1 84.42% 0.894 0.507703 0.386297 4th 60 days IN OUT 0.7156 0.5512 0.1644 lReduction IN- (IN -OUT) 51.19% 0.7156 0.394439 0.321161 5th 60 days IN OUT 0.8292 0.5106 0.3186 Reduction IN- (IN -OUT) 1 78.51% 0.8292 0.42339 0.40581 6th 60 days IN OUT 0.6898 0.5270 0.1628 Reduction IN- (IN -OUT) 49.90% 0.6898 0.363525 0.326275 PRE] MPT•ACCU RATE -RE LIABLE I,AB0P_4_'Y0alES, INC WWWPARLABS.COM REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: JAN 15 PO BOX 69 DATE: 02/05/15 MONROE, NC 28111- SAMPLE NUMBER- 117271 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- SO DATE SAMPLED- 01/08/15 TIME SAMPLED- 1020 DATE RECEIVED- 01/08/15 SAMPLER- SH RECEIVED BY- CT TIME RECEIVED- 1116 DELIVERED BY- SH TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM_ MEAN) SM 9221 E 01/09/15 1000 RE 16,075 MPN/g LABORATORY DIRECTOR P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 i'.��t(utt"f.-•j{CI:`�fi+1�SKc:',��P�f,?l=:; kFZ A& p )� PROM RT•ACCURATE •Rf il-IASL-F. L,ABC7 t-A,-U(DRIES, 11%JC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 ..__ • CITY OF MONROE MONROE WWTP 01/08/15 FECAL COLIFORM, GEOMETRIC MEAN SM 9221 E 117271 117271 1 2,057 15.44% 13,325.54 2 2,163 13.91% 15,550.79 3 2,149 12.66% 16, 977.31 4 2,401 13.62% 17,631.11 5 2,569 13.58% 18,925.65 6 2,042 13.47% 15,164.20 7 2,114 13.56% 15,583.74 16,075 r CHAIN OF CUSTODY :A50R.aT0ME5.INC. PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 www.parfabs.com Shippi'ic: Mailing_ 7-217 Graham Park Drive PO Box 411483 Charlorze, NC 28273 Chariot -Le, NC 28247-1483 fs essential irat a(I information be recorded on this Chain of CustodY document for acceptance by PAR Laboratories. Inc. and the North Carolina Department o`. Environmental and Naturai Resources. Conpany Marne (billing) I lions Address City of Monroe PO Box 69 City. State & zip code Monroe; N 28111 Point of Contact ( Steve Holden ( 704) 282-4679 sholden@monroenc.or� SSample Taken By: Ul,j' C Comments! Special Instruc 503 BIOSOLIDS REPORTING IS THIS FOR STATE or EPA REPORTING? YES JL— NO *Sample type: DW __ WW )C GWMW _ HW Soil other Sample Temp at time of samprng_ oC Sample Temp upon receipt: _ °C Preserved: Yes _ No X Teflon Liner/ Zero Headspace: Yes No N/A X Client Sample I.D. ( Sample Location I N=ber) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested X NONE -0' /S� Z� _ FECAL COLIFORM # 2 WWTP X NONE FECAL COLIFORM 3 WvvTP X NONE L FECAL COLIFORM 4 4 WWTP' - X NONE ; Z6 FECAL, COLIFORM " 5 WWTP X NONE FECAL COLIFORM 6 WV TP X NONE FECAL COLIFORM Y i WWTP X.NONE �� v ; 2-Q FECAL COLIFORM nqu� h d by.A Date/Time Received�y� Date/Time r nquished by: Daterrime Received by: DatefTime =Co-iposTe G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HIV=Hazardous Waste See Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WWTP Name: WWTP cake WQ Permit Number: WQ0001346 NPDES Number: NCO024333 Monitoring Period: From 1/1/2015 To 2/28/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) [3 Alt. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density Rl Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion Z Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Sludge g Pathogen Density Number of Excee- de ces Frequency of Analysis y Sample Type Analyticar Tech- ni ue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 13,325.54 16,075 18,925.65 MPN/g 0 bimonthly grab SM9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ] Alt. 2 (40-day bench) ❑ jAlt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ jAlt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: Monroe WWTP cake NPDES Number: NCO024333 Monitoring Period: From 1/1/2015 To 2/28/2015 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Altemative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 111 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Altemative 1 0 Alternative 2 ❑ ............................. If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ jAerobic Digestion t] Anaerobic Digestion ❑ . .. ..:_: .: If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- dences Frequency of Analysis Sample Type Analytical Tech - Waue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 13,325.54 16,075 18,925.65 MGN/g 0 bimonthly grab SM9221 E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ 1 Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) El Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) `'❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) — # /kk- a�� A4�- Signature of Preparer* Date tgnature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) py: k PROM PT•ACCLI RATE -RELIABLE I_,ABORAT®RIES, INC WW W.PARLABS.COM REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: MAR 15 PO BOX 69 DATE: 03/13/15 MONROE, NC 28111- SAMPLE NUMBER- 118023 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW DATE SAMPLED- 03/09/15 TIME SAMPLED- 0940 DATE RECEIVED- 03/09/15 SAMPLER- SH RECEIVED BY- DJ TIME RECEIVED- 1058 DELIVERED BY- SH TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 03/09/15 1120 RE 18,178 MPN/g LABORATORY DIRECTOR P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 PROMA PT•ACCLf RATE- RELIABLE L.ABOR-A rC3RIES, ING 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CITY OF MONROE MONROE WWTP ' 03/09/15 FECAL COLIFORM, GEOMETRIC MEAN • 313233ulv 9221 E 118023 Fecal Coliform metric Mean= 1 2,512 13.00% 19,323.67 2 2,475 12.64% 19,582.65 3 2,352 13.12% 17,924.63 4 2,252 12.88% 17,484.36 5 2,199 13.23% 16,617.88 6 2,460 13.47% 18,262.99 7 2,366 12.98% 18,226.07 �. CHAfN OF CUSTODY iASORA70MES.RvC PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 www.parfabs"com SFippinc: Mailing: 2217 Graham Park Drive PO Box 411453 Crarlo<<e, NC 28273 Charlotte, NC 28247-1483 is e;sentlal Thai all inrormation be recorded on this Chain of Custody document for acceptance by i AR Laboratories_ Inc. and the North Carolina Deoarin+eni of E—ironmer+;al and Naruml Resources_ Company Name (bining) City of Monroe Comments/ Special Instructions ,— Address PO Box 69 City. State & zip code Monroe. NC 28111 t of !ct & Telephone Steve Holden ( 704) 282-4679 sholden@monroenc.or Sample Taken By: 503 B10SOLIDS REPORTING IS THIS FOR STATE or EPA REPORTING? YES._X, NO *Sample type: DW WW T GWMW _ HW Soil other Sample Temp at time of sampling: 'C Sample Temp upon receipt: °C Preserved_ Yes _ No Teflon Liner/ Zero Headspace: Yes No N/A X Client Sample I.D. Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested 4 1 WVVTp X NONE 3- _ 1S q- vv _ FECAL COLIFORM # 2 WWTP X NONE FECAL COLIFORM # 3 WWTP X NONE 3.9 _ !S" � , v FECAL COLIFORM n 4 WWTP, - X NONE s. i _!� �v FECAL, COLIFORM # 5 WWTP X NONE 3, . YL3 FECAL COLIFORM N 6 WWTP X NONE 3.9 ,! S "yV FECAL COLIFORM n 7 Wvfi P X NONE p "!s �'Yd FECAL COLIFORM by: Datefrime Receive b DateTme relinquished b, : DaterFime Received by: Datef"l-ime C=Composite G=Crab DVV=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HI.V=Hazardous Waste See Cher Side A1N1N UAL.PA'I'HOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WWTP Name: WWTP cake NPDES Number: WQ0001346 NCO024333 Monitoring Period: From 3/1/2015 To 4/30/2015 Alt.1 (VS reduction)❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) LJ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ A ' T,'"TYMIT. 1 ♦ m-- .. Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CI %_,1z,1% 1111 lt.1111 lvi,4 3l,%1 Emmiv 1 kpiease check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Preparer Name and Title (type or print) 141 SigAature of Preparer* Date Steve Holden, Residual Coordinator Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF n2T ti9i9nnm ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WWTP Name: Monroe WWTP cake Monitoring Period: From 3/1/2015 To WQ Permit Number: NPDES Number: 4/30/2015 WQ0001346 NCO024333 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ . Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ .......... Class B: Alternative 1 0 Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ jAerobic Digestion 0 Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- dences Frequency of Analysis Sample Type Analytical Tech - waue Minimum Geo. Mean Maxim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 16,617.88 18,178 19,582.65 MGN/g 0 bimonthly grab SM9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) R1 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) AWL PROMPT• ACr•URATE "RELIABLE LABOP,ATORIES, INC WWW.RARLABS.COM REPORT OF ANALYSES t';VE HOLL'•;_';1\; Wi%S, _ EWA--ERPLANT PROJECT NAME: APR- 15 DATE: 0 5/ 1 8/ 1 5 v",\?'i NC' S.ti1viP11,E NUMBER- 118602 SAMPLE ID- MONROE WWTP SAMPLE MATRiX 101 - ? SAMPLED- 04/27/15 TIME SAMPLED- IOC(, DA"? RECEIVED- 04/27/15 SAMPLER- SH RECEIVED BY- DJ _..� .. C7IVED- 1 100' DELIVERED BY- SH TYPE SAi/P�E- __ ... ANALYSIS i'•.��!'.�'.'.r _5 METHOD DATE TIME BY RESULT UNI^S FE"A: _.."•1FORN' i'C•EON;. MEAN) SM 9221 E 04/27/15 1445 RE 9,759 ,✓PN/q LABORATORY DIRECTOR P.U. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) S88-8333 • Fax: (704) 588.833S R AM A 11- r'RC3Mr'T-ACCUf,'A'rr-- RCLIAM-C L,/%,B4OIz?-A'r0RIESy INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CITY OF MONROE • MONROE WWTP 04/2 7/15 FECAL COLIFORM, GEOMETRIC MEAN SM 9221 E �L= 211i 118602 Fecal Coliform Geometric Mean = Sample # 1 F. Colliform 1.877 T, Solids 17.09% 10.978.69 2 1,493 16.56% 9,015.10 3 1,411 15.99% 8.823.94 4 1.554 16.22% 9,579.46 5 1,854 16.48% 11,248.68 6 1,594 16.60% 9,603-02 7 1.529 16,39% 9,321.39 CHAIN OF CUSTODY L.J r%A-,OXEPAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 wwef.parfabs.com S 41iCvF1C, Mailinn: 7-21 7 Graham Park Drive PO Box 41 1433 NC 23273 Charlotte, NC 28241-1483 " s _,senciai o-.ai ei irsorma5an be recorded an this Chain v' Custody document for acceptance by PAR Laboraiories. Inc, and the Nirrv, .-e�oiina 0-marlmeni o: Gnvirom+ten;al and:. `slum) HLspureei. ------ C.; ^.yny Name lbinincl - Comments/ Special Instf Uciions C i tv of Monroe - AddreSs PO Box 69 _ 503 BIOSOLIDS City. State a zip code I REPORTING Monroe, NC 28111 /pint of Contact & Telephone Sieve Holden (704) 282-4679 sholden@nionroenc.org 1 Sample Taken By: S i�L) Id E� IS THIS FOR STATE or EPA REPO TING? YES NO `Sample type: DW WW -X GWMW _ HW _ soil _ other Sample Temp at time of sampling: 'C Sample Temp upon receipt: `G Preserved: Yes _ No X Teflon Liner/ Zero Headspace: Yes _ No __ NIA Client Sample I.G. ( Sample Location! Number) Comp Grab Preserv. Set Up j Date 1 Time Collection I Date / Time Analyes Requested i "I1 wwTP X NONE ,�_Z�_ is /d: �o FECAL COLIFORM d 2 WwrP X NONE ©, v0 FECAL COLIFORM „3 X NONE -L7-jS ;v I FECAL COLIFORM wWIP x NONE -L7-/ 0: J j FECAL, COLIFORM -- 5 WwTP X NONE y"Z7-j FECAL COLIFORM - -- - 6 W WTP X NONE ; vv FECAL COLIFORM v✓7 P X NONE : FECAL COLIFORM -- '<ernquished by. Date/Time J Rece�EiV by: Datefriimc / ;e1ir. ,uished by: Daterrirpe Received by: 11'Date(rme C-c-PosRe G =Grab DW=1)`nking Water WW =Wastewaier GWMW=Groundwater Monitoring Well H`.V=Hazardous waste See 0-her Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: WWTP cake NPDES Number: NCO024333 Monitoring Period: From 5/1/2015 To 6/30/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ElAlt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Theirnophilic ❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ . .. . Class B: jAlt. (1) Fecal Density CI Alt. (2) Process to Significantly Reduce Pathogens ❑ ............ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion Q Anaerobic Digestion ❑ , .: If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- dences Frequency of Analysis Sample Type na ytica Tech - Waue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 8,823.94 9,759 11,248.68 MPN/g 0 bimonthl Grab SM9221E CFU 1000 mpn per gram of total solid (dry weight Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) p Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ElAlt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) El Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) El Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Rl "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) — /0/,V— , A4n--- C P - �-//, Si ature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: Monroe WWTP cake NPDES Number: NCO024333 Monitoring Period: From 5/1/2015 To 6/30/2015 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alterative 3 ❑ Alternative 4 ❑ Alterative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Therrnophilic ❑ > :. Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ . ...>. . . ``... ` `. Class B: Alternative 121 Altemative 2 ❑ ............................................... If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Ai Drying❑ Composting ❑ jAerobic Digestion 0 Anaerobic Digestion El.. . .. . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- dences Frequency of Analysis Sample Type Analytical Tech - nioue Minimum Geo. Mean Maxim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 8,823.94 9,759 11,248.68 MGN/g 0 bimonthly grab SM9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) Rl Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ARL PROM PT- AC URATE•RE: LIABLE I,ABOF-AT®IZIES, INC. WWW.PARLABS.COM REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: JUL 15 PO BOX 69 DATE: 07/15/15 MONROE, NC 28111- SAMPLE NUMBER- 119613 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW DATE SAMPLED- 07/08/15 TIME SAMPLED- 0930 DATE RECEIVED- 07/08/15 SAMPLER- SH RECEIVED BY- DJ TIME RECEIVED- 1030 DELIVERED BY- SH TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 07/08/15 1600 RE 22,107 MPN/g LABORATORY DIRECTOR _t. — P.O. Box 411483 • Charlotte, NC 28241-1483 u Phone: (704) 588-8333 • Fax: (704) 588-8335 Am F;Z PROM PT•ACCU RATE- RELIABLE LABOPLATORIES, INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CITY OF MONROE ' MONROE WWTP ' 42193 FECAL COLIFORM, GEOMETRIC MEAN LZ • SM 9221 E 119613 1 3,965 19.45% 20,386.37 2 5,146 19.52% 26, 360.26 3 4,157 19.65% 21,158.29 4 4,219 18.98% 22,230.82 5 4,901 19.37% 25,303.62 6 3,879 1 19.48% 19,913.00 7 3,985 19.67% 20,259.41 Fecal Coliform ' 'eometric Mean 1 CHAIN OF CUS iTOD Y lASOR.a%oMFS,INC. PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 www.partabs.com Shippinc: Mailing: 2217 Graham Park Drive PO Box 411433 Charlo —ze. NC 28273 Charlotte, NC 28241-1483 ;z essenVal that all information be recorded on this Chain of Custody document :or acceptance by PAN Laboratories_ Inc. and the North Cerolina Deoartrner l o: Environmental and `taturel Resources_ Company Name (billing) irUCtlOns i Address City. State & zip code Point of City of Monroe PO Box 69 Monroe_ N C 28111 Steve Holden ( 704) 282-4679 sholden@monroenc.or ommen— pecra ns _ 503 BTOSOLIDS REPORTING Sample Taken BY: ppdlale'j IS THIS FOR STATE or EPA REPORTING? YES, NO *Sample type: DW WW Y GWMW _ HW _ Soil other Sample Temp at time of sampling: eC Sample Temp upon receipt: / 7 °C Preserved: Yes _ No X Teflon Liner/ Zero Headspace: Yes No N/A Client Sample D. ( Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested X NONE �_ S (�. 3 J FECAL COLIFORM r 2 WWTP X NONE i5' J FECAL COLIFORM 3 WVJTP X NONE 7_ J FECAL COLIFORM 4 4 WWTP ' - X NONE , Is. ; 3v FECAL. COLIFORM 5 W-WTP X NONE _ f,, �S Q �v FECAL COLIFORM f? 6 W W-f P X NONE _ _ g . 3� -'' FECAL COLIFORM m 7 wIWTP X NONE ,7,_ �� 3v FECAL COLIFORM —, ll- uc P ?elinquished by: Datelrime ReceivqdtiY- b DateMme \ AW relinquished b•: DaterT•i a Received by: DateMirne C=Ccnrposre G=Crab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well H'.V=Hazardovs Waste See 0-her Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WWTP Name: WWTP cake NPDES Number: Monitoring Period: From 7/1/2015 To 8/31/2015 WQ0001346 NCO024333 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)[] A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ =Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Aplt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion 0 n A aerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge in Pathogen Density Number ot Excee- dences Frequency of Analysis y Sample Type ytjca Tech - ni ue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 19,913.00 22,107 26,360.26 MGN/g 0 bimonthly grab SM9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) r❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ 1 Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Rl "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Preparer Name and Title (type or print) Signature of Preparer* Date Steve Holden, Residual Coordinator Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WWTP Name: Monroe WWTP cake WQ Permit Number: WQ0001346 NPDES Number: NCO024333 Monitoring Period: From 7/1/2015 To 8/31/2015 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ElAlternative 2 ❑ Alternative 3 ❑ Alterative 4 ❑ Alterative 5 ❑ Alterative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 0 Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Dige ' soon If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Num er o Excee- de es Frequency of Analysis Sample Type Analytical Tech - Minimurr Geo. Mean Maximurr Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 19,913.00 22,107 26,360.26 MGN/g 0 bimonthly grab SM9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) R1 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Rl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) P AAKR PROM PT- A C,CU RATE• RE L I A R LE LABOIZATORIES, INC W W W.PARLABS.COM REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: AUG 15 PO BOX 69 DATE: 08/31/15 MONROE, NC 28111- SAMPLE NUMBER- 120251 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW LATE SAMPY ED- 08/26/15 TIME SAMPLED- 0700 DATE RECEIVED- 08/26/15 SAMPLER- SH RECEIVED BY- DJ TIME RECEIVED- 0915 DELIVERED BY- SH TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 08/26/15 RE 10,703 MPN/g 1 LABORATORY DIRECTOR P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 AM pyr"':. PROM PT•ACOU RATE REL.IASL-E LAJ30P AT'©RIES, INTC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20, SC Cert # 99003001 CITY OF MONROE ` MONROE WWTP ` 42242 FECAL COLIFORM, GEOMETRIC MEAN • SM 9221 E 120251 1 2,248 18.81 % 11,952.15 2 1,708 19.00% 8,988.24 3 1,954 18.73% 10,431.86 4 1,812 19.03% 9,519.68 5 2,243 18.69% 12,001.58 6 2,079 18.44% 11,272.07 7 2,094 18.78% 11,148.66 Lrfecal oliform ic IVlean= 1 1 u CHAIN OF CUSTODY i�� LA50RAToRrES,,Nc. PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 www.parfabs.com Shippinc: Mailing: 2217 Graham Park Drive PO Box 411483 Charlo<<e, NC 78273 Charlotte, NC 28241-1483 I s essenral that all informa5cn be recorded on :his Chain of Custody docUnentfor acceotance by PAR Laboratories. Inc. and the North Carolina 0coarimeni o' Envimo meal and Natural Resources. Conpany Name (billing) City ofMonroe Comments/ Special Instructions Address PO Box 69 Cit`!. State & zip code Monr-oe. -,'\-)C- zsl I I Of Contact & Teiaphone Steve holden { 704) 282-4679 sholden@nlonroenc.ort� Sample Taken By: of "lif0 503 BTOSOLIDS REPORTING IS THIS FOR STATE or EPA REPORTING? YES ._, NO *Sample type: DW WW X GWMW _ HW Soil other Sample Temp at time of sa��mrrpring: OC Sample Temp upon receipt: _ O-� ,A, C,,rr ** Preserved: Yes _ No Teflon Liner/ Zero Headspace: Yes No NIA cA Client Sample I.D. ( Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested # I WWTP X NONE 4—�S' ,7:Uv _ FECAL COLIFORM # 2 WWTP X NONE ' ZG—�s 40 L) FECAL COLIFORM 3 Wvv 1 P X NONE 2G- ? J FECAL COLIFORM 4 4 WWTp - X NONE _ 2 , v0 FECAL COLIFORM # 5 WW I P X NONE �, _! ? , v v FECAL COLIFORM 6 WWTP X NONE ev FECAL COLIFORM n / WWTP X NONE 24 �/ FECAL COLIFORM I relinquished by: d relinquished by: Date/rime 9j Date(T'ime Received by: Date/Tme Date/Tme C. Cc-iposite G=Grab DW=D:-inking Water WW=Wastewater GWMW=Groundwater Monitoring Well H'.V=Hazardous Waste See G:her Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WWTP Name: WWTP cake NPDES Number: WQ0001346 NCO024333 Monitoring Period: From 9/1/2015 To 10/31/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) El Alt. C (Prior Testing)[] A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ = Thermophilic ❑ Beta Ray ❑ Gamma ❑ Ray Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": - Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion r❑ Anaerobic Digestion ❑ . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level g I in Sludge Pathogen Density Number ot Excee- Frequency of Analysis Y Sample Type na ytica Tech- i inimu Geo. Mean aximu Unitsences 2 x 10 to the 6th power per gram of Fecal Coliform total solids MPN 1 8,988.24 1 10,703.00 112,001.58 1 MPN/g 1 0 t uuu mpn per gram of total solid (dry LImonella bacterial 3 MPN per 4 grams (in lieu of fecal total solid (dry Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: grab ISM9221 E Alt.l (VS reduction) Rl Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Rl "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Preparer Name and Title (type or print) Signature of Preparer* Date Steve Holden, Residual Coordinator Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WWTP Name: Monroe WWTP cake WQ Permit Number: WQ0001346 NPDES Number: NCO024333 Monitoring Period: From 9/1/2015 To 10/31/2015 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ y Gamma Ray ❑ Pasteurization ❑ . , , ......... .... .. ...:.... .... . Class B: Alternative 1 0 Alternative 2 [3 ............................................... If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ I Composting ❑ jAerobic Digestion Rl Anaerobic Digestion ❑ . .. . . .:: .. . .... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density um er o Excee- ences Frequency of Analysis Sample Type T Analytical Tech - MinimumGeo. Mean MaximumUnits Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 8,988.24 10,703 12,001.58 MGN/g 0 bimonthly grab SM9221 E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) El Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ 1 Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) p ANK )"' PROM PT -ACCURATE- RELIABLE LABORATORIES, IWC WWW.PARLABS.COM REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: OCT 15 PO BOX 69 DATE: 11/06/15 MONROE, NC 28111- SAMPLE NUMBER- 121138 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW DATE SAMPLED- 10/29/15 TIME SAMPLED- 0850 DATE RECEIVED- 10/29/15 SAMPLER- SH RECEIVED BY- DJ TIME RECEIVED- 0940 DELIVERED BY- SH TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 10/29/15 1300 RE 10,947 MPN/g LABORATORY DIRECTOR _'✓ ��.r �/ ✓�—�'` �a' P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 py k PROMPT•ACCU RATE• RELIAEiLE I.,ABOR.AT"ORMS, i1STC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CITY OF MONROE r MONROE WWTP 42306 FECAL COLIFORM, GEOMETRIC MEAN - SM 9221 E a ". 1 o a 1,150 e o 16.41% 0 121138 7,010.04 2 2,354 17.35% 13,568.03 3 1,887 16.70% 11,301.10 4 1,881 16.85% 11,165.02 5 1,737 16.56% 10,491.57 6 1,808 16.47% 10,977.81 7 2,320 17.02% 13,633.69 Fecal Coliform ¢.. Mea � • . �� CHAIN OF CUSTODY L 50a470MES,INC. PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 www.parfabs.com shippinc: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 t ;z essential that all information be recorded on ;his Chain of Custody document for acceptance by PAR Laboratories_ Inc. and the Nowt, Ceroli-a Department Of E—irvnm m;al and Naiural Resovrces. Ccnpany Name Ibirling) Comments/ Special Instructions City of Monroe Address City. State & zip code PO Box 69 Monroe. 'N C 28111 Point of Contact & Teicphone-, Steve Holden ( 704) 282-4679 sliolden@monroenc.org Sample Taken By: Steve Holden 503 BIOSOLTDS REPORTING iS THIS FOR STATE or EPA REPORTING? YE_S .—, , NO "Sample type: OW WW GWMW HW _ Soil other Sample Temp at time of sampling_ -C_ Sample Temp upon receipt: _ 0C Preserved: Yes _ No X Teflon Liner/ Zero Headspace: Yes No N/A Client Sample I.D. ( Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested # I WWTP x NONE I, �s + _ FECAL COLIFORM # 2 WWTP X NONE r J FECAL COLIFORM #3 WWTP X NONE FECAL COLIFORM WP ' - X NONE FECAL COLIFORM # 5 WWTP X NONE � FECAL COLIFORM # 6 WWTP X NONE �v_.LS►'!�� FECAL COLIFORM j #7 wwTp X NONE FECAL COLIFORM I ' 'eiinq by: Daterl"ime co* I' Received b DaterTme relinquished by: Daterrime Received by: ' Date/Time C=CcmpoSite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HIV=Hazardous Waste See 0-her Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WWTP Name: WWTP cake NPDES Number: WQ0001346 NCO024333 Monitoring Period: From 11/1/2015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ TAlt B (Alk Treatment)❑ Alt. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": �❑ Lime Stabilization ❑ Air Drying Composting ❑ jAerobic Digestion Z Anaerobic Digestion n .............................................................................................................. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Sludge g Pathogen Density Number o Excee- n Frequency of Analysis Y Sample Type Analytical Tech- nicue inim Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 7,010.04 10,947 13,633.69 MPN/g 0 :)i-monthli grab SM9221 E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) r❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ lAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify; under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WWTP Name: Monroe WWTP cake NPDES Number: WQ0001346 NCO024333 Monitoring Period: From 11/1/2015 To 12/31/2015 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ .................. Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: C s ltetnative 1 Alternative 2 ❑ A ❑ ............................. If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Ai Drying❑ Composting ❑ Aerobic Digestion Rl Anaerobic Digestion ❑ .... ..:...... . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number ot Excee- Frequency of Analysis Y Sample Typewaue Analytical Tech - Minim Geo. Mean axim Unitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 7,010.04 10,947 13,633.69 MGN/g 0 bimonthly grab SM9221 E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) Rl Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Prepar/err Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) Soil pH & Lime Application Records For all fields where pH was reported below a pH of 6.0 in accordance with NCDA&CS, fields will be limed prior to any land application in the year 2016. As part of the land application program, the City of Monroe will track these fields. Any field that remains below a pH of 6.0 will remain a priority to be limed as soon as possible. Any field that was below a pH of 6.0 was limed prior to any residual application during the year 2015. The City of Monroe applied 229.825 tons of lime during the year 2015. The fields that had lime applied are recorded on the field sheets. During the year of 2015 the City of Monroe also limed fields UN29-1 & 2 at a rate of 2,6401bs./acre which were not applied on during this, calendar year. These fields will be applied on during the calendar year of 2016. The lime amounts are recorded on field sheets. 0 Sodium Calcium Solids, Na, Na, Ca, Magnesium Date/ Sample decimal mg/kg mg/I Na, meq/L mg/kg Ca, mg/I Ca, meq/L Mg, mg/kg Mg, mg/I Mg, meq/L SAR 1-7-15 WWTP cake 0.1595 850 135.58 5.89 13400 2137.3 106.87 1840 293.48 24.06 0.73 3-3-15 WWTP cake 0.2043 649 132.59 5.76 11900 2431.17 121.56 1700 347.31 28.47 0.67 4-27-15 WWTP cake 0.1705 2110 359.76 15.64 11600 1977.8 98.89 1890 322.245 26.41 1.98 6-24-15 WWTP cake 0.191 1070 204.37 8.89 12500 2387.5 119.38 2470 471.77 38.67 1.00 8-25-15 WWTP cake 0.2247 842 189.2 8.23 14600 3280.62 164.03 21-10 474.117 38.86 .0.82 10-26-15 WWTP cake 0.1937 829 160.58 6.98 12000 2324.4 116.22 1790 346.723 28.42 0.82 F ' , ' 1• 'f WTP cake 530 11236 284 6964 177.444 454 0.750121-7-15 4-6-15 WTP cake 0.2467 567 139.88 6.08 5920 1460.46 73.02 1050 259.035 21.23 0.89 6-24-15 WTP cake 0.1984 643 127.57 5.55 7050 1398.72 69.94 1490 295.616 24.23 0.81 9-29-15 WTP cake 0.2369 782 185.26 8.05 3860 914.434 45.72 776 183.834 15.07 1.46 .i.^ .+ ,tr.., r...,, ., -.., a ., s ... 'J., >-:t ,. , ., i i - ,.a., r ._ri.,. 3- ir- .,;. ., . .,. 1, art t. . a :-i r? a l; fir. kr,. :• 4• •+1 3-_ !• Y a l-• ^ •Y_ >,y 4-6-15 WTP ferric 0.0536 533 28.569 1.24 2150 115.24 5.76 630 33.768 2.77 0.60 6-24-15 WTP ferric 0.0374 911 34.071 1.48 2640 98.736 4.94 710 26.554 2.18 0.79 9-29-15 WTP Ferric 0.0522 795 41.499 1.80 2960 154.512 7.73 735 38.367 3.14 0.77 Page 1 of 2 Report Number: 16-012-0752 Account Number:46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR' MONROE NC 28110 Date Received: 01/12/2016 e • NAlaypo ' �� 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Every acre... Everyyear. "Tm Grower: CALVIN MORRIS 554 HASTY ROAD PEACHLAND NC 28133 Farm ID: AN-19 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Analvsis: 01/13/2016 Date Of Report: 01/14/2016 OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number Rate Class Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meg1100g meq/100g 1-1 09993 2.4 80 265 VH 151 H 320 H 1507 M 7 VL 5.9 6.71 2.2 12.8 MIN NC I L NC = 221 NC = 77 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl AI Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 1-1 - 23 M 23.7 VH 30 H 299 VH 6.2 VH 1.0 M 0.19 VL NC; 3.0 20.8 58.9 0.2 17.2 NC=48 NC=592.5 NC=188 NC=310.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble ,analysis prepared by: WaypointAnalytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. 4 by. p/cc m� G4 Pauric McGroary Page 2 of 2 Report Number: 16-012-0752 Account Number:46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 Date Received: 01/12/2016 Date Of Report: 01/14/2016 0 -1 Q-1" 0 Waypoint.,( ANALYTICAL "Every acre... Every year. "� Farm ID: AN-19 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: CALVIN MORRIS 554 HASTY ROAD PEACHLAND NC 28133 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A IbIA Ib/A Ib/A 1-1 Fescue Hay 4 1.3 50 0 182 0 5 0 0 0 0 0 NC Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 4 Report Number: 16-012-0756 Account Number: 46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110. Date Received: 01/12/2016 Waypointo ANALYTICAL 'Every acre... Every year. "rM Farm ID: UN-18 SOIL ANALYSIS REPORT Date OfAnalvsis: 01/13/2016 Date Of Report: 01/14/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: HARRY MYERS 2225 OLIVE BRANCH RD MONROE NC 28110 Analytical Method(s): Mehlich 3 OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number Rate Class Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/100g meq/100g 1-1 2.2 658 VH 81 L 277 H 1724 M 21 VL 10002 73 5.6 6.59 3.4 14.6 MIN NC L NC = 548 NC = 41 2-1 10003 2.7 88 1517 VH 34 VL 178 M 1308 M 12 VL 5.5 6.65 2.8 11.0 MIN NC M NC = 431 NC = 17 3-1 10004 2.7 85 1342 VH 200 VH 1330 H 1652 M 7 VL 6.3 1.4 13.0 NC MH NC = 285 NC = 102 4-1 2.5 117 VH 69 L H 1176 M 7 VL 10005 86 1260 6.1 6.80 1.3 9.5 NC L�M`I NC = 97 NC = 35 5-1 10006 2.4 [- 78 399 VH 1220VH 282 H 1926 M 5 VL 6.4 1.2 13.8 MIN NC L NC = 332 NC = 113 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NOaN S Zn Mn Fe Cu B SS Cl AI Field ID % % "fie off, % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 1-1 25 M 23.1 VH 66 - VH 349 VH 12.8 VH 1.1 M 0.33 VL 1.4- 15.8 59.0 0.6 23.3 NC NC = 52 NC = 577.5 NC = 413 NC = 640.0 2-1 M 18.5 VH 21 H VH 10.1 VH M VI - 0.8 13.5 59.5 0.5 25.5 118 1490 10.7 10.18 NC NC = 37 NC = 462.5 NC = 131 NC = 505.0 3-1 L 11.9 VH H VH VH M VI - 3.9 21.2 63.5 0.2 10.8 112 130 1474 13.9 10.9 10.19 NC NC = 25 NC = 297.5 NC = 188 NC = 195.0 4-1 L VH 15 M VH VH 1.1 M VL 1.9 21.9 61.9 0.3 13.7 112 19.4 1321 13.6 10.17 NC NC=25 NC=235.0 NC=94 NC=180.0 5-1 L VH H 388 VH VH 1.1 M VL 4.1 17.0 69.8 0.2 8.7 114 117.0 122 18.2 10.11 NC NC = 29 NC = 425.0 NC = 138 NC = 410.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: waypointAnalytical Virginia, Inc. d C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2, of 4 Report Number: 16-012-0756 Account Number:46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 Date Received: 01/12/2016 Date Of Report: 01/14/2016 Waypoint. ANALYTICAL i "Every acre... Every year. Farm ID: UN-18 i SOIL FERTILITY11RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401.0 Fax 804-271-6446 www.waypointanalytical.com - Grower: HARRY MYERS 2225 OLIVE BRANCH RD MONROE NC 28110 Nitrogen I Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N I P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A i Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A lb/A 1-1 Fescue Hay 4 2.2 � 50 0 250 0 0 0 0 0 0 0 NC 2_1 Fescue Hay 4 1.8 50 0 250 0 10 0 0 0 0 0 NC 3-1 Fescue Hay 4 0.0 50 0 64 0 17 0 0 0 0 0 NC 4-1 Fescue Hay 4 0.8 50 0 250 0 17 0 2 0 0 0 NC 5-1 Fescue Hay 4 0.0 50 0 50 0 15 0 0 0 0 0 NC Comments: Sample(s) : 2-1,3-1,4-1,5-1 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. Sample(s) : 2-1,4-1 Crop: Fescue Hay The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. 1 "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the �Gt�rca me GIN work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. 1 Pauric McGroary Page 3 of 4 Report Number: 16-012-0756 Account Number:46205 Send To: CITY OF MONROE. STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 Data Received: 01/12/2016 Waypoint ANALYTICAL "Every acre... Every year. "rn, Farm ID: UN-18 SOIL ANALYSIS REPORT Date Of Analysis: 01/13/2016 Date Of Report: 01/14/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: HARRY MYERS 2225 OLIVE BRANCH RD MONROE NC 28110 Analytical Method(s): Mehlich 3 OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number Rate Class Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meg1100g meq/100g 6-1 10007 1.8 67 298 VH 104 L 361 H 2O39 H 6 VL 71 0.0 13.5 MIN NC L NC = 248 NC = 53 7-1 10008 2.3 83 1319 VH 88 L 227 H 1192 M 11 VL 6.1 6.80 1.3 9.4 MIN NC L NC = 266 NC = 45 8-1 10009 2.3 78 301 VH 122 M 155 M 1230 L 13 VL 5.1 6.46 4.7 12.5 NC LH NC = 251 NC = 62 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Chloride Aluminum Sample ID K Mg Ca Na H NOsN S Zn Mn Fe Cu B SS CI Al Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 6-1 14 L 11.7 VH 95 VH 422 VH 5.1 VH 1.4 H 0.11 VL 2.0 22.3 75.5 0.2 0.0 NC NC = 29 NC = 292.5 NC = 594 NC = 255.0 7-1 18 M VH VH VH VH H VL 2.4 20.1 63.4 0.5 13.8 110.6 151 1466 14.9 11.5 10.06 NC NC = 37 NC = 265.0 NC = 319 NC = 245.0 8-1 VH 2O.8 VH H VH 2.5 H 1.8 H VL 2.5 10.3 49.2 0.5 37.6 141 148 1594 10.37 NC NC = 85 NC = 520.0 NC = 300 NC = 125.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: a f,- me G H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 4 of 4 Report Number: 16-012-0756 Account Number: 46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 Date Received: 01/12/2016 Date Of Report: 01/14/2016 Waypoeint,7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL wwW.waypointanalytical.com "Every acre... Every year. Grower: HARRY MYERS 2225 OLIVE BRANCH RD MONROE NC 28110 Farm ID: UN-18 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop [::: Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons1A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 6-1 Fescue Hay 4 0.0 50 0 250 0 15 0 0 0 0 0 NC 7-1 Fescue Hay 4 0.8 50 0 250 0 10 0 0 0 0 0 NC 8-1 Fescue Hay 4 3.1 50 0 250 0 0 0 0 0 0 0 NC Comments: Sample(s) : 7-1,8-1 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. 4 "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." y7 (Ply G� Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric•McGroary Page 1 of 2 Report Number: 16-012-0751 Account Number:46205 - Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 Date Received: 01/12/2016 WaypA 'Every acre... Every year. ">M Farm ID: UN-25 SOIL ANALYSIS REPORT Date Of Analysis: 01/13/2016 Date Of Report: 01/14/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: WAYNE MCBRIDE 3303 TRINITY CHURCH RD MONROE NC 28112 Analytical Method(s): Mehlich 3 OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil Ibs/A Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number Rate _ Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 1-1 4.2 214 VH 82 L 271 H 1141 M 10 VL 09991 120 6.1 6.80 1.3 9.5 MIN NC M NC = 178 NC = 42 3-1 09992 4.5 127 167 H 31 VL 266 H 1045 M 11 VL 6.0 6.79 1.4 9.0 MIN NC M NC = 56 NC = 16 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron "Copper Boron Soluble Salts Chloride Aluminum Sample ID Fed ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 1-1 17 M 12.5 VH 43 H 523 VH 11.0 VH 1.3 H 0.16 VL 2.2 23.8 60.1 0.5 13.7 NC NC = 35 NC = 312.5 NC = 269 NC = 550.0 3-1 M VH H VH 11.7 VH H VL 0.9 24.6 58.1 0.5 15.6 116 18.7 130 1559 12.1 10.16 NC NC=33 NC=217.5 NC=188 NC=585.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to samples) tested. Samples are,retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. me Gr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: Pori. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc. Pauric McGroary Page 2 of 2 Report Number: 16-012-0751 Account Number:46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR' MONROE NC 28110 Date Received: 01/12/2016 Date Of Report: 01/14/2016 7-7 d • Waypoint 7621 Whitepine Road, Richmond, VA 23237. Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com "Every acre... Every year. Grower: WAYNE MCBRIDE 3303 TRINITY CHURCH RD MONROE NC 28112 Farm ID: UN-25 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 1-1 Fescue Hay 4 0.8 50 0 250 0 11 0 0 0 0 0 NC 3-1 Fescue Hay 4 0.8 50 30 250 0 13 0 0 0 0 0 NC Comments: Sample(s) : 3-1 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the pow;. work,the results, or the company iri any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 4 Report Number: 16-01.2-0757 Account Number:46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 Date Received: 01/12/2016 0 s Way �®' ��- 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com "Every acre... Every year. Grower: EMERSON MCBRIDE 7210 ROCKY RIVER RD SOUTH Date Of Analysis: 01/13/2016 MONROE NC 28112 Farm ID: UN-26 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 01/14/2016 OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number % Rate Soil Class Ibs/A Mehlich 3 ppm 'Rate Reserve ppm Rate K ppm Rate Mg ppm Rate ppm Ca Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 1-1 10010 2.4 88 208 VH 35 VL 204 H 860 M 18 VL 6.3 0.7 6.9 MIN NC L NC = 173 NC = 18 2-1 10011 2.3 84 208 VH 119 M 1234 H 993 M 13 VL 6.2 1.0 8.3 MIN NC L NC = 173 NC = 61 3-1 10013 2.0 77 1211 VH 1137 H 1235 H 1089 M 12 VL 6.1 6.81 1.2 9.0 MIN NC L NC = 176 NC = 70 4A-1 10014 4.6 130 222 VH 101 M 1219 H 939 M 8 VL 5.9 6.79 1.4 8.2 IN NC M NC = 185 NC = 52 413-1 10015 1.2 62 1202 VH 78 L 246 VH 1044 M 15 VL 6.4 0.7 8.2 MIN NC L NC = 168 NC = 40 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K % Mg % Ca Na H % % % NON ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate ppm B Rate SS ms/cm Rate CI ppm Rate AI ppm 1-1 16 M 10.1 VH 22 H 562 VH 6.4 VH 1.3 H 0.12 VL NC 1.3 24.6 62.3 1.1 10.1 NC=33 NC=252.5 1 NC=138 NC=320.0 2-1 M VH H 494 VH 6.1 VH M VL NC 3.7 23.5 59.8 0.7 12.0 117 NC = 35 110.6 NC = 265.0 123 NC = 144 NC = 305.0 10.8 10.11 3-1 L 10.9 VH 26 H 487 VH 5.5 VH M VL NC 21.8 60.5 0.6 13.3 1123.9 NC = 25 NC = 272.5 NC = 163 NC = 275.0 10.9 10.11 4A-1 M VH H VH 5.2 VH 0.8 M 0.24 VL NC 3.2 22.3 57.3 0.4 17.1 119 NC = 40 110.5 128 NC = 262.5 NC = 175 1515 NC = 260.0 1 46-1 L VH VH VH 8.9 VH 1.3 H VL NC 2.4 25.0 63.7 0.8 8.5 113 110.5 NC=27 151 NC=262.5 1530 NC=319 1 NC=445.0 10.13 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble analysis prepared by: Waypoint Analytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 4 Report Number: 16-012-0757 Account Number:46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 Date Received: 01/12/2016 Date Of Report: 01/14/2016 Waypoint. ANALYTICAL 'Every acre... Every year. "� Farm ID: UN-26 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Grower: EMERSON MCBRIDE 7210 ROCKY RIVER RD SOUTH MONROE NC 28112 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron CopperrBn Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe CuTons Field ID Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 1-1 Fescue Hay 4 0.0 50 0 250 0 13 0 0 0 0 0 NC 2-1 Fescue Hay 4 0.0 50 0 250 0 11 0 0 0 0 0 NC 3-1 Fescue Hay 4 0.8 50 0 215 0 17 0 0 0 0 0 NC 4A-1 Fescue Hay 4 0.8 50 0 250 0 9 0 0 0 0 0 NC 4B-1 Fescue Hay 4 0.0 50 0 250 0 16 0 0 0 0 0 NC Comments: Sample(s) : 2-1,3-1,4A-1,4B-1 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. Sample(s) : 2-1,4A-1,4B-1 Crop: Fescue Hay The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." 60wr Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1 GtW« r"c work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 3 of 4 Report Number: 16-012-0757 Waypointe) Account Number: 46205 • Send To: CITY OF MONROE ANALYTICAL STEVE HOLDEN 'Every acre... Every year. "mr 775 TREEWAY DR MONROE NC 28110 Farm ID: UN-26 SOIL ANALYSIS REPORT Date Received: 01/12/2016 Date Of Analysis: 01/13/2016 Date Of Report: 01/14/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Grower: EMERSON MCBRIDE 7210 ROCKY RIVER RD SOUTH MONROE NC 28112 Analytical Method(s): Mehlich 3 OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number Rate Class IbslA ppm Rate ppm- Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meg1100g 5-1 2.5 125 VH 31 VL 250 H 1432 H 17 VL 10016 85 6.5 0.8 10.2 MIN NC L I NC = 104 NC = 16 6-1 10017 1.4 68 80 H 39 VL 197 H 845 M 13 VL 6.0 6.82 1.1 7.1 MIN NC L NC = 67 NC = 20 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS CI AI Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate mslcm Rate ppm Rate ppm 5-1 16 M 12.5 VH 20 M 365 VH 5.1 VH 1.7 H 0.14 VL 0.8 20.4 70.2 0.7 7.8 NC NC=33 NC=312.5 1 NC=125 NC=255.0 6-1 19 M H H VH 11.5 VH H 0.09 VL 1.4 23.1 59.5 0.8 15.5 16.8 135 1244 12.2 NC NC=40 NC=170.0 NC=219 NC=575.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: PGf�ric m� G� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: WaypointAnalytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 4 of 4 Report Number: 16-012-0757 Account Number: 46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 Date Received: 01/12/2016 Date Of Report: 01/14/2016 Waypoint-Q, ANALYTICAL 'Every acre... Every year. Farm ID: UN-26 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: EMERSON MCBRIDE 7210 ROCKY RIVER RD SOUTH MONROE NC 28112 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 5-1 Fescue Hay 4 0.0 50 0 250 0 13 0 2 0 0 0 NC 6-1 Fescue Hay 4 0.8 50 30 250 0 9 0 0 0 0 0 NC Comments: Sample(s) : 6-1 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the �Gtt��6 me work,the results, or the company In any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 2 Report Number: 16-012-0753 Account Number: 46205 Send To: CITY OF'MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 • Waypoints 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Every acre... Every year."rm Grower: LELAND WOLFE 1805 JACK DAVIS ROAD MONROE NC 28112 Farm ID: UN-27 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Received: 01/12/2016 Date Of Analysis: 01/13/2016 Date Of Report: 01/14/2016 OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil Ibs/A Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number Rate Class. ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 1-1 09994 2.4 81 312 VH 82 L 252 H 1571 M 28 VL 6.1 6.77 1.6 11.9 MIN 'NC L NC = 260 NC = 42 2-1 09995 3.0 101 167 VH 118 M 1173 H 579 L 9 VL 5.5 6.77 1.6 6.3 MIN NC M NC = 139 NC = 60 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID e FieID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 1-1 19 M 11.7 VH 35 H 355 VH 15.8 VH 0.6 M 0.15 VL 1.8 17.6 6ti.0 1.0 13.4 NC NC = 40 NC = 292.5 NC = 219 NC = 790.0 2-1 H 5.3 H 47 H 265 VH 7.9 VH VL VL 4.8 22.9 46.0 0.6 25.4 128 10.3 10.14 NC NC = 58 NC = 132.5 NC = 294 NC = 395.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g. maximum of thirty days after testing. p H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: m° G flpµ/ca Pow ,C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc. Pauric MCGroary Page 2 of 2 Report Number: 16-012-0753 Account Number:46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 Date Received: 01/12/2016 Date Of Report: 01/14/2016 F Waypoint ANALYTICAL 'Every acre... Every year.",m Farm ID: UN-27 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: LELAND WOLFE 1805 JACK DAVIS ROAD MONROE NC 28112 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A I1-1 Fescue Hay 4 1.0 50 0 250 0 9 0 0 0 0 0 NC 2-1 Fescue Hay 4 1.3 50 0 228 0 0 0 0 0 0 0 NC Comments: - Sample(s) : 2-1 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 2 Report Number: 16-012-0754 Account Number: 46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 nnte Raceivnrlr w/12/2n16 • Waypoint. ANALYTICAL "Every acre... Every year. "n,, Farm ID: UN-30 SOIL ANALYSIS REPORT Date Of Analvsis: 01/13/2016 Date Of Report: 01/14/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Grower: TOM APPENZELLER 830 CLOVER ROAD MARSHVILLE NC 28103 Analytical Method(s): Mehlich 3 OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab "fie Soil Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number Rate Class Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate P H Index meq/100g meg1100g 1-1 09996 3.0 94 388 VH 134 M 274 H 1430 M 12 VL 6.1 6.77 1.6 11.4 MIN NC M NC = 323 NC = 69 4-1 09997 2.8 93 1192 VH J9.3 55 VL 240 H 1161 M 10 VL 6.1 6.80 1.3 MIN NC M NC = 160 NC = 28 5-1 09998 2.3 84 1129 VH 54 VL 194 H 966 M 8 VL 5.7 6.75 1.8 8.4 NC LH NC = 107 NC = 28 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble salts Chloride Aluminum Sample ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS Cl At Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 1-1 21 M 16.8 VH 47 H 277 VH 18.9 VH 0.8 M 0.18 VL NC 3.0 20.0 62.7 0.5 14.0 NC = 44 NC = 420.0 1 NC = 294 1NC = 945.0 4-1 M 9.0 VH H 208 VH M VL NC 1.5 21.5 62.4 0.5 14.0 120 NC=42 NC=225.0 134 NC=213 15.8 .H NC=2900 10.6 10.18 5-1 M VH 43 H VH VH 0.5 L VL NC 1.6 19.2 57.5 0.4 21'.4 116 NC=33 110.7 NC=267.5 NC=269 1172 13.9 NC=195.0 10.2 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: flies me G� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble ,analysis prepared by: waypointAnalytical Virginia, Inc. r a C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary - — - - — ----�--- --_ -- -- - - i - - -- - - -- J Page 2 of 2 Report Number'-16-012-0754 ° Account Number:46205 Waypoint, 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 Send To: CITY OF MONROE ANALYTICAL www.waypointanalytical.com _ STEVE HOLDEN "Every acre... Every year. Grower: TOM APPENZELLER 775 TREEWAY DR 830 CLOVER ROAD MONROE NC 28110 MARSHVILLE NC 28103 Farm ID: UN-30 Date Received: 01/12/2016 Date Of Report: 01/14/2016 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 1-1 Fescue Hay 4 1.0 50 0 222 0 7 0 0 0 0 0 NC 4-1 Fescue Hay 4 0.8 50 0 250 0 8 0 0 0 0 0 NC 5-1 Fescue Hay 4 1.0 50 0 250 0 13 0 0 0 0 0 NC Comments: Sample(s) : 4-1,5-1 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." p/�a me r Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part,, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining out prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 2 Report Number: 16-012-0755 Account Number: 46205 Send To: CITY OF MONROE STEVE HOLDEN 775 TREEWAY DR MONROE NC 28110 Waypoint ANALYTICAL Every acre... Every year.". Date Received: 01/12/2016 Date Of Analysis: 01/13/2016 Farm ID: UN-29 SOIL ANALYSIS REPORT Date Of Report: 01/14/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: WILLIAM GRIFFIN 6705AUSTEN GROVE CHURCH MARSHVILLE NC 28103 Analytical Method(s): Mehlich 3 OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil Ibs/A Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 3-1 2.3 360 VH 85 L 199 H 1153 M 17 VL 09999 82 5.7 6.72 2.1 9.8 I MIN NC L I NC = 300 NC = 43 4-1 10000 1.9 76 1216 VH 165 L 238 H 1132 M 9 VL 6.5 0.6 8.4 MIN INC L NC = 180 NC = 33 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 3-1 16 M 9.0 VH 33 H 313 VH 16.4 VH 0.5 L 0.18 VL 2.2 16.9 58.8 0.8 21.4 NC NC = 33 NC = 225.0 NC = 206 NC = 820.0 4-1 M 10.5 VH H VH 10.1 VH 0.5 L VL NC 2.0 23.6 67.4 0.5 7.1 121 NC=44 NC=262.5 131 NC=194 1212 NC=505.0 10.17 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. m� G4 H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: Pogi. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: WaypointAnalytical Virginia, Inc. Pauric McGroary Page 2 of 2 Report Number: 16-012-0755 Account Number:46205 • 7621 Whitepine Road, Richmond, VA 23237 Waypoint, Main 804-743-9401 ° Fax 804-271-6446 Send To•. CITY OF MONROE ANALYTICAL www.waypointanalytical.com STEVE HOLDEN 'Every acre... Every year. Grower: WILLIAM GRIFFIN 775 TREEWAY DR 6705AUSTEN GROVE CHURCH MONROE NC 28110 MARSHVILLE NC 28103 Farm ID: UN-29 Date Received: 01/12/2016 Date Of Report: 01/14/2016 SOIL FERTILITY RECOMMENDATIONS Nitrogen_ Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A VA Ib/A Ib/A Ib/A Ib/A Ib/A 3-1 Fescue Hay 4 1.3 50 0 250 0 13 0 0 0 0 0 NC 4-1 Fescue Hay 4 0.0 50 0 250 0 7 0 0 0 0 0 NC Comments: Samples): 4-1 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M r Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the �Otur�a MC work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary