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HomeMy WebLinkAboutNC0023965_wasteload allocation_19910225NPDES DOCUMENT SCANNING COVER SHEET NPDES Permit: NCO023965 Wilmington - Northside WWTP Document Type: Permit Issuance Wasteload Allocation Authorization to Construct (AtC) Permit Modification Engineering Alternatives Analysis 201 Facilities Plan Instream Assessment (67B) Toxicity Study Permit History Date Range: Document Date: February 25, 1991 THIS DOCUMENT IS PRINTED ON REUSE PAPER - IGNORE ANY CONTENT ON 71111E REVERSE SIDE NPDES WASTE LOAD ALLOCATION PERMIT NO.: NC0023965 -Jamps r1- L-�,,bQ:.. Owl? pERMITTEE NAME: City of Wilmington / Northside W WTP Facility Status: Existing Permit Status: Renewal Major -4 Minor Pipe No.: 001 Design Capacity: 8.0 MGD Domestic (% of Flow): 96 % Industrial (% of Flow): 4 % Comments: RECEIVING STREAM: the Cape Fear River Class: SC -Swamp Sub -Basin: 03-06-17 Reference USGS Quad: K27NW (please attach) County: New Hanover Regional Office: Wilmington Regional Office Previous Exp. Date: 6/30/91 Treatment Plant Class: Class 4 Classification changes within three miles: none Requested by: Rosanne Barona Prepared by: a Reviewed by: �oD 1 j Date: 1/15/91 Date: 0P11611?19i Date: Modeler JDateRec. I# GAS ty -At 1 Coo$ Drainage Area (mil ) 97 30 Avg. Streamflow, (cfs):11D"1"- 7Q10 (cfs) 70 / Winter 7Q10 (cfs) Toxicity Limits: IWC /. -I % Instream Monitoring: 30Q2 (cfs)_ Acut � Parameters Upstream Location Downstream Location Effluent Characteristics BOD5 (m ) 30 NH3-N (mg/l) C'tirn ' D.O. (mg/1) ho D 2� TSS (mg/1) F. Col. (/100 ml) �00 ka el pH (SU)y2; c / r — /C 1 MOn1 / �r ` L rye, l 4 G 7-/ Comments: -1- Request No. 6005 FACT SHEET FOR WASTELOAD ALLOCATIONS Facility Name :City of Wilmington - Northside WWTP NPDES No. :NC0023965 FEB i g 199, Type of Waste :96% Domestic/4% Industrial Facility Status :Existing Wilmington Ronal Ofrlco Permit Status :Renewal AKA+ Receiving Stream :Cape Fear River Stream Classification:SC-Swamp Subbasin :03-06-17 County :New Hanover Stream Characteristics: Regional Office :Wilmington USGS # Date Requestor :Rosanne Barona Drainage Area: 8730 sq.mi. Date of Request :1/15/91 Summer 7Q10: 701 cfs Topo Quad :K27NW Winter 7Q10: cfa Average Flow: TIDAL 30Q2: cfs Wasteload Allocation Summary Renew with existing limits. Permitee is currently under an SOC for BODS. The permitee meets the requirements for a waiver of the 85% removal requirement for BODS and TSS. The concentration limits of 30 mg/l for each must be met however. Pretreatment information indicates metals limits for Nickel, Cyanide, and Mercury are warranted. However, these limits would be easily met by Wilmington. Recommend monitoring only. A reopener clause should be placed in the permit to allow for limits to be changed, if necessary, upon completion of a comprehensive water quality analysis of the lower Cape Fear River basin or if the facility should fail its whole -effluent toxicity test. WASTELOAD SENT TO EPA7(Major) (Y or N) (if yes, then attach schematic, toxics spreadsheet, copy of model, or if not modeled, then old assumptions that were made, and description of how fits into basinwide plan) Recommended by: Date: z 9/ Reviewed by Instream Assessment:` '� �( Date: 2 Regional Supervisor -D Date: 2 / o 3l Permits & Engineering: r`7. l}Qti Date: Q MAR 12 1991 RETURN TO TECHNICAL SERVICES BY: Existing Limits Wasteflow (MGD) : BOD5 (mg/1) : NH3N (mg/1): DO (mg/1): TSS (mg/1): Fecal Coliform (/100 ml): pH (SU) : TP (mg/1) : TN (mg/1): Recommended Limits Wasteflow (MGD) : BOD5 (mg/1): NH3N (mg/1): DO (mg/1) : TSS (mg/1): Fecal Coliform (/100 ml): pH (SU) : TP (mg/1) : TN (mg/1): CONVENTIONAL PARAMETERS Monthly Average Summer/Winter 8.0 30 monitor no limit 30 200 6.8-8.5 monitor monitor Monthly Average Summer/Winter 8.0 30 monitor no limit 30 200 6.0-8.5 monitor monitor Request No. 6005 Daily Maximum Daily Maximum Limits Chancres Due To: Parameter(s) Affected Instream Data Ammonia Toxicity Chlorine Nutrient Sensitive Waters HQW New 7Q10 flow data Special Modeling Studies New facility information Other (explanation of any modifications to past modeling analysis includidng new flows, rates, field data, interacting discharges, etc.) (See page 4 for Miscellaneous and special conditions if apply) L 41 Toxicty Limit: Chronic, Quarterly Existing Limit:1.7% Recommended Limit:1.7o TOXICS Monitoring Schedule: FEB, MAY, AUG, NOV Toxics or metals limits Existing Limits- Daily Maximum Copper (ug/1): Lead (ug/1): Zinc (ug/1): Cyanide (ug/1): Mercury (ug/1) : Chlorine (ug/1) : �njg/1): Recommended Limits Cadmium (ug/1): Chromium (ug/ 1) : Copper (ug/1): Nickel (ug/1): Lead (ug/1): Zinc (ug/1): Cyanide (ug/1) : Mercury (ug/1): Chlorine (ug/1) : Silver (ug/1) : Limits Changes Due to: Change in 7Q10 data Change in stream classification Relocation of discharge Change in wasteflow New pretreatment information Failing toxicity test Other monitor monitor monitor monitor monitor monitor monitor Daily Maximum -monitor monitor monitor .monitor monitor monitor monitor monitor monitor -monitor (onsite toxicity study, interaction, etc.) Parameter(s) Affected. C/l, Cr, Ni, pH revision; background waters are less than 6.5 su -4- i Request No. 6005 MISCELLANEOUS INFORMATION & SPECIAL CONDITIONS Miscellaneous information pertinent to the renewal or new permit for this discharge. Include relationship to the Basinwide management plan. INSTREAM MONITORING REQUIRMENTS: Upstream: N Location: Donwstream: N Location: Special Instream monitoring locations or monitoring frequencies: SPECIAL INSTRUCTIONS OR CONDITIONS SCHEDULE REQUIREMENTS: (for P&E or region to recommend.time frame for implementing new limits) ADDITIONAL "REVIEWER" COMMENTS: Additional Information attached? (yes or no) If yes, explain attachments. I 10/89 L" Facility Name Cl u� Permit tt _/Vcoa urs- CHRONIC TOXICITY TESTING REQUIREMENT (QRTRLY) The effluent discharge shall at no time exhibit chronic toxicity in any two consecutive toxicity tests, using test procedures outlined in: 1.) The North Carolina Ceriodaphnia chronic effluent bioassay procedure (North Carolina Chronic Bioassay Procedure - Revised *September 1989) or subsequent versions. The effluent concentration at which there may be no observable inhibition of reproduction or significant mortality is L 7 °Jo (defined as treatment two in the North Carolina procedure document). The permit holder shall perform Quarte-rim Quart-rimmonitoring using this procedure to establish compliance with the permit condition. The. first test will be performed after thirty days from issuance of this permit during the months of Feb , AUY, Ave,. MoJ . Effluent sampling for this testing shah be performed at the NPDES permitted final effluent discharge below all treatment processes. All toxicity testing resultsrequired as part of this permit condition will be entered on the Effluent Discharge Monitoring Form (MR-1)' for the month in which it was performed, using the parameter code'TGP3B. Additionally, DEM Form AT I (original) is to be sent to the following address: Attention: Environmental Sciences Branch North Carolina Division of Environmental Management P.O. Box 27687 Raleigh, N.C. 27611 Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in -association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should any single quarterly monitoring indicate a failure to meet specified limits, then monthly monitoring will begin immediately until such time that a single test is passed. Upon passing, this monthly test requirement will revert to quarterly in the months specified above. Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Environmental Management indicate potential impacts to die receiving stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival and appropriate environmental controls, shall constitute an invalid test and will require immediate retesting(within 30 days of initial monitoring event). Failure to submit suitable test results will constitute noncompliance with monitoring requirements. 7Q10 7o cfs Penmited. Flow R' o MGD IWC% /, 7 Y Basin & Sub -basin o 3 -06 - ►7 Receivin Stream Cam" County �nj (-fQw& Recommended by: **Chronic Toxicity (Ceriodaphnia) P/F at L-_'l %, FE9., M4y, ALajAMV, See Part 3, Condition Z _ 01/22/91 Yer 3.1 T 0% I C S R E V I E W Facility: Wllminton-Northalde WHIP NPDES Permit No.: NCO023965 Statue (E, P. or M) : E Permitted Flow: 8.0 mgd Actual Average Flow: 4.5 mgd Subbasln: 030617 Receiving Stream: Cape Fear River I --------- PRETREATMENT DATA -------------- I ---- EFLLUENT DATA---- 1 Stream Classification: Sc I ACTUAL PERMITTEDI I 7010: 701.0 ofs I Ind. + Ind. + I FREQUENCY I INC: 1.74 4 I Domestic PERMITTED Domestic I OBSERVED of Chronicl Stn'd / Bkg I Removal Domestic Act.Ind. Total Industrial Total I Eflluent Criteria I Pollutant AL Cone. I Eff. Load Load Load Load Load I Cone. Violational (ug/1) (ug/1) I 4 (6/d) (4/d) (4/d) (4/d) (4/d) I (ug/1) (4vio/4sam)l I_------ ___---- - - - - - ________ _________ ________ 1 ---- --- Cadmium 8 5.0 1 504 0.2 0.1 0.30 0.0 0.230 I I Chromium 8 20.0 1 500 0.4 1.0 1.46 1.4 1.800 I I Copper AL 3.0 1 404 2.2 0.9 3.00 0.7 2.840 I 35.0 I N Nickel 8 8.3 I 20% 0.4 0.2 0.63 2.1 2.490 I I P Lead 8 25.0 I 50% 0.4 1.6 2.01 2.1 2.490 1 100.0 1 U Zinc AL 86.0 I 60% 6.5 4.1 10.54 0.3 6.800 I 110.0 I T Cyanide 8 1.0 I 30% 0.4 0.1 0.54 0.0 0.000 1 30.0 1 Mercury S 0.025 1 04 I 0.4 I S Silver AL 0.10 1 04 I 1 E Selenium S 71.00 1 04 I I C Arsenic S 50.00 1 0% I 1 T Phenols 9 NA 89% I I I NH3-N C 04 I 1 0 T.R.Ch1or.AL 17.0 1 04 0.000 I I N =lue nd c 1,800.0 1 0.2 0.0 0.0 0.00 4.0 4.000 I 'gown 1 0.0 0.0 0.0 0.00 0.8 0.830 I 1 0.0 0.0 0.0 0.0 15.9 15.850 I 1------------- ALLOWABLE PRDCT'D PRDCT'D PRDCT'D--------- MONITOR/LIMIT --------- 1--ADTN'L RECMMDTN'S-- 1 Effluent Effluent Effluent Instream I Recomm'd 1 Cone, using using Cone. Based on Based on Based on I FREQUENCY INSTREAM I Allowable CHRONIC ACTUAL PERMIT using ACTUAL PERMITTED OBSERVED I Eff. Mon. Monitor. Pollutant I Load Criteria Influent Influent OBSERVED Influent Influent Effluent I based on Recomm'd 7 I (4/d) (ug/1) (ug/1) (ug/1) tug/1) Loading Loading Data 1 OBSERVED (YES/NO) --------- -- 1 _________ ________ _________------- --------------- -------- -------- 1 _________ -------- Cadmium S I 38.17 287.661 3.955 3.032 0.00 Monitor Monitor 1 Chromium S I 152.68 1150.645 19.248 23.730 0.00 Monitor Monitor I Copper AL I 19.08 172.597 47.460 44.929 0.61 Monitor Monitor Monitor I Monthly NO Nickel S I 39.60 477.518 13.289 52.523 0.00 Monitor Limit I Lead S I 190.85 1438.306 26.499 32.827 1.74 Monitor Monitor Monitor I NCAC NO Zinc Al, 1 820.64 4947.774 111.163 71.718 1.92 Monitor Monitor Monitor I Monthly NO Cyanide 8 1 5.45 57.532 9.967 0.000 0.52 Limit Limit I NCAC NO Mercury a I 0.10 1.438 0.000 0.000 0.01 Limit I NCAC NO Silver AL I 0.38 5.753 0.000 0.000 0.00 I Selenium S I 271.00 4084.790 0.000 0.000 0.00 1 Arsenic S 190.85 2876.613 0.000 0.000 0.00 I Phenols S �1 0.000 0.000 0.000 0.00 I NH3-N C I 0.00 0.000 0.000 0.000 0.00 l T.R.Chlo1�r.AL I 64.89 978.048 0.000 0.000 0.00 1 F(ror:c� 1 8,588.08 103,558 0.000 84.374 0.00 1 'aoro.i 0.00 0.000 0.000 21.666 0.00 Limit I Gen Aa - u 0 0 4/2+/r o I I I I I I A I N IA I L I Y I S I I I S I I R I E I S I U I L I T I S . . r pain AlA64* �o��o?Sro7 Own �,nb�cnt 5�f%en tk DAI o d'G9.L30 Ow, Tom_ 00.;Li0173 (o Via y E.. cJ�l.«;n9�o.i So��t�►��d� Qw : ��. A►GC1 DEt 4mhj"-1 6fi'o-,t v 4 0,2,10 IS-7 , F kR ° Cete c Awl- e _ rYnn;fp nnq is �tilre� - . �(CSZ.�J SG �iScl�arge is 4�, NEp��2a� u u 1 nS'h�eam vnow.ilT%. n�- f1��0 w�61e w-.Ma-iq Summer VS cv, oOnne - no ��,w + ,. SC w+,kv s facer'% °"ee/z Ae J,i-e,Cn7-S -far Cc c,Jai vl?r JYuI � �s Flo %SS EXis T]ni6 crm,rs Glow F% O _. Z3a3D5-- 3 0 Gip TMAL Fecal avo .76Au5 - 7oi PN G.r-..5 . 7Qtu,,, - /?eAll7v2 % TN, 7P ..30 z — 41, Cam, n CN,PL� Kj %O X(CS Preis-ec+.�,+eic't .s�rneaaJh.¢eL� eA/ 477 S7a`I "9(C S'fD 37DGL ° obs¢r.^ecl Cw �( 57.9a 3s- �p J 71 ;2 S LQ�t y o a 2 8o - 0;5 7- VIP 174nC. `/ °I 6 Z - CWb de 73/ — — � Lim 17 NW N lTD2 N?c.k,. i %7 v9 l l Cc{ J pin 1 �5 �I FOR AGENCY USV l STANDARD FORM A —MUNICIPAL J SECTION 17, INDUSTRIAL WASTE CONTRIBUTION TO MUNICIPAL SYSTEM Submit a description of each major Industrial facility discharging to the municipal system, using a separate Soctlon IV for each facility deurip• tion. Indicate the 4 digit Standard Industrial Classification (SIC) Code for the Industry, the major product or raw material, the flow tin Ih(,,.• send Saucesis pday), and the characteristics of the wastewater discharged from the Industrial facility Into the municipal system. Consult :able III for Standard measures of products or raw materials. (see Instructions) t• M+ler CMtairWing PNlllty (see Instructions) Name 1 401a Corning, Inc. _N Number& Street City County State zip Coda 2. P"ary Standard Industrial Classification Code (see Instructions) S. PrindPal Product or Raw Material (see Instructions) Product new Material 4. Plow Indicate the volume of water discharged Into the municipal sys. tom In thousand gallons per day and whether this discharge is Inter• mittent or continuous. S. Pretreatment Provided Indicate If Pretreatment Is provided prior to entering the municipalsystem S. Characteristics of Wastewater (see Instructions) 40111, 401c 401d 401 a 401 f 402 403a, 407b 404a 4t14b 405 310 North College Road Wilmington New Hanover North Carolina 28405 3676 Units (See Quantity Table III) _ORtical Wave Guide Fiber .": 2500 qS� Khl 40d 60 thousand gallons per day ❑ IntIormlttent (Int)bContlnuous(con) ` 1C1yes ❑No Parameter Name BOD COD TSS 0&G Ph BORON • SULFATE Parameter 00310 00340 00350 00556 00400, " 00945 Value' 55 116. .69 29 7.1 0.4 21 *Continue on Page 2 ........ IV•I This Section contain ! page. OPO eaeAOe 'Rt t PON AGENCV Uff STANDARD FORM A -MUNICIPAL -1 111 HM SECTION 8. INDUSTRIAL WASTE CONTRIBUTION TO MUNICIPAL SYSTEM Submit a daacrlpIIOn of each mobs Industrial facility discharging to the mu land. Indicate She digit Standard Industrial Classification (SIC) Code for the n1CIM1 system, wing a wparate Section IV for each facility de►frip• land tlallons per Industry, Ins malOr product Of raw mateflN, the flow ion tho-, day), and the characteristics of the wastewater, discharged from the Industrial facility Into the municipal system, COnwlt ; able III lot Standard measure of products Of raw mat4wWl, pis Instructions) 1• moor corrtrasiou M pool" . (See Instructions) Name 14018 I Corning, Inc. Number. Street City County staff sir Coo 2. pilwary Standard Industrial cla"Iflestlen core (we Instructions) , S. Pdnalpal Preduat at Raw aaatfrlal (see Instructions) Product now Material 4. Plew Indicate the volume of water dNCMrOed Into the municipal syl, tens in thousand gallons per day and whether this discharge Is Inter• mltlent or Continuous. f. pratleatmant prevNed Indicate if pretreatment Is provided prior to entering the municipal system •. Charbateristlal of wastewater (sea instructions) 402 /o{a 4•{b 404s 404b I•g 310 North College Road Wilmington New. Hanover North Carolina 3676 Units IS" QuMllty -Table III Optical Wave Guide Fiber4d.. 2500 KM 60 thousand gallons paw, day Intermittent (IntQ:Fcontlnuous(con) E3VM ❑No Parsmeter ~""' -6irometet TS Chloride Germanium Floride Number 00500 00940 - - 009�1 valuf 1226. 490 3.2 0.7 *Continue from Page 1 ........ IV-1 Me eeefifn oeeltehw ! Pogo. 4415 / Doll AGI04CY Us/ •l STANDARD FORM A—MUNICIPALI I I I IT]~ SECTION 17. INDUSTRIAL WASTE CONTRIBUTION TO MUNICIPAL SVSTEM Submit a description of each major Industrial facility discharging to the municipal System, wing a espa►aN Seellon IV for each /aelllly deltrip (ion. Indicate the a dlpll Standard Induttriai Classification (SIC) Code for the Industry, the major Product or raw material, the flow lin IN-. Sand gallon' Per day). and the CharKISrlstics of the wastewater dbcharged from the Industrial facility Into the municipal system. Consult :.,big III for standard manures of producb or raw mslwwl, (see InstructloMr Ir Wier Coml"llsw leff roollNy (Sae Instructions Noma I 4ele I Textilease Corporation M _� Numbori !street City County state =M Code !, "Mary Standard Industrial ClawlflMMen Code (we Instructions) S. ►llneleal predtrH or Raw Material (see instructions) Product Raw Material 4, Flow Indicate the volume of water dbcharged Into the municipal sys. tam In thousand gallons ow day and whether this discharge Is Inter- mittent or continuous. 1, ►"tmltntant Prevlded Indicate If pretreatment is provided prior to entering the municipal system e. Chareeterletlae of Wastewater (eas Instructions) 4eM .4M 40! seta seer II N4a 4e4Y 4e/ 1821•Dawson Street Wilmington, New Hanover North Carolina 28406 7218 Units (Sit QYttntffy T N III _Industrial Launderer. 28,500 d�e4 lbs/day 4w 55 Ihotlearld galore Per day IffIntetmltteni (int) ❑ Continuous (con) y iffy" QNo Pa`a"1e1" Name BOD5 COD TSS 0&G Ph Lead Copper parameter Number 00310 00340 00350 00556 00400 01051 01042 Value, 375 2109 440 432 9.7 1.3 0.7 *Continue on Page 2 ......, rv-t Mis eoalloss edistalne ! eI0 aae.70a !es/e. Poll AGINCv Usr STANDARD FORM A -MUNICIPAL ~ SECTION 17. INDUSTRIAL WASTE CONTRIBUTION TO MUNICIPAL SYSTEM Submit a description of each major Industrial facility dlScharging to the munlcloal Syelem, using a separate Satlon IV for each facility descrip• tlon. Indicate the 4 digit Standard Industrial Classification (SIC) Code for IM Industry, the major product or raw material, the flow lin th(,,.• Mnd 111411101111 Per day). and the characteristics of the wastewater dischargedfrom the Industrial facility Into the municipal ayslem. Consulttple III for standard measures of products or raw materials. (see Instructions) t. Wier C4e1t►Dtltleg Pllaluttr . (see Instructions) Name I 4016 I Textilease Corporation _r NumOera street CIIy County State zip Coale I. "Mary standard Industrial Clasalfleatlon Cede two Instructions) s. P11n41Pal Preduat er Ilaw Malarial (ale Instructions) Product new Metwal 4. Plow Indicate the volume of water discharged Into the municipal sys. tam In thousand gallons ow day Intl whethei this discharge is Inter• mltlent or continuous. s. Pwt►eltment Provided IMlcale It pret►eatment Is provided prior to entering the municipal system s. Charosterlstles of wastewater (see instructions) U" .Am 4016 4014 "to 4014 401 f 402 407e 441136 404a 41111411111, 400 1821 DnwGon Street Wilmington .Mew Hanvoer - North Carolina _2a(Ln6 7218 Units (See QuMtltr Table I11 Industrial Launderer 28,500 lbs/day 55 Mouseno gallons per day (11nlermlttent lint) O COnllnuous(wn) �rM ONO Parameter Name Chromium Iron Zinc Nickel Cadmium parameter Numbs► 01034 01051 , 01092 01067 01027 valve 0.2 11.1 2.0 1.3) 0.04 *Continue from Page I........ IV-1 0po $65.704 rbli sect/en ceatslns I psis. • ' ' qe r , • FOR A4111sMeV oaf, � STANDARD FORM A —MUNICIPAL 111 -ITM SECTION 17. INDUSTRIAL WASTE CONTRIBUTION TO MUNICIPAL SYSTEM susm" a description of aaeh Wiper Industrial facility discharging to the munklpal•syslem, wlfq a separate faction IV for each facility dw.rip• lion, Indicate the a dlgll Standard Industrial Clatssllcallon (SIC) Coda for the Industry, Industry, Imajor product of raw mj1a1IIh 1hrn.• ono 0010ft par day), and the CharsclerillICS of Iwastewater dMcharpM, M flow IIn*d from tM IMwtrlal facwlly into the munklpN system, Con1n ; ibis III for standard manures of products or row malertals, (see Instrlrctlaine) 1' NWM canlrNitual poollty (sea Instructions) wrne asla Southern Gravure Services Nwnaor& street "llb 2406 North 23rd Street aW gills Wilmington County sate New Hanover state esla North Carolina !Is coda set/ 28405 !• P"sq standard IMustrul t0! �79 clewlfleeflen code Iw Inrl►ucllons) !. PrInellro Product K slaw units (sN Material (see Instructions) Tame If It product N7e Plating & Etching. of Prin i - - - cylinders now Material seas �• plsw Indicate the volume of water dllCharged Into the municipal Sys. asaa 5 lam In thousand ollons per day thousand Solon$ per day and whether this discharge 1s Inter. mlllenl Of continuous. 4"b ❑ Intefmlttent lint) lb continuous (eon) a. pntfaalment Provided Indlcala If aN Cf pretrealmenl Is provided prior 10 ~ ONs entering the munklpal system s. CharaalorlNlS, of Wla -$sap (w Instructions) parameter Name Iron Cadmium Lead Nickel Istl• �iamster Numper 01051 01027 01051 01067 valve ' 2.6 0.004 0.008• 0.008 *Continue on Page 2 ...... Zinc Silver 01092 0.07 01077 1.2 IV-1 SPO 445.701 !*Irspotless f11Nbf11a 1 I+IN. I troll A46AICV U8 '1 STANDARD FORM A-MUNICIPALI I 1171� SECTION N. INDUSTRIAL WASTE CONTRIBUTION TO MUNICIPAL SYSTEM sub"'" a drerlptlon of OKh WWOr Industrial facility discharging to Iha mumltlpM system, using a wp«alo section IV for aeeh IKlllly d0►cr�p• lion. Indicate the 4 digit Standard Industrial Claasl/lcallon ISiC) Coda log Ins Industry, In melpr p►oducl a raw metfor a the flow Ian wri sand gallon" par day), and the characteristics of Ins wealewal« dlsch«ged from the Ineuet0 1lof OrIIV duc IInto ns munklpN al, the f Consult .- 111 101 slanslard measures of prodircq or raw malertall. is" Instructional 1' Ma1M cenlroutlM psemy ("a Instructions) ' Name I dell, I Southern Gravure Services Numboroll, street City County state =M era !. primary standard Indust" Classification cc" (loop IMlrw lions) s. prinalpal Provost or aaw Material (see Instructions) preducl now Material 4. slew Indicate the volume of water discharged Into the munlclpal.sys. lem In thousand gallons pee day and WhOtri« Ihil discharge If Inter• mlltenl or continuous. s. pretreatment preawed Indicate It Prolfeafmonl Is provided prier 10 «1lering the municipal system s. CMreeNrisllos of Wastewater (w Instructions) Ns 4e7a Nye 4e4a 4046 Ns 2406 North 23rd Street Wilmington New Hanover North Carolina 22 8� .. 77++96 Unit (see Quantity Tym III Plating & Etching of Printi� cylinders 46W 5 -� theuMmd p11Me law dey ❑Inletmlllonl11111 ]ContlnuousIcon) ®rM QNe Name •"« BOD COD 400 aramet« TSS 0&G Number 00310 00340 00350 00556 � valve' 232 694 32 18 *Continue from Page 1 ....... 161 sp0 a45.704 Ph Chromium Copper 00400 01034 01042 8.1 0.01 0.09 n Me Seelig" Seaft a I! p de. • � 4 roll A6116CY Wr,1 STANDARD FORM A —MUNICIPAL SECTION Jr, INDUSTRIAL WASTE CONTRIBUTION TO MUNICIPAL SYSTEM iuMlN a dMrlptlon o1 Nth Major Industrial leclllly discharging to the munklpN system, wing a gpara(d sactlon I V ter Uaeh I1eI111Y OeK►ip• tlon, Indicate the . dlgll Standard Industrial Claselflcallon ISIC) Code to► 1M Induelry, In* malo Product w raw material. O h flow tin I ri end IIMIOns per deal, and Ih@. Characoduct ter rawtic$ of the wastewater ructions, from IM IndWIFIM I1eMlly Into IM muhkipat Wgtahf Conan :fee I11 IOr standard meNurN of prOduiq er raw malerlale, lsee Instructions, 1' Buie Comlrtb"" reelN Y, Ina Instructions) wane ( d@la Coca-Cola Bottlin Wo k Nwm*eri street city County Stela =M Code !• Mmary standard Industrial Clewllleallon Coca Sue Instructions) !. ►dndpp ►r*dual or now Material (eee Instructions) Product aft Material 1. rl@w Indicate the volume of water dbchareed Into the municipal sye• term In thousand gallons per day and whether this discharge h Infer• mlllent Or continuous, s. hetwatmonl hdMdad In@Icala II stralreafmdrnl Is provided prior to enterine the municipal system s• CmarMlarl.tNe'st wnfemglar (s" Instructions) . per.. e I Nama 4aa • r'i. Numb der Volvo r si Inc. 921 Princess Street _Wilmington New Hanover North Carolina 28401 — T r 2086 Units (see Tffipg fill Bottled Soft Drinks •Mr l�._�_ � F4 saw ...�_ 60 Ihouiand @all*me per day Intermittent lint) (3 continuous icon) jPres ONsi @ro eee.�oe IV•1 7 10 @*Golan G ilobislo d ratl*. DISCHARGE SERIAL NUMBER FOR AGENCY USE 14. Description of Influent and ENlwat (W instructions) :r > r Effluent Parameter and Code 214' < x> > cu c2) (3) (4) Flow (5) (6) (7) . Million gallons per day 50050 5.,824 5-824 3;,689 7,198 ontinuous - - pH i Units 00400 7.8 7.1 7/ 7 365 G Temperature (winter) a 74028 71 71 44 75 7/7 182 G ' Temperature (summer) I OF . 74027 82 82 61 :86 7/7 183 G Focal Streptococci Bacteria Number/100 ml 74654, (Provide If available) Feel Conform Bacteria Number/100 ml 74053 (Provide if available) 237 5/ 7 260 G Total CoUfofm Bacteria Number/100 ml 74056 (Provide if available) BOD 3-day' 00310 24 197 35 27 42 7hr Chemical Okypn Demand (COD) /7 365 CDR ms/I 24 00340 (Provide if ivails"ble) h r 413 104 60 126 1/7 52 r:nm OR Total Orpnic Carbon mc) no- 006b0 (Provide if a4litable) (Either analysis Is ne"tabb) atlorir+a—Total Residual - Mali 50060 _ 0.8 0.7' 0.9 7/1 365' G DISCHARGE SERIAL NUMEER , 002 OfteriptNn of InMuent and EfMwM (aM Instructions) (Continued) . •Influent Parameter and Code e e (1) (2) Total Solids MI/I 00500 524 385 3 Total Dissolved Solids mi/t 70300 401 369 3 ToW Suspended Solids mi/I 00530 124 16 Settleable Matter (Residue) 0os 054s 7.4 0,03 Ammonia (as N) mill 00610. (Provide if available) 18.3 15.5 1(jekmi Nitropn mill 00625 (Provide if waftble) Nitrate (as N) mill 00620 is rari� if araWblel Nitrite (u N) . 00613 (Provide if avail") Phosphorus Total (u P) mil! '.' 00665 (Provida If available) 5.1 3.4 'D lead OxyOn (DO) �� 00300 . �"•�"�j� l "2 }' 4 '^Ole 1' FOR AGENCY UZR1 2.3 Effluent 8> g (3) S (4) b (S) z� (6) a (7) 24 50 416 7/7 365 hr, cons 24 44 397 .7/7 365 hr omp 24 11 25 7/7 365 hr Com 0.1 7/7 365 hr 0.0 c om 24 12.2 .18.9 •1/7 52 hr cons -24 hr 6.3 1/7 52 cons 24 2 6,7 7/7 365 hr, COMP DISCHARGE S[AIAL NUM[[le ooa IS. AIMIIeeM Waaan ter catentkwMlee CneUt the boa next to eaeb wnmeter It 1111 ereeMtl In the et/ltgnl. (W IMIrtlenMe) POA AO[NCv Vf[ Parameter er Q Pvameter c (215) _ f(215) (315) R a Bromide 71870 Cobalt Thallium 01037 01059 Chloride 00940 X Chromium Titanium 01034 01152 Cyanide Copper Tin 00720 X 01042 X 1 01102 Fluoride Iron Zinc 00951 X 01045 X 01092 S ulOde 0u1nd Lead Algicides' 01051 X 74051 Aluminum 01105 X Manganese Chlorinated or is com ' pounds 01055 X 74052 X Antimony Mercury 01097 Od and grease 71900 X 00550 X Arsenic Molybdenum Pesticides' 01002 01062 74053 Beryllium Nickel Phenols 01012 0I067 32730 Barium 01007 Selenium Surfactants 0II47 38260 X Boron 01022 Silver Radioactivity' X 01077 X 74050 Cadmium 01027 'Provide gebifte eompoubd WA/or element In Item 17. if known_ Pest fungici mOn V es x andt emi ai Nmda, and rod<nikldu) mutt be reported m terms of the exceptable common nurser'Wifled in Acceptable Cam, mon Names and Oirmlool Names Jor Nee fntndient Sfatemrnr on Pesticide Labels, 2nd Edition, En. Orvnental Protection ASency, Werhlryton. D.C. ticide June 1972, M required by Subsectwn 162.7(b) of the ReSu4tlons for the Enforcement of the Fed" Ibeectidde, Fungicide, end D-C 2 250 Act. 11-7 OISCMAROE SERIAL NUMeaft oat 1f. 'IHM Controls Chock If the follow. Ing plant controls are available l for this discharge Alternate power Source for major Pumping facility Including those for collection system lift stNlons `, }[� APS Alarm for power or 04ulpment Ialhlra MLM 17. A" MOOM Intormation FOR AO[NCV Uf[ . �; ... I � •y+l'i ,+�:II I IVY' q :! , ,.lr( '�� '1�'t�br r: j�ll 4?'� 4��n 1' �` �">t �� i' . `;1. ?. $•� �i• A NEW it. H y� y qq tiAJJADM ujs Imp , Its WASTE ATER 'TREATMENT— - PLANT'. , OIL L I IIy / 1 � � i ,�• � coin l r i I •! � . P so I 15, •;; 1, .. F , I �� •ll � ;�! „ I I ' ' /�� \ j � � tit � , , s Imngton i�; • .i II 1 30 Tel EFFLUENT OUTFAwish \ J9EACH 4 1 ,. rv• 'y '� f rA#Ap i I*AV�. • rl II•I •. I �. � � �t;� r• ;1l1 �rrl �. 11� � ! r � ' I uti `��. '� T AM PC 13' � i. y , j i I � � U I .' �M. ,• � 1 . 7 � . I I• (V •�{ bb if' /a1r pia r �. PI '. SCALE' i� IRJ N i MIL► . • I � �• �'� bI b vr �fJ1 Iy, p :i I;�. ;r�;e i` ; �• .I �: ,� Location E: Ma :h p is � •� � � �� , ��: � ' � �,.:.. 7.7 57W 77I88W T7 tibVl:. ' icy 1 ' �:Si•�4.q.1�• �'� �`,�'�` „�� .��•• `• r. I � -. ��_. . I "1y 1 . �•� ' � ' 1. �f �, ' , �..i,� � . , � f �- fie' � 1 ,' 'r►•�•' C� ' 1• �• / 0"� Y,�ti• ' •.' 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J7�; ••1� , tl •n:.:,-.:� �` It -•`\, •� •.,.•-ty� ' �\ fit 1 , Aw 54 �''� sM;;: a 'is� ,� ;,�i •� [ 'Vk__L� I. ;' �f • ^+ '.i3 tI ,} ' d, I�• •,'•,•, �' ,, "gar'•— .,_ 11�� 1 �• _ � _ _ 1�('• ,ae� it �• �' ;�� ...,erg 3�Ct\�ti •�•� x v _ly ►� ' K r r�;� rg.a.,l. ,` /_ ,�I. �::`� �• �� ': " r 30" EFFLUENT OU TFA C�!_,'�' •;' f ?rF' �. , Q '�� 1 �� � �� � '' ,r r rAM � �.: a• 1,. a 1,ui V) ` ► i .i { tl. ' " `t,• ' t. 'rr it R _ �, 1 •S/ , '� /. ,:ti i I JJ"' � � a J F '•r . ,!e"' 1'1 ' �'A 1 11 1 I' r' I y .�•�r y,+' O ' r��;••ti� ,z I t_•4(11 1 , f '� —'� 'tee .F, ,, • - r '� � • ' 1 f 4e �•,. � � ills �, >� �� � 1 _'•�,; ;•' OLr 1� �',{ •>~s��� ^r^�F-CHA F�4�i 34 TDEG .1 14 MIN. 26�- `` ' ' ► ;, ' � �, .I 4A ,� L�Ir llf'1,R I►1' I �f "i`T'ii' if • . i n 4 3 LONG . 7 7 D ? �' �l '` `h l' 1 t �i(�'' 1'•' ( ' , f ' Z ':lt� .� �+ er'i,;�n j ur;lt'' �` ,It p• ' 4 i• -.1 x,. e :•� l,'t lJ .j :. n. ` ,� 1" rw• '; y1k:rF.���! 1".:.1i: SM' �� �_ .• `�-'.1; t� : `•! .i: '�; 1 , .t• r ���i.Z /.J ��:. i tK•• ' 1 ?'� Ir ,,,'�++ I ��,. •� y'' ' 111:lt;'I 1 1 � i ,`�• '• � _'.''y� � ` l J. "f ' yt ,. '.� • '1. ( ��•_� '••Y.� � 111:11 � � M T:.L ,• C/: j�,r. �'' ��{'ti�'tl'd�'1 � ?�: t•• /lr. `.� � - ,�T�'- li,�' 17y�� •,,;` �„� V�; • U / ''� �' - 1.' V B � • t;. yr• Ls � ; y . ,•O• .�;Y jyr� �' �.�^��^.MMVV1 �tll{{r N ON warA •v��s m/I •-•• ; >:,- „i�l` .� •�� •••�' ,.. ay•1�. ��.•':: '•�. � � �— .ill• ��'�•�''�• .1 'T,rQ. W. t 77_. R7W WIL.MINGTON 77 aaW 771 ���► NPDES PRETRFATMF;NT INFORMATION REQUE-ST FOPM g1010n-z FCILITY NAME: jype NPDES NO. NC00 I � ;REQUESTER: DATE: 7 / % / 9I RM ION : PEPMIT CONDITIONS COVERING PRFTRFATMFNI a 3 9.� 5 ` r � I 1 This facility has no 'JUs and should not have pretreatment language. This facility should; and/or is developing a pretreatment program. Please include the following conditions: This facility is currently implementing Please include the following conditions - Program Development Phase I due Phase II due Additional Conditions (attached) a pretr t program. Program Implementation Additional Conditions (attached) SIGNIFICANT INDUSTRIAL USERS' (SIUs) CONTRIBUTIONS S ICJ FLOW - TOTAL: oo % MGD 1 - COMPOSITION: TEXTILE: MGD 1 METAL FINISHING: 1 OTHER: , ,.,f On g.. 11&aV, : PS, f M® ' 1 r Ckuµ s.r Ann, COD MGD 1 1 PARAMETER 1 1 Cd Cr Cu Ni Pb Zn CN Phen 1 d!�-OtherM I RECEIVED: REVI&gED 1 BY: LOAD IN LBS/DAY r PERVaTIED 0,01 ► - - n � ryM .Z � �� 50 (100 ee 5, Q5' V,- 14, 00 �D --t-1 NC o Burlington Research RECRIVED F E B 1 1991 PERMITS & ENGINEERING Burlington Research, Inc. • P. O. Box 2481 • Rnrlington, NC. 27215 • Telephone 919-584-5564 Burlington Research Analytical Services Aquatic Bloossay Testing Aquatic TbxlcRy Reduction Evoluctions AATCC Testing Services NPDES Testing Remling & Data Hondling Services PMN Aquatic Bioassay Evdtuations January 16, 1991 Mr. Rick Pinter City'_,of,..: Wilmington.:. 2311 North 23rd Street,. Wilmington, NC 28465-,' Dear Rick: Accompanying this letter are APA Reports for analyses con- ducted- on the Northside and Southside-composite and. grab effluent samples received by BRI on -December 14.. .After..re- viewing -,.the,- reports',- sign, the last page = ( Page 9 of 9 )' and mail.two (2) completed.copies of each to: .Y Central ..Files Division'of,'Environmental Management . NC DEHN. P.O.'' . Box_,_27'6:87 Raleigh,. NC 27611 Thank you.. Please. call...,i'f you have -any: questions. URLINf;TON RESEARCH; INC. ;rI Richard A'. Iiehl Executive' Vide' President Director, Environmental Laboratories RAD/lc Enclosures: APA Reports - Northside WWTP. Southside WWTP Post Office Box 2481 615 Huffman Mill Road Tel. (919) 584-5564 Burlington, NC 27215 Y' ANNUAL POLLUTANT ANALYSIS MONITORING REQUIREMENT REPORTING FORM A I. FACILITY INFORMATION: NPDES Permit No: NC0023965 Discharge (Pipe) No: 001 Year: Facility Name: City of Wilmineton Class: IV County: New Hanover James A. Loughlin WWTP (Northside) Person(s) Collecting Samples: Kipp Glaizer. Dennis Hicks Analytical Laboratory: Burlington Research. Inc. (WO► 90-12-158) OCMS Library Size (number of chemicals catalogued): 42,222 II. SAMPLING: 24 hr composite for main sample / grab sample for purgeable fraction Date Sampled: (composite sample) Sampling begun (date, time): Wednesday. December 12 1990, 0530 hrs Sampling finished (data, time): Thursday. December 13, 1990, 0530 hrs Date and time sampled (grab sample): Thursday. December 13, 1990m 0500 hrs. a Approximata concentrations reported for Top Ten Peaks are based on the ratio of the unknown peak height to the peak height of the 40 ug/L internal standard: Peak Height of Unknown --------------------------------- Peak Height of Standard (40 ug/L) A response factor of 1.0 in assumed for all unknown compounds. Page 1 of 9 A. PURGEABLE (VOLATILE ORGANIC) FRACTION Number of chemicals detected in Fraction 10 Fraction STORET Number 84085 STORET Compound Number Detection Limit Target Concentration Detected GC/MS Confirmation? Yee/No 1. Pollutants to be analyzed for: (ug/L) (ug/L) 34210 Acrolein 100 BDL YES 34215 Acrylonitrile 100 BDL YES 34030 Benzene 5 BDL YES 32101 Bromodichloromethano 5 BDL YES 32104 Bromoform 5 BDL YES 34413 Bromomethans 10 BDL YES 32102 Carbon Tetrachloride 5 BDL YES 34301 Chlorobenzene 6 BI+!%<" YES 34311 Chloroethane 10 -BDL YES 34576 2-Chloroethyl vinyl ether 10 BDL YES 32106 Chloroform 5 BDL YES 34418 Chloromethans 10 BDL YES 32105 Dibromochloromethans 5 BDL YES 34496 1,1-Dichloroethane 5 BDL YE$ 34531 1,2-Dichloroethans 5 BDL YES --"-"' 34501 1,1-Dichloroethylene 5 BDL YES 34546 trans-1,2-Dichloroethylene 5 BDL YES 34541 1,2-Dichloropropane 6- BDL YES. 34704 cis 1,3-Dichloropropene 5 BDL YES 34699 trans 1,3-Dicloropropene 5 BDL YES 34371 Ethylbenzene 8 BDL YES 34423 Methylene chloride 5 BDL YES 34516 1,1,2,2-Tetrachloroethane 7 BDL YES 34475 Tetrachloroethylene 5 BDL YES 34010 Toluene 6 BDL YES 34506 1,1,1-Trichloroethane 5 BDL YES 34511 1,1,2-Trichloroothane 5 BDL. YES 39180 Trichloroethylene 5 BDL YES 34488 Trichlorofluromethans 10 BDL YES 39175 Vinyl chloride 10 BDL YES Page 2 of 9 STCRET Compound NUMBER Detection Limit Target Concentration Detected A roximats GC/MS Confirmation? Yea/No 2. OTHER PURGRABLES (up to 10 highest peaks): (ug/L) (ug/L) Alkyl Alkans 5 11 yen Alkyl Alkans 5 8 Yes Alkyl Alkans 5 a Yes Alkyl Alkane 5 9 Yes Alkyl Alcohol or Alkyl Alkene 5 31 Yee Oxide Sydrocarban 5 9 Yea Oxide Sydrocarbon 5 20 Yes Aldehyde or Alcohol 5 8 Yes Alkyl Alkans 5 6 Yes Alkyl Alkans 5 11 Yes B. ACID EXTRACTABLE FRACTION Number of chemicals detected in Fraction 4 Fraction STORES Number 45582 STORES Compound NUMBER Detection Limit Target Concentration Detected GC/PS Confirwtian? Yes/No 1. Pollutants to be analysed for: (us/(,) (us/L) 34452 4-Chloro-3-msthylphmol 10 BDL YES 34586 2-Chlorophmol 10 BDL YES 34601 2,4-Dichlorophmol 10 BDL YES 34606 3— 4661 — 2,4-Dimethylphenol 2,4-Dinitrophmol 10 50 BDL BDL YES YES 34657 2-lbthyl-4,6-dinitrophmol 24 BDL YES 34591 2-Nitrophmol 10 BDL YEN 34646 4-Nitrophmol 50 BDL YES 39032 Pentachlcrophenol 50 BDL YES 34694 Phanol 30 BDL YES --- 1 2,4,6-Trieh oro mo 30 B YES Page 3 of 9 STORET Compound NUMBER Detection Limit Target Concentration Detected (Approximate) GC/MS Confirmation? Yes/No 2. OTHER ACID EETRACTABLES up to I hest neeke): (ug/L) (ug/L) Aliphatic Carboxylic Acid 10.0 14 Yes Aliphatic Carboxylic Acid 10.0 104 Yes Aliphatic Carboxylic Acid 10.0 4.7 Yes Aliphatic Alcohol 10.0 16 Yea C. BASE/NEUTRAL FRACTION Number of chemicals detected in Fraction 4 Fraction STORET Number 45583 STORET Compound NUMBER Detection Limit Target Concentration Detected GC/MS Confirmation? Yes/No 1. Pollutants to be analysed for: (ug/L) (ug/L) 34205 Acenapthens 10 BDL YES 34200 Acenaphthylene 10 BDL YES 34220 Anthracena 10 BDL YES 39120 Bensidine 44 BDL YES 34526 Benin (a) enthracens 10 BDL YES 34247 Benzo (a) pyrene 10 BDL YES 34230 Benzo (b) fluoranthens 10 BDL YES 34521 Sense, (eh1) perylene 30 BDL YES 34242 Banco (k) fluoranthens 10 BDL YES 34278 Bis(2-chloroethoxy) methane 10 BDL YES 34273 Bis(2-chloroethyl) ether 10 BDL YES 34283 Bia(2-chloroisopropyl) ether 10 BDL YES 39100 Bis(2-athylhexyl) phtbalate 10 26.0 YES 34636 4-Bromophenyl phenyl ether 10 BDL YES 34292 Butyl benzyl phthalate 30 BDL YES 34581 2-Chloronaphthelene 10 BDL YES 34641 4-Chlorophenyl phenyl ether 30 BDL YES 34320 Chryssns 10 BDL YES Page 4 of 9 C. BASE/NEUTRAL FRACTION (Continued) Fraction STORET Number 45583 STORET Compound NUMBER Detection Limit Target Concentration Detected GC/MS Confirmation?. Yea/No 1. Pollutants to be analyzed for: (ug/L) (ug/L) 34556 Dibenzo (a,h) anthracene 10 BDL YES 34536 1,2-Dichlorobenzene 10 BDL YES 34566 1,3-Dichlorobenzene 10 BDL YES 34571 1,4-Dichlorobenzene 10 BDL YES 34631 3,3-Dichlorobenzidine 20 BDL YES 34336 Disthyl phthalate 10 BDL YES 34341 Dimetbyl phthalate 10 BDL YES 39110 Di-n-butyl phthalate 10 BDL YES 34611 2,4-Dinitrotoluene 10 BDL YES 34626• 2,6-Dinotrotoluens 10 BDL YES 34596 Di-n-octyl phthalate 10 BDL YES 34346 1,2-Dipheny1hydiazine 10 BDL YES 34376 Fluoranthene 10 BDL YES 34381 Fluorens 10 BDL YES 39700 Hexachlorobenzene 30 BDL YES 34391 Hexachlorobutadiene 10 BDL YES 34386 Hexachlorocyclopentadiene 10 BDL YES 34396 Hexachloroethans 10 BDL YES 34403 Indeno(1,2,3-cd) pyrene 10 BDL YES 34408 Isophorone 10 BDL YES 34696 Naphthalene 10 BDL YES 34447 Nitrobenzene 30 BDL YES 34438 N-nitradonimethylamine 10 BDL YES 34428 N-nitroso-di-n-propylamine 10 BDL YES 34433 N-nitrosodiphenylamine 10 BDL YES 34461 Phenenthrene 30 BDL YES 34469 Pyrens 10 BDL YES 34551 1,2,4-Tricblorobenzene 10 BDL YES Page 5 of 9 STORET Compound NUMBER Detection Limit Target Concentration Detected (Aooroxlmate) GC/MS Confirmation? Yes/No 2. OTHER BASE/NEUTRALS (up to 10 highest peaks): (ug/L) (ug/L) Oxide Hydrocarbon 30.0 15 Yes Oxide Hydrocarbon 10.0 67 Yes Oxide Hydra carbon 10.0 185 Yes D. ORGANOCHLORIDE PESTICIDES AND PCB's Number of chemicals detected in Fraction 0 Fraction STORET Number 00188 STORET Compound S@NER Detection Limit Target Concentration Detected GC/MS Confirmation? Yes/No 1. Pollutants to be analysed for: (ug/L) (ug/L) 39330 Aldrin 0.05 <0.25* NO 39337 alpha -BBC 0.05 <0.25* NO 39338 Bata-BHC 0.05 <0.25* NO 34259 Delta-BHC 0.05 <0.25* NO 39340 Gamma -BBC (Linden*) 0.05 <0.25* NO 39350 Chlordane 0.5 <0.25* NO 39310 4,4'-DDD 0.1 <0.25* NO 39320 4,4'-DDE 0.1 <0.25* NO 39300 4,4'-DDT 0.1 <0.25* NO 39560 Desaton 0.1 <2.50* NO 39380 Dieldrin 0.01 <0.25* NO 34361 Endosulfan I (alpha) 0.05 <0.25* NO 34356 Endosulfan II (beta) 0.1 <0.25* NO 34331 Endosulfan sulfate 0.1 <0.25* NO 39390 Endrin 0.01 <0.25* NO 34366 Endrin aldehyde 0.01 <0.25* NO 39410 Haptachlor 0.05 <0.25* NO Page 6 of 9 D. ORGANOCBLORIDE PESTICIDES AND PCB's (Continued) STORET Compound NUMBER Method Detection Limit Concentration Detected GC/MS Confirmation? Yea/No 1. Pollutants to be analyzed for: (ug/L) (ug/L) 39420 Heptachlor epoxide' 0.05 <0.25* NO 39480 Methoxychlor 0.5 <0.25* NO 39755 Mirex 0.06 <0.25* NO 39540 Parathion (ethyl) 0.6 <0.25* NO 39400 Toxaphens 1.0 <0.25* NO 34671 PCB 1016 0.5 <2.5 * NO 39488 PCB 1221 0.5 <2.5 * NO 39492. PCB 1232 0.5 <2.5 * NO ' 39496 PCB 1242 0.5 <2.5 * NO 39500 PCB 1248 0.5 <2.5 * NO 39504 PCB 1254 1.0 <2.5 * NO 39508 PCB 1260 1.0 <2.5 * NO * 2. OTHER PESTICIDES (Up to 10 highest peeks) Minimum Quantitation Limit NONE E. HERBICIDES' Number•of chemicals detected in Fraction 0 Fraction STORET Number 00148 STORET Compound NUMBER Method • Detection Limit Concentration Detected GC/MS Confirmation? Yee/No 1. Pollutants to be analyzed for: (ug/L) (ug/L) 39730 2,4-D 50 BDL NO 39045 Silvex 50 BDL NO 39740 2,4,5-T 5 BDL NO Page 7 of 9 STORET Compound NUMBER Method Detection Limit Concentration Detected GC/MS Confirmation? You/No 2. OTHER BgRBICIDES (Up to 30 highest(Approximate) t peeks) (uE/L) (uE/L) NONE F. METALS AND OTHER CHEMICALS Number of Metals and Other Chemicals (as listed below) detected in Semple 9 Fraction STORET Number 78240 Page 8 of 9 Analytical Laboratory Representatives• ateven G. Yocklovich Director, Chromatography Laboratories Richard A. Diehl Director, Environmental Laboratories Date t r-, 1 Facility operator in Responsible Charge (ORCj: ✓" i I n� 4 f% (�(j�, �/ I certify that this report Is accurate and comple a to the best of knowledge: Signed: ! �• Date: Z Page 9 of 9 Tooin3 Report for DFTPP File W7M226 Date ZAQW-70 Timw 072 06, 0-D WaPS 30WIM: SZE STS Aaw3 ReqUiroMent REF, Ion Found Pass/Fail 30-6c% 178 51.1 F 68 jz% 69 1.9 P 7a V:% 67 OA F: i:7 40-W% 173 47.7 P 11 i 03 0.6 F NO KY. 150.0 P 117 5-?% 1?S 7.3 it Z-3, M-sc% 15W Z3.6 P, .36Z vix 198 2.3. P n7; 441 441/443.X, 1.0 0.7 F ,442 >40% 198 S7.5 P 443 17-23% 442 19.6 11=1 '} Burlington J Research Post Office Box 2481 • 615 Huffman MITI Road • (919) 584-5564 • Burlington, NC 27215 • Fax N (919) 584.5564 Ext. 202 CHAIN OF CUSTODY RECORD CLIENT. oP W IK, A�ft,34 Facility/Site Z3AMeS A LovahliN WU?TP CIY6) Sampler (Print) 0-e n n; S -H �, c k S Sampler. (Signature) L4V�o M,A/rk CONTACT PERSON: ?t"-K ?nel2 Phone Number. 9i5-3141- r11?q I Purchase Order #i: Oil- I4a941 SAMPLE ID SAMPLE COLLECTION SAMPLE TYPE NO. OF COW TAINERS SENT ANALYSES REQUIRED COMPOSITE HAND AUTO GRAB DATE TIME STARTED DATE TIME ENDED NMAFS 1* a.9 /41,01,10 S' AA 13 3: avo� ✓ �a "� Yo ,4t0i9 FOR CLIENT USE: Reling shed by: (SI natur) Recely d b : I ature) DatelTime /,2•13090 1:30 AX) Shipped by: ig elute) LReIdly: �Sr DatelTime l :30 AM Meth hlpment: V ^ L ff� n R FOR LAB USE ONLY: Received In Lab FROM: (Signature) Rece ed for Lab by: (Signature) Date I,m/e _. I ��► Method of Shipment: UPS White —ORIGINAL- CLIENT REPORT Canary —LABORATORY Pink —ACCOUNTING GaIdownd—AMNewi cnnceu1:1JT