WQ0001026_Residual Annual Report 2015_20160205

MA
esources, Inc.
RECE!�r � n 1 P! r, � � QJ O R
February 2, 2016
e,1r''Ste`k5 f�f. E e'
DENR/Water Quality Section FFR 0 5 2016
Non -Discharge Compliance Unit
1617 Mail Service Center r
Raleigh, NC 27699-1617
Re: 2015 Annual Report - Washington
Treatment and Land Application of Residuals
Permit No. WQ0001026
Dear Sir or Madam:
Enclosed are three copies of the 2015 Annual Report for the above referenced land
application permit.
FEB - 5 2016
Non-D i;charge
Permitting Unit
During 2015 EMA Resources, Inc. land applied 203.39 dry tons of wastewater residuals
to 113 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
dt;440�
Director of Technical Services
Brent collinskemaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Road — Mocksville, NC 27028

City of Washington
2015 Annual Report
Residuals Land Application
Permit No. WQ0001026
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax 336*751.1442
755 Yadkinville Rd — Mocksville, NC 27028
RECEI`�ED��,1rnrrr DWR
FEB - 5 201-0
Non-Discharg?
Permitting unit

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001026
County: : Beaufort County, NC
Facility Name (as shown on permit):
Land Application Operator:
Year: 2015
City of Washington
EN IA Resources Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
R1 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the pe it:
54
Total number of fields utilized for land application during the year:
5
Total amount of dry tons applied during the year for all application sites:
203.39
Total number of acres utilizes for land application during the year:
113
-Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2015 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Adam Waters - Water Resources Superintendent
Permittee Name and Title (type or print)
11ZL —26-16
Signature of Permittee Date
Z: 1/11/2016
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0001026 Laboratory: 1)
Facility Name: City of Washington 2)
Residual Source WQ # or NCO020648 3)
NPDES #: 4)
WWTP Name: Washington WWTP 5)
Residual Analvcic Dntn
A&L Laboratories
Parameter
(mg/kg)
Conc.
Limit
(mg/kga
Sample or Composite Date
4/29/15
5/21/15
10/12/15
12/17/15
Percent Solids (%)
NA
3.88
3.75
4.15
4.04
Arsenic
75
6
5
6
5
Cadmium
85
2
2
3
2
Copper
4,300
294
280
290
207
Chromium
NA
57
51
44
54
Lead
840
30
39
35
20
Mercury
57
1.5
1.5
1.7
1.2
Molybdenum
75
6
6
7
11
Nickel
420
27
29
24
29
Selenium
100
5
5
5
5
Zinc
7,500
730
708
800
610
Total Phosphorus
NA
23600
21800
17800
22100
TKN
NA
50800
51500
32000
42800
Ammonia -Nitrogen
NA
5930
6130
6750
6680
Nitrate and Nitrite
NA
2
2
2
2
r or surrace aisposai racnities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
r,
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0001026
Laboratory: 1)
Facility Name:
City of Washington
2)
Residual Source
NCO020648
3)
NPDES # or WQ#:
4)
WWTP Name:
Washington WWTP
5)
Residual Analvsis Data
A&L Laboratories
Parameter
g_•
Sample or Composite Date
®®®Potassium
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Z L--> - f c�
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Washington Total Dry Tons Applied (Annual):
termit #: WQ0001026 Cation Exchange Capacity (non 503 only):
erator: Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
".cres Used: 16.5 Acres Permitted: 16.5 Site #: BF210 Field #:
30.11
CrB
residual
Analysis Data
(Heavy
Metals and Total Phosphorus
use mg/kg,
% Solids use
Raw Percent #):
Sample or
Com-
posite
Date
q2
5/21/15
12/17/15
3
L 4
1 51
L6J7
8
9
10
11
12
o Solids
3.75
4.04
Arsenic
5
5
Cadmium
2
2
�opper
280
207
c:tiromiun
51
54
Lead
39
20
Qercury
1.5
1.2
Molyb-
denum
6
11
Nickel
29
29
selenium
5
5
Zinc
708
610
Total
Phos-
nhorus
21800
22100
nnual
Heavy Metal Field Loadings
(Calculated in lbs/acre):
Total
nT/Ac./
App.
Event
1
0.43
2
1.39
3
4
5
6
7
8
9
10
11
12
o
14
Arsenic
0.004
0.014
0.000 1
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
1 0.018
admium
0.002
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.241
0.577
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.818
'' romiurn
0.044
0.151
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.195
Lead
0.034
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.089
Mercury
0.001
0.003
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
'✓Iolyb-
ienum
0.005
0.031
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Nickel
0.025
0.081
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.106
0?1enium
0.004
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.018
Zinc
0.610
1.701 1
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.311
Total
Phos-
)horns
18.792
61.615
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
80.406
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
im aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/11 /2016
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington WQ Permit #: WQ0001026 Field #: 1 Acres Utilized:
Hunter Roost Farms Annual Dry Tons Applied: 30.11 Site #: BF210 Acres Permitted:
Operator: Hunter Roost Farms
Crop 1 Name: Small Grain
Predominant Soil Series: CrB
Crop 1 Max. PAN: 93 Crop 2 Name:
Cation Exchange Capacity (non 503):
Small Grain Crop 2 Max. PAN:
16.5
16.5
0
50
°
y o
c�
Q
Volume applied
PP
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
o
0
cc
� o
oa m
o
n �
* S
C
7
w -�
"=
* =.
* 0
TKN
mg/kg
Z 9
o �
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of CropType
yp
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/19
45500
3.75
0.431
Washington
D
<.5"
S
0.5
0.3
51500
6130
2
14.384
NA
SG
12/14
45500
4.04
0.465
Washington
D
<.5"
S
0.5
0.3
42800
6680
2
Na '"
13.173
SG
12/15
52000
4.04
0.531
Washington
D
<.5"
S
0.5
0.3
42800
6680
2
Na
15.055
SG
12/16
39000
4.04
_ 0.398
Washington
D
<.5"
S
0.5
0.3
42800
6680
2
Na '
11.291
SG
0.000
0.000
0.000 `
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
-0.000
0.000 -
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM
FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTAL&I
01
182000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
14.38a
39.519
Lime Applied
Annual lbs/acre
0.018
0
0.018 1
36
0.007
0
0.007
34
0.818
0
0.818
1338
: 0.195
0
0.195
0.089
0
1- 0.089
267
0.005
0
0.005 '1
15
0.036
0
0.036
0.106
0
1 0.106
374
" 0.018
0
0.018
89
2.311
0
2.311
2498
80.406 ::
Date
lbs/ac
Prior Years Cumulative lbs/ac
1.00D
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1st/2nd Crop
93 50
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2016 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
acility Name: City of Washington Total Dry Tons Applied (Annual):
ermit #: WQ0001026 Cation Exchange Capacity (non 503 only):
Operator: Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
.ores Used: 27.5 Acres Permitted: 27.5 Site #: BF210 Field #:
20.82
GoA
2
_residual
Analysis Data
(Heavy
Metals and Total Phosphorus
use mg/kg,
% Solids use
Raw Percent #):
Sample or
Com-
Iposite
Date
1 1
12/17/15
2
3j
L 4
5
6
7
8
9
10
11
12
o Solids
4.04
Arsenic
5
2
kadmium
opper
207
Chromiur
54
Lead
20
4ercury
1.2
I Molyb-
denum
11
Nickel
29
Selenium
5
Zinc
610
Total
Phos-
horus
22100
nnual
Heavy Metal Field Loadings
(Calculated in lbs/acre):
ITotal
')T/Ac./
App .
Event
1
0.76
2
3
L4j
5
6 1
L_7j8j
L_9j
10
11 j
12
c
"
Arsenic
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
admium
0.003
0.000
0.000 1
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.003
Copper
0.313
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.313
irornium
0.082
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.082
Lead
0.030
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Oolyb-
Jenum
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Nickel
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
eleniurn
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Zinc
0.924
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.924
ITotal
Phos-
chorus
33.459
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
33.459
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/11/2016
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington WQ Permit #: WQ0001026 Field #: 2 Acres Utilized:
Hunter Roost Farms Annual Dry Tons Applied: 20.82 Site #: BF210 Acres Permitted:
Hunter Roost Farms Predominant Soil Series: GoA Cation Exchange Capacity (non 503):
Crop 1 Name: Small Grain Crop 1 Max. PAN: 120 Crop 2 Name: Small Grain Crop 2 Max. PAN:
27.5
27.5
0
50
°
a) o
Q
Volume applied
pP
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
PP p
Acre
(Dry Tons/AC)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
Y
o
o� w
*
o
�,
�
w "
*
TKN
mg/kg
z >
�o o
�, �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre )
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
12/16
84500
1 4.04
0.518
Washington
D
<.5"
S
0.5
0.3
42800
6680
2
14.679
NA
SG
12/17
39000
4.04
0.239
Washington
D
<.5"
S
0.5
0.3
42800
6680
2
6.775
NA `>
SG
0000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 :
0.000
0.000
0.000
0.000
0.000
0.000
0.000'
0.000
0.000
0.000'
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 `
'0.000
0
0
0.000
Residuals Applications totals on FORM
FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
Of
123500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
I P
21.453''
0.000`
Lime Applied
Annuallbs/acre
0.008
0
0.008
36
0.003
0
0.003
34
0.313
0
0.313
1338
0.082
0
0.082
0.030
0
0.030
267
0.002-
0
0.002
15
0.017
0
0.017
0.044
0
0.044
374
0.008
0
0.008
89
0.924
0
0.924
2498
33.459 ::
............................
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2n Cro
p o
P
120 - 50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2016 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
ermit #:
Operator:
'.cres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
16 Acres Permitted:
16
Site #: BF210 Field #:
59.97
Ra
_residual
Analysis Data
(Heavy
Metals and Total Phosphorus
use mg/kg, % Solids use
Raw Percent #):
Sample or
1
2 j
3 j
L4]51
L6 J
7
8
9
10
11
12
Com-
5/21/15
Iposite
Date
'o Solids
3.75
Arsenic
5
Cadmium
2
Copper
280
Chromium
51
Lead
39
✓tercury
1.5
Molyb-
I
6
denum
Nickel
29
Selenium
5
Zinc
708
Total
Phos-
21800
phorus
nnual
Heavy Metal Field Loadings
(Calculated in lbs/acre):
Total
1
L2
3
4
5
6
7
8
9
10
11
12
')T/Ac./
o
App.
Event
3.75
Arsenic
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
admium
0.015
0.000
0.000 1
0.000
0.000
0.000 1
0.000
0.000
0.000 1
0.000
0.000
0.000 1
0.015
Copper
2.099
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.099
^iiromium
0.382
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.382
Lead
0.292
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.292
Mercury
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
-Aolyb-
0.045
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.045
lenum
Nickel
0.217
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.217
;lenium
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Zinc
5.307
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.307
Total
Phos-
163.413
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
163.413
)horus
"t certifv. under Denaltv of
law. that this document was nrenared under my direetinn
nr cnnervicinn in neenrdane,,
---ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
im aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z-z 1 / 11 /2016
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington WQ Permit #: WQ0001026 Field #: 5 Acres Utilized:
Land Owner: Hunter Roost Farms Annual Dry Tons Applied: 59.97 Site #: BF210 Acres Permitted:
Operator: Hunter Roost Farms Predominant Soil Series: Ra Cation Exchange Capacity (non 503):
Crop 1 Name: Bermuda -Pasture Crop I Max. PAN: 145 Crop 2 Name: Crop 2 Max. PAN:
16
16
0
�
° y
°
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
NPDES #, W #,
( Q
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry'
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
Y
a �
o w
a -•
*
o
7y ?:
N'
*
o'
�
4
w
*
* "
�
TKN
mg/kg
z Y
o
c°Qo
w
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/17
58500
3.75
0.572
Washington
D
<.5"
S
0.5
0.3
51500
6130
2
19.071
NA
Bermuda
5/18
234000
3.75
2.287
Washington
D
<.5"
S
0.5
0.3
51500
6130
2
76.285
NA
Bermuda
5/19
91000
3.75
0.889
Washington
D
<.5"
S
0.5
0.3
51500
6130
2
29.666
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000_
0.000 -
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 -'
0.000
0.000
0.000
0.000-'
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000'
0.000
TOTALS:
01
383500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
I 125.022
0.000 `
Lime Applied
Annual lbs/acre
0.037
0.015
2.099
0.382
0.292
0.011 '
0.045'
0.217
0.037
5.307
163.413
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.037
0.015 `
2.099 '
_0.382
0.292
0.011
0.045
0.2.17
0.037
5.307
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
374
1 89
1 2498
Permit PAN Limit 1st/2nd Crop
145
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2016 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
ermit #:
Operator:
".cres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
27.5 Acres Permitted: 27.5 Site #: BF210 Field #:
40.65
GoA
12
residual
Analysis
Data
(Heavy Metals and Total Phosphorus
use mg/kg, % Solids use
Raw Percent #):
Sample or
1
2
3
4
5
6
7
8
911
11
12
Com-
5/21/15
posite
Date
6 Solids
3.75
Arsenic
5
Cadmium
2
�opper
280
lChromiurn
51
Lead
39
Mercury
1.5
Molyb-
I
6
Jenum
Nickel
29
Selenium
5
Zinc
708
Total
IPhos-
21800
nhorus
nnual
Heavy
Metal Field Loadings
(Calculated in lbs/acre):
Total
1
2
3
4
5
6
L7
8
9
10
11
12
r)T/Ac./
p
App.
Event
1.48
Arsenic
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
admium
0.006
0.000
0.000 1
0.000
0.000
0.000 1
0.000
0.000
0.000
1 0.000
0.000
0.000 1
0.006
Copper
0.828
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.828
`-romiun
0.151
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.151
Lead
0.115
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.115
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
'Molyb-
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
lenum
Nickel
0.086
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.086
0,leniun
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Zinc
2.093
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.093
Total
Phos-
64.441
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
64.441
)horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
---ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
im aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z; fG;: ; 1/11/2016
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington WQ Permit #: WQ0001026 Field #: 12 Acres Utilized:
Hunter Roost Farms Annual Dry Tons Applied: 40.65 Site #: BF210 Acres Permitted:
Hunter Roost Farms Predominant Soil Series: GoA Cation Exchange Capacity (non 503):
Crop 1 Name: Small Grain Crop 1 Max. PAN: 120 Cron 2 Name: Cron 2 Max_ PAN -
27.5
27.5
0
0 =
°
V o
c�
Q
Volume applied
PP
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
A hed er
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
Y
4 ,�°
a o
�
C
o
�y
_
°
* N
0
;�
?3 `.
�
0
TKN
mg/kg
y
z >
o
°q °
2.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
Ibs/acre
( )
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/16
1
78000
3.75
0.444
Washington
D
<.5"
S
0.5
0.3
51500
6130
2
14.795
NA
SG
5/17
182000
3.75
1.035
Washington
D
<.5"
S
0.5
0.3
51500
6130
2
34.521
NA
SG
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM
FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
260000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
49.315
0.000
Lime Applied
Annual Ibs/acre
0.015
0
0.015
36
0.006
0
0.006
34
0.828
0
0.828
1338
0.151
0
0.151
0.115
0
0.115
267
0.004
0
0.004
15
0.018
0
0.018
0.086
0
0.086
374
0.015
0
0.015
89
2.093
0
2.093
2498
64441 :::: :: ....., .
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
120
--i certjty, unaer penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2016 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Washington Total Dry Tons Applied (Annual):
ermit #: WQ0001026 Cation Exchange Capacity (non 503 only):
Operator: Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
ores Used: 25.5 Acres Permitted: 25.5 Site #: BF210 Field #:
51.84
CrA
16
_residual
Analysis Data
(Heavy
Metals and Total Phosphorus
use mg/kg,
% Solids use
Raw Percent #):
sample or
1 1
2
3
4
5
L 6
7
8
9
10
11
12
Com-
5/21/15
posite
Date
o Solids
3.75
Arsenic
5
cadmium
2
Copper
280
lChromium
51
Lead
39
✓lercury
1.5
' Molyb-
6
denum
Nickel
29
Selenium
5
Zinc
708
Total
Phos-
21800
horus
,nnual
Heavy Metal Field Loadings
(Calculated in lbs/acre):
Total
F 1
2
3
4
5
6
71
L-81
9
10
11
12
17T/Ac./
H
0
App.
Event
2.03
Arsenic
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
.admium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
1.138
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.138
1-hromium
0.207
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.207
Lead
0.159
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.159
Mercury
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
denum
denum
Nickel
0.118
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.118
".elenium
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Zinc
2.879
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
2.879
Total
Phos-
88.639
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
88.639
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
7ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z./ 1/11/2016
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington WQ Permit #: WQ0001026 Field #: 16 Acres Utilized:
Hunter Roost Farms Annual Dry Tons Applied: 51.84 Site #: BF210 Acres Permitted:
Hunter Roost Farms Predominant Soil Series: C rA Cation Exchange Capacity (non 5031:
Crop 1 Name: Small Grain
Crop 1 Max. PAN: 95
Crop 2 Name:
Crop 2 Max. PAN:
25.5
25.5
0
y o(Dry,5
Q
Volume applied
pp
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., AnimalHrs.
Waste, etc)
Soil
Cond.
Wet,
Moist)
Precip.
Past 24
inches
a
F �
�.
o� w
o
o
77
m �
* �'
C
CD E
* N•
w
TKN
mg/kg
Z Y
� °
� P.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of CropType
yp
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5115
208000
3.75
1.276
Washington
D
<.5"
S
0.5
0.3
51500
6130
2
42.547
NA
SG
5/16
123500
3.75
0.757
Washington
D
<.5"
S
0.5
0.3
51500
6130
2
25.262
NA
SG
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0;000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM
FSF supp ( attach FORM FSF supp
to this for
0.000
0.000
TOTALS:
01
331500
:::::::::::::
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
67.809 1
0.000
Lime Applied
Annual lbs/acre
0.020 0.008s 1.138 0.207 0.159 0.006 - 0.024 0.118 0.020 2.879 88.639 ::
0 0 0 0 0 0 0 0 0 0
0.020 0.008 1.138 0.207 -0.159 0.006 0.024 0.118 0.020 2.879
36 34 1 1338 1 267 1 15 1 374 1 89 1 2498
95
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2016 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Page: i of 2
Report Number: 15-120-0204
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 61685
Sample Id: WASHINGTON NC WWTP
L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastem.com
Project: WASHINGTON,NC
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/29/2015 10:00:00
Date Received: 04/30/2015 00:00
Date Reported: 05/05/2015
Total Solids *
3.88
38800
100.0
JM
04/30/2015 14:44
SM-2540G
Moisture *
96.12
100.0
JM
04/30/2015 14:44
SM-2540G
Total Kjeldahl Nitrogen
5.08
50800
10.0
JM
05/01/2015 08:55
SM-4500-NH3C-TKN
Total Phosphorus
2.36
23600
100
KM
05/01/2015 12:11
SW 6010C
Total Potassium
0.24
2400
100
KM
05/01/2015 12:11
SW 6010C
Total Sulfur
0.77
7670
100
KM
05/01/2015 12:11
SW 6010C
Total Calcium
2.09
20900
100
KM
05/01/2015 12:11
SW 6010C
Total Magnesium
0.24
2420
100
KM
05/01/2015 12:11
SW 6010C
Total Sodium
0.22
2200
100
KM
05/01/2015 12:11
SW 6010C
Total Iron
47500
100
KM
05/01/2015 12:11
SW 6010C
Total Aluminum
34000
100
KM
05/01/2015 12:11
SW 6010C
Total Manganese
687
5
KM
05/01/2015 12:11
SW 6010C
Total Copper
294
5
KM
05/01/2015 12:11
SW 6010C
Total Zinc
730
5
KM
05/01/2015 12:11
SW 6010C
Ammonia Nitrogen
0.59
5930
10.0
JM
05/01/2015 08:55
SM-4500-NH3C
Organic N
4.49
44870
10.0
05/01/2015 08:55
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
05/04/2015 09:30
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
05/01/2015 12:11
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. nor may any reference be made
to the work, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining ourprior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-120-0204
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 61685
Sample Id: WASHINGTON NC WWTP
L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-WS
wwwaleastern.com
Project: WASHINGTON,NC
NC CERT#257
REPORT OFANALYSIS Date Sampled: 4/29/2015 10:00:00
Date Received: 04/30/2015 00:00
Date Reported: 05/05/2015
Total Chromium
57
5
KM
05/01/2015 12:11
SW 6010C
Total Nickel
27
5
KM
05/01/2015 12:11
SW 6010C
Total Lead
30
5
KM
05/01/2015 12:11
SW 6010C
Total Arsenic
6.0
3.0
KM
05/01/2015 12:11
SW 6010C
Total Mercury
1.5
0.4
KM
05/04/2015 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
05/01/2015 12:11
SW 6010C
pH (Standard Units) *
7.46
2.00
JM
05/01/2015 08:55
SW-9045D
Total Volatile Solids
57.00 570000
100.0
JM
04/30/2015 14:44
SM-2540G
Total Molybdenum
6
5
KM
05/01/2015 12:11
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

BIOSOUDS SAMPLE TRH NSMI1 . `• %+n.-rr � r,T crrnr�v
_
m_
ABcL Eastern II��NI�i�NIi�NI�NIN N 15-12"204
7621 Whitepine Road Richmond VA 23237 Tel: 804 -0t32,1
�A.�II�I���II�
EMA RESOURCES INC 04 30-2015
Customer Informati+ WASHINr3TON,NC 13:41:54
w, Submittec{ By
EMA Resotilrces Inc EMA Resources Inc
755 Yadkinville Rd
755 Yadliinville Rd
Mockwipe, NC 27028 Mocksville, NC 27028
Project
_ Sample Info 6tan
I_ab Number
Collect on Information
—
Container Information
PlEase Check Desired Test;
Sample Ip
(Lab Use
—
e
Only)
Type
Date
7m1e
Number
or Battles
Type
Volume
SL1
SL2
603
Metals
Nitrogen
Series
PHFWE
A0
ci
Volatile
Solids
others
�e
Grab
✓composite
�/,%aQ/s'
)�:on)TA
i
Glass
cz
t
y/
✓
Lo1
_ Grab
Blass
--- oz
— Composite
— Plastic
._pint
— Grab
Glass
— oa
-- Composite
`plastic
--pint
t
— Grab
Glass
--- dz
Comp�ite
Plastic
-----pint
t
,�,,.. ,..-
frau ca rwrl AN
c.- L:l ► W
�" t?ei l`lnsk�uct orts or Remarks
L1. Total Solids (Moisture) Total Kleldahl Nitiogen, Phosphonrs and Potassium
S1,2; Basie'Pest SL t plus Suitor, Calcium, Magnesium,Sodiuru, Iron, Aluminum, Manganese, Copper And Zinc
603 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc included in St2)
Nitrogen Scries: Total Kicidahi, Ammonium, Nitrate & Organic Nitrogen,
CCE. Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)

Page: 1 of 2
Report Number: 15-142-0204
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 62107
Sample Id: WASHINGTON NC WWTP
L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: WASHINGTON,NC
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 5/21/2015 14:00:00
Date Received: 05/22/2015 00:00
Date Reported: 05/28/2015
Total Solids "
3.75
37500
100.0
JM
05/26/2015 09:24
SM-254OG
Moisture `
96.25
100.0
JM
05/26/2015 09:24
SM-2540G
Total Kjeldahl Nitrogen
5.15
51500
10.0
JM
05/26/2015 09:04
SM-4500-NH3C-TKN
Total Phosphorus
2.18
21800
100
KM
05/26/2015 14:54
SW 6010C
Total Potassium
0.24
2360
100
KM
05/26/2015 14:54
SW 6010C
Total Sulfur
0.75
7470
100
KM
05/26/2015 14:54
SW 6010C
Total Calcium
1.88
18800
100
KM
05/26/2015 14:54
SW 6010C
Total Magnesium
0.23
2320
100
KM
05/26/2015 14:54
SW 6010C
Total Sodium
0.20
1960
100
KM
05/26/2015 14:54
SW 6010C
Total Iron
46200
100
KM
05/26/2015 14:54
SW 6010C
Total Aluminum
34300
100
KM
05/26/2015 14:54
SW 6010C
Total Manganese
669
5
KM
05/26/2015 14:54
SW 6010C
Total Copper
280
5
KM
05/26/2015 14:54
SW 6010C
Total Zinc
708
5
KM
05/26/2015 14:54
SW 6010C
Ammonia Nitrogen
0.61
6130
10.0
JM
05/26/2015 09:04
SM-4500-NH3C
Organic N
4.54
45370
10.0
05/26/2015 09:04
CALCULATION
Nitrate+ N itrite-N
<2.00
2.00
JM
05/27/2015 08:50
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
05/26/2015 14:54
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or art nor ma an reference be made
p Y P part, Y Y
to the work, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining ourprior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-142-0204
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 62107
Sample Id: WASHINGTON NC WWTP
Total Chromium
Total Nickel
Total Lead
Total Arsenic
Total Mercury
Total Selenium
pH (Standard Units)
Total Volatile Solids
Total Molybdenum
L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastem.com
Project: WASHINGTON,NC
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 5/21/2015 14:00:00
Date Received: 05/22/2015 00:00
Date Reported: 05/28/2015
51
5
KM
05/26/2015 14:54
SW 6010C
29
5
KM
05/26/2015 14:54
SW 6010C
39
5
KM
05/26/2015 14:54
SW 6010C
5.0
3.0
KM
05/26/2015 14:54
SW 6010C
1.5
0.4
KM
05/26/2015 09:00
SW-7471 B
<5.0
5.0
KM
05/26/2015 14:54
SW 6010C
7.42
2.00
JM
05/26/2015 09:04
SW-9045D
56,52 565200
100.0
JM
05/26/2015 09:24
SM-2540G
6
5
KM
05/26/2015 14:54
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

B10SOUDS S A-MPLE'FRANSMITTA w- A " F f-Ni, riT I­0rt`i-1V-%%,-
AL A&L Easterr I NI Il IIIIH 15-142-0204
7621 Whiwpine. Road Richmond VA 23217 Tel-, 80 05-2248245
4015
EMARESOURMS INC 14:0812
164� WASHINGTONAG
Customer
Submitted By AV.: 01111111101 F, I
ENIA Resources Inc EMA Resources Inc
755 Yadkinville Rd 755 Yadkinville Rd
Mocksvifle, NC 27028 Mocksvdlcy NC 27028
PmjeCt
JV
Account #
Sample Information
Lab Number
Colk-ction Information
Container Information
Please Check Desired'i-csts
Sam[Ap ID
(Lab Use
Only)
Type
Date
TKTe
Number
Pe
Type
Volume
SI-1
9
3L9
—
503
Nitrogen
Pill
GGE
Ag
Cl
Volatile
1,
Other.
of Battles
Metals
Series
Solids
ez W
---,-Grab
cornposlw
"16
!ilo
"'v piot
Glass
G
0z
/
V/
L
t
Grab
Glass
oz
Composite,
Plastic
---pint
Grab
Glass
02
Composite
plastic
_____pint
at
Grab
Glass
— oz
Composite
Flastir,
____pint
at
WUi '`di C'W IL 14q10, 4vik%ETg'WMI WRXFtYMW W-' :v -.0 vr4 o***
6: �#,
SLI - Total Solids (moisture)'Tofal Kjeldahl Nitrogen, Phosphorus and Potassium
SL2. BAsic Tust SLI plus Sulfur, Calciurn, Magn*,Sh1rnSodiWn, Iron, Aluminum, Manganese, Copper And Zino
603 Metals. Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, NicW, Selenium.
(Copper & Zino included In SL2)
Nitrogen Series- J'otat fjeldahl, Ammonium, Nitrate & Organic Nitrogen.
CCE. Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)

r
Page: 1 of 2
Report Number: 15-286-0200
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 64707
Sample Id: WASHINGTON WWTP
(2)
Waypoi nt_M
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: WASHINGTON NC
INC CERT# 257
REPORT OF ANALYSIS Date Sampled: 10/12/2015 09:15:00
Date Received: 10/13/2015 00:00
Date Reported: 10/19/2015
Total Solids
4.15
41500
100.0
JM
10/13/2015 15:00
SM-2540G
Moisture *
95.85
100.0
JM
10/13/2015 15:00
SM-2540G
Total Kjeldahl Nitrogen
3.20
32000
10.0
JM
10/14/2015 08:35
SM-4500-NH3C-TKN
Total Phosphorus
1.78
17800
100
KM
10/15/2015 13:05
SW 6010C
Total Potassium
0.22
2190
100
KM
10/15/2015 13:05
SW 6010C
Total Sulfur
0.69
6910
100
KM
10/15/2015 13:05
SW 6010C
Total Calcium
1.60
16000
100
KM
10/15/2015 13:05
SW 6010C
Total Magnesium
0.27
2690
100
KM
10/15/2015 13:05
SW 6010C
Total Sodium
0.20
1960
100
KM
10/15/2015 13:05
SW 6010C
Total Iron
93800
100
KM
10/15/2015 13:05
SW 6010C
Total Aluminum
39800
100
KM
10/15/2015 13:05
SW 6010C
Total Manganese
982
5
KM
10/15/2015 13:05
SW 6010C
Total Copper
290
5
KM
10/15/2015 13:05
SW 6010C
Total Zinc
800
5
KM
10/15/2015 13:05
SW 6010C
Ammonia Nitrogen
0.68
6750
10.0
JM
10/14/2015 08:35
SM-4500-NH3C
Organic N
2.52
25250
10.0
10/14/2015 08:35
CALCULATION
Nitrate+ N itrite-N
<2.00
2.00
JM
10/14/2015 08:35
SM-450ONO3F
Total Cadmium
3.0
2.0
KM
10/15/2015 13:05
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-286-0200
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 64707
Sample Id : WASHINGTON WWTP
(2)
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: WASHINGTON NC
NC CERT# 257
REPORT OF ANALYSIS Date Sampled: 10/12/2015 09:15:00
Date Received: 10/13/2015 00:00
Date Reported: 10/19/2015
Total Chromium
44
5
KM
10/15/2015 13:05
SW 6010C
Total Nickel
24
5
KM
10/15/2015 13:05
SW 6010C
Total Lead
35
5
KM
10/15/2015 13:05
SW 6010C
Total Arsenic
6.0
3.0
KM
10/15/2015 13:05
SW 6010C
Total Mercury
1.7
0.4
KM
10/14/2015 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
10/15/2015 13:05
SW 6010C
pH (Standard Units) *
7.51
2.00
JM
10/14/2015 08:35
SW-9045D
Total Volatile Solids
42.76 427600
100.0
JM
10/13/2015 15:00
SM-2540G
Total Molybdenum
7
5
KM
10/15/2015 13:05
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". THE MSD WAS OUT OF LIMITS FOR "K", "Mg", AND "Na". ALL OTHER QC DATA IS
ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

R�IOS�OL D��S SAMPLE
M . .
1 °
A&L Eastern AgdcuituT
age
1621 Whitepine Road Richmond VA 23237 TO: 804-743-9401 t'nx: I
lJill III aIIII1IiIfIIIiI1II III1II 1I1 6246
EMA RnClUt20ES INC
WASHINGTON NC 11:13:56
,A6c;;u,nt'
Stt),�1�
F ON
!Mr.,nQd Hy
v. a . - „
ha
COPY To
„ r
EMA Resources Inc
EMA Resources Inc
755 Yadkinville Rd 755 Y adkinville Rd
Mocksville, NC 27028 Mocksville, NC 27028
AIC
TS � l�f' L l
> TM, Rr�
I L " Number „ Co1.4� tior lnfomia t n Catatai 'r„ltifa r rn
" Pia �`
� Cie „ �Qsfs�
. ,. � ^ - � ,. ase Chaos sirbti "
ID Lab use
:• bar x °
°
Qrlfyj rFYp Date t J Mjne° erg ° '�3!p �lJ „5 1 L2 e� � p g y k w
Qtk N .tom Ay
rab
� Composite
%�� �
t
C� , j ,�
Glass
Y Rla sfic
�oz
nt
Grab
_ Composite
_ Glass
Plastic
— oz
---tnt
at
Grab
— oz
— Composite
—Glass
Plastic
—pint
Ot
_, Grab
,_ _ Composite
_ Glass
plastic
°Z
--pint
t
�t% �r �faemarks;
I"d i dttire
Tkne
Received w ",`i nature), __.
Date
. ,
TestfPa�ke a t?eiWifs t
S �ci� ltt�t`,
SL1:
• Total Solids (Moisture) Total Kjcldaltl Nilragen, F'iaospharus surd Potassium
SL2: Busic Tesl SLI plus So{fur. Calcium; MagnesivrOodiurn, Iron, Alu mhos, Manganese, ConperAnd Zinc
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium_
(Copper & Zinc included in 512)
Nitrogen Series: Toth! Kjeldahl• Ammonium, Nittute & Organic Nitrogen.
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)

Page: 1 of 2
Report Number: 15-355-0204
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
(2)
Waypoi nt M
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: WASHINGTON NC WWTP
NC CERT#257
REPORT OFANALYSIS
Date Sampled: 12/17/2015 10:15:00
Lab Number: 65893
Date Received:
12/21/2015 00:00
Sample Id : WASHINGTON NC WWTP
Date Reported:
12/23/2015
RESULT
RESULT
QUANTITATION
PARAMETER
METHOD
Total Solids
4.04
40400
100.0
JM
12/21/2015 14:10
SM-2540G
Moisture *
95.96
100.0
JM
12/21/2015 14:10
SM-2540G
Total Kjeldahl Nitrogen
4.28
42800
10.0
JM
12/22/2015 08:24
SM-4500-NH3C-TKN
Total Phosphorus
2.21
22100
100
KM
12/22/2015 11:21
SW 6010C
Total Potassium
0.34
3390
100
KM
12/22/2015 11:21
SW 6010C
Total Sulfur
0.88
8840
100
KM
12/22/2015 11:21
SW 6010C
Total Calcium
1.48
14800
100
KM
12/22/2015 11:21
SW 6010C
Total Magnesium
0.37
3690
100
KM
12/22/2015 11:21
SW 6010C
Total Sodium
0.21
2080
100
KM
12/22/2015 11:21
SW 6010C
Total Iron
49300
100
KM
12/22/2015 11:21
SW 6010C
Total Aluminum
36100
100
KM
12/22/2015 11:21
SW 6010C
Total Manganese
610
5
KM
12/22/2015 11:21
SW 6010C
Total Copper
207
5
KM
12/22/2015 11:21
SW 6010C
Total Zinc
610
5
KM
12/22/2015 11:21
SW 6010C
Ammonia Nitrogen
0.67
6680
10.0
JM
12/22/2015 08:24
SM-4500-NH3C
Organic N
3.61
36120
10.0
12/22/2015 08:24
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
12/22/2015 08:25
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
12/22/2015 11:21
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our r'epons and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-355-0204
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 65893
Sample Id : WASHINGTON NC WWTP
(2)
Waypoi nt
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° fax [phone]
www.waypointanalytical.com
Project: WASHINGTON NC WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 12/17/2015 10:15:00
Date Received: 12/21/2015 00:00
Date Reported: 12/23/2015
Total Chromium
54
5
KM
12/22/2015 11:21
SW 6010C
Total Nickel
29
5
KM
12/22/2015 11:21
SW 6010C
Total Lead
20
5
KM
12/22/2015 11:21
SW 6010C
Total Arsenic
5.0
3.0
KM
12/22/2015 11:21
SW 6010C
Total Mercury
1.2
0.4
KM
12/23/2015 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
12/22/2015 11:21
SW 6010C
pH (Standard Units) * 7.53
2.00
JM
12/22/2015 08:24
SW-9045D
Total Volatile Solids 58.76
587600
100.0
JM
12/21/2015 14:10
SM-2540G
Total Molybdenum
11
5
KM
12/22/2015 11:21
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al",
"Cr", "Fe", "Ni",
AND "P". THE MSD WAS OUT OF
LIMITS FOR "Cr". ALL OTHER QC
DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

OESC
1
Mr. Brent Collins
E4A Resources
755 Yadkinville Road
Mocksville, NC 27028
Report Summary
Friday May 01, 2015
Report Number: L760696
Samples Received: 04/22/15
Client Project:
Description: Washington NC
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1 - 800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have an
questions regarding this data package, please do not hesitate to caly
l.
Entire Report Reviewed By: L/��'�`�•/',�E��TOI. J
Leslie Newton , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 3

1
REPORT OF ANALYSIS
Mr. Brent Collins
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
May 01,2015
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
ESC Sample
# L760696-01
Date Received April 22,
2015
Description Washington NC
Site ID
Sample ID WASHINGTON WWTP
Project
Collected By Roy Whitaker
Collection Date 04/21/15 08:45
Parameter
Result Det. Limit
Units
Limit
Method
Date/Time
By Dil
Corrosivity
Non-Corrosiv
9045D
04/27/15
1534
KBC 1
Ignitability
DNI at 170 F
Deg. F
D93/101
04/27/15
1048
DR 1
Reactive CN (SW846 7.3.3.2)
BDL
0.125
mg/kg
9012B/S
04/28/15
1627
ASK 1
Reactive Sulf.(SW846 7.3.4.1)
BDL
25.
mg/kg
9034/90
04/25/15
1250
DR 1
TCLP Extraction
-
1311
04/25/15
1502
LJN 1
Mercury
BDL
0.010
mg/l
0.20
7470A
04/27/15
2217
MPT 1
Arsenic
BDL
0.45
mg/l
5.0
6010C
04/27/15
1255
LTB 1
Barium
BDL
1.4
mg/l
100
6010C
04/27/15
1255
LTB 1
Cadmium
BDL
0.45
mg/1
1.0
6010C
04/27/15
1255
LTB 1
Chromium
BDL
0.45
mg/1
5.0
6010C
04/27/15
1255
LTB 1
Lead
BDL
0.45
mg/1
5.0
6010C
04/27/15
1255
LTB 1
Selenium
BDL
0.45
mg/1
1.0
6010C
04/27/15
1255
LTB 1
Silver
BDL
0.45
mg/1
5.0
6010C
04/27/15
1255
LTB 1
TCLP ZHE Extraction
-
1311
04/26/15
1650
LJN 1
TCLP Volatiles
Benzene
BDL
0.050
mg/1
0.50
8260B
04/27/15
1924
MCB 1
Carbon tetrachloride
BDL
0.050
mg/l
0.50
8260B
04/27/15
1924
MCB 1
Chlorobenzene
BDL
0.050
mg/l
100
8260B
04/27/15
1924
MCB 1
Chloroform
BDL
0.25
mg/l
6.0
8260B
04/27/15
1924
MCB 1
1,2-Dichloroethane
BDL
0.050
mg/1
0.50
8260B
04/27/15
1924
MCB 1
1,1-Dichloroethene
BDL
0.050
mg/l
0.70
8260B
04/27/15
1924
MCB 1
2-Butanone (MEK)
BDL
0.50
mg/1
200
8260B
04/27/15
1924
MCB 1
Tetrachloroethene
BDL
0.050
mg/1
0.70
8260B
04/27/15
1924
MCB 1
Trichloroethene
BDL
0.050
mg/1
0.50
8260B
04/27/15
1924
MCB 1
Vinyl chloride
BDL
0.050
mg/l
0.20
8260B
04/27/15
1924
MCB 1
Surrogate Recovery
Toluene-d8
108.
% Rec.
114.
8260B
04/27/15
1924
MCB 1
Dibromofluoromethane
98.5
% Rec.
125.
8260B
04/27/15
1924
MCB 1
a,a,a-Trifluorotoluene
102.
% Rec.
114.
8260B
04/27/15
1924
MCB 1
4-Bromofluorobenzene
99.8
% Rec.
128.
8260B
04/27/15
1924
MCB 1
TCLP Pesticides
Chlordane
BDL
0.0050
mg/l
0.030
8081
04/30/15
1221
LKD 1
Endrin
BDL
0.0050
mg/1
0.020
8081
04/30/15
1221
LKD 1
Heptachlor
BDL
0.0050
mg/1
0.0080
8081
04/30/15
1221
LKD 1
Page 2 of 3

Mr. Brent Collins
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
Date Received April 22, 2015
Description Washington NC
Sample ID
Collected By
Collection Date
WASHINGTON WWTP
Roy Whitaker
04/21/15 08:45
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
May 01,2015
ESC Sample # L760696-01
Site ID
Project
Parameter
Result
Det. Limit
Units
Limit
Method
Date/Time
By Dil
Lindane
BDL
0.0050
mg/l
0.40
8081
04/30/15
1221
LKD 1
Methoxychlor
BDL
0.0050
mg/1
10.
8081
04/30/15
1221
LKD 1
Toxaphene
BDL
0.010
mg/1
0.50
8081
04/30/15
1221
LKD 1
Surrogate Recovery
Decachlorobiphenyl
79.7
Rec.
123.
8081
04/30/15
1221
LKD 1
Tetrachloro-m-xylene
78.3
Rec.
114.
8081
04/30/15
1221
LKD 1
TCLP Herbicides
2,4,5-TP (Silvex)
2,4-D
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
TCLP Semi-Volatiles
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate Recovery
2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
p-Terphenyl-d14
BDL
0.0020
mg/l
1.0
8151A
04/30/15
1804 KLM 1
BDL
0.0020
mg/l
10.
8151A
04/30/15
1804 KLM 1
77.8
Rec.
8151A
04/30/15
1804 KLM 1
BDL
0.10
mg/l
7.5
8270D
04/27/15
0338 ADF 1
BDL
0.10
mg/l
0.13
8270D
04/27/15
0338 ADF 1
BDL
0.10
mg/l
0.13
8270D
04/27/15
0338 ADF 1
BDL
0.10
mg/l
0.50
8270D
04/27/15
0338 ADF 1
BDL
0.10
mg/l
3.0
8270D
04/27/15
0338 ADF 1
BDL
0.10
mg/l
2.0
8270D
04/27/15
0338 ADF 1
BDL
0.10
mg/l
5.0
8270D
04/27/15
0338 ADF 1
BDL
0.10
mg/l
400
8270D
04/27/15
0336 ADF 1
BDL
0.10
mg/l
200
8270D
04/27/15
0338 ADF 1
BDL
0.10
mg/l
100
8270D
04/27/15
0338 ADF 1
BDL
0.10
mg/l
400
8270D
04/27/15
0338 ADF 1
BDL
0.10
mg/l
2.0
8270D
04/27/15
0338 ADF 1
46.8
g Rec.
87.0
8270D
04/27/15
0338 ADF 1
35.6
Rec.
67.0
8270D
04/27/15
0338 ADF 1
64.6
Rec.
120.
8270D
04/27/15
033E ADF 1
65.0
°s Rec.
122.
8270D
04/27/15
0338 ADF 1
67.8
t Rec.
148.
8270D
04/27/15
0338 ADF 1
72.2
% Rec.
149.
8270D
04/27/15
0338 ADF 1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Limit - Maximum Contaminant Level as established by the US EPA
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 05/01/15 12:57 Printed: 05/01/15 14:20
Page 3 of 3

EM,Ai Resources
755 Yadkinville Road
Mocksville, NC 27029
Report to:
Mr, Brent Collins
Description:
Phan,: 336-751-1441
Fax; 336.751-1442
on ke N y
Sample ID
III -
Analysis / Container / Preservatill Chain of Custody
Billing information;I*ES
_
Mr. Brent Collins 71,
755 Yadkinviile Road C-
MoCksviile, NC 27028
EMOM
1 SiaSS Letanan Rd
Email To,brent.Collins@vntarasourceisirye.c+ot►a. I Mo"!61S-ura 56.0sal
I tt l Morw� 6ds-'se-�95t
lent Pi cilict #
Lala Project All
tepaclilty ID #
P.i). #
a
a
rd,
z
at
�'-
Date Results Needed
ri
U
Rush? (Lab MUST Be Notified)
..J
Same MY ........._...............2CKM
z
r4
Next Pay ............................
100%
Email?
NO X _Yes
Two Day ....
.........50%
FA7f7
No Yes
•—
No r
ii
Three Day ....
.......... 254L
-^—
of ,-+
Sy
Comp/Grab Matrix
Depth
Date
Time
:titre
F
1ClP
,'/
I,
z x `
x
Matrix; 5S - Soll Gw - Groundwater WW - Wastewater OW Drinkirgg Water [XT •Other —
emarks:
Date: Time: Received by (Sign'te)
lelinqui e
Time:. Received bV (Sigr.�OtuIP)
telinquishe bY: Da
Date: Time: Re ci _d i,r ia� ny: {. prat e
Rellnquished by: ,, 1 h `1
pAenr. !"JO-➢67-5539
Far:615-PSi5STi9 � -
ry
Bi28
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Accteroum: Eib'CAi2E5 `
T11413
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I .ft: GEt 'ierrle fudge
{
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I Islam .�
pH Temp
"Old
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Flow Other _
Samples r urned via: 13 UPS oil daion
edEx. 13 Courier
Temp:��a�rottieS' ad:
f COC SLJ!rtact: _.__Y _,___NA
Ga c Trt.e; Pft Checkr� 6ai F:
lJJ

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
JJ
,wP
i
a�
I a
Facility Name: City of Washington
WWTP Name: Washington WWTP
Monitoring Period: From 5/5/2015
WQ Permit Number: WQ0001026
NPDES Number: NCO020648
To 5/5/2015
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ra ❑
y
Gamma Ra ❑
Y
Past u '
e rization ❑
Class B:
Alt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic
bic Digestion
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g �'
Number o
Excee- dences
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
MinimumGeo.
Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
4839
7311
12195
MPN/g
0
Quarterly
G
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
vector Attraction Reduction (15A N AC; 02T .1107) -Please indicate alternative nerformed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench)
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑.
No vector attraction reduction alternatives were performed ❑
C ER'1'1FICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Adam Waters - Water Resources Superintendent
Preparer Name and Title (type or print)
_ GL�
Signature of Preparer*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
t- Z6y b Z�Z 1/11/2016
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington WQ Permit Number: WQ0001026
WWTP Name: Washington WWTP NPDES Number: NCO020648
Monitoring Period: From 5/19/2015 To 5/19/2015
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
I Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
He Treatment ❑
Thermophilic ❑
Beta R
Ray ❑
Y
G aroma Ra Y
Pasteurization
Class B:
Alt. (1) Fecal Density R1
F—A-7. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion
tion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech-ni ue
q
Minimum
Geo. Mean
axim
Unitsences
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
9828
14366
19797
MPN/g
0
Quartery
G
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) 0
I Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Adam Waters - Water Resources Superintendent
Preparer Name and Title (type or print)
Signature of Preparer*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
/- ZG-iv zl-e� 1/11/2016
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:, City of Washington WQ Permit Number: WQ0001026
WWTP Name: Washington WWTP NPDES Number: NCO020648
Monitoring Period: From 10/16/2015 To 10/16/2015
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic El
Beta Ra ❑
Y
Gamma Ra Y ❑
e o
Past ux7zati n ❑
Class B:
Alt. (1) Fecal Density 21
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
er
Ana obic Digestion ❑
g
:::...:::::::.....:..:..::::::..:.................... .
<::::::::<:::::::::::<:: .........::.....:.::::::....:.:................ .
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
FrequencySample
of Analysis
y
Type
Analytical
Tech-ni ue
q
Minimum
Geo. Mean
Maximum
Unitsences
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
NTN
4878
5024
5114
MPN/g
0
Quartery
G
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) 211
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) • ❑
No vector attraction reduction alternatives were perfornied ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Adam Waters - Water Resources Superintendent Brent Collins; Director of Technical Services
Preparer Name and Title (type or print)
Signature of Preparer*
Land Applier Name and Title(ifapplicable)(type or print)
�41e � 1/11/2016
Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington
WWTP Name: Washington WWTP
Monitoring Period: From 12/21/2015 To
WQ Permit Number: WQ0001026
NPDES Number:-NC0020648
12/21/2015
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
..............
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Theirnophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization
Class B:
jAlt. (1) Fecal Density 21
Alt. (2) Process to Significantly Reduce Pathogens ❑
..............
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic,i Digestion g
.............................................................................................................. .
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
WN
5028
7378
21727
MPN/g
0
Quarterly
G
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) �
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Adam Waters - Water Resources Superintendent Brent Collins; Director of Technical Services
Preparer Name and Title (type or print)
i
Signature of Preparer*
Land Applier Name and Title (if applicable)(type or print)
l-a6-16 Z,- e -� 1/11/2016
Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

Summary Sheet
Fecal Coliforma
Pathogen Reduction
Date s ` S -15
Location #
MPN/g
Log
. 6 2-)
3, &8-*
3,68q T
�. 0
Geometric Means/g
Total Dry Solids
(� OL
Signature

Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
Temp 951- 5°C
DATE / TJ0 R �(IY•�n' °C
/. c€) ABA Sample Location
24 hr. Check tf, Sample Tyke: Grab x Composite
48 hr. Check Lfl&reservation � I1
,, f f4m 72 hr. Check
do,",
FECAL CAL COLEFORM TEST
22nd edition Standard Methods 9221 C E-2006WN)(Aqueous)
Presumptive Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPN
24 hours _ 33
487hours1-42— _
—1 1 --j -71 1 1 1 1 JEI I I Ij
1 k Y --� 3{ 3 Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 Nm'N
24 hours -^ e Q
AWN Fecal Coli%rm/g = 10 x MPN index 1100 ml MYN/g = 10 x
largest volume X % dry solids tested D. CO 1 ,3. Co 9
C1nri1'vkv f nn4rnl
Heterotrophic Plate Count 10 mL
1 mL
0.1 mL
0.01 ntL
Dilution Water Blank
Standard Methods Agar
Dilution Water Blank
Quality Control Tubes
Double Stren h S Control
Single Strength (S Control
i
EC Broth Control
Revised 2,-28-13

TeMp35� OC
----�" DATE / TEE dth �° oC
Sampled By G,0jt- t Sample Location
Received By 4-9 un 24 hr. Check _2� _ J 13 Sample Type: Grab x Composite
Analyzed By 48 hr. Check 7—( 4/3�i Preservation
Calculated By 72 hr. Check Z-!(_`� J
Recorded By YU- 5-5 ) Si
Checked By
FECAL CAS. C®LIFORM VEST
22nd edition Standard Methods 9221 C E-2006(MPN)(Aqueous)
1Precmmntive TL-%t
Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPN
24 hours '"'~
MPN Fecal Coliform/g = 10 x MPN index 1100 ml MPN/g = 10 x Y. J,- — t S = 1 ; r 19 5 wN f o
largest volume X % dry solids tested 0. DO i � 3.6 O. 063 f. cl
Cterility rnntrnl
Heterotrophic Plate Count 10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water Blank
4
Standard Methods Agar t
Dilution Water Blank
Quality Control Tubes
Double Streugth (DS) Control
Sin le Strength (SS) Control
/
EC Broth Control
Revised 2-28-93

Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
Tempi -,6 °C
DATE / T O Iq/�. & ° C
? , dD Sample Location
24 hr. Check 4 '`10 �'�5 ,1 1y Sample Type: Grab x Composite
4 -ni-15 ' f�441 48 hr. Check I(T '2 (-`4jt/e ation
72 hr. Check'
FECAL COLI'ORM TEST
22nd edition Standard Methods 9221 C E-2006(WN)(Aqueous)
Precmmntive Tect
1 111 � 1 IIII. b l I Idd ' 1 11114I' i• I II I I I1 �
1'
Fecal Coliform Test
mL Sample 0.001 1 0.0001 1 0.00001 0.000001 1 0.0000001 1 0.00000001 MIPN
24 hours
MPN Fecal Coliform/g = 10 x MPN index 1100 ml MPN/g = 10 x r — "`�
largest volume X % dry solids tested 0. O®1 -x- 3 .
Cterility irnntral
Heterotrophic Plate Count 10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water Blank
G
Standard Methods Agar L
Dilution Water Blank
t
Control Tubes
Double
EC Broth Control
Revised 2-28-13

Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
Temp 35 y.�f. oC
DATE / T1; O °C
Sample Location
Z 2b-i-K - FS- %A 24 hr. Check 4- 4 !2-Iga -2 i Sample Type: Grab x Composite
i
148 hr. Check —t. I : Preservation 'YL.flyLe--J
$--s- 172 hr. Check
FECAL CO LI'®RM TEST
22nd edition Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 1 0.000001 0.0000001 0.00060001 MPN
24 hours �.
MPN Fecal Coliform/g = 10 x MPN index / 106 ml MPN/g = 10 x 1,8 — -
largest volume X % dry solids tested D. Ob i * 3 , '-T a — (3. 0 0-3 �,L
Sterility Control
Heterotrophic Plate Count
10 mL
1 mL 0.1 mL
0.01 mL
Dilution Water Blank
<
Standard Methods Agar
G
Dilution Water Blank
G
Quality Control Tubes
Double Stren h (D§2 Control
Single Strength (SS) Control
t
EC Broth Control
v
Revised 2-28-1$

Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
Temper °C
DATE / TM ° C
Sample Location
otp'i 8:�a�t 24 hr. CheckL. Q -IS = Sample Type: Grab x Composite
48 hr. Check Er�'aL�- S 1 ',`e I Preservation
72 hr. Check tii"41—
FECAL COLEFORMt TEST
22nd edition Standard Methods 9221 C E-2006WN)(Aqueous)
Presumntive Test
• I
iL''�l�C�/:�iCIGa�°11COi��C�iOCC�iii�iiiii�®
' • : ,
iiiii©iioO�iiG�IDO©i'�iiG�iiiiiaiiiii
Fecal Coliform Test
mL Sample 0.001 0.000f 0.00001 1 0.000001 5.0000001 0.00000001 MPN
24 hours 4 - .
MPN Fecal Coliform/g = 10 x MPN index / 100 ml WN/g = 10 x
largest volume X % d solids tested
g dry V. Ubf '�"
Sterility Control
Heterotrophic Plate Count
10 mL 1 mL 0.1 mL
0.01 mL
Dilution Water Blank
C
Standard Methods Agar
C
Dilation Water Blank
<
Quality Control Tubes
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control
Revised 2-28-13

Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
Temp 45136•5 °C
�% — DATE I TUV E kk °C
'� 2 /-!`- ���✓� Sample Location
4.2b-1—a.4gupt 24 hr. Check -1.5 Sample Type: Grab x Composite
48 hr. Check 'reservation "t7'
72 hr. Check 'r- - I t - �-
5'
FECAL COLIFORM TEST
22nd edition Standard Methods 9221 C 1E-20060VN)(Aqueous)
Presumntive Test
n n
I 1111 1 11
11 ■ I III , I I ,�; Millis#.i.,i1.Irl,
-
'"
GGG;GGG©G;GGGG�t.GGGG,�
]Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 1 0.000001 0.0000001 0.00000001 MPN
24 hours / r
MPN Fecal Coliform/g = 10 x WN index 1100 ml
largest volume X % dry solids tested
Ml'N/g = 10 x 1 • - — J �j � WI&J
Sterilitv Control
Heterotrophic Plate Count
10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water Blank
Standard Methods Agar
Dilution Water Blank
Quality Control Tubes
Double Strength (DS) Control
EC Broth Control
Revised 2-28-13

Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
Temp35/3tb °C
DATE / TZ E f_., A6l - G ° C
Sample Location
4-2b-1 K 9: WaYA 24 hr. Check 13 J S��ple Type: Grab x Composite
4-w:-1s' ®r /J'M 48 hr. Check tr' - ~� ���reservation
72 hr. Check Lt - Y - ►' 4-°1
FECAL C®LI F ORM TEST
22nd edition Standard Methods 9221 C E-2006(M PN)(Aqueous)
Presumutive Test
'•; a ni
I II � I I11 I hlll 11ltll :- 1111111
} I IIIllll;
Fecal Coliform Test
ML Sample
0.001
0.0001 0.00001 1 0.000001 0.0000001 0.00000001 MPN
24 hours
MPN Fecal Coliform/g = 10 x MPN index / 100 ml MPN/g = 10 x Lt- • = 4 S 2 b a tvt
largest volume X % dry solids tested p , pp ( AL '3 • O '-T
Sferility Control
Heterotrophic Plate Count
10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water Blank
<
Standard Methods Agar
G i
Dilution Water Blank
uality Control Tubes
le Strength (DS) Control
e Strength (SS) Control
EC Broth Control
Revised 2-28-13

Summary Sheet
Fecal Coiiforms
Pathogen Reduction
Date wf q-1
Location #
MPN/g
Log
/0!3>v
41
3
If, 2 4:3
4, 'Z ,-8
/ Gl
L+.21-3 (G
Geometric Means/g
Total Dry Solids
&,a-,JKw6A
Signature

:L _
— --
1 t—� �- -
Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
NAME 'r DATE / TIME
5-1
557,
r915ka. s
TemP3s:S„ °C
Oc
Sample Location �_�(.�z-�_ �i
24 hr. Check 2S�4N Sample Type.- Crab x�Coomposite -"
48 hr. Check 3:o reservation _
72 hr. Check t-18-1`r
FECAL C®LIFORM TEST
22nd edition Standard Methods 9221 C E-2006(NON)(Aqueous)
Prnciemntnvr Ti-e '
mL Sample
0_001
0.00001 0.000001 0.0000001
0.00000001
M1PN
24 hours
+
—
-f-
+——
II.0I.0=00
-F
.--
48 hours
+
--
-
-,i-.
--
—
rg-raf Pnlifnrm TAC+
mL Sample
0.001
0.0001 0.00001 0.000001 0.0000001
0.00000001
MPN.
24 hours
--
341e
�,1
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
IY TN/g = 10 x
Sterility Control It"NO
Heterotrophic Plate Count
10 mL
1 mL 0.1 mL
0.01 mL
)Dilution Water Blank
Standard Methods Apr
Dilution Water Blank
t
Quality Control Tubes
Double Strength (DS) Control
Single Strength (SS) Control.
EC Broth Control
may,A J�
Revised 2-28-13

_ye'�
Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
NAME DATE / TIME
i
fAI
-fti (�Fk`ram�jyv,..
Temp36=S °C
Sample Location _c cc�Q
24 hr. Check -14, ! =3(ap �ple Type: Grab x Composite
48 hr. Check 70-kS �: r , reservation
72 hr. Check 5-1Y~ii :.3G
FECAL COLIFORM 'VEST
22nd edition Standard Methods 9221 C E-2006WN)(Aqueous)
Presumptive Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPN
24 hours — l �-- }- E + + liC?
48 hours 1. 1 — I I i .
Fecal Conform Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPN
24 hours „- 1 -^ 4 I I — / .. fl-
MPN Fecal Coliform/g 10 x WN index / 100 ml
largest volume X % dry solids tested
WN/g= 10x
Rtpr;iity Cnnfrnl
Reterotrophic Plate Count
10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water Blank
�-
Standard Methods Agar
Dilution Water Blank
-
Quality Control rubes
Double Strength (DS) Control
EC Broth Control
Revised 2-28-13

Temp'rs.S °C
NAME DATE / T1ME 1: ���"�� yy � oC
Sampled By t�n,�.z /�6�lcrrS� —t-1?; fL�..
Sample Location
Received By,1 ! j
51S'l,� a: aOm 24 hr. Cheep S C-�� ,? Sample Type: Grab x Composite
f---- ---c - N
Analyzed By c, Q S S-! S, 07 ,7 '/�J 48 hr. Check j �7'7-y5-+3.'r Preservation
Calculated By 4111, } s -{� `lJ`� �f:�' �%�` 72 hr. Check 5-13-15, 3t -,hwjj
Recorded By (261 5),
Checked By
FECAL C®LEFORM TEST
22nd edition Standard Methods 9221 C E 2006{MPN)(Aqueous)
Presumptive Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 JMom"
24 hours + + -t -}- —
48 hours. _
Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000041 MFN
24 hours ..� -I-
r
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
NYN/g = 10 x 6 c3
- too
c+.Ar.+.. ram,. f—I
Heterotrophic Plate Count
10 mL
✓1 mL
0.1 mL
0.01 mL
Dilution Water Blank
Z— j
Standard Methods Agar
L
Dilution Water Blank
Quality Control Tubes
Double Strength (IDS) Control
Single Strength (SS) Control
EC Broth Control
Revised 2 28-13
f

_
NAME DATE / TDM I:�.
Sampled By ��+�.� /n%ao f rs •� �-r ~lam'' :y!
.Received By
Analyzed By v �rQw t 5-15. S OgIA,-1
Calculated By .� cS� S-�.' . c�' � d �)v-
e
Recorded By
Checked By
Temp-ZS--S, °C
4. OC
Sample Location
24 hr. Check s�f -tZ a , , �, Sample Type: Grab x Composite
48 hr. Check - `t?rtN �reservation-------- � i
72 hr. CheckS-R-c5 3;310
FECAL C®LIFORM TEST
22nd edition Standard Methods 9Z21 C E-2006QiiPN)(Aqueous)
]Presumptive Test
mL Sample 0.001 0.0001 0-OOnnl I a Mnnni I U %wn%T
Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 1V.IDPN
7-4 hours -t- .j.
N.1PN Fecal Coliform/g = 10 x 1V1CPN index 1100 ml MPN/g = 10 x
largest volume X % dry solids tested 0 x 3,~� I
Heterotrophic Plate Count
10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water Blank
f
Standard Methods Agar
Z.
Dilution Water Blank
f
Quality Control Tubes
]Double Stren h (DS) Control
Single Strength (SS) Control
EC Broth Controlr-��
Revised 2 28-13

Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
mL Sampl
24 hours
48 hours
NAMM iDATE / T&ME Temper S �C°
t4. q-
�t�n -, /�%o f cs.. % S'rS l ,,J-Sample Location. = r2-a 5
1�'.d�,^, 24 hr. Check 16 •(r' a •'S1
Sample Type: Grab x Composite
-tS-i�,v=zs-oi(\ 48hr. Check s•C�y5;3:Zt�,r��reservation 46CA -
to`- 72 hr. Check-T-rg-(F. '936Ole
FECAL C®LI+®RM 'VEST
22nd edition Standard Methods 9Z21 C E-2006(1VIlL'N)(Aqueous)
Presumptive Test
0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 WN
Fermi 6_nlii'nrm Ti-ct
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000007-1 0.00000001 MPN
24 hours _-
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
//'-OCRt >C �f,i� C• f.ovo7i J
Heterotrophic Plate Count
10 mL
y) mL
0.1 mL
0.01 mL
Dilution Water Blank
Standard Methods Agar96
�-
Dilution Water Blank
Revised 2-28-13

Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
Tempa5--S- °C
G
"v n
NAME DATE / TLC f : S� y.y, �►- ° C
Sample Location
OILy�-0
24 hr. Check l I.3 nm Sample Type: Grab x Composite
48 hr. Check S-f'I — 3, ... Preservation -- A A 9�
72 hr. Check,
FECAL C®LIFORM TEST
22nd edition Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
mx, 3ampie I u.uujl 0.0001 0.00001 0.000001 0.0000001 0.00000001
MPN
24 hours
+
+-
48 hoursI
-f- I
ARN Fecal Coliform/g = 10 x WN index / 100 ml
largest volume X % dry solids tested
Fecal Colit'orm Test
lYPPN/g = 10 x (�: Z- = — / L
O.00 1 X 3..� �S b,0 J g 7.
Heterotrophic Plate Count
10 mL
+1 mL
0.1 mL
0.01 mL
][Dilution Water Blank
G �
Standard Methods Agar
Dilution Water Blank
Quality Control Tubes
Double Strength S) Control
Single Strength (SS) Control
rto f
EC Broth Control,
u
Revised 2-28-13

ri
Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
DATE /TDO
Temp�,S`_S °C
y �} °C
� Sample Location �_�[�
24 hr. Check 64-fS 3:v Sample Type: Grab x Composite
48 hr. Cheek 5�f7-Jjr 3,�reservation
72 hr. Check
FECAL C®LIF®RM TEST
22nd edition Standard Methods 9221 C E-2006(NTN)(Aqueous)
Presumptive Test
--F— I . VJL v.vvv a U.utl00Il 0.000001 1 0.0000001
0.00000001 YON
24 hours
48 hours
mL Sample
0.001
0.0001 0.00001 .. W`0.000001 0.0000001
0.00000001 MPN
24 hours
!;Z• �2
MTN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
M(PN/g = 10 x 2 0
Heterotrophic Plate Count
10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water Blank
f
Standard Methods Agar
G 1
Dilution Water )Blank
�. !
Quality Control Tubes
Double Strength (DS) Control
Sin-,Ie Strength (SS) Control
EC Broth Control
Revised 2-28-13

Date l 2 -16 v / S
Location #
cSCL-11- k
Summary Sheet
Fecal conforms
Pathogen Reduction
MPNIg
f)�
5 any
gDID
69 q
Log
3,Ogg
(019 b
f
3 . ---k04S;
Geometric Means/g
Total Dry Solids
Signature

N DATE / TIME
Sampled By
Received By 1 al - to -a -/5 I /,5
Analyzed By � � �D--1�-a�' ' '30
Calculated By
Checked By J 42_.!4��---`-
4
35/3S" D
Temp c `
C
• Sample Location
24 hr. Check J!�: il-i 57 II.Wt5ASample Type: Grab x Composite
48 hr. Check ia-1W-1si tq D� reservation 1y 4'
72 hr. Check S7 101�55W'1
FECAL C®LIFORM TEST
22nd edition Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
mL Sample 3 0.001 D5 Sj 0.0001 S5 C- 0.00001 VS CG 0.000001 S5 0.0000001 0.00000001 MPN
24 hours _ _ -- - - - _ r tq I I I I �(? I
-
48 hours ' .
- Fecal Coliform Test
mL Sample 01001 0.0001 0.00001 0.000001 70000001 0.00000001 MPN
24 hours --
M PN ]Fecal Coliform/g = 10 x NII PN index 1100 ml D"N/g = fl0 x � I • g _ J f
- 5 j i j + All- /a
largest volume X % dry solids tested Q, o O ! a4- j , �-��- 0 , 0 035 9,
J e'�
sterility enntrni
Heterotrophic Plate Count
10 mL 1 mL
0.1 mL 0.01 mL
Dilution Water Blank
e
Standard ]Methods Agar
G
Dilution Water ]Blank
�-
Quality Control Tubes
Double Strength (dDS) Control
Single Strength (SS) Control
EC Broth Control
a ve---
Revised 2-28-13

N DATL / TZM
Sampled By
Ira -1.2-/5 ' 4 ?A OA-
Received By
QPeu• 01a�t
Analyzed By
Calculated By
Checked By
`ti-•� . �-'- � "� /� -/lam--ice. /��.CU
mL Sample 0.001
24 hours
48 hours -_
mL Sample 1• 0.001
24 hours
Temp 35 °C
QQ 44.5 °C
Sample Location J
24 hr. Check 60..�3-1 ti 62-`'�1 Sample Type: Grab x Composite J
�68hr.Check-�ir•.�5 D - -5 reservation Cr&ekA -
72hr.Checkl01S-1S 10'd5''�
FECAL ComFORM TEST
22nd edition Standard Methods 9221 C 1E-2006WN)( iqueous)
Presumptive Test
0-0001 SS C 0.00001 G a.00000l o.aaoaoal
0.0001
AWN Fecal Coliform/g - 10 x WX-index / 100 ml
largest volume X % dry solids tested
Fecal Coliform Test
Infi, T 0.000001
YTNlg = 10 x S S
o.Oo1 3.&0
Sterility Control
hie Plate Count 10 UIL 1 UIL
Water Blank
Dilution Water Blank
Revised 2-28-13
0.1 niL
0.00000001
11
0.00000001 b MPN
f�
d • OC& 10
0.01 mL
9

AME
DATE / T1ME
Sampled By
][deceived By
Z. 0to�
(V -12
Analyzed By=
7-1
Calculated By
" ,
! 0 -16-1 1 CZ \
Checked By
mL Sample j`�j 0.001
24 hours —
48 hours
mL Sample 0.001
24 hours
Temp 35 oC
QQ y q. 5 °C
Sample Location J
24 hr. Check ta-�3'l , t&.w2, Sample Type: Grab x Composite
48 hr. Check
O 1 reservation Ova
ro�l�iS i -
72 hr. Check
FECAL COLIF01M TEST
22nd edition Standard Methods 021 C E 2006WN)(Aqueous)
Presumptive Test
C- 0.00001 V> c 0.000001 S5 O.o000001
0.0001
D"N Fecal Coli£orm ig = 10 x B N index 1100 and
largest volume X % dry solids tested
]Fecal Coli%rm Test
0.00001 1 0.000001
YRN/g = , 10 x {
0 , C> a at 3,(>0
0.00000001 MOPN
v
0.00000001 S MPN
19Y
. 003 b I 14
5, po0 Aj`o°/
axerwLy 4-watxva.
P(eterotrophie Plate Count
10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water Blank
Standard Methods Agar
G
Dilution Water Blank
L t
Control Tubes
Double Strength Pb) C;OntrO
_Single Strength (SS) Control
EC Broth Control
Revised 2-28-13
a

Sampled By
Received By
Analyzed By
Calculated By
Checked By
N ][DATE / TEE
!n -lam : S�iswc
22nd edition Standard Methods 9221. C E-2046(1UN)(Aqueous)
MTN Fecal Coli%rm/g = A0 x WN index 1100 ml
largest volume X % dry solids tested
Revised 2 28-13
Fecal Coliiform `Pest
Nlg L0 x Z.1, $ =
0.00t'& 3.53�11-
Sterility Control
0 "IL A mL
laic Plate Count 1L i
water Blank
Methods Agar � l
0.1. ML
Temp 35 °C
yd 3 °C
Sample Location �e P� g -� ---
S le T e. Grab x Composite
24 hr. Check 12:- 3 t13 53mp yp o
4$ hr. Check Preservation
��,�__._1�f-.iS .'��
,+a-3
72 hr. Check
om nods

Sampled By
Received By
Analyzed By
Calculated By
Checked By
AIL Sampl
24 hours
48 hours
mL Samp]
24 hours
0.001
A DATE / TUVIE
S7 lh-�
&K-
Ib-1(o"c IS2,
FECAL (C®LIFOWN1. T AN
22nd edition Standard Methods 9221 C E-2006(.1�eN)(Aqueous)
Presumptive Test
0.0001 S� G 0.00001 �S G 0-000001 155
0.0001
iV$)PN'!E'ecal Colifor®/g = 90 x 1VIPN index / 100 ml
largest volume X % dry solids tested
Fecal Coliform Test
0.00001
Temp ge; O oC
Owr"OC
Sample Location -----
lt
24 hr. Check 106:jq n&? ample Type: Grab x Composite
48 hr. Check
reservation
`"-- --
� o -�1�-� 5 f�5
72 hr. Check
0.0000001
1YN/g= 10x Z-1' g
p,pp1 - 3�5bfv
Sterility Control
(eterotrophic Plate Count
10 mL 1 HIL
L(
Dilution Water ]Blank
Standard Methods Agar i
G�
,nn..fdn,. Water blank
Revised 2-28-13
0.1 mL
T0.00000001 WN
13
0.00000001 1 N'N
1Y _
35� r '� r55 � ���/ �
p,o D
0.01 mL

N , DATE / TDN
Sampled By
Received By
Analyzed By 1~9
LU—l4,-rS 1s2�
Calculated. By
Checked By
FECAL C®LI'®RM TEST
22nd edition Standard Methods 9221 C E-2006(16' N)(Aqueous)
Presumptive Test
o.000l sS c o.00001 Ds a.aa000l �S
mL Sample -Ir
24 hours
48 hours TT--Ar
,anL Samnple 1 0.001
24 hours
Fecal Coliform Test
o.oaol 0.00001 o.00000l
MPN Fecal Colil'orm/g = lox i Wade- / 100 and
largest volume X % dry solids tested
Temp 55, 1) °C
pp � oC
Sample Location
24 hr. Check q Sample Type: Grab x Composite —
O'' S Preservation
48 hr. Clxecl:lo-t+�-1� L7�2
72 hr. Check 0-1 ) D
0.0000001 0.00000001 WN
St
0.0000001 0.00000001 MPN
YTN/g= 10x 3' ��'9 1 W0035
Sterility Control
l0mL 1mL
terotrophic ]Plate CountL I
(Dilution, Water Blank
tandard Methods Agar L i
L(
Revised 2 28-13
0.1 mL
0.01 mL

Sampled By
Received By
Analyzed By
Calculated By
Checked BY
mL Sampl
24 hours
48 hours
mL Sampl
24 hours
DATE / TIME
rn -r2-1 :o
FECAL COLIFO TEST
22nd edition Standard Methods 9221. C E-2006(I0DN)(Aqueous)
Presumptive Test
L 4.00001 - n nnnnfil
0.001 'p5 0.0001 s5
Fecal Coliform Test
0.001 0.0001 0.00001 0.000001
WN ]Fecal Colid'orm/g = 10 x 1v1Y'N index 1100 ml
largest volume X %airy solids tested
leterotrophic Plate Count 10 mL
Dilation Water Blank
Standard Methods Agar L-
Dilution Water dank
Revised 2-28-13
Temp :3,--,,o °C
gq,5"oC
n
Sample Location
24 hr. Check fo-II-Is 1 1U. "-Sample Type: Grab x _. Composite
48 hr. Check -D-t'l--15 10 - � //reservation
72 hr. Check !O-t S-t toy
0.0000001
4. S_..
0 0000001 0.00000001 M3PN
—'I— -T c t. tS
N1PN/g = 1.0 x 1, 21.>Is`�'"s G O�� � — -�) Q�`�"D
o, oo 1�- 3,6 1 p.o
Control
ImL
C,
0.1. ML
0.01 mL

Summary Sheet
Fecal Coliforms
Pathogen Reduction
Date 9 --1
Location #
MPNIg
Log
Si Lck e 1
o Z2
(A
2-
�g �e 73
5ol- -L
�2-�
�1 t- (+
5525_
!,3 f V
-�,3',-E'
Geometric Meanslg
Total Dry Solids
Signature

NAN E DATE / TOO
Sampled By ; Z/ ' po
Received By
.Analyzed By f;�; 12-15-1S ir.5-.!L
Calculated By `��J �1�� /[�vc;. i-l�-is�
Recorded By T------
Checked By
Temp 'j v °C
Sample Location (3�--
5*
24 hr. Check 12,-16-t�; J� O Sample Type- Grab x Composite
481ir. Check 1351 '-"preservation
72 hr. Check-i_T-iZ
FECAL CAL C®LIFORM TEST
22nd edition Standard Methods 9221 C E-2006(1P1)(Aqueous)
Pre+eeamntiva Tp..ci
ML Sample
0.001
0.0001
0.00001
0.000001 0.0000001
0.00000001 1VD.'N
I24 hours
+
+
4-
�}-
J
�-
±H
48 hours
+
I
mL Sample 0.001
0.0001 0.00001
0.000001
0.0000001
0.00000001 WN
24 hours
4. 8
INN Fecal Colilorm/g = 10 x NTN index 1100 ml
largest volume X %4 dry solids tested
v �r
NTN/g = lox i - 8 — 55C S 1vL�i<i�
_ C3 �:b3C8
C • jai � :3 5Q
Ctnril;+v rnnfrni
Heterotrophic Plate Count
10 mL
1 ML
0.1 mL
0.01 mL
Dilution Water Blank
41
Standard Methods :Agar
Dilution Water Blank
Quality Control Tubes
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control
Revised 2-28-13

NANMJ DATE / T
Sampled By il� z/ ✓ i �`! � 13 , i Z��
Received By � � J;kf�-)c 6 31 D
Analyzed By
Calculated By
Recorded By
Checked By e . � �
Temr�-_- °C
_n tt�� p� f� ••..t C
Sample Location c 4 �l (d-IT e;),-
.Is
24 hr. Check E2-,b_ _15DA Sample Type: Grab x Composite
48hr. CheclQZ- M-e'3N 135�4reservation �,^�
72 hr. Chec%�-d�'E--
Flj CAL COLI'®RM TEST
22nd edition Standard Methods 9221 C ]E-2006WN)(Agneous)
fL_.____—t— rp..nd
mL Sample
0.001
0.0001
0_00001
0.000001
0.0000001 0.00000001
lVld'N
24 hou.rs
i-
$
-!-
i -
4. hours
- +
-
-
—1
mml[, Sannple
0.001
0.0001 0.00061 y
w 0.006001
0.0000001 0.00000001
l�ii'N
a
24 hours
-4- —
MPN Fecal Coliforun/g = 1.0 x MPN index / 100 and
largest volume X % dry solids tested
MpN/g = lox q - D = A0= 15 C � j /v-f ej
C�Ens.:ii.t.r R•'n.e�rnll
Heterotrophic date Count
10 mL
J1 mL
0.1 mL
0.01 mL
Dilution dater Blank
4 •
Standard Methods Agar
Dilution dater Blank
Quality Control 'pubes
Double Strength (DS) Control
11-e, %,�r % .
Single Strength (w Control
EC Broth Control
` Cr tL`•.
Revised 2-28-13

NAMMI
DATE, / TIMM'
Sampled By i1= �
i�~LS ]� 1.2,46
Received By � , A. A,
1310
Analyzed By
Calculated By
a �1S-1Sf Ik3,(
Recorded By -
Checked By
Temp 2 °C
oC
Sample Location At se, 3
Is U
24 hr. Check 12,-16-1a (70 Sample Tame: Crab x Composite
48 hr. Check b9 J%:3.�4reservatiou 1 —�
72 hr. Check r ria-i' s �
FECAL COLIFORM TEST
22nd edition Standard Methods 9221 C 3E 2006WN)(A.queous)
m.. .,ae. a rro,e
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
24 hours
�'
�'
4
-� -"'
_d
EIAeN
al0
49 hours
-1-
1.
�', Sample
0.001
0.0001
0.00001
0.000001
0.0000001 0.00000001 NTN
24 hours
WN Fecal ColiformIg = 10 x MTN index 1100 ml
largest volume X % dry solids tested
MTN/g = 10 x ) , T — JT -r -:::. D Lf-P, IVkf
D,o4}
G+nr;➢i+v d^rut+rrnfl
Heterotrophic Plate Count
10 mL
1 mL
0.1 ML
0.01 mL
Dilution Water Blank
Standard Methods Agar
$
Dilution Water Flank
Quality Control Tubes
Double Strength (IDS) Control
'fit
Single Strength (SS) Control
h�
EC Broth Control
Revised 2-28-13

NAM
DATE, / Td)1E
Sampled Byy
} ' iS 1 %z
Received By _--
Analyzed By c_.
12-1r
Calculated By ��.��
Recorded By
Checked By
Temp °C
//��
J�cc
Sample Location & 4
;uk3
24 hr. Check M-16 * 1s- /,5o Sample Type: Grab 1 Composite
48 hr. Check la-1-)- a / 4'363s4reservation
72 hr. Check 1_ �-iSs�a' /��r' 5-
FECAL CAL COLIFORM TEST
22nd edition Standard Methods 9221 C ] 2006(N Ti)(Agueous)
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
NTN
24 hours
49 hours
_
mL Sample
0.001
0.0001
0.00001 -- -
- --- 0.000001
0.0000001
0.00000001
lil[l.'N
24 hours
-F
—
e2 O
YIPN Fecal Coliform/g = 10 x MPN index / 100 ml WN/g = lox 55,25 w (',J
largest volume X % dry solids tested
Warili
Heterotrophie Plate Conant
10 mL
.1 ML
0.1 mL
0.01 ML,
Dilution Water Blank
4 �
Standard Methods Agar
Dilution Water Blank
L �
Quality Control Tubes
Double Strength (]fDS) Control
Single Strength (SS) Control
EC Broth Control
U
Revised 2 28-13

DATE / TEVM
Sampled BY 1 2••5.8
Received By � - i�.-1�-17 i3 r o
Analyzed By
Calculated By
Recorded By -
Checked B
By C:
Temp_ °C
°C
Sample Location
;M3
24 hr. Cheek Zp It�-aj $e�d� Sample Type: Grab a Composite
43 hr. Check J'Z- n-'Fj [ ''4reservation �w �
72 hr. Check i-aSr-r" 124-
FE CAL COLIEFORM TEST
22nd edition Standard Methods 9221 C B-2006(10N)(Aqueous)
mL Sample
0.001
0.0001 0-00001
0.000001
0.0000001 0.00000001
WN
24 hours
dE
-1
1
1
L
tj
I
I
I . .
=
48 hours
—
+-
+
1
-1
1
1
EL SnMp➢e
0.001
- 0.0001
0.00001
0.000001
0.0000001
0.00000001
11 24 hours
_
M PN Fecal Co➢iform/g = 10 x NTN index 1100 ml
largest volume X % dry solids tested
wN/g = 10 x �.y � t� 0 14 Pi
(D. Oc)
�4na-iliAv 6'nntceai
Heterotrophie ]Plate Count
10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water Blank
Standard Methods .Agar
Dilution dater dank
Quality Control Tubes
Double Strength (ADS) Control
Single Strength (SS) Control
EC Broth Control
Revised 2-28-13
r { r

NAME' DATE' / TJ[IlO
Sampled By �— l�`15I�� /30Z
Received By � , L �-,_, i � 13/0
Analyzed By �4 � _ ;2-�1 =�� � /609
Calculated By 2r1�Gu. 1]?'!�-!$
Recorded By
Checked By � r� s2��[ -➢�, 1*',7 4
Temp °C
t� C
Sample Location 15 PII� w 6
413
24 hr. Check 150 - Sample Type: Grab x Composite
48 hr. Check PZ-P-!`9S /, ,3 55'PPreservatloAn
72 hr. Check i-''9-15 134 So
IFE CAL COLIEFO T�ST
22nd edition Standard Methods 9221 C E-2006(A411,N)(Aqueous)
VMAr'lmn ilm Toef
nag, Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
1V�N
24 hours
-
48 hours
-aF
w L Sample
0.001
0.0001
0.00001
0.0DOOR
0.0000001
0.00000001
Nl"1'N
11 24 hours
-r
—
-rI
— I
I —
=�
MPN Fecal Co➢ifform/g = 10 x DPN index / 100 ml
largest volume % % dry solids tested
M PNIg = 10 x 11� S- = 2 (S- pv fu-f ij
D.p©3�
gNwHity r..nntrnl
Heterotrophie Plate Count
10 mL
1 mL
0.1 ML
0.01 mL
Dilution Water Blank
z:- �
Standard Methods Agar
Dilution Water ]Blank
Quality Control Tubes
Double Strength (IDS) Control
Single Strength (SS) Control
Pn �. `c, -$4t �—
A,C Broth Control
b
Fevised`2-284Z

NAME
DATE' /TIME
Sampled By
Received By
l0/0
Analyzed By
.i�
��-E� d1 � 1609
Calculated By
����
DZ -)�-d5, A3 9
Recorded By
_--------
Checked By �
�i��
i2"2d—lb ; �'�ZO
Temp h °C
Q �] U oC
Sample Location c h Ld�& c -tf
-' —U_
24 hr. Check 1-2,4,-'�; /50S Sample Type: Grab x Composite
48 hr. Check b2- o-)I!Fj /35654reservation (VSJ
72 hr. Check -is-g; 13lr
FECAL COLIFORM TEST
22nd edition Standard Methods 9221 C F-20060VI N)(Agueons)
�11'/+feeefR Ye+64JP `�'PC�'
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
l�A]PN
24 hours
48 hours`-
mL Sample
0.001
0.0001
0.00001
0.000001 0.0000001
0.00000001 NTN
24laours
--d
--
-7• 8
NEPN ]Fecal Coliforna/g = 10 x YTN index / 100 and IkVN/g 10 x � . � _ — � -;:7 Peo)
largest volume X % dry solids tested . O a 1 '-Ie- 3 . v, QD s 5�
-�"+e+re9e+er 6"'nxe+e-nQ
H{eterotrophic ]Plate Count
10 ML
1 ML
0.1 mL
0.01 mL
Dilution Water Blank
Standard Methods Agar
$
Dilution Water Blank
Quality Control Tubes
Double Strength MS) Control
Va-� '�'�►v�, .
Single Strength (SS) Control
-
EC Broth Control
•�,�, �.;L
Revised"2 28-1'3

4` Analytital Results
EMA Resources, Inc.
755 Yadkinvitle Rd.
Mocksyille, NG 27028
-; Recelve Date; 04123/2015
Reported: 05/26/2015,
For: Washington WWTP
Comments:
Sample Number Pararrieter Sample ID Result Unit Method Analyzed Analyst
150'423-15'01 30'Da}+`Seitchscal.6 137-'' "ado EPA625-R-92/0. 04J24/2(11:5 WL
Respectfully
submiffed;
i
Dena.Myers.
NC .Cent #440,
NCDW`Cei t #37755,
EPA #NCO0909
PO Box 228 * Statesville, NC28687 •704/872/4697
Page 1 of 2

Client:
�/
p t F�� t�
d
-STATESViLLE ANALYTICAL
122,Court Street - P.O. Box 228
Statesville, NC 28687
Address: ~•.,.
to e- �=' � F . yp
'ifl 1f F� ( i Lr / t/
(70.4) 872.4G97
7. Chalin of ,
6s'tQdy $eeord
Contact Person, Phone # FAX#
POI �5 Requisitioned by: {Time Date),
.,
Customer
Sample IDN
Lab -ID#
Tim®Sampldei
(Grab Only)
Date Sampled
(Grab Only)
0
Matrix
-
p rameters, requested for analysis
9 y.
Is,096
I w
ww
1 V s
4 -4 V 3iA / its �j C= STP't
CL.a.G'f trc� CFI.lS'
c
r c� rv.
1
i
i
Relinquished by:
Received by:
Relinquished by:
Received by:
Composite Sampling
Time begin
Time end
Composite Sampling
Time begin
Time end
,/ l4✓ G
#`l:
am, pm Date / /
.
am, pm Date ^/ /
#2:
am, pm Date
am, pm Date /_/
�`-- T- Ime . L)S am pm. Da Sampled ! Sampled by:
t f/) s'L.df/l1
�; Time f r , pm Date; /� Transported by: �yc//�� ,rPl
i
Time am, pm Date_1 sh Holding times met:
Time am, pm Date I f_____. Compliance work:
I.
Non-compliance work:
i
Lab Comments:

Analytical. Results
EMA Resources, Inc.
755,Y;adkinville Rd.
Mocks.ville-,.-NC 27028
Rweive Date, 10/13/2016
Report ed-. 111/09/201'5
For:. Washington WWTP
Comments:
Sample Number Parameter Sample ID Result
r
Y, 16T Washington .,,,,
Respe6ffully,
submitted,
Dena Myers
NC 66ii #440,
NCDW Cert #37765,
EPA,#NCO0909
Unit Method
EPA62!;
Analyzed Analyst
111,3/2015 WL
PO Box 228 - StatesVille, NC 28687- 704/872/4697
Page 1 of 1

Client:
STATESVILLE ANALYTICAL
Street -
Address:
'Couri P.O.Box 228
Statesville, NC 28687
(704) M-4697
0
Contact Person:
IPhone #
FAX#
Chain of
PO
�J431i(
Requisitioned by:
/V C-
Date),
Custody Record
,:-,16 7-6 A/
Customer
Sample 10#
Lab-11) 0
Time Sampled
(Grab Only),
Date -Sampled
(Grab Only)
W
Matrix
S11WOO W
WW -"
rameters re
F� quested for analysis
WWY
3 & N3 es
cq4ir.e.relZ
PIA,
A
-D;/
f
lie'
7
Relinquished by:
Time to Cam>T,
Date-�()/
Sampled b :4
'y
Received by:
)y.
Time
Cam ,)O m
Date 1"'cl 1,31
Transported by:
Relinquished by:
Time
am, pm
'ate
Holding times met:_
Received by:
Time
am, pm
Date
Compliance
Composite Sampling #11:
work:
ITime begin- am, pm
Date
Non-compliance work:
Time end' am, pm
Date
Lab Comments:
Composite Sampling #2:
Time begin- am, pm
Date I
Time end am, pm
Date

Page 1 of 1
Report Number: 15-355-0708
Account Number: 46245 Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
Send To: EMA RESOURCES INC ANALYTICAL www.waypointanalytiical.com
755 YADKINVILLE RD 'Every acre... Every year. Grower: HARVEY WILLIAMSON
MOCKSVILLE NC 27028 HUNTER'S ROOST FARM
SOIL ANALYSIS REPORT Analytical Method(s):
Date Received: 12/21/2015 Date Of Analysis: 12/22/2015 Date Of Report: 12/22/2015 Mehlich 3
ID
OM
WN
.ENR
Phosphorus
Rotassium,"
Magnesium
Calciurrr
Soduim`
pH . `° °.' . •
' -Acidity
C E.0 ;
•Sample
Field ID ,
..Lab
Number
o --"
�0, :
Soil
Ibs/A
Mehiich a
Reserve
K:
Mg , .
Ca
Na , :
Soil
Buffer
H '
Rate
. ;Class
;;
ppm ;. Rate
ppm 'Rate
ppm s , ;Rate;
ppm _ -Rate
ppm Rate
-ppm q 'Rate,
pW .
Index
..meq/1O0g
meg7100g
2
22336
16
110
93 H
131 H
220 H
953 M
23 VL
5.9
6.78
1.5
8.5
MIN
M
NC = 77
NC = 67
Percent Base Saturation
Nitrate
Sulfur
Zmc
Marig'anese
:dron.. `
Copper
Boron
SoiubieSalts
.., Chloride .
Aluminum
=Sample ID
Field ID
K
Mg
Ca
Na;:
H ..:
NO3N
S
Zn
Mn
Fe
Cu
B'
SS „
Cl `
AI:.
%�
%
ppm -' Rate`
ppm '-Rate
,ppm °; Ratc
'ppm :;'� Rate
Rpm f2ate
p'pm ° Rate
.ppm Rate
ms/cm Rate"
;ppm , '-Rate
,:ppm,=
2
20 M
4.1 H
7 L
295 VH
1.3 M
0.3 VL
0.07 VL
4.0
21.6
56.1
1.2
17.6
NC=42
NC=102.5
NC=44
NC=65.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. �
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm �i x 2 = Ibs/A, Soluble by: 1 Wt . or G
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: WaypointAnalAcal Virginia, Inc.
Pauric McGroary

Page 1 of I
Report Number: 15-155-0616
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE NC 27028
(� _A&L Ea-stem-Laboratoduo.
7621'Whitepine Road Richmond, Virginia 23237 (804),*-9461_ Fax (804)27i-Wg
vAmaleastem.com
Grower:
HUNTER'S ROOST FARMS Farm ID:
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Received: 06/04/2015 Date Of Analysis: 06/05/2015 Date Of Report: 06/0512015
"Every acre... Every year. TIVI 11
'Sample
,,Organic Matter
:,Phosphorus
,PotassiumMagnesium
.Calcium
"So
PH
ACI Ity
C.E.C
ID,
rield,113-
Lab
u
Number-
ENR
Rate,
`F,"46serve­'..'
Ca"
Na
Buffer.
,H,
ppm Rate , ,
;ppm ',Rate
.Rate
PrT 14
P ate,
t
-Opirn Ra e
ppm Rat e
p",,",
Index
meq11"9'0g
meq/100'6'
13786
2.2 L 84
53 H
134 H
110
M
1100
H
24 VL
6.6
0.4
7.3
NC 44
NC 69
5
13787
8.8 VH 150
25 VH
318 VH
1338
M
1 3214
H
138 VL 1
6.5
1
1 1.6
21.5
NC 104
NC 163
12
13788
2.4 L 90
199
I VH
156 VH
71
M
685
M
21 VL
6.0
6.85
I
0.8
I5.3
NC 166
NC = 80
16
13789
2.3 L 86
127 VH
147 H
130
H
1010
H
22 VL
6.7
0.3
6.9
NC10 6
NC = 75
Fqrcent,Base Saturation'
Nktratii_­,,1111,�',
S
Sulfur
'Zind,"
" Manganese
1ron",
opper�,�.:
Boron:
�Sqllub e.Sla
Salts
Chloride
Aluminum
Sample ID
Field ID'..
K
M'
Na;9'
Mn
B
SS
CV
Al
%
0
X
0
X
9
pm;. _R
P 'Ot6
in Rate
ppi f­
'ppm�!­. Rate,
ppm %
ppm Rate
p te,
ppm a e,
`pprri, �,Raile'pprrii
Rate
mslcm'�Rate�
P Rate
pm,,
ppm
P
20 M
4.5 H
14 M
163 VH
2.1 H
0.4 L
0.12
VL
4.7
12.6
75.3
1.4
5.9
1
NC 42
1 NC = 112.5
1 NC = 88
NC = 105.0
1
1
5
VH
VH
1O M
1 VH
99
2.4 H
0.7 M
0.46
VL
3.8
13.1
74.7
0.8
7.4
�66
18.9
NC I 37
NC = 222.5
NC = 63
NC = 120.0
12
M
H
6 L
280 VH
H
0.3 VL
0.08
VL
I 7.5
11.2
I
64.6
I
1.7
I
15.5
122
13.7
�2.0
NC 46
NC= 9 2.5
NC=38
NC=100.0
16
18 M
2.7 M
L
VH
1.7H
0.4 L
0.1
VL
I 5.5
15.7
I
73.2
I
1.4
I
4.5
�
16
1170
I
NC 37
NC = 67.5
NC = 38
NC = 85.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), lbs/A This report applies to sampie(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = lbs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. by: Pxa,. or GovC.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = porn.
Pauric McGroary