20200057 Ver 1_Tab J - Chemical_Analysis_20200109

40110,
AwH E IyA
TECHNOLOGIES, INC.
2 May 2018
Mr. Robert Neal
Moffatt & Nichol
272 N. Front Street, Suite 204
Wilmington, NC 28401
RE: Chemical Data Summary
Atlantic Harbor
Carteret County Navigation Project
North Carolina
Dear Mr. Neal,
Athena Technologies, Inc. is pleased to submit this Chemical Data Summary for
Atlantic Harbor. Should you have any questions or concerns regarding the attached data
summary, please don't hesitate to contact me via the information below.
Respectfully,
J. Adam Freeze
Vice President / Geologist
1293 Graham Farm Road, PO Box 68
440, McClellanville, South Carolina 29458
,OW F-1 E r4A, [phone]
TECHNOLOGIE$. INC. www.athenatechnologies.com

40110,
AwH E IyA
TECHNOLOGIES, INC.
CHEMICAL DATA SUMMARY
ATLANTIC HARBOR
CARTERET COUNTY NAVIGATION PROJECT
NORTH CAROLINA
TABLE OF CONTENTS
Table 1: Summary of Analytical Detections — Volatile Organic
Compounds, Semivolatile Organic Compounds, and Petroleum
Hydrocarbons
Table 2: Summary of Analytical Detections — Metals and Pesticides
APPENDICES
Appendix A: Laboratory Analytical Reports — Chemical Analyses
1293 Graham Farm Road, PO Box 68
440, McClellanville, South Carolina 29458
'0w"EHA [phone]
TECHNOLOGIES, INC. www.athenatechnologies.com

TABLE 1
SUMMARY OF ANALYTICAL DETECTIONS
VOLATILE ORGANIC COMPOUNDS, SEMIVOLATILE ORGANIC COMPOUNDS, AND PETROLEUM HYDROCARBONS
ATLANTIC HARBOR
Boring ID:
Sample ID:
Sample Depth / Interval (ft bss):
Sample Type:
Analyte CAS No. EPA NOAA NOAA Units
TEL [2] ERL [s]
G1
0.5
G
AH-02-0318
G2
3.1
G
G3
5.7
G
C1
0 - 6.2
C
G1
0.5
G
AH-04-0318
G2
2.7
G
G3
4.8
G
C1
0 - 5.3
C
G1
0.5
G
G1-DUP
0.5
G/ DUP
AH-05-0318
G2
1.6
G
G3
2.7
G
C1
0 - 3.2
C
C1-DUP
0 - 3.2
C/ DUP
G1
0.5
G
AH-06-0318
G2
3.7
G
G3
6.8
G
C1
0 - 7.3
C
G1
0.5
G
AH-07-0318
G2
2.8
G
G3
5.1
G
C1
0 - 5.6
C
Volatile Organic Compounds
Acetone
67-64-1
-
-
-
pg/kg
ND
ND
ND
NA
ND
13
ND
NA
27
ND
16
ND
NA
NA
ND
ND
ND
NA
ND
ND
ND
NA
Carbon disulfide
75-15-0
131
-
-
pg/kg
ND
ND
ND
NA
ND
ND
ND
NA
11
ND
ND
ND
NA
NA
ND
ND
ND
NA
ND
ND
ND
NA
Methylene Chloride
75-09-2
667
--
--
pg/kg
ND
ND
ND
NA
7.5
7.1
5.6
NA
13
10
8.3
15
NA
NA
ND
ND
ND
NA
ND
ND
ND
NA
Toluene
108-88-3
568
-
-
pg/kg
ND
ND
3.6
NA
ND
ND
ND
NA
ND
ND
ND
ND
NA
NA
ND
ND
ND
NA
ND
ND
ND
NA
Semivolatile Organic Compounds
Acenaphthene
83-32-9
6.7
6.71
16
pg/kg
NA
NA
NA
ND
NA
NA
NA
14 J
NA
NA
NA
NA
ND
ND
NA
NA
NA
ND
NA
NA
NA
ND
Acenaphthylene
208-96-8
5.9
5.87
44
pg/kg
NA
NA
NA
ND
NA
NA
NA
32 J
NA
NA
NA
NA
52 J
45 J
NA
NA
NA
ND
NA
NA
NA
ND
Anthracene
120-12-7
47
46.9
85.3
pg/kg
NA
NA
NA
26
NA
NA
NA
50
NA
NA
NA
NA
53 J
40 J
NA
NA
NA
ND
NA
NA
NA
ND
Benzo[a]anthracene
56-55-3
75
74.8
261
pg/kg
NA
NA
NA
16 J
NA
NA
NA
150
NA
NA
NA
NA
130
100
NA
NA
NA
1.7
NA
NA
NA
ND
Benzo[a]pyrene
50-32-8
89
88.8
430
pg/kg
NA
NA
NA
16 J
NA
NA
NA
130
NA
NA
NA
NA
150
110
NA
NA
NA
ND
NA
NA
NA
ND
Benzo[b]fluoranthene
205-99-2
--
--
--
pg/kg
NA
NA
NA
32
NA
NA
NA
200
NA
NA
NA
NA
290
220
NA
NA
NA
2.5
NA
NA
NA
ND
Benzo[g,h,i]perylene
191-24-2
310
-
-
pg/kg
NA
NA
NA
12J
NA
NA
NA
79
NA
NA
NA
NA
90
67
NA
NA
NA
ND
NA
NA
NA
ND
Benzo[k]fluoranthene
207-08-9
-
-
-
pg/kg
NA
NA
NA
13 J
NA
NA
NA
68
NA
NA
NA
NA
120
98
NA
NA
NA
ND
NA
NA
NA
ND
Chrysene
218-01-9
108
108
384
pg/kg
NA
NA
NA
28
NA
NA
NA
150
NA
NA
NA
NA
120
110
NA
NA
NA
1.8
NA
NA
NA
ND
Dibenz(a,h)anthracene
53-70-3
6.2
6.22
63.4
pg/kg
NA
NA
NA
ND
NA
NA
NA
25 J
NA
NA
NA
NA
23 J
16 J
NA
NA
NA
ND
NA
NA
NA
ND
Fluoranthene
206-44-0
113
113
600
pg/kg
NA
NA
NA
31
NA
NA
NA
400
NA
NA
NA
NA
160
130
NA
NA
NA
ND
NA
NA
NA
ND
Fluorene
86-73-7
21
21.2
19
pg/kg
NA
NA
NA
ND
NA
NA
NA
15 J
NA
NA
NA
NA
ND
ND
NA
NA
NA
ND
NA
NA
NA
ND
Indeno[1,2,3-cd]pyrene
193-39-5
340
--
-
pg/kg
NA
NA
NA
8.9 J
NA
NA
NA
74
NA
NA
NA
NA
85
61
NA
NA
NA
ND
NA
NA
NA
ND
Phenanthrene
85-01-8
87
86.7
240
pg/kg
NA
NA
NA
8.4 J
NA
NA
NA
60
NA
NA
NA
NA
ND
ND
NA
NA
NA
ND
NA
NA
NA
ND
Pyrene
129-00-0
153
153
665
pg/kg
NA
NA
NA
25
NA
NA
NA
310
NA
NA
NA
NA
260
220
NA
NA
NA
1.9
NA
NA
NA
ND
Total Petroleum Hydrocarbons (TPH)
TPH - Residual 68476-53-9
-- I -- I -- I mg/kg I NA I NA I NA I ND I NA I NA I NA I 310 J I NA I NA I NA I NA 1 500 J 1 610 J I NA I NA I NA I ND I NA I NA I NA I ND
Extractable Petroleum Hydrocarbons (EPH)
C11-C22 Aromatics
-
-
-
-
mg/kg
NA
NA
NA
ND
NA
NA
NA
12
NA
NA
NA
NA
28
16
NA
NA
NA
ND
NA
NA
NA
ND
C19-C36 Aliphatics
-
-
mg/kg
NA
NA
NA
ND
NA
NA
NA
12
NA
NA
NA
NA
ND
ND
NA
NA
NA
ND
NA
NA
NA
ND
C9-Cl8 Aliphatics
-
-
-
-
mg/kg
NA
NA
NA
ND
NA
NA
NA
ND
NA
NA
NA
NA
15
ND
NA
NA
NA
ND
NA
NA
NA
ND
Volatile Petroleum Hydrearbons (VPH)
Not detected above laboratory method detection limit.
Notes
ft bss
G
C
DUP
CAS No.
EPA "I
NOAA TEL 121
NOAA ERL [3]
Ng/kg
NO
NA
Bold
Yellow Shading
J
mg/kg
,46W" IE HA
TECHNdLOGIES.INC.
= feet below sediment surface
= Grab sample
= Composite sample
= Field duplicate sample
= Chemical Abstracts Service Number
= U.S. Environmental Protection Agency (USEPA), Region 4 Ecological Risk Assessment Supplemental Guidance, Sediment Screening Values for Hazardous Waste Sites, Marine/Estuarine Sediment, Ecological Screening Value (ESV) (USEPA 2018).
= National Oceanic and Atmospheric Administration (NOAA), Screening Quick Reference Tables (SQuiRTs), Marine Sediment, Threshold Effects Levels (Buchman, M.F., 2008).
= National Oceanic and Atmospheric Administration (NOAA), Screening Quick Reference Tables (SQuiRTs), Marine Sediment, Effects Range -Low (Buchman, M.F., 2008).
= Screening criteria not established
= micrograms per kilogram
= Analyte not detected above laboratory Method Detection Limit.
= Not Analyzed
= Analyte detected above laboratory Method Detection Limit.
= Concentration exceeds respective screening criteria.
= Result is less that the Reporting Limit but greater than or equal to the Method Detection Limit and the concentration is an approximate value.
= milligrams per kilogram
1293 Graham Farm Road, PO Box 68
McClellanville, South Carolina 29458
[phone]
www.athenatechnologies.com

12
TABLE 2
SUMMARY OF ANALYTICAL DETECTIONS
METALS AND PESTICIDES
ATLANTIC HARBOR
Boring ID:
Sample ID:
Sample Depth / Interval (ft bss):
Sample Type:
NOAA NOAA
Analyte CAS No. EPA [�] Units
TEL [2] ERL [s]
AH-02-0318
C1
0 - 6.2
C
AH-04-0318
C1
0 - 5.3
C
AH-05-0318
C1
0 - 3.2
C
C1-DUP
0 - 3.2
C/ DUP
AH-06-0318
C1
0 - 7.3
C
AH-07-0318
C1
0 - 5.6
C
Metals
Antimony
7440-36-0
2
-
-
mg/kg
ND
0.075 J
ND
0.13 J
ND
ND
Arsenic
7440-38-2
7.24
7.24
8.2
mg/kg
4.5
7.8
10
8.3
1.4
0.75
Beryllium
7440-41-7
--
mg/kg
0.37
0.58
0.69
0.62
0.092
0.054 J
Cadmium
7440-43-9
0.68
0.68
1.2
mg/kg
0.045 J
0.13
0.33
0.29
ND
0.0111
Chromium
7440-47-3
52.3
52.3
81
mg/kg
19
30
38
32
4.8
3.1
Copper
7440-50-8
18.7
18.7
34
mg/kg
6.9
34
120
99
1.8
0.73
Lead
7439-92-1
30.2
30.24
46.7
mg/kg
12
23
34
27
1.8
1.5
Manganese
7439-96-5
-
mg/kg
110
150
160
140
14
9.5
Nickel
7440-02-0
15.9
15.9
20.9
mg/kg
8
12
15
12
2.3
1.2
Selenium
7782-49-2
--
--
mg/kg
0.44 J
0.74
1.1
11
0.13 J
0.037 J
Silver
7440-22-4
0.73
0.73
1
mg/kg
0.024 J
0.055 J
0.069 J
0.051 J
ND
ND
Thallium
7440-28-0
-
-
-
mg/kg
0.11
0.2
0.3
0.25
0.019 J
0.023 J
Zinc
7440-66-6
124
124
150
mg/kg
31
80
170
150
6.3
2.9
Mercury
7439-97-6
0.13
0.13
0.15
mg/kg
0.03
0.059
0.11
0.099
ND
ND
Chromium, Trivalent
16065-83-1
-
-
mg/kg
19
30
38
32
4.7
2.9
Chromium, Hexavalent
18540-29-9
-
mg/kg
ND
ND
ND
ND
0.19 J
0.19 J
Pesticides
4,4'-DDD
72-54-8
1.2
1.22
2
pg/kg
0.111
1.7
1.8
1.8
ND F1
ND
4,4'-DDE
72-55-9
2.1
2.07
2.2
pg/kg
0.23 J
1.5
4.8
4.3
0.016 J F1
ND
4,4'-DDT
50-29-3
0.7
1.19
1
pg/kg
ND
6.6
ND
ND
ND
ND
Endrin aldehyde
7421-93-4
pg/kg
ND
ND
ND
ND
0.018 J F1
ND
oxy-Chlordane
27304-13-8
-
pg/kg
ND
ND
ND
ND
0.011 JP
0.012 J p
trans -Chlordane
5103-74-2
--
pg/kg
ND
0.36 J
0.58 J
0.58 J
ND F1
ND
Notes
ft bss
= feet below sediment surface
C
= Composite sample
DUP
= Field duplicate sample
CAS No.
= Chemical Abstracts Service Number
EPA "I
= U.S. Environmental Protection Agency (USEPA), Region 4 Ecological Risk Assessment Supplemental Guidance, Sediment Screening Values for Hazardous Waste Sites, Marine/Estuarine Sediment, Ecological Screening Value (ESV) (USEPA 2018).
NOAA TEL [Z]
= National Oceanic and Atmospheric Administration (NOAA), Screening Quick Reference Tables (SQuiRTs), Marine Sediment, Threshold Effects Levels (Buchman, M.F., 2008).
NOAA ERL [3[
= National Oceanic and Atmospheric Administration (NOAA), Screening Quick Reference Tables (SQuiRTs), Marine Sediment, Effects Range -Low (Buchman, M.F., 2008).
-
= Screening criteria not established
mg/kg
= milligrams per kilogram
ND
= Analyte not detected above laboratory Method Detection Limit.
Bold
= Analyte detected above laboratory Method Detection Limit.
J
= Result is less that the Reporting Limit but greater than or equal to the Method Detection Limit and the concentration is an approximate value.
pg/kg
= micrograms per kilogram
F1
= Matrix spike and/or matrix spike duplicate recovery is outside acceptance limits.
p
= The Relative Percent Difference between the primary and confirmation column/detector is greater than 40%. The lower value has been reported.
1293 Graham Farm Road, PO Box 68
McClellanville, South Carolina 29458
,40W" E H [phone]
TECHNOLOGIES. INC- www.athenatechnologies.com

Appendix A:
Laboratory Analytical Reports — Chemical Analyses
1293 Graham Farm Road, PO Box 68
440, McClellanville, South Carolina 29458
Ax"EHA [phone]
TECHNOLOGIES. INC. www.athenatechnologies.com

TestAmerica °
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Pittsburgh
301 Alpha Drive
RIDC Park
Pittsburgh, PA 15238
Tel: [phone]
TestAmerica Job ID: 180-76196-1
Client Project/Site: North Carolina Sediment Project
For:
Athena Technologies, Inc
1293 Graham Farm Road
PO BOX 68
McClellanville, South Carolina 29458
Attn: Adam Freeze
Authorized for release by:
411812018 1:31:35 PM
Carrie Gamber, Senior Project Manager
[phone]
[e-mail]
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Table of Contents
TestAmerica Job ID: 180-76196-1
CoverPage ..............................................
1
Table of Contents .........................................
2
Case Narrative ...........................................
3
Definitions/Glossary.......................................
5
Certification Summary ......................................
6
Sample Summary .........................................
7
Method Summary .........................................
8
Lab Chronicle ............................................
9
Client Sample Results ......................................
22
QC Sample Results ........................................
58
QC Association Summary ...................................
87
Chain of Custody ..........................................
95
Receipt Checklists .........................................
104
TestAmerica Pittsburgh
Page 2 of 106 4/18/2018

Case Narrative
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Job ID: 180-76196-1
Laboratory: TestAmerica Pittsburgh
Narrative
CASE NARRATIVE
Client: Athena Technologies, Inc
Project: North Carolina Sediment Project
Report Number: 180-76196-1
TestAmerica Job ID: 180-76196-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round -off errors in calculated results
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 03/28/2018 and 03/28/2018; the samples arrived in good condition, properly preserved and on ice. The
temperatures of the 3 coolers at receipt time were 3.40 C, 4.80 C and 5.81 C.
The following samples were listed on the Chain of Custody (COC); however, no samples were received as there was a cooler delayed in
shipment. These samples were received on March 29, 2018 within temperature: AH-07-0318-G1 (180-76196-1), AH-07-0318-G2
(180-76196-2), AH-07-0318-G3 (180-76196-3), AH-07-0318-C (180-76196-4) and AH-06-0318-G1 (180-76196-5).
The container label for the following sample did not match the information listed on the Chain -of -Custody (COC): AH-04-0318-G3
(180-76196-15). The container labels list AH-04-0318-G2, while the COC lists AH-04-0318-G3. The id on the COC was used.
The Chain -of -Custody (COC) was incomplete as received and/or improperly completed. The COC lists three containers for the following
sample; however two were received.
The vials received for the TOC analysis were preserved at the laboratory per the notation on the COC: EB-02-0318 (180-76196-24)
The following samples were received outside of the holding time for freezing the volatile terracores. The terra core vials were frozen as
soon as possible after receipt. The samples have had the H qualifier applied: AH-07-0318-G1 (180-76196-1), AH-07-0318-G2
(180-76196-2), AH-07-0318-G3 (180-76196-3) and AH-07-0318-C (180-76196-4).
VOLATILES
Methylene Chloride was detected in method blank MB 180-240896/7 at a level that was above the method detection limit but below the
reporting limit. The value should be considered an estimate, and has been flagged. If the associated sample reported a result above the
MDL and/or RL, the result has been flagged.
Methylene Chloride was detected in method blank MB 180-241049/6 at a level that was above the method detection limit but below the
reporting limit. The value should be considered an estimate, and has been flagged. If the associated sample reported a result above the
MDL and/or RL, the result has been flagged.
The following analyte recovered outside control limits for the LCS associated with analytical batch 180-240736: Chloroethane. This is not
indicative of a systematic control problem because these were random marginal exceedances. Qualified results have been reported.
The continuing calibration verification (CCV) associated with batch 180-240660 recovered above the upper control limit for
Dichlorodifluoro-methane. The samples associated with this CCV were non -detects for the affected analytes; therefore, the data have
TestAmerica Pittsburgh
Page 3 of 106 4/18/20g8

Case Narrative
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Job ID: 180-76196-1 (Continued)
Laboratory: TestAmerica Pittsburgh (Continued)
been reported. The following sample is impacted: (CCVIS 180-240660/2)
TestAmerica Job ID: 180-76196-1
The continuing calibration verification (CCV) associated with batch 180-240865 recovered above the upper control limit for Carbon
Tetrachloride. The samples associated with this CCV were non -detects for the affected analytes; therefore, the data have been reported.
The following sample is impacted: (CCVIS 180-240865/2).
SEMIVOLATILES
An incorrect volume of surrogate spiking solution was inadvertently added the following samples: AH-02-0318-C (180-76196-12). Percent
recoveries are based on the amount spiked.
The following samples were diluted due to the nature of the sample matrix: AH-07-0318-C (180-76196-4), AH-06-0318-C (180-76196-8),
AH-02-0318-C (180-76196-12), AH-04-0318-C (180-76196-16), AH-05-0318-C (180-76196-21), AH-05-0318-C-DUP (180-76196-22),
(180-76196-A-4-B MS) and (180-76196-A-4-C MSD). Elevated reporting limits (RLs) are provided.
The continuing calibration verification (CCV) analyzed in batch 180-241401 was outside the method criteria for the following analyte:
Nitrobenzene-d5 (Surr) was >20% high. As indicated in the reference method, sample analysis may proceed; however, any detection for
the affected analyte is considered estimated.
PESTICIDES
The following samples were diluted due to the nature of the sample matrix: AH-02-0318-C (180-76196-12), AH-04-0318-C
(180-76196-16), AH-05-0318-C (180-76196-21) and AH-05-0318-C-DUP (180-76196-22). Elevated reporting limits (RLs) are provided.
The sample extracts were a medium yellow color after GPC clean-up.
Surrogate DCB Decachlorobiphenyl (Surr) recovery for the following sample was outside control limits on the confirmation column:
EB-02-0318 (180-76196-24). Evidence of matrix interference is present due to preceding sample analyzed; therefore, re -extraction and/or
re -analysis was not performed.
Surrogate recovery was outside acceptance limits for the following sample: (180-76196-A-8-1 MSD). The parent sample and MS
surrogates recovery was within limits. The MSD sample has been qualified and reported.
Several analytes failed the recovery criteria low for the MS/MSD of sample AH-06-0318-C (180-76196-8) in batch 180-242257.
The continuing calibration verification (CCV) associated with batch 242257 recovered outside acceptance criteria, low biased, for
delta-BHC and Endosulfan sulfate. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the
associated samples were non -detect for this analyte, the data have been reported.
The continuing calibration verification (CCV) associated with batch 241080 recovered outside acceptance criteria, low biased, for
delta-BHC and Endosulfan sulfate on MR-1 column and Endosulfan sulfate and Endrin ketone on MR-2 column. A reporting limit (RL)
standard was analyzed, and the target analyte was detected. Since the associated samples were non -detect for this analyte, the data
have been reported. Detections of these compounds were taken from their passing column, where applicable.
METALS
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GENERAL CHEMSITRY
The sample post -digestion spike (PDS) recoveries were outside criteria. Acceptable laboratory control sample (LCS) soluble and
insoluble analysis data demonstrate that the analytical system was operating in control; therefore, this condition is most likely due to a
matrix effect.
The reporting limit for Lloyd Kahn TOC analysis is a nominal value and does not reflect adjustments in sample mass processed on an
individual basis.
TestAmerica Pittsburgh
Page 4 of 106 4/18/20g8

Definitions/Glossary
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Qualifiers
GC/MS VOA
Qualifier Qualifier Description ,
H Sample was prepped or analyzed beyond the specified holding time
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
* LCS or LCSD is outside acceptance limits.
GC/MS Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC Semi VOA C
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
X Surrogate is outside control limits
F1 MS and/or MSD Recovery is outside acceptance limits.
Metals
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Pittsburgh
Page 5 of 106 4/18/2018

Accreditation/Certification Summary C
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Laboratory: TestAmerica Pittsburgh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW) State Program 4 434 12-31-18
The following analytes are included in this report, but are not accredited/certified under this accreditation/certification:
Analysis Method Prep Method Matrix Analyte
Lloyd Kahn Sediment Total Organic Carbon - Duplicates
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
Analysis Method Prep Method Matrix Analyte
2540G Sediment Percent Moisture
2540G Sediment Percent Solids
Laboratory: TestAmerica Pensacola C
The accreditations/certifications listed below are applicable to this report.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW) State Program 4 314 12-31-18
TestAmerica Pittsburgh
Page 6 of 106 4/18/2018

Sample Summary
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
180-76196-1
AH-07-0318-G1
Sediment
03/27/18 08:40
03/28/18 11:36
180-76196-2
AH-07-0318-G2
Sediment
03/27/18 08:42
03/28/18 11:36
180-76196-3
AH-07-0318-G3
Sediment
03/27/18 08:45
03/28/18 11:36
180-76196-4
AH-07-0318-C
Sediment
03/27/18 08:50
03/28/18 11:36
180-76196-5
AH-06-0318-G1
Sediment
03/27/18 09:20
03/28/18 11:36
180-76196-6
AH-06-0318-G2
Sediment
03/27/18 09:22
03/28/18 11:36
180-76196-7
AH-06-0318-G3
Sediment
03/27/18 09:25
03/28/18 11:36
180-76196-8
AH-06-0318-C
Sediment
03/27/18 09:30
03/28/18 11:36
180-76196-9
AH-02-0318-G1
Sediment
03/27/18 09:55
03/28/18 11:36
180-76196-10
AH-02-0318-G2
Sediment
03/27/18 09:57
03/28/18 11:36
180-76196-11
AH-02-0318-G3
Sediment
03/27/1810:00
03/28/18 11:36
180-76196-12
AH-02-0318-C
Sediment
03/27/1810:05
03/28/18 11:36
180-76196-13
AH-04-0318-G1
Sediment
03/27/18 10:40
03/28/18 09:30
180-76196-14
AH-04-0318-G2
Sediment
03/27/18 10:42
03/28/18 09:30
180-76196-15
AH-04-0318-G3
Sediment
03/27/18 10:45
03/28/18 09:30
180-76196-16
AH-04-0318-C
Sediment
03/27/18 10:50
03/28/18 09:30
180-76196-17
AH-05-0318-G1
Sediment
03/27/18 11:35
03/28/18 09:30
180-76196-18
AH-05-0318-G1-DUP
Sediment
03/27/18 11:37
03/28/18 09:30
180-76196-19
AH-05-0318-G2
Sediment
03/27/18 11:40
03/28/18 09:30
180-76196-20
AH-05-0318-G3
Sediment
03/27/18 11:45
03/28/18 09:30
180-76196-21
AH-05-0318-C
Sediment
03/27/18 11:55
03/28/18 09:30
180-76196-22
AH-05-0318-C-DUP
Sediment
03/27/18 11:58
03/28/18 09:30
180-76196-23
TB-02-0318
Water
03/27/18 12:30
03/28/18 09:30
180-76196-24
EB-02-0318
Water
03/27/18 12:50
03/28/18 09:30
C
0
TestAmerica Pittsburgh
Page 7 of 106 4/18/2018

Method Summary
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Method
Method Description
Protocol
Laboratory
EPA 8260B
Volatile Organic Compounds (GC/MS)
SW846
TAL PIT
8270D LL
Semivolatile Organic Compounds by GC/MS - Low Level
SW846
TAL PIT
EPA 8270D LL
Semivolatile Organic Compounds by GC/MS - Low Level
SW846
TAL PIT
8081 B_LL
Organochlorine Pesticides (GC)
SW846
TAL PIT
EPA 8081 B LL
Organochlorine Pesticides (GC)
SW846
TAL PIT
6020B
Metals (ICP/MS)
SW846
TAL PIT
7471 B
Mercury (CVAA)
SW846
TAL PIT
EPA 6020E
Metals (ICP/MS)
SW846
TAL PIT
EPA 7470A
Mercury (CVAA)
SW846
TAL PIT
1664B
HEM and SGT-HEM
1664E
TAL PEN
2540G
SM 2540G
SM22
TAL PIT
7196A
Chromium, Trivalent (Colorimetric)
SW846
TAL PIT
EPA 7196A
Chromium, Hexavalent
SW846
TAL PIT
EPA 9071E
HEM and SGT-HEM
SW846
TAL PIT
Lloyd Kahn
Organic Carbon, Total (TOC)
EPA
TAL PIT
SM 5310C
Total Organic Carbon
SM
TAL PIT
Protocol References:
1664B = 1664B
EPA = US Environmental Protection Agency
SM = "Standard Methods For The Examination Of Water And Wastewater",
SM22 = SM22
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TestAmerica Pittsburgh
Page 8 of 106 4/18/2018

Lab Chronicle
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-07-0318-G1
Lab Sample ID: 180-76196-1
Date Collected: 03/27/18 08:40
Matrix: Sediment
Date Received: 03/28/18 11:36
Batch Batch
Dil Initial
Final Batch
Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240823
03/29/18 11:32 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-07-0318-G1
Lab Sample ID: 180-76196-1
Date Collected: 03/27/18 08:40
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 77.6
Batch Batch
Dil Initial
Final Batch
Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.1985 g
5 mL 240903
03/29/18 09:21 KLG TAL PIT
Total/NA Analysis EPA 8260E
1 5 mL
5 mL 240896
03/30/18 15:26 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-07-0318-G2
Lab Sample ID: 180-76196-2
Date Collected: 03/27/18 08:42
Matrix: Sediment
Date Received: 03/28/18 11:36
Batch Batch
Dil Initial
Final Batch
Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240823
03/29/18 11:32 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-07-0318-G2
Lab Sample ID: 180-76196-2
Date Collected: 03/27/18 08:42
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 77.4
Batch Batch
Dil Initial
Final Batch
Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.0621 g
5 mL 240903
03/29/18 09:21 KLG TAL PIT
Total/NA Analysis EPA 8260E
1 5 mL
5 mL 240896
03/30/18 17:23 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-07-0318-G3
Lab Sample ID: 180-76196-3
Date Collected: 03/27/18 08:45
Matrix: Sediment
Date Received: 03/28/18 11:36
Batch Batch
Dil Initial
Final Batch
Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240823
03/ 99/18 11:32 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-07-0318-G3
Lab Sample ID: 180-76196-3
Date Collected: 03/27/18 08:45
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 83.8
Batch Batch
Dil Initial
Final Batch
Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.1219 g
5 mL 240903
03/29/18 09:21 KLG TAL PIT
0
TestAmerica Pittsburgh
Page 9 of 106 4/18/2018

Lab Chronicle
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-07-0318-G3
Lab Sample
ID: 180-76196-3
Date Collected: 03/27/18 08:45
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 83.8
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis EPA 8260B
1
5 mL
5 mL
241049
04/02/18 09:40
KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-07-0318-C
Lab Sample
ID: 180-76196-4
Date Collected: 03/27/18 08:50
Matrix: Sediment ;
Date Received: 03/28/18 11:36
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis 2540G
1
240823
03/ 99/18 11:32
CLL TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis 7196A
1
241989
04/12/18 11:38
MM1 TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-07-0318-C
Lab Sample
ID: 180-76196-4
Date Collected: 03/27/18 08:50
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 81.0
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep 3541
30.1 g
0.5 mL
241 337
04/ 22/18 03:39
BAP TAL PIT
Total/NA Analysis 8270D LL
2
1 mL
1 mL
241401
04/05/18 15:20
DLF TAL PIT
Instrument ID: CH71
Total/NA Prep 3541
30.3 g
10.0 mL
241038
04/02/18 03:41
BAP TAL PIT
Total/NA Cleanup 3640A
5.0 mL
0.5 mL
241931
04/12/18 06:12
BAP TAL PIT
Total/NA Analysis 8081 B_LL
1
242257
04/16/18 13:54
DFE TAL PIT
Instrument ID: CHGC15
Total/NA Prep 3050B
2.00 g
100 mL
241695
04/09/18 16:04
KA TAL PIT
Total/NA Analysis 6020B
1
241911
04/11/18 02:00
WTR TAL PIT
Instrument ID: M
Total/NA Prep 7471B
1.32 g
100 mL
241273
04/04/18 08:35
RJR TAL PIT
Total/NA Analysis 7471 B
1
241400
04/05/18 09:30
RJR TAL PIT
Instrument ID: K
Total/NA Prep 3060A
2.47 g
100 mL
240858
03/29/18 14:32
SES TAL PIT
Total/NA Analysis EPA 7196A
1
25 mL
25 mL
240949
03/30/18 13:18
SES TAL PIT
Instrument ID: GENESYS10S
Total/NA Prep 9071B
30.0 g
30.0 g
241004
03/31/18 06:25
CBY TAL PIT
Total/NA Analysis EPA 9071 B
1
241091
04/03/18 08:15
JAS TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis Lloyd Kahn
1
241158
04/02/18 14:55
JBF TAL PIT
Instrument ID: FLASHEA
TestAmerica Pittsburgh
Page 10 of 106 4/18/2018

Lab Chronicle
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-06-0318-G1
Lab Sample ID: 180-76196-5
Date Collected: 03/27/18 09:20
Matrix: Sediment
Date Received: 03/28/18 11:36
Batch Batch
Dil Initial Final Batch
Prepared
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1 240823
03/ 99/18 11:32 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-06-0318-G1
Lab Sample ID: 180-76196-5
Date Collected: 03/27/18 09:20
Matrix: Sediment ;
Date Received: 03/28/18 11:36
Percent Solids: 78.9
Batch Batch
Dil Initial Final Batch
Prepared C
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.3 881 g 5 mL 240 003
03/ 99/18 09:21 KLG TAL PIT
Total/NA Analysis EPA 8260B
1 5 mL 5 mL 240896
03/30/18 16:13 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-06-0318-G2
Lab Sample ID: 180-76196-6
Date Collected: 03/27/18 09:22
Matrix: Sediment
Date Received: 03/28/18 11:36
Batch Batch
Dil Initial Final Batch
Prepared
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1 240823
03/ 99/18 11:32 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-06-0318-G2
Lab Sample ID: 180-76196-6
Date Collected: 03/27/18 09:22
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 75.6
Batch Batch
Dil Initial Final Batch
Prepared
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
4.9 669 g 5 mL 240 003
03/ 99/18 09:21 KLG TAL PIT
Total/NA Analysis EPA 8260B
1 5 mL 5 mL 240896
03/30/18 16:36 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-06-0318-G3
Lab Sample ID: 180-76196-7
Date Collected: 03/27/18 09:25
Matrix: Sediment
Date Received: 03/28/18 11:36
Batch Batch
Dil Initial Final Batch
Prepared
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1 240823
03/ 99/18 11:32 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-06-0318-G3
Lab Sample ID: 180-76196-7
Date Collected: 03/27/18 09:25
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 79.3
Batch Batch
Dil Initial Final Batch
Prepared
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
4.9743 g 5 mL 240903
03/29/18 09:21 KLG TAL PIT
TestAmerica Pittsburgh
Page 11 of 106
4/18/2018

Lab Chronicle
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-06-0318-G3
Lab Sample
ID: 180-76196-7
Date Collected: 03/27/18 09:25
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 79.3
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis EPA 8260B
1
5 mL
5 mL
240896
03/30/18 17:00
KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-06-0318-C
Lab Sample
ID: 180-76196-8
Date Collected: 03/27/18 09:30
Matrix: Sediment ;
Date Received: 03/28/18 11:36
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis 2540G
1
240823
03/ 99/18 11:32
CLL TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis 7196A
1
241989
04/12/18 11:38
MM1 TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-06-0318-C
Lab Sample
ID: 180-76196-8
Date Collected: 03/27/18 09:30
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 81.5
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep 3541
30.3 g
0.5 mL
241 337
04/ 22/18 03:39
BAP TAL PIT
Total/NA Analysis 8270D LL
2
1 mL
1 mL
241401
04/05/18 18:34
DLF TAL PIT
Instrument ID: CH71
Total/NA Prep 3541
30.4 g
10.0 mL
241038
04/02/18 03:41
BAP TAL PIT
Total/NA Cleanup 3640A
5.0 mL
0.5 mL
241931
04/12/18 06:12
BAP TAL PIT
Total/NA Analysis 8081 B_LL
1
242257
04/16/18 14:10
DFE TAL PIT
Instrument ID: CHGC15
Total/NA Prep 3050B
2.00 g
100 mL
241695
04/09/18 16:04
KA TAL PIT
Total/NA Analysis 6020B
1
241911
04/11/18 02:05
WTR TAL PIT
Instrument ID: M
Total/NA Prep 7471 B
1.28 g
100 mL
241273
04/04/18 08:35
RJR TAL PIT
Total/NA Analysis 7471 B
1
241400
04/05/18 09:32
RJR TAL PIT
Instrument ID: K
Total/NA Prep 3060A
2.53 g
100 mL
240858
03/29/18 14:32
SES TAL PIT
Total/NA Analysis EPA 7196A
1
25 mL
25 mL
240949
03/30/18 13:19
SES TAL PIT
Instrument ID: GENESYS10S
Total/NA Prep 9071B
30.0 g
30.0 g
241004
03/31/18 06:25
CBY TAL PIT
Total/NA Analysis EPA 9071 B
1
241091
04/03/18 08:15
JAS TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis Lloyd Kahn
1
241158
04/02/18 15:05
JBF TAL PIT
Instrument ID: FLASHEA
TestAmerica Pittsburgh
Page 12 of 106 4/18/2018

Lab Chronicle
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-02-0318-G1
Lab Sample ID: 180-76196-9
Date Collected: 03/27/18 09:55
Matrix: Sediment
Date Received: 03/28/18 11:36
Batch Batch
Dil Initial Final Batch Prepared
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1 240823 03/ 99/18 11:32 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-02-0318-G1
Lab Sample ID: 180-76196-9
Date Collected: 03/27/18 09:55
Matrix: Sediment ;
Date Received: 03/28/18 11:36
Percent Solids: 78.4
Batch Batch
Dil Initial Final Batch Prepared C
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.1 779 g 5 mL 240 003 03/ 99/18 09:21 KLG TAL PIT
Total/NA Analysis EPA 8260B
1 5 mL 5 mL 240896 03/30/18 17:47 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-02-0318-G2
Lab Sample ID: 180-76196-10
Date Collected: 03/27/18 09:57
Matrix: Sediment
Date Received: 03/28/18 11:36
Batch Batch
Dil Initial Final Batch Prepared
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1 240823 03/ 99/18 11:32 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-02-0318-G2
Lab Sample ID: 180-76196-10
Date Collected: 03/27/18 09:57
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 59.7
Batch Batch
Dil Initial Final Batch Prepared
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.3332 g 5 mL 240 003 03/ 99/18 09:21 KLG TAL PIT
Total/NA Analysis EPA 8260B
1 5 mL 5 mL 240896 03/30/18 18:10 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-02-0318-G3
Lab Sample ID: 180-76196-11
Date Collected: 03/27/18 10:00
Matrix: Sediment
Date Received: 03/28/18 11:36
Batch Batch
Dil Initial Final Batch Prepared
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1 240823 03/ 99/18 11:32 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-02-0318-G3
Lab Sample ID: 180-76196-11
Date Collected: 03/27/18 10:00
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 46.5
Batch Batch
Dil Initial Final Batch Prepared
Prep Type Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.1891 g 5 mL 240903 03/29/18 09:21 KLG TAL PIT
TestAmerica Pittsburgh
Page 13 of 106 4/18/2018

Lab Chronicle
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-02-0318-G3
Lab Sample ID: 180-76196-11
Date Collected: 03/27/18 10:00
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 46.5
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis EPA 8260B
1
5 mL
5 mL
241049
04/02/18 10:27
KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-02-0318-C
Lab Sample ID: 180-76196-12
Date Collected: 03/27/18 10:05
Matrix: Sediment ;
Date Received: 03/28/18 11:36
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis 2540G
1
240823
03/ 99/18 11:32
CLL TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis 7196A
1
241989
04/12/18 11:38
MM1 TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-02-0318-C
Lab Sample ID: 180-76196-12
Date Collected: 03/27/18 10:05
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 57.2
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep 3541
30.2 g
0.5 mL
241 337
04/ 22/18 03:39
BAP TAL PIT
Total/NA Analysis 8270D LL
4
1 mL
1 mL
241401
04/05/18 19:02
DLF TAL PIT
Instrument ID: CH71
Total/NA Prep 3541
30.1 g
10.0 mL
241038
04/02/18 03:41
BAP TAL PIT
Total/NA Cleanup 3640A
5.0 mL
0.5 mL
241931
04/12/18 06:12
BAP TAL PIT
Total/NA Analysis 8081 B_LL
5
242257
04/16/18 14:56
DFE TAL PIT
Instrument ID: CHGC15
Total/NA Prep 3050B
1.95 g
100 mL
241695
04/09/18 16:04
KA TAL PIT
Total/NA Analysis 6020B
1
241911
04/11/18 02:09
WTR TAL PIT
Instrument ID: M
Total/NA Prep 7471B
1.31 g
100 mL
241273
04/04/18 08:35
RJR TAL PIT
Total/NA Analysis 7471 B
1
241400
04/05/18 09:34
RJR TAL PIT
Instrument ID: K
Total/NA Prep 3060A
2.55 g
100 mL
240858
03/29/18 14:32
SES TAL PIT
Total/NA Analysis EPA 7196A
1
25 mL
25 mL
240949
03/30/18 13:23
SES TAL PIT
Instrument ID: GENESYS10S
Total/NA Prep 9071B
30.1 g
30.0 g
241004
03/31/18 06:25
CBY TAL PIT
Total/NA Analysis EPA 9071 B
1
241091
04/03/18 08:15
JAS TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis Lloyd Kahn
1
241158
04/02/18 15:15
JBF TAL PIT
Instrument ID: FLASHEA
TestAmerica Pittsburgh
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Lab Chronicle
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-04-0318-G1
Lab Sample ID: 180-76196-13
Date Collected: 03/27/18 10:40
Matrix: Sediment
Date Received: 03/28/18 09:30
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240 993 03/ 99/18 08:42 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-04-0318-G1
Lab Sample ID: 180-76196-13
Date Collected: 03/27/18 10:40
Matrix: Sediment ;
Date Received: 03/28/18 09:30
Percent Solids: 39.2
Batch Batch
Dil Initial
Final Batch Prepared C
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.0511 g
5 mL 240 006 03/ 88/18 12:15 KLG TAL PIT
Total/NA Analysis EPA 8260B
1 5 mL
5 mL 240660 03/28/18 14:17 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-04-0318-G2
Lab Sample ID: 180-76196-14
Date Collected: 03/27/18 10:42
Matrix: Sediment
Date Received: 03/28/18 09:30
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240 993 03/ 99/18 08:42 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-04-0318-G2
Lab Sample ID: 180-76196-14
Date Collected: 03/27/18 10:42
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 39.1
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.0 115 g
5 mL 240 006 03/ 88/18 12:15 KLG TAL PIT
Total/NA Analysis EPA 8260B
1 5 mL
5 mL 240660 03/28/18 14:41 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-04-0318-G3
Lab Sample ID: 180-76196-15
Date Collected: 03/27/18 10:45
Matrix: Sediment
Date Received: 03/28/18 09:30
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240 993 03/ 99/18 08:42 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-04-0318-G3
Lab Sample ID: 180-76196-15
Date Collected: 03/27/18 10:45
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 46.9
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method
Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.0875 g
5 mL 240706 03/28/18 12:15 KLG TAL PIT
TestAmerica Pittsburgh
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Lab Chronicle
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-04-0318-G3
Lab Sample ID: 180-76196-15
Date Collected: 03/27/18 10:45
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 46.9
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis EPA 8260B
1
5 mL
5 mL
240660
03/28/18 15:04
KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-04-0318-C
Lab Sample ID: 180-76196-16
Date Collected: 03/27/18 10:50
Matrix: Sediment ;
Date Received: 03/28/18 09:30
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis 2540G
1
240 993
03/ 99/18 08:42
CLL TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis 7196A
1
241989
04/12/18 11:38
MM1 TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-04-0318-C
Lab Sample ID: 180-76196-16
Date Collected: 03/27/18 10:50
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 41.2
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep 3541
30.2 g
0.5 mL
241 337
04/ 22/18 03:39
BAP TAL PIT
Total/NA Analysis 8270D LL
5
1 mL
1 mL
241401
04/05/18 19:30
DLF TAL PIT
Instrument ID: CH71
Total/NA Prep 3541
30.1 g
10.0 mL
241038
04/02/18 03:41
BAP TAL PIT
Total/NA Cleanup 3640A
5.0 mL
0.5 mL
241931
04/12/18 06:12
BAP TAL PIT
Total/NA Analysis 8081 B_LL
5
242257
04/16/18 15:11
DFE TAL PIT
Instrument ID: CHGC15
Total/NA Prep 3050B
2.00 g
100 mL
241695
04/09/18 16:04
KA TAL PIT
Total/NA Analysis 6020B
1
241911
04/11/18 02:14
WTR TAL PIT
Instrument ID: M
Total/NA Prep 7471 B
1.33 g
100 mL
241273
04/04/18 08:35
RJR TAL PIT
Total/NA Analysis 7471 B
1
241400
04/05/18 09:36
RJR TAL PIT
Instrument ID: K
Total/NA Prep 3060A
2.53 g
100 mL
240858
03/29/18 14:32
SES TAL PIT
Total/NA Analysis EPA 7196A
1
25 mL
25 mL
240949
03/30/18 13:24
SES TAL PIT
Instrument ID: GENESYS10S
Total/NA Prep 9071B
30.2 g
30.0 g
241004
03/31/18 06:25
CBY TAL PIT
Total/NA Analysis EPA 9071 B
1
241091
04/03/18 08:15
JAS TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis Lloyd Kahn
1
240909
03/29/18 16:39
JBF TAL PIT
Instrument ID: FLASHEA
TestAmerica Pittsburgh
Page 16 of 106 4/18/2018

Lab Chronicle
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
F
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-05-0318-G1
Lab Sample ID: 180-76196-17
Date Collected: 03/27/18 11:35
Matrix: Sediment
Date Received: 03/28/18 09:30
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240 993 03/ 99/18 08:42 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-05-0318-G1
Lab Sample ID: 180-76196-17
Date Collected: 03/27/18 11:35
Matrix: Sediment ;
Date Received: 03/28/18 09:30
Percent Solids: 25.9
Batch Batch
Dil Initial
Final Batch Prepared C
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.0808 g
5 mL 240 006 03/ 88/18 12:15 KLG TAL PIT
Total/NA Analysis EPA 8260B
1 5 mL
5 mL 240660 03/28/18 15:28 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-05-0318-G1-DUP
Lab Sample ID: 180-76196-18
Date Collected: 03/27/18 11:37
Matrix: Sediment
Date Received: 03/28/18 09:30
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240 993 03/ 99/18 08:42 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-05-0318-G1-DUP
Lab Sample ID: 180-76196-18
Date Collected: 03/27/18 11:37
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 24.2
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.4377 g
5 mL 240 006 03/ 88/18 12:15 KLG TAL PIT
Total/NA Analysis EPA 8260B
1 5 mL
5 mL 240660 03/28/18 15:51 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-05-0318-G2
Lab Sample ID: 180-76196-19
Date Collected: 03/27/18 11:40
Matrix: Sediment
Date Received: 03/28/18 09:30
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240 993 03/ 99/18 08:42 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-05-0318-G2
Lab Sample ID: 180-76196-19
Date Collected: 03/27/18 11:40
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 28.4
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035 5.2324 g 5 mL 240706 03/28/18 12:15 KLG TAL PIT
TestAmerica Pittsburgh
Page 17 of 106 4/18/2018

Lab Chronicle
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-G2
Lab Sample ID: 180-76196-19
Date Collected: 03/27/18 11:40
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 28.4
Batch Batch
Dil
Initial
Final
Batch Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis EPA 8260B
1
5 mL
5 mL
240660 03/28/18 16:14 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-05-0318-G3
Lab Sample ID: 180-76196-20
Date Collected: 03/27/18 11:45
Matrix: Sediment ;
Date Received: 03/28/18 09:30
Batch Batch
Dil
Initial
Final
Batch Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240 993 03/ 99/18 08:42 CLL TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-05-0318-G3
Lab Sample ID: 180-76196-20
Date Collected: 03/27/18 11:45
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 16.8
Batch Batch
Dil
Initial
Final
Batch Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Prep 5035
4.9811 g
5 mL
240706 03/28/18 12:15 KLG TAL PIT
Total/NA Analysis EPA 8260E
1
5 mL
5 mL
240660 03/28/18 16:38 KLG TAL PIT
Instrument ID: CHHP3
Client Sample ID: AH-05-0318-C
Lab Sample ID: 180-76196-21
Date Collected: 03/27/18 11:55
Matrix: Sediment
Date Received: 03/28/18 09:30
Batch Batch
Dil
Initial
Final
Batch Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240 993 03/ 99/18 08:42 CLL TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis 7196A
1
241989 04/12/18 11:38 MM1 TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-05-0318-C
Lab Sample ID: 180-76196-21
Date Collected: 03/27/18 11:55
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 24.0
Batch Batch
DII
Initial
Final
Batch Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Prep 3541
30.4 g
0.5 mL
241037 04/02/18 03:39 BAP TAL PIT
Total/NA Analysis 8270D LL
5
1 mL
1 mL
241401 04/05/18 19:58 DLF TAL PIT
Instrument ID: CH71
Total/NA Prep 3541
30.4 g
10.0 mL
241038 04/02/18 03:41 BAP TAL PIT
Total/NA Cleanup 3640A
5.0 mL
0.5 mL
241931 04/12/18 06:12 BAP TAL PIT
Total/NA Analysis 8081 B_LL
5
242257 04/16/18 15:27 DFE TAL PIT
Instrument ID: CHGC15
Total/NA Prep 3050B
2.04 g
100 mL
241695 04/09/18 16:04 KA TAL PIT
TestAmerica Pittsburgh
Page
18 of 106
4/18/2018

Lab Chronicle
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-C
Date Collected: 03/27/18 11:55
Date Received: 03/28/18 09:30
Batch
Batch
Dil Initial
Prep Type
Type
Method
Run Factor Amount
Total/NA
Analysis
6020B
1
Instrument ID: M
Total/NA Prep 7471 B
Total/NA Analysis 7471 B
Instrument ID: K
Total/NA Prep 3060A
Total/NA Analysis EPA 7196A
Instrument ID: GENESYS10S
Total/NA Prep 9071 B
Total/NA Analysis EPA 9071 B
Instrument ID: NOEQUIP
Total/NA Analysis Lloyd Kahn
Instrument ID: FLASHEA
Client Sample ID: AH-05-0318-C-DUP
Date Collected: 03/27/18 11:58
Date Received: 03/28/18 09:30
1.21 g
2.55 g
1 25 mL
30.0 g
1
1
F
TestAmerica Job ID: 180-76196-1
Lab Sample ID: 180-76196-21
Matrix: Sediment
Percent Solids: 24.0
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
241911
04/11/18 02:19
WTR
TAL PIT
100 mL
241273
04/04/18 08:35
RJR
TAL PIT
241400
04/05/18 09:42
RJR
TAL PIT
100 mL
240858
03/29/18 14:32
SES
TAL PIT
25 mL
240949
03/30/18 13:30
SES
TAL PIT
30.0 g
241004
03/31/18 06:25
CBY
TAL PIT
241091
04/03/18 08:15
JAS
TAL PIT
240909
03/29/18 16:49
JBF
TAL PIT
Lab Sample ID: 180-76196-22 C
Matrix: Sediment
Batch Batch
Dil Initial
Final Batch
Prepared
Prep Type Type Method
Run Factor Amount
Amount Number
or Analyzed Analyst Lab
Total/NA Analysis 2540G
1
240793
03/29/18 08:42 CLL TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis 7196A
1
241989
04/12/18 11:38 MM1 TAL PIT
Instrument ID: NOEQUIP
Client Sample ID: AH-05-0318-C-DUP
Date Collected: 03/27/18 11:58
Date Received: 03/28/18 09:30
Lab Sample ID: 180-76196-22
Matrix: Sediment
Percent Solids: 23.9
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Prep 3541
30.0 g
0.5 mL
241037
04/02/18 03:39
BAP
TAL PIT
Total/NA
Analysis 8270D LL
4
1 mL
1 mL
241401
04/05/18 20:26
DLF
TAL PIT
Instrument ID: CH71
Total/NA
Prep 3541
30.3 g
10.0 mL
241038
04/02/18 03:41
BAP
TAL PIT
Total/NA
Cleanup 3640A
5.0 mL
0.5 mL
241931
04/12/18 06:12
BAP
TAL PIT
Total/NA
Analysis 8081 B_LL
5
242257
04/16/18 17:15
DFE
TAL PIT
Instrument ID: CHGC15
Total/NA
Prep 3050B
1.95 g
100 mL
241695
04/09/18 16:04
KA
TAL PIT
Total/NA
Analysis 6020B
1
241911
04/11/18 02:23
WTR
TAL PIT
Instrument ID: M
Total/NA
Prep 7471 B
1.19 g
100 mL
241273
04/04/18 08:35
RJR
TAL PIT
Total/NA
Analysis 7471 B
1
241400
04/05/18 09:44
RJR
TAL PIT
Instrument ID: K
Total/NA Prep 3060A 2.50 g 100 mL 240858 03/29/18 14:43 SES TAL PIT
Page 19 of 106
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4/18/2018

Lab Chronicle
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-C-DUP
Date Collected: 03/27/18 11:58
Date Received: 03/28/18 09:30
F
TestAmerica Job ID: 180-76196-1
Lab Sample ID: 180-76196-22
Matrix: Sediment
Percent Solids: 23.9
Batch Batch
Dil
Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number or Analyzed
Analyst Lab
Total/NA Analysis EPA 7196A
1
25 mL
25 mL
240949 03/30/18 13:31
SES TAL PIT
Instrument ID: GENESYS10S
Total/NA Prep 9071B
30.0 g
30.0 g
241004 03/31/18 06:25
CBY TAL PIT
Total/NA Analysis EPA 9071 B
1
241091 04/03/18 08:15
JAS TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis Lloyd Kahn
1
240909 03/29/18 16:59
JBF TAL PIT
Instrument ID: FLASHER
Client Sample ID: TB-02-0318
Lab Sample ID: 180-76196-23
Date Collected: 03/27/18 12:30
Matrix: Water
Date Received: 03/28/18 09:30
Batch Batch
Dil
Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number or Analyzed
Analyst Lab
Total/NA Analysis EPA 8260E
1
5 mL
5 mL
240736 03/28/18 21:15
FBB TAL PIT
Instrument ID: CHHP5
Client Sample ID: EB-02-0318
Lab Sample ID: 180-76196-24
Date Collected: 03/27/18 12:50
Matrix: Water
Date Received: 03/28/18 09:30
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis EPA 8260B
1
5 mL
5 mL
240865
03/29/18 21:47
KLG
TAL PIT
Instrument ID: CHHP6
Total/NA
Prep 3520C
240 mL
250 uL
241088
04/02/18 11:29
BJT
TAL PIT
Total/NA
Analysis EPA 8270D LL
1
1 mL
1 mL
241375
04/06/18 00:27
VVP
TAL PIT
Instrument ID: CH733
Total/NA
Prep 3510C
980 mL
1.0 mL
240746
03/28/18 12:35
CBY
TAL PIT
Total/NA
Analysis EPA 8081 B LL
1
241080
04/02/18 19:49
DFE
TAL PIT
Instrument ID: CHGC15
Total Recoverable
Prep 3005A
50 mL
50 mL
240953
03/30/18 13:04
KA
TAL PIT
Total Recoverable
Analysis EPA 6020E
1
241140
03/31/18 12:37
RSK
TAL PIT
Instrument ID: A
Total/NA
Prep 7470A
50.0 mL
50.0 mL
241732
04/10/18 11:20
RSK
TAL PIT
Total/NA
Analysis EPA 7470A
1
241904
04/11/18 11:08
RSK
TAL PIT
Instrument ID: K
Total/NA
Prep 1664B
986 mL
1000 mL
392275
04/01/18 14:43
BAW
TAL PEN
Total/NA
Analysis 1664B
1
392295
04/02/18 09:06
BAW
TAL PEN
Instrument ID: SPEEDVAP
Total/NA
Analysis 7196A
1
241989
04/12/18 11:38
MM1
TAL PIT
Instrument ID: NOEQUIP
Total/NA
Analysis EPA 7196A
1
25 mL
25 mL
240705
03/28/18 12:08
SES
TAL PIT
Instrument ID: GENESYS10S
Total/NA
Analysis SM 5310C
1
241245
04/03/18 17:12
CLL
TAL PIT
Instrument ID: TOC1030
Page 20 of 106
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4/18/2018

Lab Chronicle C
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
Analyst References:
Lab: TAL PEN
Batch Type: Prep
BAW = Benjamin Whatley
Batch Type: Analysis
BAW = Benjamin Whatley
Lab: TAL PIT
Batch Type: Cleanup
BAP = Brian Pino
Batch Type: Prep
BAP = Brian Pino
BJT = Bill Trout
CBY = Charles Yushinski
KA = Kayla Kalamasz
KLG = Kathy Gordon
RJR = Ron Rosenbaum
RSK = Robert Kurtz
SES = Samantha Strauser
Batch Type: Analysis
CLL = Cheryl Loheyde
DFE = David Eppinger
DLF = Donald Ferguson
FBB = Frank Bungard
JAS = Joshua Schmidt
JBF = Joshua Fritsch
KLG = Kathy Gordon
MM1 = Mary Beth Miller
RJR = Ron Rosenbaum
RSK = Robert Kurtz
SES = Samantha Strauser
VVP = Vincent Piccolino
WTR = Bill Reinheimer
TestAmerica Pittsburgh
Page 21 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-07-0318-G1
Date Collected: 03/27/18 08:40
Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result
Qualifier
RL
1, 1, 1 -Trichloroethane
ND
H
6.2
1,1,2,2-Tetrachloroethane
ND
H
6.2
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
H
6.2
1,1,2-Trichloroethane
ND
H
6.2
1,1-Dichloroethane
ND
H
6.2
1,1-Dichloroethene
ND
H
6.2
1,2,4-Trichlorobenzene
ND
H
6.2
1,2-Dibromo-3-Chloropropane
ND
H
6.2
1,2-Dichlorobenzene
ND
H
6.2
1,2-Dichloroethane
ND
H
6.2
1,2-Dichloropropane
ND
H
6.2
1,3-Dichlorobenzene
ND
H
6.2
1,4-Dichlorobenzene
ND
H
6.2
2-Butanone (MEK)
ND
H
6.2
2-Hexanone
ND
H
6.2
4-Methyl-2-pentanone (MIBK)
ND
H
6.2
Acetone
ND
H
25
Benzene
ND
H
6.2
Bromoform
ND
H
6.2
Bromomethane
ND
H
6.2
Carbon disulfide
ND
H
6.2
Carbon tetrachloride
ND
H
6.2
Chlorobenzene
ND
H
6.2
Chlorodibromomethane
ND
H
6.2
Chloroform
ND
H
6.2
Chloromethane
ND
H
6.2
Chloroethane
ND
H
6.2
cis- 1,2-Dichloroethene
ND
H
6.2
cis- 1,3-Dichloropropene
ND
H
6.2
Cyclohexane
ND
H
6.2
Dichlorobromomethane
ND
H
6.2
Dichlorodifluoromethane
ND
H
6.2
Ethylbenzene
ND
H
6.2
1,2-Dibromoethane
ND
H
6.2
Isopropylbenzene
ND
H
6.2
Methyl acetate
ND
H
31
Methyl tert-butyl ether
ND
H
6.2
Methylcyclohexane
ND
H
6.2
Methylene Chloride
ND
H
6.2
Styrene
ND
H
6.2
Tetrachloroethene
ND
H
6.2
Toluene
ND
H
6.2
trans- 1,2-Dichloroethene
ND
H
6.2
trans- 1,3-Dichloropropene
ND
H
6.2
Trichloroethene
ND
H
6.2
Trichlorofluoromethane
ND
H
6.2
Xylenes, Total
ND
H
12
Vinyl chloride
ND
H
6.2
TestAmerica Job ID: 180-76196-1
Lab Sample ID: 180-76196-1
Matrix: Sediment
Percent Solids: 77.6
MDL
Unit
D
Prepared
Analyzed
Dil Fac
3.1
6g/Kg
�
03/29/18 09:21
03/30/18 15:26
1
3.7
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.4
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.0
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.2
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.5
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.0
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.8
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
5.0
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
1.8
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.0
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.0
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
1.3
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.6
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
5.2
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.3
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.9
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.4
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.2
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
5.6
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.7
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
4.1
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.0
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.0
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.6
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
4.8
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.2
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.0
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.0
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
1.5
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.9
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.6
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.7
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.4
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.9
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
7.3
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
4.6
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.6
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.9
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
1.7
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.5
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.1
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
3.1
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
2.1
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
1.9
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
1.8
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
5.3
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
4.5
ug/Kg
03/29/18 09:21
03/30/18 15:26
1
TestAmerica Pittsburgh
Page 22 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-07-0318-G1
Lab Sample ID: 180-76196-1
Date Collected: 03/27/18 08:40
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 77.6
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 92
62- 118
03129118 09:21 03130118 15:26 1
4-Bromofluorobenzene (Surr) 95
76 - 111
03129118 09:21 03130118 15:26 1
Dibromofluoromethane (Surr) 95
72 - 116
03129118 09:21 03130118 15:26 1
Toluene-d8 (Surr) 107
80 - 129
03/29/18 09:21 03130118 15:26 1
General Chemistry
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Percent Moisture 22.4
0.1 0.1 %
03/29/18 11:32 1
Percent Solids 77.6
0.1 0.1 %
03/29/18 11:32 1 �.
Client Sample ID: AH-07-0318-G2
Lab Sample ID: 180-76196-2
Date Collected: 03/27/18 08:42
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 77.4
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
H
6.4
3.2
ug/Kg
3:�
03/29/18 09:21
03/30/18 17:23
1
1,1,2,2-Tetrachloroethane
ND
H
6.4
3.8
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
H
6.4
2.4
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,1,2-Trichloroethane
ND
H
6.4
3.1
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,1-Dichloroethane
ND
H
6.4
2.3
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,1-Dichloroethene
ND
H
6.4
3.6
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,2,4-Trichlorobenzene
ND
H
6.4
2.1
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,2-Dibromo-3-Chloropropane
ND
H
6.4
3.9
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,2-Dichlorobenzene
ND
H
6.4
5.1
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,2-Dichloroethane
ND
H
6.4
1.9
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,2-Dichloropropane
ND
H
6.4
3.1
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,3-Dichlorobenzene
ND
H
6.4
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,4-Dichlorobenzene
ND
H
6.4
1.3
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
2-Butanone (MEK)
ND
H
6.4
3.7
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
2-Hexanone
ND
H
6.4
5.3
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
4-Methyl-2-pentanone (MIBK)
ND
H
6.4
2.4
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Acetone
ND
H
26
4.0
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Benzene
ND
H
6.4
2.5
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Bromoform
ND
H
6.4
3.3
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Bromomethane
ND
H
6.4
5.7
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Carbon disulfide
ND
H
6.4
3.8
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Carbon tetrachloride
ND
H
6.4
4.2
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Chlorobenzene
ND
H
6.4
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Chlorodibromomethane
ND
H
6.4
3.1
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Chloroform
ND
H
6.4
2.7
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Chloromethane
ND
H
6.4
4.9
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Chloroethane
ND
H
6.4
3.3
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
cis-1,2-Dichloroethene
ND
H
6.4
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
cis-1,3-Dichloropropene
ND
H
6.4
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Cyclohexane
ND
H
6.4
1.6
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Dichlorobromomethane
ND
H
6.4
3.0
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Dichlorodifluoromethane
ND
H
6.4
3.7
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Ethylbenzene
ND
H
6.4
2.7
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
1,2-Dibromoethane
ND
H
6.4
3.5
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
TestAmerica Pittsburgh
Page 23 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-07-0318-G2 Lab Sample ID: 180-76196-2
Date Collected: 03/27/18 08:42 Matrix: Sediment
Date Received: 03/28/18 11:36 Percent Solids: 77.4
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Isopropylbenzene
ND
H
6.4
3.0
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Methyl acetate
ND
H
32
7.5
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Methyl tert-butyl ether
ND
H
6.4
4.7
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Methylcyclohexane
ND
H
6.4
2.7
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Methylene Chloride
ND
H
6.4
3.0
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Styrene
ND
H
6.4
1.7
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Tetrachloroethene
ND
H
6.4
2.6
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Toluene
ND
H
6.4
2.2
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
trans- 1,2-Dichloroethene
ND
H
6.4
3.2
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
trans-1,3-Dichloropropene
ND
H
6.4
2.2
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Trichloroethene
ND
H
6.4
1.9
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Trichlorofluoromethane
ND
H
6.4
1.9
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Xylenes, Total
ND
H
13
5.5
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Vinyl chloride
ND
H
6.4
4.7
ug/Kg
03/29/18 09:21
03/30/18 17:23
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1, 2-Dichloroethane-d4 (Surr)
95
62 - 118
03/29/18 09:21
03130118 17:23
1
4-Bromofluorobenzene (Surr)
96
76 - 111
03/29/18 09:21
03130118 17:23
1
Dibromofluoromethane (Surr)
96
72 - 116
03/29/18 09:21
03130118 17:23
1
Toluene-d8 (Surr)
110
80 - 129
03/29/18 09:21
03130118 17:23
1
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Percent Moisture 22.6 0.1 0.1 % 03/29/18 11:32 1
Percent Solids 77.4 0.1 0.1 % 03/29/18 11:32 1
Client Sample ID: AH-07-0318-G3 Lab Sample ID: 180-76196-3
Date Collected: 03/27/18 08:45 Matrix: Sediment
Date Received: 03/28/18 11:36 Percent Solids: 83.8
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
H
5.8
2.9
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,1,2,2-Tetrachloroethane
ND
H
5.8
3.5
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
H
5.8
2.2
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,1,2-Trichloroethane
ND
H
5.8
2.8
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,1-Dichloroethane
ND
H
5.8
2.1
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,1-Dichloroethene
ND
H
5.8
3.3
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,2,4-Trichlorobenzene
ND
H
5.8
1.9
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,2-Dibromo-3-Chloropropane
ND
H
5.8
3.6
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,2-Dichlorobenzene
ND
H
5.8
4.7
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,2-Dichloroethane
ND
H
5.8
1.7
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,2-Dichloropropane
ND
H
5.8
2.9
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,3-Dichlorobenzene
ND
H
5.8
1.9
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,4-Dichlorobenzene
ND
H
5.8
1.2
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
2-Butanone (MEK)
ND
H
5.8
3.4
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
2-Hexanone
ND
H
5.8
4.9
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
4-Methyl-2-pentanone (MIBK)
ND
H
5.8
2.2
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Acetone
ND
H
23
3.7
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Benzene
ND
H
5.8
2.3
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
TestAmerica Pittsburgh
Page 24 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-07-0318-G3
Lab Sample ID: 180-76196-3
Date Collected: 03/27/18 08:45
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
83.8
Method: EPA 8260B - Volatile Organic Compounds
(GC/MS) (Continued)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Bromoform
ND
H
5.8
3.0
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Bromomethane
ND
H
5.8
5.2
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Carbon disulfide
ND
H
5.8
3.5
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Carbon tetrachloride
ND
H
5.8
3.9
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Chlorobenzene
ND
H
5.8
1.8
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Chlorodibromomethane
ND
H
5.8
2.8
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Chloroform
ND
H
5.8
2.5
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Chloromethane
ND
H
5.8
4.5
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Chloroethane
ND
H
5.8
3.0
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
cis-1,2-Dichloroethene
ND
H
5.8
1.8
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
cis-1,3-Dichloropropene
ND
H
5.8
1.9
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Cyclohexane
ND
H
5.8
1.4
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Dichlorobromomethane
ND
H
5.8
2.7
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Dichlorodifluoromethane
ND
H
5.8
3.4
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Ethylbenzene
ND
H
5.8
2.5
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
1,2-Dibromoethane
ND
H
5.8
3.2
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Isopropylbenzene
ND
H
5.8
2.7
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Methyl acetate
ND
H
29
6.9
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Methyl tert-butyl ether
ND
H
5.8
4.3
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Methylcyclohexane
ND
H
5.8
2.4
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Methylene Chloride
ND
H
5.8
2.7
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Styrene
ND
H
5.8
1.6
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Tetrachloroethene
ND
H
5.8
2.3
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Toluene
ND
H
5.8
2.0
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
trans-1,2-Dichloroethene
ND
H
5.8
3.0
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
trans- 1,3-Dichloropropene
ND
H
5.8
2.0
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Trichloroethene
ND
H
5.8
1.7
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Trichlorofluoromethane
ND
H
5.8
1.7
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Xylenes, Total
ND
H
12
5.0
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Vinyl chloride
ND
H
5.8
4.3
ug/Kg
03/29/18 09:21
04/02/18 09:40
1
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
91
62 - 118
03/29/18 09:21
04102118 09:40
1
4-Bromofluorobenzene (Surr)
94
76 - 111
03/29/18 09:21
04102118 09:40
1
Dibromofluoromethane (Surr)
97
72 - 116
03/29/18 09:21
04102118 09:40
1
Toluene-d8 (Surr)
109
80 - 129
03/29/18 09:21
04102118 09:40
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Percent Moisture
16.2
0.1
0.1
%
03/29/18 11:32
1
Percent Solids
83.8
0.1
0.1
%
03/29/18 11:32
1
Client Sample ID: AH-07-0318-C
Lab Sample ID: 180-76196-4
Date Collected: 03/27/18 08:50
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
81.0
Method: 8270D ILL - Semivolatile Organic
Compounds
by GC/MS - Low Level
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Acenaphthene
ND
8.2
2.4
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Acenaphthylene
ND
8.2
1.8
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
TestAmerica Pittsburgh
Page 25 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-07-0318-C
Lab Sample ID: 180-76196-4
Date Collected: 03/27/18 08:50
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
81.0
Method: 8270D LL - Semivolatile Organic Compounds
by GC/MS - Low Level (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Anthracene
ND
8.2
2.1
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Benzo[a]anthracene
ND
8.2
1.6
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Benzo[a]pyrene
ND
8.2
1.8
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Benzo[b]fluoranthene
ND
8.2
2.0
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Benzo[g,h,i]perylene
ND
8.2
1.8
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Chrysene
ND
8.2
1.6
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Dibenz(a,h)anthracene
ND
8.2
1.8
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Fluoranthene
ND
8.2
2.2
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Fluorene
ND
8.2
1.6
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Indeno[1,2,3-cd]pyrene
ND
8.2
1.7
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Naphthalene
ND
8.2
1.6
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Phenanthrene
ND
8.2
2.2
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Pyrene
ND
8.2
1.9
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Benzo[k]fluoranthene
ND
8.2
2.5
ug/Kg
04/02/18 03:39
04/05/18 15:20
2
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
84
34 - 100
04102118 03:39
04105118 15:20
2
Nitrobenzene-d5 (Surr)
93
33 - 100
04102118 03:39
04105118 15:20
2
Terphenyl-d14 (Surr)
76
30- 100
04102118 03:39
04105118 15:20
2
Method: 8081B_LL - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Aldrin
ND
0.051
0.016
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
alpha-BHC
ND
0.051
0.013
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
cis -Chlordane
ND
0.051
0.013
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
beta-BHC
ND
0.051
0.013
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Chlordane (technical)
ND
0.51
0.22
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
4,4'-DDD
ND
0.051
0.014
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
4,4'-DDE
ND
0.051
0.010
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
4,4'-DDT
ND
0.051
0.019
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
delta-BHC
ND
0.051
0.016
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Dieldrin
ND
0.051
0.013
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Endosulfan I
ND
0.051
0.014
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Endosulfan 11
ND
0.051
0.011
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Endosulfan sulfate
ND
0.051
0.013
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Endrin
ND
0.051
0.020
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Endrin aldehyde
ND
0.051
0.018
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Endrin ketone
ND
0.051
0.018
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
gamma-BHC (Lindane)
ND
0.051
0.017
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
trans -Chlordane
ND
0.051
0.012
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Heptachlor
ND
0.051
0.016
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Heptachlor epoxide
ND
0.051
0.013
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Methoxychlor
ND
0.051
0.020
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
oxy-Chlordane
0.012 J p
0.051
0.011
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Toxaphene
ND
2.0
1.4
ug/Kg
04/02/18 03:41
04/16/18 13:54
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl (Surr)
62
33 - 137
04102118 03:41
04116118 13:54
1
DCB Decachlorobiphenyl (Surr)
62
33 - 137
04102118 03:41
04116118 13:54
1
Tetrachloro-m-xylene
59
26 - 120
04102118 03:41
04116118 13:54
1
TestAmerica Pittsburgh
Page 26 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment
Project
Client Sample ID: AH-07-0318-C
Lab Sample ID: 180-76196-4
Date Collected: 03/27/18 08:50
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
81.0
Method: 8081B_LL - Organochlorine Pesticides
(GC) (Continued)
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
66
26 - 120
04102118 03:41
04116118 13:54
1
Method: 6020B - Metals (ICP/MS)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Antimony
ND
0.12
0.038
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Arsenic
0.75
0.062
0.016
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Beryllium
0.054
J
0.062
0.0047
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Cadmium
0.011
J
0.062
0.010
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Chromium
3.1
0.12
0.041
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Copper
0.73
0.12
0.070
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Lead
1.5
0.062
0.022
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Manganese
9.5
0.31
0.099
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Nickel
1.2
0.062
0.038
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Selenium
0.037
J
0.31
0.037
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Silver
ND
0.062
0.0086
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Thallium
0.023
J
0.062
0.0080
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Zinc
2.9
0.31
0.21
mg/Kg
04/09/18 16:04
04/11/18 02:00
1
Method: 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
ND
0.019
0.0041
mg/Kg
04/04/18 08:35
04/05/18 09:30
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Percent Moisture
19.0
0.1
0.1
%
03/29/18 11:32
1
Percent Solids
81.0
0.1
0.1
%
03/29/18 11:32
1
Cr (III)
2.9
0.50
0.11
mg/Kg
04/12/18 11:38
1
Cr (VI)
0.19
J
0.50
0.14
mg/Kg
03/29/18 14:32
03/30/18 13:18
1
Total Petroleum Hydrocarbons
ND
210
100
mg/Kg
03/31/18 06:25
04/03/18 08:15
1
(SGT-HEM)
Total Organic Carbon - Duplicates
2700
1200
920
mg/Kg
04/02/18 14:55
1
Client Sample ID: AH-06-0318-G1
Lab Sample ID: 180-76196-5
Date Collected: 03/27/18 09:20
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
78.9
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
H
5.9
2.9
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,1,2,2-Tetrachloroethane
ND
H
5.9
3.5
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
H
5.9
2.2
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,1,2-Trichloroethane
ND
H
5.9
2.8
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,1-Dichloroethane
ND
H
5.9
2.1
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,1-Dichloroethene
ND
H
5.9
3.3
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,2,4-Trichoorobenzene
ND
H
5.9
1.9
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,2-Dibromo-3-Chloropropane
ND
H
5.9
3.6
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,2-Dichlorobenzene
ND
H
5.9
4.7
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,2-Dichloroethane
ND
H
5.9
1.7
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,2-Dichloropropane
ND
H
5.9
2.9
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,3-Dichlorobenzene
ND
H
5.9
1.9
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
TestAmerica Pittsburgh
Page 27 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-06-0318-G1
Lab Sample ID: 180-76196-5
Date Collected: 03/27/18 09:20
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
78.9
Method: EPA 8260B - Volatile Organic Compounds
(GC/MS) (Continued)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,4-Dichlorobenzene
ND
H
5.9
1.2
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
2-Butanone (MEK)
ND
H
5.9
3.4
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
2-Hexanone
ND
H
5.9
4.9
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
4-Methyl-2-pentanone (MIBK)
ND
H
5.9
2.2
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Acetone
ND
H
23
3.7
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Benzene
ND
H
5.9
2.3
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Bromoform
ND
H
5.9
3.1
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Bromomethane
ND
H
5.9
5.3
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Carbon disulfide
ND
H
5.9
3.5
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Carbon tetrachloride
ND
H
5.9
3.9
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Chlorobenzene
ND
H
5.9
1.8
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Chlorodibromomethane
ND
H
5.9
2.8
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Chloroform
ND
H
5.9
2.5
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Chloromethane
ND
H
5.9
4.5
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Chloroethane
ND
H
5.9
3.0
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
cis-1,2-Dichloroethene
ND
H
5.9
1.8
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
cis-1,3-Dichloropropene
ND
H
5.9
1.9
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Cyclohexane
ND
H
5.9
1.4
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Dichlorobromomethane
ND
H
5.9
2.8
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Dichlorodifluoromethane
ND
H
5.9
3.4
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Ethylbenzene
ND
H
5.9
2.5
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
1,2-Dibromoethane
ND
H
5.9
3.2
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Isopropylbenzene
ND
H
5.9
2.7
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Methyl acetate
ND
H
29
6.9
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Methyl tert-butyl ether
ND
H
5.9
4.3
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Methylcyclohexane
ND
H
5.9
2.5
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Methylene Chloride
ND
H
5.9
2.8
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Styrene
ND
H
5.9
1.6
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Tetrachloroethene
ND
H
5.9
2.3
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Toluene
ND
H
5.9
2.0
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
trans- 1,2-Dichloroethene
ND
H
5.9
3.0
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
trans- 1,3-Dichloropropene
ND
H
5.9
2.0
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Trichloroethene
ND
H
5.9
1.8
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Trichlorofluoromethane
ND
H
5.9
1.7
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Xylenes, Total
ND
H
12
5.1
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Vinyl chloride
ND
H
5.9
4.3
ug/Kg
03/29/18 09:21
03/30/18 16:13
1
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
99
62- 118
03/29/18 09:21
03130118 16:13
1
4-Bromofluorobenzene (Surr)
93
76 - 111
03/29/18 09:21
03130118 16:13
1
Dibromofluoromethane (Surr)
99
72 - 116
03/29/18 09:21
03130118 16:13
1
Toluene-d8 (Surr)
110
80 - 129
03/29/18 09:21
03130118 16:13
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Percent Moisture
21.1
0.1
0.1
%
03/29/18 11:32
1
Percent Solids
78.9
0.1
0.1
%
03/29/18 11:32
1
TestAmerica Pittsburgh
Page 28 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-06-0318-G2
Date Collected: 03/27/18 09:22
Date Received: 03/28/18 11:36
TestAmerica Job ID: 180-76196-1
Lab Sample ID: 180-76196-6
Matrix: Sediment
Percent Solids: 75.6
Method: EPA 8260B - Volatile Organic
Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
6.7
3.3
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,1,2,2-Tetrachloroethane
ND
6.7
4.0
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
6.7
2.5
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,1,2-Trichloroethane
ND
6.7
3.2
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,1-Dichloroethane
ND
6.7
2.4
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,1-Dichloroethene
ND
6.7
3.8
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,2,4-Trichlorobenzene
ND
6.7
2.1
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,2-Dibromo-3-Chloropropane
ND
6.7
4.1
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,2-Dichlorobenzene
ND
6.7
5.4
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,2-Dichloroethane
ND
6.7
1.9
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,2-Dichloropropane
ND
6.7
3.3
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,3-Dichlorobenzene
ND
6.7
2.1
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,4-Dichlorobenzene
ND
6.7
1.4
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
2-Butanone (MEK)
ND
6.7
3.9
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
2-Hexanone
ND
6.7
5.6
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
4-Methyl-2-pentanone (MIBK)
ND
6.7
2.5
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Acetone
ND
27
4.2
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Benzene
ND
6.7
2.6
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Bromoform
ND
6.7
3.5
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Bromomethane
ND
6.7
6.0
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Carbon disulfide
ND
6.7
4.0
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Carbon tetrachloride
ND
6.7
4.4
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Chlorobenzene
ND
6.7
2.1
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Chlorodibromomethane
ND
6.7
3.2
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Chloroform
ND
6.7
2.8
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Chloromethane
ND
6.7
5.1
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Chloroethane
ND
6.7
3.4
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
cis-1,2-Dichloroethene
ND
6.7
2.1
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
cis-1,3-Dichloropropene
ND
6.7
2.1
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Cyclohexane
ND
6.7
1.6
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Dichlorobromomethane
ND
6.7
3.1
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Dichlorodifluoromethane
ND
6.7
3.9
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Ethylbenzene
ND
6.7
2.9
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
1,2-Dibromoethane
ND
6.7
3.6
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Isopropylbenzene
ND
6.7
3.1
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Methyl acetate
ND
33
7.9
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Methyl tert-butyl ether
ND
6.7
4.9
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Methylcyclohexane
ND
6.7
2.8
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Methylene Chloride
ND
6.7
3.1
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Styrene
ND
6.7
1.8
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Tetrachloroethene
ND
6.7
2.7
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Toluene
ND
6.7
2.2
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
trans- 1,2-Dichloroethene
ND
6.7
3.4
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
trans- 1,3-Dichloropropene
ND
6.7
2.3
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Trichloroethene
ND
6.7
2.0
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Trichlorofluoromethane
ND
6.7
1.9
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Xylenes, Total
ND
13
5.7
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
Vinyl chloride
ND
6.7
4.9
ug/Kg
03/29/18 09:21
03/30/18 16:36
1
TestAmerica Pittsburgh
Page 29 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-06-0318-G2
Date Collected: 03/27/18 09:22
Date Received: 03/28/18 11:36
Surrogate
%Recovery Qualifier
1,2-Dichloroethane-d4 (Surr)
94
4-Bromofluorobenzene (Surr)
95
Dibromofluoromethane (Surr)
98
Toluene-d8 (Surr)
108
General Chemistry
Analyte
Result Qualifier
Percent Moisture
24.4
Percent Solids
75.6
Client Sample ID: AH-06-0318-G3
Date Collected: 03/27/18 09:25
Date Received: 03/28/18 11:36
TestAmerica Job ID: 180-76196-1
Lab Sample ID: 180-76196-6
Matrix: Sediment
Percent Solids: 75.6
Limits
62-118
76-111
72-116
80-129
RL MDL Unit D
0.1 0.1 %
0.1 0.1 %
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Prepared
Analyzed
DU Fac
03/29/18 09:21
03130118 16:36
1
03/29/18 09:21
03130118 16:36
1
03/29/18 09:21
03130118 16:36
1
03/29/18 09:21
03130118 16:36
1
Prepared Analyzed Dil Fac
03/29/1811:32 1
03/29/1811:32 1
Lab Sample ID: 180-76196-7
Matrix: Sediment
Percent Solids: 79.3
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
6.3
3.2
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,1,2,2-Tetrachloroethane
ND
6.3
3.8
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
6.3
2.4
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,1,2-Trichloroethane
ND
6.3
3.0
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,1-Dichloroethane
ND
6.3
2.3
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,1-Dichloroethene
ND
6.3
3.6
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,2,4-Trichlorobenzene
ND
6.3
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,2-Dibromo-3-Chloropropane
ND
6.3
3.9
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,2-Dichlorobenzene
ND
6.3
5.1
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,2-Dichloroethane
ND
6.3
1.8
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,2-Dichloropropane
ND
6.3
3.1
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,3-Dichlorobenzene
ND
6.3
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,4-Dichlorobenzene
ND
6.3
1.3
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
2-Butanone (MEK)
ND
6.3
3.7
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
2-Hexanone
ND
6.3
5.3
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
4-Methyl-2-pentanone (MIBK)
ND
6.3
2.4
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Acetone
ND
25
4.0
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Benzene
ND
6.3
2.5
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Bromoform
ND
6.3
3.3
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Bromomethane
ND
6.3
5.7
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Carbon disulfide
ND
6.3
3.8
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Carbon tetrachloride
ND
6.3
4.2
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Chlorobenzene
ND
6.3
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Chlorodibromomethane
ND
6.3
3.0
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Chloroform
ND
6.3
2.7
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Chloromethane
ND
6.3
4.9
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Chloroethane
ND
6.3
3.3
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
cis- 1,2-Dichloroethene
ND
6.3
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
cis- 1,3-Dichloropropene
ND
6.3
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Cyclohexane
ND
6.3
1.5
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Dichlorobromomethane
ND
6.3
3.0
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Dichlorodifluoromethane
ND
6.3
3.7
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Ethylbenzene
ND
6.3
2.7
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
1,2-Dibromoethane
ND
6.3
3.5
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Page 30 of 106
TestAmerica Pittsburgh
4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-06-0318-G3
Lab Sample ID: 180-76196-7
Date Collected: 03/27/18 09:25
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
79.3
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Isopropylbenzene
ND
6.3
2.9
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Methyl acetate
ND
32
7.5
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Methyl tert-butyl ether
ND
6.3
4.7
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Methylcyclohexane
ND
6.3
2.7
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Methylene Chloride
ND
6.3
3.0
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Styrene
ND
6.3
1.7
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Tetrachloroethene
ND
6.3
2.5
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Toluene
ND
6.3
2.1
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
trans- 1,2-Dichloroethene
ND
6.3
3.2
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
trans- 1,3-Dichloropropene
ND
6.3
2.2
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Trichloroethene
ND
6.3
1.9
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Trichlorofluoromethane
ND
6.3
1.8
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Xylenes, Total
ND
13
5.5
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Vinyl chloride
ND
6.3
4.7
ug/Kg
03/29/18 09:21
03/30/18 17:00
1
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
94
62- 118
03/29/18 09:21
03130118 17:00
1
4-Bromofluorobenzene (Surr)
92
76 - 111
03/29/18 09:21
03/30/18 17:00
1
Dibromofluoromethane (Surr)
95
72 - 116
03/29/18 09:21
03130118 17:00
1
Toluene-d8 (Surr)
108
80 - 129
03/29/18 09:21
03130118 17:00
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Percent Moisture
20.7
0.1
0.1
%
03/29/18 11:32
1
Percent Solids
79.3
0.1
0.1
%
03/29/18 11:32
1
Client Sample ID: AH-06-0318-C
Lab Sample ID: 180-76196-8
Date Collected: 03/27/18 09:30
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
81.5
Method: 8270D LL - Semivolatile
Organic
Compounds
by GC/MS - Low Level
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Acenaphthene
ND
8.1
2.3
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Acenaphthylene
ND
8.1
1.8
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Anthracene
ND
8.1
2.1
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Benzo[a]anthracene
1.7
J
8.1
1.5
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Benzo[a]pyrene
ND
8.1
1.8
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Benzo[b]fluoranthene
2.5
J
8.1
2.0
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Benzo[g,h,i]perylene
ND
8.1
1.7
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Chrysene
1.8
J
8.1
1.6
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Dibenz(a,h)anthracene
ND
8.1
1.8
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Fluoranthene
ND
8.1
2.1
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Fluorene
ND
8.1
1.6
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Indeno[1,2,3-cd]pyrene
ND
8.1
1.6
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Naphthalene
ND
8.1
1.6
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Phenanthrene
ND
8.1
2.2
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Pyrene
1.9
J
8.1
1.9
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
Benzo[k]fluoranthene
ND
8.1
2.4
ug/Kg
04/02/18 03:39
04/05/18 18:34
2
TestAmerica Pittsburgh
Page 31 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-06-0318-C
Lab Sample ID: 180-76196-8
Date Collected: 03/27/18 09:30
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
81.5
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
76
34 - 100
04102118 03:39
04105118 18:34
2
Nitrobenzene-d5 (Surr)
82
33 - 100
04102118 03:39
04105118 18:34
2
Terphenyl-d14 (Surr)
79
30- 100
04102118 03:39
04105118 18:34
2
Method: 8081113_LL - Organochlorine Pesticides
(GC)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Aldrin
ND
F1
0.050
0.016
ug/Kg
#
04/02/18 03:41
04/16/18 14:10
1
alpha-BHC
ND
F1
0.050
0.012
ug/Kg
#
04/02/18 03:41
04/16/18 14:10
1
cis -Chlordane
ND
F1
0.050
0.013
ug/Kg
#
04/02/18 03:41
04/16/18 14:10
1
beta-BHC
ND
F1
0.050
0.013
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Chlordane (technical)
ND
0.50
0.22
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
4,4'-DDD
ND
F1
0.050
0.014
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
4,4'-DDE
0.016
J F1
0.050
0.010
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
4,4'-DDT
ND
0.050
0.019
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
delta-BHC
ND
0.050
0.016
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Dieldrin
ND
F1
0.050
0.013
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Endosulfan I
ND
F1
0.050
0.014
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Endosulfan 11
ND
F1
0.050
0.011
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Endosulfan sulfate
ND
F1
0.050
0.013
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Endrin
ND
F1
0.050
0.020
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Endrin aldehyde
0.018
J F1 p
0.050
0.018
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Endrin ketone
ND
F1
0.050
0.018
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
gamma-BHC (Lindane)
ND
F1
0.050
0.017
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
trans -Chlordane
ND
F1
0.050
0.012
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Heptachlor
ND
F1
0.050
0.016
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Heptachlor epoxide
ND
F1
0.050
0.013
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Methoxychlor
ND
0.050
0.020
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
oxy-Chlordane
0.011
J p
0.050
0.011
ug/Kg
04/02/18 03:41
04/16/18 14:10
1
Toxaphene
ND
2.0
1.4
ug/Kg
3:�
04/02/18 03:41
04/16/18 14:10
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl (Surr)
60
33 - 137
04102118 03:41
04116118 14:10
1
DCB Decachlorobiphenyl (Surr)
62
33 - 137
04102118 03:41
04116118 14:10
1
Tetrachloro-m-xylene
61
26 - 120
04102118 03:41
04116118 14:10
1
Tetrachloro-m-xylene
69
26 - 120
04102118 03:41
04116118 14:10
1
Method: 6020B - Metals (ICP/MS)
Analyte
Result Qualifier
Antimony
ND
Arsenic
1.4
Beryllium
0.092
Cadmium
ND
Chromium
4.8
Copper
1.8
Lead
1.8
Manganese
14
Nickel
2.3
Selenium
0.13 J
Silver
ND
Thallium
0.019 J
Zinc
6.3
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.12
0.038
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.061
0.016
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.061
0.0047
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.061
0.010
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.12
0.040
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.12
0.070
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.061
0.022
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.31
0.098
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.061
0.038
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.31
0.037
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.061
0.0086
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.061
0.0080
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
0.31
0.20
mg/Kg
04/09/18 16:04
04/11/18 02:05
1
Page 32 of 106
TestAmerica Pittsburgh
4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 7471 B - Mercury (CVAA)
Analyte
Mercury
General Chemistry
Analyte
Percent Moisture
Percent Solids
Cr (III)
Cr (VI)
Total Petroleum Hydrocarbons
(SGT-HEM)
Total Organic Carbon - Duplicates
TestAmerica Job ID: 180-76196-1
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
ND
0.019
0.0043
mg/Kg
#
04/04/18 08:35
04/05/18 09:32
1
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
18.5
0.1
0.1
%
03/29/1811:32
1
81.5
0.1
0.1
%
03/29/1811:32
1
4.7
0.50
0.11
mg/Kg
04/12/1811:38
1
0.19 J
0.48
0.14
mg/Kg
03/29/1814:32
03/30/1813:19
1
ND
200
100
mg/Kg
03/31/18 06:25
04/03/18 08:15
1
2100
1200
920
mg/Kg
04/02/1815:05
1
Client Sample ID: AH-02-0318-G1
Date Collected: 03/27/18 09:55
Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: 180-76196-9
Matrix: Sediment
Percent Solids: 78.4
L
E
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1, 1, 1 -Trichloroethane
ND
6.2
3.1
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,1,2,2-Tetrachloroethane
ND
6.2
3.7
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
6.2
2.4
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,1,2-Trichloroethane
ND
6.2
3.0
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,1-Dichloroethane
ND
6.2
2.2
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,1-Dichloroethene
ND
6.2
3.5
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,2,4-Trichlorobenzene
ND
6.2
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,2-Dibromo-3-Chloropropane
ND
6.2
3.8
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,2-Dichlorobenzene
ND
6.2
5.0
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,2-Dichloroethane
ND
6.2
1.8
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,2-Dichloropropane
ND
6.2
3.0
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,3-Dichlorobenzene
ND
6.2
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,4-Dichlorobenzene
ND
6.2
1.3
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
2-Butanone (MEK)
ND
6.2
3.6
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
2-Hexanone
ND
6.2
5.2
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
4-Methyl-2-pentanone (MIBK)
ND
6.2
2.3
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Acetone
ND
25
3.9
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Benzene
ND
6.2
2.4
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Bromoform
ND
6.2
3.2
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Bromomethane
ND
6.2
5.5
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Carbon disulfide
ND
6.2
3.7
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Carbon tetrachloride
ND
6.2
4.1
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Chlorobenzene
ND
6.2
1.9
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Chlorodibromomethane
ND
6.2
3.0
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Chloroform
ND
6.2
2.6
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Chloromethane
ND
6.2
4.7
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Chloroethane
ND
6.2
3.2
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
cis- 1,2-Dichloroethene
ND
6.2
1.9
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
cis- 1,3-Dichloropropene
ND
6.2
2.0
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Cyclohexane
ND
6.2
1.5
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Dichlorobromomethane
ND
6.2
2.9
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Dichlorodifluoromethane
ND
6.2
3.6
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Ethylbenzene
ND
6.2
2.7
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
1,2-Dibromoethane
ND
6.2
3.4
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Isopropylbenzene
ND
6.2
2.9
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
Methyl acetate
ND
31
7.3
ug/Kg
03/29/18 09:21
03/30/18 17:47
1
TestAmerica Pittsburgh
Page 33 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-02-0318-G1
Lab Sample ID: 180-76196-9
Date Collected: 03/27/18 09:55
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 78.4
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed Dil Fac
Methyl tert-butyl ether
ND
6.2
4.5
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
Methylcyclohexane
ND
6.2
2.6
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
Methylene Chloride
ND
6.2
2.9
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
Styrene
ND
6.2
1.6
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
Tetrachloroethene
ND
6.2
2.5
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
Toluene
ND
6.2
2.1
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
trans- 1,2-Dichloroethene
ND
6.2
3.1
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
trans- 1,3-Dichloropropene
ND
6.2
2.1
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
Trichloroethene
ND
6.2
1.9
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
Trichlorofluoromethane
ND
6.2
1.8
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
Xylenes, Total
ND
12
5.3
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
Vinyl chloride
ND
6.2
4.5
ug/Kg
03/29/18 09:21
03/30/18 17:47 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
96
62- 118
03/29/18 09:21
03130118 17:47 1
4-Bromofluorobenzene (Surr)
96
76 - 111
03/29/18 09:21
03130118 17:47 1
Dibromofluoromethane (Surr)
98
72 - 116
03/29/18 09:21
03130118 17:47 1
Toluene-d8 (Surr)
111
80 - 129
03/29/18 09:21
03130118 17:47 1
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Percent Moisture
21.6
0.1 0.1 %
03/29118 11:32 1
Percent Solids
78.4
0.1 0.1 %
03/29/18 11:32 1
Client Sample ID: AH-02-0318-G2
Lab Sample
ID: 180-76196-10
Date Collected: 03/27/18 09:57
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 59.7
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
7.9
3.9
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,1,2,2-Tetrachloroethane
ND
7.9
4.7
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
7.9
3.0
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,1,2-Trichloroethane
ND
7.9
3.8
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,1-Dichloroethane
ND
7.9
2.8
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,1-Dichloroethene
ND
7.9
4.5
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,2,4-Trichlorobenzene
ND
7.9
2.5
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,2-Dibromo-3-Chloropropane
ND
7.9
4.8
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,2-Dichlorobenzene
ND
7.9
6.3
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,2-Dichloroethane
ND
7.9
2.3
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,2-Dichloropropane
ND
7.9
3.9
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,3-Dichlorobenzene
ND
7.9
2.5
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,4-Dichlorobenzene
ND
7.9
1.6
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
2-Butanone (MEK)
ND
7.9
4.6
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
2-Hexanone
ND
7.9
6.6
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
4-Methyl-2-pentanone (MIBK)
ND
7.9
2.9
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Acetone
ND
31
4.9
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Benzene
ND
7.9
3.1
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Bromoform
ND
7.9
4.1
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Bromomethane
ND
7.9
7.1
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
TestAmerica Pittsburgh
Page 34 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-02-0318-G2
Lab Sample
ID: 180-76196-10
Date Collected: 03/27/18 09:57
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
59.7
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Carbon disulfide
ND
7.9
4.7
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Carbon tetrachloride
ND
7.9
5.2
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Chlorobenzene
ND
7.9
2.5
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Chlorodibromomethane
ND
7.9
3.8
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Chloroform
ND
7.9
3.3
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Chloromethane
ND
7.9
6.1
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Chloroethane
ND
7.9
4.1
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
cis-1,2-Dichloroethene
ND
7.9
2.5
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
cis-1,3-Dichloropropene
ND
7.9
2.5
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Cyclohexane
ND
7.9
1.9
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Dichlorobromomethane
ND
7.9
3.7
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Dichlorodifluoromethane
ND
7.9
4.6
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Ethylbenzene
ND
7.9
3.4
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
1,2-Dibromoethane
ND
7.9
4.3
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Isopropylbenzene
ND
7.9
3.6
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Methyl acetate
ND
39
9.3
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Methyl tert-butyl ether
ND
7.9
5.8
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Methylcyclohexane
ND
7.9
3.3
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Methylene Chloride
ND
7.9
3.7
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Styrene
ND
7.9
2.1
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Tetrachloroethene
ND
7.9
3.1
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Toluene
ND
7.9
2.6
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
trans-1,2-Dichloroethene
ND
7.9
4.0
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
trans-1,3-Dichloropropene
ND
7.9
2.7
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Trichloroethene
ND
7.9
2.4
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Trichlorofluoromethane
ND
7.9
2.3
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Xylenes, Total
ND
16
6.8
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Vinyl chloride
ND
7.9
5.8
ug/Kg
03/29/18 09:21
03/30/18 18:10
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1, 2-Dichloroethane-d4 (Surr)
93
62 - 118
03/29/18 09:21
03130118 18:10 1
4-Bromofluorobenzene (Surr)
91
76 - 111
03/29/18 09:21
03130118 18:10 1
Dibromofluoromethane (Surr)
99
72 - 116
03/29/18 09:21
03130118 18:10 1
Toluene-d8 (Surr)
116
80 - 129
03/29/18 09:21
03130118 18:10 1
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Percent Moisture
40.3
0.1 0.1 %
03/29/18 11:32 1
Percent Solids
59.7
0.1 0.1 %
03/29/18 11:32 1
Client Sample ID: AH-02-0318-G3
Lab Sample
ID: 180-76196-11
Date Collected: 03/27/18 10:00
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids: 46.5
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
10
5.2
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,1,2,2-Tetrachloroethane
ND
10
6.2
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
10
4.0
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,1,2-Trichloroethane
ND
10
5.0
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
TestAmerica Pittsburgh
Page 35 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-02-0318-G3
Lab Sample
ID: 180-76196-11
Date Collected: 03/27/18 10:00
Matrix: Sediment
Date Received: 03/28/18 11:36
Percent Solids:
46.5
Method: EPA 8260B - Volatile Organic Compounds
(GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1-Dichloroethane
ND
10
3.7
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,1-Dichloroethene
ND
10
5.9
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,2,4-Trichlorobenzene
ND
10
3.3
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,2-Dibromo-3-Chloropropane
ND
10
6.4
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,2-Dichlorobenzene
ND
10
8.3
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,2-Dichloroethane
ND
10
3.0
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,2-Dichloropropane
ND
10
5.1
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,3-Dichlorobenzene
ND
10
3.3
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,4-Dichlorobenzene
ND
10
2.1
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
2-Butanone (MEK)
ND
10
6.0
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
2-Hexanone
ND
10
8.7
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
4-Methyl-2-pentanone (MIBK)
ND
10
3.8
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Acetone
ND
41
6.5
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Benzene
ND
10
4.1
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Bromoform
ND
10
5.4
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Bromomethane
ND
10
9.3
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Carbon disulfide
ND
10
6.2
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Carbon tetrachloride
ND
10
6.9
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Chlorobenzene
ND
10
3.3
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Chlorodibromomethane
ND
10
5.0
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Chloroform
ND
10
4.4
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Chloromethane
ND
10
8.0
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Chloroethane
ND
10
5.4
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
cis-1,2-Dichloroethene
ND
10
3.3
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
cis-1,3-Dichloropropene
ND
10
3.3
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Cyclohexane
ND
10
2.5
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Dichlorobromomethane
ND
10
4.9
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Dichlorodifluoromethane
ND
10
6.0
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Ethylbenzene
ND
10
4.5
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
1,2-Dibromoethane
ND
10
5.7
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Isopropylbenzene
ND
10
4.8
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Methyl acetate
ND
52
12
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Methyl tert-butyl ether
ND
10
7.6
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Methylcyclohexane
ND
10
4.4
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Methylene Chloride
ND
10
4.9
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Styrene
ND
10
2.8
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Tetrachloroethene
ND
10
4.1
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Toluene
3.6 J
10
3.5
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
trans- 1,2-Dichloroethene
ND
10
5.3
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
trans- 1,3-Dichloropropene
ND
10
3.6
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Trichloroethene
ND
10
3.1
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Trichlorofluoromethane
ND
10
3.0
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Xylenes, Total
ND
21
8.9
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Vinyl chloride
ND
10
7.6
ug/Kg
03/29/18 09:21
04/02/18 10:27
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
96
62- 118
03/29/18 09:21
04102118 10:27
1
4-Bromofluorobenzene (Surr)
94
76 - 111
03/29/18 09:21
04102118 10:27
1
Dibromofluoromethane (Surr)
99
72 - 116
03/29/18 09:21
04102118 10:27
1
Toluene-d8 (Surr)
106
80 - 129
03/29/18 09:21
04102118 10:27
1
TestAmerica Pittsburgh
Page 36 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
General Chemistry
Analyte Result Qualifier RL MDL Unit D
Percent Moisture 53.5 0.1 0.1 %
Percent Solids 46.5 0.1 0.1 %
Client Sample ID: AH-02-0318-C
Date Collected: 03/27/18 10:05
Date Received: 03/28/18 11:36
TestAmerica Job ID: 180-76196-1
Prepared Analyzed Dil Fac
03/29/18 11:32 1
03/29/18 11:32 1
Lab Sample ID: 180-76196-12 C
Matrix: Sediment
Percent Solids: 57.2
Method: 8270D ILL - Semivolatile Organic Compounds by GC/MS - Low Level
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Acenaphthene
ND
23
6.7
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Acenaphthylene
ND
23
5.1
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Anthracene
26
23
6.0
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Benzo[a]anthracene
16
J
23
4.4
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Benzo[a]pyrene
16
J
23
5.0
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Benzo[b]fluoranthene
32
23
5.7
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Benzo[g,hJ]perylene
12
J
23
5.0
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Chrysene
28
23
4.5
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Dibenz(a,h)anthracene
ND
23
5.2
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Fluoranthene
31
23
6.1
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Fluorene
ND
23
4.5
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Indeno[1,2,3-cd]pyrene
8.9
J
23
4.7
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Naphthalene
ND
23
4.5
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Phenanthrene
8.4
J
23
6.2
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Pyrene
25
23
5.5
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Benzo[k]fluoranthene
13
J
23
6.9
ug/Kg
04/02/18 03:39
04/05/18 19:02
4
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
59
34 - 100
04102118 03:39
04105118 19:02
4
Nitrobenzene-d5 (Surr)
69
33 - 100
04102118 03:39
04105118 19:02
4
Terphenyl-d14 (Surr)
58
30- 100
04102118 03:39
04105118 19:02
4
Method: 8081B_LL - Organochlorine
Pesticides (GC)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Aldrin
ND
0.36
0.11
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
alpha-BHC
ND
0.36
0.089
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
cis -Chlordane
ND
0.36
0.091
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
beta-BHC
ND
0.36
0.093
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Chlordane (technical)
ND
3.6
1.6
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
4,4'-DDD
0.11
J
0.36
0.098
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
4,4'-DDE
0.23
J
0.36
0.074
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
4,4'-DDT
ND
0.36
0.14
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
delta-BHC
ND
0.36
0.11
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Dieldrin
ND
0.36
0.091
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Endosulfan I
ND
0.36
0.098
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Endosulfan 11
ND
0.36
0.080
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Endosulfan sulfate
ND
0.36
0.094
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Endrin
ND
0.36
0.14
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Endrin aldehyde
ND
0.36
0.13
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Endrin ketone
ND
0.36
0.13
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
gamma-BHC (Lindane)
ND
0.36
0.12
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
trans -Chlordane
ND
0.36
0.084
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Heptachlor
ND
0.36
0.11
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Heptachlor epoxide
ND
0.36
0.093
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
Methoxychlor
ND
0.36
0.14
ug/Kg
04/02/18 03:41
04/16/18 14:56
5
E
TestAmerica Pittsburgh
Page 37 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-02-0318-C Lab Sample ID: 180-76196-12
Date Collected: 03/27/18 10:05 Matrix: Sediment
Date Received: 03/28/18 11:36 Percent Solids: 57.2
Method: 8081113LL - Organochlorine Pesticides (GC) (Continued)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
oxy-Chlordane ND 0.36 0.081 ug/Kg 04/02/18 03:41 04/16/18 14:56 5
Toxaphene ND 15 9.8 ug/Kg 04/02/18 03:41 04/16/18 14:56 5
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl (Surr)
65
33 - 137
04102118 03:41
04116118 14:56
5
DCB Decachlorobiphenyl (Surr)
63
33 - 137
04102118 03:41
04116118 14:56
5
Tetrachloro-m-xylene
56
26 - 120
04102118 03:41
04116118 14:56
5
Tetrachloro-m-xylene
52
26 - 120
04102118 03:41
04116118 14:56
5
Method: 6020B - Metals (ICP/MS)
Analyte
Result
Qualifier
Antimony
ND
Arsenic
4.5
Beryllium
0.37
Cadmium
0.045
J
Chromium
19
Copper
6.9
Lead
12
Manganese
110
Nickel
8.0
Selenium
0.44
J
Silver
0.024
J
Thallium
0.11
Zinc
31
Method: 7471 B - Mercury (CVAA)
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.18
0.056
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.090
0.023
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.090
0.0068
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.090
0.015
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.18
0.059
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.18
0.10
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.090
0.032
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.45
0.14
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.090
0.056
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.45
0.054
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.090
0.013
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.090
0.012
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
0.45
0.30
mg/Kg
04/09/18 16:04
04/11/18 02:09
1
I Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.030
0.026
0.0059
mg/Kg
04/04/18 08:35
04/05/18 09:34
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Percent Moisture
42.8
0.1
0.1
%
03/29/18 11:32
1
Percent Solids
57.2
0.1
0.1
%
03/29/18 11:32
1
Cr (III)
19
0.50
0.11
mg/Kg
04/12/18 11:38
1
Cr (VI)
ND
0.69
0.19
mg/Kg
03/29/18 14:32
03/30/18 13:23
1
Total Petroleum Hydrocarbons
ND
290
140
mg/Kg
03/31/18 06:25
04/03/18 08:15
1
(SGT-HEM)
Total Organic Carbon - Duplicates
14000
1700
1300
mg/Kg
04/02/18 15:15
1
Client Sample ID: AH-04-0318-G1 Lab Sample ID: 180-76196-13
Date Collected: 03/27/18 10:40 Matrix: Sediment
Date Received: 03/28/18 09:30 Percent Solids: 39.2
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
13
6.3
ug/Kg
03/28/1812:15
03/28/1814:17
1
1,1,2,2-Tetrachloroethane
ND
13
7.5
ug/Kg
03/28/1812:15
03/28/1814:17
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
13
4.8
ug/Kg
03/28/1812:15
03/28/1814:17
1
1,1,2-Trichloroethane
ND
13
6.1
ug/Kg
03/28/1812:15
03/28/1814:17
1
1,1-Dichloroethane
ND
13
4.6
ug/Kg
03/28/1812:15
03/28/1814:17
1
1,1-Dichloroethene
ND
13
7.2
ug/Kg
03/28/1812:15
03/28/1814:17
1
Page 38 of 106
TestAmerica Pittsburgh
4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-04-0318-G1
Lab Sample
ID: 180-76196-13
Date Collected: 03/27/18 10:40
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids:
39.2
Method: EPA 8260B - Volatile Organic Compounds
(GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,2,4-Trichlorobenzene
ND
13
4.1
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
1,2-Dibromo-3-Chloropropane
ND
13
7.8
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
1,2-Dichlorobenzene
ND
13
10
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
1,2-Dichloroethane
ND
13
3.7
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
1,2-Dichloropropane
ND
13
6.2
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
1,3-Dichlorobenzene
ND
13
4.0
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
1,4-Dichlorobenzene
ND
13
2.6
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
2-Butanone (MEK)
ND
13
7.3
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
2-Hexanone
ND
13
11
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
4-Methyl-2-pentanone (MIBK)
ND
13
4.7
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Acetone
ND
51
8.0
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Benzene
ND
13
5.0
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Bromoform
ND
13
6.6
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Bromomethane
ND
13
11
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Carbon disulfide
ND
13
7.6
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Carbon tetrachloride
ND
13
8.4
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Chlorobenzene
ND
13
4.0
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Chlorodibromomethane
ND
13
6.1
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Chloroform
ND
13
5.3
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Chloromethane
ND
13
9.7
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Chloroethane
ND
13
6.5
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
cis-1,2-Dichloroethene
ND
13
4.0
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
cis-1,3-Dichloropropene
ND
13
4.0
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Cyclohexane
ND
13
3.1
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Dichlorobromomethane
ND
13
6.0
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Dichlorodifluoromethane
ND
13
7.4
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Ethylbenzene
ND
13
5.4
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
1,2-Dibromoethane
ND
13
6.9
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Isopropylbenzene
ND
13
5.9
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Methyl acetate
ND
63
15
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Methyl tert-butyl ether
ND
13
9.3
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Methylcyclohexane
ND
13
5.3
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Methylene Chloride
7.5 J
13
6.0
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Styrene
ND
13
3.4
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Tetrachloroethene
ND
13
5.1
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Toluene
ND
13
4.3
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
trans- 1,2-Dichloroethene
ND
13
6.4
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
trans- 1,3-Dichloropropene
ND
13
4.4
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Trichloroethene
ND
13
3.8
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Trichlorofluoromethane
ND
13
3.7
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Xylenes, Total
ND
25
11
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Vinyl chloride
ND
13
9.3
ug/Kg
03/28/18 12:15
03/28/18 14:17
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
93
62- 118
03/28/18 12:15
03/28/18 14:17
1
4-Bromofluorobenzene (Surr)
93
76 - 111
03/28/18 12:15
03/28/18 14:17
1
Dibromofluoromethane (Surr)
99
72 - 116
03/28/18 12:15
03/28/18 14:17
1
Toluene-d8 (Surr)
113
80 - 129
03128118 12:15
03128118 14:17
1
TestAmerica Pittsburgh
Page 39 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-04-0318-G1 Lab Sample ID: 180-76196-13
Date Collected: 03/27/18 10:40 Matrix: Sediment
Date Received: 03/28/18 09:30 Percent Solids: 39.2
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Percent Moisture 60.8 0.1 0.1 % 03/29/18 08:42 1
Percent Solids 39.2 0.1 0.1 % 03/29/18 08:42 1
Client Sample ID: AH-04-0318-G2 Lab Sample ID: 180-76196-14
Date Collected: 03/27/18 10:42 Matrix: Sediment
Date Received: 03/28/18 09:30 Percent Solids: 39.1
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
13
6.3
ug/Kg
*
03/28/18 12:15
03/28/18 14:41
1
1,1,2,2-Tetrachloroethane
ND
13
7.5
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
13
4.8
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,1,2-Trichloroethane
ND
13
6.0
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,1-Dichloroethane
ND
13
4.5
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,1-Dichloroethene
ND
13
7.2
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,2,4-Trichlorobenzene
ND
13
4.0
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,2-Dibromo-3-Chloropropane
ND
13
7.7
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,2-Dichlorobenzene
ND
13
10
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,2-Dichloroethane
ND
13
3.6
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,2-Dichloropropane
ND
13
6.2
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,3-Dichlorobenzene
ND
13
4.0
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,4-Dichlorobenzene
ND
13
2.6
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
2-Butanone (MEK)
ND
13
7.3
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
2-Hexanone
ND
13
11
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
4-Methyl-2-pentanone (MIBK)
ND
13
4.7
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Acetone
13 J
50
7.9
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Benzene
ND
13
4.9
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Bromoform
ND
13
6.6
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Bromomethane
ND
13
11
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Carbon disulfide
ND
13
7.6
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Carbon tetrachloride
ND
13
8.3
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Chlorobenzene
ND
13
4.0
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Chlorodibromomethane
ND
13
6.0
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Chloroform
ND
13
5.3
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Chloromethane
ND
13
9.7
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Chloroethane
ND
13
6.5
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
cis-1,2-Dichloroethene
ND
13
4.0
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
cis-1,3-Dichloropropene
ND
13
4.0
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Cyclohexane
ND
13
3.1
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Dichlorobromomethane
ND
13
5.9
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Dichlorodifluoromethane
ND
13
7.3
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Ethylbenzene
ND
13
5.4
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
1,2-Dibromoethane
ND
13
6.9
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Isopropylbenzene
ND
13
5.8
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Methyl acetate
ND
63
15
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Methyl tert-butyl ether
ND
13
9.2
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Methyl cyclohexane
ND
13
5.3
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Methylene Chloride
7.1 J
13
5.9
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Styrene
ND
13
3.3
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Tetrachloroethene
ND
13
5.0
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
TestAmerica Pittsburgh
Page 40 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-04-0318-G2 Lab Sample ID: 180-76196-14
Date Collected: 03/27/18 10:42 Matrix: Sediment
Date Received: 03/28/18 09:30 Percent Solids: 39.1
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Toluene
ND
13
4.2
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
trans- 1,2-Dichloroethene
ND
13
6.4
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
trans- 1,3-Dichloropropene
ND
13
4.3
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Trichloroethene
ND
13
3.8
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Trichlorofluoromethane
ND
13
3.7
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Xylenes, Total
ND
25
11
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Vinyl chloride
ND
13
9.2
ug/Kg
03/28/18 12:15
03/28/18 14:41
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
95
62- 118
03128118 12:15
03/28/18 14:41 1
4-Bromofluorobenzene (Surr)
90
76 - 111
03/28/18 12:15
03/28/18 14:41 1
Dibromofluoromethane (Surr)
98
72 - 116
03128118 12:15
03128118 14:41 1
Toluene-d8 (Surr)
112
80 - 129
03/28/18 12:15
03/28/18 14:41 1
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Percent Moisture
60.9
0.1 0.1 %
03/29/18 08:42 1
Percent Solids
39.1
0.1 0.1 %
03/29/18 08:42 1
Client Sample ID: AH-04-0318-G3
Lab Sample
ID: 180-76196-15
Date Collected: 03/27/18 10:45
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 46.9
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
10
5.3
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,1,2,2-Tetrachloroethane
ND
10
6.3
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
10
4.0
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,1,2-Trichloroethane
ND
10
5.0
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,1-Dichloroethane
ND
10
3.8
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,1-Dichloroethene
ND
10
6.0
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,2,4-Trichlorobenzene
ND
10
3.4
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,2-Dibromo-3-Chloropropane
ND
10
6.4
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,2-Dichlorobenzene
ND
10
8.4
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,2-Dichloroethane
ND
10
3.0
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,2-Dichloropropane
ND
10
5.1
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,3-Dichlorobenzene
ND
10
3.3
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,4-Dichlorobenzene
ND
10
2.1
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
2-Butanone (MEK)
ND
10
6.1
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
2-Hexanone
ND
10
8.8
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
4-Methyl-2-pentanone (MIBK)
ND
10
3.9
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Acetone
ND
42
6.6
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Benzene
ND
10
4.1
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Bromoform
ND
10
5.5
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Bromomethane
ND
10
9.4
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Carbon disulfide
ND
10
6.3
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Carbon tetrachloride
ND
10
7.0
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Chlorobenzene
ND
10
3.3
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Chlorodibromomethane
ND
10
5.0
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Chloroform
ND
10
4.4
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
TestAmerica Pittsburgh
Page 41 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-04-0318-G3
Lab Sample
ID: 180-76196-15
Date Collected: 03/27/18 10:45
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids:
46.9
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Chloromethane
ND
10
8.1
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Chloroethane
ND
10
5.4
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
cis-1,2-Dichloroethene
ND
10
3.3
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
cis-1,3-Dichloropropene
ND
10
3.3
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Cyclohexane
ND
10
2.6
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Dichlorobromomethane
ND
10
4.9
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Dichlorodifluoromethane
ND
10
6.1
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Ethylbenzene
ND
10
4.5
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
1,2-Dibromoethane
ND
10
5.7
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Isopropylbenzene
ND
10
4.9
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Methyl acetate
ND
52
12
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Methyl tert-butyl ether
ND
10
7.7
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Methyl cyclohexane
ND
10
4.4
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Methylene Chloride
5.6 J
10
4.9
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Styrene
ND
10
2.8
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Tetrachloroethene
ND
10
4.2
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Toluene
ND
10
3.5
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
trans- 1,2-Dichloroethene
ND
10
5.3
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
trans- 1,3-Dichloropropene
ND
10
3.6
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Trichloroethene
ND
10
3.1
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Trichlorofluoromethane
ND
10
3.1
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Xylenes, Total
ND
21
9.0
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Vinyl chloride
ND
10
7.7
ug/Kg
03/28/18 12:15
03/28/18 15:04
1
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
94
62- 118
03128118 12:15
03/28/18 15:04
1
4-Bromofluorobenzene (Surr)
88
76 - 111
03128118 12:15
03128118 15:04
1
Dibromofluoromethane (Surr)
102
72 - 116
03128118 12:15
03128118 15:04
1
Toluene-d8 (Surr)
114
80 - 129
03/28/18 12:15
03/28/18 15:04
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Percent Moisture
53.1
0.1
0.1
%
03/29/18 08:42
1
Percent Solids
46.9
0.1
0.1
%
03/29/18 08:42
1
Client Sample ID: AH-04-0318-C
Lab Sample
ID: 180-76196-16
Date Collected: 03/27/18 10:50
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids:
41.2
Method: 8270D ILL - Semivolatile
Organic
Compounds
by GC/MS - Low Level
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Acenaphthene
14
J
40
12
ug/Kg
3�
04/02/18 03:39
04/05/18 19:30
5
Acenaphthylene
32
J
40
8.8
ug/Kg
04/02/18 03:39
04/05/18 19:30
5
Anthracene
50
40
10
ug/Kg
04/02/18 03:39
04/05/18 19:30
5
Benzo[a]anthracene
150
40
7.6
ug/Kg
04/02/18 03:39
04/05/18 19:30
5
Benzo[a]pyrene
130
40
8.7
ug/Kg
04/02/18 03:39
04/05/18 19:30
5
Benzo[b]fluoranthene
200
40
9.9
ug/Kg
04/02/18 03:39
04/05/18 19:30
5
Benzo[g,hJ]perylene
79
40
8.7
ug/Kg
04/02/18 03:39
04/05/18 19:30
5
Chrysene
150
40
7.9
ug/Kg
04/02/18 03:39
04/05/18 19:30
5
Dibenz(a,h)anthracene
25
J
40
9.0
ug/Kg
04/02/18 03:39
04/05/18 19:30
5
TestAmerica Pittsburgh
Page 42 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-04-0318-C Lab Sample ID: 180-76196-16
Date Collected: 03/27/18 10:50 Matrix: Sediment
Date Received: 03/28/18 09:30 Percent Solids: 41.2
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Fluoranthene
400
40
11
ug/Kg
04/02/18 03:39
04/05/18 19:30
Fluorene
15 J
40
7.9
ug/Kg
04/02/18 03:39
04/05/18 19:30
Indeno[1,2,3-cd]pyrene
74
40
8.1
ug/Kg
04/02/18 03:39
04/05/18 19:30
Naphthalene
ND
40
7.8
ug/Kg
04/02/18 03:39
04/05/18 19:30
Phenanthrene
60
40
11
ug/Kg
04/02/18 03:39
04/05/18 19:30
Pyrene
310
40
9.5
ug/Kg
04/02/18 03:39
04/05/18 19:30
Benzo[k]fluoranthene
68
40
12
ug/Kg
04/02/18 03:39
04/05/18 19:30
Dil Fac
5
5
5
5
5
5
5
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
69
34 - 100
04102118 03:39
04105118 19:30
5
Nitrobenzene-d5 (Surr)
77
33 - 100
04102118 03:39
04105118 19:30
5
Terphenyl-d14 (Surr)
69
30- 100
04102118 03:39
04105118 19:30
5
Method: 8081B_LL - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Aldrin
ND
0.50
0.16
ug/Kg
#
04/02/18 03:41
04/16/18 15:11
5
alpha-BHC
ND
0.50
0.12
ug/Kg
#
04/02/18 03:41
04/16/18 15:11
5
cis -Chlordane
ND
0.50
0.13
ug/Kg
#
04/02/18 03:41
04/16/18 15:11
5
beta-BHC
ND
0.50
0.13
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Chlordane (technical)
ND
5.0
2.2
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
4,4'-DDD
1.7
0.50
0.14
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
4,4'-DDE
1.5
0.50
0.10
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
4,4'-DDT
6.6
0.50
0.19
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
delta-BHC
ND
0.50
0.16
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Dieldrin
ND
0.50
0.13
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Endosulfan I
ND
0.50
0.14
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Endosulfan 11
ND
0.50
0.11
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Endosulfan sulfate
ND
0.50
0.13
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Endrin
ND
0.50
0.20
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Endrin aldehyde
ND
0.50
0.18
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Endrin ketone
ND
0.50
0.18
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
gamma-BHC (Lindane)
ND
0.50
0.17
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
trans -Chlordane
0.36 J
0.50
0.12
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Heptachlor
ND
0.50
0.16
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Heptachlor epoxide
ND
0.50
0.13
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Methoxychlor
ND
0.50
0.20
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
oxy-Chlordane
ND
0.50
0.11
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Toxaphene
ND
20
14
ug/Kg
04/02/18 03:41
04/16/18 15:11
5
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl (Surr)
80
33 - 137
04102118 03:41
04116118 15:11
5
DCB Decachlorobiphenyl (Surr)
76
33 - 137
04102118 03:41
04116118 15:11
5
Tetrachloro-m-xylene
69
26 - 120
04102118 03:41
04116118 15:11
5
Tetrachloro-m-xylene
62
26 - 120
04102118 03:41
04116118 15:11
5
Method: 6020B - Metals (ICP/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Antimony
0.075 J
0.24
0.075
mg/Kg
T 04/09/18 16:04
04/11/18 02:14
1
Arsenic
7.8
0.12
0.032
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
Beryllium
0.58
0.12
0.0092
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
TestAmerica Pittsburgh
Page 43 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-04-0318-C Lab Sample ID: 180-76196-16
Date Collected: 03/27/18 10:50 Matrix: Sediment
Date Received: 03/28/18 09:30 Percent Solids: 41.2
Method: 6020B - Metals (ICP/MS) (Continued)
Analyte
Result Qualifier
Cadmium
0.13
Chromium
30
Copper
34
Lead
23
Manganese
150
Nickel
12
Selenium
0.74
Silver
0.055 J
Thallium
0.20
Zinc
80
Method: 7471 B - Mercury (CVAA)
Analyte
Mercury
General Chemistry
Analyte
Percent Moisture
Percent Solids
Cr (III)
Cr (VI)
Total Petroleum Hydrocarbons
(SGT-HEM)
Total Organic Carbon - Duplicates
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.12
0.021
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
0.24
0.080
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
0.24
0.14
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
0.12
0.044
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
0.61
0.19
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
0.12
0.075
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
0.61
0.073
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
0.12
0.017
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
0.12
0.016
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
0.61
0.41
mg/Kg
04/09/18 16:04
04/11/18 02:14
1
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.059
0.036
0.0081
mg/Kg
-*
04/04/18 08:35
04/05/18 09:36
1
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
58.8
0.1
0.1
%
03/29/18 08:42
1
41.2
0.1
0.1
%
03/29/18 08:42
1
30
0.50
0.11
mg/Kg
04/12/1811:38
1
ND
0.96
0.27
mg/Kg
03/29/1814:32
03/30/1813:24
1
310 J
400
200
mg/Kg
03/31/18 06:25
04/03/18 08:15
1
24000
2400
1800
mg/Kg
03/29/1816:39
1
Client Sample ID: AH-05-0318-G1 Lab Sample ID: 180-76196-17
Date Collected: 03/27/18 11:35 Matrix: Sediment
Date Received: 03/28/18 09:30 Percent Solids: 25.9
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
1,1,1-Trichloroethane
ND
19
1,12,2-Tetrachloroethane
ND
19
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
19
1,1,2-Trichloroethane
ND
19
1,1-Dichloroethane
ND
19
1,1-Dichloroethene
ND
19
1,2,4-Trichlorobenzene
ND
19
1,2-Dibromo-3-Chloropropane
ND
19
1,2-Dichlorobenzene
ND
19
12-Dichloroethane
ND
19
1,2-Dichloropropane
ND
19
1,3-Dichlorobenzene
ND
19
1,4-Dichlorobenzene
ND
19
2-Butanone (MEK)
ND
19
2-Hexanone
ND
19
4-Methyl-2-pentanone (MIBK)
ND
19
Acetone
27 J
76
Benzene
ND
19
Bromoform
ND
19
MDL
Unit
D
Prepared
Analyzed
Dil Fac
9.5
ug/Kg
*
03/28/1812:15
03/28/1815:28
1
11
ug/Kg
3:�
03/28/1812:15
03/28/1815:28
1
7.3
ug/Kg
03/28/1812:15
03/28/1815:28
1
9.1
ug/Kg
03/28/1812:15
03/28/1815:28
1
6.9
ug/Kg
03/28/1812:15
03/28/1815:28
1
11
ug/Kg
03/28/1812:15
03/28/1815:28
1
6.1
ug/Kg
03/28/1812:15
03/28/1815:28
1
12
ug/Kg
03/28/1812:15
03/28/1815:28
1
15
ug/Kg
03/28/1812:15
03/28/1815:28
1
5.5
ug/Kg
03/28/1812:15
03/28/1815:28
1
9.3
ug/Kg
03/28/1812:15
03/28/1815:28
1
6.1
ug/Kg
03/28/1812:15
03/28/1815:28
1
3.9
ug/Kg
03/28/1812:15
03/28/1815:28
1
11
ug/Kg
03/28/1812:15
03/28/1815:28
1
16
ug/Kg
03/28/1812:15
03/28/1815:28
1
7.1
ug/Kg
03/28/1812:15
03/28/1815:28
1
12
ug/Kg
03/28/1812:15
03/28/1815:28
1
7.5
ug/Kg
03/28/1812:15
03/28/1815:28
1
9.9
ug/Kg
03/28/1812:15
03/28/1815:28
1
Page 44 of 106
TestAmerica Pittsburgh
4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-05-0318-G1
Lab Sample
ID: 180-76196-17
Date Collected: 03/27/18 11:35
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids:
25.9
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Bromomethane
ND
19
17
ug/Kg
03/28/18 12:15
03/28/1815:28
1
Carbon disulfide
11 J
19
11
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Carbon tetrachloride
ND
19
13
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Chlorobenzene
ND
19
6.0
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Chlorodibromomethane
ND
19
9.1
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Chloroform
ND
19
8.0
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Chloromethane
ND
19
15
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Chloroethane
ND
19
9.8
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
cis-1,2-Dichloroethene
ND
19
6.0
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
cis-1,3-Dichloropropene
ND
19
6.1
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Cyclohexane
ND
19
4.6
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Dichlorobromomethane
ND
19
9.0
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Dichlorodifluoromethane
ND
19
11
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Ethylbenzene
ND
19
8.2
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
1,2-Dibromoethane
ND
19
10
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Isopropylbenzene
ND
19
8.8
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Methyl acetate
ND
95
22
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Methyl tert-butyl ether
ND
19
14
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Methylcyclohexane
ND
19
8.0
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Methylene Chloride
13 J
19
9.0
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Styrene
ND
19
5.1
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Tetrachloroethene
ND
19
7.6
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Toluene
ND
19
6.4
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
trans- 1,2-Dichloroethene
ND
19
9.6
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
trans- 1,3-Dichloropropene
ND
19
6.6
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Trichloroethene
ND
19
5.7
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Trichlorofluoromethane
ND
19
5.5
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Xylenes, Total
ND
38
16
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Vinyl chloride
ND
19
14
ug/Kg
03/28/18 12:15
03/28/18 15:28
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
93
62- 118
03/28/18 12:15
03/28/18 15:28
1
4-Bromofluorobenzene (Surr)
90
76 - 111
03/28/18 12:15
03/28/18 15:28
1
Dibromofluoromethane (Surr)
102
72 - 116
03/28/18 12:15
03/28/18 15:28
1
Toluene-d8 (Surr)
117
80 - 129
03/28/18 12:15
03/28/18 15:28
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Percent Moisture
74.1
0.1
0.1
%
03/29/18 08:42
1
Percent Solids
25.9
0.1
0.1
%
03/29/18 08:42
1
Client Sample ID: AH-05-0318-G1-DUP
Lab Sample
ID: 180-76196-18
Date Collected: 03/27/18 11:37
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids:
24.2
Method: EPA 8260B - Volatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
19
9.5
ug/Kg
3�
03/28/18 12:15
03/28/1815:51
1
1,1,2,2-Tetrachloroethane
ND
19
11
ug/Kg
03/28/18 12:15
03/28/1815:51
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
19
7.2
ug/Kg
03/28/18 12:15
03/28/1815:51
1
TestAmerica Pittsburgh
Page 45 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-G1-DUP
Lab Sample
ID: 180-76196-18
Date Collected: 03/27/18 11:37
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids:
24.2
Method: EPA 8260B - Volatile Organic Compounds
(GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,2-Trichloroethane
ND
19
9.1
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
1,1-Dichloroethane
ND
19
6.9
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
1,1-Dichloroethene
ND
19
11
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
1,2,4-Trichlorobenzene
ND
19
6.1
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
1,2-Dibromo-3-Chloropropane
ND
19
12
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
1,2-Dichlorobenzene
ND
19
15
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
1,2-Dichloroethane
ND
19
5.5
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
1,2-Dichloropropane
ND
19
9.3
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
1,3-Dichlorobenzene
ND
19
6.0
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
1,4-Dichlorobenzene
ND
19
3.9
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
2-Butanone (MEK)
ND
19
11
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
2-Hexanone
ND
19
16
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
4-Methyl-2-pentanone (MIBK)
ND
19
7.0
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Acetone
ND
76
12
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Benzene
ND
19
7.4
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Bromoform
ND
19
9.9
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Bromomethane
ND
19
17
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Carbon disulfide
ND
19
11
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Carbon tetrachloride
ND
19
13
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Chlorobenzene
ND
19
6.0
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Chlorodibromomethane
ND
19
9.1
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Chloroform
ND
19
8.0
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Chloromethane
ND
19
15
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Chloroethane
ND
19
9.8
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
cis-1,2-Dichloroethene
ND
19
6.0
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
cis-1,3-Dichloropropene
ND
19
6.1
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Cyclohexane
ND
19
4.6
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Dichlorobromomethane
ND
19
8.9
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Dichlorodifluoromethane
ND
19
11
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Ethylbenzene
ND
19
8.2
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
1,2-Dibromoethane
ND
19
10
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Isopropylbenzene
ND
19
8.8
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Methyl acetate
ND
95
22
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Methyl tert-butyl ether
ND
19
14
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Methylcyclohexane
ND
19
8.0
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Methylene Chloride
10 J
19
9.0
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Styrene
ND
19
5.1
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Tetrachloroethene
ND
19
7.6
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Toluene
ND
19
6.4
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
trans- l,2-Dichloroethene
ND
19
9.6
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
trans- 1,3-Dichloropropene
ND
19
6.6
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Trichloroethene
ND
19
5.7
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Trichlorofluoromethane
ND
19
5.5
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Xylenes, Total
ND
38
16
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Vinyl chloride
ND
19
14
ug/Kg
03/28/18 12:15
03/28/18 15:51
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
93
62- 118
03128118 12:15
03128118 15:51
1
4-Bromofluorobenzene (Surr)
91
76 - 111
03128118 12:15
03128118 15:51
1
Dibromofluoromethane (Surr)
99
72 - 116
03/28/18 12:15
03/28/18 15:51
1
TestAmerica Pittsburgh
Page 46 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-05-0318-G1-DUP Lab Sample ID: 180-76196-18
Date Collected: 03/27/18 11:37 Matrix: Sediment
Date Received: 03/28/18 09:30 Percent Solids: 24.2
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Surrogate %Recovery Qualifier Limits
Toluene-d8 (Surr) 114 80 - 129
General Chemistry
Analyte Result Qualifier RL MDL Unit D
Percent Moisture 75.8 0.1 0.1 %
Percent Solids 24.2 0.1 0.1 %
Client Sample ID: AH-05-0318-G2
Date Collected: 03/27/18 11:40
Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
1,1,1-Trichloroethane
ND
17
1,1,2,2-Tetrachloroethane
ND
17
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
17
1,1,2-Trichloroethane
ND
17
1,1-Dichloroethane
ND
17
1,1-Dichloroethene
ND
17
1,2,4-Trichlorobenzene
ND
17
1,2-Dibromo-3-Chloropropane
ND
17
1,2-Dichlorobenzene
ND
17
1,2-Dichloroethane
ND
17
1,2-Dichloropropane
ND
17
1,3-Dichlorobenzene
ND
17
1,4-Dichlorobenzene
ND
17
2-Butanone (MEK)
ND
17
2-Hexanone
ND
17
4-Methyl-2-pentanone (MIBK)
ND
17
Acetone
16 J
67
Benzene
ND
17
Bromoform
ND
17
Bromomethane
ND
17
Carbon disulfide
ND
17
Carbon tetrachloride
ND
17
Chlorobenzene
ND
17
Chlorodibromomethane
ND
17
Chloroform
ND
17
Chloromethane
ND
17
Chloroethane
ND
17
cis-1,2-Dichloroethene
ND
17
cis-1,3-Dichloropropene
ND
17
Cyclohexane
ND
17
Dichlorobromomethane
ND
17
Dichlorodifluoromethane
ND
17
Ethylbenzene
ND
17
1,2-Dibromoethane
ND
17
Isopropylbenzene
ND
17
Methyl acetate
ND
84
Prepared Analyzed Dil Fac
03128118 12:15 03128118 15:51 1
Prepared Analyzed Dil Fac
03/29/18 08:42 1
03/29/18 08:42 1
Lab Sample ID: 180-76196-19
Matrix: Sediment
Percent Solids: 28.4
MDL
Unit
D
Prepared
Analyzed
8.4
ug/Kg
03/28/1812:15
03/28/1816:14
10
ug/Kg
03/28/1812:15
03/28/1816:14
6.4
ug/Kg
03/28/1812:15
03/28/1816:14
8.1
ug/Kg
03/28/1812:15
03/28/1816:14
6.1
ug/Kg
03/28/1812:15
03/28/1816:14
9.6
ug/Kg
03/28/1812:15
03/28/1816:14
5.4
ug/Kg
03/28/1812:15
03/28/1816:14
10
ug/Kg
03/28/1812:15
03/28/1816:14
14
ug/Kg
03/28/1812:15
03/28/1816:14
4.9
ug/Kg
03/28/1812:15
03/28/1816:14
8.2
ug/Kg
03/28/1812:15
03/28/1816:14
5.4
ug/Kg
03/28/1812:15
03/28/1816:14
3.4
ug/Kg
03/28/1812:15
03/28/1816:14
9.7
ug/Kg
03/28/1812:15
03/28/1816:14
14
ug/Kg
03/28/1812:15
03/28/1816:14
6.2
ug/Kg
03/28/1812:15
03/28/1816:14
11
ug/Kg
03/28/1812:15
03/28/1816:14
6.6
ug/Kg
03/28/1812:15
03/28/1816:14
8.8
ug/Kg
03/28/1812:15
03/28/1816:14
15
ug/Kg
03/28/1812:15
03/28/1816:14
10
ug/Kg
03/28/1812:15
03/28/1816:14
11
ug/Kg
03/28/1812:15
03/28/1816:14
5.3
ug/Kg
03/28/1812:15
03/28/1816:14
8.1
ug/Kg
03/28/1812:15
03/28/1816:14
7.1
ug/Kg
03/28/1812:15
03/28/1816:14
13
ug/Kg
03/28/1812:15
03/28/1816:14
8.7
ug/Kg
03/28/1812:15
03/28/1816:14
5.3
ug/Kg
03/28/1812:15
03/28/1816:14
5.4
ug/Kg
03/28/1812:15
03/28/1816:14
4.1
ug/Kg
03/28/1812:15
03/28/1816:14
7.9
ug/Kg
03/28/1812:15
03/28/1816:14
9.8
ug/Kg
03/28/1812:15
03/28/1816:14
7.2
ug/Kg
03/28/1812:15
03/28/1816:14
9.2
ug/Kg
03/28/1812:15
03/28/1816:14
7.8
ug/Kg
03/28/1812:15
03/28/1816:14
20
ug/Kg
03/28/1812:15
03/28/1816:14
TestAmerica Pittsburgh
Page 47 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-05-0318-G2
Lab Sample
ID: 180-76196-19
Date Collected: 03/27/18 11:40
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 28.4
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed Dil Fac
Methyl tert-butyl ether
ND
17
12
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
Methylcyclohexane
ND
17
7.1
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
Methylene Chloride
8.3 J
17
7.9
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
Styrene
ND
17
4.5
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
Tetrachloroethene
ND
17
6.7
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
Toluene
ND
17
5.7
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
trans-1,2-Dichloroethene
ND
17
8.5
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
trans-1,3-Dichloropropene
ND
17
5.8
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
Trichloroethene
ND
17
5.1
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
Trichlorofluoromethane
ND
17
4.9
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
Xylenes, Total
ND
34
14
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
Vinyl chloride
ND
17
12
ug/Kg
03/28/18 12:15
03/28/18 16:14 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
93
62- 118
03128118 12:15
03128118 16:14 1
4-Bromofluorobenzene (Surr)
89
76 - 111
03128118 12:15
03128118 16:14 1
Dibromofluoromethane (Surr)
97
72- 116
03128118 12:15
03128118 16:14 1
Toluene-d8 (Surr)
110
80 - 129
03/28/18 12:15
03/28/18 16:14 1
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Percent Moisture
71.6
0.1 0.1 %
03/29/18 08:42 1
Percent Solids
28.4
0.1 0.1 %
03/29/18 08:42 1
Client Sample ID: AH-05-0318-G3
Lab Sample
ID: 180-76196-20
Date Collected: 03/27/18 11:45
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 16.8
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
30
15
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,1,2,2-Tetrachloroethane
ND
30
18
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
30
11
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,1,2-Trichloroethane
ND
30
14
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,1-Dichloroethane
ND
30
11
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,1-Dichloroethene
ND
30
17
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,2,4-Trichoorobenzene
ND
30
9.7
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,2-Dibromo-3-Chloropropane
ND
30
18
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,2-Dichlorobenzene
ND
30
24
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,2-Dichloroethane
ND
30
8.7
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,2-Dichloropropane
ND
30
15
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,3-Dichlorobenzene
ND
30
9.6
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,4-Dichlorobenzene
ND
30
6.1
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
2-Butanone (MEK)
ND
30
17
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
2-Hexanone
ND
30
25
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
4-Methyl-2-pentanone (MIBK)
ND
30
11
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Acetone
ND
120
19
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Benzene
ND
30
12
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Bromoform
ND
30
16
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Bromomethane
ND
30
27
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
TestAmerica Pittsburgh
Page 48 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-05-0318-G3
Lab Sample
ID: 180-76196-20
Date Collected: 03/27/18 11:45
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids:
16.8
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Carbon disulfide
ND
30
18
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Carbon tetrachloride
ND
30
20
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Chlorobenzene
ND
30
9.4
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Chlorodibromomethane
ND
30
14
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Chloroform
ND
30
13
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Chloromethane
ND
30
23
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Chloroethane
ND
30
15
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
cis-1,2-Dichloroethene
ND
30
9.4
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
cis-1,3-Dichloropropene
ND
30
9.6
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Cyclohexane
ND
30
7.3
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Dichlorobromomethane
ND
30
14
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Dichlorodifluoromethane
ND
30
17
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Ethylbenzene
ND
30
13
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
1,2-Dibromoethane
ND
30
16
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Isopropylbenzene
ND
30
14
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Methyl acetate
ND
150
35
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Methyl tert-butyl ether
ND
30
22
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Methylcyclohexane
ND
30
13
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Methylene Chloride
15 J
30
14
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Styrene
ND
30
8.0
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Tetrachloroethene
ND
30
12
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Toluene
ND
30
10
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
trans- 1,2-Dichloroethene
ND
30
15
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
trans-1,3-Dichloropropene
ND
30
10
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Trichloroethene
ND
30
9.0
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Trichlorofluoromethane
ND
30
8.7
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Xylenes, Total
ND
60
26
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Vinyl chloride
ND
30
22
ug/Kg
03/28/18 12:15
03/28/18 16:38
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1, 2-Dichloroethane-d4 (Surr)
94
62 - 118
03/28/18 12:15
03/28/18 16:38 1
4-Bromofluorobenzene (Surr)
82
76 - 111
03/28/18 12:15
03/28/18 16:38 1
Dibromofluoromethane (Surr)
103
72 - 116
03/28/18 12:15
03/28/18 16:38 1
Toluene-d8 (Surr)
118
80 - 129
03/28/18 12:15
03/28/18 16:38 1
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Percent Moisture
83.2
0.1 0.1 %
03/29/18 08:42 1
Percent Solids
16.8
0.1 0.1 %
03/29/18 08:42 1
Client Sample ID: AH-05-0318-C
Lab Sample
ID: 180-76196-21
Date Collected: 03/27/18 11:55
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids: 24.0
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Acenaphthene
ND
69
20
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Acenaphthylene
52 J
69
15
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Anthracene
53 J
69
18
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Benzo[a]anthracene
130
69
13
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
TestAmerica Pittsburgh
Page 49 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-C
Lab Sample
ID: 180-76196-21
Date Collected: 03/27/18 11:55
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids:
24.0
Method: 8270D LL - Semivolatile Organic
Compounds by GC/MS - Low Level (Continued)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Benzo[a]pyrene
150
69
15
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Benzo[b]fluoranthene
290
69
17
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Benzo[g,h,i]perylene
90
69
15
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Chrysene
120
69
13
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Dibenz(a,h)anthracene
23
J
69
15
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Fluoranthene
160
69
18
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Fluorene
ND
69
13
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Indeno[1,2,3-cd]pyrene
85
69
14
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Naphthalene
ND
69
13
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Phenanthrene
ND
69
18
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Pyrene
260
69
16
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Benzo[k]fluoranthene
120
69
21
ug/Kg
04/02/18 03:39
04/05/18 19:58
5
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
58
34 - 100
04102118 03:39
04105118 19:58
5
Nitrobenzene-d5 (Surr)
65
33 - 100
04102118 03:39
04105118 19:58
5
Terphenyl-d14 (Surr)
56
30- 100
04102118 03:39
04105118 19:58
5
Method: 8081B_LL - Organochlorine Pesticides
(GC)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Aldrin
ND
0.86
0.27
ug/Kg
*
04/02/18 03:41
04/16/18 15:27
5
alpha-BHC
ND
0.86
0.21
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
cis -Chlordane
ND
0.86
0.22
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
beta-BHC
ND
0.86
0.22
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Chlordane (technical)
ND
8.6
3.7
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
4,4'-DDD
1.8
0.86
0.23
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
4,4'-DDE
4.8
0.86
0.18
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
4,4'-DDT
ND
0.86
0.33
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
delta-BHC
ND
0.86
0.27
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Dieldrin
ND
0.86
0.22
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Endosulfan I
ND
0.86
0.23
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Endosulfan 11
ND
0.86
0.19
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Endosulfan sulfate
ND
0.86
0.22
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Endrin
ND
0.86
0.33
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Endrin aldehyde
ND
0.86
0.31
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Endrin ketone
ND
0.86
0.31
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
gamma-BHC (Lindane)
ND
0.86
0.29
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
trans -Chlordane
0.58
J
0.86
0.20
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Heptachlor
ND
0.86
0.27
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Heptachlor epoxide
ND
0.86
0.22
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Methoxychlor
1.2
0.86
0.33
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
oxy-Chlordane
ND
0.86
0.19
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Toxaphene
ND
34
23
ug/Kg
04/02/18 03:41
04/16/18 15:27
5
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl (Surr)
88
33 - 137
04102118 03:41
04116118 15:27
5
DCB Decachlorobiphenyl (Surr)
84
33 - 137
04102118 03:41
04116118 15:27
5
Tetrachloro-m-xylene
69
26 - 120
04102118 03:41
04116118 15:27
5
Tetrachloro-m-xylene
67
26 - 120
04102118 03:41
04116118 15:27
5
TestAmerica Pittsburgh
Page 50 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-05-0318-C Lab Sample ID: 180-76196-21
Date Collected: 03/27/18 11:55 Matrix: Sediment
Date Received: 03/28/18 09:30 Percent Solids: 24.0
Method: 6020B - Metals (ICP/MS)
Analyte
Result Qualifier
Antimony
ND
Arsenic
10
Beryllium
0.69
Cadmium
0.33
Chromium
38
Copper
120
Lead
34
Manganese
160
Nickel
15
Selenium
1.1
Silver
0.069 J
Thallium
0.30
Zinc
170
Method: 7471 B - Mercury (CVAA)
Analyte
Mercury
(General Chemistry
Analyte
Percent Moisture
Percent Solids
Cr (III)
Cr (VI)
Total Petroleum Hydrocarbons
(SGT-HEM)
Total Organic Carbon - Duplicates
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.41
0.13
mg/Kg
3-�
04/09/18 16:04
04/11/18 02:19
1
0.20
0.053
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
0.20
0.016
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
0.20
0.035
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
0.41
0.14
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
0.41
0.23
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
0.20
0.074
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
1.0
0.33
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
0.20
0.13
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
1.0
0.12
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
0.20
0.029
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
0.20
0.027
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
1.0
0.68
mg/Kg
04/09/18 16:04
04/11/18 02:19
1
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.11
0.068
0.015
mg/Kg
*
04/04/18 08:35
04/05/18 09:42
1
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
76.0
0.1
0.1
%
03/29/18 08:42
1
24.0
0.1
0.1
%
03/29/18 08:42
1
38
0.50
0.11
mg/Kg
04/12/1811:38
1
ND
1.6
0.46
mg/Kg
03/29/1814:32
03/30/1813:30
1
500 J
700
350
mg/Kg
03/31/18 06:25
04/03/18 08:15
1
83000
4200
3100
mg/Kg
03/29/1816:49
1
Client Sample ID: AH-05-0318-C-DUP Lab Sample ID: 180-76196-22
Date Collected: 03/27/18 11:58 Matrix: Sediment
Date Received: 03/28/18 09:30 Percent Solids: 23.9
Method: 8270D ILL - Semivolatile Organic Compounds by GC/MS - Low Level
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Acenaphthene
ND
56
16
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Acenaphthylene
45 J
56
12
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Anthracene
40 J
56
15
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Benzo[a]anthracene
100
56
11
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Benzo[a]pyrene
110
56
12
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Benzo[b]fluoranthene
220
56
14
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Benzo[g,hJ]perylene
67
56
12
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Chrysene
110
56
11
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Dibenz(a,h)anthracene
16 J
56
12
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Fluoranthene
130
56
15
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Fluorene
ND
56
11
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Indeno[1,2,3-cd]pyrene
61
56
11
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Naphthalene
ND
56
11
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Phenanthrene
ND
56
15
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Pyrene
220
56
13
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Benzo[k]fluoranthene
98
56
17
ug/Kg
04/02/18 03:39
04/05/18 20:26
4
Page 51 of 106
TestAmerica Pittsburgh
4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-C-DUP
Lab Sample
ID: 180-76196-22
Date Collected: 03/27/18 11:58
Matrix: Sediment
Date Received: 03/28/18 09:30
Percent Solids:
23.9
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
48
34 - 100
04102118 03:39
04105118 20:26
4
Nitrobenzene-d5 (Surr)
58
33 - 100
04102118 03:39
04105118 20:26
4
Terphenyl-d14 (Surr)
46
30- 100
04102118 03:39
04105118 20:26
4
Method: 8081113_LL - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Aldrin
ND
0.86
0.27
ug/Kg
#
04/02/18 03:41
04/16/18 17:15
5
alpha-BHC
ND
0.86
0.21
ug/Kg
#
04/02/18 03:41
04/16/18 17:15
5
cis -Chlordane
ND
0.86
0.22
ug/Kg
#
04/02/18 03:41
04/16/18 17:15
5
beta-BHC
ND
0.86
0.22
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Chlordane (technical)
ND
8.6
3.7
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
4,4'-DDD
1.8
0.86
0.23
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
4,4'-DDE
4.3
0.86
0.18
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
4,4'-DDT
ND
0.86
0.33
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
delta-BHC
ND
0.86
0.27
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Dieldrin
ND
0.86
0.22
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Endosulfan I
ND
0.86
0.23
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Endosulfan 11
ND
0.86
0.19
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Endosulfan sulfate
ND
0.86
0.23
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Endrin
ND
0.86
0.34
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Endrin aldehyde
ND
0.86
0.31
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Endrin ketone
ND
0.86
0.31
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
gamma-BHC (Lindane)
ND
0.86
0.30
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
trans -Chlordane
0.58 J
0.86
0.20
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Heptachlor
ND
0.86
0.27
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Heptachlor epoxide
ND
0.86
0.22
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Methoxychlor
ND
0.86
0.34
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
oxy-Chlordane
ND
0.86
0.19
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Toxaphene
ND
35
23
ug/Kg
04/02/18 03:41
04/16/18 17:15
5
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl (Surr)
79
33 - 137
04102118 03:41
04116118 17:15
5
DCB Decachlorobiphenyl (Surr)
78
33 - 137
04102118 03:41
04116118 17:15
5
Tetrachloro-m-xylene
66
26 - 120
04102118 03:41
04116118 17:15
5
Tetrachloro-m-xylene
62
26 - 120
04102118 03:41
04116118 17:15
5
Method: 6020B - Metals (ICP/MS)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Antimony
0.13
J
0.43
0.13
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Arsenic
8.3
0.21
0.056
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Beryllium
0.62
0.21
0.016
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Cadmium
0.29
0.21
0.037
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Chromium
32
0.43
0.14
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Copper
99
0.43
0.25
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Lead
27
0.21
0.077
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Manganese
140
1.1
0.34
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Nickel
12
0.21
0.13
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Selenium
1.0
J
1.1
0.13
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Silver
0.051
J
0.21
0.030
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Thallium
0.25
0.21
0.028
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
Zinc
150
1.1
0.72
mg/Kg
04/09/18 16:04
04/11/18 02:23
1
TestAmerica Pittsburgh
Page 52 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 7471 B - Mercury (CVAA)
Analyte
Mercury
General Chemistry
Analyte
Percent Moisture
Percent Solids
Cr (III)
Cr (VI)
Total Petroleum Hydrocarbons
(SGT-HEM)
Total Organic Carbon - Duplicates
Client Sample ID: TB-02-0318
Date Collected: 03/27/18 12:30
Date Received: 03/28/18 09:30
TestAmerica Job ID: 180-76196-1
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.099
0.070
0.016
mg/Kg
3,'�
04/04/18 08:35
04/05/18 09:44
1
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
76.1
0.1
0.1
%
03/29/18 08:42
1
23.9
0.1
0.1
%
03/29/18 08:42
1
32
0.50
0.11
mg/Kg
04/12/1811:38
1
ND
1.7
0.48
mg/Kg
03/29/1814:43
03/30/1813:31
1
610 J
700
350
mg/Kg
03/31/18 06:25
04/03/18 08:15
1
77000
4200
3100
mg/Kg
03/29/1816:59
1
Lab Sample ID: 180-76196-23
Matrix: Water
F
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier RL
MDL
Unit D
1,1,1-Trichloroethane
ND
1.0
0.60
ug/L
1,1,2,2-Tetrachloroethane
ND
1.0
0.60
ug/L
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
0.86
ug/L
1,1,2-Trichloroethane
ND
1.0
0.45
ug/L
1,1-Dichloroethane
ND
1.0
0.63
ug/L
1,1-Dichloroethene
ND
1.0
0.55
ug/L
1,2,4-Trichlorobenzene
ND
1.0
0.77
ug/L
1,2-Dibromo-3-Chloropropane
ND
1.0
0.89
ug/L
1,2-Dichlorobenzene
ND
1.0
0.36
ug/L
1,2-Dichloroethane
ND
1.0
0.57
ug/L
1,2-Dichloropropane
ND
1.0
0.66
ug/L
1,3-Dichlorobenzene
ND
1.0
0.50
ug/L
1,4-Dichlorobenzene
ND
1.0
0.54
ug/L
2-Butanone (MEK)
ND
5.0
2.6
ug/L
2-Hexanone
ND
5.0
3.3
ug/L
4-Methyl-2-pentanone (MIBK)
ND
5.0
3.1
ug/L
Acetone
6.2
5.0
3.4
ug/L
Benzene
ND
1.0
0.60
ug/L
Bromoform
ND
1.0
0.98
ug/L
Bromomethane
ND
1.0
0.89
ug/L
Carbon disulfide
ND
1.0
0.88
ug/L
Carbon tetrachloride
ND
1.0
0.88
ug/L
Chlorobenzene
ND
1.0
0.50
ug/L
Chlorodibromomethane
ND
1.0
0.84
ug/L
Chloroethane
ND
1.0
0.90
ug/L
Chloroform
ND
1.0
0.60
ug/L
Chloromethane
ND
1.0
0.90
ug/L
cis-1,2-Dichloroethene
ND
1.0
0.71
ug/L
cis-1,3-Dichloropropene
ND
1.0
0.59
ug/L
Cyclohexane
ND
1.0
0.63
ug/L
Dichlorobromomethane
ND
1.0
0.64
ug/L
Dichlorodifluoromethane
ND
1.0
0.83
ug/L
Ethylbenzene
ND
1.0
0.51
ug/L
1,2-Dibromoethane
ND
1.0
0.50
ug/L
Isopropylbenzene
ND
1.0
0.34
ug/L
Methyl acetate
ND
5.0
1.7
ug/L
0
Prepared Analyzed
Dil Fac
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
03/28/18 21:15
1
TestAmerica Pittsburgh
Page 53 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Client Sample ID: TB-02-0318
Lab Sample ID: 180-76196-23
Date Collected: 03/27/18 12:30
Matrix: Water
Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds
(GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed Dil Fac
Methyl tert-butyl ether
ND
1.0
0.59
ug/L
03/28/18 21:15 1
Methylcyclohexane
ND
1.0
0.61
ug/L
03/28/18 21:15 1
Methylene Chloride
ND
1.0
0.36
ug/L
03/28/18 21:15 1
Styrene
ND
1.0
0.47
ug/L
03/28/18 21:15 1
Tetrachloroethene
ND
1.0
0.47
ug/L
03/28/18 21:15 1
Toluene
ND
1.0
0.46
ug/L
03/28/18 21:15 1
trans- 1,2-Dichloroethene
ND
1.0
0.67
ug/L
03/28/18 21:15 1
trans- 1,3-Dichloropropene
ND
1.0
0.58
ug/L
03/28/18 21:15 1
Trichloroethene
ND
1.0
0.69
ug/L
03/28/18 21:15 1
Trichlorofluoromethane
ND
1.0
0.87
ug/L
03/28/18 21:15 1
Vinyl chloride
ND
1.0
0.88
ug/L
03/28/18 21:15 1
Xylenes, Total
ND
2.0
0.89
ug/L
03/28/18 21:15 1
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
109
65- 121
03128118 21:15 1
4-Bromofluorobenzene (Surr)
81
80 - 120
03128118 21:15 1
Dibromofluoromethane (Surr)
107
73 - 120
03128118 21:15 1
Toluene-d8 (Surr)
101
73 - 120
03/28/18 21:15 1
Client Sample ID: EB-02-0318
Lab Sample ID: 180-76196-24
Date Collected: 03/27/18 12:50
Matrix: Water
Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
1.0
0.60
ug/L
03/29/18 21:47
1
1,1,2,2-Tetrachloroethane
ND
1.0
0.60
ug/L
03/29/18 21:47
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
0.86
ug/L
03/29/18 21:47
1
1,1,2-Trichloroethane
ND
1.0
0.45
ug/L
03/29/18 21:47
1
1,1-Dichloroethane
ND
1.0
0.63
ug/L
03/29/18 21:47
1
1,1-Dichloroethene
ND
1.0
0.55
ug/L
03/29/18 21:47
1
1,2,4-Trichlorobenzene
ND
1.0
0.77
ug/L
03/29/18 21:47
1
1,2-Dibromo-3-Chloropropane
ND
1.0
0.89
ug/L
03/29/18 21:47
1
1,2-Dichlorobenzene
ND
1.0
0.36
ug/L
03/29/18 21:47
1
1,2-Dichloroethane
ND
1.0
0.57
ug/L
03/29/18 21:47
1
1,2-Dichloropropane
ND
1.0
0.66
ug/L
03/29/18 21:47
1
1,3-Dichlorobenzene
ND
1.0
0.50
ug/L
03/29/18 21:47
1
1,4-Dichlorobenzene
ND
1.0
0.54
ug/L
03/29/18 21:47
1
2-Butanone (MEK)
ND
5.0
2.6
ug/L
03/29/18 21:47
1
2-Hexanone
ND
5.0
3.3
ug/L
03/29/18 21:47
1
4-Methyl-2-pentanone (MIBK)
ND
5.0
3.1
ug/L
03/29/18 21:47
1
Acetone
6.5
5.0
3.4
ug/L
03/29/18 21:47
1
Benzene
ND
1.0
0.60
ug/L
03/29/18 21:47
1
Bromoform
ND
1.0
0.98
ug/L
03/29/18 21:47
1
Bromomethane
ND
1.0
0.89
ug/L
03/29/18 21:47
1
Carbon disulfide
ND
1.0
0.88
ug/L
03/29/18 21:47
1
Carbon tetrachloride
ND
1.0
0.88
ug/L
03/29/18 21:47
1
Chlorobenzene
ND
1.0
0.50
ug/L
03/29/18 21:47
1
Chlorodibromomethane
ND
1.0
0.84
ug/L
03/29/18 21:47
1
Chloroethane
ND
1.0
0.90
ug/L
03/29/18 21:47
1
TestAmerica Pittsburgh
Page 54 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment
Project
Client Sample ID: EB-02-0318
Lab Sample
ID: 180-76196-24
Date Collected: 03/27/18 12:50
Matrix:
Water
Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds
(GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Chloroform
ND
1.0
0.60
ug/L
03/29/18 21:47
1
Chloromethane
ND
1.0
0.90
ug/L
03/29/18 21:47
1
cis-1,2-Dichloroethene
ND
1.0
0.71
ug/L
03/29/18 21:47
1
cis-1,3-Dichloropropene
ND
1.0
0.59
ug/L
03/29/18 21:47
1
Cyclohexane
ND
1.0
0.63
ug/L
03/29/18 21:47
1
Dichlorobromomethane
ND
1.0
0.64
ug/L
03/29/18 21:47
1
Dichlorodifluoromethane
ND
1.0
0.83
ug/L
03/29/18 21:47
1
Ethylbenzene
ND
1.0
0.51
ug/L
03/29/18 21:47
1
1,2-Dibromoethane
ND
1.0
0.50
ug/L
03/29/18 21:47
1
Isopropylbenzene
ND
1.0
0.34
ug/L
03/29/18 21:47
1
Methyl acetate
ND
5.0
1.7
ug/L
03/29/18 21:47
1
Methyl tert-butyl ether
ND
1.0
0.59
ug/L
03/29/18 21:47
1
Methylcyclohexane
ND
1.0
0.61
ug/L
03/29/18 21:47
1
Methylene Chloride
ND
1.0
0.36
ug/L
03/29/18 21:47
1
Styrene
ND
1.0
0.47
ug/L
03/29/18 21:47
1
Tetrachloroethene
ND
1.0
0.47
ug/L
03/29/18 21:47
1
Toluene
ND
1.0
0.46
ug/L
03/29/18 21:47
1
trans- 1,2-Dichloroethene
ND
1.0
0.67
ug/L
03/29/18 21:47
1
trans- 1,3-Dichloropropene
ND
1.0
0.58
ug/L
03/29/18 21:47
1
Trichloroethene
ND
1.0
0.69
ug/L
03/29/18 21:47
1
Trichlorofluoromethane
ND
1.0
0.87
ug/L
03/29/18 21:47
1
Vinyl chloride
ND
1.0
0.88
ug/L
03/29/18 21:47
1
Xylenes, Total
ND
2.0
0.89
ug/L
03/29/18 21:47
1
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
88
65- 121
03/29/18 21
1
4-Bromofluorobenzene (Surr)
89
80 - 120
03/29/18 21:47
1
Dibromofluoromethane (Surr)
85
73 - 120
03/29/18 21:47
1
Toluene-d8 (Surr)
90
73 - 120
03/29/18 21:47
1
Method: EPA 8270D LL - Semivolatile
Organic Compounds
by GC/MS - Low Level
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Acenaphthene
ND
0.20
0.068
ug/L
04/02/18 11:29
04/06/18 00:27
1
Acenaphthylene
ND
0.20
0.068
ug/L
04/02/18 11:29
04/06/18 00:27
1
Anthracene
ND
0.20
0.051
ug/L
04/02/18 11:29
04/06/18 00:27
1
Benzo[a]anthracene
ND
0.20
0.078
ug/L
04/02/18 11:29
04/06/18 00:27
1
Benzo[b]fluoranthene
ND
0.20
0.10
ug/L
04/02/18 11:29
04/06/18 00:27
1
Benzo[g,h,i]perylene
ND
0.20
0.072
ug/L
04/02/18 11:29
04/06/18 00:27
1
Benzo[a]pyrene
ND
0.20
0.055
ug/L
04/02/18 11:29
04/06/18 00:27
1
Chrysene
ND
0.20
0.084
ug/L
04/02/18 11:29
04/06/18 00:27
1
Dibenz(a,h)anthracene
ND
0.20
0.075
ug/L
04/02/18 11:29
04/06/18 00:27
1
Fluoranthene
ND
0.20
0.063
ug/L
04/02/18 11:29
04/06/18 00:27
1
Fluorene
ND
0.20
0.072
ug/L
04/02/18 11:29
04/06/18 00:27
1
Indeno[1,2,3-cd]pyrene
ND
0.20
0.089
ug/L
04/02/18 11:29
04/06/18 00:27
1
Naphthalene
ND
0.20
0.061
ug/L
04/02/18 11:29
04/06/18 00:27
1
Phenanthrene
ND
0.20
0.057
ug/L
04/02/18 11:29
04/06/18 00:27
1
Pyrene
ND
0.20
0.056
ug/L
04/02/18 11:29
04/06/18 00:27
1
Benzo[k]fluoranthene
ND
0.20
0.092
ug/L
04/02/18 11:29
04/06/18 00:27
1
TestAmerica Pittsburgh
Page 55 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: EB-02-0318
Lab Sample
ID: 180-76196-24
Date Collected: 03/27/18 12:50
Matrix:
Water
Date Received: 03/28/18 09:30
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
69
26 - 103
04102118 11:29
04106118 00:27
1
Nitrobenzene-d5 (Surr)
71
30 - 101
04102118 11:29
04106118 00:27
1
Terphenyl-d14 (Surr)
90
20- 119
04102118 11:29
04106118 00:27
1
Method: EPA 8081 B LL - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Aldrin
ND
0.0013
0.00012
ug/L
03/28/18 12:35
04/02/18 19:49
1
alpha-BHC
ND
0.0013
0.00012
ug/L
03/28/18 12:35
04/02/18 19:49
1
beta-BHC
ND
0.0013
0.00016
ug/L
03/28/18 12:35
04/02/18 19:49
1
delta-BHC
ND
0.0013
0.00035
ug/L
03/28/18 12:35
04/02/18 19:49
1
gamma-BHC (Lindane)
ND
0.0013
0.00012
ug/L
03/28/18 12:35
04/02/18 19:49
1
cis -Chlordane
ND
0.0013
0.00014
ug/L
03/28/18 12:35
04/02/18 19:49
1
trans -Chlordane
ND
0.0013
0.00013
ug/L
03/28/18 12:35
04/02/18 19:49
1
oxy-Chlordane
ND
0.017
0.00021
ug/L
03/28/18 12:35
04/02/18 19:49
1
Chlordane (technical)
ND
0.013
0.0015
ug/L
03/28/18 12:35
04/02/18 19:49
1
4,4'-DDD
ND
0.0013
0.00021
ug/L
03/28/18 12:35
04/02/18 19:49
1
4,4'-DDE
ND
0.0013
0.00011
ug/L
03/28/18 12:35
04/02/18 19:49
1
4,4'-DDT
ND
0.0013
0.00030
ug/L
03/28/18 12:35
04/02/18 19:49
1
Dieldrin
ND
0.0013
0.00013
ug/L
03/28/18 12:35
04/02/18 19:49
1
Endosulfan I
ND
0.0013
0.00015
ug/L
03/28/18 12:35
04/02/18 19:49
1
Endosulfan 11
ND
0.0013
0.00012
ug/L
03/28/18 12:35
04/02/18 19:49
1
Endosulfan sulfate
ND
0.0013
0.00030
ug/L
03/28/18 12:35
04/02/18 19:49
1
Endrin
ND
0.0013
0.00023
ug/L
03/28/18 12:35
04/02/18 19:49
1
Endrin aldehyde
ND
0.0013
0.00025
ug/L
03/28/18 12:35
04/02/18 19:49
1
Endrin ketone
ND
0.0013
0.00017
ug/L
03/28/18 12:35
04/02/18 19:49
1
Heptachlor
ND
0.0013
0.00046
ug/L
03/28/18 12:35
04/02/18 19:49
1
Heptachlor epoxide
ND
0.0013
0.00014
ug/L
03/28/18 12:35
04/02/18 19:49
1
Methoxychlor
ND
0.0013
0.00035
ug/L
03/28/18 12:35
04/02/18 19:49
1
Toxaphene
ND
0.10
0.012
ug/L
03/28/18 12:35
04/02/18 19:49
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
69
41- 124
03/28/18 12:35
04102118 19:49
1
Tetrachloro-m-xylene
76
41- 124
03128118 12:35
04102118 19:49
1
DCB Decachlorobiphenyl (Surr)
78 p
64 - 126
03/28/18 12:35
04102118 19:49
1
DCB Decachlorobiphenyl (Surr)
208 X
64 - 126
03128118 12:35
04102118 19:49
1
Method: EPA 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Antimony
ND
2.0
1.1
ug/L
03/30/1813:04
03/31/1812:37
1
Arsenic
ND
1.0
0.32
ug/L
03/30/1813:04
03/31/1812:37
1
Beryllium
ND
1.0
0.057
ug/L
03/30/1813:04
03/31/1812:37
1
Cadmium
ND
1.0
0.13
ug/L
03/30/1813:04
03/31/1812:37
1
Chromium
1.7
J
2.0
0.63
ug/L
03/30/1813:04
03/31/1812:37
1
Copper
ND
2.0
1.3
ug/L
03/30/1813:04
03/31/1812:37
1
Lead
ND
1.0
0.094
ug/L
03/30/1813:04
03/31/1812:37
1
Manganese
2.0
J
5.0
1.4
ug/L
03/30/1813:04
03/31/1812:37
1
Nickel
2.9
1.0
0.31
ug/L
03/30/1813:04
03/31/1812:37
1
Selenium
ND
5.0
0.81
ug/L
03/30/1813:04
03/31/1812:37
1
Silver
ND
1.0
0.12
ug/L
03/30/1813:04
03/31/1812:37
1
Thallium
ND
1.0
0.063
ug/L
03/30/1813:04
03/31/1812:37
1
Zinc
3.2
J
5.0
2.4
ug/L
03/30/1813:04
03/31/1812:37
1
TestAmerica Pittsburgh
Page 56 of 106 4/18/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 7470A - Mercury (CVAA)
Analyte
Result Qualifier
Mercury
ND
General Chemistry
Analyte
Result Qualifier
Total Petroleum Hydrocarbons
ND
(SGT-HEM)
Cr (III)
ND
Cr (VI)
ND
Total Organic Carbon - Duplicates
0.55 J
F
TestAmerica Job ID: 180-76196-1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.20
0.065
ug/L
04/10/1811:20
04/11/1811:08
1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
4.1
1.4
mg/L
04/01/18 14:43
04/02/18 09:06
1
10
3.2
ug/L
04/12/1811:38
1
0.010
0.0032
mg/L
03/28/1812:08
1
1.0
0.51
mg/L
04/03/1817:12
1
TestAmerica Pittsburgh
Page 57 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8260B - Volatile
Organic Compounds
(GC/MS)
Lab Sample ID: MB 180-240660/9
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 240660
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
5.0
2.5
ug/Kg
03/28/18 09:44
1
1,1,2,2-Tetrachloroethane
ND
5.0
3.0
ug/Kg
03/28/18 09:44
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
5.0
1.9
ug/Kg
03/28/18 09:44
1
1,1,2-Trichloroethane
ND
5.0
2.4
ug/Kg
03/28/18 09:44
1
1,1-Dichloroethane
ND
5.0
1.8
ug/Kg
03/28/18 09:44
1
1,1-Dichloroethene
ND
5.0
2.9
ug/Kg
03/28/18 09:44
1
1,2,4-Trichlorobenzene
ND
5.0
1.6
ug/Kg
03/28/18 09:44
1
1,2-Dibromo-3-Chloropropane
ND
5.0
3.1
ug/Kg
03/28/18 09:44
1
1,2-Dichlorobenzene
ND
5.0
4.0
ug/Kg
03/28/18 09:44
1 m
1,2-Dichloroethane
ND
5.0
1.5
ug/Kg
03/28/18 09:44
1
1,2-Dichloropropane
ND
5.0
2.5
ug/Kg
03/28/18 09:44
1
1,3-Dichlorobenzene
ND
5.0
1.6
ug/Kg
03/28/18 09:44
1
1,4-Dichlorobenzene
ND
5.0
1.0
ug/Kg
03/28/18 09:44
1
2-Butanone (MEK)
ND
5.0
2.9
ug/Kg
03/28/18 09:44
1
2-Hexanone
ND
5.0
4.2
ug/Kg
03/28/18 09:44
1
4-Methyl-2-pentanone (MIBK)
ND
5.0
1.9
ug/Kg
03/28/18 09:44
1
Acetone
ND
20
3.2
ug/Kg
03/28/18 09:44
1
Benzene
ND
5.0
2.0
ug/Kg
03/28/18 09:44
1
Bromoform
ND
5.0
2.6
ug/Kg
03/28/18 09:44
1
Bromomethane
ND
5.0
4.5
ug/Kg
03/28/18 09:44
1
Carbon disulfide
ND
5.0
3.0
ug/Kg
03/28/18 09:44
1
Carbon tetrachloride
ND
5.0
3.3
ug/Kg
03/28/18 09:44
1
Chlorobenzene
ND
5.0
1.6
ug/Kg
03/28/18 09:44
1
Chlorodibromomethane
ND
5.0
2.4
ug/Kg
03/28/18 09:44
1
Chloroform
ND
5.0
2.1
ug/Kg
03/28/18 09:44
1
Chloromethane
ND
5.0
3.9
ug/Kg
03/28/18 09:44
1
Chloroethane
ND
5.0
2.6
ug/Kg
03/28/18 09:44
1
cis-1,2-Dichloroethene
ND
5.0
1.6
ug/Kg
03/28/18 09:44
1
cis-1,3-Dichloropropene
ND
5.0
1.6
ug/Kg
03/28/18 09:44
1
Cyclohexane
ND
5.0
1.2
ug/Kg
03/28/18 09:44
1
Dichlorobromomethane
ND
5.0
2.4
ug/Kg
03/28/18 09:44
1
Dichlorodifluoromethane
ND
5.0
2.9
ug/Kg
03/28/18 09:44
1
Ethylbenzene
ND
5.0
2.2
ug/Kg
03/28/18 09:44
1
1,2-Dibromoethane
ND
5.0
2.7
ug/Kg
03/28/18 09:44
1
Isopropylbenzene
ND
5.0
2.3
ug/Kg
03/28/18 09:44
1
Methyl acetate
ND
25
5.9
ug/Kg
03/28/18 09:44
1
Methyl tert-butyl ether
ND
5.0
3.7
ug/Kg
03/28/18 09:44
1
Methylcyclohexane
ND
5.0
2.1
ug/Kg
03/28/18 09:44
1
Methylene Chloride
ND
5.0
2.4
ug/Kg
03/28/18 09:44
1
Styrene
ND
5.0
1.3
ug/Kg
03/28/18 09:44
1
Tetrachloroethene
ND
5.0
2.0
ug/Kg
03/28/18 09:44
1
Toluene
ND
5.0
1.7
ug/Kg
03/28/18 09:44
1
trans- 1,2-Dichloroethene
ND
5.0
2.5
ug/Kg
03/28/18 09:44
1
trans- 1,3-Dichloropropene
ND
5.0
1.7
ug/Kg
03/28/18 09:44
1
Trichloroethene
ND
5.0
1.5
ug/Kg
03/28/18 09:44
1
Trichlorofluoromethane
ND
5.0
1.5
ug/Kg
03/28/18 09:44
1
Xylenes, Total
ND
10
4.3
ug/Kg
03/28/18 09:44
1
Vinyl chloride
ND
5.0
3.7
ug/Kg
03/28/18 09:44
1
TestAmerica Pittsburgh
Page 58 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
MB MB
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 99 62- 118
4-Bromofluorobenzene (Surr) 95 76 - 111
Dibromofluoromethane (Surr) 98 72 - 116
Toluene-d8 (Surr) 107 80 - 129
Lab Sample ID: LCS 180-240660/3
Matrix: Sediment
Analysis Batch: 240660
Analyte
1,1,1-Trich loroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trich loro-1,2,2-trifluoroetha
ne
1,1,2-Trich loroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2,4-Trichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroform
Chloromethane
Chloroethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Cyclohexane
Dichlorobromomethane
Dichlorodifluoromethane
Ethylbenzene
1,2-Dibromoethane
Isopropylbenzene
Methyl acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
m-Xylene & p-Xylene
o-Xylene
Styrene
Tetrachloroethene
TestAmerica Job ID: 180-76196-1
Prepared Analyzed
Dil Fac
03/28/18 09:44
1
03/28/18 09:44
1
03/28/18 09:44
1
03128118 09:44
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit
D %Rec
Limits
40.0
40.2
ug/Kg
100
69 -135
40.0
43.9
ug/Kg
110
71 -125
40.0
42.1
ug/Kg
105
61 -137
40.0
43.7
ug/Kg
109
78 -118
40.0
40.9
ug/Kg
102
67 -129
40.0
39.9
ug/Kg
100
59 -128
40.0
30.3
ug/Kg
76
65 -135
40.0
37.4
ug/Kg
94
54 -129
40.0
39.1
ug/Kg
98
78 -118
40.0
41.9
ug/Kg
105
67 -123
40.0
39.9
ug/Kg
100
80 -121
40.0
40.6
ug/Kg
102
78 -118
40.0
39.7
ug/Kg
99
78 -118
40.0
45.1
ug/Kg
113
30 -150
40.0
47.4
ug/Kg
118
36 -150
40.0
42.7
ug/Kg
107
62 -145
40.0
57.1
ug/Kg
143
36 -150
40.0
42.1
ug/Kg
105
78 -118
40.0
35.8
ug/Kg
89
56 -150
40.0
35.7
ug/Kg
89
34 -150
40.0
35.6
ug/Kg
89
66 -128
40.0
39.0
ug/Kg
98
60 -137
40.0
41.6
ug/Kg
104
78 -118
40.0
37.6
ug/Kg
94
58 -140
40.0
40.8
ug/Kg
102
68 -124
40.0
35.9
ug/Kg
90
46 -150
40.0
41.6
ug/Kg
104
37 -150
40.0
43.0
ug/Kg
108
71 -120
40.0
39.4
ug/Kg
99
70 -131
40.0
40.2
ug/Kg
100
70 -133
40.0
38.3
ug/Kg
96
66 -136
40.0
57.3
ug/Kg
143
16 -150
40.0
41.0
ug/Kg
103
78 -118
40.0
43.4
ug/Kg
109
78 -118
40.0
39.7
ug/Kg
99
76 -123
80.0
93.8
ug/Kg
117
64 -140
40.0
42.3
ug/Kg
106
73 -121
40.0
42.5
ug/Kg
106
75 -124
40.0
40.1
ug/Kg
100
68 -120
40.0
40.9
ug/Kg
102
78 -118
40.0
41.1
ug/Kg
103
78 -118
40.0
39.7
ug/Kg
99
79 -119
40.0
41.6
ug/Kg
104
78 -118
Page 59 of 106
TestAmerica Pittsburgh
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 180-240660/3
Matrix: Sediment
Analysis Batch: 240660
TestAmerica Job ID: 180-76196-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
Toluene
40.0
41.2
ug/Kg
103
79 -121
trans- 1,2-Dichloroethene
40.0
42.4
ug/Kg
106
71-123
trans- 1,3-Dichloropropene
40.0
37.7
ug/Kg
94
62 -133
Trichloroethene
40.0
42.6
ug/Kg
106
76 -120
Trichlorofluoromethane
40.0
38.6
ug/Kg
96
25 -150
Xylenes, Total
80.0
82.0
ug/Kg
103
78 -118
Vinyl chloride
40.0
39.7
ug/Kg
99
53 -148
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
105
62- 118
4-Bromofluorobenzene (Surr)
93
76 - 111
Dibromofluoromethane (Surr)
103
72 - 116
Toluene-d8 (Surr)
105
80 - 129
Lab Sample ID: MB 180-240736/5
Matrix: Water
Analysis Batch: 240736
MB MB
Analyte
Result Qualifier
RL
MDL
Unit D
1,1,1-Trichloroethane
ND
1.0
0.60
ug/L
1,1,2,2-Tetrachloroethane
ND
1.0
0.60
ug/L
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
0.86
ug/L
1,1,2-Trichloroethane
ND
1.0
0.45
ug/L
1,1-Dichloroethane
ND
1.0
0.63
ug/L
1,1-Dichloroethene
ND
1.0
0.55
ug/L
1,2,4-Trichlorobenzene
ND
1.0
0.77
ug/L
1,2-Dibromo-3-Chloropropane
ND
1.0
0.89
ug/L
1,2-Dichlorobenzene
ND
1.0
0.36
ug/L
1,2-Dichloroethane
ND
1.0
0.57
ug/L
1,2-Dichloropropane
ND
1.0
0.66
ug/L
1,3-Dichlorobenzene
ND
1.0
0.50
ug/L
1,4-Dichlorobenzene
ND
1.0
0.54
ug/L
2-Butanone (MEK)
ND
5.0
2.6
ug/L
2-Hexanone
ND
5.0
3.3
ug/L
4-Methyl-2-pentanone (MIBK)
ND
5.0
3.1
ug/L
Acetone
ND
5.0
3.4
ug/L
Benzene
ND
1.0
0.60
ug/L
Bromoform
ND
1.0
0.98
ug/L
Bromomethane
ND
1.0
0.89
ug/L
Carbon disulfide
ND
1.0
0.88
ug/L
Carbon tetrachloride
ND
1.0
0.88
ug/L
Chlorobenzene
ND
1.0
0.50
ug/L
Chlorodibromomethane
ND
1.0
0.84
ug/L
Chloroethane
ND
1.0
0.90
ug/L
Chloroform
ND
1.0
0.60
ug/L
Chloromethane
ND
1.0
0.90
ug/L
cis-1,2-Dichloroethene
ND
1.0
0.71
ug/L
cis-1,3-Dichloropropene
ND
1.0
0.59
ug/L
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed
Dil Fac
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
03/28/18 18:24
1
TestAmerica Pittsburgh
Page 60 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8260B - Volatile
Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 180-240736/5
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 240736
MB MB
Analyte
Result Qualifier
RL
MDL
Unit D
Prepared Analyzed
Dil Fac
Cyclohexane
ND
1.0
0.63
ug/L
03/28/18 18:24
1
Dichlorobromomethane
ND
1.0
0.64
ug/L
03/28/18 18:24
1
Dichlorodifluoromethane
ND
1.0
0.83
ug/L
03/28/18 18:24
1
Ethylbenzene
ND
1.0
0.51
ug/L
03/28/18 18:24
1
1,2-Dibromoethane
ND
1.0
0.50
ug/L
03/28/18 18:24
1
Isopropylbenzene
ND
1.0
0.34
ug/L
03/28/18 18:24
1
Methyl acetate
ND
5.0
1.7
ug/L
03/28/18 18:24
1
Methyl tert-butyl ether
ND
1.0
0.59
ug/L
03/28/18 18:24
1
Methylcyclohexane
ND
1.0
0.61
ug/L
03/28/18 18:24
1 m
Methylene Chloride
ND
1.0
0.36
ug/L
03/28/18 18:24
1
Styrene
ND
1.0
0.47
ug/L
03/28/18 18:24
1
Tetrachloroethene
ND
1.0
0.47
ug/L
03/28/18 18:24
1
Toluene
ND
1.0
0.46
ug/L
03/28/18 18:24
1
trans- 1,2-Dichloroethene
ND
1.0
0.67
ug/L
03/28/18 18:24
1
trans- 1,3-Dichloropropene
ND
1.0
0.58
ug/L
03/28/18 18:24
1
Trichloroethene
ND
1.0
0.69
ug/L
03/28/18 18:24
1
Trichlorofluoromethane
ND
1.0
0.87
ug/L
03/28/18 18:24
1
Vinyl chloride
ND
1.0
0.88
ug/L
03/28/18 18:24
1
Xylenes, Total
ND
2.0
0.89
ug/L
03/28/18 18:24
1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
102
65- 121
03/28/18 18:24
1
4-Bromofluorobenzene (Surr)
87
80 - 120
03/28/18 18:24
1
Dibromofluoromethane (Surr)
100
73 - 120
03/28/18 18:24
1
Toluene-d8 (Surr)
99
73 - 120
03128118 18:24
1
Lab Sample ID: LCS 180-240736/3
Matrix: Water
Analysis Batch: 240736
Analyte
1,1,1-Trich loroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trich loro-1,2,2-trifluoroetha
ne
1,1,2-Trich loroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2,4-Trichoorobenzene
1,2-Dibromo-3-Chloropropane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
4-Methyl-2-pentanone (MIBK)
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit
D %Rec
Limits
10.0
10.5
ug/L
105
66 -129
10.0
9.83
ug/L
98
72 -128
10.0
10.5
ug/L
105
55 -138
10.0
10.1
ug/L
101
74 -126
10.0
9.71
ug/L
97
66 -122
10.0
10.4
ug/L
104
64 -131
10.0
7.64
ug/L
76
39 -147
10.0
7.10
ug/L
71
48 -132
10.0
9.36
ug/L
94
74 -121
10.0
9.46
ug/L
95
63 -130
10.0
9.44
ug/L
94
67 -119
10.0
9.33
ug/L
93
77 -119
10.0
9.36
ug/L
94
76 -118
20.0
17.2
ug/L
86
37 -150
20.0
15.7
ug/L
79
37 -150
20.0
15.1
ug/L
75
41 -135
Page 61 of 106
TestAmerica Pittsburgh
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 180-240736/3 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240736
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
Acetone
20.0
19.5
ug/L
98
24 -150
Benzene
10.0
10.1
ug/L
101
75 -123
Bromoform
10.0
8.85
ug/L
88
54 -136
Bromomethane
10.0
8.76
ug/L
88
37 -150
Carbon disulfide
10.0
9.27
ug/L
93
20 -150
Carbon tetrachloride
10.0
10.8
ug/L
108
58 -145
Chlorobenzene
10.0
10.8
ug/L
108
79 -124
Chlorodibromomethane
10.0
9.95
ug/L
100
63 -131
Chloroethane
10.0
14.2
ug/L
142
44 -139
Chloroform
10.0
9.68
ug/L
97
72 -123
Chloromethane
10.0
7.47
ug/L
75
49 -135
cis-1,2-Dichloroethene
10.0
9.74
ug/L
97
73 -120
cis-1,3-Dichloropropene
10.0
8.69
ug/L
87
61 -127
Cyclohexane
10.0
9.15
ug/L
92
50 -133
Dichlorobromomethane
10.0
9.01
ug/L
90
62 -127
Dichlorodifluoromethane
10.0
6.37
ug/L
64
33 -150
Ethylbenzene
10.0
10.0
ug/L
100
77 -124
1,2-Dibromoethane
10.0
9.57
ug/L
96
76-128
Isopropylbenzene
10.0
10.0
ug/L
100
74 -131
Methyl acetate
20.0
14.7
ug/L
74
49 -150
Methyl tert-butyl ether
10.0
9.08
ug/L
91
66 -130
Methylcyclohexane
10.0
9.38
ug/L
94
62 -129
Methylene Chloride
10.0
10.0
ug/L
100
66 -123
m-Xylene & p-Xylene
10.0
10.1
ug/L
101
77 -125
o-Xylene
10.0
9.82
ug/L
98
75 -124
Styrene
10.0
9.73
ug/L
97
80 -125
Tetrachloroethene
10.0
11.1
ug/L
111
76 -128
Toluene
10.0
11.4
ug/L
114
76 -129
trans- 1,2-Dichloroethene
10.0
10.6
ug/L
106
70-123
trans- 1,3-Dichloropropene
10.0
10.0
ug/L
100
61-136
Trichloroethene
10.0
9.46
ug/L
95
74 -121
Trichlorofluoromethane
10.0
12.8
ug/L
128
43 -150
Vinyl chloride
10.0
8.50
ug/L
85
52 -136
Xylenes, Total
20.0
19.9
ug/L
100
76 -124
LCS LCS
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 99 65- 121
4-Bromofluorobenzene (Surr) 102 80 - 120
Dibromofluoromethane (Surr) 102 73 - 120
Toluene-d8 (Surr) 120 73 - 120
Lab Sample ID: MB 180-240865/6
Matrix: Water
Analysis Batch: 240865
MB MB
Analyte Result Qualifier
1,1,1-Trichloroethane ND
1,1,2,2-Tetrachloroethane ND
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
1.0 0.60 ug/L 03/29/1819:45 1
1.0 0.60 ug/L 03/29/1819:45 1
Page 62 of 106
TestAmerica Pittsburgh
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8260B - Volatile
Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 180-240865/6
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 240865
MB MB
Analyte
Result Qualifier
RL
MDL
Unit D
Prepared Analyzed
Dil Fac
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
0.86
ug/L
03/29/18 19:45
1
1,1,2-Trichloroethane
ND
1.0
0.45
ug/L
03/29/18 19:45
1
1,1-Dichloroethane
ND
1.0
0.63
ug/L
03/29/18 19:45
1
1,1-Dichloroethene
ND
1.0
0.55
ug/L
03/29/18 19:45
1
1,2,4-Trichlorobenzene
ND
1.0
0.77
ug/L
03/29/18 19:45
1
1,2-Dibromo-3-Chloropropane
ND
1.0
0.89
ug/L
03/29/18 19:45
1
1,2-Dichlorobenzene
ND
1.0
0.36
ug/L
03/29/18 19:45
1
1,2-Dichloroethane
ND
1.0
0.57
ug/L
03/29/18 19:45
1
1,2-Dichloropropane
ND
1.0
0.66
ug/L
03/29/18 19:45
1
1,3-Dichlorobenzene
ND
1.0
0.50
ug/L
03/29/18 19:45
1
1,4-Dichlorobenzene
ND
1.0
0.54
ug/L
03/29/18 19:45
1
2-Butanone (MEK)
ND
5.0
2.6
ug/L
03/29/18 19:45
1
2-Hexanone
ND
5.0
3.3
ug/L
03/29/18 19:45
1
4-Methyl-2-pentanone (MIBK)
ND
5.0
3.1
ug/L
03/29/18 19:45
1
Acetone
ND
5.0
3.4
ug/L
03/29/18 19:45
1
Benzene
ND
1.0
0.60
ug/L
03/29/18 19:45
1
Bromoform
ND
1.0
0.98
ug/L
03/29/18 19:45
1
Bromomethane
ND
1.0
0.89
ug/L
03/29/18 19:45
1
Carbon disulfide
ND
1.0
0.88
ug/L
03/29/18 19:45
1
Carbon tetrachloride
ND
1.0
0.88
ug/L
03/29/18 19:45
1
Chlorobenzene
ND
1.0
0.50
ug/L
03/29/18 19:45
1
Chlorodibromomethane
ND
1.0
0.84
ug/L
03/29/18 19:45
1
Chloroethane
ND
1.0
0.90
ug/L
03/29/18 19:45
1
Chloroform
ND
1.0
0.60
ug/L
03/29/18 19:45
1
Chloromethane
ND
1.0
0.90
ug/L
03/29/18 19:45
1
cis-1,2-Dichloroethene
ND
1.0
0.71
ug/L
03/29/18 19:45
1
cis-1,3-Dichloropropene
ND
1.0
0.59
ug/L
03/29/18 19:45
1
Cyclohexane
ND
1.0
0.63
ug/L
03/29/18 19:45
1
Dichlorobromomethane
ND
1.0
0.64
ug/L
03/29/18 19:45
1
Dichlorodifluoromethane
ND
1.0
0.83
ug/L
03/29/18 19:45
1
Ethylbenzene
ND
1.0
0.51
ug/L
03/29/18 19:45
1
1,2-Dibromoethane
ND
1.0
0.50
ug/L
03/29/18 19:45
1
Isopropylbenzene
ND
1.0
0.34
ug/L
03/29/18 19:45
1
Methyl acetate
ND
5.0
1.7
ug/L
03/29/18 19:45
1
Methyl tert-butyl ether
ND
1.0
0.59
ug/L
03/29/18 19:45
1
Methylcyclohexane
ND
1.0
0.61
ug/L
03/29/18 19:45
1
Methylene Chloride
ND
1.0
0.36
ug/L
03/29/18 19:45
1
Styrene
ND
1.0
0.47
ug/L
03/29/18 19:45
1
Tetrachloroethene
ND
1.0
0.47
ug/L
03/29/18 19:45
1
Toluene
ND
1.0
0.46
ug/L
03/29/18 19:45
1
trans- 1,2-Dichloroethene
ND
1.0
0.67
ug/L
03/29/18 19:45
1
trans- 1,3-Dichloropropene
ND
1.0
0.58
ug/L
03/29/18 19:45
1
Trichloroethene
ND
1.0
0.69
ug/L
03/29/18 19:45
1
Trichlorofluoromethane
ND
1.0
0.87
ug/L
03/29/18 19:45
1
Vinyl chloride
ND
1.0
0.88
ug/L
03/29/18 19:45
1
Xylenes, Total
ND
2.0
0.89
ug/L
03/29/18 19:45
1
TestAmerica Pittsburgh
Page 63 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 180-240865/6
Matrix: Water
Analysis Batch: 240865
MB MB
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 84 65- 121
4-Bromofluorobenzene (Surr) 89 80 - 120
Dibromofluoromethane (Surr) 84 73 - 120
Toluene-d8 (Surr) 92 73 - 120
Lab Sample ID: LCS 180-240865/4
Matrix: Water
Analysis Batch: 240865
Analyte
1,1,1-Trich loroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trich loro-1,2,2-trifluoroetha
ne
1,1,2-Trich loroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2,4-Trichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Cyclohexane
Dichlorobromomethane
Dichlorodifluoromethane
Ethylbenzene
1,2-Dibromoethane
Isopropylbenzene
Methyl acetate
Methyl tert-butyl ether
TestAmerica Job ID: 180-76196-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed
DR Fac
031291181
1
03/29/18 19:45
1
03/29/18 19:45
1
03/29/18 19:45
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit
D %Rec
Limits
10.0
11.7
ug/L
117
66 -129
10.0
8.26
ug/L
83
72 -128
10.0
10.9
ug/L
109
55 -138
10.0
10.4
ug/L
104
74 -126
10.0
9.81
ug/L
98
66 -122
10.0
9.99
ug/L
100
64 -131
10.0
6.21
ug/L
62
39 -147
10.0
7.26
ug/L
73
48 -132
10.0
9.44
ug/L
94
74 -121
10.0
9.64
ug/L
96
63 -130
10.0
9.75
ug/L
98
67 -119
10.0
10.3
ug/L
103
77 -119
10.0
10.5
ug/L
105
76 -118
20.0
18.1
ug/L
91
37 -150
20.0
19.6
ug/L
98
37 -150
20.0
18.1
ug/L
91
41 -135
20.0
19.2
ug/L
96
24 -150
10.0
10.3
ug/L
103
75 -123
10.0
7.61
ug/L
76
54 -136
10.0
12.2
ug/L
122
37 -150
10.0
8.81
ug/L
88
20 -150
10.0
12.4
ug/L
124
58 -145
10.0
10.6
ug/L
106
79 -124
10.0
10.1
ug/L
101
63 -131
10.0
12.0
ug/L
120
44 -139
10.0
9.48
ug/L
95
72 -123
10.0
9.35
ug/L
93
49 -135
10.0
9.69
ug/L
97
73 -120
10.0
10.7
ug/L
107
61 -127
10.0
10.3
ug/L
103
50 -133
10.0
8.95
ug/L
89
62 -127
10.0
11.1
ug/L
111
33 -150
10.0
10.2
ug/L
102
77 -124
10.0
10.1
ug/L
101
76 -128
10.0
9.11
ug/L
91
74 -131
20.0
21.3
ug/L
106
49 -150
10.0
8.96
ug/L
90
66 -130
Page 64 of 106
TestAmerica Pittsburgh
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 180-240865/4 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240865
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
Methylcyclohexane
10.0
9.87
ug/L
99
62 -129
Methylene Chloride
10.0
9.95
ug/L
99
66 -123
m-Xylene & p-Xylene
10.0
10.4
ug/L
104
77 -125
o-Xylene
10.0
9.44
ug/L
94
75 -124
Styrene
10.0
9.66
ug/L
97
80 -125
Tetrachloroethene
10.0
11.3
ug/L
113
76 -128
Toluene
10.0
10.7
ug/L
107
76 -129
trans- 1,2-Dichloroethene
10.0
10.4
ug/L
104
70-123
trans- 1,3-Dichloropropene
10.0
10.3
ug/L
103
61-136
Trichloroethene
10.0
11.1
ug/L
111
74 -121
Trichlorofluoromethane
10.0
12.5
ug/L
125
43 -150
Vinyl chloride
10.0
9.99
ug/L
100
52 -136
Xylenes, Total
20.0
19.8
ug/L
99
76 -124
LCS LCS
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 93 65- 121
4-Bromofluorobenzene (Surr) 95 80 - 120
Dibromofluoromethane (Surr) 93 73 - 120
Toluene-d8 (Surr) 114 73 - 120
Lab Sample ID: MB 180-240896/7
Matrix: Sediment
Analysis Batch: 240896
Analyte
MB MB
Result Qualifier
RL
MDL
Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
1,1,1-Trichloroethane
ND
5.0
2.5
ug/Kg
03/30/18 09:51
1
1,1,2,2-Tetrachloroethane
ND
5.0
3.0
ug/Kg
03/30/18 09:51
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
5.0
1.9
ug/Kg
03/30/18 09:51
1
1,1,2-Trichloroethane
ND
5.0
2.4
ug/Kg
03/30/18 09:51
1
1,1-Dichloroethane
ND
5.0
1.8
ug/Kg
03/30/18 09:51
1
1,1-Dichloroethene
ND
5.0
2.9
ug/Kg
03/30/18 09:51
1
1,2,4-Trichlorobenzene
ND
5.0
1.6
ug/Kg
03/30/18 09:51
1
1,2-Dibromo-3-Chloropropane
ND
5.0
3.1
ug/Kg
03/30/18 09:51
1
1,2-Dichlorobenzene
ND
5.0
4.0
ug/Kg
03/30/18 09:51
1
1,2-Dichloroethane
ND
5.0
1.5
ug/Kg
03/30/18 09:51
1
1,2-Dichloropropane
ND
5.0
2.5
ug/Kg
03/30/18 09:51
1
1,3-Dichlorobenzene
ND
5.0
1.6
ug/Kg
03/30/18 09:51
1
1,4-Dichlorobenzene
ND
5.0
1.0
ug/Kg
03/30/18 09:51
1
2-Butanone (MEK)
ND
5.0
2.9
ug/Kg
03/30/18 09:51
1
2-Hexanone
ND
5.0
4.2
ug/Kg
03/30/18 09:51
1
4-Methyl-2-pentanone (MIBK)
ND
5.0
1.9
ug/Kg
03/30/18 09:51
1
Acetone
ND
20
3.2
ug/Kg
03/30/18 09:51
1
Benzene
ND
5.0
2.0
ug/Kg
03/30/18 09:51
1
Bromoform
ND
5.0
2.6
ug/Kg
03/30/18 09:51
1
Bromomethane
ND
5.0
4.5
ug/Kg
03/30/18 09:51
1
Carbon disulfide
ND
5.0
3.0
ug/Kg
03/30/18 09:51
1
Carbon tetrachloride
ND
5.0
3.3
ug/Kg
03/30/18 09:51
1
Chlorobenzene
ND
5.0
1.6
ug/Kg
03/30/18 09:51
1
TestAmerica Pittsburgh
Page 65 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8260B - Volatile
Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 180-240896/7
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 240896
MB MB
Analyte
Result Qualifier
RL
MDL
Unit D
Prepared Analyzed
Dil Fac
Chlorodibromomethane
ND
5.0
2.4
ug/Kg
03/30/18 09:51
1
Chloroform
ND
5.0
2.1
ug/Kg
03/30/18 09:51
1
Chloromethane
ND
5.0
3.9
ug/Kg
03/30/18 09:51
1
Chloroethane
ND
5.0
2.6
ug/Kg
03/30/18 09:51
1
cis-1,2-Dichloroethene
ND
5.0
1.6
ug/Kg
03/30/18 09:51
1
cis-1,3-Dichloropropene
ND
5.0
1.6
ug/Kg
03/30/18 09:51
1
Cyclohexane
ND
5.0
1.2
ug/Kg
03/30/18 09:51
1
Dichlorobromomethane
ND
5.0
2.4
ug/Kg
03/30/18 09:51
1
Dichlorodifluoromethane
ND
5.0
2.9
ug/Kg
03/30/18 09:51
1 m
Ethylbenzene
ND
5.0
2.2
ug/Kg
03/30/18 09:51
1
1,2-Dibromoethane
ND
5.0
2.7
ug/Kg
03/30/18 09:51
1
Isopropylbenzene
ND
5.0
2.3
ug/Kg
03/30/18 09:51
1
Methyl acetate
ND
25
5.9
ug/Kg
03/30/18 09:51
1
Methyl tert-butyl ether
ND
5.0
3.7
ug/Kg
03/30/18 09:51
1
Methylcyclohexane
ND
5.0
2.1
ug/Kg
03/30/18 09:51
1
Methylene Chloride
2.54 J
5.0
2.4
ug/Kg
03/30/18 09:51
1
Styrene
ND
5.0
1.3
ug/Kg
03/30/18 09:51
1
Tetrachloroethene
ND
5.0
2.0
ug/Kg
03/30/18 09:51
1
Toluene
ND
5.0
1.7
ug/Kg
03/30/18 09:51
1
trans- 1,2-Dichloroethene
ND
5.0
2.5
ug/Kg
03/30/18 09:51
1
trans- 1,3-Dichloropropene
ND
5.0
1.7
ug/Kg
03/30/18 09:51
1
Trichloroethene
ND
5.0
1.5
ug/Kg
03/30/18 09:51
1
Trichlorofluoromethane
ND
5.0
1.5
ug/Kg
03/30/18 09:51
1
Xylenes, Total
ND
10
4.3
ug/Kg
03/30/18 09:51
1
Vinyl chloride
ND
5.0
3.7
ug/Kg
03/30/18 09:51
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
92
62- 118
03130118 09:51
1
4-Bromofluorobenzene (Surr)
92
76 - 111
03130118 09:51
1
Dibromofluoromethane (Surr)
95
72 - 116
03130118 09:51
1
Toluene-d8 (Surr)
106
80 - 129
03130118 09:51
1
Lab Sample ID: LCS 180-240896/3
Client Sample ID: Lab Control Sample
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 240896
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,1,1-Trichloroethane
40.0
39.7
ug/Kg
99
69-135
1,1,2,2-Tetrachloroethene
40.0
36.8
ug/Kg
92
71-125
1, 1, 2-Trich loro- 1 , 2,2-trifl uoroetha
40.0
44.3
ug/Kg
ill
61-137
ne
1,1,2-Trichloroethane
40.0
40.5
ug/Kg
101
78-118
1,1-Dichloroethane
40.0
40.1
ug/Kg
100
67-129
1,1-Dichloroethene
40.0
43.0
ug/Kg
108
59-128
1,2,4-Trichlorobenzene
40.0
38.8
ug/Kg
97
65-135
1,2-Dibromo-3-Chloropropane
40.0
26.9
ug/Kg
67
54 -129
1,2-Dichlorobenzene
40.0
40.4
ug/Kg
101
78 -118
1,2-Dichloroethane
40.0
37.4
ug/Kg
94
67 -123
TestAmerica Pittsburgh
Page 66 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 180-240896/3 Client Sample ID: Lab Control Sample
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240896
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
1,2-Dichloropropane
40.0
39.5
ug/Kg
99
80 -121
1,3-Dichlorobenzene
40.0
42.2
ug/Kg
105
78 -118
1,4-Dichlorobenzene
40.0
41.7
ug/Kg
104
78 -118
2-Butanone (MEK)
40.0
30.9
ug/Kg
77
30 -150
2-Hexanone
40.0
33.9
ug/Kg
85
36 -150
4-Methyl-2-pentanone (MIBK)
40.0
32.4
ug/Kg
81
62 -145
Acetone
40.0
41.2
ug/Kg
103
36 -150
Benzene
40.0
42.5
ug/Kg
106
78-118
Bromoform
40.0
33.3
ug/Kg
83
56 -150
Bromomethane
40.0
32.1
ug/Kg
80
34 -150
Carbon disulfide
40.0
39.8
ug/Kg
99
66 -128
Carbon tetrachloride
40.0
39.1
ug/Kg
98
60 -137
Chlorobenzene
40.0
43.7
ug/Kg
109
78 -118
Chlorodibromomethane
40.0
36.6
ug/Kg
91
58 -140
Chloroform
40.0
39.6
ug/Kg
99
68 -124
Chloromethane
40.0
39.3
ug/Kg
98
46 -150
Chloroethane
40.0
37.9
ug/Kg
95
37 -150
cis-1,2-Dichloroethene
40.0
42.9
ug/Kg
107
71 -120
cis-1,3-Dichloropropene
40.0
37.6
ug/Kg
94
70 -131
Cyclohexane
40.0
41.3
ug/Kg
103
70 -133
Dichlorobromomethane
40.0
36.8
ug/Kg
92
66 -136
Dichlorodifluoromethane
40.0
56.0
ug/Kg
140
16 -150
Ethylbenzene
40.0
44.2
ug/Kg
110
78 -118
1,2-Dibromoethane
40.0
39.0
ug/Kg
98
78-118
Isopropylbenzene
40.0
42.4
ug/Kg
106
76 -123
Methyl acetate
80.0
63.3
ug/Kg
79
64 -140
Methyl tert-butyl ether
40.0
36.4
ug/Kg
91
73 -121
Methylcyclohexane
40.0
44.2
ug/Kg
111
75 -124
Methylene Chloride
40.0
41.5
ug/Kg
104
68 -120
m-Xylene & p-Xylene
40.0
42.9
ug/Kg
107
78 -118
o-Xylene
40.0
42.9
ug/Kg
107
78 -118
Styrene
40.0
41.6
ug/Kg
104
79 -119
Tetrachloroethene
40.0
45.4
ug/Kg
113
78 -118
Toluene
40.0
43.5
ug/Kg
109
79 -121
trans- 1,2-Dichloroethene
40.0
43.2
ug/Kg
108
71-123
trans- 1,3-Dichloropropene
40.0
36.1
ug/Kg
90
62 -133
Trichloroethene
40.0
43.2
ug/Kg
108
76 -120
Trichlorofluoromethane
40.0
42.4
ug/Kg
106
25 -150
Xylenes, Total
80.0
85.8
ug/Kg
107
78 -118
Vinyl chloride
40.0
40.4
ug/Kg
101
53 -148
LCS LCS
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 88 62- 118
4-Bromofluorobenzene (Surr) 93 76 - 111
Dibromofluoromethane (Surr) 101 72 - 116
Toluene-d8 (Surr) 107 80 - 129
TestAmerica Pittsburgh
Page 67 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8260B - Volatile
Organic Compounds
(GC/MS) (Continued)
Lab Sample ID: MB 180-241049/6
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241049
MB MB
Analyte
Result Qualifier
RL
MDL
Unit D
Prepared Analyzed
Dil Fac
1,1,1-Trichloroethane
ND
5.0
2.5
ug/Kg
04/02/18 08:53
1
1,1,2,2-Tetrachloroethane
ND
5.0
3.0
ug/Kg
04/02/18 08:53
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
5.0
1.9
ug/Kg
04/02/18 08:53
1
1,1,2-Trichloroethane
ND
5.0
2.4
ug/Kg
04/02/18 08:53
1
1,1-Dichloroethane
ND
5.0
1.8
ug/Kg
04/02/18 08:53
1
1,1-Dichloroethene
ND
5.0
2.9
ug/Kg
04/02/18 08:53
1
1,2,4-Trichlorobenzene
ND
5.0
1.6
ug/Kg
04/02/18 08:53
1
1,2-Dibromo-3-Chloropropane
ND
5.0
3.1
ug/Kg
04/02/18 08:53
1
1,2-Dichlorobenzene
ND
5.0
4.0
ug/Kg
04/02/18 08:53
1 m
1,2-Dichloroethane
ND
5.0
1.5
ug/Kg
04/02/18 08:53
1
1,2-Dichloropropane
ND
5.0
2.5
ug/Kg
04/02/18 08:53
1
1,3-Dichlorobenzene
ND
5.0
1.6
ug/Kg
04/02/18 08:53
1
1,4-Dichlorobenzene
ND
5.0
1.0
ug/Kg
04/02/18 08:53
1
2-Butanone (MEK)
ND
5.0
2.9
ug/Kg
04/02/18 08:53
1
2-Hexanone
ND
5.0
4.2
ug/Kg
04/02/18 08:53
1
4-Methyl-2-pentanone (MIBK)
ND
5.0
1.9
ug/Kg
04/02/18 08:53
1
Acetone
ND
20
3.2
ug/Kg
04/02/18 08:53
1
Benzene
ND
5.0
2.0
ug/Kg
04/02/18 08:53
1
Bromoform
ND
5.0
2.6
ug/Kg
04/02/18 08:53
1
Bromomethane
ND
5.0
4.5
ug/Kg
04/02/18 08:53
1
Carbon disulfide
ND
5.0
3.0
ug/Kg
04/02/18 08:53
1
Carbon tetrachloride
ND
5.0
3.3
ug/Kg
04/02/18 08:53
1
Chlorobenzene
ND
5.0
1.6
ug/Kg
04/02/18 08:53
1
Chlorodibromomethane
ND
5.0
2.4
ug/Kg
04/02/18 08:53
1
Chloroform
ND
5.0
2.1
ug/Kg
04/02/18 08:53
1
Chloromethane
ND
5.0
3.9
ug/Kg
04/02/18 08:53
1
Chloroethane
ND
5.0
2.6
ug/Kg
04/02/18 08:53
1
cis-1,2-Dichloroethene
ND
5.0
1.6
ug/Kg
04/02/18 08:53
1
cis-1,3-Dichloropropene
ND
5.0
1.6
ug/Kg
04/02/18 08:53
1
Cyclohexane
ND
5.0
1.2
ug/Kg
04/02/18 08:53
1
Dichlorobromomethane
ND
5.0
2.4
ug/Kg
04/02/18 08:53
1
Dichlorodifluoromethane
ND
5.0
2.9
ug/Kg
04/02/18 08:53
1
Ethylbenzene
ND
5.0
2.2
ug/Kg
04/02/18 08:53
1
1,2-Dibromoethane
ND
5.0
2.7
ug/Kg
04/02/18 08:53
1
Isopropylbenzene
ND
5.0
2.3
ug/Kg
04/02/18 08:53
1
Methyl acetate
ND
25
5.9
ug/Kg
04/02/18 08:53
1
Methyl tert-butyl ether
ND
5.0
3.7
ug/Kg
04/02/18 08:53
1
Methylcyclohexane
ND
5.0
2.1
ug/Kg
04/02/18 08:53
1
Methylene Chloride
2.45 J
5.0
2.4
ug/Kg
04/02/18 08:53
1
Styrene
ND
5.0
1.3
ug/Kg
04/02/18 08:53
1
Tetrachloroethene
ND
5.0
2.0
ug/Kg
04/02/18 08:53
1
Toluene
ND
5.0
1.7
ug/Kg
04/02/18 08:53
1
trans- 1,2-Dichloroethene
ND
5.0
2.5
ug/Kg
04/02/18 08:53
1
trans- 1,3-Dichloropropene
ND
5.0
1.7
ug/Kg
04/02/18 08:53
1
Trichloroethene
ND
5.0
1.5
ug/Kg
04/02/18 08:53
1
Trichlorofluoromethane
ND
5.0
1.5
ug/Kg
04/02/18 08:53
1
Xylenes, Total
ND
10
4.3
ug/Kg
04/02/18 08:53
1
Vinyl chloride
ND
5.0
3.7
ug/Kg
04/02/18 08:53
1
TestAmerica Pittsburgh
Page 68 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
MB MB
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 94 62- 118
4-Bromofluorobenzene (Surr) 96 76 - 111
Dibromofluoromethane (Surr) 102 72 - 116
Toluene-d8 (Surr) 114 80 - 129
Lab Sample ID: LCS 180-241049/3
Matrix: Sediment
Analysis Batch: 241049
Analyte
1,1,1-Trich loroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trich loro-1,2,2-trifluoroetha
ne
1,1,2-Trich loroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2,4-Trichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroform
Chloromethane
Chloroethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Cyclohexane
Dichlorobromomethane
Dichlorodifluoromethane
Ethylbenzene
1,2-Dibromoethane
Isopropylbenzene
Methyl acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
m-Xylene & p-Xylene
o-Xylene
Styrene
Tetrachloroethene
TestAmerica Job ID: 180-76196-1
Prepared Analyzed
Dil Fac
04/02/18 08:53
1
04102118 08:53
1
04/02/18 08:53
1
04102118 08:53
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit
D %Rec
Limits
40.0
40.2
ug/Kg
101
69 -135
40.0
30.9
ug/Kg
77
71 -125
40.0
45.6
ug/Kg
114
61 -137
40.0
35.9
ug/Kg
90
78 -118
40.0
41.4
ug/Kg
103
67 -129
40.0
42.7
ug/Kg
107
59 -128
40.0
36.0
ug/Kg
90
65 -135
40.0
23.5
ug/Kg
59
54 -129
40.0
38.3
ug/Kg
96
78 -118
40.0
35.9
ug/Kg
90
67 -123
40.0
38.8
ug/Kg
97
80 -121
40.0
41.0
ug/Kg
102
78 -118
40.0
39.8
ug/Kg
99
78 -118
40.0
27.0
ug/Kg
67
30 -150
40.0
27.0
ug/Kg
68
36 -150
40.0
26.5
ug/Kg
66
62 -145
40.0
32.9
ug/Kg
82
36 -150
40.0
42.8
ug/Kg
107
78 -118
40.0
28.6
ug/Kg
71
56 -150
40.0
34.1
ug/Kg
85
34 -150
40.0
38.4
ug/Kg
96
66 -128
40.0
40.3
ug/Kg
101
60 -137
40.0
41.7
ug/Kg
104
78 -118
40.0
33.6
ug/Kg
84
58 -140
40.0
40.2
ug/Kg
101
68 -124
40.0
37.8
ug/Kg
95
46 -150
40.0
40.1
ug/Kg
100
37 -150
40.0
43.0
ug/Kg
107
71 -120
40.0
36.9
ug/Kg
92
70 -131
40.0
41.6
ug/Kg
104
70 -133
40.0
35.8
ug/Kg
90
66 -136
40.0
50.0
ug/Kg
125
16 -150
40.0
41.7
ug/Kg
104
78 -118
40.0
34.1
ug/Kg
85
78 -118
40.0
40.8
ug/Kg
102
76 -123
80.0
56.0
ug/Kg
70
64 -140
40.0
33.5
ug/Kg
84
73 -121
40.0
43.7
ug/Kg
109
75 -124
40.0
40.1
ug/Kg
100
68 -120
40.0
40.9
ug/Kg
102
78 -118
40.0
40.9
ug/Kg
102
78 -118
40.0
39.1
ug/Kg
98
79 -119
40.0
43.8
ug/Kg
110
78 -118
Page 69 of 106
TestAmerica Pittsburgh
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 180-241049/3
Matrix: Sediment
Analysis Batch: 241049
TestAmerica Job ID: 180-76196-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
Toluene
40.0
41.8
ug/Kg
104
79 -121
trans- 1,2-Dichloroethene
40.0
43.3
ug/Kg
108
71-123
trans- 1,3-Dichloropropene
40.0
32.6
ug/Kg
82
62 -133
Trichloroethene
40.0
44.4
ug/Kg
111
76 -120
Trichlorofluoromethane
40.0
46.6
ug/Kg
116
25 -150
Xylenes, Total
80.0
81.8
ug/Kg
102
78 -118
Vinyl chloride
40.0
41.0
ug/Kg
103
53 -148
LCS LCS
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
84
62- 118
4-Bromofluorobenzene (Surr)
89
76-111
Dibromofluoromethane (Surr)
97
72 - 116
Toluene-d8 (Surr)
103
80 - 129
Lab Sample ID: LCSD 180-241049/4
Matrix: Sediment
Analysis Batch: 241049
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Analyte
Spike
Added
LCSD LCSD
Result Qualifier
Unit
D %Rec
%Rec.
Limits
RPD
RPD
Limit
1,1,1-Trichloroethane
40.0
43.4
ug/Kg
108
69-135
8
22
1,1,2,2-Tetrachloroethane
40.0
35.9
ug/Kg
90
71-125
15
25
1,1,2-Trichloro-1,2,2-trifluoroetha
40.0
48.1
ug/Kg
120
61-137
5
35
ne
1,1,2-Trichloroethane
40.0
39.4
ug/Kg
99
78-118
9
18
1,1-Dichloroethane
40.0
43.6
ug/Kg
109
67-129
5
15
1,1-Dichloroethene
40.0
45.2
ug/Kg
113
59-128
6
17
1,2,4-Trichlorobenzene
40.0
40.3
ug/Kg
101
65-135
11
20
1,2-Dibromo-3-Chloropropane
40.0
27.6
ug/Kg
69
54 -129
16
20
1,2-Dichlorobenzene
40.0
41.6
ug/Kg
104
78 -118
8
15
1,2-Dichloroethane
40.0
38.7
ug/Kg
97
67 -123
8
15
1,2-Dichloropropane
40.0
41.8
ug/Kg
104
80 -121
7
15
1,3-Dichlorobenzene
40.0
43.7
ug/Kg
109
78 -118
6
15
1,4-Dichlorobenzene
40.0
43.0
ug/Kg
107
78 -118
8
15
2-Butanone (MEK)
40.0
30.6
ug/Kg
76
30 -150
13
35
2-Hexanone
40.0
30.5
ug/Kg
76
36 -150
12
35
4-Methyl-2-pentanone (MIBK)
40.0
30.4
ug/Kg
76
62 -145
14
27
Acetone
40.0
38.5
ug/Kg
96
36 -150
15
35
Benzene
40.0
46.0
ug/Kg
115
78-118
7
15
Bromoform
40.0
31.5
ug/Kg
79
56 -150
10
16
Bromomethane
40.0
37.2
ug/Kg
93
34 -150
9
35
Carbon disulfide
40.0
42.0
ug/Kg
105
66 -128
9
27
Carbon tetrachloride
40.0
43.6
ug/Kg
109
60 -137
8
21
Chlorobenzene
40.0
44.2
ug/Kg
110
78 -118
6
15
Chlorodibromomethane
40.0
36.2
ug/Kg
90
58 -140
7
20
Chloroform
40.0
44.4
ug/Kg
111
68 -124
10
15
Chloromethane
40.0
38.9
ug/Kg
97
46 -150
3
35
Chloroethane
40.0
42.2
ug/Kg
105
37 -150
5
35
cis-1,2-Dichloroethene
40.0
45.4
ug/Kg
113
71 -120
5
15
TestAmerica Pittsburgh
Page 70 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Lab Sample ID: LCSD 180-241049/4
Client Sample ID: Lab Control Sample Dup
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241049
Spike
LCSD
LCSD
%Rec.
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
cis-1,3-Dichloropropene
40.0
40.0
ug/Kg
100
70 -131
8
21
Cyclohexane
40.0
45.5
ug/Kg
114
70 -133
9
28
Dichlorobromomethane
40.0
39.7
ug/Kg
99
66 -136
10
15
Dichlorodifluoromethane
40.0
53.6
ug/Kg
134
16 -150
7
35
Ethylbenzene
40.0
45.1
ug/Kg
113
78 -118
8
15
1,2-Dibromoethane
40.0
38.2
ug/Kg
96
78-118
11
15
Isopropylbenzene
40.0
43.6
ug/Kg
109
76 -123
7
19
Methyl acetate
80.0
63.5
ug/Kg
79
64 -140
13
24
Methyl tert-butyl ether
40.0
38.4
ug/Kg
96
73 -121
14
24
m
Methylcyclohexane
40.0
48.3
ug/Kg
121
75 -124
10
24
Methylene Chloride
40.0
42.5
ug/Kg
106
68 -120
6
19
m-Xylene & p-Xylene
40.0
43.3
ug/Kg
108
78 -118
6
16
o-Xylene
40.0
43.2
ug/Kg
108
78 -118
6
15
Styrene
40.0
41.6
ug/Kg
104
79 -119
6
15
Tetrachloroethene
40.0
46.0
ug/Kg
115
78 -118
5
20
Toluene
40.0
44.3
ug/Kg
111
79 -121
6
18
trans- 1,2-Dichloroethene
40.0
47.5
ug/Kg
119
71-123
9
15
trans- 1,3-Dichloropropene
40.0
35.3
ug/Kg
88
62 -133
8
21
Trichloroethene
40.0
45.2
ug/Kg
113
76 -120
2
15
Trichlorofluoromethane
40.0
49.2
ug/Kg
123
25 -150
5
35
Xylenes, Total
80.0
86.5
ug/Kg
108
78 -118
6
15
Vinyl chloride
40.0
43.5
ug/Kg
109
53 -148
6
35
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr) 92
62- 118
4-Bromofluorobenzene (Surr) 92
76 - 111
Dibromofluoromethane (Surr) 104
72 - 116
Toluene-d8 (Surr) 105
80 - 129
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
Lab Sample ID: MB 180-24103711-A Client Sample ID: Method Blank
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241401 Prep Batch: 241037
Analyte
MB MB
Result Qualifier
Acenaphthene
ND
Acenaphthylene
ND
Anthracene
ND
Benzo[a]anthracene
ND
Benzo[b]fluoranthene
ND
Benzo[a]pyrene
ND
Benzo[g,h,i]perylene
ND
Chrysene
ND
Dibenz(a,h)anth race ne
ND
Fluoranthene
ND
Fluorene
ND
Indeno[1,2,3-cd]pyrene
ND
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
3.4
0.96
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.73
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.87
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.63
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.82
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.73
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.72
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.66
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.75
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.88
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.66
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
3.4
0.68
ug/Kg
04/02/18 03:39
04/05/18 14:24
1
Page 71 of 106
TestAmerica Pittsburgh
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: 8270D LL - Semivolatile Organic
Compounds
by GC/MS
- Low Level (Continued)
Lab Sample ID: MB 180-241037/1-A
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241401
Prep Batch: 241037
MB
MB
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared Analyzed Dil Fac
Naphthalene
ND
3.4
0.65
ug/Kg
04/02/18 03:39 04/05/18 14:24 1
Phenanthrene
ND
3.4
0.90
ug/Kg
04/02/18 03:39 04/05/18 14:24 1
Pyrene
ND
3.4
0.79
ug/Kg
04/02/18 03:39 04/05/18 14:24 1
Benzo[k]fluoranthene
ND
3.4
1.0
ug/Kg
04/02/18 03:39 04/05/18 14:24 1
MB
MB
Surrogate %Recovery
Qualifier
Limits
Prepared Analyzed Dil Fac
2-Fluorobiphenyl
78
34 - 100
04102118 03:39 04105118 14:24 1 F-
Nitrobenzene-d5 (Surr)
90
33 - 100
04102118 03:39 04105118 14:24 1
Terphenyl-d14 (Surr)
87
30- 100
04/02/18 03:39 04/05/18 14:24 1
ED
Lab Sample ID: LCS 180-241037/2-A
Matrix: Sediment
Analysis Batch: 241401
Spike
LCS
LCS
Analyte
Added
Result
Qualifier
Acenaphthene
333
230
Acenaphthylene
333
251
Anthracene
333
246
Benzo[a]anthracene
333
254
Benzo[b]fluoranthene
333
250
Benzo[a]pyrene
333
275
Benzo[g,h,i]perylene
333
250
Chrysene
333
231
Dibenz(a,h)anthracene
333
258
Fluoranthene
333
257
Fluorene
333
237
Indeno[1,2,3-cd]pyrene
333
262
Naphthalene
333
213
Phenanthrene
333
237
Pyrene
333
233
Benzo[k]fluoranthene
333
255
LCS LCS
Surrogate
%Recovery Qualifier
Limits
2-Fluorobiphenyl
71
34 - 100
Nitrobenzene-d5 (Surr)
82
33 - 100
Terphenyl-d14 (Surr)
87
30- 100
Lab Sample ID: 180-76196-4 MS
Matrix: Sediment
Analysis Batch: 241401
Sample Sample
Spike
MS
MS
Analyte
Result Qualifier
Added
Result
Qualifier
Acenaphthene
ND
406
350
Acenaphthylene
ND
406
366
Anthracene
ND
406
346
Benzo[a]anthracene
ND
406
368
Benzo[b]fluoranthene
ND
406
355
Benzo[a]pyrene
ND
406
366
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 241037
%Rec.
Unit D %Rec Limits
ug/Kg
69
43-100
ug/Kg
75
43-100
ug/Kg
74
48-100
ug/Kg
76
46-100
ug/Kg
75
42-100
ug/Kg
82
46-100
ug/Kg
75
45-100
ug/Kg
69
47-100
ug/Kg
77
47-100
ug/Kg
77
47-100
ug/Kg
71
45-100
ug/Kg
79
46-100
ug/Kg
64
46-100
ug/Kg
71
46-100
ug/Kg
70
41-100
ug/Kg
76
45-100
Client Sample ID: AH-07-0318-C
Prep Type: Total/NA
Prep Batch: 241037
Unit
D
%Rec
%Rec.
Limits
ug/Kg
86
43-100
ug/Kg
90
43-100
ug/Kg
85
48-100
ug/Kg
91
46-100
ug/Kg
87
42-100
ug/Kg
90
46-100
TestAmerica Pittsburgh
Page 72 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: 8270D LL - Semivolatile Organic Compounds
by GC/MS
- Low
Level (Continued)
Lab Sample ID: 180-76196-4 MS
Client Sample ID: AH-07-0318-C
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241401
Prep Batch: 241037
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D
%Rec
Limits
Benzo[g,h,i]perylene
ND
406
347
ug/Kg
86
45-100
Chrysene
ND
406
335
ug/Kg
83
47 -100
Dibenz(a,h)anth race ne
ND
406
369
ug/Kg
91
47-100
Fluoranthene
ND
406
344
ug/Kg
#
85
47 -100
Fluorene
ND
406
357
ug/Kg
#
88
45 -100
Indeno[1,2,3-cd]pyrene
ND
406
389
ug/Kg
#
96
46-100
Naphthalene
ND
406
311
ug/Kg
76
46 -100
Phenanthrene
ND
406
338
ug/Kg
83
46 -100
Pyrene
ND
406
329
ug/Kg
81
41 -100
Benzo[k]fluoranthene
ND
406
363
ug/Kg
89
45 -100
MS MS
Surrogate
%Recovery Qualifier
Limits
2-Fluorobiphenyl
83
34 - 100
Nitrobenzene-d5 (Surr)
94
33 - 100
Terphenyl-d14 (Surr)
92
30- 100
Lab Sample ID: 180-76196-4 MSD
Client Sample ID: AH-07-0318-C
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241401
Prep Batch: 241037
Sample Sample
Spike
MSD MSD
%Rec.
RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D
%Rec
Limits
RPD
Limit
Acenaphthene
ND
410
331
ug/Kg
81
43 -100
5
27
Acenaphthylene
ND
410
355
ug/Kg
86
43 -100
3
27
Anthracene
ND
410
335
ug/Kg
82
48 -100
3
31
Benzo[a]anthracene
ND
410
337
ug/Kg
82
46 -100
9
31
Benzo[b]fluoranthene
ND
410
342
ug/Kg
83
42 -100
4
31
Benzo[a]pyrene
ND
410
367
ug/Kg
89
46-100
0
29
Benzo[g,h,i]perylene
ND
410
352
ug/Kg
86
45-100
1
38
Chrysene
ND
410
316
ug/Kg
77
47 -100
6
31
Dibenz(a,h)anthracene
ND
410
370
ug/Kg
90
47-100
0
35
Fluoranthene
ND
410
336
ug/Kg
82
47 -100
2
30
Fluorene
ND
410
340
ug/Kg
83
45 -100
5
29
Indeno[1,2,3-cd]pyrene
ND
410
378
ug/Kg
92
46-100
3
35
Naphthalene
ND
410
299
ug/Kg
3�
73
46 -100
4
19
Phenanthrene
ND
410
325
ug/Kg
3�
79
46 -100
4
32
Pyrene
ND
410
323
ug/Kg
3�
79
41 -100
2
34
Benzo[k]fluoranthene
ND
410
353
ug/Kg
86
45 -100
3
28
MSD MSD
Surrogate
%Recovery Qualifier
Limits
2-Fluorobiphenyl
84
34 - 100
Nitrobenzene-d5 (Surr)
97
33 - 100
Terphenyl-d14 (Surr)
100
30- 100
TestAmerica Pittsburgh
Page 73 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8270D LL - Semivolatile
Organic Compounds by
GC/MS - Low Level
Lab Sample ID: MB 180-241088/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 241375
Prep Batch: 241088
MB
MB
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Acenaphthene
ND
0.19
0.065
ug/L
04/02/1811:28
04/05/1814:33
1
Acenaphthylene
ND
0.19
0.065
ug/L
04/02/1811:28
04/05/1814:33
1
Anthracene
ND
0.19
0.049
ug/L
04/02/1811:28
04/05/1814:33
1
Benzo[a]anthracene
ND
0.19
0.075
ug/L
04/02/1811:28
04/05/1814:33
1
Benzo[b]fluoranthene
ND
0.19
0.097
ug/L
04/02/1811:28
04/05/1814:33
1
Benzo[a]pyrene
ND
0.19
0.053
ug/L
04/02/1811:28
04/05/1814:33
1
Benzo[g,h,i]perylene
ND
0.19
0.069
ug/L
04/02/1811:28
04/05/1814:33
1
Chrysene
ND
0.19
0.081
ug/L
04/02/1811:28
04/05/1814:33
1
Dibenz(a,h)anthracene
ND
0.19
0.072
ug/L
04/02/1811:28
04/05/1814:33
1 m
Fluoranthene
ND
0.19
0.060
ug/L
04/02/1811:28
04/05/1814:33
1
Fluorene
ND
0.19
0.069
ug/L
04/02/1811:28
04/05/1814:33
1
Indeno[1,2,3-cd]pyrene
ND
0.19
0.085
ug/L
04/02/1811:28
04/05/1814:33
1
Naphthalene
ND
0.19
0.059
ug/L
04/02/1811:28
04/05/1814:33
1
Phenanthrene
ND
0.19
0.055
ug/L
04/02/1811:28
04/05/1814:33
1
Pyrene
ND
0.19
0.054
ug/L
04/02/1811:28
04/05/1814:33
1
Benzo[k]fluoranthene
ND
0.19
0.088
ug/L
04/02/1811:28
04/05/1814:33
1
MB
MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
71
26- 103
04102118 11:28
04105118 14:33
1
Nitrobenzene-d5 (Surr)
73
30 - 101
04102118 11:28
04105118 14:33
1
Terphenyl-d14 (Surr)
79
20- 119
04102118 11:28
04105118 14:33
1
Lab Sample ID: LCS 180-241088/2-A
Matrix: Water
Analysis Batch: 241375
Analyte
Acenaphthene
Acenaphthylene
Anthracene
Benzo[a]anthracene
Benzo[b]fluoranthene
Benzo[a]pyrene
Benzo[g,h,i]perylene
Chrysene
Dibenz(a,h)anthracene
Fluoranthene
Fluorene
Indeno[1,2,3-cd]pyrene
Naphthalene
Phenanthrene
Pyrene
Benzo[k]fluoranthene
Surrogate
2-Fluorobiphenyl
Nitrobenzene-d5 (Surr)
LCS LCS
%Recovery Qualifier
60
70
Spike
Added
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
Limits
26-103
30-101
LCS LCS
Result Qualifier
11.4
12.1
11.4
12.0
12.2
12.4
12.1
11.6
11.8
13.3
12.0
12.5
11.9
11.4
12.8
12.1
Client Sample ID
Unit
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
D %Rec
57
60
57
60
61
62
60
58
59
67
60
62
60
57
64
60
Lab Control Sample
Prep Type: Total/NA
Prep Batch: 241088
%Rec.
Limits
49-100
46-100
50-100
50-100
47-100
50-100
48-100
49-100
49-100
51 -100
49-100
49-100
51 -100
50-100
47-100
47-100
Page 74 of 106
TestAmerica Pittsburgh
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
Lab Sample ID: LCS 180-241088/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 241375
Prep Batch: 241088
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
Terphenyl-d14 (Surr) 71
20- 119
Lab Sample ID: LCSD 180-241088/3-A
Client Sample ID: Lab
Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 241375
Prep Batch: 241088
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
Acenaphthene
20.0
11.9
ug/L
-
60
49 -100 4 15
Acenaphthylene
20.0
12.7
ug/L
63
46 -100 5 15 m
Anthracene
20.0
12.0
ug/L
60
50 -100 5 15
Benzo[a]anthracene
20.0
11.8
ug/L
59
50 -100 2 15
Benzo[b]fluoranthene
20.0
12.3
ug/L
62
47 -100 1 16
Benzo[a]pyrene
20.0
12.6
ug/L
63
50 -100 1 15
Benzo[g,h,i]perylene
20.0
12.0
ug/L
60
48-100 0 17
Chrysene
20.0
11.4
ug/L
57
49 -100 2 15
Dibenz(a,h)anthracene
20.0
12.3
ug/L
61
49-100 4 17
Fluoranthene
20.0
13.7
ug/L
68
51 -100 2 15
Fluorene
20.0
12.3
ug/L
62
49 -100 3 17
Indeno[1,2,3-cd]pyrene
20.0
12.6
ug/L
63
49-100 1 17
Naphthalene
20.0
12.2
ug/L
61
51 -100 2 15
Phenanthrene
20.0
12.0
ug/L
60
50 -100 5 15
Pyrene
20.0
12.5
ug/L
63
47 -100 3 18
Benzo[k]fluoranthene
20.0
12.3
ug/L
62
47 -100 2 16
LCSD
LCSD
Surrogate %Recovery
Qualifier
Limits
2-Fluorobiphenyl 62
26- 103
Nitrobenzene-d5 (Surr) 70
30 - 101
Terphenyl-d14 (Surr) 69
20- 119
Method: 8081 B_LL - Organochlorine
Pesticides
(GC)
Lab Sample ID: MB 180-241038/1-B
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 242257
Prep Batch: 241038
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Aldrin
ND
0.042
0.013
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
alpha-BHC
ND
0.042
0.010
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
beta-BHC
ND
0.042
0.011
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
cis -Chlordane
ND
0.042
0.010
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
Chlordane (technical)
ND
0.42
0.18
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
4,4'-DDD
ND
0.042
0.011
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
delta-BHC
ND
0.042
0.013
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
4,4'-DDE
ND
0.042
0.0085
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
4,4'-DDT
ND
0.042
0.016
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
Dieldrin
ND
0.042
0.010
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
Endosulfan I
ND
0.042
0.011
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
TestAmerica Pittsburgh
Page 75 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: 8081 B LL - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: MB 180-241038/1-B
Matrix: Sediment
Analysis Batch: 242257
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 241038
D Prepared Analyzed Dil Fac
Endosulfan II
ND
0.042
0.0092
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
Endosulfan sulfate
ND
0.042
0.011
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
Endrin
ND
0.042
0.016
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
Endrin aldehyde
ND
0.042
0.015
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
gamma-BHC (Lindane)
ND
0.042
0.014
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
Endrin ketone
ND
0.042
0.015
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
trans -Chlordane
ND
0.042
0.0097
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
Heptachlor
ND
0.042
0.013
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
Heptachlor epoxide
ND
0.042
0.011
ug/Kg
04/02/18 03:41
04/16/18 13:39 1 m
Methoxychlor
ND
0.042
0.016
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
oxy-Chlordane
ND
0.042
0.0093
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
Toxaphene
ND
1.7
1.1
ug/Kg
04/02/18 03:41
04/16/18 13:39 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
Tetrachloro-m-xylene
80
26 - 120
04102118 03:41
04116118 13:39 1
Tetrachloro-m-xylene
92
26 - 120
04102118 03:41
04116118 13:39 1
DCB Decachlorobiphenyl (Surr)
85
33 - 137
04102118 03:41
04116118 13:39 1
DCB Decachlorobiphenyl (Surr)
83
33 - 137
04102118 03:41
04116118 13:39 1
Lab Sample ID: LCS 180-241038/2-B
Client
Sample ID:
Lab Control Sample
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 242257
Prep Batch: 241038
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Aldrin
1.67
1.19
ug/Kg
71
37 -121
alpha-BHC
1.67
1.10
ug/Kg
66
39 -114
beta-BHC
1.67
1.24
ug/Kg
74
37 -113
cis -Chlordane
1.67
1.23
ug/Kg
74
35 -121
4,4'-DDD
1.67
1.46
ug/Kg
87
48 -119
delta-BHC
1.67
0.592
ug/Kg
36
12 -100
4,4'-DDE
1.67
1.34
ug/Kg
80
47 -118
4,4'-DDT
1.67
1.34
ug/Kg
81
29 -123
Dieldrin
1.67
1.31
ug/Kg
79
46 -119
Endosulfan 1
1.67
1.31
ug/Kg
78
36 -120
Endosulfan 11
1.67
1.25
ug/Kg
75
46 -114
Endosulfan sulfate
1.67
0.906
ug/Kg
54
40 -104
Endrin
1.67
1.28
ug/Kg
77
45 -118
Endrin aldehyde
1.67
1.28
ug/Kg
77
39 -109
gamma-BHC (Lindane)
1.67
1.11
ug/Kg
67
38 -115
Endrin ketone
1.67
1.32
ug/Kg
79
44 -114
trans -Chlordane
1.67
1.25
ug/Kg
75
36 -121
Heptachlor
1.67
1.26
ug/Kg
76
38 -122
Heptachlor epoxide
1.67
1.24
ug/Kg
74
36 -123
Methoxychlor
1.67
1.43
ug/Kg
86
34 -126
LCS LCS
Surrogate
%Recovery Qualifier
Limits
Tetrachloro-m-xylene
79
26 - 120
TestAmerica Pittsburgh
Page 76 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 8081 B_LL - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LCS 180-241038/2-B
Matrix: Sediment
Analysis Batch: 242257
LCS LCS
Surrogate %Recovery Qualifier
Limits
Tetrachloro-m-xylene
91
26 - 120
DCB Decachlorobiphenyl (Surr)
85
33 - 137
DCB Decachlorobiphenyl (Surr)
86
33 - 137
Lab Sample ID: 180-76196-8 MS
Matrix: Sediment
Analysis Batch: 242257
Analyte
Aldrin
alpha-BHC
beta-BHC
cis -Chlordane
4,4'-DDD
delta-BHC
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan 11
Endosulfan sulfate
Endrin
Endrin aldehyde
gamma-BHC (Lindane)
Endrin ketone
trans -Chlordane
Heptachlor
Heptachlor epoxide
Methoxychlor
Surrogate
Tetrachloro-m-xylene
Tetrachloro-m-xylene
DCB Decachlorobiphenyl (Surr)
LDCB Decachlorobiphenyl (Surr)
Sample Sample
Result Qualifier
ND F1
ND F1
ND F1
ND F1
ND F1
ND
0.016 J F1
ND
ND F1
ND F1
ND F1
ND F1
ND F1
0.018 J F1 p
ND F1
ND F1
ND F1
ND F1
ND F1
ND
MS MS
%Recovery Qualifier
Lab Sample ID: 180-76196-8 MSD
Matrix: Sediment
Analysis Batch: 242257
35
38
38
37
Spike
Added
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
2.04
Limits
26-120
26-120
33-137
33-137
MS MS
Result Qualifier
0.624 F1
0.572 F1
0.652 F1
0.659 F1
0.738 F1
0.352
0.687 F1
0.668
0.667 F1
0.684 F1
0.653 F1
0.550 F1
0.637 F1
0.743 F1
0.595 F1
0.673 F1
0.666 F1
0.666 F1
0.721 F1
0.693
Analyte
Sample
Result
Sample
Qualifier
Spike
Added
MSD
Result
MSD
Qualifier
Aldrin
ND
F1
2.04
0.771
alpha-BHC
ND
F1
2.04
0.701
F1
beta-BHC
ND
F1
2.04
0.810
cis -Chlordane
ND
F1
2.04
0.787
4,4'-DDD
ND
F1
2.04
0.915
F1
delta-BHC
ND
2.04
0.431
4,4'-DDE
0.016
J F1
2.04
0.839
F1
TestAmerica Job ID: 180-76196-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 241038
Unit
Client Sample ID: AH-06-0318-C
Prep Type: Total/NA
Prep Batch: 241038
%Rec.
D %Rec Limits
ug/Kg
31
37-121
ug/Kg
28
39-114
ug/Kg
32
37-113
ug/Kg
32
35-121
ug/Kg
36
48-119
ug/Kg
17
12-100
ug/Kg
33
47-118
ug/Kg
33
29-123
ug/Kg
33
46-119
ug/Kg
34
36-120
ug/Kg
32
46-114
ug/Kg
27
40-104
ug/Kg
31
45-118
ug/Kg
36
39-109
ug/Kg
29
38-115
ug/Kg
33
44-114
ug/Kg
33
36-121
ug/Kg
33
38-122
ug/Kg
35
36-123
ug/Kg
34
34-126
Client Sample ID: AH-06-0318-C
Prep Type: Total/NA
Prep Batch: 241038
%Rec.
RPD
Unit
D
%Rec
Limits
RPD
Limit
ug/Kg
#
38
37-121
21
33
ug/Kg
#
34
39-114
20
38
ug/Kg
#
40
37-113
22
37
ug/Kg
39
35-121
18
36
ug/Kg
45
48-119
21
32
ug/Kg
21
12-100
20
34
ug/Kg
#
40
47-118
20
31
Page 77 of 106
TestAmerica Pittsburgh
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 8081 B
LL - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: 180-76196-8 MSD
Matrix: Sediment
Analysis Batch: 242257
Sample
Sample
Spike
MSD
MSD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
4,4'-DDT
ND
2.04
0.805
ug/Kg
Dieldrin
ND
F1
2.04
0.804
F1
ug/Kg
Endosulfan I
ND
F1
2.04
0.846
ug/Kg
Endosulfan 11
ND
F1
2.04
0.791
F1
ug/Kg
Endosulfan sulfate
ND
F1
2.04
0.669
F1
ug/Kg
Endrin
ND
F1
2.04
0.775
F1
ug/Kg
Endrin aldehyde
0.018
J F1 p
2.04
0.888
ug/Kg
gamma-BHC (Lindane)
ND
F1
2.04
0.724
F1
ug/Kg
Endrin ketone
ND
F1
2.04
0.813
F1
ug/Kg
trans -Chlordane
ND
F1
2.04
0.799
ug/Kg
Heptachlor
ND
F1
2.04
0.817
ug/Kg
Heptachlor epoxide
ND
F1
2.04
0.862
ug/Kg
Methoxychlor
ND
2.04
0.829
ug/Kg
MSD MSD
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene 11 X 26 - 120
Tetrachloro-m-xylene 12 X 26 - 120
DCB Decachlorobiphenyl (Surr) 13 X 33- 137
DCB Decachlorobiphenyl (Surr) 12 X 33 - 137
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-06-0318-C
Prep Type: Total/NA
Prep Batch: 241038
%Rec. RPD
D %Rec Limits RPD Limit
39
29-123
19
38
39
46-119
19
32
41
36-120
21
39
39
46-114
19
29
33
40-104
19
34
38
45-118
20
31
43
39-109
18
37
35
38-115
20
38
40
44-114
19
34 m
39
36-121
18
35
40
38-122
20
38
42
36-123
18
35
41
34-126
18
35
Method: EPA 8081 B LL - Organochlorine Pesticides (GC)
Lab Sample ID: MB 180-240746/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 241080
Prep Batch: 240746
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Aldrin
ND
0.0013
0.00012
ug/L
03/28/18 10:45
04/02/18 14:25
1
alpha-BHC
ND
0.0013
0.00012
ug/L
03/28/18 10:45
04/02/18 14:25
1
beta-BHC
ND
0.0013
0.00015
ug/L
03/28/18 10:45
04/02/18 14:25
1
cis -Chlordane
ND
0.0013
0.00014
ug/L
03/28/18 10:45
04/02/18 14:25
1
Chlordane (technical)
ND
0.013
0.0015
ug/L
03/28/18 10:45
04/02/18 14:25
1
4,4'-DDD
ND
0.0013
0.00021
ug/L
03/28/18 10:45
04/02/18 14:25
1
delta-BHC
ND
0.0013
0.00034
ug/L
03/28/18 10:45
04/02/18 14:25
1
4,4'-DDE
ND
0.0013
0.00011
ug/L
03/28/18 10:45
04/02/18 14:25
1
4,4'-DDT
ND
0.0013
0.00030
ug/L
03/28/18 10:45
04/02/18 14:25
1
Dieldrin
ND
0.0013
0.00013
ug/L
03/28/18 10:45
04/02/18 14:25
1
Endosulfan I
ND
0.0013
0.00015
ug/L
03/28/18 10:45
04/02/18 14:25
1
Endosulfan II
ND
0.0013
0.00012
ug/L
03/28/18 10:45
04/02/18 14:25
1
Endosulfan sulfate
ND
0.0013
0.00029
ug/L
03/28/18 10:45
04/02/18 14:25
1
Endrin
ND
0.0013
0.00023
ug/L
03/28/18 10:45
04/02/18 14:25
1
Endrin aldehyde
ND
0.0013
0.00024
ug/L
03/28/18 10:45
04/02/18 14:25
1
gamma-BHC (Lindane)
ND
0.0013
0.00012
ug/L
03/28/18 10:45
04/02/18 14:25
1
Endrin ketone
ND
0.0013
0.00017
ug/L
03/28/18 10:45
04/02/18 14:25
1
trans -Chlordane
ND
0.0013
0.00012
ug/L
03/28/18 10:45
04/02/18 14:25
1
Heptachlor
ND
0.0013
0.00045
ug/L
03/28/18 10:45
04/02/18 14:25
1
Heptachlor epoxide
ND
0.0013
0.00014
ug/L
03/28/18 10:45
04/02/18 14:25
1
Methoxychlor
ND
0.0013
0.00034
ug/L
03/28/18 10:45
04/02/18 14:25
1
TestAmerica Pittsburgh
Page 78 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8081 B LL - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: MB 180-240746/1-A
Matrix: Water
Analysis Batch: 241080
Analyte
oxy-Chlordane
Toxaphene
MB MB
Result Qualifier RL MDL Unit
ND 0.017 0.00021 ug/L
ND 0.10 0.011 ug/L
MB MB
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene 79 41- 124
Tetrachloro-m-xylene 86 41- 124
DCB Decachlorobiphenyl (Surr) 86 64 - 126
DCB Decachlorobiphenyl (Surr) 92 64 - 126
Lab Sample ID: LCS 180-240746/2-A
Matrix: Water
Analysis Batch: 241080
Analyte
Aldrin
alpha-BHC
beta-BHC
cis -Chlordane
4,4'-DDD
delta-BHC
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan 11
Endosulfan sulfate
Endrin
Endrin aldehyde
gamma-BHC (Lindane)
Endrin ketone
trans -Chlordane
Heptachlor
Heptachlor epoxide
Methoxychlor
Surrogate
Tetrachloro-m-xylene
Tetrachloro-m-xylene
DCB Decachlorobiphenyl (Surr)
DCB Decachlorobiphenyl (Surr)
LCS LCS
%Recovery Qualifier
82
90
81
85
Lab Sample ID: LCSD 180-240746/3-A
Matrix: Water
Analysis Batch: 241080
Spike
Added
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
0.0250
Limits
41-124
41-124
64 - 126
64-126
Spike
Analyte Added
Aldrin 0.0250
alpha-BHC 0.0250
LCS LCS
Result Qualifier
0.0206
0.0182
0.0195
0.0214
0.0214
0.00864
0.0208
0.0200
0.0198
0.0220
0.0200
0.0153
0.0190
0.0220
0.0190
0.0199
0.0205
0.0216
0.0215
0.0206
TestAmerica Job ID: 180-76196-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 240746
D Prepared
Analyzed Dil Fac
03/28/1810:45
04/02/1814:25 1
03/28/1810:45
04/02/1814:25 1
Prepared
Analyzed Dil Fac
0312811810:45
0410211814:25 1
0312811810:45
0410211814:25 1
0312811810:45
0410211814:25 1
0312811810:45
0410211814:25 1
Client
Sample ID:
Lab Control Sample
Prep Type: Total/NA
Prep Batch: 240746
%Rec.
Unit
D %Rec
Limits
ug/L
83
50-120
ug/L
73
52-110
ug/L
78
50-112
ug/L
86
49-118
ug/L
86
64 -109
ug/L
35
10-100
ug/L
83
59-116
ug/L
80
43-114
ug/L
79
61-113
ug/L
88
49-119
ug/L
80
61 -109
ug/L
61
48-100
ug/L
76
61-115
ug/L
88
50-111
ug/L
76
51-112
ug/L
80
51-117
ug/L
82
49-119
ug/L
86
55-118
ug/L
86
50-123
ug/L
82
49-119
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 240746
LCSD LCSD %Rec. RPD
Result Qualifier Unit D %Rec Limits RPD Limit
0.0223 ug/L 89 50-120 8 22
0.0191 ug/L 76 52-110 5 20
TestAmerica Pittsburgh
Page 79 of 106
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 8081 B LL - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LCSD 180-240746/3-A Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241080 Prep Batch: 240746
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
beta-BHC
0.0250
0.0200
ug/L
80
50 -112
2
20
cis -Chlordane
0.0250
0.0219
ug/L
87
49 -118
2
24
4,4'-DDD
0.0250
0.0236
ug/L
94
64 -109
10
19
delta-BHC
0.0250
0.00908
ug/L
36
10 -100
5
21
4,4'-DDE
0.0250
0.0224
ug/L
90
59 -116
7
20
4,4'-DDT
0.0250
0.0213
ug/L
85
43 -114
6
22
Dieldrin
0.0250
0.0212
ug/L
85
61 -113
7
20
Endosulfan 1
0.0250
0.0224
ug/L
90
49 -119
2
22
Endosulfan 11
0.0250
0.0216
ug/L
86
61 -109
8
19
Endosulfan sulfate
0.0250
0.0165
ug/L
66
48 -100
8
21
Endrin
0.0250
0.0207
ug/L
83
61 -115
9
20
Endrin aldehyde
0.0250
0.0243
ug/L
97
50 -111
10
21
gamma-BHC (Lindane)
0.0250
0.0203
ug/L
81
51 -112
7
20
Endrin ketone
0.0250
0.0218
ug/L
87
51 -117
9
28
trans -Chlordane
0.0250
0.0216
ug/L
87
49 -119
5
25
Heptachlor
0.0250
0.0222
ug/L
89
55 -118
3
21
Heptachlor epoxide
0.0250
0.0224
ug/L
89
50 -123
4
22
Methoxychlor
0.0250
0.0218
ug/L
87
49 -119
6
22
LCSD LCSD
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene 88 41- 124
Tetrachloro-m-xylene 96 41- 124
DCB Decachlorobiphenyl (Surr) 90 64 - 126
DCB Decachlorobiphenyl (Surr) 87 64 - 126
Method: 6020B - Metals (ICP/MS)
Lab Sample ID: MB 180-241695/1-A
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241911
Prep Batch: 241695
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Antimony
ND
0.10
0.031
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Arsenic
ND
0.050
0.013
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Beryllium
ND
0.050
0.0038
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Cadmium
ND
0.050
0.0085
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Chromium
ND
0.10
0.033
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Copper
ND
0.10
0.057
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Lead
ND
0.050
0.018
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Manganese
ND
0.25
0.080
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Nickel
ND
0.050
0.031
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Selenium
ND
0.25
0.030
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Silver
ND
0.050
0.0070
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Thallium
ND
0.050
0.0065
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
Zinc
ND
0.25
0.17
mg/Kg
04/09/18 16:04
04/11/18 00:56 1
TestAmerica Pittsburgh
Page 80 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Method: 6020B - Metals (ICP/MS) (Continued)
Lab Sample ID: LCS 180-241695/2-A
Client Sample ID:
Lab Control Sample
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241911
Prep Batch: 241695
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Antimony
25.0
22.6
mg/Kg
90
80 -120
Arsenic
2.00
1.79
mg/Kg
90
80 -120
Beryllium
2.50
2.38
mg/Kg
95
80 -120
Cadmium
2.50
2.48
mg/Kg
99
80 -120
Chromium
10.0
11.1
mg/Kg
111
80 -120
Copper
12.5
11.7
mg/Kg
94
80 -120
Lead
1.00
1.01
mg/Kg
101
80 -120
Manganese
25.0
23.6
mg/Kg
94
80 -120
Nickel
25.0
23.1
mg/Kg
92
80 -120 m
Selenium
0.500
0.432
mg/Kg
86
80 -120
Silver
2.50
2.57
mg/Kg
103
80 -120
Thallium
2.50
2.52
mg/Kg
101
80-120
Zinc
25.0
22.3
mg/Kg
89
80 -120
Lab Sample ID: LCSSRM 180-241695/19-A
Client Sample ID:
Lab Control Sample
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241911
Prep Batch: 241695
Spike
LCSSRM
LCSSRM
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Antimony
0.300
0.142
J
mg/Kg
47
Arsenic
6.23
4.94
mg/Kg
79
Beryllium
1.00
0.323
mg/Kg
32
Cadmium
0.148
0.140
mg/Kg
94
Chromium
40.9
18.6
mg/Kg
45
Copper
10.0
8.82
mg/Kg
88
Lead
11.7
7.74
mg/Kg
66
Manganese
235
99.0
mg/Kg
42
Nickel
23.0
17.0
mg/Kg
74
Selenium
0.193
0.455
J
mg/Kg
236
Silver
0.300
0.0348
J
mg/Kg
12
Thallium
0.500
0.0838
J
mg/Kg
17
Zinc
48.9
29.6
mg/Kg
60
Method: 7471 B - Mercury (CVAA)
Lab Sample ID: MB 180-241273/1-A
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241400
Prep Batch: 241273
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
Mercury ND
0.017 0.0037 mg/Kg
04/04/18 08:35
04/05/18 08:59 1
Lab Sample ID: LCS 180-241273/2-A
Client Sample ID:
Lab Control Sample
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241400
Prep Batch: 241273
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Mercury
0.208
0.225
mg/Kg
108
80 -120
TestAmerica Pittsburgh
Page 81 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 7471 B - Mercury (CVAA) (Continued)
Lab Sample ID: LCSSRM 180-241273/3-A
Matrix: Sediment
Analysis Batch: 241400
Analyte
Mercury
Method: EPA 6020B - Metals (ICP/MS)
Lab Sample ID: MB 180-240953/1-A
Matrix: Water
Analysis Batch: 241140
MB MB
Analyte
Result Qualifier
Antimony
ND
Arsenic
ND
Beryllium
ND
Cadmium
ND
Chromium
ND
Copper
ND
Lead
ND
Manganese
ND
Nickel
ND
Selenium
ND
Silver
ND
Thallium
ND
Zinc
ND
Lab Sample ID: LCS 180-240953/2-A
Matrix: Water
Analysis Batch: 241140
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
TestAmerica Job ID: 180-76196-1
Client Sample ID
Spike LCSSRM LCSSRM
Added Result Qualifier Unit D %Rec
0.0400 0.0457 mg/Kg 114
Lab Control Sample
Prep Type: Total/NA
Prep Batch: 241273
%Rec.
Limits
Client Sample ID: Method Blank
Prep Type: Total Recoverable
Prep Batch: 240953
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
2.0
1.1
ug/L
03/30/1813:04
03/31/1811:51
1
1.0
0.32
ug/L
03/30/1813:04
03/31/1811:51
1
1.0
0.057
ug/L
03/30/1813:04
03/31/1811:51
1
1.0
0.13
ug/L
03/30/1813:04
03/31/1811:51
1
2.0
0.63
ug/L
03/30/1813:04
03/31/1811:51
1
2.0
1.3
ug/L
03/30/1813:04
03/31/1811:51
1
1.0
0.094
ug/L
03/30/1813:04
03/31/1811:51
1
5.0
1.4
ug/L
03/30/1813:04
03/31/1811:51
1
1.0
0.31
ug/L
03/30/1813:04
03/31/1811:51
1
5.0
0.81
ug/L
03/30/1813:04
03/31/1811:51
1
1.0
0.12
ug/L
03/30/1813:04
03/31/1811:51
1
1.0
0.063
ug/L
03/30/1813:04
03/31/1811:51
1
5.0
2.4
ug/L
03/30/1813:04
03/31/1811:51
1
Client Sample ID: Lab Control Sample
Prep Type: Total Recoverable
Prep Batch: 240953
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
500
535
ug/L
107
80-120
40.0
47.0
ug/L
118
80 -120
50.0
51.6
ug/L
103
80 -120
50.0
53.2
ug/L
106
80 -120
200
226
ug/L
113
80-120
250
235
ug/L
94
80-120
20.0
20.5
ug/L
103
80 -120
500
546
ug/L
109
80-120
500
448
ug/L
90
80-120
10.0
10.6
ug/L
106
80 -120
50.0
50.5
ug/L
101
80 -120
50.0
47.4
ug/L
95
80 -120
500
438
ug/L
88
80-120
TestAmerica Pittsburgh
Page 82 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 7470A - Mercury (CVAA)
Lab Sample ID: MB 180-241732/1-A
Matrix: Water
Analysis Batch: 241904
MB MB
Analyte Result Qualifier
Mercury ND
Lab Sample ID: LCS 180-241732/2-A
Matrix: Water
Analysis Batch: 241904
Analyte
Mercury
Method: 1664B - HEM and SGT-HEM
Lab Sample ID: MB 400-392275/1-A
Matrix: Water
Analysis Batch: 392295
MB MB
Analyte Result Qualifier
Total Petroleum Hydrocarbons ND
(SGT-HEM)
Lab Sample ID: LCS 400-392275/2-A
Matrix: Water
Analysis Batch: 392295
Analyte
Total Petroleum Hydrocarbons
(SGT-HEM)
Method: 2540G - SM 254OG
Lab Sample ID: 180-76196-16 DU
Matrix: Sediment
Analysis Batch: 240793
TestAmerica Job ID: 180-76196-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 241732
RL MDL Unit D Prepared Analyzed Dil Fac
0.20 0.065 ug/L 04/10/1811:20 04/11/1810:49 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 241732
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
2.50 2.76 ug/L 110 80 -120
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 392275
RL MDL Unit D Prepared Analyzed Dil Fac C
4.0 1.4 mg/L 04/01/18 14:43 04/02/18 09:06 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 392275
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
20.0 15.80 mg/L 79 64 -132
Client Sample ID: AH-04-0318-C
Prep Type: Total/NA
Sample
Sample
DU
DU
RPD
Analyte
Result
Qualifier
Result
Qualifier
Unit
D RPD Limit
Percent Moisture
58.8
58.0
%
1 20
Percent Solids
41.2
42.0
%
2 20
Lab Sample ID: 180-76196-22 DU
Client Sample ID: AH-05-0318-C-DUP
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 240793
Sample
Sample
DU
DU
RPD
Analyte
Result
Qualifier
Result
Qualifier
Unit
D RPD Limit
Percent Moisture
76.1
75.9
%
0.4 20
Percent Solids
23.9
24.1
%
1 20
Page 83 of 106
TestAmerica Pittsburgh
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 2540G - SM 2540G (Continued)
Lab Sample ID: 180-76196-4 DU
Matrix: Sediment
Analysis Batch: 240823
Sample Sample
Analyte Result Qualifier
Percent Moisture 19.0
Percent Solids 81.0
Lab Sample ID: 180-76196-12 DU
Matrix: Sediment
Analysis Batch: 240823
Analyte
Percent Moisture
Percent Solids
Sample Sample
Result Qualifier
42.8
57.2
Method: EPA 7196A - Chromium, Hexavalent
Lab Sample ID: MB 180-240705/10
Matrix: Water
Analysis Batch: 240705
MB MB
Analyte Result Qualifier
Cr (VI) ND
Lab Sample ID: LCS 180-240705/11
Matrix: Water
Analysis Batch: 240705
Analyte
LCr (VI)
Lab Sample ID: MB 180-240858/1-A
Matrix: Sediment
Analysis Batch: 240949
MB MB
Analyte Result Qualifier
Cr (VI) ND
Lab Sample ID: LCSI 180-240858/3-A
Matrix: Sediment
Analysis Batch: 240949
Analyte
Cr (VI)
Lab Sample ID: LCSS 180-240858/2-A
Matrix: Sediment
Analysis Batch: 240949
Analyte
Cr (VI)
DU DU
Result Qualifier Unit
19.5 %
80.5 %
TestAmerica Job ID: 180-76196-1
Client Sample ID: AH-07-0318-C
Prep Type: Total/NA
RPD
D RPD Limit
2 20
0.6 20
Client Sample ID: AH-02-0318-C
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
42.2 % 1 20 m
57.8 % 0.9 20
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
0.010 0.0032 mg/L 03/28/1812:00 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS
Added Result Qualifier Unit
0.250 0.228 m-g L
RL MDL Unit
0.40 0.11 mg/Kg
%Rec.
D %Rec Limits
91 85-115
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 240858
D Prepared Analyzed Dil Fac
03/29/1814:32 03/30/1813:08 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 240858
Spike LCSI LCSI %Rec.
Added Result Qualifier Unit D %Rec Limits
708 605 mg/Kg 85 80-120
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 240858
Spike LCSS LCSS %Rec.
Added Result Qualifier Unit D %Rec Limits
20.0 18.8 mg/Kg 94 80 -120
TestAmerica Pittsburgh
Page 84 of 106 4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
Method: EPA 7196A - Chromium, Hexavalent (Continued)
Lab Sample ID: 180-76196-16 MSI
Client Sample ID: AH-04-0318-C
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 240949
Prep Batch: 240858
Sample
Sample
Spike
MSI
MSI
%Rec.
Analyte Result
Qualifier
Added
Result
Qualifier Unit
D %Rec Limits
Cr (VI) ND
1680
1310
mg/Kg
78 75-125
Lab Sample ID: 180-76196-16 MSS
Client Sample ID: AH-04-0318-C
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 240949
Prep Batch: 240858
Sample
Sample
Spike
MSS
MSS
%Rec.
Analyte Result
Qualifier
Added
Result
Qualifier Unit
D %Rec Limits
Cr (VI) ND
47.6
39.4
mg/Kg
—
# 83 75 -125
Lab Sample ID: 180-76196-16 DU
Client Sample ID: AH-04-0318-C m
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 240949
Prep Batch: 240858
Sample
Sample
DU
DU
RPD
Analyte Result
Qualifier
Result
Qualifier Unit
D RPD Limit
Cr (VI) ND
ND
mg/Kg
NC 20
Method: EPA 9071 B - HEM and SGT-HEM
Lab Sample ID: MB 180-241004/1-A
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 241091
Prep Batch: 241004
MB MB
Analyte Result Qualifier
Total Petroleum Hydrocarbons ND
(SGT-HEM)
Lab Sample ID: LCS 180-241004/2-A
Matrix: Sediment
Analysis Batch: 241091
Analyte
Total Petroleum Hydrocarbons
(SGT-HEM)
Lab Sample ID: LCSD 180-241004/3-A
Matrix: Sediment
Analysis Batch: 241091
Analyte
Total Petroleum Hydrocarbons
(SGT-HEM)
RL MDL Unit D Prepared Analyzed Dil Fac
170 83 mg/Kg 03/31/18 06:25 04/03/18 08:15 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 241004
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
667 480 mg/Kg 72 64-132
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 241004
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
667 480 mg/Kg 72 64 -132 0 34
Page 85 of 106
TestAmerica Pittsburgh
4/18/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: Lloyd Kahn - Organic Carbon, Total (TOC)
Lab Sample ID: MB 180-240909/3
Matrix: Sediment
Analysis Batch: 240909
MB MB
TestAmerica Job ID: 180-76196-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Total Organic Carbon - Duplicates ND 1000 750 mg/Kg 03/29/18 13:34 1
Lab Sample ID: LCS 180-240909/4
Matrix: Sediment
Analysis Batch: 240909
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec. —
Analyte Added Result Qualifier Unit D %Rec Limits
Total Organic Carbon - 37800 31400 mg/Kg 83 75 -125
Duplicates
Lab Sample ID: MB 180-241158/3
Matrix: Sediment
Analysis Batch: 241158
MB MB
Analyte Result Qualifier RL
Total Organic Carbon - Duplicates ND 1000
FLab Sample ID: LCS 180-241158/4
Matrix: Sediment
Analysis Batch: 241158
Spike
Analyte Added
Total Organic Carbon - 34500
Duplicates
Method: SM 5310C - Total Organic Carbon
Lab Sample ID: MB 180-241245/6
Matrix: Water
Analysis Batch: 241245
MB MB
Analyte Result Qualifier
Total Organic Carbon - Duplicates ND
Lab Sample ID: LCS 180-241245/4
Matrix: Water
Analysis Batch: 241245
Analyte
Total Organic Carbon -
Duplicates
Lab Sample ID: LCSD 180-241245/5
Matrix: Water
Analysis Batch: 241245
Analyte
Total Organic Carbon -
Duplicates
ED
Client Sample ID: Method Blank
Prep Type: Total/NA
MDL Unit D Prepared Analyzed Dil Fac
750 mg/Kg 04/02/1813:37 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS %Rec.
Result Qualifier Unit D %Rec Limits
34500 mg/Kg 100 75 -125
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
1.0 0.51 mg/L 04/03/1815:58 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Added
Result
Qualifier Unit
D %Rec
Limits
20.0
19.1
mg/L
96
85 -115
Client Sample
ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD
LCSD
%Rec. RPD
Added
Result
Qualifier Unit
D %Rec
Limits RPD Limit
20.0
19.1
mg/L
96
85-115 0 20
TestAmerica Pittsburgh
Page 86 of 106 4/18/2018

QC Association Summary
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
GC/MS VOA
Analysis Batch: 240660
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-13
AH-04-0318-G1
Total/NA
Sediment
EPA 8260E
240706
180-76196-14
AH-04-0318-G2
Total/NA
Sediment
EPA 8260E
240706
180-76196-15
AH-04-0318-G3
Total/NA
Sediment
EPA 8260E
240706
180-76196-17
AH-05-0318-G1
Total/NA
Sediment
EPA 8260E
240706
180-76196-18
AH-05-0318-GI-DUP
Total/NA
Sediment
EPA 8260E
240706
180-76196-19
AH-05-0318-G2
Total/NA
Sediment
EPA 8260E
240706
180-76196-20
AH-05-0318-G3
Total/NA
Sediment
EPA 8260B
240706
MB 180-240660/9
Method Blank
Total/NA
Sediment
EPA 8260B
F-
LCS 180-240660/3
Lab Control Sample
Total/NA
Sediment
EPA 8260B
F
Prep Batch: 240706
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-13
AH-04-0318-G1
Total/NA
Sediment
5035
180-76196-14
AH-04-0318-G2
Total/NA
Sediment
5035
m
180-76196-15
AH-04-0318-G3
Total/NA
Sediment
5035
180-76196-17
AH-05-0318-G1
Total/NA
Sediment
5035
180-76196-18
AH-05-0318-G1-DUP
Total/NA
Sediment
5035
180-76196-19
AH-05-0318-G2
Total/NA
Sediment
5035
180-76196-20
AH-05-0318-G3
Total/NA
Sediment
5035
Analysis Batch: 240736
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-23
TB-02-0318
Total/NA
Water
EPA 8260B
MB 180-240736/5
Method Blank
Total/NA
Water
EPA 8260B
LCS 180-240736/3
Lab Control Sample
Total/NA
Water
EPA 8260B
Analysis Batch: 240865
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-76196-24
EB-02-0318
Total/NA
Water
EPA 8260E
MB 180-240865/6
Method Blank
Total/NA
Water
EPA 8260E
LCS 180-240865/4
Lab Control Sample
Total/NA
Water
EPA 8260E
Analysis Batch: 240896
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-1
AH-07-0318-G1
Total/NA
Sediment
EPA 8260B
240903
180-76196-2
AH-07-0318-G2
Total/NA
Sediment
EPA 8260B
240903
180-76196-5
AH-06-0318-G1
Total/NA
Sediment
EPA 8260B
240903
180-76196-6
AH-06-0318-G2
Total/NA
Sediment
EPA 8260E
240903
180-76196-7
AH-06-0318-G3
Total/NA
Sediment
EPA 8260E
240903
180-76196-9
AH-02-0318-G1
Total/NA
Sediment
EPA 8260E
240903
180-76196-10
AH-02-0318-G2
Total/NA
Sediment
EPA 8260E
240903
MB 180-240896/7
Method Blank
Total/NA
Sediment
EPA 8260E
LCS 180-240896/3
Lab Control Sample
Total/NA
Sediment
EPA 8260E
Prep Batch: 240903
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-1
AH-07-0318-G1
Total/NA
Sediment
5035
180-76196-2
AH-07-0318-G2
Total/NA
Sediment
5035
180-76196-3
AH-07-0318-G3
Total/NA
Sediment
5035
180-76196-5
AH-06-0318-G1
Total/NA
Sediment
5035
180-76196-6
AH-06-0318-G2
Total/NA
Sediment
5035
TestAmerica Pittsburgh
Page 87 of 106 4/18/2018

QC Association Summary
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
GC/MS VOA (Continued)
Prep Batch: 240903 (Continued)
Lab Sample ID
Client Sample ID
180-76196-7
AH-06-0318-G3
180-76196-9
AH-02-0318-G1
180-76196-10
AH-02-0318-G2
180-76196-11
AH-02-0318-G3
Analysis Batch: 241049
Lab Sample ID
180-76196-3
180-76196-11
MB 180-241049/6
LCS 180-241049/3
LCSD 180-241049/4
GC/MS Semi VOA
Prep Batch: 241037
TestAmerica Job ID: 180-76196-1
Prep Type
Matrix
Method Prep Batch
Total/NA
Sediment
5035
Total/NA
Sediment
5035
Total/NA
Sediment
5035
Total/NA
Sediment
5035
Client Sample ID
Prep Type
Matrix
Method Prep Batch
AH-07-0318-G3
Total/NA
Sediment
EPA 8260B 240903
AH-02-0318-G3
Total/NA
Sediment
EPA 8260B 240903
Method Blank
Total/NA
Sediment
EPA 8260B
Lab Control Sample
Total/NA
Sediment
EPA 8260B
Lab Control Sample Dup
Total/NA
Sediment
EPA 8260B
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
180-76196-4
AH-07-0318-C
Total/NA
Sediment
3541
180-76196-8
AH-06-0318-C
Total/NA
Sediment
3541
180-76196-12
AH-02-0318-C
Total/NA
Sediment
3541
180-76196-16
AH-04-0318-C
Total/NA
Sediment
3541
180-76196-21
AH-05-0318-C
Total/NA
Sediment
3541
180-76196-22
AH-05-0318-C-DUP
Total/NA
Sediment
3541
MB 180-241037/1-A
Method Blank
Total/NA
Sediment
3541
LCS 180-241037/2-A
Lab Control Sample
Total/NA
Sediment
3541
180-76196-4 MS
AH-07-0318-C
Total/NA
Sediment
3541
180-76196-4 MSD
AH-07-0318-C
Total/NA
Sediment
3541
Prep Batch: 241088
Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-76196-24
EB-02-0318
Total/NA
Water
3520C
MB 180-241088/1-A
Method Blank
Total/NA
Water
3520C
LCS 180-241088/2-A
Lab Control Sample
Total/NA
Water
3520C
LCSD 180-241088/3-A
Lab Control Sample Dup
Total/NA
Water
3520C
Analysis Batch: 241375
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-24
EB-02-0318
Total/NA
Water
EPA 8270D LL
241088
MB 180-241088/1-A
Method Blank
Total/NA
Water
EPA 8270D LL
241088
LCS 180-241088/2-A
Lab Control Sample
Total/NA
Water
EPA 8270D LL
241088
LCSD 180-241088/3-A
Lab Control Sample Dup
Total/NA
Water
EPA 8270D LL
241088
Analysis Batch: 241401
Lab Sample ID
Client Sample ID
180-76196-4
AH-07-0318-C
180-76196-8
AH-06-0318-C
180-76196-12
AH-02-0318-C
180-76196-16
AH-04-0318-C
180-76196-21
AH-05-0318-C
180-76196-22
AH-05-0318-C-DUP
Prep Type
Matrix
Method
Prep Batch
Total/NA
Sediment
8270D LL
241037
Total/NA
Sediment
8270D LL
241037
Total/NA
Sediment
8270D LL
241037
Total/NA
Sediment
8270D LL
241037
Total/NA
Sediment
8270D LL
241037
Total/NA
Sediment
8270D LL
241037
Page 88 of 106
TestAmerica Pittsburgh
4/18/2018

QC Association Summary
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
GC/MS Semi VOA (Continued)
Analysis Batch: 241401 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
MB 180-241037/1-A Method Blank
Total/NA
Sediment
8270D LL
241037
LCS 180-241037/2-A Lab Control Sample
Total/NA
Sediment
8270D LL
241037
180-76196-4 MS AH-07-0318-C
Total/NA
Sediment
8270D LL
241037
180-76196-4 MSD AH-07-0318-C
Total/NA
Sediment
8270D LL
241037
GC Semi VOA
Prep Batch: 240746
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-24
EB-02-0318
Total/NA
Water
3510C
MB 180-240746/1-A
Method Blank
Total/NA
Water
3510C
LCS 180-240746/2-A
Lab Control Sample
Total/NA
Water
3510C
LCSD 180-240746/3-A
Lab Control Sample Dup
Total/NA
Water
3510C
Prep Batch: 241038
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-4
AH-07-0318-C
Total/NA
Sediment
3541
180-76196-8
AH-06-0318-C
Total/NA
Sediment
3541
180-76196-12
AH-02-0318-C
Total/NA
Sediment
3541
180-76196-16
AH-04-0318-C
Total/NA
Sediment
3541
180-76196-21
AH-05-0318-C
Total/NA
Sediment
3541
180-76196-22
AH-05-0318-C-DUP
Total/NA
Sediment
3541
MB 180-241038/1-B
Method Blank
Total/NA
Sediment
3541
LCS 180-241038/2-B
Lab Control Sample
Total/NA
Sediment
3541
180-76196-8 MS
AH-06-0318-C
Total/NA
Sediment
3541
180-76196-8 MSD
AH-06-0318-C
Total/NA
Sediment
3541
Analysis Batch: 241080
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-24
EB-02-0318
Total/NA
Water
EPA 8081 B LL
240746
MB 180-240746/1-A
Method Blank
Total/NA
Water
EPA 8081B LL
240746
LCS 180-240746/2-A
Lab Control Sample
Total/NA
Water
EPA 8081 B LL
240746
LCSD 180-240746/3-A
Lab Control Sample Dup
Total/NA
Water
EPA 8081 B LL
240746
Cleanup Batch: 241931
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-4
AH-07-0318-C
Total/NA
Sediment
3640A
241038
180-76196-8
AH-06-0318-C
Total/NA
Sediment
3640A
241038
180-76196-12
AH-02-0318-C
Total/NA
Sediment
3640A
241038
180-76196-16
AH-04-0318-C
Total/NA
Sediment
3640A
241038
180-76196-21
AH-05-0318-C
Total/NA
Sediment
3640A
241038
180-76196-22
AH-05-0318-C-DUP
Total/NA
Sediment
3640A
241038
MB 180-241038/1-B
Method Blank
Total/NA
Sediment
3640A
241038
LCS 180-241038/2-B
Lab Control Sample
Total/NA
Sediment
3640A
241038
180-76196-8 MS
AH-06-0318-C
Total/NA
Sediment
3640A
241038
180-76196-8 MSD
AH-06-0318-C
Total/NA
Sediment
3640A
241038
Analysis Batch: 242257
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-4
AH-07-0318-C
Total/NA
Sediment
8081 B LL
241931
TestAmerica Pittsburgh
Page 89 of 106 4/18/2018

QC Association Summary
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
GC Semi VOA (Continued)
Analysis Batch: 242257 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-8 AH-06-0318-C
Total/NA
Sediment
8081 B_LL
241931
180-76196-12 AH-02-0318-C
Total/NA
Sediment
8081 B LL
241931
180-76196-16 AH-04-0318-C
Total/NA
Sediment
8081 B LL
241931
180-76196-21 AH-05-0318-C
Total/NA
Sediment
8081 B LL
241931
180-76196-22 AH-05-0318-C-DUP
Total/NA
Sediment
8081 BLL
241931
MB 180-241038/1-B Method Blank
Total/NA
Sediment
8081B_LL
241931
LCS 180-241038/2-B Lab Control Sample
Total/NA
Sediment
8081 B—LL
241931
180-76196-8 MS AH-06-0318-C
Total/NA
Sediment
8081 B LL
241931 F-
L180-76196-8 MSD AH-06-0318-C
Total/NA
Sediment
8081 B_LL
241931 F-
Metals
Prep Batch: 240953
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch m
180-76196-24 EB-02-0318
Total Recoverable
Water
3005A
MB 180-240953/1-A Method Blank
Total Recoverable
Water
3005A
LCS 180-240953/2-A Lab Control Sample
Total Recoverable
Water
3005A
Analysis Batch: 241140
E:
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-24 EB-02-0318
Total Recoverable
Water
EPA 6020E
240953
MB 180-240953/1-A Method Blank
Total Recoverable
Water
EPA 6020E
240953
LCS 180-240953/2-A Lab Control Sample
Total Recoverable
Water
EPA 6020E
240953
Prep Batch: 241273
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-76196-4
AH-07-0318-C
Total/NA
Sediment
7471 B
180-76196-8
AH-06-0318-C
Total/NA
Sediment
7471 B
180-76196-12
AH-02-0318-C
Total/NA
Sediment
7471 B
180-76196-16
AH-04-0318-C
Total/NA
Sediment
7471 B
180-76196-21
AH-05-0318-C
Total/NA
Sediment
7471 B
180-76196-22
AH-05-0318-C-DUP
Total/NA
Sediment
7471B
MB 180-241273/1-A
Method Blank
Total/NA
Sediment
7471B
LCS 180-241273/2-A
Lab Control Sample
Total/NA
Sediment
7471 B
LCSSRM 180-241273/3-A
Lab Control Sample
Total/NA
Sediment
7471 B
Analysis Batch: 241400
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-4
AH-07-0318-C
Total/NA
Sediment
7471 B
241273
180-76196-8
AH-06-0318-C
Total/NA
Sediment
7471 B
241273
180-76196-12
AH-02-0318-C
Total/NA
Sediment
7471 B
241273
180-76196-16
AH-04-0318-C
Total/NA
Sediment
7471 B
241273
180-76196-21
AH-05-0318-C
Total/NA
Sediment
7471 B
241273
180-76196-22
AH-05-0318-C-DUP
Total/NA
Sediment
7471E
241273
MB 180-241273/1-A
Method Blank
Total/NA
Sediment
7471B
241273
LCS 180-241273/2-A
Lab Control Sample
Total/NA
Sediment
7471 B
241273
LCSSRM 180-241273/3-A
Lab Control Sample
Total/NA
Sediment
7471 B
241273
TestAmerica Pittsburgh
Page 90 of 106 4/18/2018

QC Association Summary
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Metals (Continued)
Prep Batch: 241695
TestAmerica Job ID: 180-76196-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
180-76196-4
AH-07-0318-C
Total/NA
Sediment
3050B
180-76196-8
AH-06-0318-C
Total/NA
Sediment
3050B
180-76196-12
AH-02-0318-C
Total/NA
Sediment
3050B
180-76196-16
AH-04-0318-C
Total/NA
Sediment
3050B
180-76196-21
AH-05-0318-C
Total/NA
Sediment
3050B
180-76196-22
AH-05-0318-C-DUP
Total/NA
Sediment
3050B
MB 180-241695/1-A
Method Blank
Total/NA
Sediment
3050B
LCS 180-241695/2-A
Lab Control Sample
Total/NA
Sediment
3050B
LCSSRM 180-241695/19-A
Lab Control Sample
Total/NA
Sediment
3050B
Prep Batch: 241732
Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-76196-24
EB-02-0318
Total/NA
Water
7470A
MB 180-241732/1-A
Method Blank
Total/NA
Water
7470A
LCS 180-241732/2-A
Lab Control Sample
Total/NA
Water
7470A
Analysis Batch: 241904
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-24
EB-02-0318
Total/NA
Water
EPA 7470A
241732
MB 180-241732/1-A
Method Blank
Total/NA
Water
EPA 7470A
241732
LCS 180-241732/2-A
Lab Control Sample
Total/NA
Water
EPA 7470A
241732
Analysis Batch: 241911
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-4
AH-07-0318-C
Total/NA
Sediment
W-2—OB
241695
180-76196-8
AH-06-0318-C
Total/NA
Sediment
6020B
241695
180-76196-12
AH-02-0318-C
Total/NA
Sediment
6020B
241695
180-76196-16
AH-04-0318-C
Total/NA
Sediment
6020B
241695
180-76196-21
AH-05-0318-C
Total/NA
Sediment
6020B
241695
180-76196-22
AH-05-0318-C-DUP
Total/NA
Sediment
6020B
241695
MB 180-241695/1-A
Method Blank
Total/NA
Sediment
6020B
241695
LCS 180-241695/2-A
Lab Control Sample
Total/NA
Sediment
6020B
241695
LCSSRM 180-241695/19-A
Lab Control Sample
Total/NA
Sediment
6020B
241695
General Chemistry
Analysis Batch: 240705
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-24
EB-02-0318
Total/NA
Water
EPA 7196A
MB 180-240705/10
Method Blank
Total/NA
Water
EPA 7196A
LCS 180-240705/11
Lab Control Sample
Total/NA
Water
EPA 7196A
Analysis Batch: 240793
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-13
AH-04-0318-G1
Total/NA
Sediment
2540G
180-76196-14
AH-04-0318-G2
Total/NA
Sediment
2540G
180-76196-15
AH-04-0318-G3
Total/NA
Sediment
2540G
180-76196-16
AH-04-0318-C
Total/NA
Sediment
254OG
180-76196-17
AH-05-0318-G1
Total/NA
Sediment
254OG
180-76196-18
AH-05-0318-G1-DUP
Total/NA
Sediment
254OG
TestAmerica Pittsburgh
Page 91 of 106 4/18/2018

QC Association Summary C
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
General Chemistry (Continued)
Analysis Batch: 240793 (Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-19
AH-05-0318-G2
Total/NA
Sediment
2540G
180-76196-20
AH-05-0318-G3
Total/NA
Sediment
2540G
180-76196-21
AH-05-0318-C
Total/NA
Sediment
2540G
180-76196-22
AH-05-0318-C-DUP
Total/NA
Sediment
2540G
180-76196-16 DU
AH-04-0318-C
Total/NA
Sediment
2540G
180-76196-22 DU
AH-05-0318-C-DUP
Total/NA
Sediment
2540G
Analysis Batch: 240823
C
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-1
AH-07-0318-G1
Total/NA
Sediment
2540G
180-76196-2
AH-07-0318-G2
Total/NA
Sediment
254OG
180-76196-3
AH-07-0318-G3
Total/NA
Sediment
254OG
180-76196-4
AH-07-0318-C
Total/NA
Sediment
2540G
180-76196-5
AH-06-0318-G1
Total/NA
Sediment
2540G
m
180-76196-6
AH-06-0318-G2
Total/NA
Sediment
2540G
180-76196-7
AH-06-0318-G3
Total/NA
Sediment
2540G
180-76196-8
AH-06-0318-C
Total/NA
Sediment
2540G
180-76196-9
AH-02-0318-G1
Total/NA
Sediment
2540G
180-76196-10
AH-02-0318-G2
Total/NA
Sediment
2540G
180-76196-11
AH-02-0318-G3
Total/NA
Sediment
2540G
180-76196-12
AH-02-0318-C
Total/NA
Sediment
2540G
180-76196-4 DU
AH-07-0318-C
Total/NA
Sediment
2540G
180-76196-12 DU
AH-02-0318-C
Total/NA
Sediment
2540G
Prep Batch: 240858
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-4
AH-07-0318-C
Total/NA
Sediment
3060A
180-76196-8
AH-06-0318-C
Total/NA
Sediment
3060A
180-76196-12
AH-02-0318-C
Total/NA
Sediment
3060A
180-76196-16
AH-04-0318-C
Total/NA
Sediment
3060A
180-76196-21
AH-05-0318-C
Total/NA
Sediment
3060A
180-76196-22
AH-05-0318-C-DUP
Total/NA
Sediment
3060A
MB 180-240858/1-A
Method Blank
Total/NA
Sediment
3060A
LCSI 180-240858/3-A
Lab Control Sample
Total/NA
Sediment
3060A
LCSS 180-240858/2-A
Lab Control Sample
Total/NA
Sediment
3060A
180-76196-16 MSI
AH-04-0318-C
Total/NA
Sediment
3060A
180-76196-16 MSS
AH-04-0318-C
Total/NA
Sediment
3060A
180-76196-16 DU
AH-04-0318-C
Total/NA
Sediment
3060A
Analysis Batch: 240909
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-16
AH-04-0318-C
Total/NA
Sediment
Lloyd Kahn
180-76196-21
AH-05-0318-C
Total/NA
Sediment
Lloyd Kahn
180-76196-22
AH-05-0318-C-DUP
Total/NA
Sediment
Lloyd Kahn
MB 180-240909/3
Method Blank
Total/NA
Sediment
Lloyd Kahn
LCS 180-240909/4
Lab Control Sample
Total/NA
Sediment
Lloyd Kahn
Analysis Batch: 240949
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-4
AH-07-0318-C
Total/NA
Sediment
EPA 7196A
240858
180-76196-8
AH-06-0318-C
Total/NA
Sediment
EPA 7196A
240858
TestAmerica Pittsburgh
Page 92 of 106 4/18/2018

QC Association Summary
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
General Chemistry (Continued)
Analysis Batch: 240949 (Continued)
Lab Sample ID
180-76196-12
180-76196-16
180-76196-21
180-76196-22
MB 180-240858/1-A
LCSI 180-240858/3-A
LCSS 180-240858/2-A
180-76196-16 MSI
180-76196-16 MSS
180-76196-16 DU
Prep Batch: 241004
Lab Sample ID
180-76196-4
180-76196-8
180-76196-12
180-76196-16
180-76196-21
180-76196-22
MB 180-241004/1-A
LCS 180-241004/2-A
LCSD 180-241004/3-A
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
AH-02-0318-C
Total/NA
Sediment
EPA 7196A
240858
AH-04-0318-C
Total/NA
Sediment
EPA 7196A
240858
AH-05-0318-C
Total/NA
Sediment
EPA 7196A
240858
AH-05-0318-C-DUP
Total/NA
Sediment
EPA 7196A
240858
Method Blank
Total/NA
Sediment
EPA 7196A
240858
Lab Control Sample
Total/NA
Sediment
EPA 7196A
240858
Lab Control Sample
Total/NA
Sediment
EPA 7196A
240858
AH-04-0318-C
Total/NA
Sediment
EPA 7196A
240858
AH-04-0318-C
Total/NA
Sediment
EPA 7196A
240858
AH-04-0318-C
Total/NA
Sediment
EPA 7196A
240858
Analysis Batch: 241091
Lab Sample ID
180-76196-4
180-76196-8
180-76196-12
180-76196-16
180-76196-21
180-76196-22
MB 180-241004/1-A
LCS 180-241004/2-A
LCSD 180-241004/3-A
Analysis Batch: 241158
Lab Sample ID
180-76196-4
180-76196-8
180-76196-12
MB 180-241158/3
LCS 180-241158/4
Analysis Batch: 241245
Client Sample ID
Prep Type
Matrix
Method
AH-07-0318-C
Total/NA
Sediment
9071 B
AH-06-0318-C
Total/NA
Sediment
9071 B
AH-02-0318-C
Total/NA
Sediment
9071 B
AH-04-0318-C
Total/NA
Sediment
9071 B
AH-05-0318-C
Total/NA
Sediment
9071 B
AH-05-0318-C-DUP
Total/NA
Sediment
9071B
Method Blank
Total/NA
Sediment
9071 B
Lab Control Sample
Total/NA
Sediment
9071 B
Lab Control Sample Dup
Total/NA
Sediment
9071 B
Prep Batch m
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
AH-07-0318-C
Total/NA
Sediment
EPA 9071 B
241004
AH-06-0318-C
Total/NA
Sediment
EPA 9071 B
241004
AH-02-0318-C
Total/NA
Sediment
EPA 9071 B
241004
AH-04-0318-C
Total/NA
Sediment
EPA 9071 B
241004
AH-05-0318-C
Total/NA
Sediment
EPA 9071 B
241004
AH-05-0318-C-DUP
Total/NA
Sediment
EPA 9071B
241004
Method Blank
Total/NA
Sediment
EPA 9071 B
241004
Lab Control Sample
Total/NA
Sediment
EPA 9071 B
241004
Lab Control Sample Dup
Total/NA
Sediment
EPA 9071 B
241004
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
AH-07-0318-C
Total/NA
Sediment
Lloyd Kahn
AH-06-0318-C
Total/NA
Sediment
Lloyd Kahn
AH-02-0318-C
Total/NA
Sediment
Lloyd Kahn
Method Blank
Total/NA
Sediment
Lloyd Kahn
Lab Control Sample
Total/NA
Sediment
Lloyd Kahn
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-76196-24
EB-02-0318
Total/NA
Water
SM 5310C
MB 180-241245/6
Method Blank
Total/NA
Water
SM 5310C
LCS 180-241245/4
Lab Control Sample
Total/NA
Water
SM 5310C
LCSD 180-241245/5
Lab Control Sample Dup
Total/NA
Water
SM 5310C
TestAmerica Pittsburgh
Page 93 of 106 4/18/2018

QC Association Summary
Client: Athena Technologies, Inc
TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
General Chemistry (Continued)
Analysis Batch: 241989
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-4 AH-07-0318-C
Total/NA
Sediment
7196A
180-76196-8 AH-06-0318-C
Total/NA
Sediment
7196A
180-76196-12 AH-02-0318-C
Total/NA
Sediment
7196A
180-76196-16 AH-04-0318-C
Total/NA
Sediment
7196A
180-76196-21 AH-05-0318-C
Total/NA
Sediment
7196A
180-76196-22 AH-05-0318-C-DUP
Total/NA
Sediment
7196A
180-76196-24 EB-02-0318
Total/NA
Water
7196A
Prep Batch: 392275
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-24 EB-02-0318
Total/NA
Water
1664B
MB 400-392275/1-A Method Blank
Total/NA
Water
1664B
LCS 400-392275/2-A Lab Control Sample
Total/NA
Water
1664B
Analysis Batch: 392295
m
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-76196-24 EB-02-0318
Total/NA
Water
1664B
392275
MB 400-392275/1-A Method Blank
Total/NA
Water
1664B
392275
LCS 400-392275/2-A Lab Control Sample
Total/NA
Water
1664B
392275
TestAmerica Pittsburgh
Page 94 of 106 4/18/2018

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Page 103 of 106
4/18/2018

Login Sample Receipt Checklist
Client: Athena Technologies, Inc
Job Number: 180-76196-1
Login Number: 76196
List Number: 1
Creator: Kovitch, Christina M
Question
List Source: TestAmerica Pittsburgh
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
False
Samples are received within Holding Time (excluding tests with immediate
False
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
TestAmerica Pittsburgh
Page 104 of 106 4/18/2018

Login Sample Receipt Checklist
Client: Athena Technologies, Inc
Job Number: 180-76196-1
Login Number: 76196
List Number: 2
Creator: Watson, Debbie
Question
List Source: TestAmerica Pittsburgh
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
TestAmerica Pittsburgh
Page 105 of 106 4/18/2018

Login Sample Receipt Checklist
Client: Athena Technologies, Inc
Job Number: 180-76196-1
Login Number: 76196
List Number: 3
Creator: Conrady, Hank W
Question
List Source: TestAmerica Pensacola
List Creation: 03/30/18 04:08 PM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
False NO CUSTODY SEAL
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True 3.4°C IR-7
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
TestAmerica Pittsburgh
Page 106 of 106 4/18/2018

TestAmerica °
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Pensacola
3355 McLemore Drive
Pensacola, FL 32514
Tel: [phone]
TestAmerica Job ID: 400-151454-1
Client Project/Site: North Carolina Sediment Project
For:
Athena Technologies, Inc
1293 Graham Farm Road
PO BOX 68
McClellanville, South Carolina 29458
Attn: Adam Freeze
Authorized for release by.
411212018 12:52:45 PM
Carrie Gamber, Senior Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Table of Contents
TestAmerica Job ID: 400-151454-1
CoverPage ..............................................
1
Table of Contents .........................................
2
Case Narrative ...........................................
3 L
Detection Summary ........................................
4
Sample Summary .........................................
5
Client Sample Results ......................................
6
Definitions.........................................
13
Surrogate Summary .......................................
14
QC Association ...........................................
17 C
QC Sample Results ........................................
20
Chronicle................................................
27
Method Summary .........................................
34
Certification Summary ......................................
35
Chain of Custody ..........................................
36
Receipt Checklists .........................................
37
TestAmerica Pensacola
Page 2 of 37 4/12/2018

Case Narrative C
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Job ID: 400-151454-1
Laboratory: TestAmerica Pensacola
Narrative
CASE NARRATIVE
Client: Athena Technologies, Inc
Project: North Carolina Sediment Project F
Report Number: 400-151454-1 F
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round -off errors in calculated results. F
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 03/28/2018; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 0.0 C.
M"PH
Several samples required dilution due to the sample matrix. Elevated reporting limits (RLs) were reported.
MAEPH
Four surrogates were used for this analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance criteria
without performing re-extraction/re-analysis. The following sample contained an allowable number of surrogate compounds outside
limits: EB-02-0318 (400-151454-7). These results have been reported and qualified.
Four surrogates are used for this analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance criteria without
performing re-extraction/re-analysis. The following samples contained an allowable number of surrogate compounds outside limits:
(AH-06-0318-C (400-151454-2MS) and AH-02-0318-C (400-151454-3MS). These results have been reported and qualified.
C19-C36 Aliphatics failed the recovery criteria low for the MS of sample AH-06-0318-C (400-151454-2) in batch 400-392564.
C19-C36 Aliphatics, C9-Cl8 Aliphatics and C11-C22 Aromatics failed the recovery criteria low for the MS of sample AH-02-0318-C
(400-151454-3) in batch 400-393048. C9-C18 Aliphatics and C11-C22 Aromatics exceeded the RPD limit for the MSD of sample
AH-02-0318-C (400-151454-3) in batch 400-393048.
PERCENT SOLIDS
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Pensacola
Page 3 of 37 4/12/2018

Detection Summary
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-07-0318-C
Lab Sample ID: 400-151454-1
1 No Detections.
a
Client Sample ID: AH-06-0318-C
Lab Sample ID: 400-151454-2 L
LNo Detections.
Client Sample ID: AH-02-0318-C
Lab Sample ID: 400-151454-3
LNo Detections.
E:
Client Sample ID: AH-04-0318-C
Lab Sample ID: 400-151454-4
Analyte Result Qualifier
RL MDL Unit
Dil Fac D Method Prep Type
F
C11-C22 Aromatics 12
7.8 7.8 mg/Kg
1 MA-EPH Total/NA
C19-C36 Aliphatics 12
7.8 7.8 mg/Kg
1 MA-EPH Total/NA
Client Sample ID: AH-05-0318-C
Lab Sample ID: 400-151454-5
Analyte Result Qualifier
RL MDL Unit
Dil Fac D Method Prep Type
C11-C22 Aromatics 28
13 13 mg/Kg
1 MA-EPH Total/NA
C9-C18 Aliphatics 15
13 13 mg/Kg
1 MA-EPH Total/NA F
Client Sample ID: AH-05-0318-C-DUP
Lab Sample ID: 400-151454-6
Result Qualifier
RL MDL Unit
Dil Fac D Method Prep Type
Cnalyte
C11-C22 Aromatics 16
12 12 mg/Kg
1 MA-EPH Total/NA
Client Sample ID: EB-02-0318
Lab Sample ID: 400-151454-7
FNo Detections
This Detection Summary does not include radiochemical test results.
Page 4 of 37
TestAmerica Pensacola
4/12/2018

Sample Summary
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
400-151454-1
AH-07-0318-C
Sediment
03/27/18 08:50
03/28/18 09:44
400-151454-2
AH-06-0318-C
Sediment
03/27/18 09:30
03/28/18 09:44
400-151454-3
AH-02-0318-C
Sediment
03/27/18 10:05
03/28/18 09:44
400-151454-4
AH-04-0318-C
Sediment
03/27/18 10:50
03/28/18 09:44
400-151454-5
AH-05-0318-C
Sediment
03/27/18 11:55
03/28/18 09:44
400-151454-6
AH-05-0318-C-DUP
Sediment
03/27/18 11:58
03/28/18 09:44
400-151454-7
EB-02-0318
Water
03/27/18 12:50
03/28/18 09:44
TestAmerica Pensacola
Page 5 of 37 4/12/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-07-0318-C
Lab Sample ID: 400-151454-1
Date Collected: 03/27/18 08:50
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 80.8
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
C5-C8 Aliphatics ND
7.9 7.9 mg/Kg
* 03/29/18 13:00 03/29/18 23:44 50
C9-C10 Aromatics ND
2.2 2.2 mg/Kg
03/29/18 13:00 03/29/18 23:44 50
C9-C12 Aliphatics ND
4.1 4.1 mg/Kg
03/29/18 13:00 03/29/18 23:44 50
Surrogate
%Recovery Qualifier
Limits
a,a,a-Trifluorotoluene (fid)
96
70- 130
a,a,a-Trifluorotoluene (pid)
95
70- 130
Method: MA-EPH - Massachusetts
- Extractable Petroleum
Hydrocarbons (GC)
Analyte
Result Qualifier
RL
MDL
Unit
C11-C22 Aromatics
ND
3.9
3.9
mg/Kg
C19-C36 Aliphatics
ND
3.9
3.9
mg/Kg
C9-C18 Aliphatics
ND
3.9
3.9
mg/Kg
Surrogate
%Recovery Qualifier
Limits
1-Chlorooctadecane
46
40- 140
2-Bromonaphthalene
50
40 - 140
2-Fluorobiphenyl
68
40 - 140
o-Terphenyl
50
40- 140
General Chemistry
Analyte Result Qualifier
Percent Solids 80.8
Percent Moisture 19.2
RL MDL Unit
0.01 0.01 %
0.01 0.01 %
Prepared
Analyzed
Dil Fac
03129118 13:00
03129118 23:44
50
03/29/18 13:00
03/29/18 23:44
50
D Prepared
Analyzed
Dil Fac
03/29/18 12:30
04/04/18 02:06
1
03/29/18 12:30
04/03/18 21:07
1
03/29/18 12:30
04/03/18 21:07
1
Prepared
Analyzed
Dil Fac
03/29/18 12:30
04103118 21:07
1
03/29/18 12:30
04104118 02:06
1
03/29/18 12:30
04104118 02:06
1
03/29/18 12:30
04104118 02:06
1
D Prepared
Analyzed
Dil Fac
03/29/18 10:37
1
03/29/18 10:37
1
Page 6 of 37
TestAmerica Pensacola
4/12/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-06-0318-C
Lab Sample ID: 400-151454-2
Date Collected: 03/27/18 09:30
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 81.0
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
C5-C8 Aliphatics ND
9.6 9.6 mg/Kg
* 03/29/18 13:00 03/30/18 00:44 50
C9-C10 Aromatics ND
2.7 2.7 mg/Kg
03/29/18 13:00 03/30/18 00:44 50
C9-C12 Aliphatics ND
5.0 5.0 mg/Kg
03/29/18 13:00 03/30/18 00:44 50
Surrogate
%Recovery
Qualifier
Limits
a,a,a-Trifluorotoluene (fid)
101
70- 130
a,a,a-Trifluorotoluene (pid)
100
70- 130
Method: MA-EPH - Massachusetts
- Extractable
Petroleum
Hydrocarbons (GC)
Analyte
Result
Qualifier
RL
MDL
Unit
C11-C22 Aromatics
ND
3.9
3.9
mg/Kg
C19-C36 Aliphatics
ND
F1
3.9
3.9
mg/Kg
C9-C18 Aliphatics
ND
3.9
3.9
mg/Kg
Surrogate
%Recovery
Qualifier
Limits
1-Chlorooctadecane
49
40- 140
2-Bromonaphthalene
59
40 - 140
2-Fluorobiphenyl
73
40 - 140
o-Terphenyl
53
40- 140
General Chemistry
Analyte Result Qualifier
Percent Solids 81.0
Percent Moisture 19.0
RL MDL Unit
0.01 0.01 %
0.01 0.01 %
Prepared
Analyzed
Dil Fac
03129118 13:00
03130118 00.44
50
03/29/18 13:00
03130118 00:44
50
D Prepared
Analyzed
Dil Fac
03/29/18 12:30
04/04/18 01:38
1
03/29/18 12:30
04/03/18 20:38
1
03/29/18 12:30
04/03/18 20:38
1
Prepared
Analyzed
Dil Fac
03/29/18 12:30
04103118 20:38
1
03/29/18 12:30
04104118 01:38
1
03/29/18 12:30
04104118 01:38
1
03/29/18 12:30
04104118 01:38
1
D Prepared
Analyzed
Dil Fac
03/29/18 10:37
1
03/29/18 10:37
1
Page 7 of 37
TestAmerica Pensacola
4/12/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-02-0318-C
Lab Sample
ID: 400-151454-3
Date Collected: 03/27/18 10:05
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 61.6
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
C5-C8 Aliphatics ND
18
18 mg/Kg
0 03/29/18 13:00
03/30/18 01:44 50
C9-C10 Aromatics ND
4.9
4.9 mg/Kg
03/29/18 13:00
03/30/18 01:44 50
C9-C12 Aliphatics ND
9.1
9.1 mg/Kg
03/29/18 13:00
03/30/18 01:44 50
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
a,a,a-Trifluorotoluene (fid) 96
70- 130
03/29/18 13:00
03130118 01:44 50
a,a,a-Trifluorotoluene (pid) 95
70- 130
03/29/18 13:00
03130118 01:44 50
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed Dil Fac
C11-C22 Aromatics
ND
F1 F2
5.1
5.1
mg/Kg
04/04/18 12:45
04/09/18 17:28 1
C19-C36 Aliphatics
ND
F1
5.1
5.1
mg/Kg
04/04/18 12:45
04/09/18 12:16 1
C9-C18 Aliphatics
ND
F1 F2
5.1
5.1
mg/Kg
04/04/18 12:45
04/09/18 12:16 1
Surrogate
%Recovery Qualifier
1-Chlorooctadecane
54
2-Bromonaphthalene
55
2-Fluorobiphenyl
69
o-Terphenyl
54
General Chemistry
Analyte
Result Qualifier
Percent Solids
61.6
Percent Moisture
38.5
0
0
Limits
Prepared
Analyzed
Dil Fac
40 - 140
04104118 12:45
04/09118 12:16
1
40 - 140
04104118 12:45
04109118 17:28
1
40 - 140
04104118 12:45
04109118 17:28
1
40 - 140
04104118 12:45
04109118 17:28
1
RL MDL Unit
D Prepared
Analyzed
Dil Fac
0.01 0.01 %
03/29/1810:37
1
0.01 0.01 %
03/29/1810:37
1
TestAmerica Pensacola
Page 8 of 37 4/12/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-04-0318-C
Lab Sample ID: 400-151454-4
Date Collected: 03/27/18 10:50
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 40.2
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
C5-C8 Aliphatics ND
24 24 mg/Kg
03/29/18 13:00 03/30/18 02:43 50
C9-C10 Aromatics ND
6.8 6.8 mg/Kg
03/29/18 13:00 03/30/18 02:43 50
C9-C12 Aliphatics ND
13 13 mg/Kg
03/29/18 13:00 03/30/18 02:43 50
Surrogate
%Recovery Qualifier
Limits
a,a,a-Trifluorotoluene (fid)
95
70- 130
a,a,a-Trifluorotoluene (pid)
94
70- 130
Method: MA-EPH - Massachusetts
- Extractable Petroleum
Hydrocarbons (GC)
Analyte
Result Qualifier
RL
MDL
Unit
C11-C22 Aromatics
12
7.8
7.8
mg/Kg
C19-C36 Aliphatics
12
7.8
7.8
mg/Kg
C9-C18 Aliphatics
ND
7.8
7.8
mg/Kg
Surrogate
%Recovery Qualifier
Limits
1-Chlorooctadecane
54
40- 140
2-Bromonaphthalene
52
40 - 140
2-Fluorobiphenyl
64
40 - 140
o-Terphenyl
51
40- 140
General Chemistry
Analyte Result Qualifier
Percent Solids 40.3
Percent Moisture 59.8
RL MDL Unit
0.01 0.01 %
0.01 0.01 %
Prepared
Analyzed
Dil Fac
03129118 13:00
03130118 02:43
50
03/29/18 13:00
03130118 02:43
50
D Prepared
Analyzed
Dil Fac
03/29/18 12:30
04/04/18 02:26
1
03/29/18 12:30
04/03/18 21:27
1
03/29/18 12:30
04/03/18 21:27
1
Prepared
Analyzed
Dil Fac
03/29/18 12:30
04103118 21:27
1
03/29/18 12:30
04104118 02:26
1
03/29/18 12:30
04104118 02:26
1
03/29/18 12:30
04104118 02:26
1
D Prepared
Analyzed
Dil Fac
03/29/18 10:37
1
03/29/18 10:37
1
Page 9 of 37
TestAmerica Pensacola
4/12/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-C
Lab Sample ID: 400-151454-5
Date Collected: 03/27/18 11:55
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 24.7
Method: MAVPH - Massachusetts - Volatile Petroleum
Hydrocarbons (GC)
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
C5-C8 Aliphatics ND
76 76 mg/Kg
* 03/29/18 13:00 03/30/18 03:43 50
C9-C10 Aromatics ND
21 21 mg/Kg
03/29/18 13:00 03/30/18 03:43 50
C9-C12 Aliphatics ND
39 39 mg/Kg
03/29/18 13:00 03/30/18 03:43 50
Surrogate
%Recovery Qualifier
Limits
a,a,a-Trifluorotoluene (fid)
96
70- 130
a,a,a-Trifluorotoluene (pid)
95
70- 130
Method: MA-EPH - Massachusetts
- Extractable Petroleum
Hydrocarbons (GC)
Analyte
Result Qualifier
RL
MDL Unit
C11-C22 Aromatics
28
13
13 mg/Kg
C19-C36 Aliphatics
ND
13
13 mg/Kg
C9-C18 Aliphatics
15
13
13 mg/Kg
Surrogate
%Recovery Qualifier
Limits
1-Chlorooctadecane
50
40- 140
2-Bromonaphthalene
52
40 - 140
2-Fluorobiphenyl
64
40 - 140
o-Terphenyl
48
40- 140
General Chemistry
Analyte Result Qualifier
Percent Solids 24.7
Percent Moisture 75.3
RL MDL Unit
0.01 0.01 %
0.01 0.01 %
Prepared
Analyzed
Dil Fac
03129118 13:00
03130118 03:43
50
03/29/18 13:00
03130118 03:43
50
D Prepared
Analyzed
Dil Fac
03/29/18 12:30
04/04/18 02:36
1
03/29/18 12:30
04/03/18 21:37
1
03/29/18 12:30
04/03/18 21:37
1
Prepared
Analyzed
Dil Fac
03/29/18 12:30
04103118 21:37
1
03/29/18 12:30
04104118 02:36
1
03/29/18 12:30
04104118 02:36
1
03/29/18 12:30
04104118 02:36
1
D Prepared
Analyzed
Dil Fac
03/29/18 10:37
1
03/29/18 10:37
1
Page 10 of 37
TestAmerica Pensacola
4/12/2018

Client Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-C-DUP
Lab Sample
ID: 400-151454-6
Date Collected: 03/27/18 11:58
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 25.3
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
C5-C8 Aliphatics ND
100
100 mg/Kg
0 03/29/18 13:00
03/30/18 04:43 50
C9-C10 Aromatics ND
28
28 mg/Kg
03/29/18 13:00
03/30/18 04:43 50
C9-C12 Aliphatics ND
53
53 mg/Kg
03/29/18 13:00
03/30/18 04:43 50
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
a,a,a-Trifluorotoluene (fid) 124
70- 130
03/29/18 13:00
03130118 04:43 50
a,a,a-Trifluorotoluene (pid) 123
70- 130
03/29/18 13:00
03130118 04:43 50
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
C11-C22 Aromatics
16
12
12
mg/Kg
03/29/18 12:30
04/04/18 02:45 1
C19-C36 Aliphatics
ND
12
12
mg/Kg
03/29/18 12:30
04/03/18 21:47 1
C9-C18 Aliphatics
ND
12
12
mg/Kg
03/29/18 12:30
04/03/18 21:47 1
Surrogate
%Recovery Qualifier
1-Chlorooctadecane
41
2-Bromonaphthalene
57
2-Fluorobiphenyl
71
o-Terphenyl
42
General Chemistry
Analyte
Result Qualifier
Percent Solids
25.3
Percent Moisture
74.7
0
0
Limits
Prepared
Analyzed
Dil Fac
40 - 140
03/29/18 12:30
04/03/18 21:47
1
40 - 140
03/29/18 12:30
04104118 02:45
1
40 - 140
03/29/18 12:30
04104118 02:45
1
40 - 140
03/29/18 12:30
04104118 02:45
1
RL MDL Unit
D Prepared
Analyzed
Dil Fac
0.01 0.01 %
03/29/1810:37
1
0.01 0.01 %
03/29/1810:37
1
TestAmerica Pensacola
Page 11 of 37 4/12/2018

Client Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 400-151454-1
Client Sample ID: EB-02-0318 Lab Sample ID: 400-151454-7
Date Collected: 03/27/18 12:50 Matrix: Water
Date Received: 03/28/18 09:44
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Analyte Result Qualifier RL MDL Unit D
C5-C8 Aliphatics ND 26 26 ug/L
C9-C12 Aliphatics ND 11 11 ug/L
C9-C10 Aromatics ND 7.0 7.0 ug/L
Surrogate %Recovery Qualifier Limits
a,a,a-Trifluorotoluene (fid) 100 70- 130
a,a,a-Trifluorotoluene (pid) 100 70- 130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prepared Analyzed Dil Fac
03/29/18 19:46 1
03/29/18 19:46 1
03/29/18 19:46 1
Prepared Analyzed Dil Fac
03129118 19:46 1
03/29/18 19:46 1 E:
F
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
C9-C18 Aliphatics
ND
0.054
0.054
mg/L
04/03/18 10:59
04/09/18 14:33
1
C19-C36 Aliphatics
ND
0.054
0.054
mg/L
04/03/18 10:59
04/09/18 14:33
1
C11-C22 Aromatics
ND
0.054
0.054
mg/L
04/03/18 10:59
04/09/18 19:44
1
Surrogate %Recovery Qualifier Limits
1-Chlorooctadecane 73 40- 140
o-Terphenyl 67 40 - 140
2-Fluorobiphenyl 68 40 - 140
2-Bromonaphthalene 26 X 40 - 140
Prepared
Analyzed
Dil Fac
0410311810:59
0410911814:33
1
0410311810:59
0410911819:44
1
0410311810:59
0410911819:44
1
0410311810:59
0410911819:44
1
TestAmerica Pensacola
Page 12 of 37 4/12/2018

Definitions/Glossary
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Qualifiers
GC Semi VOA
Qualifier Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
X Surrogate is outside control limits
F2 MS/MSD RPD exceeds control limits
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
tt Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Pensacola
Page 13 of 37 4/12/2018

Surrogate Summary
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 400-151454-1
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Matrix: Sediment
Lab Sample ID
400-151454-1
400-151454-2
400-151454-3
400-151454-4
400-151454-5
400-151454-6
LCS 400-391552/2-A
LCSD 400-391552/3-A
MB 400-391552/1-A
Client Sample ID
AH-07-0318-C
AH-06-0318-C
AH-02-0318-C
AH-04-0318-C
AH-05-0318-C
AH-05-0318-C-DUP
Lab Control Sample
Lab Control Sample Dup
Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TFT-F2 TFT-P1
(70-130) (70-130)
96
95
101
100
96
95
95
94
96
95
124
123
96
95
93
92
93
93
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Matrix: Water
Lab Sample ID
400-151454-7
LCS 400-391983/4
LCSD 400-391983/13
MB 400-391983/2
Client Sample ID
EB-02-0318
Lab Control Sample
Lab Control Sample Dup
Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
Percent Surrogate Recovery (Acceptance Limits)
TFT-F2 TFT-P1
(70-130) (70-130)
100 100
100 100
108 107
101 102
Total/NA
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Matrix: Sediment Prep Tvoe: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
1COD1
Lab Sample ID
Client Sample ID
(40-140)
400-151454-1
AH-07-0318-C
46
400-151454-2
AH-06-0318-C
49
400-151454-2 MS
AH-06-0318-C
35 X
400-151454-2 MSD
AH-06-0318-C
47
400-151454-3
AH-02-0318-C
54
400-151454-3 MS
AH-02-0318-C
19 X
400-151454-3 MSD
AH-02-0318-C
58
400-151454-4
AH-04-0318-C
54
400-151454-5
AH-05-0318-C
50
400-151454-6
AH-05-0318-C-DUP
41
LCS 400-391988/2-A
Lab Control Sample
59
LCS 400-392659/2-A
Lab Control Sample
59
MB 400-391988/1-A
Method Blank
67
MB 400-392659/1-A
Method Blank
56
0
Page 14 of 37
TestAmerica Pensacola
4/12/2018

Surrogate Summary
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Surrogate Legend
1COD = 1-Chlorooctadecane
TestAmerica Job ID: 400-151454-1
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Matrix: Sediment Prep Type: Total/NA
C
Percent Surrogate Recovery (Acceptance Limits)
2BN1
FBP1
OTPH1
Lab Sample ID
Client Sample ID
(40-140)
(40-140)
(40-140)
400-151454-1
AH-07-0318-C
50
68
50
400-151454-2
AH-06-0318-C
59
73
53
400-151454-2 MS
AH-06-0318-C
49
72
42
400-151454-2 MSD
AH-06-0318-C
63
76
50
400-151454-3
AH-02-0318-C
55
69
54
400-151454-3 MS
AH-02-0318-C
55
68
21 X
400-151454-3 MSD
AH-02-0318-C
56
70
51
400-151454-4
AH-04-0318-C
52
64
51
400-151454-5
AH-05-0318-C
52
64
48
400-151454-6
AH-05-0318-C-DUP
57
71
42
LCS 400-391988/2-A
Lab Control Sample
58
71
56
LCS 400-392659/2-A
Lab Control Sample
62
70
54
MB 400-391988/1-A
Method Blank
65
73
57
MB 400-392659/1-A
Method Blank
52
62
49
Surrogate Legend
2BN = 2-Bromonaphthalene
FBP = 2-Fluorobiphenyl
OTPH = o-Terphenyl
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Matrix: Water
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
1COD1
Lab Sample ID Client Sample ID
(40-140)
400-151454-7 EB-02-0318
73
LCS 400-392483/2-A Lab Control Sample
74
LCSD 400-392483/3-A Lab Control Sample Dup
69
MB 400-392483/1-A Method Blank
75
Surrogate Legend
1COD = 1-Chlorooctadecane
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Matrix: Water Prep Twe: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
OTPH1
FBP1 2BN1
Lab Sample ID
Client Sample ID
(40-140)
(40-140) (40-140)
400-151454-7
EB-02-0318
67
68 26 X
LCS 400-392483/2-A
Lab Control Sample
72
74 66
LCSD 400-392483/3-A
Lab Control Sample Dup
59
65 58
MB 400-392483/1-A
Method Blank
66
66 61
Surrogate Legend
OTPH = o-Terphenyl
TestAmerica Pensacola
Page 15 of 37 4/12/2018

Surrogate Summary
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
FBP = 2-Fluorobiphenyl
2BN = 2-Bromonaphthalene
0
TestAmerica Pensacola
Page 16 of 37 4/12/2018

QC Association Summary
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
GC VOA
Analysis Batch: 391473
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-1
AH-07-0318-C
Total/NA
Sediment
MAVPH
391552
400-151454-2
AH-06-0318-C
Total/NA
Sediment
MAVPH
391552
400-151454-3
AH-02-0318-C
Total/NA
Sediment
MAVPH
391552
400-151454-4
AH-04-0318-C
Total/NA
Sediment
MAVPH
391552
400-151454-5
AH-05-0318-C
Total/NA
Sediment
MAVPH
391552
400-151454-6
AH-05-0318-C-DUP
Total/NA
Sediment
MAVPH
391552
MB 400-391552/1-A
Method Blank
Total/NA
Sediment
MAVPH
391552
LCS 400-391552/2-A
Lab Control Sample
Total/NA
Sediment
MAVPH
391552
LCSD 400-391552/3-A
Lab Control Sample Dup
Total/NA
Sediment
MAVPH
391552
•
Prep Batch: 391552
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-1
AH-07-0318-C
Total/NA
Sediment
5035
400-151454-2
AH-06-0318-C
Total/NA
Sediment
5035
400-151454-3
AH-02-0318-C
Total/NA
Sediment
5035
400-151454-4
AH-04-0318-C
Total/NA
Sediment
5035
400-151454-5
AH-05-0318-C
Total/NA
Sediment
5035
400-151454-6
AH-05-0318-C-DUP
Total/NA
Sediment
5035
MB 400-391552/1-A
Method Blank
Total/NA
Sediment
5035
LCS 400-391552/2-A
Lab Control Sample
Total/NA
Sediment
5035
LCSD 400-391552/3-A
Lab Control Sample Dup
Total/NA
Sediment
5035
Analysis Batch: 391983
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-7
EB-02-0318
Total/NA
Water
MAVPH
MB 400-391983/2
Method Blank
Total/NA
Water
MAVPH
LCS 400-391983/4
Lab Control Sample
Total/NA
Water
MAVPH
LCSD 400-391983/13
Lab Control Sample Dup
Total/NA
Water
MAVPH
GC Semi VOA
Prep Batch: 391988
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-151454-1
AH-07-0318-C
Total/NA
Sediment
3546
400-151454-2
AH-06-0318-C
Total/NA
Sediment
3546
400-151454-4
AH-04-0318-C
Total/NA
Sediment
3546
400-151454-5
AH-05-0318-C
Total/NA
Sediment
3546
400-151454-6
AH-05-0318-C-DUP
Total/NA
Sediment
3546
MB 400-391988/1-A
Method Blank
Total/NA
Sediment
3546
LCS 400-391988/2-A
Lab Control Sample
Total/NA
Sediment
3546
400-151454-2 MS
AH-06-0318-C
Total/NA
Sediment
3546
400-151454-2 MSD
AH-06-0318-C
Total/NA
Sediment
3546
Prep Batch: 392483
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-151454-7
EB-02-0318
Total/NA
Water
3520C
MB 400-392483/1-A
Method Blank
Total/NA
Water
3520C
LCS 400-392483/2-A
Lab Control Sample
Total/NA
Water
3520C
LCSD 400-392483/3-A
Lab Control Sample Dup
Total/NA
Water
3520C
TestAmerica Pensacola
Page 17 of 37 4/12/2018

QC Association Summary
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
GC Semi VOA (Continued)
Analysis Batch: 392564
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-1
AH-07-0318-C
Total/NA
Sediment
MA-EPH
391988
400-151454-2
AH-06-0318-C
Total/NA
Sediment
MA-EPH
391988
400-151454-4
AH-04-0318-C
Total/NA
Sediment
MA-EPH
391988
400-151454-5
AH-05-0318-C
Total/NA
Sediment
MA-EPH
391988
400-151454-6
AH-05-0318-C-DUP
Total/NA
Sediment
MA-EPH
391988
MB 400-391988/1-A
Method Blank
Total/NA
Sediment
MA-EPH
391988
LCS 400-391988/2-A
Lab Control Sample
Total/NA
Sediment
MA-EPH
391988
400-151454-2 MS
AH-06-0318-C
Total/NA
Sediment
MA-EPH
391988
400-151454-2 MSD
AH-06-0318-C
Total/NA
Sediment
MA-EPH
391988
•
Analysis Batch: 392567
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-1
AH-07-0318-C
Total/NA
Sediment
MA-EPH
391988
400-151454-2
AH-06-0318-C
Total/NA
Sediment
MA-EPH
391988
400-151454-4
AH-04-0318-C
Total/NA
Sediment
MA-EPH
391988
400-151454-5
AH-05-0318-C
Total/NA
Sediment
MA-EPH
391988
400-151454-6
AH-05-0318-C-DUP
Total/NA
Sediment
MA-EPH
391988
MB 400-391988/1-A
Method Blank
Total/NA
Sediment
MA-EPH
391988
LCS 400-391988/2-A
Lab Control Sample
Total/NA
Sediment
MA-EPH
391988
400-151454-2 MS
AH-06-0318-C
Total/NA
Sediment
MA-EPH
391988
400-151454-2 MSD
AH-06-0318-C
Total/NA
Sediment
MA-EPH
391988
Prep Batch: 392659
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-3
AH-02-0318-C
Total/NA
Sediment
3546
MB 400-392659/1-A
Method Blank
Total/NA
Sediment
3546
LCS 400-392659/2-A
Lab Control Sample
Total/NA
Sediment
3546
400-151454-3 MS
AH-02-0318-C
Total/NA
Sediment
3546
400-151454-3 MSD
AH-02-0318-C
Total/NA
Sediment
3546
Analysis Batch: 393044
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-3
AH-02-0318-C
Total/NA
Sediment
MA-EPH
392659
MB 400-392659/1-A
Method Blank
Total/NA
Sediment
MA-EPH
392659
LCS 400-392659/2-A
Lab Control Sample
Total/NA
Sediment
MA-EPH
392659
400-151454-3 MS
AH-02-0318-C
Total/NA
Sediment
MA-EPH
392659
400-151454-3 MSD
AH-02-0318-C
Total/NA
Sediment
MA-EPH
392659
Analysis Batch: 393045
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-7
EB-02-0318
Total/NA
Water
MA-EPH
392483
MB 400-392483/1-A
Method Blank
Total/NA
Water
MA-EPH
392483
LCS 400-392483/2-A
Lab Control Sample
Total/NA
Water
MA-EPH
392483
LCSD 400-392483/3-A
Lab Control Sample Dup
Total/NA
Water
MA-EPH
392483
Analysis Batch: 393048
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-3
AH-02-0318-C
Total/NA
Sediment
MA-EPH
392659
MB 400-392659/1-A
Method Blank
Total/NA
Sediment
MA-EPH
392659
LCS 400-392659/2-A
Lab Control Sample
Total/NA
Sediment
MA-EPH
392659
400-151454-3 MS
AH-02-0318-C
Total/NA
Sediment
MA-EPH
392659
TestAmerica Pensacola
Page 18 of 37 4/12/2018

QC Association Summary
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
GC Semi VOA (Continued)
Analysis Batch: 393048 (Continued)
Lab Sample ID Client Sample ID
400-151454-3 MSD AH-02-0318-C
Analysis Batch: 393049
TestAmerica Job ID: 400-151454-1
Prep Type Matrix Method Prep Batch
Total/NA Sediment MA-EPH 392659
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-7
EB-02-0318
Total/NA
Water
MA-EPH
392483
MB 400-392483/1-A
Method Blank
Total/NA
Water
MA-EPH
392483
LCS 400-392483/2-A
Lab Control Sample
Total/NA
Water
MA-EPH
392483
LCSD 400-392483/3-A
Lab Control Sample Dup
Total/NA
Water
MA-EPH
392483
General Chemistry
Analysis Batch: 391941
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-151454-1
AH-07-0318-C
Total/NA
Sediment
Moisture
400-151454-2
AH-06-0318-C
Total/NA
Sediment
Moisture
400-151454-3
AH-02-0318-C
Total/NA
Sediment
Moisture
400-151454-4
AH-04-0318-C
Total/NA
Sediment
Moisture
400-151454-5
AH-05-0318-C
Total/NA
Sediment
Moisture
400-151454-6
AH-05-0318-C-DUP
Total/NA
Sediment
Moisture
Page 19 of 37
TestAmerica Pensacola
4/12/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 400-151454-1
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Lab Sample ID: MB 400-391552/1-A
Matrix: Sediment
Analysis Batch: 391473
MB MB
Analyte
Result Qualifier
C5-C8 Aliphatics
ND
C9-C10 Aromatics
ND
C9-C12 Aliphatics
ND
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 391552
RL
MDL
Unit
D Prepared Analyzed Dil Fac
2.7
2.7
mg/Kg
03/26/1814:00 03/26/1817:44 50
0.75
0.75
mg/Kg
03/26/1814:00 03/26/1817:44 50
1.4
1.4
mg/Kg
03/26/1814:00 03/26/1817:44 50
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
a,a,a-Trifluorotoluene (fid) 93
70- 130
03126118 14:00
03126118 17:44 50
a,a,a-Trifluorotoluene (pid) 93
70- 130
03126118 14:00
03126118 17:44 50
Lab Sample ID: LCS 400-391552/2-A
Client Sample ID:
■I■I�
Lab Control Sample
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 391473
Prep Batch: 391552
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
C5-C8 Aliphatics
15.0
13.9
mg/Kg
93
70 -130
C9-C10 Aromatics
2.50
2.58
mg/Kg
103
70 -130
C9-C12 Aliphatics
17.5
17.9
mg/Kg
102
70 -130
LCS LCS
Surrogate %Recovery Qualifier
a,a,a-Trifluorotoluene (fid) 96
a,a,a-Trifluorotoluene (pid) 95
Lab Sample ID: LCSD 400-391552/3-A
Matrix: Sediment
Analysis Batch: 391473
Analyte
C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
LCSD LCSD
Surrogate %Recovery Qualifier
a,a,a-Trifluorotoluene (fid) 93
a,a,a-Trifluorotoluene (pid) 92
Lab Sample ID: MB 400-391983/2
Matrix: Water
Analysis Batch: 391983
Limits
70-130
70-130
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 391552
Spike
LCSD
LCSD
%Rec. RPD
Added
Result
Qualifier Unit
D %Rec
Limits RPD Limit
15.0
14.6
mg/Kg
98
70 -130 5 25
2.50
2.66
mg/Kg
106
70 -130 3 25
17.5
19.1
mg/Kg
109
70 -130 7 25
Limits
70-130
70-130
Client Sample ID: Method Blank
Prep Type: Total/NA
MB
MB
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
C5-C8 Aliphatics
ND
26
26
ug/L
03/29/18 14:16
1
C9-C10 Aromatics
ND
7.0
7.0
ug/L
03/29/18 14:16
1
C9-C12 Aliphatics
ND
11
11
ug/L
03/29/18 14:16
1
MB
MB
Surrogate
%Recovery
Qualifier
Limits
Prepared Analyzed
Dil Fac
a,a,a-Trifluorotoluene (fid)
101
70- 130
03129118 14:16
1
a,a,a-Trifluorotoluene (pid)
102
70- 130
03129118 14:16
1
Page 20 of 37
TestAmerica Pensacola
4/12/2018

QC Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Lab Sample ID: LCS 400-391983/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 391983
Spike
LCS
LCS %Rec.
Analyte
Added
Result
Qualifier Unit D %Rec Limits
C5-C8 Aliphatics
300
297
ug/L 99 70 -130
C9-C10 Aromatics
50.0
53.7
ug/L 107 70 -130
C9-C12 Aliphatics
350
375
ug/L 107 70 -130
LCS LCS
Surrogate %Recovery Qualifier
Limits
a,a,a-Trifluorotoluene (fid) 100
70- 130
a,a,a-Trifluorotoluene (pid) 100
70- 130
Lab Sample ID: LCSD 400-391983/13
■I■I�
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 391983
Spike
LCSD
LCSD %Rec. RPD
Analyte
Added
Result
Qualifier Unit D %Rec Limits RPD Limit
C5-C8 Aliphatics
300
301
ug/L 100 70 -130 1 25
C9-C10 Aromatics
50.0
48.6
ug/L 97 70 -130 10 25
C9-C12 Aliphatics
350
372
ug/L 106 70 -130 1 25
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
a,a,a-Trifluorotoluene (fid) 108
70- 130
a,a,a-Trifluorotoluene (pid) 107
70- 130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Lab Sample ID: MB 400-391988/1-A
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 392564
Prep Batch: 391988
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
C19-C36 Aliphatics ND
3.2
3.2 mg/Kg 03/29/18 12:30 04/03/18 20:18 1
C9-C18 Aliphatics ND
3.2
3.2 mg/Kg 03/29/18 12:30 04/03/18 20:18 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
1-Chlorooctadecane 67
40 - 140
03/29/18 12:30 04103118 20:18 1
Lab Sample ID: MB 400-391988/1-A
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 392567
Prep Batch: 391988
Analyte
C11-C22 Aromatics
Surrogate
o-Terphenyl
2-Fluorobiphenyl
2-Bromonaphthalene
MB
MB
Result
Qualifier
ND
MB
MB
%Recovery
Qualifier
57
73
65
RL
MDL Unit D Prepared
Analyzed
Dil Fac
3.2
3.2 mg/Kg 03/29/18 12:30
04/04/18 01:18
1
Limits
Prepared
Analyzed
Dil Fac
40 - 140
03/29/18 12:30
04104118 01:18
1
40 - 140
03/29/18 12:30
04104118 01:18
1
40 - 140
03/29/18 12:30
04104118 01:18
1
TestAmerica Pensacola
Page 21 of 37 4/12/2018

QC Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons
(GC) (Continued)
Lab Sample ID: LCS 400-391988/2-A
Client Sample ID: Lab Control Sample
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 392564
Prep Batch: 391988
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
C19-C36 Aliphatics
26.7
13.7
mg/Kg
52 40 -140
C9-C18 Aliphatics
20.0
11.8
mg/Kg
59 40 -140
LCS LCS
Surrogate %Recovery Qualifier
Limits
1-Chlorooctadecane 59
40- 140
Lab Sample ID: LCS 400-391988/2-A
Client Sample ID: Lab Control Sample
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 392567
Prep Batch: 391988
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
C11-C22 Aromatics
56.7
34.7
mg/Kg
61 40 -140
LCS LCS
Surrogate %Recovery Qualifier
Limits
o-Terphenyl 56
40 - 140
2-Fluorobiphenyl 71
40 - 140
2-Bromonaphthalene 58
40 - 140
Lab Sample ID: 400-151454-2 MS
Client Sample ID: AH-06-0318-C
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 392564
Prep Batch: 391988
Sample Sample
Spike
MS
Ms
%Rec.
Analyte Result Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits
C19-C36 Aliphatics ND F1
32.7
9.00
F1
mg/Kg
28 40 -140
C9-C18 Aliphatics ND
24.5
10.0
mg/Kg
41 40 -140
MS MS
Surrogate %Recovery Qualifier
Limits
1-Chlorooctadecane 35 X
40- 140
Lab Sample ID: 400-151454-2 MS
Client Sample ID: AH-06-0318-C
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 392567
Prep Batch: 391988
Sample Sample
Spike
MS
Ms
%Rec.
Analyte Result Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits
C11-C22 Aromatics ND
69.4
31.1
mg/Kg
45 40 -140
MS MS
Surrogate %Recovery Qualifier
Limits
o-Terphenyl 42
40- 140
2-Fluorobiphenyl 72
40- 140
2-Bromonaphthalene 49
40 - 140
Lab Sample ID: 400-151454-2 MSD
Client Sample ID: AH-06-0318-C
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 392564
Prep Batch: 391988
Sample Sample
Spike
MSD
MSD
%Rec. RPD
Analyte Result Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
C19-C36 Aliphatics ND F1
32.8
13.3
mg/Kg
1T� 41 40 -140 39 50
TestAmerica Pensacola
Page 22 of 37 4/12/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 400-151454-1
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Lab Sample ID: 400-151454-2 MSD Client Sample ID: AH-06-0318-C
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 392564 Prep Batch: 391988
Sample Sample Spike MSD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
C9-C18 Aliphatics ND 24.6 13.6 mg/Kg 55 40 -140 30 50
Surrogate
MSD MSD
%Recovery Qualifier
Limits
1-Chlorooctadecane
47
40 - 140
Lab Sample ID: 400-151454-2 MSD
Matrix: Sediment
Analysis Batch: 392567
Sample Sample
Spike
Analyte
Result Qualifier
Added
C11-C22 Aromatics
ND
69.7
MSD MSD
Surrogate %Recovery Qualifier Limits
o-Terphenyl 50 40- 140
2-Fluorobiphenyl 76 40- 140
2-Bromonaphthalene 63 40 - 140
Lab Sample ID: MB 400-392483/1-A
Matrix: Water
Analysis Batch: 393045
F
Client Sample ID: AH-06-0318-C
Prep Type: Total/NA
Prep Batch:391988
MSD MSD %Rec. RPD
Result Qualifier Unit D %Rec Limits RPD Limit
37.2 mg/Kg 7 53 40 -140 18 50
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 392483
MB
MB
Analyte
Result
Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
C19-C36 Aliphatics
ND
0.050
0.050 mg/L
04/03/18 10:59
04/09/18 14:04 1
C9-C18 Aliphatics
ND
0.050
0.050 mg/L
04/03/18 10:59
04/09/18 14:04 1
MB
MB
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed Dil Fac
1-Chlorooctadecane
75
40- 140
04103118 10:59
04109118 14:04 1
Lab Sample ID: MB 400-392483/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 393049
Prep Batch: 392483
MB
MB
Analyte
Result
Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
C11-C22 Aromatics
ND
0.050
0.050 mg/L
04/03/18 10:59
04/09/18 19:14 1
MB
MB
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed Dil Fac
o-Terphenyl
66
40- 140
04103118 10:59
04109118 19:14 1
2-Fluorobiphenyl
66
40- 140
04103118 10:59
04109118 19:14 1
2-Bromonaphthalene
61
40 - 140
04103118 10:59
04109118 19:14 1
Lab Sample ID: LCS 400-392483/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 393045
Prep Batch: 392483
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec
Limits
C19-C36 Aliphatics
0.400
0.221
mg/L 55
40 -140
C9-C18 Aliphatics
0.300
0.135
mg/L 45
40 -140
TestAmerica Pensacola
Page 23 of 37 4/12/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 400-151454-1
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Lab Sample ID: LCS 400-392483/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 393045
Prep Batch: 392483 L
LCS LCS
Surrogate %Recovery Qualifier
Limits
1-Chlorooctadecane 74
40 -140
Lab Sample ID: LCS 400-392483/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 393049
Prep Batch: 392483
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
Aromatics
-
0.850
—
0.599 mg/L 70 40 -140
-C11-C22
LCS LCS
�
m
Surrogate %Recovery Qualifier
Limits
o-Terphenyl 72
40- 140
2-Fluorobiphenyl 74
40- 140
2-Bromonaphthalene 66
40 - 140
Lab Sample ID: LCSD 400-39248313-A
Client Sample ID: Lab Control Sample Dup C
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 393045
Prep Batch: 392483
Spike
LCSD LCSD %Rec. RPD
Analyte
Added
Result Qualifier Unit D %Rec Limits RPD Limit
C19-C36 Aliphatics
0.400
0.223 mg/L 56 40 -140 1 50
C9-C18 Aliphatics
0.300
0.135 mg/L 45 40 -140 0 50
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
1-Chlorooctadecane 69
40- 140
Lab Sample ID: LCSD 400-392483/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 393049
Prep Batch: 392483
Spike
LCSD LCSD %Rec. RPD
Analyte
Added
Result Qualifier Unit D %Rec Limits RPD Limit
C11-C22 Aromatics
0.850
0.502 mg/L 59 40 -140 18 50
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
o-Terphenyl 59
40 - 140
2-Fluorobiphenyl 65
40 - 140
2-Bromonaphthalene 58
40 - 140
Lab Sample ID: MB 400-392659/1-A
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 393044
Prep Batch: 392659
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
C19-C36 Aliphatics ND
3.2
3.2 mg/Kg 04/04/18 12:45 04/09/18 11:38 1
C9-C18 Aliphatics ND
3.2
3.2 mg/Kg 04/04/18 12:45 04/09/18 11:38 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
1-Chlorooctadecane 56
40- 140
04104118 12:45 04109118 11:38 1
TestAmerica Pensacola
Page 24 of 37 4/12/2018

QC Sample Results
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Lab Sample ID: MB 400-392659/1-A
Client Sample ID: Method Blank
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 393048
Prep Batch: 392659
MB
MB
Analyte Result
Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
C11-C22 Aromatics ND
3.2
3.2 mg/Kg 04/04/18 12:45 04/09/18 16:50 1
MB
MB
Surrogate %Recovery
Qualifier
Limits
Prepared Analyzed Dil Fac
o-Terphenyl 49
40 - 140
04104118 12:45 04109118 16:50 1
2-Fluorobiphenyl 62
40 - 140
04104118 12:45 04109118 16:50 1
2-Bromonaphthalene 52
40 - 140
04104118 12:45 04109118 16:50 1
Lab Sample ID: LCS 400-392659/2-A
Client Sample ID: Lab Control Sample
Matrix: Sediment
Prep Type: Total/NA
Analysis Batch: 393044
Prep Batch: 392659
Spike
LCS LCS %Rec. m
Analyte
Added
Result Qualifier Unit D %Rec Limits
C19-C36 Aliphatics
26.7
13.9 mg/Kg 52 40 -140
C9-C18 Aliphatics
20.0
12.5 mg/Kg 62 40 -140
LCS LCS
Surrogate %Recovery Qualifier
1-Chlorooctadecane 59
Lab Sample ID: LCS 400-392659/2-A
Matrix: Sediment
Analysis Batch: 393048
Analyte
C11-C22 Aromatics
Surrogate
LCS LCS
%Recovery Qualifier
o-Terphenyl
54
2-Fluorobiphenyl
70
2-Bromonaphthalene
62
Lab Sample ID: 400-151454-3 MS
Matrix: Sediment
Analysis Batch: 393044
Sample
Sample
Analyte
Result
Qualifier
C19-C36 Aliphatics
ND
F1
C9-C18 Aliphatics
ND
F1 F2
MS MS
Surrogate %Recovery Qualifier
1-Chlorooctadecane 19 X
Limits
40-140
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 392659
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
56.7 35.3 mg/Kg 62 40 -140
Limits
40 - 140
40 - 140
40 - 140
Client Sample ID: AH-02-0318-C
Prep Type: Total/NA
Prep Batch: 392659
Spike
MS
MS
%Rec.
Added
Result
Qualifier
Unit
D %Rec Limits
42.5
ND
F1
mg/Kg
# 0 40-140
31.9
5.82
F1
mg/Kg
3:� 18 40 -140
Limits
40-140
Lab Sample ID: 400-151454-3 MS Client Sample ID: AH-02-0318-C
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 393048 Prep Batch: 392659
Sample Sample Spike MS MS %Rec.
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits
C11-C22 Aromatics ND F1 F2 90.3 8.90 F1 mg/Kg ;1, 10 40 -140
TestAmerica Pensacola
Page 25 of 37 4/12/2018

QC Sample Results
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 400-151454-1
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Lab Sample ID: 400-151454-3 MS
Matrix: Sediment
Analysis Batch: 393048
MS
MS
Surrogate
%Recovery
Qualifier
Limits
o-Terphenyl
21
X
40-140
2-Fluorobiphenyl
68
40-140
2-Bromonaphthalene
55
40-140
Lab Sample ID: 400-151454-3 MSD
Matrix: Sediment
Analysis Batch: 393044
Sample
Sample
Spike
Analyte
Result
Qualifier
Added
C19-C36 Aliphatics
ND
F1
42.6
C9-Cl8 Aliphatics
ND
F1 F2
31.9
MSD
MSD
Surrogate
%Recovery
Qualifier
Limits
1-Chlorooctadecane
58
40-140
Lab Sample ID: 400-151454-3 MSD
Matrix: Sediment
Analysis Batch: 393048
Sample
Sample
Spike
Analyte
Result
Qualifier
Added
C11-C22 Aromatics
ND
F1 F2
90.5
MSD
MSD
Surrogate
%Recovery
Qualifier
Limits
o-Terphenyl
51
40 - 140
2-Fluorobiphenyl
70
40 - 140
2-Bromonaphthalene
56
40 - 140
Client Sample ID: AH-02-0318-C
Prep Type: Total/NA
Prep Batch: 392659
Client Sample ID: AH-02-0318-C C
Prep Type: Total/NA
Prep Batch: 392659
MSD MSD
%Rec. RPD
Result Qualifier
Unit
D %Rec Limits RPD Limit m
21.6
mg/Kg
51 40-140 NC 50
17.5 F2
mg/Kg
55 40 -140 100 50
Client Sample ID: AH-02-0318-C
Prep Type: Total/NA
Prep Batch: 392659
MSD MSD %Rec. RPD
Result Qualifier Unit D %Rec Limits RPD Limit
51.7 F2 mg/Kg 3� 57 ZIAO - 440 141 50
TestAmerica Pensacola
Page 26 of 37 4/12/2018

Lab Chronicle
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
F
TestAmerica Job ID: 400-151454-1
Client Sample ID: AH-07-0318-C
Lab Sample ID: 400-151454-1
Date Collected: 03/27/18 08:50
Matrix: Sediment
Date Received: 03/28/18 09:44
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis Moisture
1
391941
03/29/18 10:37 CAC TAL PEN
Client Sample ID: AH-07-0318-C
Lab Sample ID: 400-151454-1
Date Collected: 03/27/18 08:50
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 80.8
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
E:
Total/NA Prep 5035
6.318 g
15.00 mL
391552
03/29/18 13:00 MKA TAL PEN
Total/NA Analysis MAVPH
50
5 mL
5 mL
391473
03/29/18 23:44 MKA TAL PEN
Total/NA Prep 3546
15.07 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392564
04/03/18 21:07 TAJ TAL PEN
Total/NA Prep 3546
15.07 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392567
04/04/18 02:06 TAJ TAL PEN
Client Sample ID: AH-06-0318-C
Lab Sample ID: 400-151454-2
Date Collected: 03/27/18 09:30
Matrix: Sediment
Date Received: 03/28/18 09:44
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis Moisture
1
391941
03/29/18 10:37 CAC TAL PEN
Client Sample ID: AH-06-0318-C
Lab Sample ID: 400-151454-2
Date Collected: 03/27/18 09:30
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 81.0
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Prep 5035
5.2 g
15.00 mL
391552
03/29/18 13:00 MKA TAL PEN
Total/NA Analysis MAVPH
50
5 mL
5 mL
391473
03/30/18 00:44 MKA TAL PEN
Total/NA Prep 3546
15.09 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392564
04/03/18 20:38 TAJ TAL PEN
Total/NA Prep 3546
15.09 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392567
04/04/18 01:38 TAJ TAL PEN
Client Sample ID: AH-02-0318-C
Lab
Sample ID: 400-151454-3
Date Collected: 03/27/18 10:05
Matrix: Sediment
Date Received: 03/28/18 09:44
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis Moisture
1
391941
03/29/18 10:37 CAC TAL PEN
Page 27 of 37
TestAmerica Pensacola
4/12/2018

Lab Chronicle
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-02-0318-C
Lab Sample ID: 400-151454-3
Date Collected: 03/27/18 10:05
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 61.6
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Prep 5035
3.756 g
15.00 mL
391552
03/29/18 13:00 MKA TAL PEN
Total/NA Analysis MAVPH
50
5 mL
5 mL
391473
03/30/18 01:44 MKA TAL PEN
Total/NA Prep 3546
15.19 g
2.0 mL
392659
04/04/18 12:45 KLR TAL PEN
Total/NA Analysis MA-EPH
1
393044
04/09/18 12:16 TAJ TAL PEN
Total/NA Prep 3546
15.19 g
2.0 mL
392659
04/04/18 12:45 KLR TAL PEN
Total/NA Analysis MA-EPH
1
393048
04/09/18 17:28 TAJ TAL PEN
Client Sample ID: AH-04-0318-C
Lab Sample ID: 400-151454-4
Date Collected: 03/27/18 10:50
Matrix: Sediment
Date Received: 03/28/18 09:44
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis Moisture
1
391941
03/29/18 10:37 CAC TAL PEN
Client Sample ID: AH-04-0318-C
Lab Sample ID: 400-151454-4
Date Collected: 03/27/18 10:50
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 40.2
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Prep 5035
4.138 g
15.00 mL
391552
03/29/18 13:00 MKA TAL PEN
Total/NA Analysis MAVPH
50
5 mL
5 mL
391473
03/30/18 02:43 MKA TAL PEN
Total/NA Prep 3546
15.29 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392564
04/03/18 21:27 TAJ TAL PEN
Total/NA Prep 3546
15.29 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392567
04/04/18 02:26 TAJ TAL PEN
Client Sample ID: AH-05-0318-C
Lab Sample ID: 400-151454-5
Date Collected: 03/27/18 11:55
Matrix: Sediment
Date Received: 03/28/18 09:44
F Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis Moisture
1
391941
03/29/18 10:37 CAC TAL PEN
Client Sample ID: AH-05-0318-C
Lab Sample ID: 400-151454-5
Date Collected: 03/27/18 11:55
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 24.7
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Prep 5035
2.16 g
15.00 mL
391552
03/29/18 13:00 MKA TAL PEN
Total/NA Analysis MAVPH
50
5 mL
5 mL
391473
03/30/18 03:43 MKA TAL PEN
Total/NA Prep 3546
15.26 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392564
04/03/18 21:37 TAJ TAL PEN
Total/NA Prep 3546
15.26 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
TestAmerica Pensacola
Page 28 of 37
4/12/2018

Lab Chronicle
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-C
Date Collected: 03/27/18 11:55
Date Received: 03/28/18 09:44
F
TestAmerica Job ID: 400-151454-1
Lab Sample ID: 400-151454-5
Matrix: Sediment
Percent Solids: 24.7
Batch
Batch
Dil Initial
Final Batch
Prepared
Prep Type Type
Method
Run Factor Amount
Amount Number
or Analyzed Analyst Lab
Total/NA Analysis
MA-EPH
1
392567
04/04/18 02:36 TAJ TAL PEN
Client Sample ID: AH-05-0318-C-DUP
Date Collected: 03/27/18 11:58
Date Received: 03/28/18 09:44
F Batch Batch
Prep Type Type Method Run
Total/NA Analysis Moisture
Client Sample ID: AH-05-0318-C-DUP
Date Collected: 03/27/18 11:58
Date Received: 03/28/18 09:44
Lab Sample ID: 400-151454-6
Matrix: Sediment
L
Dil Initial Final Batch Prepared
Factor Amount Amount Number or Analyzed Analyst Lab
1 391941 03/29/18 10:37 CAC TAL PEN
Lab Sample ID: 400-151454-6
Matrix: Sediment
Percent Solids: 25.3
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA Prep
5035
1.572 g
15.00 mL
391552
03/29/18 13:00
MKA
TAL PEN
Total/NA Analysis
MAVPH
50
5 mL
5 mL
391473
03/30/18 04:43
MKA
TAL PEN
Total/NA Prep
3546
15.25 g
2.0 mL
391988
03/29/18 12:30
KLR
TAL PEN
Total/NA Analysis
MA-EPH
1
392564
04/03/18 21:47
TAJ
TAL PEN
Total/NA Prep
3546
15.25 g
2.0 mL
391988
03/29/18 12:30
KLR
TAL PEN
Total/NA Analysis
MA-EPH
1
392567
04/04/18 02:45
TAJ
TAL PEN
Client Sample ID: EB-02-0318
Lab Sample ID: 400-151454-7
Date Collected: 03/27/18 12:50
Matrix: Water
Date Received: 03/28/18 09:44
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA Analysis
MAVPH
1
5 mL
5 mL
391983
03/29/18 19:46
MKA
TAL PEN
Total/NA Prep
3520C
931.2 mL
2.0 mL
392483
04/03/18 10:59
NTH
TAL PEN
Total/NA Analysis
MA-EPH
1
393045
04/09/18 14:33
TAJ
TAL PEN
Total/NA Prep
3520C
931.2 mL
2.0 mL
392483
04/03/18 10:59
NTH
TAL PEN
Total/NA Analysis
MA-EPH
1
393049
04/09/18 19:44
TAJ
TAL PEN
Client Sample ID: Method Blank
Lab Sample
ID: MB
400-391552/1-A
Date Collected: N/A
Matrix:
Sediment
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA Prep
5035
15.00 g
15.00 mL
391552
03/26/18 14:00
MKA
TAL PEN
Total/NA Analysis
MAVPH
50
5 mL
5 mL
391473
03/26/18 17:44
MKA
TAL PEN
Page 29 of 37
TestAmerica Pensacola
4/12/2018

Lab Chronicle
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
F
TestAmerica Job ID: 400-151454-1
Client Sample ID: Method Blank
Lab Sample ID: MB 400-391983/2
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis
MAVPH
1
5 mL
5 mL
391983
03/29/18 14:16
MKA TAL PEN
Client Sample ID: Method
Blank
Lab Sample ID: MB
400-391988/1-A
Date Collected: N/A
Matrix: Sediment
Date Received: N/A
F
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
3546
15.00 g
2.0 mL
391988
03/29/18 12:30
KLR TAL PEN
Total/NA Analysis
MA-EPH
1
392564
04/03/18 20:18
TAJ TAL PEN
Total/NA Prep
3546
15.00 g
2.0 mL
391988
03/29/18 12:30
KLR TAL PEN
Total/NA Analysis
MA-EPH
1
392567
04/04/18 01:18
TAJ TAL PEN
Client Sample ID: Method
Blank
Lab Sample ID: MB
400-392483/1-A
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
3520C
1000 mL
2.0 mL
392483
04/03/18 10:59
NTH TAL PEN
Total/NA Analysis
MA-EPH
1
393045
04/09/18 14:04
TAJ TAL PEN
Total/NA Prep
3520C
1000 mL
2.0 mL
392483
04/03/18 10:59
NTH TAL PEN
Total/NA Analysis
MA-EPH
1
393049
04/09/18 19:14
TAJ TAL PEN
Client Sample ID: Method
Blank
Lab Sample ID: MB
400-392659/1-A
Date Collected: N/A
Matrix: Sediment
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
3546
15.00 g
2.0 mL
392659
04/04/18 12:45
KLR TAL PEN
Total/NA Analysis
MA-EPH
1
393044
04/09/18 11:38
TAJ TAL PEN
Total/NA Prep
3546
15.00 g
2.0 mL
392659
04/04/18 12:45
KLR TAL PEN
Total/NA Analysis
MA-EPH
1
393048
04/09/18 16:50
TAJ TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-391552/2-A
Date Collected: N/A
Matrix: Sediment
Date Received: N/A
Batch
Batch
Dil Initial
Final Batch
Prepared
Prep Type Type
Method Run
Factor Amount
Amount Number
or Analyzed
Analyst Lab
Total/NA Prep
5035
15.00 g
15. 00 mL 391552
03/ 66/18 14:00
MKA TAL PEN
Total/NA Analysis
MAVPH
50 5 mL
5 mL 391473
03/26/18 18:44
MKA TAL PEN
Page 30 of 37
TestAmerica Pensacola
4/12/2018

Lab Chronicle
Client: Athena Technologies, Inc
TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-391983/4
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch Batch Dil Initial
Final Batch Prepared
Prep Type Type Method Run Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis MAVPH 1 5 mL
5 mL 391983 03/29/18 17:46 MKA TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-391988/2-A
Date Collected: N/A
Matrix: Sediment
Date Received: N/A
F-
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Prep
3546
Total/NA
Analysis
MA-EPH
Total/NA
Prep
3546
Total/NA
Analysis
MA-EPH
Client Sample ID: Lab Control Sample
Date Collected: N/A
Date Received: N/A
Dil
Initial
Final
Batch
Prepared
L
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
15.00 g
2.0 mL
391988
03/29/18 12:30
KLR
TAL PEN
1
392564
04/03/18 20:28
TAJ
TAL PEN
15.00 g
2.0 mL
391988
03/29/18 12:30
KLR
TAL PEN
1
392567
04/04/18 01:28
TAJ
TAL PEN
Lab Sample ID: LCS 400-392483/2-A
Matrix: Water
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Prep
3520C
1000 mL
2.0 mL
392483
04/03/18 10:59
NTH
TAL PEN
Total/NA
Analysis
MA-EPH
1
393045
04/09/18 14:14
TAJ
TAL PEN
Total/NA
Prep
3520C
1000 mL
2.0 mL
392483
04/03/18 10:59
NTH
TAL PEN
Total/NA
Analysis
MA-EPH
1
393049
04/09/18 19:24
TAJ
TAL PEN
Client Sample ID: Lab
Control Sample
Lab Sample ID: LCS
400-392659/2-A
Date Collected:
N/A
Matrix:
Sediment
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Prep
3546
15.00 g
2.0 mL
392659
04/04/18 12:45
KLR
TAL PEN
Total/NA
Analysis
MA-EPH
1
393044
04/09/18 11:47
TAJ
TAL PEN
Total/NA
Prep
3546
15.00 g
2.0 mL
392659
04/04/18 12:45
KLR
TAL PEN
Total/NA
Analysis
MA-EPH
1
393048
04/09/18 16:59
TAJ
TAL PEN
Client Sample ID: Lab Control Sample Dup
Lab Sample ID: LCSD 400-391552/3-A
Date Collected: N/A
Matrix: Sediment
Date Received: N/A
Batch
Batch Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
5035
15.00 g
15. 00 mL
391552
03/ 66/18 14:00
MKA TAL PEN
Total/NA Analysis
MAVPH 50
5 mL
5 mL
391473
03/27/18 12:12
MKA TAL PEN
Page 31 of 37
TestAmerica Pensacola
4/12/2018

Lab Chronicle
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
F
TestAmerica Job ID: 400-151454-1
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-391983/13
Date Collected: N/A Matrix: Water
Date Received: N/A
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis MAVPH 1 5 mL 5 mL 391983 03/30/18 10:48 MKA TAL PEN
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-392483/3-A
Date Collected: N/A Matrix: Water
Date Received: N/A F-
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Prep
3520C
Total/NA
Analysis
MA-EPH
Total/NA
Prep
3520C
Total/NA
Analysis
MA-EPH
Client Sample ID: AH-06-0318-C
Date Collected: 03/27/18 09:30
Date Received: 03/28/18 09:44
Dil
Initial
Final
Batch
Prepared
L
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
1000 mL
2.0 mL
392483
04/03/18 10:59
NTH
TAL PEN
1
393045
04/09/18 14:24
TAJ
TAL PEN
1000 mL
2.0 mL
392483
04/03/18 10:59
NTH
TAL PEN
1
393049
04/09/18 19:34
TAJ
TAL PEN
Lab Sample ID: 400-151454-2 MS
Matrix: Sediment
Percent Solids: 81.0
Batch Batch
Prep Type Type Method
Dil
Run Factor
Initial
Amount
Final
Amount
Batch
Number
Prepared
or Analyzed Analyst Lab
Total/NA Prep 3546
15.11 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392564
04/03/18 20:47 TAJ TAL PEN
Total/NA Prep 3546
15.11 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392567
04/04/18 01:47 TAJ TAL PEN
Client Sample ID: AH-06-0318-C
Lab Sample ID: 400-151454-2 MSD
Date Collected: 03/27/18 09:30
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 81.0
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Preep 3546
15.05 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392564
04/03/18 20:57 TAJ TAL PEN
Total/NA Prep 3546
15.05 g
2.0 mL
391988
03/29/18 12:30 KLR TAL PEN
Total/NA Analysis MA-EPH
1
392567
04/04/18 01:57 TAJ TAL PEN
Client Sample ID: AH-02-0318-C
Lab Sample ID: 400-151454-3 MS
Date Collected: 03/27/18 10:05
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 61.6
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Prep
3546
15.29 g
2.0 mL
392659
04/ 44/18 12:45
KLR
TAL PEN
Total/NA
Analysis
MA-EPH
1
393044
04/09/18 11:57
TAJ
TAL PEN
Total/NA
Prep
3546
15.29 g
2.0 mL
392659
04/04/18 12:45
KLR
TAL PEN
Total/NA
Analysis
MA-EPH
1
393048
04/09/18 17:09
TAJ
TAL PEN
Page 32 of 37
TestAmerica Pensacola
4/12/2018

Lab Chronicle
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 400-151454-1
Client Sample ID: AH-02-0318-C
Lab Sample ID: 400-151454-3 MSD
Date Collected: 03/27/18 10:05
Matrix: Sediment
Date Received: 03/28/18 09:44
Percent Solids: 61.6
Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Prep 3546
15.26 g
2.0 mL
392659 04/04/18 12:45 KLR TAL PEN
Total/NA Analysis MA-EPH
1
393044 04/09/18 12:06 TAJ TAL PEN
Total/NA Prep 3546
15.26 g
2.0 mL
392659 04/04/18 12:45 KLR TAL PEN
Total/NA Analysis MA-EPH
1
393048 04/09/18 17:18 TAJ TAL PEN
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Page 33 of 37
TestAmerica Pensacola
4/12/2018

Method Summary
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Method Method Description Protocol Laboratory
MAVPH Massachusetts - Volatile Petroleum Hydrocarbons (GC) MA DEP TAL PEN
MA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC) MA DEP TAL PEN
Moisture Percent Moisture EPA TAL PEN L
Protocol References:
EPA = US Environmental Protection Agency
MA DEP = Massachusetts Department Of Environmental Protection
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TestAmerica Pensacola
Page 34 of 37 4/12/2018

Accreditation/Certification Summary C
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Laboratory: TestAmerica Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW) State Program 4 314 12-31-18
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
Analysis Method Prep Method Matrix Analyte
Moisture Sediment Percent Moisture
Moisture Sediment Percent Solids
Laboratory: TestAmerica Pittsburgh
The accreditations/certifications listed below are applicable to this report.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW) State Program 4 434 12-31-18
TestAmerica Pensacola
Page 35 of 37 4/12/2018

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Page 36 of 37
4/12/2018

Client: Athena Technologies, Inc
Login Number: 151454
List Number: 1
Creator: Perez, Trina M
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
0.0°C IR-7
Job Number: 400-151454-1
List Source: TestAmerica Pensacola
TestAmerica Pensacola
Page 37 of 37 4/12/2018