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HomeMy WebLinkAboutWQ0000455_Residual Annual Report 2015_201602260 2015 ANNUAL REPORT LAND APPLICATION PROGRAM LEWIS FARMS AND LIQUID WASTE, INC. PERMIT #WQ0000455 Prepared For: Lewis Farms and Liquid Waste, Inc. 8155 Malpass Corner Road Currie, North Carolina 28435 Compiled By: Willcox & Mabe Soil Solutions, PLLC 1205 West Bessemer Avenue, Suite 202 Greensboro, North Carolina 27408 February 2016 willcox&mabe SOIL SOLUTIONS February 25, 2016 NCDEQ-DWR 512 North Salisbury Street, Room 640A Raleigh, North Carolina 27604 Attention: Non -Discharge Permitting Unit Reference: 2015 LAND APPLICATION ANNUAL REPORT Lewis Farms and Liquid Waste, Inc. Permit No. WQ0000455 WMSS Project No. 15-20 Ph: 01 Non -Discharge Permitting Unit: Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting requirements as specified in the above referenced permit on behalf of Lewis Farms .and Liquid Waste, Inc. (Lewis Farms). WMSS compiled this report using data gathered during the compliance year by Lewis Farms. This data includes: 1) certification form, 2) residuals analyses and pathogen / vector data, 3) application summaries and field loading rate reports, and 4) soil analyses. If there is any further information required or questions regarding this annual report please do not hesitate to contact Lewis Farms or WMSS for further assistance. Sincerely, Willcox & Mabe Soil Solutions, PLLC Martin Mabe NC Land Application/Residuals Operator #22753 Enclosures Shared/WMSS Projects/2015/15-20 Lewis Farms/2015 Annual Report/2015 ANNUAL REPORT.doc Willcox & Mabe Soil Solutions, PLLC / 1205 W. Bessemer Avenue, Suite 202 / Greensboro, NC 27408 / Rob 336.339.9128 or Martin 336.312:1396 /www.willeoxmabesoil.com TABLE OF CONTENTS SECTION NO. TITLE I Certification Form II Residuals Analyses & Pathogen / Vector Attraction Data III 2015 Application Summary and Field Loading Rate Reports IV Soil Analysis CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0000455 County: Pender Year: 2015 Facility Name (as shown on permit): Lewis Farms and Liquid Waste, Inc. Land Application Operator: Mr. Wesley Wooten Phone: 910-283-5444 Land application of residuals as allowed by the permit occurred during the past calendar year? El Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the —permit: 17 Total number of fields utilized for land appl ication during the year: 14 I Total amount of dry tons applied during the year for all application sites: 374.08 Total number of acres utilizes for land application during the year: 325.40 Part B - Annual Compiance Statement: Y Facility was compliant during calendar year 2015 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6..0 or the limit specified in the permit. w 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All .other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. I 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All,general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). x 8) All monitoring and reporting requirements in 15A NCAC 02T .1 111 were complied with (applicable to 40 CFR Part 503 regulated facilities). I 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Mr. Wesley Wooten, President a4 eZ� 2—Zev—/6 Permittee Name and Title (type or print) Signat re of Permittee Date ;E Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from PermitteeENRd Preparer) er) (12/2006 • Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)) RESIDUAL ANALYSES TCLP ANALYSES IF REQUIRED AND PATHOGEN AND VECTOR ATTRACTION REDUCTION ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding laboratory analysis. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number W00000455 Facility Name Lewis Farms and Liquid Waste, Inc. NPDES # See Below WWTP Name See Below 2015 DATA RESIDUAL ANALVSIS DATA Laboratory 1 Envirochem 2 Environment 1 3 NPDES # WQ0000193 NCO065480 W00033770 W00018755ENC1021610 VI-25-10 WQ0022052 W00032115 NC0003344 NCO030813 WWTP Name Bald Head Island Beau Rivage Carolina Plant. Castle Baykton Emerald Plantation Hampstead Pines Ham stead Town House of Raeford Kenwood Composited / Grab 03/30/15 02/16/15 07/29/15 11/30/158/15 12/14/15 12/08/15 12/16/15 03/03/15 11/23/15 Percent Solids oAowuerene i__n._ 3.31 A_...._ -A% 1.45 1.89 2.37 - 18 1. An I 1.16 1.16 1.65 1.72 Arsenic 3.05 6.76 2.50 41.40 4.59 39.90 41.80 33.90 - 5.88 28.90 Cadmium 3.05 6.76 0.96 41.40 4.59 39.90 41.80 33.90 5.88 28.90 Copper 477.00 289.00 86.00 389.00 304.00 1,350.00 186.00 845.00 207.00 508.00 Lead 3.05 7.93 3.80 41.40 23.40 39.90 41.80 33.90 5.88 28.90 Mercury 0.61 4.78 0.10 012 1.98 1.39 1.64 0.86 1.04 1.28 Molybdenum 3.29 6.76 5.00 41.40 4.59 39.90 41.80 33.90 6.06 28.90 Nickel 13.20 10.30 5.00 41.40 11.00 39.90 41.80 33.90 18.30 28.90 Selenium 3.05 6.76 5.00 41.40 4.59 39.90 41.80 33.90 6.42 28.90 Zinc 1,080.00 641.00 2,141.00 1,630.00 761.00 709.00 1,500.00 1,170.00 236.00 1,620.00 TKN 15,700.00 82,000.00 29,991.00 39,900.00 2,880.00 22,200.00 78,400.00 26,500.00 68,900.00 2,430.00 Ammonia -Nitrogen 151.00 4,170.00 3,752.00 905.00 4,620.00 4,220.00 5,890.00 7,440.60 4,520.00 2,320.00 Nitrate -Nitrogen 1 1,880.00 1 115.00 1 15.43 1 31.20 0.50 3.78 98.50 5.19 29.40 65.10 Total Phosphorus 1 32,000.00 1 39,500.00 1 25,905.00 1 13,700.00 350.00 10,800.00 1 21,900.00 13,600.00 18,300.00 1 513.00 RESIDUAL ANALVSIS DATA NPDES # WQ0030088 NCO026611 NCO042251 NCO030406 NCO022462 W00029475 WQ0023261 NCO047759 NCO057703 Co, Health Dept. WWTP Name Majestic Oaks Morehead City Pander HS Riverbend Sherwood MHP Sterling Farms Swansboro Taylor ExL Care The Cape Topsail Greens Composited / Grab 12/03/15 02/24/15 1 12/09/15 12/15/15 04/01115 12/10/15 08/11/15 01/13/15 02/16/05 07/02/15 Percent Solids 0.32 22.2 1 0.47 1.72 1.37 0.43 2.15 1.03 1.74 1.94 Arsenic 2.50 4.31 20.90 29.10 6.28- 21.60 23.30 2.50 5.58 4.85 Cadmium 0.71 4.31 7.23 29.10 6.28 7.44 23.30 0.63 5.58 4.85 Copper 381.00 744.00 219.00 808.00 317.00 258.00 426.00 1,325.00 260.00 147.00 Lead 6.50 11.90 105.00 29.10 13.30 110.00 23.30 41.00 10.40 8.50 Mercury 0.84 1.43 2.13 1.16 1.46 4.42 2.90 4.10 0.43 0.25 Molybdenum 8.00 4.31 7.87 29.10 6.28 8.14 23.30 5.00 5.58 4.85 Nickel 21.00 9.78 105.00 29.10 8.54 110.00. 23.30 13.00 15.10 6.70 Selenium 5.00 5.28 29.40 29.10 6.28 30.50 23.30 5.00 7.01 4.85 Zinc 795.00 929.00 160.00 785.00 788.00 5,910.00 4,210.00 967.00 586.00 773.00 TKN 59,927.00 .22,200.00 21,200.00 48,900.00 3,290.00 64,700.00 47,600.00 25,784.00 55,300.00 54,200.00 Ammonia -Nitrogen 603.00 546.00 3,490.00 407.00 2,840.00 1,090.00 1,670.00 458.00 4,580.00 3,720.00 Nitrate -Nitrogen 3.98 1,100.00 5,760.00 8.23 42.50 418.00 8,980.00 12.42 11.40 7,000.00 Total Phosphorus 36,265.00 18,800.00 6,900.00 20,000.00 848.00 27,600.00 26,900.00 1 7,108.00 1 24,700.00 19,300.00 Page 1 of 2 RESIDUAL ANALYSIS DATA NPDES# I NCO021342 WWTP Name Trenton Composited / Grab 07/02/16 Percent Solids 10.72 PARAMFTFRR rmn1kn dm wnrnh#1 Arsenic 2.50 Cadmium 0.50 Copper 31.00 Lead 6.60 Mercury 0.01 Molybdenum 5.00 Nickel 5.00 Selenium 5.00 Zinc 107.00 TKN 7,083.00 Ammonia -Nitrogen 477.00 Nitrate -Nitrogen 61.70 Total Phosphorus 2,306.00 Page 2 of 2 X N/A due to number of sources (SIGNATURE OF PREPARER) DATE I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 30, 2015 Bald Head Island Permit No. WQ0000455 Mineralization Rate 0.30 3.31 % Solids 6.44 DH Nitrogen (TKN) 1.570 15,700.000 31.400 Phosphorus 3.200 32,000.000 64.000 Potassium 0.230 2,300.000 4.600 PAN (injected)* 0.670 6,695.700 13.391 PAN (surface)* 0.662 6,620.200 13.240 Ammonia Nitrogen 0.015 151.000 0.302 Calcium 1.670 16,700.000 33.400 Calcium Carbonate E . --- --- --- Magnesium --- 5,560.000 11.120 Sodium --- 2,440.000 4.880 Sulfur --- --- --- Nitrate N / Nitrite N --- 1,880.000 3.760 Barium --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 80,100.00 160.200 Arsenic --- 3.05 0.006 Cadmium --- 3.05 0.006 Chromium --- 24.400 --- Copper --- 477.00 0.954 Lead --- 3.05 0.006 Mercury --- 0.61 0.001 Molybdenum --- 3.29 0.007 Nickel --- 13.20 0.026 Selenium --- 3.05 0.006 Zinc --- 1,080.00 2.160 Environmental Chemists, Inc. # 2015-03800 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Ienviroichem ANALYTICAL & CONSULTING CHEMISTS The Village Of Bald Head Island 106 Lighthouse Wynd Bald Head Island NC 28461 Attention: David Suther Lab ID Sample ID: BHI Sludge 15-08757 Site: Sludge Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax Test Method Sludge Residuals Aluminum EPA 200.7 Arsenic EPA 200.7 Cadmium EPA 200.7 Calcium EPA 200.7 Chromium EPA 200.7 Copper EPA 200.7 Lead EPA 200.7 Magnesium EPA 200.7 Molybdenum EPA 200.7 Nickel EPA 200.7 Potassium EPA 200.7 Selenium EPA 200.7 Sodium EPA 200.7 Zinc EPA200.7 Ammonia Nitrogen EPA350.1 Reporting limit elevated due to matrix interference. info@environmentalchemists.com Date of Report: Apr 17, 2015 Customer PO #: Customer ID: 08100149 Report #: 2015-03800 Project ID: Sludge Collect Date/Time Matrix Sampled by 3/30/2015 9:25 AM Solid/Sludge David Suther Results Date Analyzed 80100 mg/kg 04/15/2016 <3.05 mg/kg 04/08/2015 <3.05 mg/kg 04/07/2015 16700 mg/kg 04/02/2015 24.4 mg/kg 04107/2015 477 mg/kg 04/07/2015 <3.05 mg/kg 04/07/2015 5560 mg/kg 04/02/2015 3.29 mg/kg 04/07/2015 13.2 mg/kg 04/07/2015 2300 mg/kg 04/02/2015 <3.05 mg/kg 04/07/2015 2440 mg/kg 04/02/2015 1080 mg/kg 04/07/2015 <151 mg/kg 04/13/2015 Total Kjeldahl Nitrogen (TKN) EPA361.2 15700mg/kg 04110/2015 Nitrate+Nitrite-Nitrogen EPA353.2 1880 mg/kg 04/13/2015 Total Solids.(%) SM 2540 s 3.31 % 03/30/2015 pH SM 4500 H s 6.44 units 04/16/2015 Total Phosphorus SM4500 P F 32000 mg/kg 04/10/2016 Mercury SW848 74718 <0.610 mg/kg 04/15/2015 Report #.: 2015-03800 Page 1 of 3 enviroehem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 i, 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com The Village Of Bald Head Island Date of Report: Apr 17, 2015 106 Lighthouse Wynd Customer PO #: Bald Head Island NC 28461 Customer 1D: 08100149 Attention: David Suther Report #• 2015-03800 Project ID: Sludge Lab ID Sample ID: BHI Sludge Collect Date/Time Matrix Sampled by 15-08758 Site: 1 3/30/2015 9:30 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.37 % 04/01/2015 Fecal Density SM 9221C E MPN 24 hr503 32641 MPN/g 03/31/2015 Lab ID Sample iD: BHI Sludge Collect Date/Time Matrix Sampled by 15-08759 Site: 2 3/30/2015 9:33 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.29 % 04/01/2015 Fecal Density SM92210EMPN 24hr503 51672MPN/g 03/31/2015 Lab ID Sample ID: BHI Sludge Collect DatelTime Matrix Sampled by 15-08760 Site: 3 3/30/2015 9:35 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids {%) SM 2540a 3.27 % 04/01/2015 Fecal Density SM 9221C E MPN 24 hr 503 152P06 MPN/g 03/31/2015 Lab ID Sample ID: BHI Sludge Collect Daterrime Matrix Sampled by .. 15-08761 Site: 4 3/30/2015 9:36 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.34 % 04/01/2015 Fecal Density SM 9221C E MPN 24 hr 503 . 71857 MPN1g 03/31/2015 Lab ID Sample ID: BHI Sludge Collect Date/Time Matrix Sampled by 15-08762 Site: 5 3/30/2015 9:38 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.24 % 04/01/2015 Fecal Density SM 9221C E MPN 24 hr 503 52470 MPN/g 03/31/2015 Report *: 2015-03800 Page 2 of 3 Environmental Chemists, Inc. 1 envirochem 6602 Windmill Way, Wilmington, NC 28405 • .910.392.0223 Lab • 910.392.4424 Fax — © 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.coin The Village Of Bald Head Island Date of Report: Apr 17, 2015 106 Lighthouse Wynd Customer PO #: Bald Head Island NC 28461 Customer ID: 08100149 Attention: David Suther Report #: 2015-03800 Project ID: Sludge Lab ID Sample ID: BH1 Sludge Collect DatelTime Matrix Sampled by 15-08763 Site: 6 3/30/2015 9:41 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 8 3.34 % 04/01/2015 Fecal Density SM 9221C E MPN 24 hr 503 149701 MPN/g 03/3112015 -� Lab ID Sample ID: BHI Sludge Collect Date/Time Matrix- Sampled by 15-08764 Site: 7 i 3/30/2015 9:44 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM2540 B 3.28 % 04/01/2015 Fecal Density SM 9221C E MPN 24 hr 503 51830 MPN/g 03/31/2015 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report tt 2015-03800 , Page 3 of 3 ENVIRONMENTAL CHEMISTS, INC Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 6602 Windmill Way Wilmington, NC 284( OFFICE: 910-392-0223 FAX 910-39244, info@environmentatchemists.com 93 COLLECTION AND CHAIN OF CUSTODY CLIENT: ) � li tr, PROJECT NAME:. ��u REPORT N0: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONEIFAX: COPY TO• email: Ramnlarl Rv- / .,... RAMPI F TVPF-1 = Infh,anf_ F = Ffflnanf W = Wolf AT = Rfraam An = Rnil .RI = Rh,rina nthar- Sample Identification Collection am E c o E o ef9 `o o W cog PRESERVATION ANALYSIS REQUESTED Date Time Temp z o c o o Llu, 3 ;3 C P fi c G G } C13.3 G G I G G k7G i G G C P 7(o �- G G G � G G 7S—? 1� AU g2 -4; -�f G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: -w- - v Accepzea: v r< 1eGLea: r%= U0'�TT.. Delivered By: Received By: � �"`t� •-.c/J Date: 3 l Time:.�'--- Comments: T TURNAROUND: LEWIS FARMS WQ0000455 Bald Head Island Fe6al Coliform MPNpergram' 'Log 03/30/15 32,641 4.5138 03/30/15 51,672 4.7133 03/30/15 152,906 5.1844 03/30/15 71,857 4.8565 03/30/15 52,470 4.7199 03/30/15 149,701 5.1752 03/30/15 51,830 4.7146 Total 1 33.8776 Average 4.8397 Geometric Mean 69,129 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction requirement. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Fauns & Liquid Waste, htc WQ Permit Number. WQ0000455 _. W W11' Names Bald head blatui NpDES Nuen6er; __ WQ0000133 Monitoring period: Bront UUZOIS To 12/31/2015 P2th0Nn Reduction (I5A N[`.AC 112T -- - - .%. ++.wow aa�sa acatcvea nou aimmanve mod: Class A: t. A time/ten) ❑ Alt 13 {A Tneatrneni) ❑ Alt C 'or?estia } ❑ AIt.) (No Prior Test) Q Process to Further Reduce Patho en ❑ liable to a[tert+afive erfotmed Class A o indicate "Process to FurtherReftce Pathogens"; Cann ❑ Heat D ❑ Hest Treatment ❑ Thermo bilic ❑ Beta ❑ Gamma Ray ❑ Pasteurization ❑ :`:,:`" ; : ">'::='�:: ` ;::; :>«' : •{ • Class D: Alt. (1) FecaI Densi p Alt. 121 Process to Si ificang R.educe I Psitho c ❑ liable to alternative perfonned Class B only) indicate -Process to S 0can Reduce path ens": Stabilimtion ❑ Air Dryine ❑ I Aerobic Digestion ❑'o ):,:33�:r:; i ,':•.<niY:f .....:•.;•?�.Co:m ;..>.;..1:'.❑ Anaerobic l:::,': f•:::[�.3:�'.:S...S.y.i}'+•..,5,•.`.M 13 . .. :... : v... .�, •. .:.: {.,.:'?, k..: • .v.....,..v...: :.......:.� :•;..5,'i :ti :�::: � v-<:. ire •":'•::! If applicable to alternative Performed Class A (lass B or complete the following monitoring data: ftarnew Allowable Level Padtogen Density XmberojFrrgnency Sample Geo. Mean im Units in Sludge of Analysis Type Tech- 2 th0 to power a[hem 32,6a1 smmmce s9,129 152,906 MPN/g 0 Annual Grab per stem oFecal Coliform total solids FU 1000 mpn per gram oftotel solid (dry wet Salmonella taia 3 MPId per 4 -grams (in lieu of fecal total solid (dry colifotm wet t ector Attraction Reduction (15A WOW_ --a ceroty, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction rquirement in 15A NCAC 02T 1107 have been met " ❑ I certify, under penalty of law, that the pathogen r+equtnaments in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been weL" (Please note if you check this statement attach an explanation why you have not met one or both of the "mu some under my direction and supervision in accordance with the system r _ designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment.' David Suther, ORC Wesley Wooten, president Pmparer Name and Title (type ria#) Land Applr N d Title (ifapplicablc)(type or print) Sigtmptte of Prepar+ee Date Si of Land Applier (if applicable) Date 'Prepater is defined in 40 CFR fart 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (120W) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: February 16, 2015 Beau Riva¢e 1.45 % Solids 6.82 pH Permit No. Nitrogen (TKN) 8.200 82,000.000 164.000 Phosphorus 3.950 39 500.000 79.000 Potassium 0.530 5,300.000 10.600 PAN (injected)* 2.763 27,634.000 55.268 PAN (surface)* 2.555 25,549.000 51.098 Ammonia Nitrogen 0.417 4,170.000 8.340 Calcium 2.090 20,900.000 41.800 Calcium Carbonate E . --- --- --- Magnesium --- 3,240.000 6.480 Sodium --- 3,900.000 7.800 Sulfur --- --- Nitrate N / Nitrite N --- 115.000 0.230 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 2,030.00 4.060 Arsenic --- 6.76 0.014 Cadmium --- 6.76 0.014 Chromium --- 9.170 --- Copper - 289.00 0.578 Lead --- 7.93 0.016 Mercury --- 4.78 0.010 Molybdenum - 6.76 0.014 Nickel --- 10.30 0.021 Selenium --- 6.76 0.014 Zinc --- 641.00 1.282 Environmental Chemists, Inc. # 2015-01935 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. envirochem 6602 Windmill Way - Wilmington, NC 28405 ® (910) 392-0223 (Lab) - (910) 392-4424 (lax) 710 Bowsertown Road - Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Aqua America of North Carolina Date of Report: Feb 27, 2015 251 Merchants Circle Bldg 24-1 Customer PO #: Hampstead NC 28443 Customer ID: 08110027 Attention: Don Williams Report #: 2015-01935 Project ID: Beau Rivage WWTP Lab ID Sample ID: Collect DateITime Matrix Sampled by 15-04356 Site: Beau Rivage 2/16/2015 9:45 AM Solid/Sludge Will Coggins ( Test Method Results Date Analyzed (— Sludge Residuals Aluminum EPA200.7 2030 mg/kg 02/24/2015 Arsenic EPA200.7 <6.76 mg/kg 02/23/2015 Cadmium EPA200.7 <6.76 mg/kg 02/20/2015 Calcium EPA200.7 20900 mg/kg 02/25/2015 Chromium EPA200.7 9.17mg/kg 02/20/2015 Copper EPA200.7 289mg/kg 02/20/2015 Lead EPA200.7 7.93 mg/kg 02/20/2016 Magnesium EPA200.7 3240 mg/kg 02/25/2015 j Molybdenum EPA200.7 <6.76 mg/kg 02/20/2015 Nickel EPA200.7 10.3 mg/kg 02/20/2015 Potassium EPA200.7 6300 mg/kg 02/25/2015 Selenium EPA200.7 <6.76 mg/kg 02120/2015 i - Sodium EPA2oo.7 3900mg/kg 02/25/2015 Zinc EPA200.7 641 mg/kg 02/20/2015 Ammonia Nitrogen EPA 350.1 4170 mg/kg 02/23/2015 Total Kjeldahl Nitrogen (TKN) EPA 3512 82000 mg/kg 02/20/2015 Nitrate+Nitrite-Nitrogen EPA$53.2 115mg/kg 02/19/2016 r Total Solids (%) SM 2540 B 1.45 % 02/16/2015 j_ pH SM4500 H B 6.82 units 02/18/2015 F Total Phosphorus SM4500 P F 39500 mg/kg 02/23/2015 I_ Mercury SWW 7471E 4.78 mg/kg 02/13/2015 - Report#:: 2015-01935 Page 1 of l i I4 r-7�- :'qqql ANALYTICAL & CONSULTING CHEMISTS Aqua America of North Carolina ` 251 Merchants Circle Bldg 24-1 Hampstead NC 28443 Attention: Don Williams Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-M4 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473.5702 NCDENR: DWQ CERTIFICATE #94. DLS CERTIRCATE #37729 Date of Report: Feb 27, 2015 Customer PO #: Customer ID: 08110027 Report #: 2015-01935 Project ID: Beau Rivage WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-04356A Site: Beau Rivage 2/16/2015 9:45 AM Solid/Sludge Will Coggins Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.49 % 02118/2015 Fecal Density SM 9221 C E MPN 24 hr 503 114094 M PN/g 02/17/2015 Comment Results, except pH, reported on a dry weight basis. pH reported on an as received basis. 4 Reviewed by: Report #.: 2015-01935 Page 2 of 2 ENVIRONMENTAL CHEMISTS, INC- OFFI E 0392.02 3PAX910: 92.4425 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com Cnl I IPPIrinnl AW"I f LJAIM n= r'1ICTf%r%V Client: A uaNC PROJECT NAME. Annual Sludge Analysis REPORT NO: V �35 ADDRESS: CONTACT NAME: PO NO: REPORT TO: Don Williams PHONE/FAX: COPY TO: &,j , email: Samnled Bv: ' ilG! ,4 - SAMPI F TVPF• i = Influan+ F = Ff hmn4- W = Well CT = C4ranm Cn - 0^11 CI - Ch.A— f 'mr- Sample Identification Collection y Fay, a N a o o� �, ,., o a`o m t " m Z PRESERVATION ANALYSIS REQUESTED Date Time Temp i Z. x i; s e o a Sludge C P Nutrients/metals G G c P c�35 G G C P C� /0 G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: Date1T"ime Received By: DateMme 1. 2. I emperature wnen Kecelvea: Acceptea: ey c> ea Icesample nequesieu: Delivered By: Received By. t/ Date: .�'�6'lS� Time: Comments: TURNAROUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Beau Rivage P.O.# i Batch Size (gallons): 30000 +/- Lbs. or Gallons Used: 2000 +/- Material Used For Stabilization: Lime Initial pH 2 Hour• RTFIldn. •. wwmz•= WEENSWOMEMM " ®EMIM ®�lmlm® ®• ®���� ®� 1 1 • ®® [M® 1 1 • 1 • IM •' I 1 1 • EEME c ` tU LL to O W 7 a N O M 7 n O) O N 7 a l0 O N 7 a Cal O W 7 a O O to) 7 a N O tll 7 a N O M 7 a N C tll 7 a 00 O N 7 a O_ O N 7 n N .— O N 7 a O O O (0) 7 a cn O O f/1 7 a fM O O tll 7 a O c� o o 0).J 7 C co. c 7 C rn o N 7 C N o j C tq c to 7 C ro o N 7 C o M 7 C c In 7 C N o Ol 7 C o� o m 7 C th c W 7 C M c W 7 C o .J 7 C 0 'A 7 C 0 W 7 C U o. E O 0 M M M t- m 0 M to M et m M m N m m O M M N Co N r• N (0 N Ln N v N M N N N N O N rn Co r` r- (O r- M •— d' •— m N .= O I— L_- ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Fauns and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Beau Rivage NPDES Number: NCO065480 Monitoring Period: From I/1r2015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate Ivel achieved and alternative performed: Class A: -Alt. A (timeltemp) ❑ 1 Alt B (Alk Treatment)❑ Alt. C (Prior Testin )❑ AIt.D o Prior Test) ❑ 1 Process to Further Reduce Patho en s ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ 1 Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ray [3 Gamma Ra ❑ Pasteurization ❑ Class B: I Alt. (1) Fecal Density ❑ Alt. (2) Process to Siguificantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Patbo ens": Lime Stabilization El Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density um er o Excee- Frequency of Analysis Y Sample Type Analytical Tech - Minimum Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) la bacteria Sal:RZ (iof fecal form) I 3 MPN per 4 grams total solid (dry , weight) Vector Attraction Reduction 05A NCAC 02T .1107) - Please indicate alternative performed: A1t.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization El Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ c;EilUU11r1C r!ON STATErYI ;NT (please check the appropriate statement) © "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction.and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer Nomp and itle (type or print) Signat of Preparer* Date Land Applier Name and Title (if applicablextype or print) Signature of Land Applier (if applicable) Date *Preparer is defined. in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: July 29, 2015 Carolina Plantation 1.89 % Solids 6.6 pH Permit No. WQ0000455 Nitrogen (TKN) 2.999 29,991.000 59.982 Phosphorus 2.591 25,905.000 51.810 Potassium 0.322 3,221.000 6.442 PAN (injected)* 1.164 11,639.130 23.278 PAN (surface)* 0.976 9,763.130 19.526 Ammonia Nitrogen 0.375 3,752.000 7.504 Calcium 2.426 24,258.000 48.516 Calcium Carbonate E . --- --- --- Magnesium --- 2,095.000 4.190 Sodium --- 5,263.000 10.526 Sulfur --- --- --- Nitrate N / Nitrite N --- 15.430 0.031 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 8,457.00 16.914 Arsenic --- 2.50 0.005 Cadmium --- 0.96 0.002 Chromium --- 4.000 --- Copper --- 86.00 0.172 Lead --- 3.80 0.008 Mercury --- 0.10 0.000 Molybdenum --- 5.00 0.010 Nickel --- 5.00 0.010 Selenium --- 5.00 0.010 Zinc --- 2,141.00 4.282 Environment 1, Inc. # 64D *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. ERAT(INEW Flo hmpudA P.O. BOX 7085, 114 OAKMONT GREENVILLE, N.C. 27835-7085 CAROLINA PLANTAT.(ENVIROLINK) C/O ENVIROLINK P.O. BOX 670 BAILEY ,NC 27807 PARAMETERS PH (not to be used for reporting) Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 6.6 07/29/15 TRB 4500HB-00 8457 08/07/15 LFJ EPA200.7 <2.5 08/12/15 MTM 3113B-04 24258 08/07/15 LFJ EPA200.7 0.96 08/14/15 MTM 311313-04 86 08/17/15 LFJ EPA200.7 4 08/17/15 LFJ EPA200.7 3.8 08/10/15 MTM 311313-04 2095 08/07/15 LFJ EPA200.7 0.10 08/10/15 MTM 245.1 R3-94 <5.0 08/07/15 LFJ EPA200.7 3221 08/07/15 LFJ EPA200.7 <5.0 08/19/15 MTM 311313-04 5263 08/07/15 JMN 311111-99 2141 08/14/15 JMN 3111B-99 1.89 08/04/15 KDS 254OG-97 29991 08/04/13 RND 351.2 112-93 3752 08/05/15 AKS 350.1 112-93 25905 08/03/15 KDB 365.4-74 15.43 08/05/15 KDB 353.2 112-93 11639 08/19/15 SEJ <5.0 08/07/15 LFJ EPA200.7 DNE (252) 756-6208 FAX (252) 756-0633 ID#: 64 D DATE COLLECTED: 07/29/15 DATE REPORTS : 08/21/OA�� 15 REVIEWED BY: IM Environment 1,1nC.. P.U. Box 7035, 114 Oakmont Dr. GreeoviIle, NC 27855 CHAIN OF CUSTODY RECORD Pace I of I _nviromnen[line.con-i DISLNI ECTION Phone (252) 756-6208 • Fax Q52) '756-0633 CHLORINE NEUTRALIZED AT COLLECTION Ij crrl_O1zLNE pH CHECK (LAB) CLIENT: 64 D Week: 26 ! LTV P P P P P P CONTAINER TYPE, PIG CAROLINA PLANTAT.(ENVIROLINIC) C/O ENVIROLM I P CHEMICAL PRESERVATION P.O. BOX 670 BAILEY NC 27807 A A A A A A A A -NONE D-NAOH 930 (252) 235-4900 ui ? J ,li w B-HNO3 E HCL ac X w z e Z co LU C- H,90j F- ZINC ACETATE NAOH COLLECTION ¢ a o w 0 r `= x R z b`PI a ; Z 0. G - NATHIOSULFATE SAMPLE LOCATION DATE TIME Qa Sam le S • ' ''�'••;;y? CLASSiFiCATiON:Slu WASTEINATER(NPDES) DRINKING 4VATER Dwww SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY N SAMPLES COLLECTED BY: (Please Print) SAMPLES RECEIVED IN LAB ATi' C RELINO ISHED BY (SIG.) (SAMPLER) %e; DATE(TIME AEG/ BY ( ) `, A COMMENTS: / L . RELINQ S BY {SIG.) DATEMME RECEIVED BY (SIG.) DA iIME RELINQUISHED BY (SIG.) DATEfnME RECEIVED BY (SIG.) DATEMME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a T" for composite sample or a "G" for No— 292474 FORM H5 Grab sample in the blocks above for each parameter requested. LEWIS FARMS WQ0000455 Carolina Plantation WWTP Date Fecal Cxfarm' Log 12/11/15 1,041,667 6.0177 12/11/15 1,785,715 6.2518 12/11/15 1,083,033 6.0346 12/11/15 1,167,316 6.0672 12/11/15 1,976,285 6.2958 12/11/15 845,071 5.9269 12/11/15 465,950 5.6683 Total 42.2625 Average 6.0375 Geometric Mean '° .;09fl,6$ ' Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. , T Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910:392.0223 Lab • 910.392.4424 Fax I © 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@enviroruncntalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Dec 17, 2015 8155 Malpass Comer Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attenfion: Wesley Wooten Report #: 2015-16584 Project ID: Carolina Plantation Lab ID Sample ID: Collect DateITime Matrix Sampled by _ 15-39458 Site:1 12/10/2015 2:00 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.88 % 12/11/2015 Fecal Density SM 9221C E MPN 24 hr 503 1041667 MPN/g 12111 /2015 _ Lab ID Sample ID: Collect DateITime Matrix Sampled by 15-39459 Site: 2 12/10/2015 2:02 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids % ( ) 2540 B ° 2.80 /0 12/11/2015 Fecal Density SM 92210 E MPN 24 hr 503 1785715 MPN/g 12/11/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by to 15-39460 Site: 3 12/10/2015 2:04 PM Solid/Sludge Client Test Method Results Date Analyzed _ Total Solids (%) SM 2540 B 2.77 % 12/11/2015 Fecal Density SM 9221 C E MPN 24 hr 503 ` 1083033 MPN/g 12111 /2015 _ ! Lab ID Sample ID: Collect Date/Time Matrix Sampled by I 15-39461 Site: 4 12/10/2015 2:06 PM Solid/Sludge Client !r Test Method - Results Date Analyzed ' Total Solids (%) SM 2540 B 2.57 % 12/11/2015 Fecal DensitySM 9221C E MPN 24 hr 503 1167316 MPN/g 12/11/2015 Lab ID Sample ID: Collect DateITime Matrix Sampled by 15-39462 Site: 5 12/10/2015 2:08 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM2540 B 2.53 % 12/11/2015 Fecal Density SM 9221C E MPN 24 hr 503 1976285 MP Wg 12/11/2015 Report 1t:: 2015-18584 Page 1 o12 Environmental Chemists, Inc. envirochem 6602 Wmdn-dU Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax &,— -:�� 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Lewis Farms S Liquid Waste, INC. Date of Report: Dec 17, 2015 8155 Malpass Comer Road Customer PO 0: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2015-16584 L Project ID: Carolina Plantation i Lab ID Sample ID: Collect DatelTime Matrix Sampled by 15-39463 Site: 6 12/10/2015 2:10 PM Solid/Sludge Client '' • Test Method Results Date Analyzed " i Total Solids (%) SM 2540 B 2.84 % 12/11/2015 j Fecal Density SM92210EMPN 24hr503 845071 MPN/g 12/11/2016 ' Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-39464 Site:7 12/10/2015 2:11 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 254o B 2.79 % 12/11 /2015 �- Fecal Density SM92210EMPN 24hr503 465950 MPN/g 12/11/2015 " F Comment: Fecal Density reported on a dry weight basis. '- Reviewed by: ti Report P: 2015-18584 Page 2 of 2 ! AA Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 2841 OFFICE: 910-392-0223 FAX 910-392-44, info@environmentalchemists.com CLIENT: G�w � �„ti s � ®gam.. c� G�3��` PROJECT NAME: c�a . ✓ � � +� �� 7�c 1i` REPORT NO: ADDRESS: CONTACT NAME: PO NO: C� — REPORT TO: PHONEIFAX: COPY TO: email: sampled 13y: AlN' SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection Q m E y Y CL `o L° c c7 _ `o oa " .r `o rn rE v m �� z PRESERVATION ANALYSIS REQUESTED Date Time Temp w o z x ao v, " M z x x o o s ►- 0 o ���• g % 3/ � � iS G G DL L°— C P G G L'y C P G G it-4- _ � 3 c Z� C P G --G— !( Z.-~ P J�G�r G C P G G C P G G C P G I G C P G I G Transfer Rel' y: Date/Time Re iv By: Z We/Time 41 \ 2. Temperature when Received: Accepted: K tea•z j Kesampie Delivered By: Received By: Date; — Comments: IL TI AlNIN VHL to I 11UVr.114 AINL V C.l. 1 VK A l l KAl- ■ RUIN, KILN%. 1 &Vir 1'l. AIT1 k0L 1 Nules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Carolina Plantation NPDES Number: WQ0033770 Monitoring, Period: From I/l/2015 To I2/31/2015 Pathosen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative Oerfornied (Class A only) indicate "Process to Further Reduce Patb ens": Compost ❑ . Heat Drying ❑ Heat Treatment ❑ Themno hilic ❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ " ' Class B: Alt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Path ens": Lime Stabilization ❑ Air Drying ❑ Com ostiu ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the llowing monitoring data: Parameter Allowable Level in in Sludge Pathogen Density um er o Exce� Frequency of Analysis ys Sample Type Analytical Tech - inimu Geo. Mean aximu Unitsence-q Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 465.950 1,090,168 1,976,285 MPN/g 0 Annual Grab sM 9221 cE CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) ,-weight) 3 MPN per 4 grants total solid (dry v CCWI" A1tFUCIlUn MCDUC11011 I ILMA M-AFLl; 0L 1 A ILU / 1 - Please Innic re alternative nef icirmen: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) CI Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) p No vector attraction reduction alternatives were perkiffned ❑ l EN I lrit✓A I IUN a I -A I EIVIEtrr (ptease cnecK the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in ISA NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the "This determination has been made under my direction and supervision In accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jeff Jarmon, ORC _ Preparer bTpmq, and ' le (type or print) Signature of Preparer* Date Wesley Wooten, President Land Applier amend Title (if applicable)(type or print) 2- zy- /6 Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (2G) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 30, 2015 Castle Bay 2.37 % Solids 7.2 pH Permit No. WQ0000455 Nitrogen (TKN) 3.990 39,900.000 79.800 Phosphorus 1.370 13 700.000 27.400 Potassium 0.178 1,780.000 3.560 PAN (injected)* 1.263 12 634.700 25.269 PAN (surface)* 1.218 12,182.200 24.364 Ammonia Nitrogen 0.091 905.000 1.810 Calcium 5.710 57,100.000 114.200 Calcium Carbonate E . --- --- Magnesium --- 1,340.000 2.680 Sodium --- 6,620.000 13.240 Sulfur --- --- --- Nitrate N / Nitrite N --- 31.200 0.062 Barium --- --- --- Chloride --- --- --- Iron --- --- Aluminum --- 3,610.00 7.220 Arsenic --- 41.40 0.083 Cadmium --- 41.40 0.083 Chromium --- 41.400 --- Copper --- 389.00 0.778 Lead --- 41.40 0.083 Mercury --- 0.72 0.001 Molybdenum --- 41.40 0.083 Nickel --- 41.40 0.083 Selenium --- 41.40 0.083 Zinc --- 1,630.00 3.260 Environmental Chemists, Inc. # 2015-15877 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % F Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. ANALYTICAL & CONSULTING CHEMISTS Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.4735702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemismcom Date of Report: Dec 21, 2015 Customer PO #: Customer ID: 14020008 Report #: 2015-15877 Project ID: AquaNC-Castle Bay Sludge ! Lab ID Sample ID: Lewis Farms-AquaNC Collect Date/Time Matrix Sampled by Castle Bay 15-37833 Site: Sludge 11/30/2015 10:05 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 3610 mg/kg 12/02/2015 Arsenic EPA 200.7 <41.4 mg/kg 12/02/2015 Cadmium EPA 200.7 <41.4 mg/kg 12/02/2015 Calcium EPA 200.7 57100mg/kg 12/01/2016 Chromium EPA 200.7 <41.4 mg/kg 12/02/2015 Copper EPA 200.7 389 mg/kg 12/02/2015 Lead EPA 200.7 <41.4 mg/kg 12/02/2015 Magnesium EPA 200.7 1340 mg/kg 12/01/2015 Molybdenum EPA 200.7 <41.4 mg/kg 12/02/2015 Nickel EPA 200.7 <41.4 mg/kg 12/02/2015 Potassium EPA 200.7 1780 mg/kg 12/01/2015 Selenium EPA 200.7 <41.4 mg/kg 12/02/2015 Sodium EPA 200.7 6620 mg/kg 12/01/2015 — Zinc I EPA 200.7 1630 mg/kg 12102/2015 Total Kjeldahl Nitrogen (TKN) EPA351.2 39900mg/kg 12/15/2015 Nitrate+Nitrite-Nitrogen EPA353.2 31.2 mg/kg 12118/2015 Total Solids (%) SM 2540 B 2.37 % 12/02/2015 pH, SM 4500 H B 7.20 units 12/11/2015 Ammonia Nitrogen SM 4500 NH3 c 905 mg/kg 1211012015 Total Phosphorus SM 4500 P F 13700 mg/kg 12/15/2015 Mercury SW84674718 <0.717 mg/kg 12/02/2015 Report #.: 2015-15877 Pa°e 1 of 3 r'- LEWIS FARMS WQ0000455 Castle Bay WWTP Hate Fecal Coliform_ MPN per ° .. am: . Lag 11/30/15 12,054 4.0811 11/30/15 21,552 4.3335 11/30/15 47,414 4.6759 11/30/15 177,778 5.2499 11/30/15 14,164 4.1512 11/30/15 4,911 3.6912 11/30/15 21,098 4.3242 Total 30.5070 Average 4.3581 Geometric Mean 22,811 " Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. F Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax (' ® 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.3843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com ■ Lewis Farms & Liquid Waste, INC. Date of Report: Dec 21, 20,15 i 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Report #: 2015-15877 s Project ID: AquaNC-Castle Bay Sludge Lab ID Sample ID: Lewis Farms-AquaNC Collect Daterrime Matrix Sampled by Castle Bay 15-37834 Site: Sludge 11/30/2015 10:06 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.24 % 12/02/2015 Fecal Density SM 92210 E MPN 24 hr 503 12054 MPN/g 12/01/2015 Lab ID Sample ID: Lewis Farms-AquaNC Collect Date/Time Matrix Sampled by Castle Bay 15-37835 Site: Sludge Test Total Solids (%) Fecal Density Lab ID 15-37836 11/30/2015 10:07 AM Solid/Sludge Jay Baker Method Results Date Analyzed SM 2540 B SM 9221 C E MPN 24 hr 503 2.32 % 12/02/2015 21552 MPN/9 1210112015 Sample ID: Lewis Farms-AquaNC Collect Date/Time Matrix Sampled by Castle Bay Site: Sludge 11/30/2015 10:08 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed Total Solids (%) Fecal Density Lab ID SM 2540 B SM 9221C E MPN 24 hr 503 Sample ID: Lewis Farins-AquaNC Castle Bay 15-37837 Site: Sludge 2.32 % 12/02/2015 47414 MPN/g 12/01/2015 Collect Date/Time Matrix Sampled by 11/30/2015 10:09 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.34 % 12/02/2015 Fecal Density SM 9221C E MPN 24 hr503 177778 MPN/g 12/01/2015 - Report#:: 201 &15877 Pa°e 2 of 3 envirochem I ANALYTICAL & CONSULTING CHEMISTS 7441 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5943 Lab/Fax info@environmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Dec 21, 2015 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 i Attention: Report #: 2015-15877 Project ID: AquaNC-Castle Bay Sludge Lab ID Sample ID.- Lewis Farms-AquaNC Collect Date/Time Matrix Sampled by Castle Bay --j 15=37838 Site: Sludge 11/30/2015 10:10 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed Total Solids (%) SM 2540 B , 2.33 % 12/02/2015 Fecal Density SM 9221C E MPN 24 hr 503 14164 MPN/g 12/01/2015 Lab ID Sample ID: Lewis Farms-AquaNC Collect Date/Time Matrix Sampled by Castle Bay 15-37839 Site: Sludge 11/30/2015 10:11 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed Total Solids {%) SM 2540 B 2.24 % 12102/2015 Fecal Density SM92210EMPN 24hr503 4911 MPN/g 12101/2015 'Lab ID Sample ID: Lewis Farms-AquaNC Collect Date/Time Matrix Sampled by Castle Bay 15-37840 Site: Sludge 11/30/2015 10:12 AM Solid/Sludge Jay Baker Test Method Results Date Analyzed �f Total Solids (%} _J Fecal Density SM 2540 B SM 9221 C E MPN 24 hr 503 2.37 % 12/02/2015 21098 MPN/g 12/01/2015 Comment: Results, except pH, r ported on a dry weight basis. pH reported on an as received basis. i Reviewed by: Report P: 2015-15877 Page 3 of 3 602 ill Way lmington ENVIRONMENTAL CHEMISTS, INC OFFICE: 9r103920 2' FAX 91, NC0392�44, Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@enbironmentalchemists.com COLLECTION ANn C14AIN nR r`I ISTnnV CLIENT: Lc ; s ram,.. s PROJECT NAME: Cf f� 1- a c REPORT NO: ADDRESS: CONTACT NAME: (J, s1",,,✓ PO NO: REPORT TO: / ,,�, (,� ;c.+-� PHONE/FAX: COPY TO: email: aampiea tsy. ., .'r, C A 4L SAMPLE TYPE: I = Influent, E = Effluent, W = Weil, ST = Stream, SO = Soil, SI_ = Sludge, Other: Sample identification Collection T E N x c c 0 � .. c oa 0 m. 2 " a 2 Z PRESERVATION ANALYSIS REQUESTED to Time Temp _ o x � x H o z x o g x x o sl/ / ao C P ,I��i.�...�r�t G G 3-834 1 G G C P ; �43� G G 3 �aQy I G G l�� S C P C P )•�173� G G i C P G G C P 3 n�{o G G C P C P G G Transfer Relinquished By: Date/Time Received By: Dateffime 1. 2. o Temperature when Received: r Accepted: e- Rejected: Resample Req es d: Delivered By: Received By: t Date: if l rly"� Time: Iva Cnmmanfa- Trnu w e5n� non. ANNUAL. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WWTP Name: Castle Bay Monitoring Period: From l/l/2015 To Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: WQ Permit Number: WQ0000455 NPDES Number: WQ0018755 12/31/2015 Class A: Alt. A (timehem) ❑ 1 Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testin )❑ A1t.D (No Prior Tcst) ❑ 1 Process to Further Reduce Patho ens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 eat Drying ❑ Heat Treatment ❑ Thermo hilic [3Beta Ray [3Gamma R ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density El I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com ost ing ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ >:::: •:::: . If applicable to alternative performed (Class A or Class B) complete the following monitoring data. - Parameter Allowable Level in in Sludge Pathogen Density Numver or Excee- Frequency of Analysis Y Sample Type na r cal Tech - inimu Geo. Mean aximu Unitsenceq Fecal Coliform 2 x 10 to the 6th power of otalg odds MPN 4,911 22,811 177,778 MPN/g 0 Annual Grab sM 9221 cE CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: AIL 1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ AIL 9 (Injection) Q Alt. 10 (Incorporation) Q No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer /Name type or print) 2-24eI< Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land AppIier (if applicable) *Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM ' RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 28, 2015 Clarkton 2.18 % Solids 7.16 pH Permit No. WQ000045 pia x 10,600), ry'Ion- (Mg[Kg x a.Ot Nitrogen (TKN) 0.288 2,880.000 5.760 Phosphorus 0.035 350.000 0.700 Potassium 0.239 2,390.000 4.780 PAN (injected)* 0.410 4,098.500 8.197 PAN (surface)* 0.179 1,788.500 3.577 Ammonia Nitrogen 0.462 4,620.000 9.240 Calcium 1.610 16,100.000 32.200 Calcium Carbonate E . --- --- --- Magnesium - 1,810.000 3.620 Sodium --- 2,220.000 4.440 Sulfur --- --- --- Nitrate N / Nitrite N --- 0.500 0.001 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 6,560.00 13.120 Arsenic --- 4.59 0.009 Cadmium --- 4.59 0.009 Chromium --- 14.900 --- Copper --- 304.00 0.608 Lead - 23.40 0.047 Mercury --- 1.98 0.004 Molybdenum --- 4.59 0.009 Nickel --- 11.00 0.022 Selenium --- 4.59 0.009 Zinc - 761.00 1.522 Environmental Chemists, Inc. # 2015-05212 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Ince- envirochem 6602 WindmillWay • Wilmington, NC 28405 ® (910) 392-0223 (Lab) • (910) 392-4424 (Fax)' M 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL 8 CONSULTING (252) 473 5702 CHEMISTS NCDEN - DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town of Clarkton Date of Report: May 27, 2015 PO Box 307 Customer PO #: Clarkton NC 28433 Customer ID: 08100292 Attention: Alton Boswell Report #: 2015-05212 Project ID: Sludge Lab ID Sample ID: Collect Datarrime Matrix Sampled by 15-12003 Site: Sludge 4/28/2015 11:55 AM Solid/Sludge Alton Boswell • Test Method Results Date Analyzed Chlordane SW 846 Method 8081 W3510 <0.005 mg/L 05/12/2015 Endrin SW 846 Method 60818/3510 <0.00005 mg/L 05/12/2015 Heptachlor SW 846 Method 60818/3510 <0.00005 mg/L 05/12/2015 Heptachlor epoxide SW 846 Method 8081 B/3510 <0.00005 mg/L 05/12/2016 Lindane SW 846 Method 80818/3510 <0.00005 mg/L 05/12/2015 Methoxychlor SW 846 Method 8051 B/3510 <0.00005 mg/L 05/12/2015 Toxaphene SW 846 Method 8081 W3510 <0.005 mg/L 05/12/2015 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/13/2015 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/13/2015 2,4,6-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 05/1312015 2,4-Dinitrotoluene (TCLP) SW 846 method 627013510 <0.050 mg/L 05/13/2015 Cresol (TCLP) SW 846 method 8270/3610 <0.050 mg/L 05113/2015 Hexachloro-1,3-butadiene (TCLP) Sw 646 method 6270/3510 <0.050 mg/L 05113/2015 Hexachlorobenzene (TCLP) sw 846 method 827013510 <0.050 mg/L 05/13/2015 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/13/2015 m + p-Cresol (TCLP) SW 846 method BZ7013510 <0.050 mg/L 05/13/2015 Nitrobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 05/13/2015 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/13/2015 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 05/13/2016 Pyridine (TCLP) SW 846 method 827CW510 <0.050 mg/L 05/13/2015 2,4,5-TP SW846 Method 8151A <0.0001 mg/L 05/14/2015 2,4-D SW846 Method 8151A <0.0001 mg/L 05/14/2015 1,1-Dictiloroethylene SWO46Method 826015030 <0.01 mg/L 05/22/2016 1,2-Dichloroethane SW846 Method 8260/5030 <0.01 mg'/L 05/22/2015 Benzene SW846 Method 8260/5030 <0.01 mg/L 05/22/2015 Carbon Tetrachloride SW848 Method 8260/5030 <0.01 mg/L 05/22/2015 Report k 2016-05212 Page 1 of 4 P( ^I Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28WS (910) 392-0223 (Lab) • (910) 392-4424 (Fax) ® 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL &CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DIS CERTIFICATE #37729 Town of Clarkton Date of Report: May. 27, 2015 PO Box 307 Customer PO #: Clarkton NC 28433 Customer ID: 08100292 ` Attention: Alton Boswell Report #: 2015-05212 Project ID: Sludge Chlorobenzene SW646 Method 8260/5030 <0.01 mg/L 05/22/2015 `- Chloroform SW846 Method 8260/6030 <0.01 mg/L 05/22/2015 Methyl ethyl ketone SW846 Method 8260/5030 <0.05 mg/L 05/2212015 ',- Tetrachloroethylene SW846 Method 8260/5030 <0.01 mg/L 05/22/2015 Trichloroethylene Swe46Method 8260/5030 <0.01 mg/L 05/22/2016 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 05/22/2015 RCI Cyanide EPA 335.4 <0.124 mg/kg 05/13/2015 Analyzed outside of holding time. pH SM 4500 H e 7.16 units 04/30/2015 Sulfide SM 4500 S D 2.16 mg/kg 04/30/2015 ignitability SW 84s method 1010 >212 OF 05/15/2015 j Sludge Residuals Aluminum EPA200.7 6560 mg/kg 04/30/2015 Arsenic EPA200-7 <4.59 mg/kg 04/30/2015 i Cadmium EPA200.7 <4.59 mg/kg 04/30/2015 Calcium EPA200.7 16100 mg/kg 05/04/2015 Chromium EPA200.7 14.9 mg/kg 04/30/2015 ! Copper EPA200.7 304mg/kg 04/30/2015 Lead EPA200.7 23.4 mglkg 04/30/2016 Magnesium EPA20o:7 1810mglkg 06/04/2015 Molybdenum EPA200.7 <4.59 mg/kg 04/30/2015 Nickel EPA200.7 11.0 mg/kg 04/30/2015 Potassium EPA200.7 2390 mg/kg 05/04/2015 Selenium EPA200.7 <4.59mq/kq 04/30/2015 Sodium EPA200.7 2220 mq/kq 05/04/2016 Zinc EPA200.7 761 mg/kg 04/30/2015 Total Kjeldahl Nitrogen (TKN) EPA 351.2 2880 mg/kg 05/19/2016 Nitrate+Nitrite-Nitrogen EPA353.2 0.50 mg/kg 05/06/2015 ' Total Solids (%) SM2540 a 2•18 % 04/30/2015 Report #:: 2015-06212 Page 2 of 4 0 rolop- -. Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910)392-0223(Lab) ! (910) 392-4424 (Fax) ® 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE 037729 Town of Clarkton Date of Report: May 27, 2015 PO Box 307 Customer PO #: Clarkton NC 28433 Customer ID: 08100292 Attention: Alton Boswell Report #: 2015-05212 Project ID: Sludge Ammonia Nitrogen sM4500 NH3 C 4620 mg/kg 05/06/2015 Total Phosphorus SM4500 P F 350 mg/kg 05/12/2015 Mercury SW84674718 1.98 mg/kg 04/30/2015 TCLP Metals Arsenic EPA200.8 <0.010 mg/L 05/18/2015 Barium EPA200.8 0.063 mg/L 05/18/2015 Cadmium EPA200.8 <0.010 mg/L 05/18/2015 Chromium EPA200.8 0.014 mg/L 05/18/2015 Lead EPA200.8 <0.010 mg/L 05/18/2015 Selenium EPA200.8 <0.01,0mg/L 05/18/2015 Silver EPA 200.8 <0.010 mq/L 05/18/2015 Mercury EPA 245.1 <0.0020 mg/L 05/12/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-12004 Site: Sludge 1 4/28/2015 11:65 AM Solid/Sludge Alton Boswell Test Method Results Date Analyzed Total Solids {%) SM2540 B 2.28 % 04/30/2015 Fecal Density SM 9221C E MPN 24 hr 503 878 MPN/g 04/29/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-12005 Site: Sludge 2 4/28/2015 11:55 AM Solid/Sludge Alton Boswell Test Method Results Date Analyzed Total Solids M SM2540 B 2.06 % 04/30/2015 Fecal Density SM 9221C E MPN 24 hr 503 10680 MPN/g 04/29/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-12006 Site: Sludge 3 4/28/2015 11:55 AM Solid/Sludge Alton Boswell Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.17 % 04/30/2016 Fecal Density SM 9221C E MPN 24 hr 503 10139 MPN/g 04/29/2015 i Report #:: 2015-05212 Page 3 of 4 Environmental Chemists, Inc. • 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-W4 (Fax) 710 Bowsertown Road a Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE 094. DI.S CERTIFICATE #37729 i Town of Clarkton Date of Report: May 27, 2015 PO Box 307 Customer PO #: Clarkton NC 28433 Customer 1D: 08100292 Attention: Alton Boswell Report #: 2015-05212 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by ` 15-12007 Site: Sludge 4 4/28/2015 11:55 AM Solid/Sludge Alton Boswell Ij Test Method Results Date Analyzed J Total Solids (%) SM2540 B 2.20 % 04/3012015 Fecal Density SM 9221C E MPN 24 hr 503 10455 MPN/g 04/2912015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-12008 Site: Sludge 5 4/28/2015 11:55 AM Solid/Sludge Alton Boswell f Test Method Results Date Analyzed Total Solids (%) SM2540 B 2.23 % 04/30/2015 Fecal Density SM 9221C E MPN 24 hr 503 1794 MPN/q 04/29/2015 (w1 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-12009 Site: Sludge 6 4/28/2015 11:55 AM Solid/Sludge Alton Boswell F U Test Method Results Date Analyzed Total Solids (%) SM2M B 2.15 % 04/30/2015 Fecal Density SM 9221 C E MPN 24 hr 503 7907 MPN/g 04/29/2015 Lab ID Sample 1D: Collect Date/Time Matrix Sampled by 15-12010 Site: Sludge 7 4/28/2015 11:55 AM Solid/Sludge Alton Boswell Test Total Solids (%) Fecal Density Method SM 2540 B SM 9221 C E MPN 24 hr 503 Comment: Sludge residuals reported on dry weight basis. Reviewed by: - 4, Results 2.12 % 10378 MPN/g Date Analyzed 04/30/2015 04/29/2015 Report #:: 2015-05212 . Page 4 of 4 602 Windmill Way Wilmington, NC 2841 ENVIRONMENTAL CHEMISTS, INC OFFICE 9'10392-0223FAXM392-U Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY CLIENT: /.....� .,� �� �v PROJECT NAME: W&-J rto ` REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONEIFAX: COPY TO: email: sampiea my: o If SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m E a E o �, ,, a ` m U E_ a z PRESERVATION ANALYSIS REQUESTED ate Time Temp z _ _ $ o ti o (� C P / C P J� ! ?S C P G G C P G G `f C P lyoo� G G C P 11. G G C P G G C P IZ�� G G C P G G Transfer Relinquished By: Dateffime Received By: Date/Time 1. 2. Temperature when Received: r L Accepted: Kejectea: Kesampie K u iea: Delivered By: Received By.* Date: Time: Comments: TURNAROUND: LEWIS FARMS WQ0000455 Clarkton WWTP Date Fecal Co i.f6rm 1VI1'"Nper ° am . Log 04/28/15 878 2.9435 04/28/15 10,680 4.0286 04/28/15 10,139 4.0060 04/28/15 10,455 4.0193 04/28/15 1,794 3.2538 04/28/15 7,907 3.8980 04/28/15 10,378 4.0161 Total 1 26.1653 Average 3.7379 Geometric Mean 5 469 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. ANNUAL PATHOGEN ANU VEC F0K A'1"1'RAC 1'lUN REV(JC: l'lUN p'URM (UZ'1' Mules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Town ofClarkton NPDES Plumber: NCO21610 Monitoring Period: From 111/20I5 To 12/31/2015 Pathoten Reduction (15A NCAC' 02T _1lam _ vi.c en 1"A1A0+& 1A..n1 n..1.J.—A ....a Class A: Alt A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Pror Testing) ❑ lCompost AWD (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": ❑ Heat Drying ❑ Heat Treatment ❑ Thetmophilic ❑ Beta Ra ❑ Gamma Ra ❑ Pasteurization ❑ Class R: JAIL (I) Fecal Densi Q Alt. (2) Ptvicess to Significantly Reduce Patho ens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air 'n ❑ Composthig ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ .••.. If applicable to alternative performed (Class A or Class B) complete the Ilowing monitoring data: Parameter Allowable Level in Sludge Pathogen Density um er o Exec , Frequency e9 Y of Analysis Sample P Type Analytical Tech- Minima Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 878 5,469 10 680 MPN/ g 0 Annual Grab sm 9221 cE 7CFUU 1000 mpn per gram of total solid (dry weight) Salmonella bactena (in lieu of fecal eoliform 3 MPN per 4 grams total solid (dry Wei t AIL (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt 9 Nection) ❑ Alt. 10 (Inco oration) Q No vector attraction reduction alternatives were performed ❑ VaJw\ a jj• A's a jvl� -a jf'jj ntvan- it Tease cueeK me appropriate statement) © "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met I am aware that there are significant penalties for false certification including fine and imprisonment" Chris Hall, ORC Prep e nd Titl (type or print) Signature of Preparer* Date Wesley Wooten, President Land Applier Name anj Title (if applicable)(type or print) Signature o Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 14, 2015 Emerald Plantation 1.30 % Solids 6.55 pH Permit No. Nitrogen (TKN) 2.220 22,200.000 44.400 Phosphorus 1.080 10 800.000 21.600 Potassium 0.445 4,450.000 8.900 PAN (injected)* 0.962 9,617.780 19.236 PAN (surface)* 0.751 7,507.780 15.016 Ammonia Nitrogen 0.422 4,220.000 8.440 Calcium 1.800 18,000.000 36.000 Calcium Carbonate E . --- --- --- Magnesium 2,180.000 4.360 Sodium 11 900.000 23.800 Sulfur --- --- --- Nitrate N / Nitrite N 3.780 0.008 Barium --- --- --- Chloride ---I --- --- Iron --- --- --- Aluminum --- 2,480.00 4.960 Arsenic --- 39.90 0.080 Cadmium --- 39.90 0.080 Chromium --- 39.900 --- Copper --- 1,350.00 2.700 Lead --- 39.90 0.080 Mercury --- 1.39 0.003 Molybdenum --- 39.90 0.080 Nickel --- 39.90 0.080 Selenium --- 39.90 0.080 Zinc --- 709.00 1.418 Environmental Chemists, Inc. # 2015-16791 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. envirochem ANALYTICAL & CONSULTING CHEMISTS Aqua America of North Carolina 251 Merchants Circle Bldg 24-1 Hampstead NC 28443 Attention: Don Williams Lab ID Sample ID: 15-39950 Site: Digester Test Sludge Residuals Aluminum Arsenic Cadmium Calcium Chromium Copper Lead Magnesium Molybdenum Nickel Potassium Selenium Sodium Zinc Total Kjeldahl Nitrogen (TKN) Nitrate+Nitrite-Nitrogen Total Solids (%) pH Ammonia Nitrogen Total Phosphorus Mercury Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Jan 19, 2016 Customer PO #: Customer ID: 08110027 Report #: 2015-16791 Project ID: Emerald Plantation Sludge Collect Datefrime Matrix Sampled by 12/14/2015 2:15 PM Solid/Sludge Don Feller Method Results Date Analyzed EPA 200.7 2480 mg/kg 12121 /2015 EPA 200.7 <39.9 mg/kg 12/28/2015 EPA 200.7 t <39.9 mg/kg 12/28/2015 EPA 200.7 18000 mg/kg 12/22/2015 EPA 200.7 <39.9 mg/kg 12/28/2015 EPA200.7 1350 mg/kg 12/21/2015 EPA200.7 <39.9 mg/kg 12/28/2015 EPA200.7 2180 mg/kg 12/22/2015 EPA 200.7 <39.9 mg/kg 12/28/2015 EPA200.7 <39.9 mg/kg 12/28/2015 EPA200.7 4450 mg/kg 12/22/2015 EPA 200.7 <39.9 mg/kg 12/28/2015 EPA 200.7 11900 mg/kg 12/22/2015 EPA200.7 709mg/kg 12/21/2015 EPA351.2 22200 mg/kg 01/14/2016 EPA353.2 3.78 mg/kg 01/04/2016 SM 2540 8 1.30 % 12/16/2016 SM 4500 H B 6.55 units 12/24/2015 SM4500 NH3 C 4220 mg/kg 12/21/2015 SM 4500 P F 10800 mg/kg 01/08/2016 SWM7471B <1.39 mg/kg 12/22/2015 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: 1'0� ReportIR:: 2015-16791 Page 1 of 1 Analyilcal & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 2844 OFFICE: 910.392.0223 FAX 910-392-44' Info@environmentalchemists.com CLIENT: PROJECT NAME: 1j4,o7,v REPORT NO: $"— (p ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONEIFAX: COPY TO: email: sampled 13y: ilb,j ie//d,L SAMPLE TYPE: I = Influent, E. = Effluent, W = Well, ST = Stream, SO = Soil; SL = Sludge, Other: Sample Identification Collection r m y y a a a m c C9 C I "v „ C o w _ Z PRESERVATION ANALYSIS REQUESTED Date Time Temp w z NZt s X =x Y o .SLUZ C P CIO c uD V4 (G) G C P G G C P G G C P G G C P G G C P G G C P G C P G G C P G G C P G G Transfer Relinquished By: DatelTime Received By: DatelTime 9. 2. Temperature when Received: Accepted: Ke)ectea: mesampie me uesiea: Delivered By: 0 � �� Received By: Date: Time: Comments: TURN OUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Emerald Plantation P.O.# Batch Size (gallons): 18,000 Lbs. or Gallons Used: 450 Material Used For Stabilization: Lime Initial pH• • • wall. •. co ` _ i'i ci � � It O tll 7 a N V O (A 7 a 0) M O W 7 a t0 M O N 7 a M M O N 7 a O M O N a f� N O N 3 a N O N 7 a N O N 7 a a0 r- O N 7 a O N 7 a N O N 7 a 0) O C N 7 a-. f0 O C N 7 a Cl) O C W 7 s O Co o 0 N 7 C 2 (0 0 0 N 7 C 2 m 0 0 N 7 o 2 N c N c 2 in .- c N C 2 m .- 0 W C 2 N 0 N C 2 a N 0 N C g h N 0 tll C M:E o q 0 N C to q 0 N C n (n q 0 N C 2 rn M 0 N C 2 N V' 0 N C 2 11t 0 tll C U o. N O 0) M Co M ti M Co Co LO Co 'IT M M M N M M O M M N Co N ti N 0 N LOq- N N M N N N � N O N M � Co � f- � (0 r ul) � ct •- M •- N � � O � H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Emerald Plantation NPDES Number: VI-25-10 Monitoring Period: From 1/l/2015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T. 1106) - Please indicate level achieved and alternative performed: Class A: It. A (time/temp) ❑ 1 All B (Alk Treatment)❑ Alt. C (Prior Testin )❑ Alt.D (No -Prior Test) ❑ I Process to Further Reduce Patho ens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Com ost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ra ❑ Gamma Ray❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significant) Reduce Pathogens ❑ If a licable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization El Ai Diying ❑ Com osting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ : :::.:: , . ...•.. ; : ;:::..:.::.::: .. .. • .. • ::: ,:..:.:.:::. .::. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number of Excee- Frequency of Analysis y Sample Type na Ica Tech- inimu Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power of to petalCFU MPN 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) ❑ Alt. 2 (40-day'bench) ❑ JAIL 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization El jAlt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ ( aEK 1'a1N'leA1ON ST TEMENT (please check the appropriate statement) El "I certify, under penalty of law,, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been mot." [3"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Wesley Wooten, President Preparer Name and Title (type or print) Land Applier Name and Title (if applicablextype or print) Signature PePreparee Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 8, 2015 Hampstead Pines 1.16 % Solids 7.12 pH Permit No. WQ0000455 Nitrogen (TKN) 7.840 78,400.000 156.800 Phosphorus 2.190 21 900.000 43.800 Potassium 0.363 3,630.000 7.260 PAN (injected)* 2.774 27 741.500 55.483 PAN (surface)* 2.480 24,796.500 49.593 Ammonia Nitrogen 0.589 5,890.000 11.780 Calcium 2.980 29,800.000 59.600 Calcium Carbonate E . --- --- --- Magnesium 1,860.000 3.720 Sodium 12 200.000 24.400 Sulfur --- --- Nitrate N / Nitrite N 98.500 0.197 Barium --- --- --- Chloride --- I --- --- Iron --- --- --- Aluminum --- 1,870.00 3.740 Arsenic --- 41.80 0.084 Cadmium --- 41.80 0.084 Chromium --- 41.800 --- Copper --- 186.00 0.372 Lead --- 41.80 0.084 Mercury --- 1.64 0.003 Molybdenum --- 41.80 0.084 Nickel --- 41.80 0.084 Selenium --- 41.80 0.084 Zinc --- 1,500.00 3.000 Environmental Chemists, Inc. # 2015-16320 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. [enviroche]m ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Hampstead Pines Date of Report: Dec 21, 2015 1004 Bally Bunion Lane Customer PO #: Burgaw NC 28425 Customer ID: 09010034 Attention: J. Marty Fritz Report #: 2015-16320 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-38826 Site: Digester Sludge 12/8/2015 9:15 AM Solid/Sludge Marty Fritz Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 1870 mg/kg Arsenic EPA 200.7 <41.8 mg/kg Cadmium EPA 200.7 <41.8 mg/kg Calcium EPA 200.7 29800 mg/kg Chromium EPA 200.7 <41.8 mg/kg Copper EPA 200.7 186 mg/kg Lead EPA 200.7 <41.8 mg/kg Magnesium EPA 200.7 1860 mg/kg Molybdenum EPA 200.7 <41.8 mg/kg N ickel EPA 200.7 <41.8 mg/kg Potassium EPA 200.7 3630 mg/kg Selenium EPA 200.7 <41.8 mg/kg Sodium EPA 200.7 12200 mg/kg Zinc EPA 200.7 1500 mg/kg Total Kjeldahl Nitrogen (TKN) EPA 351.2 78400 mg/kg Nitrate+Nitrite-Nitrogen EPA353.2 98.5 mg/kg Total Solids (%) SM 2540 B 1.16 % pH SM 4500 H B 7.12 units Ammonia Nitrogen SM 4500 NH3 C 5890 mg/kg Total Phosphorus SM 4500 P F 21900 mg/kg Mercury SW846 7471 B <1.64 mg/kg Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: J, 12/14/2015 12/14/2015 12/14/2015 12/10/2015 12/14/2015 12/14/2015 12/14/2015 12/10/2015 12/14/2015 12/14/2015 12/10/2015 12/14/2015 12/11/2015 12/14/2015 12/16/2015 12/16/2015 12/10/2015 12/16/2015 12/15/2015 12/17/2015 12/09/2015 Report #:: 2015-16320 Page 1 of 1 Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 2841 OFFICE: 910.392-0223 FAX 910-392-44: info@environmentalchemists.com CLIENT: PROJECT NAME: �� REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled Bv: j • 1' &e l / SAMPLE TYPE I = Influent_ F = Fffhiant W = Wall RT = Rtranm RC1 = Rnil RI = Rhirina [lthar- Sample Identification p Collection E �, a o c o e e " `� o L E " m m J D Z PRESERVATION ANALYSIS REQUESTED Date Time Temp W Z O z x o � i - Z s - o g W ac o isto 21sC P C P G G C P G G C P G G C P G G C P G G C P G G C P G G C P C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Rec lved., Accepted: Rejemted: Resample Req es e �d: Delivered Byer 1 Received By:. Date: Time: rnmmantc• ro+o&,wo i;m. M LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Hampstead Pines P.O.# Batch Size (gallons): 8,000 Lbs. or Gallons Used: 250 Material Used For Stabilization: Lime EMME Co ` U Co 0, LL- Lo V O fn 7 a N V O N 7 d m M O N J 5- o M O w 7 cn M O 4/ J O M O M J h N O Ul 7 V N O to 7 N O w 7 a a0 , O w 7 a O w 7 a N O u) 7 a O) O O 4/ 7 a (D O O U) 7 m c+� O O f/1 7 EL O M O O w C 2:E m O O 0 C m O O N C 2 N o C 2:i !n O N C eR O 0 C 2 .- N O 0 C 2 v N O 0 C 2 ram- N O 0 C 2:i o M O N C M M O J1 C 2 co M O fA C 2 rn M O N C 2 N V O N C v� V O 41 C f U Q E O 0) M co M r- M (D M LO M M co M N M M O M O N CO N r- N CD N LD N V N M N N N N O N 0) Co r- (D U) V' M N �- CD H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Hampstead Pines NPDES Number: WQ0022052 Monitoring Period: From 1/1/2015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (timeItem) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testin )❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Patho en s ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thenno lvlic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ - Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Si ificantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization El Air Drying O 1 Composting ❑ jAcrobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density NumBer ot Excee- Frequency of Analysis Sample Type nalytical Tech - Minimum Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization p Alt 7 (Drying - Stable) ❑ Alt. 9 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) Q No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T A 107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President PreparerNaame and Title (type or print) Land Applier Name and Title (if applicable)(type or print) �;; � Signature o Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 16, 2015 Hampstead Town Center Permit No. WQ0000455 1.16 % Solids 7.22 pH Nitrogen (TKN) 2.650 26,500.000 53.000 Phosphorus 1.360 13,600.000 27.200 Potassium 0.031 307.000 0.614 PAN (injected)* 1.316 13 163.190 26.326 PAN (surface)* 0.944 9,443.190 18.886 Ammonia Nitrogen 0.744 7,440.000 14.880 Calcium 0.533 5,330.000 10.660 Calcium Carbonate E . --- --- Magnesium 603.000 1.206 Sodium 828.000 1.656 Sulfur --- --- --- Nitrate N / Nitrite N 5.190 0.010 Barium --- --- --- Chloride --- --- Iron --- --- Aluminum --- 4,250.00 8.500 Arsenic --- 33.90 0.068 Cadmium --- 33.90 0.068 Chromium --- 33.900 --- Co er --- 845.00 1.690 Lead --- 33.90 0.068 Mercury --- 0.86 0.002 Molybdenum --- 33.90 0.068 Nickel --- 33.90 0.068 Selenium --- 33.90 0.068 Zinc --- 1,170.00 2.340 Environmental Chemists, Inc. # 2015-16868 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. ANALYTICAL & CONSULTING CHEMISTS Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Curie NC 28435 Attention: Wesley Wooten Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemist&com Date of Report: Jan 11, 2016 Customer PO #: Customer ID: 14020008 Report #: 2015-16868 Project ID: Hampstead Town Center Lab ID Sample ID: Collect DatelTirne Matrix Sampled by 1540138 Site: Sludge 12/16/2015 10:25 AM Solid/Sludge wesley wooten Test Method Results Date Analyzed Sludge. Residuals Aluminum EPA 200.7 4250 mg/kg 12/21/2015 Arsenic EPA 200.7 <33.9 mg/kg 12/28/2015 Cadmium EPA 200.7 <33.9 mg/kg 12/28/2015 i Calcium EPA 200.7 5330 mg/kg 12/21/2015 Chromium EPA 200.7 <33.9 mg/kg 12/28/2015 Copper EPA 200.7 845 mg/kg 12/21/2015 Lead EPA 200.7 <33.9 mg/kg 12/28/2015 Magnesium EPA 20o.7 603 mg/kg 12/21/2015 Molybdenum EPA 200.7 <33.9 mg/kg 12/28/2015 --- Nickel EPA 200.7 <33.9 mg/kg 12/28/2015 I Potassium EPA 200.7 307 mg/kg 12/21/2015 Selenium EPA 200.7 <33.9 mg/kg 12/28/2015 ISodium EPA 200.7 828 mg/kg 12/21/2015 Zinc EPA 200.7 1170 mg/kg 12/21/2015 Total Kjeldahl Nitrogen (TKN) EPA351.2 26500 mg/kg 01/07/2016 Nitrate+Nitrite-Nitrogen EPA353.2 5.19 mg/kg 01/04/2016 Total Solids (%) SM 2540 B 1.16 % 12/17/2015 pH SM 4500 H B 7.22 units 12/24/2015 - Ammonia Nitrogen SM 4500 NH3 c 7440 mg/kg 12/21/2015 j Total Phosphorus SM 4500 P F 13600 mg/kg 01/08/2016 Mercury sw848 7471 B <0.862 mg/kg 12/22/2015 -- � Report#:: 2015-168M 0 Page 1 of 3 i Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN nF CusTnnY 6602 Windmill Way Wilmington, NC 2841 OFFICE: 910-392-0223 FAX 910.392-44: Info@environmentalchemists.com CLIENT: &—ty -Kr'V r PROJECT NAME: s�*-•.� % .,, C..�,�e,� REPORT NO: /)o" ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONEIFAX: COPY TO: email: oamptea t5y: t "re s we•+ -A__ SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection F- a w c` a o o t'. m r. c C9 y `o a. �, C tj o m G ut m g PRESERVATION ANALYSIS REQUESTED Date Time Temp z 0 0 c o w S%» f C P r` G G C P r G L ta3J C P G i� qOrq1 G �� y3 C P G 3 G G t. C P ` G G C P G G C P G G C P G I G Transfer Relinquished By: Date/Time Received By: Date/Time 2. Temperature when Received: Accepted: Rejected: Kesample Kequest Delivered By. Received By: Date, Time: ` rnmmonte- TU NA OUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Hampstead Town Center P.O.# Batch Size (gallons): 4,000 Lbs. or Gallons Used: 150 Material Used For Stabilization: Lime Initial pH M MENEM 0 • • ����� ®® 1 • ® 1 1 �® 1 • ®1 • 1 1 �® 1 1 � 1 1 c o U c°� �- In d' 7 a N 7 n M 7 a fD M 7 a M M 7 a O M 7 a 1� N o 7 a N 0 7 a N 0 7 a a0 0 7 a 0 7 a N 0 7 a O 0 7 a f0 O 0 7 a M O 0 7 a O c) o 0 u) C (0 0 0 N C 0) 0 0 N C N 0 C o N C 0 N C N 0 m C N 0 N C N 0 N C o a> 0 m C M a) 0 N C (0 t+) 0 w C 0) t+) 0 w C N v 0 N C N a 0 N C U C- O �t M co W co r` M 0 MM 1n It M M M N CM � co O M M N M N r` N 0 N LO N d' N M N N N •- N O N M �- M r- r` 0� I' M r N � � CDE �- 9 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Hamstead Town Center NPDES Number: WQ0032115 Monitoring Period: From I/1/2015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (timehem) ElAlt B (Alk Treatment)❑ Alt. C (Prior Testing)❑ Alt.D (No Prior Test) ❑ 1 Process to Further Reduce Patio ens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment [3Therm2 iilic ❑ Beta Ra ElGamma Ray ❑ Pasteurization ❑ ..:...................:.... Class B: Alt. (1) Fecal Density ❑ 1 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization p Air Drying ❑ Com osti ig D Aerobic Di estion D Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Slud a !; Pathogen Density um er o Excee- Frequency of Anal Analysis Sample Type Analytical Tech- Minimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal Coliform 3 MPN per 4 grams total solid (dry weight) __ 1- . "'Wa +'aasa 4%;uvn Kudiattlyn t lz)a°l NUAC UL 1 .1107 1— rime indicate niternative nerfhrmM- Alt.1 (VS reduction) ❑]Alt.'] Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) [I JAR. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) [3Alt. 6 (Alk. Stabilization l7 Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) [IAlt. 9 (Injection) [3 0 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ /'w'`. IDTf➢'. iR'A TYALT &4 n ♦ /*draw-1- 1 _ IF A -A it AjA a 1 A i r lvirN i kplease cheep one appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." D "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the =—a wcmusals niion nas ueen made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Wesley Wooten, President Preparer Nam and itle (type or print) V, , 2-zy—/ Signatureof Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 3, 2015 House of Raeford Permit No. WQ0000455 Wallace Plant 1.65 % Solids 7.39 nH Parameter % Mg/Kg Dry Weight % x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 6.890 68,900.000 137.800 Phosphorus 1.830 18,300.000 36.600 Potassium 0.648 6,480.000 12.960 PAN injected)* 3.030 30,301.400 60.603 PAN (surface)* 2.804 28,041.400 56.083 Ammonia Nitrogen 0.452 4,520.000 9.040 Calcium 2.200 22,000.000 44.000 Calcium Carbonate E . --- --- --- Magnesium --- 8,790.000 17.580 Sodium --- 8,240.000 16.480 Sulfur - --- --- Nitrate N / Nitrite N --- 29.400 0.059 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 11,400.00 22.800 Arsenic --- 5.88 0.012 Cadmium --- 5.88 0.012 Chromium --- 17.300 --- Copper --- 207.00 0.414 Lead --- 5.88 0.012 Mercury --- 1.04 0.002 Molybdenum --- 6.06 0.012 Nickel - 18.30 0.037 Selenium --- 6.42 0.013 Zinc --- 236.00 0.472 Environmental Chemists # 2015-02546 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) - (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 I House of Raeford -Wallace Facility Date of Report: Mar 23, 2015 Post Office box 40 Customer PO M Rose Hill NC 28458 Customer 1D: 13030026 Attention: Wayne Benton, ORC Report ##: 2015-02546 Project ID: Digestor Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-05711 Site: Sludge 3/3/2015 11:05 AM Solid/Sludge jay baker/envirochem Test Method Results Date Analyzed Chlordane SW 846 Method 80818/3510 <0.05 mg/L 03/09/2016 Endrin SW 848 Method 8081B13510 <0.0005 mg/L 03/09/2015 Heptachlor SW846 Method 808113/3510 <0.0005 mg/L 03/09/2015 Heptachlor epoxide SW 846 Method 8081BIS510 <0.0005 mg/L 03/09/2016 Lindane SW 846 Method 8081 B/3510 <0.0005 mg/L 03/09/2015 Methoxychlor SW 846 Method 8081B/3510 <0.0005 mg/L 03/09/2015 Toxaphene SW 846 Method 8081B13510 <0.05 mg/L 03/09/2015' 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/11/2015 2,4,5-Trichlorophenoi (TCLP) SW 846 method 8270/3610 <0.050 mg/L 03111/2015 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/1112015 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/11/2015 Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 03/11/2015 • Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/11/2015 Hexachlorobenzene (TCLP) SW 845 method 8270/3510 <0.050 mg/L 03/11/2015 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/11/2015 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/11/2015 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/11/2015 o-Cresol(TCLP) SW 848 method827013510 <0.050mg/L 03/11/2015 Pentachlorophenol (TCLP) SW 846 method B270/3510 <0.250 mg/L 03/11/2015 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/11/2015 2,4,5-TP SW846 Method 8161A <0.0003 mg/L 03/09/2015 __. 2,4-D SW846 Method 8151A <0.0003 mg/L 03/09/2015 1,1-Dichloroethylene SW846 Method 8280/5030 <0.01 mg/L 03/14/2015 1,2-Dichloroethane SW846 Method,826015030 <0.01 mg/L 03/14/2015 Benzene sw640 Method 8200/5030 <0.01 mg/L 03/14/2015 Carbon Tetrachloride SW846 Method.8260/5030 <0.01 mg/L 03/14/2015 Report #:: 2015-02546 Page 1 of 3 Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 -L (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING - CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 House of Raeford -Wallace Facility Date of Report: Mar 23, 2015 Post Office box 40 Customer PO #: Rose Hill NC 28458 Customer ID: 13030026 Attention: Wayne Benton, ORC Report #: 2015-02546 Project 1D: Digestor Sludge Chlorobenzerie SW846 Method 828016030 <0.01 mg/L 03/14/2015 Chloroform SW846 Method 8260/5030 <0.01 mg/L 03/14/2015 Methyl ethyl ketone SW846 Method 8260/5030 <0.05 mg/L 03/14/2015 Tetrachloroethylene SW846 Method 826015030 <0.01 mg/L 03/1412015 Trichloroethylene SW846 Method 8260/5030 <0.01 mg/L 03/14/2015 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 03/14/2015 RC I Cyanide EPA335.4 <0.122 mg/kg 03/09/2015 Sulfide SM 4500 s o 22.5 mg/kg 03/06/2015 Ignitability SW 846 method 1010 >212 OF 03/1012015 Sludge Residuals Aluminum EPA200.7 11400 mg/kg 03/11/2015 Arsenic EPA200.7 <5.88 mg/kg 03/11/2016 Cadmium EPA 200.7.- <5.88 mg/kg 03/11/2015 Calcium EPA200.7 22006 mg/kg 03/12I2015 Chromium EPA200.7 17.3 mg/kg 03/1112015 Copper EPA 200.7 207.mg/kg 03111 /2015 Lead EPA200.7 <5.88 mg/kg 03/11/2016 Magnesium EPA200.7 8790 mg/kg 03/1212015 Molybdenum EPA200.7 6.06 mg/kg 03/11/2015 Nickel EPA260.7 18.3 mg/kg 03/11/2016 Potassium EPA200.7 6480 mglkg 0311212015 Selenium EPA200.7 6.42 mg/kg 03/11/2015 Sodium EPA 200.7 8240 mg/kg 03/12/2015 Zinc EPA200.7 236 mg/kg 03/11/2015 Ammonia Nitrogen EPA350.1 4520 mg/kg 03/04/2016 Total Kjeldahl Nitrogen (TKN) EPA351.2 68900 mg/kg 03/11/2015 Nitrate+Nitrite-Nitrogen EPA353.2 29.4 mg/kg 03104/2015 Total Solids (%) SM 2540 a 1.65 % 03/09/2015 PH SM 4500 H B 7.39 units 03/06/2016 Report*: 2015-02546 Page 2 of 3 F07 7 "44 Environmental Chemists, Inc. • 6602 Windmill Way a, Wilmington, NC 28405 '- } (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL $ CONSULTING - CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 House of Raeford -Wallace Facility Date of Report: Mar 23, 2015 Post Office box 40 Customer PO M Rose Hill NC 28468 Customer ID: 13030026 Attention: Wayne Benton, ORC Report M. 2015-02546 Project ID: Digestor Sludge Total Phosphorus SM 4500 P F mg/kg 18300 m g 03/11/2015 Mercury SW846 7471E <1.04 mg/kg 03/12/2015 TCLP Metals Arsenic EPA200.8 <0.100 mg1L 03/12/2015 Barium EPA200.8 <0.100 mg/L 03/12/2016 Cadmium EPA200.8 <0.100 mg/L 03/12/2015 Chromium EPA200:8 <0.100 mg/L 03/12/2015 Lead EPA200.8 <0.100 mg/L 03/12/2016 Selenium EPA 200.8 <0.100 mg/L 03/13/2015 Silver EPA200.8 <0.100 mg/L 03/12/2015 Mercury EPA 245.1 <0.0020 mg/L 03/1812015 Comment: Sludge residuals, exc apt pH, reported on a dry weight basis. pH. reported on an as received basis. Reviewed by: Reportk 201 "2548 il Page 3 of 3 Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC6602 OFFICE: 10� 920 2Way13FAXton910392-44: NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DL5 CERTIFICATION # 37729 info@environmentalch17ists.coln COLLECTION AND CHAIN OF Cl lSTr)nv CLIENT: �►s�-+ e�- &Jo jot- PROJECT NAME: ���c � A, s� - slb c% REPORT NO: ADDRESS: CONTACT NAIVE: PO NO: REPORT TO: tj „ � ) �4 PHONE/FAX: . COPY TO: CLr:s /'{av email: Sampled Sv: i -or SAMPI F TYPF• I = Inftnnn4 F = FfPlnnnt W = W011 CT = Cfrn- Cf1 = Cni) CI - Q1-4 e Sam le Identification p Collection N � E °: �_ a `o '� _ Y o 0� d o c E " 0° �2 z PRESERVATION ANALYSIS REQUESTED Pqte Time Temp W Zo Z s v x = S = a Z y ~ x x o sLf4r, flair C P C P _ �G� G G C P A/. I f' G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 2. Temperature when Received: y Acceptea: rce ctp rtesample rrq stea: Delivered By: Received By Date: 3 �i Time: 3 �' . ) ! .-- Comments: --� TURNAROUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: House of Raeford / Wallace P.O.# Batch Size (gallons): 30,000 Lbs. or Gallons Used: 2,000 Ibs Material Used For Stabilization: Lime Initial pH >12 pH 2 Hour H 24 Hour pH Operator Date pH Temp C Corr. Factor+ cortecmd pH Time pH Temp C Corr. Factor+ Cormtod pH Time pH Temp C Corr. Factor+ Corrected pH Time pH Temp C Corr. Factor+ Corrected PH Time Initials 1/6/2013 7.10 11.1 -0.42 6.68 759 12.61 11.2 -0.41 12.20 810 12.59 11.3 -0.41 12.18 1010 12.55 12.0 -0.39 12.16 813 1/1312013 7.15 9.7 -0.46 6.69 731 .12.74 9.8 -0.46 12.28 746 12.73 9.9 -0.45 12.28 946 12.54 10.1 -0.45 12.09 755 1/2012013 7.21 9.9 -0.45 6.76 654 12.66 10.1 -0.45 12.21 659 1 12.6 10.2 -0.44 12.16 959 12.57 10.5 -0.44 12.14 707 1/26n013 7.10 9.5 -0.47 6.64 650 12.69 9.7 -0.46 12.23 700 1 12.7 9.9 -0.45 12.25 900 12.511 10.1 -0.45 12.06 705 2/4/2013 7.39 10.6 -0.43 6.96 700 2.581 10.8 -0.43 12.15 709 12.62 11.1 -0.42 .12.20 910 12.47 11.2 -0.41 12.06 713 211012015 7.33 14.2 -0.32 7.01 1 648 12.46 14.2 -0.32 12.14 658 12.47 14.4 -0.32 12.151 758 12.19 14.0 -0.33 11.86 706 2/1812015 7.22 14.3 -0.32 6.90 745 12.43 14.4 -0.32 12.11 800 12.44 14.5 -0.32 12.13 1000 12.34 14.4 -0.32 12.02 800 2/ w=5 1 7.18 14.4 -0.32 6.86 650 12:52 14.6 -0.31 12.21 704 12.54 14.7 -0.31 12.23 905 12.33 14.8 -0.31 12.02 705 3/212015 1 7.41 14.5 -0.32 7.10 645 12.51 14.7 -0.31112.201 700 12.58 14.9 -0.3 12.28 900 12.48 14.7 -0.31 12.171 705 4/1/2015 7.18 15.1 -0.3 6.88 730 12.311 15.3 -0.29 12.02 741 12.51 15.4 -0.29 12.22 941 12.451 15.5 -0.29 12.171 744 4/22/2015 7.35 15.3 -0.29 7.06 648 12.471 15.6 -0.28 12.19 701 12.46 15.6 -0.28 12.18 901 12.381 15.7 -0.28 12.101 715 4/2812015 7.24 18.0 -0.21 7.03 615 12.43 18.3 -0.2 12.23 622 12.421 18.4 1 -0.2 12.22 822 12.281 18.3 -0.20 12.081 644 5/4/2015 7.28 21.3 -0.11 7.17 640 12.38 21.5 -0.11 12.28 655 12.36 21.6 -0.1 12.26 855 12.21 21.5 -0.11 12.11 700 5/12/2015 7.44 22.3 -0.08 7.36 648 12.43 22.4 -0.08 12.35 659 12.27 22.5 -0.08 12.20 759 12.37 22.3 -0.08 12.29 701 s/1612015 7.34 23.1 -0.06 7.28 705 12.25 23.2 -0.05 12.20 725 12.21 23.4 -0.05 12.16 925 12.22 23.5 -0.05 12.18 725 5/26/2015F7�495::F2-51 2 24.2 -0.02 7.27 630 12.19 24.4 -0.02 12.17 640 12.15 24.5 -0.02 12.14 840 11.99 24.4 -0.02 11.97 645 6/3rz015 10.0031, 7.45 1 600 12.21 25.3 0.009 12.22 609 12.18 25.4 0.012 12.19 809 12.09 25.4 0.01 12.10 616 L, Q N 4 N M M M O M P N d N r` N � IA r N - O ID O ri O InO o O N c, ' O ry v N f• N O e7 n n CD Pf 0) t7 N O ID 7 G G C C O G C C C C G C C o o O o 0 0 O O o 0 0 0 0 0 0 N 0 V 9 9 7 y y 7 7 7 O to N C N G N C N G f/! G tll G C N m C N G a a $ 'ti 5 2 a;ILa. a a a a a. IL a a tL a. a 5 g 5r �. 211121 v a O O Co 1-. 0 0� M N � O O M I.- 'w 0� M N � O O M n 'D to 'W M N V .- O F �7 M M M M M M M M M N N N N N N N N N N %- V- r- %- WW- e- r- T R i LEWIS FARMS AND LIQUID WASTE, INC. WO 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: House of Raeford / Wallace P.O.# Batch Size (gallons): 30,000 Lbs. or Gallons Used: 2,000 Material Used For Stabilization: Lime Initial pH >12 pH 2 Hour H 24 Hour pH Operato Date pH Temp C Corr. Factor+ Correetea H Time pH Temp C Corr. Factor+ corrected H Time pH Temp C Corr. Factor ConWed H Time pH Temp C Corr. Faclor+ conectea pH Time Initials 6►912015 7.37 25.3 10.009 7.38 751 12.20 25.3 0.009 12.21 804 12.19 25.4 10.012 12.20 1004 12.091 25.2 1 0.01 12.10 810 6/21/2015 7.2 25.5 0.015 7.22 646 12.17 25.6 0.018 12.19 659 12.14 25.7 0.021 12.16 859 12.08 25.5-1 0.02 12.10 705 7►712015 1 7.24 26.0 0.03 7.27 1 636 12.23 26.1 0.033 12.26 649 12.19 26.2 0.036 12.23 849 12.151 26.1 0.03 12.18 703 7/18/2015 7.11 26.1 0.033 7.14 1 706 12.17 26.2 0.036 12.21 715 12.05 26.3 0.039 12.091 915 12.051 26.1 0.03 112.08 715 1,0 7/28/2015 7.35 26.2 0.036 7.39 1 716 12.26 26.3 0.039 12.30 731 12.17 26.4 0.042 12.21 931 12.12 26.2 0.04 12.16 733 8►3/2015 7.42 24.3 -0.02 7.40 701 12.21 24.5 -0.02 12.20 714 12.2 1 24.5 1 -0.02 12.19 914 12.09 24.4 -0.02 12.07 714 8/12/2015 7.2 23.9 -0.03 7.17 731 1 12.231 24.1 -0.03 12.20 740 12.16 24.2 -0.02 12.14 940 12.11 24.1 -0.03 12.08 743 8/22/2015 7.51 23.4 -0.05 7.46 701 12.24 23.5 -0.05 12.20 712 12.17 23.6 -0.04 12.13 912 12.02 23.3 -0.05 11.97 716 91112015 7.42 21.8 -0.1 7.32 651 12.35 22.0 -0.09 12.26 700 12.31 22.1 -0.09 12.22 900 12.17 21.9 -0.09 12.081 700 9/9/2015 7.26 21.1 -0.12 7.14 602 12.34 21.3 -0.11 12.23 610 12.31 21.3 -0.11 12.201 810 12.081 21.1 -0.12 11.96 610 9/1512015 7.35 20.2 -0.14 7.21 631 12.28 20.4 -0.14 12.14 641 1 12.19 20.6 -0.13 12.06 841 1 12.171 20.5 -0.14 12.04 645 9/ wo15 1 7.21 1 19.7 -0.16 7.05 1 750 12.29 19.9 -0.15 12.14 759 12.26 20.1 -0.15 12.11 1001 12.2 19.9 -0.15 12.05 805 15 •7.11 17.2 -0.23 6.88 716 12.35 17.3 -0.23 12.12 725 12.45 17.5 -0.23 12.23 925 12.38 17.4 -0.23 12.15 725 015 7.4 15.9 -0.27 7.13 744 12.38 16.1 -0.27 12.11 758 12.38 16.2 -0.26 12.12 958 12.29 16.1 -0.27 12.02 801 015 i 7.28 14.7 -0.31 6.97 722 12.48 14.9 -0.3 12.18 732 12.45 15.0 -0.3 12.15 932 12.45 14.8 -0.31 12.14 738 o15 7.37 13.2 -0.35 7.02 801 12.47 13.5 -0.35 12.13 812B2.5 2.48 13.6 -0.34 12.14 1012 12.4 13.4 -0.35 12.05 815 015 7.25 12.9 -0.36 6.89 659 12.53 12.3 -0.38 12.15 709 L 12.4 -0.38 112.121 909 1112.491 12.3 -0.38 12111 715 C � �� O N a a N O U1 a s 01 O el a 'a (G M O el a a M M O el a a O M O N 7 a A Cl! O N a N 0 fe 7 a N O y 7 a O O fA 7 a N O N a a N .- O H1 a a CD O O N a 'a 10 O O e) 7 a M O C N 7 s O l+f O O m 7 e M ID D O a 7 C g1 Cl O o a 7 C N c � ' 0 � 7 C m o a � C N O yy 7 G V N 0 co C t-- N O a C O n O a C f� q 0 m C 2 ID M 0 m C 2 W q 0 a C 2 N O 0 a C 2 1A a O m C g U a d O 'Cr O M O M ti M to M tt7 M --* M M M N M r M O M M N 00 N t%� N t0 N w N q N M N N N r N O N 0) r 00 r f- r (0 r to r 'V r M r N r r r 0 r t- M LEWIS FARMS AND LIQUID WASTE, INC. WO 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: House of Raeford / Wallace P.O.# Batch Size (gallons): 30,000 Lbs. or Gallons Used: 2,000 Material Used For Stabilization: Lime Initial pH >12 pH 2 Hour pH 24 Hour pH Operato Date pH Temp C Corr. Factor + corrected H Time pH Temp C Corr. Factor + corrected H Time pH Temp C Corr. Factor + a Cod H Time pH Temp C Corr. Factor + Corrected pH Time Initials 11/11/20151 7.41 12.2 1 -0.38 7.03 644 12.52 12.4 -0.38 12.14 700 12.54 12.5 -0.38 12.17 900 12.51 12.6 -0.37 12.14 705 11/16/2015 7.25 12.9 -0.36 6.89 750 12.44 13 -0.36 12.08 800 12.46 13.1 -0.36 12.10 1000 12.42 13.2 -0.35 12.07 800 11/28/2ol5 7.37 13.2 -0.35 7.02 716 12.45 13.1 -0.36 12.09 726 12.47 13.2 -0.35 12.12 926 12.4 13.2 -0.35 12.05 726 12/1/2015 7.28 14.7 -0.31 6.97 1 744 12.411 14.6 -0.31 12.101 752 12.42 14.7 -0.31 112.11 952 12.381 14.7 -0.31 12.071 752 12/9/2015 7.4 15.9 -0.27 7.13 722 12.391 15.8 -0.28 12.11 730 12.41 15.9 -0.27 112.14 930 12.37 15.9 -0.27 12.10 731 12/14/2015 7.11 17.2 -0.23 6.88 801 12.371 17.1 -0.24 12.13 810 12.39 17.0 -0.24 12.15 910 12.28 17.1 -0.24 12.04 1010 12/19/2015 7.21 19.7 -0.16 7.05 659 12.42 19.8 -0.16 12.26 707 12.42 19.9 -0.15 12.27 907 12.32 20.0 -0.15 12.17 715 0 (i a O NNNNNNNNNN1/iNNNN a. � G 7 a. M O 7 a M C 7 d m M G 7 a O M C o- t• N G 7 a O N O 7 a N C 7 o. O r G a O � C 7 n N � C 7 a mo C 7 a 10 O 7 a O 7 a C) n O N M O c N >>N C m c C ry O N o :3 C m o W O n f a O :3 2 c o O NNC 2 c� O 2 so O rn o 1>9 C N O N n o N> 2 G U 0. W O q O M 00 M r- M (0 M to v) M M N M . (r) O M C) N 00 N f` N (0 N to N t N ca N N N N O N Cf •- O r- f` r (0 to r- T - M r- N - v- •- O F- ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facilih` Name: Lewis Farms and Liquid Waste, Inc. WWTP Name: Wallace Chicken Processing Plant Monitoring Period: From I/l/2015 To WQ Permit Number: NPDES Number: 12/31/2015 WQ0000455 NC0003344 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerfinrmvd- Class A: Alt. A (time/tern) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ . . . . . Class B: JAIt. (1) Fecal Density❑ Alt. (2) Process to Significantly Reduce Patho ens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization p Air Drying Composting ❑y Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative peirfformed (Class A or Class B) complete the llowing monitoring data: Parameter Allowable Level in Sludge Pathogen Density °11 ro Excec- dences Frequency of Analysis Sample Type ` `ce 1'ech- Minimurr Geo. Mean M&ximuH Units Fecal Colifotm 2 x 10 to the 6th power per gran► of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Saln►onella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ JAlt. 3 (30-day bench) ❑ I Alt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization El JAR 7 (Drying - Stable) ❑ 1 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ JNo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." _Wayne Bentoq, ORC Prepare ame and Till type or rint) Land Applier Name and Title (if applicable)(type or print) Sign tune f Preparer* DOtSignature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 23, 2015 Kenwood 1.72 % Solids 6.89 pH Permit No. WQ0000455 Nitrogen (TKN) 0.243 2,430.000 4.860 Phosphorus 0.051 513.000 1.026 Potassium 0.279 2,790.000 5.580 PAN (injected)* 0.242 2,418.100 4.836 PAN (surface)* 0.126 1,258.100 2.516 Ammonia Nitrogen 0.232 2,320.000 4.640 Calcium 1.800 18,000.000 36.000 Calcium Carbonate E . --- --- --- Magnesium --- 1,810.000 3.620 Sodium --- 6,980.000 13.960 Sulfur --- --- --- Nitrate N / Nitrite N --- 65.100 0.130 Barium --- --- --- Chloride --- --- --- Iron --- --- Aluminum --- 6,630.00 13.260 Arsenic --- 28.90 0.058 Cadmium --- 28.90 0.058 Chromium --- 28.900 --- Copper --- 508.00 1.016 Lead --- 28.90 0.058 Mercury --- 1.28 0.003 Molybdenum --- 28.90 0.058 Nickel --- 28.90 0.058 Selenium --- 28.90 0.058 Zinc --- 1,620.00 3.240 Environmental Chemists, Inc. # 2015-15657 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. F"1007 --71 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax ® 710 Bowsertown Road, Manteo, NC 27954 • 252A73.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS Onslow Water & Sewer Authority Post Office Box 1415 Jacksonville NC 28541 Attention: Mark Young Lab ID Sample ID: 15-37332 Site: Digester info@environmentalcbemists.com Date of Report: Dec 15, 2015 Customer PO #: Customer ID: 08100092 Report #: 2015-15657 Project 1D: Kenwood WTP Collect Date/Time Matrix Sampled by 11/23/2015 11:40 AM Solid/Sludge M. Young/ P. Grimard Test Method Results Date Analyzed Sludge Residuals Aluminum EPA20o.7 6630 mg/kg 11/24/2015 Arsenic EPA200.7 <28.9 mg/kg 11/24/2015 Cadmium EPA2DO.7 <28.9 mg/kg 11/24/2015 Calcium EPA200.7 18000 mg/kg 11/25/2015 Chromium EPA200.7 <28.9 mg/kg 11/24/2016 Copper EPA200.7 508 mg/kg 1112412015 Lead EPA200.7 <28.9 mg/kg 11/24/2015 Magnesium EPA200.7 1810 mg/kg 11/25/2015 Molybdenum EPA200.7 <28.9 mg/kg 12/01/2015 Nickel EPA200.7 <28.9 mg/kg 11/2412015 Potassium EPA200.7 2790 mg/kg 11/25/2015 Selenium EPA200.7 <28.9 mg/kg 11/24/2015 Sodium EPA200.7 0980 mg/kg 11/25/2015 Zinc EPA200.7 1620 mg/kg -11/2412015 Total Kjeldahl Nitrogen (TKN) EPA351.2 2430 mg/kg 12/11/2015 Nitrate+Nitrite-Nitrogen EPA353.2 65.1 mg/kg 12/14/2015 Total Solids (%) SM 2540 B 1.72 % 11/24/2015 pH SM 4500 H B 6.89 units 12/11/2015 Ammonia Nitrogen SM 450o NH3 c 2320 mg/kg 12/01/2015 Total Phosphorus SM 4500 P F 513 mg/kg 12/11/2015 Mercury Sw8467471B <1.28 mg/kg 12/02/2015 Report*: 201 &15657 Page 1 of 3 SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Dec 28, 2015 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2015-17059 Project ID: Kenwood Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-40602 Site: 1 12/21/2015 11:00 AM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 a 2.65 % 12/22/2015 Fecal Density SM 9221C E MPN 24 hr 503 1132076 MPN/g 12/22/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-40603 Site: 2 12/21/2015 11:02 AM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids M SM 2540 a 2.64 % 12/22/2015 Fecal Density SM 9221C E MPN 24 hr 503 1136364 MPN/g 12122/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-40604 Site: 3 A2/21/2015 11:04 AM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 a 2.64 % 12/22/2015 Fecal Density SM 9221C E MPN 24 hr 503 492425 MPN/g 12/2212015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-40605 Site: 4 12/21/2015 11:06 AM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 a 2.55 % 12/22/2015 Fecal Density SM 9221C E MPN 24 hr 503 1176471 MPN/g 12/2212015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-40606 Site: 5 12/21/2015 11:08 AM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 s 2.60 % 12/22/2015 Fecal Density SM 9221C E MPN 24 hr 503 1923077 MPN/g 12/22/2015 Report M: 2015.17059 Page 1 of 2 [envirochem ANALYTICAL & CONSULTING CHEMISTS Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax Lab ID Sample ID: 15-40607 Site:6 Test Method Total Solids (%) SM 2540 B info@environmentalchemists.com Date of Report: Dec 28, 2015 Customer PO #: Customer ID: 14020008 Report #: 2015-17059 Project ID: Kenwood Collect DatelTime Matrix 12121 /2015 11:10 AM Solid/Sludge Results 2.64 % Sampled by wesley wooten Date Analyzed 12/22/2015 Fecal Density SM 9221C E MPN 24 hr 503 1893940 MPN/g 12/22/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-40608 Site: 7 12/21/2015 11:12 AM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.77 % 12/22/2015 Fecal Density SM 9221C E MPN 24 hr 503 866426 MPN/g 12/22/2015 Comment: Results reported on a dry weight basis. Reviewed by: Report #:: 2015-17059 Page 2 of 2 of 4= ENVIRONMENTAL CHEMISTS, INC OFFICE: 10! 920 2'3FAX910392-44 Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS; DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY CLIENT: Ciw�s i.„ s PROJECT NAME: REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: tJ4s 47 C% SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection F� d o N 0 °o o` �° E 0 _ c (7 ° `o c a " v J o L E " O IL m z PRESERVATION ANALYSIS REQUESTED DateFTime Temp w o Z x a x r, i x x a z o F w x o �� C P G G�1+ L fr�L. C P G G 1 C P G G r oC C P G G steal C P `k��'� G G .« C P 'k G G Ir�z lkgt'o� G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: Accepted: Rejecte : Resample Re ue ted: Delivered By: Received By: Date: IL Ls . Time: wf r''_nmmnntc- TI IRNAR01INn. LEWIS FARMS WQ0000455 Kenwood WWTP Date Fecal Coliform MPN per gram Log 12/21/15 1,132,076 6.0539 12/21/15 1,136,364 6.0555 12/21/15 492,425 5.6923 12/21/15 1,176,471 6.0706 12/21/15 1,923,077 6.2840 12/21/15 1,893,940 6.2774 12/21/15 866,426 5.9377 Total 1 42.3714 Average 6.0531 Geometric Mean 121292 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility fume: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Kenwood NPDES Number: NCO030813 Monitoring Period: From I/12015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (titne/tem) ❑ 1 Alt B (Alk Treatment) ❑ Alt. C or Testing) ❑ A1t.D (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density El All. (2) Process to Sigaificantly Reduce Patho ens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Coinposting ❑ JAcrobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative peirfformed (Class A or Class B) complete the followin monitorin data: Parameter Allowable Level in in Sludge Pathogen Density NUMDer ot Excec Frequency of Analysis y Sample Typeninue na tea Tech Minimum Geo. Mean Maximum Unitsenao_ Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 492,425 1,129,948 1,923,077 MPN/g 0 Annual Grab sM 9221 Ct: CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.] (VS reduction) ❑ Alt. 2 (40-day bench) ❑ JAlt. 3 (30-day bench) ❑ JAR. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ I Alt 7 (Drying - Stable) ❑ JAlt. 8 (Drying - Unstable) ❑ Aft. 9 (Injection) ❑ Alt. 10 (Incorporation) El INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) O "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." (] "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mark Young, Supervisor Wesley Wooten, President Preparer Name /nd�Title typpe r print) Land Applier Name a Title (if applicablextype or print) ,tI[ [; 2/22M e �/Z — Signature o Preparer . Date Signature Land Applier (if applicable) Date "`Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 3, 2015 Majestic Oaks WWTP Permit No. WQ0000455 0.32 % Solids 6.6 PH M I Nitrogen (TKN) 5.993 59,927.000 119.854 Phosphorus 3.627 36,265.000 72.530 Potassium 0.805 8,050.000 16.100 PAN (injected)* 1.840 18,404.180 36.808 PAN (surface)* 1.810 18,102.680 36.205 Ammonia Nitrogen 0.060 603.000 1.206 Calcium 2.240 22,400.000 44.800 Calcium Carbonate E . --- --- --- Magnesium --- 4,948.000 9.896 Sodium --- 32,325.000 64.650 Sulfur --- --- --- Nitrate N / Nitrite N -- 3.980 0.008 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 2,455.00 4.910 Arsenic --- 2.50 0.005 Cadmium --- 0.71 0.001 Chromium --- 62.000 --- Copper --- 381.00 0.762 Lead --- 6.50 0.013 Mercury --- 0.84 0.002 Molybdenum --- 8.00 0.016 Nickel --- 21.00 0.042 Selenium --- 5.00 0.010 Zinc --- 795.00 1.590 Environment 1, Inc. # 292E *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. a /I rt I n MAJESTIC OAKS (ENVIROLINK) C/O ENVIROLINK P.O. BOX 670 BAILEY ,NC 27807 PARAMETERS PH (not to be used for reporting) Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), n:g/kg Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry %%,t.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Dale Analyst Code 6.6 12/03/15 KKF 4500HB-00 2455 12/21/15 LFJ EPA200.7 <2.5 12/09/15 MTM 311313-04 22400 12/10/15 LFJ EPA200.7 0.71 12/21/15 XITM 311313-04 381 12/10/15 LFJ EPA200.7 62 12/10/15 LFJ EPA200.7 6.5 12/17/15 MTM 311313-04 4948 12/10/15 LFJ EPA200.7 0.84 12/17/15 JMN 245.1 R3-94 21 12/10/15 LFJ EPA200.7 8050 12/21/15 LFJ EPA200.7 <5.0 12/23/15 MTM 3113B-04 32325 12/11/15 JMN 3111E-99 795 12/21/15 LFJ EPA200.7 0.32 12/08/15 KDS 2540G-97 59927 12/10/15 RND 351.2 R2-93 603 12/08/15 RAJ 350.1 R2-93 36265 12/10/15 RAJ 365.4-74 <3.98 12/09/15 RND 353.2 R2-93 12166 12/14/15 SEJ 8 12/10/15 LFJ EPA200.7 ID#: 292 E DATE COLLECTED: 12/03/15 DATE REPORTED : 12/30/15 REVIEWED BY: I'llNironinexrt I, Lie. L',0_11ox^?6`5, 1.t�[ 0a.kjlaont D.L. ci col)vi):ie..\C 27� 5s CHAIN OF CUSTODY Rt-XORD a'l:a_re _�_.._ or _A_ )I:ti(til717(7110N Phooc. (2 � 2,) '>6-6-108 • f a.x t 2. +2 r 7�t;-riti ? CHLORINE rJEJTRALf�Ed AT COLLECTION r CLIENT- 292 E Week: 26 pH CHECK (LAS) MAJESTIC OAKS (ENVIROLIW M tiWA144. P P P P P P P } CONTAINER TYPE,P,G C/O ENWIROLINK P.O. BOX 670 BAILEY NC 27807 - A A A A A A A CHEMICAL PRESERVATION A -NONE D-NAOH j (252) 235-4900 v • ue i u, PCL I LU S-HNO; E-HCL rU z ' w COLLE ION n �� U a z c r- H;sr r .. ZINC. ACLT'ATE,'NAOI•i `a ?; , tz F Z (x G. NATHIOSULFATE SAMPL.ELOCATION 0AT); TIME -' u �`-.' 0 x a .9 ,c c Q O w z a --ShdbgSampk / A �{% a • $ rrib { �•• r CLASSI FICATION: WASTEWATER (NPDES) 1, DRINKING WATER DWQ,GW - - ❑ SOLID WASTE SECTION CHAIN OF CtISTODY (SrALi MAINTAINEC) DURP�PMENLQELIVERY — N SAMPLES COLLECTED BY: I {Please PtinQ COMKilENTS I SAMPLES RECEIVED IN LAB AT'..Zi_-.. _C RRIN0 0SHED BY 'SIG.) (SAMPLER) AT, TIME REt-CEiVtD BY i ' ; � ATETIME i _ 3t3 RELINQUISHED v (SIG,) DATE. -TIME RECEIVED HY ;filly.) DAT"F_;TIME RELINQUISHEDBY(SIG.i DATE. -TIME RECEIVEPBYiSIG-. DAMTIME t a Ilti tcr, n t t I Sampler must place £i "C" for Composite Sample or a "G" fol' P L.ERSE RUD illStt list oils fo ({rltt`1I titow. �N! tho I', fSt' SiL h. Fc)RM n ; �' - k,mh .', fYiI11P to ihP hltli kc ahn,r for onrh n5ran,iiar ron„actari No 9 Q Z d 1 d LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Majestic Oaks P.O.# Batch Size (gallons): 16,000 Lbs. or Gallons Used: 1,000lbs Material Used For Stabilization: Lime Initial pH >12 pH 2 Hour pH 24 Hour pH Operator Date pH Temp C Corr. Factor + Corrected pH Time pH Temp C Corr. Factor + Corrected pH Time pH Temp C Corr. Factor + Corrected pH Time pH Temp C Corr. Factor + Corrected pH Time Initials 1/15/2015 6.60 11.1 -0.42 6.18 751 12.51 11.2 -0.41 12.10 815 12.49 11.3 -0.41 12.08 1015 12.38 12.0 -0.39 11.99 815 WW 6/9/2015 7.45 25.1 0.003 7.45 630 12.21 25.3 0.009 12.22 700 12.18 25.4 0.012 12.19 900 12.09 25.4 0.01 12.10 705 WW 9/3/2015 7.18 21.1 -0.12 7.06 654 12.21 21.4 -0.11 12.10 705 12.25 21.5 -0.11 12.15 905 12.19 21.2 -0.11 12.08 707 WW 9/28/2015 7.22 21.8 -0.1 7.12 650 12.40 22 -0.09 112.31 700 12.42 22.1 -0.09 12.33 900 12.38 22.0 -0.09 12.29 715 WW 11/23/2015 7.39 17.6 -0.22 7.17 632 12.58 17.8 -0.22 12.36 645 12.62 17.9 -0.21 12.41 845 12.58 17.7 -0.22 12.36 702 WW 12/29/2015 7.33 15.4 -0.29 7.04 648 12.461 15.6 -0.28 12.18 658 12.47 15.7 -0.28 12.19 758 12.19 15.8 -0.28 11.91 706 WW C LO N d1 (D M O � �' O U) N O (o M U N U L V O 7 a V O 7 a M O 7 a M O 7 a M O 7 a ci O 7 a N O 7 a N O 7 a N O 7 M r- O 7 M r. O 7 M . O 3 M O O 7 M O O 7 M O O 7 M O O O W C 2 O O N C o O fA C 2 oo c M O N C 2 O 41 C (v O N C N O N C N O N C M O N C O N 7 C O N 7 C o � : C O N 7 C o N 3 C U C- E O � M m 00 m f` m (o m LOII- m M M M N M M O M M N 00 N r- (V (0 N rn N Nr N M N�- N CD 00 1- (O � -IT N O a� H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Majestic Oaks NPDES Number: WQ0030088 Monitoring Period: From 1/I/2015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T. 1106) - Please indicate level achieved and alternative performed: Class A: All. A (time/temp) ❑ Alt B (Alk Treatment)[] I Alt. C (Prior Testis )❑ A1t.D o Prior Test) 1 Process to Further Reduce Patho ens E3 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ray ❑ 1 Gamma Ka ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Densi [3 Alt. (2) Process to Si ificantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization El Air Drying ❑ Composting ❑ JAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the followinj monitoring data: Parameter Allowable Level in Sludge in Pathogen Density NumDer or Excee- Frequency of Analysis Y Sample Type na ica Tech - ninup inimu Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids M PN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry wei t Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed: Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAlt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization El Alt 7 (Drying -Stable) ❑ lNo JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ vector attraction reduction alternatives were performed O CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer Name and T' le (type or print) Land Applier Name and Title (if applicable)(type or print) Signatur f Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: February 24, 2015 Morehead City 22.20 % Solids 6.75 pH Permit No. WQ0000455 Nitrogen (TKN) 2.220 22,200.000 44.400 Phosphorus 1.880 18,800.000 37.600 Potassium 0.361 3,610.000 7.220 PAN (injected)* 0.814 3,869.500 7.739 surface * 0.787 3,777.000 7.554 mmonia Nitrogen 0.055 546.000 1.092 IPAN alcium 4.300 43,000.000 86.000 alcium Carbonate E . --- --- --- a esium 0.469 4,690.000 9.380 Sodium 0.414 4140.000 8.280 Sulfur --- --- --- Nitrate N / Nitrite N --- 1,100.000 2.200 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 13,100.00 26.200 Arsenic --- 4.31 0.009 Cadmium --- 4.31 0.009 Chromium --- 12.400 --- Copper --- 744.00 1.488 Lead --- 11.90 0.024 Mercury --- 1.43 0.003 Molybdenum --- 4.31 0.009 Nickel --- 9.78 0.020 Selenium --- 5.28 0.011 Zinc --- 929.00 1.858 Environmental Chemists, Inc. 2015-02252 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. envirochem 6602 Windmill Way • W.1riington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town Of Morehead City Date of Report: Mar 20, 2015 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: C. Sutton Report #: 2015-02252 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-05019 Site: Sludge Class B 2/24/2015 Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Chlordane SW 846 Method 8081B/3510 <0.05 mg/L 03/04/2015 Endrin SW 846 Method 8081B/3510 <0.0005 mg/L 03/04/2015 Heptachlor SW 846 Method 80818/3510 <0.0005 mg/L 03/04/2015 Heptachlor epoxide SW 846 Method 8081B/3510 <0.0005 mg/L 03/04/2015 Lindane SW 846 Method 8081B/3510 <0.0005 mg/L 03/04/2015 Methoxychlor SW 845 Method 8081B/3510 <0.0005 mg/L 03/04/2015 Toxaphene SW 846 Method 8081 B1351 0 <0.05 mg/L 03/04/2015 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mq/L 03/04/2015 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/04/2015 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270M10 <0.050 mg/L 03/04/2015 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/04/2015 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/04/2015 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/04/2015 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/04/2015 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/04/2015 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/04/2015 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/04/2015 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/04/2015 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 03/04/2015 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/04/2015 Paint Filter Test SW 846 Method 9095 A pass 03/19/2015 2,4,5-TP SW846 Method 8151A <0.0003 mq/L 03/09/2015 2,4-D SW846 Method 8151A <0.0003 mg/L 03/09/2015 1, 1 -Dichloroethylene SW846 Method 8260/50�0 <0.01 mg/L 03/14/2015 1,2-Dichloroethane SW846 Method 8260/5030 <0.01 mg/L 03/1412015 Benzene SW846 Method 8260/5030 <0.01 mg/L 03/14/2015 Report #:: 2015-02252 Page 1 of 4 Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town Of Morehead City Date of Report: Mar 20, 2015 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: C. Sutton Report #: 2015-02252 Project ID_ Sludge Carbon Tetrachloride SW846 Method 8260/5030 <0.01 mg/L 03/14/2015 Chlorobenzene SW846 Method 8260/5030 <0.01 mg/L 03/14/2015 Chloroform SW846 Method 8260/5030 <0.01 mg/L 03/14/2015 Methyl ethyl ketone SW846 Method 8260/5030 <0.05 mg/L 03/14/2015 Tetrachloroethylene SW846 Method 8260/5030 <0.01 mg/L 03/14/2015 Trichloroethylene SW846 Method 8260/5030 <0.01 mg/L 03/14/2015 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 03/14/2015 RCI Ignitability EPA 1030 <0.8 mm/sec 02/27/2015 Cyanide EPA 335.4 <0.125 mg/kg 03/05/2015 Sulfide SM4500 S D 0.27 mq/kq 02/27/2015 Sludge Residuals Aluminum EPA 200.7 13100 mg/kg 03/11/2015 Arsenic EPA 200.7 <4.31 mg/kg 02/27/2015 Cadmium EPA 200.7 <4.31 mg/kg 02/27/2015 Calcium EPA 200.7 43000 mg/kg 02/26/2015 Chromium EPA200.7 12.4 mg/kg 02/27/2015 Copper EPA 200.7 744 mg/kg 02/27/2015 Lead EPA 200.7 11.9 mg/kg 02/27/2015 Magnesium EPA 200.7 4690 mg/kg 02/26/2015 Molybdenum EPA 2W7 <4.31 mg/kg 02/27/2015 Nickel EPA 200.7 9.78 mg/kg 02/27/2015 Potassium EPA 200.7 4610 mg/kg 02/26/2015 Selenium EPA 200.7 6.28 mg/kg 02/27/2015 Sodium EPA200.7 4140 mq/kq 02/26/2015 Zinc EPA200J I '929 mg/kg 03/03/2015 Ammonia Nitrogen EPA 350.1 546 mg/kg 02/27/2015 Total Kjeldahl Nitrogen (TKN) EPA351.2 2�JJ200 mg/kg 03/02/2015 Nitrate+Nitrite-Nitrogen EPA353.2 1100 mg/kg 02/27/2015 Total Solids (%) SM 2540 8 ' 2.2 % 02/25/2015 Report #:. 2015-02252 Page 2 of 4 Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) e (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town Of Morehead City Date of Report: Mar 20, 2015 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: C. Sutton Report #: 2015-02252 Project ID: Sludge Total Phosphorus SM 4500 P F 18800 mg/kg 03/03/2015 pH SW 846 Method 9045D 6.75 units 02/26/2015 Mercury SW8467471B 1.43 mg/kg 02/26/2015 TCLP Metals Cadmium EPA 200.7 <0.100 mg/L 03/19/2015 Silver EPA 200.7 <0.100 mg/L 03/19/2015 Arsenic EPA 200.8 <0.100 mg/L 03/17/2015 Barium EPA 200 8 <0.100 mg/L 03/17/2015 Chromium EPA 200.8 <0.100 mg/L 03/17/2015 Lead EPA 200.8 <0.100 mg/L 03/17/2015 Selenium EPA 200.8 <0.100 mq/L 03/17/2015 Mercury EPA245.1 0.0031 mq/L 03/18/2015 Lab ID Sample ID: 15-05024 Site:1 Test Total Solids (%) Fecal Density Collect Date/Time 2/24/2015 Method SM 2540 B SM 9221 C E MPN 24 hr 503 Matrix Sampled by Solid/Sludge C.Sutton & C.Dangerfield Results Date Analyzed 22.6 % 02/25/2015 39736 MPN/g 02/25/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-05025 Site: 2 2/24/2015 Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 22.8 % 02/25/2015 Fecal Density SM 9221C E MPN 24 hr 503 21940 MPN/g 02/25/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-05026 Site: 3 2/24/2015 Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 25.0 % 02/25/2015 Fecal Density SM 9221C E MPN 24 hr 503 31937 MPN/g 02/25/2015 Report #:: 2015-02252 Page 3 of 4 Environmental Chemists, Inc. • �7,6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town Of Morehead City Date of Report: Mar 20, 2015 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: C. Sutton Report #: 2015-02252 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-05027 Site:4 2/24/2015 Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 23.2 % 02/25/2015 Fecal Density SM 9221C E MPN 24 hr 503 34439 MPN/g 02/25/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-05028 Site: 5 2/24/2015 Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 24.8 % 02/25/2015 Fecal Density SM 9221C E MPN 24 hr 503 12122 MPN/q 02/25/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-05029 Site: 6 2/24/2015 Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 22.3 % 02/25/2015 Fecal Density SM 9221C E MPN 24 hr 503 62753 MPN/g 02/25/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-05030 Site: 7 2/24/2015 Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 23.1 % 02/25/2015 Fecal Density SM 9221C E MPN 24 hr 503 38962 MPN/g 02/25/2015 Comment: Sludge residuals, excep pH, reported on a dry weight basis. pH reported on an as received basis Reviewed by: �� Report #:: 2015-02252 Page 4 of 4 6602 Windmill Way Wilmington, NC 28405 ENVIRONMENTAL CHEMISTS, I N C OFFICE: 910-392-0223 FAX 910-3924424 M NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmei�talchemists.com Analytical & Consulting Chemists fl^ 1 C/ 'r #'%Kl A KIn PU A IAI !1C f%1 10'rnr%V CLIENT: vi t, VVLLLV I IV11 /"11\1.J VI If111Y VI vvv / Vv 1 PROJECT NAME: REPORT NO: "- ADDRESS: CONTACT NAME: PO NO: d?-0033.P REPORT TO: PHONE/FAX: COPY TO: email: Sampled ti - S r� L. IJa. C. c /Ole SAMPLE TYPE: I = Influent, E = Effluent, W = Well, 51 = stream, -)u JOI1, JI- - .7uvaw, v•..�• Sample Identification Collection E T W a o` I 43 o o rn m PRESERVATION ANALYSIS REQUESTED w " = o w Date Time Temp ) F N E 0 a. c E " g] Z o Z c� v, z s c ''13 `' l� -Z —/S C F� ZZ �II 7-Clr / /v vir; e,)- G/a,ss s .S G P 4(/ RCl' A":" G G— C P G G C Y�O�iCaI r j� I�C�n�.� TS G G 3 C G q C G S q �� G C G G 7 C G Transfer quashed By: Date/Time Received By: DatelTime n 2. -- Temperature when Received: Accepted: Ret cted: Resample Request d: I� Time: t 5 4 9 Delivered By: Received K Date TURNAROUND: Comments: LEWIS FARMS WQ0000455 Morehead City WWTP Date Fecal Coliform M'N ergram Log 02/24/15 39,736 4.5992 02/24/15 21,940 4.3412 02/24/15 31,937 4.5043 02/24/15 34,439 4.5371 02/24/15 12,122 4.0836 02/24/15 62,753 4.7976 02/24/15 38,962 4.5906 Total 1 31.4536 Average 1 4.4934 Geometric Mean 312144=1 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: W20000455 WWTP Name: Town of Morehead City NPDES Number: NCO026611 Monitoring Period: From 1/1/2015 To 12/31/2015 Pathnnen Rednetien 140 VFR 503.321- Please indicate level achieved and alternative performed: Class A: Alternative I ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 0 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed Class A only) indicate "Process to Further Reduce Path ens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ray ❑ Gamma Ray 13 1 Pasteurization ❑ Class B: Alternative 121 Alternative 2 ❑ If applicable to alternative performed Class B oaf indicate "Process to Sip ficantly Reduce Pats ogeos": Lime Stabilization ❑ Air Dryinag Cornp2stina ❑ Aerobic Digestion Q Anaerobic Di estion ❑ If applicable to alternative perfvrmed Class A or Class B corn fete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density 'I"t er o dpne&sE"c� l:requency of Analysis Sample 'type Anmyncw fled' _ niclue inimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the JMPN 6th power total ssoolids Fa 12,122 31,144 62,753 MPN/g 0 Annual Grab sirs 92210E 1000 mpn per gram of total solid (dry wei t Salmonella acteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate optionperformed: Alt.I (VS reduction) ❑ Alt. 2 (404ay bench) ❑ Alt. 3 (30-day bench) ❑ 1 Alt. 4 (Spec. Oz uptake) 0 Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ lNo Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Inco oration Ej vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met" ❑ "I certilly, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonmcnL " Carl Daneerfield, WWTP Superintendent Wesley Wooten, President Pre N e and Title pe or print) Land Ap/Pli r Namc d Title (if applicable)(type or print) z0 k 41�2 —//-/41 re of P er* `DhteSigna of Land Applier (if applicable) Date *Pmparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 9, 2015 Pender Hieh School 0.47 % Solids 6.72 pH Permit No. WQ0000455 Nitrogen (TKN) 2.120 21,200.000 42.400 Phosphorus 0.690 6,900.000 13.800 Potassium 0.413 4,130.000 8.260 PAN (injected)* 1.456 14 563.000 29.126 PAN (surface)* 1.282 12,818.000 25.636 Ammonia Nitrogen 0.349 3,490.000 6.980 Calcium 0.568 5,680.000 11.360 Calcium Carbonate E . --- --- --- Magnesium --- 1,260.000 2.520 Sodium --- 12,600.000 25.200 Sulfur --- --- --- Nitrate N / Nitrite N --- 5,760.000 11.520 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 3,260.00 6.520 Arsenic --- 20.90 0.042 Cadmium --- 7.23 0.014 Chromium --- 105.000 --- Copper --- 219.00 0.438 Lead --- 105.00 0.210 Mercury --- 2.13 0.004 Molybdenum --- 7.87 0.016 Nickel --- 105.00 0.210 Selenium --- 29.40 0.059 Zinc --- 160.00 0.320 Environmentatl Chemists, Inc. # 2015-16431 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. 6..-- - L� ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Pender County Schools Date of Report: Dec 23, 2015 925 Penderlea Highway Customer PO #: Burgaw NC 28425 Customer ID: 08100094 Attention: John Shepard Report #: 2015-16431 Project ID: Pender High School Lab ID Sample ID: Collect Date/Time Matrix Sampled by + 15-39094 Site: Sludge 12/9/2015 10:15 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 3260 mg/kg 12/14/2015 Arsenic EPA 200.7 <20.9 mg/kg 12/14/2015 Reported to MDL Cadmium EPA 200.7 <7.23 mg/kg 12/14/2015 Reported to MDL Calcium EPA 200.7 5680 mglkg 12/10/2015 Chromium EPA 200.7 <105 mg/kg 12/14/2015 Copper EPA 200.7 219 mg/kg 12/14/2015 Lead EPA 200.7 <105 mg/kg 12/14/2015 Magnesium EPA 200.7 1260 mg/kg 12/10/2015 Molybdenum EPA 200.7 <7.87 mg/kg 12/14/2015 Reported to MDL Nickel EPA 200.7 <105 mg/kg 12/14/2015 Potassium EPA 200.7 4130 mg/kg 12/10/2015 Selenium EPA 200.7 <29.4 mg/kg 12/14/2015 Reported to MDL Sodium EPA 200.7 12600 mg/kg 12/11/2015 Zinc EPA 200.7 160 mg/kg 12/1412015 Total Kjeldahl Nitrogen (TKN) EPA 351.2 21200 mg/kg 12/17/2015 Nitrate+Nitrite-Nitrogen EPA 353.2 5760 mg/kg 12/19/2015 Total Solids (%) SM 2540 B 0.47 % 12/10/2015 pH SM 4500 H B 6,72 units 12/18/2015 Ammonia Nitrogen SM4500NH3C 3490mg/kg 12/17/2015 Total Phosphorus SM 4500 P F 6900 mg/kg 12118/2015 Mercury SW646 7471 B <2.13 mg/kg 12/10/2015 Report#:: 2015-16431 Page 1 of 2 F0000- __77 Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax ® 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Pender County Schools Date of Report: Dec 23, 2015 925 Penderlea Highway Customer PO #: Burgaw NC 28425 Customer ID: 08100094 Attention: John Shepard Report #: 2015-16431 Project ID: Pender High School Comment: Sludge residuals, exce t pH, reported on a dry weight basis. Reviewed by: )JL Report #:: 2015-16431 Page 2 of 2 ENVIRONMENTAL CHEMISTS, INC OFFICE1030 2 92602 Windmill Wayi3FAXt •9on 910392-44, Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY CLIENT: Oki OC7PROJECT NAME: l' EPORT NO: ADDRESS: CONTACT NAME: PO NO: y J?I REPORT TO: PHONEWAX: COPY TO: email: aampiea tsy: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection Q °' E o a o � o �� :° `o v° V _� _o` rn t E " o� m 00 _ PRESERVATION ANALYSIS REQUESTED Date Time Temp w O = c> z g u, M z s _o = w y G G C P G G C P G C P G G C P C P C P G C P G G C P G C P I G G -d Transfer Relinquished By: Daterrime Received By: Date/Time 9. 2. 17 Temperature Delivered By Comments: By: ample TURNAROUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Pender High School P.O.# Batch Size (gallons): 4000 +/- Lbs. or Gallons Used: 150 Material Used For Stabilization: Lime SEEM OEM '® '® I 1 1 M® 1 . ®1 1®M® 1 . ®® �Iwfv 1 ' �� C ` O O U t Cu 0, In V O Vl 7 a N V O (n 7 a O co O u1 7 a (D co O v1 7 a M M O 0 7 a O M O (n 7 a I� N O (n 7 a V N O Cn 7 a N O (n 7 a0 O (n 7 a � O 0 7 a N O M 7 a O O O co 7 a O O O (n 7 a m O O (n 7 a O �`'� O O N > C c0 O O 0 > C m O O N > C N o . . C N '- O 0 D C aD O N 7 C N o (n 7 C V N O 0 7 C r N 0 M 7 C O th O N 7 C ch c� O In > C th M O W C M C? o 0 C N v o W C N <i O N C U a E O O M 00 M ti M (0 M U*) M M CM M N M M O M O N w N r` N (O N LO (V N M N N N r N O N�— M M r— (O LO M N O H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Pender High School NPDES Number: NCO042251 Monitoring Period: From 1/l/2015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative Derformed: Class A: Alt. A (time/temp) ❑ Alt A (Alk Treatment)❑ Alt. C (Prior Testing)❑ Alt.D (No Prior Test) ❑ I Process to Fuiflier Reduce PathogenPathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ra 13 Gantma Ra ❑ Pasteurization ❑ - Class B: AIL (1) Fecal Density ❑ 1 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Q Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative pe med (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- Frequency �' of Analysis Sample p Type na ica Tech- ninue Minimu Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpo per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) vector Attraction Reduction tiSA 1vC;AC: 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ JAR. 3 (30-day bench) ❑ 1 Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) [] Alt. 6 (Alk. Stabilization Q JAR 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ c:>t;xI WILU TIViv STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." p "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) -- i nis tieterminauon nas Deen maae unaer my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer ��Name and /Title (type or print) Land Applier Name and Title (if applicable)(type or print) W,�✓ G��'fi Z - 2 Y /G Signature of reparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 15, 2015 River Bend 1.72 % Solids 7.07 pH Permit No. WQ0000455 Nitrogen (TKN) 4.890 48,900.000 97.800 Phosphorus 2.000 20 00.000 40.000 Potassium 0.403 4,030.000 8.060 PAN (injected)* 1.496 14 963.130 29.926 PAN (surface)* 1.476 14,759.630 29.519 Ammonia Nitrogen 0.041 407.000 0.814 Calcium 4.660 46,600.000 93.200 Calcium Carbonate E . --- --- --- Magnesium --- 2,340.000 4.680 Sodium --- 7,090.000 14.180 Sulfur --- --- --- Nitrate N / Nitrite N --- 8.230 0.016 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 3,700.00 7.400 Arsenic --- 29.10 0.058 Cadmium --- 29.10 0.058 Chromium --- 29.100 --- Copper --- 808.00 1.616 Lead --- 29.10 0.058 Mercury --- 1.16 0.002 Molybdenum --- 29.10 0.058 Nickel --- 29.10 0.058 Selenium --- 29.10 0.058 Zinc --- 785.00 1.570 Environmental Chemists, Inc: 2015-16759 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. [enviroche]m ANALYTICAL & CONSULTING CHEMISTS Town of River Bend 45 Shoreline Drive New Bern NC 28562 Attention: Brandon Mills Lab ID Sample ID: 15-39876 Site: Sludge Test Sludge Residuals Aluminum Arsenic Cadmium Calcium Chromium Copper Lead Magnesium Molybdenum Nickel Potassium Selenium Sodium Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Jan 11, 2016 Customer PO #: Customer ID: 12110004 Report #: 2015-16759 Project ID: Wastewater Collect Date/Time Matrix Sampled by 12/15/2015 9:18 AM Solid/Sludge Tom Harper Method Results Date Analyzed EPA 200.7 3700 mg/kg 12/21/2015 EPA 200.7 <29.1 mg/kg 12/28/2016 EPA 200.7 <29.1 mg/kg 12/28/2015 EPA 200.7 46600 mg/kg 12/21/2015 EPA 200.7 <29.1 mg/kg 12/28/2015 EPA 200.7 808 mg/kg 12/21/2015 EPA 2007 <29.1 mg/kg 12/28/2015 EPA 200.7 2340 mg/kg 12/21/2015 EPA 200.7 <29.1 mg/kg 12/28/2015 EPA 200.7 <29.1 mg/kg 12/28/2015 EPA 200.7 4030 mg/kg 12/21/2015 EPA 200.7 <29.1 mg/kg 12/28/2015 EPA 200.7 7090 mg/kg 12/21/2015 Zinc EPA 200.7 785 mg/kg 12/21/2015 Total Kjeldahl Nitrogen (TKN) EPA351.2 48900mg/kg 01/07/2016 Nitrate+Nitrite-Nitrogen EPA353.2 8.23 mg/kg 01/04/2016 Total Solids (%) SM 2540 B 1.72 % 12/16/2015 pH SM 4500 H B 7.07 units 12/24/2015 Ammonia Nitrogen SM 4500 NH3 C 407 mg/kg 12/21/2015 Total Phosphorus SM 4500 P F 20000 mg/kg 01/08/2016 Mercury SW8467471E <1.16mg/kg 12/22/2015 RPnrAf i6, M 5-19754 Panw 9 nf d F"""' -. --Iqqqqq Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax ® 710 Bowsertown Road, Manteo, NC 27954 • 252,473.5702 Lab/Fax M 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemismcom Town of River Bend Date of Report: Jan 11, 2016 45 Shoreline Drive Customer PO #: New Bern NC 28562 Customer ID: 12110004 Attention: Brandon Mills Report #: 2015-16759 Project ID: Wastewater Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-39915 Site: 001 12/15/2015 9:18 AM Solid/Sludge Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.70 % 12/16/2015 Fecal Density SM 9221C E MAN 24 hr 503 941177 MPN/g 12/15/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-39916 Site: 002 12/15/2015 9:19 AM Solid/Sludge Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.70 % 12/16/2016 Fecal Density SM 9221C E MPN 24 hr 503 76471 MPN/g 12/15/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-39917 Site: 003 12/15/2015 9:20 AM Solid/Sludge Test Method Results Date Analyzed Total Solids (% Fecal Density Lab ID Sample ID: 15-39918 Site:004 Test Total Solids (%) Fecal Density SM 2540 B SM 9221 C E MPN 24 hr 503 Collect Date/Time 12/15/2015 9:21 AM Method SM 2540 B SM 9221 C E MPN 24 hr 503 1.78 % 12116/2015 73034 MPN/g 12/15/2015 Matrix Sampled by Solid/Sludge Results Date Analyzed 1.72 % 12/16/2015 75582 MPN/g 12/15/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-39919 Site: 005 12/15/2015 9:22 AM Solid/Sludge Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.73 % 12/16/2015 Fecal Density SM 9221C E MPN 24 hr 503 40463 MPN/g 12/15/2015 RPM!} S" im F_1R7FO Onnn 7 ni A [enviroehem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Town of River Bend Date of Report: Jan 11, 2016 45 Shoreline Drive Customer PO #: New Bern NC 28562 Customer ID: 12110004 Attention: Brandon Mills Report #: 2015-16759 Project ID: Wastewater Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-39920 Site: 006 12/15/2015 9:23 AM Solid/Sludge Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.71 % 12/16/2015 Fecal Density SM 9221C E MPN 24 hr 503 29240 MPN/g 12/15/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-39921 Site: 007 12/15/2015 9:24 AM Solid/Sludge Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.65 % 12/16/2015 Fecal Density SM 9221 C E MPN 24 hr 503 103031 MPN/g 12/15/2015 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: P.-t 1b. o- A of A 6602 Windmill Way mington C ENVIRONMENTAL CHEMISTS, INOFFICE:: 0-392-02231FAX910392-4424 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info@onvironmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Town of River Bend WWTP PROJECT NAME: Wastewater REPORT NO: ADDRESS: 45 Shoreline Drive CONTACT NAME: Brandon Mills, ORC PO NO: New Bern NC 28562 REPORT TO: PHONE/PAX: 252.229.2813 COPY TO: email: Samdled Bv: ± b4,n 1,1,%0' ,'0 -a- r- SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection N `o . r. 318 tj a m o v£ z PRESERVATION ANALYSIS REQUESTED Date Time Temp z i c S 4 gi o Effluent 1/week 7071 X X OD,TSS,NM j2-IS-tS �: o o G G Effluent -grab 1/week C Cn Z• o r�(��11 Z X • entero I Z t 7 !� �; 10 G Effluent 2/month X 2/month G G Influent 1/week) C P b 2 f1 X _ 39gtS BOD,TSS°4q t G G6 Sludge 1/month X 12-15-1 1 G Upstream 2/month *** C P X X Total N,Total P,Chlorophyll A 2/mon:W'01; G G Downstream 2/month *** C P X X o Total N,Total P,Chlorohyll-A 2/month) G_j G C P G G Stream samples due June 1st -September 30 Transfer Relinquished By: DaterTime Received By:_ Daterrime 2. temperature when Received: Accepted: Rejected: Resample Requested: Delivered Received By: Date: Time: Comments: TURNAROUND: LEWIS FARMS WQ0000455 River Bend WWTP Date Fecal Coliform MPN per " ram Log 12/15/15 941,177 5.9737 12/15/15 76,471 4.8835 12/15/15 73,034 4.8635 12/15/15 75,582 4.8784 12/15/15 40,463 4.6071 12/15/15 29,240 4.4660 12/15/15 103,031 5.0130 Total 1 34.6851 Average 1 4.9550 Geometric Mean 909161=1 ecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: River Bend NPDES Number: NCO030406 Monitoring Period: From IW2015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (tinieh to p Alt B (Alk Treawint)-p Alt. C • To; titi p A1t.D (No Prior Test) ❑ Process toYw1herReddQe.. Paths ❑ If applicable to alternadve.performed (Class A only) indicate "PtoceM to Further Reduce Patho ens"•: Compost ❑ Heat D ❑ floret Tteahnent ❑ Rvrmohilic El Beta Ra 17 Gamma ]ta ❑ Pasteurizatibn ❑ Class B: jAlt 1 N>.- l Densi • M Alt. (2) Pmbeas to 3i' fume I Re 4 Wpatitolteds ❑ If applicable to alternative potormeO Chess I# unl )'indicate'3Ptoctss fo Significantly Redoes Pathogens"t Lime Stabilization p Aii . i . ❑ 1 Comf)osting ❑ Aerobio-Di' 'oh ❑ , aerobic Digestion [3 >:;:<>.1::.2::,, l0r o w�°;.,i:.•.,p'.:, .'•2..2:.y' (.CP f>yj5,:ti If applicable to alternative performed LClass A or Class B complete the Nowing monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number ° �e Frequency ofAnai is Ys Sample Type na c al Tech - inimu Geo. Mean aximun Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 29,240 90,161 941,177 MPN/g 0 Annual Grab sM 932t cB CPU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt. 1(VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (36-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization Q Alt 7 (Drying -Stable) ❑ JAIL 8 (Drying- Unstable) lNo ❑ Alt. 9 (I 'ection p Alt. 10 Incor lion Q vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." _ ❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel property gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including line and imprisonment." Brandon Mills, ORC Wesley Wooten, President Preparer Name and Title ( e or print) Land Applier Name and Title if applicable)(type or print) � Signature of Pneparer* ' Tea&✓ Signature of Li5nd Applier (if applicable) Date +Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 1, 2015 Sherwood Mobile Home Park Permit No. WQ0000455 1.37 % Solids 6.89 pH Parameter I % lMg[KgDryWeightl x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 0.329 3,290.000 6.580 Phosphorus 0.085 848.000 1.696 Potassium 0.471 4,710.000 9.420 PAN injected)* 0.302 3,017.500 6.035 PAN (surface)* 0.160 1,597.500 3.195 Ammonia Nitrogen 0.284 2,840.000 5.680 Calcium 3.890 38,900.000 77.800 Calcium Carbonate E . --- --- --- Magnesium -- 2,570.000 5.140 Sodium - 12,100.000 24.200 Sulfur --- --- --- Nitrate N / Nitrite N - 42.500 0.085 Barium - --- Chloride _ ___ Iron - _-_ _-- Aluminum - 1,340.00 2.680 Arsenic - 6.28 0.013 Cadmium --- 6.28 0.013 Chromium --- 8.690 --- Copper - 317.00 0.634 Lead - 13.30 0.027 Mercury 1.46 0.003 Molybdenum --- 6.28 0.013 Nickel - 8.54 0.017 Selenium --- 6.28 0.013 Zinc --- 788.00 1.576 Environmental Chemists, ►nc. 2015-03903 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. F0100- q1 Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 © (910) 392-0223 (Lab) • (910) 392-4424 (Fax) M 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL &CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Lewis Farms & Liquid Waste, INC. Date of Report: Apr 27, 2015 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report M 2015-03903 Project ID: Sherwood MHP Lab ID Sample ID: Collect DatelTime Matrix Sampled by 15-08968 Site: Digester Sludge 4/1/2015 6:30 AM Solid/Sludge J. Marty Fritz Test Method Results Date Analyzed Ammonia Nitrogen SM 4500 NH3 C 2840 mg/kg 04/24/2015 Sludge Residuals Aluminum EPA 200.7 1340 mg/kg 04/08/2015 Arsenic EPA 200.7 <6.28 mg/kg 04/07/2015 Cadmium EPA 200.7 <6.28 mglkg 04/07/2015 Calcium EPA 200.7 38900 mglkg 04/09/2015 Chromium EPA 200.7 8.69 mg/kg 04/07/2015 Copper EPA 200.7 317 mg/kg 04/07/2015 Lead EPA 200.7 13.3 mg/kg 04/07/2015 Magnesium EPA 200.7 2570mg/kg 04/09/2015 Molybdenum EPA 200.7 <6.28 mg/kg 04/07/2015 Nickel EPA 200.7 8.54 mg/kg 04/0712015 Potassium EPA 200.7 4710 mg/kg 04/09/2015 Selenium EPA 200.7 <6.28 mg/kg 04/07/2015 Sodium EPA 200.7 12100 mg/kg 04/09/2015 Zinc EPA 200.7 788mg/kg 04/07/2015 Total Kjeldahl Nitrogen (TKN) EPA351.2 3290 mg/kg 04/13/2015 Nitrate+Nitrite-Nitrogen EPA353.2 42.5 mg/kg 04/21/2015 Total Solids (%) SM 2540 B 1.37 % 04/02/2015 pH SM 4500 H B 6.89 units 04/16/2015 Total Phosphorus SM 4500 P F 848 mg/kg 04/13/2015 Mercury SW8467471B <1.46 mg/kg 04/15/2015 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis Reviewed by:. Report #:: 2015-03903 Page 1 of 1 on ENVIRONMENTAL CHEMISTS, INC OFFICE- 910-392-0 23FAXt910392-4, Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY CLIENT: PROJECT NAME:r/yti�Gc REPORT NO: ADDRESS: CONTACT NAME: ,r(jU�r,L PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: ar - /' SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection E° 2 a o oCO e o a " ` o m .c E " n� ca ma J� z PRESERVATION ANALYSIS REQUESTED Date Time Temp _ O z V o N = 0 z = Q o = W x A O C p G G C P 1� G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. _ Temperature when Received: Accepted:\/ Delivered ByI—i—ot" z— fz_ Received B Comm cesarripie !T qu stew. Date: Time: TUR AROUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Sherwood Mobile Home Park P O.# Batch Size (gallons): 20,000 Lbs. or Gallons Used: 950 LbS Material Used For Stabilization: Lime Date 3/5/20 t 5 pH 8.47 Temp� 11.7 Initial' pH Corr. Factor + -0.42 correued pH 8,05 Time 9:05 pH 13.08 Temp C 14.2 >12 pH Corr Factor+ -0.33 corrected pH 12.75 Time 9:32 pH 12.81 2 Temp C 14.8 Hour Corr. Factor + -0.33 H corlectea Lt 12.48 Time 11:50 pH 24 Temp Cl Hour Corr. Factor + p H Correct pH Time operato In jmf OLLi O j q CD� "' 5:a. O O tll OMN OVN c O �C 4Y1 v a LO IT CV O m M n (p t!7 N (N N N ~ �. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Fauns & Liquid Waste, Inc. WQ Permit Number: W00000455 WWTP Name: Sherwood Mobile Home Park NPDES Number: NCO022462 Monitoring Period: From I/l/2015 To 12/312015 Pathogen Reductions (15A NCAC 02T .11061- Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ 1 Process to Further Reduce Patlto engs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hdic ❑ Seta Ra ❑ Gamma Ray ElPasteurization ❑ Class B: Alt: t Fecal Density ❑ Alt. (2) Process to Sipificantly Reduce Patho eas ❑ If aeplicable to alternative performed (pass B onW indicate "Process to Significantly Reduce Pathogens": Lime Stabilization El Air 29 ❑ Corn stirs ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ :.: .... .._........ If aEplicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level In in Sludge Pathogen Density Umber o Excec- F enc y of Analysis y Sample p Type Tech - niallp Minimu Geo. Mean aximu Unitsces Fecal Coliform 2 x 10 to the 6th power per grate of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of focal colifonn) 3 MPN per 4 grains total solid (dry weight) vuutur ririracuou meaucilon (1,A NI:AU 02T1' .11U7)- Please indicate alternative performed: Alt.t (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying -Stable) ❑Alt. lNo 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El vector attraction reduction alternatives were performed ❑ ter.!( i "11-A i WIN STATEMENT EMENT (please check the appropriate statement) O "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify,�under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the rcq ulrements.) "This determination has been made under my direction and supervision in accordance with the system i designed to ensure that qualified personnel properly gather and evaluate the Information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." J. Marty Fritz, (ORC Lime Stabilization) Wesley Wooten, President Preparer Name and the (type or print) Land Applier Nam le (if applicable)(type or print) !✓/ 2 -2y_/C ignature otWeparer4 Date Signature of 6and Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 1 SA NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 10, 2015 Sterlin¢ Farms WWTP Permit No. WQ0000455 0.43 % Solids 7.14 pH Nitrogen (TKN) 1.000 64,700.000 129.400 Phosphorus 2.020 27,600.000 55.200 Potassium 1.010 10 300.000 20.600 PAN (injected)* 0.364 3,642.700 7.285 PAN (surface)* 0.348 3,482.200 6.964 Ammonia Nitrogen 0.032 1,090.000 2.180 Calcium 8.720 31,200.000 62.400 Calcium Carbonate E . --- --- --- Magnesium --- 5,510.000 11.020 Sodium --- 38 800.000 77.600 Sulfur --- --- --- Nitrate N / Nitrite N --- 418.000 0.836 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 2,580.00 5.160 Arsenic --- 21.60 0.043 Cadmium --- 7.44 0.015 Chromium --- 110.000 --- Co er --- 258.00 0.516 Lead --- 110.00 0.220 Mercury --- 4.42 0.009 Molybdenum --- 8.14 0.016 Nickel --- 110.00 0.220 Selenium --- 30.50 0.061 Zinc --- 5,910.00 1 11.820 Environmental Chemists, Inc. 2015-16558 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. ANALYTICAL & CONSULTING CHEMISTS Aqua America of North Carolina 251 Merchants Circle Bldg 24-1 Hampstead NC 28443 Attention: Don Williams Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchcmists.com Date of Report: Dec 29, 2015 Customer PO #: Customer ID: 08110027 Report #: 2015-16558 Project ID: Sterling Farms Lab ID Sample ID: 15-39399 Site: Sludge Test Collect Date/Time 12/10/2015 10:30 AM Method Matrix Sampled by Solid/Sludge Don Feller Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 2580 mg/kg 12/14/2015 Arsenic EPA 200.7 <21.6 mg/kg 12/14/2015 Reported to MDL Cadmium EPA 200.7 <7.44 mg/kg 12/14/2015 Reported to MDL Calcium EPA 200.7 31200 mg/kg 12/16/2015 Chromium EPA200.7 <110 mg/kg 12/14/2015 Copper EPA 200.7 258 mg/kg 12/14/2015 Lead EPA 200.7 <110 mg/kg 12/14/2015 Magnesium EPA200.7 5510 mg/kg 12/16/2015 Molybdenum EPA 200.7 <8.14 mg/kg 12/14/2015 Reported to MDL Nickel EPA200.7 <110 mg/kg 12/14/2015 Potassium EPA 200.7 10300 mg/kg 12/16/2015 Selenium EPA2o0.7 <30.5 mg/kg 12/14/2015 Reported to MDL Sodium EPA 200.7 38800mg/kg 12/21/2015 Zinc EPA MY 5910 mg/kg 12/14/2015 Total Kjeldahl Nitrogen (TKN) EPA351.2 64700 mg/kg 12/22/2015 Nitrate+Nitrite-Nitrogen EPA353.2 418 mg/kg 12/20/2015 Total Solids (%) SM 2540 B 0.43 % 12/11/2015 pH SM 4500 H B 7.14 units 12124/2015 Ammonia Nitrogen SM4500 NH3 C 1090 mg/kg 12/21/2015 Total Phosphorus SM 45M P F 27600 mg/kg 12/22/2015 Mercury SW0487471B <4.42 mg/kg 12/10/2015 Report #:: 2015-16558 Page 3 of 4 Lenviyochem ANALYTICAL & CONSULTING CHEMISTS Aqua America of North Carolina 251 Merchants Circle Bldg 24-1 Hampstead NC 28443 Attention: Don Williams Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 29, 2015 Customer PO #: Customer ID: 08110027 Report #: 2015-16558 Project ID: Sterling Farms Comment: Results, except pH, re orted on a dry weight basis. pH reported on an as received basis. Reviewed by: Report#:: 2015-16558 Page 4 of 4 Way =10 on ENVIRONMENTAL CHEMISTS, INC OFFICE: 10! 920223FAXt910392-44, Analytical $Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY CLIENT: p PROJECT NAME: REPORT NO: 15 -- 1 ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONEIFAX: COPY TO: email: Sampled tsy: ,i b,) f-e//c.- SAMPLE TYPE: 1= Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL. = Sludge, Other: Sample Identification p Collection a a T E 6. o L° o d6 3 `o o Lx " `" m o � LLi E m °7 g D z PRESERVATION ANALYSIS REQUESTED Date Time Temp w a z = � N x ^� z z = z o w o C G� Z C �133 z vo - is- /03D G # 3 � �LUQ C Eh1s� z -/v ,0o y c �G 3�3a5 Su/ 67is /•7 /o 03o #5 c 69 /67-/V -/YO-YO C E� /.7-/a /S 3D Gi3�i� 4:t 7 C i t`b SLvAcE E s o /o /s o a G SLUE c13I ES/�!'is1L zto • fS G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: Accepted: Delivered By: Received By: Kesampie meques TURNAROUND: Time: �{ Comments: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Sterling Farms P.O.# Batch Size (gallons): 60000 +/- Lbs. or Gallons Used: 850 Material Used For Stabilization: Lime MEE- NEMEE • • . •1 1 • .®�EMS : • Erem, •11 ®� 1 • C (n N M (D M O � It N a)(O Cl)M (0 0) N v) (o c O Cl)(D 0) N n L D ` V M M M M N N N O O O O O O N N N M C) M M U O O CDo O O O O O O O O O O O O O O O O O O O O O O O O O O N 0 0 w 0 0 w N N . . n UM M (A (D N (D U) U) (A (1) 0 U) 7 7 7 j � 7 D 7 7 D 7 7 7 7 7 U LL 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 C C C C C C C C C C C C C C C E E E E E E E E E E E E E E E U a O M w I- CO (n d M N— O M M p- CO U') - M N O M M t- Cfl (n M N O �t M M M M co co co M M M N N N N N N N N N N a) H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WWTP Name: Sterling Farms Monitoring Period: From 1/1/2015 To WQ Permit Number: WQ0000455 NPDES Number: WQ0029475 12/31/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ I Process to Further Reduce Patho en s ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo plulic C3 Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed(Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization El Air Drying ❑ Composting ❑ jAcrobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the followin monitoring data: Parameter Allowable Level in Sludge Pathogen Density Numuer o denoe-qExcee- Frequency of Analysis Sample 'Type Anaiytleal Tech- nimp MinimumGeo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAR. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization El All 7 (Drying - Stable) ❑ JAIt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer Name and Ti (type or print) `/./, ?-Z 1/—/c Signature df Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: August 11, 2015 Swansboro 2.15 % Solids 6.26 PH Permit No. WQ0000455 Nitrogen (TKN) 4.760 47,600.000 95.200 Phosphorus 2.690 26,900.000 53.800 Potassium 0.335 3,350.000 6.700 PAN (injected)* 2.443 24,429.000 48.858 PAN (surface)* 2.359 23,594.000 47.188 Ammonia Nitrogen 0.167 1,670.000 3.340 Calcium 6.290 62,900.000 125.800 Calcium Carbonate E . --- --- --- Magnesium --- 2,300.000 4.600 Sodium --- 4,520.000 9.040 Sulfur --- --- --- Nitrate N / Nitrite N --- 8,980.000 17.960 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 5,260.00 10.520 Arsenic --- 23.30 0.047 Cadmium --- 23.30 0.047 Chromium --- 23.300 --- Copper --- 426.00 0.852 Lead --- 23.30 0.047 Mercury--- 2.90 0.006 Molybdenum --- 23.30 0.047 Nickel --- 23.30 0.047 Selenium --- 23.30 0.047 Zinc --- 4,210.00 8.420 Environmental Chemists # 2015-10481 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. envi., 1:M ANALYTICAL & CONSULTING CHEMISTS Onslow Water & Sewer Authority Post Office Box 1415 Jacksonville NC 28541 Attention: Todd Roberts Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Aug 28, 2015 Customer PO #: Customer ID: 08100092 Report #: 2015-10481 Project ID: Swansboro WWTP Lab ID Sample 1D: Collect Date/Time Matrix Sampled by 15-24769 Site: Sludge 8/11/2015 10:15 AM Solid/Sludge Client Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 5260 mg/kg 08/21/2015 Arsenic EPA 200.7 <23.3 mg/kg 08/21/2015 Cadmium EPA 200.7 <23.3 mg/kg 08/21/2015 Calcium EPA 200.7 62900mg/kg 08/20/2015 Chromium EPA 200.7 <23.3 mg/kg 08/21/2015 Copper EPA 200.7 426 mg/kg 08/19/2015 Lead EPA 200.7 <23.3 mg/kg 08/21/2015 Magnesium EPA 200.7 2300mg/kg 08/20/2015 Molybdenum EPA 200.7 <23.3 mg/kg 08/24/2015 Nickel EPA 200.7 <23.3 mg/kg 08/21/2015 Potassium EPA 200.7 3350 mg/kg 08/20/2015 Selenium EPA 200.7 <23.3 mg/kg 08/21/2015 Sodium EPA 200.7 4520 mg/kg 08/20/2015 Zinc EPA 200.7 4210 mg/kg 08/1912015 Total Kjeldahl Nitrogen (TKN) EPA351.2 47600mg/kg 08/24/2015 Nitrate+Nitrite-Nitrogen EPA 353.2 8980 mg/kg 08/19/2015 Total Solids (%) SM 2540 B 2.15 % 08/12/2015 pH SM4500 H B 6.26 units 08/14/2015 Ammonia Nitrogen SM4500NH3 C 1670 mg/kg 08/24/2015 Total Phosphorus SM 4500 P F 26900 mg/kg 08/25/2015 Mercury SW8467471B 2.90 mg/kg 08/10/2015 RAoort#- 2015-10481 Paoe 1 of 3 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentatchemists.com Onslow Water & Sewer Authority Date of Report: Aug 28, 2015 Post Office Box 1415 Customer PO #: Jacksonville NC 28541 Customer ID: 08100092 Attention: Todd Roberts Report #: 2015-10481 Project ID: Swansboro WWTP Lab 1D Sample 1D: Collect DatelTime Matrix Sampled by 15-24777 Site: 1 8/11/2015 10:15 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.43 % 08/12/2015 Fecal Density SM 9221C E MPN 24 hr 503 4527 MPN/g 08/12/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-24778 Site: 2 8/11/2015 10:15 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.90 % 08/12/2015 Fecal Density SM 9221C E MPN 24 hr 503 1380 MPN/g 08/12/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-24779 Site: 3 8/11/2015 10:15 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.41 % 08/12/2015 Fecal Density SM 9221C E MPN 24 hr 503 1660 MPN/g 08/12/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-24780 Site: 4 8/11/2015 10:15 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.84 % 08/12/2015 Fecal Density SM 9221C E MPN 24 hr 503 3874 MPN/g 08/12/2015 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-24781 Site: 5 8/11/2015 10:15 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.24 % 08/12/2015 Fecal Density SM 9221C E MPN 24 hr 503 3125 MPN/g 08/12/2015 Report k 2015-10481 PROP. 2 of 3 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Aug 28, 2015 Post Office Box 1415 Customer PO #: Jacksonville NC 28541 Customer ID: 08100092 Attention: Todd Roberts Report #: 2015-10481 Project ID: Swansboro WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-24782 Site: 6 8/11/2015 10:15 AM Solid/Sludge Client Test Total Solids (%) Fecal Density Lab ID Sample ID: 15-24783 Site:7 Test Total Solids (%) Fecal Density Method SM 2540 B SM 9221 C E MPN 24 hr 503 Results Date Analyzed 2.45 % 08/12/2015 817 MPN/g 08/12/2015 Collect DatelTime Matrix 8/11/2015 10:15 AM Solid/Sludge Method SM 2540 B SM 9221 C E MPN 24 hr 503 Results Sampled by Client Date Analyzed 2.61 % 08/12/2015 1533 MPN/g 08/12/2015 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report #:: 2015-10481 D e A s 1 mington ENVIRONMENTAL CHEMISTS, INC OFFI E' 9 0392-0223'IFAX910392-4424s Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: ONWASA PROJECT NAME: Swansboro WWTP ONWASA) REPORT NO: L (D ADDRESS: CONTACT NAME: Allen Rhue PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE- I = Influant_ E = Ffflivanr W = Wall QT = Q*.ems.., en - Q„n et - Qi .4 .,, n« Sample Identification Collection G d E; N P N A 90 e E t� C 0 � o o a v" C J ; �, is E G W m m z' -•-•--..., PRESERVATION . _ ..,,.., ... - .....M..., .,., - ......, ...� - .,.....ate, ...�. „. ANALYSIS REQUESTED Date Time Temp w z z - e 0 x 0 x x 0 Z o w o Sludge I.95 /Os S C P y % X nutrients/metals G G 1) �} • 7 C P 11,071T x fecal density / %TS G G 2) ;'—w-!S 1o11d 7 C P x fecal densi / %TS G G 3 a-�1-� C P x fecal density / %TS G G 4) all x fecal density / %TS G G 5) it-lS la� iS 29, 2 C P x fecal density / %TS G G 6 a5 7 x fecal density / %TS G G 7) /67: s ai- 7 C P x fecal density/ %TS G G C P I r, -T I I "�� G Gd Meter reading (start): Meter reading (end): Transfer Relinquished By: Date/Time Received By: Date/Time 1. -1 f 2. I c"uNeraEure wile" rceaelvep: -t-- _Accepted:, Delivered By: Received By: ':�,, 3-� 1/L� Date Comments: :d: Time: t 5v),l LEWIS FARMS WQ0000455 Swansboro Date Fecal Coliform MPN per am Log 08/11/15 4,527 3.6558 08/11/15 1,380 3.1399 08/11/15 1,660 3.2201 08/11/15 3,874 3.5882 08/11/15 3,125 3.4949 08/11/15 817 2.9122 08/11/15 1,533 3.1855 Total 1 23.1966 Average 3.313 8 Geometric Mean 2 060 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction requirement. LEWIS FARMS OF BURGAW INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Swansboro WRF P.O.# Batch Size (gallons): 235,000 Lbs. or Gallons Used: 2000 Material Used For Stabilization: Lime Initial pH >12 pH 2 Hour pH 24 Hour pH Operator Date pH Temp C Corr. Factor + Corrected pH Time pH �TempC Corr. Factor + Corrected pH Time pH Temp C Corr. Factor + Corrected pH Time pH Temp C Corr Factor + Corrected pH Time Initials 3/9/2015 7.0 1611 0.27 6.75 9:31 12.4 14.8.30 12.1 14:55 12.3 15.2.30 12.0 17:00 TM/AWR 3/10/2015 12.1 17.8 0.21 11.9 14:55 TM C `O � N O (0 C" O r " c2 2 N O O M ' " m N m v n o r> co m N N C)O `� T. O a V O a (7 C) a M O J a Cl)(h O J a O J N O J a N O D a N O J a O J a O n a O D d C) C) J d CD CD J a C)0 J a o . C 2 0 0 . C 20 0 0 . C 2 0 0 C .- 0 . C 0 . C N 0 N C N 0 N C N 0 N C 0 . C 0 . C 0 C 0 C 0 C 0 C v Q E O V' O M 00 M r- M (..0 M L0 CO V M cM (h N CO r- M O M O N 00 N N (.0 (V LO N V (V M N N N N O N 0) 00 r--(D L0 T M (N O N E— ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Swansboro NPDES Number. WQ0023261 Monitoring Period: From I/I/2015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative Performed: Class A: AIt. A (time/tem) ❑ 1 Alt B (Alk Treatment) ❑ Alt. C Prior Testin ❑ A1t.D (No Prior Test) ❑ 1 Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma Ra ❑ Pasteurization El Class B: JAIt. (1) Fecal Deusi El Alt. (2) Process to Significantly Reduce Pathogen ❑ If applicable to alternative performed (Class B only) Indicate "Process to Significantly Reduce Pathogens": Lime Stabilization p Air aying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g ty um er o Excec- denrLiofAnatysis Frequency Sample Type na ytica I•ech- Minimurr Geo. Mean Maximur4 Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 817 2,060 4,527 MPN/g 0 Annual Grab SM 9221 CE CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal eoliform) 3 MPN per 4 gums total solid (dry wei t Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative Performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization Q Alt 7 (Drying- Stable) ❑ lNo Alt. 9 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) [l vector attraction reduction alternatives were performed ❑ CER-11FICATION STATEMENT (please check the appropriate statement) O " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Allen Rhue, ORC Wesley Wooten, President Preparer Name and Title (type or print) Land Applier Name an Title (if applicable)(type or print) (m W. iFlut6 �/ ?-Z v /� 8 Feb 16 Signature of Preparer* Date Signature o Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 13, 2015 Taylor Extended Care Permit No. WQ0000455 1.03 % Solids 8.2 pH Parameter % Mg/Kg Dry Weight x 10,000 Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002) Nitrogen (TKN) 2.578 25,784.000 51.568 Phosphorus 0.711 7,108.000 14.216 Potassium 0.380 3,799.000 7.598 PAN (injected)* 0.807 8,068.220 16.136 PAN (surface)* 0.784 7,839.220 15.678 Ammonia Nitrogen 0.046 458.000 0.916 Calcium 3.142 31,418.000 62.836 Calcium Carbonate E . --- --- --- Magnesium --- 2,467.000 4.934 Sodium --- 26,420.000 52.840 Sulfur --- --- Nitrate N / Nitrite N --- 12.420 0.025 Barium --- --- Chloride --- --- Iron --- --- Aluminum --- 3,900.00 7.800 Arsenic --- 2.50 0.005 Cadmium --- 0.63 0.001 Chromium --- 7.000 --- Copper --- 1,325.00 2.650 Lead --- 41.00 0.082 Mercury --- 4.10 0.008 Molybdenum - 5.00 0.010 Nickel --- 13.00 0.026 Selenium --- 5.00 0.010 Zinc - 967.00 1.934 Environment 1, Inc. # 381A *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. P.Q. BMX 7085 f4 ORt4N{C)i`!T; GF EENVILLE; N,C 27835.7085 HERITAGE HEALTHCARE @ TAYLOR PLACE ATTN: MICHAEL SALAMONE P.O. BOX 100 SEA LEVEL ,NC 28577 Sludge Analysis Alellind PARAUBTERS Sample Date Analyst. Code PH, Units 8,2 01115/15 TRB C500HB-00 Atuntaunn, (dry wt, basis), utg/kg 3900 01/26/15 LFJ EPA200.7 Arsenic (dry wt, basis), mg/kg <2,5 01/29/15 b•ITAI 31I3B-04 Calcium (dry wt. basis), uig/kg 31d18 01/26/15 LFJ BPA200.7 Cadmium (dry wt, basis), mg/kg 0.63 01/26/15 rMAI 3113B•04 Copper (dry w(, basis), mg/kg 1325 01/26/15 LFJ EPA200.7 Chromium, T.(th•y wt, basis),mg/kg 7 01/26/15 LFJ EPA200,7 Lead (dry weight basis), nag/kg 41 01/27/15 NPPil1 3113B-04 A•Iagnesium (dry wt, basis), mg/kg 2d67 01/26/15 LFJ EPA200.7 1•Iercury (dry wt. basis), mg/kg 4.1 01/21/15 A•1TA1 245.1 R3-94 Nickel ((Ivy wt. basis), mg/kg 13 01/26/15 LFJ EPA200.7 Potassium (dry wt. basis), mg/`kg 3799 01/26/15 LFJ LPA200,7 Selenium (dry wt. basis), ntglkg <5.0 01/30/15 A•1Th1 3113B-04 Sodium (dry wl. basis), mg/kg 26420 01/26/15 LFJ EPA200.7 Zhu (dry wt. basis), mg/kg 967 01/26/15 LTJ EPA200.7 Total Solids, % 1.03 01/14/15 KKF 2540C-97 TKN (dry wt.), nig/kg 25784 01/20/15 RND 351.2 R2-93 Ammonia Nitrogen (dry %rt.),tng/kg 458 01/20/15 SEJ 350A R2-93 Phospborns, T, (dry wt.), mg/kg 7108 01/20/15 KDB 365.4-74 Nitrate=Nitrite (dry wt.), mg/kg 12.42 01/16115 KDB 353.2 R2-93 lylolybdemm (dry wt. basis), mg/kg <5,0 01/26/15 LFJ. EPA200.7 :. ;.... ;i AX`(252)'766-0633 ID#: 381 A DATES COLLECTSDt 01/13/15 DATE REPORTRD : 02/10/15 REVIEWED BY: w � us,,ro i- fir, :�Zc c `C� ir'.U..Tien= cr' i. L-t Oakl. otu D,-. rm it irt.ul,C:nt)lLIC.<'Q?7. P.U.oue 1252:) 756-B2OS • 1 :Lt i^.j', 7 6-U53 l�I�fN{-T-c 110 ± FCHLOF(INTNP-LITRAI-rf�C)Arr-',- LEC: nON, �: �, �' i T: 331 A Week: 7 I — i -"`j� L-�• �_ ?�- pH CHECK (LAB) W-RITAGE HEALTHCARE 0 TAYLOR PLACE l�,A Xm'.WCHAELSALAMONE i ,:c; >, P P 1' P P P P P P p CONTAINECRTY?E.RIG 1.0. BOX 100, EA LEVEL NC 28577 A A A A A A A A A A CHE tN11CALPRESE WAT1r)N � �U c , 152) 225-0112 n, A • IJCY. IE O • NAO- "—' U w Cr n q o z W 8, HNO, E- HCL C H SD }' ZINC AC:E FA'"F. *NA0H COLLEC'r!ON o n: �I a ems. E o f d O w x G u ate+ ►° o U , I I ! w G-NATHIOSUI,FATE 1 SAMPLE LOCATION DATE TjME Stadse S=pte i3 e 6 a', .: <. .. :. �, >.y 11 :.. �` .rf M ---- 030 CLAS'SRI ATICkv WASTBIVATFR NPnE$ - DRINKING'A'ATER �� D4VCb•G1':' SOLID WAb•TESECTION I CHAIN OF GUS 100'Y NIA114T,,gINED WRINGS !PMENPOEUVE.RY Y N SAMPLES CCUECTEO BY: I I v%s { SN PLES RECEIVED IN UkBAT G, _''G EYiSIC t; APviPLEia OAM-11 AE RECEI YtStG ATETME COMMENTS JRFIE PNOUISHEDB�y 3z 7 - - -- I G.) 0ATE111mE RECEIVED BY (5,,.,,, GAT6MI:AE ---- — _ RELINGUISHED BY rSICL) DATETIfwtE RECEIVED pY (SG.) DAMTIbtE PLEAiSE READ IfistruclionS for Complatina this loan y) the reverse aide Sampler must pine a "C" for composite; santpte or a "G" for o ,--•a � . 2 919 � 1 FORM ns "`�"— �'� Grab Sample cn the blocks above for each Parameter reque5lea. Environmental Chemists, Inc. enviroichhem-,6602 Windmill Way • Wilmington, NC 28405 ® (910) 392-0223 (fab) - (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICRI713 #37729 Environment -1 Date of Report: Feb 09, 2015 Post Office Box 7085 Customer PO #: Greenville NC 27858 Customer ID: 08100051 Attention: Deedee Woolard Report #: 2015-00629 Project ID: Heritage Healthcare @ Taylor Place Lab ID Sample ID: Collect DatefTime Matrix Sampled by 15-01346 Site: Sludge Sample 1/13/2015 10:30 AM Solid/Sludge Patricia Davis Test Method Results Date Analyzed RCl Cyanide EPA335.4 <0.125 mg/kg 01/23/2016 Sulfide SM 4500 s D <0.250 mg/kg 01/21/2015 Ignitability SW 846meUW 1010 >212'F 02/06/2016 Comment: Reviewed by: Repcd t: 2015.00829 Page l of I Environment 1, Inc. CHAIN OF CUSTODY RECORD P.O. Box 7085. 114 Oakmont Dr. page 1 1 Greenvi Ile, NC 27858 of �11YA J111ci1uu+c,.1,Uui Phone (252) 756-6209 • Fax (252) 756-0633 DISINFECTION CHLORINE NEUTRAIIZEDATCOLLECTION 381 A � CHLORINE . Week: 7 CLMNT UV pH CHECK (LAB) T-F,TAGF, IMAL'HCARE 0 TAYLOR PLACE ,TIN: N9CEIA , f ALA.MON,B NONE p p p CONTAINERTYPE, PIG' .0. BOX zoo• A A A CHEMICALPRESERVATION RA x.EV)EI, NC 28577 ?52 225-0112F r A -NONE D-NAOH Iz-B.HNO, E-HCL cg ¢ zl e �' C-H2S0' F ZINC ACETATE/NAOH COLLECTION~ va Q v Uj a G-NATHIOSU FATE SAMPLELACATION DATE TIME tR '' Sludge Sample j . CLASSIFICATION: WASTEWATER(NPOES) DRINKINGWATER DWOIGW SOLID WASTE SECTION CHAIN OF CUSTODY MAINTAINED DURING S IPMENTIDELIVERY Y N SAMPLES COLLECTED BY. V1,5' SAMPLES RECEIVED INLABAT,°C ED_BY(SI PLE DATEMME S RECE Y(SiG Z� l ATUnME Z% D COMMENTS: SHED G) RT �/I DATFITYWE ECFJ)k-D 8 (S 4y3 E/iI� ME 1 t� i o 15 REUNOUIS .) DATU ME RECENED (SIG.) DATEMME PLEASE READ Instructi6ns for completing this form on the reverse side. Sampler muse place a "C' for composite sample or a "G" for• FORM ns Grab sample in the blocks above for each parameter requested. LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS FacilityName: 4XA L 4 14 14' P.O.# Batch Size (gallons): aSoO ffC&I10 flS Lbs. or Gallons Used: 1co 11y'- Material Used For Stabilization: Lime E MERNMEERNMEMNSWEENBMW .in= wom CO ` {± (J �A O N > N O N > Ol O N > ((pp O N a (`•i O fA 7 O O N O h O N a v O N > O y > Cp O 0 > O N > O N > m O N > (p O tll > m O N a O m O o tl/ 7 c O O N 7 c W O o N 7 c N c t17 O dl c O tll 7 c N O N 7 c N O tll 7 c N O A 7 c 'i O V) 7 c t7 O c t+! O M 7 c V7 O N 7 c V O W E c v o N 7 c U CL EO O O ch (p m r~ M (0 M LO f7 M m N M r m 0 M 0 N Co N t` N w N to N '7 N co N (� N 0 r O r r- r (D r to r .' r m r N r r r 0 r :CN4LCN1J H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Taylor Extended Care NPDES Number: NCO047759 Monitoring Period: From l/l/2019 To 12/3112019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative Derformed: Class A: Alt. A (time/temp) ❑ Ali B (Alk Treatment) [I Alt. C (Prior TesEin ) ❑ Alt.D (No Prior Test) ❑ I Process to Further Reduce Pathogen ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens". - Compost Cl Heat Drying❑ Heat Treatment ❑ Thermo folic ❑ Beta Rax ❑ Gamma Ra ❑ Pasteurization ❑ Class B: JAIL (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization p Air Drying [7 Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative perrormed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Numberot Excee- encey� Frequency of Anal s Sample Type na ica Tech- nime Minimum Geo. Mean Maximo Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry wet ht) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization Q Alt 7 (Drying - Stable) ❑Alt. 8 (Drying - Unstable) ❑ Alt. 9 (injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ Ck RTWICATION STATEMENT (please check the appropriate statement) O "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Patricia T. Davis, ORC Prepar r a and Title (type or grin Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: February 16, 2005 The Caue 1.74 % Solids 6.5 DH Permit No. rNitrogen 5.530 55,300.000 110.600 2.470 24,700.000 49.400 0.305 3,050.000 6.1 00 PAN (injected)* 1.981 19 807.400 39.615 PAN (surface)* 1.752 17 517.400 35.035 Ammonia Nitrogen 0.458 4,580.000 9.160 Calcium 2.240 22,400.000 44.800 Calcium Carbonate E . --- --- --- Magnesium --- 2,180.000 4.360 Sodium --- 3,850.000 7.700 Sulfur --- --- --- Nitrate N / Nitrite N --- 11.400 0.023 Barium --- --- --- Chloride --- I --- --- Iron --- --- Aluminum --- 4,490.00 8.980 Arsenic --- 5.58 0.011 Cadmium --- 5.58 0.011 Chromium --- 13.300 --- Copper --- 260.00 0.520 Lead --- 10.40 0.021 Mercury --- 0.43 0.001 Molybdenum --- 5.58 0.011 Nickel --- 15.10 0.030 Selenium --- 7.01 0.014 Zinc --- 586.00 1 1.172 Environmental Chemists, Inc. # 2015-01936 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 ® (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL &CONSULTING (252)473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DIS CERTIFICATE #37729 Aqua America of North Carolina 251 Merchants Circle Bldg 24-1 Hampstead NC 28443 Attention: Don Williams Lab ID Sample ID: 15-04357 Site: Sludge Date of Report. Mar 04, 2015 Customer PO #: Customer ID: 08110027 Report #: 2015-01936 Project ID: The Cape Collect Datefrime Matrix Sampled by 2/16/2015 9:00 AM Solid/Sludge Will Coggins Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 4490 mglkg 03/03/2015 Arsenic EPA 200.7 <5.58mg/kg 02/27/2015 Cadmium EPA 200.7 <5.58 mg/kg 02/27/2015 Calcium EPA 200.7 22400 mg/kg 02/26/2015 Chromium EPA 200.7 13.3 mg/kg 02/27/2015 Copper EPA 200.7 260 mg/kg 02/27/2015 Lead EPA 200.7 10.4 mg/kg 02/27/2015 Magnesium EPA 200.7 2180 mg/kg 02/26/2015 Molybdenum EPA200.7 <5.58mg/kg 02/27/2015 Nickel EPA 200.7 15.1 mg/kg 02/27/2015 Potassium EPA 200.7 3050mg/kg 02/26/2015 Selenium EPA 200.7 7.01 mg/kg 02/27/2015 Sodium EPA 200.7 3850 mg/kg 02/26/2015 Zinc EPA 200.7 586 mg/kg 03/03/2015 Ammonia Nitrogen EPA350.1 4580mg/kg 02/23/2015 Total Kjeldahl Nitrogen (TKN) EPA351.2 55300 mg/kg 02/20/2015 Nitrate+Nitrite-Nitrogen EPA353.2 11.4 mg/kg 02/18/2015 Total Solids (%) SM 2540 B 1.74 % 02/16/2015 pH SM 45M H B 6.50 units 02/1812015 Total Phosphorus SM 45W P F 24700 mg/kg 02/23/2015 Mercury SW8487471B <0.431 mg/kg 02/13/2015 Report #:: 2015-01936 Page 1 of 2 r- 7 1 Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) ® 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Aqua America of North Carolina Date of Report: Mar 04, 2015 251 Merchants Circle Bldg 24-1 Customer PO #: Hampstead NC 28443 Customer ID: 08110027 Attention: Don Williams Report #: 2015-01936 Project ID: The Cape Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-04357A Site: Sludge 2/16/2015 9:00 AM Solid/Sludge Will Coggins Test Method Results Date Analyzed Total Solids (%) sM 2540 6 1.60 % 02/18/2015 Fecal Density SM 9221 C E MPN 24 hr 503 106250 MPN/g 02/17/2015 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: �61e c Report'P.: 201"1936 Page 2 of 2 mington ENVIRONMENTAL CHEMISTS, INC OFFICE:: 0-392-02 3i1FAX910392-"245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: AquaNC PROJECT NAME: Annual Sludge Analysis REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: Don Williams PHONEIFAX: COPY TO: email: Sampled By: d c(q# w62 SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil_ SL = Sludge_ Ofhert Sample Identification oliection m am ~ ; o `o m ct� O o Va m _� L E ow J? z PRESERVATION 4 ANALYSIS REQUESTED Date Time Temp o z x= Z x xQ = W o Sludge Z 1b ts' C P 1 �JS Nutrients/metals G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By. DateMme Received By: Date/Time 1. 2. Temperature when Received: Accepted: Delivered By: Received ;ample Requested: Date: Z (0- 6 Time: 17. TURNAROUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: The Cape P.O.# Batch Size (gallons): 30000 +/- Lbs. or Gallons Used: 2000 +/- Material Used For Stabilization: Lime Initial pH >12 pH 2 Hour pH 24 Hour pH Operator Date pH Temp C Corr. Factor + Corrected pH Time pH Temp C Corr. Factor + Corrected pH Time pH Temp C Corr. Factor + Corrected pH Time pH Temp C Corr. Factor + Corrected pH Time Initials 1/20/2013 7.21 9.9 -0.45 6.76 751 12.65 10.1 -0.45 12.20 805 12.63 10.1 -0.45 12.18 1005 12.55 10.1 -0.45 12.10 810 WW 2/16/2015 6.87 14.1 -0.33 6.54 700 12.51 14.3 -0.32 12.19 715 12.53 14.3 -0.32 12.21 915 12.5 14.4 -0.32 12.18 715 WW 3/24/2015 7.13 17.8 -0.22 6.91 800 12.42 18.0 -0.21 12.21 815 12.45 18.1 -0.21 12.24 1015 12.38 18.0 -0.21 12.17 815 WW 4/15/2015 6.94 19.3 -0.17 6.77 634 12.51 19.5 -0.17 12.35 645 12.54 19.5 -0.17 12.38 845 12.45 19.5 -0.17 12.29 700 WW 5/17/2015 7.1 19.4 -0.17 6.93 715 12.26 19.6 -0.16 12.10 730 12.17 19.6 -0.16 12.01 930 12.12 19.4 -0.17 11.95 730 WW 6/16/2015 7.18 22.4 -0.08 7.10 700 12.24 23.1 -0.06 12.18 714 12.25 23.1 -0.06 12.19 914 12.19 22.9 -0.06 12.13 714 WW 7/9/2015 6.97 23.9 -0.03 6.94 730 12.23 24.1 -0.03 12.20 745 12.16 24.2 -0.02 12.14 945 12.11 24.1 -0.03 12.08 750 WW 8/11/2015 7.24 24.2 -0.02 7.22 705 12.25 23.4 -0.05 12.20 715 12.21 23.6 -0.04 12.17 925 12.02 23.3 -0.05 11.97 730 WW 9/28/2015 7.13 24.0 -0.03 7.10 630 12.35 24.3 -0.02 12.33 645 12.31 24.4 -0.02 12.29 845 12.17 24.2 -0.02 12.15 700 WW 10/13/2015 6.87 20.8 -0.13 6.74 615 12.42 21.3 -0.11 12.31 625 12.48 21.3 -0.11 12.37 825 12.28 21.1 -0.12 12.16 630 WW 12/1/2015 6.78 17.8 -0.22 6.56 640 12.31 20.4 -0.14 12.17 650 12.29 20.6 -0.13 12.16 850 12.18 20.5 -0.14 12.05 700 WW cU Lvn O N U t � (°� O 4J 7 a O (A 7 a CD rA 7 a O rn 7 a O rA 7 a O U! 7 a O tq 7 a O 41 7 a N O Ul 7 a O fn 7 a O N 7 a O rd 7 a O fA 7 a O fA 7 a fn 7 a O O OOOoOOOOOOOOOOOO Vl 7 C N 7 C O N 7 C W > C N > C N 7 C N 7 C N 7 C N 7 C co N 7 C c7 tll 7 C co N 7 C m N 7 C fA 7 C N 7 C U n N O M M 00 M rl- M 0 M rn M -,t M M M N M r M O M M N 00 N ti N M N LO N V- N (o N (V N N O N M 00 1- (0 LO"'T M N O H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 W WTP Name: The Cape NPDES Number: NCO057703 Monitoring Period: From 1/l/2015 To 12/31/2015 Pathogen Reduction (15A NCAC 02T .l 106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Att B (A1k Treatment)❑ Alt. C (Prior Testing)❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Patho ens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermo l ilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Signifcantl Reduce Pathogens": Lime Stabilization p Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion p If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number or Excee Frequency of Analysis Sample Type Analytical Tech- inimu Geo. Mean Maximud Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry wei ht Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) Vector Aitracnon Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) [] Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) Q No vector attraction reduction alternatives were performed ❑ e:JERFIFtc;ATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signatu of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: July 2, 2015 Topsail Greens 1.94 % Solids 6.11 pH Permit No. WQ0000455 Nitrogen (TKN) 5.420 54,200.000 108.400 Phosphorus 1.930 19 300.000 38.600 Potassium 0.217 2170.000 4.340 PAN (injected)* 2.586 25 864.000 51.728 PAN (surface)* 2.400 24,004.000 48.008 Ammonia Nitrogen 0.372 3,720.000 7.440 Calcium 5.310 53,100.000 106.200 Calcium Carbonate E . --- --- --- Magnesium --- 1,390.000 2.780 Sodium --- 17,000.000 34.000 Sulfur --- --- --- Nitrate N / Nitrite N --- 7,000.000 14.000 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 2,180.00 4.360 Arsenic --- 4.85 0.010 Cadmium --- 4.85 0.010 Chromium --- 7.110 --- Copper --- 1 147.00 0.294 Lead --- 8.50 0.017 Mercury --- 0.25 0.001 Molybdenum --- 4.85 0.010 Nickel --- 6.70 0.013 Selenium --- 4.85 0.010 Zinc --- 773.00 1.546 Environmental Chemists # 2015-08338 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc., envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax rt ® 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com i i G.W. Water Services Date of Report: Aug 03, 2015 1219 Old Folkstone Road Customer PO #: Sneads Ferry NC 28460 Customer ID: 09020031 Attention: Gregory Wright Report #: 2015-08338 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 15-19677 Site: Sludge 7/2/2015 8:16 AM Solid/Sludge Stephen Crews Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 2180 mglkg 07/13/2015 Arsenic EPA 200.7 <4.85 mg/kg 07/09/2015 Cadmium EPA 200.7 <4.85 mglkg 07/09/2015 Calcium EPA 200.7 53100mglkg 07/14/2015 Chromium EPA 200.7 7.11 mglkg 07115/2015 Copper EPA 200.7 147 mglkg 07/09/2015 Lead EPA 200.7 8.50 mglkg 07/09/2015 Magnesium EPA 200.7 1390 mglkg 07/14/2015 Molybdenum EPA 200.7 <4.85 mglkg 07/09/2015 Nickel EPA 200.7 6.70 mg/kg 07/09/2015 Potassium EPA 200.7 2170 mglkg 07/14/2015 Selenium EPA 200.7 <4.85 mg/kg 07/09/2015 Sodium EPA200.7 17000mg/kg 07/14/2016 Zinc EPA 200.7 773 mglkg 07/09/2015 Total Kjeldahl Nitrogen (TKN) EPA351.2 54200 mg/kg 07/14/2015 Nitrate+Nitrite-Nitrogen EPA353.2 7000 mg/kg 07/08/2015 Total Solids (%) SM 2540 B 1.94 % ' 07/09/2015 pH SM 4500 H a 6.11 units --07/10/2015 Ammonia Nitrogen SM 4500 NH3 C 3720 mglkg 07/14/2015 Total Phosphorus SM 4500 P F 19300 mglkg 07/14/2015 Mercury SW8467471B <0.253mg/kg 07/22/2015 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: ` Report P: 2015-08338 Page 1 of 1 s_con.uiar� C�sn�a� CUENT: Gregory H. Wright ADDRESS: 1219 Old Folkstone Rd. Sneads Ferry NC. 28460 Bampw By: S e A e n s"Ple l�rtli�lcatlon E-' 1�111®,,'ME,'TAL CHEMISTS, UC «� �.,►, ,�,,, , . lQ cwwwA1x • N tDtM DLL C®lm m 'm P Vm O"W—' M tM PAX lo; tM PROJECT NAME: REPO CONTACT NAME: PO NI REPORT TO: PHON COPY TO: JUN SAMPLE TYPE: l nkftww, E • Efn w • wru, XT • sm o,InsnonooUE �� o0 NO: i *AX: 90 • Boil, sL a Xlt ., ANALYBWTED 0 O :OIr1AT10M: i�r i�,1101, OM � wwu 1M r im) M we fIW MM Na�ENaa�ea. aM M -- --- - — TwgnraWro when Rsc*,md: d :. RMamp D*Nvand By: RacNvad By: qN� ConM wM: s . - N LEWIS FARMS AND UQUID WASTE, INC. N m WQ W00455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS N Facility Name: /c,oS4 f 1 c rrE of P•O•# Batch Size (gallons): -7C L' Lbs. or Gallons Used: 3 7 L 4L Material Used For Stabilization: Lima Ln 2 Hour pH Z =.= {10Q N M N d o o d e e d g o d o o 0 m o o 0 0 �i o c c o 0 0� 0 0 o d d d a M �, 0 chi a a iL a a S a a U a aa. m a a v M MIA M No r l9 O N N CD W a0 PI!PhH MN V- Oco N N N NN NrM r r r r m A Cn ►+ V N LD U1 a rrn D m � N - - I --- ------ -- -- - - - — �'--- - - - -- '- — - - LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: / p f1SQ G/'e e �S A.O.# Batch Size (gallons): 7. Duo Lbs. or Gallons Used: 3 Sy K Material Used For Stabilization: Lime BONN Lo a ONE El . zMan w IMME 'EM, um"Mm'. Rumm"2a WOMMIM EMEM9".. MIMIMMMIMMM MM MM MMMEIM MMIMM MAIM MMME MMMIMM M WMM M MMM MAIM MM MmiiMEMIMM MAIM ME IM IMMEM MMME EMM MMM MAIM EM MMMM M MIM M ME! MMMMMM MM EMMEEMMMM MMM AIM EMI M MMMMMMEM -- MMMM MAIM EM MMMIMM M IN =11M 1EM MMMMM - M ME ME =11M EM ME MMM ME 11M mml IMM MMM =ME AIM G Ln N a) w M O (- V L0 N m tD M n- r. - m v h O n .o in n �? V Ir Vi M M MN N N T r O O O O O O o r N N' ry i'? t9 n O! ? V O O O O O O O O O O O O O G C: C: p 6 G O O C O G O G U N N V/ YI N YI 1 N 1 O 0 N N N V! N N O gy� 7 w N U 7 7 7 7 O 2 7 7 7 7 7 7 7 O G G C £ C C C G C C G C C C u �- o. o. a a a a. tL i% a. a a. n. a a a E 2 2 M1 2 f 0 EO O CO ti c0 In �t (7 N r O O O c0 lfJ et M N �— O 0) Co 1� c0 tt M N +— O �1 co V) co M M M M M M M N N N N C�1 N N N N N�- H N LEWIS FARMS AND LIQUID WASTE, INC. N m WQ W0045S ALKAUNE S TABUZA TION- OF WASTEWATER BIOSOIJDS � Faciti Name: '� cn hl I @04 r L=r*c,+5 P.O.# Batch Size (gallons): 7, 00 0 Lbs. or Gallom Used: .3 � �' � MaterlaWsed Fm Stabtlhation: Lime 24 Hour pH p c> o O O is y7 a a N1 o d a a M M d 3 IFL o n q N d C7 .7 .0 a a a N d > a: .- tY O > a m» �- o a O > a F d > a` • O d 9 a ao C] G 7 n O j 5 1 O n o o C 2 m 0 /o 7 am "'1 cpp C 10i d r d ty o G a e1 d iy o d ei d C t�i d i► d q d o d u a E O Q <! aD n M M !O M CV)3 M CM M M CA N 10 N r. N <D N �[� CN N M N N N N N• oD — r• V- to *- 'a •- e �- M �- N �- �- O e- t O m a 91 T D r m N 11 C9 N LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: 7-DP54 , I Greens P.O.# Batch Size (gallons): Lbs. or Gallons Used: a- Material Used For stabilization: Lime • R . . • . •. ��® ®®��® ■�ram ���� ���� �� �� dC V u- N O N a N O N a Gl C7 N a w C N a •o G fq a G tlD li O tlJ n V O Ip a r C Iq a O G to ii I O O a N a; Ill a M CSC! W a ,p •! a Pf C; Iq a � O � �� IO CSo � W o � c � O o 3 O � O �� c � rO v Cf of 01 7 N o G I ll Q G U a d O el O m Co M ti M (� O M d �J M M N M r M 0 M 0 N 00 N n N l0 N O N qt N M N �y N �- N O N W 00 P w 0 �t M N +- O H LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name:7opsed GrteAS ROM Batch Size (gallons): 2 &p 6 Lbs. or Gallons Used: Material Used For Stabilization: Lime ffimmm BMW =_ u V N v, N v CA t'i t� co O 0 h 'V N N IID u1 N W tD to m m ^ s m C o in W N O O C O O P7 6 O ry O O O o G G O m m m 0 m m m m m m m Ci N UPa 0 O n o e ? n o U FLo. E a. d IL n. d n. R. fl. U o• O g O M 00 M r, M (Q U) M M N M r' O O 00 r, W lA +Q M N r O M 00 h 0 W) %t M N r O F•- CO CO C9 N N N N N N N N N N r r r r r r r r r r ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: W00000455 W VM Name: Topsail Greens NPDES Number: DEH / Local Monitoring Period: From 1/1/2015 To 12/31/2015 Pathogen Redaction (15A NCAC 02T .1106) -Please indicate level achieved and alternative performed: Class A: Alt A (time/temp) ❑ I Alt B (Alk Treatment) ❑ 1 Alt C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ N applicable to alternative performed (Class A o Indicate "Process to Further Reduce Pathogens": Compost ❑ HcatDrying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ lAlt. 1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ Class B: If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Pathogens. Lime Stabilization El Air Drying ❑ Composting ❑ lAerobic Digestion, ❑ i es ' bic D tio n ❑ Anaerobic H applicable to alternative performed Class A or Class B complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Exceo ° Frequency of Analysis Sample Type Tcc� Geo. Mean Maximunj Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids NWN CFU 1000 min per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 AeN per 4 grams total solid (dry I wei Vector Attraction Redaction (15A NCAC 02T .1107) - Please indicate atternative perfoMen: Altl (VS reduction) ❑ Alt 2 (40-day bench) ❑ Alt 3 (30 day bench) ❑ Alt 4 (Spec. OZ uptake) ❑ Alt 5 (14-Day Aerobic) ❑ Alt. 6 (AK Stabilization Q Alt 7 (Drying -Stable) ❑Alt 8 (Drying -Unstable) ❑ Alt 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T A106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate.the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Stephen V. Crews, ORC Preparer Name and Title (type or print) Signa of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) D Date LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: July 2, 2015 Trenton Permit No. WQ0000455 10.72 % Solids 12.4 pH (taken from lime stabilization event) % x 10,000 g /K x 0.002 Nitrogen (TKN) 0.708 7,083.000 14.166 Phosphorus 0.231 2,306.000 4.612 Potassium 0.070 696.000 1.392 PAN (injected)* 0.252 2,520.500 5.041 PAN (surface)* 0.228 2,282.000 4.564 Ammonia Nitrogen 0.048 477.000 0.954 Calcium 25.367 253,673.000 507.346 Calcium Carbonate E . --- --- --- Magnesium --- 172 234.000 344.468 Sodium --- 1,250.000 2.500 Sulfur --- --- --- Nitrate N / Nitrite N --- 61.700 0.123 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 2,847.00 5.694 Arsenic --- 2.50 0.005 Cadmium - 0.50 0,001 Chromium --- --- Co er --- 31.00 0.062 Lead --- 6.60 0.013 Mercury --- 0.01 0.000 Molybdenum --- 5.00 0.010 Nickel --- 5.00 0.010 Selenium --- 5.00 0.010 Zinc --- 107.00 0.214 Environment 1, Inc. # 268 B *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Emwahmang 90 Blue TOWN OF TRENTON WWTP ATTN: TONY HAWKINS HAWKINS WASTEWATER 202 MY. 41 W. TRENTON ,NC 28585 PARAMETERS Aluminum -(dry wt. basis), mg/kg Arsenic (drywt.�basis), mg/kg Calcium (dry wt. bas' ),.. mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Sodium Adsorption Ratio �3 Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg hd Digester Analysis Method Date Analyst Code 2847 07/27/15 LFJ EPA200.7 <2.S 0711SIlS MTM 3113B-04 2S3673 07/27/1S LFA EPA200.7 <0-S 07/16/15 KM 3113B-04 31 07/27/1S LFJ EPA200.7 6.6 07/13/1S MTM 3113B-04 172234 07/27/15 LFJ EPA200.7 <0.008 07/10/1S MTM 24S.1 R3-94 <S.0 07/27/1S LFJ EPA200.7 696 07/27/15 LFJ EPA200.7 <S-0 . 07/16/15 MTM 311311-04 <12SO 07/27/15 JMN 3111B-99 107 07/28/1S JMN 3111E-99 0.01 07/28/15 . LFJ 10.72 07/06/1S SDB 2540G97 7083 07/09/15 KDB 3S1.2 R2-93 477 07/07/15 KDB 3S0.1 R2-93 2306 07/09/1S AKS 36S.4-74 61.70 07/07/1S RND 3S3.2 R2-93 2282 07/10/1S SEJ <S-0 07/27/1S LFJ EPA200.7 ID#: 268 B DATE COLLECTED: 07/02/15 DATE REPORTED s 07/30/15 REVIEWED BY,; e::__ Patnogen and Vector Attraction f3eduction Log LEWIS FARMS OF EURGAW, INC. W00000455 Facility Name: w►sp ��+��o� Batch Size (gallons): "ZO Q Lbs. or Gallons Used: Material Used for Stablization: Lj •�� Fedor + INN Operator in Responsible Charge Signature : hL Date Temp. c correction Factor 40 Plus 0.45 39 Plus 0.42 38 Plus 0.39 37 Plus 0.36 38 Plus 0.33 35 Plus 0.30 34 Plus 0.27 33 Plus 0.24 32 Pius 021 31 Pius 0.18 30 Plus 0.15 29 Plus 0.12 28 Pius 0.00 27 Plus 0.08 28 Pius 0.03 25 0 24 Minus 0.03 23 Mnus 0.00 22 Mims 0.09 21 Minus 0.12 20 M m 0.15 19 Mnus 0.18 18 Minus 0.21 17 Minus 0.24 1e Minus 0.27 15 Minus 0.30 14 Minus 0.33 13 nus 0.36 12 Mrtus 0.39 11 Mnus 0.42 10 nus 0.45 02/24/2016 08:50 . STAPLES 0600 PAGE 01 Woolen Ferming $ Seed 910 283-2500 p.1 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FOR)VI (02T Rules) F-MU .Name: Lewis -?arts & Liquid Waste, Inc. WQ permit Number, KQoo 45; WW1r1PName: Trenton NPDES Number: NC007 -42 Monitoring Period: From UMD115 To i?./31t2015 Pathogen Reduction (15A NCAC 02T .11M - Please indicate level achieved and alternative performed CkasA.- I Alt A(tiiDelteo+.sl n 1sty ti.s,4•r.....��.... _. _ Hlivable is ost r Hav lass B:icablt: to rabikadi obic Di 1 A lt.D (No 1?tlor MR Air Process to Furtber ,Reduce a "process to Further Vwduee P Treatment -K.. "Process to QeLilcable to alternative rfor�oted Gass A or Class B) com lets the followal monitoring data: parameter Wlatwable Level Pathogen Density 11° ° gBwVQ,,ay ,cy Sample iaSludge inim Geo. Mean aximun Unite " orAnaysia Tape aclr It x 10 to the MPH 6th poVMr per gram of CFU Fecal Coliform total sol;cls ! O—O0 mpn. per gmnx of total Mid (city vrei s ;c+lmanclla bwtwia 31l - p�4 sminsdry 0A lieu of fecal total solid ( coliformI Im"4 htYI I I Feetoir Attraction eduction (15A, MCAC 02T -1107) - Please in Tecate alternative errordcted: if ! (VS.rrciaction) [] Alt. 2 (40-clay bench) U Alt- 3 (3 -day each) ❑ ATt. 4 (Spec. O: ttptaim) r7 !t .S !]A„C1Fn• Aerobic) C3 Alt fi (�11., StabilizRtion Alt 7 (Dryictg - Stablo) E A1L 8 (Drying -Unstable a it 9 (injection) Q Alt.10 (Inoorporation) [j No sector anu:tclion reduction alternatives tyre 'ERTIFI'CA9170N STAx'EM, EIVT [isIesse t4fark rto-...,.,,....4-6- ....a_ ---A% lied'orma ❑ I rrrtiiyr, under pmnlh+ erllw, d.at trig padtogen regtalrentents jS 15A NCAC 02T.1106 and ti c vector attraction reduction reuiremeat in 13A NCAC 02T .1107 have b egg Mal,- r•1 "I oerlit'j,.•-.1., pcy.dof v1 law, Mat Inp pat ngwn wrqutrmnouts in 1SA V10AC QZT.11iM ann t vector aftmeeten t cducltuu mquarement in 15A NCAC 02T .1107 have .tot bm met." (phase n y if YOU chtot:li thin statcuaerti attach an exp1 oafian why you b2ft.not race one tn• both of the tlr0pdltetrntit thion has bees tntule ;u,d y tlit nrtfnti ,m d 0Y 11'oisa w� w,l„nW stir ttlr gfttr gtRped ly lr lure' #tar'I'lii7•d peraoneet y, uperly gather and evaluate the inrp�gHnn nerd ( dvpst�,t; tMilt the pn�4jt;tt Ai1Jl •ea (VA• a trardtiot rgJ1161161t f'N1111MnwVAU bmlu 1111tgw n+fl. 1 .uu nwurr tjlAT Tatft OF% J111M)lAunut 11011A 66 rai 1T ha cerducalcon including rive and Imprisottttoeat." Tony HawI:uas, ORC sl v a PielratterhTnr�a•�d'1'rim l;'PaorP'llif) l.nndAppcQ; dMtotlnl)Till Signature oft-re-parei't Dale Sin _ Rend- lies if APP ( appliaabl..) a Vreparer is definer) ITT 40 CFR Part 503.9(r) ®td MA NCAC 2'1' ,1102 lu f DE•vK FORM PVRF 02T (12I2006) 2015 APPLICATION SUMMARY LEWIS FARMS Permit # WQ 0000455 2015 RESIDUALS APPLICATIONS APPLICATION SUMMARY r` FIELD X ACRES , TOTAL ;TOTAL x < �'flZ , Nv 'V";TOTAL M TOTAL L2 14.30 57,500 5.97 6.68 4.27 L3 18.90 52,000 2.90 0.47 0.29 L4 24.50 68,000 6.50 3.37 3.26 L5 23.30 320,500 24.79 10.33 12.48 L6 5.80 36,000 5.27 3.73 3.73 L7 8.10 57,000 3.07 1.81 3.97 L8 31.80 358,000 24.77 35.59 0.73 L9 36.70 212,000 18.87 7.55 7.66 LIO 14.20 93,500 2.65 2.70 3.24 wi 35.60 990,000 68.12 68.29 39.02 W2 39.20 240,000 16.51 0.00 23.63 W3 24.20 483,500 31.67 23.68 20.86 W4 12.50 30,672 672 150.90 46.18 46.62 AW-F 1 36.30 135,000 12.10 -L 16.29 0.00 Totals [21A IA34672jl M6nIZM2J Metric Tons 339.30 FIELD LOADING RATE REPORTS ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: AQ000045S Annual Dry Tons Applied: 5.97 Owner: Lewis Farms Operator: Lewis Farms Site #: ! Field #: L2 Acres Utilized: 14.30 Acres Permitted: 14.30 Application Method- S/INC Volatilization Rate**: 0.5 Minoralmoffn.. D.t.. an of Predominant Soil Goldsboro - GoA :Date, Gals. Ga1sJ Acre % TS DT/ Acre Residual Source Site Cond. Metals Ibs/ac Nutrients (lbs/ac As Cd Cu. Pb Hg o Ni Se Zn PAN 1 PAN2 p Crop l Crop 21 TKN NH3 N2-143 2015 16.000 1,119 1.72 0.08 Kenwood G/D 0.005 0.005 0.082 0.005 0.000 0.005 0.005 0.005 0.260 0.20 0.08 wheat 039 0.37 0.01 2015 37.500 2,622 1.94 0.21 Topsail Greens 0/1) O.OD2 0.002 0.062 0.004 0.000 0.002 0.003 0.002 0.328 6.11 4.07 9.19 Com wheat 23.00 1.58 2.97 2015 4.000 280 10.721 0.13 Trenton G/D 0.001 0.000 0.008 0.002 0.000 0.001 0.001 0.001 0.027 0.57 0.58 Com 1.77 0.12 0.02 7 Total 57,500 Annual Ibs/acre 0.007 0.007 0.152 0.010 0.000 0.008 0.005 0.008 0.615 6.68 417 8.85 Current Cumulative Ibs/acsr 030 0.21 72.25 3.66 0.05 0.39 1.75 0.38 84.57 149 50 Permit PAN Unit lst/2ad Crop Prior Years Cumulative Ibs/scre 0.29 0.21 72.10 3.65 0.05 0.M 1.74 0.37 83.95 Permitt C.P.L.R.',•• 36 34 1,338 267 15 n/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." Lime :,in,App. Date Lba/A X �I� G✓� Z (SignaturCof LandApplier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, injection/Incorporation -1.0 ***C.P.I..R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 WMMS, PLLC DENR FORM FSF (7/2002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewil Farms Permit #: WOON0455 Annual Dry Tons Applied: 2.90 Owner: Lewis Farms Operator. Lewis Farms Site A 1 Field#: L3 Acres Utilized: 18.9 Acres Permitted: 18.9 Application Method*: S/JNC Volatilization Rate'": 0 5 Minrrattsafine Rae*- an a/ Predominant Soil Goldsboro- GoA Is— .r o...F -a Anoi Date Gals.' GOW Afire % TS DTI Acre Restdual Source Site Cond. Metals Ibslac NutrJents lac As I Cd Cu I Pb Jig I Mo Ni I Se Zn IPANI PAN21 P Cro •l Cro 2 T13N NIB N2-N3 2015 36,000 1905 1.72 0.14 Kenwood G/D 0.008 0.008 0.139 0.008 0.000 0.009 0.008 0.008 0.443 0.26 0.08 0.14 Corn Wheat 0.66 0.63 0.02 2015 16.000 947 0.47 0.02 Ponder HS Q/D 0.001 0.000 0.007 0.003 0.000 0.000 0.003 0.001 0.005 0.21 0.21 0.23 Corn Wheat 0.70 0.12 0.19 Total 52.000 Annual tbt/acre 0.009 0.008 0.146 0.011 0.000 0.008 0.011 U09 Current Cumulative lbsfaereem78.02 4.19 0.04 0.59 2.09 0.57 Prior Years Cumulative I ac.77.88 4.18 0.04 OS8' 2.08 0.56 Permits GP.L R."+'1.3381 267 15 1n!s 374 89 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are significant penalties for submitting false information, Including the possibility of lines and imprisonment for knowing violations." 0.448 105.26 104.81 12.498 OX 0.29 0.37 136 50 Permit PAN Limt 190nd Crop Lime Ants. Date Lbs/Ac -2 e (signaturvorLand Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation "Volatilization Rate: Surface - 0.5. Injeetion/Incorporation -1.0 "**C.P.L.R : Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 DENR FORM FSF (7/2002) Mod. WMMS, PLLC ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit N: WOOOQ04SS Annual Dry Tons Applied: 6.50 Owner: Lewis Farms Operator: Lewis Farms Site 9: 1 Field 0: L4 Acres Utilized: 24.50 Acres Permitted: 24.50 Application Method*: S/INC Volatilisation Rate**! 0.4 o..._. me *. Predominant Sail Goldsboro - GoA Date Gals. caw Acre % IS DT/ Acre Residual Source Site Coadr Metals lbs/ac Nuirlents Ibs/ae As Cd I Cu I Pb HR Mo Ni Se Zn PAN 1 PAN 2 P Crop 1 Crop 21 TKNZ NH3 N2-N3 2015 2015 64,000 4,000 2,612 163 2.37 1.03 0.26 0.01 Castle Bay ay Carrxremm G/D G/D 0.021 0.000 0.021 0.000 1 0.201 0.019 0.021 0.001 0.000 0.000 0.021 0.000 0.021 0.000 0.021 0.000 0.842 0.014 3.26 0.11 3.26 7.07 0.10 Corn Corn Wheat 20.60 0.36 0.47 0.01 0.07 0.00 LTbla]l 68,000 Annual Ibs/acre 0.021 0.021 0.219 0A22 0.000 0.021 0.022 0.021 0.855 3.37 3.26 7.17SKI= Current Cumulative Ibs/acre 0.53 0.29 56.53 0.58 0.30 56.96 3.79 0.07 3.37 148 50 Permit PAN Limt lst/2nd Crop Prior Years Cumulative Iizsraere 0.51 0.26 56.31 0.56 030 56.94 3.77 OAS 2.51 PermittCP.L.IL+*+ 36 34 1,338 267 15 n/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." Lime App. Date Lbs/A x 44�G�.�� 2-2t1_/X (Signature of Land Applier) Date *Application Method: S - Surface, IN - injection, INC- Incorporation "Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 WMMS, PLLC DENR FORM FSF (7/2002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit#: W000004M Annual Dry Tons Applied: 24.79 Owner: Lewis Farms Operator: Lewis Farms Site 0: 1 Field#: L5 Acres Utilized: 23.30 Acres Permitted: 23.30 Predominant Soil Goldsboro - GoA Application Method*: INC Volatilization Rate**: 6.5 Minarotiwati- Ra*®. in of v_..__ Date 2015 Gals. 254,500 G81sJ Acre 10,923 % TS 1.S9 DT/ Acre 0.86 Residual Source Pla CarolinaioG/D Site- Cond. Metals Ibsise Nutrients Ibs/ac ._. As 0.004 Cd 0.002 Cu 0.148 Pb 0.007 He 0.000 I Mo 0.009 NJ-r-s-e-f 0.009 0.0091 Zu 3.686 PAN 1 7.60 PAN 2 9.21 P 44.60 Crop 1 Coro Crop 2 wheat TKN 51.64 NH3 6.46 N2-N3 0.03 2015 66,000 2.833 1.72 0.20 � erBend G/D 0.012 0.012 0.328 0.012 0.000 0.012 0.017, 0.0121 0.319 2.73 3.27 8.13 Corn wheat 19.87 0.17 0.00 Tota! L320,500 05 10.33 12.48 52.73 Annual Ibs/acre 0,016 0.013 0.476 0.018 0.001 0.020 0.020 0.020�56. Current Cumulative Ibs/aere 0.43 0.26 29.81 2.19 0.11 0.29 2.01 0.33 56 148 50 Permit PAN Limt lst/2nd CropDate Prior Years Cumulative lba/aere 0.41 0.24 29.33 2.17 0.11 0.27 1.99 0.31 52.55 Permltt C.P.LR.*** 36 34 1,338 267 LS n/a 374 89 2,498 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information. submitted. I am aware that there are significant penalties for submitting false information, Including the'possibility or fines and imprisonment for knowing violations." Lim A Lbs/A X ,� ✓ 2- z y_le (Signalure.417 Land Applier) Date •Application Method: S - Surface, IN - Injection, INC - incorporation "Volatilization Rate: Surface- 0.5, Injection/Incorporation -1.0 •**C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 DENR FORM FSF (712002) Mod. WMMS, PLLC ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit 11, W00000455 Owner: Lewis Forms Operator: Lewis Farms Site #: 1 Field 9: L6 Acres Utilized: 5.80 Application Method*: S/INC Volatilization Rate**: 0.5 Annual Dry Tons Applied: 5.27 Acres Permitted: 5.90 Predominant Soil Goldsboro - GoA Mineralimatinn Rnto- !n OIL crw..-- _r o_r__J .f.w. Date' GAS.-. GaIsJ Acre % TS DT / I Acre Residual Source Site Cont. Metals Ibs/ac : NuWeatsMlbs/ac As Cd Cu Pb H11 i Mo Ni Se Zn PAN 1 PAN 21 P Cro 1 Cro 2 TKN NH3 N2-N3 201$ 36.000 10.000 2.18 0.91 Clarman G/D 0.008 0.008 0.553 0.043 0.004 0.008 0.020 0.6M 1.384 3.73 3.73 0.64 Corn Wheat 5.24 &40 0.00 Total 36,000 Annual Ibs/scre 0.008 0.008 0.553 0.043 0.004 0.008 0.020 0.009 1384 3.73 Current Cumulative ibs/acre 0.39 0.08 13.99 1.51 0.04 0.21. 0.64 0.16 30.04 148 0.07 1333 1.47 0.04 0.20 0.62 0.15 2&66 Prior Years Cumulative Ibs/sereF36 Permitt C.P.L.R.*** 34 1,338 267 IS n/a 374 89 2,498 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." 3.73 0.64 50 Iftrinit PAN Limt lst/2nd Crop Lime App. Date Lbs/A x IIAI0111 �/ 2- 2 c/-/G (Signatu of LandApplier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilizdtion Rate: Surface- 0.5, Injection/Incorporation - 1.0 ***C.P.LR.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 WMMS, PLLC DENR FORM FSF (7/2002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit N: 3XO0000455 Annual Dry Tons Applied: 3.07 Owner: Lewis Farms Operator. Lewis Farms Site N: 1 Field N: L7 Acres Utilized: 8.10 Acres Permitted: 8.10 Application Method": S Volatilization Rate": 0.5 Minor att"rinn Rb#- an "i Predominant Soil Goldsboro - GoA Date 2015 2015 Gals. 53.000 4,000 Gals./ Acre 6.543 494 % TS 1.30 1.16 DTI Acre 0.35 0.02 Residual Source «� 'rotvn em Center Site Cond. G/D G/D Metals bs/ac) Nutrients (I As 0.028 0.002 Cd 0.028 0.002 Cu 0.958 0.040 Pb 0.028 0.002 Hj O.ODI O.D001 No 0.028 0.002 Ni 0.028 0.002 Se 0.028 0.002 I n 0.503 0.056 PAN 1 1.81 PAN 2 3.52 0.45 P 7.66 0.65 Crop 1 Com Crop 2 What What TKN 15.75 1 1.27 NI113 2.99 0.361 N2-N3 0.00 0.00 Total 57,000 LLL Annual Ibsiscre 0.030 0.030 0.998 0.030 0.001 0.030 0.030 0.0301 0.559 1.81 3.97 8.31 Current Cumulative Ibs/acre 0.13 0.10 36.15 2.11 0.01 0.20 0.90 0.16 51.23 148 50 Permit PAN Limt Ist/2nd Crop Prior Years Cumulative Ibs/acre 0.10 0.07 35.15 2.08 0.01 0.I7 0.87 0.13 50.68 Permitt C.P.L.R."* 1,339 267 15 1 Na 374 89 7,499 "l certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." Lime A . Date Lbs/A x (Signature Land Applier) Date *Application Method: S - Surface. IN - Injection, INC - Incorporation **Volatilization Rate: Surface- 0.5, injection/incorporation - 1.0 •'*C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 WMMS. PLLC DENR FORM FSF (72002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: W 0000455 Annual Dry Tons Applied: 24.77 Owner: Lewis Farms Operator: Lewis Farms Site #: 1 Field #: L8 Acres Utilized: 31.80 Acres Permitted: 31.80 Application Method*: S Volatilization Rate**: 0.5 Mineralization hate_ an *1 Predominant Soil Grantham - Gr Erm.ow of Aa�G...l dAOG DBtc Gals. Galsd Atka % TS DT / Acre Residual Source Site Cond. Metals (Ibs/ae Nutrients Ibs/ae) As Cd Cu I Pb Ha I Mo Ni Se Zn PAN 1 PAN 2 P Crap 1 Cro 2 TKN NH3 N2-N3 96,000 3,019 032 0.04 Maj2015 VVWTP sue s 0/1) 0.000 0.000 0.031 0.001 0.000 0.001 0.002 0.000 0.064 0.73 0.73 2.92 Com Wheat 4.83 0.05 0.00 2015 262.000 9,239 2.15 0.74 S%vRmb0f0 G/D 0.034 0.034 0.629 10.034 0.004 0.034 0.034 0.034 6.220 34.86 39.74 Corn 70.32 2.47 13.27 Total 358.000 Annual tbs/acre 0.035 0.0341 0.660 0.035 0.004 0.035 0.036 0.035 6.284 3559 0.73 42.661 Current Cumulative lbs/acre 0.27 0.15 13.16 1.19 0.03 0.26 0.85 0.26 43.34 137 50 JPermlt PAN Limt lst2nd Crop Prior Years Cumulative Ibs/aere 0.24 0.11 12.50 1.16 0.03 0.22 0.82 0.23 37.05 Pcrmitt C P.L.R.*** 36 34 1,338 267 15 n/a 374 89 2,498 "1 certify. under penalty of law, that this document vas prepared under my direction or supervision in accordance with a system designed to assure thatqualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of tines and imprisonment for knowing violations." Lime App. Date Lbs/A X Amol 2-zy-14' (Signature oPtand Applier) Date *Application Method: S - Surfacer IN - Injection, INC - Incorporation **Volatilization Rate: Surface-0.5, lrl ection/incorporation -1.0 •.*C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Ratc of 1.0 DENR FORM FSF (712002) Mod. WMMS, PLLC ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit M. W00000455 Annual Dry Tons Applied: 18.87 Owner: Lewis Farms Operator: Lewis Farms Site 1i: 1 Field q: L9 Acres Utilized: 36.70 Acres Permitted: 36.70 Predominant Soil Grantham - Gr Application Method*: S/1NC Volatilization Rate**: 0.5 Mineralization Rate: 3n *i ra..nee..roeer .a AAOZ Date Gals. GalsJ Acre % TS DT / Acre Residual Source Site Cond. Metals (lbs/ac) utrients lbs/ac As Cd Co Pb Hg Me Ni I Se Zn PAN I PAN 2 P I Crop 1 Crop 2 TIKN NH3 N2-N3 2015 78,000 2,125 331 0.29 Bald dead Island G/D 0.002 0.007, 0.280 0.002 0.000 0.002 0.008 0.002 0.634 2.12 1.81 18.77 Corn Wheat 4.25 0.04 OSl 2015 134,000 3,651 1.45 0.22 Beaultivev G/D 0.003 0.003 0.128 0.004 0.002 0.003 0.005 0.003 0.283 5.43 5.85 17.44 Com wheat 36.21 1.84 _ 0.05 Total 212,000 Annual Ibs/acre 0.005 0.005 0.407 0.005 0.002 0.005 0.012 0.005 0.917 7.55 Current Cumulative lbs/acre 0.41 0.20 53.99 3.24 0.05 0.54 1.67 10.49 7658 137 Prior Years Cumulative lbs/sere 0.40 0.19 53.58 3.24 0.05 0.53 1.66 OAS 75.66 Fermin C.P.L.R.*** 36 34 1,338 267 15 We 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." 7.66 36.22 50 Permit PAN Limt lst/2nd Crop Llme App. Date Lbs/A X- (Signatur6 of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 DENR FORM FSF (712002) Mod. WMMS, PLLC ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: W00000455 Owner: Lewis Farms Operator. Lewis Farms Site #: 1 Field #: L10 Acres Utilized: 14.20 Application Method*: S Volatilization Rate**: OS Annual Dry Tons Applied: 2.65 Acres Permitted: 1410 Predominant Soil Norfolk - NoA Mineralization Rate: 30 '/n ttnuc. of V..fn.d AnCl- Date Gals. Gals./ Acre % TS DT / Acre Residual - -Source Site Cond. Metals lbslac Nutrients Maine As Cd Cu Pb H9 Mo Ni Se Zn PAN 1 PAN 2 P Crop] Cro2 TKN NH3 N2-N3 2015 2015 32,000 61.500 2,254 4,331 1.16 0.43 0.11 0.08 1'lampawal pines . rcr mg anus WYM G/D G/D 0.009 0.003 0.009 0.001 0.041 0.040 0.009 0.017 0.000 0.001 0.009 0.001 0.009 0.017 0.009 0.005 0.327 0.918 2.70 2.70 0.54 4.77 4.29 Conn whew Whew 17.09 10.05 1.28 0.17 0.02 0.06 Total 93,500 Annual ibs/acre 0.012 0.010 0.081 0.026 0.001 0.010 0.026 0.014 1.245 2.70 3.24 9.06 Current Cumulative Ibslarre 0.13 0.11 40.35 2.10 0.02 0.23 0.% 0.17 61.17 131 50 Permit PAN LIM Is0nd Crop Prior Years Cumulative Ibs/acre 0.12 0.10 40.27 2.07 0.02 0.22 0.94 0.16 59.92 Permitt C.P.L.R.**' 36 34 1,338 267 15 n/a 374 89 1 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Lime App. Date Lbs/A X - (Signatu of Land Applicr) Date *Application Method: S - Surface. IN - Injection. INC - Incorporation '*Volatilization Rate: Surface - 0.5,, Injection/Incorporation - 1.0 *"C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 WMMS. PLLC DENR FORM FSF (7/2002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit 4: W00000455 Annual Dry Tons Applied: 68.12 Owner:. Lewis Farms Operator: Lewis Farms Site /h W Field M 1 Acres Utilized: 35.60 Acres Permitted: 35.60 Predominant Soil Grantham - Gr Application Method*: S Volatilization Rate**.- 0.5 n ..-. 1.. Date 2015 Gals:: 990,000 GauJ Aare 27.809 % TS 1.65 DT / Acre 1.91 Residual Source . House of Raeford Site Cond. G/D As Cd I Cu 0.023 0.023 0.792 Metabs lbs/ac I 'Pb H 0.023 0.004 ---- ------ Mo Ni Se Zn 0.023 0.070 0.025 0.903 -- - IavYiC VI nucluru 4V70 Nutrfenh PAN I PAN 21 P CroP 1 68.29 39.02 70.03 soybean Ibs/se I Cron 2 TKN NH3 N2-N3 wheat 263.67 17.30 0.11 Total 990,000 Annual ibs/sere 0.023 0.0231 0.792 0.023 0.004 0.023 0.070 0.02S 0.903 68.29 39.02 70.03 Current Cumulative tbs/acre 0.20 0.19 71.93 3.87 0.03 0.35 1.96 032 10235 146 M Permit PAN Limt lst/2nd Crop Prior Yeses Cumulative fbs/acrc 0.17 0.17 71.04 3.84 0.03 0.32 1.89 E0.2 101dS Permits C.P.[.R."• 36 34 1,338 267 15 n/a 374 2,498 "I certify, under penalty of law. that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." Lime App. Date Lbs/A X (Signature of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation •0Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0 "0C.P.I..R.: Cumulative Pollutant I..oading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 WMMS, PLLC DENR FORM FSF (7/2002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit N: W00000455 Owner: Lewis Farms Operator: Lewis Farms Site N: W Field N: 2 Acres Utilized:.39.20 Application Method*: _ S Volatilization Rate**: 0.5 Annual Dry Tons Applied: 16.51 Acres Permitted: 39.20 Mine�nlFrofrnn rloln. 2n of Predominant Soil Grantham - Gr Date ' 2015 Gals. 240,000 Gals./ Acre 6,122 _ % TS 1.65 DT/ Acre 0.42 Residual Source dousef R oaeford Site Cond. G/D Metals . Ibs/ac) Nutrients bs/ac As 0.005 Cd 0.005 Cu 0.174 Pb 0.005 Hg 0.001 Mo 0.005 Ni 0.015 Se 0.005 Zn 0.199 PAN 1 PAN 2 23.63 P 15.42 Crop 1 Crop 2 wheat TifCN 58.05 NH3 N2-N3 3.81 0,02 Torat 1 240.000 Annual lbs/aere 0.005 0.005 0.174 0.005 0.0011 0.005 0.0151 0.005 0.199 0.00 123.0 Current Cumulative Ibs/acre 0.27 0.19 13.93 1.78 0.02 75.18 0.63 033 26.2t 146 Prior Years Cumulative lbs/acre 0.26 0.18 13.751 1.77 0.02 75.18 0.62 033 26.02 Permitt C.P.L.R.*** 36 34 1,338 267 15 n/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1 15.42 50 JPermlt PAN Limt Ist/2nd Crop LlmeApp. Date Lbs/A x alkw��2- ?- (Signatufe of Land Applier) Date *Application Method: S - Surface. IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injcction/Incorporation 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 WMMS, PLLC DENR FORM FSF (7/2002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: W00000455 Owner: Lewis Farms Operator: Lewis Farms Site #: W Field #: 3 Acres Utilized: 24.20 Application Method*: SANC Volatilization Rate": 0.5 Annual Dry Tons Applied: 31.67 Acres Permitted: 24.20 Predominant Soil Woodington - Wo Minarall-ya inn tutu. 7n oL a Date. 2015 VVTL 62400 WT'sJ Acre 2,583 % TS 0.43 DT/ Acre 0.05 Residual Source Stcri ag nrma Site Cond. Ql) Metals Ibs/se Nutrients (Ibs/ac) As 0.002 Cd 0.001 Cu 0.024 I Pb 0.010 HelMo. 0.000 0.001 Nil 0.010 Se 0.003 Za 0.547 PAN 1 PAN 2 0.32 P 2.56 Crop 1 Crop 2 wheat TKN 5.99 NH3 0.10 N2-N3 0.04 2015 421,000 17,397 1.74 1.26 110 Caw G/D 0.014 0.014 0.656 0.026 0.001 0.014 .0.038 0.018 1.479 23.68 20.54 6236 Soybean Wheat 139.61 11.56 0.03 Total 483,500 Annual lbsfacre 0.016 0.015 0.690 0.036 0.001 0.015 0.048 0.021 2.027 23.68 20.86 64.91 Current Cumulative Ibsfacre 0.33 0.14 76.38 3.95 0.06 0.25 1.73 0.28 97.85 112 50 Permit PAN Lemt lst/2nd CropDate Prior Years Cumulative Ibs/acre 0.31 0.13 75.70 3.91 0.06 0.24 1.68 0.26 95.92 Permitt C.P.L,R.*** 36 34 1,338 267' 15 n/a 374 89 1 2,499 "I certify, under penalty of law, that this document was prepared under my direction or, supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." LimeApp. Lbs/A x (Signatu of land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Injection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 WMMS. PLLC DENR FORM FSF (712002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: W 0000455 Annual Dry Tons Applied: 150.90 Owner: Lewis Farms Operator: Lewis Farms Site #: W Field #: 4 Acres Utilized: 12.50 Acres Permitted: 1250 Application Method*: INC Volatilization Rate**-- III o_.- 9A e. Predominant Soil Woodington - We Date 2015 2015 Cls. 672 30,000 Gals./ Acre 54 2,400 % TS 2210 1.37 DTI Acre 11.93 0.14 Residual Source Morehead City s ename Park r obiie Site Cond. G/D G/D Metals bs/ac) Nutrients Ibs/ac As 0.103 0.002 Cd 0.103 0.002 Cu 17.759 0.097 Pb 0.284 10.004 H 0.034 0.000 Mo. 0.103 0.002 Ni 0.233 0.092 Se 0.126 0.002 Zn 22.175 0.216 PAN 1 46.18 PAN 2 46.18 0.44 P 448.75 0.23 Crop1 Crop2 TKN . NH3 N2-N3 soybean wheac wheat 529.90 0.90 13.03 0.79 26.26 0.01 Total 1 30,672 Annual lbs/acre 0.105 0.105 17.846 0.289 0.035 0.105 0.236 0.128 22.391 46.18 46.62 448.98 Current Cumulative ibslacre 0.32 0.18 34.17 1.57 0.06 0.32 0.83 0.26 46.00 I12 50 Permit PAN Limt Ist/2nd Crop Prior Years Cumulative lbs/acre 0.21 0.07 16.33 1.28 0.03 0.21 0.59 0.13 23.61 Pcrmitt C»P.LR.•"" 361 34 1,338 267 15 1 nla 374 89 2.498 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Lime Apo. Date Lbs/A x G✓ 2 - 2 y-/& (Signature of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation "Volatilization Rate: Surface - 0.5. Injection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 WMMS, PLLC DENR FORM FSF (7/2002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit M. W00000455 Annual Dry Tons Applied: 12.10 Owner: Allen H. Wooten Operator: Lewis Farms SIte #: AW Field #: Ft Acres Utilized: 36.30 Acres Permitted: 36.30 Predominant Soil Goldsboro - GoA Application Method*: INC Volatilization Rate**: 1.0 Mineralization Rate! 30 wnu"n at0..rwrd AM, Date Gals. GalsJ Acre % TS DT / Acre Residual Source Site Cond. Metals Ibsiae Nutrients Ibs/ac As Cd I Cu Pb A Me Ni Se Zn PAN 1 PAN 2 . P Cro1 Cro 2 TKN NH3 N2-N3 2015 135,000 3,719 2.15 033 Swa-bo- G/D 0.016 0.016 0.284 0.016 0.002 0.016 0.016 0.016 2.807 16.29 17.94 %heaat 31.74 1.11 5.99 Coral 135,000 Annual ibs/acre 0.016 0.016 0.284 0.016 0.002 0.016 0.016 0.016 L907 16.29 0.00 17.94 Current Cumulative Ibs/acre 0.02 0.02 0.28 0.02 0.00 0.02 0.02 0.02 L81 112 50 Permit PAN Limt Istl2nd Crop Prior Years Cumulative lba/acre 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Permitt C,P.LR.***. 36 34 1,338 267 15 n/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel. properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Lime App. Date Lbs/Acl x G✓�%L 2-2�/7� (Signureat of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of l.0 DENR FORM FSF (72002) Mod. WMMS, PLLC SOIL- ANALYSIS REPORTS It should be noted that the majority of residuals land applied under NCDENR Permit No. WQ0000455 achieve pathogen reduction and vector attraction reduction requirements through alkaline stabilization. Therefore, the material being land applied is adding lime through most of the land application events. The pH's ranging from 5.0 to 7.1 on all fields is well suited for the growth of the corn, soybean, wheat and coastal bermuda. G"A-k Martin Mabe Agronomist Page 1 of 4 Report Number: 16-020-0613 Account Number: 08361 Waypoint, Send To: WILLCOX & MABE SOIL SOLUTIONS, PI ANALYTICAL 1205 W. BESSEMBER AVE' Every acre... Every year. SUITE 202 GREENSBORO NC 27408 Submitted By: ROBB SOIL ANALYSIS REPORT Date Received: 01/20/2016 Date Of Analysis: 01/21/2016 Date Of Report: 01/21/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: LEWIS FARMS AND LIQUID WAS PROJ# 15-20 Analytical Method(s): Mehlich 3 OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil Ibs/A Mehilch 3 M3 phosphorus Saturation Ratio K M g Ca Na Soll Buffer H Field ID Number Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/100g meq/100g AW-F1 16295 1.1 68 211 VH 51 L 56 H 388 M 7 VL 6.2 0.4 3.0 L NC=176 NC=26 JJ01 16296 1.2 70 234 VH 53 L 54 H 372 M 6 VL 6.2 0.3 2.8 L NC=195 NC=27 JJ02 16298 1.2 69 215 VH 56 L 64 H 458 M 7 VL 6.3 0.4 3.4 L NC=179 NC=29 JR-F1 16299 11 68 229 VH 53 L 52 H 366 M 6 VL 6.3 0.3 2.7 L NC=191 NC=27 L02 1.6 192 VH 113 VH 84 M 684 H 16300 75 6 VL 6.6 0.3 4.7 L NC=160 NC=58 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID , Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS CI AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm AW-F1 10 L 4.6 H 18 M 1.3 M 4.4 15.6 64.7 1.0 13.3 266 VH 0.3 VL NC = 21 NC = 115.0 NC = 113 NC = 65.0 JJ01 10 L 4.6 H 10 M 0.9 M 4.9 16.1 66.4, 0.9 10.7 295 VH 0.3 VL NC NC=115.0 NC=63 NC=45.0 JJ02 8 VL 4.3 H 24 H 1.1 M 4.2 15.7 67.4 0.9 11.8 292 VH 0.3 VL NC = 17 NC = 107.5 NC = 150 NC = 55.0 JR-F1 8 VL 4.4 H 10 M 1.0 M 5.0 - 16.0 67.8 1.0 11.1 295 VH 0.3 VI - NC =17 NC=110.0 NC=63 NC=50.0 L02 9 VL 5.6 H 11 M. 1.5 M 6.2 14.9 72.8 0.6 6.4 271 VH 0.4 L NC NC=140.0 NC=69 NC 75.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts permillion), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc. by: ?,W,. me 60w r/ Pauric McGroary Page 2 of 4 Report Number: 16-020-0613 • Account Number:08361 Waypoint(D Send To: WILLCOX & MABE SOIL SOLUTIONS, PI ANALYTICAL 1205 W. BESSEMBER AVE Every acre... Every year."m SUITE 202 GREENSBORO NC 27408 Submitted By: ROBB Date Received: 01/20/2016 Date Of Report: 01/21/2016 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: LEWIS FARMS AND LIQUID WASQ PROJ# 15-20 Sample ID Yield Goal Lime Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Field ID Intended Crop Tons/A N P205 K20 Mg S Zn Mn Fe Cu B Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A AW-F1 Adjust pH to 6.0 0 0.0 24 2 0 JJ01 Adjust pH to 6.0 0 0.0 26 2 0 JJ02 - Adjust pH to.6.0 0 0.0 16 0 0 JR-F1 Adjust pH to 6.0 0 0.0 28 2 0 L02 ' Adjust pH to 6.0 0 0.0 0 2 0 Comments: Sample(s) : JJ01,JJ02,JR-F1 Crop: Adjust pH to 6.0 Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." QAWi� mF G r Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1 work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 3 of 4 - -- - -- ----- ---- -- - Report Number: 16-020-0613 ' Account Number:08361 Waypoint Send To: WILLCOX & MABE SOIL SOLUTIONS, PI ANALYTICAL 1205 W. BESSEMBER AVE Every acre... Everyyear.'4M SUITE 202 GREENSBORO NC 27408 Submitted By: ROBB SOIL ANALYSIS REPORT Date Received: 01/20/2016 Date Of Analysis: 01/21/2016 Date Of Report: 01/21/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: LEWIS FARMS AND LIQUID WAS PROJ# 15-20 Analytical Method(s): Mehlich 3 OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil Class Ibs/A Mehllch 3 M3 Phosphorus Saturation'Ratio K M g Ca Na Soil Buffer H Field ID Number Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g L03 16301 1.4 71 188 VH 118 VH 86 H 659 H L NC=157 NC=60 6 VL 6.6 0.3 4.6 L04 16302 1'44.8 +71 185VH 114 VH 82 M 678 H L NC=154 NC=58 6 VL 6.4 0.4 L05 16303 1.6 75 196 VH 121 M 91 M 716 H L NC=163 NC=62 6 VL 6.5 0.4 5.1 L06 16304, 1.5 74 183 VH7 110 H 82 H 648 H 5 VL 6.6 0.3 4.5 L NC=152 NC=56 L07 16305 1.1 68 218 VH 53 L 53 H 370 M 4 VL 6.2 0.3 2.7 L NC=182 NC=27 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS CI AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm L03 11 L 5.7 H 12 M 1.8 H 6.6 15.6 71.6 0.6 6.5 283 VH 0.5 L NC = 23 NC = 142.5 NC = 75 NC = 90.0 L04 12 L 5.6 H 11 M 1.6 H 6.1 14.2 70.6 0.5 8.3 272 VH 0.4 L NC = 25 NC = 140.0 NC = 69 NC = 80.0 L05 10 L 5.9 H 12 M 1.7 H 6.1 14.9 70.2 0.5 7.8 283 VH 0.4 L NC = 21 NC = 147.5 NC = 75 NC = 85.0 L06 10 L 5.4 H 11 M 1.6 H 6.3 15.2 72.0 0.5 6.7 272 VH 0.4 L NC = 21 NC = 135.0 NC = 69 NC = 80.0 L07 8 VL 4.3 H 10 M 0.9 M 5.0 16.4 68.5 0.6 11.1 283 VH 0.3 VL NC = 17 NC = 107.5 NC = 63 NC = 45.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A; Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. by: Patio me (1=a'�,J� Pauric McGrovary Page 4 of 4 Report Number: 16-020-0613 • Account Number:08361 Waypoint.(D Send To: WILLCOX & MABE SOIL SOLUTIONS, PI ANALYTICAL 1205 W. BESSEMBER AVE "Every acre ... Every year."T, SUITE 202 GREENSBORO NC 27408 Submitted By: ROBB Date Received: 01/20/2016 Date Of Report: 01/21/2016 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: LEWIS FARMS AND LIQUID WAS PROJ# 15-20 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A L03 Adjust pH to 6.0 0 0.0 0 2 0 L04 Adjust pH to 6.0 0 0.0 0 2 0 L05 Adjust pH to 6.0 0 0.0 0 2 0 L06 ' Adjust pH to 6.0 0 0.0 0 2 0 L07 Adjust pH to 6.0 0 0.0 27 2 0 Comments: Sample(s) : L07 Crop: Adjust pH to 6.0 Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. "The recommendations are based on research data and experience, but NO GUARANTEE -or WARRANTY expressed or implied, conceming crop performance is made." Q Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1 AWi6 m� G work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 4- Report Number: 16-020-0615 Account Number:08361 Waypoint.(D Send To: WILLCOX & MABE SOIL SOLUTIONS, PI ANALYTICAL 1205 W. BESSEMBER AVE "Every acre ...Every year. "m SUITE 202 GREENSBORO NC 27408 SOIL ANALYSIS REPORT Date Received: 01/20/2016 Date Of Analysis: 01/21/2016 , Date Of Report: 01/21/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: LEWIS FARMS AND LIQUID WAS PROJ# 15-20 Analytical Method(s): Mehlich 3 OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number , �o Rate Soil Class lbs/A Mehllch3 M3 ppm Rate Phosphorus saturation Ratio K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil PH Buffer Index H' meq/100g megN00g L08 16313 1.2 L 69 231 VH NC=192 80 M NC=41 54 M 398 M 4 VL 5.9 6.87 0.6 3.3 1 L09 16314 1.3 72 224 VH 78 M 51 M 311 M 5 VL 6.0 T- 0.5 3.0 L NC=187 NC=40 L10 16315 1.3 72 212 VH 74 M 47 M 358 M 5 VL 6.0 0.4 2.8 L NC = 177 NC = 38 W01 16316 0.8 63 187 VH 55 L 19 L 150 L 7 VL .076.86 0.7 1.8 VL NC = 156 NC = 28 W02 16317 0.8 64 200 VH 57 L 15 L 120 L 4 VL 5.4 6.89 0.4 1.3 VL NC = 167 NC = 29 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Chloride Aluminum Sample ID Field ID K eke Mg % Ca % Na % H % NO3N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate CI ppm Rate AI ppm L08 11 L 2.4 M 10 M 3.3 VH 6.2 13.6 60.3 0.5 18.2 NC=23 NC=60.0 NC=63 332 VH NC=165.0 0.4 L L09 11 L 2.4 M 10 10 M 3.3 VH 6.7 14.2 61.5 0.7 16.7 NC=23 NC=60.0 3 323 VH NC=165.0 0.4 L L10 6.8 14.0 63.9 0.8 14.3 9 VL NC = 19 2.1 L NC = 52.5 10 M NC = 63 311 VH 3.1 VH NC = 155.0 0.3 VL W01 7.8 8.8 41.7 1.7 38.9 7 VL NC=15 1.6 L NC=40.0 5 L NC=31 197 VH 3.4 VH NC=170.0 0.2 VL W02 11.2 9.6 46.2 1.3 30.8 8 VL NC=17 1.6 L NC=40.0 5 L NC=31 196 VH 3.6 VH NC=180.0 0.2 VL Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. by: P,w« OF 60'wr Pauric McGroary Page 2 of 4 Report Number: 16-020-0615 Account Number: 08361 O' Way ■ ■t," p (D Send To: WILLCOX & MABE SOIL SOLUTIONS, PI ANALYTICAL 1205 W. BESSEMBER AVE "Every acre ... Every year. SUITE 202 GREENSBORO NC 27408 Date Received: 01/20/2016 Date Of Report: 01/21/2016 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: LEWIS FARMS AND LIQUID WAS PROJ# 15-20 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N F2% KZO Mg S Zn Mn Fe Cu B Field ID Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A L08 Adjust pH to 6.0 0 0.8 26 2 0 L09 Adjust pH to 6.0 0 0.0 29 2 0 L10 Adjust pH to 6.0 0 0.0 33 2 0 W01 Adjust pH to 6.0 0 0.8 61 3 0 W02 Adjust pH to 6.0 0 0.8 65 3 0 Comments: Sample(s) : 1-09,1-10 Crop: Adjust pH to 6.0 Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : W01,W02 Crop: Adjust pH to 6.0 Apply dolomitic lime to raise pH and improve the magnesium level. If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, conceming crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 3 of 4 Report Number: 16-020-0615 Account Number: 08361 Waypoint. Send To: WILLCOX & MABE SOIL SOLUTIONS, PI ANALYTICAL 1205 W. BESSEMBER AVE Every acre ... Every year."m SUITE 202 GREENSBORO NC 27408 SOIL ANALYSIS REPORT Date Received: 01/20/2016 Date Of Analysis: 01/21/2016 Date Of Report: 01/21/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: LEWIS FARMS AND LIQUID WAS PROJ# 15-20 Analytical Method(s): Mehlich 3 OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab o �o Soil Ibs/A Mehllch 3 M3 Phosphorus saturation Ratio K Mg Ca Na Soil Buffer H Field ID Number Rate Class :ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g W03 16318 0.8 64 199 VH 56 L 15 L 119, L 4 VL 5.3 6.89 0.4 1.3 VL NC = 166 NC = 29 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm W03 10 L 1.6 L 5 L 3.6 VH 11.0 9.6 45.8 1.3 30.8 194 VH 0.2 VL NC=21 NC=40.0 NC=31 NC=180.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by ffl pWi° Pe Gow C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: WaypointAnalytic:al Virginia, Inc. Pauric McGroary Page 4 of 4 Report Number: 16-020-0615 • Account Number: 08361 Waypoint. Send To: WILLCOX & MABE SOIL SOLUTIONS, PI ANALYTICAL 1205 W. BESSEMBER AVE Every acre ...Every year. ",m SUITE 202 GREENSBORO NC 274.08 Date Received: 01/20/2016 Date Of Report: 01/21/2016 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: LEWIS FARMS AND LIQUID WAS PROJ# 15-20 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A W 03 - Adjust pH to 6.0 0 0.8 65 3 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, conceming crop performance is made." ?or;, me r Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary i Page 4 of 4 Report Number: 15-027-0508 Account Number:45819 Send To: S&ME (1588) MARTIN MABE 3718 OLD BATTLEGROUND RD GREENSBORO NC 27410-2314 L A&L Eastern Laboratories 7621 Whftepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-W6 www.aleastem.com Grower: Submitted By: MARTIN MABE LEWIS FARMS Farm ID: JOB#1588-95-010 SOIL ANALYSIS REPORT Analytical Method(s): Date Received: 01/27/2015 Date Of Analvsis: 01/28/2015 Date of Rennrt. n1/2R/gm_j; Mehlich 3 OrganicMatter, Phosphorus , Potassluhi'�-` ' '.;;,Magnesium: ' Calcium. . . Sodium. pH Acidity C.E.0 Sample ID Lab % Rate ENR Mehuch 3: Reserve ...K•,' u: ` _:._ ;, .'M g:.,. ,. Ca . Na Soil ' Buffer H Field ID Number Ibs/A.' , ppm. Rate ppm Rate ppm: . Ra; a-- ppm " `Rate `ppm ' Rate. ppm Rate pH Index meq/100g meq/100g W04 11661 2.4 L 81 170 VH 83 L 169 M 1983 VH 18 VL NC=142 NC=42 71 0.0 11.6 61 H IRSH 1088 7 • NC=51 NC=70 6.2 NC=44 NC=64 Percent,Base'Safuiation Nitrate . `r ' Sulfur, 2incr' :; x =' angaFjes®. ,.;; ;::alron .;; 'F ••;Copper; . Boron solubtesalta .. •Chloride • Aluminum . Sample ID Fleld*ID K M g Ca Na H NON _ : ; S :. B 'SS CI AI % % _ . %. % 3 ppm Rate ppm Rafe 'ppm .:'Rate, .p ,.,.. m, Mate; ;ppm:,., -Rate ;ppm `- Rate ppm Rate mslcm ;Rate: ppm Rate ppm W04 17 M 16.1 VH 12 M 306 VH 4.6 VH 0.5 L 1.8 12.1 85.5 0.7 0.0 NC = 35 NC = 402.5 NC = 75 NO = 230.0 L NC=42 NC=130.0 1 NC=44 NC=75.0 JQ I 1 1 4rn 1 NC = 27 NC = 105.0 1 NC = 38 NC = 65.0 lam I Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pod. me 61,wr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary