NC0000396_Mercury Field Blank information_20200102

Action History (UTC-05:00) Eastern Time (US & Canada)
Submit by Anonymous User 1/2/2020 9:50:14 AM (Supplemental Submittal)
Submit by Bennett, Bradley 1/6/2020 9:58:42 AM (Supplemental Info Submittal)
• Bennett, Bradley assigned the task to Bennett, Bradley 1/6/2020 9:57 AM
• The task was assigned to Thedford, Wren, Bennett, Bradley 1/2/2020 9:50 AM

Initial Review Information
Updated ID#:* IWORTANf:FEVIBAERSl-IOLLDVERFYand revise here ifnecessary.
NC0000396
How should this project be handled?*
r File r Discard
Information Submitted on 1/2/2020
Submitter Information
Name: Teresa Williams
Who is subrritting the inforrretion?
Email Address:* [e-mail]
Submittal Information
The Division of Water Resources (DWR) is providing this site to allow for the upload of required supplemental
information associated with discharge monitoring reports (DMR). All DMR data is required to be submitted
electronically through the eDMR system and should not be submitted here. Division staff will reviewall
uploaded documents and will only maintain required information. Documents such as laboratory reports are not required
to be submitted and will not be maintained in the system.
Project Information:
Rease SUDDly the Dernit nun ber for this
Existing ID#* PerrritNurrber
NC0000396
Exarrples: NOKxxxxxx or NO&xxxxx
Facility Name:* Asheville Steam Electric Station
County: Buncombe
Please upload all files that need to be
submited. *
dick the upload button or drag and drop files here to attach docurrent
12-23-19 12520B ASVL PLT November 2019
1.62 MB
NPDES DMR.pdf
Only pdf files are accepted.
Comments about the attachments:
The weekly low level Hg field blank sample collected November 26, 2019 did not meet quality control criteria. Per
division guidance the sample has been noted in the comments and the associated lab report attached.
* V By checking the box and signing box below, I certify that:

• I have given true, accurate, and complete information on this form;
• I agree that submission of this Supplemental Information form is a "transaction" subject to Chapter 66, Article 40 of the
NC General Statutes (the "Uniform Electronic Transactions Act)
• I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes
(the "Uniform Electronic Transactions Act');
• I understand that an electronic signature has the same legal effect and can be enforced in the same way as a written
signature; AND
• I intend to electronically sign and submit the Supplemental Information form."
Full Name: Teresa Williams
Signature:
Date Submitted: 01/02/2020

fDUKE
ENERGY.
PROGRESS
Submitted Electronically
File No.: 12520B
December 23, 2019
ATTN: Central Files
NCDEQ, Division of Water Resources
1617 Mail Service Center
Raleigh NC 27699-1617
Subject: Asheville Steam Electric Generating Plant
Buncombe County
NPDES Number NC0000396
Discharge Monitoring Report (DMR)
Dear Sir or Madam:
Garry A. Whisnant
Plant General Manager
Asheville Steam Electric Plant
Duke Energy Progress
ASVL PLT J 200 CP&L Or
Arden, NC 28704
o: 828-687.5211
t: 828.687-5204
Barry whrsnant®duk"nergy com
In accordance with condition I.A. (18) 1., replaced by electronic signature and submission
guidelines, the November 2019 NPDES eDMR for Duke Energy Progress's Asheville Steam
Electric Plant — NPDES Permit Number NC0000396 has been submitted.
The Outfall 001 weekly low-level mercury field blank sample collected on November 26, 2019
did not meet quality control criteria in accordance with EPA Method 1631E. Per Division
guidance ("NPDES Mercury Requirement- EPA Method 1631 Additional Information"), mercury
field blank sample has been noted in the eDMR comments section, and the associated analytical
report is attached to this cover letter and uploaded electronically to the eDMR Supplement Data
Upload server.
Please contact Ms. Teresa Williams at [phone] or Mr. Matthew Fields at [phone]
with any questions concerning the data in this submittal.
Best regards,
Gary Fou�
Asheville Operations Superintendent

NPDES PERMIT NO.: N00000396 PERMIT VERSION: 3 1
FACILITI',NAME: Asheville Steam Electric Power PlantCLASS: PC-1
OIYNER NAME: Duke Energy Progress LLC ORC: Matthew Holcomb Fields
GRADE: PC-1 ORC HAS CHANGED: No
rDMR PERIOD: 11-2019 (November 2019) VERSION: 10
COMPLIANCE STATUS: Compliant CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Buncombc
ORC CERT NUMBER: 1003106
STATUS: Submitted
St! BNIISSION DATE: 12i190019
12A 812019
ORC/Certifier Signature: Matthew Fields E-Mail: matthew.fie lds-'�i.dukc-cncrgy.corn Phone #:[phone] Date
By this signature. I certify that this report is accurate and complete to the best of my kno«ledge.
The permince shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permitlee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part ILEA of
the NPDES permit.
12?1912019
ermilteelSobmitler Signature:*** Gary Fouts E-Mail=gary.fouts-Fr.duke-energy.com Phone #_828-687-5211 Date
Permittee Address- 200 CPL Dr Arden NC 28704 Permit Expiration Date; 11/30/2023
certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and W, icf, true.
accurate, and complete. 1 am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Asheville Steam Electric Plant, Pace Analytical Services, Inc. Environmental Testing Solutions, Duke Energy Analytical Laboratory
CERTIFIED LAB H: 5055, 40, 12. 37. 248
PERSON(s) COLLECTING SIMPLES: Matthew Fields. R.W Smith, J C Green
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by N isiting http,fiportal.ncdenrorg/web/wq,swp.-ps.-npdcs/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data,
* No Flow. -Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period,
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittce: If signed by other than the permitice. then delegation of the signatory authority must be on file With the state per 15A NCAC 2B
.0506(b)(2)(D),

NPDES PERMIT NO.: NCO000396 PERMIT VERSION: 3 1
FACILITY NAME: Asheville Steam Electric Power PlantCLASS: PC.I
OWNER NA11E: puke Energy Progress LLC ORC: Matthew Holcomb Fields
GRADE: PC-1 ORC HAS CHANGED: No
eD\IR PERIOD: 11-2019(November2019) VERSION: 10
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: V103106
STATUS: Submitted
SAMPLING LOCATION: DOWNSTREAM DISCHARGE NO.: 001
... *No Reporting Reason. ENFRUSE-- No Flow•ReuseiRecycic ENVWTHR -No Visitation-Adcrose Wcalher; NOFLOW -No Flow. HOLIDA►' -No Visitation- Holiday

Nf DES PERMIT NO.: NCO000396 PERMIT VERSION: 3 1
FACILITN' NAME: Asheville Steam Electric Power PlantCLASS: PC-1
OWN ER,N,1\IE: Duke Energy Progress LLC ORC: Matthew Holcomb Fields
GRADE: PC-1 ORC IIAS CIIANGED: No
eDNIR PERIOD: 1 l 2019 (November 2019) VERSION, 10
PERMIT STATUS: Active
COUNTI': Buncombe
ORC CERT \UMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: DOWNSTREAM DISCHARGE NO.: 001 (Continue)
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NPDES PERMIT NO.: N00000396 PERh11T VERSION: 3 1
FACILITY NAME: Asheville Steam Electric Power PlaniCLASS: PC -I
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Flolcomb Fields
GRADE: PC-1 ORC I[AS CIIANGED: No
eDMR PERIOD: 11-2019 (November 2019) VERSION: 10
PERMITSTATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO,: 001 NO DISCHARGE*: NO
••" No Reporting Reason ENFRUSE , No Flow-ReuselRecycle: ENV WTl1R . No Visitation - Adverse Wcathcr; NOFLOW No Flow. HOLIDAY - No Visitation - Holiday

NPDES PERMIT NO.: NCO000396 PERMIT VERSION: 3 1
FACILITY NAME: Asheville Steam Electric Power PlanICLASS: PC4
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Ilolcomb Fields
GRADE: PC -I ORC HAS CHANGED: No
eDMR PERIOD: 11-2019 (November 2019) VERSION: 10
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT,NUNIBER: 1003 [06
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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•"" No Reponing Rcason. ENFRUSE No Flow-Reuse,Recycle; ENVWTIIR -.No Visitation - Adverse Weather: NOFLOW „ No Flow. HOLIDAY No Visitation Holiday

NPDES PERMIT NO.: N00000396 PERMIT VERSION: 3 1
FACILITY NAME: Ashcv tile Steam Electric Power PlantCLASS: PC-1
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Holcomb Fields
GRADE: PC-1 ORC 11AS CHANGED: No
eD,NI R PER IOD: 11 -2019 (November 2019) VERSION:10
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
•••• No Reporting Reason ENFRLSE No Flow-RcuseAtecycle, ENVIVTHR No Vtsimnon - Adverse Weather. NOFLOW w No Flow; HOLIDAY- No Visitation - Holiday

NPDES PERMIT NO.: NCO000396 PERMIT VERSION: 3 1
FACILITY NAME: Asheville Steam Electric Power PlantCLASS: PC -I
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Holcomb Fields
GRADE: PC -I ORC IIAS CIIANGED: No
eDMR PERIOD: 11-2019 (November 2019) VERSION: 10
PER\IIT STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: UPSTREAM DISCHARGE NO.: 001
*— No Reposing Reason ENFRUSE- No Flow-ReusuRecycle, ENVWTIIR- No Visuauon- Ad%crse Weaihcr, NOFLOW - No Flow, HOLIDAY - No Visitation -Holiday

NPDES PERMIT NO.: NC0000396 PERMIT VERSION: 3.1 PER:IIIT STATUS: Active
FACILITY NAME: Asheville Steam Electric Power PlantCLASS: PC -I COUNTY: Buncombe
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Holcomb Fields ORC CERT NUMBER: 1003106
GRADE: PC -I ORC IIAS CHANGED: No
eDMR PERIOD: 11-2019 (November 2019) VERSION: 10 STATUS: Submitted
SAMPLING LOCATION: UPSTREAM DISCHARGE NO.: 001 (Continue)
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•"• No Reporting Reason ENFRLSE- No Flow•Reusc.Rccycle, ENVWTIIR- No Visitation - Adverse Weather: NOFLOW -No Flow. HOLIDAY No Visitation Holiday

NPDES PERMIT NO.: NC0000396 PERMIT VERSION: 3 1
FACILITY ,NAME: Asheville Steam Electric Power PlaniCLASS: PC -I
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Ilolcomb Fields
GRADE: PC -I ORC HAS CIIANGED- No
eDMR PERIOD: 11-2019 (November 2019) VERSION: 10
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT \UMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001A NO DISCHARGE*: NO
•••' No Reporiing Reason ENFRUSE - No Flow-ReusciRccycle. ENV WTHR - No Visitation - Adverse Weather; NOFLON No Flow, HOLIDAY- No Visitation - Holiday

INPDES PERMIT NO.: NC0000396
PERMIT VERSION: 3 1
PERMIT STATUS: Active
FACILITY NAME: Asheville Steam Electric Power P1anICLASS: PC -I
COUNTY- Buncombe
OWNER NAME: Duke Energy Progress LLC
ORC: Malthety Holcomb Fields
ORC CERT NUMBER: 1003106
GRADE: PC-1
ORC 1[AS CHANGED: No
eDMR PERIOD: 11-2019 (November 2019)
VERSION: 10
STATUS: Submitted
SAMPLING LOCATION:
EFFLUENT DISCHARGE NO.: 001B NO DISCHARGE*: NO
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NPDES PERMIT NO.: NC0000396 PERMIT VERSION: 3 1
F_►C[LITV NAME: Asheville Steam Electric Power Plan1CLASS: PC -I
OWNER NAME: Duke Energy Progress LLC ORC: Malthew Ilolcomb Fields
GRADE: PC -I ORC I[AS CI[ANGED: No
eD%IR PERIOD: 11-2019 (November 2019) VERSION: 10
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001C NO DISCHARGE*: YES
****No Repatttng Reason ENFRLSE No Flaw-RcuswRecycle, ENVWPIR - No Visaation Adverse %%eailter, NOFLOW - No Flaw, IIOLIDAY � No Visuauan - Holiday

NPDES PERMIT NO.: NC0000396 PERMIT VERSION: 3 1
FACILITY NA,\IE: Asheville Steam Clectric Po%%cr PlantCLASS: PC -I
OWNER NAME: duke Energy Progress LLC ORC: Matthew Ifolcomb Fields
GRADE: PC-1 ORC HAS CHANGED: No
eD,NIR PERIOD: l 1-2019 (November 3019) VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 0011) NO DISCHARGE*: NO
I
'—No Rcponing Reason ENFRUSE - No Flow-RcosclRecycle, ENVWTIiR -- No Vishation Ad%erse Weather NOFLOW No Flow. IIOLIDAN' No Visitation Holiday

NPDES PER►[[T NO.: NC0000396 PERMIT VERSION: 3 l
FACILITY NAME: Asheville Steam Electric Power PlantCLASS: PC -I
ON\NER NAME: duke Energy Progress LLC ORC: Matthew Holcomb Fields
GRADE: PC -I ORC IIAS CIIANGED: No
eDNIR PERIOD: 11-2019 (November 2019) VERSION: 10
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NU NIBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: DOWNSTREAM DISCHARGE NO.: 001E
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NPDES PERMIT NO.: NC0000396 PERMIT ►VERSION: 3 1
FACILITY NAME: Asheville Steam Electric Power P1antCLASS: PC -I
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Ilolcomb Fields
GRADE: PC -I ORC HAS CHANGED: No
eDNIR PERIOD: 1 I-2019 (November 2019) 1'ERSION: 1 0
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
010• tin Reporting Reason. ENFRUSE .. No Flow•ReuseiRecycle, ENV%VTHR -No Visitation - Ad%erse Weathcr; NOFLOW -NO Flow, HOLMAN' . No Visitation- Holiday

NPDES PERMIT NO.: NCO000396 PERMIT VERSION: 3 1
FACILITY NAME: Asheville Steam Electric Power PlaniCLASS: PC-1
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Ilolcomb Fields
GRADE: PC-1 ORC HAS CHANGED: No
eD,%[R PERIOD: 11-2019 (November 2019} VERSION: 10
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: YES
"" No Reponing Reason. ENFRUSE - No Flow•RcuscMccycle. ENVWTHR - No Visitation - Adccrsc Weather, NOFLOW - No Flow. HOLID,k - No Visitation Holiday

NPDES PERMIT NO.: NC0000396 PER.**[1T VERSION: 3 1
FACILITYNAME. Asheville Steam Elcctrtc Power P1antCLASS: PC-1
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Ilolcomb Fields
GRADE: PC- I ORC HAS CHANGED: No
eD,NIR PERIOD: 11-2019 (November 2019) VERS[ON: 10
PERM I STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 005 NO DISCHARGE*: YES
•"' No Rcporttnu Reason. ENFRUSE .. No Flaw-RcuselRecycle, ENV WTIIR -- No Visitation Adverse Weather, NOFLOW - No Flaw, I [OLIDAY - No Visitation Holiday

NPDES PERMIT,NO.: NC0000396 PERMIT VERSION: 3 1
FACILITY NAN1E: Asheville Sieam Electric Power PlanICLASS: PC -I
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Holcomb Fields
GRADE: PC. I ORC HAS CIIANGED: No
eDdIR PERIOD: 11 -20 19 (November 2019) VERSION: 10
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: ]003I%
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 101 NO DISCHARGE*: YES
"" No Retioning Reason. ENFROSE No Flow-Reuse,Recycle: ENVWTHR No Visiiaiion Adverse Weather; NOFLOW . No Flow, HOLIDAY No Visuaiion Holiday

NPDES PERMIT NO.: NC0000396 PERMIT VERSION: 3 1
FACILITY NAME: Asheville Steam Electric Power PlantCLASS: PC-1
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Ilolcomb Fields
GRADE: PC-1 ORC 11AS CHANGED. No
rD,%IR PERIOD: 11-2019 (November 2019) VERSION: 10
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: 1003106
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 101 NO DISCHARGE*: YES (Continue)
WWWWOMENEWE
---- NO iccportmg Kcason tNFRi:St- No Flow-Reusc.Rccycle, EN**'%k'TIIR - No Visilauon Advcrse'Acwher. NOFLOII No Flow. HOLIDAY - No Vlsimoon Iloliday

NPDES PERMIT NO.: NC0000396 PERMIT VERSION: 3 1
FACILITY NAME: Asheville Stcam Electric Power PlantCLASS: PC -I
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Holcomb Fields
GRADE: PC-1 ORC HAS CHANGED: No
eD,%IR PERIOD: 11-2019 (November 2019) VERSION: 1 0
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NU,►1AER: 1003106
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 101 NO DISCHARGE*: YES (Continue)
""No Reponing Rcason, ENFRUSE ^ No Flow-Rcusc/Recycic, ENVWTHR - No Visitation - Adverse Weather; NOFLOW -No Flow. HOLIDAY � No Visitation Holiday

NPDES PERMIT NO.: NC0000396 PERMIT VERSION: 3 1
FACILITY NAME: Asheville Steam Electric Power PlantCLASS: PC -I
OWNER NAME: Duke Energy Progress LLC ORC: Matthew Holcomb Fields
GRADE: PC -I ORC HAS CHANGED. No
eDtiIR PERIOD: 11-2019 (November 2019) VERSION: 10
Report Comments:
Qualifiers included for the following parameters
M I - Matrix spike recovery exceeded QC Iimus Batch accepted based on laboratory control sample (LCS ) recovery
Applied to Outfall 001 - Bromide. Fluoride on 11/12119, Chloride on I Ul Br 19
CO - Result confirmed by second analysis
App] ied to Outfall 001 - Hg field blank on 11126/19.
PERMIT STATUS: Active
COUNTY: Buncombe
ORC CERT NUMBER: 1003106
STATUS: Submitted
The uKnury field blank sample from 11/26/19 did not meet quality control criteria. The analytical report is uploaded with the electronic copy of the November 2019 DMR

#=CL#
December 09, 2019
LIMS USE: FR - MATTHEW FIELDS
LIMS OBJECT ID: 92455341
92455341
Project:
Pace Project No.:
RE:
Mr. Matthew Fields
Duke Energy Progress, Inc.
,
Outfall 001 11/26
Dear Mr. Fields:
Enclosed are the analytical results for sample(s) received by the laboratory on November 26, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
cc:Ms. Mariea Keezel, Duke Energy
Program Manager, Duke Energy
Ms. Teresa Williams, Duke Energy Progress, Inc.
Mr. Robert Wylie, Duke Energy Progress, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 18
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 18
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92455341001 FIELD BLANK EPA 1631E 1 PASI-ARDT
92455341002 OUTFALL 001_2019/11/26_0805_N EPA 1664B 1 PASI-CHH
EPA 200.7 Rev 4.4 1994 11 PASI-AKQ
EPA 1631E 1 PASI-ARDT
SM 2540C-2011 1 PASI-ACJL
SM 2540D-2011 1 PASI-ACJL
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
SM 4500-Cl-E-2011 1 PASI-AGC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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205 East Meadow Road - Suite A
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Page 3 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Sample:FIELD BLANK Lab ID:92455341001 Collected:11/26/19 08:05 Received:11/26/19 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 1631E Preparation Method: EPA 1631E1631E Mercury,Low Level
Mercury 0.673 ng/L 12/09/19 15:34 7439-97-6 C011/27/19 15:320.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Sample:OUTFALL
001_2019/11/26_0805_N
Lab ID:92455341002 Collected:11/26/19 08:05 Received:11/26/19 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 1664BHEM, Oil and Grease
Oil and Grease ND mg/L 12/04/19 10:255.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Arsenic 130 ug/L 12/02/19 04:14 7440-38-211/27/19 01:2110.0 1
Beryllium ND ug/L 12/02/19 04:14 7440-41-711/27/19 01:211.0 1
Cadmium ND ug/L 12/02/19 04:14 7440-43-911/27/19 01:211.0 1
Chromium 5.9 ug/L 12/02/19 04:14 7440-47-311/27/19 01:215.0 1
Copper ND ug/L 12/02/19 04:14 7440-50-811/27/19 01:215.0 1
Lead ND ug/L 12/02/19 04:14 7439-92-111/27/19 01:215.0 1
Nickel 13.4 ug/L 12/02/19 04:14 7440-02-011/27/19 01:215.0 1
Selenium 53.3 ug/L 12/02/19 04:14 7782-49-211/27/19 01:2110.0 1
Silver ND ug/L 12/02/19 04:14 7440-22-411/27/19 01:215.0 1
Hardness, Total(SM 2340B)144000 ug/L 12/02/19 04:1411/27/19 01:216621
Zinc ND ug/L 12/02/19 04:14 7440-66-611/27/19 01:2110.0 1
Analytical Method: EPA 1631E Preparation Method: EPA 1631E1631E Mercury,Low Level
Mercury 3.24 ng/L 12/09/19 14:43 7439-97-611/27/19 15:320.50 1
Analytical Method: SM 2540C-20112540C Total Dissolved Solids
Total Dissolved Solids 290 mg/L 11/26/19 21:2825.0 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids 14.3 mg/L 12/02/19 18:262.5 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Bromide 0.18 mg/L 11/27/19 13:37 24959-67-90.10 1
Fluoride 0.62 mg/L 11/27/19 13:37 16984-48-80.10 1
Analytical Method: SM 4500-Cl-E-20114500 Chloride
Chloride 18.9 mg/L 11/27/19 21:00 16887-00-61.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
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Page 5 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
512534
EPA 1664B
EPA 1664B
1664 HEM, Oil and Grease
Associated Lab Samples:92455341002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2748049
Associated Lab Samples:92455341002
Matrix:Water
Analyzed
Oil and Grease mg/L ND 5.0 12/03/19 10:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2748050LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/L 36.340 91 78-114
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2748051MATRIX SPIKE SAMPLE:
MSSpike
Result
35514803001
Oil and Grease mg/L 72.1 M139.2 161 78-1148.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
512113
EPA 1631E
EPA 1631E
1631E Mercury,Low Level
Associated Lab Samples:92455341001, 92455341002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2746316
Associated Lab Samples:92455341001, 92455341002
Matrix:Water
Analyzed
Mercury ng/L ND 0.50 12/09/19 14:05
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2746317
Associated Lab Samples:92455341001, 92455341002
Matrix:Water
Analyzed
Mercury ng/L ND 0.50 12/09/19 14:36
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2746318
Associated Lab Samples:92455341001, 92455341002
Matrix:Water
Analyzed
Mercury ng/L ND 0.50 12/09/19 15:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2746319LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ng/L 4.875 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2746320MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92455341002
2746321
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ng/L 25 77 71-12571 7253.24 22.4 20.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511984
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
200.7 MET
Associated Lab Samples:92455341002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2745902
Associated Lab Samples:92455341002
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 12/02/19 04:07
Beryllium ug/L ND 1.0 12/02/19 04:07
Cadmium ug/L ND 1.0 12/02/19 04:07
Chromium ug/L ND 5.0 12/02/19 04:07
Copper ug/L ND 5.0 12/02/19 04:07
Hardness, Total(SM 2340B)ug/L ND 662 12/02/19 04:07
Lead ug/L ND 5.0 12/02/19 04:07
Nickel ug/L ND 5.0 12/02/19 04:07
Selenium ug/L ND 10.0 12/02/19 04:07
Silver ug/L ND 5.0 12/02/19 04:07
Zinc ug/L ND 10.0 12/02/19 04:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745903LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 495500 99 85-115
Beryllium ug/L 474500 95 85-115
Cadmium ug/L 475500 95 85-115
Chromium ug/L 463500 93 85-115
Copper ug/L 478500 96 85-115
Hardness, Total(SM 2340B)ug/L 3070033100 93 85-115
Lead ug/L 473500 95 85-115
Nickel ug/L 469500 94 85-115
Selenium ug/L 483500 97 85-115
Silver ug/L 243250 97 85-115
Zinc ug/L 475500 95 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745904MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92455341002
2745905
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 103 70-130104 0500130646649
Beryllium ug/L 500 97 70-13096 1500ND484481
Cadmium ug/L 500 99 70-13099 0500ND496498
Chromium ug/L 500 95 70-13094 15005.9 479 474
Copper ug/L 500 99 70-13098 1500ND496492
Hardness, Total(SM 2340B)ug/L 33100 92 70-13088 133100144000174000173000
Lead ug/L 500 97 70-13097 1500ND483485
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745904MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92455341002
2745905
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nickel ug/L 500 95 70-13095 050013.4 489 490
Selenium ug/L 500 109 70-130110 150053.3 600 604
Silver ug/L 250 101 70-130100 1250ND253251
Zinc ug/L 500 98 70-13098 0500ND497497
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511969
SM 2540C-2011
SM 2540C-2011
2540C Total Dissolved Solids
Associated Lab Samples:92455341002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2745846
Associated Lab Samples:92455341002
Matrix:Water
Analyzed
Total Dissolved Solids mg/L ND 25.0 11/26/19 21:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745847LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids mg/L 250250 100 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92454834008
2745848SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 117 1118
Parameter Units
Dup
Result QualifiersRPDResult
92455353006
2745849SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 251 4242
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
512462
SM 2540D-2011
SM 2540D-2011
2540D Total Suspended Solids
Associated Lab Samples:92455341002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2747895
Associated Lab Samples:92455341002
Matrix:Water
Analyzed
Total Suspended Solids mg/L ND 2.5 12/02/19 18:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2747896LABORATORY CONTROL SAMPLE:
LCSSpike
Total Suspended Solids mg/L 262250 105 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92455292002
2747897SAMPLE DUPLICATE:
Total Suspended Solids mg/L 12.2 212.0
Parameter Units
Dup
Result QualifiersRPDResult
92455315001
2747898SAMPLE DUPLICATE:
Total Suspended Solids mg/L 22.7 1025.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 11 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
512017
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Associated Lab Samples:92455341002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2745958
Associated Lab Samples:92455341002
Matrix:Water
Analyzed
Bromide mg/L ND 0.10 11/27/19 11:37
Fluoride mg/L ND 0.10 11/27/19 11:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745959LABORATORY CONTROL SAMPLE:
LCSSpike
Bromide mg/L 2.42.5 97 90-110
Fluoride mg/L 2.62.5 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745960MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92455228001
2745961
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromide mg/L 2.5 100 90-110103 32.5ND 2.5 2.6
Fluoride mg/L 2.5 110 90-110109 02.5ND 2.8 2.8
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745962MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454827004
2745963
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromide mg/L 2.5 103 90-110104 12.5ND 2.6 2.6
Fluoride mg/L 2.5 109 90-110110 12.5ND 2.8 2.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 12 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
512193
SM 4500-Cl-E-2011
SM 4500-Cl-E-2011
4500 Chloride
Associated Lab Samples:92455341002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2746716
Associated Lab Samples:92455341002
Matrix:Water
Analyzed
Chloride mg/L ND 1.0 11/27/19 20:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2746717LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride mg/L 19.920 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2746718MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454824004
2746719
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride mg/L M6106990-11062 010346352352
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2746720MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454395001
2746721
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride mg/L 10 93 90-11094 0104.8 14.1 14.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 18
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92455341
Outfall 001 11/26
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Result confirmed by second analysis.C0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 18
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92455341
Outfall 001 11/26
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92455341002 512534OUTFALL 001_2019/11/26_0805_N EPA 1664B
92455341002 511984 511998OUTFALL 001_2019/11/26_0805_N EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92455341001 512113 512184FIELD BLANK EPA 1631E EPA 1631E
92455341002 512113 512184OUTFALL 001_2019/11/26_0805_N EPA 1631E EPA 1631E
92455341002 511969OUTFALL 001_2019/11/26_0805_N SM 2540C-2011
92455341002 512462OUTFALL 001_2019/11/26_0805_N SM 2540D-2011
92455341002 512017OUTFALL 001_2019/11/26_0805_N EPA 300.0 Rev 2.1 1993
92455341002 512193OUTFALL 001_2019/11/26_0805_N SM 4500-Cl-E-2011
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/09/2019 04:56 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 18
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