HomeMy WebLinkAboutNC0088226_Renewal (Application)_20200103 ' St
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MICHAEL S.REGAN ....•,,,
Secrrfary
LINDA CULPEPPER NORTH CAROLINA
()irr,n:, Environmental Quality
January 03, 2020
Wells Fargo Bank, N.A.
Attn: John Cranfill
550 S Tryon St Ste 180
Charlotte, NC 28208
Subject: Permit Renewal
Application No. NC0088226
Duke Energy Center dewatering system
Mecklenburg County
Dear Applicant:
The Water Quality Permitting Section acknowledges the January 3, 2020 receipt of your permit renewal application and
supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW permitting
branch. Per G.S. 150B-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The
permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a
timely manner to requests for additional information necessary to allow a complete review of the application and renewal
of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deq.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerely,
Lk(1120
Wren Thedford
Administrative Assistant
Water Quality Permitting Section
ec: WQPS Laserfiche File w/application
North Ca ro ra Department of Env ronmenta! uality Dotson of Water Resources
P Q I
DE Q ?Iooresv e Regan Off ce 1610 East Center Avenue,Surte 301 I Mooresviifa,North Caro:na 2 115
.. . . ..r.� 704-6E3-1699
�Ir
ECS SOUTHEAST, LLP "Setting the Standard for Service"
Imummrti Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F-1078
NC Registered Geologists Firm C-406
.:.4 rg Firm 3239
January 2,2020
NCDEQ/DWR/NPDES Unit
Attn:Wren Thedford
1617 Mail Service Center
Raleigh, NC 27669-1617 RECEIVED
JAN032019
Reference: Request for NPDES Permit Application Renewal
Wells Fargo Tryon Street GWR-NPDES Permit NC0088226 NCDEQ/DWR/NPDES
500 Block of South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project 49-1234-E
Dear Mr.Thedford:
ECS Southeast, LLP (ECS), on behalf of Childress Klein Properties and Wells Fargo, N.A., is requesting
approval for renewal of the existing system that is currently operating and has National Pollutant
Discharge Effluent System (NPDES) permit NC0088226. The permit includes the capture of site rain
water and de-watering groundwater from the site subgrade parking garage but also de-watering
groundwater from the adjacent subgrade parking garage at "The Green at Wachovia". Additionally, the
captured water is routed through an on-site water treatment system designed by Aquapura, Inc. that
utilizes the water for on-site needs such as in cooling towers thereby lowering the amount of municipal
water required. The attached renewal has been signed by Mr. John Cranfill of Childress Klein an
authorized signee for the permit.
BACKGROUND INFORMATION
The subject site is the Wells Fargo Tryon Street GWR (WFTS-GWR) which includes the tower and
subgrade parking deck at 550 South Tryon Street, located at the 500 block of South Tryon Street in
Charlotte, Mecklenburg County, North Carolina. The WFTS-GWR site is bound by Church Street to
the northwest, Levine Avenue of the Arts to the northeast, Stonewall Street to the southwest and
South Tyron Street. Currently, the site is operating NPDES permit No. NC0088226 and discharging
groundwater to a storm sewer located in South Tryon Street. The storm sewer ultimately discharges to
Little Sugar Creek, a Class C surface water in the Catawba River Basin. Figures 1 and 2 indicate the
location of this site and outfall location. No sludge waste is generated as part of the treatment process.
Filters are replaced as needed and properly disposed of off-site.
Permit Sampling
In accordance with the existing NPDES permit, the system includes treatment of the water prior to
discharge, via the Aquapura system. The permit also requires that the discharge be monitored,
sampled, and reported. Additionally, a monthly discharge monitoring report (DMR) is required to be
submitted to the NCDEQ, DWQ. The DMR requires the monthly monitoring, including the collection of
grab effluent samples for laboratory analysis, and reporting. Once per quarter, additional grab samples
of the effluent are required to be collected and submitted for laboratory analysis for chronic toxicity
with results submitted to the NCDEQ. ECS does not recommend changes to the scheduled sampling. A
copy of the most recent post treatment data (from November 2019) collected prior to discharge in
accordance with the current permit and reporting is included as an attachment to this application.
ECS Capitol Services,PLLC • ECS Honda,LLC • ECS Mid-Atlantic,LLC • ECS Midwest,LLC • ECS Southeast,LLP • ECS Texas,LLP
www.ecslimited.com
Request for r NPDES Permit Renewal
Wells Fargo Tryon Street GWR
Charlotte, North Carolina
ECS Project 49-1234-E
January 2, 2020
Permit Modification
No changes are proposed to the system or permit since the prior renewal.
SUMMARY AND CLOSING
Wells Fargo, N.A. is requesting a renewal for the permit related to the system that has been operating
under permit number NC0088226. Should more detailed figures and information be required, they can
be provided to the NCDEQ, upon request.
If there are questions regarding this submittal, or a need for further information, please contact us at
(704) 525-5152.
Respectfully submitted,
ECS SOUTHEAST, LLP
fit, , �l
Christopher D. Orrell, P.G. Matthew H. McDuffie, P.G.
Project Manager Principal Geologist
cc: John Cranfill, Childress Klein
Attachments:
NPDES Permit Application—Short Form C-GW
Figures
November 2019 Laboratory Data
2
NPDES PERMIT APPLICATION
1
NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities.
Mail the complete application to:
N. C. Department of Environment and Natural Resources
Division of Water Quality / NPDES Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
NPDES Permit Number NC0088226
If you are completing this form in computer use the TAB key or the up - down arrows to move from one
field to the next. To check the boxes, click your mouse on top of the box. Otherwise,please print or type.
1. Contact Information:
Owner Name Well Fargo, N.A. - Wells Fargo Tryon Street GWR
Facility Name Wells Fargo Tryon Street GWR
Mailing Address 550 South Tryon Street, Suite 180
City Charlotte
State / Zip Code North Carolina 28202
Telephone Number (704)330-2545
Fax Number ( )
e-mail Address john.cranfill@childressklein.com
2. Location of facility producing discharge:
Check here if same as above
Street Address or State Road 500 Block of South Tryon Street
City Charlotte
State / Zip Code North Carolina 28202
County Mecklenburg
3. Operator Information:
Name of the firm, consultant or other entity that operates the facility. (Note that this is not referring to the
Operator in Responsible Charge or ORC)
Name Childress Klein Properties
Mailing Address 550 South Tryon Street
City Charlotte
State / Zip Code North Carolina 28202
Telephone Number (704)330-2545
Fax Number ( )
4. Ownership Status:
Federal ❑ State ❑ Private ® Public ❑
Page I of 3 C-GW 03/05
NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities.
5. Products recovered:
Gasoline ® Diesel fuel ® Solvents ® Other
6. Number of separate discharge points: 1
Outfall Identification number(s) 001
7. Frequency of discharge: Continuous ❑ Intermittent 121
If intermittent:
Days per week discharge occurs: varies (batch discharge) Duration: varies
(batch discharge)
8. Treatment System Design flow 0.087 MGD
9. Name of receiving stream(s) (Provide a map showing the exact location of each outfall, including
latitude and longitude):
unknown tributary to Little Sugar Creek in Catawba River Basin: Lat 35°12'25.5" N, Lon
80°50'52.8". A map is attached.
10. Please list all additives to the treatment system, including chemicals or nutrients, that
have the potential to be discharged.
Antiscalant/antifoulant. These compounds are removed by the system prior to discharge.
11. Is this facility located on Indian country? (check one)
Yes ❑ No
12. Additional Information
All applicants (including renewals):
> A USGS topographical map (or copy of the relevant portion) which shows all outfalls
> A summary of the most recent analytical results (effluent data, if available) containing the
maximum values for each chemical detected
NEW Applicants only:
> Engineering Alternative Analysis
• Description of remediation treatment system components, capacities, and removal
efficiency for detected compounds.
> If the treatment system will discharge to a storm sewer, written approval from the
municipality responsible for the sewer.
> A list of any chemicals found in detectable amounts at the site, with the maximum
observed concentration reported for each chemical (the most recent sample must be
collected less than one year prior to the date of this application)
> For petroleum-contaminated sites-Analyses for Volatile Organic Compounds (VOC) should
be performed. Analyses for any fuel additives likely to be present at the site and for phenol
and lead should also be performed.
Page 2 of 3 C-GW 03/05
NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities.
For sites contaminated with solvents or other contaminants - EPA Method 624/625
analysis should be performed.
13. Applicant Certification
I certify that I am familiar with the information contained in the application and that to the
best of my knowledge and belief such information is true, complete, and accurate.
John Cranfill Senior Chief Engineer
Printed name of Person Signing Title
Si a of Applicant Date
North Carolina General Statute 143-215.6 (b)(2) provides that: Any person who knowingly makes any false
statement representation, or certification in any application, record, report, plan, or other document files or
required to be maintained under Article 21 or regulations of the Environmental Management Commission
implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or
monitoring device or method required to be operated or maintained under Article 21 or regulations of the
Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable
by a fine not to exceed $25,000, or by imprisonment not to exceed six months, or by both. (18 U.S.C. Section
1001 provides a punishment by a fine of not more than$25,000 or imprisonment not more than 5 years, or both,
for a similar offense.)
Page 3 of 3 C-GW 03/05
FIGURES
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Outfall Facility .
Latitude: 35°12'25.5" N 35°13'28.5" N + --_,_...}
Longitude: 80°50'52.8" W 80°50'55.3"W
Stream Class: C , Facility Location
Subbasin 03-08-34 HUC: 03050103
Receiving Stream UT to Little Sugar Creek Wells Fargo Tryon Street GWR NC0088226
Mecklenburg County
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LEGEND
® Dewatering System Location
Dewatering Wells and Piping NN' Permitted Dewatering System Sewer Outfall(001)
SOURCE: FIGURE 2
Mecklenburg County Property Ownership De-Watering System and
Land Records Information System Discharge Location Plan
(POLARIS) Wells Fargo Tryon Street N
via Internet NPDES Permit NC0088226
INIMINOPE171113
2009 Aerial Photograph Charlotte, North Carolina
SCALE: As Noted ' ECS PROJECT NO. 49-1234-D
I
LAB DATA
Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pac.labs.com (704)875-9092
November 27, 2019
David Valentine
ECS Southeast, LLP
1812 Center Park Dry
Suite D
Charlotte, NC 28217
RE: Project: Wells Fargo Monthly
Pace Project No.: 92454537
Dear David Valentine:
Enclosed are the analytical results for sample(s) received by the laboratory on November 20, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
taylor.ezell@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Chris Orrell,ECS Southeast,LLP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 17
Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacelabs.com (704)875-9092
CERTIFICATIONS
Project: Wells Fargo Monthly
Pace Project No.: 92454537
Pace Analytical Services Charlotte
9800 Kincey Ave.Ste 100, Huntersville,NC 28078 South Carolina Certification#:99006001
Louisiana/NELAP Certification#LA170028 Florida/NELAP Certification#:E87627
North Carolina Drinking Water Certification#:37706 Kentucky UST Certification#:84
North Carolina Field Services Certification#:5342 VirginiaNELAP Certification#:460221
North Carolina Wastewater Certification#: 12
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 North Carolina Wastewater Certification#:40
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
Massachusetts Certification#:M-NC030 VirginiaNELAP Certification#:460222
North Carolina Drinking Water Certification#:37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 17
Pace Analytical Services,LLC
® 9800 KinceyAve. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacelabs.com (704)875-9092
SAMPLE ANALYTE COUNT
Project: Wells Fargo Monthly
Pace Project No.: 92454537
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92454537001 001 EPA 1664B HH 1 PASI-C
EPA 200.7 Rev 4.4 1994 DS,SH1 3 PASI-A
EPA 8260D GAW 63 PASI-C
SM 2540D-2011 CJL 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 17
Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aeAnaIicaI Huntersville,NC 28078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: Wells Fargo Monthly
Pace Project No.: 92454537
Sample: 001 Lab ID: 92454537001 Collected: 11/19/19 15:00 Received: 11/20/19 09:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method:EPA 1664B
Oil and Grease ND mg/L 5.0 1 11/26/19 14:07
200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994
Copper ND ug/L 5.0 1 11/21/19 01:43 11/25/19 20:30 7440-50-8
Lead ND ug/L 5.0 1 11/21/19 01:43 11/25/19 20:30 7439-92-1
Zinc ND ug/L 10.0 1 11/21/19 01:43 11/25/19 20:30 7440-66-6
8260D MSV Low Level Analytical Method:EPA 8260D
Acetone ND ug/L 25.0 1 11/25/19 14:57 67-64-1
Benzene ND ug/L 1.0 1 11/25/19 14:57 71-43-2
Bromobenzene ND ug/L 1.0 1 11/25/19 14:57 108-86-1
Bromochloromethane ND ug/L 1.0 1 11/25/19 14:57 74-97-5
Bromodichloromethane ND ug/L 1.0 1 11/25/19 14:57 75-27-4
Bromoform ND ug/L 1.0 1 11/25/19 14:57 75-25-2
Bromomethane ND ug/L 2.0 1 11/25/19 14:57 74-83-9 v2
2-Butanone(MEK) ND ug/L 5.0 1 11/25/19 14:57 78-93-3
n-Butylbenzene ND ug/L 1.0 1 11/25/19 14:57 104-51-8
Carbon tetrachloride ND ug/L 1.0 1 11/25/19 14:57 56-23-5
i Chlorobenzene ND ug/L 1.0 1 11/25/19 14:57 108-90-7
Chloroethane ND ug/L 1.0 1 11/25/19 14:57 75-00-3
Chloroform ND ug/L 5.0 1 11/25/19 14:57 67-66-3
Chloromethane ND ug/L 1.0 1 11/25/19 14:57 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 11/25/19 14:57 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 11/25/19 14:57 106-43-4
Dibromochloromethane ND ug/L 1.0 1 11/25/19 14:57 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 1.0 1 11/25/19 14:57 106-93-4
Dibromomethane ND ug/L 1.0 1 11/25/19 14:57 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 11/25/19 14:57 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 11/25/19 14:57 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 11/25/19 14:57 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 11/25/19 14:57 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 11/25/19 14:57 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 11/25/19 14:57 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 11/25/19 14:57 75-35-4
cis-1,2-Dichloroethene ND ug/L . 1.0 1 11/25/19 14:57 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 11/25/19 14:57 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 11/25/19 14:57 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 11/25/19 14:57 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 11/25/19 14:57 594-20-7
1,1-Dichloropropene ND ug/L 1.0 1 11/25/19 14:57 563-58-6
cis-1,3-Dichloropropene ND ug/L 1.0 1 11/25/19 14:57 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 11/25/19 14:57 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 11/25/19 14:57 108-20-3
Ethylbenzene ND ug/L 1.0 1 11/25/19 14:57 100-41-4 '
Hexachloro-1,3-butadiene ND ug/L 1.0 1 11/25/19 14:57 87-68-3
2-Hexanone ND ug/L 5.0 1 11/25/19 14:57 591-78-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date: 11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 17
Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.patelabs.tom (704)875-9092
ANALYTICAL RESULTS
Project: Wells Fargo Monthly
Pace Project No.: 92454537
Sample: 001 Lab ID: 92454537001 Collected: 11/19/19 15:00 Received: 11/20/19 09:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Analytical Method:EPA 8260D
p-Isopropyltoluene ND ug/L 1.0 1 11/25/19 14:57 99-87-6
Methylene Chloride ND ug/L 5.0 1 11/25/19 14:57 75-09-2
4-Methyl-2-pentanone(MIBK) ND ug/L 5.0 1 11/25/19 14:57 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 11/25/19 14:57 1634-04-4
Naphthalene ND ug/L 1.0 1 11/25/19 14:57 91-20-3
Styrene ND ug/L 1.0 1 11/25/19 14:57 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/25/19 14:57 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/25/19 14:57 79-34-5
Tetrachloroethene ND ug/L 1.0 1 11/25/19 14:57 127-18-4
Toluene ND ug/L 1.0 1 11/25/19 14:57 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 11/25/19 14:57 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 11/25/19 14:57 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 11/25/19 14:57 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 11/25/19 14:57 79-00-5
Trichloroethene ND ug/L 1.0 1 11/25/19 14:57 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 11/25/19 14:57 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 11/25/19 14:57 96-18-4
Vinyl acetate ND ug/L 2.0 1 11/25/19 14:57 108-05-4
Vinyl chloride ND ug/L 1.0 1 11/25/19 14:57 75-01-4
Xylene(Total) ND ug/L 1.0 1 11/25/19 14:57 1330-20-7
m&p-Xylene ND ug/L 2.0 1 11/25/19 14:57 179601-23-1
o-Xylene ND ug/L 1.0 1 11/25/19 14:57 95-47-6
Surrogates
4-Bromofluorobenzene(S) 100 % 70-130 1 11/25/19 14:57 460-00-4
1,2-Dichloroethane-d4(S) 105 % 70-130 1 11/25/19 14:57 17060-07-0
Toluene-d8(S) 97 % 70-130 1 11/25/19 14:57 2037-26-5
2540D Total Suspended Solids Analytical Method:SM 2540D-2011
Total Suspended Solids ND mg/L 2.5 1 11/22/19 21:41
REPORT OF LABORATORY ANALYSIS
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Date: 11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 17
Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnaI ical Huntersville,NC 28078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: Wells Fargo Monthly
Pace Project No.: 92454537
QC Batch: 511846 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM,Oil and Grease
Associated Lab Samples: 92454537001
METHOD BLANK: 2745139 Matrix: Water
Associated Lab Samples: 92454537001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 11/26/19 14:03
LABORATORY CONTROL SAMPLE: 2745140
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 37.4 94 78-114
MATRIX SPIKE SAMPLE: 2745141
92454537001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L ND 40 37.1 92 78-114
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: Wells Fargo Monthly
Pace Project No.: 92454537
QC Batch: 510822 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92454537001
METHOD BLANK: 2740508 Matrix: Water
Associated Lab Samples: 92454537001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper ug/L ND 5.0 11/25/19 20:05
Lead ug/L ND 5.0 11/25/19 20:05
Zinc ug/L ND 10.0 11/25/19 20:05
LABORATORY CONTROL SAMPLE: 2740509
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Copper ug/L 500 470 94 85-115
Lead ug/L 500 467 93 85-115
Zinc ug/L 500 457 91 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2740510 2740511
MS MSD
92454191001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Copper ug/L 24.2 500 500 502 513 96 98 70-130 2
Lead ug/L ND 500 500 484 496 96 99 70-130 3
Zinc ug/L 151 500 500 624 645 94 99 70-130 3
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2740512 2740513
MS MSD
92454537001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Copper ug/L ND 500 500 476 481 95 96 70-130 1
Lead ug/L ND 500 500 481 482 96 96 70-130 0
Zinc ug/L ND 500 500 487 484 97 96 70-130 1 I
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date: 11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 17
Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite100
aceAnalytical
Huntersville,NC 28078078
www.pacelabs.eom (704)875-9092
QUALITY CONTROL DATA
Project: Wells Fargo Monthly
Pace Project No.: 92454537
QC Batch: 511601 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Associated Lab Samples: 92454537001
METHOD BLANK: 2744248 Matrix: Water
Associated Lab Samples: 92454537001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/25/19 11:28
1,1,1-Trichloroethane ug/L ND 1.0 11/25/19 11:28
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/25/19 11:28
1,1,2-Trichloroethane ug/L ND 1.0 11/25/19 11:28
1,1-Dichloroethane ug/L ND 1.0 11/25/19 11:28
1,1-Dichloroethene ug/L ND 1.0 11/25/19 11:28
1,1-Dichloropropene ug/L ND 1.0 11/25/19 11:28
1,2,3-Trichlorobenzene ug/L ND 1.0 11/25/19 11:28
1,2,3-Trichloropropane ug/L ND 1.0 11/25/19 11:28
1,2,4-Trichlorobenzene ug/L ND 1.0 11/25/19 11:28
1,2-Dibromoethane(EDB) ug/L ND 1.0 11/25/19 11:28
1,2-Dichlorobenzene ug/L ND 1.0 11/25/19 11:28
1,2-Dichloroethane ug/L ND 1.0 11/25/19 11:28
1,2-Dichloropropane ug/L ND 1.0 11/25/19 11:28
1,3-Dichlorobenzene ug/L ND 1.0 11/25/19 11:28
1,3-Dichloropropane ug/L ND 1.0 11/25/19 11:28
1,4-Dichlorobenzene ug/L ND 1.0 11/25/19 11:28
2,2-Dichloropropane ug/L ND 1.0 11/25/19 11:28
2-Butanone(MEK) ug/L ND 5.0 11/25/19 11:28
2-Chlorotoluene ug/L ND 1.0 11/25/19 11:28
2-Hexanone ug/L ND 5.0 11/25/19 11:28
4-Chlorotoluene ug/L ND 1.0 11/25/19 11:28
4-Methyl-2-pentanone(MIBK) ug/L ND 5.0 11/25/19 11:28
Acetone ug/L ND 25.0 11/25/19 11:28
Benzene ug/L ND 1.0 11/25/19 11:28
Bromobenzene ug/L ND 1.0 11/25/19 11:28
Bromochloromethane ug/L ND 1.0 11/25/19 11:28
Bromodichloromethane ug/L ND 1.0 11/25/19 11:28
Bromoform ug/L ND 1.0 11/25/19 11:28
Bromomethane ug/L ND 2.0 11/25/19 11:28 v2
Carbon tetrachloride ug/L ND 1.0 11/25/19 11:28
Chlorobenzene ug/L ND 1.0 11/25/19 11:28
Chloroethane ug/L ND 1.0 11/25/19 11:28
Chloroform ug/L ND 5.0 11/25/19 11:28
Chloromethane ug/L ND 1.0 11/25/19 11:28
cis-1,2-Dichloroethene ug/L ND 1.0 11/25/19 11:28
cis-1,3-Dichloropropene ug/L ND 1.0 11/25/19 11:28
Dibromochloromethane ug/L ND 1.0 11/25/19 11:28
Dibromomethane ug/L ND 1.0 11/25/19 11:28
Dichlorodifluoromethane ug/L ND 1.0 11/25/19 11:28
Diisopropyl ether ug/L ND 1.0 11/25/19 11:28
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date: 11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 17
Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
aceAnalytical
Huntersville,NC 28078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: Wells Fargo Monthly
Pace Project No.: 92454537
METHOD BLANK: 2744248 Matrix: Water
Associated Lab Samples: 92454537001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethylbenzene ug/L ND 1.0 11/25/19 11:28
Hexachloro 1,3 butadiene ug/L ND 1.0 11/25/19 11:28
m&p-Xylene ug/L ND 2.0 11/25/19 11:28
Methyl-tert-butyl ether ug/L ND 1.0 11/25/19 11:28
Methylene Chloride ug/L ND 5.0 11/25/19 11:28
n-Butylbenzene ug/L ND 1.0 11/25/19 11:28
Naphthalene ug/L ND 1.0 11/25/19 11:28
o-Xylene ug/L ND 1.0 11/25/19 11:28
p-Isopropyltoluene ug/L ND 1.0 11/25/19 11:28
Styrene ug/L ND 1.0 11/25/19 11:28
Tetrachloroethene ug/L ND 1.0 11/25/19 11:28
Toluene ug/L ND 1.0 11/25/19 11:28
trans-1,2-Dichioroethene ug/L ND 1.0 11/25/19 11:28
trans-1,3-Dichloropropene ug/L ND 1.0 11/25/19 11:28
Trichloroethene ug/L ND 1.0 11/25/19 11:28
Trichlorofluoromethane ug/L ND 1.0 11/25/19 11:28
Vinyl acetate ug/L ND 2.0 11/25/19 11:28
Vinyl chloride ug/L ND 1.0 11/25/19 11:28
Xylene(Total) ug/L ND 1.0 11/25/19 11:28
1,2-Dichloroethane-d4(S) % 103 70-130 11/25/19 11:28
4-Bromofluorobenzene(S) % 99 70-130 11/25/19 11:28
Toluene-d8(S) % 99 70-130 11/25/19 11:28
LABORATORY CONTROL SAMPLE: 2744249
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane ug/L 50 51.1 102 70-130
1,1,1-Trichloroethane ug/L 50 46.4 93 70-130
1,1,2,2-Tetrachloroethane ug/L 50 50.0 100 70-130
1,1,2-Trichloroethane ug/L 50 47.9 96 70-130
1,1-Dichloroethane ug/L 50 45.6 91 70-130
1,1-Dichloroethene ug/L 50 45.7 91 70-130
1,1-Dichloropropene ug/L 50 49.2 98 70-130
1,2,3-Trichlorobenzene ug/L 50 47.3 95 70-130
1,2,3-Trichloropropane ug/L 50 52.5 105 70-130
1,2,4-Trichlorobenzene ug/L 50 47.0 94 70-130
1,2-Dibromoethane(EDB) ug/L 50 51.3 103 70-130
1,2-Dichlorobenzene ug/L 50 47.6 95 70-130
1,2-Dichloroethane ug/L 50 44.2 88 70-130
1,2-Dichloropropane ug/L 50 47.1 94 70-130
1,3-Dichlorobenzene ug/L 50 47.2 94 70-130
1,3-Dichloropropane ug/L 50 50.4 101 70-131
1,4-Dichlorobenzene ug/L 50 46.7 93 70-130
2,2-Dichloropropane ug/L 50 47.6 95 69-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 17
Pace Analytical Services,LLC i
ace Analytical® 9800 Kincey Ave. Suite 78
Huntersville,NC 28078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: Wells Fargo Monthly
Pace Project No.: 92454537
LABORATORY CONTROL SAMPLE: 2744249
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
2-Butanone(MEK) ug/L 100 103 103 64-135
2-Chlorotoluene ug/L 50 48.0 96 70-130
2-Hexanone ug/L 100 113 113 66-135
4-Chlorotoluene ug/L 50 48.4 97 70-130
4-Methyl-2-pentanone(MIBK) ug/L 100 105 105 70-130
Acetone ug/L 100 107 107 61-157
Benzene ug/L 50 47.0 94 70-130
Bromobenzene ug/L 50 49.4 99 70-130
Bromochloromethane ug/L 50 47.2 94 70-130
Bromodichloromethane ug/L 50 48.1 96 70-130
Bromoform ug/L 50 51.3 103 70-130
Bromomethane ug/L 50 47.1 94 38-130 v3
Carbon tetrachloride ug/L 50 48.4 97 70-130
Chlorobenzene ug/L 50 47.2 94 70-130
Chloroethane ug/L 50 40.4 81 37-142
Chloroform ug/L 50 46.3 93 70-130
Chloromethane ug/L 50 40.3 81 48-130
cis-1,2-Dichloroethene ug/L 50 45.0 90 70-130
cis-1,3-Dichloropropene ug/L 50 51.0 102 70-130
Dibromochloromethane ug/L 50 50.9 102 70-130
Dibromomethane ug/L 50 47.6 95 70-130
Dichlorodifluoromethane ug/L 50 42.9 86 53-134
Diisopropyl ether ug/L 50 47.3 95 70-135
Ethylbenzene ug/L 50 47.8 96 70-130
Hexachloro-1,3-butadiene ug/L 50 46.6 93 68-132
m&p-Xylene ug/L 100 95.3 95 70-130
Methyl-tert-butyl ether ug/L 50 48.1 96 70-130
Methylene Chloride ug/L 50 43.0 86 67-132
n-Butylbenzene ug/L 50 46.2 92 70-132
Naphthalene ug/L 50 49.8 100 70-130
o-Xylene ug/L 50 48.9 98 70-131
p-Isopropyltoluene ug/L 50 47.0 94 70-130
ug/L Styrene u /L 50 49.8 100 70-130
Y
Tetrachloroethene ug/L 50 49.3 99 69-130
Toluene ug/L 50 45.7 91 70-130
trans-1,2-Dichloroethene ug/L 50 45.4 91 70-130
trans-1,3-Dichloropropene ug/L 50 49.9 100 70-130
Trichloroethene ug/L 50 46.9 94 70-130
Trichlorofluoromethane ug/L 50 44.1 88 63-130
Vinyl acetate ug/L 100 97.8 98 55-143
Vinyl chloride ug/L 50 48.0 96 70-131
Xylene(Total) ug/L 150 144 96 70-130
1,2-Dichloroethane-d4(S) % 95 70-130
4-Bromofluorobenzene(S) % 99 70-130
Toluene-d8(S) % 98 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
' REPORT OF LABORATORY ANALYSIS
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Date: 11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 17
Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.eom (704)875-9092
QUALITY CONTROL DATA
Project: Wells Fargo Monthly
Pace Project No.: 92454537
MATRIX SPIKE SAMPLE: 2744251
92454676008 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane ug/L ND 20 22.7 113 73-134
1,1,1-Trichloroethane ug/L ND 20 24.6 123 82-143
1,1,2,2-Tetrachloroethane ug/L ND 20 23.7 119 70-136
1,1,2-Trichloroethane ug/L ND 20 23.2 116 70-135
1,1-Dichloroethane ug/L ND 20 24.2 121 70-139
1,1-Dichloroethene ug/L 0.52J 20 25.2 123 70-154
1,1-Dichloropropene ug/L ND 20 26.2 131 70-149
1,2,3-Trichlorobenzene ug/L ND 20 23.5 118 70-135
1,2,3-Trichloropropane ug/L ND 20 23.9 119 71-137
1,2,4-Trichlorobenzene ug/L ND 20 22.7 114 73-140
1,2-Dibromoethane(EDB) ug/L ND 20 23.8 119 70-137
1,2-Dichlorobenzene ug/L ND 20 21.2 106 70-133
1,2-Dichloroethane ug/L ND 20 23.0 115 70-137
1,2-Dichloropropane ug/L ND 20 23.4 117 70-140
1,3-Dichlorobenzene ug/L ND 20 21.0 105 70-135
1,3-Dichloropropane ug/L ND 20 24.1 120 70-143
1,4-Dichlorobenzene ug/L ND 20 20.9 104 70-133
2,2-Dichloropropane ug/L ND 20 25.2 126 61-148
2-Butanone(MEK) ug/L ND 40 49.7 124 60-139
2-Chlorotoluene ug/L ND 20 21.4 107 70-144
2-Hexanone ug/L ND 40 56.4 141 65-138 M1
4-Chlorotoluene ug/L ND 20 21.8 109 70-137
4-Methyl-2-pentanone(MIBK) ug/L ND 40 51.4 128 65-135
Acetone ug/L ND 40 52.4 131 60-148
Benzene ug/L ND 20 23.9 120 70-151
Bromobenzene ug/L ND 20 21.6 108 70-136
Bromochloromethane ug/L ND 20 24.3 121 70-141
Bromodichloromethane ug/L ND 20 23.5 118 70-138
Bromoform ug/L ND 20 22.3 111 63-130
Bromomethane ug/L ND 20 28.8 144 15-152
Carbon tetrachloride ug/L ND 20 24.9 125 70-143
Chlorobenzene ug/L ND 20 21.7 109 70-138
Chloroethane ug/L ND 20 22.7 113 52-163
Chloroform ug/L ND 20 24.0 120 70-139
Chloromethane ug/L ND 20 22.2 111 41-139
cis-1,2-Dichloroethene ug/L ND 20 23.8 119 70-141
cis-1,3-Dichloropropene ug/L ND 20 23.9 120 70-137
Dibromochloromethane ug/L ND 20 22.9 115 70-134
Dibromomethane ug/L ND 20 22.9 115 70-138
Dichlorodifluoromethane ug/L ND 20 23.2 116 47-155
Diisopropyl ether ug/L ND 20 23.8 119 63-144
Ethylbenzene ug/L ND 20 22.3 111 66-153
Hexachloro-1,3-butadiene ug/L ND 20 27.1 136 65-149
m&p-Xylene ug/L ND 40 44.6 111 69-152
Methyl-tert-butyl ether ug/L ND 20 24.0 120 54-156
Methylene Chloride ug/L ND 20 23.2 116 42-159
n-Butylbenzene ug/L ND 20 23.2 116 70-139
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 17
Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.com (704)875-9092
i
QUALITY CONTROL DATA
Project: Wells Fargo Monthly
Pace Project No.: 92454537
MATRIX SPIKE SAMPLE: 2744251
92454676008 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Naphthalene ug/L
ND 20 22.4 112 61-148
o-Xylene ug/L ND 20 21.8 109 70-148
p-Isopropyltoluene ug/L ND 20 22.1 111 70-146
Styrene ug/L ND 20 22.4 112 70-135
Tetrachloroethene ug/L 0.95J 20 23.1 111 59-143
Toluene ug/L ND 20 22.3 112 59-148
trans-1,2-Dichloroethene ug/L ND 20 24.6 123 70-146
trans-1,3-Dichloropropene ug/L ND 20 24.0 120 70-135
Trichloroethene ug/L ND 20 23.2 116 70-147
Trichlorofluoromethane ug/L ND 20 23.9 120 70-148
Vinyl acetate ug/L ND 40 50.4 126 49-151
Vinyl chloride ug/L ND 20 26.6 133 70-156
Xylene(Total) ug/L ND 60 66.4 111 63-158
1,2-Dichloroethane-d4(S) % 102 70-130
4-Bromofluorobenzene(S) % 101 70-130
Toluene-d8(S) % 99 70-130
SAMPLE DUPLICATE: 2744250
92454537001 Dup
Parameter Units Result Result RPD Qualifiers
1,1,1,2-Tetrachloroethane ug/L ND ND
1,1,1-Trichloroethane ug/L ND ND
1,1,2,2-Tetrachloroethane ug/L ND ND
1,1,2-Trichloroethane ug/L ND ND
1,1-Dichloroethane ug/L ND ND
1,1-Dichloroethene ug/L ND ND
1,1-Dichloropropene ug/L ND ND
1,2,3-Trichlorobenzene ug/L ND ND
1,2,3-Trichloropropane ug/L ND ND
1,2,4-Trichlorobenzene ug/L ND ND
1,2-Dibromoethane(EDB) ug/L ND ND
1,2-Dichlorobenzene ug/L ND ND
1,2-Dichloroethane ug/L ND ND
1,2-Dichloropropane ug/L ND ND
1,3-Dichlorobenzene ug/L ND ND
1,3-Dichloropropane ug/L ND ND
1,4-Dichlorobenzene ug/L ND ND
2,2-Dichloropropane ug/L ND ND
2-Butanone(MEK) ug/L ND ND I
2-Chlorotoluene ug/L ND ND
2-Hexanone ug/L ND ND
4-Chlorotoluene ug/L ND ND
4-Methyl-2-pentanone(MIBK) ug/L ND ND
Acetone ug/L ND ND
Benzene ug/L ND ND
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 17
Pace Analytical Services,LLC
eAnalytical iv9800Hulntersvlle,NC'
te 100
ac 280788
vrww.paeelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: Wells Fargo Monthly
Pace Project No.: 92454537
SAMPLE DUPLICATE: 2744250
92454537001 Dup
Parameter Units Result Result RPD Qualifiers
Bromobenzene ug/L ND ND
Bromochloromethane ug/L ND ND
Bromodichloromethane ug/L ND ND
Bromoform ug/L ND ND
Bromomethane ug/L ND ND
Carbon tetrachloride ug/L ND ND
Chlorobenzene ug/L ND ND
Chloroethane ug/L ND ND
Chloroform ug/L ND ND
Chioromethane ug/L ND ND
cis-1,2-Dichloroethene ug/L ND ND
cis-1,3-Dichloropropene ug/L ND ND
Dibromochloromethane ug/L ND ND
Dibromomethane ug/L ND ND
Dichlorodifluoromethane ug/L ND ND
Diisopropyl ether ug/L ND ND
Ethylbenzene ug/L ND ND
Hexachloro-1,3-butadiene ug/L ND ND
m&p-Xylene ug/L ND ND
Methyl-tert-butyl ether ug/L ND ND
Methylene Chloride ug/L ND ND
n-Butylbenzene ug/L ND ND
Naphthalene ug/L ND ND '
o-Xylene ug/L ND ND
p-lsopropyltoluene ug/L ND ND
Styrene ug/L ND ND
Tetrachloroethene ug/L ND ND
' Toluene ug/L ND ND
trans-1,2-Dichloroethene ug/L ND ND
trans-1,3-Dichloropropene ug/L ND ND
Trichloroethene ug/L ND ND
Trichlorofluoromethane ug/L ND ND
Vinyl acetate ug/L ND ND
Vinyl chloride ug/L ND ND
Xylene(Total) ug/L ND ND
1,2-Dichloroethane-d4(S) % 105 109
4-Bromofluorobenzene(S) % 100 98
Toluene-d8(S) % 97 99
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 17
Pace Analytical Services,LLC
Kincey Ave.
te 100
aceAnalytical 9800Hun ersv Ile,NC128078
www.pacelabs.cam (704)875-9092
QUALITY CONTROL DATA
Project: Wells Fargo Monthly
Pace Project No.: 92454537
QC Batch: 511342 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92454537001
METHOD BLANK: 2743220 Matrix: Water
Associated Lab Samples: 92454537001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 11/22/19 21:34
LABORATORY CONTROL SAMPLE: 2743221
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 260 104 90-110
SAMPLE DUPLICATE: 2743222
92454525001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 846 792 7
SAMPLE DUPLICATE: 2743223
92454667001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 948 1250 28 D6
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacNaba.com (704)875-9092
QUALIFIERS
Project: Wells Fargo Monthly
Pace Project No.: 92454537
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
LABORATORIES
PAST-A Pace Analytical Services-Asheville
PAST-C Pace Analytical Services-Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
v2 The continuing calibration verification was below the method acceptance limit.The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit.Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date: 11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 17
Pace Analytical Services,LLC
aceAnalytical 9800 Kinsey Ave. Suite100
Huntersville,NC 28078078
www.pacalaba.com (704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Wells Fargo Monthly
Pace Project No.: 92454537
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92454537001 001 EPA 1664B 511846
92454537001 001 EPA 200.7 Rev 4.4 1994 510822 EPA 200.7 Rev 4.4 1994 510849
92454537001 001 EPA 8260D 511601
92454537001 001 SM 2540D-2011 511342
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:11/27/2019 01:49 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 17
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�� � Quote#: DW Location Code: Sufficient Volume N NA
samples Received on Ice N NA
Coll ted By si nature): Turnaround Date Required: Immediately Packed on Ice: VOA - 8eadspace Acceptable Y N NA
(,?.).Yes [ ]No USDA Regulated Soils N
Samples in Holding Time afIs N
Sample Disposal: Rush: Field Filtered(if applicable): Residual Chlorine Present Y N A
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"Matrix Codes(Insert in Matrix box below):Drinking Water(DW),Ground Water(GW),Wastewater(WW), Lead Acetate Strips: _,
Product(P),Soil/Solid(SL),Oil(OL),Wipe(WP),Air(AR),Tissue(TS),Bioassay(B),Vapor(V),Other(OT) LAB USE ONLY:
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(1- Cooler 1 Temp Upon Receipt:04 oC
Radchem sample(s)screened(<500 cpm): Y N NA Samples received via: Cooler 1 Therm Corr.Factor: 0 oC
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