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NCG140216_MONITORING INFO_20190125
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. Iv U& yDal DOC TYPE ❑HISTORICAL FILE tZ MONITORING REPORTS DOC DATE ❑ r) Le) O f a 5 YYYYMMDD Ze Environmental Quality Stormwrater Discharge Outfall (SDO) Qualitative ]Monitoring Report Forguidance on filling out this form, please visit ht s://de .nc. ov/about/divisions/ener -mineral-land- resources/ener -mineral-land- ermits/stormwater- ermits/n des-industrial-sw#tab4 Permit No.: NICI_I_I_I_I_rrI_I_I or Certificate of Coverage No.: N/C/G/ / 1 y/a Facility Name: 31 d a 151, County: W a r Phone No. ^ q I q 5,s' 4 as ? Inspector: OJ Date of Inspection: -zs-—l8 Time of Inspection: Q,v( REGEIv 1-l-' ,BAN t 5 2019 Total Event Precipitation (inches): .so z CENTRAL1=1 C,\NR SECT10i 1 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: JJ Outfall No. _ I Structure (pipe, ditch, etc.): c3+ ��- Receiving Stream: Describe the industrial activities that occur within the Loutfall drainage area: C0 vt C" G!� IL- r r 9 A ,1 c.T 1'111\ Pagel of 2 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 4eo w 4 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ty e N c 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 C2) 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 Q 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: (J 2 3 4 5 7. Is there any foam in the stormwater discharge? O Yes ® No. 8. Is there an oil sheen in the stormwater discharge? OYes ® No. 9. Is there evidence of erosion or deposition at the outfall? o Yes 4D No. to. Other Obvious Indicators of Stormwater Pollution: List and describe N o N r- Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE NOr. NCG14 d A f G 4 FACILITY NAME: C . �. a) v d PERSON COLLECTING SAMPLES IP. a f +t CERTIFIED LABORATORY A., lab # 5 i Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: zo I SAMPLING PERIOD: ❑ July -December January -June COUNTY Q., (( c� PHONE NO. ( 4tI ) SS`f - ADD TO LISTSERVE? [-]YES [eft EMAIL: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trout ❑Other Outfall No. Date Sample Collected (mo/dd/yr OR No FLOW)1 pH (Standard Units) TSS (mg/L) Event Duration (minutes) Total Rainfall° (in) In Tier 2 Monthly Monitoring? (y/n) # of Months inTier 2 Sampling - 6-92 100 ' - - - i 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above- 2 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit, Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/I. For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011.60/30/2015 Last Revised 7/13/11 Page 1 of Z Date of last pH meter calibration: / 11 Z- /-Z 19 ({t 1 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outtall No. Date Sample Collected 1 (mo/dd/yr) pH (Standard Units) TPH using method 1664A SGT-HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total Rainfall ° (in) New Motor Oil Usage (gal/month) In Tier 2 Monthly Monitoring? (v/n) # of Months in Tier 2 Sampling2 6-9 15 1002,1 - - - U I HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCE5 AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO HAVE YOU CONTACTED THE REGION? YES ❑ NO [►�� REGIONAL OFFICE CONTACT NAME: Mail Oriainal and one coov of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample for at end of monitorigperiod in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED, "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." e � % 2_ zolK (Signature of Permittee) (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 r TABLE 9.2 ANALYTICAL MONITORING REQUIREMENTS -PROCESS WASTEWATER READY MIXED CONCRETE COMPANY- PLANT # DISCHARGE UNITS- EFFLUENT SAMPLE SAMPLING CHARACTERISTIC LIMITATIONS LOCATION SCHEDULE pH Standard 6.0 — 9.0' Each Outfal12 . Quarterly Total Suspended Solids (TSS) mg/L 30 mg/L3 Each Outfa112 Quarterly Settleable Solids mUL 5 mUL Each Outfail2 Quarterly Total Petroleum Hydrocarbons°, mg/L 15 mg/L Each OutfaJI2 Quarterly Event Duration Minutes Not applicable Each Outfa112 Quarterly Flows Gallons/Day Not applicable Each Outfal12 Quarterly New Motor Oil Usage Gallons/ Month Not applicable Not applicable Quarterly Total Volume of Wastewater 'Discharged (HQW) Not applicable 50% of summer 7Q10 Flow Not Applicable Quarterly Notes: 1. pH range for saltwaters is 6.8 — 8.5. 2. Samples shall be collected at each process wastewater outfall during a discharge event. 3. TSS effluent limitation HQW is 20 mg/L and 10 mg/L for Trout or PNA waters. 4. Only required for sites where vehicle maintenance activities occur and process wastewater commingles with stormwater_ 5. Flow may be measured continuously or calculated. 6. See 15A NCAC 02B .0224 and general permit for explanation. 7. All samples must be grab samples. Grab samples shall be collected within the first 30 minutes of discharge from a process wastewater outfall. 8. If no discharge occurs during a sampling period, record "No Flow" or "No Discharge" within 30-days of the end of the sampling period and file with SPPP. 9. Commingled discharges must be collected during a measurable storm event. A measurable storm event is an event that results in an actual discharge from the permitted site outfails. The previous measurable storm event must have been at least 72 hours prior. 10. For each sampled measurable storm event the total precipitation must be recorded using an on -site rain gauge. 11. The permittee shall complete the analytical samplings in accordance with the schedule specified above, unless adverse weather conditions prevent sample collection. Inability to sample due to adverse weather conditions must.be documented in the SPPP and reported on the appropriate DMR form (Appendix A). 12. For commingled discharges, a minimum of 60 days must separate each monitoring event unless monthly monitoring has been instituted under a Tier Two response 13. The permittee shall compare monitoring results to the above -referenced effluent limitations for each discharge characteristic. Exceedances of effluent limitations will result in a violation of permit conditions and may be subject to enforcement. 14. Failure to monitor process wastewater quarterly per permit terms immediately institutes monthly monitoring for all parameters. After six months of monthly monitoring, the permitee may make a request in writing to the Division of Water Quality to return to a quarterly monitoring schedule. (�IaneAnafytical" WW..peoelab$.=n April 30, 2018 Jay Watkins Ready Mix Concrete 3610 Bush Street Raleigh, NC 27609 RE: Project: Plant 31 Capital Blvd Pace Project No.: 92382337 Dear Jay Watkins: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 400 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on April 25, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNUNELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 10 aceAnalytical 410 W*wPacelabs.carn Project: Plant 31 Capital Blvd Pace Project No.: 92382337 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shah not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 10 aceAnalytical wwwpecelabs.wm SAMPLE ANALYTE COUNT Project: Plant 31 Capital Blvd Pace Project No.: 92382337 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92382337001 Outfall #1 Plant 31 SM 2540D RAY 1 PASI-E REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 10 Pace Analytical Services, LLC aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NG 28078 wwwpacelabs.wm (704)875-9092 ANALYTICAL RESULTS Project: Plant 31 Capital Blvd Pace Project No.: 92382337 Sample: Outfall #1 Plant 31 Lab lD: 92382337001 Collected: 04/25/18 09:05 Received: 04/25/18 16:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 3.6 mglL 2,5 1 - 04/27/18 11:32 Date: 04/30/2018 02:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 10 aceAnalytical www.p"iabs.com QUALITY CONTROL DATA Project: Plant 31 Capital Blvd Pace Project No.: 92382337 QC Batch: 408249 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92382337001 METHOD BLANK: 2265174 Matrix: Water Associated Lab Samples: 92382337001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL NO 2.5 04/27/16 11:28 LABORATORY CONTROL SAMPLE: 2265175 Spike Parameter Units Conc. Total Suspended Solids mg1L 250 SAMPLE DUPLICATE: 2265176 92382423002 Parameter Units Result Total Suspended Solids mg/L 26.4 LCS LCS Result % Rec . 228 91 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875.9092 % Rec Limits Qualifiers 90-110 Dup Result RPD Qualifiers 31.4 17 D6 SAMPLE DUPLICATE: 2265177 92382426001 Dup Parameter Units Result Result Total Suspended Solids mglL 155 160 RPD Qualifiers 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/30/2018 02:13 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 10 aeeAnalXical wwwpm;Wabs.eorrr QUALIFIERS Project: Plant 31 Capital Blvd Pace Project No.: 92382337 DEFINITIONS Pace Analytical Services, LLG 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit, TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. POL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenyl a mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC institute. LABORATORIES PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04/30/2018 02:13 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 10 5ac e A na ly tica / WWW..pamabs.mm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Plant 31 Capital Blvd Pace Project No.: 92382337 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 26078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92382337001 Outfall #1 Plant 31 SM 25401) 408249 0 Date: 04/30/2018 02:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 10 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Recelpt(SCUR) Page 1 of 2 J +/ Document No.: Issuing Authority. F-CAR-CS-033-Rev.06 Pace Carolinas Quallty Office Laboratory receiving samples: Asheville ❑ Edeno Greenwood ❑ Huntersville ❑ Raleig Mechanicsville❑ Client Name: t P q 9232337 Project Courier: ❑Fed Ex Ouk ❑USPs Client ❑ Commercial ❑Pace []Other: Y'9238233-7 _ Custody Seal Present? ❑Yesseals Intact? ❑Yes . P t/���,� Date/Initials Person Examining Content-. < Packing Material: ❑Bubble Wrap ❑Bubble Bags ef7fNone ❑ Other Biological Tissue F en? Thermome er: �r r'�' ❑Yes ❑No N/A iR Gun ID: r�- TYPe once: t"!et ❑Blue ❑None Cooler Temp CC): 2— b Correction Factor: Add ubtrac ('C) . Temp should be above freezing to 6'C Cooler Temp Corrected {'C): _ ❑Samples out oftemp criteria. Samples on Ice, cooling process has begun USDA Regulated soil ?I/A, water sample) Did samples orlgi a in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internati , I�YPt rUn inrludlne Hawaii ar.A Puertn Aicnh l—IYPs n Comments/Discrepancy: Chain of Custody Present? es on. ON/, 1. Samples Arrived within I-Inld Time? s ONO N/A 2. Short Hold Time Analysis (<72 hr.)? OYes rX /A 3. Rush Turn Around Time Requested? Dyes o N/A q. SufflCient Volume? es Na []N/A S. CorrectContalners Used? -Pace Contain ers Used? Y es No ©N/A No ❑Y/A 6. Contalners Intact? Yer No ❑N/A- 7. Dissolved analysis: Samples Field Filtered? ❑Y Na 24., 8. Sample Labels Match CDC? -Includes Oate/Time/ID/Analysis Matrbc X. []NO ❑N/A 9. Heads pace in VOA Vials (>5-6mm)? DYes ONO N/A 10. Trip Blank Present? Trip Blank Custod Seals Present? ❑Y. Yes ONO No N/A N/A COMMENT5/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTWICATION/RESOLUTION Person contacted: DateMme: Field Data Required? ❑Yes ❑No Project Manager SCURF Review: V 1 7 Date: t j U'5--o Project Manager SRF Review: (1 �i.� i Date: t',' c•}?-, '�E Ni Page 8 of 10 Document Name: Document Revised: February 7, 2018 $C8fiF12�,,tyCB�, Sample Condition Upon Recelpt(SCUR) Page f of 2 1" Document No.: Issuing Authority: F-CAR-CS•033-Rev,06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorinatlon is verified and within the acceptance range for preservation samples. Escceptions: VOA, Coliform, TOC, Oil and Grease, DRO/9015 (water) DOC, LLHg "Bottom half of box is to list number of bottle Project #;WO ";'."9238-23.3_._+- ISue Dale: 05109/18" PM: ,AMB_; 'CLIENia'-_ 92=Ready Ed b Z u c rs a E ae m —'I v v c m a E 9 dm m ayy 2 N c T a E > n m a n 1 7 ti to n a n a y E dr ca ry n Z UU• m n E C) Z m m eZf m Zas .! a E n ry a m ti A a U a E u CL m a C� N o E v 7*+ Y z m Z n E iu ¢ ;� a f: v i ^ 4 d 2 ° j Oi of an 7 m 4 N v c O = E a V E ¢ c a7 a - V x z J p n J. M t9 m7 a Z -Ur• 4 O > E 0 a d _ d Z a A d O a7 ] 2 C ¢ D E 0 Lb = v Q O > E a C) Y o r N Oa 4 7 Z d A y Y i d 2 y N f h w i F m A E of �+ $ z m n J o a4 m x O Z n E 4 E 0 l7 4 ? M c u N E f a E a 0 1 2 3 -NN\N I N 1111 5 N- 6 7 I I B 9 10 11 I i 12 f pH Adjustment Log for Preserved Samples Sample ID Type of Preservative FiH upon reccfpt Date preservation adjusted Time preservation adjusted Amount of Preservative added F Lot 9 Nate: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy at this form will be sent to the North Carolina DEHNR Cer0fication Office {f.e. out of hold, incorrect preservative, out of temp, incorrect containers. Page 9 of 10 0 n 0 CHAIN -OF -CUSTODY I Analytical Request Document d, —u The Chain-ot-CusIony is a LEGAL DOCUMENT, All relevant fields must be campleled accurately. d Suction A $"Lion B Section C Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit ht_ps://dea.nc.yoov/about/divisions/energy-mineral-land- resources/energy-mi neral-land-permits/stormwater-permits/npdes-industrial-sw#tab-4 Permit No.: NICI_I_I_l 1_I—I_I or Certificate of Coverage No.: N/C/G/ I yl 0l? Facility Name: Cad Q v v d 18 �- _ County: (, i o4 k e_- - r --Phone No. q l q -53q - A4 g j Inspector: Date of Inspection: 16 fill I -L o t Q _ Time of Inspection: 1; o b PA4 R EC E I V E L) �r JAN 2 5 2019 Total Event Precipitation (inches): CENTRAL. FILLS Ersl'J aECTIO" I All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. i Receiving Stream: Structure (pipe, ditch, etc.): CY , `i-c l Describe the industrial activities that occur within the outfall drainage area: `26a -^ T Pro dAJf-tA - Page] of 2 0 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: k 1-$L'if' ar.sw-/t 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): o tj-e- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 V 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 V 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? Q Yes 4 No. 8. Is there an oil sheen in the stormwater discharge? QYes 0 No. 9. Is there evidence of erosion or deposition at the outfall? O Yes ! No. to. Other Obvious Indicators of Stormwater Pollution: List and describe /V o Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE NO. NCG14 O A I f'o FACILITY NAME: 1-i ei PERSON COLLECTING SAMPLES V vti . I CERTIFIED LABORATORY Lab # _ 7�( Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: Z0 1 9 SAMPLING PERIOD: Erjuiy-December ❑ January -June COUNTY WlIt- e- PHONE NO. { ) ADD TO LISTSERVE? ❑YES []NO EMAIL: DISCHARGING TO CLASS. []SA ❑HQW ❑PNA []Trout [}Other Outfall Na. Date Sample Collected (mo/dd/yr OR NO FLOW)1 pH (Standard Units) TSS (mg/L) Event Duration (minutes) Total 4 Rainfall (in) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier 2 Sampling' 5-92 100 ' - - - - zei8 , g �f. 40 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. 1 If a value is In excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit, Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 T55 benchmark values are 100 mg/l, except when discharging to ORW, HQW, Trout, and PNA waters where they are SO mg/I. 4 For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Date of last pH meter calibration: I,� Z�ZC i Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gat of new motor oil/month — averaged over a calendar year. Outfall No. Date Sample Collected (mo/dd/yr)' pH (Standard Units) TPH using method 1664A 5GT--HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total a Rainfall (in) New Motor ail Usage (gal/month) In Tier 2 Monthly Monitoring? Mo (y/n) k of Months in Tier Z Sampling z 6-9 1s 100 ' - - a i HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENC S AT ANYONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO [� HAVE YOU CONTACTED THE REGION? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail Orieinal and one copy of this OMR (includine all "No flow" & "No Discharge" reports) within 30 days of recut of sample (or at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete, am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 TABLE 9.2 ANALYTICAL MONITORING REQUIREMENTS -PROCESS WASTEWATER READY MIXED CONCRETE COMPANY - PLANT # DISCHARGE EFFLUENT SAMPLE SAMPLING CHARACTERISTIC UNITS LIMITATIONS LOCATION SCHEDULE pH Standard 6.0 — 9.0' Each Outfa112 Quarterly Total Suspended Solids (TSS) mg/L 30 mg/L3 Each Outfa112 Quarterly Settleable Solids mUL 5 mL/L Each Outfai12 Quarterly Total Petroleum Hydrocarbons4 mg/L 15 mg/L Each Outfal12 Quarterly Event Duration Minutes Not applicable Each Outfa112 Quarterly Flows Gallons/Day Not applicable Each Outfa112 Quarterly New Motor Oil Usage Gallons/ Month Not applicable Not applicable Quarterly Total Volume of Wastewater Not applicable 50% of summer Not Applicable Quarterly Discharged (HOW) 7010 Flow Notes: 1. pH range for saitwaters is 6.8 — 8.5. 2. Samples shall be collected at each process wastewater outfall during a discharge event. 3. TSS effluent limitation HQW is 20 mg/L and 10 mg/L for Trout or PNA waters. 4. Only required for sites where vehicle maintenance activities occur and process wastewater commingles with stormwater. 5. Flow may be measured continuously or calculated. 6. See 15A NCAC 02B .0224 and general permit for explanation. 7. All samples must be grab samples. Grab samples shall be collected within the first 30 minutes of discharge from a process wastewater outfall. 8. If no discharge occurs during a sampling period, record "No Flow" or "No Discharge" within 30-days of the end of the sampling period and file with SPPP. 9. Commingled discharges must be collected during a measurable storm event. A measurable storm event is an event that results in an actual discharge from the permitted site outfalls. The previous measurable storm event must have been at least 72 hours prior. 10. For each sampled measurable storm event the total precipitation must be recorded using an on -site rain gauge. 11. The permittee shall complete the analytical samplings in accordance with the schedule specified above, unless adverse weather conditions prevent sample collection. Inability to sample due to adverse weather conditions must be documented in the SPPP and reported on the appropriate DMR form (Appendix A). 12. For commingled discharges, a minimum of 60 days must separate each monitoring event unless monthly monitoring has been instituted under a Tier Two response 13. The permittee shall compare monitoring results to the above -referenced effluent limitations for each discharge characteristic. Exceedances of effluent limitations will result in a violation of permit conditions and may be subject to enforcement. 14. Failure to monitor process wastewater quarterly per permit terms immediately institutes monthly monitoring for all parameters. After six months of monthly monitoring, the permitee may make a request in writing to the Division of Water Quality to return to a quarterly monitoring schedule. aceAnalytical www.pacelabs.com 9800 Kinsey Ave. Suite 100 Nuntersville, NC 28078 (704)875-9092 October 19, 2018 Jay Watkins Ready Mix Concrete 3610 Bush Street Raleigh, NC 27609 RE: Project: Capital Blvd Plant 31 Pace Project No.: 92403358 Dear Jay Watkins: Enclosed are the analytical results for sample(s) received by the laboratory on October 12, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, 0 Q0— q1') , +UlI Angela Baioni angela.baioni@pacelabs.com (704)875-9092 i Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 10 1,,'AlGeAnalytical 9800 Kincey Ave. Suite 100 Huntersville, r 28078 wmv.pacelabs.cam (704)875.9092 CERTIFICATIONS Project: Capital Blvd Plant 31 Pace Project No.: 92403358 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analyticai Services, LLC, Page 2 of 10 /7P`a1ceAna1XicaJ www.pamlabs.cnm 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Capital Blvd Plant 31 Pace Project No.: 92403358 Analyses Lab ID Sample 10 Method Analysts Reported Laboratory 92403358001 Plant3l Capital Blvd Outfall 1 SM 254OD-2011 SOB 1 PASt-E REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 10 7.,Palcce Analytical � ~rwrw.pacelabs.cam 9800 Kincey Ave. Suite'i00 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Capital Blvd Plant 31 Pace Project No.: 92403358 Sample: Plant3l Capital Blvd Lab ID: 92403358001 Callected: 10/11/18 13:00 Received: 10/12/18 16:06 Matrix: Water Outfall 1 Parameters Results Units Report Limit ' DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 4.6 mg/L 2.5 1 10/15/18 13:27 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 08:43 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 10 �lRalceAnalytical ,yvw� pscelebs. can 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Capital Blvd Plant 31 Pace Project No.: 92403358 QC Batch: 436237 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540E) Total Suspended Solids Associated Lab Samples: 92403358001 METHOD BLANK: 2400381 Matrix: Water Associated Lab Samples: 92403358001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL NO 2.5 10/15/18 13:15 LABORATORY CONTROL SAMPLE: 2400382 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 242 97 90-110 SAMPLE DUPLICATE: 2400383 92403352001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 5.6 6.7 18 D6 SAMPLE DUPLICATE: 2400384 92403353001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L ND NO Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 08.43 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 10 117ceAnalytfcal 9800 Kincey Ave. Suite 100 kuntersville, NC 28078 wm+:Paceldbs.tcvrt i (704)873-9092 QUALIFIERS Project: Capital Blvd Plant 31 Pace Project No.: 92403358 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/19/2018 08:43 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 10 /'PaceAnalytical www,pacelabs.c= i 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project; Capital Blvd Plant 31 Pace Project No.: 92403358 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92403358001 Plant3l Capital Blvd Clutfall 1 SM 254OD-2011 436237 REPORT OF LABORATORY ANALYSIS Analytical Batch This report shall not be reproduced, except in full. Date: 10/19/2018 08:43 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 10 Uucurllt:nt Name: WC11111rr.t Rovlw j; February 7, :v'1B Sample Cwldidan Upon Aaceipt(SCuft) ' _ Page 1 of 2 keAnal�Cat^ Jucurneni No,: —7 �F Issiling Authority: CAR CS 033-Aev,O& Pace CaroVilas Quality off;a: Laboratory receiving samples: Asheville Edeno Greenwood ❑ iluntersville lwloi!1l� j (v!eEhJrIiCSv(Ile(J . = i iY;r~Yrllf�r ' Client N. iW 92403353 ks:• .: �;a: Courler: �F'd Ex ❑UPS ❑USPS jClicnt �� III II I� �I ❑Commercial ❑Pace ❑other:_ L 92403358 Custody Seal Present? ❑ A. silo Seats intact? ❑yr:5 Iy �/� 0 _ � � _f d]1CItI1111J1s PdrSJn Ex �Inll+iug Cu,itents: / Qf���/� FiJ Packing Material: ❑Bubble Wrap ❑Bubble flags Otllone ❑ Other Blulorical TissutFroten? Thcrmom e : i7 un l D: / _ ❑Yes ❑Tin �f j ltl d 0.� Type ur Ice: NleE ❑W- QNol+e Cooler Teinp ('C): a-- Carrectiors Facto ,9 Adt ubtrac: j`CJ d _ 1) Temp should be aLcvL: freez;n;; to G`C Cooler Temp Corrected ('Cl: i. _ [ISa+aslls act c1i :a ou 1:1: szia. S;.rl:::!es ,+i_, i.::ilfg pre:cs ^as bLu.o USDA Regulated Soil (Ft NIA, watar sample) Did samples oriq` ate in a g arandrl, tone Within the Unhed St_tes: CA, NY, or SC icheck main)? old saalples t:04ir:aw iron) a fureign source {inwmm:nn lly�, Myes r7CiYa usc!udiue Itawail and Paerta Wcol? nyes r1 a ------- _— _ Comments/Discrep-ancy: Chain of Custody Present? Samples Arrived within Hold Tlme? �s— El NO CIN/A 2. — - '- Short Hold Time Analysis (472 hr.)? Rush Turn Ae round Time Requested? Yes ;o �N/n ❑yet fl jJiih� 4, -- --- --- - - S+rfficicrt y'o}unt_? - _ es nrlo ttJa S. - corru-t Camaeflel S USE;i? YYY , 1 u, -Pace C01113ifle.rs Ui,eLl F©flo 7. _ -- Container Intact? _ , ��]4cs :Jo - LIMA Dissoivcd analysis: Samples Field filtered? Sample Labels Match COC? -tyres C14u ©N/a 9, i -Includes pate/Tltne/]D/Analysis htatriz; �,_ _, 1 i HeadspaceInVOAVraIsf>5.5MIn)? ©Yes ❑No N/A _ _ 10. Trip Blank Plasent? - QYes 1-34V INIA 11. Trip 6};1;;%: Cu.cl„dV Sells Plescnt? i COMA MN rS/SA` I'LF DIS01F.PANCY CLIENT NOTIF10,T10N/RESOLUTION Person Contacted: Project Nlarrager 5CURF Revlrrly: Project NI:rnarer SRF Revievr: Date/Time: CIP -- - - - - t ricldoataR:yv;rid7 IjYC: Elmo tw ID of split rorltainer-a: Data: Dates -- Page 8 of 10 . �PaceAnal iCal' Document Narne: - DccClnent Revised:�— �nrpie Condition Upon Recelpt(SCUI{) I i of 2 —_ Document No.: lssuing Authority: f•CAR-CS-033-Rev.06 Pace Carelirtas Quality Office *Check marls tap half of box if pH and/or dechlorination Is verified and within the acceptance range for preservation Samples, Exceptions: VOA, cD forrn,'rOC, Olt and Grease, UktO/8015 (walao DOC, LLIIU *'Bottom half of box is to list nuinber of bottle Project h I wog . 924033 o PM: AMD Due Date: 10/26/18 CLIENT: 92—Ready Mix F _ pl-I Adjustinerlt Log for Preserved Samples Sample lD Type of Preservative pH upon raceipt Uat� preservation adjusteJ Tine preservation } Amount utplCSelv�t':�0 ice II ��^ adjusted I adticd i � f Nate: V,'l:ecr:ver there is a discrepancy affecting f crm, Curo!tna rnplas, a copy of this fa: n; refill he sect t:::110 Af1,:t urc ,r : jli:zv i;'O- Out al hclo, ia.:rrect p(nsenVat;vc. a.:t cf tep1l), incurcc�ct soraainers. Page 9 of 10 F CHAIN -OF -CUSTODY 1 Analytical Request Document .... •,� The Chsiz-at-Custoay i D L-ii,L DOCUMENT. All rclevan; f9ePds musl 5^ cnmplesed asa,ila;' ly. Serlion A j•lc:ion $ Sectian C Rcgoi,�li ;;36:a: ...... _ c:vP'jvct infu:lnnian: Invnicr to m—miow 1 C.is 1 {Cc�s:::+r.4'• I itOaSy �1,. Crsrr,:.:: :rcrt i s JAY L Ya'crn: f;�r::.:. I 'r.fif <Srr. St: c.•t �� t':'•r 7�;> a. �� �,3 ��. c-+j....—:CJ. �,:h-'��Cnrro�<<r.: ---•-t.-_.-.. __.-- � ^:n;:crt - ---'--'--- AC:k�•ar: �. _` _.». «.. R.•ryaf:nnn A—Cv'.•. I[�a -ti �h hll: :ltiiC 1 I ! e.,:r.:'•a Cr:fr;r rt. ��,......_..�....._ �:rcd Q�o�;: '' •n:. !.q C�_7?�} r p:a p. : ai-_. S.trr.=a:_r. Cc^r+ilk a� ',~�a,_ -l—'ax P��?[ob;c:'lv�.rl:r. :as',�n:,LTs,rc �+:r _. Sl..,f: fisiatinn.,r, _ i+rar�•�.y---•--- � .Ir, :y n�; n::iu - : C. �)�T vlr�--9 y � Request SAMPLE ID � V a �TFeZI END 0a, rt Qng ChAra;te r. per boL Y'r ,a ,cl u• u i rl .'rai: �i 1 C lAy 0.9 r I u0 ,,.• j Srmpic Ws rws. be uniqua 71— -.s w c.r `p v O V !E � r � � � O � c� � � C • i f/�� 'DAF;: 71N'Z f1AT= TI': �, JoLU .id II} 1i !� 47 L d7 ..12:?. •i - - ;OwlQNAL CO"PlYTSREUNgUISHtUBYIAJFRUATIaN 71 ATE .� -. ZtM2 ACCEi'ZO gyr6P=lWF30u . ... . OATF,��'- ;t, .SAMPLE CONDMONS . f�%t�`'� I?acre so1i►�S 1inOco. +....I..Y { I SAMPLER 1:A.'.4E ANJ SICNATUR£ f ' • ...; • . - .. PRI14 r -,m� of SAM PLEB: r ? _ • _ SIGNATURE of SAt:1 PLER: -- i 4AT' Si3neN: h a M �• ci e STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE N0. NCG14 0 �Z— I (or FACILITY NAME: twf ; l 7 1,/ PERSON COLLECTING SAMPLES vttial _ 5 t" CERTIFIED LABORATORY P bc— Lab Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: Z0I � 1 SAMPLING PERIOD: pluly-December ❑ January -June COUNTY PHONE NO. { } ADD TO LISTSERVE? []YES ❑NO EMAIL: DISCHARGING TO CLASS: []SA ❑HQW ❑PNA ❑Trout ❑Other Outfall No. Date Sample Collected (mo/dd/yr OR NO FLOW)� pH {Standard Units) TSS (mg/L( Event Duration (minutes) Total ` Rainfall (ml In 71er 2 Monthly Monitoring? (y/n) # of Months in Tier 2 Sampling, - - 6-9 100 2,3 CFt ITA F r [MR S n A i t If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each autfali here. Please make sure to mark the Sample period above. r if a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. ' T55 benchmark values are 100 mg/l, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/l. For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 1 Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outfall No. Date Sample Collected 1 (mo/dd/yr} pH (Standard Units) TPH using method 1664A SGT HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total a Rainfall (in) New Motor Oil Usage (gal/month) In Tler 2 Monthly Monitoring? (yjn) # of Months in Tier 2 Sampling; 6-9 15 100 , I HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OLJTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO ❑ HAVE YOU CONTACTED THE REGION? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Maii Orieinal and one conv of this DMR fincludine all "No Flow" & "No Discharae" reports) within 30 days of receipt of samole for at end of monitoring period in case of "No Flow" to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFIG4 TION FQR ANY INF RMATI N REPORTED. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date} Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 S77M MCDEW R Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Porguidance onfilling out this form, please visit, http•llportal.ncde&r.Qre/we wy f w5isu/nFdeaw#tab-4 Permit No.: �/�/�/_/ _/,/�/_/_/ or Certificate of Coverage No.: W.C1;JQ—qjb-&Jj / Facility Name: ' }7lWr ZZ County: hi k Inspector, boy Date of Inspection: Time of Inspection 1Z 1Q, 25 AY Total Event Precipitation (inches): I V Phone No. 514`554- Zagr7 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See i formation below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a 'representative storm event" or "measureahle storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event" However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: or Designee) Pagel of 2 SwU-242, Last modified lo/2S/2012 1. Outfall Description: Outfall No. Structure Cpip itch, c.) Receiving Stream: Describe_Lhe industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc,): _ .--_W Wr_ — 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 6) 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: (j7 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: b 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes No 9. 1s there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be Indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 p w O O CHAIN -OF -CUSTODY! Analytical Request Document Co The Chain -of -Custody Is a LEGAL DOCUMENT -AN relevant fields must to completed accumieiy. M a Sa';6m A Section B Section C r .... I P-44W 4 Cuax tn$o Iion: i Rnqu"d Pfaloct Infon neo. tmra:co Wcrr udon: Paae : } of , Aeadv Mel C.an'vata Report Tw.. Ja vi jwu I nacre]670Bush8 Copy To: Compa y 11[a.aaC Mi0 rocs.,.A✓*4 Fg., PwcAsse Order*: race DucePawCown Oue pau: Prp Oti N: J 1 t race rrollro N. NC 1 - ftequeaetl Anat is F"Ilewoa JN - I t. • i r.Tnu eves ? Q caurcl= = Preservatives Y omromm. ow 3 u 8 :? wwlv.. w.a. ww SAMRLE ID CL Cbw"o START END a+� .Ono per cox. vwrr vrn � P F.!,. QMQ. fr° TIME DATE TIME �,�� a:: ,:�' -;, � •i ` Ply 3 � �, � ;�- � Z� f � � 7.- T- =12 '-4'^ �%;}. i=;�wK - tip,: -���,��_ LL_"� _ '.r;; S'.' J�I1OfI1C/iAL"1�111lF1r6' �; +7�' STf Ii`FQ.IA7ION-/.�-1 p;.I�- :,a}..v� s; ,icy. .R,4. ,:� ..1�• �710FF•. •t�J.. .. -.�.. v- TIlIE, ..t ^.mow w.L'3J111a�y`�f.C;Of�ffMai:i.. -_C-_ ..ram. .< :1• .!�JiY.. "�.! .Y, -f :'"Sy�{l:L: - .�.•taa Y! w}r-� :>F { v�-• ::Y wi :�- .:OW7tR2: - .?: ;'tv4J't. � .� 1..} �:. . -�1:-..+� !I J Z, I 4 t stwaLsx,(L ari�aluo'stcr+Aiuiie PRWTN4vw of SAMPLER: s o w SIGNAURE of SAMPLER: QATE S19ma; _lCeAnaliftal" amw:pacafeba.corn December 27, 2017 Jay Watkins Ready Mix Concrete 3610 Bush Street Raleigh, NC 27609 RE: Project: Plant 31 Capital Blvd Pace Project No.: 92368001 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Jay Watkins: Enclosed are the analytical results for sample(s) received by the laboratory on December 21, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, cq Angela Baioni angela.baionl@pacelabs.com (704)875-9092 Project Manager Enclosures J.9 REPORT OF LABORATORY ANALYSIS Thls repast sha8 not be reproduced, except in full, without the wrkfen consent of Pace Analytical Services, LLC. Page 1 of 10 _ aceAmliftal wwrcpa�bacom ! Project: Plant 31 Capital Blvd Pace Project No.: 92368001 Pace Analytical Services, LLC 9800 KlnceyAve. Suits ioo Huniersvllle. NC 28078 (704)M-W92 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 633 VrginialVELAP Certification #: 46DD25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLC. Page 2 of 10 ceAnalytrcal. - %wMcpicelebsoom Project: Plant 31 Capital Blvd Pace Project No.: 92369001 Lab ID Sample ID 92368001001 Outfall 91 Plant 31 SAMPLE ANALYTE COUNT Method Analysts SM 2540D NMH REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In hAl, without the written Consent of Pace Analytical Services, LLC. Po" Anaiydeal Services, LLC 9800 Kfncey Ave. Suits 100 Huntersville, NC 28078 Q04)875.9092 Analytes Reported Laboratory PASI-E Page 3 of 10 ceAnalytical a .cam ANALYTICAL RESULTS Pace Analytical t»rvicea, LLC 9800 KlnceyAve. Suite 100 Huntersville, NC 28078 (704)875.9092 Project: Plant 31 Capital Blvd Pace Project No.: 9236BOD1 Sample: Outfall #1 Plant 31 Lab ID: 92368001001 Collected: 12120/17 14:30 Received: 12/21/17 14:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed GAS No. 4uat 25400 Total Suspended Solids Total Suspended Solids Data: 12127/2017 09:32 AM Analytical Method: SM 2540D 9.9 mglL 2.9 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pats Analytical Services, LLC. 12122/1714:24 Page 4 of 10 ceAnalyt�cal www 6=kbe.Iwn QUALITY CONTROL DATA Project: Plant 31 Capital Blvd Pace Project No.: 92368001 QC Batch: 392160 Analysis Method: SM 2540D QC Batch Method, SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92368001001 METHOD BLANK: 2175740 Matrix: Water Associated Lab Samples: 92368001001 Blank Reporting Parameter Units Result Limit Analyzed Quallfiers Total Suspended Solids mg1L ND 2.5 12122117 14:10 Pace Analytical Services, LLC 9800 KlnceyAve. Suite 100 Huntersvilte, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2175741 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 256 102 9D-110 SAMPLE DUPLICATE: 2175742 923676650DI Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 22.6 31.4 33 D6 SAMPLE DUPLICATE: 2175743 9236BOD4001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 65.2 67.7 4 Results presented on this page are In the units Vrdicalad by the'Unt4" column ucept whate an altemete unit is presented to the rlgM of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2017 09:32 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 10 Pace Analytical Services, LLC acem1alytical s OM Kinney Ave. Sulfa HuMersville, NC 28076 arVW.P aooun (704)675-M2 QUALIFIERS Project Plant 31 Capital Blvd Pace Project No.: 92368001 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anaiyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitfile by EPA Method 0260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in U. Date: 12/27/2017 0g:32 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 10 ceAnalytical wrrw.p=Pkbasom QUALITY CONTROL DATA CROSS REFERENCE TABLE Project Plant 31 Capital Blvd Pace Project No.: 92368001 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (7041875-9092 Lab ID Sample ID - QC Batch Method QC Batch Analytical Method 92368001001 Outfall 01 Plant 31 SM 2540D 392160 Date: 12/2712017 139:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproducecl, except In full, without the written consent of Pace Analydtal Services, LLC. Analytical Batch Page 7 of 10 Ate' s Fii:F2"r}i✓r;,+..''-.:., f.. D66merit'1436et - - = '0olurrrent Revised: July 25, 2027 Sample CondEt[ori'tj onlReeel SJSLURJI�.'J{! 3•'.--�r: Pa e ] of 1 ! 8C�ARlCal' DacumenttJd:s1 "'` ISiuingAuthorlty: J F CAR-05 033aiev.03 ::e�Yy I Pace Quality Office r —1 dbordtoyf lecefvin&-samples --Greenwoad ---- — -. r,,•� , - 0-- — Hurite�s iE18i � 'Raleigh Mechanlcsville0•-•• - - ' Client Name: `F W0 9236800 1 Upon Receipt.. Project q: - l Commercial ❑Pace Uusps Went UPS ❑Other:_ ❑ � Custody Sea! Present? ❑Yes &lo Seats Intact? ❑yes I 923661 Date/Inldals Person Examining Contents - Packing Material: ❑Bubble Wrap ❑bubble Bags 21 ne ❑ Other Biological Tissue Frozen? Thermometer: []Yes []No TA ❑ IR Gun ID: �� 2 ` wet ❑Blue ❑None Typo of Ice: .,_.-..�,..Ar- -��.— .,__._...-----. �__ ..----.—.----�'�•----.-•--.�Sasnples.aut�ltemp�[Leda.Samt�les.onhr.coo➢ni ProSee�{___..._....._ „_ Cf at•trw} has begun USDA Regulated Sol] A, water sample} Did samples or' nate I varantlne zone vAthln the United States: CA, NY, of SC (check maps)? old sasrples originate raun a foreign source lint r Zonally, ❑Yes InducitcHawallandPuertoRico)?❑Yes No Ccunments/Discrepancr Chain of Custody Present? Ye No ©N/A 1. Samples Arrived withialloldTime? Yes No /A 2. Short hold Time Anal s e72 hr.)? Elyes ❑N/A 3. Rush Turn Around Time Requested? OV. Na N/A A. Sufflcieet Volume? es [:IN. ❑N/A S. Correct Containers Used? .-Pace Contalners Used? n Ow No ❑N/A NA 6. Containers Intact? Yes ❑No ❑N/ 7. Dissolved analysis: Samples Field Filtered? Yes ONO N/A a. Sample labels Match CRC? -Includes Date/Time/ID/Anal Is Matrix: Yes ❑No ❑N/A 9. Headspme In VOA Vialsfs-" r ro? QYu Of N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ©Yes Yes ❑No ❑No JN/A N/A 22. C11ENTNDTIFICATION/RESOLLIFTI N Person Contacted: Comments/Sample Discrepancy: Project Manager SCURF Review: Date/Time: Date: Field Data Required? LEYes ❑No Project Manager SRF Review, T n 3-j Date: q No(e; whenever there Is a discrepancy affecting North Carolina compliance samples, a copy ofthls form w1R be sent to the North Caroline DEkNR Certification Office lie. Out of hold, Incorrect preservative, out of temp, Incorrect containers) •i r Page H,of 10 *Check mark top half of box if gltall � Mo ------ verified -and -within -the acceptame-renge-ior--- preservation samples. ` "Bottom half of box is to list number of bottles ig n6f e` y�.�n�ntReylsed:Jylyr25,2017 •,,� is. n:liAan:ii;hipr SCUfi.{� �':•` - Pate 2bf 2' iiltenk'�ipi �� .'"''�`��'� r•. ^ >' --�S171rig Authority: 5-439 Re"v.43:r; as ti�a Pace Quality office W0# : 923fi30®1 PH: AND Due Date: 01/08/18 CLIENT: 92—Reedy Mix Y p R a � pp f0 l 3 —S �S N �s 4 \ 5 6 7 9 4 10 \ \ 11 \�]\ 12 \ \ pH Adjustment Log for ke' served Samples Sample ID Type of Preservative pH upon receipt Date preseivatioA adjusted Time Pieserwtlarl adjusted. Amount of Preservative added Lot a Page 9 of 10 ALT-19;AWF MAY p 4 2.11, NCDEHR pvvR SECTION Stormwater Discharge Outtall (SDO) Qualitative Monitoring Report For cquidnnce 6nfi lin� out this form, please visit: r1 dear. r wei lr tiv t r . Permit N,o.:1_I—I_/ or Certificate of Coverage No.: N/C/G/ "11_1/ 4l?11/ �1 Facility Name: C I B I Ud f Iay1f 3 i County: W Av< Phone No, 41 �i' 654—ZDWY Inspector: Odmad d S+ad tl Date of Inspection: Tinie of l6spection: I :Do MrW+ Total Event Precipitation (inches); -4 WL Was.this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below,) [? r?s ❑ No Please verify whether Qualitative Noiiitoilitg nrirst be peiforrned during a "representative storm event" or "meosureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitadv.e monitoring to be - performed during a "representative storm event" or- during a "measureable storm event:" However, some permits do not have this regLIJrelnetit. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 'inches,a.f rainfall anti that is &eceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred.. A single storm event may contain up to 10 consecutive hours of no precipitation, I A "measurable storm event" is a storm event that results in an actual diseharge from the ,permitted site outfall. The previous tneasura.hle storm evert must have been at least 72 hours prior. The 72-hour storm interval does not apply if the perniittee is able to document that a shorter interval -is representative for local storm events during the sampling period, and the pernrittee obtains approval frorn the local DWQ Regional Office. l By this signature, 1 certify that this report is accurate and complete to the best of my knowledge: (Signature of Permitt. e or esignee) 11age 1 of 2 SW(J-242; Last niodit'ied 7/3 r/2013 1. Outfall Description: Outfall No. I Structure (pipe, i t �c.) Receiving Stream: Describe the industrial activities that oc�i ur with' the outfall drainage area: 2. Color: describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: ctfAr 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weal{ chlorine odor, etc.): u17" 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: © 2 3 4 S S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: t) 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes V AIITN 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe ML21J IR— Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5wii-242, fast modified 7/31/2013 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division -of Water Quality General.Permit No. NCG060000 Date submitted y I t 11— j CERTIFICATE OF COVERAGE NO. NCG06 0 Z Lb SAMPLE COLLECTION YEAR 20n — FACILITY NAME C& ; -Al e]yt pk&a. 31 FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY 1 ky-f ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTiNG SAMPLES ha 1 U DISCHARGING TO SALTWATERS? [—]YES [�NO LABORATORY_ pAL1& Lab Cert. # PLEASE REMEMBER TO'SiGN ON THE REVERSE -' Part A: Stormwater Benchmarks and Monitoring Results Total event -rainfall 2 Y or ❑ No discharge this period" Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD; mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark - 100or. 0 Within 6.0 — 9.0 120 30 1000 Soo ' Only appliesto facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at a,M outfalls. You must still submit this discharge monitoring report with a checkmark here, 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of newmotor oil per month? Q yes no (if yes, complete Part.B) Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No, Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50 6.0 — 9.0 - ' Only applies to facilities that use/Process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this -discharge monitoring report.with a checkmark here. 4See General permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SWU-249 Last Revised: October 19. 2012 Page.] of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. * 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. a TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab „results Lor at end of •monitoring period _in_the case of_"No Discharge" reports) ta: Division of Water Quality, Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry'of the person or persons who manage the system, or those persons directly responsible for gathering the- information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date). Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wglws/sulnpdessw#tab-4 SWU-249 Last Revised: October 18. 2012 Page 2 of 2 *FOR.PART A AND PART.B MONITORING RESULTS: • ,A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. ,, TIER 3; HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑NOgR IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑. REGIONAL OFFICE CONTACT NAME: Moil an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lob results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I.certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information -submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Sh /1 7 (Date) Additional copies-of.this form may be dbwnloaded at: http://,portal.ncdenr.org/web/wq/ws[s_uLnpdessw#tab-4 SWU-249 Last Revised: October 18. 2012 Page 2 of 2 T co m 0 O iq CHAIN -OF -CUSTODY 1 Analytical Request Document Arralytc2i The Chain -of -Custody is a LEGAL DOCUMENT. Ali relevant fields must be completed accurately. Seetlon A secCuo a Section C Required Giant Information: R,Qairtd Project lnfarmeHon: invoice [nfarrrution: Pd ¢: 1 I Ot t .. Company: Rsuoy Wx Com mtu Report To. Jay Watkins 7domocs: 3610 Bush $treat Copy To: Ralo O, NC 27609 ~ Email' - , .a � yt ('7•cGC, �K Purchosa order♦: Phcnt: (9i9j79o-t520 Fax Prdjact Namc: , gt•rTFALL Requesu'd Due De3t. Projetz C: IIASFIx U"hN was udCE r Cn Wr Nw o GU7 U m Warta Pro[uct SAMPLE ID � =l P a i `s � sTanT One Character Par box. w'+^ WP (A-Z.0.91 , .l T. y, Ni of a r Sample tds must tr■ unrqua z..,.. rsLLI % _ L s OAT.E T prole 0 Q U END �+ v FT. A, � 7 2 � E 2 Z l7 •... � O N .Its^y .ti i:y� r i U i l•I� CZA4KW.Z NILr,�' 'NaU"iF....Mf#�L�G�,[�' of SAMPL U � h F ha v izi 2 d ' 0 } Ice Anallcal www.pacelabs.com 1 ANALYTICAL RESULTS Project: Outfall Plant 31 Capital Blvd Pace Project No.: 92335465 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2807E (704)875-9092 Sample: Outfall #1 Plant 31 Lab ID: 92335465001 Collected: 03/31/17 11:00 Received: 03/31/17 17:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 3.4 mg1L 2.5 1 04/05/17 10:00 Date: 04/06/2017 08:11 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 10 aceAnalytical, Document Name: ESI Tech Spec Sample Condition Upon Recelpt(SCUR) cument Revised: Sept. 21, 2016 DoPage 1 of 2 Document No.: F-CAR-QA-003-Rev.02 Issuing Authority: I Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh® Mechanicsville❑ MEN; .. Client Name: 0# 92335455 Project W Courier: ❑Fed Ex ❑UPS ❑USPS [WIlient 11111111 ❑Commercial ❑Pace ❑Other: 9233°i I Custody Seal Present? ❑Yes GND Seals Intact? ❑Yes ?NO Date/initials Person Examining Contents: Packing Material: ❑Bubble Wrap []Bubble Bags [None ❑Other, ✓� Thermometer: ® IR Gun ID: '� 15-3492_ Type of Ice: ewet []Blue ❑None (]Samples on ice, cooling process has begun Correction Factor: Addo.6 Cooler Temp Corrected I°C): 3 , 01ological Tissue Frozen'? []Yes ❑No O/A Temp should be above ,,,ff���rr,e,,!!l///ezing to 6°C USDA Regulated Soil ( N/A, water samp4e) ()id samples originate in (—]Yes allo quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, including Hawaii and Puerto Rico)? ❑Yes , Comments/Discrepancy: Chain of Custody Present? ❑ ❑ I. Samples Arrived within Hold Time? 121 ❑ ❑ 2. short Hafd Time Analysis (472 hr.j? ❑ ff ❑ 9. Rush Turn Around Time Requested? ❑ M ❑ 4. Sufficient Volume? ❑ ❑ 5. Correct Containers Used? -Pace Containers Used? ❑ ❑ ❑ ❑ 6. Containers Intact? © ❑ 7. Samples Field Filtered? © 8. Note if sediment is visible in the dissolved container Sample Labels Match COC? Includes Date% Time/1D/Analysis © ❑ 9. Headspace in VC1A Vials (>5-6mm)? Yes No Trip blank Present? Trip Blank Custody 5eals Present? Yes Yes No No N/ N/A 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: DateMme: Field Data Required? ❑Yes ❑No Project Manager SCURF f Review: fl/ Date: Project Manager SRF q Note: Whenever Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) t s i S Page 8 of 10 0! 9 n v v R v f M 2 ti m i i i a z r _CL C m '03 'T f N R M A, I w � n O 1 I N � � I � M tG mtD 1Z `I C 3 o 5 � rn n I o d� a b � R 'R a ro m I i K' R I( t A 0 r Item# BP4U-125 mL Plastic Unpreserved (N/A) (CI-) BP3U-250 mL Plastic Unpreserved (NIA) BP2U-500 mL Plastic Unpreserved (N/A( BP1U-1 liter Plastic Unpreserved (NIA) 13133S-250 mL Plastic H2504 (pH < 2) (CI-) BP3N-250 mL plastic HNO3 (pH < 2) BP3Z-250 mL Plastic ZN Acetate & NaOH (>9) BP3C-250 mL Plastic NaOH (pH > 12) (CI-) wGFU-Wide•mouthed Glassjar Unpreserved AG1U-1 IiterAmber Unpreserved (NIN (CI-) AGSH-1 liter Amber HCI (pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (Ct-) AG15-1 liter Amber H2SO4 (pH < 2) AG3S-250 mL Amber H2504 (pH < 2) pzzzzzz A63A(DG3A)-250 mt Amber NH4CI (N/A)(CI-) DG9H-40 mL VOA HCI (N/A) I VG9T-40 mL VOA Na25203 (N/A) _ VG9U-40 mLVOA Unp (N/A) DG9P-40 mL VOA H3PO4 (N/A) VOA% (6 vials per kit)-503S kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SP5T-125 mL Sterile Plastic (NIA — lab) SP2T-2SO rn L Sterile Plastic (NIA — tab) zzzzzzBRA-250 mL Plastic (NH2)2SO4 (9.3-9,7) Cubitainer VSGU-20ml-StintillationviaLs (NIA) ! GN i J 0 frD� rr zt v � c O�q N� n W K 0 oQ W Ln — 9- RCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report !'or�rtulutrce nrl fillrrl� Ullt tfr1C'01'nr, 11IcC75e (/iSIC: � i�'.rIi1U1*iiI.11CLIQnr".L�I'nJ 4YeI1�If'/i7jldi'S-�IUI'1t1LVdtCI"I Permit No.: �i/c/_/_I_hI_L _I —I or Certificate of Coverage No.: N/C/ l-/ -i Facility Name: CSVI- fat _Blmd Eiat 3 t Comity: W �k[ Phone No. q 1 q_- 554- LOSS I luspector: Date of Inspection:. 3!,411.1_`7 Time ol* Iilspect(on: _L 1 00 out P-t . Total Event Precipitation (inches): Iy2 Was this a "Representative Storm Event" or "Measureahle St01-111 Fveiit" as defined by the permit? (See information below.) { ') Yes ❑ No Please verrfy whetherQuolitative Morritorhrq roust he per formed din-ing a "representative Storm event "or "measm-euble storm event" (requirements vaty, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be, perforwed dUr'ing a "representative st(n'rn event" Or clrrr"ing a "nleasureable storm event." However, some permits do not have this t•ecluiremetlt. Please refer to these derinitions, if applicable. A "representative storm event" is a storm event that measiires greater than 0.1 incites of rainfall and that is preceded by al least 72 hour's (3 days) in whirl no storm event nteasm-iog greaten Chair O. I Inches has occurred. A Single storlii. event may Coist'.dn up to 10 c:onset:ufive IIOLII"S of uo precipilabon. A "measurable storm event" is a stortn event that I•esults in an actual discharge from the permitted site oul-rall. The Itr•evious nteasclrahle siol•rrt (:vent must have been at least 72 how's prior. The 72-hour scorn( interval does not apply if the pertnittee is able to clOCUntent that a shorter interval is representative for local storm emits during the sampling period, and the permittee obtains approval frow the local DWQ Regional Office. By this signa€tn•c, l cc;rtiry That this reiJart is accurate altd conlltletc to the Itesl of my knowledge: (Siglial:ul•e of Permilage of;Designee) Ilaoe 1 or SMI-2421 Last imidified 7/31 /2r113 1. Outfall Description; Outfall No. I Structure (pipe, ET?c.) Receiving Stream: Describe the industrial activities that oc ur with] the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CI1?JAr 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): N0"_ 4. Clarity; Choose the riurnber which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: } © 2 3 4 S 5. Floating Solids: Choose the number which best describes the arnount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: © 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount orsuspended solids in the stormwater discharge, where J is no solids and 5 is extremely muddy: V 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes S. Is theca an oil sheen in the stormmwater discharge? Yes 9. Is there evidence of erasion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe 4 2PJ -e- _ w Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, bast modified 7/31/2013 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCGO60000 Date submitted q / f 1 f -1 CERTIFICATE OF COVERAGE NO. NCG05A Z _ _f- SAMPLE COLLECTION YEAR 'Zd n FACILITY NAME 1 FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY WKilt- I _ ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES na Y f h 014 DISCHARGING TO SALTWATERS? DYES [XNO LABORATORY P Lab Cert. 4 y. 1 PLEASE REMEMBER TO SIGN ON THE REVERSE -i Part A: Stormwater Benchmarks and Monitoring Results Total event roinfoll a or F1 No discharge this period3 Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units Col), mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 mi Enterococci , Colonies per 100 ml Benchmark - 100 or 50' Within 6.0-9.0 120 30 1000 Soo t 3 1 I n 3 I I I I Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For samolins periods with no discharge at any outfalls. You must ,till submit this discharge monitoring report with a checkmark here. `See General Permit text, Table 3, identifying the especially sensitive receiving crater classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Q yes no (if yes, complete Part B) Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, me/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gallmo Benchmark - 30 100 or 50 6.0 — 9.0 - unry apones to raan[ies that use/process meats. The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any. outfalls, you must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SWU-249 Last Revised: October 19. 2012 Pagc I of "FOR PART A AND PART S MONITORING RESULTS: 0 A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART 11 SECTION G. 0 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALI_ T IGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. o TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUT FAT_!_? YES ❑ No ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the tab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wglwslsu/ngdesswntab-4 SWrU-219 L,i�t Revi,,ed: October 18. 2012 Pn�c 2 of--, "FOR PART A AND PART.B MONITORING RESULTS: Y A BENCHMARK EXCEEDANCE TR{GGERS TIER 1 REQUIREMENTS. SEE PERMIT PART it SECTION G. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge' reports within 30 da s o recei t of the fob results for at end o mcnitoring period in the case o "No Discharge" reports)to: Division of Water Quality Attn: DWQ Central Giles 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED, "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who rnanage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my Knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Knowing violations." (Signature of Perm sh //:z (Date) Additional copies of this form may be downloaded at: http://port3l.ncdenr.orgfwebZwg/ws/sv/npdesswl$tab-4 SWTJ-749 L,,,ct P%cvicerl: October IS. 2012 Pagc 2 of 2 CHAIN -OF -CUSTODY 1 Analytical Request Document :: AJralyfe2! The Criain-ef-Custody is a LEGAL DOCUMENT. Alt relevant fields must be compteted accurately. Section 6 Section C SeCUDn A Required Prolect Information: inroile tnfwrnation: Pa 0 : 1 I Of 1 Required Client lntermation: Report To: Jar YJ9lkins A@ention: Company. Aeuoy Mix Conmew Copy Ia: Company Nana' I . Adorosc., 36s0 BUSK SIroM Re'4latory,A Agency Ral�,gn,NCg7C-09 r Z r G./-'f PuerlUax Order s; paces Quoin: PhonL: (9i9179o-1520 Fax Prajau Name , OUTFAlL Pace Project Monoger. gpin-caioni(!bpncelpl+y,wm. Eii to l Locudoa Requosied Due Dole: Projcu8: t..� Jci' Poca P10flc o — Z COLLECTED Preservatives rµtarx crce , urri.y x e err 0 g 16 tWrarer ws u e P, SRMPL E 1d o'. amr P a TrARI Etr0 o `a I • � u Y w 0— Characrnr per box. wiNr wp q :m l Sampla Ids must pe unique r4 7. 0 ? w O m a !— c� PA i S x Z O r Ov I i I /1q_ /6r I3tV117�u (,,ttv f'cr-- C_ H131//?_ I f?�10 13, f I Y 11 A/ I _ I MINT Mamc of w ro 0 0 0 DAIE i i :i•s � m N IL Pace Analytical Services, LLC aceAnalical o 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 sw w.pacelabs.crom (704)875-9092 ANALYTICAL RESULTS Project: Outtall Plant 31 Capital Blvd Pace Project No.: 92335465 Sample: Outfali #1 Plant 31 Lab ID: 92335465001 Collected: 03/31/17 11:00 Received: 03/31117 17:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 3.4 mglL 2.5 1 04/05/17 10:00 Date: 04/06/2017 08:11 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical services, LLC. Page 4 of 10 Document Name: ESI Tech Spec Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 1 of 2 oocumentNo.: _ Issuing Authority: I �� ;.d'ii(;eAnalytca! F-CAR-QA-063-Rev.02 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh® Mechanicsville❑ • Client Name: Project v W®# : 92335465 q�I Courier: ❑Fed Ex []UPS ❑USP.S Client ❑ Commercial ❑Pace ❑Other: 92333465 Custody Seal present? ❑Yes gNo Seals Intact? ❑Yes Po � 1 Date/initials Person Examining Contents: 4 Packing Material; ❑Bubble Wrap ❑Bubble Sags None ❑Other:__ Thermometer; IR Gun ID; I$-3g92 Typo of Ite: �4vet ❑Blue ❑None ❑Samples an ice, cooling process has begun ® __.. _ Correction Factor:Addo 6 Cooler Temp Corrected (°C): 3.1 Biological Tissue Frozen? ❑Yes ❑No (c 'i/A Temp should be above ,,,ff���rre,,,//////ezing to 6'C USDA Regulated Soil (I !N N/A, water sample) Did samples originate inToul arantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, ❑Yes bdNo including Hawaii and Puerto Rito)? ❑Yes . jib Comments/Discrepancy; Chain of Custody Present? ❑ ❑ 1. Samples Arrived within Hold Time} Or ❑ ❑ 2. Short Hold Time Analysis (02 hr.)? ❑ ❑ 3. Rush Turn Around Time Requested? ❑ M ❑ A. Sufficient Volume? a,❑ ❑ S. Correct Containers Used? -Pace Containers Used? ❑ ❑ ❑ ❑ 5. Containers Intact? © ❑ 7. Samples field Filtered? — ❑ 8. Note if sediment is visible in the dissolved container Sample Labels Match COC? -Includes OatePime/ID/Analysis _❑ f� f ❑ ❑ 9, Headspace in VOA Vials (>5-Gmm)? Yes No N 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑ Yes El❑ Yes ❑ No No N/ ❑ N/A -- 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: I Comments/Sample Discrepancy: Date/Time: Field Data Required? UYes ❑No Project Manager SCURF Review: I j t 7 Date: Project Manager SRF Note; Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i e. Out of hold, incorrect preservative, out of temp, incorrect containers) — - Page 8 of 10 n> m 0 0 1 v m d K m I I ro T � 1 CL m r+ a r 0 3� d pQ � N rD 3 m a Q I n CA b a K d n Sl a � m � n m i N u p Cl V T c! S W N F+ Itemir zzzSKU-125 mL Plastic Unpreserved (N/A) (Cl-) OP3U-250 mL Plastic Unpreserved (N/A) BP2U-50O mL Plastic Unpreserved (N/A) —� BP1U-1 liter Plastic Unpreserved (N/A) *V BP35.250 mL Plastic H25O4 (pH < 2) (Cl-) V XA A X BP3N-250 mL plastic HNO3 (pH <2) BP3Z«250 mL Plastic ZN Acetate & NaOH (>94 MC-250 mL Plastic NaOH (pH > 12) (CI-) f ! WGFU•wide-mouthed Glass jar Unpreserved l AG1U-1 liter Amber Unpreserved (N/A) (Cl-) / AGIH-1 liter Amber HCI (pH < 2) AG3U-250 mLAmber Unpreserved (N/A) (Cl-) AG IS-1 liter Amber H2$O4 (pH < 2) ^— i AG3S-250 mL Amber H2SO4 (pH < 21 AG3A(OG3A)-250 mL Amber NH4CI (N/A)(0-) OG9H-40 mL VOA HCI (N/A) VG9T-40 mt VOA Nn2S2O3 (N/A) VG9U-40 mL VOA Unp (N/A) I OG9P4D mL VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) • SPST-125 mL Sterile Plastic (N/A— Iab) ( SPZT-250 mi-Sterile Plastic (N/A —lab) IZzz/ I3P3A-250 mL Plastic (NH2)2SO4 (9.3.9.7) Cubltainer VSGU-20 mLScintillation vials (N/A] i GNGN I O rr zt r 3 M •• 40 � � U r' ro c A c d K Q p o zn st � ro r da4b L- \ N A NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling outthis farm, please visit: http_//12ortal.ncdenr.org/web/Ir/n12des-stormwater/ Permit No.: N/C/_/_/_/_/ _/�/�/ or Certificate of Coverage No.: N/C/G/./ A/d/Z:/ /'/G/ Facility Name: l A."- 31 cot ❑►;1 Is I V10 County: _ Inspector: Date of Ins Time of In,, {NAKY I Phone No. gFjg .SSA{ -Zo$7 Total Event Precipitation (inches): , 15 , JUL 14 2016 DWR SECTION Was this a "Representative Storm Event" or "Measureable St'o m hveii ' °a�s�defined��blyIthe permit? (See information below.) [� Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, i certify that this report is accurate and complete to the best of my knowledge: (Sign/ure(Kf Permittee or Designee) Page 1 of 2 SWU-242, Last modified 7/31/2013 1. Outfall Description: Outfall No. Structure (pip ditch tc.) Receivine Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: C a_ur 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): �P00j2 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 6) 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes CID 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe N 6N Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 sWU-242, Last modified 7/31/2013 PaceAnalyfical' CHAIN -OF -CUSTODY I Analytical Request Document The ChMn-al-Custody is a LEGAL DOCUMENT. All relevant holds must be completed accurately. a, Pepe. 01 Section A Soctlon 6 Sedlon C 2056316 Requlrnd Giant Infmmatlow Reguirad Propel Inle.maftm, Irwaica Information: Y: - ReDw,10., AMlcnl�wr: r ee z7 L� Copy To., ComperryNsme: REGULATORY AGENCY Address: F NPOES I'"' GROUNDWATER i• ORINKINGWATER f UST r' RCRA r OTHER EmaL1l To: Purchau Order No.: Paco auNc Rarmewe: Ph _ Pf led Name: E 61 SMa L,ocaHnn Zr%b f t `- �teeo m STATE: - - - -- Requested DueDattlTAAT: "actNumtor. Zg �/ 7H PxcPF.C.t. t^� 1 . Requested Analysi3 Fittrtred (Y!N} 9ectlan D Matrix Codae — 2 PAgelnaCliorn lnrorr.aecr, MATRIX I coo€ 9 COLLECTED Pl9servativus s` CHnklrq e. DW wal ,° xa water WT waste water vow rn. oour� sTARr ccv Pos re Lmnrluw L) Z Pnlduct P e w ! SuIVSoFd St _. _ r. SAMPLE Ip al of WIDO WP U 1' w w - m .� (A•Z,0.tiI.-) Air AR -ample ID9 MUST BE UNIQUE TLtsuo rS 0 0 w ¢a h b Olhc. OT 0 (] ayp -^ =Q ri7 W to '= Z) X i Z z y a I-D. DATE TMMF DATE TIM6 _ ]UC Pace Project NoJ Lab 1 i � / l R i 3 S 6 7 8 9 10 11 iz ADDITIONAL WMMENTS REL114=21HEDBYIAFFUJATION: DATE TIME A AFPI PA1PTIME SAMPLECONDVTiONS L i`r ORIGINAL PLER NAME AND SIGNATURE v m PRINT Name or SAMPLER: E c m C; a U .R aTE SS17ned SIGNATURE of SAMPLER: sAlrAroD7YY}: � r++ "+,nW3,1 Nem- vy ,-9> .o hrs,am Y" — Acwgov P-WA NF r .AO d y pa%.",l lrr- a.+ in Wn. d--g R ar I,a% ue, , . P, lie eny rca pva v Tt U asrs. F-AI.t.-W2Drev.07, 15-6tay-2007 aceAnalytical. r www.pacelabs.cnm f I ANALYTICAL RESULTS Project: PLANT 31 CAPITAL BLVD Pace Project No.: 92303404 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Sample: OUTFALL #11PLANT 31 Lab ID: 92303404001 Collected: 06128116 15:55 Received: 06/29/16 15:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 2.6 mg1L Date: 07/01/2016 02:17 PM 2,5 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fur, without the written consent of Pace Analytical Services, Inc.. 06/30/16 13:16 Page 4 of 9 eAna"cal Document Name: Condition Upon Recel Document No.: F-RAL•CS-001-Rev.04 Sim Client Name: Project q: Courier: ❑Fed E:x ❑UPS ❑USPS Client ❑ Commercial ❑Pace ❑other: Custody Seal Present? ❑Yes ONO Seals Intact? []Yes K]No Document Revised: May 24, 2Ulb Page 1 of 2 Issuing Authority: Pace Raleigh Quality Office Page 2 of 2 for internal Use ONLY r LSO#:92303404 9I23��� 03404 bate/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap ❑Bubble Bags eNa ❑0ther. Thermometer: T1505 Type of toe: Wet ❑Slue ❑None E]Samplesonicecoolingprocesshasbegun Correction Factor: O.O'C Cooler Temp Corrected ('C): 3 ,Z T Biological Time Frozen? Dyes ONO VN/A Temp should be above fr ez4to 6'C USDA Regulated Sell ( $N/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or 5C {check maps)? Did Samples originate from a foreign source (int!n)btionally, nYes V No Ineludine Hawarrand Puerto Riml? 11Yes o —1 Comments/Discrepancy- Chain Of Custody Present? Ifies []No ❑NJA 1. Samples Arf ived within Hold Time? Yes []No []N/A 2. Short Hold Time Analysis (�7Z hr.)? Oyes N!A 3. Rush Turn Around Time Requested? ❑yes N/A 4. Sufficient volume? es No E JNL/A 5. Correct Containers Used? es ges ONO ❑N/A 6. -Pace Containers Used? ❑NO NJA Containers Intact? t" []No N/A 7. Samples Field Filtered? []Yes ❑No WIA 8. Note if sediment is visible in the dissolved contalner Sample Labels MatchCOC? es ©No ❑NJA 9. -includes Date/rime/ID/Analysis Matrix: All containers needing acid/base preservation have been 10. checked? Yes []No ❑NJA All containers needing preservation are found to be in compliance with EPA recommendation?+. (HNOI, H2SO_ HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanlde) yes ❑NO ❑N/A mo+cxw0 Exceptions: VOA, C011form, TOC, Olt and Grease, DRO/8015 (water) DOC,LLHI; les Q No N A Samples checked for dechlorination? dYes ❑No PNJA 11. Heads ace in VGA Vials (>5-6mm)? ❑Yes []No /A 12. Trip Blank Present? ❑Yes ❑No NIA 13, Trip Blank Custody Seals Present? []Yes []No XNJA Pace Trl p Blank Lot p (if p urchased): CLIENT NO RCAMNIRESOLUTION Person Contacted: Date/Time: Comments/Sample Discrepancy: Fkld Data Required? ❑Yes [:]No Project Manager SCURF Review: � _ f ll 16 Date: L `?o -I �Q Project ManagerSRFReview: _ _ Hr F 1 _ Date: [Q"'-.�ro—tL _ Note: Whenever there is a dlscrepancy affecting North Carolina comptiance samples, a COPY of this form will be sent to the North Carolina DEHNR Certification Office (Le. Out of hold, Incorrect preservative, out of temp, Incorrect containers) Page 8 of 9 r:����o} GENERAL PERMIT NO. MC G140000 CERTIFICATE OF COVERAGE N0. INCG1l4 (9 Z I f FACILITY NAME: I AV14- 31 a v PERSON COLLECTING SAMPLES 4 -ij CERTIFIED LABORATORY P k t--� Lab # Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEA SAMPLING PERIOD: uly-December ❑ January -June COUNTY U XYY- PHONE NO. (q) K )_ SS11 0 $7 ADD TO LISTSERVE? RYES ❑NO EMA@L: DISCHARGING TO CLASS: ❑SA ❑FICIVV ❑PNA [—]Trout ❑Other. Outfall No. Date Sample Collected (mo/dd/yr OR NO FLOW)1 pH (Standard Units) (mg/L) Event Duration (minutes) TotalTSS 4 Rainfall (in) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier 2 Sampling2 - - 64 1&` I . o !tzo . �aAJ NOV I D fVIRALFILES 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. 2 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TS5 benchmark values are 100 mg/l, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/I. ° For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outfall No. Date Sample Collected 1 (mo/dd/yr) PH (Standard Units) TPH using method .1664A 5Gi'-HEM (mg/L) Total Suspended Event Solids duration (mg/L) (minutes) Total n Rainfall (in) New Motor Oil Usage (gal/month) In tier 2 Monthly Monthly Monitoring? (y/ri) # of Months tier 2 Sampling2 Ei-9, 15� 1002'3 - - - - HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANYONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO HAVE YOU CONTACTED THE REGION? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail Original and one copy of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample (or at end of monitoring_period in case of "No Flow")_to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUSTSIGN THIS CERTIFICATIOiV FOR ANY IIVF0RMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance With a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are 'gnificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." w /D r (Signature of Per ee (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7113111 Page 2 of 2 11C&DENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forgrridance on filling out this form, !lease visit:http;/.�p.or-�al.ncdoni-.org/webLw-ws s r s w# - Permit No.: N/C/_/_/_/_/_/_/ / or Certificate of Coverage No.: N/C/G/L/- / 6/ Facility Name: Plgni 31 Cad"4w OND County: W hy-e Phone No. 40- S 54 - Zb$7 Inspector: Date of Inspection: Time of Inspection: ll' w1 Total Event Precipitation (inches): P 5-> Was this a "Representative Storm Event" or °Measureable Storm Event" as defined by the permit? (See information below.) R Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "meosureahle storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 Hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signatur96f PeYmittee or Designee) Page 1 of 2 SWIG-242, Lastmodilied 10/25/2012 1. ®u><tfail Description: Cutfall No. I Structure (pip , disc tc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: P—,euL# p yed Coyle rty-4,c VlAKf 2. ;Color. Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Gj-ea,✓ T 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weals chlorine odor, etc.): IVDu-a- 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: /) ly 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: Z) 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: & 2 3 4 5 i. Is there any foam in the stormwater discharge? Yes I� v. is there an oili sheen in the stormwater discharge? Yes Is there evidence of erosion or deposition at the outfall? Yes �f i (D. Other Obvious indicators of Storrnwater Pollution: List and describe U0Ua- Dote: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure, These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 /5a?ceAna1Xica1 I' wwwpacerabs.can Laboratory Report Jay WAtkins Ready Mix Concrete PO Box 27326 Raleigh, NC 27611 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875r9092 Page 1 of 1 Report Date: 10/31/2014 Date Received: 10/16/2014 Project: PLANT #31 CAPITAL BLVD Pace Project No.: 92221749 Sample: QUTFALL #1lPLANT 31 Lab ID: 92221749001 Collected: 10/15/14 12:15 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Suspended Solids 38.0 mg/L 2.8 10/22/14 09:49 Reviewed by: Laura J Cooper laura.cooper@pacelabs.com Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 Page 1 of 3 Document Name: Samplo Condition Upon Dowment Revised: Apr1104, rob. R ecelpt (SICUR) fpage 1 of 2 Doounnent No.: IssulngAuthorldes: F-RAL-CS-001-trov,02 Pace AshevilfeQualft Officit'- ClientName: Whore Received: Huntersville 0 Asheville 'Eden Couilor (Circle): - Fed Ex UPS LISPS CiammoTdal pace. Other Custody Sea] on Cooler/Box Present: yes no Sqgls intact.Eno ?'kcJ5fh9 MAtedal: 0 134bbla, wrap" —Bubble—eggs *0�q, 7 elicle, Thernionietor Used. IR Gun SN:12204��e of 1,,. Blue None, C]:Sampleta on fee. Doering P1C;�ese-.,has ,bQ.4un:.- - ' IR Oun Back Up SN.122096371 j Temp., Correction Factor: Add if Su®r ct.—ZZ d Bate Inillals of personpersonax , a mt , ning-". CorrqptoO Cooler T Biological Tissue.la Fr6zen: Yes go oontents/Pr 0 It a p. C: I m check Temp �s houtd be above freezing to VC continents: Custody Present: Ay`- Mo EIWA 4. - - Chaimof Custody -Filled Out: ONo QWA 2. Chain of Custodi Relingirlshad-. zffl" ONo 04A 3. Sampler -Name & Signature on COO, 0�e3 MNo [14A 4:1 -Samtes ArLIved Wth In Hold Time: �rYss 0 No OWA 5- Short Hold Time Anal yos'(<72hr), .0yea MIA 6. Rush Turn Around Tlhie Requ2sted: 0Ym Wo ON' A. 7. sufficlent.volume: Yes- ONo bIVA 8. Corre6t Containers Uaod: �Ckea; ONo DWA: 9, 4, Pace Containers Used., G;T&, ONO, 11NiA Containers intact- 2yea C3N* Ow 10,: Filtered volume received for Dissolved tests ©Yee EINa JMA li, z.77, Sample Labals match COC: a, Qo OWA 12. -includes date/tIme/iDlAnalysis . Maw: All containsis neecling'preservatlon have been chocked. a Elko OwA 13. All 6Atalnem needlino praswaWn are found to be in ONo 011VA Compliance with EPA recommendation. ox"Ptlorw VOA. QVlfvnn,T0C,0&G,WI-DR0(waW) Samples checked for deQb lodnation: 0 Y03 ONo &wk .14. z Beads ace in VOA Vials >6mm):, OYip. ONo fiWA 16. Trip Blank Present: 'Clyeii ONo XWA 16. Trip Blank Custody Seals Present. 13yos Me, /MA [Pace Trip Blank Lot# If Client Notl0cationi Resolution: Field Data Required? Person Gontacled!, Date/Time: C' Ommen'W Resolution: SCURF ISRF Review:, It WEX Now. Whene4ar there Is a diiorepanzy affecting North 0"Ing oompflancs sempWs, a copy of this form YAII be sent to the North Carolina DEHNR Cortfication -Ciffice, ( i.e out of had, Inorwract preservallyaj out of tamp, (noarrect Dontslnars) Page :,CiiAlA4-OF-CUSTOQY 1 A�alyt��a., ., � e +�; �ii,,�': •;;,.! ; _ -��, �'=�� � � �-�-�- aceco Arralytical The Chain-&-Cucio* is a LEGAL DOWmENT.-AA rcJevam EetW moat �s pl&.cd o=rateh+. °cn 7 section Aa section c Requhad Clio -a lrh�: RagvirRd PrciW Wcone:hrt:- • - �nvoix ::•: - t No.: Section D taaM: Codes R�pghvQLiYrtl lldcrr!latiCn esattmc•r 000e Drlrk*g Wetcr DW 9 eg'- CC}LLECTEO z: PreservatiF�s Water WT Wxta Walor WW Product p compown START m enelcam (F,7 soirsoac SL SAMPLE IDVAN w ,°� U4Z 0 B 1 r1 Air AR tu K Z S mpfa of MUST aC UNi0UE- Tlwo TS O, z Other OT �t to J b it w D d.,% Z V m - _ DATE TIME DATE TIME I S m Z 2 Z 1821781 REGULATOR* AGEiidV-•; NPDEs i GROUND WATER '�` cmmuNG wA. TER r• UST F' RCRA r- QIliER 51irLot�tfon .+� = STATE ; . x Fr• �; his. FiitQTed (�YlNi. . ,•:; po.,Lm�. Pace Proled Pfol Lab LD- t : At7Dit TONAL I:OMl6�►RS ' DATFX. raw B7.1.11> YhLt f' k DA1E r � ; •'• SAMPLE CO iY01i10lt5 . .t- ;• t_ a Sheri ER NAAff 'AND VGNATURE ¢ o ORIGINAL' o Y 1 pRN1,4� ofSAhFP LER: ? S(GNaT' ^Eb15s(FFLE ? t r' �' V• n ; i;� ✓��, L'.y 4` rtl x ., i �, FM J: ti r'P, c..LYr�.. .1.�.... .y.�L.,' :i. •�.;, t! .x�:%-. , (M0.:tifT-^=�_.' .-`a _ ,. _•_ _.. �. . ,.''T' -�-.—.........w..,.-.,....,�.....�........,...............�._,...��,_,.....+...,...k..,..........,�,c.�„_..........,.....lct."...,...s,^...w.�_.....•....1....-..:K..�..,.,..r-._.,__.,„....w.._._.......w�...r,...r:-....•:�..V.a=-.4!'rw-023: ,. _ _ - _ �tC •�. evA7.. :'a•#'ay.•Y'�7 ._ .-_.., ...-,... NCDENR Stormwater Discharge Dutfall (SD®) Qualitative Monitoring Report For guidance on filling out thisform,please visit: lttr��:// �_�+raLn_cle�tr.r�r wyhjv Wtisj! tInIue";Sky#wtI-4 PermitNo.: N/C/W/`/�/_/_/_/_/ or Certificate of Coverage No.: Facility Name: Pla-t 31 I no.tom. 91.,2 County: _ _ _ 6�01C—c Phone No. a _ Inspector: AA Date of Inspection: Time of Inspection: Total Event Precipitation (inches): . V Was this a "Representative Storm Event" or "Measumable Storm Event" as defined by the permit? (See information below.) ("Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to beY performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. i 1 A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than I 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. ! A "measurable storm event" is a storm event that results in an actual discharge from the 1 permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter [ interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature ofPermittee or Designee) RECEIVED RECEIVE® MAR 13 Z014 CENTRAL FILES page 1 of 2 CENTRAL FILES swu-242, Last modified 10/25/2012 DWQISOG D1NO/BOG I. Outfall Description: Outfall No. I Structure (pipe, itc , etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (fight, medium, dark) as descriptors: n"4 _ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): A -lc,.&. 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 2 3 4 5 5. Bloating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: V 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: �p 2 3 4, 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes l o ) 10. Other Obvious Indicators of Stormwater Pollution: List and describe IJCI . Mote: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, Last modified IOJ25/2012 STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING! FORM GENERA! PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE NO. NCG14Q FACILITY NAME: Pt"; -31 Cap�4.A PERSON COLLECTING SAMPLES Mo cW3_ CERTIFIED LABORATORY_ rays Lab #— Q 1 Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: z-6 I Y - _ SAMPLING PERIOD: ❑ July -December O January -June COUNTY L,/-IL. PHONE NO. (!319 -) S.FY --?pF-7 ADD TO LISTSERVE? ❑YES ❑NO EMAIL: DISCHARGING TO CLASS: []SA ❑HQW ❑PNA ❑Trout ❑Other Outfall No. Date Sample Collected {mo/dd/yr OR NO FLOW)' PH (Standard Units) T55 {mg/L} Event Duration (minutes) Total a Rainfall (in) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier 2 2 Sampling - - 6-92 100Z a 71 �l 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. z If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit, Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/l. `For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outfall No. Date Sample Collected (mo/dd/yr)1 pH (Standard Units} TPH using method 1664A SGT-HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total Rainfalla (in) New Motor Oil Usage (gal/month) 2 Tier In InTier# Monthly Monitoring? Wri) of Months in Tier 2 z Sampling 6-92 15z 1002,3 - - - - - HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO [� HAVE YOU CONTACTED THE REGION? YES []NO ❑ REGIONAL OFFICE CONTACT NAME: Mail Original and one coDv of this DMR (including all "No Flow" & "No Discharge" renorts) within 30 days of receipt of sample (or at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 3r3�1 (Signatur of Permittee) (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 aceAnalytical www.pacefaffscom MD Capps Ready Mix Concrete PO Box 27326 Raleigh, NC 27611 Project: PLANT #31 Pace Project No.: 92192352 Sample: OUTFALL 1 Parameters Total Suspended Solids Reviewed by: `- Nikitia Jones -Jackson nikitia.jones@pacelabs.com Laboratory Report Lab ID: 92192352001 Collected: 03/03/14 12:25 Results Units Report Limit Analyzed 9.8 mg/L 2.6 03/10/14 20:00 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 Page 1 of 1 Report Date: 03/11/2014 Date Received: 03107/2014 Matrix: Water Qualifiers North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Urginia/VELAP Certification #: 460222 Page 1 of 3 1Y. ccAnalytical Chain of Custody lqz .5s�Z-- Report Results to: Bill Results to: E standard Report Delivery Ready Mixed Concrete Ready Mixed Concrete Rush Report Delivery (w/ surcharge) P.O.Box 27326 P.O.Box 27326 Requested Due Date: Raleigh, NC 27611 Raleigh, NC 27611 Y)lb Gapes Project Reference: Plants #31 ATTN: IgbA WWWOR ATTN: Je44-W450" Purchase Order #: Phone: 919-790-1520 cja5 w4" Sampled By: Mb(�Dna _ SampeaDese an :,Or1%ostt M.'�..-.L"-�.�•' a� - '.fe .?u:..lhr+c.. ' j Q1i3vr.OY W"21 .`D �' .'P t. ���i[� .. '1 stop'' E3 ,:' i[]I �...... Dy� VLu_- a= 70-4 }.^ a ,.rtw :_1 • ' nail .�sr a Lueted IT `s-,'i� 1f, pc�13. I '.'c�°=5—�+•i�. - Outfall 1 G -3` 311y 2-Zt- JL- Sw TSS S�utfaliZ- G Sw TSS 3elinquished by (signature) Rec iced sig ture D e Time For Lab Use Only Temperature at receipt: Temp-. C` telinquished signature) Received by (signat e) D e Time lellnquished by (signature) Received by(signature) Date Time a N Document Name: Sample Cond€lion Upon Document Revised: April 04, 2013 �E ArralyFlc�l. Receipt (SCUR) ___Page IV 2 Document No,: Issuing Authorities: F-R L-CS-00i-rev:02 Pace Asheville Quality Otftce Client lame:. 1 Where Received: ❑ Iluntersville ❑ Asheville ❑ Eden Raleigh Courier (C€rcle): Fed Ex UPS USPS C[len Commercial pace. Other Custody Seal on CoalerlBox Present: yes .' no Seals,intact „�1 yes ❑ no Packing Material Bubble Wrap s None Other Circle Thermometer Used: IR Gun N:122065387Type of Ice: Wet Blue .None Samples on ice, cooling process has begun IR Gun B P 371. Temp Correction Factor: Add/ ubtract, Corrected Coo ierTamlr.: C . Temp. should be above freezing to 6°C La C Date and Initials of person examining co to Pre ry ' •Blological Tissue is Froz@n:..Yes N NIA check: Comments: . Ch21nt)T'C"stOd .Present:..., . _.-_.'. ... Yes:❑Ho' '..f�YfA 1:...:.__.,_..-_._r...:-......._...-.- _..;..:.. _-._.. .. ... ,,.....,.._ ...._. Chain of Custod�Fil€ed Out: Yes -.❑No .ONlA 2., Cha€6_bf Custod Relinquished: Yes :❑No ❑N1A- 3. Sampler Name & Sl nature on COCi No Yeg ON..' ❑NIA 4.' Sam les Arrived Wthin Hold Time:.. - Yes ❑No' ❑NIA 5.: Short Hold Time Ania1) sfs <72hr): []Yes o ❑NIA 6_ Rush T,urn,Around-Tline Requested: 171Ye5 116. ❑NIA 7.. Sufficlent_Volume: , .IYes ❑No ❑NIA Correct ConWners-Used: -Pace Containers Used: Yes . ❑l`io Yes- ❑No ©WA ❑N11A 9.. Contalners rntact Yes 0No ' ❑NIA 10. Filtered volurrle:recefved.for Dissolved tests ❑Yes ON. NIA 11, Sample Labeis.match COC:• . -Includes dateltimeliDlAnalys€s Matrix: Yes ONo ©NIA 12.. All contalnem needing'preservatfon have been checked. All contafn 'rs needing preservation are found to be In compliance with EPA recommendation. exceptions VOA, goliform, TOC, O&G, VJI-SRO (water) - III r is es ❑No as ❑iJo xy Yes ONo C]N!A ❑NIA 73. Samples checked for dechlor€nation: Yes ❑No ❑NIA 14, Headspace in VOA Vials ( >.6mm : ❑Yes ❑No NIA 15, Trip Blank Present Tr€p Blank Custody Seals Present _ Pace Trip Blank Lot # (if purchased): 'ElYes ❑No ❑Yes ❑No __ X!NfA - f NIA r 16: Client NotI%Dat1on7 Resoiutlon: Field Date Required? Y 1 N Person Contacted: DatelTlme: Commentsl Resolution: SCURF JSRF pate~ Place label here f J r � 'Review:: - // j`__� Note: Whenever there is a discrepancy affecting North Carolina compliance W®# I ' 92192j 52 Samples, a copy of this form will be sent to the North Carolina DEHNR I Certification Office (i.e out of hold, Incorrect preservative, out of temp, incorrect contaihers) I I I • � 821 33 Page 3 of 3