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HomeMy WebLinkAboutNCG140129_MONITORING INFO_20190125STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. y C) DOC TYPE HISTORICAL FILE Q, MONITORING REPORTS DOC DATE ❑ G���I�1°�� YYYYMMDD l mkonrnental QuQllry Stormwater Discharge Outfall (SDO) Qualitative Monitoring Deport For guidance on filling out this form, please visit https://deg.nc.rov/about/divisions/energy-mineral-land- resources/energy„mineral-land hermits/stormwater-permits/npdes-industrial-sw#tab-4 Permit No.: NICI^I_I_I 1_I_I_I or Certificate of Coverage No.: N/C/GI /1 al /l Zlgl Facility Name: County: Phone No. Cj r C(— 5({ 4 -{6 Z 7 Inspector: Date of Inspection: Time of Inspection: " - CENTRAL i=11 rS Total Event Precipitation (inches): Cjy pVfR SECTION All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature ePeftnittee or Designee) 1. Outfall Description: Outfall No. Structure (pipe,< tc etc.): Receiving Stream: the industrial activities that occur within the outfall drainage area: 1 . -k t . i Pagel of 2 U 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: _ C1 Par 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 06 U-z 4. Clarity: Choose the number which best describes the clarity of the discharge, where l is clear and 5 is very cloudy: l% 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? Q Yes 0- 8. Is there an oil sheen in the stormwater discharge? ©Yes 0 0. 9. Is there evidence of erosion or deposition at the outfall? O Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may he indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 TABLE 9:1 ANA_LYTICAL MONITORING'REQUIREMENTS-STORMWATER READY MIXED CONCRETE COMPANY - PLANT # DISCHARGE UNITS. BENCHMARK. SAMPLE SAMPLING CHARACTERISTIC VALUES LOCATION SCHEDULE pH Standard Within range 6.0 to 9.0 , Each Outfall Semi -Annually Total Suspended Solids (TSS) mg/L 100 mg/L2 Each Outfall' Semi -Annually Total Petroleum Hydrocarbons mg/L 15 mg/L Each Outfail' Semi -Annually Event Duration Minutes Not applicable Each Outfall' Semi -Annually Total Rainfall Inches Not applicable Each Outfall' Semi -Annually New Motor Oil Usage3 Gallons/ Month Not applicable Not applicable Semi -Annually Notes: 1. Samples shall be collected at each stormwater discharge outfail unless representative outfall status has been granted and documented by the Division of Water Quality. A copy of the letter granting representative outfall status shall be kept on site. 2. TSS benchmark for ORW, HWQ, Trout or PNA waters is 50 mg/L. 3. Only required for sites where vehicle maintenance activities occur. 4. All samples must be grab samples. Grab samples shall be collected within the first 30 minutes of discharge from a stormwater discharge outfall (SDO). 5. All samples must be collected during a measurable storm event. A measurable storm event is an event that results in an actual discharge from the permitted site outfalls. The previous measurable storm event must have been at least 72 hours prior. If no discharge occurs during a sampling period, a monitoring report indicating "No Flow" must be submitted within 30-days of the sampling period. 6. For each sampled measurable storm event the total precipitation must be recorded using an on -site rain gauge. 7. The permittee shall complete the analytical samplings in accordance with the schedule specified above, unless adverse weather conditions prevent sample collection. Inability to sample due to adverse weather conditions must be documented in the SPPP and reported on the appropriate DMR form (Appendix A). 8. A minimum of 60 days must separate each monitoring event unless monthly monitoring has been instituted under a Tier Two response 9. The permittee shall compare monitoring results to the above -referenced benchmark values for each discharge characteristic. Exceedances of benchmark values require the permittee to increase monitoring, increase management actions, increase record keeping, and/or install stormwater Best Management Practices (BMPs) in a tiered program, as specified by the general permit. 10. Failure to monitor semi-annually per permit terms immediately institutes monthly monitoring for all stormwater parameters. After six months of monthly monitoring, the permitee may make a request in writing to the Division of Water Quality to return to a semi-annual monitoring schedule. w STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE No. NCG14 0 1 FACILITY NAME: p 3 PERSON COLLECTING SAMPLE LW�i Fz'� CERTIFIED LABORATORY Lab # Lab # OPTIONAL INFO: Part A. Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: 2ol e) SAMPLING PERIOD: ❑ July -December ® January -June COUNTY U 0� PHONE N0. i�J 5`I4-f 6= ADD TO LISTSERVE? []YES ❑NO EMAIL: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trout []Other Outfall No. Date Sample Collected (mo/dd/yr OR NO FLOW)1 pH (Standard Units) TSS (mg/L) Event Duration (minutes) Total , Rainfall (in) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier 2 Sampling2 - - 6-92 1002, -15 I t ! • So AJ 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfail here. Please make sure to mark the sample period above. 2 if a value is In excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/l, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/I. A for each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date:7/1/2011-60/30/2015 I Last Revised 7/13/11 Page 1 of 2 Date of last pH meter calibration: Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar Year. Outfall No. Date Sample Collected jmo/dd/yr)F pH (Standard Units) TPH using method 1664A SGT-HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total Rainfalla (in) New Motor Oil Usage (gal/month) Month) In Tier 2 y i Monitoring? (y/n) # of Months in Tier 2 Sampling2 6-9 is 2.100 ' - - - - I HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO HAVE YOU CONTACTED THE REGION? YES [ NO [] REGIONAL OFFICE CONTACT NAME: Maii Original and one coon of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample (or at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS_CERTIFlG4TIQl fQR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of i/2s/r (Date) Permit Date: 7/1/2011-60/30/2D15 Last Revised 7/13/11 Page 2 of 2 TABLE 9.2 ANALYTICAL MONITORING REQUIREMENTS.=PROCESS WASTEWATER READY MIXED CONCRETE COMPANY PLANT # DISCHARGE EFFLUENT SAMPLE SAMPLING CHARACTERISTIC UNITS LIMITATIONS LOCATION SCHEDULE pH Standard 6.0 — 9.0' Each Outfal12 Quarterly Total Suspended Solids (TSS) mg/L 30 mg/L3 Each Outfallz Quarterly Settleable Solids mL/L 5 mL/L Each Outfa112 Quarterly Total Petroleum Hydrocarbons4 mg/L 15 mg/L Each Outfa112 Quarterly Event Duration Minutes Not applicable Each Outfallz Quarterly FIow5 Gallons/Day Not applicable Each Outfall2 Quarterly New Motor Oil Usage4 Gallons/ Month Not applicable Not applicable Quarterly Total Volume of Wastewater Not applicable 50% of summer Not Applicable Quarterly Discharged (HOW) 7Q10 Flow Notes: 1. pH range for saltwaters is 6.8 — 8.5. 2. Samples shall be collected at each process wastewater outfall during a discharge event. 3. TSS effluent limitation HQW is 20 mg/L and 10 mg/L for Trout or PNA waters. 4. Only required for sites where vehicle maintenance activities occur and process wastewater commingles with stormwater. 5. Flow may be measured continuously or calculated. 6. See 15A NCAC 02B .0224 and general permit for explanation. 7. All samples must be grab samples. Grab samples shall be collected within the first 30 minutes of discharge from a process wastewater outfall. 8. If no discharge occurs during a sampling period, record "No Flow" or "No Discharge" within 30-days of the end of the sampling period and file with SPPP. 9. Commingled discharges must be collected during a measurable storm event. A measurable storm event is an event that results in an actual discharge from the permitted site outfalls. The previous measurable storm event must have been at least 72 hours prior. 10. For each sampled measurable storm event the total precipitation must be recorded using an on -site rain gauge. 11. The permittee shall complete the analytical samplings in accordance with the schedule specified above, unless adverse weather conditions prevent sample collection. Inability to sample due to adverse weather conditions must be documented in the SPPP and reported on the appropriate DMR form (Appendix A). 12. For commingled discharges, a minimum of 60 days must separate each monitoring event unless monthly monitoring has been instituted Under a Tier Two response 13. The permittee shall compare monitoring results to the above -referenced effluent limitations for each discharge. characteristic. Exceedances of effluent limitations will result in a violation of permit conditions and may be subject to enforcement. 14. Failure to monitor process wastewater quarterly per permit terms immediately institutes monthly monitoring for all parameters. After six months of monthly monitoring, the permitee may make a request in writing to the Division of Water Quality to return to a quarterly monitoring schedule. IceAnalytical (� w�rw.PeCelab3.00m November. 16, 2018 Jay Watkins Ready Mix Concrete 3610 Bush Street Raleigh, NC 27609 RE: Project: Plant 17 #1 Pace Project No.: 92407103 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Jay Watkins: Enclosed are the analytical results for sample(s) received by the laboratory on November 13, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 8 Pace Anaiytical Services, LLC 9800 100 aceAnalj cal neyAve. Suite Huntersville, NC 28078 788 www pacelabs.com (704)875-9092 CERTIFICATIONS Project: Plant 17 #1 Pace Project No.: 92407103 Eden Certification IDS 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certifcation #: 633 North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shatl not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 8 Pace Analytical Services, LLC aceAnalytical ® 98a0 Kincey Ave. Suite 100 Huntersville, NC 28078 wwwpecelabs.own (704)875-9092 SAMPLE ANALYTE COUNT Project: Plant 17 #1 Pace Project No.: 92407103 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92407103001 Plant 17 #1 SM 254OD-2011 SOB 1 PASI-E REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 8 aceAnalytical www.pacalabs.com le ANALYTICAL RESULTS Project: Plant 17 #1 Pace Project No.: 92407103 Pace Analytical Services; LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Plant 17 #1 Lab ID: 92407103001 Collected: 11/12/18 14:30 Received: 11/13/18 12:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 85.1 mg1L 4.0 1 11/14/18 14:30 Date: 11/16/2018 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 4 of 8 aceAnalytical www.pacalabs.wm Il Project: Plant 17 41 Pace Project No.: 92407103 QUALITY CONTROL DATA QC Batch: 442315 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2WD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92407103001 METHOD BLANK: 2427917 Associated Lab Samples: 92407103001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 2427918 Parameter Units Total Suspended Solids mg/L 4 SAMPLE DUPLICATE: 2427919 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2427920 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers N❑ 2.5 11114/18 14:27 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 236 94 90-110 92406957003 Dup Result Result 9.8 11.4 92406957004 Dup Result Result ND ND RPD Qualifiers 15 D6 RPD Qualifiers ` Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11/1612018 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 8 r,. aceAnalytical www..peoelabs.com QUALIFIERS Project: Plant 17 #1 Pace Project No.: 92407103 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilfe, NC 26078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. POL - Practical 0uantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-E)iphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. 110-101;7_AI[*]V11*1 PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/16/2018 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 8 aceAnalytical w+vw.pac�latu.00m Project: Plant 17 #1 Pace Project No.: 92407103 Lab ID Sample ID 92407103001 Plant 17 #1 Date: 11/16/2018 09:16 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE QC Batch Method QC Batch Analytical Method SM 254OD-2011 442315 4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch Page 7 of 8 0 _ ro 'Ole w I � OWN -OF -CUSTODY lftt ,1 !' --�► CM6-aFCw w*FIs aLw uDQOAwff -C TO*" macarw+ce er+ec y 92407103". •rA+aa Ca�akrrPtispwtlre •" �y- �, ,scoots Att5 F.- Ta "s,.,...a.. w .xwn..,.�cwawlr��+ •r4 ulseau.> w,ac.w.� 10-16-��t PJJ Y.o.P—.aL(a1 dtQ 'lN tliisplc add.(�reiwia+a wfita. CaMT4r 2M C949COW Ltld•WdtWW - -PJVRMlIia�.•- K�.\%li ]4�:'1-'�'i:.i:�}".•�+SaFr.- 1 �djeRKa�%lY bef suit ca~Qtr. 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(SrpssnraJ DasURam _ � 'f n..... �+' Enyironmen tal Quality Stormwater Discharge Outfall (SD®) Qualitative Monitoring Report For guidance on filling out this forni, please visit hUs:Hdcq.ne.gov/about/divisions/energy-mineral-]and- resources/energy-mineral-land pernvts/stomiwater-permits/npdes-industrial-sw#tab-4 Permit No.: NIG_l�l�l I I I I or Certificate of Coverage No.: NIC/G111�1 �1I ZI1 Facility Name: 3 -Z- �T County: Z),t(-k A— Phone No. q j Q - 54 4 -16 Z 7 Inspector: O-e4 r r- Date of Inspection: Time of Inspection: d,9.3 Total Event Precipitation (inches): 5 L> CENTRAL F"ES OWR SECTION ! All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature SfPefinittee or Designee) 1. Outfall Description: Outfall No. I Structure (pipe itc tc.): Receiving Stream: Describe the industrial activities that o within the outfaIl drainage area: �fa�i mt� Caxrt,,4 Page] of 2 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: (1 trY 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): N v' 4. Clarity, : Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 23 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 6) 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: IP 2 3 4 5 7. Is there any foam in the stormwater discharge? Q Yes ( 'N0. 8. Is there an oil sheen in the stormwater discharge? QYes al o. 9. Is there evidence of erosion or deposition at the outfall? o Yes *No. 10.• Other Obvious Indicators of Stormwater Pollution: List and describe Moov' Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 TABLE 9:1 ANALYTICAL MONITORING REQUIREMENTS-S_TORMWATER READY MIXED CONCRETE COMPANY -- PLANT # DISCHARGE UNITS BENCHMARK SAMPLE SAMPLING CHARACTERISTIC VALUES LOCATION SCHEDULE pH Standard Within range 6.0 to 9.0 Each Outfall' Semi -Annually Total Suspended Solids (TSS) mg/L 100 mg/L2 Each Outfall' Semi -Annually Total Petroleum Hydrocarbons3 mg/L 15 mg/L Each Outfall' Semi -Annually Event Duration Minutes Not applicable Each Outfall' Semi -Annually Total Rainfall Inches Not applicable Each Outfall' Semi -Annually New Motor Oil Usage Gallons/ Month Not applicable Not applicable Semi -Annually Notes: 1. Samples shall be collected at each stormwater discharge outfall unless representative outfall status has been granted and documented by the Division of Water Quality. A copy of the letter granting representative outfall status shall be kept on site. 2. TSS benchmark for ORW, HWQ, Trout or PNA waters is 50 mg/L. 3. Only required for sites where vehicle maintenance activities occur. 4. All samples must be grab samples. Grab samples shall be collected within the first 30 minutes of discharge from a stormwater discharge outfall (SDO). 5. All samples must be collected during a measurable storm event. A measurable storm event is an event that results in an actual discharge from the permitted site outfalls. The previous measurable storm event must have been at least 72 hours prior. If no discharge occurs during a sampling period, a monitoring report indicating "No Flow" must be submitted within 30-days of the sampling period. 6. For each sampled measurable storm event the total precipitation must be recorded using an on -site rain gauge. 7. The permittee shall complete the analytical samplings in accordance with the schedule specified above, unless adverse weather conditions prevent sample collection. Inability to sample due to adverse weather conditions must be documented in the SPPP and reported on the appropriate DMR form (Appendix A). 8. A minimum of 60 days must separate each monitoring event unless monthly monitoring has been instituted under a Tier Two response 9. The permittee shall compare monitoring results to the above -referenced benchmark values for each discharge characteristic. Exceedances of benchmark values require the permittee to increase monitoring, increase management actions, increase record keeping, and/or install stormwater Best Management Practices (BMPs) in a tiered program, as specified by the general permit. 10. Failure to monitor semi-annually per permit terms immediately institutes monthly monitoring for all stormwater parameters. After six months of monthly monitoring, the permitee may make a request in writing to the Division of Water Quality to return to a semi-annual monitoring schedule. STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE N0. NCG14_t�1 2 FACILITY NAME: 1" W�_ 1 q',-.3 4WU 51�_ PERSON COLLECTING SAMPLES r CERTIFIED LABORATORY Lab # Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR. ZQ ) g I SAMPLING PERIOD: 9 July -December ❑ January -June COUNTY . JI L,�f PHONE NO. ) ADD TO LISTSERVE? ❑YES ❑NO EMAIL: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trout ❑Other Outfall No. Date Sample Collected ( mo/dd/yr OR NO FLOW)1 PH {standard Units) TSS lmg/L) Event Duration (minutes) Total 3 Rainfall (in) In Tier 2 Monthly Monitoring.? (y/n) # of Months in Tier t 2 Sampling - - 6-9 1002, - - Jlzs S 1 0 TO s 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfail here. Please make sure to mark the sample period above. 2 If a value is In excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/l. `For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page i of 2 Date of last pH meter calibration: ///ZL,(9 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gat of new motor oil/month — averaged over a calendar year. Outfall No, Date Sample Collected (mo/dd/yr)' PH (Standard Units) TPH using method 1664A SGT=HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total Rainfall' (in) New Motor Oil Usage (gal/month) In Tier 2 Monthly Monitoring? (y/n) it of Months in Tier 2 2 Sampling 6-9 15 100 ' - - - - I HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO HAVE YOU CONTACTED THE REGION? YES []NO ❑ REGIONAL OFFICE CONTACT NAME: Mail Original and one copy of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample for at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION f013_ANY INFORMATION RiEPORTEA: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significapt penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit Date: 7/1/2011-60/30/2015 (Date) Last Revised 7/13/11 Page 2 of 2 TABLE 9.2 ANALYTICAL MONITORING REQUIREMENTS -PROCESS WASTEWATER . READY MIXED CONCRETE COMPANY —PLANT # DISCHARGE EFFLUENT SAMPLE SAMPLING CHARACTERISTIC UNITS LIMITATIONS LOCATION SCHEDULE pH Standard 6.0 — 9.0' Each Outfallz Quarterly Total Suspended Solids (TSS) mg/L 30 mg/L3 Each Outfal12 Quarterly Settleable Solids mUL 5 mUL Each Outfa,12 Quarterly Total Petroleum Hydrocarbons4 mg1L 15 mg/L Each Outfalh Quarterly Event Duration Minutes Not applicable Each Outfal12 Quarterly Flow$ Gallons/Day Not applicable Each Outfailz Quarterly New Motor Oil Usage Gallons/ Month Not applicable Not applicable Quarterly Total Volume of Wastewater Not applicable 50% of summer Not Applicable Quarterly Discharged (HQW) 7010 Flow Notes: 1. pH range for saltwaters is 6.8 — 8.5. 2. Samples shall be collected at each process wastewater outfall during a discharge event. 3. TSS effluent limitation HQW is 20 mg/L and 10 mg/L for Trout or PNA waters. 4. Only required for sites where vehicle maintenance activities occur and process wastewater commingles with stormwater. 5. Flow may be measured continuously or calculated. 6. See 15A NCAC 02B .0224 and general permit for explanation. 7. All samples must be grab samples. Grab samples shall be collected within the first 30 minutes of discharge from a process wastewater outfall. 8. If no discharge occurs during a sampling period, record "No Flow" or "No Discharge" within 30-days of the end of the sampling period and file with SPPP. 9. Commingled discharges must be collected during a measurable storm event. A measurable storm event is an event that results in an actual discharge from the permitted site outfalls. The previous measurable storm event must have been at least 72 hours prior. 10. For each sampled measurable storm event the total precipitation must be recorded using an on -site rain gauge. 11. The permittee shall complete the analytical samplings in accordance with the schedule specified above, unless adverse weather conditions prevent sample collection. Inability to sample due to adverse weather conditions must be documented in the SPPP and reported on the appropriate DMR form (Appendix A). 12. For commingled discharges, a minimum of 60 days must separate each monitoring event unless monthly monitoring has been instituted under a Tier Two response 13. The permittee shall compare monitoring results to the above -referenced effluent limitations for each discharge characteristic. Exceedances of effluent limitations will result in a violation of permit conditions and may be subject to enforcement. 14. Failure to monitor process wastewater quarterly per permit terms immediately institutes monthly monitoring for all parameters. After six months of monthly monitoring, the permitee may make a request in writing to the Division of Water Quality to return to a quarterly monitoring schedule. 0 co IV ca a. CH1U" CIWO V Analytical Request Document r aw..r<�wl:.srw�coowl�r•c..u�lnwc • 92407103 • [ Y' Z.M1 �+ ' nib �� �J�� �� T � LwdTa: ^ wv.awilva W .rrVc r�4 RJ+.a.ne+dd. W I,Ar.R4rt.�0.4U>osaa• Igatedil. W mc+l.4t.. � � lil+,.e,.el iS rdwn tLltrt, pDw3r,tMowifan. (iLtim�a W gtarbic.d4 k0arvd+..waha. bww�w. �.rd�at:h l7f7v,M u.waYwd.P�1O� Caq"TO: SksIMgIAdWesa: CIOtOtnv Ptcl.aM Siatc Safi hof Zen. [ 1►r ( 1 trT 1 1 � I I !r f�rti �_. ':'��,.,_"+ .+ri �,' `r_q7 i=_•r ]I �o- `,� �.if � , i-a rl=`�s�n'.� •r~)- a �`. a't; t!a. h11Et. � sylbr!�'t�.•' ��+`'_::'' Pt+crx:, ; 9tglFadlty 1p a: Ca�.t+Mwd�7 Fnu1L R�yf 'l{S (per 1 I rc (I No �•� � c� d.4 r�c°`r l at Y`S)�• `� _ � � L ,$r�i"''•%'ss 'tM'• .t4 `" QAwcgmd ow (Pam. 1 Pu,3na.(ldw F. Dri Pws iD St.Spa` QxKe1! DW LocatW"Cady--gel.- - ,� q"Isq�m.e ' Tunwrpnd Coo Pv, ' [ • ] r.s [ 1 � � ' Y . 2ti j7:• � •' 'sip' y , - Un Via Dnposae R-adL• FWU caa"sd (d oppGaa *. J%I -. . =-^ . - ...v... ts [ S Puce a -ow-PALL.l 1.er.a L 1 /ww.: [ 1 S. ENV 1 1 r� MY 1 I l DP,r ( 1 3 out' 1 1 I:V,r L 15 DAY°6"..i 1. I T- 1 I no 1,{*; i ".' �i,,. �,. i llMwa: (IfptlbWarpsApp,•J ,fir. �' '�. £ '` .- ' ! �•`s"ate-yf�.�+f " 5`'; "M=UCodn OMoc%mMnubCmb.k—)!h6ddt�Watcr laW]Growd Water IGWL W"Cwr"(Ww► PmduG PL SA5WN CQ OLI. W Air TIMM (eL VaPw M OUW CI} ( LSLL I w{WP'L WIL i�Le�+aT I F - ,q lk � C-i` ai..- r.• Wsinn.r ID SarttPle MMIc• C Grab GrabomPd ! Cer.R.d CP[� 4 Cart,Padltf fnd -Iles Sol d:w CV,s •., t. �.-., : ,'l'V, S ' ::.�, Y Dam'- ::,skns w Date�. Tkne ' -7,'t:i �:�5 �, t' _i�,�'!j'.''ri+C+tv"'°• "P,.�ILS'�`',•],J::"':w^.�` L»�r-r 'A:l. `�a 'i1.I x�CRY )S!+ir•J:"'�:''.^'Li')ii`i, :.,tH � i' ,i. �`� .eW. :Yd��'�-4�'rof2r�y:;eyi.7"`.`.:a-�•>,ec'-f�``':i?�:�:!S C h:SS . y-• ef.,! t� _ i �}:'rr::'°�'.L. ''� 'Arw"s•�^ Lr:si:�ef'•Iw Qnton,.r,a.m.dslSp.d,.l CE+SdRaSalPmalb1. 11.4"17s: �"r1!!�F. -::�!!!'q•:"�S;r:N4l1S�.'Liti:�,: .HOtl%Slti�M�#�j"tia✓il `�"hKi?J!UASisZ';�u`., Cali YWnWAilwie"INo.:-=�'^ I,••:;"-�. _ _°r�i�,:. Psd3P�}!b[ayl��' y �� i r°"; t� �c�,'� '-� � ,�}�`S` �') tom.=� ^/ice 5y/�;�?�/y4�:�/'1.�L�{ �:` a r i'tiu 5.1 '�'iT .�� •r. ' e��M" �i _IIF}.i] rar ,G � 4 :�.- l Y. 'Ar•,?.%L��I' VS.ri' 4 t...v4K. '.S."k. 1.�V-if� )�ri(�WC(i'ItxTD��.nR�Pt a�b _+ai:pkk ::5„4i. •N'r ;'s�Ex�- .i. "r: v-.Catit"4'tx. itta•L�I�ge;��`, y ,;`tlxm, r J . i- " .v. ReAnuuh+ed Ml�co�nafxrr• is�oueue] Datens t]ma��:MY1CtXH'InEOxllfi- A'. t il'cQ �'r...Y •.G... ter... r[P" ,-r --'� »s4'afr`�� �'' bYlCanPr1Y•�I,aC] ITatNTi+c M[eired lfy(Cm,pa+rr 1 OaoeJlLne: i�1�Y'"; �? - _.-..�. ••'• •• ✓:,.- 'ter , , ti:: _ A. H•..a:�.--.1:: fiinr5`a. -7�'Crb!•vi�-� �'--c��•"..YT•'•n: v�,�`�'' _+� y D11Yy.•�Y-.: �F.,rY.`1;'J.s•�:tir.�.17 ... _ .:... �. ndtgutn.der/cnmw.rl•l nutslr�.: +tacorea4vlca�+r.lsa'r�n.s7 DaLe/ThaC: le AnalXical www.pacelabs.= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersvOle, NC 28078 (704)875-9092 November 16, 2018 Jay Watkins Ready Mix Concrete 3610 Bush Street Raleigh, NC 27609 RE: Project: Plant 17 #1 Pace Project No.: 92407103 Dear Jay Watkins: Enclosed are the analytical results for sample(s) received by the laboratory on November 13, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, (b*a' `-hi . `-� Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 8 e (�5aneAnalytical wwwpacelab&mn CERTIFICATIONS Project: Plant 17 #1 Pace Project No.: 92407103 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 (704)B75-9092 Page 2 of 8 aceAnaIXical www.pecelabs.wrn r Project: Plant 17 #1 Pace Project No,: 92407103 SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 {704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92407103001 Plant 17 #1 SM 254OD-2011 SOB 1 PASI-E REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Anatytical Services, LLC. Page 3 of 8 aceAnaiXicais xwwpacafabs.can ANALYTICAL RESULTS Project: Plant 17 #1 Pace Project No.: 92407103 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Plant 17 #1 Lab liD: 92407103001 Collected: 11112/18 14:30 Received: 11/13/18 12:45 Matrix; Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 85.1 mg1L 4.0 1 11/14/18 14:30 Date: 11/16/2018 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 8 e aceAnalytical wwwparBlabs.mm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huniersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Plant 17 #1 Pace Project No.: 92407103 QC Batch: 442315 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92407103001 METHOD BLANK: 2427917 Matrix: Water Associated Lab Samples: 92407103001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 11/14/18 14:27 LABORATORY CONTROL SAMPLE: 2427918 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 236 94 90-110 SAMPLE DUPLICATE: 2427919 92406957003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 9.8 11.4 15 D6 SAMPLE DUPLICATE: 2427920 92406957004 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 11/16/2018 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 8 axAnalytical wwvrpacelebs.com QUALIFIERS Project: Plant 17 #1 Pace Project No.: 92407103 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. POL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyz ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyze is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute, LABORATORIES PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /16/2018 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 8 aceAnalytical www.paceJsbs.com Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 {704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Plant 17 #1 Pace Project No.: 92407103 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92407103001 Plant 17 #1 SM 2540D-2011 442315 Date: 11/16/2018 09:16 AM y REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, exoepi in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 8 .j STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE NO. NCG14 n t Z FACILITY NAME: 4-wow 65 4F 11 PERSON COLLECTING SAMPLES F CERTIFIED LABORATORY Lab # 9— Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: 20 r) SAMPLING PERIOD: ® July -December ❑ January -June COUNTY bo,( A PHONE NO. ( ) ADD TO LISTSERVE? ❑YES ❑NO EMAIL: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trout ❑Other Outfall No. Date Sample Collected tmo/dd/yr OR NO FLOW) pH (standard units) TSS (mg/L) truant Duration (minutes) Total a Rainfall (in) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier 2 Samplingl - - 6-9 100 ' - - - t V _U il-ow — Z-4 H 71-5 5e, C 'I RAL FUS u "K z5tu I lunj i 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. If a value is In excess of the benchmark, or outside the benchmark range ifor pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until consecutive samples are below the benchmark or within the benchmark range. ' T55 benchmark values are 100 mg/I, except when dischafging to ORW, HQW, Trout, and PNA waters where they are 50 mg/I, For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date; 7/1/2011-60/30/2015 I Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outfall No. Date Sample Collected Imo/dd/yr)' pH (Standard Units) TPH using method 1654ASGT-HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total a Rainfall (in) New Motor Oil Usage (gal/month) In liar 2 Monthly Monitoring? (y/n) 11 of Months in Tier 2 Sampiine 6-9 is 100 ' - , I HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO HAVE YOU CONTACTED THE REGION? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAIVE: Mail Original and one coon of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample for at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FQR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." NYw 4-L� 7-11.1 1 Q, (Signature of Per ittee) (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 �i�� NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http-//nortai.ncdenr org/we-/wq/ws/su/nndessw#tab-4 Permit No.: hl/.C/_ Facility Name: I County: _ burw Inspector: Date of inspection. Time of Inspection: Total Event Precipitation (inches)- or Certificate of Coverage No.: h/C/-G/L 1VA-1L/2/V Phone No. - W o >r 64A Was this a "Representative Storm Event" or "Measureable Storm Event' as defined by the permit? (See information below.) ❑ Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to he performed during a "representative storm event" or during a "measureable storm event" However, some permits do not have this requirement Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee ! obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signaturbofi�ermittee or Designee) Pagel of 2 SWU-242, LastmodJRed 10/25/2012 Ne Otw far Zpa HAWW- 2017 1. Outfall Description: Outfall No. Z Structure (pip , di c , etc.) Receiving Stream: Describe the i dustrial activities that occur within the outfall drainage area: lI eixw M" t"A Ak'u r%. 4�p 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, Last modified 10/25/2012 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. http:./,IpQIUI,ucdel]r.org/3yeb.4wA4ws/su/npdes!,w#tab-4 Permit No.: N/- /_/-/-/_/-J-J_/ or Certificate of Coverage No.: hilCIfil afb-/J Z)v Facility Name: pl om-r 01 55 - County: 3k.r16&" -- Phone No. - 644 - ib a I Inspector ` F uw 4 Date ofInspectoo . _iZ IZA 11 7 _ Time of Inspection: 1,25 Pr` - Total Event Precipitation (inches): • 50 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or `measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event" However, some permits do not have this requirement Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event' Is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee L obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: of Permittee or Designee) Pagel of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. I Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): K)ata$ 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: Q 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 (P 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 7. a. 1 9) 3 Is there any foam in the stormwater discharge? 4 5 Yes Is there an oil sheen in the stormwater discharge? Yes No a 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stonnwater Pollution: List and describe MQW Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, Last modified 10/25/2012 ac0nalytical r wm Pmainbs.cam December 27, 2017 Jay Watkins Ready Mix Concrete 3610 Bush Street Raleigh, NC 27609 RE: Project: Plant 17 HWY 55 Pace Project No.: 92368000 Pace Analytical Services, LLC 991O KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Jay Watkins: Enclosed are the analytical results for sample(s) received by the laboratory on December 21, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me_ Sincerely, 01*0., " Angela Baloni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. U.C. Page 1 of 10 Pace Analytical Services, LLC Iac) eAnalyticaf® 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 wompficalabrMcom i704j875-9092 CERTIFICATIONS Project: Plant 17 HWY 55 Pace Project No.: 92368000 Eden CeWfication IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Ddnking Water Certification #: 37738 VirginiaNELAP Certification M 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent or Pace Analytical Services, LLC, Page 2 of 10 Pace Analytical Services, LLC aceAmIXical a e800 K ntar Ave. Suite 100 Huntensviiie, NC 2807$ wwwPI0gh 6G" (704)BT5-9092 SAMPLE ANALYTE COUNT Project: Plant 17 HWY 55 Pace Project No.: 92368000 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92368000001 Outfal1 #1 Plant 17 SM 2540D NMIi 1 PASI-E REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 10 aceAnalytical wiw:pzowaft.cam ANALYTICAL RESULTS Pace Analytical Servlces, LLC 9800 Kincey Ave. Sulte 100 Huntersvine. NC 28078 (704)875-9092 Project: Plant 17 HWY 55 Pace Project No.: 92388000 Samplo: Outfall #1 Plant 17 Lab ID: 92368000001 Collected: 12120117 15:30 Received: 12/21/17 14:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 2540D Total Suspended Solids Total Suspended Solids Dale: 1212712017 09:32 AM Analytical Method: SM 2540D 71.5 mg1L 5.2 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, with,out the written consent of Pace Analytical Services, I.L.C. 12/22/17 14:23 Page 4 of 10 gWnalytical www.peoakbs,com QUALITY CONTROL DATA Project: Plant 17 HWY 55 Pace Project No.: 92368000 QC Batch: 392150 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92368000001 METHODBLANK: 2175740 Matrix: Water Associated Lab Samples: 92368000001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 12/22/17 14:10 Pace Analytical Services, LLC 9800 Kincey Ave. Sulte 100 Huntersvi0e, NC 28078 (704)875.9092 LABORATORY CONTROL SAMPLE: 2175741 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Sofids mg1L 250 256 102 90-110 SAMPLE DUPLICATE: 2175742 Parameter Total Suspended Solids SAMPLE DUPLICATE: 2175743 Parameter Total Suspended Solids 92367665001 Dup Units Result Result RPD Qualifiers mg/L 22.6 31.4 33 D6 92368004001 Dup Units Result Result RPD Qualifiers mglL 65.2 67.7 4 Results presented on this page are in the units indicated by the'Unite column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fall, Date: 12127l2017 09:32 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 10 ceAnaliftal o WWWpacefaba.com QUALIFIERS Project: Plant 17 HWY 55 Pace Project No.: 92368000 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and bellow the adjusted reporting limit, MOIL - Adjusted Method Detection Limit, POL- Practical QuanBtation'Limit. RL - Reporting Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HunlerSAlle, NC 28078 {704j875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte Is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNl - The NELAC Institute. LABORATORIES PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF'LABORATORY ANALYSIS This report shall not be reprod uced, except In full, Date: 12/2712017 09:32 AM without the written consent of Pace Analytical Services, LLC, Page 6 of 10 IceAnalytical wwwPa ghft.mm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Plant IT HWY 55 Pace Project No.: 92368000 Pace Analytical Services, LLC 9800 KincayAve. suite 100 Hunrersville, NC 28078 (704)875-8082 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92368000001 Dutfall #1 Plant 17 SM 2540D 392160 Date: 12127/2017 D9:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 10 iheMae= r Client Name: P— e, Fed Ex UIRS. USPS C16 Courlert 0 t [:)Commercial Elpace []other: Custody Seal Present?, []Yes to seals Intact? []Yes Pai:kino Material-. []Bubb]eWrap [38ubble Bags Thermometer: ri I (LCI e) -10 7 -Ad Authority. aqfi� --,Mj-CKafilC5VjIIeL7] If S Ra e 0#'92368000 Dit*/InWalt Person Earnfnfing Caotents-O�- 2-- ❑ Othei Blologlat Tissue Frozen? OEM! ONoo DYes []No j'NjA m "un ow: 7VP6011cal P' . cartection S e±nr-, Cooler 13LCorw;t&d4X). b&above4eezin&tobY USDA Regulated Soll 04NA water sarnpfeE Did samples OrIjinate 111' Oquarantine zone %VMIn the United CA, NY, or, 5; (check maps)? old laqlasotOnate from a roreign sour" (]At I0 ralk, Oye Cko 1rtdlvdjj Huyall and Fuuto Rkoj? E3Yes 01 Chain ofCustod I Present? 411�� W. CINIA 1, Sam -ples ArrlJed vjlthln.KoI4 Tim? Yes nNo QN/A 2, Shoit Hold 1111me AwlyiN (i72 hr.)'? . INA E❑ 3. Rush.Turn Ar6undTIFrolteguened?- EIN/A 4. sufficlentVoiume? es 13No Co0ect CoMalneis Used? ..-Pace 6nialners Used? as 13N0 ON/A []Ito ON/A 6.1 _CbrItAners Intact? lift r, ]W'jk 7. Dissolved anal �5: Si les Field Filtered? Y . No CkA 8. Sample Lab& much cou -Includes Date nme/iQjAnalVsIs MatrW ffY. [3NO OWA- 9. Heatlspaci In VDA Vials (,5-6m{h�3- []Yes ONO IA 30. Trlp'llankfteserilt? -Trio BlankCustody soals Present? 13yes E]yts- []NO CIND A33. NIA CUENTNOTIFICATION/lIESOLUTION Person Contacted:- CDmintfitVSa*le Discrepancy; I Datemmt; Field Dateflecialred? UYu UNo Project Meniier- SCURF Rawl,ew: Dot, Project Monapr SKF Review- LAI, TJ oat Nca: Wlte"'"'r there 13 a dumponvi affecibig hor�LbOrollro cornpilance samples, @COPY "is form will 1100nttO thtflorkh CEWIM OEHNR Certification Office JI.e. Out of hold, Incorrect Orejervativt, but ofteinp, %corricicontairlirs) % r Q a �r y t 'W4 �js71. ,v ,..`Do¢titn tl ex 4:Rc�vised: July 25, 2017 1 " ciC$A!%iSam leCorididori' n R ! S':k'� Paget of 2- Do�ulrten`t_;Hc'ti`' '+AISsoingAutharlty: °`Ciieci<mark topfialftsfbox _iipHandJ rhlOd ati.auL�c preservation samples. -----' PM: RMB 1/08/18 **Bottom half of box is to lust number of bottles CLIENT: 92-Rteody Mix _, zp d ti - `7 's F - aaprr V A y V .Sa�'.. CL .E• C d g S a 6 Nt Q u nl R c n Z p aj 49 z _ .. 7. 7 �ti c iV 3 Xf �• P -S3 13 V ipf❑�xJry{.ti 3 son 011 I ones on memo MOOMIN ELI 1 0 memo a loan pH Adjustment tag for preserved samples Sample w Typa or PremVit[ve PH ppoa tetelpt Date pans , Oodadlusted. Thee ptetstva W ad]utted• Rmwmi of prae3wadn added tat d /..j Y' - ^I•jr •ii, t11C• ��::G:�w4f{Z-r-IS.:'�.': ..�F.'. :`n :R .N�.•. J_ %-\: 1' —:iN'T �:..Y/ �J.14"�i�3'..-J'4 •. T.. �.S' :.lk'.cC�?hti•A¢i;'b!n�.�.i�}.f£ts+isY,ii-i?jx.: �?rS,i!L1;7., i?ti:.'i,.,_ .ir.:.n°�'4'4 • r,_'-. i•,p �1 '..Ydl1°AI73fyfi+W� ' CHAIN -OF -CUSTODY f Analyfica! Request Document The Chain -of -Custody is a LEGAL DOCUmEN7. All relevant fields must be completed accurately. Sxtlon A Seellon aSection e Requi-d Cae d raft~lan: Roquirad Pr *-" Ir,tofrtitat{on: Invoice allonnaderc Fpage _ i Of t Caft5o+'P• Ruady k5w Cgr4Me Re,porl Ta: Watka4 AnwnWn' AgGem. 2610 BUM GO"] Cagy TO' Company Name Ratefat,., NO 21610 Aodro s: Ettui :� 0 f-wi d r - at _ 4-04 Pu d— Orders Pace 014101 P",w- i fm Prale[t Name; Se E� CaaaM,ers Pace prdera Manager, a.bai%-A0pecetebe_wm $taG JLocaOan' Requeatad Dw Data Prnlea O' Ki S Paco Prase k NC ' Re wcted o FMawtl !N 7 • ,, "u coon s S COLLECTED z Preservatives - :- D*n qO w Dw w smWMV w n rm 1 3 2$ Y SAMPLE ID ;°g"' g START END " a r Om Chera}tM Per boa. M �. (AZ al AR reIliDATE IF- I TIMEA B31 I L"1(l:s i L -1 k. A�M�Y•4v�� �1iMENi,+ .�:i--. ry _ �AElLNGt}ISi®AY �alfiiV.�4T10N^' T`-C. ;s_pATI':rt :'1; rr�� ?aid±:', 'vL' _ - r1Y1AFFgylllpN :CAiLlfii "_'' 2� - t^k1 :' i:4•' _ _ ( - � :--�.`:. �.:. •.Y- •:.�T.`.((..s.: '�•~ - :'-%•'+: riw... s./)h re.h'r M� lti`�/:�' ..y,�_•_.v =.^1:.'i�.'.�it:C L1�,�,.�: /�� i 4UIPlERlaA1iE,AND-SIGNA711RE v PRINT Name of SAMPLER. I F � � 3, 11-4 IF -H SIGNATURE at SAMPLER; OATS Si9nad: i � O D O m a a NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For cguidance on filling qut this form, Please visit: Imp; portal mcdenr.orgf webIIr•/nodes-stormwater/ Permit No.: �1/�/_/_/_/_/—/—/—/ or Certificate of Overage No.: p/ Facility Name: Plank 1`7 Ik" 5.5 _ County: ^ BArin 0-A' _ Phone No. a 19 - 54Y -16 Z% Inspector:______ Date of Inspection: Time of Inspection: MAY 0 4 — Total Event. Precipitation (inches]: 51 CFNTF�,gL PFIL Was this a "Representative Storm Event" or "Measureable Storm Event" as dec��}s p 6 t? (See information below.) R"Y�s ❑ No Please verify whether Qualitative Monitori11r1 roust be performed during a "representative storm event" or "rrleasureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be T performed during a "reps:esentative storm event" or during a "measureable storhi event." hlowevel•, some permits do not have this requirement. Please refer to these definitions, ifapplicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall anti that is preceded by at least 72 hours (3 days) in which no storm event measuring greater Chan 0.1 inches has occurred. A single storm event may cantailr up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-11our storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Pe/mit{ee or Designee] Page 1 of 2 SW11-242, Last modified 7/31/2013 1. Outfall Description: Outfall No. Structure (pip ditch tc.) Receiving Stream: Describe the industrial activities that occur wit4in the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: — M&� ' 3, Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weals chlorine odor, etc.): 1JDp-e- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: d 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: O 2 3 4 5 6. Suspended Solids. Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: �1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes V 9. Is there evidence of erosion or deposition at the autfall? Yes CN 10. Other Obvious Indicators of Stormwater Pollution: List and describe LV t11) `r— Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, fast modified 7/31/2013 1. Outfall Description: Outfall No. _2 Structure (pipe itch, tc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color, Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Q . a 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 © 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and S is the surface covered with Floating solids: 1 V 3 4 5 &. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 6) 3 4 5 7. Is there any foam in the stormwater discharge? Yes l o 8. Is there an oil sheen in the stormwater discharge? Yes U 9. Is there evidence of erosion or deposition at the oLrtfalI? Yes 00 10. Other Obvious ludicators of Stormwater Pollution: Gist and describe Dote: Low clarity, high solids, and/or the presence of foan-r, oil sheen, or erosion/deposition may be indicative of pollutant exposure. (These conditions warrant further investigation. Page 2 of 2 SWU-242, last modified 7/33,/2613 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division,of Water Quality General.Permit No. NCG060000 Date submitted gIZ5 l 11 CERTIFICATE OF COVERAGE NO. NCG06_Q Z SAMPLE COLLECTION YEAR FACILITY NAME ('& 1 FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES it LMbj (V DISCHARGING TO SALTWATERS? [—]YES YNO LABORATORY. P 14L`e- ab Cert. # GI PLEASE REMEMBER TO'SIGN ON THE REVERSE -Y` Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall s . S/ or ❑ No discharge this period3 Outfall No.. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD; mg/L Oil and Grease, mg/L Fecal .Coliform , Colonies per 200 ml Enterococci , Colonies per 100 mi Benchmark 100 or 5D' Within 6.0-9.0 120 30 1000 Soo 1Z - 12.1 N 11 lb,S 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new. motor oil per month? ❑ yes 5no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55-gal of new motor oil/month. Outfali No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, .Standard units New Motor oil Usage, Annual average gal/mo Benchmark - 30 100 or 50 6.0 — 9.0 Only applies to facilities that use/process meats. The total. precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report -with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water, classifications where the more protective benchmark applies. (ice complete Part.B) SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. O 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART It SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT,ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports,_ within 30 day_s of reteipt_of the_tab results (or at end of monitoring period in the case of- "No Discharge" reports1aa: Division of Water Quality Attn: DWQ-Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST.SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with -a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the- information, the information -submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties -for submitting false information, including the possibility of fines and imprisonment for knowing: violations." (Signature of Pe .SCt I0 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.orQ/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 18. 2012 Page 2 of') ZAnalytical * CHAIN -OF -CUSTODY / Analytical Request document The Chan-d•Cudady La a LEGAL DOCUMENT. An rslevant fields must be campinmd accurately. paw.d SectSectionA Section B Sxlion t: Required Client lnhmtaUon: Roqutrad Pra)ect lntormeliort: Imaca Intor"Ilm: Ca pwv: Report Ta: Altwboa: I/�'/�4 2 0 9 7580 Addrass: Copy To, Company Nwmv RI:iiCFiAtC►Ry AGEIiCI :. - a4dreso: r NPOVS r GROUNDWATER I ' DRINKING WATER f UST i." RCRA I— OTHER ErMO Tp1 r Purchase �t� � Order No.: Pax Cant• • VUwf Zir 141 two Raf§amnea: PfpMO: Far: Ptajon Name: t� •� , 8ka �. �� Manegrr. ,STATE: - Raquaslnd Due DaAerlRi: Project .y Number 1 I i 66 P•r. Prone A. Requested Ang1plow F31U"w1'(YINI Section MaudtCodes 5 x' R•quir•e CJwd 14kwwwn MATRIX t CODE COLLECTED PfCSCNBhVES 7.: ' Drinkirm Watm bW 8 U W wr WT 1Nasta Water ww U catmosrm CZPPOSTE cl •.'. P-aduc! P 91�Mr [r+�.Cnnu i s aitsohd SL SAMPLE ID oil pa wOIL 1A2.0.9l.-) Ah AR p w a �r^. `'",.'. "��` r\ .' . • 4- Sarttpie 1p5 MIfST BE UNIQUE Tissue T5 O rLj k •".^ `•^'=.`„ ,• „,,_.% Outer OT32 X 10 DATE TIME wr£ TIME # 2 x x z 2 o , A(ix Pace Pro'ect f•oJ Lab I.D_ 9 :i4Mh7 qmml Milo (fik �a 4 6, .7 10 11 12 AWITIONAL COIgIIlENf9 ..:... � , .. ' K�{.lFigiil3fi q 6Yt RFFI:JIITIFNNi{��- -' tw*-`:.` � _ ;iwl- ...: , - ,.:OVAky'i PIIJRTION DR78 ;'•11k .:: SAMPLE COMDI[MMS S ORIGINAL snHrslnzwvr�et�+a�(alArurtE u PRINT Marne of 9AMPLM. o u t) -4 DATE Slgnvd SIGNATURE d SAMPLM, [ice F -kmp UM NJae By rgrung ma farm yaa ore strepllnq Pecan NET 3C dy parmsrt ixmsuw epremnrj m uw eturgne[ 1.5% per mon[nlar •rry moicce not pe16 wMMn 30 drays, F-ALL-O-720rev.07. 15-may-2007 /IeAnalytical- ~Pacelabsxom ANALYTICAL RESULTS Project: PLANT 17 HWY 55 Pace Project No.: 92338351 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Sample: OUTFALL #1 PLANT 17 Lab ID: 132338351001 Collected: 04/24/17 09:13 Received: 04/25/17 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids • 12.2 mg/L 3.3 1 04/26/17 13:41 Sample: OUTFALL #2 PLANT 17 Lab ID: 92338351002 Collected: 04/24/17 09:16 Received: 04/25/17 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2640D Total Suspended Solids Total Suspended Solids Date: 04/2712017 03:05 PM Analytical Method: SM 2540D 40.2 mg1L 3.8 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 04/26/17 13:42 Page 4 of 10 Document Name: ESI Tech Spec Document Revised; Sept. 21, 2016 at;EAn,h,►,��! r Sample Condition Upon Recef SCUR) Page i of 2 �'r" Document NO.: ; Issuing Authority: F-CAR-QA-003-Rev.02 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh® Mechanicsville[] Sample • Client Name: Project It: Courlev ❑ d Ex ❑UPS USPS Mflient ❑ Commercial ❑Pace ❑Other: Custody Seal Present? ❑Yes la Seals Intact? Dyes iWo WO#:92338351 1111111111111111111111 Date/Wtlals Person Examining Contents: Packing Material: ❑Bubble Wrap ❑Bubble Bags one ❑Other: Thermometer: )eWet ® IR Gun ID: IS-3492 Type of kw❑8lue ❑None ❑Samples an ice, coaling process has begun Correction Factor: Add0.6 Cooler Temp Corrected {'Cl: � Biological Tissue Frozen? []Yes [7]No #/A Temp should be above RuaranVne ev g to 6•C USDA Regulated Soil {N/A, water sample) pid mrTtpfes originate in zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (;nt rnationally, ENS 9No including Hawaii and Puerto Rico)? ❑Yes INo Comments/Discrepancy: Chain of Cust Present? ❑ I. Samples Arrived within Hold Time? ET D 11 Z. Short Hold Time Analysts (02 hr.)? ❑ 3. Rush Turn Around rim eRequested 7 ❑ ❑ 4. Sufficient Volume? © LJ 1 5. Correct Containers used? -Pace Containers Used? ❑ ❑ Cl E. Containers Intact? ❑ ❑ 7. Samples Field Filtered? S. Note if sediment Is visible in the dissolved Container Sample Labels Match COC? -includes Date/TimeAD/Analysis 3, Headspace in VOA Vials (>5-6mm)? Yes Ho A lo. Trip Blank Present? Trip Blank Custody Seals Present? Yes © No EJ N N A A i 12, CLIE r NOTIFICATION/RESOLUTION Person Contacted: Comments/sample Discrepancy: Date/Time: Field Data Required? ❑Yes ❑No Project Manager SCURF ^1[ I y ^� Review: 11 I� Date: Project Manager SRF Review: i ) I v Oats: i_ " of / Nate: Whenever there is a discrepancy affecting North Carolina compliance samples, a COPY of this fat will be sent to the North Clrofina DEHNR Certification Office li.e. Out of hold, Incorrect preservative, out of temp, incorrect containers) Page 8 of 10 S �a H O a m rw its 2 a K � ti V A � fD C1 m 0 g6 � h 6 0 Item# * �, ,w in m a ro zzzzzzzzz, 2z BP4U-125mL Plastic Unpreserved (NIA) (CI-) 3 m EL SP3U-250mL Plastic Unpresorved IN/A) Iv a a or BPZU-SOOmL Plastic Unpreserved(N/A) - CL O r' SPIU•IliterPlastir.Unpreserved(N/A) Cr O s as _ - BP3S-250 mL Plastk H2SO4 (pH < Z) (q.) --•- in r. C 8P3N-250 mL plastic HNO3 (pH < 21 e� tp G' C X n ZZXXX BP32-250 mL Plastic ZN Acetate & NaOH (>9) rD �; I 6 BP3C-250 mL Plastic NaOH (pH > 12) (C1•) n rp R WGFU-Wide-mouthedG lass jar Unpreserved O Qj i AG1U-1 liter Amber Unpreserved (N/A) {Cl-} Cr CL Ob rt p � zzzzzzz AGiH-1 liter Amber MCI (p14 < Z) w S O AGIV-250 mL Amber Unpreserved (NIA) (Cl-) 3 w 0 AG1S-1 liter Amber H2SO4 (pH < 2) A03S-250 mL Amber HZ04 (PH ,c 21 AG3A(VG3A)-250 mL Amber NH40(N/A)(CI-) OG9H-40 ml VOA HCl (N/A) a - VG9T-40ml. VOA Na2S203 (NIA) I � VG9U-40 mL V6A Unp (NSA) OG9P-4O mL V0A H3 PO4 (NIA) rC12 3 VOAK (6 vials per kit}5035 kit (N/A) Z 33 WGK (3 vials par kit)-VPH/Gas kit (NIA) IN SP57-125mLSterile Plastic (NJA—tab) I OIL `0. W SP27 250 mL Sterile Plastic (N/A— lab) 0 MA-250mL Plastic (NHZ)2504 (9.3-9.7) 3 x Cubkalnar m r nt U \� Iv VSGU-20 mi Scrntllladon vials (NIA) GN ` r,p r+ -4 b q tr r NCDENR Stormwater Discharge Outfall (S®O) Qualitative Monitoring Report rorcguidance On fillilrc7 orrt this for•ril, please visit: half:/ jpQrtat.ncderlL.Qs' wet)/It•liipdes-stornitvater( Permit No.: /C/—I—I—I—/—/ -I_I or Certificate of Coverage No.: Facility Name: _ FIQnk 1`7 Ik Cotlllty: b%tTVVA- % ! Phone No, a !g- 5,14y,-167 Inspector: � _ riSkoro Date of'inspection: y17-g117 Time of Inspectiow 9-1.lb AV't _......_..____ _ Total Event Precipitation (inches): �L 51 Was this a "Representative Storm Event" or "MeasureaWe Storm Event" as defined by the permit? (Seca information below,.) Evr'*Ye s ❑ No Please verity, rvhellierQtrerlitative Mouil:orinq must lie performed dcuhi q a "representatives[nrrn even!"or "merrsureoble storm evamt" (requirements vory, depending of) the permit). Qualitative monitoring requirenlents vary. Most permits recitlire qualitative monitoring to be performed during a "representative: storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicahle. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall anti chat is preceded by at least 72 hours (3 Clays) io whic'll no sturnl event measuring greater lhau 0.1 inches has or.curred, A single storm event may contain ill) to 10 conseculive hours of no precipil.lbon. A "measurable storm event" is a st.orlll event that results in at) actual discti!al-ge frnlli the permitted site nutfall. The previous measurable stnlrnl evens must have been at leasl 72 hotirs prim-. The 72-hour storm interval (toes not apply if the perlllitt['e is able to clncurrleilt Chill a shori-er interval is representative for local storm events during the sampling period, and the permit[ee. obtains approv 11 frulll [lie local DWQ Regional Office. 13y this signature, i certify [hat this report is accurate and Complete Co the hest ol, lily knowledge: (Sigliatllre of* Pt/rnilfee or Designee) Page 1 of 2 SWU-'242, LAst modiI�od 7/31/2013 1. Outfall Description: Outfall No. f Structure (pip ditch te.) Receiving Stream: Describe the industrial activities that oqur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: ` e _ 3. Odor; Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): k OA>t 4. Clarity: Choose the number which Kest describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and S is the surface covered with floating solids: d 2 3 4 5 6. Suspended Solids: Choose the number which best describes the arnount of suspended solids in the stormwater discharge, where i is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes n 9. Is there evidence of erosion or deposition at the Outfall? Yes CN 10. Other Obvious Indicators of Stormwater Pollution: List and describe 1V C1 0 `r- Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 7/31/2013 1. Outfall Description: Outfall No. 2- Structure (pipe(Sch, tc.) Receiving Stream: Describe the industrial activities that occur within tiie outfall drainage area: Z. Color; ]Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: t&. f oo'. 3, Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _MboJ ( ?-. Clarity: Choose the number whicli best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: S. [Floating Solids: Choose the number which best describes the amount of floating solids it) the stow rnwater discharge, kvhece 1 is no solids and 5 is the surface covered with Floating solids: 1 l/ 3 4 S 6. Suspended Solids: Choose the number which best describes the ar-nount of suspended solids in the stormwater discharge, where i is no solids and 5 is extremely muddy: 1 6) 3 d 5 `l. is there any foaro in the stormwater discharge? Yes C90 8. Is there an oil sheeii irl the stormwater discharge? Yes t to 47. ]s there evidence of erosio►� or deposition at the outfall? Yes tVo 10. Other Obvious iridicators of Storrov)-ater Polluticii: List and describe �,9_� Note: Lola clarity, high solids, and/or the prasence of foaili, oil Sneed, r, �i osio,r/rle �Gsiclan 'tray be indicative of pollutant e;.posure. These conditions warrant fnrcl:wr investigaii-3n. Page 2 of 2 SwU-242, r,ast modified 7/31/2013 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted g174 li CERTIFICATE OF COVERAGE NO. NCGOGJ2 It FACILITY NAME WVII IL 1 COUNTY VIAtud�_ PERSON COLLECTING SAMPLES VPso �.�11J6,6(0 LABORATORY I> AL`e b Cert. # qI _ Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR FACILITY ACTIVITIES INCLUDE (check all that apply): use/process meats [ use animal fats/byproducts DISCHARGING TO SALTWATERS? DYES (YNO PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total evens rainfall 1-Y.-St or ❑ No discharge this perio? Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 ml Enterococci', Colonies per 100 ml Benchmark 100 or 504 Within 6.0 — 9.0 1 120 30 1000 Soo �z. 4 -1 ►% 1 1 ( I ' On}y applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. a For sampling periods with no discharge at anv outfalls. You must still submit this discharge monitoring report with a checkmark here. °Sae General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? [I yes 2�no Part B: Vehicle Maintenance Area Monitoring -Results: only for facilities averaging > 55 gal of new motor oillmonth. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark 30 100 or 50 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. The total precipitation must be recorded using data from an on -site rain gauge. For sampling periods with no discharge ate outfalls, you must still submit this discharge monitoring report with a checkmark here. °See General ?ermit text, Table 3, identifying the especialiy sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part 6) SWU-249 Lasr Revised: October 18. 2012 Pa c: I of *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES 1N A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B, o TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES FINOCK IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt athe lab resuits for at end of monitoring period in the case of "No Discharge" reports) ta: Division of Water Quality Attn: DWQ Centraf Files 1617 fAail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATfQN FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of S1# 117 (Date) Additional copies of this form may be downloaded at: htt artal.ncdenr.ar web w ws su n desswtttab 4 S wu-=19 Lair Revizcd: October 1 ti, 2012 Page 2 oi' a aceAnaljftal .—n CHAIN -OF -CUSTODY I Analytical Request Document Tha Charof-Custody is a LEGAL DOCUMFKT. All relevant HOICIS MUSI boCQMPIetW OCCUrdt:ly. yr Raclin A Suction R Section C Requirad Cftnt lnkwmtk)n: Required Prqca Informal1w: Inv= Intaimaflor; "": hfaa Report To: Aft—b— 2097590 Add�: Copy To: Company Noma: AdzImoc NPOES GROUND WATER PRINKING WATER F IX5T f- RCRA OTHER Eman Toll 4D Ord& 11.,� Pam Woo :1 _ (_1q*t'tW 'III,. Ra?a�a: J rF,-- PhpnO:I Pmlccl Nomo: F..— V. Manager. STATE, Requested Qwo Patwrrm. Piclact Number, PmA.e 0: Requested Ana pis Fifteired, Section D fftLrbLGc4ss P-401f-d Cb.11 Hun—L— MATRIX f =E 13'i�ki.g wai'l Dw COLLECTED pirservi6ves watoc WT wasid wzttT ww U Compass 00NIPOSTE 0 soivso�id SL SAMPLE ID Oil 01. m m WPG All AR uj SomfycINPAUSTOEUNIQUE Tissue TS 01her OT X 0 61 d 6 q r; It § - � m DATE TIME OATE TIME I D x z z 2 o Pace Frojact NoJ Lab 1,13, *1 f6t+ C! x 60. rwo-, wgfislwE .3 7- 8. : 121 1 JAI AnVITIONAL 6MEMENTit E 411i . i AL . SAMPLE CONDIMNS SAMPLER NAME AN, 0 SJGNATUFM t; ORIGINAL PRINT Name of SAMPLER: PATE Signed SIGNATURE of SAMPLER: ' hmpoftent NC40 BY w2mg bI3 .1onn Y.9 art wco[ag Pe *s NET ]0 COY P%Ylrar-t UYMS and agnt" . IA. OW901 e 1.5% Per nv Il . F-ALL-0-0201roV.07.15-h1ay-2007 Arl--7 aceAnalytical wwwpacelabs.c= ANALYTICAL RESULTS Project: PLANT 17 HWY 55 Pace Project No.: 92338351 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL #1 PLANT 17 Lab ID: 92338351001 Collected: 04/24/17 09:13 Received: 04125/17 14:55 Matrix: Water Parameters Results units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 1 12.2 mg1L 3.3 1 04/26/17 13:41 Sample: OUTFALL #2 PLANT 17 Lab ID: 92338351002 Collected: 04/24117 09:16 Received: 04/25/17 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 40.2 mg1L 3.8 1 04/26/17 13:42 Date: 04/27/2017 03:05 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 10 Document Name; ESI Tech Spec Document Revised: Sept. 21., 2D16 : SampleConditionU onRace ipti5CUR) _ Page 1OF2 /A,aceAnal ka!Document No.: Issuing Authority: F-CAR-QA-003-Rev.02 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenvuood ❑ Huntersville ❑ Raleigh® Mechanicsville[] • • Client Dame; rU�lO . 92i3383 ,�►1 kra Project t3: Courier: ❑ d Ex ❑UPS ❑uSPS l 2nnt �l EIS I B l I ICI �I II ❑ Commercial ❑Pace []other: 92338351 Custody Seal Present? ❑Yes Pvo Seals Intact? Oyes ` No Pack€ng Material: i/ ❑Bubble Wrap ❑Bubble Bags �No:ie ❑Other: Oate flniUats Person E:rarrrl n ing Contents;06—,,,_ a-113-1:31- Thermometer: ®IRGun ID: ,Wet Type aflee: ❑Blue []None 05ampleson ice, cooling process has begun Correction Factor: kddo 6 _IS-3492_ Cooler Temp Corrected J'Q Biological Tissue Frozen? []Yes ❑No OIA Temp should be above fr�ez€ng — to VC T— USDA Regulated Soil ( 1�7j N/A, water sample) Did samples originate in a ❑Yes Kno uarantlne zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (lnt rnationaily, including Hawaii and Puerto Rico)? Oyes No Comments/Discrepancy: Chain of Custody Present? © 0 11 i Samples Arrived within Hold7ime? © El2, Short Hold lime Analysis (<72 hr.)? ❑ 3. Rush Turn Around lime Requested? ❑ 15 © 4. Sufficient Volume? 5. Correct Containers Used? -Pace Containers Used? ff © 0 El d Containers Intact? Ll ❑ 0 1 7. Samples Field Filtered? 8. Note if sediment Is visible in the dissolved container Sample Labels Match COC? E -Includes clate/Time/ID/Analysis - 9. Headspace in VOAVials (>5.6mm)7 0 Yes No 4A 10. Trip Blank Present? Trip Blank Custody Seals Present? Yes YYes No N N A A 1 11. CLIENT NOTIFICATION/RBOLUTION Person Contacted: Comments/Sample Discrepancy: Project Manager SCURF Review, Project Manager SRF y ��� 1 It-) Review: � ! Field Data Required? L)Yes LJNo Date/Time: Date: � - Zi 1 ;1 ~V Datet d" zo ✓( I Hate: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wilt be sent to the North Carolina DEHNR Certifcation C ffrce li.e. Out of hold, Incorrect preservative, cut of temp, incorrect containers) Page 8 of 10 u w ro Co o. 0 5 R S vro n Q� C 9 tb R m t 0 n m y m F d p �' fb f/Y a mg o h � A to m -4 rn Ln + w ra ICamft j�� - a zzzzz ._ __ 8P4L1-125mLPiastic Unpreserved(N/A}(CI-) K M O 3 ^ SP30.250mL Plastic Unpreserved (N/A) EL pl lu BPZU•500mL Plastic Unpreserved (N/A) N w 3 7 CL O 3 SP1U-1 liter Plastic Unpreserved (N/A) Q o a _S v AIX 8P3S-750 ml, Plastic H2504 (pH < 2) (CI-) �• o MU-250 mL Plastic HNO3 (PH < 2) X h n BP3Z-250 ml. Plastic ZN Acetate & NaOH (>9) 7 3 Fi MC-250mL wa5VC NaOH (pH> 22) (0-) °J WGFU-Wide-mouthed Glass Jar Unpreserved � � 1 0 C AG1U-1 liter Amber Unpreserved {N/A) (CI-) tT 0 �, m --zzzzzzzzz2z—, AG1H-1 IltarAmber MCI (phi <2) M •e O AG3U-250 MLAmber Unpreserved (N/Al (CI-) �. ?; O RGiS-1 liter Amber H2SO4 (pH < 2) AW S-250 mL Amur H2SO4 (pH -4 2) AGM(DMA)•250 mL Am her N H4C1 (N/d.)(G- ) OG9H40 mL VOA HCI (N/A) a VG9T-40 mL VOA Na2S203 (NIA) M VG9U•4D mL VOA Un0 IN/A) xa OG9P-40 ml. VOA H3PO4 (N/A) 0-0 r : M •- VOAH (b vials per kit)-5035 kit (N/A) Z 33 _ CD V/GK (3 vials per kit)-VPH/Gas kit (NIA) SPST-125mLSterIlgPlastic (N1R-lab) � SPZT 250 mLSterile Plastic (N/A- tab) A Q, •C B!i r- P3 BA-250 mL Plastic (NHZ)2504 (9.3-9.7) x o M I Cubitalner q_1 V,5QU-20 mL Scintillation vials (N/A) GN d �W4 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report horguidance on filling out this form, please visit: http://oortal.ncdenr.Qrg/web/lr/nodes-stormwate� Permit No.: _/ or Certificate of Coverage No.: 1./+�/O_/ Facility Name: 6UL( SS County: buyInAWK I W, Phone No. 91 Q - S T4 —1,67 `1 Inspector: mij L Date of Inspection: 511S Oh Time of Inspection: ? ., Nb r Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" asp4bed by the permit? (See information below.) ��� I Yes ❑ No / Q Please verify whether Qualitative Monitoring must be performed during a `representative storm event" or "measureable storm event" (requirements vary, depending on the permit).Nl� Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge From the permitted site outfall. The previous measurable storm event must have been at least 72 hours i prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (SiOatr(e of Permittee or Designee) Page 1 of 2 SWU-242, Last modified 7/31/2013 1. Outfall Description: Outfall No. i Structure (pipe itch, tc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Cl-eAr 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 00" 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and S is very cloudy: 6 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: () 2 3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes G 9. Is there evidence of erosion or deposition at the outfall? Yes N� 10. Other Obvious Indicators of Stormwater Pollution: List and describe +l. OA-)—1 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may he indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 7/31/2013 A�� NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http:/.li2oijal.ncdenr.org/web/lrinpdes-stormwatert Permit No.: N/C/_/_/�/�/ _//_ / or Certificate of Coverage No.: Facility Name: en# 1'f jj(Aw 5S County: �rinuw�. Phone No. Inspector: ReAJ-W1d Uln'SkCKo _ _ .-- Date of Inspectio] 14 lb ^ Time of Inspection: ''1 40 dr+ Total Event Precipitation (inches): ^e Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) O"Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "rneasureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." however, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall j and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 10.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative For local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Sigj�Ktu✓e of Permittee or Designee) Page 1 of 2 SWU-242, Last modified 7/31/2013 1. Outfall Description: Outfall No. & Structure (pipe�tc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Q+Ea*% e h-c.re.4e -NAM- 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: C 6-Ar 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): poA..'e 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: lv 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 6 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes B. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes 6 10. Other Obvious Indicators of Stormwater Pollution: List and describe lRiv &� -e Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 7/31/2013 tr PkeAnalytica!" CHAIN -OF -CUSTODY I Analytical Request Document The Chain•of-Cushy is a LEGAL DOCUMENT. Ad relevant fielU must be completOd accurat". Pau.: n7 Section A Section a Section C •w Rcquned Chu,! Inlo,mation: Required Prgeet lnlom:alion: Invoiee Wormatian; Company: To: A;tection: 2056307 UU&; C,A toa-:16-4tR?port Address; f 51—, Cagy To-, Cornoany Name REGULATORY AGENCY 'PlAk b Atltlrcas, NPDES GROUND WATER :" DRINKING WATER UST RCRA OTHER F.wq To W /� Partner+_ Order No.: 4 Ph fqx P.vjet%Name: o°ee r'rop-•a Site Location 5 �J' �.j Rc -u Wd Due oatw7AT: Pr01ElCt Kur•.b^_.. ?wu MolM x {. �--. Requested Analysis Filtered (YIN) $°ttion 6 Hattie Catics RequlrtoMATRIX .f. 0(70F o t COLLECTED Preservatives Y' pnnvinc Water Dtv U e VJ, WT (j V7]^.te Nrllttr N:VI -rr07utt F COMMUTE VMT Campo ENU GWIU V W ? SAMPLE !D w� wa Sar:rplt rDs ilJa^t S[ i;NICI;E Tissur 7$ p U it OIhBr .,. O w C V EOD I Trn L 3 y I _ _ z' ° Lab I.D. — DATE TIM.— DATC T INIE :1 O .�,� Pace project No./ 1-7 G 7 I ! i cZ,t T I 8 i i t 1 —� t 16 i 1 f E I I 1 Ae.^i'fE,Na�Ct3M11�lFNT$ I R?LINgi;t5NED 8YlAFi•1LIATiDN 7Ac �t4"._- AN[:E Ep tAFF41AfIH it I pA7E 7iME Sirs:'•_f. ;::JNCI',!UNS ' I -� �V[ � I 1 ...._ _ __,.__,_..,. _1 � Wit/ ti ✓` '�-� ? , i `\t �at41 v ialt./t `l � 1 . F � SAMPLER NAME AN-7 $7L r,.. - 0 Er �;a'ceAnaiyfical' www.pacehtb&corn ANALYTICAL RESULTS Project: HWY 5S PLANT #17 Pace Project No.: 92298601 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL #1 PLANT # 17 Lab ID: 92298601001 Collected: 05/18116 19:40 Received: 05/20/16 14:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 16.8 mglL 2.6 1 05/24/16 11:37 Sample: OUTFALL #2 PLANT # 17 Lab ID: 92298601002 Collected: 05/18/16 19:40 Received: 05/20/16 14:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids 31.0 mg1L 5.0 1 05/24/16 11:37 Date: 06/20/2016 02:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 9 DOCLlnleh�No.. Issuing Authorlty: -001-reV.05 Face Raleigh Quality Office Client Name; WO#: 92298601­­- Pro ject fi �Rtl C0Courier:::ed Ex k ❑Ups DUSPS PdCL� RP" Cf2en[' E]Other:— 92298601 Ctl;tody Seal Present? Dyes 0,10 Seals Intact? Dyes �No hate/initials Person El(amining Conte rits'. - L(O !1'l(A61V,IAwl,1I: , FIBLitiblv bVf up 06obh.e Bogs 'ON -one 000w; — *4EF thornivnieter: /I !R SR: 1220653V E)w sm 121.00,411 Type of ice: owet ❑Da!,. [1%one []Samplet� on ice, cooling process has be " Flctxr.'D,Wc ('00ler Temp Corrected ('C); Biological Tissue Frozen? Dyes [INo N/A USDA Ac,;:.A;j[ed ;nil r lnt! ljrti'P.d States- CA, NY, or SC (check maps)? Did samples originate front a foreign source (inIFall0rallY, M - ii— and Puerto Ricoh nYes NO Q COMMENTS: I. Yes D1,10 014/A /dye$ DNo ON/A 2. Jiai.il of :ustozlv Kelinclulshed? &Y,-s No D,/A 3. SimWel-Narn� and/or Sipniture ell COC? (fZ/Yes ONo MN/A 4. SaniplpsAriv�-dvdt�jln FjoldTinie? b�es OND EINIA 5. Short - Bold Time Analysis J 02 hr)? DY6s 0JNo'_ D N/A Turn Around Time Requested? OYes No ©N/A 7. �Rush SufficientVolunle? ry. '1J N. ON/A_ 8. rorrectCuntalners, Used? Yes ye 5 ONO ©NIA 9. - Pace Containers Used? Y, DNo ONIA oTst*,tincr> Intw F No CJN(A 10. oYes 0 Pic 1ANIA 11. 1 Jolt If sediment Is visible in the dissolved container 12. t.Aok roalch C(1(7.7 Yes ©No ONIA loallix: o­:,, r.;L-Jw!, :lriss4n valion are found x, no ul 1, �iq fl, q t� J,11) I.Ci,.,: WaoH >7 Sulfide, NpOH;-121 Cyanide) Cr1Yes DNu EJNJA VO& Coliroffii, TOC. Oil Jlu(I Grease, v. LHg es No ONIA 14. il-implo:, :re, ked for �es Dft ©NIA 'es [2i"l- ON �iLa- space in V0A Viah, (;,5-6mrn)? DY., [11,�o N/A 15. fi`:) 'Wilik Present? Dyes []NO 051,11A 16. I lip Scats Present? OYLS Dtqo N/A Pacc Trip clank Lot ft (if Durchased): CLIENT NOTINCATIONIRESOLUTION Field Data Required? OYes 0No Person Contacted: Date/Time: Coniments/Resolution: PrOjECt Manager SCURF Review: Date: Project Manager SRF Review: LX\ u bate; i Is a discrepancy affecting NorthCarolina compliance Samples, a copy of tills form,/H be sentto the NorthCarolina DEIINRCedification Office (i.e. Z'.,! ho,!o ; . lriC;lrqrt rirt?Seivaii,,o, t)tj,, oftcmp, IncoreLo C011t3inerS) Page 8 of 9 �U v SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT { " for North Carolina Division of Water Quality General Permit No. NCG060000 V��k Date submittedCERTIFICATE OF COVERAGE NO. NCG' 61 FACILITY NAME rat K%r t7 14w 5f COUNTY PERSON COLLECTING SAMPLES mirtuid W,54cwd_ LABORATORY {tea G �e Lab Cert. # G( f _ Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR Z C f FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ❑ use animal fats/byproducts DISCHARGING TO SALTWATERS? ❑YES [iV0 PLEASE REMEMBER TO SIGN ON THE REVERSE --1 Total event rainfall 2�, N or ❑ No discharge this perioa`3 Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark - 100 or 50 Within 6.0 — 9.0 120 30 1000 500 1 I ,a G•Z 0 1 Only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies, Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes [Rno Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 3D 100 or 5046.0 -• 9.0 - 1 Only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if es, complete Part B) SWU-249 Last Revised: October 18, 2012 Page 1 of 2 s 7 '0�011 PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring_ period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 7h tI (L (Signature,,Aflgrmittee) (Date) Additional copies of this form may be downloaded at:.http:/ZRortal.ncdenr.org/web/`wg/ws/`su/­npdessw#tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 TLRM''','llfRDISCHARGE OUTFAtL �SD©) - Semi-Annu aaI MONITORNG FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE NO. INCG.24_.o I C% FACILITY NAME: -i- PERSON COLLECTING SAMPLES T&IS CERTIFIED LABORATORY C _ Lab # Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: Zo I SAMPLING PERIOD: [ July -December [] January -June COUNTY PHONE NO. (3A )_ 5L41 -/A Z 7 ADD TO LISTSERVE? []YES ❑NO EMAIL: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trout 0OYher Outfall No. Date Sample Collected (mo/dd/yr OR 1 NO FLOW] pH (Standard Units) TS5 (mg/L) Event Duration (minutes) i atal 4 Rainfall (in) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier z 2 Sampling » - 6-92 1002'3 1 !o S �� .� o NOV_ DWR S 2 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. z If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. B TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/I. For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. EIVED 2M4 Q FILES ZCTION Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar vear Outfall No. Date Sample Collected (mo/dd/yr); pH (Standard Units) TPH using method 1664A SGT-HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total Rainfalla (in) New Motor Oil Usage (gal/month) In In Tier TierZ Monthly Monitoring? (y/h) # of Months in Tier 2 2 Sampling 6-92 152 1002.3 - - - - - HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANYONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO ffT-' HAVE YOU CONTACTED THE REGION? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail Original and one copy of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample (or at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGIV THIS CERTIFICATION FOR ANY WFORMAT1O1V REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance With a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that t re are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." /D (Signature P ittee) (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 "I A NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit. httR//portal.ncdennorg/web/wq/ws/su/nodessw#tab-4 Permit No.: N/C/_/_/_/_/_/_/_/ or Certificate of Coverage No.: N/C/C/j/#/ Facility Name: PlArif 1 County: D wr wN r i Phone No. 9 l (44 -116 Z 7 Inspector: S Date of lnspectior . lb,r iS %1 Time of Inspection: Arm Total Event Precipitation (inches): o JO Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) EKYes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureahle storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be� performed during a "representative storm event" or during a "measureable storm event." However, same permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storin event that measures greater than 0.1 inches of rainfall 1 and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has Occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. !� i A "measurable storm event" is a storm event that results in an actual discharge from the l permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. _ __ __ By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature oAer�ttee or Designee) Page 1 of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description. Outfall No. { Structure (pip dot , etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: _T far 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Qln it 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 m. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes �. is there an ah sheen in the stormwater discharge? Yes iv �. Is there evidence of erosion or deposition at the outfall? Yes [Vo 10, Other Obvious -indicators of Stormwater pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2of2 SWU-242, Last modified 10/25/2012 AtIt . NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http://portal.ncdenr.org/wpb/-w—qLws/su/npdessw#tab-4 Permit No.: N/C/_/_/_/�/_/_/_/ or Certificate of Coverage No.: 71- Facility Name: County: r ' Phone No. Inspector: Lau W&TWbss Date of Inspection: Time of Inspection: /D/ Z7 AM Total Event Precipitation (inches): 1540 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signatugof 06rmittee or Designee) Page 1 of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. Z Structure (pip ditch c.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: C f A C 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Nhi-,-C 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: © 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 ® 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 TIN V 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe P 0 n "L Dote: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 aceAnalXical www.pacelabs.mm Jay Watkins Ready Mix Concrete PO Box 27326 Raleigh, NC 27611 Project: PLANT #17 HWY 55 Pace Project No.: 92221762 Sample: OUTFALL #1I1PLANT 17 Parameters Total Suspended Solids Sample: OUTFALL #21PLANT 17 Parameters Total Suspended Solids Reviewed by: Laura J Cooper Laboratory Report Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 1 Report Date: 10/31/2014 Date Received: 10/16/2014 Lab ID: 92221762001 Collected: 10/15/14 10:21 Matrix: Water Results Units Report Limit Analyzed Qualifiers 19.5 mg/L 3.2 10/22/14 09:59 Lab ID: 92221762002 Collected: 10/15/14 10:27 Matrix: Water Results Units Report Limit Analyzed Qualifiers 48.8 mg/L 6A 10/22114 M59 laura.cooper@pacelabs.com Raleigh Certification IDS 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 Page 1 of 3 Document Naftle. Sample Condition Upon DoWMent Revised: April 04,2013 -Recelpt (SCU.R) Page I of 2 Document No.: Issuing AuthodOes, F-FOAL-,CS-001-rov.02 Pace Asheville Quality office Client Name, Where Received: El Huntersylile Asheville [] Eden Nlelgh Cou ri to), Fed Ex UPS LISPS iS Commercial pow .Other custoil _WSQ�al on CoolorlSox Present: [] Yes 60 seals intact, )21'yw [ no K4itdrlall' [j Mble Wrap 'Bubb) E3 None nOiher Circle TheimornoterUsed: 1110.un SN122001' too: 6wf Blue None' [] $amplas on ice, 66difid process has_ begunIR Gun Smok Un SN: 122065371 Tamp C6rrectlon Factor: Add I Su tr ct 0.6 0 Re and Initlala ;f person qzamlnlno Corrected Cooler T'e'mp,., C Blo . I . ogic.a.1 Tissue Is Frozen. Yes'No Conte rose allo _jernA should be above freezing to M comments: ChdIn-'of0tistodyPreson1* oy" -ow 0HAA I.- - Chain of.Witody-Fillod Out Yes.11140 OWA 2...- Chain, of'custody RellnSwIshed. 'FLYRs ow UwA 3. _Sam pI0,r,,NaMa_.& Signature on COC: 15YO ONO 0 wX 4. Samples Arrived within Hold Time: L-K.. NO OWA 6.. " _14101w"M a short �fttd-.V o Anal ysls'(<7211r): OYQ%^ ORA B. Rush 44 bround Time Requested. , 1 Dyes OwA 7. es ElNo 'OKA 8. Corraat bgnlslners Used: ffy,a ONO. 0-W-A B. •Pe00,606talners Used: ON. MiA Containers Intact: J;ryas ONO E3wA ilb. Flllemt 6iurrio -received for Dissolved testa pes ONO OiA 11. Sample-lUbels match t=: 0?. ph. OWA 112.: All have bean Checked,, ONo ONJA All opnt8iriais beading preservation are found to be In eyes rlNo OWA bornOia4db-.'with EPA recornmeadauixt t�* L-1 4161K Tor, O&G, WORD (tyataq� 14qes ONo- fbr dechlorlm tion: OYev ONO )?rWA .14, '0'J1qV0AVials ( krrirn: 0yes 13NO fi3WA 15. Trlp"6,6 TF6sont­ OY. PNI Nlrl 16. trip, f, nk,`68tody -Seals Present CjYes ONO XNJA 1I'gce:Tflobiank Lot #(Ifpurchwe ClIont!Notifloation'/ Resolution' Field Data Required? y I N _v--!Porson Contacted: DatefrInne. QOMA96W. Resolution: t�RF Date: w SGfJ Place iabel here 4) Al Notes vr+hanever AID= rice -, 12. - 1 7, 62 Thera Is a d1scrapancy affectirto North Carolina cam (lance 1A sornpqs. qoopyof this form Will be sent to the North.Cerollna OEHNR ` C13rttfic`�tinri Office (ire out othold, Inoorrent proservallve, out of temp, Ifteorf6ot rontalners) t92222176 77 % Page 2 of 3 0'��J U-SiODY I Ana IyticaI Re quest�Documerot... .. ' _„ 9..p..gy�-,...f - •'�,^,:,,_ f'�' "' .. .,s:.^?.. !'t. � _:S:t:; ' . F t�-.. ,a• [ :..^-,-,....[ r,aTr, '1 r' ot-C:rstOd,R iS a LEAC DQGUSNEiIIT �dx rck ra fitfdt mu9t bB comPtetetl aCaurateh'• • 0 n •. 1IM f NPDES r ORMINDWATERf' M Codas SAMPLEID il VApe 'VVP Ak AR }Timsue TS• •I►7� • • •.� r Pace . .., NOJ Lab 11 . 1�� [� _... -- .•kA1v1aM MIY.�F.. GnNwn wie-hnn wr•.x�wn�MW. PwMiNGi��il..la.enaMY�./�W.�aaM fww.i.w.Mbb r�h.nwoM l,FllLww�mMW ♦�.vN iwM.W.•..^YI'�.vt�i i f. F4M I -0-020mv,07. 15-mw-?nn7 aj'& A:Z= RECEIVED MCDENR Stormwater Discharge Outfall (SDO) APR o 1 2014 Qualitative Monitoring Report: CENTRAL FILES DWQIBOG Forguidance 017 filling out thisfor'n7, please visit: hrti?: Permit No.: lV/C/_/_/_/_/_/T/�/ or Certificate of Coverage No.: N&IC j% 1 /y/? Facility Name: iP'lo.:4 11. _ tt"j-, 5 County: % L0A Phone No. gig-,gqq-1L-1 — inspector: Y%A 0. cc F2P. _ Date of Inspection: ', l 1h Time of Inspection: I c -. -e Qrn Total Event Precipitation (inches): 1� Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) VIY'es ❑ No Please verify 1.147ceher Qualitative Monitoring anist be performed during a "repre,.senl-otnle storn7 event" ar• `•r77easrlreoble storm event (requirernents vary, depending on the lie rr77it). Qualilative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "rneasureabie storm event," However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 130L1r5 (3 days) in which no storr3l event measuring greater than 0.1 inches has Occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storn-i event- that results in an actual discharge from the permitted site outfall. The prevrious measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, J certify that this report is accurate and complete to the best of my knowledge: (Signature olfermittee or Designee) Page 1 of 2 swu-2Q, Las[ niodirod 10/25/2012 1. Outfall Description: _ Outfall No. 1 Structure (pipe, itc , etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: N-r- 3. Odou n Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids. Choose the number which best describes the amount of Floating solids in the stormwater discharge, where 1 is no solids and S is the surface covered with floating solids: cif 2 3 4 5 6, Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4. 5 7. Is there any foam in the stormwater discharge? Yes B. Is there an oil sheen in the stormwater discharge? Yes 7� 9. Is there evidence of erosion or deposition at the outfall? Yes Vo 10, Other Obvious indicators of Stormwater Pollution: List and describe iti) V,\-� Mote: Low clarity, high solids, and/or the presence of foams, oil sheen, or erosion/deposition may he indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 Styli-242, Listmadified 10/25/2012 ff NCDENR Storrnwater Discharge ®utfall (SD®) Qualitative Monitoring Deport For guidance on filling out thisform, please visit: lit CLt/Elf �ry �l_. el rt3.s�i;;/�` Iyf lLti .ta n icl: ti is sfi,ik)A Permit No.: N&I—/_/_/_/_/_/_/ or Certificate of Coverage No.: Facility Name:-?'1z1,4 0 HIli 5 y County: Phone No. q14-54q-lte,'jj Inspector: A40 c4f cs Date of Inspection: ? ! Time of Inspection: la.1fS-A,�. Total Event Precipitation (inches): -?1 _ Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) V*Y�es ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable .storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureal) le storm event." However, I some permits do not have this requirement. Please refer to these definitions, if applicable. € t I A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall i i and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no ! precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature offermittee or Designee) Page 1 of 2 5WU-242, Last modified 10/25/2012 1. Outfall Description. Outfall No. ,1 Structure (pipe, , etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: P1. nj 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Q�,lr 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 Q 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 CJ! 3 4 S 6, Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4- 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes )lo 9. Is there evidence of erosion or deposition at the outfall? Yes 1� 10. Other Obvious Indicators of stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWii-242, Last modified 10/25/2012 ST®RMWATER DISCHARGE OUTFALL (S®®) m Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE NO. NCG14 D 1 a 9 FACILITY NAME: on+ (-i w• PERSON COLLECTING SAMPLES CERTIFIED LABORATORY frau Lab # C Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: 1 U1 tj. SAMPLING PERIOD: ❑ July -December © January -June COUNTY b i.,h.,L, PHONE NO. (9i 4 ADD TO LISTSERVE? ❑YES ❑NO EMAIL: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trout [:]Other Ou#fall No. Date Sample Collected (mo/dd/yr OR NO FLOW)1 PH (Standard Units TSS (mg/L) Event Duration (minutes) Total a Rainfall (in) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier 2 Samplingz - - fi-92 1002' - - - - 1J• W l .; S10 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. z If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. a TSS benchmark values are 100 mg/l, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/l. A For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Part 13: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor o!I/month — averaged over a calendar year Out#al! No. Date Sample Collected (mo/dd/yr}; pH (Standard Units) TPH using method 1664A SGT HEM {mg/L} Total Suspended Solids {mg/L} Event Duration {minutes} Total Rainfalla (in) New Motor Oil Usage (gal/month) Month! In Tier 2 y Monitoring? (y/n} # of Months in Tier 2 Z Sampling 6-92 15Z 100", - - - - HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO d HAVE YOU CONTACTED THE REGION? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail Original and one coov of this DMR [including all "No Flow" & "No Discharge" reports] within 30 days of receipt of sample (or at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." {Signature drl:�ermittee} alaby_ (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2of2 aceAnalytrcal www.pacarab.c= Laboratory Report MD Capps Ready Mix Concrete PO Box 27326 Raleigh, NC 27611 Project: PLANTS #17 Pace Project No.: 92193592 Pace Analytical Services, Inc. 9B00 KinceyAve. Suite 1o0 Huntersville, NC 28078 (704)875-9092 Page 1 of 1 Report Date: 03/25/2014 Date Received: 03/18/2014 Sample: OUTFALL 1 Lab ID: 92193592001 Collected: 03/17/14 10:41 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Suspended Solids 3.5 mg/L 2,5 03/22/14 11:38 Sample: OUTFALL 2 Lab ID: 92193592002 Collected: 03/17/14 10:46 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Total Suspended Solids 25.5 mg/L 3.1 03/22/14 11:39 Reviewed by: Nikitia .tones -Jackson nikitia.jones@pacelabs.com Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 Page 1 of 3 Report Results to: Ready Mixed Concrete P.O.Box 27326 Raleigh, NC 27611 Mb faef-:Y ATTN: lGii4nSAA6&n. Phone. 919-796-'1520 ►caf4 Chain of Custody Bill Results to: Ready Mixed Concrete P.O.Box 27326 Raleigh, NC 27611 :J'X� �;� ATTN: JQW1.1wiIsen Standard Report Delivery Rush Report Delivery (w/ surcharge) Requested Due Date: Project Reference: Plants #17 Purchase Order #: Sampled By: 02,/)LWp.t L M -0� e' IN I W.1 tali k�.� WOMEN 1. - - No 6-�-L� 0 Ew �K Outfall I G Sw TSS Y6 31t7ily Clutfall 2 G Sw TSS Relinquished by (signature) ReceiAed-by at D e Time z4 1" �� I .. M(Av ForLabUse Only Relinquished *'signature) Received by {signature) Da Time Temperature at receipt: Relinquished by (signature) Received by (signature) Date Time L--- I Temp: C' n 0 Document Name: Sample Condition Upon Document Revised: April 04, 2013 ZAnaVi-cal A receipt SCUR Page 1 of 2 Document No.: Issuing Authorities: F- L-CS- 01-rev:02 Pace Asheville QualityOffice Client Name., Where Received: Hunfersyille pnoo Eden Raleigh Courier (Circle): - Fed Ex UPS USPS Commercial Pace .Other Custody Seal on Cooler/Box Present: -yesSeals intact. yesEl no Packing Material: Bubble Wrap: lublags No Other Circle Thermometer Used: I.R Gu SN:122065387Type of tee: Wet Blue None E] Samples on ice, cooling process has begun IR Gun B 1 Temp Correctlon Factor: Add btract� r �. C Corrected Cooler Temp.: 0 r C Biological Tissue is Frozen: Yes No NIA Temp should be above freezing to VC Comments: Rate arid tnittals of person examining check t s Pr o Chain o€Custod Present s--[]No --ON/ A- 1.._..... Chain of Custody Fllied Out: Yes ©No. ❑rV1A 2,. Chain of. Custody Relinquished: Yes ❑No ❑N/A 3. Sampler Name& Signature on COC: Yos ❑No ❑NIA 4. Sa" ples Arrived within Hold Time: Yes -QNo ❑NIA 5.. Short Hold Time Analysis (<2hr): Dyes VNo ❑NIA 6. Rush Turn Around Time Requested: Dye's No ❑NIA 7. Suffioient Volume: es ❑No DWA g. Correct Containers Used: -Pace' Containers. Used: as ❑No VYes ❑No ❑NIA ❑NIA 9. . Containers Intact: es ONO ❑NIA 10. Filtered volums-received for Dissolved tests DYes ONO NIA 11. Sample Labels match COC: -includes dateltime/lD/Analysis Matrix: Yes No ❑NrA 12, All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptions; VOA, coliform, TOC, O&G, WI-ARO (water) es. ❑No Yes ❑No Z—fyes ❑No. ❑NIA ❑NIA 13. Samples checked for dechlorination': es ❑No ❑NIA 14, Heads pace In VOA Vials ( >6mm): []Yes ONO NIA 15. Trip Blank Present. Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased}_ Dyes ONO ❑Yes ONO NIA VNIA 16, Client Notification! Resolution: Field Data Required? y 1 N Person Contacted: Date/Time: Comments/ Resolution: SCURF ISRF Date: Review:: Note: Whenever there is a discrepancy affecting North Car li0,Mpin samples, a copy of this form will be sent to the North Carolina DEHNR Certification -Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) Place label here Page 3 of 3