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HomeMy WebLinkAboutNCG140112_MONITORING INFO_20181211STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. DOC TYPE ❑HISTORICAL FILE [$ MONITORING REPORTS DOC DATE p � o f � I c� 1 � YYYYMMDD ANNUAL SUMMARY DISCHARGE MONITORING REPORT (DMR) — STORMWATER SUBMIT TO CENTRAL OFFICE* General Permit No. NCG140000 Calendar Year o4)lef 'Report ALL STORMWATER monitoring data on this form (include "No Flow"( " c $e' Benchmark Exceedances) from the previous calendar year to the DEQ by M��i Certificate of Coverage No. NCG 14 ❑U [j]❑[ Facility Name: . - /�fi�y/ � CENTH-AL FILES County: &k%7 _ _ . Phone Number: {t;? 2 7 f.1 - 1?%yk Total no. of SDOs monitored Certified Laboratory4/��,�t� ire �_ Lab # /— Lab # Stormwater Discharge Outfall (SDO) No. VMA Outfall? Yes ❑ NoX Is this outfall currently in Tier 2 for any parameter? Yes ❑ No 0 Was this outfall ever in Tier 2 during the past year? Yes ❑ No If this outfall was in Tier 2 last year, was monthly monitoring discontinued? Yes, enough consecutive samples below benchmarks to decrease frequency ❑ Yes, received approval from DEMILR to reduce monitoring frequency ❑ Other ❑ Outfa I 1 N°' __�____ Total Rainfall; inches - Total. Suspended Solids (TSS), ...:m lI :. H , .. SLI., . on po ar.. (EPA Method 1664 SGT-FIE�li )) r mg1l (VMA) New Motoi Oil :Usage (gallmo.) ffappfrca6le Stormwater Benchmarks Irrriicale NO FLOWN appficabfe Circle Benchmark 100150 6.0-9.0 L J >SS gallmo, average requires T55 and Non -polar O&G monitoring Date Sample' Collected, moldd/yr ' ti - t Permit Date 8/1/2017 — 6/30/2022 Last Revised 8-22-2015 Certificate of Coverage No. NCG 14 ❑0❑❑ CERTIFICATION "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my know[edge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." [Required by 40 CFR §72 Signature /v^ Date Mail Annual Summary Stormwater WAR to the NCDEQ Central Office: Note the address is correct— Central Files is housed in DWR (not DEMLR) I.C. Department of Environmental Quality (DEQ) Division of Water Resources Attn: DWR Central Files 1617 Flail Service Center Raleigh, IBC 27699-1617 Central Files Telephone (919) 807-6300 Questions? Contact DEM!_R Stormwater Permitting Staff in the Central Office at: (919) 707-9220 Permit Date 8/112017 — 6/3012022 Last Revised 8-22-2075 ElMommmq % hmumbd Wastewater ZD: 10 114 OAKMONT DRIVE -- - - - -- - ---- - - ---� -- - - - PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 ARGOS READY MIXED(6214 WILLIAMSTON) QUINN VAUGHAN 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAMETERS PH (not to be used for reporting) Total Suspended Residue, mg/l Stormwater Analysis Method Discharge Date Analyst Code 8.4 11/13/18 JMS 4500HB-11 <2.6 11/14/18 ]TH 2540D-II ID#: 1095 DATE COLLECTED: 11/12/18 DATE REPORTED : 11/15/18 REVIEWED BY: EVN-Irorirrsent 1, Inc. t CHAIN OF CUSTODY RECORD P.O. Box 7085, 114 Oakmont Dr. Page I of Greenville. NC 27858 environment 1 inc.com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION Phone (252) 756-6208 • Fax (252) 756-0633 CHLORINE pHCHECK (LAB) CLIENT: logs Week:39 Ij uv p p CONTAINER TYPE, PIG ►RGOS READY M1XED(6214 WILLIAMSTON) ❑ NONE )UINN VAUGHAN 020 E. 5TH ST. CHEMICAL PRESERVATION ,VASHINGTON NC 27889 A A A - NONE D - NAOH o E 252) 717-0318 U 0 o d z0 z O' G] LU � B HNO, E HCL _ a U � o w C- HzSO4 F- ZINC ACETATE/NAOH COLLECTION J m o p S .. 2 < G - NATHiOSULFATE SAMPLE LOCATION DATE TIME r1 , Stormwater Discharge 1.7 I Eq C 1 CLASSIFICATION: L j WASTEWATER(NPDES) DRINKING WATER DWOIGW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING WMENT/DELIVERY Y N SAMPLES D BY: (Please Print) SAMPLES RECEIVED IN LAB AT"� °C RELINQUISHED BY (SIG:) (SAMPLER) j D IME 1�5-1,2 RE EIVED BY ( ) DATElRME COMMENTS: Au RELINQUIS D BY (A.) DATEITIME RECEI B (SIG.) DATEITIME } h3h -V a-v RELINQUISHED BY (SIG.) DATEMME RECEIVED BY (SIG.) DATETIME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for NO 338701 t,FORM #5 Grab sample in the blocks above for each parameter requested. e. SAMPLING INSTRUCTIONS AND FORM COMPLETION FAILURE TO PROPERLY CHILL, CHEMICALLY PRESERVE, COLLECT IN PROPER BOTTLE TYPES, MEET REQUIRED HOLDING TIMES, NEUTRALIZE CHLORINE IN CHLORINE SENSITIVE SAMPLES, AND SEAL COOLERS WITH TAPE WILL RESULT IN SAMPLES BEING REJECTED BY THIS LABORATORY AS PER NORTH CAROLINA REGULATORY CODE. 1) Samples not falling within the required guidelines will need to be re -collected. The client will be contacted and informed of any deviation and asked to collect another set of samples. The client may request the laboratory to proceed with the analyses of the current samples. Any samples analyzed outside of the required guidelines will be "qualified". This means that a note will be included on the sample result and "Chain of Custody" specifying the deviation. The laboratory is also required to send a letter to the State noting the deviations. 2) Sample Temperature. Samples for compliance monitoring must be chilled with wet ice to a temperature of 6C or less. Freezing is not permitted. Samples delivered to the lab shortly after collection may not have had enough time to be chilled below 6C. In this case the temperature at time of collection must be noted in the space provided. The samples will meet the requirements of the regulation if there is a temperature drop from the time of collection until received in the lab. Regardless, all samples should be packed in wet ice using as much ice as will fit in the cooler. 3) Sample Chemical Preservation. Many samples require a chemical preservation such as Sulfuric Acid or Sodium Hydroxide. The laboratory will either provide the preservative in the sample bottle, or in the case of 40 ml. Volatiles Vials, provide a bottle of Acid with detailed descriptions on how to collect the sample. Never rinse sample bottles before collecting samples. Any residue or liquid in the bottle is required for proper chemical preservation. The lab must verify proper chemical preservation upon arrival in the lab and will note this information in the spaces provided on the front of this form. 4) Chlorine Neutralization. Some samples require that any Total Chlorine Residual be removed at the time of collection. The lab will provide the proper neutralizing agent in the sample bottle when technically possible. There are some samples (Total Kjeldahl Nitrogen and Ammonia Nitrogen) where this is not possible due to interferences between the required chemical preservation (Acid) and the dechlorinating agent. Therefore, these samples must be de -chlorinated at the time of collection before being placed in our sample bottles. Sodium Thiosulfate is the chemical of choice to neutralize chlorine. It must be added to your sample and then the sample checked for Total Chlorine before the sample is poured in our bottle. Facilities using chlorine for disinfection should have a means of measuring Total Chlorine. Non -chlorinated sample sources will not need to be checked. The person neutralizing the chlorine must put his initials in the "Chlorine Neutralized at Collection" row on the front of this form above the proper parameter. Samples such as Coliforms (which have Thiosulfate in the bottles shipped from the lab) will be checked for proper neutralization upon arrival in the lab. It is also required that you note the "Total Chlorine at Collection" on the front of this form for any sample locations applicable. This value would be before any neutralization is performed. 5) A "C" for Composite Sample or a "G" for Grab Sample should be placed in the box for all requested parameters. Grab temperatures as well as Composite start dates and times can be recorded in the "comments" section. 6) Other information required to be completed by the client are: Collection Date and Collection Time for each sample location Temperature at Time of Collection Printed name of -person or persons collecting samples Signature, Date, and Time samples are relinquished Other added sample locations and analyses required Type Of Disinfection Deletion on the form for any samples which are not needed (example: dry upstream location) Any other information felt to be pertinent should be included in the "Comments" section CONSIDERATIONS: Coliform and Enterococci samples have a holding time of hours from time of collection to time of analysis. Therefore, samples should be collected as late in the day as possible to allow enough time for transportation, checking in at the lab and analysis. SOD, Nitrate, Ortho Phosphorus, Settleable Matter, Turbidity, Color, and M BAS samples have a 48 hour holding time. The lab reserves the right to establish required sample collection and delivery dates in order to meet the required holding times. CAUTION Sample bottles may contain acids or other corrosive and potentially harmful chemicals. Laboratories are required to add these chemicals for certain analyses in order to comply with EPA preservation requirements. Use extreme care when opening and handling the shipping container and bottles. If any chemical should get into your eyes, on your skin or on your clothes, flush liberally with water and seek medical attention. Material Safety Data Sheets (MSDS) are available upon request which specify proper handling and personal protection. ANNUAL SUMMARY DISCHARGE MONITORING REPORT (DMR) — STORMWATER SUBMIT TO CENTRAL OFFICE* General Permit No. NCG140000 Calendar Year cZ019 *Report ALL STORMWATER monitoring data on this form (include "No Flow'T'No Discharge" and Benchmark Exceedances) from the previous calendar year to the DEQ by MARCH 1 of each year. Certificate of Coverage No. NCG14 Om©® Facility Name: AS ,��r9i /y%�'�E� County: g2,l�rr� Phone Number. QS.Z )_ 'jQ, - 31-49 _ Total no. of SDOs monitored Certified Laboratory,&N/idr (_ Lab # (U Lab # Stormwater Discharge Outfall (SDO) No. VMA Outfall? Yes ❑ Nog Is this outfall currently in Tier 2 for any parameter? Yes ❑ No 0 Was this outfall ever in Tier 2 during the past year? Yes ❑ No g] If this outfall was in Tier 2 last year, was monthly monitoring discontinued? Yes, enough consecutive samples below benchmarks to decrease frequency ❑ Yes, received approval from DEMLR to reduce monitoring frequency ❑ Other ❑ Outfall No. Total Rainfall; inches -- Total Suspended p Solids TSS (.. ..�, ..'.m /I,Napplicable.' H p � SU. Non -polar 08r,G (ESA Method 1664 SGT-HEM , ( }}� : mgll (VMA)_ _ New Motor Oil Usage (gallmo.) lrapplfcabre Stormwater Benchmarks Indicate NO FLOW ff applicable Circle Benchmark 0 100�5fl 6.0-9.0 1 b >55 galfine. average requires TSS and Non -polar C&Q monitoring Date Sampler Collected molddlyr . R E C E IVIE, ki nv y A OMR CENTRAL FILL .'S DVTR SEA I i c rq Permit Date 8/1/2017 — 6/30/2022 Last Revised 8-22-2015 Certificate of Coverage No, NCG14 ❑❑❑❑ CERTIFICATION I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false informationt1-0cluding the possibility of fines and imprisonment for knowing violations." Required by 40 CFR §122.2 Signature Date ,111-46 Mail Annual Summary Stormwater DMR to the NCDEQ Central Office: Note the address is correct — Central Files is housed in D WR (riot DEMLR) N.C. Department of Environmental Quality (DEQ) Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files Telephone (919) 807-6300 Questions? Contact DEMLR Stormwater Permitting Staff in the Central Office at: (919) 707-9220 Permit Date 811/2017 — 6/30/2022 Last Revised 8-22-2015 Eflwohumml T, kwno wmuo Was tewater:ID:-10 P.O. BOX 7085, 114 OAI(iVIONT DFiIV ---PHONE (252) 756-6208 GREENVILLE, N.C. 27835-7085 FAX (252) 756-0633 ARGOS READY MIXED(6214 WILLIAMSTON) QUINN VAUGHAN 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAMETERS PH (not to be used for reporting) Total Suspended Residue, mg/l Stormwater Analysis Method Discharge Date Analyst Code 6.4 04/25/18 Hl'IN1 4500HB-11 2.9 .04/26/18 KDS 2540D-11 ID#: 1095 DATE COLLECTED: 04/24/18 DATE REPORTED : 04/27/18 REVIEWED BY: Environment 1, Inc. CHAIN OF CUSTODY RECORD P.O. Box 7085, 114 Oakmont Dr. Page I of Greenville, NC 27858 environment] inc.com Phone (252) Fax (252) 756-0633 DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION CHLORINE Ij CLIENTo w Week: 13 Ij uv pH CHECK (LAB) P P CONTAINER TYPE, PIG .EADY MIX CONCRETE (WILLIAMSTON) ❑ NONE IR. MIKE ODOM 020 E. 5TH ST. CHEMICAL PRESERVATION VASHINGTON NC 27889 A A �o E�-- A -NONE D-NAOH 013 252) 325-2004 z-j w Z LU B- HNO3 E HCL 00 a cc_ LU C - H2SO, F - ZINC ACETATEINAOH COLLECTION !;C-c a F o 6 ¢ 26 G - NATHIOSULFATE SAMPLE LOCATION DATE TIME y a.r p Stormwater Discharge a`r' j$ a✓�(,' I CLASSIFICATION: WASTEWATER(NPDES) DRINKING WATER DWOIGW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURI�MENT/DELIVERY N SAMPLES COLLECTED BY: (Please Print) SAMPLES RECEIVED IN LAB AT02(_°C R INO ISHED BY (SIG.) (SAMPLER) DATEf{ IM R ❑ BY DATEIrIME COMMENTS: RELINQUISHED B SIG.) DATE(IiME 17RECEIVED SIG.) DATEJIIME Z C3 RELINQUISHED BY (SIG.) DATE/TIME RECEIVED SIG. DATE TlME — - I il 61 - - PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G"for 0 341855 FORM #5 Grab sample in the blocks above for each parameter requested. SAMPLING INSTRUCTIONS AND FORM COMPLETION FAILURE TO PROPERLY CHILL, CHEMICALLY PRESERVE, COLLECT IN PROPER BOTTLE TYPES, MEET REQUIRED HOLDING TIMES, NEUTRALIZE CHLORINE IN CHLORINE SENSITIVE SAMPLES, AND SEAL COOLERS WITH TAPE WILL RESULT IN SAMPLES BEING REXCTED BY THIS LABORATORY AS PER NORTH CAROLINA REGULATORY CODE. 1) Samples not falling within the required guidelines will need to be re -collected. The client will be contacted and informed of any deviation and asked to collect another set of samples. The client may request the laboratory to proceed with the analyses of the current samples. Any samples analyzed outside of the required guidelines will be "qualified". This means that a note will be included on the sample result and "Chain of Custody" specifying the deviation. The laboratory is also required to send a letter to the State noting the deviations. 2) Sample Temperature. Samples for compliance monitoring must be chilled with wet ice to a temperature of 6C or less. Freezing is not permitted. Samples delivered to the lab shortly after collection may not have had enough time to be chilled below 6C. In this case the temperature at time of collection must be noted in the space provided. The samples will meet the requirements of the regulation if there is a temperature drop from the time of collection until received in the lab. Regardless, all samples should be packed in wet ice using as much ice as will fit in the cooler. 3) Sample Chemical Preservation. Many samples require a chemical preservation such as Sulfuric Acid or Sodium Hydroxide. The laboratory will either provide the preservative in the sample bottle, or in the case of 40 mi. Volatiles Vials, provide a bottle of Acid with detailed descriptions on how to collect the sample. Never rinse sample bottles before collecting samples. Any residue or liquid in the bottle is required for proper chemical preservation. The lab must verify proper chemical preservation upon arrival in the lab and will note this information in the spaces provided on the front of this form. 4) Chlorine Neutralization. Some samples require that any Total Chlorine Residual be removed at the time of collection. The lab will provide the proper neutralizing agent in the sample bottle when technically possible. There are some samples (Total Kjeldahl Nitrogen and Ammonia Nitrogen) where this is not possible due to interferences between the required chemical preservation (Acid) and the dechlorinating agent. Therefore, these samples must be de -chlorinated at the time of collection before being placed in our sample bottles. Sodium Thiosulfate is the chemical of choice to neutralize chlorine. It must be added to your sample and then the sample checked for Total Chlorine before the sample is poured in our bottle. Facilities using chlorine for disinfection should have a means of measuring Total Chlorine. Non -chlorinated sample sources will not need to be checked. The person neutralizing the chlorine must put his initials in the "Chlorine Neutralized at Collection" row on the front of this form above the proper parameter. Samples such as Coliforms (which have Thiosulfate in the bottles shipped from the lab) will be checked for proper neutralization upon arrival in the lab. It is also required that you note the "Total Chlorine at Collection" on the front of this form for any sample locations applicable. This value would be before any neutralization is performed. 5) A "C" for Composite Sample or a "G" for Grab Sample should be placed in the box for all requested parameters. Grab temperatures as well as Composite start dates and times can be recorded in the "comments" section. 6) Other information required to be completed by the client are: Collection Date and Collection Time for each sample location Temperature at Time of Collection Printed name of person or persons collecting samples Signature, Date, and Time samples are relinquished Other added sample locations and analyses required Type Of -Disinfection Deletion on the form for any samples which are not needed (example: dry upstream location) Any other information felt to be pertinent should be included in the "Comments" section CONSIDERATIONS: Coliform and Enterococci samples have a holding time of 6 hours from time of collection to time of analysis. Therefore, samples should be collected as late in the day as possible to allow enough time for transportation, checking in at the lab and analysis. BOD, Nitrate, Ortho Phosphorus, Settleable Matter, Turbidity, Color, and WAS samples have a 48 hour holding time. The lab reserves the right to establish required sample collection and delivery dates in order to meet the required holding times. CAUTION Sample bottles may contain acids or other corrosive and potentially harmful chemicals. laboratories are required to add these chemicals for certain analyses in order to comply with EPA preservation requirements. Use extreme care when opening and handling the shipping container and bottles. If any chemical should get into your eyes, on your skin or on your clothes, Hush liberally with water and seek medical attention. Material Safety Data Sheets (MSDS) are available upon request which specify proper handling and personal protection. STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVJ FACILITY NAME: A PERSON COLLECTING CERTIFIED LABORATC RAGE NOS NC sir14� Q� MPLES _L�+r(oS' _ 1��/iCLu �Il�tll5nir+►�..� i X� Lab # Lab # OPTIONAL INFO: Part A: Stormwater Monitorine Requirements REC NsEMPLE COLLECTION YEAR: aG17 nI~ r 0 7 2SAMPLING RIOD: July -December ❑ January -June COUNTY �6Z.4g , 1 RA FIP_HQNE NO. (2,12 1 u vr[ C,TIADDTO LISTSERVE? ❑YES ONO EMAIL: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trout ❑Other, Outfall No. Date Sample Collected (mo/dd/yr OR NO FLOW)t pM {Standard Units) TSS (mg/L) Event Duration (minutes} Total Rainfall , (in) In Tier Monthly Monitoring? (y/n) # of Months in z Tier 2 Sampling - r7'�� / Zv /t & 4 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfali here. Please make sure to mark the sample period above. z if a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/l, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/l. For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outfall No. Sample Date Sam p Collected (mo/dd/yr)l pH (Standard Units( TPH using method 1664A SGT-HEM (mg/i) Total Suspended Solids (mg/L) Event Duration (minutes) Total Rainfall° (in) New Motor Oil Usage (gal/month) In Tier 2 Monthly Monitoring? (y/n' # of Months in Tier 2 2 Sampling 6-9 15 100 Z,3- - - HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDS ES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO 1[ HAVE YOU CONTACTED THE REGION? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail Original and one copy of this DMR(including all "No Flow" & "No Dischar e" reports) within 30 days of recei t of sample or at end of monitoring eriod in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualifi personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons 5KItly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware th ere aA;gnificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ure of Permitteej Permit Date:7/1/2011-60/30/2015 /Z-4/-i7 (Date] Last Revised 7/13/11 Page 2 of 2 EIMADT01mmimq % horpoTmOd Wastewater ID: 10 P.O. BOX 7085, 114OAKMONT DRIVE- - PHONE (252) 7564208 GREENVILLE, N.C. 27835-7085 FAX (252) 756-0633 READY MIX CONCRETE (WILLIAMSTON) MR. MIKE ODOM 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAMETERS PH (not to be used for reporting) Total Suspended Residue, mg/I Stormwater Analysis Method Discharge Date Analyst Code 7.8 11/09/17 KDS 4500HB-11 1.6 11/10/17 KAC 2540D-11 ID#: 1095 DATE COLLECTED: 11/09/17 DATE REPORTED : 11/13/17 REVIEWED BY: Environment 1, Inc. CHAIN OF CUSTODY RECORD P.O. Box 7085, 114 Oakmont Dr. Page Iof Greenville, NC 27858 environment] inc.com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION Phone (252) 756-6208 • Fax (252) 756-0633 CHLORINE CLIENT: 1095 Week:39 uv pHCHECK (LAB) READY Iti9IX CONCRETE (WILLIANISTON) ❑ NONE P P CONTAINER TYPE, PIG NIR. NI1KE OD01I CHEMICAL PRESERVATION 1020 E. 5TH ST. WASHINGTON NC 27889 A A o A -NONE D-NAOH (252) 325-2004 E ui U z 1-4 w Z °; rn w � B - HNO3 E - HCL OO z C LU = F ¢ �� w C - HZSO, F - ZINC ACETATE/NAOH COLLECTION o g Vj ¢ y a G - NA THIOSULFATE a SAMPLE LOCATION DATE TIME Stormwater Discharge �� ' TEN IE s I � C I CLASSIFICATION: WASTEWATER(NPDES) DRINKING WATER DWOIGW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY N SAMPLES COLLECTED BY: (Please Print) SAMPLES RECEIVED IN LAB AT _ °C R lNQU1SHE Y (SIG.) (SAMPLER) lull E�� RE D BY G COMMENTS: �� 1� 9717ji, Gr./'r jajE (+ RELINQUISHED B SIG.) DATE/T1ME ECENE Y IG.)K—)Iy, D TEMME t1 RELINQUISHED BY (SIG.) DATE/TIME RECEIVE SIG. DATE/TIME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C"for composite sample or a "G" for N 2 337564 FORM as Grab sample in the blocks above for each parameter requested. SAMPLING INSTRUCTIONS AND FORM COMPLETION FAILURE TO PROPERLY CHILL, CHEMICALLY PRESERVE, COLLECT IN PROPER BOTTLE TYPES, MEET REQUIRED HOLDING TIMES, NEUTRALIZE CHLORINE IN CHLORINE SENSITIVE SAMPLES, AND SEAL COOLERS WITH TAPE WILL RESULT IN SAMPLES BEING REJECTED BY THIS LABORATORY AS PER NORTH CAROLINA REGULATORY CODE. 1) Samples not falling within the required guidelines will need to be re -collected. The client will be contacted and informed of any deviation and asked to collect another set of samples. The client may request the laboratory to proceed with the analyses of the current samples. Any samples analyzed outside of the required guidelines will be "qualified". This means that a note will be included on the sample result and "Chain of Custody" specifying the deviation. The laboratory is also required to send a letter to the State noting the deviations. 2) Sample Temperature. Samples for compliance monitoring must be chilled with wet ice to a temperature of 6C or less. Freezing is not permitted. Samples delivered to the lab shortly after collection may not have had enough time to be chilled below 6C. In this case the temperature at time of collection must be noted in the space provided. The samples will meet the requirements of the regulation if there is a temperature drop from the time of collection until received in the lab. Regardless, all samples should be packed in wet ice using as much ice as will fit in the cooler. 3) Sample Chemical Preservation. Many samples require a chemical preservation such as Sulfuric Acid or Sodium Hydroxide. The laboratory will either provide the preservative in the sample bottle, or in the case of 40 mi. Volatiles Vials, provide a bottle of Acid with detailed descriptions on how to collect the sample. Never rinse sample bottles before collecting samples. Any residue or liquid in the bottle is required for proper chemical preservation. The lab must verify proper chemical preservation upon arrival in the lab and will note this information in the spaces provided on the front of this form. 4) Chlorine Neutralization. Some samples require that any Total Chlorine Residual be removed at the time of collection. The lab will provide the proper neutralizing agent in the sample bottle when technically possible. There are some samples (Total Kjeldahl Nitrogen and Ammonia Nitrogen) where this is not possible due to interferences between the required chemical preservation (Acid) and the dechlorinating agent. Therefore, these samples must be de -chlorinated at the time of collection before being placed in our sample bottles. Sodium Thiosulfate is the chemical of choice to neutralize chlorine. It must be added to your sample and then the sample checked for Total Chlorine before the sample is poured in our bottle. Facilities using chlorine for disinfection should have a means of measuring Total Chlorine. Non -chlorinated sample sources will not need to be checked. The person neutralizing the chlorine must put his initials in the "Chlorine Neutralized at Collection" row on the front of this form above the proper parameter. Samples such as Col iforms (which have Thiosulfate in the bottles shipped from the lab) will be checked for proper neutralization upon arrival in the lab. It is also required that you note the "Total Chlorine at Collection" on the front of this form for any sample locations applicable. This value would be before any neutralization is performed. 5) A "C" for Composite Sample or a "G" for Grab Sample should be placed in the box for all requested parameters. Grab temperatures as well as Composite start dates and times can be recorded in the "comments" section. 6) Other information required to be completed by the client are: Collection Date and Collection Time for each sample location Temperature at Time of Collection Printed name of person or persons collecting samples Signature, Date, and Time samples are relinquished Other added sample locations and analyses required Type Of'Disinfection Deletion on the form for any samples which are not needed (example: dry upstream location) Any other information felt to be pertinent should be included in the "Comments" section CONSIDERATIONS: Coliform and Enterococci samples have a holding time of 6 hours from time of collection to time of analysis. Therefore, samples should be collected as late in the day as possible to allow enough time for transportation, checking in at the lab and analysis. BOD, Nitrate, Ortho Phosphorus, Settleable Matter, Turbidity, Color, and MBAS samples have a 48 hour holding time. The lab reserves the right to establish required sample collection and delivery dates in order to meet the required holding times. CAUTION Sample bottles may contain acids or other corrosive and potentially harmful chemicals. Laboratories are required to add these chemicals for certain analyses in order to comply with EPA preservation requirements. Use extreme care when opening and handling the shipping container and bottles. If any chemical should get into your eyes, on your skin or on your clothes, flush liberally with water and seek medical attention. Material Safety Data Sheets (MSDS) are available upon request which specify proper handling and personal protection. STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT No. NCG140000 CERTIFICATE OF CO ERAGE NO. NCG14_Q_�_ j_o? FACILITY NAME: -e e.­ PERSON COLLECTING SAMPLES r CERTIFIED LABORATORY&dt i-vo rj C,4 Lab # Imo_ Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: ( 6/ -_ SAMPLING PERIOD: ❑ July -December X January -June COUNTY n PHONE NO. Qr2)_ qI1- 3lY� ADD TO LISTSERVE? ❑YES ZNO EMAIL: DISCHARGING TO CLASS: ❑SA ❑HCRW ❑PNA []Trout ❑Other Qutfall No. Date Sample Collected (mo/dd/yr OR NO FLOW)t pH (Standard units) TSS (mg/L) Event Duration (minutes) Total a Rainfall (in) In Tier 2 Monthly Monitoring? (y/n) is of Months in Tier 2 Sampling2 - 6-9 100 , - y`7 A S- ' If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. 2 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. a TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/I. `For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outfall No. Date Sample Collected (mo/dd/yr)1 pH (Standard Units) TPH using method 1664A SGT-HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total s Rainfall (in) New Motor Oil Usage (gal/month] In Tier 2 Monthly Monitoring? (Y/n) # of Months in Tier 2 . 2 Sampling 6-9 15 100 ' - HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO X HAVE YOU CONTACTED THE REGION? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail Original and one coov of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample (or at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUSTSIGN THIS CERTIFICATION FOR ANYINFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those perso 9812irectly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aZartthe are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." u&�r-/^7 (S' nature of Permittee) (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 EEw'DF@mH(M % hwT LOB .Wasfewntex� Ip ''chp P.O. BOX 7D85, 114 OAKMONT DRIVE -- — ---� -- - PHONE�(252) 756-6208 GREENVILLE, N.C. 27835-7085 FAX (252) 756-0633 READY MIX CONCRETE (WILLIAMSTON) MR. MIKE ODOM 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAMETERS PH (not to be used for reporting) Total Suspended Residue, mg/l Stormwater Analysis Method Discharge Date Analyst Code 6.7 04/26/17 KKM 4500HB-00 12 04/27/17 SDB 2540D-97 ID#: 1095 DATE COLLECTED: 04/25/17 DATE REPORTED : 04/28/17 REVIEWED BY: -Environment 1, Inc. P.O. B(7x-7085, 114 Oakmont Dr. Greenville. NC 27858 CHAIN OF CUSTODY RECORD Page —I— of _;_ environment 1 inc.com DISINFECTION Phone (252j 756-6208 • Fax (252) 756-0633 CHLORINE NEUTRALIZED AT COLLECTION CHLORINE CLIENT: 1()95 Week: 13 pHCHECK (LAB) UV P P CONTAINER TYPE, PIG READY MIX CONCRETE (WILLIAMSTON) ❑ NONE MR. MIKE ODOM CHEMICAL PRESERVATION 1020 E. 5TH ST. WASHINCTON NC 27889 A A A - NONE D - NAOH E o (252) 325-2004 v z_ 4 J „F 6 w _ 2 cn C B - HN01 E - HCL =C r z r ¢ w C - VO, F -ZINC ACETATE/NAOH COLLECTION U ¢ o o LL a ¢ 8 U_ �.. ° a r ¢ G - NATHIOSULFATE a SAMPLE LOCATION DATE TIME Stormwater Discharge 25 {/�J M 0 upl CLASSIFICATION: WASTEWATER(NPDES) LjDRINKING WATER LjDWQIGW Ij SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY N SAMPLES COLLECTED BY: (Please Print) SAMPLES RECEIVED IN LAB AT oC R NQ ISHE Y (SIG.) (SAMPLER) DATTErnMME REC D BY G.) DA�TJEMME COMMENTS: y' I./ /•W r RELINQUISHED (SIG.) DATEITIME RECEIVED (S .) DATE/TIME L ' UL RELINQUISHED BY (SIG.) DATEITIME RECEIVED BY (SIG.) DATEMME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C° for composite sample or a "G" for FORM #5 Grab sample in the blocks above for each parameter requested. N 2 330329 I SAMPLING INSTRUCTIONS AND FORM COMPLETION FAILURE TO PROPERLY CHILL, CHEMICALLY PRESERVE, COLLECT IN PROPER BOTTLE I TYP' ES, MEET REQUIRED HOLDING TIMES, NEUTRALIZE CHLORINE IN-'(HLORINE SENSITIVE SAMPLES, AND SEAL COOLERS WITH TAPE WILL RESULT IN SAMPLES BEING REJECTED BY THIS LABORATORY AS PER NORTH CAROLINA REGULATORY CODE. 1) Samples not falling within the required guidelines will need to be re -collected. The client will be contacted and informed of any deviation and asked to collect another set of samples. The client may request the laboratory to proceed with the analyses of the current samples. Any samples analyzed outside of the required guidelines will be "qualified". This means that a note will b.0 included on the sample result and "Chain of Custody" specifying the deviation. The laboratory is also required to send a letter to the State noting the deviations. ..r s'r .• j 2) Sample Temperature. Samples for compliance monifbring must be chilled with wet ice to a temperature of 6C br less. Freezing is not permitted. Samples delivered to the lab shortly after collection may not have had enough time to be chilled below 6C. In this case the temperature at time of collection must be noted in the space provided. The samples will meet the requirements of the regulation if there is a temperature drop from the time of collection until received in the lab. Regardless, all samples should be packed in wet ice using as much ice as will fit in the cooler. 3) Sample Chemical Preservation. Many samples require a chemical preservation such as Sulfuric Acid or Sodium -Hydroxide. The laboratory will either provide the preservative in the sample bottle, or in the case of 40 ml. Volatiles Vials, provide a bottle of Acid with detailed descriptions on how to collect the sample. Never rinse sample bottles before collecting samples. Any residue or liquid in the bottle is required for proper chemical preservation. The lab must verify proper chemical preservation upon arrival in the lab and will note this information in the spaces provided on the front of this form. 4) Chlorine Neutralization. Some samples require that any Total Chlorine Residual be removed at the time of collection. The lab will provide the proper neutralizing agent in the sample bottle when technically possible. There are some samples (Total Kjeldahl Nitrogen and Ammonia Nitrogen) where this is not possible due to interferences between the required chemical preservation (Acid) and the dechlorinating agent. Therefore, these samples must be de -chlorinated at the time of collection before being placed in our sample bottles. Sodium Thiosulfate is the chemical of choice to neutralize chlorine. It must be added to your sample and then the saniple checked for Total Chlorine before the sample is poured in our bottle. Facilities using chlorine for disinfection should have a means of measuring Total Chlorine. Non -chlorinated sample sources will not need to be checked. The person neutralizing the chlorine must put.his initials in the "Chlorine Neutralized at Collection" row on the front of this form above the proper parameter. Samples such as Coliforms (which have Thiosulfate in the bottles shipped from the lab) will be checked for proper neutralization upon arrival in the lab. It is also required that you note the "Total Chlorine at Collection" on the front of this form for any sample locations applicable. This value would be before any neutralization is performed. 5) A "C" for Composite Sample or a "G" for Grab Sample should be placed in the box for all requested parameters. Grab temperatures as well as Composite start dates and times can be recorded in the "comments" section. 6) Other information required to be completed by the client are: Collection Date and Collection Time for each sample location Temperature at Time of Collection Printed name of person or persons collecting samples Signature, Date, and Time samples are relinquished Other added sample locations and analyses required Type Of Disinfection Deletion on the form for any samples which are not needed (example: dry upstream location) Any other information felt to be pertinent should be included in the "Comments" section CONSIDERATIONS: Coliform and Enterococci samples have a holding time of 6 hours from time of collection to time of analysis. Therefore, samples should be collected as late in the day as possible to allow enough time for transportation, checking in at the lab and analysis. BOD, Nitrate, Ortho Phosphorus, Settleable Matter, Turbidity, Color, and MBAS samples have a 48 hour holding time. The lab reserves the right to establish required sample collection and delivery dates in order to meet the required holding times. CAUTION Sample bottles may contain acids or other corrosive and potentially harmful chemicals. Laboratories are required to add these chemicals for certain analyses in order to comply with EPA preservation requirements. Use extreme care when opening and handling the shipping container and bottles. If any chemical should get into your eyes, on your skin or on your clothes, flush liberally with water and seek medical attention. Material Safety Data Sheets (MSDS) are available upon request which specify proper handling and personal protection. STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE NO. NCG14& j_L zZ FACILITY NAME: &&/�1t1 (inrnc�c C,z_ PERSON COLLECTING SAMPLES &a,,& ,�'✓ruA CERTIFIED LABORATORY 1►enftupm. 1 Lab # ib Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements RECEIVED SAMPLE COLLECTION YEAR: 0?D14 SAMPLING �)4 luly-December ❑ January -June C COUNTY e% D PHONE NO. ADD TO LISTSERVE? []YES NO EMAIL: DISCHARGING TO CLASS: ❑]SA ❑HQW ❑PNA []Trout []Other Outfall No. Date Sample Collected (mo/dd/yr OR NO FLOW)t pH (Standard units) 7SS (mg/L) Event Duration (minutes) Total a Rainfail (in) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier 2 2 Sampling 5-9 100 . - - 12-Z 4- t G ' if "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sampie period above. 2 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/I. For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. JAN 17 2017 I NTRAL FILES WR SECTION Permit Date: 7/1/2011-50/30/2015 Last Revised 7/13/11 Page 1 of 2 6 � c q J � � 2 R / z\ � .� Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outfall No. Date Sample Collected (mo/dd/yr)1 pH (Standard Units) TPH using method 1669A SGT-HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total RainfaNa (in) New Motor Oil Usage (gal/month) ,; In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier 2 2 Sampling 6-9 15 100 ' r HAS YOUR FACILITY HAD a OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES [-]NO HAVE YOU CONTACTED THE REGION? YES ❑ N0;6 REGIONAL OFFICE CONTACT NAME: Mail Original and one coov of this DMR Uncludinp, all "No Flow" & "No Discharge" reports) within 30 days of receint of sample for at end of monitoring period in case of "No Flow" to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those person erectly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware there significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Sigpddture of Permittee) l-IZnry (Date) Permit Date:7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 ERw'w@10H(@M I hcm Nd P.O. BOX 7085, 114 OAKMONT GREENVILLE. N.G. 27835-7085 .'.Wastewater I,y: 10 ' IVE PHONE (252) 756-6208 FAX (252) 756-0633 READY MIX CONCRETE (WILLIAMSTON) MR. MIKE ODOM 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAIIF',TEKS Stormwater Analvsis Method Discharge Date Analvst Code PH (not to he used for reporting) 8.3 12/29/16 SDB 4500HB-00 "rota) Suspended Residue, mg/1 <2.7 12/30/16 KDS 2540D-97 ID#: 1095 DATE COLLECTED: 12/29/16 DATE REPORTED : 01/03/17 REVIEWED BY: Environment 1, Inc. CHAIN OF CUSTODY RECORD P.O. Box 70$5, 114 Oakmont Dr. Greenville, NC 27858 Page I of environment l ine.com DISINFECTION Phone *(252) 756-6208 • Fax (252) 756-0633 CHLORINE NEUTRALIZED AT COLLECTION CHLORINE Ij pH CHECK (LAB) CLIENT: 1095 Week: 39 UV p p CONTAINER TYPE, PIG READN' 11IN CONCRETE (WILLIA,ISTON) ❑ NONE AIR. ,HIKE OI)O\i CHEMICAL PRESERVATION 1020 E. 5TH ST. WASHINGTON NC 27889 A A CnA-NONE D-NAOH cm E F (252) 325-2004 z � Uj LU � B - HNO3 E - HCL 00 J cc 0 Z c w C- H2SO, F- ZINC ACETATEINAOH COLLECTION U Q o o �" ¢ 8G t - NATHIOSULFATE a SAMPLE LOCATION DATE TIME 5[ormuater Discharge p �+-� ! CLASSIFICATION: WASTEWATER(NPDES) DRINKING WATER DWOIGW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED PMENTIDELIVERY DURINn__ N SAMPLES COLLECTED BY: (Please Print) SAMPLES RECEIVED IN LAB ATO °C LINO ISHED BY (SIG.) (SAMPLER) DATEI IME RECEI ED BY (SIG D TEfnME COMMENTS: RELINQUIS D BY IG.) ME DE61 RECEIVE (SIG.) ATEMME r �f Alt �5b ' G RELINQUISHED BY SIG.) DATEIIME RECEIVED SIG. ATEITIME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C° for composite sample or a °G" for - FORM #5 Grab sample in the blocks above for each parameter requested. N o __ 3 12 5.4 1 SAMPLING INSTRUCTIONS AND FORM COMPLETION FAILURE TO PROPERLY CHILL, CHEMICALLY PRESERVE, COLLECT IN PROPER BOTTLE TYPES, MEET REQUIRED HOLDING TIMES, NEUTRALIZE CHLORINE IN CHLORINE SENSITIVE SAMPLES, AND SEAL COOLERS WITH TAPE WILL RESULT IN SAMPLES BEING REJECTED BY THIS LABORATORY AS PER NORTH CAROLINA REGULATORY CODE. 1) Samples not failing within the required guidelines will need to be re -collected. The client will be contacted and informed of any deviation and asked to collect another set of samples. The client may request the laboratory to proceed with the analyses of the current samples. Any samples analyzed outside of the required guidelines will be "qualified". This means that a note will be included on the sample result and "Chain of Custody" specifying the deviation. The laboratory is also required to send a letter to the State noting the deviations. 2) Sample Temperature. Samples for compliance monitoring must be chilled with wet ice to a temperature of 6C or less. Freezing is not permitted. Samples delivered to the lab shortly after collection may not have had enough time to be chilled below 6C. In this case the temperature at time of collection must be noted in the space provided. The samples will meet the requirements of the regulation if there is a temperature drop from the time of collection until received in the lab. Regardless, all samples should be packed in wet ice using as much ice as will fit in the cooler. 3) Sample Chemical Preservation. Many samples require a chemical preservation such as Sulfuric Acid or Sodium Hydroxide. The laboratory will either provide the preservative in the sample bottle, or in the case of 40 ml. Voiatiles Vials, provide a bottle of Acid with detailed descriptions on how to collect the sample. Never rinse sample bottles before collecting samples. Any residue or liquid in the bottle is required for proper chemical preservation. The lab must verify proper chemical preservation upon arrival in the lab and will note this information in the spaces provided on the front of this form. 4) Chlorine Neutralization. Some samples require that any Total Chlorine Residual be removed at the time of collection. The lab will provide the proper neutralizing agent in the sample bottle when technically possible. There are some samples (Total Kjeldahl Nitrogen and Ammonia Nitrogen) where this is not possible due to interferences between the required chemical preservation (Acid) and the dechlorinating agent. Therefore, these samples must be de -chlorinated at the time of collection before being placed in our sample bottles. Sodium Thiosulfate is the chemical of choice to neutralize chlorine. It must be added to your sample and then the sample checked for Total Chlorine before the sample is poured in our bottle. Facilities using chlorine for disinfection should have a means of measuring Total Chlorine. Non -chlorinated sample sources will not need to be checked. The person neutralizing the chlorine must put his initials in the "Chlorine Neutralized at Collection" row on the front of this form above the proper parameter. Samples such as Coliforms (which have Thiosulfate in the bottles shipped from the lab) will be checked for proper neutralization upon arrival in the lab. It is also required that you note the "Total Chlorine at Collection" on the front of this form for any sample locations applicable. This value would be before any neutralization is performed. 5) A "C" for Composite Sample or a "G" for Grab Sample should be placed in the box for all requested parameters. Grab temperatures as well as Composite start dates and times can be recorded in the "comments" section. 6) Other information required to be completed by the client are: Collection Date and Collection Time for each sample location Temperature at Time of Collection Printed name of person or persons collecting samples Signature, Date, and Time samples are relinquished Other added sample locations and analyses required Type Of Disinfection Deletion on the form for any samples which are not needed (example: dry upstream location) Any other information felt to be pertinent should be included in the "Comments" section CONSIDERATIONS: Coliform and Enterococci samples have a holding time of hours from time of collection to time of analysis. Therefore, samples should be collected as late in the day as possible to allow enough time for transportation, checking in at the lab and analysis. BOD, Nitrate, Ortho Phosphorus, Settleable Matter, Turbidity, Color, and MBAS samples have a 48 hour holding time. The lab reserves the right to establish required sample collection and delivery dates in order to meet the required holding times. CAUTION Sample bottles may contain acids or other corrosive and potentially harmful chemicals. Laboratories are required to add these chemicals for certain analyses in order to comply with EPA preservation requirements. Use extreme care when opening and handling the shipping container and bottles. If any chemical should get into your eyes, on your skin or on your clothes, flush liberally with water and seek medical attention. Material Safety Data Sheets (MSDS) are available upon request which specify proper handling and personal protection. �l"'` - .-S.TORMWATER.DISCHARGE-OUTFALL (SDO) - Semi-Annuai MONITORING FORM - GENERAL PERMIT NO. NCG140000 CERTIFICATE OF C ERAGE No. NCG14Q _L L FACILITY NAME: PERSON COLLECTING S MPLES- CERTIFIED LABORATORY arm- - V%f_ Lab # !a Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: ?Gt(- SAMPLING PERIOD: ❑ July -December January -June COUNTY ^ PHONE NO. (adZ j 17fZ' JVVP -- ADD TO LISTSERVE? ❑YES O EMAIL: DISCHARGING TO CLASS: nSA ❑HQW ❑PNA ❑Trout ❑Other Outfall No. Date Sample Collected (mo/dd/yr OR NO FLOW)1 pH [Standard Units) TSS (mg/L) Event Duration (minutes) Total 4 Rainfall (in) In Tier 2 Monthly Monitoring? n (y/ ) # of Months in Tier z 2 Sampling - - 6-9 100 2,3- - - - 1 A 4!r rp- A Dw "' LES I If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the Sample period above. 2 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/l. 4 For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 6aw —Part B:• Vehicle Maintenance Activity Monitoring Requirements for facilities using > SS gal of new motor oil/month — averaged over a calendar year. butfall ' No. Date Sample Collected (mo/d'd/Yr) pH ..: (Standard- Units)., TPH using method 1664A SGT-HEM ;(mg/L)------; Total Suspended _Solids (mg/L) Event Duration -(minutes) Total A Rainfall (in) New Motor Oil Usage (gal/month) In Tier 2 Monthly Monitoring? (Y/n) # of Months in Tier 2 2 Sampling 6-9 15 100 HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDS CES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NOZ HAVE YOU CONTACTED THE REGION? YES ❑ NOZ REGIONAL OFFICE CONTACT NAME: Mail Original and one copy of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample (or at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons dire responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that t e are ficant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permit Date:7/1/2011-60/30/2015 _of-f-Ile (Date) Last Revised 7/13/11 Page 2 of 2 NC 60 NO / / Eaw'UmEM % RommOod P.O. BOX 7085, 114 OAKMONT GREENVILLE, N.C. 27835-7086 READY MIX CONCRETE (WILLIAMSTON) MR. MIKE ODOM 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAMETERS PH (not to be used for reporting) Total Suspended Residue, mg/l Stormwater Analysis Method Discharge Date Analyst Code 6.9 02/25/16 CMC 4500HB-00 3.9 02/26/16 SDB 2540D-97 FAX (252) 756-0633 ID#: 1095 DATE COLLECTED: 02/24/16 DATE REPORTED : 02/29/16 REVIEWED BY: / = h:nvunEuncnt 1, 111c, CHAIN OF CUSTODY RECORD P.O. Rox 7085„) 14 Onknront Dr. Vage ! of I Greenville, NC 27858 environtile nll inc.com DISINFFCI'ION I'lume (252) 756-6208 • Fix (252) 756-0633 CHLORINE NEUTRALIZED AT COLLECTION Ij CH1.0[ZW1. pHCHECK (LAB) CLIENT: 1095 Week- 13 lJV p p CONTAINER TYPE, P/G READY MIX CONCRETE (WILLIAMSTOm NONE: MR. MIKE ODOM CHEMICAL PRESERVATION 1020 E. 5TH ST. WASHINGTON NC 27889 A A `r' A - NONE D • NAOH zo E (252) 325-2004 ? � w z w C B HNO E- HCL Cr o L z Cl) a = w w w C- H,SO, F- ZINC ACETATE/NAOH COLLECTION v c w 2 8 txcc G NATHIOSULFATE SAMPLE LOCATION DATE TIME 'ID- 'Cr)W¢ o F Stormwater Discharge �l� i� 1 CLASSIFICATION: WASTEWATER (NPDES) ORINKINGWATER DWQIGW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING kIIPMENT/DELIVERY N SAMPLES COLLECTED BY: (Please Print) SAMPLES RECEIVED IN LAB AT (J �L'C jRrIN0 1SHED Y (SIG.) (SAMPLER) DATFJTIME REC D BY IG DATE/t1ME COMMENTS: a-�s�c� 1 `,� G RELINQUISHED B . 'IG.) DATEITIME RECD BY (SIG OATFJTIM`E� �a K' �� I RELINQUISHED BY (SIG.) DATEITIME RECEIVED BY ( IC DATEMME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for N o 303.480 FOAM +rs Grab sample in the blocks above for each' parameter requested. STORM WA TERDISCHARGE-OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF C ERAGE NO. NCG14 5 _L L .2 FACILITY NAME: PERSON COLLECTING S MPLES- CQA.110t CERTIFIED LABORATORY C^G Lab # !a Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: ?61l- SAMPLING,,P,yEE��RIO��D: ❑ July -December January -June COUNTY PHONE NO. (292 ? 17t.1-X/YF ADD TO LISTSERVE? ❑YES O EMAIL: DISCHARGING TO CLASS: nSA ❑HQW ❑PNA ❑Trout []Other Outfall No. Date Sample Collected (mo/dd/yr OR NO FLOW}1 pH -ar. [Stand d . Units} TS5 {mg/L} Event Duration {minutes} Total 4 Rainfall (in} In Tier 2 Monthly Monitoring? (Y/n) H of Months in Tier 2 Samplingz - - 6-9 1001, - - - ' If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. 2 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/l, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/L For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outfall No, Date Sample collected r (ma/dd/yr) -PH.—.- . Standard � { ) Units 7PH using method 16S4A SGT-HEM =(m /Lj g .Total Suspended Soli ds' (mp,/l) Event Duration (rriinutes): Total a Rainfall (in) New Motor Oil usage .. (gal/month) In Tier 2 Monthly Monitoring) Wri) # of Months in.Tier2 . z Sampling HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDE CES AT ANYONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NOe HAVE YOU CONTACTED THE REGION? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail Original and one co Py of this DMR(including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample or at end of monitoring period in case of "No Flow" to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons dire responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that to acre jjyAficant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee Permit Date:7/1/2011-60/30/2015 197-4( go 0 (Date) Last Revised 7/13/11 Page 2 of 2 1. EmW'UmmH&W 90 hc TOW P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 READY MIX CONCRETE (WILLIAMSTON) MR. MIKE ODOM 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAMETERS PH (not to be used for reporting) Total Suspended Residue, mg/l Stormwater Analysis Method Discharge Date Analyst Code 6.9 02/25/16 CMC 4500HR-00 3.9 02/26/16 SDB 2540D-97 wastewater ID: 10 —_---PHONE (252) 756- 2208 FAX_(252) 756-0633 ID#: 1095 DATE COLLECTED: 02/24/16 DATE REPORTED : 02/29/16 REVIEWED BY: Environment 1, Inc. CHAIN OF CUSTODY RECORD P.O. Box 7085,.(14 Oakmont Dr. Greenville. NC 27858 Page 1 of environment] inc.com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION Phone (252) 756-6208 • Fax (252) 756-0633 CHLORINE CLIENT: 1095 Week: 13 pH CHECK (LAB) Ij UV P P CONTAINER TYPE, PIG READY INUX CONCRETE (WILLIANISTON) ❑ NONE NIR. MIKE ODOM 1020 E. 5TH ST. CHEMICAL. PRESERVATION WASHINGTON NC 27889 A A A - NONE D - NAOH E o (252) 325-2004 z LLI z � � B - HNO3 E - HCL O JO � O Z p� _ � 5 t w C - H2SO, F - ZINC ACETATE/NAOH COLLECTION w � 8 S LL 2 F, G - NATHIOSULFATE SAMPLE LOCATION DATE I TIME Storm -water Discharge /G /Z�''�D �Q 1 CLASSIFICATION: WASTEWATER (NPDES) DRINKINGWATER DWUGW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED OURINIPMENT/DELIVERY N SAMPLES COLLECTED BY: (Please Pdnt) SAMPLES RECEIVED IN LAB AT Q °C R NQ ISHED Y (SIG.) (SAMPLER) DATEMME REC D BY I DATEIl1ME COMMENTS: RELINQUISHED B IG.} DATEMME RECD BY (SIG DATFJTIME RELINQUISHED BY (SIG.) DATEMME RECEIVED BY (I DATEMME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G for FORM #5 Grab sample in the blocks above for each parameter requested. No - - _ 303480 SAMPLING INSTRUCTIONS AND FORM. COMPLETION FAILURE TO PROPERLY CHILL, CHEMICALLY PRESERVE, COLLECT IN PROPER BOTTLE TYPES, MEET REQUIRED HOLDING TIMES, NEUTRALIZE CHLORINE IN CHLORINE SENSITIVE SAMPLES, AND SEAL COOLERS WITH TAPE WILL RESULT IN SAMPLES BEING REJECTED BY THIS LABORATORY AS PER NORTH CAROLINA REGULATORY CODE. 1) Samples not falling within the required guidelines will need to be re -collected. The client will be contacted and informed of any deviation and asked to collect another set of samples. The client may request the laboratory to proceed with the analyses of the current samples. Any samples analyzed outside of the required guidelines will be "qualified". This means that a note will be included on the sample result and "Chain of Custody" specifying the deviation. The laboratory is also required to send a letter to the State noting the deviations. 2) Sample Temperature. Samples for compliance monitoring must be chilled with wet ice to a temperature of 6C or less. Freezing is not permitted. Samples delivered to the lab shortly after collection may not have had enough time to be chilled below 6C. In this case the temperature at time of collection must be noted in the space provided. The samples will meet the requirements of the regulation if there is a temperature drop from the time ofcollection until received in the lab. Regardless, all samples should be packed in wet ice using as much ice as will fit in the cooler. 3) Sample Chemical Preservation. Many samples require a chemical preservation such as Sulfuric Acid or Sodium Hydroxide. The laboratory will either provide the preservative in the sample bottle, or in the case of40 mi. Volatiles Vials, provide a bottle of Acid with detailed descriptions on how to collect the sample. Never rinse sample bottles before collecting samples. Any residue or liquid in the bottle is required for proper chemical preservation. The lab must verify proper chemical preservation upon arrival in the lab and will note this information in the spaces provided on the front of this form. 4) Chlorine Neutralization. Some samples require that any Total Chlorine Residual be removed at the time of collection. The lab will provide the proper neutralizing agent in the sample bottle when technically possible. There are some samples (Total Kjeldahl Nitrogen and Amtnonia Nitrogen) where this is not possible due to interferences between the required chemical preservation (Acid) and the dechlorinating agent. Therefore, these samples must be de -chlorinated at the time of collection before being placed in our sample bottles. Sodium Thiosulfate is the chemical of choice to neutralize chlorine. It must be added to your sample and then the sample checked for Total Chlorine before the sample is poured in our bottle. Facilities using chlorine for disintection should have a means of measuring Total Chlorine. Non -chlorinated sample sources will not need to be checked. The person neutralizing the chlorine must put his initials in the "Chlorine Neutralized at Collection" row on the front of this form above the proper parameter. Samples such as Coliforms (which have Thiosulfate in the bottles shipped from the lab) will be checked for proper neutralization upon arrival in the lab. It is also required that you note the "Total Chlorine at Collection" on the front of this form for any sample locations applicable. This value would be before any neutralization is performed. 5) A "C" for Composite Sample or a "G" for Grab Sample should be placed in the box for all requested parameters. Grab temperatures as well as Composite start dates and times can be recorded in the "comments" section. 6) Other information required to be completed by the client are: Collection Date and Collection Time for each sample location Temperature at Time of Collection Printed name of person or persons collecting samples Signature, Date, and Time samples are relinquished Other added sample locations and analyses required Type Of Disinfection Deletion on the form for any samples which are not needed (example: dry upstream location) Any other information felt to be pertinent should be included in the "Comments" section CONSIDERATIONS: Coliform and Enterococci samples have a holding time of 6 hours from time of collection to time of analysis. Therefore, samples should be collected as late in the day as possible to allow enough time for transportation, checking in at the lab and analysis. BOD, Nitrate, Ortho Phosphorus, Settleable Matter, Turbidity, Color, and MBAS samples have a 48 hour holding time. The lab reserves the right to establish required sample collection and delivery dates in order to meet the required holding times. CAUTION Sample bottles may contain acids or other corrosive and potentially harmful chemicals. Laboratories are required to add these chemicals for certain analyses in order to comply with EPA preservation requirements. Use extreme care when opening and handling the shipping. container and bottles. If any chemical should get into your eyes, on your skin or on your clothes, Hush liberally with water and seek medical attention. Material Safety Data Sheets (MSDS) are available upon request which specify proper handling and personal protection. r STORMWA TER -DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF C RAGE NO. NCG14D- L FACILITY NAME: a C ' Go lot" #a PERSON COLLECTING SAMPLES 6 M CERTIFIED LABORATORY4Ajef&A ,&ft+ !L rc Lab # 10 Lab # OPTIONAL INFO: Part A. Stormwater Monitoring Requirements RECEIVED SAMPLE COLLECTION YEAR: aO 19 DEC 0 4 2015 SAMPLING PERIOD: duly -December ❑ January-JuneCENTRAL FILES COUNTY /�24r, -- DWR SECTION PHONE NO. (2faj ri%,Z - <<i ADD TO LISTSERVE? DYES ®NO EMAIL: DISCHARGING TO CLASS: [_]SA ❑HQW ❑PNA ❑Trout [-]Other w a Outfall No r� " r Date Sample{ fr . Collected s t NOFLOW). w P (Standard v Um nits u �,TSS f 5 Event s : { Duration =x tMonitoring. minutes j,.'(in)'{y Total x. a .,. Rainfall .In'Tie 2'< t•: Monthly / nj Ka ,,. # of Months in -Tier ; z 2 Sampling M ' If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. 2 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/I. °For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date:7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 . I Part B: 4i�hicie Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. iF ' pH TPH.using method Total Suspended,' Event Total ,.New Motor Oil �� hly # of Months . Outfall . � Date Sam le � ., P (Standard ,, 1664A�SGT HEM Solids :, . Duration 4 Rainfall usage in Tler Z ­ No. . Collected i Units]=ln�gll) ..... (m/L. ) (minutes) (in) (gal/itfonth) + Monitoring. ;.., 'Sampling (ma/dd/yr} :°°', (y/n) HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NOg HAVE YOU CONTACTED THE REGION? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail Original and one copy of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample (or at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED. - "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those person irectly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware =there si nificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �... (Sig(ature of Permittee) (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 Cf EE40mmmV Ala kc(mmumbd wastewater iD: iv fP.O. BOX 7485, 11, OAKMONT DRIVE -�� --- - - PHONE (252) 755-6208 GREENVILLE, N.C. 27835-7085 FAX (252) 756-0633 READY MIX CONCRETE (WILLIAMSTON) MR. MIKE ODOM 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAMETERS PH (not to be used for reporting) Total Suspended Residue, mg/I 0 Stormwater Analysis Method Discharge Date Analyst Code 7.9 10/28/15 CMC 4500HB-00 <2.8 10/29/15 KDS 2540D-97 ID#: 1095 DATE COLLECTED: 10/27/15 DATE REPORTED : 10/30/15 REVIEWED BY: Environment 1, Inc. CHAIN OF CUSTODY RECORD P.O. 13ox 7D85, 114 Oakmont Dr. Page I of Greenville, NC 27858 environment] inc.aom DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION Phone (252) 756-6208 • Fax (252) 756-0633 Ij CHLORINE pHCHECK (LAB) CLIENT. logs Week:39 Ij UV P P CONTAINER TYPE,P/G READY MIX CONCRETE (WILLIANISTON) ❑ NONE N1R. N1IKE ODOM CHEMICAL PRESERVAMON 1020 E. 5TH ST. WASHINGTON NC 27889 A A wA - NONE D - NAOH E o (252) 325-2004 Z � LLB,- z I G Cn � B - HNO, E - HCL 08 cc 0 w z p c � C- H2SO4 F- ZINC ACETATE/NAOH w COLLECTION o uU CL a U_ c x G - NATHIOSULFATE SAMPLE LOCATION DATE TIME Slormwater Discharge /d X l `S !7u 1 CLASSIFICATION: WASTEWATER(NPDES) DRINKING WATER DWOIGW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY 0 N SAMPLES COLLECTED BY: (Please Print) las b� ewM SAMPLES RECEIVED IN LAB AT °C R INOUISIHEED BY (SIG.) (SAMPLER) DATEMME RE Y } DATEMME COMMENTS: RELI BY ) DATE/TIME 4ECEIVE (SIG.) DATEMME r Wgj EUNOUISHED BY (SIG.) DATEMME RECEIVED BY (SIGV U D MMME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for N 0 306241 FORM as Grab sample in the blocks above for each parameter requested. SAMPLING INSTRUCTIONS AND FORM COMPLETION FAILURE TO PROPERLY CHILL, CHEMICALLY PRESERVE, COLLECT IN PROPER BOTTLE TYPES, MEET REQUIRED HOLDING TIMES, NEUTRALIZE CHLORINE IN CHLORINE SENSITIVE SAMPLES, AND SEAL COOLERS WITH TAPE WILL RESULT IN SAMPLES BEING REJECTED BY THIS LABORATORY AS PER NORTH CAROLINA REGULATORY CODE. 1) Samples not falling within the required guidelines will need to be re -collected. The client will be contacted and informed of any deviation and asked to collect another set of samples. The client may request the laboratory to proceed with the analyses of the current samples. Any samples analyzed outside of the required guidelines will be "qualified". This means that a note will be included on the sample result and "Chain of Custody" specifying the deviation. The laboratory is also required to send a letter to the State noting the deviations. 2) Sample Temperature. Samples for compliance monitoring must be chilled with wet ice to a temperature of 6C or less. Freezing is not permitted. Samples delivered to the lab shortly after collection may not have had enough time to be chilled below 6C. In this case the temperature at time of collection must be noted in the space provided. The samples will meet the requirements of the regulation if there is a temperature drop from the time of collection until received in the lab. Regardless, all samples should be packed in wet ice using as much ice as will fit in the cooler. 3) Sample Chemical Preservation. Many samples require a chemical preservation such as Sulfuric Acid or Sodium Hydroxide. The laboratory will either provide the preservative in the sample bottle, or in the case of 40 mi. Volatiles Vials, provide a bottle of Acid with detailed descriptions on how to collect the sample. Never rinse sample bottles before collecting samples. Any residue or liquid in the bottle is required for proper chemical preservation. The lab must verify proper chemical preservation upon arrival in the lab and will note this information in the spaces provided on the front of this form. 4) Chlorine Neutralization. Some samples require that any Total Chlorine Residual be removed at the time of collection. The lab will provide the proper neutralizing agent in the sample bottle when technically possible. There are some samples (Total Kjeldahl Nitrogen and Ammonia Nitrogen) where this is not possible due to interferences between the required chemical preservation (Acid) and the dechlorinating agent. Therefore, these samples must be de -chlorinated at the time of collection before being placed in our sample bottles. Sodium Thiosulfate is the chemical of choice to neutralize chlorine. It must be added to your sample and then the sample checked for Total Chlorine before the sample is poured in our bottle. Facilities using chlorine for disinfection should have a means of measuring Total Chlorine. Non -chlorinated sample sources will not need to be checked. The person neutralizing the chlorine must put his initials in the "Chlorine Neutralized at Collection" row on the front of this form above the proper parameter. Samples such as Coliforms (which have Thiosulfate in the bottles shipped from the lab) will be checked for proper neutralization upon arrival in the lab. It is also required that you note the "Total Chlorine at Collection" on the front of this form for any sample locations applicable. This value would be before any neutralization is performed. 5) A "C" for Composite Sample or a "C" for Crab Sample should be placed in the box for al I requested parameters. Grab temperatures as well as Composite start dates and times can be recorded in the "comments" section. 6) Other information required to be completed by the client are: Collection Date and Collection Time for each sample location Temperature at Time of Collection Printed name of person or persons collecting samples Signature, Date, and Time samples are relinquished Other added sample locations and analyses required Type Of Disinfection Deletion on the form for any samples which are not needed (example: dry upstream location) Any other information felt to be pertinent should be included in the "Comments" section CONSIDERATIONS: Coliform and Enterococci samples have a holding time of 6 hours from time of collection to time of analysis. Therefore, samples should be collected as late in the day as possible to allow enough time for transportation, checking in at the lab and analysis. BOD, Nitrate, Ortho Phosphorus, Settleable Matter, Turbidity, Color, and MBAS samples have a 48 hour holding time. The lab reserves the right to establish required sample collection and delivery dates in order to meet the required holding times. CAUTION Sample bottles may contain acids or other corrosive and potentially harmful chemicals. Laboratories are required to add these chemicals for certain analyses in order to comply with EPA preservation requirements. Use extreme care when opening and handling the shipping container and bottles. If any chemical should get into your eyes, on your skin or on your clothes, flush liberally with water and seek medical attention. Material Safety Data Sheets (MSDS) are available upon request which specify proper handling and personal protection. STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE NO. NCG14 I Z FACILITY NAME: keab. M+� V .78 PERSON COLLECTING SAMPLES Og f`/V " CERTIFIED LABORATORY,6nyir-mr"e& /j jeLab# Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: ZoJS c, SAMPLING PERIOD ❑ July -December :Sj�fffnuary-June COUNTY MOO; ^ PHONE NO. (A&- 2-3 Y cz::9 ADD TO LISTSERVE? []YES RW EMAIL: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trout ❑Other Outfalf No'.— Date Sample Collected mo dd rOR / /Y NO FLOW i ), pH ( Standard Units) �,,, , TSS' (mg/0 Event Duration, .=Rainfall (minutes) Total a = (in) in Tier 2 Monthly Moritoring (Y/n ) # of Months en Tier x .2xSampling 2. 5-4 100 - G Z 13.1` 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. 2 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/l. "For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date:7/1/2011-60/30/2015 RECEIVED JUL 13 2015 CENTRAL FILES DWR SECTION1, Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outfall No. Date Sam le p Collected (mo/dd/yr} pH (Standard Units) TPH using method 1664A SGT-HEM (mg/L) `. - Total Suspended Solids°':. „ (mg%L) Event Duration (minutes) Total Rainfall° (in) New Motor Oil usage (gal/month) . In Tier 2 Monthly. Monitorng? (yin),100 # of Months', in Tier,2 ; 7 Sampling HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDEN AT ANYONE OUTFALL {INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO� HAVE YOU CONTACTED THE REGION? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail Original and one copy of this DMR fincludine all "No Flow" & "No Discharee" reoorts) within 30 days of receipt of sample (or at end of monitorine period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those per ons it y esponsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aw that t are significant enalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4 (Sig of rmittee) [Dat Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 ENW,ummul % hCupo mmW P.Q. BOX 7085, 114 OAKM-ON T DRfVE= GREENVILLE. N.C. 27835-7085 READY MIX CONCRETE (WILLIAMSTON) MR. MIKE ODOM 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAMETERS PH (not to be used for reporting) Total Suspended Residue, mg/l Stormwater Analysis Method Discharge Date Analyst Code 8.1 06/26/15 TRB 450011B-00 <2.8 06/29/15 KKF 254OD-97 ID#: 1095 DATE COLLECTED: 06/26/15 DATE REPORTED : 06/29/15 REVIEWED BY: 756-6208 756-0633 STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM GENERAL PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE NO. NC/G•14_01 L 7- FACILITY NAME: , PERSON COLLECTING SA PLES 4Ar ds vw-. CERTIFIED LABORATORY G. Lab # ZQ Lab # OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: ze2ly SAMPLING PERIOD: July -December ❑ January -June COUNTY 144d;^ PHONE NO. (z52) °% 4'Z-3/ ADD TO LISTSERVE? ❑YES1�41'Q0 EMAIL: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trout ❑Other, Outfall No. Date Sample Collected (mo/dd/yr OR NO FLOW)' pH {Standard Units) TSS [mg/L) Event Duration [minutes) Total 4 Rainfall [in) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier Z 2 Sampling - 6-92 100 , - - - - o �Z Z3D 1 If "NO FLOW" or "NO DISCHARGE, Enter "N0 FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. z If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/l. For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. Outfall No. Date Sam Sample p Collected 1 (mo/dd/yr) pH (Standard Units) TPH using method 1664A SGT-HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total a Rainfall (in) New Motor Oil Usage (gal/month) In Tier 2 Monthly Monitoring? (Y/n) i# of Months in Tier 2 Sampling2 6-92 152 100 .3 - - - - - I HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO HAVE YOU CONTACTED THE REGION? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail Original and one coov of this DMR fincludinR all "No Flow" & "No Discharge" rewrtsl within 30 days of receipt of sample for at end of monitorinR period in case of "No Flow" to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure thatEmittee) el properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those ersonsi or gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am a re tificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." D -Z3-1 (Sig at (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 Eimwohmmg[WAla hw mbe was tewate r'. I D.'. .1. 0.. P.O. BOX 7085, 114 6j�KMONT pRIVE PHONE (252) 756-6208 GREENVILLE. N.C. 27835-7085 FAX (252) 756-0633 READY MIX CONCRETE (WILLIAMSTON) MR. MIKE ODOM 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAMETERS Stormwater Analysis Metbod Discharge Date Analyst Code PH (not to be used for reporting) 6.2 10/16/14 TRS 4500HS-00 Total Suspended Residue, mg/1 <2.7 10/17/14 LW 254OD-97 ID#: 1095 DATE COLLECTED: 10/15/14 DATE REPORTED : 10/20/14 REVIEWED BY: STORMWATER DISCHARGE OUTFALL (S®O) - Semi -Annual MONITORING FORM GENERAL PERMIT No. NCG140000 CERTIFICATE OF COVERAGE NO. NCG14 L Z SAMPLE COLLECTION YEAR: 70141 FACILITY NAME: Rr4 ���Co"cam , D��...��SAMPLING PERIOD: ❑July -December �anuary-June PERSON COLLECTING SAMPLES {/y$ �,CV;vN a4 COUNTY Pktlf ' CERTIFIED LABORATORYw[fU11�vr} 1 Lab # �� PHONE NO. LZS?] T Lab # ADD TO LISTSERVE? ❑YES RSNO EMAIL: OPTIONAL INFO: DISCHARGING TO CLASS: [—]SA ❑HQW ❑PNA ❑Trou er Part A: Stormwater Monitoring Requirements Outfall No. Date Sample Collected (mo/dd/yr OR NO FLOW)' PH (standard Units] TSS (mg/L) Event Duration [minutes} Total , Rainfall (in} In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier z 2 Sampling - - 6-9 100 , - - - - 3v G d SS' 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. 2 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/l, except when discharging to ORW, HOW, Trout, and PNA waters where they are 50 mg/l. For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Part 6: Vehicle Maintenance Activity Monitoring Requirements for facilities using > 55 gal of new motor oil/month -- averaged over a calendar year. Outfall No. Date Sample Collected (mo/dd/yr) PH (Standard Units) TPH using method 1664A SGT-HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total Rainfall' (in) New Motor Oil Usage (gal/month) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier 2 Sampling 6-9 15 100 . - - - - - HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO ❑ HAVE YOU CONTACTED THE REGION? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail Orieinal and one copy of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample (or at end of monitorinjR period in case of "No Flows to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUSTSIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were. prepared under my direction or supervision in accordance with a system designed to assure that qualified peLsonnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those per so s dire r ponsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware iialth a signif�cant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." U LJ -1 Z-1 (Signature of Perm9 ee) (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 mmAumfluml Ala hcwpo® mho I We SLewateY ID- 10 GREENVILLE, N.C. 27835-7085 FAX (252) 756-0633 READY MIX CONCRETE (WILLIAMSTON) MR. MIKE ODOM 1020 E. 5TH ST. WASHINGTON ,NC 27889 PARAAfETERS PH (not to be used for reporting) Total Suspended Residue, mg/l Stormwater Analysis A•Iethod Discharge Date Analyst Code 7.7 05/01/14 TRB 4500HB-00 11 05/02/14 A1DD 2540D-97 ID#: 1095 DATE COLLECTED: 04/30/14 DATE REPORTED : 05/05/14 REVIEWED BY: �4_ GENERAL. PERMIT NO. NCG140000 CERTIFICATE OF COVERAGE NO. NCG14 SAMPLE COLLECTION YEAR: 240141 FACILITY NAME: �ti°td„ 1�li� 1p�LP (��11Ql, Ali,d *SAMPLING PERIOD: [] July -December January -June PERSON COLLECTING M LES +'�f_�17 �.t y;rN COUNTY MG!$+�^ CERTIFIED LABORATORYF4W1'f0hP%4ef 1 Lab # L PHONE NO. (ZS24 Lab # ADD TO LISTSERVE? []YES P5ND EMAIL: OPTIONAL INFO: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trou her Part A: Stormwater Monitoring Requirements Outfall No. Date Sample Collected (ma/dd/yr OR NO FLOW)1 PH (Standard Units) TSS (mg/L} Event Duration (minutes) Total , Rainfall (in) In Tier 2 Monthly Monitoring? (y/n) # of Months in Tier z 2 Sampling - - 6-9 23 100 ' - - - - 3v G S'Al 1 If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" or "NO DISCHARGE" for each outfall here. Please make sure to mark the sample period above. Z If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit, Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/I, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/I. For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Fart 5- vehide roainttenance '�ciivi y Morittw ing 1enuii enrents for ac ilitier, using i 55 gal of kkevf 1T1r4C,E o!I/rrioiiUi — ave aced over a cafe idaar Year. Outfall No. Date Sample Collected i (mo/dd/yr) pH (Standard Units) TPH using method 1664A SGT-HEM (mg/L) Total Suspended Solids (mg/L) Event Duration (minutes) Total a Rainfall (in) New Motor Oil Usage (gal/month) In Tir 2 Monthly Monitoring? (y/n) # of Months in Tier 2 Sampling' 6-9 15 100 , - - - - - HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANYONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO ❑ HAVE YOU CONTACTED THE REGION? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail Original and one copy of this DMR f including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample for at end of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified Pasonnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those perso s dire r ponsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware a th a signific t penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." J5—) Zr JV (Signature of Permi ee) (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2 of 2 ERwohmW % hmpTOA Iil I ��'�+� _ r. �L x ��,.. s a�a irWx �Ryyy3**�.�¢ rxt xt -v� yn jn+c�- _..gJ�-., .*a.c•f�z���`3�. ws--�.t.s e+ v- y �.bri AYing�Wat Cx i-D 377k5 +^--• 1D- - :�.�.x._:..��._X:#-:._..:����.,t..:.;:5.:c:.x��.--"...<rrl.�tr-��..si�*.r��-a'' ' 4-`u�c•3�•;c.� :s�d.�c'�.: �....�°�,_x:� ,.. ,��.res_.ati- _: _.-�. � - P.O. BOX 7085, 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27835-7085 FAX (252) 756-0633 READY MIX CONCRETE (WILLIAMSTON) MR. MIKE ODOM 1020 E. 5TH'ST. WASHINGTON ,NC 27889 Stornmater Analysis Method PARA1•IETERS Discharge Date Analyst Code PH (not to he used for reporting) 7.7 05/01/14 TRB 4500HB-00 Total Suspended Residue, nig/l 11 05/02/14 MDD 254OD-97 ID#: 1095 DATE COLLECTED: 04/30/14 DATE REPORTED : 05/05/14 REVIEWED BY: