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NCG140005_MONITORING INFO_20160311
bTORMWATER DIVISION CODING SHEET RESCISSIONS . PERMIT NO. DOC TYPE ❑COMPLETE FILE -HISTORICAL DATE OF RESCISSION ❑ �f �., OL YYYYMMDD STORMWATER DISCHARGE OUTFALL (SDO) - Semi -Annual MONITORING FORM ..= GENERAL PERMIT NO. NCG1:40000 11u CERTIFICATE OF COVERAGE NO. NCG14 0 0 0 5 FACILITY NAME:��'� � r� Cct-,r 1 PERSON COLLECTING SAMPLES a LQ CERTIFIED LABORATORY �L 'i�_ Lab # Lab ft OPTIONAL INFO: Part A: Stormwater Monitoring Requirements SAMPLE COLLECTION YEAR: A(D(:::� _oQ N SAMPLING PERIOD-f ff July -December ❑ January -June COUNTY `LJi tt _ PHONE NO. (,Z . ADD TO LISTSERVE? []YES ENO EMAIL: DISCHARGING TO CLASS: ❑SA ❑HQW ❑PNA ❑Trout Other , I;�,,.,t=F.�-:s•:�,. : �K,,-S A5 i_- i 1 T 1 f 6 i r a.i•r '. t,.;d.- .�-;. 1-�:.. .,,.D:�aCtoer llSeac_mtept,! ,l,,:et:,;<r,:ir.G�,• ?,.. �`: - :11 1 nv+�?i'1Tr 71'2 -,. NO FLOW)c #_.a.�a ,Iw-.x- :P :r,,�f �`t,i:`,.�i::a�y..p`Hx._•:'�::.fi.-- A�:,•••.,.5}�.�r� _ ...Ursits4l',. 7 z,..r' [, r a i.• r,i.:::�,i-" i '2 : .<,r;_.,�},.].y�.:.am�,:._,;:�v�- -�i.. t T- S-«sS ..�,�'at.;-E ,r .t ;.x�. : 4s:' .ix, ..1.-,,.... .> - CY .. T:i:.. : i.:7: '.I-!. .,E,t of :.rf: =s=31':^ P.M., Duration : :,i f ..r�.�f_..E 1{minutes .�: cl .1,..1:i_ i ...i x 7w :=Y.-. �.?:: Y.. otax :.:,^:7:;: cr}..�,^r��y :cfa*,�s^ i`". � ,,,Rainfall...:.-� r i3 .5% ":.� �- .,�;IVlonita�in 1iit{1e ,.:Y..,. c.«-,A- ii_.Z:� :.i ulk:::1:4:v.F:: ^i 3�i:- f .,a: MInTnie.r'?=f2= `;�_.£�.;,.�..� k;',.�. 'F L:� ^:�• Lf.'.ci ji:i- g ? -� wiY!-}T ] 'a-�7:hs7 ., ..i, .i, y �yln� .�i F:lE-' ..; : i��,#. vof�fvlanths-m,Tie'r; ]«��a:w°.r:� R" : -�.,,Z'Sam x_µ ss �� "rC .. Y..••y t r a :' .. _ t a i f' r[,,. , - _....1:6Y': -_ .-. ..c �::-.. t. }. .. f w ..� .�:-s�.r_-_.-••_... ..4. -�1 :.. „ .k..1-Y-.' -, 1..', ....:[.....ft. - .�'^s• ..s :- '.�.: .r�...i, Tx'. a r'r�„� .s.^-, .11. ^...I:::i,... _-.s, W �Yt.,. ~�7r.< v..� s - ° S. _:S `Yl-.,.«...... �.�:11+"� � R t MAR 11 INR SE +� If "NO FLOW" or "NO DISCHARGE, Enter "NO FLOW" ar "NO D15CHARGE" for each outfall here. Please make sure to mark the sample period above. If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range. 3 TSS benchmark values are 100 mg/l, except when discharging to ORW, HQW, Trout, and PNA waters where they are 50 mg/l. "For each sampled measurable storm event the total precipitation must be recorded using data from an on -site rain gauge. Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 1 of 2 Part R: Vehicle Maintenance Activity Monitorine Requirements for facilities using > 55 gal of new motor oil/month — averaged over a calendar year. - _ .i. t ��,��•� Outfall� r No. r.,,y--2,°':.:.;;�:'i�i%:m'°�°-�''..:fs:i =Qv J. �1. s."�6'?.a15, L+.,,,,"-,,;2•1'p•} Date:Sample� =M`r =;, .� Collected i Y......-—T.�. :d i...y.. ,...: ��_-t"`. �''` . "H. -.�. Standard �, :; ,.. i _ Units} �� ° 1 . _ .,.f t F Ks.`aS f,, k^a� ':� Z� 7 RUN_�°<. PHrus�n method7otalSuspended _�56dAYSG7=NEM. �.� �i x w (mg/E1''�(mJ;IL}:fi�Iminutes} �. z Y;.,: _ ".'.�',f _ .-i'.'_1":.,y:i'._.,.Z...:..�5,`t�::^1"+a::.::.c•"•:-...vI",:J:f_'^s."Y': :-:°•-wa c� �<�i.'''{�'S'+, ..„ �., Sohdsa. �: »' , , �:>.;_.. s:..'L' .�.� _ - _ •4 fv:,• „'. .rim r . Z , �' r=u=Events, �v Duration = st, -WY :s: 3t7�r#2.c I T�� .l�i%� .i •`._ ' �; S .r� ` :Total. a all , =ipiin} �' �,�_ y�F:X.,.S F i.• s.?S..T"w,."=. .3.:i4 :. Y s �� —'xlezx. :New:MotorFOil^ i:."Month) Usage 3�-g- .(gal/month); * .4 �' `i`�'3"?� - �..i l"iy'^.. A'yr`. m+i_.T�„- Y'.:rk^�• -.:i�`.L�"JF�.-.:�:' =.-"` - �,IntTierZ 5 �:•� -x y ..-.. Monitorin 7 g =. kyl .'J.^a-.lkesz:'..1-'. ",.T'il{.'."'.Ns-� LM^%�i:tti" T,HKGrit t €It;of�Monti�syt, q a'�� Sam hn p�. gv �; ::±r:="-..L.°r"�•'r'=Y_,.A.°, HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ Nefri HAVE YOU CONTACTED THE REGION? YES ❑ NOO REGIONAL OFFICE CONTACT NAME: Mail OriRinal and one copv of this DMR (including all "No Flow" & "No Discharge" reports) within 30 days of receipt of sample (or at end_ of monitoring period in case of "No Flow") to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons direct re ponsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that th a are ignificant nalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of er tee) (Date) Permit Date: 7/1/2011-60/30/2015 Last Revised 7/13/11 Page 2'of 2 NCDEN Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: httl2://portaLncdenr.org/web/wq/ws/sti /nsib sw#tab-4 Permit No.: NYC/�/ _/_ /_ / _/_/T/ or Certificate of Coverage No.: Facility Na Y� tL �M C1�/ter County: J' !r Inspector: Date of Inspection: Time of Inspection: Phone No. Total Event Precipitation (inches): _C- i i Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Ive—mciff—Em Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. -A "representative storm event" is a storm event that measures greater than 0A inches of rainfall and that is preceded by at least 72 hours (3 days) in'which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains am)roval from the local DWO Regional Office. By this signat ce tify that this report is accurate and complete to the best of my knowledge: . _' / (Signature oi`PE—rmittee or Designee) Pagel of 2 SWU-242, Last modified 10/25/2012 WSA 1. Outfall Description: Outfall No. 51-2001 Structure (pipe, ditch, etc_.) i 1 Gc 1 Receiving Stream: ki—I Describe the industrial activities. that occur within the outfai�drainarea: n_ _ _ r 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium; dark) as descriptors: l,A U(-e_ W--;,I =) 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weals chlorine odor, etc.): _ L:1r r'k _ 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1) 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 0 B. Is there an oil sheen in the stormwater discharge? Yes ( o) 9. Is there evidersce of erosion -or deposition'at the -outfall? Yes, - 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242. Last modified 10/25/2012 aceMalytical wwwpecelabs.c= November 13, 2015 Mr. Johnny Baines Eastern Environmental Management PO Box 4030 518 S. Pearl Street Rocky Mount, NC 27803 RE: Project: DPD - Greenville Pace Project No.: 92274349 Dear Mr. Baines: Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 _ Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 03, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell , taylor.ezell@pacelabs.com Project Manager Enclosures cc: Ms. Cathy Baines, Eastern Environmental Management REPORT OF LABORATORY ANALYSIS This report shal} not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 a ce Analytical ` www.pswabs.com Pace Analytical Services, Inc, 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704+1875-9092 CERTIFICATIONS Project: DPD - Greenville Pace Project No.: 92274349 Charlotte Certification Ids 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VEIAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc., Page 2 of 11 aceAnalytical www.pacelabs.00m SAMPLE ANALYTE COUNT Project: DPD - Greenville Pace Project No.: 92274349 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 ` (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92274349001 SDO-1 EPA 1664E JMS 1 PASI-C SM 2540D SAM 1 PASI-A SM 254OF MJP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalytical' www.pacelabsmm ANALYTICAL RESULTS Project: DPD - Greenville Pace Project No.: 92274349 Pace Analytical Services, Inc, 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704�875-9092 Sample: SDO.1 Parameters Lab ID: 92274349001 Collected: 11/02/15 11:30 Results Units Report Limit DF Received: 11/03115 09:30 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg[L 5.0 1 11/12/15 07:39 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 39.8 mglL 2.6 1 11/04/15 10:20 254OF Total Settleable Solids Analytical Method: SM 2540F Total Settleable Solids ND mLILJhr 0.10 1 11I03115 22:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /13/2015 12:44 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 aceAnalytical L wwwpecelabs.com QUALITY CONTROL DATA Project: DPD - Greenville Pace Project No.: 92274349 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 - (704)875-9092 QC Batch: GCSV123181 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92274349001 METHOD BLANK: 1604434 Matrix: Water Associated Lab Samples: 92274349001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg1L ND 5.0 11/12/15 07:35 LABORATORY CONTROL SAMPLE: 1604435 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mglL 40 33.7 84 78-114 MATRIX SPIKE SAMPLE: 1604436 92275153001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL ND 40 35.0 88 78-114 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11113/2015 12:44 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalyticaI wwvrpecelabs.c= QUALITY CONTROL DATA Project: DPD - Greenville Pace Project No.: 92274349 QC Batch: WET141198 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92274349001 % METHOD BLANK: 1598226 Associated Lab Samples: 92274349001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL_ SAMPLE: 1598227 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1598228 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1598229 Parameter Units Total Suspended Solids mglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 11/04/1510:18 Spike LCS Conc. Result 250 242 92274504001 Dup Result Result 78.0 78.0 92274481001 Dup Result Result 28.4 7.0 Pace Analytical Services, Inc., 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 97 90-110 RPD Qualifiers 0 RPD Qualifiers 121 D6 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shO not be teproduced, except in full, Date: 11/13/2015 12:44 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 l aceAnalytrcal c www.pawabs.com QUALITY CONTROL DATA Project: DPD - Greenville Pace Project No.: 92274349 QC Batch: WET141192 Analysis Method: SM 254OF QC Batch Method: SM 254OF Analysis Description: 254OF Total Settable Solids Associated Lab Samples: 92274349001 METHOD BLANK: 1598139 Associated Lab Samples: 92274349001 Parameter Units Total Settleable Solids mUUhr Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 11/03/1522:35 SAMPLE DUPLICATE: 1598140 92274350001 Dup Parameter Units Result Result Total Settleable Solids mIJIJhr ND ND RPD Qualifiers Paco Analytical Services, Inc. 9800 Kincey Ave. Suite 500 _ Huntersville• NC 28078 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/1312015 12:44 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnalytical WWW..pecelebs.com QUALIFIERS Project: DPD - Greenville Pace Project No.: 92274349 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference INC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethyivinyl ether, Styrene, and Vinyl chloride. Aseparate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N- Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. A 1=IeL'It� ie7:71 �'] PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1111312015 12:44 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalytical i W"..pacelabs.cam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 - Huntersville, NC 28078 (704)875-9092 Project: DPD - Greenville Pace Project No.: 92274349 Analytical Lab lD Samplo ID QC Batch Method QC Batch Analytical Method Batch 92274349001 S130-1 EPA 1664B GCSV123181 92274349001 SDO-1 SM 2540D VVET141198 92274349001 SDO-1 SM 254OF VVET141192 Date: 11/13/2015 12:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 uocument ivame: �aceAmlytiCal" Sample Condition U on Recall Document Number: F-CHR-CS-003-rev.16 LIUGUI I ICl It r%vViacm, may IV, LV i V SCUR Page 1 of 2' Issuing Authority: Pace Huntersville Quality Office Client Name: u 5 f n TA V My,, {- Courier: Fed EC UPC] USP❑ Clier❑ Commercl;0 Pace Other - Custody Seal on CoolerlBox Present: ❑ yes Seals intact: ❑ yes Packing Material: ❑ Bubble Wrap ubble Bags ❑ None [ Other Thermometer Used: IR Gun 140 Type of Ice: We Blue None Tema Correction Factor T1 No Correction Page 2 of 2 Is for Internal Use Only ❑ no Samples on ice, cooling process has begun 3 ' - Corrected Cooler Tem 5. C p•� Biological Tissue Is Frozen: Yes No rA Date and Initials of person examining contents: //• / S Temp should be above freezing to WC Comments: -�, Chain of Custody Present: ❑ s 6 ONIA 1 • Chain of Custody Filled Out: es ONO ❑ IA 2. Chain of Custody Relinquished: ©Yes ❑N/A I Sampler Name & Signature on COC: 01.1-1PNO ❑NIA 4, Samples Arrived within Hold Time: 17 les PNO ❑NIA 5. Short Hold Time Analysis <72hr : es ❑No ❑NIA 6, Rush Turn Around Time Requested.* Dyes ® o ©NIA 7• L Sufficient Volume: es_ ❑No ❑NIA $, Correct Containers Used: DYes,,O No ❑NIA g. -Pace Containers Used: Yes ❑No ❑NIA Containers Intact: tOYes ❑No ❑NIA 10., Filtered volume received for Dissolved tests ❑Yes ❑No ❑NA 11, Sample Labels match COC: Byes ONO ❑N/A 12. -Includes dateltime/1D/Anal sis Matrix: All containers needing preservation have been checked. Oyes ONO ❑ 6A 1 All containers needing preservation are found to be in ❑Yes ONO. ❑N!A compliance with EPA recommendation. exceptions: VOA, collrorm, TOC, O&G, WI-DRO (water) / ❑Yes �INo Samples checked for dechlorination: Dyes ONO NIA 14. Heads ace in VOA Vials >6mm : Dyes ONO 0415. Trip Blank Present: Dyes ONO NrA A6, Trip Blank Custody Seals Present []Yes ONO !A Pace Trip Blank Lot # if purchased): Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: Y /. Date: lI } SRF Review: Hate: t Note: Whenever there is a dis-t epancy affecting North Carolirla compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (l.e out of hold, Incorrect preservative, out of temp, incorrect containers) WOi{ : 92274349 1111111111111111111111 92274349 Page 10 of 11 uucumen[ flame:cet L pP Sam le Condition Upon Rei CU �.aceArk?lytica!• -- - — Document Number. F-CHR-CS-003-rev.16 Client Name: 5 r~�n rn✓, M y,� �- LJUC:VII Ier It ncv IJcu. IVIGY IV, Fv 4 V Page 1 of 2" Pace Huntersville Ouali Office Page 2 of 2 is for internal Use Only Courier: UPL] USP❑ Clier❑ommerc!LJ. Pace. Other Custody Seal on Cooler/Box Present: Elyes no Seals intact: ❑ yes ❑ no r,--( Uj Ogg, = Packing Material: ❑ Bubble Wrap ubbie Bags ❑ None Q Other Thermometer Used: IR Gun 140 Type of Ice; UWeBlue None Samples on ice, cooling process has begun Temo Correction Factor T1 No Correction Corrected Cooler Temp.:�. tJ •C Temp should be above freezing to 6°C Biological Tissue is' Frozen: Yes No rp Comments: Date and Initials of person examining contents: _ F> �!• / S Chain of Custody Present: ❑ s a ❑NIA 1. Chain of Custody Filled Out: D,es ❑No ❑ IA 2. Chain of Custody Relinquished: Dyes ❑NIA 3. Sampler Name & Signature on COC: 1311-1—pNo ONIA 4. Samples Arrived within Hold Time: Elles PNo ❑N/A 5. Short kold Time Analysis <72hr : es ONO ❑NrA 6. Rush Turn Around Time Requested: Dyes o ❑NIA 7. t Sufficient Volume: es ONO ❑NIA S. Correct Containers Used: -Pace Containers Used: i OYes No DyesDNo ❑NIA ❑NIA 9. Containers Intact: ❑Yes ONO El NIA 10._ Filtered volume received for [Dissolved tests ❑Yes ❑No ❑NIA 11. Sample Labels match COC: -includes dateltime/]D/Anal sis Matrix: E y s ONO t/ ❑NIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, oolirorm, TOC, O&G, W-DRO (water) Dyes ONO Dyes ❑No /% ❑Yes 0No ❑NrA ❑NIA 1 . Samples checked for dechiorination: ❑Yes ❑No NIA 14. Headspace in VOA Vials ( >6mm): Dyes ONO ofir 15. Trip Blank Present: Trip Blank Cuustody Seals Present Pace Trip Blank Lot # if purchased): Dyes ONO ❑Yes ONO NIA P11 1A AB. Client Notification) Resolution: Field Data Required? Y 1 N Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: Date: !f S SRF Review: Date: I( Note: Whenever there is a discrepancy affecting North Caroli a compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, Incorrect preservative, out of temp, Incorrect containers) WOiI : 92274349 1111111111111111111111 92274349 Page 10 of 11 'iPn 1 1cis l' ace a yt w .pacelahs.com Section A Section B Required Client Information: Required P CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. Ail relevant fields must be completed accurately. Section C Invoice Info i C_JI :MLt �c on �� Add To' Purchase Order No.: Pau 5 Role 'hone: Fax: ProjdctNelme: .fr �� �. Pau tequeslod Due DotefTAT: Project Number. Pea Soction D Matrix Codes Required Chet mtormaeon MATRIX I CODE a � COLLECTED Drinking water DW 0 zo water WT SS22 u Waste Water Ww v m romPOSITE coemosne V Product P - i START ENMRAe ul SOVSOIitI $L gVVP N SAMPLE ID oil OL � � W f A-Z, 0.9 ! ,•j Air AR ¢ Sample IDs MUST BE UNIQUE Tissue TS p a 4 IF - Other Or V rm• z X OU J J ZE o N DATE TIME DATE TIME 0 Page: f of nnalion: 1475489 ne: REGULATORY AGENCY NPDES 17- GROUNDWATER F DRINKING WATER F- UST r RCRA F OTHER Site Location A ` ` Gj2� � STATE: ! � L. Requested Analysis Filtered {Y!N) y z Preservatives } Z m 7- z z '2 p 1*, Pace Project No.! Lab I.D. ADDITIONAL COMMENTS RELINQUISHED BY! AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION' DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE ORIGINAL PRINT Name of SAMPLER: SIGNATURE of SAMPLER: �Irrpo tam Note: By sinning this lam You are accepting Pxa's NET 30 day payreont terms and agma'vg to Into durgos of 1.5% Por month Im adv :r rk;,3 —t p ld mthe, 30 days. y o_ r G m y U Z_ R 2 j 1Y m m= U m� E f f ~ LO cn F-ALL-G-020rev.07,45-May-2007