NCG100066_MONITORING INFO_20161110

STORMWATER DIVISION CODING SHEET
RESCISSIONS
PERMIT NO.
DOC TYPE
N��U1.
❑COMPLETE
�o
FILE -HISTORICAL
DATE OF
RESCISSION
❑
c2oI� II I
YYYYMMDD

s
aceAnalytical
www.pac8bb&c=
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
October 18, 2016
Chuck Hoffman
Mid -Atlantic Associates, Inc
409 Rogers View Court
Raleigh, NC 27610
RE: Project: Louia Motor Company R2083.00
Pace Project No.: 92315536
NC' (r /00064�0
/ReCE/ D
Je
NOV 102016
CENTRgL FE
DWR SECT, NS
Dear Chuck Hoffman:
Enclosed are the analytical results for sample(s) received by the laboratory on October 11, 2016,
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
cc: Ron Davis. Mid Atlantic Associatees. Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 12

aceAnalytical'
..psodizbs_cm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Louia Motor Company R2083.00
Pace Project No.: 92315536
Indiana Certification IDs
7726 Moller Road, Indianapolis, IN 46268
Illinois Certification #: 200074
Indiana Certification #: C-49-06
Kansas/NELAP Certification #:E-10177
Kentucky UST Certification #: 0042
Kentucky WW Certification #:98019
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Ohio VAP Certification #: CL-0065
Oklahoma Certification #: 2014-148
Texas Certification #: T104704355-15-9
West Virginia Certification #: 330
Wisconsin Certification #: 999788130
USDA Soil Permit #: P330-10-00128
South Carolina Certification #: 99006001
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaA/ELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 12

s
aceAnalytrcal
www.pacdabswm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Louia Motor Company R2083.00
92315536
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92315536001
Outfall No. 1
EPA 1664B
JMS
1
PASI-C
EPA 8015 Alcohol -Glycol
BJW
1
PASI-I
EPA6010
SH1
1
PASI-A
SM 2540D
MLS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 12

aceAnalyticala
wwwpacefahscom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Louia Motor Company R2083.00
Pace Project No.: 92315536
Sample: Outfall No. 1 Lab ID: 92315536001 Collected: 10/08/16 11:30 Received: 10/11/16 10:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons ND mg/L 5.0 1 10/18/16 08:45
8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol
Ethylene glycol ND mg/L 5.0 1 10/14/16 14:26 107-21-1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Lead 13.4 ug/L 5.0 1 10/13/16 01:30 10/15/16 11:34 7439-92-1
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 19.2 mg/L 5.0 1 10/13/16 13:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2016 04:27 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 12

aceAnalylrcal
www.para&abscom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Louia Motor Company R2083.00
Pace Project No.: 92315536
QC Batch: 333506
QC Batch Method: EPA 1664B
Associated Lab Samples: 92315536001
METHOD BLANK: 1848166
Associated Lab Samples: 92315536001
Parameter Units
Total Petroleum Hydrocarbons mglL
LABORATORY CONTROL SAMPLE: 1848167
Parameter Units
Total Petroleum Hydrocarbons mg1L
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 SGT-HEM, TPH
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 10/18/16 08:45
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 16.2 81 64-132
MATRIX SPIKE SAMPLE: 1848168
92315461001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mglL ND 20 15.3 76 64-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2016 04:27 PM without the written consent of Pace Analytical Services, LLC, Page 5 of 12

aceAnalytical
www4mcelaftscotrt
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Louia Motor Company R2083.00
Pace Project No.: 92315536
QC Batch: 356395
QC Batch Method: EPA 8015 Airohol-Glycol
Associated Lab Samples: 92315536001
METHOD BLANK: 1648541
Associated Lab Samples: 92315536001
Parameter Units
Ethylene glycol mglL
LABORATORY CONTROL SAMPLE: 1648542
Parameter Units
Ethylene glycol mglL
QUALITY CONTROL DATA
Analysis Method: EPA 8015Alcohol-Glycol
Analysis Description: EPA 8015 Modified
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 10/14/16 13:19
Spike LCS
Conc. Result
25 26.0
LCS % Rec
% Rec Limits Qualifiers
104 60-129
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1648543 1648544
MS MSD
50156559001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mglL ND 25 25 28.8 27.5 115 110 23-157 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1011812016 04:27 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 12

aceAnalytical a
Nwtvpacefahs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Louia Motor Company R2083.00
Pace Project No.: 92315636
QC Batch: 332780
QC Batch Method: EPA 3010A
Associated Lab Samples: 92315536001
METHOD BLANK: 1844059
Associated Lab Samples: 92315536001
Parameter Units
Lead ug1L
LABORATORY CONTROL SAMPLE: 1844060
Parameter Units
Lead ug/L
QUALITY CONTROL DATA
i
Analysis Method: EPA 6010
Analysis Description: 6010 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 10/15/16 10:57
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 486 97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1844061 1844062
MS MSD
92314813028 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 463 473 92 94 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2016 04:27 PM without the written consent of Pace Analytical Services, LLC,
Page 7 of 12

aceAnalytrcal"
www.pacdab&c m
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersvilie, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Louia Motor Company R2083.00
Pace Project No.: 92315536
QC Batch: 332948 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92315536001
METHOD BLANK: 1845096
Associated Lab Samples: 92315536001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
1845097
Parameter
Units
Total Suspended Solids
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 10/13/1613:32
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 244 98 90-110
SAMPLE DUPLICATE: 1845098
92315452002 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 15.6 16.8
SAMPLE DUPLICATE: 1845099
92315605001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 53.0 52.0
RPD Qualifiers
7 D6
RPD Qualifiers
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/1812016 04:27 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12

aceAnalyticals
www.yaralabs.=
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2BO78
[phone]
QUALIFIERS
Project: Louia Motor Company R2083.00
Pace Project No.: 92315536
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenythydrazine decomposes to and cannot be separated From Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenytamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyto is a combined concentration,
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-I Pace Analytical Services - Indianapolis
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2016 04:27 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 12

s
aceAnalytical
www.pacelabs.c=
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Louia Motor Company R2083.00
Pace Project No.: 92315536
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92315536001
Outfall No. 1
EPA 1664E
333506
92315536001
Outfall No. 1
EPA 8015 Alcohol -Glycol
356395
92315536001
Outfall No. 1
EPA 3010A
332780 EPA 6010
92315536001
Outfall No. i
SM 2540D
332948
Date: 10/18/2016 04:27 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
333055
Page 10 of 12

Sample Condition Upon Receipt(SCUR) Page 1 of 2
aceAnalytical Document No.: Issuing Authority:
F-CAR-CS-033-Rev.00 Pace Quality Office
Page 2 of 2 for Internal Use ONLY
• • •• Client Name: E�o� ��������
Project 1
A�'� , A -- i�-�: ICE t� 1-�� � _ Courier; Fed Ex ❑UPS ❑USPS [_]Client II III
III IIII III
111111111
❑ Commercial ce ❑Other: `!
92315536
Custody Seat Present? Dyes � Seals Intact? r❑YeS-�'_ ❑No
� Date/Initials Person Examining Contents: j Lj " 1 i U_
Packing Material: ❑Bubble Wrap Qi u; bble Bags ❑None ❑Other:
Thermometer:
0M1 et ❑ Blue ❑None amples an ice, tooting process has be n
El ER Gun ID: Type of ice:
Correction Factor: Cooler Temp Corrected ('C): •� _ Biological Tissue Frozen? ❑Yes ❑No . /A
Temp should be above freezi g to 6'C
USDA Regulated Soil ( /A, water sample)
Did samples on site in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internati
MYes rIN15 including Hawaii and Puerto Rico)? ❑Yes I o
Comm a nts/Discrepancy:
Chain of Custody Present?
es
(—]No
❑N/A
1.
Samples Arrived within Hold Time?
QYes
[]NO
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
Offo
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
Ott-
❑N/A
4.
Sufficient Volume?�es
[]No
❑N/A
5.
Correct Containers Used?
Ors
[]No
❑N/A
6.
-Pace Containers Used?
QYe<
❑No
❑N/A
Containers Intact?
[-]No
[]N/A
7.
Samples Field Filtered?
❑Yes
[]No
❑pl/k
8. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
Yes
[:]No
[]N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
All containers needing acid/base preservation have been
1D.
checked and documented on page two of SCURF?
QYEs
❑No
❑N/A
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015
(water) DOC, LLHg
11.
Samples checked for dechlorination? ❑Yes ❑No N/A
Heads ace in VOA Vials (>S-6mm)?
[]Yes
Q o
[]NIA
12.
Trip Blank Present?
OYes
[:]No
Trip Blank Custody Seals Present?
❑Yes
❑No
;t//A13.
Pace Trip Blank Lot ff (if purchased):
CLIENT NOTIFICATION/RESOLUTION Field Data Required? ❑Yes ❑No
Person Contacted: Date/Time:
Comments/Sample
Discrepancy:
Project Manager SCURF Review: j` I - Date:
Project Manager SRF Review: y Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville Raleigh[] Mechanicsville❑
Page 11 of 12

i'
,ace Analytical
cQ".
Section A
Required Client Inlormalion
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT, All relevant (aids must be completed accuralety.
Section B Section C
Required Protect Inlormellon: Invoice Information
�o
r
Pago: of
QL
Company Mid -Atlantic Associates, Inc.
RePon To. Chuck Hoffman ([e-mail])
Attention: Chuck Hoffman
Address 409 Rogers View Court
copy To Ron Davis ([e-mail]
Company Name, Mid -Atlantic Associates. inc,
REGULATORY AGENCY
Raleigh, NC 27610
Address 409 Rogers View Court, Raleigh, NC
NPDES I GROUND WATER — DRINKING WATER
(- UST f- RCRA F OTHER
Email To [e-mail]
Purchase Order No.: R2083.00
Paco ounce
Rolorence:
Phone: [phone]
Fax: [phone]
project Name. Louie Motor Company
Pace Project Nicole Gasiorowski
I
Site Location
Mange.
STATE:
NC
Requested Duo DaterrAT: Standard
Protect Number, RP083,00
Pace Prolde to --
Requested
Analysis
Filtered
JY1N)
Section D Valid Matrix Codes
2
ii
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Required Cecm lnlonnauon MATRI% CODE
E
COLLECTED
Preservatives
'>
N
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N
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ORIN INOWAIEn DW
WATER WT
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WASTEWATER WW
PRODUCT P
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Sample IDs MUST BE UNIQUE TtssuE is
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DATE
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Pace Project No) Lab 1.06
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Outfall No. 1
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Rainfall (inches): i 00)
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9
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ADDITIONAL COMMENTS
RELINQUISHED Y 1 AF ILIATTIION`
DATE
TIME
ACCEPTED BY ! AFFILIATION
DATE
TIIM} E
SAMPLE CONDITIONS
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SAMPLER NAME AND SIGNATURE
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PRINT Namo of SAMPLER:
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SIGNATURE of SAMPLE l
DATE SI ned
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(MMrDD/YY):
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ImAodani Noin: By signing that lean you ion aecephng Paco s NET 3D day pnynTvnt remit and agraaing It Tale chnigue of 1,5% poi nmnth rat nny invoices not paid w,thin 30 days. FALL-0•020rev.08, 12.Oc1.2007

ace Analytical
www.pacefaes,com
May 11, 2016
C cT l o bob(
Chuck Hoffman RECEIVED
Mid -Atlantic Associates, Inc
409 Rogers View Court JUN 0 S 2016
Raleigh, NC 27610 CENTRAL FILES
DWR SECTION
RE: Project: LOUTA MOTOR COMPANY
Pace Project No.: 92296552
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Chuck Hoffman:
Enclosed are the analytical results for sample(s) received by the laboratory on May 05, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
/"1
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
cc: Ron Davis, Mid Atlantic Associatees, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 12

Pace Analytical Services, Inc.
aceAnalXical ® 9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
www.Pacefabs.aom [phone]
CERTIFICATIONS
Project: LOUTA MOTOR COMPANY
Pace Project No.: 92296552
Indiana Certification IDs
7726 Moller Road, Indianapolis, IN 46268
Ohio VAP Certification #: CL-0065
Illinois Certification #: 200074
Oklahoma Certification #: 2044-146
Indiana Certification #: C-49-06
Texas Certification #: T104704355-15-9
Kansas/NELAP Certification #:E-10177
West Virginia Certification #: 330
Kentucky UST Certification #: 0042
Wisconsin Certification #: 999788130
Kentucky WW Certification #:98019
USDA Soil Permit #: P330-10-00128
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, H u ntersvil le. NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Vrginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
FloridalNELAP Certification #; E87W South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 Virginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 12

aceAnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
LOUTA MOTOR COMPANY
92296552
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92296552001
OUTFALL NO. 1
EPA 1664B
JMS
1
PASI-C
EPA 8015 Alcohol -Glycol
BJW
1
PASI-I
EPA 6010
CDF
1
PASI-A
SM 2540D
MJP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 12

aceAnalyiical
www.paoelebs.cam
ANALYTICAL RESULTS
Pate Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: LOUTA MOTOR COMPANY
Pace Project No.: 92296552
Sample: OUTFALL NO. 1 Lab ID: 92296552001 Collected: 05/05/16 10:10 Received: 05/05/16 12:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH Analytical Method: EPA 16646
Total Petroleum Hydrocarbons ND mg1L 5.0 1 05/10/16 07:35
8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol
Ethylene glycol ND mg1L 5.0 1 05/10/16 10:37 107-21-1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Lead 8.6 ug1L 5.0 1 05/09/16 13:00 05/10/16 21:35 7439-92-1
2640D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 15.7 mg1L 4.2 1 05/06/16 15:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/11/2016 02:42 PM without the written consent of Pace Analytical Services, Inc..
Page 4 of 12

aceAnaIXical
www.pacelehs.com
Project: LOUTA MOTOR COMPANY
Pace Project No.: 92296552
QC Batch: GCSV124923
QC Batch Method: EPA 1664B
Associated Lab Samples: 92296552001
METHOD BLANK: 1729350
Associated Lab Samples: 92296552001
Parameter Units
Total Petroleum Hydrocarbons mg1L
LABORATORY CONTROL SAMPLE: 1729351
Parameter Units
Total Petroleum Hydrocarbons mg1L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 SGT-HEM, TPH
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 05/10/16 07:08
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 16.2 81 64-132
MATRIX SPIKE SAMPLE: 1729352
35242589001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg1L 6.4 20 19.9 67 64-132
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in Full,
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acmnalytical
"W.pacolahs.com
Project: LOU IA MOTOR COMPANY
Pace Project No.: 92296552
QC Batch: GCSV119584
QC Batch Method: EPA 8015 Alcohol -Glycol
Associated Lab Samples: 92296552001
METHOD BLANK: 1535166
Associated Lab Samples:
Parameter Units
Ethylene glycol mg1L
QUALITY CONTROL DATA
Analysis Method: EPA 8015 Alcohol -Glycol
Analysis Description: EPA8015 Modified
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 05109/16 13:21
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1535167
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Ethylene glycol mg1L 25 37.5 150 60-129 L3
MATRIX SPIKE $ MATRIX SPIKE DUPLICATE: 1535168 1535169
MS MSD
60218404001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone, Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg1L ND 25 25 35A 29.0 142 116 23-157 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the resuM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/11/2016 02:42 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 12

aceAnalytical
WW'paca/8h&Cam
Project: LOUTA MOTOR COMPANY
Pace Project No.: 92296552
QC Batch: MPRP121650
QC Batch Method: EPA 3010A
Associated Lab Samples: 92296552001
METHOD BLANK: 1728523
Associated Lab Samples: 92296552001
Parameter Units
Lead ug/L
LABORATORY CONTROL SAMPLE: 1728524
Parameter Units
Lead uglL
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 6010
Analysis Description: 6010 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 05/10/16 20:53
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 483 97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1728525 1728526
MS MSD
92296617002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 486 496 97 99 75-125 2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/11/2016 02:42 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 12

(�5a'cieAnalytical
wwwpacefabs.coar
QUALITY CONTROL DATA
Project: LOUTA MOTOR COMPANY
Pace Project No.: 92295552
Pace Analytical Servicas,Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: WET144744
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92296552001
METHOD BLANK: 1728081
Matrix: Water
Associated Lab Samples: 92296552001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND
2.5 05/06/16 15:35
LABORATORY CONTROL SAMPLE: 1728082
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 250
100 90-110
SAMPLE DUPLICATE: 1728083
92296411001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg1L
79.7 76.7 4
SAMPLE DUPLICATE: 1728084
92296408001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg[L
ND
ND
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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aceAnalytical
www.pacalahs.cam
QUALIFIERS
Project: LOUTA MOTOR COMPANY
Pace Project No.: 92296552
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-1 Pace Analytical Services - Indianapolis
ANALYTE QUALIFIERS
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/11/2016 02:42 PM wthout the written consent of Pace Analytical Services, Inc.. Page 9 of 12

6
acmnalytical
wwwpacelabs.sam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical ServiC�s,Jnc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
LOU TAMOTOR COMPANY
92296552
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92296552001
OUTFALL NO. 1
EPA 1664E
GCSVI24923
92296552001
OUTFALL NO. 1
EPA 8015 Alcohol -Glycol
GCSVl19584
92296552001
OUTFALL NO. 1
EPA 3010A
MPRP121650 EPA6010 1CP119431
92296552001
OUTFALL NO. 1
SM 2540D
WET144744
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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Document Name:
Document Revised: 19FEB2016
5Z
Sample Condition Upon Recelpt(5CUR)
Page i of 2
Document No.:
Issuing Authority:
cale
I
!
F-CHR-CS-003-rev.18
Pace Huntersville Quality Office
Client Name:
Project q;
Courier: ❑Fed Ex� ❑UPS _ ❑USPS ❑Client
❑ Commercial ®Pace ❑Other:
WO# : 92296552
111111111111111111111
92296552
Custody Seal Present? Dyes LINO Seals Intact? ❑Yes [!gN5
Dale/Initials Person Examrningtontents:��S—
Packing Material: ❑Bubble Wrap [� ubble Bags ❑None [:]Other:
Thermometer: &11505 ❑ Type of ice: et ❑ Blue ❑None LIS%mples on ice, cooling proce s has begun
Correction Factor: 0.0°C Cooler Temp Corrected ('C): �'� ,�'� Biological Tissue Frozen? ❑Yes Z7 ❑N/A
Temp should be above free 'fig to 6'C
USDA Regulated Soil ( N/A, water sample)
Did sampl s o ' inate in a quarantine zone within the United States: CA, NY, or 5C (check maps)? Did samples originate from a foreign source (inte_rnat€ally,
myes �Na Includina Hawaii and Puerto Rico)? Dyes �No
COMMENTS:
Chain of Custody Present?
Yes
❑No
❑N/A
1.
Chain of Custody Filled Out?
UYeses
❑No
❑NIA
2.
Chain of Custody Relinquished?
g es
ON.
❑N/A
3.
Sampler Name and/or Signature on COC?
b4,
❑No
❑N/A
4.
Samples Arrived within Hold Time?
J24es
❑No
❑N/A
5.
Short Hold Time Analysts (<72 hr.)?
❑Yes
KI*o�
❑N/A
6.
Rush Turn Around Time Requested?
Oyes
hjNd/ []N/A
7.
Sufficient Volume?
Ye
[_-]NO
❑N/A
8,
Correct Containers Used?
Q es
❑No
[]N/A
9.
-Pace Containers Used?
Yes
❑No
❑N/A
_
Containers Intact?
es
[:]No
❑N/A
10.
Filtered Volume Received for Dissolved Tests?
❑Ye
o
❑N/A
11. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
es
❑No
❑N/A
12.
-Includes Date/Time/ID/Analysts Matrix;
All containers needing acid/base preservation have been
Z
13
checked?
)
[]No
❑N/A
All.conta€ners needing preservation are found to be in
compliance with EPA recommendation?
(HNO3, HrSO,, HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide)
es
[-]Na
[-)N/A
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC,LLHg
Yes
❑No
❑N/A
Samples checked for dechlorination
❑Yes
CA
❑N/A
14.
Headspace In VOA Vials (>5-6mm)?
es
❑N/A
15, �V C,`1U L3Trip
Blank Present?
Elves❑N/A
IN.
16,
Trip Blank Custody Seals Present?
❑Yes
❑N/A
Pace Trip Blank Lot q (if purchased):
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Resolution:
Date/Time:
Field Data Required? ❑Yes []No
Project Manager SCURF Review: N Date:
Project Manager SRF Review: L Date: 15A
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
.Out of hold, incorrect preservative, out of temp, incorrect containers) Page 11 of 12

w aceAnalytical"
i w.Nv antrinas tam
CHAIN -OF -CUSTODY I Analytical Request Document
The Chairl-of-Cuetcd'J is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C Page: of
Required Client Information: Required Project Inlannation: Invoice Information,
Company: Mid -Atlantic Associates, Inc. Report To: Chuck Hoffman ([e-mail]) Attentrort Chuck Hoffman
Address 409 Rogers View Court
Copy To: Ron Davis ([e-mail]
Company Name: Mid -Atlantic Associates, ino.
REGLILATORY.AGENCY -
Raleigh, NC 27610
Address: 409 Rogers View Court, Raleigh, NC
i NPDES f GROUND WATER F- DRINKING WATER
F UST F RCRA F OTHER
Email To: [e-mail]
Purchase Order No.: R2083.00
Pace Qucte
Rafemnea:
Phone: [phone]
fax [phone]
Project Name Louia Motor Company
Pace Profecf Nicole Gasiorowski
<site Location
Wluger.
'
STATE:
NC
Requcatcd Due DaterrAT: Stamrard
Project Number. R2063.00
Pace Profile e: _
Requested'
Analysis
Filtered
(YIN)
.
Section D Valid Matrix Codes
a
y
Z
Required CeeM Information MJ I% CODE
a
CQLLECTED
Preservatives
N
Y
N
Y
MW*n*.-7ER DW
'"
o
U
II
2
O
01
WATER WT
WASTE WATER Ww
a
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COMPOSITE
COMPOSITE
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K
START
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J
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SAMPLE ID WIPE WP
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�,'
o
O
U
dr
=
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(A-2, 0-9 1.-)
p
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CD
~
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OOTTHER OT
Sample IDS MUST BE UN SQUE TIME Ts
O
w
a.
IL
M
¢
0
H _
O
(.�
m
L
U
V LJ l �✓
#
x
w
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c
N
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c
F
w
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a
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DATE
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TIME
a
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x
S
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x
2
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OUtfall No. 1
WT
G
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td : !D
7
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1
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4 , ;
x
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Rainfall (inches):
2.
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`5
-6
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laIt
- ;� .•ADD1TtONAL'COMMENTS•�'
- REL_INQUISHEDBYIAF TiON+'
_ •DATE-
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„" :. ''tA_CCEPTEDBYIAFFILJAIT6N.'6 .,
DATE _^
;,'.TIME`
SAMPLr;CONDITIONS
Tit
20
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SAMPLER NAME AND SIGNATURE'r r
- ,- `•
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PRINT Name of SAMPLER: UT:74
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5[GNATURE at SAMPLER: [MMTDofYYj: �,qr —_ GQ l t0
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-• S
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Nmportant Nola: By signing this farm you are accepting Pace's NET 30 day paymem iem and agreting to Late charges of 1.5% Per menlh iM . .. net paiO+sLhln 30 (lays, F-ALL-Q-024n:V.48, 12-Oct-2007
N

M-'Dd Atlantic
Engineering & Environmental Solutions
April 21 2014
NCDENRIDWQ
Attention: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: STORMWATER SAMPLING RESULTS
LOUTA MOTOR COMPANY
2647 EAST HIGHWAY 64
LEXINGTON, DAVIDSON COUNTY, NORTH CAROLINA
-PERMIT NCG100066-)
MID -ATLANTIC JOB NO. 000R2083.00
To Whom It May Concern:
409 Rogers View Court
Raleigh, NC 27610
office 919.250,991 B
facsimile 919.250.9950
MAAONLINE.COM
Attached please find the Stormwater Discharge Monitoring Report and analytical report
for the sampling conducted at the above -referenced site. A stormwater sample was
collected from Outfall 001 on April 7, 2014 and analyzed for total suspended solids (TSS),
pH; -total recoverable lead, oil and grease and ethylene glycol. With the exception of TSS,
the analytical results reported all other parameters below their respective benchmark
values or within their benchmark range. Based on the results of this sampling event, a Tier
One Response has been implemented at the facility. If you have any questions or need additional
information, please contact me at 919-250-991 S
Sincerely,
MID -ATLANTIC ASSOCIATES, INC.
el. q___
Charles B. Hoffman, P.G.
Project Geologist
Attachments: Stormwater Discharge Monitoring Report
Laboratory Analytical Report
EXPERIENCED CUSTOMER FOCUSED INNOVATIVE

L.
J
Mid Atlantic
Engineering & Environmental Solutions
April 21, 2014
Mr. Wendell Louia
Louia Motor Company
2647 East Highway 64
Lexington, NC 27292
Subject: STORMWATER SAMPLING RESULTS
LOUTA MOTOR COMPANY
2647 EAST HIGHWAY 64
LEXINGTON, DAVIDSON COUNTY, NORTH CAROLINA
PERMIT NCGl00066
MID -ATLANTIC JOB NO. 00OR2083.00
Dear Mr. Louia:
409 Rogers View Court
Raleigh. NC 27610
office 919.250.9918
facsimile 919.250.9950
MAAONI_INE.COM
Attached please find three copies of the Stormwater Discharge Monitoring Report (DMR) for the
above -referenced site. Please follow the instructions below to complete this sampling event.
1. Sign and date each DMR on page 2;
2. Forward the first two copies of the report along with the attached cover letter to the
Division of Water Quality; and _
3. Insert the third copy (labeled "FILE") into Appendix C of your Stormwater Pollution
Prevention Plan.
The analytical results from this sampling event indicated the stormwater sample collected from
Outfall 001 exceeded the established benchmark value for TSS. Based on these results, a Tier
One Response should be implemented at the facility. Please complete the attached Tier One
Response Form, evaluate the facility practices and file the completed form in Appendix C
of your SPCC. As always, if you have any questions or need additional information, please
contact me at 919-250-9918.
Sincerely,
MID -ATLANTIC ASSOCIATES, INC.
el... c,
Charles B. Hoffman, P.G.
Project Geologist
Attachments: Cover Letter
Stormwater Discharge Monitoring Report
Laboratory Analytical Report
Tier One Response Form
EXPERIENCED CUSTOMER FOCUSED INNOVATIVE