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NCG060364_MONITORING INFO_20190403
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. IV DOC TYPE ❑HISTORICAL FILE �j. MONITORING REPORTS DOC DATE ❑ p� b J �J � q �J YYYYMMDD STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000 Date submitted 3z*'/ / 2 D/ 9 CERTIFICATE OF COVERAGE NO. NCG060 3 IC � FACILITY NAME Al-A4 COUNTY P - PERSON COLLECTING SAMPLES Ups+ L°/24v4 LABORATORY ,6�/'r1r'f-^t0h 4 / C.ffnir/na b Cert. # A E G I* I ► i!✓.' D APR 0 5 2019 SAMPLE COLLECTION YEAR Za/I SAMPLE PERIOD gJan-June ❑ July -Dec or OMonthlys ,Wq,j ,4 (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply RSA [20ther bi Y'C4 CENTRAL FILES FACILITY ACTIVITIES INCLUDE (check all that apply): "AAM SECTION ❑ use/process meats ®'use animal fats/byproducts PLEASE REMEMBER TO•SIGN ON'THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall z 3�Lnor ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 - 9.0 120 30 10001 500L Parameter Code - C0530 00400 00340 00556 31616 61211 Z 1 1-124� / �% �/• �. / 3 c;2,0 < S, a z r fir.•- , s . RIP Z /1< ' Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 'For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Wonthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes ®'no Permit Date.11/1/2018-05/31/2021 (If ge , complete Part B) SWU-249, Last Revised 11/5/2018 Page 1 of 2 Part.B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > SS gal of new motor oil/month. Outfall No. Date Sample Collected (mo/dd/yr) 24hour rainfall amount, InchesZ New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/O Parameter Code, - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B *FOR PART A AND PART B.MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALLTRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION.B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO 1F YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case 4 "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee Permit Date: 11/1/20IM5/31/2021 Date SWU-249, Last Revised 11/5/2018 Page 2 of 2 .r Environmental Chemists, Inc. �t�enyirochem� ANALYTICAL & CONSULTING CHEMISTS 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Butterball-Farrnviile Date of Report: Apr 02, 2019 3628 South Fields St. Customer PO #: Farmville NC 27828 Customer ID: 17080036 Attention: Don Genova Report #: 2019-04763 Project ID: Storm Water Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-11994 Site: outfali 1 3/21/2019 12.30 PM Water Don Genova Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 03/27/2019 Residue Suspended (TSS) 5M 2540 D 11.1 mg1L 03/25/2019 pH SM 4500 H 8 6.93 units 03/25/2019 COD SM 5220D <20 mglL 03/29/2019 Comment: Reviewed by: _Vol Ab Report #:: 2019.04763 Page 1 of 1 6602 Windmill Way M ENVIRONMENTAL. CHEMISTS, INC OFFICE: 9IG-32-02 3iImingtonFAX910-392-44245 Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info@environmentatchemists_com COLLECTION AND CHAIN OF CUSTODY Client: Butterball-Farmville PROJECT NAME: Storm Water (am -IA �� # � � REPORT NO: ADDRESS: 3628 South Fields Street CONTACT NAME: 0,017. (aA?0t--q PO NO: Farmville, NC 27828 REPORT TO: Don Genova PHONE/FAX:919.252.1326 COPY TO: email: dgenova®butterball.com Sampled By: a4 -iI-4 SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO Soil, SL = Sludge, Other: Collection a = PRESERVATION c cC7 e� ow Sample Identification E n `o `a o M m� a N o 0 0 ANALYSIS REQUESTED Date Time Temp v, `� a " z x x Z ZI�a I /13a J, C P 1)0 1 G �� X TSS, COD pH, Oil and Grease zl/j70� ,�� C G rsr 2) 3 S7-1 C I P 1#rl X 1TSSCC0-D)pH, Oil and Grease 14 1 .91.7 9 1 G Z l,,Ikr 12: 3o s'r- C P ! C P G G C P = G G C P G G C P G G C P G G Transfer Relinquished By: DatefTime ReceivedBy: Date/Time 1. Z l/,%,- 19 // Phi _ Z Z S,37 2. Temperature when Received: 1l Accepted: Rejected: Resample quested: Delivered By: Received By: Date: 3 2 Time: S Comments: TURNAROUND: w�envro:chem �k. ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info a,environnientalehemists.com Butterball-Farmville Date of Report: Apr 02, 2019 3628 South Fields St. Customer PO #: Farmville NC 27828 Customer ID: 17080036 Attention: Don Genova Report #: 2019-04764 Project ID: Storm Water Lab lD Sample ID: Collect DatelTime Matrix Sampled by 19-11995 Site: outfall 2 3/21/2019 12:30 PM Water Don Genova Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 03/27/2019 Residue Suspended (TSS) SM 2540 D 9.5 mg/L 03/25/2019 pH SM 4500 H 6 6.88 units 03/25/2019 COD SM 5220D 22 mglL 03)29/2019 Comment! Reviewed by: Report M: 2019.04764 Pape t of i ill Way mington rTw nd ENVIRONMENTAL CHEMISTS, INC OF ICE' 9 0-392-02 3'tFAX910-39244245 NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info@anvironmentalchemists.com Anaiyiieal & Consulting Chemists COLLECTION AND CHAIN OF CUSTODY' Client: Butterball-Farmville PROJECT NAME. Storm WaterDc.7` 1/,2 � REPORT NO: ADDRESS: 3628 South Fields Street CONTACT NAME: 90,, L 01,001 F PO NO: Farmville, NC 27828 REPORT TO: Don Genova PHONEIFAX:919.252.1326 COPY TO: email: dgenova@butterball.com Sampled By: doi 7 10n 0 vA SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection K H a G A a 8E 1 CC7 'o C� o rn " ix QW m 3 z PRESERVATION ANALYSIS REQUESTED Date Time Temp z z x= a o z o o 1) C P X X TSS, COD, RH, Oil and Grease G G C P G G 2) C P X X ITSS, COD, pH, Oil and Grease G G ,D I J:3 Q r C P q � � l� � '' O► � d' r1�4 I'P 41r7 4D G " !Z= 3D S7- C P / fi111 G93 Zl.h�„ 1?:gyp ST C P COD G �J 2/f�lr� �2'30 �• r C P 14 ii/h G C P G G C P G G Transfer Relinquished By: DateMme Received By: DateMme 2. 3 -2Z ^3 Temperature When Received: 3 . 7 Accepted: Rejected: Resample Requested: Delivered By: __Received By: Date: 3 " Z Timer Comments: 41L TURNAROUND: r �4 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted /Q Tv "y 2a/*' CERTIFICATE OF COVERAGE NO. NCG06 0-3-•6 # SAMPLE COLLECTION YEAR ZQ /? FACILITY NAME Ur.r fir 6a /� f.��nrLi /�� Fl�f /s'!� // FACILITY ACTIVITIES INCLUDE (check all that apply); COUNTY f r t Y' C � �� � Eluse/process meats Q use animal fats/byproducts PERSON COLLECTING SAMPLES _ _ 9On C� / �� R_ DISCHARGING TO SALTWATERS? []YES ®NO LABORATORYP'57,;►'',-,n,qnf• / Lab Cert. # it Il bQ1� ILLS PLEASE REMEMBER TO SIGN ON THE REVERSE 4 CEN� �❑�i0i'' Part A; Stormwater Benchmarks and Monitoring Results DW' Total event rainfall rf A; "or ❑ No discharge this period Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease,' mg/L Fecal Coliform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark - 100 or 50 Within 6.0-9.0 120 30 1000 S00 a Z'r1 P r 4 6.9 -C Z 9 2 os zIfPr Z3? 7• S.1 67 1 Only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. aSee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes 2rno Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark 30 100 or 50 6.0 - 9.0 - Only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. aSee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part B) SWU-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO XC IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one col2y of this DMR including all "No Discharge" re orts within 30 daysof receipt of the lab results or at end o monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) /o (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 r SWU-249 Last Revised: October 18, 2012 Page 2 of 2 0 env{i�rochem . ANALYTICAL & CONSUL_TfNG CHEMISTS Environriiental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalcliemists.com Butterball-Farmville Date of Report: Jul 06, 2018 .................................................................................. ...-_...... ............... ._..................... "3628'S6utH*Fields Sti_ Customer PO #: Farmville NC 27828 Customer ID: 17080036 Attention: Don Genova Report #: 2018-10235 Project ID: Storm Water Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-25708 Site: outfall 1 6/26/2018 2:00 AM Water client Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 06/28/2018 Residue Suspended (TSS) SM 254o D 19.5 mg/L 06/27/2018 pH SM 45oo H B 6,96 units 06/27/2018 COD SM 5220D 29 mg/L 07/02/2013 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-25709 Site: outfall 2 6/26/2018 2:00 AM Water client Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg1L 06/27/2018 Residue Suspended (TSS) -SM 254o D 238 mg/L 06/27/2018 pH SM45ao H B 7.52 units 06/27/2018 COD SM 522oD 67 mg/L 07/02/2018 Comment: Reviewed by: Report,l:: 2018-10235 Paw 1 of 1 ti SEMI-ANNUAL. STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted /4 9-1-2 2,0/,? CERTIFICATE OF COVERAGE NO. NCG06 0 3 G FACILITY NAME �� 7" /!� Lt1 1/ fa��+�i /I! )' lVJ COUNTY P, �f PERSON COLLECTING SAMPLES IlOnn o v.f LABORATORYLab Cert. # Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 20 /00 FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats Z use animal fats/byproducts DISCHARGING TO SALTWATERS? ❑YES ®NO PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall z / %/ 1.'or ❑ No discharge this period Outfall No. Sample Collected, .. mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease,' mg/L Fecal Coliform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark - 100 or 5D Within 6.0— 9.0 120 30 1000 500 o KZ zriP /9 6. 29 4 s 1-71,11111 ti/f *el z 6 //r Z 3 r 7. S-A a' 7 C ,s- Hid Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. QSee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes 2 no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. zThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at anv outfalls, you must still submit this discharge monitoring report with a checkmark here. QSee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (ifyes, complete Part 13) SWU-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS; • A BENCHMARK EXCEEDANCE TRIGGERS TIER I REQUIREMENTS, SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO Rr IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES [] NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the tab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." y (Signature of Permittee) /a (Date Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 F� y - enw�roc�iem- ANALYTICAL& CONSULTING CHEMISTS Environ rental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910-392.0223 Lab • 910-392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.coTn Butterball-Farmville Date of Report: Jul 06, 2018 .... ...................... . ..... 3628'866 i'l=ieltls St. .......... ........ ..... ........................... ..................... Customer PO #: .........._................... Farmville NC 27828 Customer ID: 17080036 Attention: Don Genova Report #: 2018-10235 Project ID: Storm Water Lab II) Sample ID: Collect Date/Time Matrix Sampled by 18-25708 Site: outfall 1 6/26/2018 2:00 AM Water client Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 06/28/2018 Residue Suspended (TSS) SM 2540 D 19.5 mg/L 06/27/2013 Phi SM 4500 H B 6.96 units 06/27/2018 COD SM 5220D 29 mg/L 07/02/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-25709 Site: outfall 2 6/26/2018 2.00 AM Water client Test Oil & Grease (O&G) Residue Suspended (TSS) Method EPA 1664 -SM 2540 Q Results Date Analyzed <5 mg/L 238 mg/L 06/27/2018 06/27/2018 PH SM 4500 H s 7.52 units 06/2712018 COD SM 5220D 67 mg/L 07/02/2018 Comment: Reviewed by: tQ7t�1Q O Report rs:: 2018-10235 Paoe 1 M 1 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted f 14,7 Za!'? RFrFlt/F—D CERTIFICATE OF COVERAGE NO. NCG0r6 0 3 S 4 FACILITY NAME 9u41fr 6a I! FvPj 1W111 COUNTY f PERSON COLLECTING SAMPLES Don NO v LABORATORY 6fmi d-P Lab Cert. # Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR Z a / 7 IAN 1 y.2018 FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ® use animal fats/lAVOR 'AM DISCHARGING TOSALTWATERS? ❑YES ZMMATION PROCESSING UN17 PLEASE. REMEMBER TO SIGN ON THE REVERSE Total event rainfall zY- or ❑ No discharge this period3 Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark - 100 or 50 Within 6.0 — 9.0 120 30 1000 500 Z4. •73 I AV4 .� ;L 1 Ito/7 Sr. 7.0 EHE Only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any out€ails. You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark 30 100 or 50 6.0 — 9.0 - Only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part B) S W U-249 Last Revised: October 18, 2012 Page i of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 doss ot receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under•penalty of law, that this document•.and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 9 0-.4,7 Zaijv (Date) Additional copies of this form may be downloaded'at: http.1/portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 �en��Frochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, INC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway Jacksonville, NC 28540 a 910.347.5843 Lab/Fax i nfnCenvironmentalchemists.com ...---........Butterball-Farmville.----....... --.... ...... _-.-...-...-._-- — __. __ __..._r.-_.....--Date.of-Report:---Jan-09; 2018— ---.....-....._.................... ---- 3628-South-Fields-St. CUStdRler PO-#: Farmville NC 27828 Customer 10: 17080036 Attention: Don Genova Report #: 2017-20016 Project ID: Storm Water i_ab lD Sample ID: Collect Date/Time Matrix Sampled by 17-48539 Site: outfall 2 12/20/2017 5:00 PM Water client Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 12/22/2017 Residue Suspended (TSS) SM 2540 D 55.5 mg/L 12/21/2017 pH SM 4500 H B 7.09 units 12/27/2017 COD SM 5220D 98 mg/L 12/22/2017 Comment: Reviewed by: XWda .�..— 6 ReportW: 2017-20ole �"�riv3rn�hern, ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com Client: Butterball-Farmville j PROJECT NAME: Storm Water �u7� �q ll�a REPORT NO: Cp ADDRESS: 3628 South Fields Irtreet CONTACT NAME: PO NO: Farmvlile, NC 278 8 REPORT TO: Don Genova PHONEIFAX:919.252.1326 COPY TO: email: dgenova@butterball.com Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification I Collection m m w w E o c� G _ E o �j a. 4 �_ o a+ u cLU m z PRESERVATION ANALYSIS REQUESTED �� Da Time TempU z z = g z o i = z o ~ w p 1 j C P X X TSS, COD, pH, Oil and Grease G G C P i G G 2 { C P X X ITSS, COD, pH, Oil and Grease I G G `s r C P �d� G B� zap s"r/'7 sr C P x CaD G 93 Zap c s f4l T C P G u SIT C TSS' G I C P G G II C P II G G I Transfer ; # Relinquished B DatetTime R ived By: Date/Time 1. � Z D /ors // Pi'I � �� �\•'S D 2. �! Temperature when Received: Delivered By: Comments: I Accepted: Re' cted: Resample Requested: Received By:__„__ Date: �I Time: i �jI TURNAROUND: g !61, 7-1 �,� env�irochem�� ur ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 13owsertown Road, Manteo, NC 27954 - 252-473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax iiifo@etiviroiiinentatchemists.com __..___Butterball-Farmvilie-. ---- - .---_--_- .—Date-of-Report:---Jan-09�-2018 - - -- - _...................................._..- - 3628-South-Fields-St. ---- Custam—erPO-#: —Y`T--- Farmville NC 27828 Customer ID: 17080036 Attention: Don Genova Report #: 2017-20015 Project ID: Storm Water Lab ID Sample ID: Collect Date/Time Matrix Sampled by '17-48538 Site: outfall 1 12/20/2017 6:00 PM Water client Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 6 mg1L 12/22/2017 Residue Suspended (TSS) SM 2540 D 24.3 mg1L 12/21/2017 pH SM 4500 H B 6.73 units 12/27/2017 COD SM 5220D 29 mg/L 12/22/2017 Comment: Reviewed by: _- ?nantala 6-- .10 Report #:: 2017-20015 Pnn. t of I ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: OLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentaichemists.com Client: Butterball-Farmville I PROJECT NAME: Storm Water Dy+7,� �� j J' REPORT NO: (} ! I ADDRESS: 3628 South Fields Street CONTACT NAME: PO NO: i Farmville, NC 27828 REPORT TO: Don Genova PHONEIFAX:919.252.1326 COPY TO: lemail. dgenova@butterball.com Sampled By:. ' 4 SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Identification Collection m s m o— UTime m n PRESERVATION ALYSIS REQUESTED ANSample a TempDa x o x° oz 1 j ii C P X X TSS, COD, pH, Oil and Grease l i G G iI C P I G G 2 ►.I C P X X TSS, COD, pH, Oil and Grease f i G G A l D It 6 P,*7 S t C P kV,3� x L D r f dL G�PQsP I I G C P Ca A3 Z► p� sr x �'tf i � .9� 2aI P" ST C X 7-,PP G it C P G G li C P 11 G G it Transfer Relinquished By: Date/Time Received By: Date/Time �., 2. ,I Temperature when Rece Delivered By: Comments: J: Reject d: Resample R que ted: Received By: P ate: 1 23 `j Time: TURNAR UND: 9 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 20 17 RECEIVED JUL 0 'ii11 CERTIFICATE OF COVERAGE NO. NCG06 O 3 6 q SAMPLE COLLECTION YEAR Z 0 / % CENTRAL FILES FACILITY NAME &�> , -, / ^./i FACILITY ACTIVITIES INCLUDE (check all that apply): DWR SFCT101.1 COUNTY P, h' RECEIVED ❑ use/process meats Fuse animal fats/byproducts PERSON COLLECTING SAMPLESn0✓ DISCHARGING TO SALTWATERS? ❑YES XNO LABORATORY Ale lgh4h/f►C. j Lab Cert. 4 JUL 0 7 N17 CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 �� Part A: Stormwater Benchmarks and Monitoring Results DWR SECTION Totol event rainfall z or ❑ No discharge this periad3 Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark - 100 or 50 Within 6.0-9.0 120 30 1000 500 a Zo 1 � of. O j 3 q D /Yr9 /!izl a 04CZO / 7 747 7,0 /7JI Dnly applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. a For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor ail per month? ❑ yes krno Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50 6.0 — 9.0 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part B) SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3; HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ®' IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results or at end o monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 3 T6, , z pi 7 (Date) Additional copies of this form may be downloaded at:.http://portal.ncdenr.org/web/wq/ws/su/npdesswlttab-4 S W U-249 !--I Last Revised: October 18, 2012 Page 2 of 2 aceAnalytical www.pstelab.7.com June 29, 2017 DON GENEVA BUTTERBALL LLC 3628 S. FIELDS ST Farmville, NC 27828 RE: Project: FARMVILLE OUTFALL 1 Pace Project No.: 92345158 Pace Analytical Services, LLC 6741 Conference Orive Raleigh, NC 27607 (919)834-4964 Dear DON GENEVA: Enclosed are the analytical results for sample(s) received by the laboratory on June 21, 2017. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, V� Terri Page for Kristi Dancy kristi.dancy@pacelabs.com (336)623-8921 Project Coordinator Enclosures cc: BECKY MERCER, BUTTERBALL LLC REPORT OF LABORATORY ANALYSIS Y; This report shall not be reproduced, except in full, without the written consent of Pace Analytical services, LLC. Page 1 of 17 Pace Analytical Services, LLC VaceAnalVtica!® 6701 Conference Drive t / � Raleigh, NC 27607 fI/ www.pacelabs.com (919)834-4984 CERTIFICATIONS Project: FARMVILLE OUTFALL 1 Pace Project No.: 92345158 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NCO30 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 17 Pace Analytical Services, LLC ® 6701 Conference Drive aceAnalytical Raleigh, NC 27607 •+ wwwpacefabs.com (919)834-4984 SAMPLE SUMMARY Project: Pace Project No.: FARMVILLE OL)TFALL 1 92345158 Lab ID Sample ID Matrix Date Collected Date Received 92345158001 Al Water 06/20/1718:00 06/2111714:05 92345158002 A2 Water 06/20/1718:00 06/21/1714:05 92345158003 A3 Water 06120/1718:00 06/2111714:05 92345158004 A4 Water 06/20/1718:00 0612111714:05 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 17 aceAnalytical wvrw.paCela&S.CoM Project: FAR MVILLE OUTFALL 1 Pace Project No.: 92345158 Lab ID Sample ID 92345158001 Al 92345158002 A2 92345158003 A3 92345158004 A4 SAMPLE ANALYTE COUNT Method SM 2540D EPA 1664B SM 5220❑ EPA 9040 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical: Services, LLC 6701 Conference drive Raleigh, NC 27607 (919)834-4984 Analysts Analytes Reported GT8 1 JMS t CJH1 1 NMH 1 Page 4 of 17 acmnalytical ww .pm1abs.c= ANALYTICAL RESULTS Project: FARMVILLF OUTFALL 1 Pace Project No.: 92345158 Pace Analytical Services, [LC 6701 Conference Drive Raleigh, NC 27607 s" (919)834-4984 Sample: Al Lab ID: 92345158001 Collected: 06/20117 18:00 Received: 06/21/17 14:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Total Suspended Solids Date: 06/29/2017 09:59 AM Anatytical Method: SM 2540D 8.0 mg/L 2.6 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, 06/23/17 11:41 Page 5 of 17 2eAnalytical —pecefebs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-49B4 Project: FARMVILLE OUTFALL 1 Pace Project No.: 92345158 Sample: A2 Lab Id: 92345158002 Collected: 06/20/17 18:00 Received: 06/21/17 14:05 Matrix: Water Parameters Results Units I Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mglL 5.0 1 06/28/17 06:18 V Date: 06/29/2017 09.59 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 6 of 17 • acmnalytical www.pacelabs.com ANALYTICAL RESULTS Project: FARMVILLE OUTFALL 1 Pace Project No.: 92345158 Pace Analytical Services, L•LC 6701 Conference Drive Raleigh, NC 27607 , {919}834-4984 Sample: A3 Lab Ib: 92345158003 Collected: 06/20/17 18:00 Received: 06/21/17 14:05 Matrix: Water Parameters Results Units Report limit DF Prepared Analyzed CAS No. Qual 5220D COI} Analytical Method: SM 5220D Chemical Oxygen Demand 34.0 mg/L 25.0 1 06/28/17 02:10 Date: 06/29/2017 09:59 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 17 aceAnalytical www.pacelahsmm ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: FARMVILLE OUTFALL 1 Pace Project No.: 92345158 Sample: A4 Lab ID: 92345158004 Collected: 06120/17 18:00 Received: 06/21/17 14:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 9040 pH pH Date: 06/29/2017 09:59 AM Analytical Method: EPA 9040 6.5 Std. Units 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 06/23/17 13:00 H1,H6 Page 8 of 17 Pace Analytical Services, IaLC /� Analytical 6701 Conference Drive Raleigh, NC 27607 WWW.Peseleb&C0M (919)634-4964 QUALITY CONTROL DATA Project: FARMVILLE OUTFALL 1 Pace Project No.: 92345158 OC Batch: 366270 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated lab Samples: 92345158001 METHOD BLANK: 2030405 Matrix: Water Associated Lab Samples: 92345158001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 06/23/17 11:40 LABORATORY CONTROL SAMPLE: 2030406 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 266 1D6 90-110 SAMPLE DUPLICATE: 2030407 92345198001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 6.1 213 189 5 D6 SAMPLE DUPLICATE: 2030408 92345150001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 600 600 0 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/29/2017 09:59 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 17 . aceAnalytical wwwpacelab&Mn QUALITY CONTROL DATA Project: FARMVILLE OUTFALL 1 Pace Project No.: 92345158 QC Batch: 366286 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN Associated Lab Samples: 92345168004 SAMPLE DUPLICATE: 2030513 Parameter pH 92345158004 Dup Units Result Result Std. Units 6.5 6.5 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Max RPD RPD Qualifiers 0 9 H1,H6 Results presented on this page are in the units indicated by the" Units" column except wti ere an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Sidi, Date. 06/29/2017 09:59 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 17 aceAnalytrcal wwwpacefabs.cont QUALITY CONTROL DATA Pace Analytical Services, kLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: FARMVILLE OUTFALL 1 Pace Project No.: 92345158 QC Batch; 366791 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92345158002 METHOD BLANK: 2033178 Matrix: Water Associated Lab Samples: 92345158002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg1L ND 5.0 06128117 06:17 LABORATORY CONTROL SAMPLE: 2033179 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 37.2 93 78-114 MATRIX SPIKE SAMPLE: 2033180 92345526001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL ND 40 36.8 92 78-114 Results presented on this page are in the units indicated by the "Units" column except where an altemate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 06/29/2017 09:59 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 17 aceAnalytical www.Pacelablcom Project: FARMVILLE OUTFALL 1 Pace Project No.: 92345158 QC Batch: 366600 QC Batch Method: SM 5220D Associated Lab Sampies: 92345158003 METHOD BLANK: 2032040 Associated Lab Samples: 92345158003 Parameter Units Chemical Oxygen Demand mg[L LABORATORY CONTROL SAMPLE: 2032041 Parameter Units Chemical Oxygen Demand mg/L Pace Analytical Services, LLC 6701 Conference Drive Raieigh, NC 27607 (919)834-4984 QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 06/28/17 02:10 Spike LCS LCS % Rec Cone, Result % Rec Limits Qualifiers 750 778 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2032042 2032043 MS MSD 92344982001 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand mg/L 21.OJ 750 750 852 833 111 108 90-110 2 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2032044 2032045 MS MSD 92345160003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand mg/L 178 750 750 954 996 103 109 90-110 4 3 R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/29/2017 09:59 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 17 ace Analytical www.pacwabs.cam QUALIFIERS Project: FARMVILLE QUTFALL 1 Pace Project No.: 92345158 `a14yL`Ii11119HR DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL- Practical Quantitation Limit. RL- Reporting Limit. Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 , (919)834-4984 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/29/2017 09:59 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 17 aceAnalytical _pecelabs.Mm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: FARMVILLE OUTFALL 1 Pace Project No.: 92345158 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 {919}834-4984 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92345158001 Al SM 2540D 366270 92345158004 A4 EPA 9040 366286 92345158002 A2 EPA 1664B 366791 92345158003 A3 SM 5220D 366600 Date: 06/29/2017 09:59 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Without the written consent of Pace Analytical Services, LLC. Analytical Batch Page 14 of 17 Document Name; UI le'cn spec Document Hevlteo: kept. '21, ZU16 aceAnalytiea! Sample Condhton U on Recei t SCUR Pa e 1 of 2 Document No.: Issuing Authority; c rear a.rva.wa.. n, I ._._ ,..,u . —-- Laboratory receiving samples: Asheville ❑ Edeno Greenwood ❑ Huntersville ❑ Raleigh® Mechanicsville❑ Client Name: �Project? WO# : 92345158 � 1 IIIl6��6ii11 Irf I pYpY I I I Cc Fier ❑ Cam mercfal Fede ❑UPS ❑pSher_ [:]Client9��Ilil jr451158 III ■pp f 11!! li Custody Seat Present? []Yes No Seats Intact? ❑Yes e _ Dale/Initials Person Examining fantenwk..I b `•- ' Packing Material; ❑Bubble Wrap ❑Bubble Bags Nano ❑Dthr:r: Thermometer: ❑ ®IR Gun ID: , IS-3492 _ Type of ke: We[ Bluo ❑Hone ❑ process Samples an ice, cooling has begun Correction Factor: sue.os Cooler Temp Corrected ('Q: r Biological Tissue Frozen? ❑Yes ONO 1/A Temp should be above tr g to 6'C USDA Regulated i! { N/A, watersamptel Did samples a mate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did simples originate from a foreign source (int tional IV, ❑Yes o including Hawaii and Puerto Rico!? (:]Yes/.UHo {ommern s/Discrepancy: Cha In of CustodyPresent? Ll t, Samples Arrived within Hold Time? �. Short Hold Time An■ s 02 ht.)? U Rush Turn Around Time Requested? 4. Sufficient Volume? S. Correct Containers Used? -Pace Containers Used? �55_t"�In 6. Containers Intact? 7. Samples Field Filtered? 8. Note i( sediment is visible in the dissolved container Sample Labels Match CDC? � -Includes Oate/Tirne/i6/Analysis .., 9. Headspace in VOA Vials >5.6mm ? El Yes L1 No WA 10. Trip Rlank Present? Trlp Blank Custody Seals Presmt? Yes Yes No No NA "fik It. CLIENT NOTIRCAT1ON/RESOLUTION Person Contacted: Cemments/Sample Discrepancy: Date/rime; Field Data Required? ❑Yes UNO Project Manager SCURF -� f Review: f� Date: Project ManageraRF , , Review: ���//%M IP date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a COPY of this form will be sent to the North Ground OEHNR Certifkation Office (Le. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 15 of 17 �CeAltdlytiCa!- CHAIN-OF-CUSTODY I Analytical Request Document The Chat -WA shay is a LEGAL OOCULfEtTT. M m* and fi&W3 moat be =Tpk ed acvnarely. P.a: deeUu` A SaetlaD Lt Saeilae C at Repeal cat kewme s., R� aa.mMt bet"som krIckv konvidwi `"°°"Ta 2144057 '8w1Ye l-411 CC C. a G dva Shaer Tc. il i e14- -N c—Ta a GVLAUKVACENCYr . x $ �/1% Jry, Irre HADE�a� s F GROUNDWATER F- DRIHwATER UST i RCRA f OTHER �y �Z/7p2i a. 4 Br � � Pun *&/ m C,*w No_ r Sao Lacallen STATE ; agiaat-d Due DaprTAT: N-er, Pxrrr Raquasted AMli"t nit arsd (T/M . . >^ . Sawdm D Yam! Cady P. WadCTeNlOd� ru s ' COLLECTED Primwelivas -X sDW*k ? W�Ar Ow wal. WSW w1 U 8T. ka& wola v p g F — SAMPLE ID all CL �i}• J.-T. W7-Da1:4 Ar AR 8aapI. IfM MUST OE ONQUE T... TS GVrr OT U � � � � A w O U °c g C DATE TIME 7 2 2 I z z a Ur y M Paco Pro act N*J Lab I.O. '61 Mwh za7.F 6 P.q .61 11 SA9 1 `a 1 s e i 0 TD n Tx ADDno,"LCOtulEm :: RLLBtQU9 MoTI AFF0.MTSON DATE TIME ACCEPTED OT I AFFYIATTDIE DATE .- .TtLE: . SMIPLECOMDITTDRS ' •TyRa !! � 1 ! SAMPLER NAME AND SN.NATURE ORIGINAL Pima Nema arsrulPT.M On �a IrA R R q • SIQNATtrRE o, sA�eaEle DATE 64"d Z & �� -a `, 7 • aa�br hapwti an am}oy re acvo gr.u�rET»an oas+a<i>a-+w,e y..nenww,a..aT.lfV r..wr n.o,n.-a on rev. aoa f` FALL-Q-WD •A7. 1SWy-713137 O LD CU LR M umunlelll ivamC: C 1 lem N)pc Sans le Condition up" on Recet t se dCGAOy AWI ' m Docuent l c_rAos-mmoe., no *Check mark top half of box If pH and/or dechlorinatlon Is verified and within the acceptance range for preservation samples. "Bottom half of box Is to list number of bottles Projei �uiuimrru -ev "u: Dept. ar, �Uta Page 2 of 2 -- — _ WOW 92345158 PM: KPD Due Dale: 06/30/17 CLIENT: 91-Bullerba! a T z. ? LL .yY. n m ? .Sf a m .f�yaQ n m 2 y C 6 m n .Yy a m 0. m Z m a st 3 a v a u a V a a a > t 2 3 d 5 6 7 B 4 16 11 12 pH Adjustment Log for Preserved Samples sample IQ Type of Preservative pN upon recatpt Oats pnservadon adl+ated Time preservation odfutted Arnount of Pros mdw added tot a Page 17 of 17 ace Analytical wwwpacefabs.com June 28, 2017 DON GENEVA BUTTERBALLLLC 3628 S. FIELDS ST Farmville, NC 27828 RE: Project: FARMVILLE OUTFALL 2 Pace Project No.: 92345160 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear DON GENEVA: Enclosed are the analytical results for sample(s) received by the laboratory on June 21, 2017. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Terri Page for Kristi Dancy kristi.dancy@pacelabs.com (336)623-8921 Project Coordinator Enclosures cc: BECKY MERCER, BUTTERBALL LLC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 17 accAnalytical / rnvw.pacela,5s.com Project: FAR MVILLEOUTFALL2 Pace Project No.: 92345160 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Charlotte Certification IDs 9800 KinceyAve. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #; 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #; 99030001 VirginiafVEI AP Certification #; 460222 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 2 of 17 aceAnalytfical www.pacelebsx= SAMPLE SUMMARY Project: FARMVILLE OUTFALL 2 Pace Project No,: 92345160 Lab ID Sample ID Matrix Date Collected Date Received 92345160001 131 Water 06/20/1718:00 06/2111714:05 92345160002 B2 Water 06/2011718:00 06/21/1714:05 92345160003 133 Water 06/20/1718:00 06121/1714:05 92345160004 B4 Water 06120/1718:00 0612111714:05 REPORT OF LABORATORY ANALYSIS Thls report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Pace Analytical Services, !_LC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 3 of 17 aceAnalytical _pscelabs.com Project: FARMVILLE OUTFALL 2 Pace Project No.: 92345160 Lab ID Sample ID 92345160001 61 92345160002 B2 92345160003 63 92345160004 B4 SAMPLE ANALYTE COUNT Method SM 2540D EPA 1664E SM 5220D EPA 9040 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Tull, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services. LLC 6701 Conference Drive Raleigh, INC 27607 (919)834-4984 Analytes Analysts Reported GTB 1 JMS 1 CJH1 1 NMH 1 Page 4 of 17 lacieAnalyticalo www.AetafSb&=" ANALYTICAL RESULTS Project: FARMVILLE OUTFALL 2 Pace Project No.: 92345160 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: S1 Lab ID: 92345160001 Collected: 06/20/17 18:00 Received: 06/21/17 14:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 475 mg/L 25.0 1 06/23/17 09:17 D6 Date: 06/2812017 04:02 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 17 aceAnalytrcal www.pacWabs.com ANALYTICAL RESULTS Project: FARMVILLE OUTFALL 2 Pace Project No.: 92345160 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: 62 Lab ID: 92345160002 Collected: 06/20/17 18:00 Received: 06/21/17 14:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 06/28117 06:19 Date: 06/28/2017 04:02 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Without the written consent of Pace Analytical Services, LLC. Page 6 of 17 aceAnalytical www.pecalab&=n ANALYTICAL RESULTS Project: FARMVILLE OUTFALL 2 Pace Project No.: 132345160 Pace Analytical Services, +-LC 6701 Conference Drive Raleigh, NC 27607 (919)834-49B4 Sample: E13 Lab ID: 92345160003 Collected: 06/20/17 18:00 Received: 06/21/17 14:D5 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5220D COD Analytical Method: 5M 5220D Chemical Oxygen Demand 178 mg/L 25.0 1 06/28/17 02:10 R1 Date: 06/28/2017 04:02 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 17 aceAnalytical e —pacelabs.corn ANALYTICAL RESULTS Project FARMUILLE OUTFALL 2 Pace Project No.: 92345160 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: S4 Lab ID: 92345160004 Collected: 06/20/17 18:00 Received: 06/21/17 14:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 9040 pH Analytical Method: EPA 9040 pH 7.0 Sid. Units 0.10 1 06/22/17 15:06 H1.H6 Date-. 06/28/2017 04.02 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 17 aceAnalylical. wrvwpacefalecotn QUALITY CONTROL. DATA Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-49 B4 Project: FARMVILLE OUTFALL 2 Pace Project No.: 92345160 QC Batch: 366216 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92345160001 METHOD BLANK: 2029978 Matrix: Water Associated Lab Samples: 9234,5160001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 06123I17 09:12 LABORATORY CONTROL SAMPLE: 2029979 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 256 102 90-110 SAMPLE DUPLICATE: 2029980 92345160001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 475 502 6 5 06 SAMPLE DUPLICATE: 2029981 92345090001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg1L 83.1 82.7 1 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2017 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 17 aceAnalytrcal wtvwpacelabs.com Project: FARMVILLE OUTFALL 2 Pace Project No.: 92345160 QC Batch: 366112 QC Batch Method: EPA 9040 Associated Lab Samples: 92345160004 SAMPLE DUPLICATE: 2029570 Parameter Units Std. Units pH QUALITY CONTROL DATA Analysis Method: EPA 9040 Analysis Description: 9040 pH EDEN 92344883001 Dup Result Result RPD 7.8 7.8 0 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Max RPD Qualifiers 9 H1,H6 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the rtght of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date'. 06/28/2017 04:02 PM without the written consentof Pace Analytical Services, LLC. Page 10 of 17 aceAnalXical. wwwpacelab&com QUALITY CONTROL DATA Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: FARMVILLE OUTFALL 2 Pace Project No.: 92345160 QC Batch: 366791 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92345160002 METHOD BLANK: 2033178 Matrix: Water Associated Lab Samples: 92345160002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 06128117 06:17 LABORATORY CONTROL SAMPLE: 2033179 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 37.2 93 78-114 MATRIX SPIKE SAMPLE: 2033180 92345526001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL ND 40 36.8 92 78-114 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/2812017 04702 PM without the written consent of Pace Analytical Services, t.LC. Page 11 of 17 aceAnalvfical wwwpacefabs.corn QUALITY CONTROL DATA Project: FARMVILLE OUTFALL 2 Pace Project No.: 92345160 OC Batch: 366600 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92345160003 METHOD BLANK: 2032040 Associated Lab Samples: 92345160003 Parameter Units Chemical Oxygen Demand mi LABORATORY CONTROL SAMPLE: 2032041 ` Parameter Units Chemical Oxygen Demand mg1L Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 06/28/17 02:10 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 778 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2032042 2032043 MS MSD 92344982001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qua[ Chemical Oxygen Demand mi 21.OJ 750 750 852 833 111 108 90-110 2 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2032044 2032045 MS MSD 92345160003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand mg1L 178 750 750 954 996 103 109 90-110 4 3 R1 Results presented an this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2017 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 17 acMnalytical www.patefab&CM QUALIFIERS Project: FARMVILLE OUTFALL 2 Pace Project No.: 92345160 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit, PQL- Practical Quantitation Limit. RL- Reporting Limit. Pace Analytical Services, !LC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 S - Surrogate 1,2-Diphenyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SVV846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260, N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2017 04:02 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 17 aceAnalytical o —pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: FARMVILLE OUTFALL 2 Pace Project No.: 92345160 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92345160001 B1 SM 2540D 366216 92345160004 B4 EPA 9040 366112 92345160002 B2 EPA 16646 366791 92345160003 B3 SM 5220D 366600 Date. 06/28/2017 04.02 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch Page 14 of 17 UDCumem ivamu: &;w socn spec aw. �snvu+eus nev�xps. Sam leeonditlon U on Recei t[SCUR} Page I of 2 I uro ace Ai131ytrcal` Document No.: Issuing Authority: F-CAR-CA-003-Rev.02 Pace Quality Office laboratory receiving samples: Asheville ❑ Eden[] ❑ Huntersville ❑ Raleigh® Mechaniesvillerl yG�reee%nwood INEM [[lent Name- ��\I l u " WO# : 92345 1 60 Prole, Courier: ❑Fed clups cusps ❑Client � ❑ Commorciaf ce ❑other: � 9234516B — Custody Seal Present? ❑Yes Seals Intad? []Yes O - �� / 1 / Pack]ngMaredal: ❑Bubble Wrap ubble Bags []None❑Other: Thermometer: Date/tnldals Person Examining Cent* yre! M IR ciun ID: _ IS-3492 _ TYpe oe 1 : ❑Bloc ❑Hene ❑Samples an Ice, cooling process has begun Correction Factor: Cooler Tamp Corrected I'Cf: f Biological Tiuue Froze ©Yes QNo /A tuaai .� . e, Temp should be above freer' o 6'C n? USDA Regulated Sol /A, water sample► Did samples or . to In a quarantine tone within the United States: CA, NY, or SC (check maps)? Bid samples originate from a foreign source (lntem ❑Yes o including Hawaii and Puerto alfo)? []Yes No Comm ems/Dlscre ancy. Chain or Custody present? 1. Samples Arrived within Hold Time? 11 2. 5hort Hold Time Analysis (472 hr.)? 2MI D 3. RushTum Around Time R uerted7 4. Suffldent Volume? 5. Correct Containers Used? -Pace Containers Used? Ei U 0 6. Containers Intact? Samples Field Filtered? ❑ 8. Note if sediment Is visible In the dissolved container Sample Wbels Match 000? •includes Datc/Time/ID/Anairsis VV 9. Readspace in VOA Vials (a5.6mm)7 Yes No N. 10. Trip Blank Present? tripBlank Custod Seals Present? Yes ❑ Yes No N ❑ No N I1. CLIENT NOTIFICATION/RESOLUTION Field Data Requ3nsd? ❑Yes ❑No Person Contacted:' Date/Time: Comments/Sample Discrepancy: Project Manager SCURF Review- r� Date: Project Manager SRF t ' i Review; Date: Note: Whenever there Ise dherepancyoffectinis North Cwolinacompliamesamples, acopyolihlsformwillbesent totheNonhCarcirnaDEHNRCendkationOftkehe. Out of hold, incorrect presenralive. out of temp, incorrect containers) Page 15 of 17 0 /92 CHAIN -OF -CUSTODY! Analytical Requesi Document The Chaw,01Z,." la a LEGAL DOCUMN7. M lekvm r.kft W.Af be *0.v1cW a=v&Wy, SscUonA secoon 0 sacd— C ftw� R.Q.k.d CkM kft-NAM Rcluko Pr.0d 1rftTw6= rnam "mnwi , "ROV-48 4e C p" o,, .1 2144058 Cow St .D TO. Z REQULATqW F NPDES ;- GROUNDWATER r- DRINIQNG WATER F LIST CRCRA r- OTHER Ord. W.; Z.7.CT.P J-J" P�a F-qwa Due DaWTAT: r room P"Tow, ,ftwaftd Anatyab FUwrod 5-1— D 1144. od,ftm W.W ow W� W1 wm%a W.L SAMPLE ID W" 11p Abr AR Tie— TS ODW in X CAXLECTE-D Wyy COE 0 . A14SBN9jiWa p ;F I M Cz 0 " - z 1-7 V =9 1 Pace Project No.! Lab I.D. IT.E CAM nM-- e. e. AMMMAL60WOM '..,,;RELVKWMFMDffYIAFFXLILTM,.,. ArAMPT EDDY/ SAMPLE CMnrncM Mug- 1S 4, V-0 V ORiGINAL PFMTW.-0SMPLEFL D— S"APPAP.1 LE ZO X-V Z,1/ 7 W—by W4,0ea k— Y,. — —" P. .E7 V-tpr— — —.0—M . ---g. 0 1 M —m W v k.c— -ow w 30Mr. F*11-Q4Z0mv.0,r, irw&r-2007 >b 3 b K 'R 2 a 9 A 9 Z D f.1. 3 7 c a p � � D n to N O 3 Iib n � 6 N � � d o � N y� n e yn n V n n� M Items BP4U425 mL PlaSTiC Unpreserved (N/N (0-1 MU•250 ml Plastic Unpreserved (NIA) BP2L1-5W mt Plastic Unpreserved jN/Af BP1U-1 liter Plastic Unpreserved {NIA) M-250 mL Plastic 42504 (pH < 2) (LI) ELM-250 mL pbStic 44NO3 (pH <21 BP32-250 mL Plastic 2N Acetate & MOH (>9) BP3C-ZW mL Ptastk N20H jpH> 12) JO-) WGFU-Wide mouthed Glass jar Un preserw!d AGIU-1 liter Amber Unpreserved (N/A) (Cl-) AG1H-1 Wier Amber HCl (pH <2) AG3U-250 mL Amber unprgs4ne0 INIA)(CI-) AG15.1 liter Amber H25D4 (pH <21 AG35.250 mLAmber H2SO4 (pH <21 AG3A(DG3A)•25DmL Amber NH4CI (N/A)(C1.) DG9H•40 mL VOA HCI (NIA) V69T-40 Mt VOA Na2S203 (NIA) VG9L]-40 mL VOA Unp (N/A) OOP-40 mL VOA H3PD4 (WA) VOAK (d vials per Idq-5035 kit (NIA) V/GR (3 Vials per W*VPH/Gas kh (N(A) SPST-125 mLSterile Plastic (NIA- tab► SPZT-250 MtSterile Pkastic (NIA - tab) BP3A-250 mL Plastic (NH2)2504 (9.3.9.7) Cubltalner VSGU-20mL%ntillattonvials INIA) GN r ry 0- CL p/ 3 C jC d eT . 3 v c 5' ° m x H ° ^ m -- o ° w a � 3 m C 7 CL a0 a c un ro Q 0 ^ 0 sAn ° o e�i C o 3 n O 2 M n r 3 E. -4 o 3 ' N n fi n w C. : Cr IT W r+ v aceAnalytical "wpacerabsccan Lorenzo Falls Goldsboro Milling Company PO Box 10009 Goldsboro, NC 27532 Project: MILL 4 OUTFALL 1&,2 Pace Project No.: 92324306 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 // (919)834-49B4 30 RECEIVED Page 1 of 2 lJ Laboratory Report ?,01i CENTRAL FILES DVVR SECTION Report Date: 01/10/2017 Date Received: 12/21/2016 Sample: Ai-A7 (OUTFALL 1) Lab ID. 92324306001 Collected: 12/20/16 20:00 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 2540D Total Suspended Solids 8.2 mg1L 2.5 12/22/16 13:30 EPA9040 pH 6.6 Sid. Units 0.10 12/23/1612:15 HJ,H6 EPA 16646 Oil and Grease N❑ mglL 5.0 12/30/16 06:56 SM 25406 Total Solids 60.0 mglL 25.0 12/27/16 11:26 D6 EPA 350.1 Nitrogen, Ammonia 0.065 mg1L 0,010 12/28/16 15:19 SM 4500-CI-E Chloride 2.1 mglL 1.0 01/03/17 17:51 SM 5220D Chemical Oxygen Demand 12.0 mg1L 10.0 12/27/16 23:23 Sample: B1-B7 (OUTFALL 2) Lab ID: 92324306002 Collected: 12/20/16 20:00 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 254DD Total Suspended Solids 66.5 m91L 6.2 12/22/16 13:30 EPA9040 pH 6.6 Std. Units 0.10 12/23/16 12:15 H1,H6 EPA 1664E Oil and Grease ND mglL 5.0 12/30/16 06:57 SM 2540B Total Solids 463 mglL 25.0 12/27/16 11:27 EPA350.1 Nitrogen, Ammonia 3.4 mglL 0.030 D111011713:24 M1 SM 4500-CI-E Chloride 59.2 mglL 4.0 01/03/17 18:06 SM 5220D Chemical Oxygen Demand 39.0 mglL 10.0 12/27/16 23:23 ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 \Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Reviewed by: vim` Terri Page terd.page@pacelabs.com Charlotte Certification iDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 . North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 Page 1 of 6 aceAnalytical wwwpecefabac m Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 633 VirginiafVELAP Certification #: 460025 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 2 of 2 Page 2 of 6 Laboratory receiving samples-. Asheville C1 EdenD Document Nairti� : . ; , -- L. Document No,:. I` -t� .1 - F-CAR-CS-033-Rev.01 Greenwood Ej liultCerstiH nA(i1Ment,fIw5*ed: Sept. 21,200 Pate 1W_ JjsukurAuthofity: ' A . . . . . . . . . . . W Client Name; 6c"W-Lr- M,11(� . projact", ca urler: Fed UPS USPS []Client IN 11111111 C] Commercial. ace 92324306 Custody Seat Present? [jYes rho/Seals3Intact? [:]yes 3j- Date/iftItIals Person EwInN Cwt&M, �f Pa'cklrig Material: 05ubblewrip 0Bubble Rags 13t,40110 [)othr.^ Type of fee; et -[]8rue .[314civ DarnpIesonkewokngpr0c4uWb CorrecIW(a6orWJ-k Cooler Tomp Cwected ('Cj; C.r Slologleal Ti.isue Fro36n? E]Yes []ND 9@VA- Temp should be above f USDA Regulated Wkwattw-rnple) 0yes •M_ Charn afounq Present? Yet Cj% 0I 1. 7- Sant-keh-ed iithrn "d TIm el 611i" 173RO" f'1HJA I Shart Htild nme Analysis (Q2 hr.)? o 7_ _.RUsh Turn Are" Tbne Requested? aye,- to )lVA -6' 4. s4fickrit Volume? 51* Coirtict Containers Used?' -Pate Lmurners Used? CIRO CIIVA C Containers Inlaa? Yei[�rlo. _[1741AL C]t A 7. Sam ples Field Fdtefed? �Ciiis--Uao MCA & Nctttfsedinaitj Is �Islbfe In Oe disfakti container Smpla labels match Coc? 4x;au4iSD&kn—AD'Ana lysrs Matdl-__16�v / []Ila (3111A 9. eleaftacq In VOA Vlals (>5-6mm)? %) J11A 1-10. Top BlarikPiesent? 702 WanYCLtstody Seals WeWt?. []Yes [1yes 0:40 QII*.— �/A, 11. CU Fiff UOMFICATIOWKSOLUTI ON • Fkkf Data Re4ukt& DYes 0110 PeiwnCoilacttd: DatAlrWo: Commenti/Sample Wscrepancy. rt C-C2. projeck &JanMse SCURF Date: Prqject Manager SRP RwOw. Date. put . �af- W'A�,IO!TOP!m il!kll tof ti", Page 3 of 6 uocomentNo-:,: ✓— 4mnutnortty: 'y _ _ F{AR{S_-0_3.3-Aey.ol: . :•: Check mark top half of box If PH and/or dechlorination -.Rroje F0 • 923243 is verified and within the acceptance rangy for ! Pfi. THP 06 preservation samples. 1 buej date: el/@6 o/17 — CLIENT: 91-Go1duP11jj ttom-ltal(-vf�bac-Is-toifst-numberaftrottles _. -'- son 0 in ONE I HIM in logo I pH A" ustment Log for Preserved Samples •SwOoLD 7ypeofProaer-40e PHoponM Wpt .p yruerv+tlonsdJlatee• lime"W"Llca e>lastee ATomtofNPAVIttve Wed lots Page 4 of 6 CM IL CHAIN -OF -CUSTODY I Analytical Request Document 3G@/3l)31jd!(dl TheCK*—&C -xar R a LECAL COCUWZJa. AF a� r� —.9 be — Demd .ma tey. � ca SaeDee A S.eben S Swbn C / a To: oem 2072223 Aon La Q/� d dt Ji S. C .riF• Cady T¢ f A.I //6� CI. REGULATORY AGENCY F4,^w 1fe ,✓ Z7 P Z 1= r NPDFS r cRovND WATER r oRINlQNc WAFER r UST r RCRA r OTHER E' 7, i^/ �/ PWan 6�aerl-w: Ne a sec /VC Z7,1720 7,ca6 F ,: 1_pr3- a63p a' r,7 / /1 sy !"� 1/ I .� ° °"K 61Sa Lotadon _'� SrAM' R.p...ad 0- D—TAT; wnDar, wa+. C Raquwb,d AnaySIS Fllmmd (YIN) - ... . rt.a.a.ra..eeA,m..ae� MmrsI+=05 ' `s COLLECTED P,USUAIBi z 3- I enntYp w.s. ow wr � ow 6 a wl � wMa } �} 3tn ��e� OL .. ga3a SAMPLE ID ro. � u a - {a..Zb91_) An AR w S d $ S—,,a1D,WATEELPJH E Th OS C S Z A a U r O a 679 g a10 Z z n DATE TJME D�,>: TIME '�' 7 S s :1 O Pate Proj&d NoJ Lab I.D. : 671 VJIVC yP-7 1 vri C zanfe Is,," i s s 1s e �7'Z040p 19m ! vq ,o A0WMALC6MMeP S .FMJ*QU 3"MUY/AFHWn0N DATE nME ACCC"EDEYrAFFWAT10M DATE Twa SAMPLE CORWT�ONS ORIGINAL EA�Vt.ER!✓AI,E ANQ S,GruTURE ;a fi,. xx rawrw.n.a,Sw•LE2CDon Gega-f z L A € € =XATnRE M EAMPLER� DATE la�ba 2, I (/` C 1 471 a V v1 'MgwN Ili'0,--1 p —ao-01p Pint-1 M4,O —r piwip a--".0,3%P.—W ,—M and—. "a F-AU-0-020O,/A7. 1$-"W-n07 ///� �(/�CRAIN-OF-CUSTODY I Analytical Request Document iiellf ldi F_ [ `-{`-u" CnuLncfam°r a a LEGAL OOCUtAEfR. NI reMv�rrz tbltla meet be oomP�dna .coXeury. O 0 r S.ctlan A Secyon S"flon C R.yrawd C1 a EFarn aeon: R.Ry Peep �roieue°ti >rMvco a —WN Rapm, T . 2072224 .. 11 4,14 :,..rr T,,r,. Iq P ' S.f t 1dr -pl.. °ep Ta 'Pre I / C.. R£GuLATORY AGENCY• . _: ✓.�� /}/� 7.?Zg •f^ ��1,6, r NPDES f' GR4l1NC WATER f' URWgNG WATER r UST i RCRA I• OTTER I/Z Ev. we+�or°w Na p, G Ar.2 dw She Lautlon • TE STA /+ yC. Rvgw.e.e D— C.I.ITAT: Vml°ct NI.Mw .r. >�.n�1 RaguesWd AtM"ft FB:aMCI (TIN) .. ' S-5— 0 M.trk C.e.. A.oi.eCA..-ft . MAT" , C a COLLECTED Presewetivgs Y > &n ft vr.rr C— Wn g u vvam&water vP+r cn..aNrc $oIVStlIC SL m SAMPLE ID a,d Cx a s4Y WP (A-Z 0-0I,-] Av AR ' C. k=,r BE UMOUE 76*' TSOT x w TCITE�a T.- o n 6 r W � a � U � � p^ � � � � = = u i 2 � O � � Pace Pro N*J Lab I.O. + G ZaDer z A JIVI G aL�'c ! G eD �I 1 r s a S 4' G ZD P 1 7 G der P� a +: AoWnONAL CMm E!rm .. RELMOUMMEO BY I AFFLMMOM DATE TIME `'.4000PIm aft AF UATko DATL 7TYQ 5MIPLE COWMONS icy ZO DPr 9 o LA nm l2..ZI•('Z� r •s✓ 6AMPLER MAM E AMC STOMA11AW ORIGINAL � Y� ��� s�• PRWmt el SAYPLM OA7Y Skn.°ZQ E ee ! S$ Sn"TIRtS.t uMPLEA: 2a�6 Mir K F-ALL-C-027w Ulr.+S4AM'2WI SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 12 J4. ZOO CERTIFICATE OF COVERAGE NO. NCG060 34 FACILITY NAME Ga Urlu,-s COUNTY Pi tf PERSON COLLECTING SAMPLES 9417 0/✓C LABORATORY (QcP dim /y tea Lab Cert. tt Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR ZD 1r�. RECEIVED FACILITY ACTIVITIES INCLUDE (check all that apply): IAN 3 1 Z017 ❑ use/process meats Wuse animal fats/byproducts DISCHARGING TO SALTWATERS? ❑YES YNO CENTRAL FILES DWrR SECTION PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ./ Total event rainfall 2 k1f or ❑ No discharge this period Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark - 100 or 50 Within 6.0--9.0 120 30 1000 500 I �oDPC &I'L 91A .6 /a tia Zo Arc lDi d 6. S 3 9 14__10 �9 1 Only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes krno Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50 6.0 — 9.0 Only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part Bj SWU-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART li SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO kr IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring_ period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 276991617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) IQ 3917 2d/7 (Date) Additional copies of this form may be downloaded at: http://portal_ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted o2 7 j"- I y ZO/6 CERTIFICATE OF COVERAGE NO. NCG06 U 3 6* q FACILITY NAME C>O&J COUNTY /01 f_7" PERSON COLLECTING SAMPLES 044 K'P-17ay4 LABORATORY PAOe A14 f v7'ICR f Lab Cert. # Part A: Stormwater Benchmarks and Monitoring Results RECEIVED % JUL 2 9 1016 s" SAMPLE COLLECTION YEAR 00 /�_ CENTRAL FIL FACILITY ACTIVITIES INCLUDE (check all that apply): DWR SECTIC ❑ use/process meats 2use animal fats/byproducts DISCHARGING TO SALTWATERS? []YES &10 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall z or ❑ No discharge this period3 Outfall No. Sample Collected, mo/dd/yr TSS, mg/L . pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 ml `Enterococci , Colonies per 100 ml Benchmark - 100 or 50 Within 6.0 —9.0 120- 30 1000 , Soo T T,;I Ira 3 0 • klp. Only applies to facilities that use/process meats. zThe total precipitation must be recorded using data from an on -site rain gauge. s For sampling periods with no discharge at aM outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes Nrno Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L T55; mg/L pH; ' " Standard units - New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504, 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. The total precipitation must be recorded using data from an on -site rain gauge, 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes• complete Part' B)' " SWU-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PAIN B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART if SECTION B. * TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NOS' IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results for at end o monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) aV �G6 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/wslsun desswtstab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 aceAnalytica! i If www.paca)abs.com Lorenzo Falls Goldsboro Milling Company PO Box 10009 Goldsboro, NC 27532 Project: DETENTION POND Pace Project No.: 92304122 Sample: Al-A7 Method SM 2540D EPA 9040 SM 2540B EPA 350.1 SM 4500-CI-E SM 5220D ANALYTE QUALIFIERS Parameters Total Suspended Solids PH Total Solids Nitrogen, Ammonia Chloride Chemical Oxygen Demand V�CC�o6o��� Laboratory Report RECEIVED JUL 2 9 2016 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NO 27607 (919)834-4984 Page 1 of 1 CENTRAL FILES Report Date: 07/21 /2016 OWR SECTION Date Received: 07/06/2016 V / Lab ID: 92304122001 Collected: 07/05116 23:00 Matrix: Water Results Units Report Limit Analyzed Qualifiers 7.7 mg/L 3.3 0710711616:00 6.4 Std. Units 0.10 07/08/16 10:15 H1,H6 56.0 mglL 25.0 07/08/1616:18 0.18 mg1L 0.010 0712111611:42 2.1 mg1L 1.0 07/16/16 02:27 23.0 mg1L 10.0 07/08/1614:50 H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. � Reviewed by: \—A'XX; Terri Page terri,page@pacelabs.com Asheville Certification lDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginialVELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 Page 1 of 10 DOCtrment Name.. Sample Condition 11 a n Re aCe,4rfalyfrCal Document No.: . F-RAL-CS-001-Rev,o ' o Client Name: C �]Yla �V1�11�,1ti`� Project Courier: Fed Ex ❑UPS ❑U;PS J Cpent Cl Commercial HPace ❑Other: Custody Seal Present? []Yes ONo Seals Intact? ❑Yes 6, Document Revised: May 24, 2016 Paige 1 of 2 Issuing Authority: Pace Raleigh Quality Off €ce Packing Material: ❑Bubble Wrap ❑Bubble Bags ,None ❑Other: Date/mItlals Person Examinln8 Conten4AL"u Thermometer: T1$05 Type_I tee;., Wet ❑Blue ❑None []Samples on ice, cooling process has begun Correction Factor: 0.0'C Cooler Temp Corrected ('C): C biological Tissue frozen? ❑Yes [:]No ON/A Temp should be aboveleezing to VC USDA Regulated So€E (,V J N/A, water sample) Did samp! originate in a quarantine zone within the United States; CA, NY, or5C (check maps)? Did samples originate from a foreign source €inte�rrr��tionally, ❑Yes It Iadudlna Hawall and Puerto Rlcol? r71Yes qw Comments/Discrepancy.- Chain of Custody Present? ^^ Yes QNo, N/A 1. J Samples Arrived within Hold Time? Yes QNa ONIA 2. Short Hold Time Analysts e72 hr.)? Yes UZ. QNjA 3. Rush Turn Around Time Requested? ❑Yes Na NIA A. Sufficient Volume? es No NIA 5, Correct Containers Used? Yes []No ❑NIA 6. -Pace Containers Used? No N A Containers Intact? Jos s No NIA 7. Samples Field Filtered? Des ONO EdNIA 8. Note H sediment Is visible In the dissolved container Sample Labels MatchCOC? Yes []NO ❑NIA 9. -Includes Date/71me ID/Anal sls Matrix: All containers needing acid/base preservation have been 10. Hr,ePita Checked? . (Yes []No ❑N/A All containers needing preservation a re found to be In r "OPH^ compliance with EPA fecommendation? / H"pe.: (HNDs, HAN HCt<2, NaOH >9 Sulfide, NaOH>12 Cyanide) rp—fives ❑No ❑NIA r,.Q,vwr= Exceptions: VOA, Coliform, TOC, Oil and Grease, OR2/8015 (water) DOC,LLHg es No LNIA _ Samples checked for dechlorinatlon? Yes ❑No N A 11. _ _v Heads ace In VOA Vials (>5-6mm)? QYes UNo A 12. Trip Blank Present? ❑Yes QNo /A U. Trip Blank Custody Seals Present? ❑Yes ❑No VN/A Pace Trip Blank Lot H (if purchasedl: CLIENT NOTiFiCATioN/REsoLuTTON Person Contacted: comments/Sample Discrepancy: Project Manager SCURF Review; Date/time: Date: Project Manager SRF Reviewl _ Date: Note. Whenever there is ad iv-repancy affecting north Carolina 6ompliance samples, a copy of this farm veil be sent to Out of hold, Incorrect preservative, out of temp, Incorrect containers) , Field Data Required? OYes []NO th Carolina DEHNR Certification Office (Le. Page 2 of 10 0 CHAIN -OF -CUSTODY 1 Analytical Request Document o -- -• The Chain -of -Custody is a LEGAL DOCUMENT. Al relevant fields must be completed euurately. ca acflon A section a section C :ogalred Alan: MortnaHen: Roqulrod "Ov[ Womulloo: tnvatao wonnatlon: anoinr: a7CCosoara Marna c..iF d m;tl RoPo t To' 4:/ G l? Anont,on: y .. 74c d 6.0 Adf, , 3b;_y r~ f. ccor Te canoim NJ" .4 - M // .. a ✓rlie � Addle=:3 6 Z,S' Gr f /1 r faf^ . t Pacras Order /: Pava paola r71a7 d 4wne: ! •� Fax P' P•C•ed Na-e, Oetentien Paid Pete PC tact Mafarref: b,'n QibSo 4%o=1ass cOn, 7 Sttrte r l.bEMn'. •, :eguos:ad Due hate: i.Mpct it Pave Prom w.. ux•fi, Wce 3 9 COILECTEO Z Preservatives } o-... wr. va• • Fi V 3 V �' 2 �Yrr x riasl VJlR '.YN K W t�v SAMPLE ID Ong w �r.+aw .--"- a 5rART END og n vt 5 ([l'' jj/ �/] Z ClrK�cLar por Loi. n' W- a z 4 ` %' '1 ` v .W � �' e�� ..•yy91di feEISS be V=S�Q7D� W Snug sS +[ ul W $ 1 sz fE y g a g o z P a N K K n u i o c= E 2S SUMMON AOpR10NOS.QpYtYE,rQ[! �'-r.' 'Rfa,JTlq[iSHEDeYf OA7f;, . �': hCC�£P,1F318V!},RF4tA.T1aN ='uKS.YME .>31PmL'srcCffpH6 NT Halve PL'cR� e $ a d z3t r'r.0 in�.� A 0 I N V O � Gi V G1 N+ A 41 N V v b 6P4U-225 mL Plastic Unp RMU-250'm1 Plastic Unp v BPM-500 mL Plastic Unp SPIU-1 liter Plastic Unp i� SP35-250 mL Plastic H2SO4 a 7 MN-2S0 mL plaStit HNO3 BP3Z-250 mL PleStic ZN Aceta[B m BP3C-250 mL Plastt N20H 5 C 9 WGFU-wlde-mouthed Glass jar Unp ^m AGiU-1 liter Amber Unp m e ,ter AM-1 Mar Amber F40 m 3 AG3U-25DmL Amber Unp , ie H AGiSt ftr Amber H2504 AG35-250mLAmber H2504 a p C '1 AG-AA(DG3A)-250 mL Amber NH4a CDG9H tI 40 mLVOA Hcl a � to VGST-40 mL VOA Na2S203 VG%U 40mLVOAUnp S y c. 'a DG9P40 rnL VDA H3PO3 7 N ro VOAK 16 vials per kit}-503S kit VIGK (3 +dais per klt)-V PHJGas kit SPST-125 mLSter'dee Plastic i a 3PZT-2$0 mLStcrilePlastic SP3A-2W mL Plastic (NH2)2504 Cubitainer VSGU-20 mt Selntillation vials 6 a GN H f..' ENCO Laboratories Accurate. Timely. .responsive. Innovative. 4810 Executive Park Court, Suite 111 Jacksonville FL, 32216-6069 Phone; 904.296.3007 FAX: 904.296.6210 Friday, July 15, 2016 Pace Analytical (PA007) Attn: Terri Page 205 East Meadow Rd Eden, NC 27288 RE: Laboratory Results for Project Number: Detention Pond, Project Name/Desc: 92304122 ENCO Workorder(s): BZ03155 Dear Terri Page, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, July 8, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained In this report are In compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chris Tompkins Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full, Page 1 of 7 Page 5of10 www.encolabs.com SAMPLE SUMMARY/ LABORATORY CHRONICLE Client ID: Al-A7 Lab ID: BZ03155-01 Sampled: 07/05/16 23:00 Received: 07/09/16 11:00 Parameter Hold DatelTimefsl Prep DatelTlmefsl Analysis DaIg/liEnr(s) EPA 1664E 08/02/16 07/12/16 10:18 07/12/16 13:47 FINAL This report relates only to the sample as reeelved by the laboratory, and may only be reproduced in full. Page 2 of 7 Page 6 of 10 www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: AI-A7 Lab ID: BZ031SS-01 Analvte Results fun APE. E.QL 9= MethQd Notes Oil & GreaSe (HEM) 0.844 3 0.633 1.32 mg/L EPA 1664B FINAL 3h15 report relates only to the sample as received by the laboratory, and may only be reproduced kn full. Pape 3 of 7 Page 7 of 10 www.encolabs.com ANALYTICAL RESULTS Description: Al-A7 Lab Sample 10,. BZ03155-01 Received: 07/08/16 11:00 Matrix: Water Sampled:07105/16 23:00 Work Order: 8Z03155 Project: 92304122 Sampled By: Classical Chemistry Parameters ^- D%CV lvkson vii oiMfiedaW61e(AC 442] Analvte OCAS Numher] Re ul Flag nits PFF MDL POL Batch Method Ani Py Note Oil & Grease (HEM) [C-0007]^ 0.844 3 1 0.264 0.633 1.32 6G12004 EPA 16546 07/12/16 13:47 SMA FINAL This report relates only to the sample as received b7 the laboratory, and may, onty be reproduced in full. Page 4 of 7 Page 8 of 10 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 5GI2004 - EPA 16645 Blank (602004-111-1(1) Prepared: w/12J2016 10:18 Analyzed: 07/12/2016 13:47 Spike Source %REC RPD Anal Re5ult Elaa P— L Units Level Resul[ %REC Limits RPD Limit Notes Oil & Grease (HEM) 0.615 U 1.28 mg/L LCS (6G12004-BSI) Prepared: 07/12/2016 10:18 Analyzed: 07/12/2016 13:47 Spike Source a/uREC RPD Analyze Resin Elag P91 Sinks Level gesyR %REC Limits RPD Limit Notes Od & Grease (HEM) 148 5,00 mg/L 149 99 78-114 LCS Dup (6G12004-BSD1) Prepared: 07/12/2016 10:18 Analyzed: 07/12/2016 2:47 Spike Source a/oREC RPD Analldg Re"It Flag P-1 Slnits level Result %REC Limits RPD . Limit Notes Oil & Grease (HEM) 142 5.00 mg/L 151 94 78-114 4 Matrix Spike (6G12004-MS1) Prepared: 07/12/2016 10:18 Analyzed: 07/12/2016 13:47 Source: BZ02855-01 Spike Source %REC RPD Analyt Result Flu NX units Level Result a/aREC Limits, RPD mil; Notes Oil & Grease (HEM) 154 5.00 mg/L 147 9.40 98 78-114 FINAL This report relates only to the sample as rmeNed by the Laboratory, and may only be reproduced in full. Page 5 of 7 Page 9 of 10 axe www.encolabs.com FLAGS/NOTES AND DEFINITIONS e The analyte was detected in the associated method blank. b The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MOL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted far actual sample preparation data and moisture content, where applicable. E The concentration Indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantltation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, diluton factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration Is reported. FINAL Ttds report relates only to the sample as received by the laboratory, and may only bereproduced In full. Page 6 of 7 Page 10 of 10 aceAnalytical wwwpacarabs.com Laboratory Report Lorenzo Falls Goldsboro Milling Company PO Box 10009 Goldsboro, NC 27532 Project: DETENTION POND Pace Project No.:92304120 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 1 Report Date: 07/21 /2016 Date Received: 07/06/2016 Sample: B1-B7 Method Parameters Lab ID: 92304120001 Collected: 07/05/16 23:00 Matrix: Water Results Units Report Limit Analyzed Qualifiers SM 2540D Total Suspended Solids 150 mg1L 16.1 07/07/16 15:59 EPA9040 pH 6.7 Std. Units 0.10 0710811610:15 H1,H6 SM 2540B Total Solids 544 mg1L 25.0 07/08/16 16:17 EPA 350.1 Nitrogen, Ammonia 6.5 mg/L 0.050 07/21/16 11:40 SM 4500-CI-E Chloride 33.5 mg1L 1.0 07/16/16 02:24 M1 SM 5220D Chemical Oxygen Demand 38.0 mg/L 10.0 07/08/16 14:50 ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Reviewed by: \_� Terri Page terri.page@pacelabs.com Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A. Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginialVELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia[VELAP Certification #: 460025 Page 1 of 4 Uacument Name:. Document Revised: May24, 2015 CBAnalyfrCal ` Sample Condition Upon Rece1 t(SCUR Pa e 1 of 2 r Document No.: Issuing Authority: F-RAIL-CS•001-Rev.04 Pace Raleigh Qualit Office : Pago 2 of 2 for iinntteernal Use ONLY � Client Name. {�� } Q9 (� 12�if f ` r nl - praJe� W�iR • .JL �ii4 Uh 1 f Courier: []fed Ex UPS USPS Client ❑ Commercial (Pace ❑Other.1 l92304120 '' ' Custody Sea) Present? ❑Yes VNo Seals intact? []Yes ZNa Rate/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap []Bubble Bags (Non ❑Other:_ Thermometer. T1505 Type of I - Wat ❑slue []None (ISamples on ke, cooling process has begun Correction Factor: D.01C Cooler Temp Corrected (•C): Biological Tissue Frozen? ❑Yes ❑No ON/A Temp should be above freezing to 6'C - USDA Regulated Solt( 0 N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check: maps)? Rid samples originate from a foreign source (interpationally, ; ©iJ �Yes No Inrl,idine Hawallnnd puartn AIrnl) r-IYAt f'71N Comments piscre nc : Chain of Custody Present? _ byes []No j3N/A 1. Samples Arrived within Hold Time? &6Yes QNo QyLA .2. _ _Short Hold Time Analysts (<72 hr.)? _ Yes Olslo ©N/A 3. Rush Tum Around Time Re uested7 QYes 4No OyLA 4. Sufficient Volume? Yes No N A S. Correct Containers Used? Yes ©No EIN/A 6. -Pace Contalners Used? A. No N/A Containers Intact? Yes ©No QN/A 7. Sam ples Field Filtered? w QYes ❑No &fNIA 8. Note ifsedlmentisvlslbieinthe dissolved container Sample labels MatchCOC? Yes ❑No ©N/A 9, -includes Date ime/lD/Ana! sls Matrix: All containers needing acid/base preservation have been 10, wcjp,,, checked? . Q Yes [3No ON/A All containers needing preservation are found to be in ( "P'"°r compliance with EPA recommendation? HUN ai« (HNO3, HrSA,. HCI<2, NaOH >9 SvItide, NaOH>12 Cyanlde) Yes []No ©NIA r.arsn.0 Exceptions: VOA, Gollform, TOC, oil and Grease, Zy'es DRO/9015 (water) DOC,LL E]No ONIA 5amYtes checked for dechlorinatlon? Vfyes No ©N/A II, HeadspaceinVDAVlais >5-6mm? dyes ❑No &A 12. Trip Blank Present? Ayes []NO ANIA 13. Trip Blank Custody Seals Present? ©Yes ❑No IAN/A Pace Trip Blank Lot d (if purchased); CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Project Manager SCURF Review. Project Manager SRF Review., _�1 _./ Note: Whenever there Is a discrepancy affecting North Carolina Compllance Out of hold, Incar(act preservative, out of temp, incorrect containers) Fluid Rats Required? ❑Yes ❑No Date/Time: Data: _ _d —i [ r, Date: a copy of this form win be sent to the North Carolina OEHNR Certification Office (Le. Page 2 of 4 CHA[NOF-CUSTODY 1 Analytical Request Document the Chaln.of-Custody Is a LEGAL DOCUMENT. All relevant fields must be completed aeearatL-ly. i cdm A Seaton 6 Swedan G I iaqui^ed a"'rt Ww° ficm Rle4wirmd PM]MI wwmumm: to lco tnlamsnSew Page: of D :aRgen .. Go;-P 1— rw fA%mq C jFend W'4 Report TV ,a,,,,yr�,r, Attarmen: tN.�nnu•462f - J . r r apy To: COmpotr�' Harty: �e �17 , .t . - cauit t; Pan Q.nm; Y R— W 26 Fes" .? PrgsctN.me CeteralonPMe Paw PrcOdManager, dd aibawa xenWa.am. SlaMlLa6W*n:- !: tecWt.ted 0Date. Pntjea A. Pa¢ Pwbw W. aunt Is FW wad MAMA =E COLLECTED 0t—n WPM Dw 4II Y� yyyyrr rna. wr.. Sty .jj 9g 3 1 � _ � 9 SAMPLE. ID a 5o"e a S �? s ART £NR M p a y cta OmChuarwwbox. yw wa K a r : q 7f ' 9'3U`l " * Sampte MS TrAist ba ankw raw. rs w n 'E tt5p C p 7Q A 'ri DATE TIME GATE THE 67 .I llP.h i '-13• � � G' syil �lP�, � 7 8 '9 -41 42; " .• , AAf7tr7QHe1 COIOIL^!f3 .. WEL'r+p{A» 6 BY) AFFMAT10H o+Ue •,rmF '..: ACcFrrm 6Y 1 AFAuATtaw. ' vAse TtNRE' . 9AllrrLc calxATlOnq ... sl KER %AMEAJtD SMATURE PRINT flurp of SAMPLERz {>On L/ n,+ i/ SZGHA TYRE ar.SAMPLEA: 11A7 N n}•�: i4P Z U a 0 4 H Iters� BP4tY125mLPIaStic Urip A � BPW-250ml. Plastic Unp BPZU-500 ml-Plastic Unp BP1U-1 liter Plastic Unp 0 BMS-250 mL Plastic H2504 a c BP3N-250 mL plastic HUO3 SPU-250 mL Plastic ZN Acetate m i MCr250 mL Plastic NaOH WGN-Wide-mouthed Glass jar Unp + c Y AGIU-1 Mer Amber Unp m C6 v s^ w AG14-1 liter Amber HCI Q I+! AG311-250 mL Amber Unp A Cg AG15.111ter Amber H2SO4 N p s AG35-250 mLAmber H2504 ' i AGM(DG3A}-25p m LAmper NH4d CIP { f DG94440 mL VOA HO 3 � °1 a CL LA VG9?AO mL VOA N32SZ03 VM-40 mLVQA UnP st � t DG9P40 mL VGA H3PO4 VOAK (6 vials per kill-5035 kit 1 V/GK (3 vials per fdt)-YPH/Gas kit 5PST I25 mLStrsile Plastic e 4 „ d 4 SPZT-250 mLWrilePtas6c C BP3A-2 0 mL Plastic (Nk2)2SO4 Cubitolner s x t VSGU-20 mL Sciatinabon vials GN PRE) SEMI-ANNUAL STORMWATER DISCHARGE MO IT0R1WREP,0RT for North Carolina Division of Water Quality General Permit No. NCG060006 Date submitted CERTIFICATE OF COVERAGE NO. NCG06 U 3 E JL FACILITY NAME r—q 11"P+ l /e FeP d /h, / / COUNTY Pr ft PERSON COLLECTING SAMPLES 00,74 d GPh C vQ LABORATORY P4,-e %n9 A,,hr4 I Lab Cert. # . f Part A: Stormwater Benchmarks and Monitoring Results s Rervt) MAR 3 I 2016 SAMPLE COLLECTION YEAR Z ° y CENTRAL FILE FACILITY ACTIVITIES INCLUDE (check all that apply): DWR SECTION 5 ❑ use/process meats Buse animal fats/byproducts N DISCHARGING TO SALTWATERS? ❑YES RNO PLEASE REMEMBER TO SIGN ON THE REVERSE -) Total event rainfall 2 Z •- f' or ❑ No discharge this period3 Outfall No. Sample Collected, mo/dd/yr . TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 mi Enterococci , Colonies per 100 mi Benchmark - 100 or 50 Within 6.0 — 9.0 120 30 1000, '4 S00 1 / 3 .Z 2 / j 1 Ur -2 .2 ��4 ZZ Z /1- 9S'- 7 LZ / Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at pM outfalls. You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than SS gallons of new motor oil per month? ❑ yes Eno Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfali No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies, (if yes, complete Part B) SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FORTH E SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART It SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one_copy of this DMR> including all "No Discharge" retsorts, within_30 days of receipt of the lab results (ar at end of monitories period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed'to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) / D /94 ,- /e- (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web%_wq/ws/suLrnpdesswntab-4 S WU-249 Last Revised: October 18, 2012 �2of2 i STORMWATER DISCHARGE MONITORING REPORT RECEIVED for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG0600 Date submitted Z / / ?` / 9 CERTIFICATE OF CO�XjERAGE NO. NCGO6 Q 3 6 q FACILITY NAME D &11 tA0' 64 / 1— ZZI;P11/P fPPd._1111 COUNTY Pi f PERSON COLLEP ING SAMPLES Doi Cy LABORATORYr►-?4MAf4/ 4PtrlfLab Cert. # Part A: Stormwater Benchmarks and Monitoring Results FEB 2 6 2019 CENTRAL FILES SAMPLE COLLECTION YEAR DWR SECTION SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ?R Monthlys FP6 t,,ar y (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA [:]Zero -flow [:]WaterSupply [—.]SA ®other ,0i Ar.4 FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats Muse animal fats/byproducts PLEASE REMEMBER TO SIGN 'ON THE REVERSE 4 Total event rainfall z _T/� or n No discharge this period' Outfall No. STORMWATER DISCHARGE MONITORING REPORT RECEIVED for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG0600 Date submitted Z / / ?` / 9 CERTIFICATE OF CO�XjERAGE NO. NCGO6 Q 3 6 q FACILITY NAME D &11 tA0' 64 / 1— ZZI;P11/P fPPd._1111 COUNTY Pi f PERSON COLLEP ING SAMPLES Doi Cy LABORATORYr►-?4MAf4/ 4PtrlfLab Cert. # Part A: Stormwater Benchmarks and Monitoring Results FEB 2 6 2019 CENTRAL FILES SAMPLE COLLECTION YEAR DWR SECTION SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ?R Monthlys FP6 t,,ar y (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA [:]Zero -flow [:]WaterSupply [—.]SA ®other ,0i Ar.4 FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats Muse animal fats/byproducts PLEASE REMEMBER TO SIGN 'ON THE REVERSE 4 Total event rainfall z _T/� or n No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L oil and Grease, mg/L Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark - 100 or 50' Within 6.0 — 9.0 120 30 10001 Soo, Parameter Cade - C0530 00400 00340 00556 31616 61211 I! z a/ . 7,f 33 < -s- 1 Only appliesto facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes Egno Km complete Part B) Permit Date: 11/1/2018-05/31/2021 SWU-Z49, Last Revised 11/5/2018 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Date Sample Collected [mo/dd/yr} 24-hour rainfall amount, inches z New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or SO mg/O Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR including all "No Discharge" reports _within 30 days of receipt of the lab results far at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of.fines and imprisonment for knowing violations." Signature of Permittee r Permit Date:11/1/2018-05/31/2021 Z / AteL ea / y Date SWU-249, Last Revised 11/5/2018 Page 2 of 2 A "M enirochem .. s i ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 gowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax t 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Butterbail-Farmville Date of Report: Feb 21, 2019 3628 South Fields St. Customer PO #: Farmville NC 27828 Customer ID: 17080036 Attention: Don Genova Report #: 2019-02369 Project ID: Storm Water Lab lD Sample ID: Collect Date/Time Matrix Sampled by 19-06020 Site: outfali 2 2/11/2019 5:00 PM Water Don Genova Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 Residue Suspended (TSS) SM 2540 0 pH SM 4500 H B <5 mg/L 02/14/2019 7.2 mg/L 02/13/2019 6.78 units 02/13/2019 COD SM 5n0D 33 mg/L 02/14/2019 Comment: n Reviewed by: _Rau,�1 Report C 2019-02369 Page 1 of 1 "44C NAIL. ;i�tivl.}T�OGherij ENVIRONMENTAL CHEMISTS, INC NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 lnlo@environmentatchemists.com Client: B utterball- Farm vil le PROJECT NAME: Storm Water &,y A4/l 0.2 REPORT NO: ADDRESS: 3628 South Fields Street CONTACT NAME: D' rj0no4-q PO NO: Farmville, NC 27828 REPORT TO: Don Genova PHONE/FAX:919.252.1326 COPY TO: email: dgenova@butterball.com Sampled By: agn go.-i-P-A SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection a N a �+ & E c3 ti ct7 B `oa. � " o G .2 E' " OW a g J PRESERVATION ANALYSIS REOIiESTED Date Time Temp ? _ 3 2 = a z a W o 1) C P X X TSS, COD, pH, Oil and Grease G G C P G G 2 C P X X TSS, COD, pH, Oil and Grease G G n C Xi G � ,/ Fr°,6 ,9 Pry �.� C P G ea G i .r r C P � a G C P G G C P G G Transfer Relinquished By: Daterrime R ived By: Date�me 1. !�° PAW /;9111A,!p � � 1- 2. Temperature when Received: Tj [1 Accepted: Delivered By: Received By: Comments: TURNAROUND: STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000 Date submitted 7 A-10i ZO 114 CERTIFICATE OF COVERAGE NO. NCG06 0 3 S"41 SAMPLE COLLECTION YEAR Z 01 4 FACILITY NAME 914tVV- AP COUNTY p� �'T SAMPLE PERIOD ❑ lan-June ❑July -Dec PERSON COLLECTING SAMPLES DO,, �for� or ®Mnnthlys lT r7 �' nonth) 11 LABORATORY,^^,,, 44/ /'ii/�ilfr Lab Cert. # DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA C ❑Zero -flow [:]watersupply ❑SA REC,F"P—D ®Other pits/ FEB 18 w01g FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ® use animal fats/byproducts CEN i f-,LES DWR SECTION Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall' / or ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark 100 or 504 Within 6.0 — 9.0 120 30 10001 5001 Parameter Code C0530 00400 00340 00556 31616 61211 1 Ta l S• 'f C s ii/ 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes D?Ino (if yes, complete Part B) Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Qutfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L° Parameter Code - 46529 NCOIL 00S52 C0530 Footnotes from Part A also apply to Part B *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B, • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO X IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR, including all -"No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: - Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment For knowing violations." Signature of Permittee Date Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 2 of 2 Butterball-Farmville 3628 South Fields St. Farmviile NC Attention: Dan Genova Lab ID Sample ID: 19-02132 Site: outfall 2 Environmental Chemists, Inc, 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info a environmentalchemists.coni Date of Report: Jan 24, 2019 Customer PO M 27828 Customer ID: 17080036 Report M 2019-00851 Project ID: Storm Water Collect DatelTime Matrix Sampled by 1/13/2019 11:00 PM Water Don Genova Test Method Results Date Analyzed Oil & Grease (O&G) EPA 18sa <5 mg/L 01/15/2019 Residue Suspended (TSS) SM 2540 D 5.4 mg/L 01/16/2019 pH SM 4500 H 8 6.61 units 01/17/2019 COD SM 5220D <20 mg/L 01/18/2019 Comment: Reviewed by: ._ C� Report#:: 20ts-0oa51 Page 1 of 1 Way ENVIRONMENTAL CHEMISTS, INC OOFFFIC in910-3 2-0223iFAX 910-392-4424$ 0=0 info®en�ironmentalchemists.com Analytical & Consufting Chemists NCpENR: DWO CERTIFICATION # 94 NCpFiNS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY Client: Butterball-Farmvilie PROJECT NAME: Storm Water i, aru)fAl/ #-2 REPORT NO. ADDRESS: 3628 South Fields Street CONTACT NAME: D41r7 l 14�40&4 PO NO: Farmville, NC 27828 REPORT TO: Don Genova PHONE/FAX:919.252.1326 COPY TO: email: dgenova@butterball.com Sampled By: !/ SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection 1 a E n" m a $ o o .. 5 c v a m o f r E o w m"' -5 2. z PRESERVATION ANALYSIS REQUESTED Date Time Temp U c z , i 9 °A n = x i o W iz o 1) C P X X TSS, COD, pH, Oil and Grease G G C P G G 2 C P X X I I ITSS, COD, pH, Oil and Grease G G 1/ /� - f r' C �32 PH Z19p 9 �EE G1 J 12JA', /) "I S T C P X 7-AP 20/9 G n L� 3 /3J4e S T C P z- Za/9 G C P � C ,L7 G C P G G C P G G Transfer Relinquished By: Date/Tlme Received By: PateMme 2. Temperature when Received: Accepted: Delivered By: Received By: Comments: 5 Time: IS4-__�_. litRTiT_rLS1T1M STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000 Date submitted 7 T,4 n z e/ 9 CERTIFICATE OF COVERAGE NO. NCG06 0 3 6 4 FACILITY NAME _ Bk ) #14C ~ rA�M v► II P �!!O /% COUNTY AI '/ f PERSON COLLECTING SAMPLES Dan_ ge i �a LABORATORY 64g1*,jr Lab Cert. # T SAMPLE COLLECTION YEAR Z & /(? SAMPLE PERIOD ❑ Jan -June July -Dec or ❑ Monthlys (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA RECEDED Other DI tcA JA �F�CILu t ACTIVITIES INCLUDE (check all that apply); ❑ use/process meats Ouse animal fats/byproducts CEMTRAL FILES E)WR S-E-CTION PLEASE REMEMBER TO SIGN ON:THE REVERSE --) Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall' / !12 "or ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units GOD, mg/L Oil and Grease, mg/L Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark 100 or 50' Within 6.0 — 9.0 120 30 10001 500` Parameter Code - C0530 00400 00340 00556 31616 61211 I► Jr 7 q C S, .� cs Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You mast still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes Yno (Ifyes, complete Part B) Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches New Motor Oil or Hydraulic Oil Usage Non -Polar 0&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original cooK ot this DMR including all "No Discharge" reports, within 30 days of recer t of the lab results or at end of manitorin period -in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permi"ee Permit Date: 11/112018-05/31/2021 Date 7Q„ 2 01 t SWU-249, Last Revised 11/5/2018 Page 2 of 2 Environmental Chemists, Inc. ANALYTICAL & CONSULTING CHEMISTS 6602 Windmill Way, Wilmington, NC 28405 . 910,392,0223 Lab . 910.392.4424 Fax 710 Bowsertown I Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5943 Lab/Fax info@environmentalchemists.com Butterball-Farmville Date of Report: Dec 29, 2018 3628 South Fields St. Customer PO #: Farmville NC 27828 Customer ID: 17080036 Attention: Report #: 2018-20780 Project ID: Storm Water Lab lD Sample 1D: A Collect Date/Time Matrix Sampled by 18-52363 Site: outfall 1 12/14/2018 7:00 PM Water client Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 12/1812018 Residue Suspended (TSS) SM 2540 D 14 8 mglL 12/1812018 pH SM 4500 H B 6.95 units 12/20/2018 COD SM 5220D 74 mg1L 12/24/2018 Lab ID Sample ID: a Collect DatelTime Matrix Sampled by 18-52364 Site: outfall 2 12/14/2018 7:00 PM Water client Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 12/1812018 Residue Suspended (TSS) SM 2540 D 128 mg/L 12/18/2018 pH SM4500 H B 6.77 units 12/20/2018 COD SM 52200 100 mg/L 12/24/2018 Comment: Reviewed by f CA Report :: 018-24780 61112 ndmill Way ion ENVIRONMENTAL CHEMISTS INC OFFICE: 91G-392 2 3'IFAX9910- 224 i+ `v ` info@environmentalchemists.com Analytical & Consulting Chemists NCDENR: DWG CERTIFICATION # 94 NCDHiiS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY Client: Butterball-Farmville PROJECT NAME: Storm Water D+, f� II# % REPORT NO: �� 2�7 U ADDRESS: 3628 South Fields Street CONTACT NAME: 0a i 910n e z-q PO NO: Farmville, NC 27828 REPORT TO: Don Genova PHONE/FAX:919.252.1326 COPY TO: email: dgenova@butterball.com Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection I-' d W 9 o Q a 5 U Cl .. - m S c a c� o �, u E a Am m a z PRESERVATION ANALYSIS REQUESTED Date Time Temp¢u � z -, z r z , o 1) C P X X TSS, COD, pH, Oil and Grease G G C P G G 2) C P X X I ITSS, COD, pH, Oil and Grease G G � NDec 7 P� s-r. c P A Ft G A/ c 7 P S 7- C P G / `f' % G A Iy.Djc 7f" �,7- C P z C Ia G C P G G C P G G Transfer Relinquished By: Date/Tirne Re ived By: DatefTime 2. Temperature when Received: Accepted: Delivered By: R LTime: ,s_ 6602 Windmill Way on, NC `l ENVIRONMENTAL CHEMISTS, INC OFFICE: 9 03 2 2 3`IFAX9t10392-44245 -e + e'a� NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentatchomists.corn Analyfical & Consulting Chemists COLLECTION AND CHAIN OF CUSTODY Client: Butterball-Farmville PROJECT NAME: Storm Water (Oyf%q /j REPORT NO: (� ADDRESS: 3628 South Fields Street CONTACT NAME: ,9aq Giollw-i PO NO: Farmville, NC 27828 REPORT TO: Don Genova PHONEIFAX:919.252.1326 COPY TO: email: dgenova@butterball.com Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection C; F �n ID o a s '� a «° o "v �� o rn n e a CW m '' z PRESERVATION ANALYSIS REQUESTED Date Time Temp m z _, U x o N S x x z o r w T o 1) C P X X TSS, COD, pH, Oil and Grease G G C P G G 2) C P X1 I X I I TSS, COD, pH, Oil and Grease G G y o A117 sr G 7-s r G C P 1` nl�c 7 J" S 7` C P ca.0 G C P I G G C P G G Transfer Relinquished By: Daterrime Received By: Date/Time 2. Temperature when Received: ,G, I Accepted Delivered 8y: Received Comments: Time: tt-2' :S -ow .-"% �.1 Central Files: APS _ SWP _ 9/24/2015 r Permit Number NCG060364 Program Category NPDES SW Permit Type Food/Tobacco/Soaps/Cosmetics/Public Warehousing Stormwater Discharge COC Primary Reviewer rick.riddle Coastal SWRule Permitted Flow Facility Permit Tracking Slip Status Project Type In draft New Project Version Perm it C lass if [cation COC Permit Contact Affiliation DIVED SEP 3 0 2013 CENTRAL FILES DWR SECTION Facility Name MajorlMinor Region Goldsboro Milling Company Farmville Feed Mill Minor Washington Location Address County 3648 S Fields St Pitt Facility Contact Affiliation Farmville NC 27828 James Jacobs 3648 S Fields St Owner Farmville NC 27828 Owner Name Owner Type Goldsboro Milling Company Non -Government Owner Affiliation James Jacobs 3648 S Fields St Dates/Events Farmville NC 27828 Scheduled Orig Issue App Received Draft Initiated Issuance Public Notice Issue Effective Expiration 7/23/2015 9/17/2015 Regulated Activities Requested /Received Events RO staff report requested 7/27115 r RO staff report received 9/24/15 Outfall 1 Waterbody Name Streamindex Number Current Class Subbasin Middle Swamp 27-86-26-5 C;Sw,NSW 03-04-07 North Carolina Department of Environmental Quality Pat McCrory Governor James Jacobs Goldsboro Milling Company P.O. Box 1009 Goldsboro, NC 27532 Dear Mr. Jacobs: Donald R. van der Vaart Secretary September 24, 2015 Subject: General Permit No. NCG060000 Goldsboro Milling Company Fartnville Feed Mill COC NCG060364 Pitt County In accordance with your application for a discharge permit received on July 23, 2015, we are forwarding herewith the subject certificate of coverage to discharge under the subject state —NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated October 15, 2007 (or as subsequently amended). Please take notice that this certificate of coverage is not transferable except after notice to the Division of Energy, Mineral, and Land Resources, The Division may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Energy, Mining, and Land Resources, or permits required by the Division of Water Resources; Coastal Area Management Act, or any other federal or local governmental permit that may be required. If you have any questions concerning this permit, please contact Richard Riddle at telephone number (919) 807-6375. Sincerely; 4"�' ��e. for Tracy E. Davis, P.E., CPM, Director Division of Energy, Mineral and Land Resources cc: Washington Regional Office Central Files Stormwater Permitting Program File Division of Energy, Mineral and Land Resources Energy Section • Geological Survey Section • Land Quality Section 1612 Mail Service Center, Raleigh, North Carolina 27699-1612 • Telephone 919-707-9200 / FAX: 919-715-8801 S12 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http://portal,ncdenr.org/web/Ir/ An Equal Opportunity\ Affirmative Action Employer— 50% Recycled \ 10% Post Consumer Paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES GENERAL PERMIT NO. NCG060000 CERTIFICATE OF COVERAGE No. NCG060364 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Goldsboro Milling Company is hereby authorized to discharge stormwater from a facility located at Goldsboro Milling Company Farmville Feed Mill 3648 South Fields Street Farmville Pitt to receiving waters designated as Middle Swamp, a class C, Sw, NSW water in the Neuse River Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, 11, 1II, and IV of General Permit No. NCG060000 as attached. This certificate of coverage shall become effective September 24, 2015. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day September 24, 2015. for Tracy E. Davis, P.E., Director Division of Energy, Mineral, and Land Resources By the Authority of the Environmental Management Commission _ r1am^' .1 •� '��� � NO, 4B � C ft$ f _ ;Airpon �t 1 f ♦ • r7 p 77035'53" u ik � • f �4 r -� L NCG060364 N W E S Map scale 1: 24, 000 • Y�6 GoNZ �440 Farmille Feed Mill x�. 1?sfil •• 45; all SMar�boro 8M, 23. F-1 i A _ Goldsboro Milling Company Farmville Feed Mill Latitude: 350 35' 35" N Longitude: -770 35' 53" W County: Pitt Receiving Stream: Middle Swamp Stream Class: C; Sw; NSW Index Number: 27-86-26-5 (Neuse) Facility Location P ARFAIIA Division of Energy, Mineral and Land Resources Land Quality Section National Pollutant Discharge Elimination System NCDENR NCG060000 i+++nreo mN —D Note RESCRjRCcp NOTICE OF INTENT FOR AGENCY USE ONLY Date Received Year Month Dav Certificate ofCovera e eck # unt Permit Assi ed to td National Pollutant Discharge Elimination System application for coverage under General Permit NCG060000: STORMWATER DISCHARGES associated with activities classified as: SIC (Standard Industrial Classification) 20 Food and Kindred Products SIC 21 Tobacco Products SIC 283 Drugs SIC 284 Soaps, Detergents, & Cleaning Preparations; Perfumes, Cosmetics, & Other Toilet Preparations SIC 422 Public Warehousing and Storage (except 4226) For questions, please contact the DEMLR Regional Office for your area. See page 4. Do Not use this NOl for renewals. (Please print or type) 1) Mailing address of owner/operator address to which all permit correspondence will be mailed): Name Goldsboro Milling Company Street Address PO Box 1009 City Goldsboro, NC 27532 Telephone No. 919-778-3130 2) Location of facility producing discharge: Facility Name Goldsboro Milling Company Farmville Feed Mill Facility Contact Mr. James Jacobs Facility Address 3648 South Fields Street Facility City Farmville, NC 27828 Facility County Pitt Telephone No. Pending_ Fax: Pending Email james.jacobs@goldsboromilling.com 3) Physical Location Information: RED'F1IVCD J11L 23 2015 DENrq_ S70jRMUv r R i'QUALI t p� vG Please provide a narrative description of how to get to the facility (use street names, state road numbers, and distance and direction from a roadway intersection). The site is located at the intersection of South Fields Street and Wallace Street in Farmville, NC (A copy of a county map or USGS quad sheet with the facility clearly located must be submitted with this application.) 4) Latitude 35' 35' 35" N Longitude -77' 35' 53"W 5) This NPDES Permit Application applies to which of the following: x New or Proposed Facility ❑ Existing Date operation is to begin: August 2015 �F. 5-9 3 3 03 SWU-221 r 7. 7, 5 9 `1 733 Page 1 of 4 Last revised 6/24114 NCG060000 N.O.I. 6) Standard Industrial Classification: Provide the 4-digit Standard Industrial Classification code (SIC code) that describes the primary industrial activity at this facility. SIC code: 2048 7) Activities a) Provide a brief narrative description of the types of industrial activities and products manufactured at this facility: grain storage and preparing feed for livestock. b) Check all activities occurring at this facility: None of the activities listed below ❑ use or process meats ❑ use or process animal fats/byproducts 8) Discharge points 1 Receiving waters: How many discharge points (ditches, pipes, channels, etc.) convey stormwater from the property? Two What is the name of the body or bodies of water (creek, stream, river, lake, etc.) that the facility stormwater discharges end up in? Drainage ditches that flow into an unnamed tributary of Middle Swamp Receiving water classification: C; Sw: NSW Is this a 303(d) listed stream? No Has a TMDL been approved for this watershed? Not Applicable If the site stormwater discharges to a separate storm sewer system, name the operator of the separate storm sewer system (e.g. City of Raleigh municipal storm sewer). Not Applicable 9) Does this facility have any other NPDES permits? X No ❑ Yes If yes, list the permit numbers for all current NPDES permits for this facility: 16) Does this facility have any Non -Discharge permits (ex: recycle permit)? X No ❑ Yes If yes, list the permit numbers for all current Non -Discharge permits for this facility: 11) Does this facility employ any best management practices for stormwater control? ❑ No X Yes (Show any structural BMPs on the site diagram.) If yes, please briefly describe: covered storage areas, secondary containment, gravel surfaces 12) Does this facility have a Stormwater Pollution Prevention Plan? ❑ No ❑ Yes If yes, when was it implemented? Pending 13) Are vehicle maintenance activities occurring at this facility? X No ❑ Yes 14) Hazardous Waste: a) Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility? X No ❑ Yes SWU-221 Page 2 of 4 Last revised W24114 NCG060000 N.O.I. b) Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste generated per month) of hazardous waste? X No ❑ Yes c) Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste generated per month) of hazardous waste? XNo ❑ Yes d) Is hazardous waste stored in the 100-year flood plain? X No ❑ Yes If yes, include information to demonstrate protection from flooding. e) If you answered yes to questions b. or c., please provide the following information: Type(s) of waste: How is material stored: Where is material stored: How many disposal shipments per year_ Name of transport 1 disposal vendor: Vendor address: 15) Certification: North Carolina General Statute 143-215.6B (i) provides that: Any person who knowingly makes any false statement, representation, or certification in any application, record, report, plan, or other document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000). I hereby request coverage under the referenced General Permit. I understand that coverage under this permit will constitute the permit requirements for the discharge(s) and is enforceable in the same manner as an individual permit. I certify that I am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete, and accurate. Printed Name of Person Signing: Carl F. Bonner, PE with Terracon Consultants, Inc. Title: Agent 1 Consulting Engineer for the Owner (Signature of Applicant) July 21, 2015 (Date Signed) This Notice of Intent must be accompanied by a check or money order for $100.00, made payable to: NCDENR. Do not send the check or money order separately. Page 3 of 4 SWU-221 Last revised 6124114 NCG060000 N.O.I. Final Checklist This application will be returned as incomplete unless all of the following items have been included: ❑ Check for $100 made payable to NCDENR. Must be included with this application (not sent separately). ❑ This completed application and all supporting documents. ❑ A site diagram showing, at a minimum, (existing or proposed): (a) outline of drainage areas, (b) stormwater management structures, (c) location of stormwater outfalls corresponding to the drainage areas, (d) runoff conveyance features, (e) areas where materials are stored, loaded, and unloaded, (f) impervious areas, (g) site property lines. ❑ Copy of county map or USGS quad sheet with the location of the facility clearly marked on the map. Mail the entire package to: Stormwater Permitting Unit Program Division of Energy, Mineral and Land Resources 1612 Mail Service Center Raleigh, North Carolina 27699-1612 Note The submission of this document does not guarantee coverage under the General Permit. For questions, please contact the DEMLR Regional Office for your area. DEMLR Regional Office Contact Information: Asheville Office ...... (828) 296-4500 Fayetteville Office ... (910) 433-3300 Mooresville Office ... (704) 663-1699 Raleigh Office ........ (919) 791-4200 Washington Office ...(252) 946-6481 Wilmington Office ... (910) 796-7215 Winston-Salem ...... (336) 771-5000 Central Office ......... (919) 807-6300 Page 4 of 4 SWU-221 Last revised 6124114 UNITED STATES — DEPARTMENT OF THE INTERIOR — GEOLOGICAL SURVEY �ga*tetron } ��• �- �r Y — • • BM �.A • �J 1 �; RM 25.5 25.9 „Crafts rr .. f �, WT •' ` y�i </ - ;;Airport f i 1 f -t � f,. •� � P 0w t �� y I I mo✓ aT artmn SITE AN s, ORFOL �,� u BI 28,2 [] p j ■ ..:. ,,, sour SU99 , jr— St Johrn f ° • i _ _ ,255 yyf '�Marlboro 1 DS go dls Sal --'T l °. � � lJ I � n 'elm 4 \� 7LQ�i•\� SCALE 1:24 000 1 .5 0 Ka OMETERS 1 2 1000 0 METERS low 20M 1 .5 0 1 MILES 1000 0 1000 20M 3000 4000 5m 0000 7000 8000 90DO 10 000 FM N CONTOUR INTERVAL 2 METERS NATIOML GEODETIC VERMAI DATt1M OF 1929 QUADRANGLE FARMVILLE, NC 1981 7.5 MINUTE SERIES (TOPOGRAPHIC) 'INDICATES WHICH MAP SITE IS LOCATED ON "-"r"w. TOPOGRAPHIC VICINITY MAP EXHIBIT CB r>mwrr 72157038 STORM WATER COMPLIANCE SERVICES RLW AS SHOWN caeamaar rxw 0asi'4'°xE FARMVILLE FEED MILL CBIMRF swcrnsrrso-z 3648 SOUTH FIELDS STREET +I App�sd By CB JULY 2015 114 Wn eMe NC FARMVILLE. NC I (2521 U3.1WOeacm 232 i600 252 -0= 1 1 STORMWATER PERMIT WESTERN BOUNDARY RAILROAD 1+' 1 GRAIN BINS ' . ' i t i 1Ile IZL 1 I ! FAT E GRAIN SIN TO BE STORAGE REMOVED I TANKS i U i FEED MILL SOYBEAN OIL - ELEVATED STORAGE U V�: TOWER i TANKS I _ i 1 I L MAINTENANCE SHOP FOR FEED MILL NUTRIENT WAREHOUSE SUpptDAm TANKS a WAREHOUSE & RETAIL + STORE LEASED TO 1 w SOUTHERN STATES 1 i 1 i 1 GRAVEL I i 1 i 1 CONCRETE PAD (FORMER DIESEL 1 FUEL TANK PAD) ; SCALE OFFICE OUTFACE #2 CONCRETE -- -- -- -- -- -- -- -- _ SCALE ONCRET GRAVEL COVERED I BROKEN ASPHALT i � / r r / i r i r i LOADING RAMP GRAVEL DOCK , / r OFFICE , ;�� / �y� 5p GRAVEL COVERED BROKEN ASPHALT LOADING DOCK OUTFALL#1 j DITCH - - '' " N ROCK LINED SWALE ' it LEGEND — — — SITE NOT TO SCALE FTSI TRUCK SCALE cJ TANK IN CONTAINMENT DROP INLET I TWS DAM" 15 FIR GEWt& LOCATION ONLY, NA 6 NOT MENDED FOR OWTRUCTION PI1 OSU WALLACE STREET NOTE: OUTFALL PIPES DISCHARGE INTO THE DITCH /' No w1w p'"""ft 51TE ©IAGRAM CB 72557ljoa Drawer RLw scme. ASSHOWN wN 1 kiramn STORM WATER COMPLIANCE SERVICES cn«xsder. C�MRF FkNo. C •u�ap ; tlr mW�� FARMVILLE FEED MILL swcrz+srme-s AppmvW BY. 3648 SOUTH FIELDS STREET CB JULY 2055 37� �0°� ortye m^serorle taC 2859G FARMVILLE, NC