NCG020865_COMPLETE FILE - HISTORICAL_20140320

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
IV CCU O 96
DOC TYPE
Fl� HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ �q � `i � 3 a t�
YYYYMMDD

AF-IrMA
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Energy, Mineral, and Land Resources
Land Quality Section
Tracy E. Davis, PE, CPM
Director
March 20, 2014
CERTIFIED MAIL 7013 2630 0002 0760 5246
RETURN RECEIPT REQUESTED
Frank R. Morton dba J.J. Morton & Son Construction
3121 New Bern Highway
Jacksonville, NC 28546
Dear Mr. Morton:
Pat McCrory, Governor
John E. Skvarla, III, Secretary
An inspection conducted on March 18, 2014 showed that your facility known as Rocky
Run Road Pit on Rocky Run Road in Jacksonville, NC is operating without a permit for
Elimination System permit for coverage under General Permit NCG020000 for
STORMWATER DISCHARGES associated with activities to discharge stormwater, mine
dewatering wastewater and process wastewater to the surface waters of North Carolina.
More information can be found on the Division's website at:
http://portal.nedenr.org/web/Ir/npdes-stormwater
I have enclosed an application form (Notice of Intent) for your convenience. Should you
have any questions concerning the application form (Notice of Intent), please do not hesitate to
contact me at 910-796-7372. You are required to apply for this permit within 30 days of
receiving this correspondence or a Notice of Violation may be requested. I thank you for
your cooperation with this matter.
Sincere) ,
Karl Hammers
Land Quality Section
Wilmington Regional Office
Encl: NOI
cc: LQS File 67-73
Wilmington Regional Office
127 Cardinal Drive Extension, Wilmington, North Carolina 28405 Phone: [phone] Fax [phone]

Print this form to PDF
Return PDF of this form to DLR CO by email. cc DLR RO and DWQ SPU
MINING PERMIT APPLICATION REVIEW FORM
for the N(40ZD
DIVISION OF WATER QUALITY -PEtJD��
THIS SECTION TO BE FILLED OUT BY DLR:
Project Name: Rocky Run Road Mine DLR Permit #: 67-73 County: Onslow Address: 3121 New Bern
Hwy., Jacksonville, NC 28546
YES NO Date Commencing
Is this mine a new mine? r r
Have land disturbing activities
started? Date? r r
Latitude:34.7630 Longitude:-77.2670
Please return comments to (at DLR CO): Judy Wehner
Comments due by: 815111
SECTION BELOW TO BE FILLED OUT BY DWQ:
Is the RO concerned that the operation, as proposed, would violate standards of water quality? NO
Comments: n
Watershed/Stream Name & Classification: 01� G • NSU-)
�-'� �� wla, �r-,-r,�c-c�.nr�D�.e�
DWQ Compliance Status Crc, �t
o`u'`Mr `�.'a° Yu'`f` _ ' YES NO
NPDES permit required?
7
>l�sa s-�ormwa��.
.I LrrU-;1-_KX
NPDES permit existing?
r (Permit #
If an NPDES permit is not required, is DWQ'Cri
still concerned about wetland degradation
by dewatering?
Should permittee contact DWQ RO
immediately? (e.g. to schedule a site visit if
I— RO Contact Name:
mine has already begun digging or is
Contact Reason:
dewatering without DWQ permit)
401 Wetland Cert. required?
401 Wetland Cert. existing?
r Permit #
r
Does :DWQ RO currently have enough
,information to determine if a 401
L
certification,is required?
1
N
Rev September 2010

Print this form to PDF
Retum PDF of this form to DLR CO by email. cc DLR RO and DWQ SPU
YES NO
Are wetlands disturbed at,this site?
Does DWQ RO suspect or know of nearby
r u�
(--
wetlands to the site?
'Is a wetland delineation required prior to
By: LIJD or r bonsultant
POnsite? r
r
DWQ issuingthe permit?
p
?
Or Offsite .
_��
Stream Determination Needed?
r
i
Stream Determination Completed?
C
Does DWQ RO need a statement that no
SSAQ—
wetlands/streams are disturbed
for this project from applicant?pQ
.Buffer Determination Needed?
Ll
Buffer Determination Completed?
r
Recycle system permit existing?*
CPermit #
New Recycle System permit required?*
r
Enough information to determine?
Non -discharge permit existing?*
CPermit #
CI
Will wastewaters discharge to HQW waters
r
�`/Q10
Unknown (permittee determine): r
with a 7Q10=0? **
Flow:
C Has Violation
'DWQ
rr ' O&M Requirements
Doesrequire DLR to hold the permit
so DWQ it further
HConcerns
C/
(e.g. can review or
rr
r O Otther.her. R Reaa son:
because DWQ requires more -information)?
RO contact:
El Hold Until:
Mine must wait to dewater until an O&M
plan is approved?
*The NPDES SW and WW_permit NCG020000 covers closed -loop recycle systems, designed to exclude all stormwater run-off from
the system and operate at or below two -feet of freeboard. These systems may be permitted by a Non -discharge Recycle System
Permit from the Aquifer Protection Section (APS) OR may instead be permitted under NCG020000 to eliminate an additional permit.
Recvcle systems that do not meet those criteria are considered discharoina systems. and are subiect to the NCG020000 discharoe
permit,
**To obtain 7Q10 Rows, permittees must contact the DWQ Sto►mwater Permitting Unit. If DWQ does not have a flow estimate for a
specific stream, permittees will be asked to obtain one. Permittees should contact J. Curtis Weaver at the USGS: 919-571-4043, for
more information on obtaining a 7Q10 Row. USGS will not determine a 7Q10 flow for tidally influenced waterbodies.
Reviewed bv:
DWQ RO Surface Water: L-' Regional Office: Date-
RO Aquifer Protection Section: Regional Office: Date:
SPU DWQ Central Office Reviewer (if applicable):
Rev September 2010

ROCKY RUN ROAD PIT
ONSLOW COUNTY, NORTH CAROLINA
PROJECT NARRATIVE
Prepared for:
J.J. MORTON & SON CONSTRUCTION
31.21 NEW BERN HWY.
JACKSONVILLE, NC 28546
Prepared by:
PARAMOUNTE
L ]L-
e M (-- I " a F- rR I N G I rj C.
5911. Oleander Drive, Suite 201
Wilmington, NC 28403
Project # 11 142.PE
July 2011
y\ C.
7 -s
�T- -
SEAL
036235
G'HE
Al 2011

ROCKY RUN ROAD PIT
ONSLOW COUNTY, NORTH CAROLINA
Project 411142.PE
Table of Contents
Design Narrative
Maintenance
Erosion and Sedimentation Control Specification
Calculations

ROCKY RUN ROAD PIT
ONSLOW COUNTY, NORTH CAROLINA
Project �17142TE
DESIGN NARRATIVE
J.J. Morton & Son Construction proposes to disturb approximately 28.10 acres off of Rocky Run Road in
Onslow County, North Carolina to excavate a proposed dirt mine. In addition to this NCDENR Mine
Permit, the applicant has also submitted to Onslow County for a Special Use Permit and will also be
applying for two NCDOT driveway permits. There are no federal permits associated with this project.
In addition to the excavation area, the applicant will be reserving a 3.8-acre portion of his property to use
for storing inert wood debris. The inert debris area will be located behind the mine and therefore will not
be visible to the public. This is unrelated to the mine operation, and he will be applying for a Land
Clearing and Inert Debris Landfill permit from the NCDENR Division of Waste Management. .
The 28.10 acres of disturbance shall include two haul roads totaling 1.40 acres, a processing area of 11.30
acres, and an excavation area of 15.20 acres. Both haul roads are existing dirt roads. Both begin at the
state maintained Rocky Run Road (S.R.1413) and lead to the proposed excavation area. The dirt removed
from the excavation area will be taken off site and supplied to various sources of need in the region. The
mine operation will commence between the hours of 7 a.m. and 6 p.m. Monday through Saturday.
The excavation area is located on the northeastern part of Frankie R. Morton's property. The nearest
property line is approximately 219 feet from the excavation area. There are no structures or residences
within sight of the proposed excavation area and the location is also secluded in regard to visibility and
noise. Also note that all runoff from construction activities shall be contained internally within the
excavation area and that no runoff will be leaving the site and draining to adjacent properties.
All necessary dewatering activities will occur within the limits of the mine as illustrated on the design
plans. No runoff from dewatering activities will leave the mine site. It is proposed to store all
groundwater within the excavation area; as a result, the overall excavation area will be divided into three
smaller excavation areas. It is proposed to excavate the proposed area to the groundwater elevation (the
groundwater table has been identified by field inspection at el. 32.0), once the groundwater elevation is
reached, an earthened berm will be constructed to divide the excavation pit starting from the
groundwater elevation to the top of berm (el. 42.00). Once the earthened berm is constructed, the
excavation area will be divided into Excavation Area 21, Excavation Area �'2, and Excavation Area r3.
While Excavation Area fl is being mined, the water will be pumped and stored within the provided
volume within Excavation Areas n2 & r3. Once Excavation =1 is complete, the water will be pumped out
of Excavation Area -2 and stored in the Volume provided within Excavation Areas rl & r3 in order to
excavate Area ;2. Finally, once Excavation R2 is complete, the water will be pumped out of Excavation
Area 1'3 and stored within Excavation Areas #1 & #2. Please find calculations enclosed illustrating
adequate dewatering storage volumes available during the excavation of each area.
In regard to sedimentation and erosion control measures, it is proposed to establish a temporary
construction entrance at the beginning of each of the two access roads and place silt fence along the

downgrade -side of the excavation area. Please refer to the design plans and notes for further detail
regarding the sedimentation and erosion control measures.
MAINTENANCE
Contractors shall be responsible for periodic inspection and maintenance of all indicated erosion control
devices in accordance with the plans and specifications. In addition, inspection and any necessary
maintenance will be required immediately following any significant storm event. Any erosion control
measure that fails to function as intended shall be repaired immediately. Upon completion of
construction and the establishment of stabilized ground cover, the property owner shall be responsible
for any on going site maintenance.

EROSION AND SEDIMENTATION CONTROL SPECIFICATION
PART 1-GENERAL
1 A RELATED DOCUMENT
A. Drawings and general provisions of the Contract, including General and Supplementary
Conditions and Division 1 Specification Sections, apply to this Section.
1.2 WORK INCLUDED
A. Contractor shall take every reasonable precaution throughout construction to prevent the
erosion of soil and the sedimentation of streams, lakes, reservoirs, other water impoundments,
ground surfaces, or other property as required by State and Local regulations.
B. Contractor shall, upon suspension or completion of land -disturbing activities, provide
protection covering for disturbed areas. Permanent vegetation shall be established at the earliest
practicable time. Temporary and permanent erosion control measures shall be coordinated to
assure economical, effective, and continuous erosion and sediment control throughout the
construction and post construction period.
1.3 RELATED SECTIONS
A. Related Sections — The following Sections contain requirements that relate to this Section:
1. 01011 — Existing Underground Utilities
2. 01015 —Special Conditions for this Contract
3. 01070 —Shop Drawings, Project Data & Samples
4. 02200 — Earthwork, Excavation Trenching, and Backfilling
5. 02230 — Site Clearing
b. 02240 — Dewatering
7. 02485 — Seeding General Areas
1.4 REGULATORY REQUIREMENTS
A. Contractor shall be responsible for prevention of damage to properties outside the construction
limits from siltation due to construction of the project. The Contractor will assume all
responsibilities to the affected property owners for correction of damages that may occur.
Erosion control measures shall be performed by the Contractor, conforming to the requirements
of, and in accordance with plans approved by applicable state and local agencies and as per the
erosion control portion of the construction drawings and these specifications. The Contractor
shall not allow mud and debris to accumulate in the streets. Should the Contractor pump water
from trenches during construction, appropriate siltation preventative measures shall be taken
prior to discharge of pumped water into any storm drain or stream.

PART 2 -PRODUCTS
2.1 Open mesh biodegradable mulching cloth.
2.2 Fertilizer shall be 10-10-10 grade or equivalent.
2.3 Lime shall be dolomitic agricultural ground 1 limestone containing not less than 10 percent
magnesium oxide.
2.4 Phosphate shall be 20 percent super phosphate or equivalent.
2.3 Provide grass seed mixture as shown on the plans.
2.6 Silt fence shall consist of non -biodegradable filter fabric (Trevira, Mirafi, etc.) wired to
galvanized wire mesh fencing and supported by metal posts.
2.7 NCDOT Class B stone for erosion control.
PART 3 - EXECUTION
3.1 CLEARING
A. Clearing and grubbing shall be scheduled and performed in such a manner that subsequent
grading operation and erosion control practices can follow immediately thereafter. Excavation,
borrow, and embankment operations will be conducted such that continuous operation. All
construction areas not otherwise protected shall be planted with permanent vegetative cover
within 21 calendar days after completion of active construction.
3.2 STABILIZING
A. The angle for graded slopes and fills shall be no greater than the angle that can be retained by
vegetative cover or other adequate erosion control devices or structures. All disturbed areas not
to be paved and left exposed will, within 21 calendar days of completion of any phase of
grading, be planted or otherwise provided with either temporary or permanent ground cover,
devices, or structures sufficient to restrain erosion.
3.3 REGULATORY .REQUIREMENTS
A. Whenever land disturbing activity is undertaken on a tract, a ground cover sufficient to restrain
erosion must be planted or other wise provided within 21 calendar days on that portion of the
tract upon which further active construction is to being undertaken.
B. If any earthwork is to be suspended for any reason whatsoever for longer than 21 calendar
days, the areas involved shall be seeded with vegetative cover or otherwise protected against
excessive erosion during the suspension period. Suspension of work in any area of operation
does not relieve the Contractor of the responsibility for the control of erosion in that area.

,n
PART 4 - CONSTRUCTION PHASE
4.1 PRACTICES
A. Avoid dumping soil or sediment into any streambed or watercourse. Backfill for stream
crossings shall be placed dry and compacted to minimize siltation of the watercourse, where
applicable.
B. Maintain an undisturbed vegetative buffer where possible between a natural watercourse and
trenching and grading operations.
C. Avoid equipment crossings of streams, creeks, and ditches where practicable.
PART 5 - SEDIMENT CONTROL FEATURES
5.1 GENERAL
A. All devices (silt fences, retention areas, etc.), for sediment control shall be constructed at the
locations indicated prior to beginning excavation on the site. All devices shall be properly
maintained in place until a structure or paving makes the device unnecessary or until directed
to permanently remove the device.
5.2 DESIGN APPLICATIONS
A. Mulch shall be used for temporary stabilization of areas subject to excessive erosion, and for
protection of seed beds after planting where required.
1. jute, mesh, etc. should be installed as per manufacturer's instructions.
B. Silt fences shall be used at the base of slopes and in drainage swales to restrict movement of
sediment from the site. Straw bales may be required for reinforcement.
C. Riprap shall be used at the proposed outfall pipes as indicated on plans.
D. Establish vegetative cover on all unpaved areas disturbed by the work.
1. Preparation of Seedbed. Areas to be seeded shall be scarified a depth of 6 inches until a
firm, well -pulverized, uniform seedbed is prepared. Lime, phosphorous, and fertilizer
shall be applied during the scarification process in accordance with the following rates.
a. Lime — 2 ton per acre
b. Nitrogen —100 pounds per acre
C. P2O5 — 200 pounds per acre
2. Seeding. Disturbed areas along roads and ditches shall be permanently seeded with 10-20
pounds per acre of centipede during the period from March through September. Seeding
performed during the period from April to August shall be temporarily seeded with'40
pounds per acre of German Millet. The permanent vegetative cover will be over seeded at
the earliest possible time as specified above.
3. Mulch all areas immediately after seeding. Mulch shall be applied and anchored as
specified hereinbefore.

5.3 MAINTENANCE
A. The Contractor shall be responsible for maintaining all temporary and permanent erosion
control measures in functioning order. Temporary structures shall be maintained until such
time as vegetation is firmly established and grassed areas shall be maintained until completion
of the project. Areas which fail to show a suitable stand of grass or which are damaged by
erosion shall be immediately repaired.
5.4 REMOVAL OF SEDIMENT CONTROL DEVICES
A. Near completion of the project, when directed by the Owner's agent, the Contractor shall
dismantle and remove the temporary devices used for sediment control during construction.
All erosion control devices in seeded areas shall be left in place until the grass is established.
Seed areas around devices and mulch after removing or filling temporary control devices.
END OF SECTION 02410

-PARAMOUNTE
r N G 1 N r=- C- R I N G I N C
Project Name; Rocky Run Road Pit
Client_
Frank Morton
Project Number:
11142.PE
Prepared By:
GLM
Date:
7/11/11
Excavation Area #1 - Volume of Groundwater to be Removed
CONTOUR
CONTOUR AREA INCR.
ACCUM.
VOLUME
VOLUME
[so ft]
[Cu ft]
[cu ft]
17.0
84,966
0
0
18.0
89,070
87,018
87,018
19.0
93,272
91,171
178,189
2C.0
97,570
95,421
273,610
21.0
101,965
99,768
373,378
22.0
106,456
104,211
477,588
23.0
111,045
108,751
5B6,339
24.0
115,731
113,388
699,727
25.0
120,513
118,122
817,849
26.0
125,393
122,953
940,802
27.0
130.369
127,881
1,068.683
28.0
135,442
132,906
1,201,588
29.0
140,610
138,026
1,339.614
30.0
145,876
143,243
1,482.857
' 31.0
151,239
148,558
1,631,415
32.0
156,698
153,969
1,785,383
Excavation Areas #2 & #3 - Total Storage Volume
INCR.
ACCUM.
CONTOUR
CONTOUR AREA
VOLUME
VOLUME
_ [sq ft]
[cu ft]
r [cu ft]
32.0
315,251
0�
0
33.0
326,277
320,764
320,764
34.0
337,449
331,863
652,627
35.0
348,764
343,107
995,734
36.0
360,213
354,489
1.350,222
37.0
371,779
365,996
1.716,218
38.0
383,458
377,619
2,093,837
39.0
395,250
389,354
2,483,191
40.0
407,156
401,203
2.884,394
41,0
419,175
413,166
3,297,559
42.0
431,307
425,241
3,722,800
"Total volume of water to be relocated
'Total storage volume available above water table
The total volume of water to be relocated during Excavation #1 is 1,785,383 cubic feet.
The total storage volume available in Excavation Areas #2 & #3 above the water table is 3,722,800 cubic feet.
Therefore, there is adequate storage area for the groundwater from Excavation #1 to be temporarily relocated to
Excavation Areas #2 & #3.

PARAMOUNTE
E n G i " E F_ R 1 N G. I " G
Project Name: Rocky Run Road Pit
Client:
Frank Morton
Project Number:
11142.PE
Prepared By:
GLM
Date:
6/29/11
Excavation Area #2 - Volume of Groundwater to be Removed
INCR.
ACCUM.
CONTOUR
CONTOUR AREA
VOLUME
VOLUME
[sq ft]
[cu ft]
[cu ftj _
17.0
77,628
0
0
18.0
82,122
79.875
79.875
19.0
86.731
84,427
164,302
20.0
91.454
89,093
253,394
21.0
96.288
93,871
347.265
22.0
101,212
98,750
446,015
23.0
106,223
103,718
549,733
24.0
111,321
108,772
658,505
25.0
116,506
113,914
772,418
26.0
121,778
119,142
891,560
27.0
127,135
124,457
1,016,017
28.0
132,578
129.857
1,145,873
29.0
135,105
135,342
1,281,215
30.0
143,718
140,912
1,422,126
31.0
149,417
146,568
1,568,694
32.0
155,200
152,309
1,721,002 `Total volume of water to be relocated
Excavation Areas #1 & #3 - Total Storage Volume
CONTOUR CONTOUR AREA INCR. ACCUM.
VOLUME VOLUME
[sq ft]
]cu ft]
[cu ft]
32.0
316,749
0
0
33.0
327,460
322,105
322,105
34.0
338,329
332,895
654.999
35.0
349,337
343.833
998,832
36.0
360.476
354.907
1,353,739
37.0
371.729
366,103
1,719,841
38.0
383,097
377,413
2.097,254
39.0
394,577
388,837
2,486,091
40.0
406,171
400,374
2,886,465
41.0
417.879
412,025
3,298.490
42.0
429,699
423,789
3,722,279 Total storage volume available above water table
The total volume of water to be relocated during Excavation #2 is 1,721,002 cubic feel.
The total storage volume available in Excavation Areas #1 & #3 above the water table is 3,722,279. cubic feet.
Therefore, there is adequate storage area for the groundwater from Excavation #2 to be temporarily relocated to
Excavation Areas #1 & #3.

_D ARAMOUNTE
r n c_-. N E_ f. FZ I N C. . I N G
Project Name: Rocky Run Road Pit
Client:
Prank Morton
Project Number:
11142.PE
Prepared By:
GLM
-Date:
6/29/11
Excavation Area #3 -Volume of Groundwater to be Removed
CONTOUR
CONTOUR AREA
INCR.
ACCUM
VOLUME
VOLUME
[sq ft]
[cu ft]
[cu ft]
17,0
90,914
0
0
18.0
94,988
92,951
92,951
19.0
99,141
97,065
190,016
20.0
103,374
101,258
291.273
21.0
107,687
105,531
396,804
22.0
112,180
109,934
506,737
23.0
116.554
114,367
621.104
24.0
121,107
118,831
739,935
25.0
125.739
123.423
863,358
26.0
130,442
128,091
991.448
27.0
135,215
132,829
1,124,277
28.0
140,055
137,635
1, 261, 912
29.0
144,960
142,508
1,404,419
30.0
149,927
147,444
1,551,863
31.0
154,957
152,442
1,704, 305
32.0
160,051
157,504
1,861,809
Excavation Areas #1 & #2 - Total Storage Volume
CONTOUR CONTOUR AREA INCR. ACCUM.
VOLUME VOLUME
_
[sq ft]
jcu ft]
[cu ftj
32.0
311,898
0
0
33.0
323,323
317,611
317,61.1
34.0
334,930
329,127
646.737
35.0
346.703
340,817
987,554
36.0
358,629
352,666
1,340.220
37.0
370,670
364,650
1,704,869
38.0
382,825
376,748
2,081,617
39.0
395,093
388,959
2,470,576
40.0
407,473
401,283
2,871,859
41.0
419,968
413,721
3,285.579
42.0
432.574
426,271
3,711,850
'Total volume of water to be relocated
`Total storage volume available above water table
The total volume of water to be relocated during Excavation #3 is 1,861,809 cubic feet.
The total storage volume available in Excavation Areas #1 & #2 above the water table is 3,711,850. cubic feet.
Therefore, there is adequate storage area for the groundwater from Excavation #3 to be temporarily relocated to
Excavation Areas #1 & #2.

Beverly Eaves Perdue
Governor
LTIFWA
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Coleen H, Sullins
Director
February 24, 2011
CERTIFIED MAIL '
RETURN RECEIPT REQUESTED
CERTIFIED RECEIPT #7007 0220 0000 8216 7190
Frankie R. and Gloria J. Morton
3121 Newbern Highway
Jacksonville, NC 28546
Subject: NOTICE OF VIOLATION NOV-2011-PC-0149
Failure to Obtain General Stormwater Permit (NCG010000)
Stream Standard Violation for Turbidity
Removal of Best U*eage . V S vc:7,,9
Project: Frank Morton Property
Dear Mr. and Mrs. Morton:
Dee Freeman
Secretary
On September 23, 2010, Division Representatives, Linda Willis (Division of Water Quality,
Surface Water Protection Section) and Karl Hammers (Division of Land Resources), inspected
your site as a result of a fish kill complaint from a concerned citizen. Division Representatives
discovered a discharge of muddy water to the Unnamed Tributary to the Little Northeast Creek,
from the Frank Morton Property.
During the site investigation, Division Representatives noted a large excavated pit that was being
dewatered and discharged to a network of ditches that were hydrologically connected to the
Unnamed Tributary to the Little Northeast Creek. The water being pumped from the excavated
pit caused a water quality standard violation in the Unnamed Tributary to the Little Northeast
Creek, The Unnamed Tributary to the Little Northeast Creek is a class C, NSW, water of the
State. The discharge from the excavated pit to the unnamed tributary was 1.,000 NTU
(Nephelometric Turbidity Units). The turbidity in the Unnamed Tributary, downstream from the
discharge from the dewatering activities was 1,000 NTU. The stream standard for turbidity for
class C water is 50 NTU.
A file review indicated you had not filed an Erosion and Sedimentation Control Plan with DLR
at least 30 days prior to beginning this land -disturbing activity of approximately l l acres off
Rocky Run Road, in Onslow County, North Carolina. By failing to do so, you were also in
violation with the Division of Water Quality for failure to obtain a General Permit (NCGO10000)
to discharge stormwater under the National Pollutant Discharge Elimination System (NPDFS) in
accordance with Title 15A North Carolina Administrative Code 2B .0100. Please be advised that
N. C. Division of Water Quality
Wilmington Regional Office
127 Cardinal Drive Extension, Wilmington, NC 28405
Phone: [phone] FAX: [phone] L
Customer Service: 1-877$23-6748
Internet: www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer
NorthCarolina
Naturally

NOV-2011-PC-0149
Frankie Morton Property
this violation and any future violations are subject to civil penalty assessments of up to
$25,000.00 per day, per violation.
The Division of Land Resources has sent the General Permit to you along with the approval of
9 your Erosion and Sedimentation Control Plan on December 7, 2010. Adherence to the approved
Plan is an enforceable component of the General Permit. The General Permit not only requires
that you follow the specifications of the approved Plan, but also includes the installation of a rain
gauge, regular inspections of stormwater discharges and erosion control devices, and record
keeping requirements.
As a result of the site investigation and a file review, the following violations are noted:
Item I. Failure to Secure Stormwater General Permit NCGOIOOOO
Site visits and a file review confirmed that a Sedimentation and Erosion Control plan approval
had not been applied for or secured for the land disturbing activity; therefore, coverage under the
NPDIaS General Permit to discharge stormwater from land disturbing activities had not been
secured in accordance with the provision of G.S. 143-215.L This General Permit is applicable to
point source discharges from construction activities disturbing one or more acres of land. The
submission of a proposed Erosion and Sedimentation Control Plan to the Division of Land
Resources or delegated local program shall be considered to take the place of a Notice of Intent
for coverage under this General Permit for those projects requiring this Permit coverage.
Coverage under this General Permit shall become effective upon issuance of an approval for the
Erosion and Sedimentation Control Plan by the Land Quality Section of the Division of Land
Resources or delegated local program. Prior to the commencement of construction and land
disturbing activities approval of the Erosion and Sedimentation Control Plan shall be obtained.
Item I1. Stream Standard Violation
15A NCAC 02B .0211 (3)k: Turbidity; the turbidity in the receiving water shall not exceed 50
Nephelometric 'Turbidity Units (NTU) in streams not designated as trout waters and 10 NTU in
streams, lakes or reservoirs designated as trout waters; for lakes and reservoirs not designated as
trout waters, the turbidity shall not exceed 25 N'f U.
Item III. Removal of Best Useage
15A NCAC 02B .0211 (2)
The waters shall be suitable for aquatic life propagation and maintenance of biological integrity,
wildlife, secondary recreation, and agriculture; sources of water pollution which preclude any of
these uses on either a short-term or long-term basis shall be considered to be violating a water
quality standard.
Requested Response
Accordingly, you are directed to respond to this letter in writing within 30 calendar days of
receipt of this Notice. Your response should be sent to this office at the letterhead address. Your
response should include the following:
1. Explain the reasons for discharging without a valid permit.

NOV-2011-PC-0149
Frankie Morton Property
2. Provide a detailed list of the actions taken to resolve the violations found at the site. This
should include a detailed list of the activities taken to remediate the turbidity violation in
stream as well as ongoing efforts that are being taken to ensure no future water quality
standard violation will occur as a result of land disturbing activities at this site.
Furthermore, if the excavated pit requires any dewatering, you are hereby requested to apply for
an individual NPDES Permit for wastewater discharge. Any discharges from the pit must be of
sufficient quality to avoid water quality standard violations. Division Representative, Linda
Willis, advised you in September to discontinue all dewatering from the pit.
Thank you for your attention to this matter. This Office is considering sending a
recommendation for enforcement to the Director of the Division of Water Quality regarding
these issues and any future/continued violations that may be encountered. Your above -
mentioned response to this correspondence will be considered in this process. This office
requires that the violations, as detailed above, be abated immediately. These violations and
any future violations are subject to a civil penalty assessment of up to $25,000.00 per day
for each violation. Should you have any questions regarding these matters, please contact Linda
Willis at [phone] or myself at [phone].
Sincerely,
Rick Shiver
Regional Supervisor
Division of Water Quality
Surface Water Protection Section
cc: DWQ CO Files
Katie Merritt-WBS Compliance & Permits Unit
Water Quality-WiRO NCGO10 Onslow
Land Quality-WiRO Dan Sams for Karl Hammers

4V
NC®ENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins
Governor Director
February 24, 2011
CERTIFIED MAIL
RETURN RECEIPT RE QUESTED
CERTIFIED RECEIPT #7007 0220 0000 8216 7190
Frankie R. and Gloria J. Morton
3121 Newbern Highway
Jacksonville, NC 28546
Subject: NOTICE OF VIOLATION AN-Z011 -PC -009
Failure to Obtain General Stormwater Permit (NCGO10000)
Stream Standard Violation for Turbidity
Removal of Best Useage
Project: Frank Morton Property
Dear Mr. and Mrs. Morton:
Dee Freeman
Secretary
On September 23, 2010, Division Representatives, Linda Willis (Division of Water Quality,
Surface Water Protection Section) and Karl Hammers (Division of Land Resources), inspected
your site as a result of a fish kill complaint from a concerned citizen. Division Representatives
discovered a discharge of muddy water to the Unnamed Tributary to the Little Northeast Creek,
from the Frank Morton Property.
During the site investigation, Division Representatives noted a large excavated pit that was being
dewatered and discharged to a network of ditches that were hydrologically connected to the
Unnamed Tributary to the Little Northeast Creek. The water being pumped from the excavated
pit caused a water quality standard violation in the Unnamed Tributary to the Little Northeast
Creek. The Unnamed Tributary to the Little Northeast Creek is a class C, NSW, water of the
State. The discharge from the excavated pit to ,the unnamed tributary was 1,000 NTU
(Nephelometric Turbidity Units). The turbidity in the Unnamed Tributary, downstream from the
discharge from the dewatering activities was 1,000 NTU. The stream standard for turbidity for
class C water is 50 NTU.
A file review indicated you had not filed an Erosion and Sedimentation Control Plan with DLR
at least 30 days prior to beginning this land -disturbing activity of approximately l 1 acres off
Rocky Run Road, in Onslow County, North Carolina. By failing to do so, you were also in.,
violation with the Division of Water Quality for failure to obtain a General Permit (NCGOICOOO)
to discharge stormwater under the National Pollutant Discharge Elimination System (NPDES) in
accordance with Title 15A North Carolina Administrative Code 2B .0100. Please be advised that
N. C. Division of Water Quality
Wilmington Regional Office
127 Cardinal Drive Extension, Wilmington, NC 28405
Phone: [phone] FAX: [phone]
Customer Service: 1-877-623-6748
Internet: www.ncwaterquality.org
o°rt NhCarolina
An Equal Cpportunity l Affirmative Aetion Employer

N OV-2011-PC-0149
Frankie Morton Property
this violation and any future violations are subject to civil penalty assessments of up to
$25,000.00 per day, per violation.
The Division of Land Resources has sent the General Permit to you along with the approval of
your Erosion and Sedimentation Control Plan on December 7, 2010. Adherence to the approved
Plan is an enforceable component of the General Permit. The General Permit not only requires
that you follow the specifications of the approved Plan, but also includes the installation of a rain
gauge, regular inspections of stormwater discharges and erosion control devices, and record
keeping requirements.
As a result of the site investigation and a file review, the following violations are noted:
Item I. Failure to Secure Stormwater General Permit NCGO10000
Site visits and a file review confirmed that a Sedimentation and Erosion Control plan approval
had not been applied for or secured for the land disturbing activity; therefore, coverage tinder the
NPDES General Permit to discharge stormwater from land disturbing activities had not been
secured in accordance with the provision of G.S. 143-215.1. This General Permit is applicable to
point source discharges from construction -activities disturbing one or more acres of land. The
submission of a proposed Erosion and Sedimentation Control Plan to the Division of Land
Resources or delegated local program shall be considered to take the place of a Notice of Intent
for coverage under this General Permit for those projects requiring this Permit coverage.
Coverage under this General Permit shall become effective upon issuance of an approval For the
Erosion and Sedimentation Control Plan by the Land Quality Section of the Division of Land
Resources or delegated local program. Prior to the commencement of construction and land
disturbing activities approval of the Erosion and Sedimentation Control Plan shall be obtained.
Item It. Stream Standard Violation
15A NCAC 02B .0211 (3)k: Turbidity; the turbidity in the receiving water shall not exceed 50
Nephelometric Turbidity Units (NTU) in streams not designated as trout waters and 10 NTU in
streams, lakes or reservoirs designated as trout waters; for takes and reservoirs not designated as
trout waters, the turbidity shall not exceed 25 NTU.
Item III. Removal of Best Useage
15A NC AC 02B .0211 (2)
The waters shall be suitable for aquatic life propagation and maintenance of biological integrity,
wildlife, secondary recreation, and agriculture; sources of water pollution which preclude any of
these uses on either a short-term or long-term basis shall be considered to be violating a water
quality standard.
Requested Response
Accordingly, you are directed to respond to this letter in writing within 30 calendar days of
'receipt of this Notice. Your response should be sent to this office at the letterhead address. Your
response should include the following:
1. Explain the reasons for discharging without a valid permit.

NOV-2011-PC-0149
Frankie Morton Property
2. Provide a detailed list of the actions taken to resolve the violations found at the site. This
should include a detailed list of the activities taken to remediate the turbidity violation in
stream as well as ongoing efforts that are being taken to ensure no future water quality
standard violation will occur as a result of land disturbing activities at this site.
Furthermore, if the excavated pit requires any dewatering, you are hereby requested to apply for
an individual NPDLS Permit for wastewater discharge. Any discharges from the pit must be of
sufficient quality to avoid water quality standard violations. Division Representative, Linda
Willis, advised you in September to discontinue all dewatering from the pit.
Thank you for your attention to this matter. This Office is considering sending a
recommendation for enforcement to the Director of the Division of Water Quality regarding
these issues and any future/continued violations that may be encountered. Your above -
mentioned response to this correspondence will be considered in this process. This office
requires that the violations, as detailed above, be abated immediately. These violations and
any future violations are subject to a civil penalty assessment of up to $25,000.00 per day
for each violation. Should you have any questions regarding these matters, please contact Linda
Willis at [phone] or myself at [phone].
Sincerely,
Rick Shiver
Regional Supervisor
Division of Water Quality
Surface Water Protection Section
cc: DWQ CO Files
Katie Merritt-WBS Compliance & Permits Unit
Water Quality-WiRO NCG010 Onslow
Land Quality-WiRO Dan Sams for Karl Hammers

CDENR
North Carolina Department of Environment and Natural Resources
Division of. Land Resources
Land Quality Section
James D. Simons, PG, PE Beverly Eaves Perdue, Governor
Director and State Geologist Dee Freeman, Secretary
December 7, 2010
LETTER OF APPROVAL WITH NIOD.IFICATIONS AND PERFORtNIANCE
RESERVATIONS
Frankie R. and Gloria J. Morton
3121 New Bern Highway
Jacksonville, NC 28540
RE: Project Naine: Frankie R. Morton & wife Gloria J. Morton
Project ID: ONSLO-2011-028 Acres Approved: 16.8
County: Onslow, NCSR 1413, White Oak
River Basin: White Oak Stream Classification: Other
Submitted By: Betty Bullock, John L. Pierce & Associates, P.A.
Date Received by LQS: December 7, 2010
Plan Type: Revised
Dear Mr. and Mrs. Morton. -
This office has reviewed the subject erosion and sedimentation control plan and hereby issues this
Letter of Approval with Modifications and Performance Reservations. A list of the modifications
and reservations is attached. This plan approval shall expire three (3) years following the date of
approval, if no land -disturbing activity has been undertaken, as is required by Title 15A NCAC 413
.0129. Should the plan not perform adequately, a revised plan will be required (G.S. 113A-54.1)(b).
Please be advised that Title 15A NCAC 4B .01 18(a) requires that a copy of the approved erosion
control plan be on file at the job site. Also, you should consider this letter to give the Notice
required by G.S. 113A-61.1(a) of our right of periodic inspection to insure compliance with the
approved plan.
North Carolina's Sedimentation Pollution Control Program is perfonliance-oriented, requiring
Protection of existing natural resources and adjoining properties.. If, following the commencement
ofthis project, it is determined that the erosion and sedimentation control plan is inadequate to meet
the requirements of the Sedimentation Pollution Control Act of 1973 (North Carolina General
Statute 1 13A-51 thru 66), this office may require revisions to the plan and implementation of the
revisions to ensure compliance with the Act.
Wilmington Regional Office
127 Cardinal Drive Extension, Wilmington, North Carol'ma 28405 Phone:[phone] Fax [phone]

Letter of Approval with Modifications and Performance Reservations
Frank -le R. Morton & wife Gloria J. Morton
December 7, 2010
Page 2 of 3
Acceptance and approval of this plan is conditioned upon your compliance with Federal and State
water quality laws, regulations, and rules. In addition, local city or county ordinances or rules may
also apply to this land -disturbing activity. This approval does not supersede any other permit or
approval.
Please be aware that your project will be covered by the enclosed NPDES General Stofmwater
Permit NCGOl OOOO (Construction Activities). You should first become familiar with all of the
requirements for compliance with the enclosed general permit.
Please note that this approval is based in part on the accuracy of the information provided in the
Financial Responsibility Form, which you have provided. You are requested to file an amended
form if there is any change in the information included on the form. In addition, it would be helpful
if you notify this office of the proposed starting date for this project. Please notify us if you plan to
have a preconstruction conference.
Your cooperation is appreciated.
Sincerely,
Daniel Sams, PE
Regional Engineer
Land Quality Section
Enclosures: Certificate of Approval
Modifications and Performance Reservations
NPDES Permit
cc: Betty Bullock, John L. Pierce &, Associates, P.A.

Letter of Approval with Modifications and Performance Reservations
Frank -le R. Morton & wife Gloria J. Morton
December 7, 2010
Page 3 of 3
IINIODIFICATIONS AND PERFORMANCE RESERVATIONS
Project Name: Frankie R. TvIorton & wife Gloria. J. Morton Site Stablization
Project ID: ONSLO-2011-028
County: Onslow
1. This plan approval shall expire on December 31, 2014, if no land disturbing activity has been undertaken, as is
required by Title 1 5A NCAC 4B.0029,
2. The developer is responsible for the control of sediment on -site. If the approved erosion and sedimentation control
measures prove insufficient, the developer must take those additional steps necessary to stop sediment from leavine this
site. Each sediment storage device must be inspected after each storm event. Maintenance and/or clean out is necessary
anytime the device is at 50% capacity.
3. Any and all existing ditches on this project site are assumed to be left undisturbed by the proposed development unless
otherwise noted. The removal of vegetation within any existing ditch or channel is prohibited unless the ditch or channel
is to be regarded with side slopes of 2 horizontal to 1 vertical or less steep. Bank slopes may be mowed, but stripping of
vegetation is considered new earth work and is subject to the same erosion control requirements as new ditches.
4. The developer is responsible for obtaining any and all permits and approvals necessary for the development of this
project prior to the commencement of this land disturbing activity. This could include agencies such as the Division of
Water Quality's'stormwater regulations, their enforcement requirements within Section 401 of the Clean Water Act, the
U.S. Army Corps of Engineers' jurisdiction of Section 404 of the Clean Water Act, the Division of Coastal
Management's CAMA requirements, the Division of Solid Waste Management's landfill regulations, the Environmental.
Protection Agency and/or The U.S. Army Corps of Engineers jurisdiction of the Clean Water Act, local County or
110nicipalities' ordinances, or others that may be required. This approval -cannot supersede any other permit or approval;
however, in the case of a Cease and .Desist Order from the Corps of Engineers, that Order would only apply to wetland
areas. All high ground would still have to be in compliance with the N.C. Sedimentation Pollution Control Act.
5. If any area on site falls within the jurisdiction of Section 401 or 404 of the Clean Water Act, the developer is responsible
for compliance with the requirements of the Division of Water Quality, the Corps of Engineers and the Environmental
Protection Agency (EPA) respectively. Any erosion control measures that fall within jurisdictional wetland areas must
be approved by the aforementioned agencies prior to installation. The Land Quality Section must be notified of a
relocation'of the measures in question to the transition point between the wetlands and the uplands to assure that the
migration of sediment will not occur. If that relocation presents a problem or contradicts any requirements of either
DWQ, the Corps, or the EPA, it is the responsibility of the developer to inform the Land Quality Section regional office
so that an adequate contingency plan can be made to assure sufficient erosion control remains on site.
6. Any borrow material brought onto this site must be from a legally operated mine or other approved source. Any soil
waste that leaves this site can be transported to a permitted mine or separately permitted construction sites without
additional permits. Disposal at any other location would have to be included as a permit revision for this approval.
7. This permit allows for a land disturbance, as called for on the application plan, not to exceed 16.8 acres. ] xceeding that
acreage will be a violation of this permit and would require a revised plan and additional application fee. Any addition in
impervious surface, over that already noted on the approved plan, would also require a revised plan to verify the
appropriateness of the erosion control measures and stormwater retention measures.
S. The construction detail for the proposed silt fence requires reinforcing wire and steel posts a maximum of eight (8) feet
apart. Omission of the reinforcing wire is a construction change that necessitates more posts for support, i.e., the spacing
distance needs to be reduced to no greater than six (6) feet apart.
9. A graveled construction entrance must be located at each point of access and egress available to construction vehicles
during the grading and construction phases of this project. Access and egress from the project site at a point without a
graveled entrance will be considered a violation of this approval. Routine maintenance of the entrances is critical.
10. The 'North Carolina Sedimentation Pollution Control Act mandates a short time frame in which to re-establish vegetative
groundcover. Slopes (including cuts, fills, and ditch banks) left exposed will, within 21 calendar days after completion of
any phase of grading, be planed or otherwise provided with Groundcover sufficient to permanently restrain erosion.

me 2.00) 30) 0 NOV - Zo 11 - PC - 4/ 4
FINANCIAL_ RESPONSIBILITY/OWNERSHIP FORM
SEDIMENTATION POLLUTION CONTROL ACT
No person may initiate any land -disturbing activity on one or more acres as covered by the Act before this
form and an acceptable erosion and sedimentation control plan have been completed and approved by the
Land Quality Section, N.C. Department of Environment and Natural Resources. (Please type or print and, if
the question is not applicable or the e-mail and/or fax information unavailable, place NIA in the blank.)
Part A.
Project Name Frankie R. Morton & wife Gloria J. Morton
2. Location of land -disturbing activity: County Onslow City or Township White Oak.
Highway/Street NCSR 1413 Latitude 34045'51.0" Longitude 77016'24.8"
3. Approximate date land -disturbing activity will commence: October 10. 2010
4. Purpose of development (residential, commercial, industrial, institutional, etc.): Residential
5. Total acreage disturbed or uncovered (including off -site borrow and waste areas): 16.80 acres
6. Amount of fee enclosed: $ 1105.00. The application fee of $65.00 per acre (rounded up to the next
acre) is assessed without a ceiling amount (Example: a 9-acre application fee is $450).
7. , Has an erosion and sediment control plan been filed? Yes X No Enclosed
8. Person to contact should erosion and sediment control issues arise during land -disturbing activity:
Name Frankie R. Morton E-mail Address
Telephone [phone] „ Cell # - Fax #
9. Landowner(s) of Record (attach accompanied page to list additional owners):
Frankie R. Morton & wife Gloria J. Morton [phone]_
Name Telephone
3121 New Bern Highway
Current Mailing Address Current Street Address
Jacksonville NC 28540
City State Zip City
State
Fax Number
10. Deed Book No. 3009 Page No. 252-254 Provide a copy of the most current deed.
Part B.
Zip
Person(s) or firm(s) who are financially responsible for the land -disturbing activity (Provide a
comprehensive list of ail responsible parties on an attached sheet):
Frankie R. Morton & wife Gloria J. Morton
Name
3121 New Bern Highway
Current Mailing Address
E-mail Address
Current Street Address
Jacksonville NC 28540
City State Zip City State Zip
Telephone_(910)340-2606 Fax Number

AJ
NCDENR
North. Carolina Department of Environment and Natural Resources
Division of Land Resources
Land Quality Section
James D. Simons, PG, PE Beverly Eaves Perdue, Governor
Director and State Geologist Dee Freeman, Secretary
September 24, 2010 .
NOTICE OF VIOLATIONS OF THE
SEDIMENTATION POLLUTION CONTROL ACT
CERTIFIED MAIL
RETURN RECEIPT REQUESTED 7010 0290 0003 0834 4063
Frankie R. and Gloria J. Morton
3121 New Bern Highway
Jacksonville, NC 28546
RE: Project Name: Frank Morton Property
Project ID: ONSLO-2011-028
County: Onslow
Compliance Deadline:. 30 days from receipt
Dear Mr. and Mrs. Morton:
On September 23, 2010, personnel of this office inspected a project located on Rocky Run Road,
Jacksonville in Onslow County, North Carolina. This inspection was performed to determine
compliance with the North Carolina Sedimentation Pollution Control Act (Act) of 1973. The
inspection revealed a land -disturbing activity of approximately 11 A acres being conducted.
It is our understanding that you and/or your firm are responsible for this land -disturbing
activity. The purpose of this letter is to.inform you that this activity was found to be in violation of
the Act, G.S. 113A-50 to 66, Title 15A, North Carolina Administrative Code (NCAC), Chapter
4. If you feel that you are not responsible for the following violations, please notify this office
immediately.
Wilmington Regional Office
127 Cardinal Drive Extension, Wilmington, North Carolina 28405 Phone: [phone] Fax: [phone]

Notice of Violations
Project :- Frank Morton Property
September 24, 2010
Page 2 of 3
The violations that were found are:
Failure to file an erosion and sedimentation control plan with this office 30 or more days prior to
initiating any land -disturbing activity that will disturb more than one acre on a tract, failure to
secure this off ce's prior approval of the plan for any land -disturbing activity prior to beginning
the land -disturbing activity. G.S. 113A-54(d)(4), G.S. 113A-57(4) and 15A NCAC 4B. 0107(c).
The area of disturbance was measured with a measuring wheel and calculated to be
approximately J l acres. A permit application was not submitted prior to the land
disturbing activity.
2. Failure when a land -disturbing activity that will disturb more than one acre is undertaken on a
tract, to install sedimentation and erosion control devices sufficient to retain the sediment
generated by the land -disturbing activity within the boundaries of the tract during construction
upon and development of the tract. G.S. 113A-57(3).
Sediment was observed outside the boundaries of the tract.
;. Failure to take all reasonable measures to protect all public and private property from damage by
such land -disturbing activities. 15A NCAC 4B .0105.
A permit application could have been submitted. - A sediment basin' could have been
installed to trap the sediment.
Failure to retain along a lake or natural watercourse a buffer zone of sufficient width to corifine
visible siltation by natural or artificial means within the 25 percent of that portion of the buffer
zone nearest the land -disturbing activity. G.S. 1 I3A-57(1).
Sediment and muddy water was observed in the stream downstream of the land
disturbing, activity.
To correct these violations, you must:
Submit three (3) copies of an approvable sedimentation and erosion control plan and the
appropriate plan review fee to this office. Until the required plan has been approved, no
land -disturbing activity may be conducted, except that which is necessary to bring the site
into compliance. Until an erosion and sedimentation plan has been approved, any
land -disturbing activity, except that which is necessary to bring the site into compliance,
will constitute additional violations of the Act. Following our review of the plan within 30
days of receipt, this office will notify you that the plan has been approved, approved with
modifications or disapproved. Following approval of the plan, all land -disturbing activity
on the site must be conducted in accordance with the terms of the approved plan, the Act
and the implementing rules.

Notice of Violations
Project :- Frank Morton Property
September 24, 2010
Page 3 of 3
2. Install adequate measures to prevent any additional sediement from entering the
stream.
The violations cited herein may be referred to the Director of the Division of Land Resources (James
D. Simons, PG, PE) for appropriate enforcement action, including civil penalty.'assessments for an
initial one -day violation and/or a continuing violation. The penalty for an initial one -day violation
may be assessed in an amount not to exceed $5,000.00. The Division of Land Resources is not
required to provide a time period for compliance before assessing an initial penalty for the violations
cited herein. Please be advised that a civil penalty may be assessed for the initial day of violations
regardless of whether the violations are corrected within the time period set out below.
In addition, if the violations cited herein are not corrected within 30 days of receipt of this notice,
this office may request that the Director take appropriate legal action against you for continuing
violations pursuant to NCGS 113A-61.1 -and 113A-64. A penalty'may be assessed from the date of
the violation, pursuant to NCGS 13A-64(a)(1), and for each day of the continuing violation in an
amount not to exceed $5,000.00 per day.
Please be advised that any new land -disturbing activity associated with this project should not begin
until the area presently disturbed is brought into compliance with the Act. When corrective actions
are complete, you should notify this office so that work can be inspected. You. should not assume
that the property is in compliance with the Act until we have notified you. After installation, all
erosion control measures must be maintained in proper working order until the site is completely
stabilized.
We solicit your cooperation, and would like to avoid taking further enforcement action. At the same
time, it is your responsibility to understand and comply with the requirements of the Act. Copies of
the relevant statute and administrative rules may be examined at this office or will be sent to you
upon request. Should you have questions concerning this notice or the requirements of the Act
please contact either Karl Hammers [phone] or me at your earliest convenience.
'Sincerely, -r
Daniel Sams, PE, ME
Regional Engineer
Land Quality Section
Enclosures: Sedimentation. Inspection Report
Financial Responsibility Form
Erosion Control Plan Checklist
cc: State Sedimentation Specialist
Regional Water Quality Supervisor

e r.
North Carolina Department of Environment and Natural Resources
Land Quality Section:' 127 Cardinal Drive Extension, Wilmington, NC 28405 (910)
796-7215
County: Onslow Project: Frank Morton Property
Person financially responsible: Frankie and Gloria Morton
Address: 3121 New. Bern Highway Jacksonville, NC 28546
1.
2
3.
4.
5.
6.
7
8.
Project Location: Rocky Run Road, Jacksonville
Weather and sail conditions: . Sunny, workable
Is site currentiv under notice of violation? No
River basin: White Oak
Project #: ONSLO-2011-028
Pictures: Yes - Digital
Initial inspection
Is the site in compliance with S.P.C.A. and rules? No If no, check violations below:
Violations:
✓ a. No approved plan, G.S. 113A-57(4) and 15A NCAC 4B .O107(c)
✓ e. Insufficient measures to retain sediment on site, G.S. I I3A-57(3)
✓ f. Failure to take all reasonable measures, 15A NCAC 4B .0105.
✓ g. Inadequate buffer zone, G.S. 113A-57(i)
Potential NPDES Permit Violation? Yes
Describe: Sediment damage to a stream
Has sedimentation damage occurred since last inspection? Yes If Yes, where? (check all that apply)
✓ LakefNatural watercourse off the tract
✓ LakefNatural watercourse on the tract
Description: Sediment damage has entered a stream on site and the sediment has entered a stream south of
Rocky Run Road
Degree of damage: Severe
Contact made with (name): Frank Morton . Title: Owner.
Inspection report: Sent Report Date given/sent: September 24, 2010
9. Corrective action needed:
1. Submit an adequate sedimentation and erosion control plan for approval, covering all areas
disturbed or to be disturbed.
2. Install adequate measures to prevent any additional sediment from entering the stream.
10. Comments: Sediment and muddy water was observed in the stream downstream of the site. A pump was
discharging muddy water from a large pit on site at the start of the inspection. During the
inspection the pump was turned off and removed from the pit. Some sod tivas installed on the
slopes of the pond during the inspection. No additional soil disturbance should be conducted
until a permit is obtained,
Reported by: Karl Hammers Others present: Linda Willis
Date of inspection: September 23, 2010 Time arriving on site: 10:30 AIM Time leaving site: 2:30 PM
cc: Linda Willis, DWQ
Yes

Permit: NCGO10000
SOC:
County: Onslow
Region: Wilmington
Compliance Inspection Report
Effective: 12/07/10 Expiration:
Effective: Expiration:
Contact Person: Frankie R Morton
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 09/23/2010
Primary Inspector: Linda Willis
Secondary Inspector(s):
DWQ Tracking No: NCR003010
Title:
Entry Time: 01:00 PM
Reason for Inspection: Routine
Permit Inspection Type: Construction Stormwater
Facility Status: Q Compliant E Not Compliant
Question Areas:
i Construction
(See attachment summary)
Certification:
Owner: Frankie R Morton & Wife Gloria J Morton
Facility: Frankie R. Morton & wife Gloria J. Morton
NCSR 1413
Jacksonville NC 28546
Phone:
Exit Time: 03:00 PM
Phone:
Phone: [phone]
Inspection Type: Compliance Evaluation
Page: 1

Permit: NCR003010
Inspection Date: 0912312010
Inspection Summary:
Owner - Facility: Frankie R Morton & Wife Gloria J Morton
Inspection Type: Compliance Evaluation
DLR or Local Program Ins ep ction
# Is this inspection related to a DLR 1 local program inspection?
Reason for Visit: Routine
■ ❑
# If Yes, what was the DLR / local program inspection date? 09/23/2010
E & SC Plan Yes No NA NE
Is the site following its approved Erosion and Sedimentation Control Plan as indicated on DLRILocal Program ❑ i ❑ ❑
Inspection Report?
Comment: No E&SC Plan existed at the time of the inspection,
Erosion Control Measures Yes No NA NE
Is the site maintaining their erosion control measures as indicated on DLRILocal Program Inspection Report? ❑ ■ ' ❑ Cl
Comment: None
Approved E&SC Plan
Is a copy of the approved E&SC plan on site?
Comment: Construction without an E & SC Plan
Rain Gauge
Is a rain gauge present on the site at the time of inspection?
Comment: None
Rain Gauge Records
Is rain gauge data measured and recorded?
Comment: None
Yes
No
NA
NE
❑
i
❑
❑
Yes
No
NA
NE
❑
N
❑
Cl
Yes
No
NA
NE
❑
■
❑
❑
Inspection Records
Are inspection records of erosion & sedimentation control measures and stormwater discharges complete?
Comment: None
Other NCGO10000 Permit Conditions
Is the site compliant with other conditions of the NCGO10000 permit?
❑ i ❑ ❑
Yes No NA NE
❑ ®❑ ❑
Comment: No E&SC was secured.
Other Water Quality Issues Yes No NA NE
Is the site free of any other Water Quality issues as noted during the inspection? ❑ M ❑ ❑
Comment: Water Quality Standard violation for turbidity and removal of best useage.
Page: 2

County: ONSLOW Sample ID: AB63864
River Basin WOK oF'tt° rER 1�{� PO Number ft 10W7974 4
Report To WIROSP O� nl� Dale Received: 09123/201Do
� Time Received: 013:20
Collector. t. WILLIS
LabWOrks LoginlD SMATHIS
Region: WIRO
10
Sample Matrix: SURFACEINATER Report Generated:
Data Reported: 10101D
105I2010
Loc. Type: RIVEWSTREAM
Emergency Yes/No YES VisitlD
COC Yes/No YES
Loc. Descr.: 1919 ROCKY RUN RD N UT TO NE CREEK
Location ID! WIROSPNLC Collect Date: 0912212010 Collect Time: 13:45 Sample Depth
Result/
Method
Analysis
CAS #
Analyte Name
PQL
Units
Validated by
—
Qualifier
Reference
Date
LAB
Sample temperature'at receipt by lab •
0.8
°C
9123110
SMATHIS
MIC
BOD, 5-Day in liquid
2
32
mg1L
XPHA5210B
9/23/10
MOVERMAN
Turbidity
1
1000 J7
NTU
APHA213OB-20th
9/23/10
MOVERMAN
WET •
Chemical Oxygen Demand in liquid
20
3300
mg/L
Hach 8000
9124/10
MOVERMAN
NUT
NH3 as N in liquid 0.02 0.71 mg/L as N LaC10-107-06-1-d 9124/10 CGREEN
Total Kjeidahl N as N in liquid 0.2 72 mgtL as N Lachat107.06-2-H 9124110 CGREEN
NO2+NO3 as N in liquid 0.02 0.02 U mg1L as N Lac10-107-04-1-C 9124110 CGREEN
OCT 0 8 2010
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 {9191 733-3908
For a deIaIed descflp ion of the qua kfier codes refer io DIi;r 1"! rc�1 •5vgh4v�yh s nT_r,n: rcl ns, .i%l P_FtA �111a1 fri_ .r:24a IiifL,(il+, n al_ i.J� s rl y+en(v�gr];rli Inffr In5xi51�
Page 1 of 1

COUNTY: CY6 (c,
RIVER BASIN t WVjJ_£--
REPORT TO : WIRO
SIIIPPED'BY : Courier
COLLECTOR(S) :
Estimated BOD Range:
Seed: Chlorinated:
DIVISION OF WATER QUA -0 F,6m Lab Number :
W❑ SAMPLE TYPE a `f Date Received : /o
PRIORITY Time Received ; t:
AMBIENT QA � STREAfv1 ❑ EFFLUENT Received By
COMPLIANCE CHAIN 0 ' DY LAKE t INFLUENT
®EMERGENCY C SPECIAL STUDY ESTUARY Data Released:
COMPLAINT Visit ID F Date Reported:
Station Location: _I q 1 c�__ROC�,}�. _ N L� `�C Nt
Remarks:
Station # t' '
Date Begin (yy/mm/dd)
Date End (yy/mm/dd) Time Begin
I C_,1 Cg I a;t,
Time End
Value Type - A, H,
Composite- I•, S, 13C
7C
BOD 310 mg/L I
Chloride 940 mg/L
}(
NH3 as N 610 mg/L
Li- Lithium 1132 ug/L
COD High 340 mg/L
Chl a: 70953 µg/L
k
TKN as N 625 mg/L
Mg.- Magnesium 9: mg/L
COD Low 335 mg/L
.
NO2 plus NO3 as N 630 mg/L
Mn- Manganese I pg/L
Conform: MF Fecal 31616 91100 mis
P: Total as P 665 mg/L
Na- Sodium 929 mg/L
Coliform: MF Total 31504 4/100 mis
Color: True 80- C.U.
PO4 as P 70507 mg/L
As- Arsenic:Total ) µg/L
Coliform: Tube Fecal 31615 9/100 mis
Color: (pH ) 83 c.u.
P; Dissolved as P 666 mg/L
Se- Selenium 1147 µg/L.
Coliform: Fecal Strep 31673 9/100 MIS
Color: pH 7.6 82 C.U.
K- Potassium mg/L
1
Hd Mercury 7190t µg/L
Residue: Total 500 mg/L
Cyanide 720 mg/L
Cd- Cadmium 1027 µg/L
Ba- Barium µg/L
Volatile 505 mg/L
Fluoride 951 mg/L
Cr- Chromium:Total 1034 µg/L
Organochlorine Pesticides
Fixed 510 mg/L
Formaldehyde 71880 mg/L
Cu- Copper 1042 µg/L
Organophosphortts Pesticides
Residue: Suspended 530 mg/L
Grease and Oils 556 mg/L
Ni- Nickel 1067 µg/L
jOrgarronitrogen Pesticiedes
Volatile 535 mg/L
Hardness Total 900 mg/L
Pb- Lead 1051 µg/L
Acid Herbicides
Fixed 540 mg/L
Specific Cond. 95 - µmhos/cm2
Zn- Zinc 1092 µg/L
pH 403 units
MBAS 38260 mg/L
V- Vanadium µg/L
Base/Neutral&:Acid Fxtractable Organics
Acidity to pH 4.5 436 mg/L
Phenols 32730 µg/L
Ag- Silver 1077 µg/L
TPH Diesel Range
1
Acidity to pH 8.3 435 mg/L.
Sulfate 945 mg/L
Al- Aluminum 1 105 µg/L
Alkalinity to pH 8.3 415 mg/L
Sulfide 745 mg/L
Be- Beryllium 1012 µg/L
Purgeable Organics (VOA bottle req'd)
Alkalinity to pH 4.5 410 mg/L
Boron: Total 1022 µg/L
Ca- Calcium 916 mg/L
TPH Gasoline Range
TOC 680 mg/L
Tannin & Lignin 32240 µg/L
Co- Cobalt 1037 µg/L
TPH/8TEX Gasoline Range
Turbidity 82079 NTU
Hcxavalent Chromium 1032 µg/L
Fe --Iron 1045 µg/L,
Phytoplankton
Coliform Total Tube 31308 ri/100 mis
COMMENTS
:
LAB USE ONLY
Temperature
on arrival (0Q-
Sample Point % (2)
Conductance (94)
3�3,L �s
Water Temp-C (10)
►
D.O. (300)
o , s� )
pH (400)
y', t c�
8.3 Alkalinity (822
4.5 Alkalinity (431)
4.5 Acidity (82243)
9.3 Acidity (92242)
Secchi depth m
Salinity ppi (480)
Precipit-ln/day (45)
Cloud Cover % (32)
Wind Dir-Deg (36
Sinn Flow Sev (13
i
Turbidity Severity (13
Wind Velocity -mph
Mean Strm Depth-ft (64)

Report to: _WIRO
NC DENIM)WQ Laihoratory
Sample Anomaly Report (SAR)
Ub Number: • AB63864
Station Location: 1919 ROCKY
RUN RD, ,N UT
TO NE CRK
Sample Type: STREAM
Date collected: 9/22/10
Affected Parameter(s)
TURBIDITY
Sample 1D:,
County: ONSLOW
Priority: EMER, COC,
COMPLAINT, KILL
Date received: 9/23/10
Anal ,Oical Area (check onc):
❑ W CI -I ❑ rNI ETA LS
❑NUT ®m1CR0
The following anomalieS occurred (clieck all that apply):
❑Samples
❑improper container used
❑VOA vials with hcadspacc
❑Sulfide samples with headspace
❑Samples not received, but listed on fieldsheet
❑Samples received, but not listed on I ieldsitect
❑A9islabeled as to tests, preservatives, etc.
❑Holding time expired
❑Prior to receipt in lab
❑After receipt in lab
❑histlfliclent quantity for analysis
❑Sample exhibits gross non -homogeneity
❑Sample not chemically preserved properly
0pE-1 out of r:uzge (record 1)1-1):
❑Improper chemical
❑Residual chlorine preseut in s:lmple
❑Color interferencc
❑I Ietivv emulsion formed during extraction
❑Sample bottle broken in lab - no reportable results
Region: WILtMINGTON
Collector: L WILLIS
Date analyzed: 9/23/10
❑VOA ❑SVOA
❑PEST
❑Quality Control
❑Instrument lbiiure — no rcportabic restdls
❑Analyst error— T10 rcporlahle resrlll;
❑Surrogates
❑None added
❑Recovery oulside acceptance limits
❑Spike recovery
[]None added
[]Recovery outside acceptance limits
❑Failed to meet criteria for precision
❑internal standards
❑Blank contamination
❑QC data reported outside of,controls (e.g., QCS, I.CS)
❑Incorrect procedure used
❑SOP intentionally modified xvith QA and Branch l lead
approval
❑Invalid insu-uMena calibration
❑Elevated dctcction limits due to:
❑Insufficient sample volume
®Otltier (specify):The turbidity result exceeded the upper calibration range of -the instrument and should be considered
estimated.
Comments: When an undiluted sample was analyzed, the extremely high turbidity caused interference in the meter, which resulted in
a very low turbidity value to be shown. We did not think this was correct, so dilutions were prepared. When the sample was run under
multiple dilutions, the value continued t10 increase. Dilutions were only carried out until it was clear that the result was above our
calibration range of' 1000 ntu.
Corrective Action:
❑Samples were rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sa311ple(s) 011 hold until:
®Sample reported with qualification. Data qualification code used:J7
❑Other (explain):
Notification lZcquircd7 ❑Yes ❑ No
Person Contacted: Date:
Form completed by: gd-i" �Lj�� �/2,,.Date: 9/24/2010
d Chemist Review (initial):
l 310CHEM K.O
t_1METALS
❑PEST
❑v0A
Branch Mead Review (initial):
QA/QC Itcview (inilicj�e�
q�
�f7
QnlromislLatwr:aorylSn k
❑Sven
Logged into datAase by (initi:d): '"'1.-/ fill -)
i0 23 41Jbs

`n- ' Q 'WO Laboratory .Ycction.
12esul
is
County:
ONSLOW
Sample ID:
AB63865
River Basin
WOK
�0 W Ar QQ
PC Number #
1OW7975
Report To
WIROSP
O G
Date Received:
0912312010
T
I
10
Time Received:
08:20
Collector:
L WILLIS
�_
ti
y
a
Labworks LoginlD
SMATHIS
Region:
WIRO
r
Report Generated:
101SM0
Sample Matrix:
SURFACEWATER
4
Date Reported:
10105/2010
Loc. Type:
RIVERISTREAM
Emergency Yes1No YES
VisitlD
COC Yes/No
YES
Loc. Descr.: S UT ON ROCKY RUN ROAD
Location ID:
WIROSPNLC
Collect Date: 0912217010
Collect Time: 15:00
Sample Depth
CAS #
Analyte Name
LAB
Safnple temperature at receipt by lab
MIC
BOD, 5-Day in liquid
Turbidity
WET
Chemical Oxygen Demand in (quid
NUT
NH3 as N in liquid
POL
Result/
Qualifier
0.8
Units
`C
Method
Reference
Analysis
Date
9123110
Validated by
SMATHIS
2
2 U G8
mg/L
APHA5210B
9123110
MOVERMAN
1
8.1
NTU
APHA2130B-20th
9123/10
MOVERMAN
20
31
mg/L
Hach 80DO
9/24110
MOVERMAN
0.02
0.43
mg/L as N
Lac1O-107-06-1-J
9124110
CGREEN
Total Kjeldahl N as N in iiquid 0.2 1.0 mg/L as N Lachat107-06-2-H 9124/10 CGREEN
NO2+NO3 as N in liquid 0.02 0.02 U mg1L as N LaC10-107-04-1-c 9124110 CGREEN
RECEIVED
OCT 08 2010
sue:
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 19191 733-3908
For a detailed description of She q up ner codes refer to h;N_l1 rtt.„qv ,�,r, orq_hien lL3 nitia,��InJ)e-rhnss dDnJa (1�aelifi C[ris5_:hnr�!'nprt�nryenL erq!wg nyxy;}•�� I�rr"r.,2?y�t�s4 :;{�
Page 1 of 1

COUNTY:
�V15{per
RIVER BASIN:
REPOR C TO :
WIRO
SHIPPED BY:
Courier
COLLECTORS):
Estimated BO➢ Range:
DIVISION OF WATER QUA et
C
y
RM Io �15
W SAMPLE TYPE
PRIORITY
❑ AMBIENT. QA 0 STREAM EFFLUENT
COMPLIANCE CH S Y LAKE INFLUENT
BEMERGENCY C SPECIAL STUDY ESTUARY
COMPLAINT Visit ID�]
Station Location: _ . YY, I'kC i' ",_y—�0�1, t
Lab Number
Date Received
Time Received
Received By:
Data Released:
Date Reported
Seed:
Chlorinated:
Remarks:
`-
Station # I L..W
Date Begin (yy/mm/dd)
End (yy/mm/dd)
Date End
Time Begin
11,11ime End
ValueType-A,H,
Composite-T,S,B
)010CH;�
1bI Dq I �
##, irJOC
SUS
SOD 310 mg/L
Chloride 940
COD High 340 mg/[-
Chl a: 70953
COD Low 335 mg/L
Coliform: MF Fecal 31616 #/100 mis
Coliform: MF Total 31504 #/100 rnls
Color: True 80
Coliform: Tube Fecal 31615 #/100 mis
Color: (pH) 83
Coliform: Fecal Strep 31673 9/100 mis
Color: pH 7.6 82
Residue: Total 500 mg/L
Cyanide 720
Volatile 305 mg/L
Fluoride 951
Fixed 510 mall.
Formaldehyde 71880
Residue: Suspended 530 mg/L
Grease and Oils 556
Volatile 535 mg/L
Hardness Total 900
Fixed 540 mg/L
Specific Cond, 95
pH 403 units
MBAS 38260
Acidity to pH 4.5 436 mg/L
Phenols 32730
Acidity to pH 8.3 435 mg/L
Sulfate 945
Alkalinity to pH 8.3 415 mg/L
Sulfide 745
Alkalinity to pH 4.5 410 mg/L
Boron: Total 1022
TOC 690 mg/L
Tannin & Lignin 32240
x
Turbidity 82079 NTU
Hexavalent Chromium 1032
Coliform Total Tube 31508 #/100 mis
CONINIENTS
:
Sample Point % (2) Conductance (94)
1155
Secchi depth m Salinity ppt (480)
4 1
c.U.
C.U.
c.u. ,
µmhos/cm2
NH3 as N 610
TKN as N 625
NO2 plus NO3 as N 630
P: Total as P 665'
PO4 as P 70507
P: Dissolved as P 666
K- Potassium
Cd- Cadmium 1027
Cr- Chromium:Total 1034
Cu- Copper 1042
Ni- Nickel 1067
Pb- Lead 1051
Zn- Zinc 1092
V- Vanadium
Ag- Silver 1077
Al- Aluminum 1 105
Be- Beryllium 1012
Ca- Calcium 916
Co- Cobalt 1037
Fe- Iron 1045
m
Li- Lithium 1 132 ug/1-
Mg- Magnesium 9: mg/L
Mn-Manganese I µg/L
Na- Sodium 929 mg/L
As- Arsenic:Total I µg/L
Se- Selenium 1 147 µg/L
Hg- Mercury 71901 µg/L
Ba- Barium µg/L
Organochlorine Pesticides
Organophosphorus Pesticides
Organonitrogen Pesticiedes
Acid Herbicides
µg/L
Base/Neutral&Acid Extractable Organics
µg/L
TPH Diesel Range
µg/L
µg/L
Purgeablc Organics {VOA bottle req'd)
mg/L
TPH Gasoline Range
lzg/L
TPH/BTEX Gasoline Range
µg/I-
Phytoplankton
Water Temp-C (I0) D.O. (300) pH (400) 8.3 Alkalinity (822 4.5 Alkalinity(431) 4.5 Acidity(82
Precipit-1n/day (45) Cloud Cover % j2) Wind Dir-Deg (36 Strm Flow Sev (13 Turbidity Severity (13 Wind Velocity.
O (O
LAB USE ONLY
Temperature
on arrival ("Q: D -
8.3 Acidity (82242)
Mean Strm Depth-ft (64)

r
County:
ONSLOW
Sample ID:
AB63865
River Basin
WOK
CF 1NAT�tR
O�
PO Number #
10W7975
Report To
WIROSP
Q�
Date Received:
09/2312010
�
Time Received:
Collector:
L WILLIS
?
p
�v
08:20
Region:
W1RO
r
Labworks LoginlD
SMATHIS
1
Report Generated:
1015/10
Sample Matrix:
SURFACEWATER
1�
Date Reported:
1010512014
Loc. Type:
RIVERISTREAM
Emergency Yes/No
YES
VisitlD
COC Yes/No
YES
Loc. Descr.: S UT ON ROCKY RUN ROAD
Location ID:
WIROSPNLC
Collect Rate: 09/2212010
Collect Time: 15:00
Sample Depth
CAS #
Analyte Name
LAB
Sample temperature at receipt by lab
MIC
BOD, 5-Day in liquid
Turbidity
WET
Chemical Oxygen Demand in liquid
NUT
NH3 as N in liquid
PQL
Result/
Qualifier
0,8
Units
°C
Method
Reference
Analysis
Date
9123110
Validated by
SMATHIS
2
2 U G8
mg/L
APHA52103
9123110
MOVERMAN
1
8,1
NTU
APHA213O6-201h
9123110
MOVERMAN
20
31
mglL
Hach 6000
9124110
MOVERMAN
0.02
0.43
mg/L as N
Lacl0-107-06-1-J
9/24/10
CGREEN
Total K}eldahl N as N in liquid 0.2 1,Q mg/L as N Lachatl07-06-2-H 9/24/10 CGREEN
NO2+NO3 as N in liquid C.02 0.02 U mg/L as N Lacl0-107-04-1-c 9124110 CGREEN
1-011
MIM
NGv 0 8 ZM
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a aetalled dandpllon of the Quahfier copes refer 90 h,J1t„!!��}at _cd L�nien/y��}�hr4tn(finjplt�zhPsgl}IaDp1A C{N1C.5 — t�,(16'L�IS�J.S.�I� � ^�fhh•�,q�l bhlA.K�1 ';r��g;,cis{?,
Page 1 of 1

COUNTY,-'
on• [OcC)
RIVER BASIN:
U y�rty� zr�
REPORT TO.:
WIRO
SHIPPED BY:
Courier
COLLECTOR(S) :
lam} 1 11 cT
Estimated BOD Range:
-
DIVISION OF WATER QUAICJ S F RM
0 SAMPLE TYPE
PRIORITY
AMBIENT QA 1E STREAM EFFLUENT
COMPLIANCE CH PS Y LAKE ❑ INFLUENT
EMERGENCY C SPECIAL STUDY ESTUARY
MCOMPLAINT Visit ID�
Station Location: ;� . LKT 8'Y� t'\ockk_� �.L.. COL
Lab Number:
Date Received : �•
Time Received
Received By
Data Released :
Date Reported
. Seed:
Chlorinated:
Remarks:
Station # L L..i,U
Date Begin (yy/mm/dd)
Date End (yy/mm/dd)
Time Begin
rime End
Value Type - A, 11,
Composite-T, S, B
oR 17�j�,.
## !St✓t,
I I so
BOD 310
COD High 340
COD Low 335
Coliform: MF Fecal 31616
Coliform: MFTotal 31504
Coliform: Tube Fecal 31615
Coliform: Fecal Strep 31673
Residue. Total 500
Volatile 305
Fixed 510
Residue: Suspended 530
Volatile 535
Fixed 540
pH 403
Acidity to pH 4.5 436
Acidity to pH 8.3 435
Alkalinity to pH 8,3 415
Alkalinity to pH 4.3 410
TOC 680
j( Turbidity 82079
Coliform Total Tube 31508
COMMENTS :
mg/L
Chloride 940 mg/L
NH3 as N 610 mg/L
Li- Lithium 1132 ug/L
mg/L
Chl a: 70953 µg/L
),�-
TKN as N 625 mg/L
Mg- Magnesium 9: mg/L
mg/L
X
NO2 plus NO3 as N 630 mgtL
Mn- Manganese I[ µg1L
#/100 mis
P: Total as P 665' mg/L
Na- Sodium 929 mg/L
#/100 mis
Color: True 80 C.U.
PO4 as P 70307 mg/L
As- Arsenic:Total 1 µg/L
#/100 mis
Color: (pH) 83 C.U.
P: Dissolved as P 666 mg/L
Sc- Selenium 1 147 µa/L
#1100 mis
Color: pH 7.6 82 C.U.
K- Potassium mg/L
Hg- Mercury 71901 µg/L
mg/L
Cyanide 720 mg/L
Cd- Cadmium 1027 µg/L
Ba- Barium µg/L
mg/L
Fluoride 951 mgfL'
Cr- Chromium:Total 1034 µg/L
Organochlorine Pesticides
mg/L
Formaldehyde 71880 mg/L
Cu- Copper 1042 µg/L
Organophosphorus Pesticides
mg/L
Grease and Oils 556 mg/L
Ni- Nickel 1067 µg/L
Organonitrogen Pesticiedes
mg/L
Hardness Total 900 mg/L
Ph- Lead 1051 µg/L
Acid Herbicides
mg/L
Specific Cond. 95 µmhos/cm2
Zn- Zinc 1092 µg1L
units
MBAS 38260 mg/L
V- Vanadium µg/L
Base/Neutral&Acid Extractable Organi
mg/L
Phenols 32730 µg/L
Ag- Silver 1077 µg/L
TPH Diesel Range
mg/L
Sulfate 945 mg/L
Al- Aluminum 1105 µg/L
mg/L
Su€fide 745 mg/L
Be- Beryllium 1012 µg/L
Purgeable Organics (VOA bottle req'd)
mg/L
Boron: Total 1022 µg/L
Ca- Calcium 916 mg/L
TPH Gasoline Range
mg/L
Tannin & Lignin 32240 µg/L
Co- Cobalt 1037 µg1L
TPH/BTEX Gasoline Range
NTU
Hexavalent Chromium 1032 µg/L,
Fe- Iron 1045 µg/L
Phytoplankton
4/100 mis
Sample Point % (2) Conductance (94)
!s5 s
Secchi depth m Salinityppt (480)
1 9�
Water Temp-C (10) 1
�_-) �. r
D.O. (300)
,a'aD
pH (400)
( •(c,�
Precipit-In/day (45) -
(0
Cloud Cover % 32)
jO
Wind Dir-Deg
LAB USE ONLY
Temperature
on arrival CC): t
.3 Alkalinity (82214.5 Alkalinity (431) 45 Acidity (82243)13.3 Acidity (82242)
Flow Sev (13[Turbidity Severity (13
Str­m Depth-fr (64)

Report to: —WIRO
NC DENR/DWQ Laboratory
Sample Anomaly Report (SAR)
Lab Number-. AB63865
Station Location: S. UT on Rocky
Run Road
ample Type: stream
Date collected: 9/22/10
Affected Parameter(s):
1101)
Sample 1D: #2LW
County: Onslow Region
Priority: COC/Emergency/com Collector:
plaint
Date received: 9/23/10 Date analyzed:
Analytical Area (check one):
❑WCI-1 ❑METALS
❑NUT NMICRO
The following anomalies occurred (check all that apply):
❑Samples
❑ Improper container used
❑VOA vials with headspace
❑Suiftde samples with headspace
❑Samples not received, but listed on fieldshcet
❑Samples received, but not listed on fieldshect
❑Mislabeled as to tests, preservatives, etc.
❑Flolding time expired
01'rior to receipt in lab
❑After receipt in lab
❑Insufficient quantity for analysis
❑Sample exhibits gross non -homogeneity
❑Sample not chemically preserved properly
❑pl l out of range (record pl-l):
❑Improper chemical
❑Residual chlorine present in sample
❑Color interference
❑i-leavy emulsion formed during extraction
[]Sample bottle broken in lab - no reportable results
❑Other (specify):
White Oak
Linda Willis
9/23/10
❑VOA ❑SVGA
❑PEST
❑Quality Control
❑Instrument failure —no reportable results
❑Analyst error — no reportable results
❑Surrogates
❑None added
[]Recovery outside acceptance limits
❑Spike recovery
❑None added
❑Recovery outside acceptance limits
❑Failed to meet criteria for precision
[]Internal standards
❑Blank contamination
❑QC data reported outside of controls (e.g., QCS, LCS)
❑Incorrect procedure used
❑SOP.intentionally modified with QA and Branch Hcad
approval
❑Invalid instrument calibration
❑Elevated detection limits dirt to:
❑Insufficient sample volume
Comments: 100% sample dilution was not run. Oxygen usage for all the other dilutions was less than 2 mg/L, The reported value is
an Es'nMATED less than value and is calculated for the dilution using the most amount of sample.
Corrective Action:
❑Samples were.rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code used:G8
❑Other (explain):
Notification Required? ❑ Yes ❑ No
Person Contacted: Date: ll
Form completed by: jA. Desa
Lead Chemist Review (initial):
B10CH1,M _ ri
❑METALS
Branch Mead Review (initial):
`QC Review (initial):
QMFormALaboratory�s AR
❑PEST
❑VOA
Date: 1011 /2010
❑SVOA
Logged into database by (initial): Ate
1012310ldbs

r ,
County:
ONSLOW
Sample ID:
A863930-�
River Basin
WOK
QF W A reR
PO Humber #
1OW8040
Report To
Qy
Received:
WIROSP
Date
0912412010
r
Time Received:
08:20
Colkeotor:
L WILLIS
d
Labworks LoginiD
SMATHIS
Region:
WIRO
Report Generated:
1015110
Sample Matrix;
WASTEWATER
Date Reported:
10/0512010
Loc. Type:
EFFLUENT
Emergency Yes/No YES
Visi-dD
COC YeslNo
YES
j
r/yq Jn
jQ , 6Q - 10
Loc. Descr.: 3 DISCHARGE FROM PIT
Location ID:
WIROSPNLC
Collect Date: 0912312010
Collect Time: 14:00
Sample Depth
CAS # Analyte Name POI. Result { Units Method Analysis
Validated by
Qualifier Reference [late
LAB
Sample temperature at receipt by lab 0.6 °C 9124110 SMATHIS
MIC
Turbidity 1 1000 R NTU APHA2130B-20th 9/24110 MOVERMAN
OCT a 8 2010
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27599.1623 t9191 733-3908
F.,. d.l.d dd"csipwoIihe q..Iifer codes re lerta h_tRa�!t'4!.Irl,{ty�j, ,hrn M.hMr_7{�t�'c�ajrir.Ltti.£4hg:jj tjb?.gi�.Rl!AI;rqCc2e3 �hn�;;_,4.":,RlP.!<�S?.n!n�t�`.gM4�!7 i�R;.La�11Z",.5.Lh -gip.!'
Page 1 of 'I

DIVISi o
you
❑ SAMPLE TYPE
COUNTY:
Q rls(c,
PRIORITY
RIVER BASIN:
��vye�e--Gct`C�
AMBIENT QA STREAM
© EFFLUENT
REPORT TO-z
WIRO
COMPLIANCE © CHAIN OF CUSTODY LAKE
INFLUENT
SHIPPED BY:
Courier
EMERGENCY C SPECIAL STUDY ESTUARY
COLLECTOR(S) :',
�t t �,
X COMPLAINT Visit ID�
Estimated BOD Range: Station Location--, I t Sc�tAt
Seed: Chlorinated: Remarks: 3
Station # Elk CW
TDate Begin (yy/mm/dd)
JO� M3
Date End (yy/mm/dd)
IOUC{ ���
Time Begin
## ly0c
f �me End
lgac
Value Type - A, II,
Composite-T, S, B
BOD 310 mg/L
Chloride 940 mg/L
NH3 as N 610 mg/L
Li- Lithium 1132 ug/L
COD High 340 mg/L
Chi a: 70953 µg/L
TKN as N 625 mg/L
Mg- Magnesium 9.' mg/L
COD Low 335 mg/L
NO2 plus NO3 as N 630 mg/L
Mn- Manganese 1 C ug/L
Coliform: MF Fecal 31616 9/100 mis
P•. Total as P 665 mg/L
Na- Sodium 929 mg/L
Coliform: MF Total 31504 4/100 mis
Color: True 80 C.U.
PO-4 as P 70507 mg/L
As- Arsenic:Total 1 µg/L
Coliform: Tube Fecal 31615 #/100 mis
Color: (pH) 83 c.u.
P: Dissolved as P 666 mg/L
Se- Selenium 1147 µg/L
Coliform: Fecal Strep 31673 NI106 mis
Color: pH 7.6 82 C.U.
K- Potassium mg/L
Hg- Mercury 7190( µg/L
Residue: Total 500 mg/L
Cyanide 720 mg/L
Cd- Cadmium 1027 µglL
Ba- Barium µg/L
Volatile 505 mg/L
Fluoride 951 moll.
Cr- Chromium:Total 1034 µg/L
Organochlorine Pesticides
Fixed 510 mg/L
Formaldehyde 71880 mg/L -
Cu- Copper 1042 µg/L
Organophosphorus Pesticides
Residue: Suspended 530 mg/L
Grease and Oils 556 mg/L
Ni- Nickel 1067 µg/L
OrganonitTogen Pesticiedes
Volatile 535 mg/L
Hardness Total 900 mg/L
Pb- Lead 1051 µg/L
Acid Herhicides
Fixed 540 mg/L
Specific Cond. 95 µmhos/cm2
Zn- Zinc 1092 µg/L
pH 403 - units
MBAS 38260 mg/L
V- Vanadium µg/L
Base/Neutral&Acid Extractable Organics
Acidity to pH 4.5 436 mg/L
Phenols 32730 µg/L
Ag- Silver 1077 µg/L
TPH Diesel Range
Acidity to pH 8.3 435 mg/L
Sulfate 945 mg/L
Al- Aluminum 1 t05 µg/L
Alkalinity to pH 8.3 415 mg/l,
Sulfide 745 mg/L
Be- Beryllium 1012 µg/L
Purgeable Organics (VOA bottle req'd)
Alkalinity to pH 4.5 410 mg/L
Boron: Total 1022 µg/L
Ca- Calcium 916 mWL
TPH Gasoline Range
TOC 680 mg/L
Tannin & Lignin 32240 ug/L
Co- Cobalt 1037 µWL.
TPH/BTEX Gasoline Range
Turbidity 82079 NTU
Hexavalent Chromium 1032 µg/l-
Fe- Iron 1045 µg/L
Phytoplankton
Conform Total Tube 31508 9/I00 MIS
COMMENTS
: _
LAB USE ONLY
Temperature
on arrival (°C):
_ _
Sample Point % (2)
Conductance (94)
99,StuS
Water Temp-C (10)
D.O. (300)
pH (400)
8.3 Alkalinity (822
4.5 Alkalinity (431)
4.5 Acidity (82243)
8.3 Acidity (82242)
Secchi depth m r
Salinity ppt (480)
Q
Precipit-ln/day (45)
O
Cloud Cover % (32)
Wind Dir-Deg (36
Strm Flow Sev (13
ySeverity (13
Turbidity
CYYI
Wind Velociry-mph
Mean Strm Depth-ft (64)

-M:DWO faborator'v.Section
Wesults
County:
ONSLOW
Sample ID:
A663038
V1A-r
River Bas1n
WOK
�O R�
PO Number #
10W8040
Report To
WIROSP
O G
Date Received:
09i2412010
Ui
>_
r
Time Received:
08:20
Collector:
L WILLIS
_I
O Y
Labwor" LoginlD
SMATHIS
Region:
WiRO
Report Generated:
1015110
Sample Matrix:
WASTEWATER
Dale Reported:
10105/2010
Loc. Type:
EFFLUENT
Emergency Yes/No
YES
VisidD
COC Yes/No
YES
.yyt�n
�Q 62' It?
Loc. Descr.: 3 DISCHARGE FROM PIT
Location ID:
WIROSPNLC
Collect Date: 0912312010
Collect Time; 14:00
Sample Depth
CAS # Analyte Name PQL Result/ Units
Qualifier
LAB
Sample temperature at receipt by lab 0.6 °C
MIc
Turbidity 1 1000 R NTU
1
Method Analysis Validated by
Reference Date
9I24110 SMATHIS
APHA2130B•201h 9124110 MOVERMAN
OPT
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 19191 733.3908
Fora dela clad description olthe qualifier codes relertc!L11i1g,:C.6 r-c5t�r7 r�,y vehl4jglah-inft',I trtle�hn .Ihf S.1.?1 k..S�jrd!irlir_C nd p; '�(fin„Y�rrt3l,pr�4s�nr,nr?�!y±�;htY{q.R?I.,'si-�,tfnfiR,;rq}�y�i.:;�
Page 1 of 1
k.

DIVISI O C
W❑
101�
RM SAMPLE TYPE
COUNTY: flst.y PRIORITY
RIVER BASIN: F7 AMBIENT F7 QA F —] STREAM ©£FFLiJENT
REPORT TO : W1RO COMPLIANCE © CHAIN OF CUSTODY F� LAKE ❑ INFLUENT
SHIPPED BY: Courier 7 EMERGENCY C SPECIAL STUDY ESTUARY
COLLECiOR(S) : t '� �l It - L. eCOMPLAINT Visit ID�El
Estimated SOD Range:
Station Location` Scum ('ice
Seed: Chlorinated:
Remarks:
Station # L4VrU, -W
Date Begin (yylmm/dd)
Date End (yylmm/dd949
Time Begin
Time End
Value Type - A, 11,
Composite-T, S, B
3
rod
Oct ��3
0
BOD 310
mg/L
Chloride 940
mg/L.
NH3 as N 610
mg/L
Li- Lithium 1 132 ug/L
COD High 340
mg/L
Chi a: 70953
µ g/L
TKN as N 625
mg/L
Mg- Magnesium 9: mg/L
COD Low 335
mg/L
NO2 plus NO3 as N 630 mg/L
Mn- Manganese 1C µg/L
Colifonn: MF Fecal 31616
4/100 mis
R Total as P 665
mg/L
Na- Sodium 929 mgtL
Coliform: MF Total 31504
#/100 MIS
Color: True 80
C.U.
PO4 as P 70507
mg/L
As- Arsenic -.Total I µglL
Coliform: Tube Fecal 31615
0100 mis
Color: (pH) 83
C.U.
P: Dissolved as P 666
mg/L
Se- Selenium 1 147 µg/L
Coliform: Fecal Strep 31673
4/100 MIS
Color: pH 7.6 82
c.u,
K- Potassium
mg/L
Hg- Mercury 7190( µg/L
Residue: Total 500
mg/L.
Cyanide 720
mg/L
Cd- Cadmium 1027
µgfL
Ba- Barium µg/L
Volatile 505
mg/L
Fluoride 951
mg/L
Cr- Chromium:Total 1034 µg/L
Organochlorine Pesticides
Fixed 510
mg/L
Formaldehyde 71890
mg/L
Co- Copper 1042
µg/L
Organophosphorus Pesticides
Residue: Suspended 530
mg/L
Grease and Oils 556
mg/L
Ni-Nickel 1067
µg/L
Organonitrogen Pesticiedes
Volatile 535
mg/L
Hardness Total 900
mg/L
Pb-Lead 1051
µg/L
Acid Herbicides j
Fixed 540
mg/L
Specific Cond. 95
µmhos/cm2
Zn- Zinc 1092
µg/L
pH 403
units
MBAS 38260
mg/L
V- Vanadium
µg/L
BaseNeutral&Acid Extractable Organics
Acidity to pH 4.5 436
mg/L
Phenols 32730
µg/L
Ag- Silver 1077
µg/L
TPH Diesel Range
Acidity to pH 8.3 435
mg/L
Sulfate 945
mg/L
Al- Aluminum 1105
µg/L
Alkalinity to pH 8.3 415
mg/L
Sulfide 745
mg/L
Be- Beryllium 1012
µg/L
Purgeable Organics (VOA bottle req'd)
Alkalinity to pH 4.5 410
mg/L
Boron: Total 1022
µg/L
Ca- Calcium 916
mg/L
-TPH Gasoline Range
TOC 680
mg/L
Tannin & Lignin 32240
µWL
Co- Cobalt 1037
µg/L
TPH/BTEX Gasoline Range
Turbidity 82079
NTU
Hexavalent Chromium 1032
µg/L
Fe- Iron 1045
µg/L
Phytoplankton
Coliform Total Tube 31508
#I100 MIS
COMMENTS:
LAB USE ONLY
Temperature S „
°C): lIG
on arrival
Sample Point % (2)
Conductance (94)
Wager Te (10)
D.O. (3.010)
pHar(400)
8.3 Alkalinity (822
4.5 Alkalinity (431)
4.5 Acidity (82243)
8.3 Acidity(82242)
9q• 5 l.-,J
=mpr-C
G�. • T - C-
. �1-
�l e c>T
Secchi depth rn
Saliniryppt (480)
Precipit-ln/day (45)
Cloud Cover % (32)
Wind Dir-Deg (36
Strm Flow Sev (13
Turbidity Severity (13 Wind Velocity -mph
Mean Strm Depth-ft (64)
0
EEC 4 t �rn e.

Report to: _WIRO
Lab Number:
Station Location:
,ample Type:
Date collected: 9/23/10
Affected Parameter(s):
NC DENR/DWQ Laboratory
Sample Anomaly Report (SAR)
AB63938 Sample ID
Discharge from pit County: Onslow
Effluent
Turbid
station # 3
Region: White Oak
Priority: COC/ Emergency Collector:
Date received: 9/24/10 Date analyzed
Analytical Area (check one):
❑ WCH ❑METALS
❑NUT ®MICRO
The following anomalies occurred (check all that apply):
❑Samples
❑ Improper container used
❑VOA vials with headspace
❑Sulfidc samples with headspace
❑Samples not received, but listed on fieldsheet
❑Sainples received, but not listed on fieldsheet
❑Mislabeled as to tests, preservatives, etc.
❑I folding time expired
❑Prior to receipt in lab
❑After receipt in lab
❑Insufficient quantity for analysis
[]Sample exhibits gross non-honiogencity
❑Sample not chemically preserved properly
❑pl-I out of range (record pfl):
❑Improper chemical
❑Residual chlorine present in sample
❑Color interference
❑Heavy emulsion formed.during extraction
❑Samp€e bottle broken in lab - no reportable results
t5dOtber (specify): See LomYA c'Xt-
L.Willis
9/24/10
❑VOA ❑SVGA
❑PEST
❑Quality Control
❑Instrument failure— no reportable results
❑Analyst error — no reportable results
❑Surrogates
❑None added
❑Recovery outside acceptance limits
❑Spike recovery
❑None added
❑Recovery outside acceptance limits
❑Failed to meet criteria for precision
❑Internal standards
❑Blank contamination
❑QC data reported outside of controls (e.g., QCS, LCS)
❑Incorrect procedure used
❑SOP intentionally modified with QA and Branch I lead
approval
❑Invalid instrument calibration
❑Llevated detection limits due to:
❑Insufficient sample volume
Comments: This sample exceeded the upper calibration range of 1000 NTU. The reported value should be considered estimated.A
Corrective Action:
❑Samples were rejected by DWQ Lab. Authorizcd by: Date:
❑Accepted and analyzed after notifying the collector or contaci person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code.used:.i7
❑Other (explain):
Notification Required? ❑ Yes ❑ No
Person Contacted: Date: _
Form completed by:
Lead Chemist Review (initial)
DDIOCHEM _ty.2 ❑E'CS'I
[]METALS ❑VOA
Branch l lead Review (initial):
QA/QC Review (initial):
) mslLabomrory\SAR '
Date: 9/24/2010
❑SVOA
Logged into database by (initial): 1017h o
10123101dbs

r
County:
ONSLow
Sample ID:
A663939 '
�1A iF
River Basin
WOK
F
O R
pG
PO Number q
10WS041
Report To
WIROSP
�O�
Date Received:
0912412010
j
Time Received:
08:20
CaUeclor.
L WILLIS
1 z
Labwarks LoginlD
SMATHIS
Region:
WIRD
Report Generated:
1015110
Sample Matrix:
WASTEWATER
Date Reported:
10105/2010
Loc. Type:
EFFLUENT
Emergency Yes/No YES
VisitlD
COC Yes/No
YES'
' C) , / _ ° I 0
Loc. Descr-: 4 Cn� OVERFLOW STRUCTURE
i�
Location ID:
WIROSPNLC
Collect Dale. 0912312010
Collect Time: 14:15
Sample Depth
CAS 4 AnalAnal t�Na_me PQL Units
Result! Method Analysis Validated by
Qualifier Reference Date
LAB
Sample temperature at receipt by lab 0.6 °C 9/24/10 SMATHIS
MIC
Turbidity 1 1000 J7 NTU APHA213013-20th 9/24110 MOVERMAN
RECEIVER
OCT 0 S 2010
-------------
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a Jetaded dear bhon of the 9uaiificr cod- rOL, In ,,^.14r! r F' dl { r. AR?.6 :"fxi8t}--'nhl ��4LLCSLFlz itif.?.C2?!.;.?_4S3_� tLC-; _s .Ctn�1" n�1_r,�t� n� C�'15r;hkyl:i:'h P!F!1.r.,1.,
Page 1 of 1

COUNTY:�'�
RIVER BASIN
REPORT T3 :
WiRO
SHIPPED BY:
Courier
COLLFCTOR(S):
CjLroJ; L4tt�r�
Estimated BOD Range:
Seed:
Chlorinated:
DIVISION OF WATER QUAL Cooatj} 5 4(
W❑ SAMPLE TYPE
PRIORITY
AMBIENT' QA El STREAM ® EFFLUENT
El COMPLIANCE CHAIN OF CiISTODY LAKE INFLUENT
EMERGENCY C SPECIAL STUD � ESTUARY Iq
FZICOMPLAINT Visit ID
Lah Number : ✓ M
Date Received: • .2 4• , J
Time Received :'.
Received By
Data Released: {
Date Reported : jl
Station Location: 4 COD C7C?�A�t�t�.. �� C [���_j�5� n +
Remarl:s��tk
Station # •-L4Vert0-L)
Date Begin (yy/mm/dd)
1a /C57
Date End (yy/mm/dd)
a
Time Begin
I##
Time End
Value Type - A, 11,
Composite=£, S, B
BOD 310 mg/L
Chloride 940 mg/L
NH3 as N 610 mg/L
Li- Lithium 1132 ug/L
COD High 340 mg/L
Chl a: 70953 µg/L.
TKN as N 625 mg/L
Mg- Magnesium 9. mg/L
COD Low 335 mg/L
NO2 plus NO3 as N 630 mg/L
Mn- Manganese 1 C µg/L
Colifonn: MF Fecal 31616 #/to0 MIS
P: Total as P 665- mg/L
Na- Sodium 929 mg/L
Cohform: MF Total 31504 #/100 MIS
Color: True 80 C.U.
PO4 as P 70507 mg/L
As- Arsenic -,Total 1 µg/L
Coliform: Tube Fecal 31615 #/100 mis
Color: (pH) 83 C.U.
P: Dissolved as P 666 mg/L.'
Se- Selenium 1147 Jtg/I_
Coliform: Fecal Strep 31673 0/100 MIS
Color: pH 7.6 82 C.U.
K- Potassium mg/L
Hg- Mercury 7190t µg/L,
Residue: Total 500 mg/L
Cyanide 720 mg/L
Cd- Cadmium 1027 µg/L
Ba- Barium µg/L
Volatile 505 mg/L
Fluoride 951 mg/L
Cr- Chromium:Total 1034 µg/I
Organochlorine Pesticides
Fixed 510 mg/L
Formaldehyde 71890 mg/L
Cu- Copper 1042 µg/L
Organophosphorus Pesticides
Residue: Suspended 530 mg/L
Grease and Oils 556 mg/L
Ni- Nickel 1067 µg/L
Organonitrogen Pesticiedes
Volatile 535 mg/L
Hardness Total 900 mg/L
Pb- Lead 1051 µg/L
Acid Herbicides
Fixed 540 mg/L
Specific Cond. 95 µmhos/cm2
Zn- Zinc 1092 ug/L
pH 403 units
MBAS 38260 mg/L
V- Vanadium µWL
Base/Neutral&Acid Extractable Organics
Acidity to pH 4.5 436 mg/L
Phenois 32730 µg/l,
Ag- Silver 1077 µg/L
TPH Diesel Range
j
Acidity to pH 8.3'435 mg/L
Sulfate 945 mg/L
Al- Aluminum 1105 µg/L
F
Alkalinity to pH 8.3 415 mg/L
Sulfide 745 mg/L
Be- Beryllium 1012 µg/L
Purgeable Organics (VOA bottle req'd)
i
Alkalinity to pH 4.5 410 mg/L
Boron: Total 1022 ug/L
Ca- Calcium 916 , mg/L
TPH Gasoline Range
TOC 680 mg/i.
Tannin & Lignin 32240 µg/L
Co- Cobalt 1037 µg1L
TPH/BTEX Gasoline Range
Turbidity 82079 NTU
Hexavalent Chromium 1032 µg/L
Fe- Iron 1045 µg/L
Phytoplankton
Coliform Total Tube 31508 41100 mis
COMMENTS
:
LAB USE ONLY
Temperature
on arrival (°C):
Sample Point % (2)
Conductance (94) 1
Water Temp-C (10)
D.O. (300)
pli (400)
8.3 Alkalinity (922
4.5 Alkalinity (431)
4.5 Acidity (82243)
8.3 Acidity (82242)
Secchi depth m
Salinity ppt (480)
Precipit-1n/day (45)
Cloud Cover % (32)
Wind Dir-Deg (36
Strm Flow Sev (13
Turbidity Severity ( 13
r--7y:�rn c�_
Wind Velocity -mph
Mean Strm Depth-ft (64)

County:
ONSLOW
Sample 10:
AB63939
River Basin
WOK
pF %t'1Arfi4
PO Number #
1OW8041
QG
Report To
WIROSP
Date Received:
09/2412010
_a=
Time Received:
08:20
collector.
L WILLIS
Labworks LoginlD
SMATHIS
Region:
VVIRO
Report Generated!
106110
Sample Matrix:
WASTEWATER
Date Reported:
10105/2D10
Lon,Type:
EFFLUENT
Emergency Yes1No YES
VisitlD
,
COC Yes/No
YES -
.yylJjl
1 l_. t o
Loc.I]escr.: 4 AOVERFLOW STRUCTURE
r °7UW
lfJ
Location 1D:
WIROSPNI.0
Collect Date: 0912312010
Cllect T oime; 14:15
Sample Oepth
CAS # Anal t�.e. Name PQL Result/ Units Method Analysis Validated by
Qualifier Reference Date
LAB
Sample temperature at receipt by lab 0.6 °C 9124110 SMATHIS
M!C
Turbidity 1 1000 R NTU APHA21308-20th 9/24/10 MOVERMAN
r � Q � ti010
N0�
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 1919) 733-3908
For Geraaed tlescnPlbn of the 9ueOer co6es wfer to b11i�;lP `S!L_t.Li4;.•� nJMr,nr'. .a }rr;grAj}:eYfSPY is E};'Y rs, ;� �u_IY�� 1.4aJn,_;iarnl nrdEW��i wztylye,.t7i ,t�gnh.'•.:'.478Y5Si4_'
Page 1 of 1

DIVISION OF WATER QUAL
—0 SAMPLE TYPE
COUNTY: �� PRIOR H-1' row-
RIVERRiiS[N: tL_ AMBIENT QA STREAM EFFLUENT
REPORT TO: W1R0 COMPLIANCE CHAIN OF CUSTODY LAKE DINFLUENT
SHIPPED BY: Courier EMERGENCY C SPECIAL STUDY El ESTUARY
COLLECTORS): L& i`s,' [fat COMPLAINT Visit ID
Lab Number:
Date Received: 2g• ,
Time Received: z_
Received By
Estimated SOD Range-. Station Location:
Seed: Chlorinated: Remarks;-,L,�
Station #-�t``f'rl#-
Date Begin-(yy/mm/dd)
Date End (yy/mm/dd)
Time Begin
Time End
14- IS—
Value Type - A, H,
Composite-T, S, B
BOD 310 mg/L
Chloride 940 mg/L
JNH3asN610
mg/L
Li= Lithium 1132 ug/L
COD High 340 mg/L
Chl a; 70953 ltg/L
TKN as N 625 mg/L
Mg- Magnesium 9. mg/L
COD Low 335 mg/L
NO2 plus NO3 as N 630 mg/L
Mn- Manganese I µg/L
Coliform: MF Fecal 31616 #/100 MIS
P: Total as P 665 - mg/L
Na- Sodium 929 mg/L
Coliform; MF Total 31504 #1100 mks
Color: True 80 C.U.
PO4 as P 70507 mg/L
As- Arsenic:Total l µg/L
Coliform: Tube Feca! 31615 #/100 mis
Color: (pH ) 83 C.U.
P'. Dissolved as 11666 mg/L
Se- Selenium 1147 µg/L
Coliform: Fecal Strep 31673 9/100 MIS
Color: pH 7.6 82 c_u.
K- Potassium mg/L
Hg- Mercury 71901 µg/L
Residue: Total 500 mg/L
Cyanide 720 mg/L
Cd- Cadmium 1027 µg/L
Ba- Barium µg/L
Volatile 505 mg/L
Fluoride 951 mg/L
j Cr• Chromium:Total 1034 µg/L
Organochlorine Pesticides
Fixed 510 mglL
Formaldehyde 71890 m tL
Cu- Copper 1042 µg/L
Organophosphorus Pesticides
Residue: Suspended 530 mg/L
Grease and Oils 556 mg/L
Ni- Nickel 1067 µg/L
Organonitrogen Pesticiedes
Volatile 535 mg/L
Hardness Total 900 mg/L
Pb- Lead 1051 µg/L
Acid Herbicides
Fixed 540 mg/L
Specific Cond. 95 µmhos/cm2
Zn- Zinc 1092 µg/L
pH 403 units
MBAS 38260 mg/I.
V- Vanadium µg/L
Base/Neutral&Acid Extractable Organics
Acidity to pH 4.5 436 mg/L
Phenols 32730 µg/L
Ag- Silver 1077 µg/L
TPH Diesel Range
Acidity to pH 8.3 435 mg/L
Sulfate 945 mg/L
Al- Aluminum 1105 µg/L
j
Alkalinity to pH 8.3 415 mg/L
Sulfide 745 mg/L
Be- Beryllium 1012 µg/L
Purgeable Organics (VOA bottle req'd)
Alkalinity to pH 4.5 410 mg/L
Boron: Total 1022 µg/L
Ca- Calcium 916 mg/L
TPH Gasoline Range
TOC 680 mg/L
Tannin &: Lignin 32240 µg/L
Co- Cobalt 1037 AWL
TPH/BTE•X Gasoline Range
Turbidity 82079 NTU
Hexavalen[ Chromium 1032 µg/L
Fe- Iron 1045 µglL
Phytoplankton
Coliform Total Tube 31508 4/100 mis
COMMENTS:
Temperature
an
LAB USE ONLY
arrival (°C): D • `-rC i
_
Sample Point % (2)
Conductance (94)
Water Temp-C (10)
D.O. (300)
pH (400)
9.3 Alkalinity (822
4.5 Alkalinity (431)
4.5 Acidity (92243)
8.3 Acidity (82242)
Seechi depth m
Salinity ppt (490)
Precipit-in/day (45)
Cloud Cover % (32)
Wind Dir-Deg (36
Starr Flow Sev (13
Turbidity Severity (13
l✓`��YYI 'E�
Wind Velocity -mph
Mean Strm Depth-ft (64)

Report to: —WIRO
Lab Number:
Station Location:
sample Type:
Date collected:
NC DENWDWQ Laboratory
Sample Anomaly Report (SAR)
A1363939 Sample ID:
@ overflow County: Onslow
structure
Effluent
9/23/10
Affected Parameter(s): Turbidity
station # 4
Region
Priority: COG Emergency Collector:
Date received: 9/24/10 Date analyzed
Analytical Area (check one):
❑ WCI-I ❑mE,rALS
❑NU1' ®MICRO
The following anomalies occurred (check all that apply):
❑Samples
❑lmproper container used
❑VOA vials with lieadspace
❑Sulfide samples with headspace
❑Samples not received, but listed on fieldsheet
❑Samples received, but not listed on fieldshect
❑Mislabeled as to tests, preservatives, etc.
❑Holding time expired
❑Prior to receipt in lab
❑After receipt in lab
❑Insufficient quantity for analysis
❑Sainple exhibits gross non -homogeneity
❑Sample not chemically preserved properly
❑pl-I out of range (record pl-1):
❑Improper chemical
❑Residual chlorine present in sample
❑Color interference
❑Ideavy emulsion formed during extraction
❑Sample bottle broken in lab - no reportable results
❑Other (specify):
White Oak
L.Willis
9124/ 10
❑ VOA ❑SVGA
❑PL'-Sf
❑Quality Control
❑Instrument failure — no reportable results
❑Analyst error — no reportable results
❑Surrogates
❑None added
❑Recovery outside acceptance limits
❑Spike recovery
[]None added
❑1ecovery outside acceptance limits
Ell -ailed to meet criteria for precision
❑]nternal standards
❑Blank contamination
❑QC data reported outside of controls (e.g., QCS, LCS)
❑Incorrect procedure used
❑SOP intentionally modified with QA and Branch Head
approval
❑Invalid instrument calibration
❑Elevated detection limits due to:
❑Insufficient sample volume
Comments: This sample exceeded the upper calibration range of 1000 NTU. The reported value should be considered estimated.A
Corrective Action:
❑Samples were rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code used:J7
❑Other (explain):
Notification Required? ❑ Yes ❑ No
Person Contacted: Date: I _
Form completed by:
Lead Chemist Review (initial):
WBIOCHEM _kD ❑PEST_
❑METALS ❑VOA
BranchIdcadReview(initial) ,t_�%�7/41
QA/QC Review (initial):
)rms11-aboratory�S nR
Date: 9/24/2010
❑SVGA
I-ogged into database by (initial): IilI7%/J
10+2710tdbs

err n"W7 La-bowtorv.Section.
12es2 lts
_
County:
ONSLOW
Sample ID:
A863940
River Basin
WOK
pF WAlf
PO Number d
1OW8042
pGy
Dale Received:
0912412010
Report To
WIROSP
`Q=
�?
Time Received:
08:24
Collector.
L WILLIS
Labworks LoginlD
SMATHIS
Region:
WIRO
Report Generated:
10l5110
Sample Matrix:
WASTEWATER
Date Reported:
_ 10/05/2010
Loc. Type:
EFFLUENT
Emergency Yes/No YES
VlsillD
/
(Q f
COG YeSINo
YES
Loc. ❑escr.: S DISCHARGE INTO UT TO NE CREEK
Location DD:
WIROSPNLG
Collect Date: D912312010
Collect Time: 14:21
Sample depth
ResulY
Method
Analysis
GAS #
Analyte Name PQL
Units
Validated by
-
Qualifier
Reference
Date
LAB
Sample temperature at receipt by lab
0.6
°G
9/24110
SMATHIS
MIC
Turbidity 1
1000 J7
NTU APHA213013-20th
9/24110
MOVERMAN ,
WET
Chemical Oxygen Demand in liquid 20
36
mg1L Hach 8000
9124110
MOVERMAN
r
OCT 08 2010
Laboratory Section>> 1623 Mai! Service Center, Raleigh, NC 27699.1623 [phone]
For a detailed descripllon of the Wlifiier codes refer to Mlry1r2dml - '1S' �3r?h,t.i�1S4�.1C5h9.`:t)PAKIaIpren,%Lav&.!!i ma -A !S.n, Y�q.11p-In_Ailri!, rMprhm5.1:��'.
Page 1 of 1

COUNTY:
RIVER BASIN
REPORYTO : WIRO
SHIPPED BY: Courier
COLLECTORS):
Estimated ROD Range:
Seed: Chlorinated:
darah
DIVXMOK I 'f L FORM
�pU,jOt
W� SAMPLE TYPE
PRIORITY
AMBIENT QA
STREAM
❑ EFFLUENT
COMPLIANCE CHAIN OF CUSTODY
LAKE
INFLUENT
eEMERGENCY
C SPECLaL STUDY
COMPLAINT Visit ID�
ESTUARY
Station Location:
C�s�C rY � LA�tta �•{ .'4-C, k{�rit
Remarks:
Lab Number :
Date Received:
Time Received:
Received By:
Data Released
Date Reported
Station # htVer>; Lw Date Begin (yylmm/dd)
5 I'Dl�q i-D3
Date End (yy/min/dd)
lajo fa
Time Begin
I'A z-
1-ime End
Value Type- A, Ii,
Composite-T, S, B
BOD 310 mg/L
Chloride 940 mg/L
NH3 as N 610 mg/L
Li- Lithium 1132 ug/L
COD High 340 mg/L
Chl a: 70953 µel
TKN as N 625 mg/L
Mg- Magnesium 9: mg/L
COD Low 335 mgfl_
NO2 plus NO3 as N 630 mg/L
Mn- Manganese 1C µg/L
Coliform: MF Fecal 31616 #/100 MIS
P: Total as P 665 mg/L
Na- Sodium 929 mg/L,
Coliform: MF Total 31504 #/100 mis
Color: True 80 C.U.
PO4 as P 70507 mg/L
As- Arsenic.Total 1 µg/L
Coliform: Tube Fecal 31615 4/100 mis
Color: (pH) 83 C.U.
P: Dissolved as P 666 mg/L
Se- Se€enium 1 147 µg/L
Coliforrw Fecal Strep 31673 2/100 mis
Color: pH 7.6 82 C.U.
K- Potassium mg/L
Hg- Mercury 71901 µg/L
Residue: Total 500 mg/L
Cyanide 720 mg/L
Cd- Cadmium 1027 µg/L
Ra- Barium µg/L
Volatile 505 mg/L
Fluoride 951 mgfL
Cr- Chromium:Total 1034- µg/L
Organochlorine Pesticides
Fixed 510 mg/L
Formaldehyde 71880 mg/L -
Cu- Copper 1042 µg/L
Organophosphorus Pesticides
Residue: Suspended 530 mg/L
Grease and Oils 556 mg/L
Ni- Nickel 1067 µg/L
Organonitrogcn Pesticiedes
Volatile 535 mg/L
Hardness Total 900 mgJL
Pb- Lead 1051 µg/L
Acid Herbicides
Fixed 540 mg/L
Specific Cond. 95 µmhos/cm2
Zn- Zinc 1092 Pg/L
pH 403 units
MBAS 38260 mg/L
V- Vanadium µg/L
Base/Neutral&Acid Extractable Organics
Acidity to pH 4.5 436 mg/L
Phenols 32730 µg/L
Ag- Silver 1077 µg/L.
TPH Diesel Range
j
Acidity to pH 8.3 435 mg/L.
Sulfate 945 mg/L.
Al- Aluminum 1 105 µg/L
Alkalinity to pH 8.3 415 mg/L
Sulfide 745 mg/L
Be- Beryllium 1012 µg/L
Purgeable Organics (VOA bottle req'd)
'
Alkalinity to pH 4.5 410 mg/L
Boron: Total 1022 µg/L
Ca- Calcium 916 mg/L
TPH Gasoline Range
TOC 680 mg/L
Tannin & Lignin 32240 µg/L
Co- Cobalt 1037 µg/L.
TPH/RTEX Gasoline Range
Turbidity 92079 NTU
Hexavalent Chromium 1032 µplL d
Fe- Iron 1045 µg/L
Phymplankton
Coliform Total Tube 31508 9/100 Ms
COMMENTS
:
LAB USE ONLY
Temperature
on arrival ('Q: �`
Sample Point % (2)
Conductance (94)
Wat__err�JJTemp-C (10)
D.O. (300)
0
pH (400)
3 d 1�
8.3 Alkalinity (822
4.5 Alkalinity (431)
4.5 Acidity (82243)
8.3 Acidity(82242)
Secchi depth m
Salinity ppt (480)
Precipit-In/day (45)
Cloud Cover % (32)
Wind Dir-De.(36
Stan Flow Sev (13
Turbidity Severity (13
Wind Velocity -mph
Mean Stint Depth-ft (64)

_ •..
�Nt" nIWO Laboratory .Section (Results
County:
ONSLOW
Sample fD:
AB63940 +
River Basin
WOK
VJA7�
D R
PO Number
1OW8042
t
Q�
Report To
WiROSP
0
Ui
Date Received;
Time Received;
09/24/2010
08:20
Collector:
L WILLIS
<
Labworks LoginTD
SMATHIS
Region:
WIRO
Report Generated:
1015110
Sample Matrix:
WASTEWATER
Gate Reported:
1010512010
Loc. Type:
EFFLUENT
Emergency YeslNo
YES
VisitlD
/
—14 iQ I
CDC Yes/No
YES
Loc. Deser.: 5 DISCHARGE INTO UT TO NE CREEK
Location ID:
WIROSPNLC
Collect Date: 0912312010 Collect Time: 14:21
Sample Depth
Result/
Method Analysis
CAS #
Anatyte Name POL
Uni ts Validated by
Qualifier
Reference Date
LAB
Sample temperature at receipt by lab
0.6
C 9124110 SMATHIS
MlC
Turbidity 1
1000 H NTU APHA213013-20th 9/24110 MOVERMAN
wEY
Chemical Oxygen Demand in liquid 2.0
— —
36
__ -
mglL Hach 8000 9r24110 MCVERMAN
_—„ z_-
�..
� - _,.�-' SLY,:.•:.._
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a dMailed desc plicn of the qualifier codes rercr to ittr�,��1'yll�l.ngSit'7r �fg:}..P�7:'�rr'n�n Kta!(.�.f2nY4h.�-i�i iA57P.1_d 45ieli d_.s�.LrBP$-1. r f�f'.46aIurQ. GS :4ieh!�! $7 tA."n l��l��'�n_}.is:�
Page 1 of 1

DIV 1 L FORM
low?0�'�
Lab Number:
D
"PRIORITY
SAMPLE TYPE
Date Received :
_ Z . !
COUNTY :-#ots�
RIVER BASIN' .
F7AMBIENT QA
STREAM E EFFLUENT
Time Received
Received By:
REPORT TO :
WIRO
COMPLIANCE CHAIN OF CUSTODY
❑ LAKE INFLUENT
SHIPPED BY:
Courier
EMERGENCY C SPECLIL STUDY
®COMPLAINT
El ESTUARY
11
FL
Data Released
COL,I.ECTOR(S) :
I,_g ( t S Li6J-1--
Visit ID�
Date Reported:
Estimated BOD Range:
Station Location: E Ai5C-t'LCR QkA—U u • 1 • +C,
Seed:
Chlorinated:
Remarks:Aa
Station # 4A*erk'
_tZ
Date Begin (yylmm/dd)
Date End (yy/mm/dd)
Time Begin
Time End
Value Type -A, H,
Composite=f, S, B
5
�3)3
�
## ly._(
1y�1
BOD 310 mg/L
Chloride 940 mg/L
NH3 as N 610 mg/L
Li- Lithium 1132 ug/L
COD High 340 - mg/L
Chl a: 70953 µg/L
TKN as N 625 mgfL
Mg- Magnesium 9: mg/L
COD Low 335 mg/L
NO2 plus NO3 as N 630 mg/L
Mn- Manganese 1C µg/L.
Coliform: MF Fecal 31616 #/100 mis
P: Total as P 665 mg/L
Na- Sodium 929 mg[L
Coliform: MF Total 31504 9/100 MIS
Color: True 80 c.u.
PO4 as P 70507 mg/L
As- Arsenic:Total I µg/L
Coliform: Tube Fecal 31615 41100 mis
Color: (pH ) 83 c.u.
P: Dissolved as P 666 mgA.
Se- Selenium 1147 µg/L
Coliform; Fecal Strep 31673 41100 mis
1
Color: pH 7.6 82 cos.
K- Potassium mg/L
Hg- Mercury 7190( µg/L
Residue: Total 500 Mel,
Cyanide 720 mg/L
Cd- Cadmium 1027 µg/L
Ba- Barium µg/L
Volatile 505 mg/L
Fluoride 951 mg/L
Cr- Chromiurn:Total 1034 µg/L
Organochlorine Pesticides
Fixed 510 mg/L
Formaldehyde 71880 mg/L
Cu- Copper 1042 11g1L.
Organophosphorus Pesticides
Residue: Suspended 530 mg/L
Grease and Oils 556 mp,/L
Ni-Nickel 1067 µg/L
Organonitrogen Pesticiedes
Volatile 335 mg/L
Hardness Total 900 mglL
Pb- Lead 1051 µg/L
Acid Herbicides
Fixed 540 mg/L
Specific Cond. 95 µmhos/om2
Zn- Zinc 1092 µg/L
pH 403 units
MBAS 38260 mg/L
V- Vanadium µg/L,
Base/Neutral&Acid Extractable Organics
Acidity to pH 4.5 436 mg/L
Phenols 32730 µg/L
Ag- Silver 1077 µg/L
TPH Diesel Range
Acidity to pH 8.3 435 mg/L
Sulfate 945 mg/L
Al- Aluminum 1105 µg/1-
Alkalinity to pH 8.3 415 mg/L
Sulfide 743 mg/L
Be- Beryllium 1012 µg/L•
Purgeable Organics (VOA bottle req'd)
Alkalinity to pH 4.5 410 mg/L
Boron: Total 1022 gtg/L
Ca- Calcium 916 mg/L
TPH Gasoline Range
TOC 680 mg/L
Tannin & Lignin 32240 µg/L
Co- Cobalt 1037 µg/L.
TPH/BTEX Gasoline Range
Turbidity 82079 NTU
Hexavalent Chromium 1032 µg/L.
Fe- iron 1045 µg/L
Phytoplankton
Coliform Total Tube 31508 #/1o0 mis
COMMENTS;
LAB USE ONLY
Temperature
on arrival ('Q: �`
Sample Point % (2)
Conductance (94) 1
tS� 1.15
Wate�r}Temp-C (10)
D.O. (300)
pll (400)
8.3 Alkalinity (822
4.5 Alkalinity (431) 14.5
Acidity (82243)
8.3 Acidity(82242)
Secchi depth m
Salinity ppt (480)
0
Precipit-In/day (45)
qD
Cloud Cover % (32)
G
Wind Dir-Deg (36
Strm Flow Sev (13
Turbidity Severity (13
EX err to
Wind Velocity-mp
Mean Strm Depth-ft (64)

Report to: _WIRO
NC DENR/DWQ Laboratory
Sample Anomaly Report (SAR)
Lab Number:
Station Location:
sample Type:
Date collected:
AB63940
Discharge into UT
to NE crk.
Effluent
9/23/ 10
Affected Parameter(s): Turbidi
County: Onslow
Sample ID: station # 5
Region: White Oak
Priority: COC/ Emergency Collector:
Date received: 9/24/10 Date analyzed
Analytical Area (check one):
❑wal ❑METALS
❑NUT ®MICRO
The following anomalies occurred (check all that apply):
❑Samples
❑Improper container used
❑VOA vials with headspace
❑Sulfide samples with headspace
❑Samples not'received, but listed on fieldsheet
❑Samples received, but not listed on fieldsheet
❑Mislabeled as to tests, preservatives, etc.
❑]-folding time expired
[]Prior to receipt in lab
❑After receipt in lab
El Insufficient quantity for analysis
❑Sample exhibits gross non -homogeneity
❑Sample not. chemicaily preserved properly
❑pH out of range (record pH):
[]Improper chemical
❑Residual chlorine present in sample
❑Color interference
❑14cavy emulsion formed during extraction
❑Sarnple bottle broken in lab - no reportable results
❑Other (specify):
L.Willis
9/24/ l 0
❑VOA ❑SVGA
❑PEST
❑Quality Control
❑Instrument failure— no reportable results
❑Analyst error— no reportable results
❑Surrogates
❑None added
❑Recovery outside acceptance limits
❑Spike recovery
❑None added
❑Recovery outside acceptance limits
❑tailed to meet criteria for precision
❑Internal standards
❑Blank contamination
❑QC data reported outside of controls (e.g., QCS, I_CS)
❑Incorrect procedure used
❑SOP intentionally modified with QA and Branch I -lead
approval
❑Invalid instrument calibration
Ell-Ilevated detection limits due to:
❑Insufficient sample volume
Comments: This sample exceeded the upper calibration range of 1000 NTU. The reported value should be considered estimated.A
Corrective Action:
❑Samples were rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code used:J7
❑Other (explain):
Notification Required? ❑ Yes ❑ No
Person Contacted: Date:
Form completed by: A. Desa
Lead Chemist Review (initial):
[I&BIOCHEM —I ❑PEST
❑METALS ❑ VOA
Branch I lead Review (initial): /710
QA/QC Review (irliti
Date: 9/24/2010
❑SVOA
Logged into database by (initial): (Rff 101711)
]rms%aboratonyNSAR ' ' L=3/0I dbs

COUNTY:
RIVER BASIN
REPORT TO :
SHIPPED BY:
COLLFCYOR(S)
( �:t'l A_e Cr
W IRO
Courier
Estimated BOD Range:
Seed: Chlorinated:
DIVISION_ OF WATER QUALITY" - LAB FORM
W❑ SAMPLE TYPE
PRIORITY
El AMBIENT QA T STREAM GI'FLUENT
COMPLIANCE F7_1 CIIAIN OF CUSTODY LAIN: 1 INFLUENT
rM EMERGENCY C SPECIAL STUDY " ESTUARY
COMPLAINT Visit IDu��--]
Station Location: jq 19 PIOC' �ti �, rr�, t-CF 4-r i\it Ca^P tiCJ
Remarks:
Lab Number.
Date Received!
Time Received:
Received By
Data Rcfcased
Date Reported ;
Station # i Lam'
Date Begin (yy/mmldd)
I D'I C i -�
Date End (yy/mm/dd)
,GIo �.
Time Begin
# �3��
Time End
1350
Value Type- A, 1l,
Composite-T, S, B
j!
BOD 310 mg/L
Chloride 940 mg/L
7C
NH3 as N 610 mg/L
IJ- Lithium 1 132 ug/1,
COD High 340 mg/L
Chl a: 70953 µg/L
k
TKN as N 625 mg/L
Mg- Magnesium 9: mg/L
COD Low 335 mWl'
1C
NO2 plus NO3 as N 630 mg/l.
Mn- Manganese IC pg/L
Coliform: MF Fecal 31616 #/100 mis
P: Total as P 665" mg/L
Na- Sodium 929 mg/L
Coliform: N4F'Fotai 31504 #/100 MIS
Color: True 80 C.U.
PO4 as P 70507 , mg/L
As- Arsenic:Total 1 pg/L
Coliform: Tube Fecal 31615 9/100 mis
Color: (pH ) 83 C.U.
P: Dissolved as P 666 mg/L
Se- Selenium 1 147 ltg/L
Coliform: Fecal Strep 31673 9/100 mis
Color: p11 7.6 82 c.u.
K- Potassium mg/I.
Hg- Mercury 71901 µg/L
Residue: Total 500 mg/L
Cyanide 720 mg/L
Cd- Cadmium 1027 µg/L
Ba- Barium AWL
Volatile 505 mg/L
Fluoride 951 mg/L
Cr- Chromium:Total 1034 pg/L
Organochlorine Pesticides
Fixed 510 Mg/L
Formaldehyde 71880 mg/L -
Cu- Copper 1042 jig/1-
Organophosphonts Pesticides
Residue: Suspended 530 mg/L
Grease and Oils 556 mg/L
Ni- Nickel 1067 ` µg/L
Organanitrogen Pesticiedes
Volatile 535 mg/L
Hardness Total 900 mg/L
Pb- Lead 1051 µg/L
Acid Herbicides
Fixed 540 mg/L
Specific Cond. 95 pmhos/cm2
Zn- Zinc 1092 pg/L
pH 403 units
MBAS 38260 mg/L
V- Vanadium ltg/l.
B ase/Neutral &Acid Extractable Organics
Acidity to p11 4.5 436 mg/L
Phenols 32730 Awl-
Ag- Silver 1077 µg/L
TPH Diesel Range
Acidity to pH 8.3 435 mg/L
Sulfate 945 mg/L
Al- Aluminum 1 l05 µgA-
Alkalinity to pH 8.3 415 mg/L
Sulfide 745 mg/L
Be- Beryllium 1012 pg/L
Purgeabte Organics (VOA bottle req'd)
Alkalinity to pH 4.5 410 mg/L
Boron: Total 1022 µg/L
Ca- Calcium 916 mg/L
TPH Gasoline Range
TOC 680 mg/L
Tannin & Ugnin 32240 pg/L
Co- Cobalt 1037 AWL
TPH/BTL'N Gasoline Range
Turbidity 82079 NTU
Hexavalent Chromium 1032 pg/L
Fe- Iron 1045 µg/L
Phytoplankton
Coliform Total'Fube 31508 #/l00 mks
COMMENTS
:
LAB USE ONLY
Temperature
on arrival CC).
Sample Point % (2)
Conductance (94)
Water Temp-C (10)
D.O. (300)
p1l (400)
8.3 Alkalinity (822
4.5 Alkalinity (431) 14.5
Acidity (82243)
8.3 Acidity (82242)
Secchi depth m
Salinity ppl (480)
Precipit-In/day (45)
Cloud Cover % (32)
Wind Dir-Deg (36
Strm Flow Sev (13
Turbidity Severity (13
Wind Velocity -mph
Mean Strm Deplh-ft (64)

COUNTY: �t15iDciv
RIVER BASIN:
REPORTTO: WIRO
SIIIPPEI) BY; Courier
cc�t_t.>.crnH3s� -. �ti i v\ Is. iC, IiL�01,
Estimated BOD Range:
Seed: Chlorinated:
DIVISION OF WATER QUALITY - LAB FORM
PRIORITY
ED AMBIENT QA
❑ COMPLIANCE CHAIN OF CUSTODY
171 EMERGENCY ESPECIAL STUDY
COMPLAINT Visit ID�
Station Location:
Remarks:
W❑ SAMPLE TYPE
0 STREAM EFFLUENT
❑ LAKE ; INFLUENT
ESTUARY
Lab Number:
Date Received '.
Time Received
Received By
Data Released
Date Reported
Station # L L AJ
�
hate Begin (yy/mm/dd)
L2 ,C a.
Date End (yy/mm/dd)
It { •�
Time Begin I-End
## 15C� I s�
Value Type - A, H, Composite-T, S, B
11301)310ime
mg/L
Chloride 940 mg/L
NH3 as N 610 MO-
Li- Lithium 1132 ug/L
COD High 340 mg/L
Chl a: 70953 µg/I,
x-
TKN as N 625 ' mg/L
Mg- Magnesium 9. mg/L
COD Low 335 mg/L
X
NO2 plus NO3 as'N 630 mg/l.
Mn- Manganese K pg/L
Coliform: MF Fecal 31616 9/100 MIS
P: Total as P 665' mg/L
Na- Sodium 929 mg/L
Coliform: MF Total 31504 #/100 cols
Color. True 80 C.U.
PO4 as 1' 70507 mg/L
As- Arsenic:Total 1 pg/L
Coliform: Tube Fecal 31615 #/] 00 MIS
Color: (pH ) 83 cm.
P: Dissolved as 0-666 mg/L
Se- Selenium 1147 µg/L
Coliform- Fecal Strep 31673 4I100 MIS
Color: pl 17.6 82 C.U.
K- Potassium mg/L
Hg- Mercury 7190, pg/L
Residue. Total 500 mg/L
Cyanide 720 mg/L
Cd- Cadmium 1027 pg/L
Ba- Barium pg/L
Volatile 505 mg/L
Fluoride 951 mg1L
Cr- Chromium:"Total 1034 µg/L
Organochlorine Pesticides
Fixed 510 mg/L
Formaldehyde 71880 mg/L
Cu- Copper 1042 µg/L
Organophosphorus Pesticides
Residue: Suspended 530 mg/L
Grease and Oits 536 mg/L
Ni- Nicket 1067 µg/L
Organonitrogen Pesticiedes
Volatile 535 mg/L
Hardness Total 900 mg/L.
Pb- Lead 1051 pg/L
Acid Herbicides
Fixed 540 mg/L
Specific Cond. 95 µmhos/cm2
Zn- Zinc 1092 pg/L
pi1403 units
MBAS 38260 mg/L
V- Vanadium µg/L
BaSe/Neulral&Acid Extractable Organics
Acidity to pH 4.5 436 mg/L
Phenols 32730 µg/L
Ag- Silver 1077 pg/L
TPH Diesel Range
i
Acidity to pl 18.3 435 mg/L,
Sulfate 945 mg/L
Al- Aluminum 1105 µg/L
Alkalinity to pH 8.3 415 mg/L,
Sulfide 745 mg/I.
Be- Beryllium 1012 µg/L
Purgeable Organics (VOA bottle req'd)
Alkalinity to pll 4.5 410 mg/L
Boron: Total 1022 µg/L
Ca- Calcium 916 mg/L
TPH 0asotine Range
TOC 680 mg/L
Tannin & Lignin 32240 µg/1.
Co- Cobalt 1037 µg/L
TPIUBTEX Gasoline Range
X
Turbidity 82079 NTU
Hexavalent Chromium 1032 µg/L
Fe- Iron 1045 pg/L
Phytoplankton
Coliform Total 'rube 31508 #/Ioo mis
COMMENTS:
LAB USE ONLY
Temperature
on arrival ('Q:
Sample Point % (2)
Conductance (94)
l� s3.�
Water Temp-C (10)
D.O. (300)
pH (400)
9.3 Alkalinity (822
4.5 Alkalinity (431)
4.5 Acidity (82243)
8.3 Acidity (82242)
Secchi depth m
Salinity ppt (480)
Precipit-Wday (45)
Cloud Cover %`( 2)
10
Wind Dir-Deg (36
Strm Flow Sev (13
Turbidity Severity (13
Wind VelocitY-mft
Mean Strm Depth-ft (64)
r

COUNTY : o tlSlC [L
RIVER BASIN:
REPORTTO: WIRO
SHIPPED BY: Courier
Estimated ROD Range:
Seed:
DIVISION OF WATER QUALITY - LAB FORM
W� SAMPLE TYPE
PRIORITY
AMBIENT QA STREAM LN EFFLUENT
COMPLIANCE CHAIN OF CUSTODY El LAKE INFLUENT
y� EMERGENCY C SPEC1AL STUDV ESTUARY
QCOMPLAINT Visit ID�� e3
Station Location: m J l S,s-V o_ q.9— Gt`ri L_
Chlorinated: Remarks: "I
Lab Number:
Date Received :
Time Received
Received 11),
Data Released
Date Reported
Station # wit lw
'3
Date Begin (yylmm/dd)
1C)
Date End (yy/mrn/dd)
lo�� t I
'Time Begin
#g lam} Oc
'Time End
11-toG
Value Type - A, ] 1,
Composite-T, S, B T_
ROD 310 mg/L I
COD High 340 mg/L
COD Low 335 mg/L
Coliform: MF Fecal 31616 41100 mis
Coliform: MF Total 31504 9/100 mis
Coliform: Tube Fecal 31615 9/100 MIS
Coliform: Fecal Strep 31673 9/100 mis
Residue: Total 500 mg/L
Volatile 505 mg/L
Fixed 510 mg/L
Residue: Suspended 530 mg/L
Volatile 535 mg/L
Fixed 540 mg/l.
pH 403 units
Acidity to pH 4.5 436 mg/l.,
Acidity to pH 8.3 435 mgJl.
Alkalinity to p11 8.3 415 mg/L
Alkalinity to pl14.5 410 mg/L
TOC 680 mg/L
Turbidity 82079 NTU
Col iform Total Tube 31508 7/100 mis
:
Chloride 940 mg/l,
NH3 as N 610 mg/l.
I
Li- Lithium 1132 up1L
Chl a:70953 µg/L
TKN as N 625 mg/L
Mg- Magnesium 9. mg/L
NO2 plus NO3 as N 630 mg/L
Mn- Manganese IC µg/L
P: Total as P 665 mg/L
Na- Sodium 929 mg/L
Color: True 80 c'u.
PO4 as P 70507 mg/L
As- Arsenic:Total I µg/L
Color: (PI1) 83 c.u.
P: Dissolved as P 666 mg/L
Se- Selenium 1 147 ug/L
Color: pH 7.6 82 c.u.
K- Potassium mg/L
1Ig- Mercury 7190, µg/L
Cyanide 720 mg/l,
Cd- Cadmium 1027 µg/1.
Ra- Barium µg/L
Fluoride 951 mg/L
Cr- Chromium:Totaf 1034 µg/L
Organochlorine Pesticides
Formaldehyde 71880 mg/L
Cu- Copper 1042 µg/L
Organophosphorus Pesticide;
Grease and Oils 556 mg/L
Ni- Nickel 1067, jig/I,
Organonitrogen Pesticiedes
Hardness Total 900 mg/L
Pb- Lead 1051 µg/L
Acid I lerbicides
Specific Cond. 95 µmhos/em2
Zn- Zinc 1092 µg/L
MBAS 38260 mall-
V- Vanadium µg/L
Base/Neutral&Acid Extraciable Organics
Phenols 32730 µg/1-
Ag- Silver 1077 µg/L
TPH Diesel Range
Sulfate 945 mg/I..
AI- Aluminum ! I05 µg/L
I
Sulfide 745 mg/i.
Be- Beryllium 1012 µg/L
Purgeable Organics (VOA bottle req'd)
Boron; Total 1022 µg/L
Ca- Calcium 916 mg/L
TPH Gasoline Range
Tannin & Lignin 32240 µg/L
Co- Cobalt 1037 µg/L
TPH/BTEX Gasoline Range
Hexavalent Chromium 1032 µg/L
Fe Iron E045 µg/L
Ph)zoplankton
COMMENTS
LAB USE ONLY
Temperature
on arrival (°C):
Sample Point % (2)
Conductance (94)
99 �
Water Temp-C (10)
L4-Uc
D.O. (300)
p11 (400)
8.3 Alkalinity (822
4.5 Alkalinity (431)
4.5 Acidity (82243)
8.3 Acidity (82242)
Secchi depth in
Salinity ppt (480)
0
Precipit-lnlday (45)
0
Cloud Cover°/ (32)
0
Wind Dir-Deg (36
Strm Flow Sev, (13
Turbidity Severity (13
1 ai-k-cam e
Wind Vclocity-mphMean
Sirm Depth-ft (64)

DIVISION OF WATER QUALITY - LAB FORM
W� SAMPLE TYPE Date Received
COUNTY: �x1��� PRIORITY Time Received
RIVER BASIN: AMBIENT QA STREAM © EFFLUENT Received By:
REPORT TO : W1R0 COMPLIANCE CHAIN OF CUSTODY El LAKE s INFLUENT'
SHIPPED BY: Courier EMERGENCY C SPECIAI. STUD ESTUARY Data Released
COLLFCTOtz(s) : ci;f �¢ r .1� COMPLAINT Visit ID Date Reported
f
Estimated BOD Range: Station Location: ,'1 �� C�l,`£�1`�-c�--t...`• ��`.l[t`c�.L��CLeL
Seed: Chlorinated:` Remarl:s�L4 u L�� c fv ,S� �,ti_ .�s,,j✓s,
i
Station # d-iVCr" Date Begin (yy/mm/dd) Date End (yy/ntm/dd Begin Time End Value "T ) Time g� ype - A, I I, Composite= I', S, B
BOD 310
COD Iiigh 340
COD Low 335
Coliform: MF Fecal 31616
Col iform: MF Total 3 15 04
Coliform: Tube Fecal 31615
Coliform: Fecal Strep 31673
Residue: Total 500
Volatile 505
Fixed 510
Residue: Suspended 530
Volatile 535
Fixed 540
pH 403
Acidity to pH 4.5 436
Acidity to pH 8.3 435
Alkalinity to pI-f 8.3 415
Alkalinity to pH 4.5 410
TOC 680
Turbidity 82079
ColifonnTotal'Tube 31508
COMMENTS :
mgll
L Chloride 940 mg/L N113 as N 6l0 mg/L Li- Lithium 1132 ug/L
Chl a-. 70953 µg/L TKN as N 625 MPR _ Mom- Maenesium 9' mg/L
41100 mis
#/100 m1s
Color: True 80
#/100 mis
Color: (pH ) 83
#/l OD mis
Color: pH 7.6 82
g/L
Cyanide 720
2/1,
Fluoride 951
mc/1.
Formaldehyde 71880
mg/L
Grease and Oils 556
mg/L
Hardness Total900
rng/L
Speeilic Cond. 95
units
MBAS 38266
mg/L
Phenols 32730
mg/L.
Sulfate 945
mg/L
Sulfide 745
mg/L
Boron: Total 1022
mg/L
Tannin & Lignin 32240
NTU
Hexavalent Chromium 1032
#/100 mis
NO2 plus NO3 as N 630
P: Total as P 665'
c.u.
PO4 as P 70507
C.U.
P: Dissolved as P 666
C.U.
K- Potassium '
mg/L
Cd- Cadmium 1027
mg[L
Cr- Chromium:Total 1034
mg/L
Cu- Copper 1042
mg/L
Ni- Nickel 1067
mg/L
Pb- Lead 1051
µmhos/cm2
Zn- Zinc 1092
mg/L
V- Vanadium
µgA,
Ag- Silver 1077
mg/L
Al- Aluminum 1 105
mg/L
Be -Beryllium 1012
µg/l.
Ca- Calcium 916'
µgIL
Co -Cobalt 1037
uc/L
Fe- Iron 1045
Sample Point % (2)
Conductance (94)
Water Temp-C (10)
D.O. (300)
J
pl1(400)
8.3 Alkalinity (822
4.5 Alkalinity (431)
4.5 Acidity (82
Secchi depth m
Salinity ppt (480)
Precipit-In/day (45)
Cloud Cover % (32)
Wind Dir-Deg (36
Strm Flow Sev (13
"Turbidity Severity (13
Wind Velocity
Mn-Manganese I( µg/L
Na- Sodium 929 mg/L
As- Arsenic:Total l µg/l,
Se- Selenium 1147 µgll_
I Ig- Mercury 7190( µy,1L
Ba- Barium µg/L
Organochlorine Pesticides
Or gano phosphorus Pesticides
Drganonitrogen Pesticiedes
Acid Herbicides
Base/Neutral&Acid Extractable_
T'PH Diesel Ranee
Purgeable Organics (VOA bottle
T'PH Gasoline Range
TPH/BTEX Gasoline Range
Phvtonlankton
LAB USE ONLY
Temperature
on arrival CC):
8.3 Acidity (82242)
Mean Strm Depth-ft (64)
ics

COUNTY:
I-
RIVER BASIN:
RF,POR"rTO:
WIRO
SHIPPED BY:
Courier
Estimated 130D Range:
Seed: Chlorinated:
DIVISION OF WATER QUALITY - LAB FORM
W❑ SAMPLE TYPE
PRIORITY
❑ AMBIENT QA STREAM ❑ EFFLUENT
COMPLIANCE 0 CHAIN OF CUSTODY LAKE INFLUENT
EMERGENCY C SP> CIAL STUDY I=STUARY
COMPLAINT Visit IDL
Station Location: i5cV1 CQI
Remarks: `1 �1.*1 `i) 1'��iC�;�C���i=1�`_� Ica_•r �aa icily %ors[
Lab Number
Date Received:
Time Received :
Received By:
Della MUSed
Date Reported
Station 4-t4VCrk-C_L1
Date Begin (yylmnildd)
iG�oc{ �.D�
Date End (yy/mm/dd)
iO�flr ��.
Time Begin
8a 1'-�'ZI
Time End
I�Z 1
(
Value Type - A,11,
Composite-T, S, B
BOD 310 mg/L
I
Chloride 940 mg/L
NH3 as N 610 mg/l,
t-i- Lithium 1 132 ug/l.
COD High 340 mg/L
Chl a: 70953 µg/L
TKN as N 625 mg/L
Mg- Magnesium 9: mg/L
COD Low 335 mg/L
NO2 plus NO3 as N 630 mg/L
Mn- Manganese lC µg/L
Coliform: MF Fecal 31616 4/I00 mis
P: Total as P 665 mg/L
Na- Sodium 929 mg/L
Colifotm: MF Total 31504 ##/100 MIS
Color: True 80 C.U.
PO4 as P 70507 ' mg/L
As- Arsenic:Total 1 og/L
Coliform: Tube Fecal 31615 #/100 MIS
Color'. (pH ) 83 C.U.
P: Dissolved as 11666 mg/L
Se- Selenium 1147 µg/L
Coliform: Fecal Strep 31673 9/I00 mis
Color: pH 7.6 82 c.u.
K- Potassium mg/L
11g- Mercury 71901 µell_
Residue. Total 500 mg/L
Cyanide 720 mg/L
Cd- Cadmium 1027 µg/L
Ba- Barium µg/L -
Volatile 505 mg/1,
Fluoride 951 mg/L
Cr- Chromium:Tolat 1034 µg/L
Organochlorine Pesticides
Fixed 510 mg/L
Formaldehyde 71980 mg/L -
Cu- Copper t042 µg/L
Organophosphorus Pesticides
Residue: Suspended 530 mg/L
Grease and Oils 556 mg/L.
Ni- Nickel 1067 ' µg/L
lorganonitTOgen Pesticiedes
Volatile 335 mg/1-
Hardness Total 900 mg/L
Pb- Lead 1051 µg/L
Acid Herbicides
Fixed 540 mg/L
Specific Cond. 95 µmhos/em2
Zn- Zinc 1092 pg/L
p1i 403 units
MBAS 38260 mg/1.
V- Vanadium µg/t,
Base/Neutral&Acid Extractable Organics
Acidity to pli 4.5 436 mg/L
Phenols 32730 pglL
Ag- Silver 1077 µg/L
TPLI Diesel Range
Acidity to pH 8.3 435 mg/L
Sulfate 945 mg(L
Al- Aluminum 1105 µg/L
f
Alkalinity to p11 8.3 415 mg/L
Sulfide 745 mg/L
Be- Beryllium 1012 µg/L
Purgeable Organics (VOA bottle req'd)
'
Alkalinity to pH 4.5 410 mg/L
Boron: Total 1022 µg/L
Ca- Calcium 916 mg/L
TPH Gasoline Range
TOC 680 mg/L
Tannin & Lignin 32240 Iig/L
Co- Cobalt 1037 )1g/L
TPH/BTE-X Gasoline Range
Turbidity 82079 NTU
Hexavalent Chromium 1032 µg/L
Fe- Iron 1045 µg/L
Phytoplank(on
Cohform Total Tube 31508 #1/100 MIS
C0,10MENTS
:
LAB USE ONLY
Temperature
an arrival CC):
Sample Point %(2)
Conductance (94)
,�?o u s
Water'rernp-C (10)
D.O. (300)
O
pH (400)
3 ��13
8.3 Alkalinity (822
4.5 Alkalinity (431)
4.5 Acidity (82243)
8.3 Acidity (82242)
Secchi depth m
Salinity ppt (480)
C)
Precipit-In/day (45)
Claud Cover'/6 (32)
1 Wind Dir-Deg (36
Stan Flow Sev (13
Turbidity Severity (13
Wind Velocity -mph
Mean Stan Depth-ft (64)

Report to: LL" iY�� Gojct..L6,I(LS N ATER QUALITY SECTION Pagt,of }
CF1.A_l OF CUSTODY (COC) RECORD
`C DENRAMIQ LABOR_aTORY (check one): I J CEN'TRAL I I ARO (I WaRO
Investigation of: tQ E LCi CZ) c 1 7 4
Sarnp[e collector (print name) + ��• ^
and Div]-1 forms completed by: �C,, u:�, i �t S Sampie collector's signature:
Field storage conditions and location (when applicable):
LaCi:Use On!}'.
STATION NO,
STATION LOCATION
DATE
TPvIE
S{At%VLED
NUMBER
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Time
.11 uished by (signature):
Date
Time
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Date
Time
Zelinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Aethod of Shipment (circle one): Cate Courie Hand -delivered Federal Express UPS Other:
security Type and Conditions: (
Sey
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1
'TRALABORATORY CHAIN OF CUSTODY - Lab Use Only

Report to: V';, Co WATER QUALITY SECTION Page ) of I
CHAIN OF CUSTODY (COC) RECORD
NC IIENR/DWQ LABORATORY (check one): I ]'CEN'TRAL [ I ARO [ I WaRO
For Investigation of:
R�c�' (�
Sample collector (print name)
and DM-1 forms completed by:
��"
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Sample collector's signata
Field storage conditions and location (when applicable):
. ' Lali Uie.Onty. _
STATION NO.
STATION LOCATION
DATE
SAMPLED
'TIME
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CONTAINF[LS
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Relinq ' hed by (signature):
Date
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Date
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Relinquished by (signature):
Date
Time
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Date
Time
Relinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Method of Shipment (circle one):
; State C Hand -delivered Federal Express UPS Other:
Security Type and Conditions:
Sealed by: _
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Report to: ��;� WATER QUALITY SECTION
CHAIN OF CUSTODY (COC) RECORD
VC DENRfDWQ LABORATORY (check one): 'wCE,NTRAL 1 1 ARO l I WaRO
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Lab:Usc.Only-`..
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Date
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ITRALABORATORY CHAIN OF CUSTODY - Lab Use Onl

Y11-
N.C. DIVISION OF -WATER QUALITY
Water Quality Section
ComplaarntlEmergency Report Form
11 WILMINGTON REGIONAL OFFICE
Received by
Time '1d " 'o A/fi�
Emergency Complaint ✓City County z()11AD— A riJ _
Report Received From
Agency,
Phone No.
Check One: Fish Kill Spill Bypass Animal
NPDES N.D.
CW>
StormYw,�ater Wetland Other, Specilj4_- IQ4-ey , Lf!/jL62.[
7-
Nature of Referral 1`112. S.-nal 1 ,r�[pyJ AeD 191.9 J�-�G[CJr
0
Time and Date
Location of AreaAffected` . O V
Surface Waters
Other Agencies
Classifrcation
Investigafion Details f d l
`/?/ 'Al �d ui�ilsq �.Nl `1G1. kp c�.�4LM
Investigator Date
S:1WQS4SHELLSIREP0RT.SHL
EPA Region IV [phone] Pesticides 7334M6 Emergency Management 733-3867 Wildlife Resources 733-7291
Solid and Hazardous Waste 733-2178 Marine Fisheries 726-7021 Water Supply 733-2321 Coast Guard MSO 343.4861
127 Cardinal Drive Extension, Wilmington, H.C. 28405-3845 0 Telephone [phone] • Fax [phone]

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Report tv. WUi12D, LltJa.L6,(Lts WATER QUALITY SECTION
CHAIN OF CUSTODY (COC) RECORD
Page or
NC DFNR/DWQ LABORATORY (check one): I 1 CENTRAL I I ARO I I WaRO
Investigation of:
sample collector (print name)
and DM -I fom-s completed by:
L_w' CC ��' 1�t S
Sample collector's signaturz\
Field storage conditions and location (when applicable):
Cab.Uie Onl}• :: '
STATION' N0,
STATION LOCATION
DATE
S.kNfPLCD
T➢ F
SAMPLED
NUMBER
OF
CONTAINERS
�atr,13
5
t T
Re1flouished by (signature):
D e
M
Time
10 :3
Received b (signature)
Da
Time
Z C�
,nquished by (signature):
Date
Time
Receive by (signature):
D to
Time
Re] ingtiished by (signature):
Date
Time
Received by (signature):
Date
Time
Method of Shipment (circle one):
f=ItIcluri), Hand -delivered Federal Express UPS Other.
Security Type and Conditions:
Seale 'by:
11roken b'
:NTRALABORATORY CHAIN OF CUSTODY - Lab Use Only
`:LA_B,,NUM13ERS
I�QNIBEu
;A?iAL 'SES :: : '
.RELINQUfSHED -,
RECFIV>WD
DATA
Ti[viC
FROM
THROUGII
BOTTLCS".
:REQUESTED
BY =
BY
pt
GOV.
.. . ,
..
-
C.
,
:
7 _'777:
'T.