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NCG080249_MONITORING INFO_20150617 (FIX)
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V Cc, �soa4 9 DOC TYPE I ❑ HISTORICAL FILE {MONITORING REPORTS DOC DATE ❑ YYYYMMDD 1* Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted Co - 11- 2. Di 5 CERTIFICATE OF COVERAGE NO. NCG08 0 2 H di FACILITY NAME Kt;nan Transc-mr+, "(- COUNTY SohnS-ane. PERSON COLLECTING SAMPLES _ _Tem Ht+�sF+b�r�e r LABORATORY Tes'1- Ameri cp. Lab Cert. # Z(o OV Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2.015 SAMPLE PERIOD 0 Jan -June ❑ July -Dec or ❑ Monthly' (month) DISCHA NG TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA RE El - ❑Zero -flow [:]WaterSupply [:]SA JUN 17 2015 ❑Other CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 DWR SECTION Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr 00530 00400 00556 Total Suspended Solids, mg/L pH, Standard units Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L New Motor Oil Usage, Annual average gal/mo Benchmark - 50 or 100 see permit Within 6.0 — 9.0 is - Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfal l No. Date Sample Collected, mo/dd/yr 00556 00530 00400 Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L Total Suspended Solids, mg/L pH, Standard units Permit Limit - 15 50 or 100 see permit 6.0 — 9.0 1 5- Z-7 - 2.01 s 2 • �1 / ! 3a fa • 2 I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. Cj S\VU-250 last revised April 11, 2013 Page I of 2 STORM EVENT CHARACTERISTICS: Date 3317,7/15 (first event sampled) Total Event Precipitation (inches): _ 1, EL - Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART ii SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within_ 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality T Attm DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee e. i/ ?o/s (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/webZwq/ws/su/npdessw#tab-4 SWIJ-250 last revised April 1 1. 2013 Iliac 2 of'2 Kenan Transport LLC Sampling Plan Page 10 Figure 2 Storm Water Sampling Record Sampler's Name: Date:��_0otfallNumber: Storm Begin Time- 1 have verified that no storm event measuring greater than 0.1 inches has occurred in the 72 hour prior to this storm event and that all information recorded herein is accurate and t ue to the bgst of my knowledge. Siguature: Flow Begin Time: _ (a auj�!D PH Test Method: pa / meter Storm End Time: amMm Grab Sample Time: -i amjp- PH: (1, , Storm Duration: hours h Total Precipitation: l ' inches ;3 ies'=tAmenca THE LEADER IN ENVIRONMENTAL TESTING ` 'W I`='I ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Savannah r' 5102 LaRoche Avenue Savannah, GA 31404 w r Tel: (912)354-7858 7 TestAmerica Job ID: 680-112986-1 f Client Project/Site: Stormwater Sampling / Selma, N.C. For: Transport Services Co, Inc Kenan Transport Co. 4338 Buffalo Road f,. Selma, North Carolina 27576-5606 Attn: Jerry Hershberger fi .........I.... LINKS Review your project results through TotdACCEc s a. Have a Question? )Ask — The O Expert �iS1t 115 dt:' wwwltestamericainc.tocn ` Authorized for release by: 6/3/2015 2:50:21 PM Michele Kersey, Project Manager 1 (912)354-7858 michele.kersey@testamericainc.com The test results in this report meet all 2003 NEL4C and 2009 TNt requirements for accredited parameters. exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the a -mad address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sampie(s) as received by the laboratory. Definitions/Glossary Client: Transport Services Co, Inc Project/Site: Stormwater Sampling 1 Selma, N.C. Qualifiers General Chemistry Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the M U Indicates the analyte was analyzed for but not detected. Glossary Abbreviation %R CFL CNF DER Dil Fac DL, RA, RE, IN DLC MDA £DL MDC MDL ML NC ND PQL QC RER RL RPD TEF TEQ TestAmerica Job ID: 680-112986-1 i. and the concentration is an approximate value. These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis Percent Recovery Contains Free Liquid Contains no Free Liquid . Duplicate error ratio (normalized absolute difference) Dilution Factor Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample Decision level concentration Minimum detectable activity Estimated Detection Limit Minimum detectable concentration Method Detection Limit Minimum Level (Dioxin) Not Calculated Not detected at the reporting limit (or MDL or EDL if shown) Practical Quantitation Limit Quality Control Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) Relative Percent Difference, a measure of the relative difference between two points Toxicity Equivalent Factor (Dioxin) Toxicity Equivalent Quotient (Dioxin) TestAmerica Savannah Page 2 of 12 Sample Summary Client: Transport Services Co, Inc TestAmerica ,lob ID: 680-112986-1 Project/Site: Stormwater Sampling I Selma, N.C. - --- - ------------- ------....--. Lab Sample ID Client Sample ID Matrix Collected Received 680-112986-1 Stormwater Oittall # 1 Water 05/27/15 19:20 05/29/15 10:05 TestAmerica Savannah Page 3 of 12 Case Narrative 11 Client: Transport Services Co, Inc TestAmerica Job ID: 680-112986-1 Project/Site: Stormwater Sampling I Selma, N.C. ?1 Job ID: 680-112986-1 Laboratory: TestAmerica Savannah F61 Narrative CASE NARRATIVE Client: Transport Services Co, Incf Project: Stormwater Sampling ! Selma, N.C. Report Number: 680-112986-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the , :-�! reporting limits are adjusted relative to the dilution required. '1s RECEIPT The sample was received on 5/29/2015 10:05 AM; the sample arrived in good condition, properly preserved and, where required, on ice The temperature of the cooler at receipt was 1.20 C. OIL AND GREASE AND TPH Sample Stormwater Outfall # 1 (680-112986-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A The samples were prepared and analyzed on 0610212015. Insufficient sample volume was available to perform a matrix spikelmatdx spike duplicate/sample duplicate (MS/MSDIDUP) associated with 385701. No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. TOTAL SUSPENDED SOLIDS Sample Stormwater Outfall # 1 (680-112986-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples were analyzed on 06101/2015, No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. TestAmerica Savannah Page 4 of 12 Client Sample Results Client: Transport Services Co, Inc Project/Site: Stormwater Sampling 1 Selma, N.C. Client Sample ID: Stormwater Outfail # 1 Date Collected: 05/27/15 19:20 Date Received: 05/29115 10:05 General Chemistry Analyte Result Qualifier RL Oil & Grease (HEM) 2.9 J 5.2 Total Petroleum Hydrocarbons 1.7 J 5.2 (1664A) Analyte Result Qualifier RL Total Suspended Solids 39 2.4 -M TestAmerica Job ID: 680-112986-1 Lab Sample ID: 680-112986-1 Matrix: Water L. MDL Unit D Prepared Analyzed Dil Fac 1.5 mg/L 06l0211511:25 061021151538 1 i 1.5 mg/L 06102/1511:25 06/0211515:38 1 ; RL Unit D Prepared Analyzed Dil Fac 2.4 mglL 06/01115 11;32 1 _ f TestAmerica Savannah Page 5 of 12 QC Sample Results Client: Transport Services Co, Inc Project/Site: Stormwater Sampling 1 Selma, N.C. Method: 1664A - HEM and SGT-HEM ^Lab Sample ID: MB 680-385620121-A Matrix: Water Analysis Batch: 385701 MB MB Analyte Result Qualifier RL Oil & Grease (HEM) 5.2 U 5.2 Total Petroleum Hydrocarbons 5.2 U 5.2 [ (1664A) M TestAmerica Job ID: 680-112986-1 ti .......... .................. - .............. ....-.-....... --- ----...--- -- ------ -- ------ _ , Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 385620 MDL Unit D Prepared Analyzed Dil Fac 1.5 mg/L 06102/1511:25 06/0211515:38 1 - 1.5 mglL 06/0211511:25 06/0211515:38 1 Method: 2540 D-2011 - Total Suspended Solids Dried at 103-105°C ! �� Lab Sample ID: MB 680-385444/1 Matrix: Water Analysis Batch: 385444 Analyte I Total Suspended Solids Lab Sample ID: LCS 680-385444/2 Matrix: Water Analysis Batch: 385444 I Analyte ToW Suspended Solids Lab Sample ID: LCSD 680-385444/3 Matrix: Water Analysis Batch: 385444 I Analyte Total Suspended Solids MB MB Rrsulf OualHirr 1.0 U Client Sample ID: Method Blank Prep Type: Total/NA --- RL RL Unit D Prepared Analyzed Dil Fac 1.0 1.0 mg1L 0610111511:20 1 zr� Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 20.0 17.5 mglL 88 80 - 120 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike LCSD LCSD %Ree. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 20.0 19.0 mglL 95 80 - 12D 8 25 TestAmerica Savannah Page 6 of 12 QC Association Summary Client: Transport Services Co, Inc Project/Site: Stormwater Sampling 1 Selma, N.C. General Chemi 'f I TestAmerica Job ID'. 680-112986-1 Analysis Batch: 385444 Lab Sample 1D Client Sample ID Prep Type Matrix Method Prep Batch 680-112986-1 Stormwater Outfatl # 1 Total/NA Water 2540 D-2011 LCS 680-385444/2 Lab Control Sample Total/NA Water 2540 D-2011 LCSD 680-385444/3 Lab Control Sample Dup Total/NA Water 2540 D-2011 MB 680-385444/1 Method Blank Total/NA Water 2540 D-2011 Prep Batch: 385620 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-112986-1 Stormwater Outfatl # 1 Total/NA Water 1664A MB 680-385620/21-A Method Blank Total/NA Water 1664A Analysis Batch: 385701 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-112986-1 Stormwater Outfatl # 1 Total/NA Water 1664A 385620 MB 680-385620121-A Method Blank Total/NA Water 1664A 385620 TestAmerica Savannah ,may; Page 7 of 12 Client: Transport Services Co, Inc Lab Chronicle TestAmerica Job ID; 680-112986-1 •— Project/Site: Stormwater Sampling / Selma, N.C. Client Sample ID: Stormwater 4utfall # 1 Date Collected: 05/27/15 19:20 Date Received: 05/29/15 10:05 i Batch Batch Prep Type Type Method Run Total/NA Prep 1664A TotallNA Analysis 1664A Instrument ID: NOEQUIP Total/NA Analysis 2540 D-2011 Instrument ID: NOEQUIP Lab Sample ID: 680-112986-1 -- --- Matrix: Water ---- - --- - - - - -- -- -- -- ---- .. .. .. N--" Dil Initial Final Batch Prepared Factor Amount Amount Number or Analyzed Analyst Lab 480 mL 500 mL 3856 00 06/02 5 15 11:25 ALC TAL SAV {a 1 480 mL 500 mL 385701 06/02/15 15:38 ALC TAL SAV . 1 418 mL 1000 mL 385444 06/01/15 11:32 LBH TAL SAV ; '_- U. Laboratory References:. TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 , �4 TestAmerica Savannah Page 8 of 12 Certification Summary Client: Transport Services Co, Inc TestAmerica Job ID: 680-112986-1 Project/Site: Stormwater Sampling 1 Selma, N.C. Laboratory: TestAmerica Savannah - -- - - --- - - The certifications listed be#cw are applicable to this report. Authority Program EPA Region Certification ID Expiration Date North Carolina (WWISN) State Program 4 269 12-31-15 Pennsylvania NELAP 3 68-00474 06-30-15 Virginia NELAP 3 460161 06-14.15 ' Certification renewal pending - certification considered valid. TestAmerica Savannah Page 9 of 12 Method Summary � Client: Transport Services Co, Inc TestAmerica Job ID: 680-112986-1 Project/Site: Stormwater Sampling 1 Selma, N.C.) Method Method Description Protocol Laboratory 1664A HEM and SGT-HEM 1664A TAL SAV 2540 D-2011 Total Suspended Solids Dried at 103-105°O Ei SM TAL SAV Protocol References: 1664A = EPA-821-98-002 r.— SM = "Standard Methods For The Examination Of Water And Wastewater', ° Laboratory References: TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 r -- TestAmerica Savannah Page 10 of 12 Serial Number 79850 ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD TestAmeca �' Ci ( rjC 76 THE LEADER IN ENVIRONMENTAL TESTING 0 Te mmertca Savannah Website: www.testamericainc.com 5102 LaRoche Avenue Phone: (912) 354-78SB Savannah, GA314D4 Fax: (912) 352 Q165 O Alternate Laboratory NameA=ation Phone: Fax: PROJECT REFERENCE PROJECT NO, PROJECT LOCATION (STATE) 4j L MATRIX TYPE REQUIRED ANALYSIS PAGE OF TAL (LAB) PROJEC I MANAGER P.0 NUMBER CONTRACT NO, ¢ Q O ` `w o (n ¢ Z o o o a a o 2 I I STANDARD REPORT DELIVERY Q DATE DUE EXPEDITED REPORT DELIVERY CD (SURCHARGE) DATE DUE LI6YT {SITE) P j CLIENT PHONE r CLIENT FAX CLIENT NA E CLIENT E-MAIL f IENTADDREW 77 S_l5UJJ r 0 1 �? m �' , ': T T �:. NUMBER OF COOLERS SUBMITTED PER SHIPMENT OMPANY CONTRACTINGTHIS WORK (If applicable) SAMPLE SAMPLE IDENTIFICATION NUMBER OF CONTAINERS SURMfTTED KS REMARKS PATE TIME aft 1 € l 680-112986 Chain of Custody LINOUISHED Y: (SIGNATURE) I DATE ` � TIME f� RELINQUISHED BY: p( wwaE) DATE TIME RELINQUISHED BY' (s KAn1REI DATE TIME RECEIV Y: (SIGNATURE) TIME RECEIVED BY: (SIGNATURE) DATE TIME RECCIVED BY, (Sf3NATJRE) DATE i1ME LABORATORY USE ONLY RECIVED F LA �RY (&MA DATE TIME 14-FS % l V .� CUSTODY INTACT CUSTODY CD SEAL NO. NO 0 SAVANNAH LOG NO LABORATORY REMARKS 0` VLa(F r I TAL8240680(1006) Login Sample Receipt Checklist Client: Transport Services Co, Inc Login Number: 112986 List Number: 1 Creator: White, Menica R Question Answer Radioactivity wasn't checked or is </= background as measured by a NIA survey meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True is the Field Samplers name present on COC? N/A There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time, True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vot. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is NIA <6mm (1/4"). Multiphasic samples are not present. True Samples do not require sp4itting or compositing. True Residual Chlorine Checked. N/A Job Number: 680-112986-1 List Source: TestAmerica Savannah L Comment i A [12 TestAmerica Savannah Page 12 of 12 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCGO80000 Date submitted 1 / 13 / z o i (,o CERTIFICATE OF COVERAGE NO. N0008 0 Z q 3 FACILITY NAME lLern `rro.ns0or4-, LLC- COUNTY _:Y-0 V) n " +-0 n e- PERSON COLLECTING SAMPLES :Y- S!-+' LABORATORY rest- Ame+ic.A Lab Cert. t# Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2-0 1 S SAMPLE PERIOD ❑ Jan -June ❑ July -Dec c rrr� or El monthly' month RECDISC�HAIT @G TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA �A� 2 z�16 ❑Zero -flow ❑Water Supply [:]SA ❑Other CENTRAL FILES DWR SECTION PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _✓no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr 00530 00400 00556 Total Suspended Solids, mg/L pH, Standard units Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L New Motor Oil Usage, Annual average gal/mo Benchmark - 50 or 100 see permit Within 6.0— 9.0 15 - Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall No. Date Sample Collected, mo/dd/yr 00556 00530 00400 Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L Total Suspended Solids, mg/L pH, Standard units Permit Limit - 15 50 or 100 see permit 6.0 — 9.0 0 I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page I of 2 STORM EV sNT CHARACTERISTICS: Date I I i I,5 (first event sampled) Total Event Precipitation (inches): 0, `d Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports within 30 days of receipt of the lob results (or at end of monitoring_ period in the case of "No Discharge" reports)to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of vi i 3 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 P, ■cE, N ,d0"D& 4NTA0E GROUP, INC. Advantage Tank Lines • BXl Cryogenic Transportation • DistTech • Jack 8. Kelley • KAG Logistics • Klemm Tank Lines KAG West • Kenan Transport • North Canton Transfer . Petro Chemical Transport • Transport Service Co. November 13, 2014 Division of Water Quality ATTN: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RECEIVw,:-_UPS : 1Z 6V9 340 02 9427 1547 NOV 17 2014 CENTRAL FILES DWR SECTION RE: 2014 2nd Half SDO Monitoring Report Permit No. NCG080249. To Whom It May Concern, Please find enclosed Kenan Transport, LLC's monitoring report for the above reference permit number for the 2nd half of 2014. Please don't.hesitate to contact me directly with any questions or concerns at 630/472-5934 or james.king@thekag.com. Respectfully Submitted, James King, CHMM Director of Environmental Quality and Compliance 2001 Spring Road Oak Brook, IL 60523 Office:630-472-5934 1 Fax: 630-472-0495 Cell: 630-853-4395 www.thekag.com 2001 Spring Road, Suite 400 • Oak Brook, IL 60523 • 630-472-5900 • 630-472-0495 (fax) • www.thekag.com Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG080000 Date submitted CERTIFICATE OF COVERAGE NO. N0008 D 2_ 1-i 9 FACILITY NAME 1<enan -F dn�2g � , LL (- COUNTY e _ PERSON COLLECTING SAMPLES _Te rry 1're��hhe raer LABORATORY Awtt-i c c, Lab Cert. # ZG 9 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR so4,- SAMPLE PERIOD ❑ Jan -June ❑X July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑ Water Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON THE REVERSE --> Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes ✓no (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfal I No. Date Sample Collected, mo/dd/yr 00530 00400 00556 Total Suspended Solids, mg/L pH, Standard units Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L New Motor Oil Usage, Annual average gal/ma Benchmark - 50 or 100 see permit Within 6.0 - 9.0 15 - Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall No. Date Sample Collected, mo/dd/yr 00556 00530 00400 Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L Total Suspended Solids, mg/L pH, Standard units Permit Limit - 15 50 or 100 see permit 6.0 - 9.0 1 ►al+s/�� 5- z 19 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 5WU-250 last revised April 11, 2013 Page I of 2 STORM EVENT CHARACTERISTICS: Date i0h5/)'-f (first event sampled) Total Event Precipitation (inches): Z �- Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AAND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on final and one copy of this DMR including all "No Discharge," reports, within 30 days of receipt of the lab results or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1 A13\ 0 1� (Da e) Additional copies of this form may be downloaded at: http1/Dortal.ncdenr.org/web/wq/ws/su/npdesswl#tab-4 SWU-250 last revised April 11, 2013 Page 2 of 2 THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 TestAmerica Job ID: 680-106381-1 Client Project/Site, Stormwater Sampling - Selma, NC For: Transport Services Co, Inc Kenan Transport Co. 1301 Boulder Road Greensboro, North Carolina 27409-9106 Attn: Matt Brinkman Authorized for release by: 1012812014 1:53:13 PM Michele Kersey, Project Manager 1 (912)354-7858 michele.kersey@testamericainc.com The test results in this report meet all 20031dELAC and 2005 TN! requirements for accredited parameters. exceptions are noted in this report This report may not be reproduced except in full and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature_ Results relate only to the items tested and the sample(s) as received by the laboratory. H Definitions/Glossary Client:'Transport Services Co, Inc TestAmerica Job ID: 680-106381-1 Project/Site: Stormwater Sampling - Selma, NC Qualifiers General Chemistry Qualifier Qualifier Description U Indicates the analyte was analyzed for but not detected, ----- —-.-.-.,..-.,.-.-......-._._...,._....- .,-. Glossary Abbreviation O %R CFL CNF DER Dil Foc DL, RA, RE, IN OLD MDA EDL MDC MDL ML NC ND PQi. QC RER RL RPD TEF TEQ These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis Percent Recovery Contains Free Liquid Contains no Free Liquid Duplicate error ratio (normalized absolute difference) Dilution Factor Indicates a Dilution, Re -analysis. Re -extraction, or additional Initial metalslanion analysis of the sample Decision level concentration Minimum delectable activity Estimated Detection Limit Minimum detectable concentration Method Detection Limit Minimum Level (Dioxin) Not Calculated Not detected at the reporting limit (or MID or E D L if shown) Practical Quantitation Limit Quality Control Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) Relative Percent Difference, a measure of the relative difference between two points Toxicity Equivalent Factor (Dioxin) Toxicity Equivalent Quotient (Dioxin) TestAmerica Savannah Page 2 of 12 Sample Summary Client:'Transport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC TestAmerica Job ID: 680-106381-1 Lah Sample ID Client Sample 1D Matrix Collected Received 680-106381-1 Storm Water Ouffall #1 Water i 0/15/14 1100 10117114 10:06 TestAmerica Savannah Page 3 of 12 Case Narrative Client:'Transport Services Co, Inc TestAmerica Job ID: 680-106381-1 Project/Site: Stormwater Sampling - Selma, NC - - - Job 1D: 680-106381-1 Laboratory: TestAmerica Savannah Narrative CASE NARRATIVE j !i Client: Transport Services Co, Inc Project: Stormwater Sampling - Selma, NC { Report Number: 680-106381-1 m With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the !« reporting limits are adjusted relative to the dilution required. RECEIPT The sample was received on 10/17/2014 1 D:06 AK the sample arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 2.60 C. OIL AND GREASE AND TPH Sample Storm Water Outfall #1 (680-106381-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A. The samples were prepared and analyzed on 1012312014. Insufficient sample volume was available to perform a matrix spike/matrix spike duplicatelsample duplicate (MSIMSD/DUP) associated with batch 355086. No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. TOTAL SUSPENDED SOLIDS Sample Storm Water Outfail #1 (680-106381-1) was analyzed for total suspended solids in accordance with SM 25400. The samples were analyzed on 10/21/2014. No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page Page 4 of 12 TestAmerica Savannah Client Sample Results Client: .Transport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC Client Sample ID: Storm Water Outfall #1 Date Collected: 10/15/14 13:00 Date Received: 10/17/14 10:06 General Chemistry Anal Result Qualifier RL MDL Unit Oil & Grease (HEM) 5.2 U 5.2 1.5 mg1L Total Petroleum Hydrocarbons 5.2 U 5.2 1.5 mg/L (1664A) Analyte Result Qualifier RL RL Unit Total Suspended Solids 19 5.0 5.0 mg/L F91 TestAmerica Job ID: 680-106381-1 -- Lab Sample ID. 680-106381-1 Matrix: Water .......................... —.—... ,.............. ,..,........ ...-.-.-.--.-._ . ----- . ' -- L " l D Prepared Analyzed DII Fac 1012 3/ 14 14:41 1012 3114 1720 1 1h 10/23114 14:41 10123114 17:20 1 =J D Prepared Analyzed DII Fac I %; 10121/1410:30 1 i TestAmerica Savannah Page 5 of 12 Client: Transport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC QC Sample Results TestAmerica Job ID: 680-106381-1 IE Method: 1664A-_HEM SGT-HEM _and ^Lab Sample ID: MB 680-355055121-A Client Sample ID: Method Blank F r Matrix: Water Prep Type: TotaI1NA Analysis Batch: 355086 Prep Batch: 355055 MB M8 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Oil & Grease (HEM) 5.3 U 5.3 1.5 mg1L 10/23/14 14:41 10/23/14 17:20 1 IIII s IIII Total Petroleum Hydrocarbons 5.3 U 5.3 1.5 mg1L 10/23/14 14A1 10/23/14 17:20 1 _ (1664A) Lab Sample ID: LCS 680-355055122-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: TotalINA Analysis Batch: 355086 Prep Batch: 355055 o Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Oil a Grease (HEM) 40,7 41.3 mglL 101 78- 114 Total Petroleum Hydrocarbons 20,4 20.7 mg/L 101 64 - 132 (1664A) Lab Sample ID: LCSD 680-355055123-A Client Sample ID: Lab Control Sample Dup =_ Matrix: Water Prep Type: Total/NA - -- Analysis Batch: 355086' Prep Batch: 355055 Spike LCSD LCSD %Rec. RPD i Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Oil & Grease (HEM) 42.7 44.2 mg1L 103 78 - 114 7 18 Total Petroleum Hydrocarbons 21.4 22A mg1L 104 64 - 132 7 34 (1664A) Method: 2540 D-2011 - Total Suspended Solids Dried at 103-105°C J Lab Sample ID: MB 680-35452811 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 354528 Me Me Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 5.0 U 5,0 5.0 mgfL 10121114 09:56 1 Lab Sample ID: LCS 680-35452812 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 354528 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 13,8 12.5 mglL 91 80- 120 Lab Sample ID: LCSD 680-354528/3 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 354528 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 13,8 14.0 mg/L 102 80- 120 11 25 TestAmerica Savannah Page 6 of 12 ClienCTransport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC General Chemistry Analysis Batch: 354528 I Lab Sample ID Client Sample ID 680-106381-1 Storm Water Outfall #1 LCS 680-35452812 Lab Control Sample LCSD 680-35452813 Lab Control Sample Dup MB 680-35452811 Method Blank Prep Batch: 355055 j Lab Sample iD Client Sample ID 680-106381-1 Storm Water Outfall #1 LCS 680-355055/22-A Lab Control Sample LCSD 680-355D55123-A Lab Control Sample Dup i MB 680-355055121-A Method Blank Analysis Batch: 355086 ,' Lab Sample ID Client Sample ID 680-106381-1 Storm Water Outfall #1 LCS 680-355055122-A Lab Control Sample LCSD 680-355055/23-A Lab Control Sample Oup I MB 680-355055121-A Method Blank QC Association Summary Prep Type Matrix I UW1II1M —dEer Total/NA Water Total/NA Water Prep Type Matrix Total/NA Water Total/NA Water Total/NA Water TotallNA Water Prep Type Matrix Total/NA Water TotaUNA Water Total/NA Water Total/NA Water BE TestAmerica Jab ID: 680-106381-1 -- - rn, Method 2540 D-2011 Prep Batch 2540 D-2011 2540 D-2011 (' f 2540 D-2011 Method Prep Batch 1664A ^� 1664A 1664A ..i 1664A Method Prep Batch 1664A 355055 1664A 355055 �r 1664A 355055 -` 1664A 355055 TestAmerica Savannah Page 7 of 12 C lie r)CTran sport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC Client Sample ID: Storm Water Outfall #1 Date Collected: 10115/14 13:00 Date Received: 10/17/14 10:06 Batch Batch Prep Type Type Method Run Total/NA Prep 1664A Total/NA Analysis 1664A Instrument ID: NoEquip Total/NA Analysis 2540 D-2011 Instrument ID: NOEQUIP Lab Chronicle Dil Initial Factor Amount 478 mL 1 478 mL Final Batch Amount Number 500 mL 355C55 500 mL 355086 1 2C0 mL 200 mL 354528 Laboratory References: TAL $AV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 HE TestAmerica Job ID: 680-106381-1 ---- Lab Sample ID: 680-106381-1 -- Matrix: Water --I Prepared or Analyzed Analyst Lab 10123114 14:41 ALC TAL SAV i 10123114 17:20 ALC TAL SAV C t -1 k 10121/14 10:30 LBH TAL SAV -nn--- lam: 3 k__ TestAmerica Savannah Page 8 of 12 Certification Summary Client -'Transport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC R] TestAmerica Job ID: 680-106381-1 %r Laboratory: TestAmerica Savannah The certifications listed below are applicable to this report. j Authority Program EPA Region Certification ID Expiration Date North Carolina (WWISW) State Program 4 269 12-31-14 I Pennsylvania NELAP 3 66-00474 06-30-15 Virginia NELAP 3 460161 06-14-15 TestAmerica Savannah Page 9 of 12 Method Summary E111, Client: Transport Services Co, Inc TestAmerica Job ID: 680-106381-1 - - Project/Site: Stormwater Sampling - Seima, NC Method Method Description Protocol Laboratory 1664A HEM and SGT-HEM 1664A TAL SAV I-_Y Fi I 2540 D-2011 Total Suspended Solids Dried at 103-105°C SM TAL SAVe Protocol References: 1664A = EPA-821-98-002 A SM = "Standard Methods For The Examination Cf Water And Wastewater', Laboratory References: -� TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 I ��l TestAmerica Savannah Page 10 of 12 Serial Number 81271 L ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD f TestAmeric a ` r"Mspex- VC-F /! !�-� a~ �I � �!-7 l� THE LEADER IN ENVIRONMENTAL TESTING 0 TestAmerica Savannah Website: www.testamericainc.com 5102 LaRoche Avenue Phone: (912) 354.7858 Savannah, GA31404 Fax: (912) 352-0165 � Alternate Laboratory Name/Location Phone: Fax: PROJECT REFERENCE PROJECT NO. PROJECT LOCATION (STATE) c— MATRIX TYPE REQUIRED ANALYSIS PAGE OF TAL {LAB) PROJECT MANAGER P.O.NUMBER CONTRACT NO. U ca w j a a a o " Q 0 o v� °C _ Z o `n o o � o Q o STANDARD REPORT DELIVERY 0 DATE DUE EXPEDITED REPORT Q DELIVERY (SURCHARGE) DATE DUE LIENT (SITE) 17 CLIENT PHONE [�( Cp7 - a a N CLIET FRX -CLIENT NAME f CLIENT E-MAIL t cG+Xj m p w N CUENTADDRE S _ f�V � L ( J ;z�tL— r� `� r it J `¢ m r r t"" Y r NUMBER OF COOLERS SUBMITTED PER SHIPMENT., I COMPANY CONTRALTI G THIS WORK i! a li able I pp 1 SAMPLE SAMPLE IDENTIFICATION a�� o 0 NUMBER OF CONTAINERS SUBMITTED REMARKS DATE TIME 10 0 680-106381 Chain of Custody RybNOUISHED BY: prNArURE) DATE. TIME to> RELINQUISHED BY: 1sIGNATURQ DATE TIME RELNQU1SHED BY: (SIGNATURE) DATE TIME EC IVED :(SIGNATURE) DATE TIME RECEIVED BY: (SIGNATVRE) DATE TIME AECEIVEDBY: (SiCNASURI:) DATE TIME LABORATORY USE ONLY RECEIVED FOR LABORATORY BY: IRA E (sICNA RU � �� TIME r � CUSTODY INTACT YES O NO 0 CUSTODY SEAL NO. SAVANNAH L��NO. D LABORATORY REMARKS � Q_ L TAL8249-680(1008) Login Sample Receipt Checklist - 1 Client: Transport Services Co, Inc Job Number: 680-106381-1 Login Number: 106381 List Source: TestAmerica Savannah List Number. 1 Creator: Kicklighter, Marilyn D Question Answer Comment , �) Radioactivity wasn't checked or is <1= background as measured -by a NIA - survey meter. "( The cooler's custody seal, if present, is intact. True t Sample custody seals, if present, are intact. True I The cooler or samples do not appear to have been compromised or True € —" tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? NIA There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vot, for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is NIA <6mm (114"). Multiphasic samples are not present. True Samples do not require splitting or compvsiUng. True Residual Chlorine Checked. NIA TestAmerica Savannah Page 12 of 12 � � Y Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water -Quality General Permit No. NCG080000 Date submitted 7- ZZ - 2c)iLA CERTIFICATE OF COVERAGE NO. NCGO8 0 -Z ti R FACILITY NAME KN. an LLC_ COUNTY �ahr\s�ne PERSON COLLECTING SAMPLES v Ure � LABORATORY T 4,l , mew A Lab Cert. f# Z cl Comments on sample collection or analysis: RECEIVED JUL 2 8 2014 SAMPLE COLLECTION YEAR 2 of y CENTRAL FILES SAMPLE PERIOD XJan-June ❑July -Dec or ❑ Monthly' Tnn morpth�OG DISCHARGING TO CLASS ❑ORW ❑HQW [-]Trout ❑PNA ❑Zero -flow []Water Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes vino (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr 00530 00400 00556 Total Suspended Solids, mg/L pH,, Standard units Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L New Motor Oil Usage, Annual average gal/mo Benchmark - 50 or 100 see permit Within 6.0 - 9.0 15 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) O utfa I I No. Date Sample Collected, mo/dd/yr 00556 00530 00400 Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L Total -Suspended Solids, mg/L pH, Standard units Permit Limit - 15 50 or 100 see permit 6.0 - 9.0 LO �. O I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date /ZD t (first event sampled) Total Event Precipitation (inches): 0. `1 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations_" of `I 2y jo) (Dat ) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw##tab-4 SNA'U-250 last revised April 11, 2013 Pale 2 of 2 V, IN, 1 i O TestAmenca . S THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT --,� TestAmerica Laboratories, Inc. TestAmerica Savannah 5102 LaRoche Avenue ,;:: .�,• Savannah, GA 31404 Tel: (912)354-7858 v TestAmerica Job ID: 680-102598-1 �.e Client Project/Site: Stormwater Sampling - Selma, NC For: Transport Services Co, Inc 2001 Spring Rd. -.�. �. Suite 400 Oak Brook, Illinois 60523 Attn: James King 0 Authorized for release by: 71812014 12:35:55 PM Michele Kersey, Project Manager I (912)354-7858 michele.kersey@testamericainc.com ..........,.... LINKS ............ Review your project results th r ��ough C..,, TOU ril5lt [!5 fit: www.testam�ca inc,comE The test results in this report meet all 2003 NFLAC and 2009 TNl requirements for accredited parameters. exceptions are noted in this report. This report may not be reproduced except in full, and with wntten approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Definitions/Glossary Client: Transport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC Qualifiers General Chemistry Qualifier Qualifier Description ! " l TestAmerica Job ID: 680-102598-1 U Indicates the analyte was analyzed for but not detected. NE Glossary - - - - - Abbreviation These commonly used abbreviations may or may not be present In this report. o Listed under the "0" column to designate that the result is reported on a dry weight basis I .. %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid Ep DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalstanion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration t n. MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MID or E D L if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEE Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Savannah Page 2 of 12 Sample Summary Client: Transport Services Co, Inc TestAmerica Job ID: 680-102598-1 Project/Site: Stormwater Sampling - Selma, NC Lab Sample ID Client Sample ID Matrix collected Received 680-102598-1 Storm Water Outfall #1 Water 06120Y14 12:30 06/23/14 09:30 TestAmerica Savannah Page 3 of 12 Client: Transport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC Job ID: 680-102598-1 Laboratory: TestAmerica Savannah Narrative Case Narrative CASE NARRATIVE Client: Transport Services Co, Inc Project: Stormwater Sampling -Selma, NC Report Number: 680-102598-1 11 TestAmerica Job ID: 680-102598-1 - r With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required. RECEIPT The sample was received on 6/2312014 9:30 AK the sample arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 24.20 C. NOTE: Per Jim King, please proceed with analysis for samples received outside of temperature. OIL AND GREASE AND TPH Sample Storm Water Outfall #1 (680-102598-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A. The samples were prepared and analyzed on 07/01/2014, No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. TOTAL SUSPENDED SOLIDS Sample Storm Water Outfall #1 (680-102598-1) was analyzed for total suspended solids in accordance with SM 2540D, The samples were analyzed on 06/2612014, No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page Page 4 of 12 TestAmerica Savannah Client: Transport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC Client Sample ID: Storm Water Outfall ##1 Date Collected: 06120114 12:30 Date Received: 06123/14 09:30 F, General Chemistry j Analyte Oil & Grease (HEM) Total Petroleum Hydrocarbons (1664A) Analyte Total Suspended Solids Client Sample Results Result Qualifier RL MDL Unit 5.2 U 5.2 1.4 mg/L 5.2 U 5.2 1.4 rrmglL Result Qualifier RL RL Unit 16 5,0 5.0 mg/L 7 TestAmerica Job ID: 680-102598-1 L Lab Sample ID: 68O-102598-1 Matrix: Water r-- D Prepared Analyzed DII Fac 07101/1415:03 071011141T43 1 ww` 07101/1415:03 07101/1419:43 1 G D Prepared Analyzed Dil Fac J 06126114 11:09 1 TestAmerica Savannah Page 5 of 12 Client: Transport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC Method: 1664A - HEM and SGT-HEM Lab Sample ID: MB 680-337163/21-A Matrix: Water Analysis Batch: 337231 Analyte Oil & Grease (HEM) Total Petroleum Hydrocarbons (1664A) Lab Sample ID: LCS 680-337163122-A Matrix: Water Analysis Batch: 337231 QC Sample Results MB MB Result Qualifler RL MDL Unit 4.9 U 4.9 1.4 m91L 4.9 U 4.9 1.4 mglL Spike LCS LCS TestAmerica Job ID: 680-102598-1--- Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 337163 D Prepared Analyzed DII Fact{ 07/01114 15'.03 07101114 19:43 1 07/01/14 1&03 07/01114 19:43 1 rf L. Client Sample ID: Lab Control Sample i Prep Type: TotalINA !. Prep Batch: 337163 I� %Rec. i Analyte Added Result Qualifier Unit D %Rec Limits Oil & Grease (HEM) 39.4 36.8 mg1L 93 78- 114 Total Petroleum Hydrocarbons 19.7 21.1 mg1L 107 64 - 132 (1664A) Lab Sample ID: LCSD 680-337163/23-A i Client Sample ID: Lab Control Sample Dup i Matrix: Water Prep Type: Total/NA Analysis Batch: 337231 Prep Batch: 337163 i Spike LCSD LCSD %Rec, RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Oil & Grease (HEM) 39.9 40.3 mg1L 101 78- 114 9 18 Total Petroleum Hydrocarbons 20.0 20.8 mglL 104 64. 132 1 34 4 (1664A) Method: 2540 D-2011 - Total Suspended Solids Dried at 103-105°C Lab Sample ID: MB 680-336374/1 Client Sample ID: Method Blank Matrix:.Water Prep Type: Total/NA Analysis Batch: 336374 MB Me Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 5,0 U 5.0 5.0 1 99 06126114 10:44 1 Lab Sample ID: LCS 680-33637412 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 336374 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 20.0 22.0 mglL 110 80- 120 Lab Sample ID: LCSD 680-33637413 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 336374 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 20,0 24.0 mg/L 120 80 - 120 9 25 TestAmerica Savannah Page 6 of 12 Client: Transport Services Co, Inc Project/Site. Stormwater Sampling - Selma, NC General Chemistry Analysis Batch: 336374 Lab Sample ID CllentSample ID 680.102598-1 LCS 680-33637412 LCSD 680-33637413 I i MB 680-33637411 Prep Batch: 337163 Lab Sample ID 680-102598-1 LCS 680-337163122-A LCSD 680.337163123-A I MB 680-337163121-A Analysis Batch: 337231 Lab Sample ID 680-102596-1 LCS 680-337163122-A LCSD 66C-337163/23-A MB 68C-337163121-A Storm Water Outfall #1 Lab Control Sample Lab Control Sample Dup Method Blank QC Association Summary Prep Type Matrix Total/NA Water Total/NA Water Total/NA Water Total/NA Water Client Sample ID Prep Type Matrix Storm Water Outfall #1 TotaUNA Water Lab Control Sample TotaUNA Water Lab Control Sample Dup TotallNA Water Method Blank TotallNA Water 31 TestAmerica Job ID: 680-102598-1 -- - i I ._.. Method 2540 D-201 t 2540 D-2011 2540 D-2011 2540 D-2011 Method 1664A 1664A 1664A 1664A Prep Batch w Prep Batch E 'i a, Client Sample ID Prep Type Matrix Method Prep Batch Storm Water Outfall # 1 Total/NA Water 1664A 337163 Lab Control Sample TOtal1NA Water 1664A 337163 ; Lab Control Sample Dup TOtal1NA Water 1664A 337163 Method Blank Total/NA Water 1664A 337163 TestArnerica Savannah Page 7 of 12 Lab Chronicle Client: Transport Services Co, Inc Project/Site'. Stormwater Sampling - Selma, NC Client Sample ID: Storm Water Outfall #1 Date Collected: 06120/1412:30 Date Received: 06/23114 09:30 Batch Batch oil Initial Prep Type Type Method Run Factor Amount Total/NA Prep 1664A 485 mL Total/NA Analysis 1664A 1 485 mL Instrument ID: NoEquip Final Batch Amount Number 500 mL 337163 500 mL 337231 Total/NA Analysis 2540 D-2011 1 200 mL 200 mL 335374 Instrument ID: NOEOUIP Laboratory References: TAL SAV = TestAmehra Savannah, 5102 La Rothe Avenue, Savannah, GA 31404, TEL (912)354-7858 R] TestAmerica Job ID: 680-102598-1 -- . Lab Sample ID: 680-102598-1 Matrix: Water ( r, jIL I Prepared 1� or Analyzed Analyst Lab 07/01/14 15:03 ALC TAL SAV 07101l14 19:43 ALC TAL SAV _ 06/26114 11:09 LBH TAL SAV — TestAmerica Savannah Page 8 of 12 Certification Summary Client: Transport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC Laboratory: TestAmerica Savannah The.certirications listed below are applicable to this report, M TestAmerica Job ID: 680-102598-1 Authority Program EPA Region Certification ID Expiration Date North Carolina (WWISW) State Program 4 269 12-31-14 Pennsylvania NELAP 3 68-00474 06-30-15 Virginia NELAP 3 460161 06-14-15 TestAmerica Savannah 'r/ � toy a Page 9 of 12 Method Summary Client: Transport Services Co, Inc Project/Site: Stormwater Sampling - Selma, NC TestAmerica Job ID: 680-102598-1 -[ Method 1564A 2540 D-2011 Method Description HEM and SGT-HEM Total Suspended Solids Dried at 103-105°G Protocol 1664A SM Laboratory TAL SAV TAL SAV Protocol References; 1664A = EPA-821-98-002 SM = "Standard Methods For The Examination Of Water And Wastewater', Laboratory References: TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 TestAmerica Savannah I 'd M r._. v�. Page 10 of 12 a V, Serial Number 77307 ANALYSIS REQUEST AND CHAIN OR CUSTODY RECORD TestAmeri c THE LEADER 1N ENVIRONMENTAL TESTING r m TestAmerica Savannah Website: www-testamerirairic.com 5102 LaRoche Avenue Phone: (912) 054-7858 Savannah, GA 31404 Fax (912) 352-61 65 Alternate Laboratory Name/Location Phase: Fax: PR ECT RI FERENC 'THY J p( 11I j TAL{LAB) PROJECT MANAGER PROJECT NO. P.O. NUMBER PROJECT LOCATiOW (STATE} k) C CONTRACT NO. r �? F «o 0 MATRIX TYPE Lu o p cc 0 N . a z o 4p a o a HEQUIREE)ANALYSIS - PAGE, QF f — — STANDARD REPORT DELIVERY DATE DUE --- EXNF:DITEf]RwPORT DELIVERY (SURCHARGE) DATE DUE --- LiENi (SITE } P CLIENT NA V)L 5,PO ['7— CLIENT PHONE CLIENT FAX CLIENTS MAIL .b -NA Y V%e {� Jka + . C O M CLIENTAOD�S r� �- C�n��r k�C1 7� 1 c . �.. r �• _� _ NUMBER OF COOLERS SUBMITT> p NER SHIPMENT COMPANY OONTRADTI G THIS WORK (ii applicable) SAMPLE SAMPLE IDENTIFICATION NUMBEH OF CONTAINERS SUBM[TTEO REMARKS DATE TIME L� a�rn S ©� c�tl.a t- Out 6( �_ (; _ 5�►�P{ems �� I 680-102598 Chain of Custody -- INQUISHE : [SIGNA7URE V DATE' TIME RELINQUISHED BY: [SIGNATURE) � DATE TIME REUNOUiSHED BY. (SIGNATURE) DATE TIME EIVED BY: pGNATUHE) DA E TOME RECEIVED BY:tsIMATURr) DATE TIME HEGEfVED BY: (srNATURE) — OATS TIME LABORATORY USE ONLY E TIME CUSTODY INTACT CUSTODY SAVANNAH LABORATORY REMARKS RECEIVED FOR LABORATORY BY: T/DF [srGNATuR[I YES jj,"!L oC NO srALNo. I �- --1 �S. /, _ Client: Transport Services Co, Inc Login Number: 102598 List Number: 1 Creator: Kicktighter, Marilyn D Question Login Sample Receipt Checklist Answer Comment Job Number: 680-102598-1 f List Source: TestAmerica Savannah ti ` F a� Radioactivity wasn't checked or is <!= background as measured by a survey NIA r--_—� meter. 7/ The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. ; F2� The cooler or samples do not appear to have been compromised or True —� tampered with. Samples were received on ice. False melted Cooler Temperature is acceptable. True Cooler Temperature is recorded. True 24.2 C COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? NIA There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True one 500-amber glass rec broken for Oil & Grease Sample collection dateltimes are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol, for all requested analyses, incl. any requested True MSIMSDS Containers requiring zero headspace have no headspace or bubble is NIA <6mm (114"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked, NIA TestAmerica Savannah Page 12 of 12 ICE N ©V.4NTAGE GROUP, INC. Advantage Tank Lines • BXl Cryogenic rransportation • oistrech • Jack B. Kelley • KAG Logistics • Klemm Tank Lines KAG !Nest • Kenan Transport • North Canton Transfer • Petro Chemical Transport • Transport Service Co. July 24, 2014 Division of Water Quality ATTN: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 VIA UPS: I 6V9 340 02 9281 3894 RE: SDO Monitoring Report Permit No. NCGO80249 To Whom It May Concern, Please find enclosed Kenan Transport, LLC's monitoring report for the above reference permit number for the 151 half of 2014. Please don't hesitate to contact me directly with any Questions or concerns at 630/472-5934 or james.king@thekag.com. thekag.com. Respectfully Submitted, qxwm James King, CHMM Director of Environmental Quality and Compliance 2001 Spring Road Oak Brook, IL 60523 Office:630-472-5934 i Fax: 630-472-0495 Cell: 630-853-4395 www.thekag.corn 2001 Spring Road, Suite 400 • Oak Brook, IL 60523 • 630-472-5900 • 630-472-0495 (fax) • www.thekag.com