NCG060039_COMPLETE FILE - HISTORICAL_20111123 (FIX)

STORMWATER DIVISION CODI
NCG PERMITS
PERMIT NO. jV C" D�3
DOC TYPE A HISTORICAL FILE
❑ MONITORING REPOP
DOC DATE o A ri P a 3
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Division of Energy, Mineral & Land Resources
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Land QualitySection/Stormwater Permitting
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Pollutant Discharge Elimination System
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PERMIT NAME/OWNERSHIP CHANGE FORM
FOR AGENCY USE ONLY
Date Received
Year
Month
Day
I. Please enter the permit number for which the change is requested.
NPDES Permit (or) Certificate of Coverage
N C $ 0 N G G 0 6 0 0 3 9
II. Permit status prior to requested change.
a. Permit issued to (company name): Grifols Therapeutics Inc.
b. Person legally responsible for permit: Sergi Roura
First M l Last
RFc,ENED
to 0 2018
Facility name (discharge):
d. Facility address:
President, North American Facilities
Title
8368 US Hwy 70 Business West
Permit Holder Mailing Address
Clayton NC 27520
City State Zip
[phone] [phone]
Phone Fax
Grifols Therapeutics Inc.
8368 US Hwy 70 Business West
Address
Clayton NC 27520
City State Zip
e. Facility contact person: David D. Auge [phone]
First I M11 Last Phone
Ill. Please provide the following for the requested change (revised permit).
a. Request for change is a result of: ❑ Change in ownership of the facility
® Name change of the facility or owner
If other please explain:
b. Permit issued to (company name):
Grifols Therapeutics_ LLC
c. Person legally responsible for permit:
Juan Antonio Garcia Diaz
First M I Last
President, Grifols Therapeutics LLC
Title
8368 US Hwy 70 Business West
Permit Holdcr Mailing Address
Clayton NC 27520
City State Zip
[phone] juanantonio.garcia a)grifols.com
Phone E-mail Address
d. Facility name (discharge):
Grifols Thera eutics LLC
e. Facility address:
8368 US Hwy 70 Business West 1/
Address
Clayton NC 27520
City State Zip
E Facility contact person:
David D Auge
First MI Last
[phone] [e-mail]
grifols.com
Phone E-mail Address
N. Permit contact information (if different from the person legally responsible for the permit)
Revised Jan. 27, 2014

NPDES PERMIT NAME/OWNERSHIP CHANGE FORM
Page 2 of 2
Permit contact: David D Auge
First M I Last
Manager, Environmental /
Title
8368 US Hwy 70 Business West
Mailing Address
Clayton NC 27520
City State Zip
[phone] [e-mail]
Phone - E-mail Address
V. Will the permitted facility continue to conduct the same industrial activities conducted prior
to this ownership or name change?
® Yes
❑ No (please explain)
V1 Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is required for an ownership change request. Articles of incorporation are
not sufficient for an ownership change.
The certifications below must be completed and signed by hoth the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Certification is sufficient.
PERM ITTEE CERTIFICATION (Permit holder prior to ownership change):
1, , attest that this application for a name/ownership change has been reviewed and is accurate and
complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned as incomplete.
Signature Date
APPLICANT CERTIFICATION
I, Juan Antonio Garcia Diaz, attest that this application for a name/ownership change has been reviewed
and is accurate and complete to the best of my knowledge. I understand that if all required parts of this
application are not completed aiad LhaLif all required supporting information is not included, this application
package will be returned a inc n
Signature\j Date
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Revised Jan. 27.2014

pF WArEi4 Beverly Eaves Perdue, Governor
CIO� q� Dee Freeman, Secretary
>_ North Carolina Department or Environment and Natural Resources
a -c
Coleen IF. Sullins, Director
Division of Water Quality
SURFACE WATER PROTECTION SECTION
PERMIT NAME/OWNERSHIP CHANGE FORM
Please enter the permit number for which the change is requested.
NPDES Permit (or) Certificate of Coverage
N C 1 S 10 N 1 G 1 G- rr``
Permit status prior to requested change. O '3 2 V
a. Pert -nit issued to (company name): Talecris Biotherapeutics, Inc.
b. Person legally responsible for permit: Mary J Kuhn
First MI- Last
Executive Vice President of Operations
'Title
8368 US 70 Bus. Hwy W
Permit Holder Mailing Address
Cla�ton NC 27520
City State Zip
[phone] [phone]
Phone Fax
c. Facility name (discharge): Talecris Biotherapeutics, Inc.
d. Facility address: 8368 US 70 Bus. Hw y W
Address
Clayton NC 27520
City State lip
e. Facility contact person: David D. Auge (919)3 9-4375
First / MI / Vast Phone
Please provide the following for the requested change (revised permit).
a. Request for change is a result of: ❑ Change in ownership of the facility
® Name change of the facility or owner
If other please explain:
b. Permit issued to (company name):
c. Person legally responsible for permit:
e. Facility address:
f Facility contact person:
GOVfi.G/fir� >/f'.L 9/rJ Q,i'�
Grifols Therapeutics
Matt' J Kuhn
First MI Last
_ President, North American Manufacturing Operations
Title
8368 US 70 Bus. Hwy W
Permit I folder Mailing Address
Clayton _NC 27520
City Kt4hnstate Zip
[phone] Marykwtr rr grifols.com
Phone E-mail Address
Grifols Therapeutics
8368 US 70 Bits. Hwy
Address
Clayton NC 27520
City state Zip
_ David D _Auge
First M1 Last
(9 19-359-43 75) _ David,auge ra grifols.com
Phone E-mail Address
Revised 812008

PERMIT NAME/OWNERSHIP CHANGE FORM
'Page 2 of 2
IV. Permit contact information (if different from the person legally responsible for the pert -nit)
Permit contact:
First Ml Last
Title
Mailing Address
Ci(y State zip
(
Phone E-mail Address
V. Will the permitted facility continue to conduct the same industrial activities conducted prior
to this ownership or name change?
® Yes
❑ No (piease explain)
VI. Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
® This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is required for an ownership change request. Articles of incorporation are
not sufficient for an ownership change.
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Certification is sufficient.
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
I, Mary J. Kuhn; attest that this application for a name/ownership change has been reviewed and is accurate
and complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned as incomplete.
rl'21 201 f
Signature Date
APPLICANT CERTIFICATION
I, Mary J. Kuhn, attest that this application for a name/ownership change has been reviewed and is accurate
and complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned as incomplete.
If Zo I
Signature Date
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Water Quality
Surface Water Protection Section
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Revised 712008

`0
�0F wA LIZ9
e ce Yed
�trOW. D/r-u Vi v!
0 ewclx_ '/ 111.2_512_,�)l /
/ Beverly Caves Perdue, Governor
L e Dee Freeman, Secretary
Nort Carolina Department of Environment and Natural Resources
Colcen H. Sullins, Director
Division ol' WdtCr Quality
SURFACE WATER PROTECTION SECTION
PERMIT NAME/OWNERSHIP CHANGE FORM
Please enter the permit number for which the change is requested.
NPDES Permit (or} Cet•tificate of Coverage
N C S 0 N C ,G. 1 0
Permit status nLior to requested change. kj C 0 r0 0
a. Permit issued to (company name): Talecris Biothera eutics, Inc...
b. Person legally responsible for permit: Mary J Kuhn
First MI last
Executive Vice President of Operations
Title
8368 US 70 Bus. Hwy W
Permit I lolder Mailing Address
Clayton NC 27520
City State Zip
[phone] [phone]
Phone Fax
c. Facility name (discharge): Talecris B iot herapeu tics, Inc.
d. Facility address: 8368 US 70 Bus,,Hwy W
Address
Clayton NC 27520
City State Zip
e. Facility contact person: David D. Au e 919) 359-437S
First / MI / Last Phone
Please provide the following for the requested change (revised permit).
a. Request for chatzge is a result of: ❑ Change in ownership of the facility
® Name change of the facility or owner
If other please explain:
b. Permit issued to (company name):
c. Person legally responsible for permit;
Grifols Therapeutics _
Mary J Kuhn
First MI Last
President, North American Manufacturing Operations_
Title
8368 US 70 Bus. Hwy W
Permit 1-lolder Mailing Address
Clayton NC 27520
City
+tAhn State "Zip
(919 ) 359-4393 Mar y (@,grifols,com
Phone E-mail Address
d. Facility name (discharge): Grifols Therapeutics
e. Facility address: 8368 US 70 Bus. Hwy W
Address
Clayton NC 27520
City State Zip
f. Facility contact person: David T D Auge
First MI Last
(919-359-4375) David.auge@grifoIs, cot n
Phone E-mail Address
Revised 812008

•
PERMIT NAMEIOWNERSHIP CHANGE FORM
Page 2 of 2
1V. Permit contact information (ifdifferent from the person legally responsible for the permit)
Permit contact:
First MI Last
Title
Mailing Address
City State Zip
Phone F-mail Address
V Will the permitted facility continue to conduct the same industrial activities conducted prior•
to this ownership or name change?
® Yes
❑ No (please explain)
VI Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
® This completed application is required for both name change and/or ownership change
requests.
❑ Lcgal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is required for an ownership change request. Articles of incorporation are
not sufficient for an ownership change.
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Cettiftcation is sufficient.
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
1, Mary J. Kuhn, attest that this application for a name/ownership change has been reviewed and is accurate
and complete to the best of my knowledge. I understand that if all required pacts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned as incomplete.
Signature Date
APPLICANT CERTIFICATION
I, Mary J. Kuhn, attest that this application for a name/ownership change has been reviewed and is accurate
and complete to the best of my knowledge. 1 understand that if all required pants of this application are not
completed and that if ail required supporting information is trot included, this application package will be
returned as incomplete.
o I
Signature Date
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Water Quality
Surface Water Protection Section
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Revised 712008

North Carolina Department of Environment and Natural Resources
Division of Water Quality
Stormwater Upset, Spill, or Bypass 5-Day Reporting Form
(Please Print or Type Use Attachments if Needed)
Permittee: _Talecris Biotherapeutics, Inc.
Facility Name
Incident Started:
Incident Ended
Level of Treatment:
Clayton site
Date: _August 8, 2011
Date: _August 8, 2011
Permit Number: COC Number NCG0600039
County: _Johnston
Time: 1800
Time: 2200
_X_None _Primary Treatment _Secondary Treatment ,Chlorination/Dis infection Only
Estimated Volume of Spill/Bypass: 62 gallons _(must be given even if it is a rough estimate)
Did the Spill/Bypass reach the Surface Waters? _Yes _X_No
If yes, please list the following:
Volume Reaching Surface Waters: Surface Water Name:
Did the Spill/Bypass result in a Fish Kill? Yes _X—No
Was WWTP compliant with permit requirements? Yes No—X_ NA
Were samples taken during event? —X_Yes No
Source of the_Upset/Spill/Bypass (Location or Treatment Unit):
Cooling tower west of E510.
Cause or Reason for the Upset/Spill/Bypass:
The leak appears to have been caused by a pump failure at the base of the cooling tower.
Describe the Repairs Made or Actions Taken:
The pump was removed from service and the water diked and stopped.
Spill/Bypass Reporting Form (August 1997)

Stormwater Upset, Spill, or Bypass 5-Day Reporting Form
Page 2
Action Taken to Contain Spill, Clean Up and Rem ediate the Site (if applicable):
NA
Action Taken or Proposed to be Taken to Prevent Occurrences:
Grifols is planning on the removal of the cooling tower.
Additional Comments About the Event:
24-Hour Report Made To: Division of Water Quality _X_ Emergency Management
Contact Name: Mitch Hayes _ Date: August 11, 2011 Time: 0900
Other Agencies Notified (Health Dept, etc): None
Person Reporting Event: David Auge Phone Number: 919-359-4375
Did DWQ Request an Additional Written Report? _Yes _X_No
If Yes, What Additional Information is Needed:
Spill/Bypass Reporting Form (August 1997)

NC®ENR
North Carolina Department of Environment and Natural Resources
Division at Water Quality
Beverly Eaves Perdue Charles Wakild, P. E.
Governor Director
December 4, 2012
Sargi Roura
Grifols Therapeutics Inc
8368 Highway 70 West
Clayton, INC 27520
Dee Freeman
Secretary
Subject: NPDES Stormwater Permit Coverage Renewal
Grifols Therapeutics Inc
COC Number NCG060039
Johnston County
Dear Permittee:
In response to your renewal application for continued coverage under stormwater General Permit NCG060000
the Division of Water Quality (DWQ) is forwarding herewith the reissued General Permit. This permit is
reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of
Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October
15, 2007 (or as subsequently amended). -
The following information is included with your permit package:
• A new Certificate of Coverage (COC)
• A copy of General Permit NCG060000
• A copy of the Technical Bulletin for the General Permit
• Two copies of the Discharge Monitoring Report (DMR) Form
• Two copies of the Qualitative Monitoring Report Form
The General Permit authorizes discharges of stormwater, and it specifies your obligations for discharge
controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself
with all the changes in the reissued permit. Your facility has six (6) months from the time of receipt of the
permit to update your current SPPP to reflect all new permit requirements.
The first sample period of your permit begins January 1, 2013. Your facility must sample a "measureable
storm event" beginning during the periods beginning January 1 and July 1 of every year (or, if applicable,
report "No Flow," as outlined in Part III, Section E). Also, please note that Tier 3 Actions in Part 11 of your
permit are triggered by benchmark exceed ances on four occasions beginning on the effective date of this
permit and do not count prior exceedances.
The more significant changes in the General Permit since your last COC was issued are noted either in the
Draft Permit Fact Sheet that accompanied the public notice (http: /portal.ncdenr.or /�/wq ws/su/current-
notices), or in the Response to Comments / Summary of Changes and Technical Bulletin documents that are
posted on the Stormwater Permitting Unit's website with the new General Permit. Please visit
http://portal.ncdenr.orp/web/wq/ws/suZnpdessw (click on 'General Permits' tab) to review that information
for your specific General Permit carefully.
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury SI, Ralegh, North Carolina 27604
Phone: 919-"r17-6300 i FAX [phone]".;2
Internet: wwvv.rimaterquality.ong
One
NorthCarol ina
An EqualEm; er

Sargi Roura ,
December 4, 2012
Page 2 of 2
Some of the changes include:
• Part II:
• Section A: The Stormwater Pollution Prevention Plan (SPPP) section, if applicable, has been updated
to the most current language of our permits. Additional conditions for specific industry sectors have
been added to the SPPP requirements in some cases.
• Sections B, C: Failure to perform analytical stormwater monitoring may result in the Division requiring
that the permittee begin a monthly sampling scheme.
• Sections B, C: A lower TSS benchmark of SO mg/I for HQW, ORW, PNA and Tr Waters applies to these
more sensitive waters.
• Sections B, C: The monitoring parameter Oil & Grease (O&G) has been replaced by the parameter
Total Petroleum Hydrocarbons (TPH) for vehicle maintenance areas, and in some cases, other
analytical monitoring requirements.
• Sections B, C, D: Inability to sample due to adverse weather must be recorded in the SPPP, or in
separate on -site records if your General Permit does not require an SPPP. Adverse weather is defined
in the "Definitions" section of the permit.
• Sections B, C: The term "Representative Storm Event" has been replaced by "Measurable Storm
Event." A measurable storm event is defined in the permit.
• Section D: If the permittee fails to respond effectively to problems identified by qualitative
monitoring, DWQ may require the permittee to perform corrective action.
Please review Parts III and IV to understand the Standard Conditions of your new NPDES General Permit,
including Compliance and liability, Reporting, Monitoring and Records requirements; Operation and
Maintenance obligations; and Definitions. Please note that all samples analyzed in accordance with the terms
of this permit must be submitted to the Division on Discharge Monitoring Report (DMR) forms available on
the Stormwater Permitting Unit's website above. DMR forms must be delivered to the Division no later than
30 days from the date the facility receives the sampling results from the laboratory. Also note that existing
permittees do not need to submit a renewal request prior to expiration unless directed by the Division.
Your coverage under the General Permit is transferable only through the specific action of DWQ. This permit
does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it
relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law,
rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit
package, please contact the Division's Stormwater Permitting Unit at [phone].
Sincerely,
for Charles Wakild, P.E.
cc: DWQ Central Files
Stormwater Permitting Unit Files
Raleigh Regional Office

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE No. NCG060039
STORMWATER
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Grifols Therapeutics Inc
is hereby authorized to discharge stormwater from a facility located at:
Grifols Therapeutics Inc
8368 Hwy 70 W
Clayton
Johnston County
to receiving waters designated as NEUSE RIVER, a class WS-IV;NSW waterbody in the Neuse
River Basin in accordance with the effluent limitations, monitoring requirements, and other
conditions set forth in Parts I, I1, III, and IV of General Permit No. NCG060000 as attached.
This certificate of coverage shall become effective December 4, 2012.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this 4th day of December, 2012.
for Charles Wakild, P.E,, Director
Division of Water Quality
By Authority of the Environmental Management Commission

Hayes, Mitch
From: Richmond, Martin
Sent: Thursday, August 04, 2011 8:59 AM
To: Auge, David
Cc: Smith, Danny; Hayes, Mitch; Valentine, Thad
Subject: RE: Talecris--North Pond Sediment Removal
Attachments: image001.gif; image002.gif
David — go ahead and do what you need to do.
Mitch — this is site where they are breaching a dam and draining a pond, which turns out to be their permitted
stormwater outfall. This was not brought up during our site meeting with the Corps, and I feel like I'm having to approve
permit violations. There is also a large construction site adjacent. I would simply like to ensure the work they are doing
is not causing the excessive sediment in the sample collection.
Thad — this is the one. Please update when you get a chance.
Thanks, Martin
From. Auge, David [mailto:[e-mail]]
Sent: Wednesday, August 03, 2011 7:47 PM
To: Richmond, Martin
Subject: Fwd: Talecris--North Pond Sediment Removal
Just need confirmation that our approach is acceptable. Please respond.
David
Sent from my iPhone
Begin forwarded message:
From: "Auge, David" <[e-mail]>
Date: July 28, 2011 8:43:36 AM EDT
To: "[e-mail]" <martin.richmond@ncdenr.g_ov>,
"lames.c.lastinger(@usace.army.mil" <lames.c.lastingerPusace.army.mil>
Cc: Ginny Ferrara <[e-mail]>, Michael Hall <HaIIMSRobg.com>
Subject: FW: Talecris--North Pond Sediment Removal
Gentlemen,
Thank you for reviewing our efforts to alleviate the siltation issue resulting in stormwater permit TSS
exceedances. In summary, the excessive silt is causing our monthly TSS readings of the stormwater
outfall to exceed the 100 mglL limit.
Please respond with your approvallcomment concerning our approach to address this problem before the
end of the day.

We are preparing to begin the project as soon as possible and would like a confirmation, through this e-
mail of your consent.
Thanks.
David D. Auge
Manager, Environmental, Safety and Security
Grifols, Inc.
8368 US 70 Business West
Clayton, NC 27520
Phone: [phone]
Cell: [phone]
Fax: [phone]
[e-mail]
Please consider your environmental responsibility before printing this e-mail
"Attilude is the difference between Ordeal and Adventure."
From: Auge, David
Sent: Monday, July 25, 2011 4:59 PM
To: 'martin. rich [e-mail]'
Cc: Michael Hall; 'Ginny Ferrara'
Subject: FW: Talecris--North Pond Sediment Removal
Martin,
Thanks for reviewing our situation. As discussed during today's phone conversation, the silt
buildup in the north pond, has caused stormwater permit violations during recent testing.
Talecris (now Grifols) requests to remove the sediment in the newly formed stream bed to
alleviate the problem. As I understand from our discussion, since we are still in the
construction/maintenance phase, removal of the sediment and improvement of the BMP is
within the normal scope of what is expected.
A description of the steps and our concern about how to reach the excessive silt is explained in
the e-mail below sent to James Lastinger of the Corp of Engineers. Our intent is to remove the
check dam and the accumulation of liquefied sediment behind it, and then backfill with native
soil, as necessary, to maintain the current channel. This fill will be tapered into the existing
grade and seeded to prevent downcutting and erosion of the banks.
We would like to begin this work as soon as possible. Please let us know if this approach is
acceptable to you. I am available in the office if you have additional questions or comments.
Thanks again for your assistance.
David D. Auge
Manager, Environmental, Safety and Security
Grifols, Inc.
8368 US 70 Business West
Clayton, NC 27520
Phone: [phone]

North Carolina Department of Environment and Natural Resources
Division of Water Quality
`o) W A r�RQG
Stormwater Upset, Spill, or Bypass 5-Day Reporting Form
(Please Print or Type Use Attachments if Needed)
Permittee: _Talecris Biotherapeutics, Inc.
Facility Name: Clayton site
Incident Started
Incident Ended:
Level of Treatment:
Date: _August 3,2011_
Date: —August 3, 2011
Permit Number: COC Number_NCG0600039
County: _Johnston
Time: 0600
Time: 1600
_X_None Primary Treatment _Secondary Treatment _Chlorination/Dis infection Only
Estimated Volume of Spill/Bypass: 75 gallons _(must be given even if it is a rough estimate)
Did the Spill/Bypass reach the Surface Waters? _X_Yes ,No
If yes, please list the following:
Volume Reaching Surface Waters: _75
Did the Spill/Bypass result in a Fish Kill?
Was WWTP compliant with permit requirements?
Surface Water Name: Tributary to the Neuse River_
Yes _X_No
Were samples taken during event? _X_Yes No
Yes No_X_ NA
Source of the UpsetlSpiIIIBVpass (Location or Treatment Unit)
A leak from the Alpha Zone 1 Glycol surge tank on top of B300.
Cause or Reason for the Upset/Spill/Bypass:
The leak appears to have been caused by a brake in the piping from the tank through the roof.
Describe the Repairs Made or Actions Taken:
The remaining ethylene glycol was removed from the system, the storm drain was protected by spill socks
and maintenance personnel began repairing the li ne.
Spill/Bypass Reporting Form (August 1997)

WWTP Upset, Spill, or Bypass 5-Day Reporting Form
Page 2
Action Taken to Contain Spill, Clean Up and Rem ediate the Site (if applicable):
NA
Action Taken or Proposed to be Taken to Prevent Occurrences:
Grifols is reviewing maintenance procedures for roof mounted Glycol tanks.
Additional Comments About the Event:
24-Hour Report Made To: Division of Water Quality _X_ Emergency Management
Contact Name: Mitch Hayes - Date: August 3, 2011 Time: 1645
Other Agencies Notified (Health Dept, etc)
None
Person Reporting Event: David Auge Phone Number: �919-359-4375
Did DWQ Request an Additional Written Report? —Yes _X_No
If Yes, What Additional Information is Needed:
Spill/Bypass Reporting Form (August 1997)

Cell: [phone]
Fax: [phone]
[e-mail]
Please consider your environmental responsibility before printing this e-mail
"Attitude is the difference between Ordeal and Adventure. "
From: Michael Hall [mailto:[e-mail]]
Sent: Friday, July 22, 2011 11:13 AM
To: [e-mail]
Cc: Ginny Ferrara; Auge, David
Subject: Talecris--North Pond Sediment Removal
James:
Good morning. Thank you for taking the time to talk with me this morning. After my discussion with
you, 1 spoke with David Auge at Talecris, Ginny Ferrara, one of our construction managers, and the
contractor that will remove the sediment. Our assessment is that we cannot, without causing
considerable impact, access the check dam and sediment accumulation with matting and a backhoe.
Our recommendation is to use a long -reach track hoe. With this equipment, we can access a more
limited area of the former pond bed, and reach across the rest of the area with the arm on the track
hoe. This is consistent with the intent of the approach you recommended, insofar as it minimizes the
impact to the potential wetlands area. The intent is to remove the check dam and the accumulation of
liquefied sediment behind it, and then backfill with native soil, as necessary, to maintain the current
channel. This fill will be tapered into the existing grade and seeded to prevent downcutting and erosion
of the banks.
It is Talecris's intent to begin this work as soon as possible. Please let us know if this approach is
acceptable to you without a permit. I am available in the office if you have additional questions or
comments. Thanks again for your assistance with this.
Mike
rinGBRICN 6 GCRC
Michael Hall, PG
Managing Scientist
O'BRIEN & GERE
2610 Wycliff Road, Suite 104
Raleigh, NC 27607
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North Carolina Department of Environment and Natural Resources
Division of Water Quality
`obCF w A r�RQ,✓
65
l
0 Niii� 'C
Stormwater Upset, Spill, or Bypass 5-Day Reporting Form
(Please Print or Type Use Attachments if Needed)
Permittee: Talecris Biotherapeutics, Inc.,
Facility Name
Incident Started
Incident Ended
Level of Treatment:
Clayton site
Date: June 27,2011
Date: July 1, 2011
Permit Number: COC Number NCG0600039
County: Johnston
Time: 1800.
Time: 1230
_X_None _Primary Treatment _Secondary TreatmentChlorination/Disinfection Only
Estimated Volume of Spill/Bypass: 88 gallons (must be given even if it is a rough estimate)
Did the Spill/Bypass reach the Surface Waters? X Yes No
If yes, please list the following. -
Volume Reaching Surface Waters: 88
Did the Spill/Bypass result in a Fish Kill?
Was WWTP compliant with permit requirements?
Surface Water Name
Yes ,X_No
Were samples taken during event? _X_Yes No
Tributary to the Neuse River
Yes No—X_ NA
Source of the Upset/Spill/Bypass Location or Treatment Unit):
The ethylene glycol was traced back to a leaking HVAC cooling coil on unit #146. HVAC unit #146 is on the
east side of B300 and serves B300 filling.
Cause or Reason for the Upset/Spill/Bypass:
A leaking HVAC cooling coil on unit #146
Describe the Repairs Made or Actions Taken:
The pressure trend data which is how we gage system volume change shows that about Monday of this
week we started to have a pressure drop indicative of a leak. Prior to that the trends look pretty flat.
Spill/Bypass Reporting Form (August 1997)

North Carolina Department of Environment and Natural Resources
Division of Water Quality
System remains a little low .... Once we let it stabilize for a few days we will top off to get it back to
normal.
Maintenance is working on a repair which will be a challenge to repair in place. Alternate plans (i.e.
removal to repair) up to and including ordering a replacement coil are in the works.
Spill/Bypass Reporting Form (August 1997)

WWTP Upset, Spill, or Bypass 5-Day Reporting Form
Page 2
Action Taken to Contain Spill, Clean Up and Remediate the Site (if applicable):
A vacuum truck from Garco arrived at Clayton about 7 p.m on Friday July 1, 2011. The truck removed glycol
from the stormwater ditch and from the pool at the terminus of the ditch. Total volume of water containing 2%
ethylene glycol was 6,632 gallons.
Action Taken or Proposed to be Taken to Prevent Occurrences:
Grifols is reviewing the policy of allowing roof mounted HVAC units to discharge condensate to the roof —
storm drain versus the process sewer.
Additional Comments About the Event:
24-Hour Report Made To: Division of Water Quality X_ Emergency Management
Contact Name: Mandy Hall _ Date: July 1, 2011 Time: 1630
Other Agencies Notified (Health Dept, etc): None
Person Reporting Event: David Auge Phone Number: _919-359-4375
Did DWQ Request an Additional Written Report? —Yes X—No
If Yes, What Additional Information is Needed:
Spill/Bypass Reporting Form (August 1997)

Standard Operating Procedure for SSO Calls
oo goy
1. Gather Required Information:
Date of call 06 IQki {O
Time of call
. n
Name of caller
Caller phone #
` 113
Facility name �r
County -T-0 514L71
Permit # (if available) _ NC 6 00 3
Start date 10 rx" Start time o6 f 0{ ((O AM PM
End date l .(D I o f 1 /0 End Time I p 0 (OPM
�M Estimated volume
54UrJ gall C01) Location
`u I T
�ll��Cal Cause
2� J
Steps taken to correct
IN
Rood of 13 IX" �3a 0 0368 HL,., `rd G
a
%[v,c4���eLe_iuer vein- l(� 0"-N eXr)YIS-('1 1--11,kl-
(I iPrPIn,.. Grin .x nnti% otn�nc. 4o fv cf C—e',-i.x
Did SpiII1SSO reach surface waters No
Name of Surface Water-�
Volume reaching surface waters ``
Conveyance �A&(n 5-tuAr- `tu.c�i�� �� 1,��[f�•+C+S or{o`
Did Spill/SSO result in fish kill q', ;-
Received by 0.k1A Co 6r^
2. Enter Spill/SSO into Access: W-A Q",'
Open the Microsoft Access file S:laccesslnotice24_2 (OR) S:laccessllncident
Open the required form
At the bottom left of the form, click on the right arrow -asterisk symbol to bring up the next blank form
Fill in the form and close Access
3. Enter into RIMS
Log into the public portal version of B1MS(http:llbims.enr.state.nc.us:7001/Welcome.do)
Go to Tasks, Incident, Enter Incident
For SSO, fill in the SSO and 24 hour forms, record the incident number, then save the file and close.
For Spills, check the type of spill box, fill in the Incident report, record the incident number and close..
4. Comments:

-B1 �S 26o5bz821P
Standard Operating Procedure for SSO Calls
1. Gather Required Information:
Date of call D a2j
Time of call
Name of caller
Caller phone # C 3SR Cj �3' L(>_�
Facility.name -Ta'/ _ GY f S -91 �4 D o_(-!kL,_(f _
County j Ott Y) �o ki
Permit # (if available) UC
=fL D (p 0 a ,3q
it Start date, b/ a 1 Start time J 5 (�M� PM
End date to y Ia�_7� End Time Z U AM PM
I 0o-f Estimated volume
` - , ,,✓ Location
Cause
I li-,vkl�Steps taken to co J
� U ,
Did Spill/SSO reach surface waters
Name of Surface Water
Volume reaching surface waters
Conveyance
Did Spill/SSO result in fish kill
Received by '--
2. Enter S HYSSO into Access:
cs.
Open the Microsoft Access file S:laccesslnotice24_2 (OR) S:laccessllncident
Open the required form
At the bottom left of the form, click on the right arrow -asterisk symbol to bring up the next blank form
Fill in the form and close Access
3. Enter into RIMS
Log into the public portal version of BIMS(http://bims.enr.state.nc.us:70011Welcome.do)
Go to Tasks, Incident, Enter Incident
For SSO, fill in the SSO and 24 hour forms, record the incident number, then save the file and close.
For Spills, check the type of spill box, fill in the Incident report, record the incident number and close..
4. Comments:

Of W ATF9
07 Form CS-SSO
a �
Collection System Sanitary Sewer Overflow Reporting Form
PART I
This form shall be submitted to the appropriate DWQ Regional Office within five days of the first knowledge of
the sanitary sewer overflow (SSO).
Permit Number : NCG060039 (WQCS# if active, otherwise use treatment plant NC/M#)
Facility: Taleuis- Clayton
Incident # 1
Telecris 3otherapeutics
Owner:
Region: Raleigh
City: Clayton
County: Johnson
Source of SSO (check applicable) : ❑ Sanitary Sewer
Pump Station
SPECIFIC location of the SSO (be consistent in description from past
reports or documentation - i.e. Pump Station 6,
Manhole at Westalt & Bragg Street, etc.) : 8388 Hwy 70VJest, Near Trader 16
Latitude (degrees/minute/second): 35/37/02
Longitude(degrees/minute/second)• 7WS101
Incident Started Dt: 10-21-2005 Time 11:57 am
Incident End D _10-21-0200 Time t2:07 pm
(mm-dd-yyyy) hh:mm AM1PM
(mm-dd-yyyy) hh:mm AM/PM
Estimated volume of the SSO: 10 gallons
Estimated Duration (Round to nearest hour`) —
Describe how the volume was determined: es°"°"b�ec«"soleaCsevaoons
Weather conditions during SSO event:suny, clear skies
Did SSO reach surface waters? 11 YesR]Nell Unknown
Volume reaching surface waters (gallons): None
Surface water name: Neuse
Did the SSO result in a fish kill? ❑ Yes ❑✓ No ❑ Unknown if Yes, what is the estimated number of fish killed?
SPECIFIC cause(s) of the SSO:
❑ Severe Natural Condition ❑ Grease
❑ Roots
❑ Inflow and Infiltration ❑ Pump Station Equipment Failure ❑ Power outage
❑ Vandalism ❑ Debris in line
❑ Other (Please explain in Part II)
Immediate 24-hour verbal notification reported to'. Jenny Atkins
0 DWQ ❑ F-mergency Mgmt. Date (mm-dd-yyyy):
10-21-2005 Time (hh:mm AM/PM): 1:35pm
If an SSO is ongoing, please notify Regional Office on a daily basis until SSO can be stopped.
Per G.S. 143-215.1C(b), the responsible party of a discharge of 1,000 gallons or more of untreated wastewater to surface
waters shall issue a press release within 48-hours of first knowledge to all print and electronic news media providing general
coverage in the county w ere a ischarge occurred. When 15,000 gallons or more of untreated wastewater enters surface
waters, a public notice shall be published within 10 days and proof of publication shall be provided to the Division within 30 days.
Refer to the referenced statute for further detail.
The Director, Division of Water Quality, may take enforcement action for SSOs that are required to be reported to Division unless it
is demonstrated that: ,
1) the discharge was caused by severe natural conditions and there were no feasibie alternatives to the discharge; or
2) the discharge was exceptional, unintentional, temporary and caused by factors beyond the reasonable control of the Permittee
and/or owner, and the discharge could not have been prevented by the exercise of reasonable control.
Part IE must be completed to provide a justification claim for either of the above situations. This information will be the basis
for the determination of any enforcement action. Therefore, it is important to be as complete as possible.
WHETHER OR NOT PART II IS COMPLETED, A SIGNATURE IS REQUIRED AT THE END OF THIS FORM.
CS-SSO Form October 9, 2003 Page 1

ofwnrFq
"' �c Form CS-SSO
o -c
Collection System Sanitary Sewer Overflow Reporting Form
PART I I
ANSWER THE FOLLOWING QUESTIONS FOR EACH RELATED CAUSE CHECKED IN PART I OF THIS FORM
AND INCLUDE THE APPROPRIATE DOCUMENTATION AS REQUIRED OR DESIRED
COMPLETE ONLY THOSE SECTIONS PERTAINING TO THE CAUSE OF THE SSO AS CHECKED IN PART I
In the check boxes below, NA = Not Applicable and NE = Not Evaluated
A HARDCOPY OF THIS FORM SHOULD BE SUBMITTED TO THE APPROPRIATE DWQ REGIONAL OFFI CE
UNLESS IT HAS BEEN SUBMITTED ELECTRONICALLY THROUGH THE ONLINE REPORTING SYSTEM
Severe Natural Condition {hurricane, tornado, etc.
Describe the" severe natural condition" in detail.
How much advance warning did you have and what actions were taken in preparation for the event?
Comments:
Grease (Documentation such as cleaning, inspections, nforcement
actions past overflow reports, educational material and distribution date
etc. should be available upon request.)
When was the last time this specific line (or wet well) was cleaned?
Do you have an enforceable grease ordinance that requires new or retrofit of grease traps/interceptors? 0Yed0 No ❑NA ❑NE
Have there been recent inspections and/or enforcement actions taken on nearby restaurants or ether ❑YX No ❑NA ❑NE
nonresidential grease contributors?
Explain.
Have there been other SSOs or blockages in this area that were also caused by grease? ❑YeE] No NA NE
When?
If yes, describe them:
Have cleaning and inspections ever been increased at this location? ❑YesEl No ❑NA ❑NE
Explain.
CS-SSO Form October 9, 2003 Page 2

Have educational materials about grease been distributed in the past?
When?
and to whom?
Explain?
If the SSO occurred at a pump station, when was the wet well and pumps last checked for grease
accumulation?
Were the floats clean?
Comments:
Roots
Do you have an active root control program?
Describe
❑YesD No ❑ NA ❑ NE
❑Yes❑ No❑NA [IN E
❑YesD No ❑ NA ❑ NE
Have cleaning and inspections ever been increased at this location because of roots? ❑Yew! No ❑NA ❑ NE
Explain:
What corrective actions have been accomplished at the SSO location (and surrounding system if
associated with the SSO)?
What corrective actions are planned at the SSO location to reduce root intrusion?
Has the line been smoke tested or videoed within the past year? ❑Yes❑ No [j NA ❑ NE
If Yes, when?
Comments:
Inflow and Infiltration
Are you under an SOC (Special Order by Consent) or do you have a schedule in any permit that ❑ Yej--] No ❑NA ❑NE
addresses IV
CS-SSO Form October 9, 2003 Page 3

Explain if Yes:
What corrective actions have been taken to reduce or eliminate I & I related overflows at this spill location
within the last year?
Has there been any flow studies to determine 1/1 problems in the collection system at the SSO location? ❑Yes❑ No ❑NA ❑NE
If Yes, when was the study completed and what actions did it recommend?
Has the fine been smoke tested or videoed Wthin the past year? 11 Yes❑ No NA NE
If Yes, when and indicate what actions are necessary and the status of such actions:
Are there 1/1 related projects in your Capital Improvement Plan? 11 Yes❑ No LJ NA U NE
If Yes, explain:
Have there been any grant or loan applications for Ill reduction projects? Yes[] No NA ONE
If Yes, explain:
Do you suspect any major sources of inflow or cross connections with storm sewers? ❑Yes❑ No [-I NA ❑ NE
If Yes, explain.
Have all lines contacting surface waters in the SSO location and upstream been inspected recently? ❑Yes❑ No ❑NA ONE
If Yes, explain:
What other corrective actions are planned to prevent future Ill related SSOs at this location?
Comments:
Pump Station Equipment Failure (Documentation of testing, records etc.,
shoul be provided upon request.)
What kind of notification/alarm systems are present?
Auto-dialer/telemetry (one-way communication)
❑Yes
CS-SSO Form October 9, 2003 Page 4

Audible Dyes
Visual []Yes
SCADA (two-way communication) []Yes
Emergency Contact Signage ❑Yes
Other ❑Yes
Describe the equipment that failed?
What kind of situations trigger an alarm condition at this station (i.e. pump failure, power failure, high
water, etc.)? r-
Were notification/alarm systems operable? Yes❑ No UNA LJ NE
If no, explain:
if a pump failed, when was the last maintenance and/or inspection performed?
What specifically was checked/maintained?
If a valve failed, when was it last exercised?
Were all pumps set to alternate?
Did any pump show above normal run times prior to and during the SSO event?
Were adequate spare parts on hand to fix the equipment (switch, fuse, valve, seal, etc.)?
Was a spare or portable pump immediately available?
If a float problem, when were the floats last tested? How?
If an auto -dialer or SCADA, when was the system last tested? How.)
Comments:
[]Ye,[] No ❑NA❑NE
❑Yesu No❑NA❑NE
❑Yes❑ No ❑ NA ❑ NE
❑Yes❑ No❑NA❑NE
CS-SSO Form October 9, 2003 Page 5

Power outage (Documentation of testing, records, etc., should be
provided of alternative power source upon request.)
What is your alternate power or pumping source?
• - Generator
Did it function properly? ❑Yes❑ No ❑NA❑NE
Describe?
When was the alternate power or pumping source last tested under load?
If caused by a weather event, how much advance warning did you have and what actions were taken to
prepare for the event?
Comments:
Vandalism
Provide police report number:
Was the site secured?
❑ Yes❑ No ❑ NA ❑ NE
If Yoe hnv,f,?
Padlocked Control Panel
Have there been previous problems with vandalism at the SSO location? ❑Yes❑ No DNA ONE
If Yes, explain:
What security measures have been put in place to prevent similar occurrences in the future? ❑Yes❑ No ❑ NA ❑ NE
Comments:
Debris in fine (Rocks, sticks, rags and other items not allowed in the
collection system, etc.)
What type of debris has been found in the lire?
How could it have gotten there?
Are manholes in the area secure and intact? Ye No NA NE
CS-SSO Form October 9, 2003 Page 6

When was the area last checked/cleaned?
Have cleaning and inspections ever been increased at this location due to previous problems Wth debris? ❑Yes❑ No [-I NA ❑NE
Explain.
Are appropriate educational materials being developed and distributed to prevent future similar ❑Yes❑ No ❑NA ❑NE
occurrences?
Comments:
Other (Pictures and a police repart_should be available upon request.)
Describe:
A leak in a passivation drain line resulted in a 10 gallon spill to the stormdrain
Were adequate equipment and resources available to fix the problem? ❑Yes❑ No ❑ NA ❑NE
If Yes, explain:
If the problem could not be immediately repaired, what actions were taken to lessen the impact of the
SSO?
Comments:
For DWQ Use Only:
DWQ Requested an Additional Written Report:
If Yes, What Additional Information is Needed:
Comments:
❑Yes No❑NA❑NE
CS-SSO Form October 9, 2003 Page 7

As a representative for the responsible party, I certify that the information contained in this report is True and accurate
to the best of M knowledge.
Person submitting claim:
Signature: JX=i.Z
Telephone Number. 91 9.359-4375
Date: 1 0-26-2005
Title: HES Manager -Environmental
Any additional information desired to be submitted should be sent to the appropriate Division Regional Office within five days of first
knowledge of the SSO with reference to the incident number (the incident number is only generated when electronic entry of this form
is completed, if used),
CS-S80 Form October 9, 2003 Page 8

op VN A rgq
�' 09 Form CS-SSO
Collection System Sanitary Sewer Overflow Reporting Form
PART l
This form shall be submitted to the appropriate DWQ Regional Office within five daysof the first knowledge of
the sanitary sewer overflow (SSO).
Permit Number: NCG060039
Facility: Talecris - Clayton
Owner: Talecris Biotherapeutics
City: laytnn
(WQCS# if active, otherwise use treatment plant NCNVQ#)
Incident# 1
Raleigh
County: Johnson
Source of SSO (check applicable) : 0 Sanitary Sewer ❑ Pump Station
SPECIFIC location of the SSO (be consistent in description from past reports or documentation - i.e. Pump Station 6,
Manhole at WestalI & Bragg Street, etc.) : 8388 Hwy 7o West, Near Traljer 16
Latitude (degrees/minute/second): 35137102
Incident Started Dt: 09-15-2005 Time, 1:00 pm
(mm-did-yyyy) hi AMi
Estimated volume of the SSO:
5
Longitude(degrees/minuteisecond). 78/25101
Incident End p .09-15-2005 Time, 1:20 pm
(mm-dd-yyyy) hh:mm AM/PM
gallons Estimated Duration (Round to nearest hour);-•
Describe how the volume was determined: Estmaretmdonksibleobs eons
Weather conditions during SSO event: Sunny, clear Skies
Did SSO reach surface waters? ❑ Yes ❑ No❑ Unknown Volume reaching surface waters (gallons) None
Surface water name: Neuse
Did the SSO result in a fish kill? ❑ Yes 0 No ❑ Unknown If Yes, what is the estimated number of fish killed?
SPECIFIC cause(s) of the SSO:
❑ Severe Natural Condition ❑ Grease ❑ Roots
❑ Inflow and Infiltration ❑ Pump Station Equipment Failure ❑ Power outage
❑ Vandalism ❑ Debris in line ❑� Other (Please explain in Part II)
immediate 24-hour verbal notification reported to: Jenny Atkins
El DWQ ❑ Emergency Mgmt. Date (mm-dd-yyyy): 09-15-2005 Time (hh:mm AM/PM): 2:00pm
If an SSO is ongoing, please notify Regional Office on a daily basis until SSO can be stopped.
Per G.S. 143-215.1C(b), the responsible party of a discharge of 1,000 gallons or more of untreated wastewater to surface
waters shall issue a . press release within 48-hours of first knowledge to all print and electronic news media providing general
coverage in the county—w-Fe—r—eU 7eischarge occurred. When 15,000 gallons or more of untreated wastewater enters surface
waters, a public notice shall be published within 10 days and proof of publication shall be provided to the Division within 30 days.
Refer to the referenced statute for further detail.
The Director, Division of Water Quality, may take enforcement action for SSOs that are required to be reported to Division unless it
is demonstrated that-
1) the discharge was caused by severe natural conditions and there were no feasible alternatives to the discharge; or
2) the discharge was exceptional, unintentional, temporary and caused by factors beyond the reasonable control of the Permittee
and/or owner, and the discharge could not have been prevented by the exercise of reasonable control.
Part II must be completed to provide a justification claim for either of the above situations. This information will be the basis
for the determination of any enforcement action. Therefore, it is important to be as complete as possible.
WHETHER OR NOT PART II IS COMPLETED, A SIGNATURE IS REQUIRED AT THE END OF THIS FORM.
CS-SSO Form October 9, 2003 Page 1

of wnrF9
Form CS-SSO
Collection System Sanitary Sewer Overflow Reporting Form
IVNA+ PART I I
ANSWER THE FOLLOWING QUESTIONS FOR EACH RELATED CAUSE CHECKED IN PART I OF THIS FORM
AND INCLUDE THE APPROPRIATE DOCUMENTATION AS REQUIRED OR DESIRED
COMPLETE ONLY THOSE SECTIONS PERTAINING TO THE CAUSE OF THE SSO AS CHECKED IN PART I
In the check boxes below, NA = Not Applicable and NE = Not Evaluated
A HARDCOPY OF THIS FORM SHOULD BE SUBMITTED TO THE APPROPRIATE DWQ REGIONAL OFFICE
UNLESS IT HAS BEEN SUBMITTED ELECTRONICALLY THROUGH THE ONLINE REPORTING SYSTEM
Severe Natural Condition (hurricane, tornado, etc.)
Describe the "severe natural condition" in detail.
How much advance warning did you have and what actions were taken in preparation for the event?
Comments:
Grease (Documentation such as cleaning, inspections, enforcement
actions, past overflow reports, educational material and distribution date
etc. should be available upon request.)
When was the last time this specific fire (or wet well) was cleaned?
Do you have an enforceable grease ordinance that requires new or retrofit of grease trapsfinterceptors? ❑YILI No ❑ NA DNE
Have there been recent inspections and/or enforcement actions taken on nearby restaurants or other ❑YeSEI No El NA ❑NE
nonresidential grease contributors?
Explain.
Have there been other SSOs or blockages in this area that were also caused by grease? ❑Y,,C No ❑NA NE
When?
If yes, describe them:
Have cleaning and inspections ever been increased at this location? ❑YeF—1 No ❑ NA ❑ NE
Explain.
CS-SSO Form October 9, 2003 Page 2

Have educational materials about grease been distributed in the past?
When?
and to whom?
Explain?
If the SSO occurred at a pump station, when was the wet well and pumps last checked for grease
accumulation?
Were the floats clean?
Comments:
Roots
Do you have an active root control program?
Describe
❑Yes❑ No❑NA❑NE
❑Yes❑ No❑NA❑NE
❑Yesu No ❑ NA ❑ NE
Have cleaning and inspections ever been increased at this location because of roots? Yell No ❑NA❑NE
Explain:
What corrective actions have been accomplished at the SSO location (and surrounding system if
associated with the SSO)?
What corrective actions are planned at the SSO location to reduce root intrusion?
Has the line been smoke tested or videoed Wthin the past year? ❑Yes❑ No [I NA ❑ NE
If Yes, when?
Comments:
Inflow and Infiltration
Are you under an SOC (Special Order by Consent) or do you have a schedule in any permit that ❑YesE] No ❑NA IDNE
addresses Ill?
CS-SSO Form October 9, 2003 Page 3

Explain if Yes:
What corrective actions have been taken to reduce or eliminate I & I related overflows at this spill location
within the last year?
Has there been any flow studies to determine Ill problems in the collection system at the SSO location? ❑Y,J] No [INA ONE
If Yes, when was the study completed and what actions did it recommend?
Has the line been smoke tested or videoed within the past year? 13 Yej--] No 11 NA M NE
If Yes, when and indicate what actions are necessary and the status of such actions:
Are there 1/1 related projects in your Capital Improvement Plan? 11 Yes❑ No U NA U NE
If Yes, explain:
Have there been any grant or loan applications for Ill reduction projects? Ll Ye1D No NA NE
If Yes, explain:
Do you suspect any major sources of inflow or cross connections with storm sewers? ❑Yes❑ No ❑NA ❑NE
if Yes, explain:
Have all lines contacting surface waters in the SSO location and upstream been inspected recently? ❑YesD No ❑NA ❑NE
If Yes, explain:
What other corrective actions are planned to prevent future 1/1 related SSOs at this location?
Comments:
Pump Station Equipment Failure Documentation of testing,records etc,
shoul be provided u on request.)
What kind of notification/alarm systems are present?
Auto-dialer/telemetry (one-way communication) ❑Yes
CS-SSO Form October 9, 2003 Page 4

Audible ❑Yes
Visual ❑Yes
SCADA (two-way communication) ❑Yes
Emergency Contact Signage ❑Yes
Other Oyes
Describe the equipment that failed?
What kind of situations trigger an alarm condition at this station (i.e. pump failure, power failure, high
water, etc.)?
Were notification/alarm systems operable? 11 Yes❑ No U NA U NE
If no, explain:
If a pump failed, when was the last maintenance and/or inspection performed?
What specifically was checked/maintained?
If a valve failed, when was it last exercised?
Were all pumps set to alternate?
Did any pump show above normal run times prior to and during the SSO event?
Were adequate spare parts on hand to fix the equipment (switch, fuse, valve, seal, etc.)?
Was a spare or portable pump immediately available?
If a float problem, when were the floats last tested? How?
If an auto -dialer or SCADA, when was The system last tested? How?
Comments:
❑Yes❑ No❑NA❑NE
❑Yes❑ No ❑NA [IN E
❑Yes❑ No❑NA❑NE
❑Yes❑ No❑NA❑NE
CS-SSO Form October 9, 2003 Page 5

Power outage (Documentation of testing, records, etc., should be
provided of alternative power source upon request.)
What is your alternate power or pumping source?
On -Site Gen&ator MATS
Did it function property? ❑Yes❑ No ❑NA ❑NE
Describe?
When was the alternate power or pumping source last tested under load?
If caused by a weather event, how much advance warning did you have and what actions were taken to
prepare for the event?
Comments:
Vandalism
Provide police report number:
Was the site secured?
If Yoe hnuf?
Padlocked Control Panel
Have there been previous problems with vandalism at the SSO location?
If Yes, explain:
❑ Yes❑ No ❑ NA ❑ NE
No IJNA LJNE
What security measures have been put in place to prevent similar occurrences in the future? ❑Yes❑ No ❑ NA ❑ NE
Comments:
Debris in line (Rocks, sticks, rags and other items not allowed in the
collection system, etc.)
What type of debris has been found in the line?
How could it have gotten there?
Are manholes in the area secure and intact? Ye No NA NE
CS-SSO Form October 9, 2003 . Page 6

When was the area last checked/cleaned?
Have cleaning and inspections ever been increased at this location due to previous problems with debris? 0Ye10 No ❑NA ❑NE
Explain:
Are appropriate educational materials being developed and distributed to prevent future similar ❑Y,,C No ❑NA ❑NE
occurrences?
Comments:
Other (Pictures and a police repo_rt_should be available upon request.)
Describe:
Pipeline elevation must be modified.
Were adequate equipment and resources available to fix the problem? AYe.0 No ❑ NA ❑ NE
If Yes, explain:
If the problem could not be immediately repaired, what actions were taken to lessen the impact of the
SSO?
Comments:
For DWO Use Only:
DWQ Requested an Additional Written Report:
If Yes, What Additional Information is Needed:
Comments:
11Yez] No❑NA❑NE
CS-SSO Form October 9, 2003 Page 7

As a representative for the responsible party, I certify, that the information contained in this report is true and accurate
to the best of my knowledge,
Person submitting claim: Davii o. Auge
Talecils Motherapowirs
Signature
Tolephone Number: 919-359-4375
Date: 09-19-2005
Title, HES Manager - Environmental
Any add;tional information desired to be submitted should be sent to the appropriate Division Regional Office within five days of first
knowledge of the SSO with reference to the incident number (the incident number is only generated when electronic entry of this form
is completed, if used).
CS-SSO Form October 9. 2003 Page 8

w
GRIFOLS
GRIFOLS
�d C C-0 6'0 03 y
September 4, 2015
NC DENR Division of Water Duality
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Dear NC DENR,
Attached is the Representative Outfall Status Request for Grifols Therapeutics, Inc.
SO ely,
,C
David D. Aug , P.E., CHMM
ESS Manager, Environmental
/cm
8368 U.S. 70 Bus Hwy West
Clayton, NC 27520
Tel. [phone] .
www.grifols.com

e or
�w
NCDENR
EN�I�Ow.KM AMO N.vux RCfOIAGLb
Division of Water Quality / Surface Water Protection
National Pollutant Discharge Elimination System
REPRESENTATIVE OUTFALL STATUS (ROS)
REQUEST FORM
FOR AGENCY USE ONLY
Date Received
Year
Month
Da
if a facility is required to sample multiple discharge locations with very similar storm water discharges, the
permittee may petition the Director for Representative Outfall Status (ROS). DWQ may grant Representative
Outfall Status if stormwater discharges from a single outfall are representative of discharges from multiple
outfalls. Approved ROS will reduce the number of outfalls where analytical sampling requirements apply.
If Representative Outfall Status is granted, ALL outfalls ore still subject to the qualitative monitoring
requirements of the facility's permit --unless otherwise allowed by the permit (such as NCG020000) and DWQ
approval. The approval letter from D WQ must be kept on site with the facility's Stormwater Pollution
Prevention Plan. The facility must not* DWQ in writing if any changes affect representative status.
For questions, please contact the DWQ Regional Office for your area (see page 3).
(Please print or type)
1) Enter the permit number to which this ROS request applies:
Individual Permit (or) Certificate of Coverage
NI IC S I� N IC G 0 6 0 0 3 9
2) Facility Information:
Owner/Facility Name Grifols Therapeutics Int
Facility Contact David Auge _
Street Address 8368 Highway 70 West
City Clayton _ _ _ ' State NC ZIP Cade 27520
County Johnston E-mail Address david.auge2grifols.com
Telephone No. [phone] _ Fax: [phone]
3) List the representative outfalls) information (attach additional sheets if necessary):
Outfall No. 3 is representative of Outfall No. 1
Outfalls' drainage areas have the same or similar activities? Yes o No
Outfalls' drainage areas contain the same or similar materials? VYes o No
Outfalls have similar monitoring results? ❑ Yes ❑ No No data*
Outfall No. 3 is representative of Outfall No. 2
Outfalls' drainage areas have the same or similar activities?
%es.
❑ No
Outfalls' drainage areas contain the same or similar materials?
Yes
u No
Outfalls have similar monitoring results?
❑ Yes
❑ No c/No data*
Outfall(s) is representative of Outfall(s)
Outfalls' drainage areas have the same or similar activities?
❑ Yes
❑ No
Outfalls' drainage areas contain the same or similar materials?
❑ Yes
❑ No
Outfalls have similar monitoring results?
❑ Yes
❑ No o No data*
*Non-compliance with analytical monitoring prior to this request may prevent ROS approval. Specific
circumstances will be considered by the Regional Office responsible for review.
Page 1 of 4
SWU•ROS-2009 Last revised 12l30/2009

Representative Outfall Status Request
4) Detailed explanation about why the outfalls above should be granted Representative Status:
(Or, attach a letter or narrative to discuss this information.) For example, describe how activities and/or
materials are similar.
Grifols Therapeutics is_a pharmaceutical manufacturing_facility that incorporates approximately 242 acres
and is located 2.75 miles southeast of Clayton on Highway 70 east. The facilit s manufacturing operations
and processes are primarily conducted indoors within the buildings shown on the attached drawing with the
exception of raw material receiving, wastewater treatment, and bulk material storage and handling.
As a result of recent expansion activities to address future production requirements, the plant site will
ultimately have five outfalls. An outfall associated with the Plasma logistics Center (PLC) located on the
western side of the site and two outfalls associated with the North Fractionation Facility (NFF], as shown on
the attached_ drawing. The stormwater runoff associated with the outfalls from PLC and NFF will be
comparable to Outfall Nos. 1 and 2 since the land use activities are consistent between both south and
north sides of the property._ Furthermore analytical sampling between outfalls nos. land 2 are consistent
with the requested outfall no. 3 location as reflected in the attached monitoring data. In addition the
existing togography of the Grifols site all drains to the proposed outfall no. 3 located prior to leaving the
property -thereby making -a representative outfall for the stormwater runoff water quality associated with
the plant site.
5) Certification:
North Carolina General Statute 143-215.6 B(I) provides that:
Any person who knowingly makes any false statement, representation, or certification In any application, record,
report, plan, or other document filed or required to be maintained under this Article or a rule implementing this
Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case
under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device
or method required to be operated or maintained under this Article or rules of the [Environmental Management]
Commission Implementing this Article shall be guilty of a Class 2 misdemeanor which may Include a fine not to exceed
ten thousand dollars ($10,000).
I hereby request Representative Outfall Status for my NPDES Permit. I understand that ALL outfalls are still
subject to the qualitative monitoring requirements of the permit, unless otherwise allowed by the permit
and regional office approval. I must notify DWQ in writing if any changes to the facility or its operations take
place after ROS is granted that may affect this status. If ROS no longer applies, I understand I must resume
monitoring of all outfalls as specified In my NPDES permit.
I certify that I am familiar with the information contained in this application and that to the best of my
knowledge and belief such information is true, complete, and accurate.
ame of Person Signing: eO(1 V1 _- /,3
(Date Signed)
Please note: This application for Representative Outfall Status Fs subject to approval by the
NCDENR Regional Office. The Regional Office may inspect your facility for compliance with the
conditions of the permit prior to that approval.
Final Checklist for ROS Regnest
This application should include the following items:
sl/ This completed form..
Page 2 of 4
SVVU-ROS-2009
Last revised 12rM2009

Representative Outfall Status Request .
r� Letter or narrative elaborating on the reasons why specified outfalls should be granted representative
I status, unless all information can be included in Question 4.
d Two (2) copies of a site map of the facility with the location of all outfalls clearly marked, including the
/ drainage areas, industrial activities, and raw materials/finished products within each drainage area.
d Summary of results from monitoring conducted at the outfalls listed in Question 3,
D Any other supporting documentation.
Mail the entire package to:
NC DENR Division of Water Quality
Surface Water Protection Section
at the appropriate Regional Office (See map and addresses below)
Notes
The submission of this document does not guarantee Representative Outfall Status (ROS) will be granted as
requested. Analytical monitoring as per your current permit must be continued, at all outfalls, until written
approval of this request is granted by DWQ. Non-compliance with analytical monitoring prior to this request
may prevent ROS approval. Specific circumstances will be considered by the Regional Office responsible for
review.
For questions, please contact the DWQ Regional Officefor your area.
Asheville Regional Office
2090 U.S. Highway 70
Swannanoa, NC 28778
Phone [phone]
FAX [phone]
Fayetteville Regional Office
Systel Building,
225 Green St., Suite 714
Fayetteville, NC 28301-5094
Phone [phone]
FAX [phone]
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115
FAX [phone]
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Phone [phone]
FAX [phone]
Washington Regional Office
943 Washington Square Mail
Washington, NC 27889
Phone [phone]
FAX [phone]
Page 3 of 4
SWU-ROS-2009 Last revised 1213012009

Representative Outfall Status Request
Wilmington Regional Office Phone [phone]
127 Cardinal Drive Extension Water Quality Main FAX [phone]
Wilmington, NC 28405
Central Office
Phone [phone] Mail Service Center
FAX [phone] Raleigh, NC 27699-1617
Winston-Salem Regional Office Phone [phone]
585 Waughtown Street FAX [phone]
Winston-Salem, NC 27107
Page 4 of 4
SWU-ROS•2009 Last revised 12/3012009

ER-06A - EMS Communication Log - External
2015
Updated on:8/31/15
„ Initial Communication
Response
Date
Phone # of email
Employee
Name .
Company
-
5ubjd'c of Communication
Date
Action Taken
address. _
- - _... -
_ _.. -- -
_ . Initials ..
NCDENR, Division
1628 Mai! Service Center
Quarterly Air Permit Reporting for S02 and
1130/2015
Steve Hall
of Air Quality
Raleigh, NC 27699-1628
NOX
11302015
Steve Hall
NCDENR, Division
1628 Mail Service Center
Semi -Annual Air Permit Reporting for Fuel
of Air Quality
Raleigh, NC 27699-1628
Usage
Must the new Biennial Compliance Report
His answer was no.
2/32015
Matthew Mahler
NCDENR, Division
919-791-4200
referenced in Air Permit No. 03380R18
42044
We must only keep a
DDA.
of Air Quality
A.10.C.iii. Be submitted to the agency
copy on site for
inspection purposes.
LEPC,.Fire
NC Emergency Management
Tier II Report -Chemicals kept on site at a
pt
pt
220/2015
Department, Police
4326 Mail Service -Center
volume greater than 10,000 bs
Department
Raleigh, NC 27699
3/202015
Carlos Bagley
Johnston County
PO Box 22631
Closure of Stormwater Permits for NFF
Stormwater District
Smithfield, NC 27577
and the East Parking Lot anion
4232015
Will Wilke
NCDENR, Division
of Air Quality
919-791-42o i
Annual Air Inspection
4272015
Steve Hall
NCDENR,.Division
1617 Mail Service Center
Semi -Annual Stonnwater Report
of Water Quality
Raleigh, NC 27699
5172015
Gary Perlmutter
NCDENR, Division
-Quality
g19-791-4200
RMP Inspection
of Air:
4
6152015
DHHS - Division of
1645 Mail Service Center
Exit Light Shipment Notification
Radiation Protection
Raleigh, NC 27699-1645
5/152015
Gary Perlmutter
NCDENR, Division
919-791-4200
RMP Notice of Violation from Recent
6142015
Responded to notice
DDA.
of Air Quality
_ t
Inspections
7112015
EPA - TRIMe
Software
Toxic Release Inventory
-
Version: 6/30/16 Signature: Effective Date: Page 1 of 2 Pages
9

ER-06A - EMS Communication Log - External
2015
Updated on:8/31/15
Date .�
N�a a
Cam 'J
Phone# orema:I' :
"k�
�. RCS: ,
$uh�ect ofiCommurncation
Date "`.
Actian Taken
Employee
an
-
A
„
1 1f�als.
atliiress:. _ :
f7
72015
James Warren
Town of C Layton
919-553-1536
jowarren(d3townofci ayton.
Request permission to commence direct
POTW
discharge from the MBBRs.
ne.o
7212015
Steve Hall
NCDENR, Division
1628 Mail Service Center
Quarterly Air Permit Reporting for S02 and
of Air Quality
Raleigh, NC 27699-1628
NOX
7212015
Steve Hall
NCDENR, Division
1628 Mail Service Center
Semi -Annual Air Permit Reporting for Fuel
of Air Quality
Raleigh, NC 27699-1628
Usage
7202015
US Department of
via intemet:
Monthly Construction Progress Report of
Commence
econhelp.oensus.gov/Cprs
the West Warehouse
Carlos Bagley
Johnston County
Carlos was at the site, Bradley
Discuss the status of how to change the
724/2015
and Bradley
Stormwater District
joined the meeting via 919-a07
Stormwater permit to properly include the
Bennett
and the permit writer
6300.
new areas constructed at the site.
from NCDENR
NCDENR Raleigh
Mr. Hayes was confirming that all items
8/31=15
Mitch Hayes
Regional Office
919-791-4200
listed for tax certification qualify for that
loertification.
Version: 6/30/15 Signature: Effective Date: Page 2 of 2 Pages

a
,RnNill No, 011ifill Lxistim: Outfall Nut� 7
Bain No. t OulNll

GIRVOLS
8368 U.S. 70 Bus. West
Clayton, NC 27620
Dav1d S. Graham
ESS III
Tel [phone]
Fax [phone]
Cell 919.724.5979
[e-mail]
April 13, 2015
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
To whom it may concern:
Attached you will find the analytical SOO monitoring report followlhg a representative storm event for the Grifols
Therapeutics Clayton, NC facility. If you have any questions, please don't hesitate to contact meat 919-359-5473
Sincerely,
David S. Graham
ESS HI

It
d Oorriptete••Ite 's"i, 2; ar" 8.;41so Goinpletp ? ?
Itetri.4 Ef Rest+icted Delivery is aeslred: _ .
Q Print Your Heine and address on the reverse
ao that ' can,retiii `the Gard to you.
Q Attach this c' W to the back of the maliplece,
anon the front ii.s*e periiiits.
1. Ar{Icle Addrea to g'
X. ❑
9. FtwdVed by (Printed MUW C. Date
RA, dales address d fmdnt ftom Item 1? IQ
if YEB enter dettvary address 621uw •- •.©.
Division of Water Quality"ill!
h
Attn;. DWQ Central.Flies APR
1617 Mall Service Center s©rv(aelype
Ralelgh NC 27699-1617 ❑ cerl!'OA M t�cpr8as
"
4,jipp5sr_jd,jt'. Retur'Recelytfor handlae
-Cl l44u Mail,,,U.'o
4. Rostrigted fbpllvci7r? (Fxfra ies) r ,ee
I
7012 34b© 0003 710 -
2-Ames Number _ I
1 4968
{t}anara►hcm service tabep I
PS Form 3811, February 2004 Domestic Retum Receipt 10R59 +M•tb4o 3

0 —
aC6AngV 'cal*
www«pgcerebA.com
Laboratory Report
Sam Vedder
Grifols Therapeutics, Inc:
8368 US 70 West
Clayton, NC 27520
Project: Monthly Stormwater Outfells
Pace Project No.: 92243016
Pace Analytical Services, Inc.
6701 Conference drive
Raleigh, NC 27007
[phone]
Page 1 of 1
Report Date: 04/02/2015
Data Received: 03/27/2015
Sample: Outfall #1
Lab [l): 92243016001 Collected: 03/26116 13:35
Matrix: Water
Parameters
Results
Units
Report_Urnit
Analyzed
Qualifiers
On and Grease
ND
mg1L
5.0 .
04/01115 09:48
'total Suspended Solids
6.5
mg1L
4.6
03/31,11510:28
Chemical Oxygen Demand
NO
mg1L
26.0
0=0116 08:50
„03/2611513:45
Sample: Outfall #2
Lab ID: 92243016002 Collected:
Matrix: Water
Parameters
Results
Units
Report Limit
Analyzed
Qualifiers
Oil and Grease
No
mg1L
6.0
04/01115 09:48
Total Suspended Solids
9.6
mg1L
2.6
03/31M510:28
Chemical Oxygen Demand
ND
mg1L
25.0
03/30/15 08:50
Reviewed
Nicole Gastorowskl
[e-mail]
Raleigh Certification IDs
0701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Klncey Ave, Ste "100, Hunlersvllle, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 6342
North Carolina Wastewater Certincatlon IP 12
South Carolina Certification#: 99000001
North Carolina 9loassay Cerillication #: 16
North Carolina Drinldng Water Certification #: 37731
FlorldalWCLLAP Cerilllcanon a: E87627
Kentucky UST Certification #: 84
West Vlrglnia Certification #: 357
VlrginlalVELAP CerUtleation #: 460221
Page 1 of 3

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Page 14: Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Permit No NCG060000, or Certificate of Coverage No.: N CGO60039
Facility Name: Grifols Therapeutics _
County: Johnston Count' Phone No.919-359-5473
Inspector: David S. Graham
Date of Inspection: 312612016
By this signature, i certify that this report Is accurate and complete to the best of my knowledge:
1.Dutfail Description
Outfall No,.:' ::',:::, °;',,;1::Structure (pipe, ditch, etc.) Stream
Recelving Stream: tributary to the Meuse River
Describe the Industrial activities that occur within the outfall drainage area: Pharmaceutical Mfg.
2. Color
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium,
dark) as'descrlptors: Clear with a light brown tlnt
3.Odor
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor,
etc.): - None
4. Clarity
Choose the number which best describes the clarity of the discharge where 1 Is clear and 10 Is very
cloudy:
1 2 ® 4 5 6 7 8 9 10
Page 1
SWU-242-020705

6. Floating Solids
Choose the number which best describes the amount of floating solids in the stormwater discharge where
Lis no solids and 10 Is the surface covered with floating solids:
1 2 3 4 5 6 7 8 9 10
S. Suspended Solids
Choose the number which best describes the amount of suspended solids in the stormwater discharge
where no solids and 10 is extremely muddy.
1 2 3 4 5 6 7 8 9 10
7. Foam
Is there any foam In the stormwater discharge? Yes Na
S. Oil Sheen
Is there an oil sheen in the stormwater discharge? Yes(D
9. Deposition at Outfall
Is there deposition of material (sediment, etc.) at or Immediately below the outfall? YG
10. Erosion at outfall
Is there erosion at or Immediately below the outfall? Yes No
11.'Other Obvious Indicators of Stormwater Pollution
List and describe None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, deposition or erosion may be
Indicative of conditions that warrant further investigation and corrective action.
Page 2
5 W U-242-020705

GENERAL PERMIT NO. NCG120000
CERTIFICATE OF COVERAGE NO. NCGO60039
FACILITY NAME Grifols Themoeutics
PERSON COLLECTING SAMPLES D;Iijd S. Graham
CERTIFIED LABORATORY Pace Analytical
Part A: Specific Monitoring Requirements
STORMWAITKR DISCHARGE OUTFALL (S)DO)
MONITORING REPORT
SAMPLES COLLECTED DURING CALENDAR YEAR. 2015
(This monitoring report is due at the Division no later than 30 days from the date
the facility receives the sampling results from the laboratory)
COUNTY hhnston
PHONE NO. [phone]
Lab #NCZffW cent #067
PLEASE SIGN ON THE REVERSE 4
Outfalll�
Date
....SiTn-P'A'e--Co6
mold
00530!-.,.
emicat F)
-�"Ch Oxygen Demand—
and; eill
- G reas
. .... .. .
­-:4TAuU1 Sispiuded Sollds,�-­.-
-Benchaa,k'
120
30
03-26-15
-<25.0
<5.0
6.2
-1
Note. Ifyou report a sampled value in excess of the benchmark value, you must implement Tier I or Tier 2 responses. See General Permit text.
Dom this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes Xno
(if yes, complete Part 13)
Part B: Vehicle Maintenance Activity Monitorincr Requirements
Outfan,
No..
�I:Date<
;­Szm e ,Coliecttd,—.0il
-- ----
. . .....
—:00400,--­­­-­<
apd
Total Suspended
"tkhdiidtunits'
c�:New MotorOSIUm Usage,
Bencbm2rk
.30
-.100...
... ....... "
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier I or Tier 2 responses.
See General Permit tmct
STORM EVENT CHARACTERISTICS:
Date 0-26-15 (first event sampled)
Total Event Precipitation (mches): .24
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
A= DWQ Central Fflw
NCDMWDWQ
1617 Mail Service Center
Raleigh
, NC 27699-1617
SWU-248-102107
Page 1 of 2

STORMWATER DISCHARGE OUTF'ALL (SDO)
MONITORING REPORT
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are signfficant penalties for submitting, false information, including
the possibility of fives and imprisonment for knowing violations."
(Signature of Permitted)
/Y lynoe C Zo/S
..(Date)
SVX-248-102107
Page 2 of 2

Page 14: Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Permit No NCGO60000 or Certificate of Coverage No.: N. CG060039
Facility Name: Grifols Therapeutics
County: Johnston County Phone No.919-369-6473
Inspector: David S. Graham
Date of Inspection: 3/2612016
By this signature, I certify that this report Is accurate and complete to the best of my knowledge:
(Signature of Pailrmittee. or. Designee)
1.Oddill Description
0utfall No. <':'.': '- 2 Structure (pipe, ditch, etc.) ditch exiting existing pond_ _
Receiving Stream: tributary to the Neuse River
Describe the Industrial activities that occur within the outfall drainage area: Pharmaceutical Mfg.
2. Color
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium,
dark) as descriptors: Clear with alight brown tint
3.Odor
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor,
etc.): None
4. Clarity
Choose the number which best describes the clarity of the discharge where 1 is clear and 10 Is very
cloudy:
1 0 3 4
Page 1
SWU-242-020705
10

6. Floating Solids
Choose the number which best describes the amount of floating solids In the stormwater discharge where
Is no -solids and 10 Is the surface covered with floating solids:
2 3 4 5 6 7 8 9 10
6. Suspended Solids
Choose the number which best describes the amount of suspended sollds In the stormwater discharge
where no solids and 10 is extremely muddy:
1 a 3 4 5 6 7 8 9 10
7. Foam
Is there any foam In the stormwater discharge? Yes No
8. Oil Sheen
Is there an oil sheen in the stormwater discharge? Yes
8. Deposition at Outfall
Is there deposition of material (sediment, etc.) at or Immediately below the outfall? Ye(D
10. Erosion at Outfali
Is there erosion at or Immediately below the outfall? Yes No
11.Other Obvious Indicators of Stormwater Pollution
List and describe Done
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, deposition or erosion may be
Indicative of conditions that warrant further investigation and corrective action.
Page 2
SWU-242-020705

GENERAL PERMPr NO. NCG120000
CERTIFICATE OF COVERAGE NO. NCGO60039
FACiLiTY NAME Grif is Therapeutics
PERSON COLLECTING SAMPLES David S. Graham
CERTIFIED LABORATORY Pace Aa diffleal
Part A. Specific Monitoring Requirements
STORMWATERDISCHARGE OUTFALL (SDO)
MONITORING REPORT
SAMPLES COLLECTED DURING CALENDAR YEAR 2015
(This monitoring report is due at the Division no later than 30 days from the date
the facility receives the sampling results from the laboratory.)
COUNTY JohnstoA
PHONE NO. [phone]
- Lab #NCJW W cent 4067
PLEASE SIGN ON TIE REVERSE ->
�No r
y Sample Collected, -
00340-:
00556
00400
00530
ChexnucaE Oxygen=Demand,
17
-: Oil and„Grease;.
-'m
-pH;,
-unitsMA
Total Suspended Solids,
•'
" 420'
' 30
6.0 = 9.0
100
2
03-26-15
<25.0
C5-0
6S .
9.6
Note: if you report a sampled value in excess of the benchmark value, you must implement Tier, 1 or Tier 2 responses. See General Permit text
Does this facility.perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per maanth? -yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activl oulteAngRequirements
Na r= s
"Date;:;.-=00556L
Sample C011ec6ed,YOiI
00530
00400
andGirease,
yTotal Suspended So[ids,
„A:pH, ,
Standard units-
=:New`Motor,Oil:Ussge,
= Avera a annual lhno
Benchmark
Note: if you report a sampled value in excess of the benchmark value, or outside the benchmark range for pli, you must implement Tier 1 or Tier 2 responses.
See General Permit text
STORM EVENT -CHARACTERISTICS -
Date 03-26-15 {first event sampled)
Total Event Precipitation (inches): 24
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Attu: DWQ Central Fles
NCDENW DWQ
1617 Mail Service Center
Raleigh. NC 276*1617
SWU 248-102107
Pane 1 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or personas who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for !mowing violations."
(Signature of Fermittee) (Date)
SWU-248-102307
pave. 7 of 7

1 r
aceAnalyiical
rAwpBGSWICOM
Laboratory Repoi f
Sam Vedder
Grifols Therapeutics, Inc:
8368 US 70 West
Clayton, NC 27520
Pace Analytical aervicas, Inc.
6701 Conference Drive
Rakdoh, NC 27607
(910)834-49M
Page 1 of 1
.Report. Date: 07/1012015
Date Recehied: 07/02/2015
Project: STORMWATER
Pace Project No.: 92257041
Sample: OUTFALL 01 Lab ID: 92267041001 • -Collected: 67101/1511:30 Matrix: Water
Parameters
Oil and Grease
Total Suspended SoAds
Chemical Oxygen Demand
Sample: OUTFALL 02
Result
Parameters Resul
Oil and Grease
Total Suspended Solids
Chemical Oxygen Demand
Revlewed try:
Nicole Gasiorowski
nlcole.gasiorowski®pacelabs.com
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
s
is
Units
Report Limit,
Analyzed Qualifiers
ND
MOIL
0711011510:48
ND
mg1L
_5.0
5.6
0710711512:41
21.0
mg1L
10.0
07/0811516:00
Lab !D: 92267041002 Collected: 07/01/15 11:45' Matrix: Water
Units
Report Limit
Analyzed Qualifiers
ND
mg1L
6.0
07/10/1510:49
ND
mg1L
2.5
07i0711512:42
ND
mgll-
10.0
07/08/1516:00
Charlotte Certification IDs .
98DO KinceyAve. Ste 100. Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certifleation 0: 99OD6001
Asheville Certification Ids
2225 Riverside Drive, Asheville, NC 28804
FlorldalNELAP Certification #: E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification M 37712
North Carolina Bloassay Certification M 16
North Carolina Drinking Water Certification #: 37731
FloridalNELAP Certification #: E87627
Kentucky UST Certificatlon #: 84
West Virginia Certiflcallon M 357
Vlrginla/VE AP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certifleatlon #: 356
VlrgWaIVELAP Certification #:460222
Page 1 of 3

OewaLca" n:
r -
May ib, 2015`
f 2'
'Page 2 of 2 to for Internal Use bnly
Client Name: 64t4
Courlor (Circle): Fed Ex UPS LISPS CUoiit s'Comfierclal t ac .Other
Custody Seal an GoolorfBox Present: Ej yea no Seats Intact: yes ❑ no
Packing Matorlal: ❑ Bubble Wrap 0 Bubble Begs ❑ None Other
Circlo Thermometer Used; IR (run SN:122066387Type of Ice; � Blue None �smplea on lee, cooling proms him begun
Ili Gun Sack Un A.-ii isxri
Temp Correction Paster Add !.S btract � �C
%
Vote and Initlels of person exam n ng; .
-
-
`
Correatod Cootor Tomp: r
8totogfcat Tlaeuo le Frozen: Yes No
•.
con f prh arYA110�!-
Tamp should be above 6eaztng id6.O
Cornreonta:
shack
Chain of Custody Piecort:
Yes Ho QWA
1.
Chain of Custody Filled Out:
No . ❑WA
2.
3. +
Chain of Cuslody Relinquished, _. Y tto ❑rvr;
Sam IerName&3 tiaturaon.000:t:�s•
Ya kouf7NtA
4 r�r;
Samples Anlvad within Hotd Time:.. ..-...�_, Yes- ❑No=• WA
5,
Short Hold TEmti Ansf !a s72hr : s
raltii o� CIWall
9;
Rush *urn Around.Tlma Re uestedt
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7.
Sufficient Volume:
- E3No :.17NlA
Correct Contelners Uaed:
Ho ly A
9,
-Pace.Contalnera Used'
�J/Y Ho' ,ONIA
Containers Intact;
Ye. ❑No, '06
10,
Filtered volume raosived for.Dlssolved tests' .
"Wii t: 4' 1261A
11.
Semple Labels match COO.
t a QNo 'bW-A'
12:
Artcludea date1dme11OfAnel 13 Matrix: -00✓
All conlainers rtw4i g pteservalfan have toeen eheaka •
&Yna ❑No QwA
13,
All containers nsoding preservation -are found to be in
dlyz ❑No ❑WA
camolenos whir EPA rr+ccmmands0(m.
exc. iota VOA MArm, i OK WI-DRO water
Dyes.. ❑No
Samples checked for dechlorlriallon:
Orsi-QRo lliuA
14.
Heeds ace InMOAVIals >$mrn .
My" ONo WA
15:
-
Trip Blank Present:
C]raa'.❑No ' NiA
-WA
1t3:
Trip Blank Custody goals Present
by. ONo -,
Pace Tip Blank Lot # H urchased :
Client Notigaatlonl Rosolutlori' Field Date Required? Y f N,
Parson Contacted: t)aialTlme:
Comments/ Resolution: _ . __—
n_�_9225�:7041
SCURF 18RF i v 1G Data: ff II ll :"ll II
Review:: •
Nola; Whanovsr there is a dlaorepanoy etfecting North Caro:Ina compllence 92257041
aempte3, a oopy af.thls forrri wtil be sent to the Nord Carotin MNR
Gertulceuon Office { Le out of hold. Inoarrect pMernttve, out of tamp, (It no'ausi aVanaOls)
IneorceCt oontelners)
""" �Of 3

0
CHAIN-OF-CUSTODY.I Anaiytical:Request Document
The Cheri-o€duEody 8 e LEGAL DOCU�+ E T. ADte*vam fields must be.00mpleYed accu ab*. a
3ec6W A Sedan 6 saaoo C
' Aegihad Moat kgoraafi= d riot %Ik mdom :orot, 16evwtioR 1 Of ,
cov%WV. - Grdbix PAPW Ta Gritola
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0 -I
(�IaceAnalX�cal*
xewpacel+r st m
Laboratory Report
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 1 of 1
Sam Vedder
Report Date: 66/0912015
Grifol§ Therapeutics; 6ri .
Date Received: 05/29/2015
8368 US 70`West
Clayton, NC 27520
Project: Stnmrxater
Pace Project No.: 92251949
Sample: Outfall #1
Lab ID: 92251949001 Collected: 05/28/15 09:08
Matrix: Water
Parameters
Results Units
Report Limit Analyzed
Qualifiers
Oil and Grease
NO mg/L
5.0 06/03/16 13:17
Total Suspended Solids
NO mg/L
4.5 06/02/1513:28
Chemical Oxygen Demand
NO mg1L
10.0 06109/15 12:30
M1
Sample: Outfall #2
Lab ID: 92251949002 Collected: 05/28/15 09:20 Matrix: Water
Parameters
Results Units
Report Limit
Analyzed Qualifiers
Oil and Grease
ND mg1L
5.0
06/03/15 13:17
Total Suspended Solids
NO mg1L
2.6
06/0211513:28
Chemical Oxygen Demand
NO mg/L
10.0
0610911512:30
ANALYTE QUALIFIERS
tvll Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
Reviewed by:
Nicole Gesiorowski
nicole.gasierawskl®pacelabs.com
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification M 67
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersvllle, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FlortdalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Ccrtlficatlon #: 37712
North Carolina Sloassay Certification M. 16
North Carolina Drinking Water Certification #: 37731
Flodda/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginlaNEt.AP Certification #: 460221
North Carolina Wastewater Certification #. 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virglnia/VELAP Certification M 460222
Page 1 of 5

- r
Dorwinent Name: Sampla Co» ditlon t
• _ _ ReceE t BCUR _
Imurdent Revlsed; Moy 16,,2016'
Page 1 of: ' 1 --
Muing Atithorkies:
Pace FtatBlah Qualitv'Offloe
'Page 2 of 2 4 foi Internal Use Only
Cifent Name: -
Courier (Circlo): Fed Ex UPS U8P6 . Client Commercial, , Paoe Other
Custody Seat on Coolirlsox Present: C] yea �'' no Seals intact: Z ye4 Q no
Packing Material: 11 eubblo Wrap a Bags N Other
Circle.Thermomota_ r Usodr lR dun :1220$53BTTy of I do,W Blue None 8amplas on top, Cgofing process has begun
tR 6u,n gS,..k Lin 7[
Temp Coir®ctlori'Factor `Add l tracC`]
Corrected COOIor Tony: C
Tamp atrould be shove fieezli+� la $'C
—Biologlcal,Tiaarta is Fran Yeo No
Cammantar
eta and Initial oT peraan e mining
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mmpliar= with EPA raoomniendclion.
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Comments! ResoluNcn:
SCURF dlkPI �Lj Data,...S- iW Q ' ��� 1'949
Review:. 5 "31-+ pp.ppM: ;� , n E -
wto: whwmer thane is a dlsuapo*.i1Yodlag Norw dwowo coin l nca
camptas, a coPll of lhte forr6 will ba sent tothv North CetoMa DEKNR
Cedlltoit'lorr Qtfce I,e out of hold, lnconact protervattvo, oul of temp,
.. .... _. .. i>7aorroctaantelnors) .=.�,..,:a-�.: � -- - _ • .
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Page 2 of 5

O
CHAIWOF-CUSTODY'TAnaljtdal Regdest-'Document
.The Chain-o€Giistodjr is a LEGAL- DOCUMENT. An mwvar fields must ba oompteted acmwate*.. a
Section A •Sotdon a: ' SetiYian c • _ ..
Raq,e&ed Coam h4o mld.-, - _ •. Regtiiw Project Ifft Iiatum :: 1 . - , .•' �IYO�O 00. i Of t
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Page 4 of 6

O
N
CHAIN -OF -CUSTODY I Analytic al Request. Document
The Chaki-d-Custody is a LEGAL DOCUMENT. AJI relevard Bards must be completed aoa¢ m*- a
Secum A €aelion a SCCGM C
Vilna craw bdanym Rerw Ragwred PeejeCt lMorntodac I ,1, a Wonnanan: Pa I Of I
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1

ceAnaly qa1 *
wowpemaraesWrs
Sam Vedder
Grifols Therapeutics, Inc.
8368 US 70 West
Clayton, NC 27520
Project: STORMWATER
Pace Project No,: 02260197
Sample: OUTFALL 01
Laboratory Report
Pace Analytical Services, Ina
8701 Conference Drive
Raleigh, NC 27607
(910)834-4Ma4
Page 1 of 1
Report Date: 07/2912015
Date Received: 07/24/2015
Lab lA: 92260197001 Collected: 0712311510:20 Matrix:' Water
Parameters Results
Units
Report Limit
Analyzed Qualifiers
Oil and Grease '
ND
mgtL
5.0
07/29/15 10:00
Total Suspended Solids
6.7
mg/L
=2.5
07/28115 14:09
Chemical Oxygen Demand
ND
MOIL
%0
07/29/15 09:15
Sample: OUTFALL#2
Lab 10. 92260197002 Collected:' 07/23/1510:35 Matrix: Water
Parameters Results
Units
Report Umit
Analyzed Qualifiers
Oil and Grease
ND
mg/L
6.0
07/29/1510:01
Total Suspended Solids
ND
m01L
2.5
07/28/1814:10
Chemical Oxygen Demand
ND
mg/L
10.0
07/29/16 09:16
Reviewed by:
Nicole Gaslorowski
nicole.gasiorowskl®pacelabs.com
Raleigh Certification IDs
6701 Conference Drive. Raleigh, NC 27607
North Carolina Wastewater CerflfEcaOon 0: 67
Charlotte Certification IDe
9800 Kln'ceyiAve. Ste loO,-HuntersvlAe, NC 28078
North Carolina Drinking Water Certification #; 37706
North Carolina Field Services Certification #: 6342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification 10s
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification 0: 37712
North Carolina Bloassay Certification M 16
North Carolina Drinkfn0 Water CerUfiGHUGn #: 37731
Florlda/NEt.AP Certification #:'E87827
Kentucky UST Certification #: 84
West Virginla Certification #: 357
VirplaNELAP Certificallon #: 460221
North Carolina Wastewater CarUticatlon #: 40
South Carolina Certification #-. 99030001
West VIrgINa Certificallon #: 356
VirgintaNELAP Certification #: 480222
Page 1 of 3

c?CBA1181�+t1C81
'
I]ocument Name; Sample Condition Upon
.. R del t' SCUR .
t]ocument Revfsed: May 16'2016'.
Fa e 1 of 2•..
Document No.:
F-RAL-C"01-rev.03
Issuing Authodlles:
Pace Ralel Quaq Offlce . '.
. "Pap2 of 2 Is for hitemal Use Qnry
Client Name; _
Courier (Circle); Fed Ex UPS' -LISPS Client Comnlerclal ace Other
Custody Seal on Cooledeox Present: Q yea no Seals intact: ayes 0 no
PeckEng 14latsrlal; 0 Bubble Wrap . B35371
�!ldone. Other
Clrefa Thormomotor Us_ ed: IR Oun '122086a of Ico Wet Blue None ❑ asmples on Ice, coaling pr000sa his begun
IR Qun l3
Temp Conaetloo Factor: Add�6ubtract C
ZC
Date and In e ao perexIing
Corrected Cooler Temp.:
BlofagloW Tissue Is Frozen; Yos No
Temp should be above floaxing to 94C
Comments:
Chain of Cuatody Present;
e. ,ONo El MA
1.
Chain of Custod Filled Out:
' . Yoe . ❑No . ❑N1A
2.
Chain of Custod •ReNn ulshad:
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3.
Sampler Neme Slgnsturevn COG:
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Correct Containers Used
Yes '❑Ns mWA
9.
-Pace Containers Used:
. a! :C3N6 owA
Containers Intact:
s: ❑No IINfA
10.
Filtered volume receNed for OEssolved tests
C3Yn • ❑Ne VVA
11.
Sample Labels match COC:
❑No 6NfA
12.
-includes dWe10melll}/Anal sEa Matrix:
All containers needing preservation have been checked.
ri, ❑No gNrA
13.
All containers needing preservation are found to be In
Yea ❑No 13MA
oompllancaWi EPA!EWroco,nnrandoflon.
osv V0A, oosrorm,rac:oao,wi-or;o
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Samples checked for dechlorinollon:
es 07 o _ ❑MIA
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Trip Blank Present;
3
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❑Yes ❑Nc 31NIA
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Client Notificatlonf ReaoluHon: • Field Data Required? Y ! N
nap m�..�-
rereon-�omac�ea: ..o.o, . ,......
Comments/ Resatullon:
SCURF ISRF ante:
Review:: �1
Note'. Whonovar there is a disuepanry stfedhg North Ceml3ne oompllsoce
eemplea, a copy of thie form W3 be sent to the North Caroena DEHNR
cvrUflceuon dfftco (I.e out of hold, Incon' Opiasuivative, out of lamp,
Incori+ect cantalnero)
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Page 2 of3
i

CHAIN -OF -CUSTODY 'I Analytical Request'Doct
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October 20, 2008
S. Daniel Smith
Surface Water Protection Regional Supervisor
Raleigh Regional Office
North Carolina Department of
Environment and Natural Resources
1628 Mail Service Center
Raleigh, NC 27699-1628
Re: Notice of Violation NOV-2008-OC-0008
Notice of Recommendation of Enforcement
Talecris Biotherapeutics, Inc.
Permit Number NCG060039
Johnston County, NC
Dear Mr. Smith:
8368 U5 70 West
Clayton NC 27520
4 OCT 2 2 2008
On October 10, 2008, Talecris Biotherapeutics, Inc. ("Talecris") received your October 8, 2008
Notice of Violation and Notice of Recommendation of Enforcement ("NOV") regarding a leak of 30%
ethylene glycol in water or "anti -freeze" (the "Substance") discovered at Talecris on September 17,
2008. We appreciate your attention to this matter and enclose herein Talecris's timely response to the
NOV.
Preliminarily, we note that the NOV states that the discharge was in violation of N.C.G.S. 143-
215.1(a)1 because it is illegal to discharge wastewater without a permit. This statement is not correct as
applied to Talecris. Talecris is permitted for stormwater discharge pursuant to its NPDES Permit No.
NCG060039 and the Substance was discharged through a permitted outfall. Thus, although Talecris
may have violated its stormwater permit, it did not discharge wastewater without a permit as alleged
within the NOV.
Next, the Division of Water Quality ("DWQ") requests discussion of potential secondary
containment options for the Substance at Talecris. Secondary containment is not viable due to the
configuration and nature of the system. As you may be aware, Talecris, a biopharmaceutical company,
is one of the largest producers and marketers of human plasma -derived protein therapies in the world.
Plasma contains many therapeutic proteins, which 'Calecris extracts through a process called
fractionation at our facility in Clayton, North Carolina. From this fractionated plasma, we manufacture,
produce, and distribute therapies (i.e. drugs) that extend and enhance the lives of people suffering from
chronic and acute, often life -threatening, conditions. Throughout the process, we must maintain and
www.talecris.com
■

Ta&p��
regulate the product at tightly controlled temperatures, which requires us to operate multiple, robust
refrigeration systems.
The E-447 chilled glycol system is the cooling system for approximately two-thirds of the
facility's HVAC cooling needs. The Substance is the cooling media supplied to air handling units that
support manufacturing areas that operate at 65 to 70 degrees F. This system consists of approximately
10,000 linear feet of distribution piping ranging from in diameter from 24" to a/4" with a total system
volume of approximately 100,000 gallons. It serves five buildings on site.
The Substance is constantly circulated within the pipes over the course of the five buildings, and
there is no storage tank serving as a reserve for the Substance. Therefore, secondary containment is
conceptually and technologically infeasible.
Finally, we are disappointed that the DWQ states its intent within the NOV to recommend an
assessment of a civil penalty. Upon review of Talecris's response, we respectfully request that DWQ
reconsider this matter. If this matter is to be recommended for civil penalty, however, Talecris requests
that the civil penalty be minimal and that this response, Talecris's five (5) day report ("Report") and any
other applicable information be considered in DWQ's recommendation. In particular, the civil penalty
should be minimal because of the following factors:
I. The Leak Was Accidental And Was Immediately Caused By Sudden Equipment
Failure.
On or about July 30, 2008, an independent contractor involved with removing and replacing an
air handling unit reconfigured piping that was integral to a cooling system on the roof of a building on
Talecris's property. As part of this work, the contractor configured the system to terminate with a unique
butterfly valve (the "valve") which was previously in place. The valve successfully served to cap the
cooling pipe for approximately eight (8) weeks without leak or incident. As set forth within its Report,
on September 17, 2008 at 7:10 a.m., Talecris discovered a fluid (the Substance) leaking from the valve.
Approximately thirteen (13) hours earlier, an independent contractor working on the roof of the building
observed the valve pipe and valve functioning without a leak.
As previously reported, and as referenced within the NOV, Talecris believes that no more than
6,033 pounds or 634 gallons of the Substance was released. Talecris has determined that the immediate
cause of the leak was a failure of the valve. Although Talecris now believes that securing the valve with
a cap would have prevented this leak, the proper, uninterrupted function of the valve over the preceding
eight (8) weeks did not alert Talecris or its contractors to any specific or immediate risk.
Due to the relatively small volume of the Substance passing through the valve (as compared to
the 100,000 gallons total Substance charge within the cooling system) computer -control sensors did not
indicate a loss of the Substance or impact to system function at any time. Talecris was not alerted until
an electrical contractor on the roof of the building observed the Substance and, following Talecris
procedures, reported the leak. Accordingly, if assessed, the amount of any civil penalty should be low
because the leak was, at base, an accident which resulted from the sudden failure of the valve that
showed no signs of damage or defect.
www.talecris.com
0M

Ta&S!t�
II. Talecris Responded Diligently To The Release And Has Taken Measures To
Minimize The Risks Of Future Releases.
Upon discovering the leak, Talecris acted immediately to stop the leak and recover the
Substance. A new cap was installed on the cooling pipe to cover the leaking valve. Talecris also
contacted GARCO, Inc. ("GARCO") to act as its environmental response contractor. GARCO promptly
arrived at the property and, using three vacuum trucks, captured and removed the Substance from the
Talecris property. Rocks were also washed, and the wash water was collected by the vacuum trucks.
The work was designed to reduce any impacts to Talecris's property, and to prevent adverse impacts to
public resources or health.
Since the release, Talecris has taken extraordinary measures to prevent a future similar
occurrence. First, all cooling pipes and valves have been inspected for integrity and design. Second,
Talecris is updating the standard operating procedures for all work conducted on pipes at its facility.
Third, Talecris has modified its Job Hazard Analysis procedures to require worker verification of the
requirements for pipe work within the Hazardous Work Permit. Fourth, all maintenance personnel and
contractors have been and will be trained to stress the importance of pipe work requirements.
III. Any Adverse Impacts Were Limited To Talecris's Private Property.
Following entry into the storm sewer, the Substance proceeded into a natural depression on
Talecris's private property and ultimately joined overflow water from Talecris's permitted stormwater
discharge pond. (See Attached Map). The overflow from the pond travels approximately half of a mile
before discharging into the Neuse River pursuant to Talecris's Stormwater NPDES Permit No.
NCG060039 ("Outflow #1").
Due to the relatively small scale of the release and Talecris's quick response, the Substance did
not adversely impact public resources. Fortunately, flow levels from the permitted stormwater discharge
pond were high at the time of the release due to recent precipitation. As the Substance entered the pond
overflow, it was diluted by the high water flow and the long distance (more than half a mile) to Outflow
#1. Discharge water testing at Outflow #1 revealed 15,600 ppm ethylene glycol. Research supports that
much higher levels are required to cause harm to fish (150,000 ppm for bluegill). In addition,
observations revealed no impact to fish or other wildlife in either the Neuse River or the overflow creek
from the permitted stormwater discharge pond. To the contrary, live fish were observed swimming
normally in the overflow creek from the permitted stormwater discharge pond. Accordingly, the civil
penalty should be minimal because the total impact was limited to the natural depression area wholly
contained on Talecris's private property.
IV. Additional Factors Set Forth Within N.C. Cen. Stat. § 143B-282.1(b).
• The Degree and Extent of Harm
There was no harm to public health as a result of the leak. There is also no evidence of adverse
impacts to the public resources of the State. In particular, no fish were killed in the Neuse River or
www.tatecris.com

Ta&Eq�
within the overflow water discharge from Talecris's stormwater retention pond. Rather, impact to fish
was limited to the small natural depression on Talecris's private property. While approximately 50
small fish (bluegills) were found dead and removed from the water, other fish and wildlife were
apparently unharmed and were re -located as part of the response effort. Thus, the extent of harm was
limited to a small area and was quickly contained and abated.
• The Duration and Gravity of the Violation
The duration of the release was relatively short. The valve which failed had been observed intact
approximately 13 hours prior to observation of the leak. When Talecris became aware of the leak, it was
immediately stopped and Talecris initiated swift and thorough recovery efforts. These response and
recovery efforts were completed within approximately six (6) hours. Furthermore, the short duration is
supported by evidence that the impact to fish was limited to a small, natural depression on Talecris's
private property and that the Substance was not permitted to reach Outflow 41 in high levels on the day
of the incident. Finally, the gravity of the violation was low. The release was an accident and was
immediately caused by the failure of a valve which was compromised.
• Effects on Ground or Surface Water Quantity or Quality or on Air Quality
Air quality and groundwater quality were not affected by the leak. Surface water impacts were
limited to the small area of natural depression on Talecris's private property. The low levels of the
Substance which reached Outflow #1 did not have noted effects upon surface water quality.
• The Cost of Rectifying the Damage
There are no ongoing impacts to the environment as a result of the release. Accordingly, there
are no further costs required to rectify the damage. However, Talecris did expend considerable
resources to reduce any impacts, and prevent such releases in the future. First, Talecris expects that the
costs incurred through its environmental contractor, GARCO, will exceed $10,000. Furthermore,
Talecris spent approximately $1,000 for expedited laboratory testing analysis to determine the levels of
the Substance within the area of natural depression on its property, and at Outflow 91.
Talecris has also devoted considerable time by various employees and company management to
investigate the incident and employ measures to prevent the risks of future similar occurrences. The
investigation of the incident required 65 employee -hours and involved the participation by numerous
management and technical personnel, including the vice president, principle of construction
management company, engineers, safety professionals, and mechanics. Inspections of pipes and valves
at the facility has required 224 employee -hours, and an additional 26.5 employee -hours have been spent
in additional training activities.
• The Amount Saved by Noncompliance
www.falecris.com

Ta&qt�
Other than the cost of a cap in place of the failed valve, there were no avoided costs which were
the cause of the release. The cost of the cap is negligible — approximately $30.00. Moreover, had the
cap been in place, Talecris would not have lost approximately $35,000 worth of the Substance.
• Whether the Violation Was Committed Willfully or Intentionally
Talecris did not commit any violation willfully or intentionally.
• The Prior Record of the Violator
Talecris has a permit to discharge stormwater pursuant to NPDES Permit No. NCG060039. It
has never been issued an NOV relating to the permit. Talecris is also a partner in the Environmental
Stewardship Program established by the Pollution Prevention Branch of the North Carolina Department
of Environment and Natural Resources (NC DENR).
Talecris also has a strong record of environmental stewardship in other areas. For instance,
under its NPDES Stormwater Permit, Talecris is required to conduct semi-annual testing of its
stormwater system. Talecris, however, voluntarily conducts the semi-annual testing on a monthly basis.
These tests and their costs are voluntarily assumed by Talecris in order to ensure surface water
protection.
Talecris has also been a member of the Wildlife Habitat Council (WHC) since 2007 and received
its certification in 2008. Partnership with WHC provides Talecris with an opportunity to demonstrate
responsible corporate environmental stewardship by formulating and implementing a balanced and
operative wildlife management program at its property in Clayton, NC. Talecris has set aside
approximately 89 acres of its facility to be managed as wildlife habitat. The area consists of forestland,
grassland, and surface water features. In particular, two small creeks that drain to the Neuse River are
located and protected within the wildlife habitat.
• The Costs to the State of the Enforcement Procedures
The costs to the State of the enforcement procedures have been minimal as Talecris has worked
diligently to provide the necessary information to DWQ (and other regulatory bodies) in a timely and
cooperative fashion.
www.fatecris.com
0�

Ta&sq�
In conclusion, Talecris requests that DWQ not recommend the assessment of a civil penalty in
this matter. If DWQ proceeds to recommend a civil penalty, then Talecris requests that the civil penalty
be minimal in light of the information provided and referenced above. Please contact me if you have
any questions.
Sincerely,
Karen H. Cook
Director, ESS
CC: Mary Kuhn, Sr. VP, Operations
Aaron Golub, Corporate Counsel
www.talecris.com

Talecris Biotherapeutics, Inc.
Clavton, North Carolina
Red Circle = Natural Low Area on Talecris Property
Blue Circle = Outfall #1

of W A rFR —9�/
U����� C
October 8, 2008
CERTIFIED MAIL 7006 0810 0002 6049 6959
RETURN RECEIPT REQUESTED
Ms. Karen H. Cook
Director, Environmental, Safety, & Security
Talecris Biotherapeutics, Inc.
8368 US 70 West
Clayton, North Carolina 27520
Michael F. Easley, Governor
William G. Ross, Jr., Secretary
North Carolina Department of Environment and Natural Resources
Subject: Notice of Violation NOV-2008-OC-0008
Notice of Recommendation of Enforcement
Talecris Biotherapeutics, Inc.
Permit Number NCG060039
Johnston County
Dear Ms. Cook:
Coleen 14. Sullins, Director
Division of Water Quality
The Raleigh Regional Office has conducted a review of the information you provided to our office concerning the
ethylene glycol discharge that occurred at the Talecris Biotherapeutics facility on September 17, 2008. The 5-day report
indicated that the discharge resulted from a failed butterfly valve from the B300 Building glycol cooling system, The
amount of ethylene glycol released to surface waters was reported to be 6,033 pounds or 634 gallons. The discharge
caused a fish kill of various sizes and species.
Please explain how secondary containment for the ethylene glycol cooling system will be provided to prevent future
discharge occurrences. The discharge that occurred violate N.C.G.S. 143-215.1(a) I which state that it is illegal to
discharge wastewater without a permit, which may result in assessment of civil penalties of up to $25,000 per violation
per day.
It is the intent of the Raleigh Regional Office, Division of Water Quality, to foreword a recommendation to the
Director for the assessment of civil penalties for discharging ethylene glycol without a permit September 17, 2008.
Please respond within 10 days receipt of this letter to the above requests. Please provide any information you
would like for us to consider in our recommendation for enforcement.
Sincerely,
R
S. Daniel Smith
Surface Water Protection Regional Supervisor
Raleigh Regional Office
CC
Np" Caro ina
)atlurally
North Carolina Division of Water Quality Raleigh Regional Office Surface Water Protection Phone [phone] Customer Service
Internet: www.ncwatcrt628 Mail Service Center Raleigh, NC 27699-1628 FAX [phone]
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Ta ecr®s
aIO CPAPEUTICS
September 22, 2008
Mr. David Mayes
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Dear Mr. Hayes:
8368 US 70 West
Clayton NC 27520
Karen H. Cook
Director
Environmental, Safety, & Security
Tel [phone]
Fax [phone]
Cell 919.270.4855
karen,[e-mail]
On Wednesday, September 17, 2008, an ethylene glycol leak was discovered from the B300 processing
building cooling system at Talecris Biotherapeutics, Inc. located at 8368 US 70 west, Clayton, NC
27520. The leak, located on the roof of the building, was first discovered at 7:10 a.m. Personnel were
unable to immediately quantify the release or determine whether a reportable quantity of ethylene glycol
had been released. Nevertheless, out of an abundance of caution, the release was reported via telephone
to the appropriate agencies on the day it was discovered.
This letter and attachments serve as the written follow-up report of the release.
Date and Time of Release: The ethylene glycol release was discovered at 7:10 a.m. on September 19,
2008. The release occurred from a valve on the B300 Building cooling system. Approximately 13 hours
earlier (at approximately 6 p.m. on Tuesday, September 16), the same valve was observed by an
employee working for a Talecris contractor. At that time, no leakage was observed.
A review of the glycol system operating parameters did not indicate a change in operating conditions
indicative of loss of ethylene glycol from the system. No personnel were on the roof the night of the
incident. As a result, "Talecris cannot determine when the leak started.
Source and Cause of the Release: The release occurred from the facility's glycol cooling system. It was
caused by failure of a valve on the system.
Estimate of Release Amount: Talecris cannot determine the precise amount of ethylene glycol that was
released. The volume of the glycol system is approximately 100,000 gallons. The system is dynamic in
that the glycol is in constant circulation. Operators determine that glycol must be added to the system
when the system has difficulty holding temperature and pressure parameters. Glycol had not been added
to the system since 2007. Since the system is in constant circulation, specific system volume is difficult
to determine. To estimate the release quantity, Talecris calculated both an Absolute Worst Case Release
Estimate as well as a Likely Release Estimate as specified on Attachment 1.

7 C.0
[3f (1Tris
HERA PFU TICS
Using the Absolute Worst -case formulas and assumptions identified in Attachment 1, it is possible that
17,276 pounds reached surface waters. Again, as detailed in Attachment 1, however, Talecris believes
that it is more likely that approximately 6,033 pounds of ethylene glycol reached surface waters. The RQ
for ethylene glycol is 5,000 pounds.
Media to Which the Pthylene Glycol was Released: The released ethylene glycol reached a depression at
the end of the storm water pipe. Discharge from this depression joins with other water sources and flows
to the Neuse River, a distance approximately one mile away,
The facility's storm water system collects storm water from building roofs and storm drains, carries the
water tluough a pipe and discharges into a depression in a creek bed. Downstream from the storm water
discharge, the overflow from a retention pond also enters the creek bed (see Diagram 1). In the 24-hour
period preceding the release, over 0.5 inches of rain had fallen on the facility, so storm water flows were
high.
Once the release was identified, the depression was pumped out, to the extent possible, and the rocks
were power washed. The wash water was also collected.
Actions Taken in Response: Immediately upon discovery, the release was stopped by installing a blind at
the leaking pipe. Talecris also immediately contacted Garco to initiate clean-up. Garco brought three
vacuum trucks to the site and collected any liquid with a pink hue. As noted above, storm water in the
depression was also collected. Rocks with pink staining were washed and the wash water was collected.
Once the ethylene glycol solution reached the facility's storrii water depression, its concentration was
naturally diluted. To confirm that harmful concentrations were not released to the Neuse River, samples
at the outfall were taken on the morning of September 19"', when the highest concentrations would be
expected At that time, the samples contained 1.5% ethylene glycol.
Known health risks or required medical attention: Talecris is unaware that anyone required medical
attention as a result of the release. Fifty dead fish, however, were found on Talecris' property, between
the discharge of the storm water system and where the retention pond overflow enters the creek bed. Tile
majority of the fish were fingerlings, 3-4 inches in size, and appeared to be bluegill and black bass.
Three of the bluegills were 6 inches in length.
Talecris has taken the incident very seriously and responded quickly to stop, contain and remediate the
release. Please contact me if you have additional questions.
Sincerely,
Karen H. Cook
Director, ESS
www.talecris.com
0■

Standard Operating Procedure for SSO Calls
1. Gather Required Information:
f Date of call q 1'"l (cs _
/ Ilevel Time of call
)rn Name of callerok U ' SJl„zc),-
Caller phone # 31,q 35� Lj 3 r75-
*CU�z,�iek Q Facility name : —rc..�j C&A5
County 1C (10• -
UU j6t�ec-'-\5) Permit # (if available) [ECG D(e0039
Start date cil-n Start time
End date _A/ End Time
j 00 AM PM
AM PM
Estimated volumer�c Q)
ff Location QQ&A
033A?, �63�(gc it
vdoolipsr taken to c
ff
I
DDD�/
ause_ Q�e C tIJ� I R le—Uc .
r ct Jh.�QeQ '—k C Z tUC4
reach surface waters
Name of Surface Water
Volume reaching surface waters
Conveyance S m we_4A ftA),CJ
Did Spill/SSO result in fish kill
CAJ
Received by_�
2. Enter into BIMSfi�c
Log into the public portal version of BIMS(http://bims.enr.state.nc.us:7001/Welcome.do)
Go to Tasks, Incident, Enter incident
For SSO, fill in the SSO and 24 hour forms, record the incident number, then save the file and close.
For Spills, check the type of spill box, fill in the Incident report, record the incident number and close..
3. Comments:

Ta(DIOTII fRAPf UTlC.S
Attachment 1: Worst -Case Release Calculations
Absolute worst case release:
Absolute worst case is based on the fact that the system was refilled with 7000 gallons between 9/17/08
and 9/22/09. However, this is not a likely amount released because the system had not been refilled since
2007, and Utilities had noticed in June 2008 that levels were low in other areas of the system.
7000 gallons of 30% ethylene glycol added to the system
= 2100 gallons pure ethylene glycol
= 19782 lb pure ethylene glycol
Amount recovered:
3807 gallons @ approx. 7% ethylene glycol
= 266 gallons pure ethylene glycol
= 2506 lb pure ethylene glycol
Worst case Volume Reaching Surface Waters (gallons):
2100 gallons — 266 gallons = 1834 gallons
= 17276 lb
Likely release amount:
3000 gallons of 30% ethylene glycol
= 900 gallons pure ethylene glycol
= 8539 lb pure ethylene glycol
Amount recovered:
3807 gallons @ approx. 7% ethylene glycol
= 266 gallons pure ethylene glycol
= 2506 lb pure ethylene glycol
Likely Volume Reaching Surface Waters (gallons):
900 gallons — 266 gallons = 634 gallons
= 6033 lb
�r J Pot-1AA �ticct�(�P 41c'/
www. talecris.com
0■

,0� VJ It TER
roc oq Form CS-SSO
Collection System Sanitary Sewer Overflow Reporting Form
PART I
This form shall be submitted to the appropriate DWQ Regional Office within five days of the first knowledge of
the sanitary sewer overflow (SSO).
Permit Number: NCGO60039 (WQCS# if active, otherwise use treatment plant NCIWQ#)
Facility: TALECRIs- cLArroN Incident#
Owner:
TALECRIS BIOTHERAPEUTICS Region: RALEIGH
City: CLAYTON County: JOHNSTON
Source of SSO (check applicable) : Sanitary Sewer Pump Station
SPECIFIC location of the SSO (be consistent in description from past reports or documentation - i.e. Pump Station 6,
Manhole at Westall & Bragg Street, etc.) : Near East Pond of Property
Latitude (deg reeslminutelsecond): 35/37/02 Longitude(degrees/minute/second) 78/25/01
Incident Started Dt: 09-16-2008 Time &'00 pm Incident End Dt 09-17-2008 Time.
7:10 a. m
(mm-dd-yyyy) hh:mm AM/PM (mm-dd-yyyy) hh:mm AMIPM
Estimated volume of the SSO: SEC A iTA 46N gallons Estimated Duration (Round to nearest hour);
Describe how the volume was determined: Estimated based on flawrate and observation
Weather conditions during SSO event: Dry. Rain slopped at beginning of avant.
Did SSO reach surface waters? 0 Yes❑No❑ Unknown Volume reaching surface waters (gallons): see attached
Surface water name: UNN-Nmeb -FRt9ytT*('� t-o tJCPLAAE RI1)6rit
Did the SSO result in a fish kill? ❑ Yes ❑ No ❑ Unknown If Yes, what is the estimated number of fish killed?50
SPECIFIC cause(s) of the SSO:
❑ Severe Natural Condition ❑ Grease ❑ Roots
❑ Inflow and Infiltration ❑ Pump Station Equipment Failure ❑ Power outage
❑ Vandalism ❑ Debris in line 0 Other (Please explain in Part 11)
Immediate 24-hour verbal notification reported to: Stephanie Brixey [phone]
0 DWQ ❑ Emergency M mt. Date (mm-dd yyyy): 09-17-2008 Time (hh:mm AM/PM): to:aoam
If an SSO is ongoing, please notify Regional Office on a daily basis until SSO can be stopped.
Per G.S. 143-215.1C(b), the responsible party of a discharge of 1,000 gallons or more of untreated wastewater to surface
waters shall issue a press release within 48-hours of first knowledge to all print and electronic news media providing general
coverage in the county where discharge occurred. When 15,000 gallons or more of untreated wastewater enters surface
waters, a public notice shall be published within 10 days and proof of publication shall be provided to the Division within 30 days.
Refer to the referenced statute for further detail.
The Director, Division of Water Quality, may take enforcement action for SSOs that are required to be reported to Division unless it
is demonstrated that
1) the discharge was caused by severe natural conditions and there were no feasible alternatives to the discharge; or
2) the discharge was exceptional, unintentional, temporary and caused by factors beyond the reasonable control of the Permittee
and/or owner, and the discharge could not have been prevented by the exercise of reasonable control.
Part II must be completed to provide a justification claim for either of the above situations. This information will be the basis
for the determination of any enforcement action. Therefore, it is important to be as complete as possible.
WHETHER OR NOT PART II IS COMPLETED, A SIGNATURE IS REQUIRED AT THE END OF THIS FORM.
CS-SSO Form October 9, 2003 Page 1

O OF VJA r�9�G
Form CS-SSO
y r
o Y Collection System Sanitary Sewer Overflow Reporting Form
PART I I
ANSWER THE FOLLOWING QUESTIONS FOR EACH RELATED CAUSE CHECKED IN PART I OF THIS FORM
AND INCLUDE THE APPROPRIATE DOCUMENTATION AS REQUIRED OR DESIRED
COMPLETE ONLY THOSE SECTIONS PERTAINING TO THE CAUSE OF THE SSO AS CHECKED IN PART I
In the check boxes below, NA = Not Applicable and NE = Not Evaluated
A HARDCOPY OF THIS FORM SHOULD BE SUBMITTED TO THE APPROPRIATE DWQ REGIONAL OFFICE
UNLESS IT HAS BEEN SUBMITTED ELECTRONICALLY THROUGH THE ONLINE REPORTING SYSTEM
Severe Natural Condition hurricane tornado, etc.
Describe the "severe natural condition" in detail.
How much advance warning did you have and what actions were taken in preparation for the event?
Comments:
Grease (Documentation such as cleaning, inspections, enforcement
actions, past overflow reports, educational material and distribution date,
etc. should be available upon request,)
When was the last time this specific line (or wet well) was cleaned?
Do you have an enforceable grease ordinance that requires new or retrofit of grease traps/interceptors? ❑Yesu No ❑NA❑NE
Have there been recent inspections and/or enforcement actions taken on nearby restaurants or other ❑ Yes❑ No ❑ NA ❑ NE
nonresidential grease contributors?
Explain.
Have there been other SSOs or blockages in this area that were also caused by grease? YesO No D NA 11 NE
When?
If yes, describe them:
Have cleaning and inspections ever been increased at this location? ❑Yell] No ❑NA ❑NE
Explain.
CS-SSO Form October 9, 2003 Page 2

Have educational materials about grease been distributed in the past?
When?
and to whom?
Explain?
If the SSO occurred at a pump station, when was the wet well and pumps last checked for grease
accumulation?
Were the floats clean?
Comments:
Roots
Do you have an active root control program?
Describe
1JYe,El No❑NA❑NE
❑Y"D No❑NA❑NE
❑Yell No❑NA❑NE
Have cleaning and inspections ever been increased at this location because of roots? ❑Yes❑ No ❑NA ❑NE
Explain:
What corrective actions have been accomplished at the SSO location (and surrounding system if
associated with the $SO)?
What corrective actions are planned at the SSO location to reduce root intrusion?
Has the line been smoke tested or videoed within the past year? ❑ Yes❑ No ❑ NA ❑ NE
If Yes, when?
Comments:
Inflow and Infiltration
Are you under an SOC (Special Order by Consent) or do you have a schedule in any permit that ❑Yes❑ No ❑NA ENE
addresses IV
CS-SSO Form October 9, 2003 Page 3

Explain if Yes:
What corrective actions have been taken to reduce or eliminate I & I related overflows at this spill location
within the last year?
Has there been any Row studies to determine 1f1 problems in the collection system at the SSO location? ❑Yes❑ No ❑NA ❑ NE
If Yes, when was the study completed and what actions did it recommend?
Has the line been smoke tested or videoed within the past year? Ll YesD No ONAU NE
If Yes, when and indicate what actions are necessary and the status of such actions:
Are there III related projects in your Capital Improvement Plan? 11 Yes❑ No DNA 11 NE
If Yes, explain:
Have there been any grant or loan applications for 1/1 reduction projects? Yes❑ No ONADNE
If Yes, explain:
Do you suspect any major sources of inflow or cross connections with storm sewers? ❑ YesA.] No ❑NA ❑NE
If Yes, explain:
Have all lines contacting surface waters in the SSO location and upstream been inspected recently? ❑Yes❑ No ❑NA ❑NE
If Yes, explain:
What other corrective actions are planned to prevent future III related SSOs at this location?
Comments:
Pump Station Equipment Failure Documentation of testing, records etc
shoul be provided upon request.)
What kind of notificationtalarm systems are present?
Auto-dialerlteiemetry (one-way communication) []Yes
CS-SSO Form October 9, 2003 Page 4

Audible Elyes
Visual Dyes
SCADA (two-way communication) ❑Yes
Emergency Contact Signage Dyes
Other ❑Yes
Describe the equipment that failed?
What kind of situations trigger an alarm condition at this station (i.e. pump failure, power failure, high
water, etc.)?
Were notificationlalarm systems operable? Yell No NA NE
If no, explain:
If a pump failed, when was the last maintenance and/or inspection performed?
What specifically was checked/maintained?
If a valve failed, when was it last exercised?
Were all pumps set to alternate?
Did any pump show above normal run times prior to and during the SSO event?
Were adequate spare parts on hand to fix the equipment (switch, fuse, valve, seal, etc.)?
Was a spare or portable pump immediately available?
If a float problem, when were the floats last tested? Now?
If an auto -dialer or SCADA, when was the system last tested? Flow?
Comments:
❑Yes❑ No❑NA❑NE
❑YeZI No❑NA❑NE
❑ Yes❑ No ❑ NA ❑ NE
❑Yes❑ No❑NA❑NE
CS-SSO Form October 9, 2003 Page 5

Power outage Documentation of testing, records etc. should be
provided of alternative power source upon request.)
What is your alternate power or pumping source?
• e
Did it function properly? ❑YeL]No❑NACINE
Describe?
When was the alternate power or pumping source last tested under load?
If caused by a weather event, how much advance warning did you have and what actions were taken to
prepare for the event?
Comments:
Vandalism
Provide police report number:
Was the site secured? ❑ Yeo No ❑ NA ❑ NE
If Voa hnW?
Padlocked Control Panel t--1
Have there been previous problems with vandalism at the SSO location? Yesu No LINA U NE
If Yes, explain:
What security measures have been put in place to prevent similar occurrences in the future? 11 Y,,D No ❑ NA ❑ NE
Comments:
Debris in line Rocks sticks rags and other items not allowed in the
collection system, etc.)
What type of debris has been found in the line?
How could it have gotten there?
Are manholes in the area secure and intact? YAJ No NA NE
CS-SSO Form October 9, 2003 page 6

When was the area last checked/cleaned?
Have cleaning and inspections ever been increased at this location due to previous problems with debris? ❑Yes❑ No ❑NA ❑NE
Explain:
Are appropriate educational materials being developed and distributed to prevent future similar ❑Yes❑ No(INAElNE
occurrences?
Comments:
Other (Pictures and a police report should be available upon request.)
Describe:
RLVTCP F�+ VhLVb FkIL b . j1eLCkSjNi, CAL(,J L Oft_ TIJ C Rt;Of ht3-q) Lo_ I\ 110a -IW bfzA 10.
Were adequate equipment an� es available to fix the problem? ❑ YesO No ❑ NA ❑ NE
If Yes, explain:
If the problem could not be immediately repaired, what actions were taken to lessen the impact of the
SSO? We stopped the leak and removed the material within six hours of discovery.
Comments:
For DWQ Use Only:
DWQ Requested an Additional Written Report:
If Yes, What Additional Information is Needed:
Comments:
QYeso No1JNA❑NE
CS-SSO Form October 9, 2003 Page 7

As a representative for the responsible party, I certify that the information contained in this report is true and accurate
to the best of my knowledge.
Person submitting claim: David Auge
Signature: 2,
Telephone Number: 919-359-4375
Date: 09-19-08
Title: ESS Manager, Environmental
Any additional information desired to be submitted should be sent to the appropriate Division Regional Office within five days of first
knowledge of the SSO with reference to the incident number (the incident number is only generated when electronic entry of this form
is completed, if used).
CS-SSO Form October 9, 2003 Page 8

Attachment 1
Absolute worst case release:
Absolute worst case is based on the fact that the system was refilled with 7000 gallons
between 9/17/08 and 9/22/08. However, this is not a likely amount released because the
system had not been refilled since 2007, and Utilities had noticed in June 2008 that levels
were low in other areas of the system.
7000 gallons of 30% ethylene glycol added to the system
= 2100 gallons pure ethylene glycol
= 19782 lb pure ethylene glycol
Amount recovered:
3807 gallons a approx. 7% ethylene glycol
= 266 gallons pure ethylene glycol
= 2506 lb pure ethylene glycol
Worst case Volume Reaching Surface Waters (gallons):
2100 gallons -- 266 gallons = 1834 gallons
= 17276 lb
Likely release amount:
3000 gallons of 30% ethylene glycol
= 900 gallons pure ethylene glycol
= 8539 lb pure ethylene glycol
Amount recovered:
3807 gallons @ approx. 7% ethylene glycol
= 266 gallons pure ethylene glycol
= 2506 lb pure ethylene glycol
Worst case Volume Reaching Surface Waters (gallons):
900 gallons -- 266 gallons = 634 gallons
= 6033 lb

Diagram l:
o�a►N �
s6rm
Wa*Qv
No+ -b scA.le.
aet o�r►�N
g
rRheook-6%
powtot

w A r�RQ�
p C
April 22, 2005
Mr. David Auge
Taiecris Biotherapeutics, Inc.
8368 Highway 70 West
Clayton, NC 27520
Dear Mr. Auge:
• Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
Subject: Permit No. NCG060039 _
Talecris Biotherapeutics, Inc. (q 3S5, 75
Formerly Bayer Corporation
Johnston County
Division personnel have reviewed and approved your request to change the your name under the General Permit,
received on April 19, 2005.
Please find enclosed the revised Certificate of Coverage. The terms and conditions contained in the General
Permit remain unchanged and in full effect. This revised Certificate of Coverage is issued under the requirements of
North Carolina General Statutes 143-215.1 and the Memorandum of Agreement between North Carolina and the U.S.
Environmental Protection Agency.
If you have any questions, please contact the Stormwater Permitting Unit at [phone], extension 502.
Sincerely,
Alan W. Klimek P. E.
cc: DWQ Central Files
Raleigh Regional Office, Water Quality Section
Stormwater Permitting Unit
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North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone [phone] Customer Service
Internet: h2o.enr.state.nc.us 512 N. Salisbury St, Raleigh, NC 27604 FAX [phone]
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STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE No. NCG060039
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
TALECRIS BIOTHERAPEUTICS, INC
is hereby authorized to discharge stormwater from a facility located at
TALECRIS BIOTHERAPEUTICS, INC
8368 HIGHWAY 70 WEST
CLAYTON
JOHNSTON COUNTY
to receiving waters designated as a UT to the Neuse River, a class C NSW stream, in the Neuse River Basin in
accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, I11, IV,
V, and VI of General Permit No. NCG060000 as attached.
This certificate of coverage shall become effective April 22, 2005.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day April 22, 2005,
Alan W. Klimek, Director
Division of Water Quality
By Authority of the Environmental Management Commission

POWHATAN QUI
NORTH CAROLINA-1
7.5 MINUTE SERIES
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355 "1 NW RALE!GH 19 MI.�
:LA YrON) CLAYTON 2.6 Mr: 133 25, 734' 735 2180000 FEET 731902
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566
Mr. Joseph Lemanski
Talecris Biotherapeutics
P.O. Box 507
Clayton, NC 27520-
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
November 14, 2005
V G G�6D3�
SUBJECT: Laboratory Certification Maintenance Inspection
Dear Mr. Lemanski :
Alan W. Klimek, P.E. Director
Division of Water Quality
s
k ,
kF� 1
Enclosed is a report for the inspection performed on, Nov. 07, 2005 by Mr. David�Eivingston'"
No deficiencies or lettered comments and/or recommendations are cited in this report, J.-response is
not required. We appreciate the fine job you and your staff are doing. As a certification requirement,
your laboratory must continue to carry out the requirements set forth in 15A NCAC 2H .0800.
Copies of the checklists completed during the inspection may be requested from this office.
Thank you for your cooperation during the inspection. If you.wish to obtain an electronic copy of this
report by email, or if you have questions or need additional information please contact us at 919-733-
3908.
Sincerely,
James W. Meyer
Laboratory Section
Enclosure
cc: David Livingston
Raleigh Regional Office
1n` Carolina
VNaturally
Laboratory Section 1623 Mail Service Center; Raleigh, NC 27699-1623
4405 Reedy Creek Road; Raleigh, NC 27607
Phone [phone] / FAX [phone] / Intemet: www.dwglab.org
An Equal OpportunitylAffirmaNe Action Employer - 50% Recycledll0°% Post Consumer Paper

�r
LABORATORY NAME:
ADDRESS:
CERTIFICATE NO:
DATE OF INSPECTION:
TYPE OF INSPECTION:
EVALUATOR:
LOCAL PERSON(S) CONTACTED:
I. INTRODUCTION:
On -Site Inspection Report
Talecris Biotherapeutics
P.O. Box 507
Clayton, NC 27520
#566
11 /7/2005
Maintenance
Mr. David G. Livingston
Mrs. Laura Bulluck
This laboratory was inspected to verify its compliance with the requirements of 15A NCAC 2H .0800
for the analysis of environmental samples.
II. GENERAL COMMENTS:
The laboratory is spacious and well equipped. All facilities and equipment are well maintained.
Records are well kept and most data looked good. Some further quality control procedures need to
be implemented.
III. DEFICIENCIES, REQUIREMENTS, COMMENTS AND RECOMMENDATIONS:
There are no deficiencies or comments in this report
IV. PAPER TRAIL INVESTIGATION:
This consisted of comparing data reported on DMR's submitted to this Division with the values
obtained on laboratory bench worksheets. All data reviewed for the months of July, August, and
September 2005 indicated no problems in proper transfer of data for reporting purposes.
V. CONCLUSIONS:
No response is required.
Report prepared by: David G. Livingston Date: 11/10/2005

o=�F W A TFRQG
LUr
—I
KAREN COOK
BAYER CORPORATION
PO BOX 507
CLAYTON, NC 27520
Dear Permittee:
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
August 23, 2002
Subject: NPDES Stormwater Permit Renewal
Bayer Corporation
COC Number NCG060039
Johnston County
In response to your renewal application for continued coverage under general permit NCG060000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983,
The following information is included with your permit package:
A new Certificate of Coverage
A copy of General Stormwater Permit NCG060000
A copy of a Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or
decree.
If you have any questions regarding this permit package please contact Aisha Lau of the Central Office Stormwater
and General Permits Unit at [phone], ext. 578
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Stormwater & General Permits Unit Files
Raleigh Regional Office
NCernDENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

Michael F. Eastey, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Gregory J. Thorpe, Ph.D.
Acting Director
Division of Water Quality
Dccemhcr 27, 2001
KAREN COOK
BAYER CORH)RATION
P (.) BOX 507
CI.,AYTON, NC 27520
Subject: NPI)ES Stormwatcr Permit Renewal
13AYER CORPORATION
COC Number NC(1060 }3y
,Inlrnstan Cnunly
Dear I'crrrlittec:
Your lacilify is Currently CoVered liu slurmwafCr dischuruC under General I'cruiil NCG060000. This permil expires
on Au�'usl 31. 2002, The Division Slaff is Currently in the proecsS Of [—CWI-itin�" this hCrmit :Old is scherlErled trr h.rvC
the permit reissued by late summer of 2Uf12. Once the hCrmit is re]SSUCLI, your fucilily would he el for
conlinued COVCra�tC under the rciSSUCd hcrn3it.
In order to assure your' continued CnveragC under the "Cneral permil, you must apply to file Division of Water
Quality (DWG)) lair renewal ol' your permit cnveragc. TO make this renewal process easier, we are informing you in
advance that your permit will he expiring. 1 riCIOSCd you will find a General Permit Coverage Renewal
Application Form. Tl application must be completed and returned by M-,irch 4, 2002 m order to assure Con€inucd
covcru�Cu under the general permit.
F�LIILirc to rcqueSt renewal within this lime period may result in a Civil assessment of al least $250.00. Lar4ticr
pcnallics may be assessed depending nn the dClinqucrrcy ol'll request. Disel of stor'mwtner from your facility
Wit}inut cnver:r"C under a valid storniWWer NPDI:S permit would constitute a viol,ttilim nil NCGS 143-215.1 and
could result in assessments ofcivil penal oh up to S 10.000 per Lilly.
Please nole that recent federal Ic,ist.rtinn has extended the "no CxpOsurc exClusion" to ,rl] ohcrator:S of indusu6nl
facililies in any ol'the I I categories ul' ",turn water discharges associafcd will] indusfr'ial activity." (exccpl
construction activitiCS). If you Icel your fucilily can certify a condition of "no exposure", i.e. ll laCilty industrial
malCrials and operations arc not CxposCd to StormwatCr, you Can apply for the no exposure exCht,ion. For additional
information Contact the Central Office Stormwatcr Staff mcmher lislcd below or clieck the Stormwmer & Gcncral
Pernlils Unit Wch Site at filth_//li2o.cnr.state.nc.us/SU/SIOrn►wutcr'.11tnil
11' file subject storniwaler discharge to walct:s ol' the state has hccn 1C1'111IM11Cd. plCase CorrlhlCte the enclosed
Rescission Request Furor. Mailing instructions are listed nil the hollow ol•ll form. You will he nolilicd ~viler the
rescission process has hccn conil
if you hove ally questions rCgarding IhC permit renewal procedures hleasC conlact Joe Albimon of the Ralcigh
Rcuional Oflicu at 919-571-4700 or Aish,r f au of the Gmtrzil Office Storrnwatur Unit at [phone]. cxt. 57Y
Sincerely.
131'arllcy 13ennclt. SupCrvisor
Stormwatcr and Guncral PCrmils Unit
cc: Ccntr'al Files
RalCi��h Rcuional OlTice
A�a
NCDENR
N. C. Division of Water QuaNy 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1- 800-623-7748

State of North Carolina
Department of Environment, Health and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27604
James B. Hunt, Jr., Governor ®�- 7 1 � ��n Howard, Jr., P. E.
Jonathan B. Howes, Secretary R[ r Director
April 30, 1993 m4y 0 � 1993
B. R. Morris DEH N R- RAL RO
Miles, Inc.
500 Grant Street
Pittsburg, PA 15219
Subject: General Permit No. NCGO60000
Miles, Inc.
COC NCGO60039
Johnston County
Dear Mr. Morris:
In accordance with your application for discharge permit received on September 30, 1992, we are
forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general
permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated
December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division
of Environmental Management. The Division of Environmental Management may require modification or
revocation and reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area
Management Act or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Mr. Steve Ulmer at telephone number 919n33-
5083.
cc
Sincerely,
Original Signed BY
Goleen H. Sullins
A. Preston Howard, Jr., P.E.
Raleigh Regional Office
Pollution Prevention Pays
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
! ! :: ►! ► III
STORMWATER DISCHARGES
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Miles, Inc.
is hereby authorized to discharge stormwater from a facility located at
Miles, Inc.
US Hwy 70 East, two miles east of Clayton
Clayton
Johnston County
to receiving waters designated as an unnamed tributary to the Neuse River in the Neuse River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III
and IV of General Permit No. NCGO60000 as attached.
This Certificate of Coverage shall become effective April 30,1993,
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day April 30, 1993.
Original Signed Sy
Coleen H. Sullins
A. Preston Howard, Jr., P.E., Director
Division of Environmental Management
By Authority of the Environmental Management Commission

i
355W NW PALL!,- 09 Mr.N,
POWHATAN DUI
NORTH CAROLINA—J,
7.5 MINUTE SERIES (
SW/4 SELMA 15, GU/
'LAYTON) CLA /'2.6 Mf; >33 25' 734 735 Z 180000 FEES 736
lz
ic
—14
rl
}I •�//�, ( j 00 ~ ]90] ; �� �. l� g Cem295
\ 1570 I n -1
loo
Povfttan
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"i 0 Ab - Cem ii S Sop i ,lrr
Frl
76 so
pij
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66
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6
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2521,
em. a "; !'• .� ,�• .\` = - \�. 7 Park ��•
�yaM 242
f 'Ch ��

April 22, 2005
Mr. David Auge
Talecris Biotherapeutics, Inc.
8368 Highway 70 West
Clayton, NC 27520
Dear Mr. Auge:
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
Subject: Permit No. NCG060039
Talecris Biotherapeutics, Inc.
Formerly Bayer Corporation
Johnston County
Division personnel have reviewed and approved your request to change the your name under the General Permit,
received on April 19, 2005.
Please find enclosed the revised Certificate of Coverage. The terms and conditions contained in the General
Permit remain unchanged and in full effect. This revised Certificate of Coverage is issued under the requirements of
North Carolina General Statutes 143-215.1 and the Memorandum of Agreement between North Carolina and the U.S.
Environmental Protection Agency.
If you have any questions, please contact the Stormwater Permitting Unit at [phone], extension 502.
Sincerely,
Alan W. Klimek P. E.
CC DWQ Central Piles
Raleigh Regional Office, Water Quality Section
Stormwater Permitting Unit
Nort�hhCarolma
Nalurally
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone [phone] Customer Service
Internet: h2o.enr.state.no.us 512 N. Salisbury St. Raleigh, NC 27604 FAX [phone]
An Equal OpportunitylAHirrnative Action Employer — 50% RecycledltWo Post Consumer Paper

f- f ,
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE No. NCG060039
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
TALECRIS BIOTHERAPEUTICS, INC
is hereby authorized to discharge stormwater from a facility located at
TALECRIS BIOTHERAPEUTICS, INC
8368 HIGHWAY 70 WEST
CLAYTON
JOHNSTON COUNTY
to receiving waters designated as a UT to the Neuse River, a class C NSW stream, in the Neuse River Basin in
accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I,11, 111, IV,
V, and VI of General Permit No. NCG060000 as attached.
This certificate of coverage shall become effective April 22, 2005,
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day April 22, 2005.
Alan W. Klimek, Director
Division of Water Quality
By Authority of the Environmental Management Commission

7 e ZVZ 3r '• , d,
35- 3-' 3C-)
POWHATAN QUI
NORTH CAROLINA-JI
7.5 MINUTE SERIES
_ - SWA SELMA 15' OUP
135 it/ NW RALEtG+`,' rg Mr..\
1AYTON) CCArrON 2.6 Mr; 733 25'134 735 2180000 FEET 736
f
19002
/ I I70,
r-�� , �i _ter-�'r i•' — _ _ / 511 �! , `� - .�`-~
Powhatan
Ch
,11�1 •)� �� 190i 'Cem��� • •,C
.New Bethhi \\ , ✓ - t`�� i/ - �
300 `
72 • • - - ', :r- `` 300 \ . I II Lr ' n_ . I , '`1 `, .` ' 1f1 ,I
��gs• j ysx o , sue. . • \ ' ' a ��^ \� ` \.�-v��-� • ` `'
,76" ^:\` .W Faso'
-267
�� A •�• '+, - �` �` .., / ��1 �\), 11 'rt I
�: _ .jo -� •III `, 1\ �_ / +_ 1$
• \ » . c • 1 \ L 063~ • ,a I — II. :Icem \ � Ij7l� tl•
Ceam ]SSG
1 �` n ` �''`•
nthesda d50
em
a<'e }os
250
_��em a .I • I l ° • U I` \�J��F% ": 250 railer
a l -•�' 1 �� _ `I �� �•/ Park 1 )
Kt L'ielk �M z r1 �- _

Fj .' •F'._ �s ,` "T.k'a" .^r'4,r11, a� E`f�.'q"F .qu
y} �,y �:,, "Y.�•l A r.i \ si. L d?�..Y�Iry t . Mi'. �'� jy. ' � +d :ti.
Ta ecris
810THfRAPEUTlCS
r
!J
f l) • �, i t) P-Ai rii H
April 4, 2005
Ken Schuster
Raleigh Regional Office
Department of Environment and Natural Resources,
Department of Water Quality
1628 Mail Service Center
Raleigh, North Carolina 27699-1628
Dear Mr. Schuster:
Clayton site
8368 Hwy 70 West
Clayton, North Carolina 27520
David D. Auge
HES Manager, Environmental
Tel [phone]
Fax [phone]
Cell 919.270 6913
[e-mail]
In response to our phone conversation last week, I am sending you the shutdown schedule as well as a summary
of the RCRA inspection from last week.
At approximately 9:45 a.m. on March 30, 2005, two inspectors from NC DENR Hazardous Waste Section began
an inspection of the Clayton, NC site. Mr. Dick Denton, the Regional Compliance Officer and Mr. Michael Williford,
Eastern Region Compliance Supervisor. The inspection was triggered by anonymous complaints. In addition, the
inspectors would also conduct our annual RCRA inspection.
An anonymous complaint had been telephoned into EPA, Region 4 in Atlanta (3/25/05) and again into NC DENR
(date unknown). The complaint alleges that hazardous waste is being dumped to the ground at Clayton. Dumping
of this waste creates a hazard to the environment and poses a safety hazard to employees.
Ed George, Manager of Maintenance and Facilities was asked by David Auge to discuss the recently discovered
drain line break with the inspectors.
After hearing about the chronology of the discovery of the suspected pipe -breaks, follow-up investigation, and the
action plan, the inspectors concluded that the Hazardous Waste Section did not have jurisdiction. The waste was
not hazardous and was not traveling off -site.
Mr. Williford suggested that Talecris contact you concerning the complaint.
onmental
CC. Dick Denton, NCDENR, 1424 Carolina Avenue, Washington, NC 27889
www.talecris.com
■

tart Finish CN1R RESP
Activity Activity prigLDurj
Cat LL"
ID Description bur!D
if Fractionation ShutdownSchedule
Shutdown•
PR - PRE49HtU!"DOM
I
i
raft/Open Fractionation S/D
telSubmit Punchlist Items
Pool (5 Days Prior to S!D
It + III Suspension
I CleardRemove Zone 1 Equipment
F
f
CCR
WO I
Start)
MS1176
Draft/Open Fractionation SID CCR
40
40
1
8
29MAR05
08:00AMA
06APR05
03:59PM
BAY
RHAYE
C
Last
0 Last
W
E
MS1196
Create/Submit Punchlist Items WO
24
24
1
24
31MAR05
08:OOAM
04APR05
03:59PM
BAY
JHAME
MS1146
Last Pod (5 Days Prior to SID Start)
0
0
S
0
03APRO5
06:59AM`
BAY
JSELL
MS1156
Last II + III Suspension
48
48
S
0
03APR05
07:010AM
05APR05
06:59AM
BAY
JSELL
MSF075
Clean/Remove Zone 1 Equipment
72
72
S
0
05APR05
07:OOAM
08APR05
06:59AM
BAY
MLYNE
MS1136
Warm Up 350/348 (Centrifuge motors
running24h)
48
48
S
0
06APR05
07:OOAM
08APR05
06:59AM
BAY
MLYNE
R
I
warm Up 350/348 (Centrifuge
Remove Floor Scales I pH
Pre -Construction Safety
motors running24h)
Probes
Walkthrough
MS1186
Remove Floor Scales / pH Probes
3
3
1
0
07APR05
01:OOPM
07APR05
03:59PM
BAY
DCAYT
MS1166
Pre -Construction Safety Walkthrough
1
1
S
0
08APRO5
06:OOAM
08APRO5
06:59AM
BAY
JMARR
SD - 94HDC MV
€
i
I
Start 2005 Fractionation
Fractionation Down
Fractionation Shutdown
® Punchlist Work
I Reinstall Floor Scales/pH
Shutdown Milestone
Work
Fractionation Area
I
l
Probes
,; •
MS1000
Start 2005 Fractionation Shutdown
Milestone
0
0
S
0
08APRO5
07:OOAM`
BAY
EGEOR
MSF100
Fractionation Down
0
0
S
0
08APRO5
07:OOAM
BAY
MLYNE
MSF200
Fractionation Shutdown Work
184`
184`
S
0
08APR05
07:00AM
15APRO5
10:59PM
BAY
MLYNE
MSF910
Punchlist Work - Fractionation Area
48
48
S
0
13APR05
11:00PM
15APRO5
10:59PM
BAY
MLYNE
MS1150
Reinstall Floor Scales/pH Probes
3
3
S
5
15APRO5
03:OOPM
15APR05
05:59PM
BAY
DCAYT
MS6650
Begin Rough Clean Fractionation Area
0
0
S
0
15APRO5
11:OOPM
BAY
MLYNE
;
II
Begin Rough Clean Fractionation Area
I
® Fractionation Shutdown Work Complete
MSF900
Fractionation Shutdown Work Complete
0
0
S
0
15APR05
10:59PM
BAY
MLYNE
Data Date 31 MARD5 D7:ODAM
Run Date 01APR05 17:26
O Primavera Systems, Inc.
Early Bar
Progress Bar
Critical Activity
FRAC - Percent Complete < 100 (Do Not Modfy)
sr1 of 10
�
Bayer Healthcare
B300 Fractionation Shutdown Schedule
Detailed Schedule Layout
, , -, R-
RGD Pmjed Management Inc
��
Revsom
roved
Pro Management, Inc.
J �ect

1Adivity
Activity
Orig
Rem
Cal
I Total
I Start
Finish
CNiR.
RESP
ID
Description
Dur
Dur
ID
Float
MS1138
Fractionation Area - Cool Down to +5C
24
18
S
0
15AP1105
16APR05
BAY
MLYNE
0 Fractionation Area - Cool Down to +5C
1
11:O0PM
04:59PM
B Fractionation i a - Cool Down to 5C
MS1140
Fractionation Area - Cod Down to -5C
24
18
S
0
16APR05
17APR45
BAY
MLYNE
05:00PM
10:59AM
O Resume Processing Fractionation
MSF950
Resume Processing Fractionation
0
0
S
0
20APR05
BAY
JSELL
08:59PM
MS1122
First II +III Suspension
36
36
S
82
21APRO5
22APR05
BAY
JSELL
❑ First II +'11I
Suspension
09:OOAM
08:59PM
® Fina1
Release Fractionation
MSF999 Final Release Fractionation
0
0
S
0
26APR05
BAY
MLYNE
06:59AM
i
# 1 Floor Drain Repairs
PR = PRE.SHUTl A411M .
onfim
design for floor drains and
I
place order
DR1560
Confirm design for floor drains and place
6*
2*
1
22
30MAR05
31MAR05
DHEUE
order
12:00PMA
09:59AM
Fabricate floor drains
DR1550
Fabricate floor drains
40*
40*
1
22
31MAR05
07APR05
DHEUE
10:00AM
09:59AM
order s
creenings for backfill
DR1450
Order screenings for backfill
1
1
1
33
31MAR05
31MAR05
DHEUE
12:00PM
12:59PM
Order
rt boxes from Brian Flack
DR1490
Order dirt boxes from Brian Rack
1
1
1
41
31MAR05
31MAR05
DHEUE
12:00PM
12:59PM
Order
S piping for drain repairs
jf
DR1510
Order SS piping for drain repairs
1
1
1
13
31MAR05
31MAR05
DHEUE
12:00PM
12:59PM
DR1580
Secure Tyvek protective suites for excavation
6
6
1
46
31MAR05
01APR05
Dr El)E
Secure
Tyvek protective suites for
excavation
12:OOPM
09:59AM
I Deliver
open top dumpsters
DR1500
Deliver open top dumpsters
2
2
1
41
01APR05
01APR05
DHEUE
01:OOPM
02:59PM
I Sti
ge screenings for backfill
DR1460
Stage screenings for backfill
2
2
1
33
04APR05
04APRO5
DHEUE
Delivery of SS piping
2
2
1
13
01:OOPM
04APRO5
02:59PM
04APRO5
DHELIE
I De
ivery of SS piping
DR1530
01:OOPM
02:59PM
❑
re-fab plumbing bends
DR1520
Pre-fab plumbing bends
10
10
1
13
06APR05
07APR05
DHEUE
09700AM
10:59AM
DR2000
Fab/Install Isolation Barriers
8
8
S
0
07APR05
08APR05
BAY
DHEUE
Fabltnstall Isolation Ba
ers
10DOPM
05:59AM
Install Filter Media on Returns
i
DR2010
Install Fitter Media on Returns
3
3
S
0
08APR05
06 R05
BAY
DFlEUE
03:0OAM
05:59AM
SD - SMJiDdIM� �
e I
DR1430 Open East doom to room 3013 3 3 S 0 08APR05 08APR05 DHEUE Open East doors to room 3013
07:OOAM 09:59AM I I
1 1 I I I
Sheet 2 of 10

Activity
Activity
Orig
Rem
Cat
Total
I Start
Finish
CNTR
RESP
ID
Description
Our
Dur
ID
Float
+
i
DR1440
Install ramp to 3013
2
2
S
0
OMM05
013APR05
DHEUE
Install ramp to 3013
I
10:OOAM
11:59AM
!
Remove Wall between Rm
fl Reinstall Wall between
3013 & Rm 350 I
I
Rm 3013 & Rm 350 II
DR1441
Remove Wag between Rm 3013 & Rm 350
4
4
S
1
08APRO5
10:OOAM
OaAPRO5
01:59PM
DFfUE
DR1442
Reinstall Wall between Rm 3013 & Rm 350
10
10
S
5
15APR05
15APRO5
Dt LIE
08:OOAM
05:59PM
I I
DR1810
Layout & Mark floor cuts
1
1
S
4
08APR05
08APRO5
DHELE
I
Layout & Mark floor cuts
10:00AM
10:59AM
Install Floor Protection
DR1820
Install Floor Protection
2
2
S
0
OSAPRO5
08APRO5
DHEUE
10:OOAM
11:59AM
DR1840
Mark floor cuts for WestUia pads
Sawcut for Westfalia operating pads
1
2
1
2
S
S
127
127
OSAPRO5
11:OOAM
08APRO5
08APRO5
11:59AM
08APR05
DHEUE
DFElJE
I
I
Mark floor cuts for Westfalia
I Sawcut for Westfalia operating
pads
pads
DR1850
12:OOPM
01:59PM
€
DR1860
Demo for Westfalia operating pads
4
4
S
127
OSAPRO5
08APR05
DHEUE
I Demo for Westfalia operating
pads
02:OOPM
05:59PM
1 of
DR2020
Locate UIG Conduits (3 Locations)
3
3
S
2
08APRO5
08APRO5
Ka
DIfUE
Locate u1G Conduits 13
Locations)
10:OOAM
12:59PM
DR1000
Mobilize equipment
3
3
S
0
08APR05
08APR05
DFELIE
I Mobilize equipment
12:OOPM
02:59PM
DR101 Q
Loc 1 Saw cut concrete
3
3
S
0
OSAPRO5
08APRO5
DHELE
I Loc 1 Saw cut concrete
03:OOPM
05i59PM
DR1020
Loc 1 Remove concrete
2
2
S
10
08APR05
OWRO5
DF EUE
1 Loc 1 Remove concrete
06:OOPM
07:59PM
I Loc 2 Saw cut concrete
DR1030
Loc 2 Saw cut concrete
5
5
S
0
08APRO5
08APRO5
DFIEUE
06:OOPM
I 10:59PM
DR1070
Loc 1 Excavate to expose plumbing
5
5
S
10
OaAPRO5
09APRO5
DFttJE
I Loc 1 Excavate to expose plumbing
08:OOPM
12:59AM
j
I Loc 2 Remove concrete
DR1040
Loc 2 Remove concrete
3
3
S
0
08APR05
09APR05
DHELE
11:OOPM
01:59AM
Loc 3 Saw cut ooncrete
I Loc 3 Saw cut concrete
DR1050
3
3
S
0
OSAPRO5
09APRO5
DHEUE
11:OOPM
01:59AM
'
I Loc 1 Take measurements for new SS plumbing
DR1100
Loc 1 Take measurements for new SS
plumbing
1
1
S
10
09APR05
01:OOAM
09APRO5
01:59AM
DF ELIE
i
I Loc 3 Remove concrete
DR1060
Loc 3 Remove concrete
2
2
S
2
09APR05
09APR05
DHELE
02:OOAM
03:59AM
DR1130
Loc 1 Remove damaged plumbing
2
2
S
10
09APR05
09APR05
DHELE
I Loc 1 Remove damage tl plumbing
02:00AM
03:59AM
DR1670
Loc 4 Saw cut concrete
3
3
S
0
09APR05
09APR05
DHELIE
I Loc 4 Saw cut concretel
02:OOAM
04:59AM
I
Sheet 3 of 10

Activity
Activity
Qrig
Rem.
Cal
Total
Start
Finish
CNTR
RESP
ID
Description
Dur
Dur
1D
Float129
DR1160
Fabricate plumbing for Loc 1
4
4
S
16
09APR05
09APRO5
D-EUE
I Fabricate plumbing for
Lac 1
02:OOAM
05:59AM
I Lac 2 Excavate to expose
plumbing
DR1080
Loc 2 Excavate t0 expose plumbing
8
8
S
0
09APRO5
09APRO5
D -ELIE
02:OOAM
09:59AM
j
I Lac 1 Set up sump pump
DR1620
Loc 1 Set up sump pump
1
1
S
10
09APR05
09APRO5
DHEUE
04:OOAM
04:59AM
DR1090
Loc 3 Excavate to expose plumbing
5
5
S
2
09APRO5
09APRO5
OFELIE
I Lac 3 Excavate to expose
plumbing
04:OOAM
08:59AM
I
I
I Lac 4 Remove concrete
DR1680
Loc 4 Remove concrete
2
2
S
0
09APR05
09APRO5
DF ELiE
05:OOAM
06:59AM
E
I Lac 1 Jet plumbing both
directions
DR1630
Loc 1 Jet plumbing both directions
4
4
S
10
09APR05
09APRO5
DHEUE
05:OOAM
08:59AM
I Lac 4 Excavate to expose
plumbing
DR1690
Loc 4 Excavate to expose plumbing
6
6
S
0
09APR05
OMPR05
DF BJE
07:00AM
12:59PM
I
I Loc 3 Take measurements
for new SS plumbing
DR1120
Loc 3 Take measurements for new SS
1
1
S
2
09APR05
09APR05
DHEUE
plumbing
09:OOAM
09:59AM
DR1650
Loc 1 Muck out excavation
2
2
S
10
09APR05
09:OOAM
09APRO5
10:59AM
DHEL1E
I Loc 1 Muck out excavation
DR1110
Loc 2 Take measurements for new SS
1
1
S
0
09APRO5
09APR05
DHEUE
I Loc 2 Take measurements for new SS plumbing
plumbing
10:00AM
10:59AM
I`
I Loc 3 remove damaged plumbing
DR1150
Loc 3 remove damaged plumbing
2
2
S
2
09APRO5
09APRO5
DHELIE
10:OOAM
11:59AM
I Location 3 Fabricate Plumbing
DR1180
Location 3 Fabricate Plumbing
6
6
S
6
09APR05
10:OOAM
09APRO5
03:59PM
DHELIE
1 Loc 1 Camera plumbing
DR1640
Loc 1 Camera plumbing
1
1
S
10
09APRO5
OMPR05
DFEUE
11:DOAM
11:59AM
DR1140
Loc 2 Remove damaged plumbing
2
2
S
1
09APR05
09APR05
Dl tl
I Loc 2 Remove damaged plumbing
11:00AM
1Z59PM
I Fabricate plumbing for Loc 2 I
DR1170
Fabricate plumbing for Loc 2
8
8
S
0
09APRO5
09APRO5
DHEUE
11:00AM
06:59PM
[
I Loc 3 set up pump
DR1610
Loc 3 set up pump
1
1
S
2
09APRO5
09APR05
DHEL1E
12:DOPM
12:59PM
I Loc 1 install new plumbing
DR1190
Loc 1 install new plumbing
4
4
S
10
09APRO5
09APRO5
DHEUE
12:OOPM
03:59PM
I Loc 4 Take measurements for new SS plumbing
DR1700
Loc 4 Take measurements for new SS
1
1
S
0
09APRO5
09APR05
DHEL)E
plumbing
01:00PM
01:59PM
DR1470
Jet drains
4
4
S
1
09APR05
09APRO5
EX-ELIE
_..._-----------
------------ ---------.-........ .._._:
I Jet drains
01:OOPM
04:59PM
I Loc 3 Jet plumbing both directions
DR1590
Loc 3 Jet plumbing both directions
4
4
S
2
OMPRO5
09APRO5
DHEUE
Loc 4 Remove damaged plumbing
2
2
S
1
0
01:OOPM
09APR05
04:59PM
09APRO5
DHEL E
I
I Loc 4 Remove damaged plumbing
DR1710
02:OOPM
03:59PM
I
i
Sheet 4 of 10

Activity
Activity
prig
I Rem
Cal.
Total
I Start
Finish
CNTR
RESP
ID
Description
Our
Dur
ID
Float
DR1720
Fabricate plumbing
4
4
S
5
09APRO5
09APRO5
DFEUE
I
I Loc 4 Fabricate plumbing
ILoc4
02:OOPM
05:59PM
( I
I Loc 4 Set up sump pump
DR1730
Loc 4 Set up sump pump
1
1
S
0
09APR05
09APRO5
DFELIE
04:OOPM
04:59PM
i
DR1220
Loc 1 backfill and tamp
2
2
S
10
09APRO5
09APRO5
DFEUE
I Loc 1 backfill and tamp
04:OOPM
05:59PM
I Camera drains
DR1480
Camera drains
1
1
S
1
09APRO5
09APR05
DFEUE
05:OOPM
05:59PM
j
I Loc 3 Muck out excavation
j
DR1600
Loc 3 Muck out excavation
2
2
S
2
09APRO5
09APRO5
D -EL E
05:OOPM
06:59PM
1 Loc 4 Jet plumbing both
directions
DR1740
Loc 4 Jet plumbing both directions
3
3
S
0
09APR05
09APR05
DFElJE
05:OOPM
07:59PM
I Loc 1 Install Vapor barrier
I
and dowels
DR1250
Loc 1 Install Vapor barrier and dowels
3
3
S
10
09APRO5
09APRO5
DFEUE
06:OOPM
08:59PM
DR1660
Loc 3 Camera plumbing
1
1
S
2
09APR05
09APRO5
DFELIE
li
I Loc 3 Camera plumbiig
07:OQPM
07:59PM
I Loc 2 install new plu
DR1200
Loc 2 install new plumbing
6
6
S
0
09APR05
10APR05
DFEUE
07:OOPM
12:59AM
j
Ibing
I Loc 4 Muck out excavation
DR1750
Loc 4 Muck out excavation
2
2
S
0
09APR05
08:00PM
09APR05
09:59PM
DFEUE
DR1210
Loc 3 install new plumbing
3
3
S
2
09APRO5
09APR05
DFEUE
I Loc 3 install new plumbing
08:OOPM
10:59PM
I Loc 4 Camera plumbing
DR1760
Loc 4 Camera plumbing
1
1
S
0
09APR05
09APR05
DFEUE
10:OOPM
10:59PM
{I
DR1770
Loc 4 Install new plumbing
2
2
S
0
09APRO5
10APR05
DFEIJE
I Loc 4 Install new plumbing
11:OOPM
12:59AM
I
I Loc 3 backfill and tamp
DR1240
Loc 3 backfill and tamp
3
3
S
2
09APRO5
11:OOPM
1OAPRO5
01:59AM
DFEUE
DR1230
Loc 2 Backfill and tamp
3
3
S
0
10APR05
01:OOAM
10APR05
03:59AM
DI-EUE
I Loc 2 Backfill and tamp
I Loc 4 Backfill and tam
I Loc 3 Install Vapor barrier
€
and dowels
DR1780
Loc 4 Backfdl and tamp
3
3
S
0
10APR05
01:OOAM
10APRO5
03:59AM
DFELE
DR1270
Loc 3 Install Vapor barrier and dowels
3
3
S
2
10APRO5
1OAPRO5
DFEIJE
02:OOAM
04:59AM
DR1260
Loc 2 Install Vapor barrier and dowels
3
3
S
0
10APR05
10APRO5
DFELIE
I Loc 2 Install Vapor barrier and dowels
04:OOAM
06:59AM
I Loc 4 Install Vapor b mer and dowels
DR1790
Loc 4 Install Vapor barrier and dowels
3
3
S
0
10APR05
10APRO5
DFELJE
04:0OAM
06:59AM
Project Contingency)
DR1279
Project Contingency
30
30
S
0
10APR05
11APR05
DFELJE
0T00AM
12:59PM
1.
I Pour sub -slab concrete all locations
DR1280
Pour sub -slab concrete all bmtions
4
4
5
Q
11APR05
11APRO5
DFELJE
01:00PM
04:59PM
Sheet 5 of 10

Activity Activity
Orig
Rem
I Cal
T.W
Start
I Finish
CNTR
RESP
APR b
ID Description
Dur
Dur
ID
Float
•W. c.-
DR1290 Install insulation all locations
2
2
S
2
11APR05
11APR05
DI-EUE
I Install insulation all locations j
05:OOPM
06:59PM
DR1340
Concrete cure time for sub -slab
4
4
S
2
11APRO5
11APR05
DFEUE
I Concrete cure time for sub -slab
07:OOPM
10:59PM
I Loc 4 dowels and rebar
I Loc t dowels, rebar and trench drain prep
DR1800
Loc 4 dowels and rebar
4
4
S
4
11APR05
11:00PM
12APRO5
02:59AM
DFBUE
DR1300
Loc 1 dowels, rebar and trench drain prep
6
6
S
2
11APR05
12APR05
DFELE
11:00PM
04:59AM
I Loc 2 dowels, rebar, and trench drain prep
DR1310
Lac 2 dowels, rebar, and trench drain prep
6
6
S
2
11APRO5
12APR05
Df EUE
11:OOPM
O4:59AM
I Loc 3 dowels, rebar, and trench drain prep
DR1320
Loc 3 dowels, rebar, and trench drain prep
6
6
S
2
11APR05
12APR05
DFELE
11:OOPM
04:59AM
DR1330
Pour top slab all locations
4
4
5
0
12APR05
12APR05
DI-ELIE
i
I Pour top slab all locations
07:OOAM
10:59AM
IN Cure time for top slab 1
DR1350
Cure time for top slab
36
36
S
0
12APR05
13APR05
DFiEUE
11:OOAM
M59PM
I
I Prep for epoxy flooring all locations
DR1360
Prep for epoxy flooring all locations
2
2
S
0
13APR05
14APR05
STO
DHEUE
11:OOPM
12:59AM
1 Installation of StoncladUT
I Cure time for Stonclad UT j
DR1370
Installation of StondadUT
2
2
S
0
14APR05
01:OOAM
14APR05
02:59AM
STO
DFEUE
DR1380
Cure time for Stondad UT
10
10
S
0
14APRO5
14APR05
STO
D-EUE
03:OOAM
12:59PM
I
DR1390
Prime and Crack treat perimeter
3
3
S
0
14APRO5
14APR05
STO
DFIEUE
I Prime and Crack
treat perimeter
1
01:OOPM
03:59PM
9 Cure for crack treatment
I Finish coat ill
€
DR1400
Cure for crack treah-ent
15
15
S
0
14APR05
04:OOPM
15APR05
O6:59AM
STO
DI EIIE
DR1410
Finish coat flooring
1
1
S
0
15APRO5
15APR05
STO
DHaJE
07:OOAM
07Z9AM
0 Final flooring cure
time
DR1420 Final flooring cure time 15 15 S 0 15APR05 15APR05 STO DFELE
08:OOAM 10:59PM
€
M02--Tloor RepairsITBOI)
SD-SHUTD(71AIfY
.k
i
FL3014 Repair/Rework Floor Rm 3014 120 120 S 48 08APR05 13APRO5 STO DF IIE
Repair/Rework Floor
Rm 3014
0370OPM 02:59PM
FL0347 Topcoat Floor Rm 347 72 72 S 96 OSAPROS 11APR05 STO DFEUE
Topcoat Floor Rm 347
03:OOPM 02:5913M
Sheet 6 of 10

[. Activity Aedvity
Orig
Rem
Cal
I
Total
Start
Finish
CNTR
RESP
ID Description
Dur
Dur
ID
Float
SD - SHUTDQVNV
j
M,
FR3015 Repair/Replace FRP Cuing Rm 3015
48
48
S
120
08APR05
1OAPR05
E3 Repair/Replace FRP Ceiling
Rm 3015
03:00PM
1 02:59PM
ID-EUE
M04 - High Speed Curtain Replacement
SD - S 4A DO1MV
L.
CT3030 Replace High Speed Door Curtain Rm 3030
24
24
S
128
08APR05
09APR05
DHEUE
3 Replace High Speed Door
Curtain Rm 3030
1
07:OOAM
I 06:59AM
CT3030A Replace High Speed Door Curtain Rm
24
24
S
128
09APR05
10APR05
DHEtJE
❑ Replace High Speed Door
Curtain Rm 3030A
3030A
1
07:00AM
I 06:59AM
M05 Monorail•
j
i
SD - SFUTIX 1Tf
i
MR3014 Certify Beam Monorails Rm 3014
9
9
D
611
08APR05
08APR05
MAC
I Certify Beam Monorails
Rm 3014
1
1
10:0OAM
I 0&59PM
I
I
MR0348 Certify Beam Monorails Rm 348
12
12
D
44
11APR05
11APR05
MAC
JMCLE1
0 Certify Beam Monorails
Rm 348
1
07:0OAM
I 0659PM
I
MR0350
Certify Beam Monorails Rm 350
12
12
D
44
11APR05
11APR05
MAC
JMCf_E
0 Certify Beam Monorails Rm 350
07:00AM`
O6:59PM
;
U01 CentrifuAea
i
PR. PRESFNTDO411i1�
E
sue Insulation Purchase Order li
VR1010
Issue Insulation Purchase Order
40
40
1
23
29MAR05
06APRO5
BAY RGOTT
1
08:00AMA
03:59PM
Procure
Valve Replacement Resources f
VRIO30
Procure Valve Replacement Resources
4D
40
1
32
29MAR05
06APR05
BAY
RGOTf
08:OOAMA
03:59PM
l Pre -shutdown
All V
if
Insulation Investigation
Ive Parts Received Onsite
VR1050
Pre -shutdown Insulation Investigation
4
4
1
36
01APR05
08:0DAM`
01APR05
11:59AM
HAL
RGOTT
VR1020
All Valve Parts Received Onsite
0
0
1
60
01APR05
BAY
RGOTT
11:59AM`
wicki
g Compound Received Onsite
VR1040
Wicking Compound Received Onsite
0
0
1
68
01APRO5
BAY
RGOTT
11:59AM"
SD - SI UTDOVIAV
i
Evacuate R-22 System
I
j
_
VR1000 Evacuate R 22 System 12 S 80 07APR05 OIAPR05 BAY RGOTT
1
j
1
07:O0PM
I
06-.59AM
I
I
Sheet 7 of 10

Activity
Activity
Orig
Rem
Cal
Total
I Start
Finish
CNTR
RESP
wR
ITIKI
ID
Description
Our
Our
1D
Float
111122 ...
JAi i i i 1 141 -1127..r.. 2 ..... 12 ....
VRC010
Remove Valve Body Insulation - Bank C
12
12
S
80
09APRO5
09APRO5
HAL
RGOTT
I Remove valve Body insulation - Bank C
07:OOAM
06:59PM
❑ Remove/Replace Valve Bodies - Bank C '
VRCO20
Remove/Re*ce Valve Bodies - Bank C
24
24
S
80
09APRO5
10APR05
BAY
RGOTI-
07:00PM
06:59PM
I Pressure Test - Bank C
VRCO30
Pressure Test - Bank C
4
4
S
80
10APR05
10APR05
BAY
RGOTT
07:OOPM
10:59PM
D Repair Any Leaks (Wicking) - Bank C
VRC04O
RepairArry Leaks (Wicking) - Bank C
12
12
S
80
10APRO5
11APRO5
BAY
RGOTT
11:00PM
10:59AM
0 Re -Insulate Valve Bodies - Bank C
VRC050
Re -Insulate Valve Bodies - Bank C
12
12
S
80
11APRO5
11APR05
HAL
RGOTT
11:OOAM
10:59PM
VRC060
Vacuum Check - Bank G
4
4
S
80
11APRO5
12APRO5
BAY
RGOTT
1 Vacuum Check - Bank C €
11:00PM
02:59AM
I Refill R-22 - Bank C
VRC070
Refill R-22 - Bank C
4
4
S
80
12APR05
12APRO5
BAY
RGOTT
03:OOAM
06:59AM
i
i .I.
n
E
VRA010
Remove Valve Body Insulation - Bank A
12
12
S
80
08APR05
08APRO5
HAL
RGOTT
I Remove Valve Body insulation - Bank A
07:OOAM
06:59PM
0 Remove Valve Body Insulation - Bank B
VRB010
Remove Valve Body Insulation - Bank B
12
12
S
80
08APRO5
09APR05
HAL
RGOTT
07:QOPM
06:59AM
❑ RemovelReplace Valve Bodies - Bank A
VRA020
RemovetReplace Valve Bodies - Bank A
24
24
S
104
08APRO5
09APR05
BAY
RGOTT
OTOOPM
06:59PM
❑ RemovelReplace Valve Bodies - Bank B
VRB020
Remove/Replaoe Valve Bodies - Bank B
24
24
S
92
09APR05
10APR05
BAY
RGOTT
07:OOAM
06:59AM
I Pressure Test - Bank A
VRA030
Pressure Test - Bank A
4
4
S
104
09APR05
07:OOPM
09APR05
M59PM
BAY
RGOTT
I
VRA040
Repair Any Leaks (Mcking) - Bank A
12
12
S
104
09APRO5
10APRO5
BAY
RGOTT
0 Repair Any Leaks (Wicking) - Bank A
11:00PM
10:59AM
I Pressure Test - Bank
VRB030
Pressure Test - Bank B
4
4
S
92
10APR05
10APRO5
BAY
RGOTT
07:OOAM
M59AM
I
G Re -Insulate Valve Bodies - Bank A
VRA050
Re -Insulate Valve Bodies - Bank A
12
12
S
104
10APRO5
10APR05
HAL
RGOTT
11:00AM
10:59PM
0 Repair Any Leaks (Wck€ng) - Bank B
VRB040
Repair Any Leaks (VVicking) - Bank B
12
12
S
92
10APR05
10APRO5
BAY
RGOTT
11:00AM
10:59PM
I Vacuum Check - Bank A
VRA060
Vacuum Check- Bank A
4
4
S
104
10APR05
11APRO5
BAY
RGOTT
11:OOPM
02:59AM
i
VRB050
Re -Insulate Valve Bodies - Bank B
12
12
S
92
10APRO5
11APRO5
HAL
RGOTT
0 Re -Insulate Valve Bodies
- Bank B
11:00PM
10:59AM
I Refill R-22 - Bank A
VRA070
Refill R-22 - Bank A
4
4
S
104
11APR05
11APRO5
BAY
RGOTT
03:00AM
06:59AM
I Vacuum Check - Bank
'
B
VRB060
Vacuum Check - Bank B
4
4
S
92
11APR05
11APRO5
BAY
RGOTT
11:00AM
Q2:59PM
I Refill R-22 - Bank B
VRB070
Refill R-22 - Bank B
4
4
S
92
11APRO5
11APRO5
BAY
RGOTT
0100PM
06:59PM
Sheet 8 of 10

Activity Activity
Orig
Rem
Cal
Total
Start
Finish
j CNTR
RESP
ID Description
Dur
Dur
ld
Float
I2 - Iceplug Inspections
SD SD-SHUTDOVIN
3
i
IP1000 Fire Supression System Iceplug Inspections
6
6
S
170
08APR05
08APR05
BAY
BKUNT
Fire Supression System Iceplug Inspections
1
0TOOAM I
12:59PM
1Ethanol
sD - % rpom
ET1000
LOTTO Fractionation Ethanol/Crude System
4
4
S
0
08APR05
08APR05
BAY
LOTTO Fractionation EthanollCrude System
02:OOAM
05:59AM
EthanollCrude System Protected
ET1010
EthanoVCrude System Protected 0 0 S 0 OSAPR05 BAY
05:59AM
I Remove Lo1T0 Fractionation Ethanol/Crude Sys,
ET1020
Remove LOTTO Fractionation Ethanol/Crude 4 4 S 78 17APR05 17APRD5 BAY
System
11:OOAM
02:59PM
'
I
O Ethanol System Back Up
ET1030
Ethanol System Bads Up 0 0 S 78 17APRO5 BAY
02:59PM
j
I
1 f
System Maintenance.
sD-SFU7DOm
RO1010
RO System Down
0
0
S
160
08APR05
SAY
TTEZA4
RO System Down
06:59AM
RO System Maintenance
RO1020
RO System Maintenance 24
24 S 160
08APRO5 09APR05 BAY
TTEZA0
OTOOAM
06:59AM
RO System Back Up
RO1030
RO Systern Bads Up 0
0 S 160
09APRO5 BAY
TTEZA
06:59AM
SD - SFPJn]OVIM
--
i
r
EM3042
Construction Clean 1 Room 3013
8
8
5
0
15APR05
15APRO5
GL8
lc- Clean 1 Room 3013
1
03:001PM
10:59PM
JU-EUE
EM3014 Construction Clean I Room 3014
8
8
S
0
15APR05
15APR05
GLB
DHEUE
i
I Construction Clean !Room 3014
03:OOPM
10:59PM
I
EM3015 Construction Clean 1 Room 3015
8
8
S
0
15APR05
15APRO5
GLB
DHELE
I Construction C loan i Room 3015
1
03:001PM
10:59PM
EM3016
Construction Clean / Room 3016
8
8
S
0
15APR05
15APR05
GLB
1hIEL1E
I Construction Clean I Room 3016
I
I
03:0OPM
10:59PM
Sheet 9 of 10

Activity
Activity
Orig
I Rem
Cal
Total
I Start
Finish
CNTR
RESP
MIT
—
ID
Description
Our
Our
ID
Float
+cr W.
-
EMW30
Construction Clean 1 Room 3030
B
8
S
O
15APR05
15APR05
GLB
DI EL1E
I Construction Clean !Room 3030
-
03:OOPM
10:59PM
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Sheet 10 of 10

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
August 23, 2002
KAREN COOK
13AYER CORPORATION
PO BOX 507
CLAYTON. NC 27520
Subject: NPDES Stormwater Permit Renewal
Bayer Corporation
COC Number NCG060039
Johnston County
Dear Permittee:
In response to your renewal application for continued coverage under general permit NCG060000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215. I and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983.
The following information is included with your permit package:
A new Certificate of Coverage
A copy of General Stormwater Permit NCG060000
A copy of a 'Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or
decree.
If you have any questions regarding this permit package please contact Aisha Lau of the Central Office Stormwater
and General Permits Unit at [phone], ext. 578
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Stormwater & General Permits Unit Files
Raleigh Regional Office
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone]
e�M
NCDENR
Customer Service
1- 800-623-7748

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE No. NCG060039
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215. I, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
BAYER CORPORATION
is hereby authorized to discharge stormwater front a facility located at
BAYER CORPORATION
8368 HWY 70 WEST
CLAYTON
JOHNSTON COUNTY
to receiving waters designated as a Uf to the Neuse River, a class C NSW stream, in the Neuse River Basin in
accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, 1I, III,
IV, V, and VI of General Permit No. NCG060000 as attached.
`Phis certificate of coverage shall become effective September I, 2002.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day August 23, 2002.
for Alan W. Klimek, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Gregory J. Thorpe, Ph.D,
Acting Director
Division of Water Quality
Dcccmhcr 27, 2001
KART N COOK
BAYER CORPORATION
P O BOX 507
CLAYTON. NC 27520
Subject: NPDES Storrnwater Permit Renewal
BAY13R CORPORATION
COC Number NCC;060039
Johnston Cotntly
Dear Pcrnittce:
Your facility is currently C0VC1-Cd for stormwaler clisch,ll-gC under General Permit NCG060000, This permit expires
On August 3I. 2002. The Division staff is cun-cntly in the process of rewriting this permit and is scheduled to ItavC
the permit reissued by IatC suntnrCr of2002. Once the hcrnrit is reissued, your facilily would be eligible Misr
Continued covera"C under the rcissuccl hcrrnit.
hi order tO assure your continued CovcragC under the general hcrrnit, you MUM apply to 111C Division of Water
Quality (DWQ) for rcncwal OI' your permit coverage. To make this renewal process easier, we are informing you in
advance that yOur permit will he expiring. Enclosed you will find a General Permit Coverage Renewal
Application Form. The application must be completed and wturned by March 4. 2002 in Order to assurC continued
covcra"C under the gCncrul hcrnlil.
Failure Ur rcyucst rcncwal within this tirnC I7criod may result in a civil assessment of at least $250.00, Larger
perraltcs may he assessed depending On the delinquency of the rcyucst. Discharge of storrmwalcr 1'1-0111 your facility
without COvcragC under a valid storrnwater NII)ES permit would constitute a violation of NCGS 143-215.1 and
Could result in assessments Of civil pena111CS of up [o $10,000 per day.
Please note Ihal reccnl fcdcr:tl ICgislaliun hays cxtcncicd the "ncs CxposurC exclusion" 10 all nper,rtorS 01- industrial
facilitiCs in auly of the I I CattCgories of "storm water discharges aSsociartcd with industrial activity." (except
construction activities). II you feel your facility can certify a Condition 01' "ncs Cxhosure", i.e. the facilty indusu•ial
1ma1CrialS and operations a1-C not exposed tO stormwaler. you can apply for the no exposure exclusion. Fur additional
information contact the Central Office Stormwaler Stuff ntenthcr listed below or check the Stormwaler S, General
Permits Unit Web Site al hltpalh2O.cnr.suite.nc.us/suls[csrnnvalCr.Ittnl
11' the suhjcct StUrnlwaalCI' discharge In walcrs of Ille s1,11C has hccn lerminatcd, 111CLISC ConlhlCtc 111c enclosed
Rescission Request Form, M;iiling instructions are listed on the holtom of the form. You will he notified when the
rescission process has been completed.
1f you have array qucs[inns rCgarding the perrnit r'Crtewal procedures please contact Joe Alhiston cs1 ilic Raleigh
Regional Of licc at 919-571-4700 Or Aisha Lau Of the Central Othee Storntwaler knit at [phone], ext. 578
Sincerely,
Bradley licrincti, Supervisor
StOrnlwatCr and General P121-1161S Unit
CC: Central Files
161ci,11 Re-ioulal 01" icu
NCDENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
DEBORAH H. BARBOUR
BAYER CORPORATION
P0BOX 507
CLAYTON, NC 27520
LTX.;WA
IqT 0 W
_ 4�1�A
[�EHNF1
September 11, 1997
Subject: Reissued Stormwater General Permit for Certificate of Coverage No. NCG060039
Johnston County
Dear Permittee:
In response to your renewal application for continued coverage under the subject permit, the Division
of Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit
is reissued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection agency
dated December 6, 1983.
The following information is included with your permit package:
■ A copy of the stormwater general permit.
. A Stormwater Pollution Prevention Plan Certification Form. This form certifies that you have
developed and implemented the Stormwater Pollution Prevention Plan (SPPP) required in your
permit. This form must be completed and returned to the Division within 30 days of receipt of
this letter. DO NOT send the SPPP with the signed form.
■ Five copies of Analytical Monitoring forms.
■ Five copies of Qualitative Monitoring forms.
in A copy of a Technical Bulletin on the stormwater program with outlines program components
and addresses frequently asked questions.
■ A corrected Certificate of Coverage if you indicated a name or address change on the Renewal
Form returned to the Division.
Your certificate of coverage is not transferable except after notice to DWQ. The Division of Water
Quality may require modification or revocation and reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by
DWQ or permits required by the Division of Land Resources, Division of Air Quality, Coastal Area
Management Act or any other Federal or Local governmental permits that may be required.
If you have any questions concerning this permit or other attached documents, please contact the
Stormwater Group at telephone number [phone]
Sincerely,
fp A. Preston 9Howard, Jr., P. E.
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50%a recycled/ 10% post -consumer paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE NO. NCG060039
STORMWATER DISCHARGES
In compliance with the provision of North Carolina General Statute 143-215,1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and
the Federal Water Pollution Control Act, as amended,
BAYER CORPORATION
is herby authorized to discharge stormwater from a facility located at:
8368 HIGHWAY 70 WEST
CLAYTON,NC
JOHNSTON COUNTY
to receiving waters designated as in the River Basin
in accordance with the effluent limitations, monitoring requirements and other conditions set forth in Pans I,
11, 111 and IV of General Permit No. NCG060000 as attached.
This Certificate of Coverage shall become effective September 15, 1997
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day October 10,1997
for A. Preston Howard, Jr., P.E., Director
Division of Water Quality
By Authorization of the Environmental Management Commission

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
January 22, 1997
Mr, Jayme Clark
Bayer Corporation
8368 US 70 West
Clayton, NC 27540
soda
D FE M F 1
Subject: Stormwater Sampling Requirements
NPDES Stormwater Permits
Dear Mr. Clark:
As per our phone conversation earlier today, the Division is responding to your request for
confirmation on the sole use of grab samples for stormwater permit monitoring. As discussed in our
phone conversation, the Stormwater Group decided in 1995 that the use of "grab" samples was sufficient
for analytical stormwater monitoring for all NPDES stormwater permits including those that originally
required composite stormwater sampling.
In addition, you were made aware that we have discontinued the monitoring window of April
through November and are allowing stormwater monitoring all twelve months of the year. However, I
failed to mention that we have adjusted our definition of a "representative storm event". A copy of the
revised definition is enclosed with this confirmation.
If you have any further questions regarding the contents of this letter, please feel free to contact nie
at 919/ 733-5083, extension 545,
Sincerely,
(f
Steve Ulmer
Engineer, NPDES Stormwater Group
enclosure
cc: Permits and Engineering file, NCG060039
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equai Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

State of North Carolina
Department of Environment, Health and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27604
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
April 30, 1993
B. R. Morris
Miles, Inc.
500 Grant Street
Pittsburg, PA 15219
A. Preston Howard, Jr., P. E.
Director
Subject: General Permit No. NCGO60000
Miles, Inc.
COC NCGO60039
Johnston County
Dear, Mr. Morris:
In accordance with your application for discharge permit received on September 30, 1992, we are
forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general
permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated
December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division
of Environmental Management. The Division of Environmental Management may require modification or
revocation and reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other. permits which may be required by the
Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area
Management Act or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Mr. Steve Ulmer at telephone number 919/733-
5083.
cc
Sincerely,
Original Signed By
Coleen H. Sullins
A. Preston Howard, Jr., P.E.
Raleigh Regional Office
Pollution Prevention Pays
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
STORMWATER DISCHARGES
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution, Control Act, as amended,
Miles, Inc.
is hereby authorized to discharge stormwater from a facility located at
Miles, Inc.
US Hwy 70 East, two miles east of Clayton
Clayton
Johnston County
to receiving waters designated as an unnamed tributary to the Neuse River in the Neuse River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, I1, I1I
and IV of General Permit No. NCGO60000 as attached.
This Certificate of Coverage shall become effective April 30,1993,
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day April 30, 1993.
original Signed By
Coleen H. Sullins
A. Preston Howard, Jr., P.E., Director
Division of Environmental Management
By Authority of the Environmental Management Commission

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EXMIRATION DATE -D 8- 31- q -1

The ClEayton News -stair
Page 7A '
Wednesday, June 8, 2011
Broken pipe causes
leakat Talecris
i that while the board "
"
a continues to -disagree'
-.OnMay31TalecrisBiotherapeutics
t. 8 ntling, the, time and
discovered a broken drain line leading
;d in a protracted legal "
from -its plant in on U.S. 70 Business
further appeal not worth
' io the Johnston County wastewater.
troatinent facility.
ial analysis, the -board's :.
The broken pips: released an esti-.
unitment is to the educa- .
mated 20,000 gallons of water cop-
idents," said. board chair-
taining dissolved minerals from 'the.*
trickland. "A's it, puts the
reverse osmosis water purification
:ion behind it,'the,board
process into an' unnamed tHbrttary in "
Mention to what matters
the Neuse River Basin. The'leak has
ling:quality. educational
been repaired, and the company has
for all the children .of .
notified the .North Carolina Division
unty.."
of Water Quality.
Dr. Ed Croom,.iri sup-
Samples of'water•-downs tream
;cision to end the appeal,
from "the" discharge were. collected,;.,.
ement, " I am confident
and` tested after the discharge, and "
d has '(eached:a resolu-
the -resulting report. determined that.;
the best interest of our-
no fish were killed as a result of the
,aging in'a lengthy and .
discharge.:"
it would have directed
North Carolina law requires that "
! funding'away from our
municipalities, industries and others
)nce again; our board of
that operate wastewater collection
demonstiratedcommit-
or treatment" systems issue public
iudents'and the citizens
notices in the event of a wastewater"
;ounty."
discharge."
theipeAl portion of the
-the -'Sea trail.
reported that the town
received a. $300,,000
;;North Carolina Parks
in Trust fund that will
December purchase of
tdton the -south side of:
,er that will d'eveloped
aewest park. The town
under $2 million for
public hearing_6n the
Jacob - s
J Wm `n� Fun
. � is. open for
.
;ap f,
busir�ess!
11 a ,j7pm
4
%'s Ju `�' , `4 M dAS-u nl- 4.
Wed: '$6' e Thur..$6 0 .'Fri. $6 .';.; Sa_ t.-$6
7 Son-SkcW Includes freefounthin d,ririks, free popcorn '
and free hotdogs, $8 :to include frozen drinks.
Now booking birthday Parties' up to .
20 children for '$149
Includes coke, pinata, soft drinks or Juice, ,paper goods in.'the
birthday'bash,room for one hour, plus unlimited.jump'n' Fun.'
birthday child receives Jump n' Fun tee shirt! .
10 -children or less only $89 includes dl! of ,above! ,
Now"acceptirlg Friday: and 'Saturdav nightdrop off Daycare
$8.00 per hour from `6PM: to 11 PM '

I F±=F NR
AIANUFACTUR ING
UTIL./MAINT./TANK F.AP"
ADMIPJ15TRATION
WAREHOUSE
ENV IRMWENTAL
OA
PARKING ,? ROADS
UTILITIES EASEMENT
DRAIN DISPOSAL GUIDELINES STORMWATER GUIDELINES
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