NCG030436_COMPLETE FILE - HISTORICAL_20140225 (FIX)

PERMIT
DOC TYP
DOC DAl
STORMWATER DIVISION Cl
NCG PERMITS
HISTORICAL FILE
MONITORING RE
YYYYMMDD

Parnell, David
From: Georgoulias, Bethany
Sent: Tuesday, February 25, 2014 10:17 AM
To: Parnell, David; Holley, John; Jones, Gabi; Dupree, Joe; Valentine, Thad; Pageau, Karyn;
Rodgers, Ashley
Cc: Bennett, Bradley; Pickle, Ken
Subject: RE: Accu Fab Inc Inspection
Hi Dave,
I'll plan to go. I'll meet you at RRO.
Thanks,
Bg
Bethany Georgoulias, Environmental Engineer
NCDENR 1 Division of Energy, Mineral, and Land Resources
Storrnwater Permitting Program
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N. Salisbury Street, Raleigh, NC 27604
919 / 807-6372 (phone); 919 / 807-6494 (fax)
Website: h!ip:Hportal.ncdenr.org/web/Ir/stormwater
E-mail correspondence to andfrom this address may be suhjeci to the North Carolina Public Records tan, and may be disclosed to third parties.
From: Parnell, David
Sent: Monday, February 24, 2014 4:27 PM
To: Georgoulias, Bethany; Holley, John; Jones, Gabi; Dupree, Joe; Valentine, Thad; Pageau, Karyn; Rodgers, Ashley
Subject: Accu Fab Inc Inspection
I will be conducting a Compliance Evaluation Inspection at the above facility on Thursday February 27 at
10AM. It is located at 801 Beacon Lake Drive, Raleigh. Those who would like to accompany me can meet me
in the RRO Lobby at 9:40AM or meet me at the site at 10AM. The facility has landed on Tier 2 due to
exceedences of Zinc in their stormwater. They have attempted to isolate the source of the Zinc and would like
for me/us to see their site.
Let me know if you'd like to attend.
Dave Parnell
Environmental Senior Specialist
North Carolina Department of Environment & Natural Resources
Division of Energy, Minerals, and Land Resources
Raleigh Regional Office
3800 Barrett Drive
Raleigh, NC 27609
0: [phone]
F: [phone]
E-mail correspondence to and from this address maybe subject to,the North Carolina Public Records Law
and maybe disclosed to third parties.

Parnell, David
From: Sonya Walsh [[e-mail]
Sent: Tuesday, February 18, 2014 7:15 AM
To: Parnell, David
Subject: RE: RE:
Good Morning,
I am mailing in a "No Flow" forthe month of January. We had some rain but it did not produce enough flow to pull
samples. I did send in all the analytical reports for periods January 2013 thru June 2013 and July 2013 thru December
2013. i also sent in copies of the roof sampling results and a. map of the building that shows the approximate area on the
roof in which we pulled the samples. I am hoping to get another zinc sampling from the outfalls this month.
Thank you,
Sonya Walsh
Environmental Safety and Health Manager
From: Parnell, David[mailto:[e-mail]]
Sent: Monday, February 17, 2014 4:50 PM
To: Sonya Walsh
Subject: RE:
Sonya,
Mailing of monitoring report should go to your usual mailing address. Send in the usual stormwater report, but put "no
flow" or "0 Flow". I am reviewing your roof situation with the permitters this week — I do not have your file handy, but
if you have received your January results and not sent them to me, please do so. I will check the files later to see what I
have received.
Thanks,
Dave Parnell
From: Sonya Walsh [mailto:SWalsh(&accufabnc.com]
Sent: Monday, February 17, 2014 3:29 PM
To: Parnell, David
Subject:
Good Afternoon,
I am mailing in the "No Flow" report for the month of January. I know that I send two copies to the Division of Water
Quality. Is there anyone else that should receive a copy?
FYI: I also would like to say that I appreciate your time and assistance with this issue. You are a pleasure to work with.
Thank you,
Sonya Walsh

6�G�LL611fCB��
ACCU—FAB„ INC.
Go
am
,0 ' �� • 801 BEACON LAKE DR. • RALEIGH. NC 27610-1377
919.212.6400 • FAX [phone]
�e�CT A1A11101•p��O@ SalesQAceuFabNC.Com '" RFQAMCCuFabNC.com
urww.Acc uFa bN C.cam
- o
January 21,2014
Attn: John Holley
Regional Engineer
Division of Energy, Minerals and Land Resources
1628 Mail Service Center
Raleigh, NC 27699-1628
Dear John Holley,
Enclosed you will find copies of the Semi-annual Stormwater Discharge Monitoring Reports, Analytical Results, and the
Chain of Custody for the periods of January 2013 thru June 2013 and July of 2013 thru December of 2013. 1 have also
enclosed the roof top analytical results along with a map of our building showing the approximate locations where the zinc=
samples were taken and the outfall locations.
The analytical results revealed that outfall #2 has exceeded the permitted benchmark value for the zinc total, recoverable for
both of the periods stated. Since activating tier one in April 2013, we took analytical sampling from the roof at different
intervals and we have found that Accu-Fab's roof is the source that is causing the exceeded benchmark on the zinc total,
recoverable. Accu-Fab completed an addition to the existing building approximately six years ago. The new roof is made of
galvalume which is an aluminum zinc alloy. With this statement, outfall #2 catches most the runoff from the new part of the
building and outfall #1 catches the runoff from the older building which in my opinion is why outfall #1 is not beyond the
permitted benchmark. I do believe that the zinc is traveling to the older roof and outfall#1 may eventually exceed the
permitted benchmark. Due to 2013 being the first year that we have had a benchmark for zinc total, recoverable, I do not
have any past analytical results to compare these with. I feel strongly that the exceeded benchmark is not caused by Accu-
Fab's manufacturing process and is indeed beyond our best management practices. I feel that there may he other roofs with
the same issue. I feel certain that all buildings with this type of roof are not performing analytical reporting on storm water
due to the nature of their business therefore; it may an unrecognizable issue at this time. 1 have also mailed this same letter
and packet to Bradley Bennett, Supervisor of the Stormwater Permitting Unit.
Please review our paperwork and advise me as to what Accu-Fab can do to resume full compliance.
This is in reference to General Permit Number NCG 030000, which became effective on November 1, 2012.
If you have any questions, please notify me.
Thank you,
Sonya Walsh
Environmental Safety and Health Manager
swalshnaccufab nc.com
Office: 919-212-6400 x155
Fax: [phone]
Cell: 919-215-3244
An ISO 9001:2000 Registered Company

r p
Parnell, David
From: Sonya Walsh [[e-mail]] — Q�
Sent: Tuesday, January 14, 2014 1017 AM
To: Parnell, David
Subject: Storm water results
Good Morning,
left you a voice mail.this morning letting you know that our analytical results are in. Outfall #2 is still reading high on
the zinc total @ .60mg/I and our benchmark is .067 mg/I. All of the other analytical results are within the benchmark
values including the zinc total in outfall #1 which is reading .046 mg/l. Please give me a call as soon as you can.
Thank you,
Sonya Walsh
Environmental Safety and Health Manager
Sonya Walgh
SafatyPlannfag I0�an�8
Accu-Fab, I.r>Id.'
g 1$.21L,B�OO.x1�6
019:212.2333 [ axJ
www.Acclu abNC:corn
�i��ubexCf /*
Sonya Walsh
Safety/Planning Manager f 6
www.accufabnc.com
919-212-6400 x l 55
919-215-3244 Cell
919-212-2333 Fax
A[DCU-IFAB. INC.'
CONTRACT MANUFACTURING I
3

1�;a'ceAnalyfical'
wwwpacelabs.com
January 08, 2014
Ms. Sonya Walsh
ACCU FAB
801 Beacon Lake Dr.
Raleigh, NC 27610
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
RE: Project:otormwater SarnplesD
Pace Project No:: 92185137
Dear Ms. Walsh:
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Nuntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 31, 2013.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNl standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page
[e-mail]
Project Manager
Enclosures
Q pCCREO
Al
•9g�.fp�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
Page 1 of 29

aceAnalytical"
wwwpeaslaDs.cam
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Charlotte Certification [Ds
9800 Kincey Ave. Ste 100, Huntersville, INC 28078
FloridalNELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Cortiflcation IDs
2225 Riverside Dr., Asheville, NC 28804
Flodda/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #; 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirgintaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 29

aceAnalytical"
wwwpacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project:
Stormwater Samples
Pace Project No.:
92185137
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92185137001
Outfall 1
EPA 1664B
CLW
1
PASI-C
EPA 200.7
JMW
3
PASI-A
EPA625
Bpi
58
PASI-C
EPA624
CAM
34
PASI-C
SM 2540D
DAS
1
PASI-A
92185137002
Outfall 2
EPA 1664B
CLW
1
PASI-C
EPA 200.7
JMW
3
PASI-A
EPA625
RES
58
PASI-C
EPA624
CAM
34
PASI-C
SM 2540D
DAS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reprad uced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 29

aceAnalXical `
—pacelabs.oam
Project: Stormwater Samples
Pace Project No.: 92185137
Method: EPA 16648
Description: 1664 SGT-HEM, TPH
Client: ACCU FAB
Date-. January 08,2014
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
General Information:
2 samples were analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below,
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 29

acmnalytical o
wwwpacalabs.own
Project: Stormwater Samples
Pace Project No.: 92185137
Method: EPA 200.7
Description: 200.7 MET ICP
Client: ACCU FAB
Data: January 08, 2014
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
PROJECT NARRATIVE
General Information:
2 Samples were analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed vrithin the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 29

aceAnalytical
www.pacelsbs. cm
Project: Stormwater Samples
Pace Project No.: 92185137
Method: EPA 625
Description: 625 MSSV
Client: ACCU FAB
Date: January 08,2014
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 2728B
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
General Information:
2 samples were analyzed for EPA 625. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H3: Sample was received or analysis requested beyond the recognized method holding time.
• Outfall 1 (Lab 10: 92185137001)
• Outfall 2 (Lab ID: 92185137002)
Sample Preparation:
The samples were prepared in accordance with EPA 625 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 0EXT125412
A matrix spike and/or matrix spike duplicate (MSIMSD) were performed on the following sample(s): 92185017001
Ri: RPD value was outside control limits.
• MSD (Lab ID: 1116360)
• 2,4-Dinitrophenol
• 2-Nitrophenol
• 4,6-Dinitro-2-methylphenol
• 4-Nitrophenol
• Phenol
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytcal Services, Inc.. Page 6 of 29

(�IaceAnalytical"
www pacalam cam
Project: Stormwater Samples
Pace Project No.: 92185137
Method: EPA 625
Description: 625 MSSV
Client: ACCU FAB
Date: January 08, 2014
Additional Comments:
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 2BO78
[phone]
This reporl shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 29

acmnalyfical
www.pacdabs.com
Project: Stormwater Samples
Pace Project No.: 92185137
Method: EPA 624
Description: 624 Volatile Organics
Client: ACCU FAB
Date- January 08, 2014
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 2BB04
[phone] [phone]
PROJECT NARRATIVE
General Information:
2 samples were analyzed for EPA 624. All samples were received in acceptable condition with any exceptions noted below,
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
1-13: Sample was received or analysis requested beyond the recognized method holding time.
• Outfall 1 (Lab 10: 92185137001)
• Outfall 2 (Lab ID: 92185137002)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: MSV125424
L0: Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
• LCS (Lab ID: 1116001)
• Bromomethane
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc- Page 8 of 29

aceAnalytical
wwwpacelabs.carn
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Method: SM 2640D
Description: 2540D Total Suspended Solids
Client: ACCU FAB
Date: January 08. 2014
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
General Information:
2 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
1-13: Sample was received or analysis requested beyond the recognized method holding time.
• Outfall 1 (Lab ID: 92185137001)
• Outfall 2 (Lab ID: 92185137002)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below,
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9600 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 9 of 29

(�IacieAnalytical
www.pacelsbs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater Samples
Pace Project No.: 92185137
Sample: Outtall 1 Lab ID: 92186137001 Collected: 12/10/13 09:25 Received: 12/31/13 09:10 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons
NO mglL
5.0
1
01/06/14 09742
200.7 MET ICP
Analytical Method: EPA 2003 Preparation
Method: EPA
200.7
Capper
NO mglL
0.0050
1
01/04/14 08:55
01/07/14 21:48
7440-50-8
Lead
NO mg1L
0,0050
1
01/04/14 08:55
01/07/14 21 A8
7439-92-1
Zinc
0.046 mg1L
0,010
1
01/04/14 08:55
01/07/14 21:48
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
NO mglL
0.0050
1
01/06/14 09:00
01/07114 14:48
83-32-9
Acenaphthylene
NO mg1L
0,0050
1
01/06/14 09:00
01/07114 14:48
208-96-8
Anthracene
NO mg/L
0.0050
1
01/06/14 09:00
01/07114 14:48
120-12-7
Benzo(a)anthracene
ND mg1L
0,0050
1
01/06114 09:00
01/07114 14:48
56-55-3
Benzo(a)pyrene
ND mglL
0.0050
1
01/06/14 09:00
01/07/14 14:48
50-32-8
Benzo(b)fluoranthene
NO mglL
0,0050
1
01/06/14 09:00
01/07/14 14:48
205-99-2
Benzo(g,h,i)perylene
ND mglL
0.0050
1
01/06/14 09:00
01/07/14 14A8
191-24-2
Benzo(k)fluoranthene
NO mglL
0.0050
1
01/06/14 09:00
01107/14 14:48
207-08-9
4-Bromophenylphenyl ether
NO mg1L
0,0050
1
01/06114 09:00
01/07/14 14:48
101-55-3
Butylbenzylphtha late
NO mg1L
0.0050
1
01/06/14 09:00
01/07/14 14:48
85-68-7
4-Chloro-3-methylphenol
NO mg1L
0,0050
1
01/06/14 09:00
01/07/14 14:48
59-50-7
bis(2-Chloroethoxy)methane
NO mglL
0.010
1
01/06114 09:00
01/07/14 14:48
111-91-1
bis(2-Chloroethyl) ether
NO mglL
0.0050
1
01/06/14 09:00
01107/14 14:48
111-44-4
bis(2-Chloroisopropyl) ether
NO mglL
0.0050
1
01/06/14 09:00
01/07/14 14:48
108-60-1
2-Chloronaphthalene
NO mglL
0,0050
1
01/06/14 09:00
01/07/14 14:48
91-58-7
2-Chlorophenol
NO mglL
0.0050
1
01/06/14 09:00
01/07/14 14:48
95-57-8
4-Chlorophenylphenyl ether
NO mg1L
0.0050
1
01/06/14 09:00
01/07/14 14A8
7005-72-3
Chrysene
NO mglL
0.0050
1
01/06/14 09:00
01/07/14 14A8
218-01-9
Dibenz(a,h)anthracene
NO mglL
0.0050
1
01/06/14 09:00
01/07/14 14:48
53-70-3
3,3'-Dichlorobenzidine
NO mg1L
0.025
1
01/06/14 09:00
01/07/14 14:48
91-94-1
2,4-Dichlorophenol
NO mg1L
0.0050
1
01/06/14 09:00
01/07/14 14:48
120-83-2
Diethylphthalate
NO mg11-
0.0050
1
01/06/14 09:00
01/07/14 14748
84-66-2
2,4-Dimethylphenol
NO mglL
0.010
1
01/06/14 09:00
01/07/14 14A8
105-67-9
Dimethylphthalate
NO mg1L
0,0050
1
01/06/14 09:00
01/07/14 14:48
131-11-3
Di-n-butylphthalate
NO mg1L
0.0050
1
01/06/14 09:00
01/07/14 14:48
84-74-2
4,6-Dinitro-2-methylphenol
NO mg1L
0.020
f
01/06/14 09:00
01/07/14 14:48
534-52-1
2,4-Dinitrophenol
NO mglL
0.050
1
01/06/14 09:00
01/07/14 14A8
51-28-5
2,4-Dinitrotoluene
NO mg1L
0.0050
1
01/06/14 09:00
01/07/14 14A8
121-14-2
2,6-Dinitrotoluene
ND mg1L
0.0050
1
01/06/14 09:00
01/07/14 14:48
606-20-2
Di-n-octylphthalate
NO mglL
0.0050
1
01/06/14 09:00
01/07114 14:48
117-84-0
bis(2-Ethylhexyl)phthalate
ND mg1L
0.0050
1
01/0611409:00
01/07/14 14:48
117-81-7
Fluoranthene
ND mg1L
0.0050
1
01/06/14 09:00
01/07/14 14:48
206-44-0
Fluorene
ND mglL
0.0050
1
01/06/14 09:00
01/07/14 14:48
86-73-7
Hexachloro-1,3-butadiene
ND mglL
0.0050
1
01106/14 09:00
01/07/14 14:48
87-68-3
Hexachlorobenzene
NO mg1L
0,0050
1
01/06/14 09:00
01/07/14 14:48
118-74-1
Hexachlorocyclopentadiene
NO mglL
0.010
1
01/06/14 09:00
01107/14 14A8
77-47-4
Hexachloroethane
NO mg1L
0.0050
1
01/06/14 09:00
01107/14 14A8
67-72-1
1ndeno(1,2,3-cd)pyrene
NO mglL
0,0050
1
0110611409:00
0110711414A8
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2014 04:10 PM without the written consent of Pace Analytical Services, tnc.. Page 10 of 29

leAnalytrcal
IYW W.11aCBf8bA.4�Wft
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside pr,
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater Samples
Pace Project No.: 92185137
Sample: Outfall 1
Lab ID: 92185137001
Collected: 12/10/13 09:25
Received: 12/31/13 09:10 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Quat
625 MSSV
Analytical Method: EPA625
Preparation Method: EPA625
Isophorone
ND mg1L
0.010
1
01/06/14 09:00
01/07/14 14:48
78-59-1
Naphthalene
ND mg/L
0,0050
1
01/06/14 09:00
01/07/14 14:48
91-20-3
Nitrobenzene
ND mg/L
0.0050
1
01/06/14 09:00
01/07/14 14:48
98-95-3
2-Nitrophenol
ND mg/L
0,0050
1
01/06/14 09:00
01/07/14 14:48
88-75-5
4-Nitrophenol
ND mg1L
0.050
1
01106/14 09:00
01/07/14 14:48
100-02-7
N-Nitrosodimethylamine
ND mg/L
0.0050
1
01/06/14 09:00
01/07/14 14:48
62-75.9
N-Nitroso-di-n-propylamine
ND mg/L
0.0050
1
01/06/14 09:00
01/07/14 14:48
621-64-7
N-Nitrosodiphenylamine
ND mg/L
0.010
1
01/06/14 09:00
01/07/14 14:48
86-30-6
Pentachlorophenol
ND mg/L
0.010
1
01/06/14 09:00
01/07/14 14:48
87-86-5
Phenanthrene
NO mg/L
0,0050
1
01/06/14 09:00
01/07/14 14:48
85-01-8
Phenol
ND mg/L
0.0050
1
01/06/14 09:00
01/07/14 14:48
108-95-2
Pyrene
ND mg/L
0.0050
1
01/0611409:00
01/07/14 14:48
129-00-0
1,2,4-Trichlorobenzene
ND mg/L
0.0050
1
01/0611409:00
01/07/14 14:48
120-82-1
2,4,6-Trichlorophenol
ND mg1L
0.010
1
01/06/14 09:00
01/07/14 14:48
88-06-2
Surrogates
Nitrobenzene-d5 (S)
50 %
10-120
1
01/06/14 09:00
01/07/14 14:48
4165-60-0
H3
2-Fluorobiphenyl (S)
50 %
15-120
1
01/06/14 09:00
01/07/14 14:48
321-60-8
Terphenyl-d14 (S)
91 %
11-131
1
01/06/14 09:00
01/07/14 14:48
1718-51-0
Phenol-d6 (S)
19 %
10-120
1
01/06/14 09:00
01/07/14 14:48
13127-88-3
2-Fluorophenol (S)
26 %
10-120
1
01/06/14 09:00
01/07/14 14:48
367-12.4
2,4,6-Tribromophenol (S)
99 %
10-137
1
01/06/14 09:00
01/07/14 14A8
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND mg/1-
0.0020
1
01/03/14 14:57
71-43-2
H3
Bromodichloromethane
ND mg1L
0.0020
1
01/03/14 14:57
75-27-4
H3
Bromoform
ND mg1L
0.0020
1
01/03/14 14:57
75-25-2
H3
Bromomethane
ND mg1L
0.0020
1
01/03/14 14:57
74-83-9
H3,L3
Carbon tetrachloride
ND mg1L
0,0020
1
01/03/14 14:57
56-23-5
H3
Chlorobenzene
ND mg1L
0.0020
1
01/03114 14:57
108-90-7
H3
Chloroethane
ND mg1L
0.0020
1
01/03/14 14:57
75-00-3
H3
Chloroform
ND mg1L
0.0020
1
01/03/1414:57
67-66-3
H3
Chloromethane
ND mg1L
0.0020
1
01/03/14 14:57
74-87-3
H3
Dibromochloromethane
ND mg1L
0.0020
1
01103114 14:57
124-48-1
H3
1,2-Dichlorobenzene
ND mg1L
0.0020
1
01/03/14 14:57
95-50-1
H3
1,3-Dichlorobenzene
ND mg1L
0.0020
1
01/03114 14:57
541-73-1
H3
1,4-Dichlorobenzene
ND mg/L
0.0020
1
01/03/14 14:57
106-46-7
H3
1,1-Dichloroethane
ND mg1L
0.0020
1
01/03/14 14:57
75-34-3
H3
1,2-Dichloroethane
ND mg/L
0.0020
1
01/0311414:57
107-06.2
H3
i,t-Dichloroethene
ND mg/L
0.0020
1
0110311414i57
75-35-4
H3
cis- 1,2-Dichloroethene
ND mg/L
0.0020
1
0110311414:57
156.59-2
H3
trans-1,2-Dichloroethene
ND mg/L
0.0020
1
01/0311414:57
156-60-5
H3
1,2-Dichloropropane
ND mg/L
0.0020
1
01/0311414:57
78-87-5
H3
cis-1,3-Dichloropropene
NO mg/L
0.0020
1
01/03/1414:57
10061-01-5
H3
trans-1,3-Dichloropropene
ND mg/L
0,0020
1
01/03/1414:57
10061-02-6
H3
Ethylbenzene
NO mg1L
0.0020
1
01/03/1414:57
100-41-4
H3
Methylene Chloride
ND mg/L
0,0020
1
01/03/14 14:57
75-09-2
H3
1,1,2,2-Tetrachloroethane
ND mg/L
0.0020
1
01/03/1414:57
79-34-5
H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /08/2014 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 29

(�5a'cmnalytical*
www.paoalabs.ow
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater Samples
Pace Project No.: 92185137
Sample: Outfall 1 Lab ID: 92185137001 Collected: 12/10/13 09:25 Received: 12/31/13 09:10 Matrix: Water
Parameters
624 Volatile Organics
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1, 2-Trich loroeth ane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichioroethane-d4 (S)
2640D Total Suspended Solids
Total Suspended Solids
Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 624
NO mglL
0,0020
1
0110311414:57
127-18-4
H3
NO mg/L
0.0020
1
01/0311414:57
108-88-3
H3
NO mg/L
0,0020
1
0110311414:57
71-55-6
H3
NO mg/L
0.0020
1
0110311414:57
79-00-5
H3
ND mg/L
0,0020
1
0110311414:67
79-01-6
H3
NO mg/L
0.0020
1
01103/1414:57
75-69-4
H3
ND mg/L
0.0020
1
01/03/1414:57
75-01-4
H3
98 %
70-130
1
01/03/1414:57
460-00-4
100 %
70-130
1
01/03/14 14:57
2037-26-5
108 %
70-130
1
01/03/1414:57
17060-07-0
Analytical Method: SM 25401)
6.6 mg1L 5.0 1 01/0311415:02 H3
Sample: Outfall 2 Lab ID: 92185137002 Collected: 12/10/13 09:10 Received: 12/31/13 09:10 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
1664 SGT HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
NO mg/1-
5.0 1
01/06/14 09:43
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA
200.7
Copper
NO mg/L
0.0050 1
01/04/1408:55
01/07/14 21:51
7440-50-8
Lead
NO mg/L
0.0050 1
01/04/14 08:55
01/07/14 21:51
7439-92-1
Zinc
0.60mg1�
0.010 1
01/04/14 08:55
01/07/14 21:51
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
NO mg/L
0.0050 1
01/06/14 09:00
01/07/14 15:20
83-32-9
Acenaphthylene
NO mg/L
0.0050 1
01/06/14 09:00
01/07/14 15:20
208-96-8
Anthracene
NO mg/L
0.0050 1
01106/14 09:00
01/07/14 15:20
120-12-7
Benzo(a)anthrace ne
NO mg/L
0.0050 1
01/06/14 09:00
01/07/14 15:20
56-55.3
Benzo(a)pyrene
NO mg/L.
0.0050 1
01106114 09:00
01/07/14 15:20
50-32-8
Benzo(b)fluoranthene
NO mg/L
0.0050 1
01/06114 09:00
01/07/14 15:20
205-99-2
Benzo(g,h,i)perylene
NO mg/L
0.0050 1
01/06/14 09:00
01107/14 15:20
191-24-2
Senzo(k)fluoranthene
NO mg/L
0.0050 1
01/06/14 09:00
01107/14 15:20
207-08.9
4-Bromophenylphenyt ether
NO mg&
0.0050 1
01/06/14 09:00
01/07/14 15:20
101-55-3
Butylbenzylphthatate
NO mg/L
0.0050 1
01/06/14 09:00
01/07/14 15:20
85-68-7
4-Chloro-3-methylphenol
NO mg/L
0.0050 1
01/06/14 09:00
01/07/14 15:20
59-50-7
bis(2-Chloroethoxy)methane
NO mg/L
0.010 1
01/06/14 09:00
01/07/14 15:20
111-91-1
bis(2-Chloroethyl) ether
NO mg/L
0.0050 1
01/06/14 09:00
01/07/14 15:20
111-44-4
bis(2-Chloroisopropyl) ether
NO mg1L
0.0050 1
01/06/14 09:00
01/07/14 15:20
108-60-1
2-Chloronaphthalene
NO m911-
0.0050 1
01/06/14 09:00
01107/1415:20
91-58-7
2-Chlorophenol
NO mg1L
0,0050 1
01106/1409:00
01/0711415:20
95-57-8
4-Chlorophenylphenylether
NO mg/L
0.0050 1
01/06/14 09:00
01/07/14 15:20
7005-72-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
Date: 01/08/2014 04;10 PM
without the written consent
of Pace Analytical Services, Inc..
Page 12 of 29

aceAnalytical
—pacelabs.com
Project: Stormwater Samples
Pace Project No.: 92185137
Sample: Outfall 2
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, fnc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 92185137002 Collected: 12110113 09:10 Received: 12/31/13 09:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA625 Preparation Method: EPA625
Chrysene
ND mg/L
0,0050
1
01/06/14 09:00 01/07/14 15:20
218-01-9
Dibenz(a,h)anthracene
ND mg/L
0.0050
1
01/06/14 09:00 01107/1415:20
53-70-3
3,3'-Dichlorobenzidine
NO mg/L
0.025
1
01/0611409:00 01/07/14 15:20
91-94-1
2,4-Dichlorophenol
ND mg/L
0.0050
1
01/06/14 09:00 01/07/14 15:20
120-83-2
Diethylphtha late
ND mg/L
0.0050
1
01/06/14 09:00 01/07/14 15:20
84-66-2
2,4-Dimethylphenol
ND mg/L
0.010
1
01/06/14 09:00 01/07/14 15:20
105-67-9
Dimethylphthalate
ND mg/L
0.0050
1
01/06/14 09:00 01/07/14 15:20
131-11-3
Di-n-butylphthalate
ND mg/L
0.0050
1
01/06/14 09:00 01/07/14 15:20
84-74-2
4,6-Dinitro-2-methylphenol
ND mg1L
0.020
1
01/06/14 09:00 01/07/14 15:20
534-52-1
2,4-Dinitrophenol
ND mg/L
0.050
1
01/06/14 09:00 01/07/14 15:20
51-28-5
2,4-Dinitrotoluene
ND mg1L
0.0050
1
01/06/14 09:00 01/07/14 15:20
121-14-2
2,6-Dinitrotoluene
ND mg1L
0.0050
1
01/06/14 09:00 01/07/14 15:20
606-20-2
Di-n-octylphthalate
ND mg/L
0.0050
1
01/06/14 09:00 01/07/14 15:20
117-84-0
bis(2-Ethylhexyl)phihalate
ND mg1L
0.0050
1
01/06/14 09:00 01/07/14 15:20
117-81-7
Fluoranthene
ND mglL
0.0050
1
01/06/14 09:00 01/07/14 15:20
206-44-0
Fluorene
ND mglL
0.0050
1
01/06/14 09:00 01/07/14 15:20
86-73.7
Hexachloro-1,3-butadiene
ND mglL
0.0050
1
01/06/14 09:00 01/07/14 15:20
87-68-3
Hexachlorobenzene
ND mglL
0.0050
1
01/06/14 09:00 01/07/14 15:20
118-74-1
Hexachlorocyclopentadiene
ND mglL
0.010
1
01/06/14 09:00 01/07/14 15:20
77-47-4
Hexachloroethane
ND mg1L
0,0050
1
01106/14 09:00 01/07/14 15:20
67-72-1
Indeno(1,2,3-cd)pyrene
ND mg1L
0.0050
1
01/06/14 09:00 01/07/14 15:20
193-39-5
Isophorone
ND mg1L
0.010
1
01/06/14 09:00 01/07/14 15:20
78-59-1
Naphthalene
ND mg1L
0.0050
1
01/06/14 09:00 01/07/14 15:20
91-20-3
Nitrobenzene
ND mg1L
0.0050
1
01/06/14 09:00 01/07/14 15:20
98-95-3
2-Nitrophenol
ND mg/L
0.0050
1
01/06/14 09:00 01/07/14 15:20
88-75-5
4-Nitrophenol
ND mg/L
0.050
1
01/06/14 09:00 01/07/14 15:20
100-02-7
N-Nitrosodimethylamine
ND mg1L
0.0050
1
0110611409:00 01/07/14 15:20
62-75-9
N-Nitroso-di-n-propylamine
ND mg/L
0,0050
1
01/06/14 09:00 01107/1415:20
621-64-7
N-Nitrosodiphenylamine
ND mg1L
0.010
1
01/0611409:00 01/07/14 15:20
86-30-6
Pentachlorophenol
ND mg/L
0.010
1
01/06/14 09:00 01/07/14 15:20
87-86-5
Phenanthrene
ND mg/L
0.0050
1
01/0611409:00 01/07/14 15:20
85.01-8
Phenol
ND mg/L
0.0050
1
01/06/14 09:00 01/07/14 15:20
108-95-2
Pyrene
ND mg/L
0.0050
1
01/0611409:00 01/0711415:20
129-00-0
1,2,4-Trichlorobenzene
ND mg/L
0.0050
1
01/06/14 09:00 01/07/1415:20
120-82-1
2,4,6-Tdchlorophenol
ND mg/L
0.010
1
01/06/14 09:00 01/0711415:20
88.06-2
Surrogates
Nitrobenzene-d5(S)
50 %
10-120
1
01/0611409:00 01/0711415:20
4165-60-0
2-Fluorobiphenyl(S)
53 %
15-120
1
01/06/14 09:00 01/07/14 15:20
321-60-B
Terphenyl-d14 (S)
97 %
11-131
1
01/06/14 09:00 01/07/14 15:20
1718-51-0
Phenol-d6(S)
19 %
10-120
1
01/0611409:00 01/07/14 15:20
13127-88-3
2-Fluorophenol (S)
30 %
10-120
1
01/06/14 09:00 01/07/14 15:20
367-12-4
2,4,6-Tribromophenol (S)
86 %
10-137
1
01/06/14 09:00 01/07/14 15:20
118-79-6
624 Volatile Organics
Analytical Method: EPA624
Benzene
ND mglL
0.0020
1
01/03/1414:41
71-43-2
Bramodichloromethane
ND mg1L
0.0020
1
01/03/1414:41
75-27-4
Bromoform
ND mg1L
0.0020
1
01/03/1414:41
75-25-2
REPORT OF LABORATORY ANALYSIS
H3
H3
H3
H3
This report shall not be reproduced, except in full,
Date: 01108/2014 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 29

aceAnalytical
wwwpacefabs.com
Project: Stormwaler Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall 2
Parameters
Lab ID: 92185137002
Results Units
Collected: 12/10/13 09:10
Report Limit OF
Received: 12/31/13 09:10 Matrix: Water
Prepared Analyzed CAS No.
Qual
624 Volatile Organics
Analytical Method: EPA624
Bromomethane
NO mg/L
0.0020
1
01/03/14 14:41
74-83.9
H3,L3
Carbon tetrachloride
NO mg1L
0.0020
1
01/03/14 14:41
56-23-5
H3
Chlorobenzene
ND mg1L
0.0020
1
01/03/14 14:41
108-90-7
H3
Chloroethane
NO mg/L
0.0020
1
01/03/14 14:41
75-00-3
H3
Chloroform
ND mglL
0.0020
1
01/03/14 14:41
67-66-3
H3
Chloromethane
NO mglL
0.0020
1
01/03/14 14:41
74-87-3
H3
Dibromochloromethane
NO mglL
0,0020
1
01/03/14 14:41
124-48-1
H3
1,2-Dichlorobenzene
NO mglL
0.0020
1
01/03/14 14:41
95-50-1
H3
1,3-Dichlorobenzene
NO mgfL
0.0020
1
01/03/14 14:41
541-73-1
H3
1,4-Dichlorobenzene
NO mg1L
0,0020
1
0110311414:41
106-46-7
H3
1,1-Dichloroethane
ND mg/L
0,0020
1
0110311414:41
75-34-3
H3
1,2-Dichloroethane
NO mg/L
0.0020
1
01/0311414741
107-06-2
H3
11-Dichloroethene
ND mg/L
0.0020
1
0110311414:41
75-35-4
H3
cis- 1,2-Dichloroethene
ND mg/L
0,0020
1
0110311414:41
156-59-2
H3
trans-1,2-Dichloroethene
NO mg/L
0.0020
1
0110311414:41
156-60-5
H3
1,2-Dichloropropane
NO mg/L
0,0020
1
01103/1414:41
78-87-5
H3
cis- 1,3-Dichloropropene
ND mg/L
0.0020
1
01/03/14 14:41
10061-01-5
H3
trans-1,3-Dichloropropene
ND mg/L
0,0020
1
0110311414:41
10061-02-6
H3
Ethylbenxene
NO mg/L
0.0020
1
01/03/14 14:41
100-41-4
H3
Methylene Chloride
ND mg/L
0.0020
1
01/03/14 14:41
75-09-2
H3
1,1,2,2-Tetrachloroethane
ND mg/L
0.0020
1
01103/1414:41
79-34-5
H3
Tetrachloroethene
NO mg/L
0,0020
1
0110311414:41
127-18-4
H3
Toluene
NO mg/L
0.0020
1
01/03/14 14:41
108-88-3
H3
1,1,1-Trichloroethane
NO mg/L
0,0020
1
0110311414:41
71-55-6
H3
1, 1, 2-Trich loroethane
NO mg/L
0.0020
1
0110311414:41
79-00-5
H3
Trichloroethene
ND mg/L
0.0020
1
0110311414:41
79-01-6
H3
Trichlo rofluoro methane
ND mg/L
0.0020
1
0110311414:41
75-69-4
H3
Vinyl chloride
NO mg/L
0.0020
1
01/03/14 14:41
75-01-4
H3
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
1
01/03/14 14:41
460-00-4
Toluene-d8 (S)
99 %
70-130
1
01/03/14 14:41
2037-26-5
1,2-Dichloroethane-d4 (S)
108 %
70-130
1
01/03/14 14:41
17060-07-0
25400 Total Suspended Solids Analytical Method: SM 2540❑
Total Suspended Solids ND mg/L 2.5 1 01/03/14 15:02 H3
Date: 01/08/2014 04:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 29

aceAnalj cal e
wwwpacalabs.com
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: GCSV116366 Analysis Method: EPA 1664B
QC Batch Method: EPA 16648 Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92185137001, 92185137002
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1116372
Matrix: Water
Associated Lab Samples: 92185137001, 92185137002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mg1L
ND 5.0
01/06/14 09:34
LABORATORY CONTROL SAMPLE:
1116373
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 16.5
83 64-132
MATRIX SPIKE SAMPLE: 1116374
92185319001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L ND 20 17.1 86 64-132
Date: 01/0812014 04:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc -
Page 15 of 29

aceAnalytical o
wwwpacelabs.com
Project: Stormwater Samples
Pace Project No.: 92185137
Pate Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(82B)254-7176
QUALITY CONTROL DATA
QC Batch: MPRP114985 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92185137001, 92185137002
METHOD BLANK: 1116219
Associated Lab Samples: 92185137001, 92185137002
Parameter Units
Copper mg/L
Lead mg1L
Zinc mg1L
Matrix: Water
Blank Reporting
Result Limit
Analyzed
ND 0.0050
01/07/14 20:39
ND 0.0050
01/07/14 20:39
ND 0.010
01/07/14 20:39
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1116220
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Copper mg1L .5 0.48 96 85-115
Lead mglL .5 0.48 95 85-115
Zinc mglL .5 0.48 96 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1116221
MS
92185132002 Spike
Parameter Units Result Conc.
Copper mglL ND .5
Lead mglL ND .5
Zinc mg/L ND .5
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1116223
MS
92185318001 Spike
Parameter Units Result Conc.
Copper mg1L 0,020 .5
Lead mglL ND .5
Zinc mg1L 0.017 .5
Date: 01/08/2014 04:10 PM
1116222
MSD
Spike MS
MSD
MS
MSD
% Rec
Conc. Result
Result
% Rec
% Rec
Limits
RPD
.5 0.50
0.48
98
93
70-130
4
.5 0.44
0.42
88
85
70-130
3
.5 0,50
0.47
91
87
70-130
5
1116224
MSD
Spike MS
MSD
MS
MSD
% Rec
Conc. Result
Result
% Rec
% Rec
Limits
RPD
.5 0.50
0.51
96
97
70-130
1
.5 0,47
0.47
94
94
70-130
0
.5 0.50
0.50
97
97
70-130
0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fuit,
without the written consent of Pace Analytical Services, Inc..
Qual
Qual
Page 16 of 29

aceAnalytfical
wwwpecelabs.wm
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Or,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV125424 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92185137001, 92185137002
METHOD BLANK: 1116000
Associated Lab Samples: 92185137001, 92185137002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichloroethane
mg1L
ND
0.0020
01/0311414:26
1,1,2,2-Tetrachloroethane
mg/L
ND
0.0020
0110311414:26
1,1,2-Trichloroethane
mg/L
ND
0.0020
01103/1414:26
1,1-Dichloroethane
mg1L
ND
0.0020
01/03/14 14:26
1,1-Dichloroethene
mg/L
ND
0.0020
01103/1414:26
1,2-Dichlorobenzene
mg/L
NO
0,0020
01103/1414:26
1,2-Dichloroethane
mg/L
NO
0.0020
01103/1414:26
1,2-Dichloropropane
mg/L
NO
0.0020
01/03/14 14:26
1,3-Dichlorobenzene
mg/L
NO
0.0020
01/0311414:26
1,4-Dichlorobenzene
mg/L
NO
0.0020
01/03/14 14:26
Benzene
mg/L
NO
0,0020
01103/1414:26
Bromodichloromethane
mg1L
ND
0.0020
0110311414:26
Bromoform
mg/L
NO
0.0020
01/03/14 14:26
Bromomethane
mg/L
ND
0,0020
01/03/14 14:26
Carbon tetrachloride
mg/L
NO
0.0020
01/03/14 14:26
Chlorobenzene
mg/L
ND
0.0020
01103/1414:26
Chloroethane
mg/L
NO
0.0020
01103/1414:26
Chloroform
mg/L
ND
0.0020
01/03/14 14:26
Chloromethane
mg/L
NO
0.0020
01103/1414:26
cis-1,2-Dichloroethene
mg1L
ND
0.0020
01/0311414:26
cis-1,3-Dichloropropene
mg1L
ND
0.0020
01/03/14 14:26
Dibromochloromethane
mg1L
ND
0.0020
01/0311414:26
Ethylbenzene
mg1L
ND
0.0020
01/0311414:26
Methylene Chloride
mg/L
ND
0.0020
01/03/14 14:26
Tetrachloroethane
mg1L
ND
0.0020
01/03/14 14:26
Toluene
mg1L
ND
0.0020
01103/1414726
trans-1,2-Dichloroethene
mg/L
ND
0.0020
01/0311414:26
trans- l,3-Dichloropropene
mg1L
ND
0.0020
01/0311414:26
Trichloroethene
mg/L
ND
0,0020
01/03/1414:26
Trichlorotluoromelhane
mg/L
ND
0.0020
01/03/14 14:26
Vinyl chloride
mg1L
ND
0.0020
01/03/14 14:26
1,2-Dichloroethane-d4 (S)
%
108
70-130
01/03/14 14:26
4-Bromofluorobenzene (S)
%
98
70-130
01/03/14 14:26
Toluene-d8 (S)
%
99
70-130
01/03/14 14:26
LABORATORY CONTROL SAMPLE: 1116001
Spike
Parameter Units Conc.
1,1,1-Trichloroethane mg/L .02
1,1,2,2-Tetrachloroethane mg/L .02
1,1,2-Trichloroethane mg1L .02
Qualifiers
LCS
LCS % Rec
Result
% Rec Limits
0.020
98 52-162
0.014
71 46-157
0.016
78 52-150
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
This report shall not be reproduced, except in full,
Date: 01 /08/2014 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 29

lacmnalXical"
www.pacefahs.com
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace AnalyticaI Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1116001
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1-Dichloroethane
mg/L
.02
0.023
116
59-155
1,1-Dichloroethene
mg/L
.02
0.025
127
1-234
1,2-Dichlorobenzene
mg/L
.02
0.013
64
18-190
1,2-Dichloroethane
mg/L
.02
0.023
114
49-155
1,2-Dichloropropane
m91L
.02
0.022
109
1-210
1,3-Dichlorobenzene
mg/L
.02
0.013
65
59-156
1,4-Dichlorobenzene
mg/L
.02
0,014
72
18-190
Benzene
mg1L
.02
0.020
102
37-151
Bromodichloromethane
mg/L
.02
0,021
104
35-155
Bromoform
mg/L
.02
0.016
81
45-169
Bromomethane
mg/L
.02
0,049
244
1-242 LO
Carbon tetrachloride
mg/L
.02
0.018
90
70-140
Chlorobenzene
mg/L
.02
0,016
78
37.160
Chloroethane
mg/L
.02
0.036
182
14-230
Chloroform
mg/L
.02
0,021
106
51.138
Chloromethane
mg/L
.02
0.030
149
1-273
cis-1,2-Dichloroethene
mg/L
.02
0.023
115
68.146
cis- 1,3-Dichloroprope ne
mg1L
.02
0.021
103
1-227
Dibromochloromethane
mg1L
02
0.016
82
53-149
Ethylbenzene
mg1L
.02
0.017
87
37-162
Methylene Chloride
mg1L
.02
0.025
123
1-221
Tetrachloroethene
mg/L
.02
0.015
75
64-148
Toluene
mg/L
.02
0.018
88
47-150
trans-1,2-Dichloroethene
mg/L
.02
0.024
120
54-156
trans-1,3-Dichloropropene
mg1L
.02
0.020
102
17-183
Trichloroethene
m91L
.02
0.015
75
71-157
Trichlorofluoromethane
mg1L
.02
0.023
117
17-181
Vinyl chloride
mg/L
.02
0.031
156
1-251
4-BromoflUDrobenzene (S)
%
90
70-130
Toluene-d8 (S)
%
106
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1116005
MS
92184592002 Spike
Parameter Units Result Conc.
MSD
Spike
Cone.
1116006
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1.1,1-Trichloroethane
mg/L
NO
.02
.02
0,025
0.024
127
118
46-171
7
1,1,2,2-Tetrachloroethane
mg/L
NO
.02
.02
0,022
0,020
111
101
73-159
9
1,1,2-Trichloroethane
mg/L
NO
.02
.02
0.023
0.021
115
104
64-152
10
1,1-Dichloroethane
mg/L
ND
.02
.02
0.024
0,022
122
112
43-172
8
1,1-Dichloroethene
mg1L
ND
.02
.02
0.025
0,023
126
116
48-189
8
1,2-Dichlorobenzene
mg/L
ND
.02
.02
0.022
0.021
112
104
54-154
8
1,2-Dichloroethane
mg/L
ND
.02
.02
0,024
0.022
121
109
42-171
10
1,2-Dichloropropene
mg1L
ND
02
.02
0.023
0.021
114
105
55-157
8
1,3-Dichlorobenzene
mg/L
ND
.02
.02
0.022
0.021
110
103
57-148
6
1,4-Dichlorobenzene
mg/L
NO
02
.02
0.022
0.021
112
103
58-149
8
Benzene
mg/L
ND
.02
.02
0.024
0.022
120
112
54-163
7
Bromodichloromethane
mg/L
NO
02
.02
0.023
0.021
117
107
56-152
9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2014 04:10 PM without the written consent of Pace Analytical Services, Inc. Page 18 of 29

1�;a'ceAnalytical"
wwwpacelahs.com
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1116005
MS
92184,992002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1116006
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Bromoform
mg1L
NO
.02
.02
0,023
0,021
115
105
53-151
9
Bromomethane
mg1L
ND
.02
.02
0.025
0.025
126
123
10-200
2
Carbon tetrachloride
mg1L
ND
.02
.02
0.024
0.023
122
113
41.175
7
Chlorobenzene
mg1L
ND
.02
.02
0.023
0.022
114
108
67-152
6
Chloroethane
mg/L
ND
.02
.02
0.023
0.021
115
107
23-200
7
Chloroform
mg1L
ND
.02
02
0,024
0,023
122
113
51-166
8
Chloromethane
mg1L
NO
.02
.02
0.024
0.022
120
112
40-175
7
cis-1,2-Dichloroethene
mg1L
NO
.02
.02
0,024
0.022
118
108
45-174
9
cis-1,3-Dichloropropene
mg1L
ND
.02
.02
0.023
0.021
114
104
38-146
10
Dibromochloromethane
mg/L
ND
.02
.02
0.023
0,021
115
105
65-144
9
Ethylbenzene
mg/L
ND
.02
.02
0.023
0.021
114
107
57-152
6
Methylene Chloride
mg/L
ND
.02
.02
0.021
0.020
106
98
40-167
8
Tetrachloroethene
mg1L
ND
.02
.02
0.024
0.022
118
111
59-155
6
Toluene
mg1L
ND
.02
.02
0.023
0.021
116
107
47-162
8
trans- 1,2-Dichloroethene
mg/L
ND
.02
.02
0.024
0.022
122
112
47-178
8
trans- 1,3-Dichloropropene
mg1L
ND
02
.02
0.023
0.021
116
106
39-148
9
Trichloroethene
mg1L
ND
.02
.02
0.023
0.022
114
108
60-153
6
Trichlorofluoromethane
mg/L
ND
02
.02
0.026
0.024
129
120
42-199
7
Vinyl chloride
mg/L
ND
.02
.02
0.025
0.023
123
114
46-176
8
1,2-Dichloroethane-d4 (S)
%
111
109
70-130
4-Bromofluorobenzene (S)
%
97
98
70-130
Toluene-d8 (S)
%
100
99
70-130
Date: 01108I2014 04:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 29

(�IaceAnalytical @
wwwpecelabs.cam
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT125412 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92185137001, 92185137002
METHOD BLANK: 1116357
Associated Lab Samples: 92185137001, 92185137002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,2,4-Trichlorobenzene
mg/L
NO
0.0050
01/07/1413A3
2,4,6-Trichlorophenot
mg/L
NO
0.010
01107/1413:43
2,4-Dichlorophenol
mg/L
NO
0.0050
01/07/1413:43
2,4-Dimethylphenol
mg/L
NO
0.010
01/0711413:43
2,4-Dinitrophenol
mg1L
NO
0,050
0110711413:43
2,4-Dinitrotoluene
mg/L
NO
0.0050
0110711413:43
2,6-Dinitrotoluene
mglL
NO
0.0050
01/0711413:43
2-Chloronaphthalene
mg/L
ND
0.0050
0110711413:43
2-Chlorophenol
mg/L
NO
0,0050
0110711413:43
2-Nitrophenol
mg/L
ND
0.0050
0110711413:43
3,3'-Dichlorobenzidine
mglt
NO
0.025
0110711413:43
4,6-Dinitro-2-methylphenof
mg1L
NO
0.020
01107M413:43
4-Bromophenylphenyl ether
mg/L
ND
0.0050
01/07/14 13:43
4-Chloro-3-methylphenol
mg1L
ND
0.0050
01/07/1413:43
4-Chlorophenylphenyl ether
mg/L
NO
0.0050
01/07/14 13:43
4-Nitrophenol
mg/L
NO
0,050
01107/1413:43
Acenaphthene
mg1L
ND
0.0050
01107/1413:43
Acenaphthylene
mg1L
ND
0,0050
0110711413:43
Anthracene
mg/L
ND
0.0050
0110711413:43
Benzo(a)anthrace ne
mg/L
ND
0,0050
0110711413:43
Benzo(a)pyrene
mg1L
NO
0.0050
0110711413:43
Benzo(b)fluoranthene
mg1L
NO
0,0050
0110711413:43
Benzo(g,h,i)perylene
mg/L
ND
0.0050
01/07/1413:43
Benzo(k)fluoranthene
mg/L
ND
0.0050
01107/1413:43
bis(2-Chloroethoxy)methane
mg/L
ND
0,010
01107/1413:43
bis(2-Chloroethyl) ether
mg/L
NO
0.0050
01107/14 13:43
bis(2-Chloroisopropyl) ether
mg/L
NO
0,0050
01/07/14 13:43
bis(2- Ethyl hexyl)phthalate
mg1L
NO
0.0050
01107/1413:43
Butylbenzylphtha late
mg/L
NO
0,0050
0110711413A3
Chrysene
mg/L
NO
0.0050
0110711413:43
Di-n-butylphthalate
mg/L
NO
0,0050
0110711413:43
Di-n-octylphthalate
mg/L
NO
0,0050
0110711413:43
Dibenz(a,h)anthracene
mg/L
NO
0.0050
01107/1413:43
Diethyl phthalate
mg/L
NO
0,0050
01107/141143
Dimethylphthalate
mg/L
NO
0.0050
0110711413:43
Fluoranthene
mg/L
NO
0.0050
01/0711413A3
Fluorene
mg/L
NO
0.0050
01/0711413:43
Hexachloro-1,3-butadiene
mg1L
NO
0.0050
01107/1413:43
Hexachlorobenzene
mg/L
NO
0.0050
01/0711413:43
Hexachlorocyclopentadiene
mg/L
NO
0,010
01107/1413:43
Hexachloroethane
mg/L
NO
0.0050
01/07/1413:43
Indeno(1,2,3-cd)pyrene
mg/L
ND
0.0050
01/0711413:43
Isophorone
mg1L
NO
0.010
0110711413:43
REPORT OF LABORATORY ANALYSIS
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shalt not be reproduced, except in full,
Date: 01/08/2014 04:10 PM without the written consent of Pace Analytical Services, Inc,. Page 20 of 29

aceAnalytical"
www.pacalabs. com
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26804
[phone]
QUALITY CONTROL DATA
METHOD BLANK: 1116357
Associated Lab Samples: 92185137001, 92185137002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
N-Nitroso-di-n-propylamine
mglL
NO
0.0050
01/07/14 13:43
N-Nitrosodimethylamine
mg1L
ND
0,0050
01107/1413:43
N-Nitrosodiphenylamine
mg1L
NO
0.010
01107/1413:43
Naphthalene
mg1L
ND
0.0050
01107/1413:43
Nitrobenzene
mg1L
ND
0,0050
01107/1413:43
Pentachlorophenol
mglL
NO
0.010
01/0711413:43
Phenanthrene
mglL
NO
0,0050
01/07/14 13:43
Phenol
mglL
NO
0.0050
01/07/14 13:43
Pyrene
mglL
NO
0.0050
01/07/14 13:43
2,4,6-Tribromophenol (S)
%
94
10-137
01/07/14 13:43
2-Fluorobiphenyl (S)
%
68
15-120
01/07/14 13:43
2-Fluorophenol (S)
%
40
10-120
01/07/14 13:43
Nitrobenzene-d5 (S)
%
68
10-120
01/07/14 13:43
Phenol-d6 (S)
%
28
10-120
01/07/14 13:43
Terphenyl-d14 (S)
%
103
11-131
01/07/14 13:43
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1116358
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
mglL
.05
0.038
76
44-142
2,4,6-Trichlorophenol
mg1L
.05
0,047
93
37-144
2,4-Dichlorophenol
mg1L
.05
0.045
90
1-191
2,4-Dimethylphenol
mg1L
.05
0,046
93
32-119
2,4-Dinitrophenol
mg1L
.25
0.25
102
1-181
2,4-Dinitrotoluene
mglL
.05
0,054
109
39-139
2,6-Dinitrototuene
mg1L
.05
0.054
109
50-158
2-Chloronaphthalene
mg1L
.05
0,040
80
60-118
2-Chlorophenol
mg1L
.05
0.041
82
23-134
2-Nitrophenol
mglL
.05
0,047
95
29-182
3,3'-Dichlorobenzidine
mg1L
.1
0.099
99
1-262
4,6-Dinitro-2-methylphenol
mglL
.1
0.11
108
1-181
4-Bromophenylphenyl ether
mglL
05
0.061
102
53-127
4-Chloro-3-methylphenol
mg/L
.1
0.089
89
22-147
4-Chlorophenylphenyl ether
mg1L
.05
0.049
98
25-158
4-Nitrophenol
mg1L
.25
0,11
46
1-132
Acenaphthene
mg1L
.05
0.045
91
47-145
Acenaphthylene
mg1L
.05
0.046
93
33-145
Anthracene
mg1L
.05
0.050
100
1-166
Benzo(a)anthracene
mg1L
.05
0.050
100
33-143
Benzo(a)pyrene
mglL
.05
0.054
107
17-163
Benzo(b)fluoranthene
mglL
.05
0.049
98
24-159
13enzo(g,h,i)perylene
mglL
.05
0.049
98
1-219
Benzo(k)fluoranthene
mglL
.05
0,048
96
11-162
bis(2-Chloroethoxy)methane
mglL
.05
0.044
88
33-184
bis(2-Chloroethyl) ether
mg1L
.05
0:040
80
12-158
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
This report shall not be reproduced, except in full,
Date: 01I0812014 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 29

aceAnalytical
wwwp6cviabs.com
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1116358
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(B28)254-7176
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huniersville, NC 28078
[phone]
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Qualifiers
bis(2-Chloroisopropyl) ether
mg1L
.05
0.039
79
36.166
bis(2-Ethylhexyl)phthalate
mg1L
.05
0,053
106
8-158
Butylbenzylphtha late
mg1L
.05
0.052
103
1-152
Chrysene
mg1L
05
0.051
102
17-168
Di-n-butylphthalate
mg1L
.05
0.048
96
1-118
Di- n-octylphthalate
mg1L
.05
0.054
108
4-146
Dibenz(a,h)anthracene
mg1L
.05
0.052
104
1-227
Diethylphthalate
mg1L
.05
0.045
90
1-114
Dimethylphthalate
mg1L
.05
0.044
88
1-112
Fluoranthene
mg1L
.05
0.053
106
26-137
Fluorene
mg1L
.05
0.048
97
59-121
Hexachloro-1,3-butadiene
mg1L
.05
0.039
77
24-116
Hexachlorobenzene
mg1L
.05
0.045
91
1-152
Hexachlorocyclopentadiene
mg1L
.05
0.058
116
25-150
Hexachloroethane
mg1L
.05
0.034
69
40-113
Indeno(1,2,3-od)pyrene
mg1L
.05
0.053
105
1-171
Isophorone
mg1L
.05
0.049
97
21-196
N-Nitroso-di-n-propytamine
mg1L
.05
0.037
75
1-230
N-Nitrosodimethylamine
mg1L
.05
0.027
53
25-150
N-Nitrosodiphenylamine
mg1L
.05
0.041
83
25-150
Naphthalene
mg1L
.05
0.043
85
21-133
Nitrobenzene
mg1L
.05
0.047
93
35-180
Pentachlorophenol
mg1L
.1
0.10
104
14-176
Phenanthrene
mg1L
.05
0,049
98
54-120
Phenol
mg1L
.05
0.020
41
5-112
Pyrene
mg1L
.05
0.053
105
52-115
2,4,6-Tribromophenol (S)
%
117
10-137
2-Fluorobiphenyl (S)
%
90
15-120
2-Fluorophenol (S)
%
55
10-120
Nitrobenzene-d5 (S)
%
90
10-120
Phenol-d6 (S)
%
39
10-120
Terphenyl-dl4 (S)
%
105
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1116359
1116360
MS
MSD
92185017001
Spike
Spike MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc. Result
Result
% Rec % Rec
Limits
RPD Qual
1,2,4-Tdchlorobenzene
mg1L
ND
.1
.1 0.061
0.074
61
74
44-142
19
2,4,6-Trichlorophenol
mg1L
ND
.1
.1 0.066
0.088
66
88
37-144
28
2,4-Dichlorophenol
mg1L
ND
.1
.1 0.063
0.086
63
86
1-191
30
2,4-Dimethylphenol
mg1L
ND
.1
.1 0.065
0.088
65
88
32-119
30
2,4-Dinitrophenol
mglL
NO
5
.5 0.33
0.46
66
93
1-181
33 R1
2,4-Dinitrotoluene
mglL
ND
1
.1 0.081
0.095
81
95
39-139
16
2,6-Dinitrotoluene
mg1L
ND
A
.1 0,078
0.095
78
95
50-158
20
2-Chloronaphthalene
mg1L
ND
.1
.1 0.061
0.074
61
74
60-118
20
2-Chlorophenol
mglL
ND
A
.1 0,060
0.079
60
79
23-134
28
2-Nitrophenol
mglL
ND
.1
.1 0.065
0.088
65
88
29-182
31 R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2014 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 29

aceAnalytical
-Pacelabs.com
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1116359
MS
92185017001 Spike
Parameter Units Result Cone.
MSD
Spike
Cone.
1116360
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
3,3'-Dichlorobenzidine
mg/L
ND
2 .2
0.086
0.089
43
45
1-262
4
4,6-Dinitro-2-methylphenol
mg/L
NO
.2 .2
0.13
0.18
67
92
1-181
31 R1
4-Bromophenylphenyl ether
mg1L
NO
,1 .1
0.073
0.089
73
89
53-127
19
4-Chloro-3-methylphenol
mg1L
NO
.2 .2
0.13
0.17
64
87
22-147
30
4-Chlorophenylphenyl ether
mg/L
NO
,1 .1
0.074
0.089
74
89
25-158
19
4-Nitrophenol
mg/L
ND
.5 .5
0.21
0.31
43
63
1-132
38 R1
Acenaphthene
mg/L
NO
.1 .1
0.068
0.082
68
82
47-145
18
Acenaphthylene
mg/L
NO
.1 .1
0.071
0.084
71
84
33-145
17
Anthracene
mgfL
NO
.1 .1
0.073
0.087
73
87
1-166
18
Benzo(a)anthracene
mglL
NO
.1 .1
0.070
0.085
70
85
33-143
19
Benzo(a)pyrene
mg1L
ND
.1 .1
0.076
0.093
76
93
17-163
20
Benzo(b)Ruoranthene
mg1L
ND
.1 A
0.06E
0,081
68
81
24-159
17
Benzo(g,h,i)perylene
mg/L
ND
.1 A
0.070
0.087
70
87
1-219
21
Benzo(k)(luoranthene
mg1L
ND
.1 .1
0.064
0.080
64
80
11-162
22
bis(2-Chloroethoxy)methane
mg/L
ND
.1 .1
0.066
0.082
66
82
33-184
22
bis(2-Chloroethyl) ether
mg/L
ND
.1 .1
0.059
0.071
59
71
12-158
18
bis(2-Chloroisopropyl) ether
mg/L
ND
.1 .1
0.061
0.072
61
72
36-166
17
bis(2-Ethythexyl)phthalate
mg/L
ND
,1 .1
0.072
0.087
72
87
B-158
19
Butylbenzylphthalate
mg/L
ND
.1 .1
0.070
0.086
70
86
1-152
20
Chrysene
mg/L
ND
.1 .1
0.071
0.087
71
87
17-168
20
Di-n-butylphthalate
mg/L
ND
.1 .1
0.070
0.083
70
83
1-118
18
Di-n-octylphthalate
mg/L
ND
.1 .1
0.075
0,093
75
93
4-146
21
Dibenz(a,h)anthracene
mg/L
ND
A .1
0.073
0.093
73
93
1-227
24
Diethylphthalate
mg/L
ND
,1 ,1
0,066
0,079
66
79
1-114
18
Dimethylphthalate
mg/L
ND
.1 .1
0.065
0.077
65
77
1-112
18
Fluoranthene
mg/L
ND
.1 .1
0.078
0.093
78
93
26-137
18
Fluorene
mg/L
ND
1 1
0.073
0.087
73
87
59-121
18
Hexachloro-1,3-butadiene
mg/L
ND
1 1
0.061
0.073
61
73
24-116
19
Hexachlorobenzene
mg/L
NO
1 1
0.065
0.079
65
79
1-152
19
Hexachlorocyclopentadiene
mg/L
ND
1 1
0.084
0,11
84
105
25-150
23
Hexachloroethane
mg/L
ND
1 1
0.055
0.064
55
64
40-113
16
Indeno(1,2,3-cd)pyrene
mg/L
ND
1 1
0.075
0.092
75
92
1-171
20
Isophorone
mg/L
ND
1 1
0.074
0.091
74
91
21-196
21
N-Nitroso-d i-n-propyla mine
mg/L
ND
1 1
0.057
0.069
57
69
1-230
20
N-Nitrosodimethyta mine
mg/L
ND
1 1
0.049
0.064
49
64
25-150
26
N-Nitrosodi phenyla mine
mg/L
ND
1 1
0.060
0.070
60
70
25-150
16
Naphthalene
mg/L
ND
1 1
0.067
0.082
67
82
21-133
20
Nitrobenzene
mg/L
ND
1 1
0.069
0.085
69
85
35-180
21
Pentachlorophenol
mg/L
ND
.2 .2
0.14
0.18
68
92
14-175
30
Phenanthrene
mg/L
ND
1 1
0.070
0,084
70
84
54-120
18
Phenol
mg1L
ND
1 1
0.036
0.051
36
51
5-112
35 R1
Pyrene
mg/L
NO
1 1
0,073
0.088
73
88
52-115
18
2,4,6-Tribromophenol (S)
%
82
109
10-137
2-Fluorobiphenyl (S)
%
69
85
15-120
2-Fluorophenol (S)
%
46
67
10-120
Nitrobenzene-d5 (S)
%
68
85
10-120
Phenol-d6 (S)
%
37
55
10-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2014 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 29

aceAnalytical
wwwpacclabs. com
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1116359 1116360
MS MSD
92185017001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Terphenyl-d14 (S) % 74 90 11-131
Date: 01/0812014 04:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 24 of 29

'ceAnalytical
(�
—pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Or,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Stormwater Samples
Pace Project No.: 92185137
QC Batch: WET128921 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92185137001, 92185137002
METHOD BLANK: 1116016
Associated Lab Samples: 92185137001, 92185137002
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE: 1116017
Parameter Units
Total Suspended Solids mg1L
SAMPLE DUPLICATE: 1116018
Parameter Units
Total Suspended Solids mg1L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 2.5 01/0311415:01
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 256 102 80-120
92185137001 Dup
Result Result RPD Qualifiers
6.6 6.6 0
SAMPLE DUPLICATE: 1116019
92184997001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 11.6 12.0 3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2014 04:10 PM without the written consent of Pace Analytical Services, Inc..
Page 25 of 29

(�IacieAnalytical
www.pacalabs. com
Project: Stormwater Samples
Pace Project No.: 92185137
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28604
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit,
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
[phone]
This report shall not be reproduced, except in full,
Date: 01/08/2014 04:10 PM without the written consent of Pace Analytical Services, Inc,. Page 26 of 29

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 205 East Meadow Road - Suite A 2225 Riverside Dr.
IieAnayical Eden, NC 27288 Asheville, NO 28804
wa'tepacerabs.mm [phone] [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stormwater Samples
Pace Project No.: 92185137
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NO 28078
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92186137001
Outfall 1
EPA 16649
GCSVI16366
92185137002
Outfall 2
EPA 16648
GCSVI16366
92185137001
Outfall1
EPA200.7
MPRP/14985
EPA200.7
92185137002
Outfall2
EPA200.7
MPRP/14985
EPA200.7
92185137001
Outfall1
EPA625
OEXT/25412
EPA625
92185137002
Outfall2
EPA625
OEXT/25412
EPA625
92185137001
OutfaEE 1
EPA624
MSV/25424
92185137002
Outfall2
EPA624
MSV/25424
92185137001
Outfall 1
SM 2540D
WET/28921
92185137002
Outfall 2
SM 2540D
WET/28921
Date: 01/08/2014 04:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytioal Services, Inc..
Analytical
Batch
ICP/13613
ICP/13613
MSSV/8631
MSSV/8631
Page 27 of 29

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Page 28 of 29

�ceAnaly�rca!'
CHAIN -OF -CUSTODY I Analytical Request document
The Cfwinof-G GAL DOCUMENT, All rtlevafd Tklds muse be completed aaaaetsly.
P-f v1
t'NPDES
F GROUNDWATER r OMMONGWATER
OTHER
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'4
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quaaity General Permit No. NCG030000
Date submitted 21 12�_
CERTIFICATE OF COVERAGE NO. NCG03,0_ LL J
FACILITY NAME lq(- C-LL- Fah _ nC .
COUNTY LA )'.r f-- _ _
PERSON COLLECTING SAMPLES �r,ni ti I1 a
LABORATORY _12,aC, (- P nA I W +i Cal 6b Cert. #
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR (3
SAMPLE PERIOD ❑ Jan -June ❑v'Juiy-Dec
or ❑ Monthly) (month)
DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA
❑Zero-fiow ❑Water Supply ❑SA
❑Other C'I N 5 U _
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?'
Outfall No.
bate Sample
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non-Pofar0&G/
Total Petrltlevth
Hydrocarbons
Organics Total Toxic
s
Benchmarks =_=>
_
-
100 mg/L or 50 mg/L
6.0 - 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 rn#L
1 mg/L
I10L
hnlLs�.
o
I
�.
► 3
r�
b
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 111112012-1013112017 5WU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
_Sonya t�a,lsh ...
Name (Print name)
E oironmt--(NAR1 Sa�r1_ a1 {Y1an ��-
Title (Print title) nn
o� I
114
{Signature (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, NO, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX mpLiL", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
No discharge this period?'
Outfall No.
Date Sample
Collected
{mo]dd/yr)
244hour rainfall
amount,
Incfiesa
Non -polar O&G/TPH by
SPA 1564 (5GT-HEMj
f
Total Stir nded Solids
4
-
:t " pH
Benchmarks =__>
-
-
15 mg/L
100 nig/uik.56 iiig/L* r c
.-,..Co — 9.0 5U
Footnotes from Part A also apply to this Part B
' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

4Y
Note: if you report a sample value in excess of the ,benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
iF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an ori_ lnal and one copy- of this DMR, including all "No Discharae" reports. within 30 dovs of receipt of the lab results (or at end of monitoring period
in the case of No Discharae" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
ra14
(Signature of P ittee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

aceAnalytical.
www.pacelabs.cam
April 25, 2013
Ms. Sonya Walsh
ACCU FAB
801 Beacon Lake Dr.
Raleigh, NC 27610
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
RE: Project: Roof-Top•Sampfel
Pace Project No.: 92155205
Dear Ms. Walsh:
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9600 Kincey Ave. Suite 100
Huntersville. NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on April 19, 2013. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page
[e-mail]
Project Manager
Enclosures
pCCRF�
TNI
REPORT OF LABORATORY ANALYSIS
;his report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 9

aceAnalytical
www.pecerabs.crovn
Project: Roof Top Sample
Pace Project No.: 92155205
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
'2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Asheville Certification Ids
2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 Virginia(VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 26076
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 9

aceAnalytical
wwwpacWabs.=
Project: Roof Top Sample
Pace Project No.: 92155205
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(B28)254-7176
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92155205001 New Roof Top EPA 200.7 JMW 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 9

aceAna,(Xical
www.pacNabs.mn
Project: Roof Top Sample
Pace Project No.: 92155205
Method: EPA 200.7
Description: 2003 MET ICP
Client: ACCU FAB
Date: April 25, 2013
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below. .
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 9

lacmnalytical.
wwwpacefats.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Paco Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Roof Top Sample
Pace Project No.: 92155205
Sample: Now Roof_Top_l Lab ID: 92155205001 Collected: 04/12/13 07:48 Received: 04119/13 12:57 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET 1CP
Zinc
Date: 04/25/2013 04:27 PM
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
0:14-mg1L 0.010 1 04/23/1310:55 04/24/1316:41 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 9

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalj ca! 205 East Meadow Road - Suite A 2225 Riverside Dr, 9800 Kincey Ave. Suite 100
www.pacelals.cnm Eden, NC 27288 AshevIle, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: Roof Tap Sample
Pace Project No.: 92155205
QC Batch: MPRP113129
Analysis Method: EPA 200.7
QC Batch Method: EPA200.7
Analysis Description: 2003 MET
Associated Lab Samples. 92155205001
METHOD BLANK: 961329
Matrix: Water
Associated Lab Samples: 92155205001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Zinc
mg1L
ND 0.010
04/2411315:48
LABORATORY CONTROL SAMPLE:
961330
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Zinc
mg1L
.5 0.48
96
85-115
MATRIX SPIKE SAMPLE:
961331
92155158001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Zinc
mg1L
0.064 ,5
0.53
93
70-130
MATRIX SPIKE SAMPLE:
961333
92155205001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Zinc
mg1L
0,14 ,5
0.63
98
70-130
SAMPLE DUPLICATE: 961332
92155351001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Zinc
mg1L
215 ug/L 0.22
0
SAMPLE DUPLICATE: 961334
92155255002 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Zinc
mg/L
45.1 uglL 0.045
0
Date: 04/25/2013 04:27 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 9

acmnalytical
wwwpaCaJabs.com
Project: Roof Top Sample
Pace Project No.: 92155205
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
.1 - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDI- -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded dale are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(0) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 04/25/2013 04:27 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 9

acmnalyfrcal
ffmpacafaftc=
Project: Roof Tap Sample
Pace Project No.: 92155205
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92155205001 New Roof Top EPA200.7 MPRP113129 EPA 200.7 ICP111963
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/25/2013 04:27 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 9

CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chmnwf-Custody is a LEGAL DOGUMEW M relevant fields must be oompleted accurately,
aceArralytical - • . . - ..' � .. _ . .. • _ - . '
i' -alirir:Daadatn:cdm
`Secton A r.; 5ecdon B Section G Pagai T of -
. Required Cited framrristion _ Wnsd Project ir>fiwmaiw_n. _ hivo�k>brtnatlpr - -
Cor . -. .- Report Ta .. , e
Jr:
1609296
Address ;' ry e Cil
CoPYTa:. f r- - Co^pany Name: _ s� t n
Dr-R_EGULAT4,.�IGs
Address s [ NPpES Gl�011NDlyllATERj y_ DftIN1gNG WATER;
£mall TO: Puchase Order Nl - -. Paw 0-43 ' - . � � . - Rates
i- UST [" .RCRA G ; OTHER
Pho J- --' dame: _ '. _JR
!Sltet.oca"�Eo
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Requeatied.Dua DatdFP,T - ; Pro)ect Nrariber. .. - rf •Pepe-Pnt®e ix - . - r - - ' S q7 ' N-�; ' q
Section D 17atrix Lades t - e a - : z i = - _ , t•�
a 4 x-+s t T V4..
h ;:7 ✓ W f e �,� 1 ^t °' 1 „i -
E= l s ; OIiE D t Presefvabves
q.qukeec�enrinr6ri5uon MArx�z'reoo G ETE.
Water
Water , .- YDVwi .. U - - -- .. r - d
COMPOSME- COMPOSITE Productwater ww Erw.C�tnE
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SAMPLE m w �, W Y
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days:-� - _ F-lilL�-020rev 07 15-May 2007 -�� 0, .

�Ice Analytical
www.pacelabs.com
May 13, 2013
Ms. Sonya Walsh
ACCU FAB
801 Beacon Lake Dr.
Raleigh, NC 27610
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
RE: Project: Zi cn sample
Pace Project No,: 92156905
Dear Ms. Walsh:
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hurtersville, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on May 06, 2013, The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
\JI+,+
Terri Page
[e-mail]
Project Manager
Enclosures
IkCCR
't
TN
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 9

aceAnalyiical
wwwp8cWsbs.c=
Project: Zinc sample
Pace Project No.: 92156905
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
CERTIFICATIONS
[phone]
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40
FloridalNELAP Certification #: E87648 South Carolina Certification #; 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report 5hA9 not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 9

lacieAnalytical's
wrw.pacelabs.com
Project: Zinc sample
Pace Project No.: 92156905
Pace Ana lyticaI Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9D92
Analytts
Lab ID Sample ID Method Analysts Reported Laboratory
92156905001 Roof Top Roll up door EPA 200.7 JMW 1 PASI-A
92156905002 Rood Top #2 EPA 200.7 JMW 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 9

e Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
lac,
Analytical 205 East Meadow Road - Suite 2225 Riverside Dr. 9800 KinceyAve . Suite 100
wwwpace7abscom Eden, NO 27288 Asheville, NO 28804 Huntersville, NO 28078
[phone] (828)254-71176 [phone]
PROJECT NARRATIVE
Project: Zinc sample
Pace Project No.: 92156905
Method: EPA 200.7
Description: 200.7 MET ICP
Client: ACCU FAB
Date: May 13, 2013
General Information:
2 samples were analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation. -
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 9

(�Iacmnalyfical
wwwpacelabsxom
Project: Zinc sample
Pace Project No.: 92166905
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANAL1!TICA - ESUJS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: Roof Top RLII up.door> Lab ID: 92156905001 Collected: 04/29/13 15:30 Received: 05/06113 14:45 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 0.39 mg1L 0.010 1 05/08/13 12:20 05/09/13 21:14 7440-66-6
Sample: 'Rood'Top #2 Lab ID: 92156905002 Collected: 05/06/13 12:30 Received: 05/06/13 14:45 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 0:fifi mg/L 0.010 1 05/08/13 12:20 05/09/13 21;17 7440-66-6
k.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2013 09:25 AM without the written consent of Pace Analytical Services, Inc- Page 5 of 9

aceAnalytical
www.P8Caf8b5.00m
Project: Zinc sample
Pace Project No.: 92156905
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Or.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
DUALITY CONTROL DATA
QC Batch: MPRPI13250 Analysis Method: EPA200.7
QC Batch Method: EPA200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92156905001, 92156905002
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 26078
[phone]
METHOD BLANK: 970311 Matrix: Water
Associated Lab Samples: 92156905001, 92156905002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Zinc mg1L ND 0.010 05/09/13 20:15
LABORATORY CONTROL SAMPLE: 970312
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Zinc mg1L .5 0.50 100 85-115
MATRIX SPIKE SAMPLE: 970313
92156925004 Spike
MS
MS
% Rec
Parameter Units
Result Conc.
Result
% Rec
Limits Qualifiers
Zinc mg/L
171 ug/L .5
0,67
100
70-130
MATRIX SPIKE SAMPLE: 970315
92156905002 Spike
MS
MS
% Rec
Parameter Units
Result Conc.
Result
% Rec
Limits Qualifiers
Zinc mg1L
0.66 .5
1.2
104
70-130
SAMPLE DUPLICATE: 970314
92156838001 Dup
Parameter Units Result Result RPD Qualifiers
Zinc mg/L ND .0075J
SAMPLE DUPLICATE. 970316
Parameter
Zinc
Date: 05/13/2013 09:25 AM
92156993001 Dup
Units Result Result
mg/L 36.1 ug/L 0,035
RPD Qualifiers
3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 9

acmnalytical
www.padslatts.com
Project: Zinc sample
Pace Project No.: 92156905
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene,
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except 1n full,
Date: 05/1312013 09:25 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 9

acmnalytical
Nww.pacefifto m
Project: Zinc sample
Pace Project No.: 92156905
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92156905001 Roof Top Roll up door EPA 200.7 MPRPI13250 EPA 200.7 ICP112072
92156905002 Rood Top #2 EPA 200.7 MPRPI13250 EPA 200.7 ICP112072
Date: 05/13/2013 09:25 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 9

a�
CHAIN-QF CUSTODY I Analytical Request document
The Chain -of -Custody Is a LEGAL DOCUMENT AN relevant fields anpl must be ceted axuratefy.
. , aeeAnal kal' t
SectforrA. SecUon B Section C. P29e' °E
RequtrW CGent Information., - _ . - Required Protect hiformatio_n: - - hrvoice Information.
Report To:' - - - .. . _ Attention:-
Copy To. _ Cormany. NamREG Ui`A AG NC!Y ^ - y
:f NPE E I-' AGROUND WATEE3bRai�KI9 kTE
Emal o: _ [. Purchase Cofer No-, (' UST r - RCRAYi-. �.r. OTHER - c
F Proje�.t Name: mod. - .'°°xj-•a•�x
Sitetl..6on
! Ragiresfed Due AT;-.;.r P[a(ert Nwriber. --- -- - Pace Prafire 4: - y}°.• �S74iT�" f~r•• s 'l
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Regaireddient 6hlna5an----..... unrRni-r coot= -r ,. ..EOLL.ECTEb `
Water
Waste Water ' WW ' m U
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SAMPLE [D� W�P
{A2091) r. Air;-;.. AR o w_ a':Q
Sample IDs MUST BE UNIQUE Issue `- l"5 O ,,
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• + _DATE. r.rTllkE., -!}ATE -: -.TIME i �'j 7 2' 2 S, 2 Q� . {' a �• ti .Pace>.Proyeet:No1.I,.ah:i.D. -
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s�iE)%RFiJhIQU �Z,,,�t-,m"—! n �.�:- AzCdzC---�:mNe �S �� fi��v�i.a 31ht_ .% SAMPLE GOHI]171ON8
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PRINTeif 5?JYIPLER:
ORIGINAL rm
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ra 9m yarhra Hoes By agog tha !wm Yas die accep6g Pads NET 3o my wyn+w learn end egeeag b late 0l;75% 1 rK enntF far a ry lis ciza paid wKttin 3p days � F 4LL-0 02Vier.07 15 M2j -2007 �

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
{
March 20, 2013
Ms. Sonya Walsh
ACCU FAB
801 Beacon Lake Dr.
Raleigh, NC 27610
RE: Project: WW Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Ms. Walsh:
Enclosed are the analytical results for sample(s) received by the laboratory on February 27, 2013.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page
[e-mail]
Project Manager
Enclosures
pCCRF��
TNI
REPORT OF LABORATORY ANALYSIS
This report Shal) not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 23

aceAnalXical
wwwpiceiabs.com
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Charlotte Certification iDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analydcal Services, Inc„
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 23

leAnalytical
wwwpscefsbs.com
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 2BO78
[phone]
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92149470001 Outfall 1 SM 2540D
CHM
1
PASi-E
EPA 1664E
CLW
1
PASI-C
EPA200.7
SH1
3
PASI-A
EPA625
RES
58
PASI-C
EPA 624
CAM
35
PASI-C
92149470002 Outfall 2 SM 25400
CHM
1
PASI-E
EPA 1664B
CLW
1
PASI-C
EPA200.7
SH1
3
PASI-A
EPA 625
RES
58
PASI-C
EPA624
CAH
35
PASI-C
REPORT OF LABORATORY ANALYSIS Page 3 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
www.pacefaes.com
Project: VWV Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Method: SM 2640D
Description: 2540D Total Suspended Solids
Client: ACCU FAB
Date: March 20, 2013
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
General Information:
2 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: EDEN111112
131: RPD value was outside control limits.
• DUP (Lab ID: 931740)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 23

acmnalytical
wwwpacata8s.c rn
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Method: EPA 1664B
Description: 1664 SGT-HEM, TPH
Client: ACCU FAB
Date: March 20, 2013
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
PROJECT NARRATIVE
[phone]
General Information;
2 samples were analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below,
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below,
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 23

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acmnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwpacelabscom Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
PROJECT NARRATIVE
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Method: EPA 200.7
Description: 2003 MET ICP
Client: ACCU FAB
Date: March 20. 2013
General Information:
2 samples were analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below,
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments;
REPORT OF LABORATORY ANALYSIS Page 6 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical a 205 East Meadow Road - Suite 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
ww aysmm Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
PROJECT NARRATIVE
Project: VWV Testing 02/26/13
Pace Project No.: 92149470
Method: EPA 625
Description: 625 MSSV
Client: ACCU FAB
Date: March 20, 2013
General Information:
2 samples were analyzed for EPA 625. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 625 with any exceptions noted below.
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS Page 7 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

e
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
aceAnalytical
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.pacelabs.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
PROJECT NARRATIVE
Project: VWV Testing 02/26/13
Pace Project No.: 92149470
Method. EPA 624
Description: 624 Volatile Organics
Client: ACCU FAB
Date: March 20, 2013
General Information:
2 samples were analyzed for EPA 624. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS Page 8 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,

aceAnalytica!®
www.pacelaftom
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sarnple:rOutfall l-, Lab ID: 92149470001 Collected: 02126/13 13:40 Received: 02127/13 14:40 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 20.1 mg/L 3.7 1 03/04/13 09:01
1664 SGT-HEM, TPH Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons NO mg/L 5.0 1 03/01/13 09:10
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Capper
NO mg1L
0,0050
1
03101/13 13:10
03/04/13 22:51
7440-50-8
Lead
NO mg1L
0.0050
1
03/01/13 13:10
03/04/13 22:51
7439-92-1
Zinc
0:030-mg1L
0.010
1
03101/13 13:10
03/04/13 22:51
7440-66-6
625 MSSV
Analytical Method: EPA625 Preparation Method:
EPA625
Acenaphthene
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
83-32-9
Acenaphthylene
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
208-96-8
Anthracene
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
120-12-7
Benzo(a)anthracene
ND mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
56.55-3
Benzo(a)pyrene
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:19
50-32-8
Benzo(b)(luoranthene
NO mg1L
0.0050
1
03105/13 19:59
03/12/13 03:19
205-99-2
Benzo(g,h,i)perylene
NO mg1L
0,0050
1
03/05/13 19:59
03/12/13 03:19
191-24-2
Benzo(k)fluoranthene
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:19
207-08-9
4-Bromophenylphenyl ether
NO mg1L
0.0050
1
03105/13 19:59
03/12/13 03:19
101-55-3
Butylbenzylphtha late
NO mg1L
0,0050
1
03105/13 19:59
03/12/13 03:19
85-68-7
4-Chloro-3-methylphenol
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:19
59-50-7
bis(2-Chloroethoxy)methane
NO mg/L
0.010
1
03/05/13 19:59
03/12/13 03:19
111-91-1
bis(2-Chloroethyl) ether
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
111-44-4
bis(2-Chloroisopropyl) ether
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:19
108-60-1
2-Chloronaphthalene
ND mg1L
0.0050
.1
03/05/13 19:59
03/12/13 03:19
91-58-7
2-Chlorophenal
ND mg1L
0,0050
1
03/05/13 19:59
03/12/13 03:19
95-57-8
4-Chlorophenylphenyl ether
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:19
7005-72-3
Chrysene
ND mg1L
0,0050
1
03/05113 19:59
03/12/13 03:19
218-01-9
Dibenz(a,h)anthracene
ND mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
53-70-3
3,3'-Dichlorobenzidine
NO mg1L
0,025
1
03/05113 19:59
03/12/13 03:19
91-94-1
2,4-Dichlorophenol
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:19
120-83-2
Diethylphthalate
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
84-66-2
2,4-Dimethylphenol
NO mg/L
0.010
1
03/05/13 19:59
03/12/13 03:19
105-67-9
Dimethylphthalate
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
131-11-3
Di-n-butylphthalate
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:19
84.74-2
4,6-Dinitro-2-methylphenol
NO mg/L
0.020
1
03/05/13 19:59
03/12/13 03:19
534-52-1
2,4-Dinitrophenol
NO mg/L
0.050
1
03/05/13 19:59
03/12/13 03:19
51.28-5
2,4-Dinitrotoluene
NO mg/L
0.0050
1
03/0511319:59
031121130319
121-14-2
2,6-Dinitrotoluene
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
606-20-2
Di-n-octylphthalate
NO mg/L
0,0050
1
03/05/13 19:59
03/12/13 03:19
117-84-0
bis(2-Fthylhexyt)phthalate
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
117-81-7
Fltioranthene
ND mg1L
0,0050
1
03/05/13 19:59
03/12/13 03:19
206-44-0
Fluorene
ND mg1L
0.0050
1
03/05/13 19:59
03112/13 03:19
86-73-7
Hexachloro-1,3-butadiene
ND mg/L
0,0050
1
03/05/13 19:59
03/12/13 03:19
87-68-3
Hexachlorobenzene
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
118-74-1
Date: 03/20/2013 11:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
without the written consent
of Pace Analytical
Services,
Inc..
Page 9 of 23

aceAnaIXical
ww,wpacerebs.coin
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Sample: Outfall 1 Lab ID: 92149470001 Collected: 02126113 13:40 Received: 02/27/13 14:40 Matrix: Water.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quaff
625 MSSV Analytical Method: EPA625 Preparation Method: EPA625
Hexachlorocyclopentadiene
NO mg1L
0.010
1
03/05/13 19:59
03/12/13 03:19
77-47-4
Hexachloroethane
NO mg/L
0.0050
1
03/05/13 19:59
03/12113 03:19
67-72-1
Indeno(1,2,3-cd)pyrene
NO mg/L
0.0050
1
03/0511319:59
03/1211303:19
193-39-5
Isophorone
NO mg1L
0.010
1
03/05/13 19:59
03/12/13 03:19
78-59.1
Naphthalene
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:19
91-20-3
Nitrobenzene
NO mg/L
.0.0050
1
03/05/13 19:59
03/12/13 03:19
98-95-3
2-Nitrophenol
ND mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
88-75-5
4-Nitrophenol
NO mg/L
0,050
1
03/05/13 19:59
03/12/13 03:19
100-02-7
N-Nitrosodimethylamine
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:19
62-75-9
N-Nitroso-di-n-propylamine
ND mg1L
0,0050
1
03/05/13 19:59
03/12/13 03:19
621-64-7
N-Nitrosodiphenylamine
NO mg1L
0.010
1
03/05/13 19:59
03/12/13 03:19
86-30-6
Pentachlorophenol
NO mg/L
0.025
1
03105/13 19:59
03/12/13 03:19
87-86-5
Phenanthrene
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
85-01-8
Phenol
NO mg/L
0.0050
1
03/05/13 19:59
03/12/13 03:19
108-95-2
Pyrene
ND mg/L
0.0050
1
03/05/13 19:59
03/12/13 0319
129-00-0
1,2,4-Trichlorobenzene
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:19
120-82-1
2,4,6-Trichlarophenol
NO mg/L
0,010
1
03/06/13 19:59
03/12/13 03:19
88-06-2
Surrogates
Nitrobenzene-d5 (S)
42 %
10-120
1
03/05/13 19:59
03/12/13 03:19
4165-60-0
2-Fluorobiphenyl (S)
43 %
15-120
1
03105/13 19:59
03/12/13 03:19
321-60-8
Terphenyl-d 14 (S)
77 %
11-131
1
03105/1319:59
03112/1303:19
1718.51-0
Phenol-d6 (S)
24 %
10-120
1
03/05/13 19:59
03/12/13 03:19
13127-88-3
2-Fluorophenol (S)
36 %
10-120
1
03/05/13 19:59
03/12/13 03:19
367-12-4
2,4,6-Tribromophenol (S)
90 %
10-137
1
03/05/13 19:59
03/12/13 03:19
118-79-6
624 Volatile Organics
Analytical Method: EPA624
Benzene
NO mg1L
0.0050
1
03/09/13 02:50
71-43-2
Bromodichloromethane
NO mg/L
0,0050
1
03/09/13 02:50
75-27-4
Bromoform
NO mg/L
0.0050
1
03/09/13 02:50
75-25-2
Bromomethane
NO mg/L
0,010
1
03/09/13 02:50
74-83-9
Carbon tetrachloride
NO mg/L
0.0050
1
03/0911302:50
56-23-5
Chlorobenzene
NO mg/L
0,0050
1
03/013/13 02:50
108-90-7
Chloroethane
ND mg/L
0.010
1
03/09/13 02:50
75-00-3
Chloroform
ND mg/L
0.0050
1
03/09/13 02:50
67-66-3
Chloromethane
NO mg/L
0,0050
1
03/09/13 02:50
74-87-3
Dibromochloromethane
NO mg/L
0.0050
1
03/09/13 02:50
124-48-1
1,2-Dichlorobenzene
NO mg1L
0.0050
1
03/09/13 02:50
95-50-1
1,3-Dichlorobenzene
NO mg1L
0.0050
1
03/09/13 02:50
541-73-1
1,4-Dichlorobenzene
NO mg/L
0.0050
1
03/09/13 02:50
106-46-7
1,1-Dichloroethane
NO mg/L
0.0050
1
03/09/13 02:50
75-34-3
1,2-Dichloroethane
NO mg/L
0,0050
1
03/09/13 02:50
107-06-2
1,1-1)ichloroethene
NO mg/L
0.0050
1
03/09/13 02:50
75-35-4
cis-1,2-Dichloroethene
NO mg/L
0.0050
1
03/09/13 02:50
156-59-2
trans- 1,2-Dichloroethene
NO mg/L
0.0050
1
03/09/13 02:50
156-60-5
1,2-Dichloropropane
ND mg/L
0.0050
1
03/09/13 02:50
78-87-5
cis-1,3-Dichloropropene
ND mg/L
0,0050
1
0310911302:50
10061.01-5
trans-1.3-Dichloropropene
ND mg1L
0.0050
1
03/09/13 02:50
10061-02-6
Date: 03/20/2013 11:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 23

e
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
aceAnalytical
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave, Suite 100
awwpace+abs com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
ANALYTICAL RESULTS
Project: WO Testing 02/26/13
Pace Project No.: 92149470
Sample: OuNall 1
Lab ID: 92149470001 Collected: 02/26/13 13:40
Received: 02/27/13 14:40
Matrix: Water
Parameters
624 Volatile Organics
Elhylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroeth ane
1,1,2-Trichloroethane
Trichloroethene
Tdchlorofluoromethane
Vinyl chloride
Surrogates
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 624
NO mg1L
0.0050
1
03/09/13 02:50
100-41-4
NO mg1L
0.0050
1
03/09/13 02:50
75-09-2
NO mg1L
0.0050
1
03/09/13 02:50
79-34-5
ND mg1L
0.0050
1
03/09/13 02:50
127-18-4
ND mg1L
0.0050
1
03/09/13 02:50
108-88-3
ND mg/L
0.0050
1
03/09/13 02:50
71-55-6
NO mg1L
0.0050
1
03/09/13 02:50
79-00-5
NO mg/L
0.0050
1
03/09/13 02:50
79-01-6
NO mg1L
0,010
1
03/09/13 02:50
75-69-4
NO mg1L
0.0050
1
03/09/13 02:50
75-01-4
99 %
70-130
1
03/09/13 02:50
1868-53-7
95 %
70-130
1
03/09/13 02:50
460-00-4
102 %
70-130
1
03/09/13 02:50
2037-26-5
104 %
70-130
1
03/09/13 02:50
17060-07-0
Sample: Outf5ll'2 Lab ID: 92149470002 Collected: 02/26/13 14:00 Received: 02/27/13 14:40 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Total Suspended Solids
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
200.7 MET ICP
Copper
Lead
Zinc
625 MSSV
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)Ruoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
4-Bromophenylphenyl ether
Butylbenzylphtha late
4-Chloro-3-methyl phenol
bis(2-Chloroethoxy)metharie
bis(2-Chloroethyl) ether
Analytical Method: SM 2540D
ND mglL 2.5 1 03104/13 09:03
Analytical Method: EPA 1664E
NO mg/L 5.0 1 03/01/13 09:10
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
NO mg1L
0,0050
1
03/01/13 13:10 03/04/13 22:54
7440-50-8
NO mg1L
0.0050
1
03/01/13 13:10 03/04/13 22:54
7439-92-1
0.10.mg1L
0.010
1
03/01/13 13:10 03/04/13 22:54
7440-66-6
Analytical Method: EPA625
Preparation Method: EPA625
NO mg1L
0.0050
1
03/05/13 19:59 03/12/13 03:52
83-32-9
NO mg/L
0.0050
1
03/05/13 19:59 03/12/13 03:52
208-96-8
NO mg/L
0.0050
1
03/05/13 19:59 03/12/13 03:52
120-12-7
NO mg/L
0.0050
1
03/05/13 19:59 03/12/13 03:52
56-55-3
NO mg/L
0.0050
1
03/05/13 19:59 03/12/13 03:52
50-32-8
NO mg/L
0.0050
1
03/05/13 19:59 03/12/13 03:52
205-99-2
NO mg/L
0.0050
1
03/05/13 19:59 03/12/13 03:52
191-24-2
NO mg/L
0,0050
1
03/05/13 19:59 03/12/13 03:52
207-08-9
NO mg/L
0.0050
1
03/05/13 19:59 03/12/13 03:52
101-55-3
ND mglL
0.0050
1
03/05/13 19:59 03/12113 03:52
85-68-7
ND mglL
0.0050
1
03/05/13 19:59 03/12/13 03:52
59-50-7
NO mg1L
0,010
1
03/05/13 19:59 03/12/13 03:52
141-91-1
NO mg1L
0.0050
1
03/05/13 19:59 03/12113 03:52
111-44-4
Date: 03/20/2013 11:15 AM REPORT OF LABORATORY ANALYSIS Page 11 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc„

aceAnaljftal
www.pacelabs.com
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - SulteA
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunteraville, NC 28078
[phone]
Sample: OuHall 2 Lab ID: 92149470002 Collected: 02/26/13 14:00 Received: 02127113 14:40 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
625 MSSV Analytical Method: EPA625 Preparation Method: EPA625
bis(2-Chloroisopropyl) ether
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
108-60-1
2-Chloronaphthalene
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
91-58-7
2-Chlorophenot
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
95-57-8
4-Chlorophenylphenyl ether
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
7005-72-3
Chrysene
ND mg1L
0,0050
1
03105/13 19:59
03/12/13 03:52
218-01-9
Dibenz(a,h)anthracene
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
53-70-3
3,3'-Dichlorobenzidine
ND mglL
0.025
1
03/05/13 19:59
03/12/13 03:52
91-94-1
2,4-Dichlorophenol
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
120-83-2
Diethylphthalate
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
84-66-2
2,4-Dimethylphenol
ND mg1L
0,010
1
03/05/13 19:59
03/12/13 03:52
105-67-9
Dimethylphthalate
ND mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
131-11-3
Di-n-butylphthalate
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
84-74-2
4,6-Dinitro-2-methylphenol
NO mg1L
0.020
1
03/05/13 19:59
03/12/13 03:52
534-52-1
2,4-Dinitrophenol
ND mglL
0.050
1
03/05/13 19:59
03/12/13 03:52
51-28-5
2,4-Dinitrotoluene
ND mglL
0.0050
1
03/05/13 19:59
03/12/13 03:52
121-14-2
2,6-Dinitrotoluene
ND mglL
0.0050
1
03/05/13 19:59
03/12/13 03:52
606-20-2
Di-n-octylphth a late
ND mg11-
0,0050
1
03/05/13 19:59
03/12/13 03:52
117-84-0
bis(2-Ethylhexyl)phthalate
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
117-81-7
Fiuoranthene
NO mg1L
0,0050
1
03/05/13 19:59
03/12/13 03:52
206-44-0
Fluorene
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
86-73-7
Hexachloro-1,3-butadiene
ND mg1L
0,0050
1
03/05/13 19:59
03/12/13 03:52
87-68-3
Hexachlorobenzene
ND mglL
0,0050
1
03/05/13 19:59
03/12/13 03:52
118-74-1
Hexachlorocyclopentadiene
ND mglL
0.010
1
03/05/13 19:59
03/12/13 03:52
77-47-4
Hexachloroethane
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
67-72-1
Indeno(1,2,3-cd)pyrene
ND mglL
0.0050
1
03/05/13 19:59
03/12/13 03:52
193-39-5
Isophorone
ND mg1L
0.010
1
03/05/13 19:59
03/12/13 03:52
78-59-1
Naphthalene
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
91-20-3
Nitrobenzene
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
98-95-3
2-Nitrophenol
NO mg1L
0.0050
1
03/05113 19:59
03/12/13 03:52
88-75-5
4-Nitrophenol
NO mg1L
0.050
1
03/05/13 19:59
03/12/13 03:52
100-02-7
N-Nitrosodimethylamine
NO mg1L
0.0050
1
03/05/13 19:59
03/12/13 03:52
62-75-9
N-Nitroso-di-n-propylamine
NO mg1L
0.0050
1
03/05113 19:59
03/12/13 03:52
621-64-7
N-Nitrosodiphenylamine
NO mg1L
0,010
1
03/05/13 19:59
03/12/13 03:52
86-30-6
Pentachlorophenol
NO mglL
0.025
1
03/05/13 19:59
03/12/13 03:52
87-86-5
Phenanthrene
ND mglL
0.0050
1
03/05/13 19:59
0311211303:52
85-01-8
Phenol
NO mglL
0.0050
1
03/05/13 19:59
03/12/13 03:52
108-95-2
Pyrene
ND mglL
0.0050
1
03/05/13 19:59
03/12/13 03:52
129-00-0
1,2,4-Trichlorobenzene
ND mglL
0.0050
1
03/05/13 19:59
03/12/13 03:52
120-82-1
2,4,6-Trichlorophenol
ND mglL
0.010
1
03/05/13 19:59
03/12/13 03:52
88-06-2
Surrogates
Nitrobenzene-d5 (S)
48 %
10-120
1
03/05/13 19:59
03/12/13 03:52
4165-60-0
2-Fluorobiphenyl (S)
47 %
15-120
1
03/05/13 19:59
03/12/13 03:52
321-60-8
Terphenyl-d14(S)
83 %
11-131
1
0310511319:59
03/12/13 03:52
1718-51-0
Phenol-d6 (S)
15 %
10-120
1
03/05/13 19:59
03/12/13 03:52
13127-88-3
2-Fluorophenol (S)
28 %
10-120
1
03/05/13 19:59
03/12/13 03:52
367-12-4
2,4,6-Tribromopheriol (S)
63 %
10-137
1
03/05/13 19:59
03/12/13 03:52
118-79-6
Date: 03/20/2013 11:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 23

aceAnalXical
%%W P8oelabS' WM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Sample: Outfall 2 Lab ID; 92149470002 Collected: 02/26/13 14:00 Received: 02/27/13 14:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
624 Volatile Organics Analytical Method: EPA624
Benzene
ND mg1L
0.0050
1
03/09/13 03:06
71-43-2
Bromodichloromethane
ND mg1L
0.0050
1
03/09/13 03:06
75-27-4
Bromoform
ND mg/L
0.0050
1
03/09/13 03:06
75-25-2
Bromomethane
ND mg/L
0,010
1
03/09/13 03:06
74-83-9
Carbon tetrachloride
ND mg/L
0.0050
1
03/09/13 03:06
56-23-5
Chlorobenzene
ND mg/L
0.0050
1
03/09/13 03:06
108-90-7
Chloroethane
ND mg/L
0.010
1
03/09/13 03:06
75-00-3
Chloroform
ND mg1L
0.0050
1
03/09/13 03:06
67-66-3
Chloromethane
ND mg1L
0,0050
1
03/09/13 03:06
74-87-3
Dibromochloromethane
ND mg/L
0.0050
1
03/09/13 03:06
124-48-1
1,2-Dichlorobenzene
ND mg/L
0.0050
1
03/09/13 03:06
95-50-1
1,3-Dichlorobenzene
ND mg/L
0.0050
1
03/09/13 03:06
541-73-1
1,4-Dichlorobenzene
ND mg/L
0.0050
1
03/09/13 03:06
106-46-7
1,1-Dichloroethane
ND mg/L
0.0050
1
03/09/13 03:06
75-34-3
1,2-Dichloroethane
NO mg/L
0.0050
1
03/0911303:06
107-06-2
1,1-Dichloroethene
ND mg/L
0.0050
1
03/09/13 03:06
75-35-4
cis-1,2-Dichloroethene
ND mg1L
0.0050
1
03/09/13 03:06
156-59-2
trans-1,2-Dichloroethene
ND mg1L
0,0050
1
03/09/13 03:06
156-60-5
1,2-Dichloropropane
ND mg1L
0.0050
1
03/09/13 03:06
78-87-5
cis- 1,3-Dichloropropene
ND mg/L
0,0050
1
03/09/13 03:06
10061-01-5
trans-1,3-Dichloropropene
ND mg1L
0.0050
1
03/09/13 03:06
10061-0276
Ethylbenzene
ND mg/L
0,0050
1
03/09/13 03:06
100-41-4
Methylene Chloride
ND mg1L
0.0050
1
03/09/13 03:06
75-09-2
1,1,2,2-Tetrachloroethane
ND mg/L
0.0050
1
03/09/13 03:06
79-34-5
Tetrachloroethene
ND mg1L
0.0050
1
03/09/13 03:06
127-18-4
Toluene
ND mg/L
0.0050
1
03/09/13 03:06
108-88-3
1,1,1-Trichloroethane
ND mg1L
0.0050
1
0310911303:06
71-55-6
1,1,2-Trichloroethane
ND mg/L
0.0050
1
0310911303:06
79-00-5
Trichloroethene
ND mg1L
0.0050
1
03/09/13 03:06
79-01-6
Trichlorofluoromethane
ND mg1L
0,010
1
03/09/13 03:06
75-69-4
Vinyl chloride
ND mg1L
0.0050
1
03/09/13 03:06
75-01-4
Surrogates
Dibromocuoromethane (S)
100 %
70-130
1
03/09/13 03:06
1 B68-53-7
4-Bromofluorobenzene (S)
93 %
70-130
1
03/09/13 03.06
460-00-4
Toluene-d8 (S)
100 %
70-130
1
03/09/13 03:06
2037-26-5
1,2-Dichloroethane-d4 (S)
105 %
70-130
1
03/09/13 03:06
17060-07-0
Date: 03/20/2013 11:15 AM REPORT OF LABORATORY ANALYSIS Page 13 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

(�IaneAnalyfical
wwwpacelms.cwn
Project: WVV Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: EDEN/11112 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples. 92149470001. 92149470002
METHOD BLANK: 931736 Matrix: Water
Associated Lab Samples: 92149470001, 92149470002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 03/04/13 08:56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
931739
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250 228 91
80-120
SAMPLE DUPLICATE: 931740
92149410004 Dup
Parameter
Units
Result Result RPO
Qualifiers
Total Suspended Solids
mg/L
2700 2930
8 R1
SAMPLE DUPLICATE: 931741
Parameter
Total Suspended Solids
92149602001 Dup
Units Result Result
mg1L 192 250
RPD Qualifiers
26
Date: 03/20/2013 11:15 AM REPORT OF LABORATORY ANALYSIS Page 14 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

1�;a'ceAnalXical
wwwpacelabs.mn
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: GCSV/14059 Analysis Method: EPA 1664B
OC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples. 92149470001, 92149470002
METHOD BLANK: 930783 Matrix: Water
Associated Lab Samples: 92149470001, 92149470002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg1L ND 5.0 03/01/13 09:02
LABORATORY CONTROL SAMPLE: 930784
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 17.8
89
64-132
MATRIX SPIKE SAMPLE:
930785
92149488001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum hydrocarbons
mg/L
ND 20
17.5
87
64-132
Date: 03/20/2013 11:15 AM REPORT OF LABORATORY ANALYSIS Page 15 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

o Pace Analytical Services, Inc, Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr, 9800 Kincey Ave. Suite 100
_paoelalu can Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
(336)623-B921 [phone] [phone]
QUALITY CONTROL DATA
Project: WW Testing 02/26/13
Pace Project No.: 92149470
QC Batch: MPRP112723
Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92149470001, 92149470002
METHOD BLANK: 930720
Matrix: Water
Associated Lab Samples: 92149470001, 92149470002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Lead
mg/L
ND 0,0050
03/04/13 21:30
LABORATORY CONTROL SAMPLE:
930721
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits Qualifiers
Lead
mg1L
.5 0.49
98
85-115
MATRIX SPIKE SAMPLE:
930722
92149603001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Lead
mg1L
ND .5
0.50
99
70-130
MATRIX SPIKE SAMPLE:
930724
92149607001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Lead
mglL
ND .5
0.48
96
70-130
SAMPLE DUPLICATE: 930723
92149603002 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Lead
mg/L
ND ND
SAMPLE DUPLICATE: 930725
92149608001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Lead
mg1L
ND ND
Date: 03/20/2013 11:15 AM REPORT OF LABORATORY ANALYSIS Page 16 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
wwwpacelabs.com
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/22264 Analysis Method: EPA624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92149470001, 92149470002
METHOD BLANK: 935336
Associated Lab Samples:
Parameter
92149470001, 92149470002
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
11,1-Trichloroethane
mg1L
NO
0.0050
03109/13 00:37
1,1,2,2-Tetrachloroethane
mg1L
NO
0.0050
03/09/13 00:37
1,1,2-Trichloroethane
mg/L
NO
0.0050
03/0911300:37
1,1-Dichloroethane
mg/L
ND
0.0050
03/09/13 00:37
1,1-Dichloroethene
mglL
ND
0.0050
03/09/13 00:37
1,2-Dichlorobenzene
mg/L
NO
0.0050
03/09/13 00:37
1,2-Dichloroethane
mg/L
NO
0.0050
03/09/13 00:37
1,2-Dichloropropane
mg1L
ND
0.0050
03/09/13 00:37
1,3-Dichlorobenzene
mg1L
NO
0.0050
03/09/1300:37
1,4-Dichlorobenzene
mg/L
NO
0.0050
0310911300:37
Benzene
mg/L
NO
0.0050
03/09/13 00:37
Bromodichloromethane
mg/L
ND
0,0050
03/09/13 00:37
Sromoform
mg/L
NO
0.0050
03/09/13 00:37
Hromomethane
mg/L
NO
0.010
03/09113 00:37
Carbon tetrachloride
mg/L
NO
0.0050
03/09/13 00:37
Chlorobenzene
mg/L
NO
0.0050
03/09/13 00:37
Chloroethane
mg/L
NO
0.010
03/09/13 00:37
Chloroform
mg/L
ND
0.0050
03/09/13 00:37
Chloromethane
mg/L
NO
0.0050
03/09/13 00:37
cis-1,2-Dichloroethene
mg/L
NO
0.0050
03/09/13 00:37
cis- 1,3-Dichloropropene
mg/L
NO
0.0050
03/09/13 00:37
Dibromochloromethane
mg/L
ND
0,0050
03/09/13 00:37
Ethylbenzene
mg/L
NO
0,0050
03/09/13 00:37
Methylene Chloride
mg/L
ND
0,0050
03/09/13 00:37
Tetrachloroethene
mg/L
NO
0,0050
03/09/13 00:37
Toluene
mg/L
NO
0,0050
03109/13 00:37
trans-1,2-Dichloroethene
mg1L
NO
0.0050
03/09/13 00:37
trans-1,3-Dichloropropene
mg/L
NO
0,0050
03109/13 00:37
Trichloroethene
mg/L
NO
0.0050
03109/13 00:37
Tdchlorofluoromethane
mg/L
NO
0,010
03/09/13 00:37
Vinyl chloride
mg/L
NO
0,0050
03109/13 00:37
1,2-Dichloroethane-d4 (S)
%
105
70-130
03109/13 00:37
4-Bromofluorobenzene (S)
%
95
70-130
03/09/13 00:37
Dibromofluoromethane (S)
%
100
70-130
03109/13 00:37
Toluene-d8 (S)
%
100
70-130
03/09113 00:37
LABORATORY CONTROL SAMPLE: 935337
Spike LCS LCS
Parameter Units Conc. Result % Rec
1. 1. 1 -Trichloroethane mg/L .02 0.017
1,1,2,2-Tetrachloroethane mg1L .02 0.019
Date: 03/20/2013 11:15 AM
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
83 52-162
93 46-157
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, Inc„
Page 17 of 23

aceAnalytical
wwwpecalabs.=n
Project: WVV Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 935337
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,2-Trichloroethane
mg/L
.02
0,020
100
52-150
1,1-Dichloroethane
mg/L
.02
0.018
89
59-155
1,1-Dichloroethene
mg/L
.02
0.018
89
1-234
1,2-Dichlorobenzene
mg/L
02
0.019
97
18-190
1,2-Dichloroethane
mg1L
.02
0.018
90
49-155
1,2-Dichloropropane
mg1L
02
0.019
97
1-210
1,3-Dichlorobenzene
mg1L
.02
0.018
91
59-156
1,4-Dichlorobenzene
mg1L
.02
0.019
95
18-190
Benzene
mg/L
.02
0,018
89
37-151
Bromodichloro methane
mg/L
.02
0.018
89
35-155
Bromoform
mg/L
.02
0,017
83
45-169
Bromomethane
mg/L
.02
0.019
95
1-242
Carbon tetrachloride
mg/L
02
0.016
82
70-140
Chlorobenzene
mg/L
.02
0.018
91
37-160
Chloroethane
mg/L
.02
0,018
92
14-230
Chloroform
mg/L
.02
0.017
87
51-138
Chloromethane
mg/L
.02
0,015
75
1-273
cis-1,2-Dichloroethene
mg/L
.02
0,018
89
68-146
cis-1,3-Dichloropropene
mg/L
.02
0.019
95
1-227
Dibromochloromethane
mg/L
.02
0,018
92
53-149
Ethylbenzene
mg/L
.02
0.018
88
37-162
Methylene Chloride
mg/L
.02
0,023
114
1-221
Tetrachloroethene
mg/L
.02
0.017
87
64-148
Toluene
mg/L
.02
0,018
90
47-150
trans-1,2-Dichloroethene
mg/L
.02
0.019
94
54-156
trans-1,3-Dichloropropene
mg/L
.02
0,019
96
17-183
Trichloroethene
mg/L
.02
0.016
82
71-157
Trichlorofluoromethane
mg/L
.02
0.017
84
17-181
Vinyl chloride
mg[L
.02
0.013
65
1-251
1,2-Dichloroethane-d4 (S)
%
103
70-130
4-Bromofluorobenzene (S)
%
95
70-130
Dibromofluoromethane (S)
%
102
70-130
Toluene-d8 (S)
%
101
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Date: 03/20/2013 11:15AM REPORT OF LABORATORY ANALYSIS Page 18 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytrcal
www.pacabbs.mn
Project: VVW Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT121063 Analysis Method:
QC Batch Method: EPA 625 Analysis Description;
Associated Lab Samples: 92149470001, 92149470002
EPA 625
625 MSS
METHOD BLANK: 932988
Matrix: Water
Associated Lab Samples: 92149470001, 92149470002
Blank Reporting
Parameter
Units Result Limit
Analyzed
1,2,4-Trichlorobenzene
mg1L
ND
0.0050
03112/1301:43
2,4,6-Trichlorophenol
mg1L
ND
0.010
03/12/13 01:43
2,4-Dichlorophenol
mg1L
ND
0,0050
03/12/13 01:43
2,4-Dimethylphenol
mg/L
NO
0.010
03/12/13 01:43
2,4-Dinitrophenol
mg/L
NO
0,050
03/12/13 01:43
2,4-Dinitrotoluene
mg/L
NO
0.0050
03/12/13 01:43
2,6-Dinitrotoluene
mg1L
ND
0.0050
03/12/13 01:43
2-Chloronaphihalene
mg1L
NO
0.0050
03/12/13 01:43
2-Chlorophenol
mg1L
ND
0.0050
03/12/13 01:43
2-Nitrophenol
mg1L
ND
0.0050
03/12/13 01:43
3,3'-Dichlorobenzidine
mg/L.
ND
0.025
03/12/13 01:43
4,6-Dinitro-2-methylphenol
mg/L
NO
0.020
03/12/13 01:43
4-Bromophenylphenyl ether
mg/L
NO
0.0050
03/12/13 01:43
4-Chloro-3-methylphenol
mg/L
NO
0.0050
03/12/13 01:43
4-Chlarophenylphenyl ether
mg/L
NO
0.0050
03/12/13 01:43
4-Nitrophenol
mg1L
ND
0.050
03/12/13 01:43
Acenaphthene
mg1L
ND
0.0050
03/12/13 01:43
Acenaphthylene
mg/L
ND
0.0050
03/12/13 01:43
Anthracene
mg1L
ND
0.0050
03/12/13 01:43
Benzo(a)anthracene
mg1L
ND
0.0050
03/12/13 01A3
Benzo(a)pyrene
mg/L
NO
0.0050
03/12/13 01:43
Benzo(b)fluoranthene
mg/L
NO
0,0050
03/12/13 01:43
Benzo(g,h,i)perylene
mg1L
NO
0.0050
03/12/13 01:43
Benzo(k)fluoranthene
mg/L
NO
0,0050
03/12/13 01:43
bis(2-Chloroethoxy)methane
mg/L
NO
0.010
03/12/13 01:43
bis(2-Chloroethyl) ether
mg1L
ND
0.0050
03/12/13 01:43
bis(2-Chloroisopropyl) ether
mg1L
ND
0.0050
03/12/13 01:43
bis(2-Ethylhexyl)phthalate
mg1L
ND
0.0050
03112 I3 01:43
Butylbenzylphthalate
mg1L
ND
0.0050
03/12/13 01:43
Chrysene
mg/L
NO
0,0050
03/12/13 01:43
Di-n-butylphthalate
mg/L
NO
0.0050
03/12/13 01:43
Di-n-octylphthalate
mg/L
NO
0,0050
03112/13 01:43
Dibenz(a,h)anthracene
mg/L
NO
0,0050
03/12/13 01:43
Diethylphthalate
mg/L
NO
0.0050
03/12/13 01:43
Dimethylphthalate
mg/L
NO
0,0050
03112/13 01:43
Fluoranthene
mg/L
NO
0.0050
03/12/13 01:43
Fluorene
mg/L
NO
0.0050
03/12/13 01:43
Hexachloro-1,3-butadiene
mg/L
NO
0.0050
03/12/13 01:43
Hexachlorobenzene
mg1L
ND
0.0050
03/12/13 01A3
Hexachlorocyclopentadiene
mg1L
ND
0.010
03/12/13 01A3
Hexachloroethane
mg1L
ND
0.0050
03/12/13 01:43
Indeno(1,2,3-cd)pyrene
mg/L
ND
0.0050
03/12/13 01:43
Isophorone
mg1L
ND
0.010
03/12/13 01A3
Date: 03/2012013 11:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc..
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 23

aceAnalytical
www.pec.Webs.com
Project: 1hM! Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-B921
Pace Ana lytIcaI Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
METHOD BLANK: 932988
Matrix: Water
Associated Lab Samples:
92149470001, 92149470002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
N-Nitroso-di-n-propylamine
mg/L
NO
0.0050
03/12/13 01:43
N-Nitrosodimethyla mine
mg/L
NO
0.0050
03/12/13 01:43
N-Nitrosodiphenylamine
mg/L
NO
0.010
03/12/13 01:43
Naphthalene
mg/L
NO
0.0050
03/12/13 01:43
Nitrobenzene
mg1L
ND
0.0050
03/12/13 01:43
Pentachlorophenol
mg1L
ND
0.025
03/12/13 01:43
Phenanthrene
mg1L
ND
0.0050
03/12/13 01:43
Phenol
mg/L
NO
0.0050
03112/13 01:43
Pyrene
mg/L
NO
0.0050
03/12/13 01:43
2,4,6-Tribromophenol (S)
%
95
10-137
03/12/13 01:43
2-Fluorobiphenyl (S)
%
71
15-120
03/12/13 01:43
2-Fluorophenol (S)
%
49
10-120
03/12/13 01:43
Nitrobenzene-d5 (S)
%
71
10-120
03/12/13 01:43
Phenol-d6 (S)
%
29
10-120
03/12/13 01:43
Terphenyl-d14 (S)
%
100
11-131
03/12/13 01:43
LAE30RATORY CONTROL SAMPLE 8 LCSD: 932989
932990
Spike
LCS
LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD
RPD Qualifiers
1,2,4-Trichlorobenzene
mg/L
.05
0.026
0.028
52 56
44-142
7
30
2,4,6-Trichlorophenol
mg1L
.05
0.034
0,042
67 83
37-144
21
30
2,4-Dichlorophenol
mg/L
.05
0.030
0,036
61 72
1-191
17
30
2,4-Dimethylphenol
mg1L
.05
0,030
0,036
60 71
32-119
17
30
2,4-Dinitrophenol
mg/L
.25
0.23
0.24
90 96
1-181
6
30
2,4-Dinitrotoluene
mg/L
.05
0,039
0.043
78 86
39-139
9
30
2,6-Dinitrotoluene
mg/L
.05
0.034
0.038
68 76
50-158
12
30
2-Chioronaphthalene
mg/L
.05
0.031
0.035
62 70
60-118
12
30
2-Chlorophenol
mg/L
.05
0.029
0.035
58 69
23-134
18
30
2-Nitrophenol
mg/L
.05
0.031
0.038
62 77
29-182
21
30
3,T-Dichlorobenzidine
mg/L
1
0.085
0.093
85 93
1-262.
9
30
4,6-Dinitro-2-methylphenol
mg/L
.1
0,095
0,10
95 101
1-181
6
30
4-Bromophenylphenyl ether
mg/L
.05
0.039
0.044
78 89
53-127
13
30
4-Chloro-3-methylphenol
mg/L
.1
0,079
0.093
79 93
22-147
16
30
4-Chlorophenylphenyl ether
mg/L
.05
0.036
0.043
73 86
25-158
16
30
4-Nitrophenol
mg/L
.25
0,19
0.21
76 85
1-132
12
30
Acenaphthene
mg/L
.05
0.036
0.041
71 83
47-145
15
30
Acenaphthylene
mg/L
.05
0.034
0.040
69 81
33-145
16
30
Anthracene
mg1L
.05
0.042
0.046
85 92
1-166
8
30
Benzo(a)anthrace ne
mg/L
.05
0.045
0.048
91 96
33-143
6
30
Benzo(a)pyrene
mg/L
.05
0.047
0.050
93 100
17-163
7
30
Benzo(b)fluoranthene
mg/L
.05
0,045
0.048
89 96
24-159
7
30
Benzo(g,h,i)perylene
mg/L
.05
0.047
0.050
94 100
1-219
6
30
Benzo(k)fluoranthene
mg/L
.05
0.043
0.045
86 91
11-162
5
30
bis(2-Chloroethoxy)methane
mg/L
.05
0.027
0.032
55 65
33-184
17
30
bis(2-Chloroethyl) ether
mg/L
.05
0.028
0.034
55 67
12-158
20
30
Hate: 03/20/2013 11:15 AM REPORT OF LABORATORY ANALYSIS Page 20 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

1-158ceAnalytical"
WW1V.p8Cfil8bS.QD.m
Project: WW Testing 02/26/13
Pace Project No.: 92149470
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE & LCSD; 932989
Parameter Units
Spike
Cone.
bis(2-Chloroisopropyl) ether
mg1L
.05
bis(2-Ethylhexyl)phthalate
mg1L
.05
Butylbenzylphtha late
mg1L
.05
Chrysene
mg1L
.05
Di-n-butylphthalate
mg1L
.05
Di-n-octylphthalate
mg1L
.05
Dibenz(a,h)anthracene
mg/L
.05
Diethylphtha late
mg1L
.05
Dimethylphthalate
mg1L
.05
Fluoranthene
mg1L
.05
Fluorene
mg1L
.05
Hexachloro-1,3-butadiene
mg1L
.05
Hexachlorobenzene
mg1L
.05
Hexachlorocyciopentadiene
mg1L
.05
Hexachloroethane
mg1L
.05
Indeno(1,2,3-cd)pyrene
mg1L
.05
Isophorone
mg1L
.05
N-Nitroso-di-n-propylamine
mg1L
.05
N-Nitrosodimethylamine
mg1L
.05
N-Nitrosodiphenylamine
mg/L
.05
Naphthalene
mg1L
.05
Nitrobenzene
mg1L
.05
Pentachlorophenol
mg1L
.1
Phenanthrene
mg1L
.05
Phenol
mg1L
.05
Pyrene
mg1L
.05
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl(S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
[phone]
932990
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD
0.019
0,023
38
46
36-166
21
30
0,042
0.045
83
90
8-158
7
30
0.040
0,043
80
87
1-152
8
30
0.045
0.048
90
95
17-168
6
30
0.041
0.044
81
87
1-118
7
30
0.045
0.049
90
98
4-146
9
30
0.047
0.050
93
100
1-227
7
30
0.040
0.045
81
89
1.114
10
30
0,037
0,042
75
84
1-112
12
30
0,048
0.051
97
102
26-137
5
30
0.039
0.045
77
89
59-121
15
30
0,025
0.026
49
51
24-116
4
30
0,041
0.045
82
90
1-152
9
30
0,023
0.026
47
52
25-150
11
30
0.021
0.023
42
46
40-113
8
30
0.047
0.050
95
100
1-171
5
30
0,027
0.033
53
65
21-196
20
30
0.034
0.041
68
81
1-230
18
30
0,019
0,023
38
46
25-150
19
30
0.039
0.043
77
87
25-150
11
30
0,029
0,033
58
66
21-133
13
30
0.025
0.030
50
59
35-180
17
30
0.078
0.088
78
88
14-176
12
30
0.041
0.044
82
88
54-120
7
30
0.017
0.020
34
41
5-112
18
30
0.043
0,046
86
92
52-115
7
30
105
115
10-137
63
74
15-120
40
48
10-120
61
73
10-120
26
33
10-120
93
92
11-131
Qualifiers
Date: 03/2012013 11:15 AM REPORT OF LABORATORY ANALYSIS Page 21 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
wwwpacelahs.com
Project: WW Testing 02/26/13
Pace Project No.: 92149470
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunters0e, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 fisted analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyt ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
R1 RPD value was outside control limits.
�FIi�[rklE���7F�I�7rRifRN�L�.I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 22 of 23

aceAnalytical
W*Wpacdabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: VWV Testing 02/26/13
Pace Project No.: 92149470
Lab ID Sample ID QC Batch Method
92149470001
Outfall 1
SM 2540D
92149470002
Outfall 2
SM 2540D
92149470001
Outfall 1
EPA 1664B
92149470002
Outfall 2
EPA 1664E
92149470001
Outfall 1
EPA 200.7
92149470002
Outfall 2
EPA 200.7
92149470001
Outfall 1
EPA625
S2149470002
Outfall 2
EPA625
92149470001
Outfall 1
EPA 624
92149470002
Outfall 2
EPA 624
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
QC Batch
Analytical Method
Batch
EDENl11112
EDEN111112
GCSV114059
GCSV114059
MPRP112723
EPA 200.7
ICP111606
MPRP112723
EPA 200.7
ICP111606
OEXT121063
EPA 625
MSSW7459
OEXTY21063
EPA625
MSSVf7459
MSV122264
MSV122264
Date: 03120/2013 11:15 AM REPORT OF LABORATORY ANALYSIS Page 23 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Sectim A SOC&M 8
RoquIred Cben2 Itch mwAOM RsquiNW urged kft..tzam
[Add�t ICCvv TIX
CHAIN -OF -CUSTODY I Analytical Request Document
Thy ChakK*Q�odyi3aLEC,ALDOCUMENT. All reWiaMfields must b000n*elnda=r*ety
Pau-
Ate 160�01
7, -.714 7-T -
Section 0 Ma b codes
pAWA-dCkrrIhkMmGM
DrbWng W2W DW
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COLLECTED
%whber WT
COMPOSM
wasu waterWW
Product P
COkVKW%
CrAff
r9AYSOM SL
8
SAMPLE ID 01 OL
40 .
Wpo WP
(A-7- 0-9 0 e) Air AR
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7
SavOe Da MUST BE UNDUE -Tkmm TS
0
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O%ff GT
C5
Z
S
0
DATE
TIME
OAIE
TNRP
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0
G-RIG'tf,,jAL DE
SIGNATURE OSAMPff�Q. V
,d
F-ALL-0-
CC*MHXNS

w
Semi-annual Stormwater Discharge Monhoring Re art
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted L"
CERTIFICATE OF COVERAGE NO. NCG03 Q
FACILITY NAME A�.f 1 - �a Ln c .
COUNTY r3
PERSON COLLECTING SAMPLES
LABORATORY PJO-i-- �), i� _ Lab Cert. #
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTIO YEAR L 3 _
SAMPLE PERIOD [Z.lan-June ❑ July -Dec
or ❑ Monthly' (month J
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
[;�Q her '
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
No dischorge this period?z
Outfall No.
Date Sample
,
Collected
(mo/dd/yr)
24-hour rainfall
amount,
inches
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
s
Organlcs
Benchmarks
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
1 mg/L
n
` 7
!
I Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the- requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-24S, last revised 10/25/2012
Paee 1 of 3

Facitities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certiNond the requirement=for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed.in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. i further certify that this facility is implementing the all the provisions of the
solvent management plan included in the stormwater Pollution Prevention Plan."
2ac)inq,q —WILL
Name (Print ame)
En►)i, r Dnm . a(117/16 r
Title (Print title)
/3 /13
(Signs ure) Date
Note: Results must be reported In numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mall", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General permit text.
Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar O&G/TPH by
EPA 1i664 (SGf--HEM)
Total Su+�lnded Solids
pH
8enchmar*3 --_>
_
-
15 mg/L
100 mg/tor 50 mg/L•
16.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART Ii SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, includina all "No Discharae" reports, within 30 days of receiat of the lab results (or at end ofmonitorina period
in the case of "No Discharge" reports) ta:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
Permit Date:111112012-1013112017
SWU-245, last revised 10/25/2012
Page 3 of 3

aceARalytical.
f www.pacalabsxam
I
June 17, 2013
Ms. Sonya Walsh
ACCU FAB
801 Beacon Lake Dr.
Raleigh, NC 27610
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 2728E
[phone]
RE: Project: Special Zinc
Pace Project No.: 92160935
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Ms. Walsh:
Enclosed are the analytical results for sample(s) received by the laboratory on June 10, 2013. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page
[e-mail]
Project Manager
Enclosures
PCCRA-
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnalytical
wwwpacefabs.corn
Project: Special Zinc
Pace Project No.: 92160935
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden. NC 2728B
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida[NELAP Certification #: E87648
Massachusetts Certification #; M-NC030
North Carolina Drinking Water Certification #: 37712
[phone]
Pace Analytical Services, Inc.
2225 Riverside dr.
Asheville, NO 28804
CERTIFICATIONS
[phone]
North Carolina Wastewater Certification #: 40
South Carolina Certification #; 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #; 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NO 28078
[phone]
This report shall not be reproduced, except in fait,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 10

aceAnalytical
wwwpocelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 272BB
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
{828)254-7176
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Special Zinc
Pace Project No.: 92160935
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92160935001 Old Roof Top EPA 200.7 JMW 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in futl,
without the written consent of Pace Analytical Services, Inc,. Page 3 of 10

aceAnalytical
wwwpocalabs.com
Project: Special Zinc
Pace Project No.: 92160935
Method: EPA 200.7
Description: 200.7 MET ICP
Client: ACCU FAB
Date: June 17, 2013
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments. -
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of pace Analytical Services, Inc.. Page 4 of 10

PacoAnalytical Services,
Paco Analytical
PaceAnalyticalServices, Inc.
aeAnalyical
25East Meadow Rod- Suite
i
2225 Riverside Dr.
9800 KiiceyAve. Suite 100
wwwpacelabs.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
ANALYTICAL RESULTS
Project: Special Zinc
Pace Project No.: 92160935
Sample -Old-Roof) Lab ID: 92160935001 Collected: 06/07/13 08:37 Received: 06/10/13 13:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 0.1 f-Mg- 0.010 1 06/12/13 17:15 06/13/13 23:27 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 0611712013 08:51 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

aceAnalXical
wwwpaceiabs.com
Project: Special Zinc
Pace Project No.: 92160935
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: MPRP113535 Analysis Method: EPA200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92160935001
METHOD BLANK: 991365
Associated Lab Samples: 92160935001
Parameter Units
mg1L
Zinc
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.010 06/13/13 22:36
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 991366
Spike
LCS
LCS
% Rec
Parameter Units
Conc.
Result
% Rec
Limits Qualifiers
Zinc mg/L
.5
0.50
99
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 991367
991368
MS
MSD
92160737001
Spike
Spike MS
MSD
MS MSD % Rec
Parameter Units Result
Conc.
Conc. Result
Result
% Rec % Rec Limits RPD Qual
Zinc mg/L 0.064
.5
.5 0.56
0.55
99 97 70-130 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 991369 991370
MS MSD
92160951001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Zinc mg/L 0.073 .5 .5 0.57 0.57 100 100 70-130 0
Date: 06/17/2013 08:51 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 10

550AnalXical
www.pacefabs.com
Project: Special Zinc
Pace Project No.: 92160935
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Ashevilie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
INC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chforoethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TIN - The NE LAC Institute.
Ind=PI.�`ial:7I��
PASI-A Pace Analytical Services -Asheville
REPORT OF LABORATORY ANALYSIS
[phone]
This report shall not be reproduced, except in full,
Date: 06/17/2013 08:51 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

aceAnaJytical
W*W p8oWabk$' Wm
Project: Special Zinc
Pace Project NO„ 92160935
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92160935001 Old Roof Top EPA 200.7 MPRPI13535 EPA 200.7 ICP112330
Date: 06/17/2013 08:51 AM
REPORT OF LABORATORY ANALYSIS
This report shall not t)e reproduced, except in full,
without the written consent of Pace Analybcal Services, Inc..
Page 8 of 10

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Page 10 of 10

���
NCDENR
North Carolina Department of Environment and Natural Resources
Beverly Eaves Perdue
Governor
Gregory Page
Accu Fab Inc
801 Beacon Lake Dr
Raleigh, NC 27610
Dear Permittee:
Division of Water Quality
Charles Wakild, P. E.
Director
December 4, 2012
Dee Freeman
Secretary
Subject: NPDES Stormwater Permit Coverage Renewal
Accu Fab Incorporated
COC Number NCG030436
Wake County
In response to your renewal application for continued coverage under stormwater General Permit NCG030000
the Division of Water Quality (DWQ) is forwarding herewith the reissued General Permit. This permit is
reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of
Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October
15, 2007 (or as subsequently amended).
The following information is included with your permit package:
• A new Certificate of Coverage (COC)
• A copy of General Permit NCG030000
• A copy of the Technical Bulletin for the General Permit
• Two copies of the Discharge Monitoring Report (DMR) Form
• Two copies of the Qualitative Monitoring Report Form
The General Permit authorizes discharges of stormwater, and it specifies your obligations for discharge
controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself
with all the changes in the reissued permit. Your facility has six (6) months from the time of receipt of the
permit to update your current SPPP to reflect all new permit requirements.
The first sample period of your permit begins January 1, 2013. Your facility must sample a "measureable
storm event" beginning during the periods beginning January 1 and July 1 of every year (or, if applicable,
report "No Flow," as outlined in Part III, Section E). Also, please note that Tier 3 Actions in Part II of your
permit are triggered by benchmark exceedances on four occasions beginning on the effective date of this
permit and do not count prior exceedances.
The more significant changes in the General Permit since your last COC was issued are noted either in the
Draft Permit Fact Sheet that accompanied the public notice (http:I/portal.ncdenr.org/web/wq/ws/su/current-
notices), or in the Response to Comments / Summary of Changes and Technical Bulletin documents that are
posted on the Stormwater Permitting Unit's website with the new General Permit. Please visit
http://Portal.ncdenr.org/web/wQ/ws/su/npdessw (click on 'General Permits' tab) to review that information
for your specific General Permit carefully.
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Raleigh, North Carolina 27604
Phone: [phone] FAX: 919$07•t•492
Internet vn,,w ncwaterquality.oro
An Equal Op�rorienily 1 AYrmative Action Er -'oyar
One
NorthCarclina
NaturalZil

Gregory Page
December 4, 2012
Page 2 of 2
Some of the changes include:
Part II:
• Section A: The Stormwater Pollution Prevention Plan (SPPP) section, if applicable, has been updated
to the most current language of our permits. Additional conditions for specific industry sectors have
been added to the SPPP requirements in some cases.
• Sections B, C: Failure to perform analytical stormwater monitoring may result in the Division requiring
that the permittee begin a monthly sampling scheme.
• Sections B, C. A lower TSS benchmark of 50 mg/I for HQW, ORW, PNA and Tr Waters applies to these
more sensitive waters.
• Sections 8, C: The monitoring parameter Oil & Grease (O&G) has been replaced by the parameter
Total Petroleum Hydrocarbons (TPH) for vehicle maintenance areas, and in some cases, other
analytical monitoring requirements.
• Sections B, C, D: Inability to sample due to adverse weather must be recorded in the SPPP, or in
separate on -site records if your General Permit does not require an SPPP. Adverse weather is defined
in the "Definitions" section of the permit.
• Sections B, C: The term "Representative Storm Event" has been replaced by "Measurable Storm
Event." A measurable storm event is defined in the permit.
• Section D: If the permittee fails to respond effectively to problems identified by qualitative
monitoring, DWQ may require the permittee to perform corrective action.
Please review Parts III and IV to understand the Standard Conditions of your new NPDES General Permit,
including Compliance and Liability, Reporting, Monitoring and Records requirements; Operation and
Maintenance obligations; and Definitions. Please note that all samples analyzed in accordance with the terms
of this permit must be submitted to the Division on Discharge Monitoring Report (DMR) forms available on
the Stormwater Permitting Unit's website above. DMR forms must be delivered to the Division no later than
30 days from the date the facility receives the sampling results from the laboratory. Aiso note that existing
permittees do not need to submit a renewal request prior to expiration unless directed by the Division.
Your coverage under the General Permit is transferable only through the specific action of DWQ. This permit
does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it
relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law,
rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit
package, please contact the Division's Stormwater Permitting Unit at [phone].
Sincerely,`
for Charles Wakild, P.E.
cc: DWQ Central Files
Stormwater Permitting Unit Files
Raleigh Regional Office

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030436
STORM WATER
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Accu Fab Inc
is hereby authorized to discharge stormwater from a facility located at:
Accu Fab Incorporated
801 Beacon Lake Dr
Raleigh
Wake County
to receiving waters designated as Crabtree Creek, a class QNSW waterbody in the Neuse River
Basin in accordance with the effluent limitations, monitoring requirements, and other
conditions set forth in Parts I, 11, 111, and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective December 4, 2012.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this 41h day of December, 2012.
�"-'t' (� / tde""V'?
for Charles Wakild, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

MCH30436
00%*
two
4 m=A
ACLU-FAB� INN. s
August 13, 2007
SW General Permit Coverage Renewal
Stormwater Permitting Unit
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
To Whom It May Concern:
ACCU-FAB, INC.
801 BEACON LAKE DR.. RALEIGH, NC 27610-1377
[phone] • FAX [phone]
www.aQcufabno.com 1 salesPaccufabnc.com
This letter is in reference to Permit# NCG 030000, which became effective on
September. 1, 2002 and shall expire at midnight on August 31, 2007. Accu-Fab Inc. mailed
a renewal application on January 30, 2007, to SW General Permit Coverage Renewal. To
date, we have no knowledge of receipt or any dialogue assuring that Accu-Fab, Inc. will
be issued a new permit. We have left several messages with your office personal
requesting information on the permit application and we have had no response; therefore,
we will assume that if we have not received any information by the end of Accu-Fab's
current permit expiration date of August 31, 2007, midnight that the current permit will
remain effective until the new permit is obtained.
If you have any questions, please notify me via
E-mail: swalsh c,accufabnc.com
Phone: [phone] ext. 155
Sincerely,
U
Sonya Walsh
Enviro mental Safety Manager
egg Page
President
4n IRn 9001-2000 C.Prtifpd Cmmnanv

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P,E., Director
Division of Water Quality
August 23, 2002
GREGORY W PAGE
ACCU FAB INCORPORATED
801 BEACON LAKE DRIVE.
RALEIGH, NC 276101377
Subject: NPDE-S Stormwater Permit Renewal
ACCU FAB INCORPORATED
COC Number NCG030436
Wake County
Dear Permittee:
In response to your renewal application for continued coverage under general permit NCG030000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued Stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandurn of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983.
The Following information is included with your permit package:
* A new Certificate of Coverage
* A copy of General Stormwater Permit NCG030000
* A copy of the Analytical Monitoring Form (DMR)
* A copy of a Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or,
decree.
If you have any questions regarding this permit package please contact Bill Mills of the Central Office Stormwater
and General Permits Unit at [phone]. ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Stormwater & General Permits Unit files
Raleigh Regional Office
eMADE NCNR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030436
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
ACLU FFAB INC
is hereby authorized to discharge stormwater from a facility located at
ACLU FAB INCORPORATED
801 BEACON LAKE DRIVE
RALEIGH
WAKE COUNTY
to receiving waters designated as Crabtree Creek, a class C NSW stream, in the Neuse River Basin in accordance
with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, I1, Ill, IV, V, and VI
of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective September 1, 2002.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day August 23, 2002.
for Alan W. Klimek, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
• � „�irni, ID.
Gregory J. Thorpe, Ph.D.
Acting Director
Division of Water Quality
December 27, 2001
GREGORY W PAGE
ACCU FAB INCORPORATED
801 BEACON LAKE DR
RALEIGH, NC 27610
Sub_ ect: NPDES Stormwater Permit Renewal
ACCU FAB INCORPORATED
COC Number NCG030436
Wake County
Dear Permittee:
Your facility is currently covered for stormwater discharge under General Permit NCG030000. This permit expires
on August 31, 2002. The Division staff is currently in the process of rewriting this permit and is scheduled to have
the permit reissued by late summer of 2002. Once the permit is reissued, your facility would be eligible for
continued coverage under the reissued permit.
In order to assure your continued coverage under the general permit, you must apply to the Division of Water
Quality (DWQ) for renewal of your permit coverage. To make this renewal process easier, we are informing you in
advance that your permit will be expiring. Enclosed you will find a General Permit Coverage Renewal
Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued
coverage under the general permit.
Failure to request renewal within this time period may result in a civil assessment of at least $250.00. Larger
penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility
without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and
could result in assessments of civil penalties of up to $10,000 per day.
Please note that recent federal legislation has extended the "no exposure exclusion" to all operators of industrial
facilities in any of the I I categories of "storm water discharges associated with industrial activity," (except
construction activities). If you feel your facility can certify a condition of "no exposure", i.e. the facilty industrial
materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional
information contact the Central Office Stormwater Staff member listed below or check the stormwater & General
Permits Unit Web Site at htipaHh2o.enr.state.nc.us/su/stortttwatcr.hlmI
If the Subject stormwater discharge to waters of the state has been terminated, please complete the enclosed
Rescission Request Form. Mailing instructions arc listed on the bottom of the form. You will be notified when the
rescission process has been completed.
If you have any questions regarding the permit renewal procedures please contact Joe Albiston of the Raleigh
Regional Office at 919-571-4700 or Bill Mills of the Central Office Stormwater Unit at [phone], ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Raleigh Regional Office
e��
NCDENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1- 800-623-7748

r
State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
Kerr T. Stevens, Director
Mr. Gregory W. Page
ACCU-FAB, Inc.
7513 Hwy 64
Knightdale, North Carolina 27545
Dear Mr. Page:
LT.X;WA
NCDENR
March 19, 1999
Subject: General Permit No. NCG030000
ACCU-FAB, Inc.
COC NCG030436
Wake County
In accordance with your application for discharge permit received on March 3, 1999, we are forwarding
herewith the subject certificate of coverage to discharge under the subject state - NPDES general permit. This
permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum
of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable
to you, you have the right to request an individual permit by submitting an individual permit application. Unless
such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division of
Water Quality. The Division of Water Quality may require modification or revocation and reissuance of the
certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act
or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contactAisha Lau at telephone number 919/733-
5083 ext. 578.
Sincerely,
ORIGINAL, SIGNED BY
WILLIAkI > : _ -�AiLLS
Kerr T. Stevens
cc: Raleigh Regional Office
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030436
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Gregory W. Page, Robert J. Karbas, and Craven B. Page
are hereby authorized to discharge stormwater from a facility located at
ACCU-FAB, INC.
725 Beacon Lake Drive
Raleigh
Wake County
to receiving waters designated as Crabtree Creek, a class C NSW stream in the Neuse River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, II, 111,
IV, V and VI of General Permit No. NCG030000 as attached.
This Certificate of Coverage shall become effective March 19, 1999.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day March 19, 1999.
ORIGINAL SIGNED BY
WILLIAM C. MILLS
Kerr T. Stevens, Director
Division of Water Quality
By Authority of the Environmental Management Commission

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Environmental Safety and Health Manager
19 dri-a .y,a, a.
Sonya Walsh
Safety/Planning Manager
www.accufabnc.com
9 19-212-6400 x 155
919-215-3244 Cell
919-212-2333 Fax
O6 1 IRrt /*�**C?4AHof 2r
AAdL'
1=LPFAB, INC
CONTRACT MANUFACYURMAG

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030436
STORMWATER
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Accu Fab Inc
is hereby authorized to discharge stormwater from a facility located at:
Accu Fab Incorporated
801 Beacon Lake Dr
Raleigh
Wake County
to receiving waters designated as Crabtree Creek, a class C;NSW waterbody in the Neuse River'
Basin in accordance with the effluent limitations, monitoring requirements, and other
conditions set forth in Parts 1, 11, 111, and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective December 4, 2012.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this 41h day of December, 2012.
for Charles Wakild, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

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SITE ADDRESS
SM BTEACP4 LAKE DRIVE
RALEIWI, NC 27610
NSKA OTT LIMITS
YES
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ACLU-FAB. INC
SM RIEACON LAKE DR
RAUEIGK NC 27610
i19-2T2-alOD OFFICE
019-212-2333 FAX
TOTAL. LAND AREA
11165 AC
MAP REFERENCE
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rATERSNED
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NO -I
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PROPOSED USE
WANCHOUSE
pTW 1-Yf Ax1�
EXISTING wARfHOuSE
M570 SF
PROPOSED EXPANSION
21,600 SF
TOTAL BUILIKNG AREA
(EASTNG AND PROPOSED)
75,170 SF
BLIlDINO LOT COVERAGE
16.= (TOTAL OLD OUT)
FLOOR AREA RATIO
16.3Z (TOTAL OLD OUT)
BUILDING SETBACKS
FRONT 5W
SIDE 20' (40' AC
REAR 5D' (100 . F}R)
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BUILDING HEIGHT
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EIOSTTNG', 24'
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AREA
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NET CHANGE N NOERN40US
31.67E (TOTAL BLD OJT)
TOTAL VSA
(EMSTINC AND PROPOSED)
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THE SMFT OF MAXWJW EiFt YMENT PLUS ONE (1) SPACE
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59 SPACES PROVIDED
(NCL 4 HQ
SURVEY INFORMATION BY'
NEWCOMB LAND SURVEYORS
ALL CDNSTITJCTION CONFORM
TO CITY of RALEIGH STANDARDS AND
En,uT SPFaNS
FINAL PLAN - RELEASED FOR CONSTRUCTION
t 044-0/ rEv� PER CITY OF RALSOH tar F�rEW
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Phony: 919-847-8J00
244 W Millbrook Rood, ROle/gh, NC 276C9 Fox: 919-847-21JO
P. 0. Bnr 17705, 9oie.gA, NC 27619 E-m&k D/lrceod-e-mc-cam
LATEST FEVB1p/1 DATE p7-tiB-D7
�oACT NO 07-a

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
0E \NAT '
UJ 7
GREGORY W PAGE
ACCU FAB INCORPORATED
801 BEACON LAKE DRIVE
RALEIGH, NC 276101377
Dear Permittee:
Alan W. Klimek, P.E., Director
Division of Water Quality
August 23, 2002
Subject: NPDES Stormwater Permit Renewal
ACCU FAB INCORPORATED
COC Number NCG030436
Wake County
In response to your renewal application for continued coverage under general permit NCG030000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued Stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983.
The following information is included with your permit package:
* A new Certificate of Coverage
* A copy of General Stormwater Permit NCG030000
* A copy of the Analytical Monitoring Form (DMR)
* A copy of a Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or
decree.
If you have any questions regarding this permit package please contact Bill Mills of the Central Office Stormwater
and General Permits Unit at [phone], ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Stormwater & General Permits Unit Files
Raleigh Regional Office
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone]
'A
NCDENR
Customer Service
1-800-623-7748

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Gregory J. Thorpe, Ph.D.
Acting Director
Division of Water Quality
December 27, 2001
GREGORY W PACE
ACCU FAB INCORPORATED
801 BEACON LAKE DR
RALEIGH, NC 27610
Subject: NPDES Stormwater Permit Renewal
ACCU FAB INCORPORATED
COC Nunihcr NCG030436
Wake County
Dear Permittee:
Your Facility is currently covered for stormwater discharge under General Permit NCG030000. This perinit expires
on August 31, 2002, The Division staff is currently in the process of rewriting this pertnit and is scheduled to have
the permit reissued by late summer of 2002, Once the permit is reissued, your facility would be eligible for
continued coverage under the reissued permit.
In order to assure your continued coverage under the general permit, you must apply to the Division of Water
Quality (DWQ) for renewal of your pertnit coverage. To make this renewal process easier, we are informing you in
advance that your permit will be expiring. Enclosed you will Find a General Permit Coverage Renewal
Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued
coverage under the general permit.
Failure to request renewal within this time period may result in a civil assessment of at least $250.00. Larger
penalties may be assessed depending on the delinquency of the request. Discharge of'stormwater from your facility
without coverage under a valid stormwater NPDIvS permit would constitute a violation of NCGS 143-215.1 and
could result in assessments of civil penalties of up to $10,000 per day.
Please note that recent federal legislation has extended the "no exposure exclusion" to all operators of industrial
facilities in any of the 1 I categories of "storm water discharges associated with industrial activity," (except
construction activities). If you feel your facility can certify a condition of "no exposure", i.e. the facilty industrial
materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional
information contact the Central Office Stormwater Staff member listed below or check the Stormwater & General
Permits Unit Web Site at http://h2o,enr.state.nc.trs/su/Stortnwatet-.litml
If the subject stormwater discharge to waters of the state has been terminated, please complete the enclosed
Rescission Request Form. Mailing instructions are listed on the bottom of the form. You will be notified when the
rescission process has been completed.
If you have any questions regarding the permit renewal procedures please contact Joe Albiston of the Raleigh
Regional Office at 919-571-4700 or Bill Mills of the Central Office Stormwater Unit at [phone], ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Raleigh Regional Office
47A
NCDERR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

•
State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
Kerr T. Stevens, Director
Mr. Gregory W. Page
ACCU-FAB, Inc.
7513 Hwy 64
Knightdale, North Carolina 27545
Dear Mr. Page:
r�
NCDENR
March 19, 1999
Subject: General Permit No. NCG030000
ACCU-FAB, Inc.
COC NCG030436
Wake County
In accordance with your application for discharge permit received on March 3, 1999, we are forwarding
herewith the subject certificate of coverage to discharge under the subject state - NPDES general permit. This
permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum
of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable
to you, you have the right to request an individual permit by submitting an individual permit application. Unless
such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division of
Water Quality. The Division of Water Quality may require modification or revocation and reissuance of the
certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act
or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Aisha Lau at telephone number 919/733-
5083 ext. 578.
cc: Raleigh Regional Office
Sincerely,
ORIGINAL'UPCINED BY
WILLIAM C. IWILLS
Kerr T. Stevens
P.O. Box 29535, Raleigh, North Carolina 27626-0535
An Equal Opportunity Affirmative Action Employer
Telephone [phone] FAX [phone]
50% recycled/ 10% post -consumer paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTTF-1-C-A-T-E-0-F-C-0-V-E-R-A-L7E-N-o.-IVM30436
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Gregory W. Page, Robert J. Karbas, and Craven B. Page
are hereby authorized to discharge stormwater from a facility located at
ACCU-FAB, INC.
725 Beacon Lake Drive
Raleigh
Wake County
to receiving waters designated as Crabtree Creek, a class C NSW stream in the Neuse River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, I1, III,
IV, V and VI of General Permit No. NCG030000 as attached.
This Certificate of Coverage shall become effective March 19, 1999.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day March 19, 1999.
ORIGINAL SIGNED BY
WILLIAM C. MILLS
Kerr T. Stevens, Director
Division of Water Quality
By Authority of the Environmental Management Commission

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LWKWA
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
September 27, 2010
Sonya Walsh, Manager
Safety & Production Control
Accu-Fab, Inc.
801 Beacon Lake Road
Raleigh, NC 27610
Subject: Technical Assistance
Stormwater Permit NCG030436
Wake County
Dear Sonya:
Thank you for the opportunity to visit Accu-Fab, Inc., tour the facility and discuss with you the subject
permit and requirements. The following is a summary of our discussion:
1. While all NPDES permits require a NC certified laboratory to analyze samples collected
pursuant to the permit, North Carolina certification procedures do not apply to stormwater-only
discharges at the time. However, any monitoring must be conducted in accordance with EPA
approved test procedures. This includes measuring pH properly within the 15-minute hold
time. As we discussed during my visit to Accu-Fab, you are practicing proper methodology
when standardizing your meter and analyzing your samples. pH can be temperature -sensitive
and pH values can change when exposed to air.. Fortunately, you have been recording your pH
readings when collecting the samples. Please use the instantaneous, in -situ readings when
reporting pH values.
2. It is also recommended that you amend the reports previously submitted to the Division to
include the Field Parameter monitoring of pH. This would include amending the Qualitative
Monitoring Sheet, Stormwater Discharge Outfall monitoring report, indicating as such in a cover
letter and then re -submitting these to the Division.
All elements of your existing Stormwater Program were well -organized and the outfall observed during
my visit was in good condition. As indicated, all production is occurring inside the confines of your
facility.
Please continue to maintain your Stormwater Program at such a quality level.
Sincerely,
Mandy Hall
WWTP Consultant
cc: RRO File one
Stormwater Permitting Unit NorthCarolina
Naturally
North Carolina Division of Water Quality Raleigh Regional Office Surface Water Protection Phone [phone] Customer Service
Internet: www ncwaterqualily. org 1628 Mail Service Center Raleigh, NC 27699-1628 FAX [phone]
An Equal Opportun4y/Affirmative Action Employer — 50% Recycled110% Post Consumer Paper

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCG030000 SAMPLES COLLECTED DURING CALENDAR YEAR:
CERTIFICATE OF COVERAGE NO: NCG03 (This monitoring report is due at the Division no later than 30 days from
�- - -
,� the date the facility receives the sampling results from the laboratory.)
FACILITY NAME C- r a r G. COUNTY
PERSON COLLECTING SAMPLES ' 'i g PHONE NO. 9j.q L Q — (�, �( �� F - (SS
CERTIFIED LABORATORY Lab #
Lab # PLEASE SIGN ON THE REVERSE 4
Part A: Specific Monitoring Requirements
r :0utfall' _
`', Date
x. .00530
:.00400,:; �
�' <.01051' .
:. 00556 ,,
� i8141
r' No
Sample Collected,;!
Total Suspended Solids,
; PH, '
Lead, mg/L
,Oel and Grease `
f
Total 6p Orgam
i
mo/ddl
in°
Staiadai d
e. 1
E '
a H
A r 1 i
r
U
unrts
. a..
100.
-Within 6 0 =:9 0
o-t
r 5. q
N D
.q
Note: If you report a sampled value. in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes
o
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
Outfall ;:
No
...
=Date 4
Sample Collected,
�k 00556
_.,,r•00530 Y-_ .,,:
;y..' OQ400
Oil and Grease,
Total Suspended Solids„
Q
pH, t�{'
Standard units
�"
' New.Motor Otl Usage,
AnniEal-aver"a a alliiio
-
Beuchmark'
-. £r�,�;
, - 4 .,
`.J'i,y & c '-� .z•h!'.. }
:,: 30:,: r
1Q0 i r1X -
�•.. r. : x
r r
6U,
f... i90•.
r
r
i
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
STORM EVENT CHARACTERISTICS:
Date 0 oq(tirst event sampled)
Total ven Precipitation (inches): 1.0
0
Date (list each additional event sampled this reporting period, "and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
0
cr1
C:
a:
2N
i
CIQ
'Liu
z
S WU-245-102107
Page 1 of 2

1 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or
manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject
to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for
electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.3I).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent
management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the
discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I
certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater
runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management
plan included in the Stormwater Pollution Prevention Plan."
, on(Aa ,
Name (Print ame)
aI ryl::; F
Titl nt title)
1D9d A
(Signature) , (Date)
- - "I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a.system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
(Signature of
(L A�
(Date
S WU-245-102107

f�9rT MAlgOf p�t0
October 30, 2009
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
To Whom It May Concern:
^CCU-FAB, 1 NC.
801 BEACON LAKE DR. - RALEIGH. NC 27610-1377
919.212.6400 • FAX [phone]
SalesQAccuFabNC.com ' RFG0ftccuFabNC.com
www.AccuFabFfC.com
Enclosed you will find a copy of the Storm Water Discharge Outfall Monitoring Report, Analytical
Results, and the Chain of Custody for the period of July of 2009 thru December of 2009.
This report is in reference to General Permit Number NCG 030000, which became effective on
November 1, 2007.
If you have any questions, please notify me via.
Lo C
Sonya W11$h
Environmental Safety Manager
[e-mail]
919-212-6400 x155
919-212-2333 Fax
An ISO 9001:2000 Registered Company

aceAnaljftal
wwwpawabacom
f
October 14, 2009
Ms. Sonya Walsh
ACCU PAB
801 Beacon Lake Dr.
Raleigh, NC 27610
RE: Project: Stormwater Testing
Pace Project No.: 9253627
Dear Ms. Walsh:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincoy Ave. Suite 100
Huntersviile, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on September 22, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sin rely,
Tammie Easter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
- Y
Page 1 of 22

aceAnalytical'
www.p"ab&C"
r
Project: Stormwater Testing
Pace Project No.: 9253627
Sample: Outfall #1
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 9253627001 Collected: 09/22/09 08:40 Received: 09/22/09 14:40 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664A
Oil and Grease NO mg/L 5.0 1 09/24/09 10:44
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead ND mg/L 0.0050 1 09/24/09 12:00 09/25/09 22:03 7439-92-1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 83-32-9
Acenaphthylene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 208-96-8
Anthracene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 120-12-7
Benzo(a)anthracene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 56-55-3
Benzo(a)pyrene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 50-32-8
Benzo(b)fiuoranthene
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 205-99-2
Benzo(g,h,i)peryiene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 191-24-2
Benzo(k)fluoranthene
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 207-08-9
4-Bromophenylphenyl ether
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 101-55-3
Butylbenzylphthalate
NO rnA
0.0062
1
09/23/09 00:00 09/25/09 00:34 85-68-7
4-Chloro-3-methylphenol
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 59-50-7
bis(2-Chloroethoxy)methane
ND mg/L
0.012
1
09/23/09 00:00 09/25/09 00:34 111-91-1
bis(2-Chloroethyl) ether
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 111-44A
bis(2-Chloroisopropyl) ether
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 108-60-1
2-Chloronaphthalene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 91-58-7
2-Chlorophenol
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 95-57-8
4-Chlorophenylphenyl ether
ND mgA-
0.0062
1
09/23/09 00:00 09/25/09 00:34 7005-72-3
Chrysene
NO mg/L
, 0.0062
1
09/23/09 00:00 09/25/09 00:34 218-01-9
Dibenz(a,h)anthracene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 53-70-3
3,3'-Dichlorobenzidine
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 91-94-1
2,4-Dichlorophenol
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 120-83-2
Diethylphthalate
ND mg&
0.0062
1
09/23/09 00:00 09/25/09 00:34 84-66-2
2,4-Dimethylphenol
NO mg1L
0.012
1
09/23/09 00:00 09/25/09 00:34 105-67-9
Dimethylphthalate
NO mg1L
0.0062
1
09/23/09 00:00 09/25/0900:34 131-11-3
Di-n-butylphthalate
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 84-74-2
4,6-Dinitro-2-methylphenol
NO mg/L
0.025
1
09/23/09 00:00 09/25/09 00:34 534-52-1
24-Dinitrophenol
ND mg/L
0.062
1
09/23/09 00:00 09/25/09 00,34 51-28-5
2,4-Dinhrotoluene
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 121-14-2
2,6-Dinitrotoluene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 606-20-2
Di-n-octylphthalate
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 117-84-0
bis(2-Ethylhex)4)phthalate
NO mg/L
0,0062
1
09/23/09 00:00 09/25/09 00:34 117-81-7
Fluoranthene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 206-44-0
Fluorene
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 86-73-7
Hexachloro-1,3-butadiene
NO mg/L
0.0062
1
09/23/09 00:00 09125/0900:34 87-68-3
Hexachlorobenzene
ND mgtL
0.0062
1
09/23/09 00:00 09/25/09 00:34 118-74-1
Hexachlorocyclopentadlene
ND mg/L
0.012
1
09/23/09 00:00 09/25/09 00:34 77-47A
Hexachloroethane
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 67-72-1
Indeno(1,2,3-cd)pyrene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 193-39-5
Isophorone
ND mg/L
0.012
1
09/23/09 00:00 09/25/09 00:34 78-59-1
Naphthalene
NO mg/L
0.0062
1
09/23/09 00:00 09/25/09 00.34 91-20-3
Date: 10/14/2009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 3 of 22
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
e 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalytical Asheville, NC 28804 Huntersville, NC 28078
�:n�eraea.com
[phone] [phone]
ANALYTICAL RESULTS
Project: Stormwater Testing
Pace Project No.: 9253627
Sample: OuNall #1
Parameters
Lab ID: 9253627001 Collected: 09/22/09 08:40
Results Units Report Limit DF
Received: 09/22/09 14:40 Matrix: Water
Prepared Analyzed CAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Nitrobenzene
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 98-95-3
2-Nitrophenol
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 88-75-5
4-Nitrophenol
ND mg/L
0.062
1
09/23/D9 00:00 09/25/09 00:34 100-02-7
N-Nitrosodimethylamine
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 62-75-9
N-Nitroso-di-n-propylamine
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 621-64-7
N-Nitrosodiphenylamine
ND mg/L
0.012
1
09/23/09 00:00 09/25/09 00:34 86-30-6
Pentachlorophenol
ND mg/L
0.031
1
09/23/09 00:00 09/25/09 00:34 87-86-5
Phenanthrene
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 85-01-8
Phenol
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 108-95-2
Pyrene
ND mg/L
0.0062
1
09/23/09 00:00 09/25/09 00:34 129-DO-0
1,2,4-Trichlorobenzene
ND mg/L
0.0062
1
D9/23/09 00:00 09/25/09 D0:34 120-82-1
2,4,6-Trichlorophenol
ND mg/L
0.012
1
09/23/09 00:00 09/25/09 00:34 88-D6-2
Nitrobenzene-d5 (S)
55 %
10-120
1
09/23/09 00:00 09/26/09 00:34 4165-60-0
2-Fluorobiphenyl (S)
61 %
15-120
1
09/23/09 00:00 09/25/09 00:34 321-6D-8
Terphenyl-d14 (S)
60 %
11-131
1
09/23/09 00:00,09/25109 00:34 1718-51-0
Phenol-d6 (S)
21 %
10-120
1
09/23/09 00:00 09/25/09 00:34 13127-88-3
2-Fluorophenol (S)
34 %
10-120
1
09/23/09 00:00 09/25/09 00:34 367-12-4
2,4,6-Tribromophenol (S)
78 %
10-137
1
09/23/09 00:00 09/25/09 00:34 118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND mg/L
0.0050
1
09/28/09 22:67 71-43-2
Bromodichloromethane
ND mg/L
0.0050
1
09/28/09 22:57 75-27-4
Bromoform
ND mg/L
0.0050
1
09/28/09 22:57 75-25-2
Bromomethane
ND mg/L
0.010
1
09/28/09 22:57 74-83-9
Carbon tetrachloride
ND mg/L
0.0050
1
09/28/09 22:57 56-23-5
Chlorobenzene
ND mg/L
0.0050
1
09/28/09 22:57 108-90-7
Chloroelhane
ND mglL
0.010
1
09/28/09 22:57 75-00-3
Chloroform
ND mg/L
0.0050
1
09/28/09 22:57 67.66-3
Chloromethane
ND mg1L
0.0050
1
09/28/09 22:57 74-87-3
Dibromochloromethane
ND mg1L
0.0050
1
09/28/09 22:57 124-48-1
1,2-Dichlorobenzene
ND mg/L
0.0050
1
09128/0922:57 95-50-1
1,3-Dichlorobenzene
ND mg/L
0.0050
1
09/28/09 22:57 541-73-1
1,4-Dichlorobenzene
ND mg/L
0.0050
1
09/28/09 22:57 106-46-7
1,1-Dichl6roethane
ND mg/L
0.0050
1
09/28/09 22:57 75-34-3
1,2-Dichloroethane
ND mg/L
0.0050
1
09/28/09 22:57 107-06-2
1,1-Dichloroethene
ND mg/L
0.0050
1
0912810922:57 75-35-4
cis-1,2-Dichloroethene
ND mg/L
0.0050
1
09/28/09 22:57 156-59-2
trans-1,2-Dichloroethene
ND mg/L
0.0050
1
09/28/09 22:57 156-60-5
1,2-Dichloropropane
ND mg/L
0.0050
1
09/28/09 22:57 78-87-5
cis-1,3-Dichloropropene
ND mg/L'
0.DO50
1
09/28/09 22:57 10061-01-5
trans-1,3-Dichloropropene
ND mg/L
0.0050
1
09/28/09 22:57 10061-02-6
Ethylbenzene
ND mg/L
0.0050
1
09/28/09 22:57 100-41-4
Methylene Chloride
ND mg/L
0.0050
1
09/28109 22:57 75-09-2
1,1,2,2-Tetrachloroethane
ND mg/L
0.0050
1
09/28/0922.57 79-34-5
Tetrachloroethene
ND mg/L.
0.0050
1
09/28/09 22:57 127-184
Toluene
ND mg/L
0.0050
1
09/28/09 22:57 108-88-3
1,1,1-Trichloroethane
ND mg/L
0,0050
1
09/28/09 22:57 71-55-6
Date: 10/14/2009 04:55 PM
REPORT OF LABORATORY ANALYSIS Page 4 of 22
This report shall not be reproduced,
except In full,
without the written consent of Pace Analyticat Services, Inc..
a „1 •Geo�p
� i

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr. 98M Kincey Ave. Suite 100
aceAnalyfica! Asheville, NC 26804 Huntersville, NC 28078
- www.pac04ne.00m [phone] [phone]
ANALYTICAL RESULTS
Project: Stormwater Testing
Pace Project No.: 9253627
Sample: Outfall #1
Parameters
Lab ID: 9253627001 Collected: 09/22/09 08:40
Results Units Report Limit DF
Received: 09/22/09 14:40 Matrix: Water
Prepared Analyzed CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624
1,1,2-Trichloroethane
ND mg/L
0.0050
1
09/28/09 22:57 79-00-5
Trichloroethene
ND mg1L
0.0050
1
09/28/09 22:57 79-01-6
Trichlorofluoromethane
ND mg/L
0.010
1
09/28/09 22:57 75-69-4
Vinyl chloride
ND mg/L
0.0050
1
09/28/09 22:57 75-01-4
Dibromofluoromethane (S)
107 %
88-113
1
09/28/09 22:57 1868-53-7
4-Bromofluorobenzene (S)
95 %
86-111
1
09/28/09 22:57 460-00-4
Toluene-d8 (S)
103 %
92-105
1
09/28/09 22:57 2037-26.5
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
09/28/09 22:57 17060-07-0
25400 Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
15.4 mg/L
2.5
1
09/24/09 16:11
9040 pH
Analytical Method: EPA 9040
pH
6.8 Std. Units
0.10
1
09/25/09 17:30 H6
Sample: Outfall #2
Lab ID- 9253627002 Collected: 09/22/09 08:20
Received: 09/22/09 14:40 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664A
Oil and Grease 13.8 mg/L 5.0 1 09/24/09 10:44
200.7 MET 1CP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead ND mg/L 0.0050 1 09/24/09 12:00 09/25/09 22:07 7439-92-1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 83-32-9
Acenaphthylene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 208-96-8
Anthracene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 120-12-7
Benzo(a)anthracene
ND mg/L
0.0050
1
09/24/09 00:00 10(13/09 04:20 56-55-3
Benzo(a)pyrene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 50-32-8
Benzo(b)fluoranthene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 205-99-2
Benzo(g,h,i)perylene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 191-24-2
Benzo(k)fluoranthene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 207-08-9
4-Bromophenylphenyl ether
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04.20 101-55-3
Butylbenzylphthalate
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 85-68-7
4-Chloro-3-methylphenot
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 59-50-7
bis(2-Chloroethoxy)methane
ND mg/L
0.010
1
09/24/09 00:00 10/13/09 04-20 111-91-1
bis(2-Chloroethyl) ether
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 111-44-4
bis(2-Chloroisopropyl)ether
ND mg/L
0,0050
1
09/24/0900:00 10/13/0904:20 108-60-1
2-Chloronaphthalene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 91-58-7
2-Chlorophenol
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 95-57-8
4-Chlorophenylphenyi ether
ND mg/L
0.0050
' 1
09/24/09 00:00 10/13/09 04:20 7005-72-3
Chrysene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 218-01-9
Dibenz(a,h)anthracene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 53-70-3
Date: 10/14/2009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 5 of 22
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
1� COgo

aceAnalytical
www pacerabb.wm
I
Project: Slormwater Testing
Pace Project No.: 9253627
Sample: Outfall #2
Parameters
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 268o4
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 9253627002 Collected: 09/22/09 08:20 Received: 09/22/09 14:40 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
3,3'-Dichlorobenzidine
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 91-94-1
2,4-Dichlorophenol
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 120-83-2
Dtethylphthalate
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04.20 84-66-2
2,4-Dimethylphenol
NO mg/L
0.010
1
09/24/09 00:00 10/13/09 04:20 105-67-9
Dimethylphthalate
NO mglL
0,0050
1
09/24/09 00:00 10/13/0904:20 131-11-3
Di-n-butylphthalate
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 84-74-2
4,6- Din itro-2-methylphenol
NO mg/L
0.020
1
09/24/09 00:00 10/13/09 04:20 534-52-1
2,4-Dinitrophenot
NO mg/L
0.050
1
09/24/09 00:00 10/13/09 04:20 51-28-5
2,4-Dinitrotoluene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 121-14-2
2,6-Dinitrotoluene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 606-20-2
Di-n-octylphthalale
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 117-84-0
bis(2-Ethylhexyl)phthalate
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 117-81-7
Fluoranthene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 206-44-0
Fluorene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 86-73-7
Hexachloro-1 ,3-butadiene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 87-68-3
Hexachlorobenzene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 118-74-1
Hexachlorocyclopentadiene
NO mg/L
0.010
1
09/24/09 00:00 10/13/09 04:20 77-47-4
Hexachloroelhane
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 67-72-1
Indeno(1,2,3-cd)pyrene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 193-39-5
Isophorone
NO mg/L
0.010
1
09/24/09 00:00 10/13/09 04:20 78-59-1
Naphthalene
ND mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 91-20-3
Nitrobenzene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 98-95-3
2-Nitrophenol
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 88-75-5
4-Nitrophenol
NO mg/L
0.050
1
09/24/09 00:00 10/13/09 04:20 100-02-7
N-Nitrosodimethylamine
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 62-75-9
N-Nitroso-di-n-propylamine
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 621-64-7
N-Nitrosodiphenylarnine
NO mg/L
0.010
1
09/24/09 00:00 10/13/09 04:20 86-30-6
Pentachlorophenol
NO mglL
0.025
1
09/24/09 00:00 10113/09 04:20 87-86-5
Phenanthrene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 85-01-8
Phenol
NO mg/L
0.0050
1
09/24/09 00:00 10/13109 04:20 108-95-2
Pyrene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 129-00-0
1,2,4-Trichlorobenzene
NO mg/L
0.0050
1
09/24/09 00:00 10/13/09 04:20 120-82-1
2,4,6-Trichlorophenol
NO mg/L
0.010
1
09/24/09 00:00 10/13/09 04:20 88-06-2
Nitrobenzene-d5 (S)
52 %
10-120
1
09/24/09 00:00 10/13/09 04:20 4165-60-0
2-Fluorobiphenyt (S)
59 %
15-120
1
09/24/09 00:00 10/13/09 04:20 321-60-8
Terphenyl-dl4 (S)
54 %
11-131
1
09/24/09 00:00 10/13/09 04:20 1718-51-0
Phenol-d6 (S)
20 %
10-120
1
09/24/09 00:00 10/13/09 04:20 13127-88-3
2-Fluorophenol (S)
27 %
10-120
1
09/24/09 00:00 10/13/09 04:20 367-12-4
2,4,6-Tribromophenol (S)
49 %
10-137
1
09/24/09 00:00 10/13/09 04:20 118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
NO mg/L
0.0050
1
09/28/09 23:21 71-43-2
Bromodichloromethane
NO mg/L
0.0050
1
09/28/09 23:21 75-27-4
Bromoform
NO mgA-
• 0.0050
1
09/28/09 23:21 75-25-2
Bromomethane
NO mg/L
0.010
1
09/28/09 23:21 74-83-9
Carbon tetrachloride
NO mg1L
0.0050
1
09/28/09 23:21 56-23-5
Chlorobenzene
NO mg/L
0.0050
1
09/28/09 23:21 108-90-7
Date: 10/14/2009 04:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
In full,
without the written consent of Pace Analytical Services, Inc..
V
Page 6 of 22

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAna4 tical Asheville, NC 28804 Huntersville, NC 28078
- *ww. &wM
[phone] [phone]
ANALYTICAL RESULTS
Project: Stormwater Testing
Pace Project No.: 9253627
Sample: Outfall #2 Lab ID: 9253627002 Collected: 09/22/09 08:20 Received: 09/22/09 14:40 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
624 Volatile Organics Analytical Method: EPA 624
Chloroethane
ND mg/L
0.010
1
09/28/09 23.21
75-00-3
Chloroform
NO mg/L
0.0050
1
09/28/09 23:21
67-66-3
Chloromethane
NO mg/L
0,0050
1
09/28/09 23:21
74-87-3
Dibromochloromethane
NO mg/L
0.0050
1
09/28/09 23:21
124-48-1
1,2-Dichlorobenzene
ND mg/L
0.0050
1
09/28/09 23:21
95-50-1
1,3-Dichlorobenzene
NO mg/L
0.0050
1
09/28/09 23:21
541-73-1
1,4-Dichlorobenzene
NO mg/L
0.0050
1
09/28/09 23:21
106-46-7
1,1-Dichloroethane
NO mg/L
0.0050
1
09/28/09 23:21
75-34-3
1,2-Dichloroethane
NO mg/L
0.0050
1
09/28/09 23:21
107-06-2
1,1-Dichloroethene
NO mg/L
0.0050
1
09/2810923:21
75-35-4
cis-1,2-Dichloroethene
NO mg/L
0.0050
1
09/28/09 23:21
156-59-2
trans- 1,2-Dichloroethene
NO mg/L
0.0050
1
09/28/09 23:21
156-60-5
1,2-Dichloropropane
NO mg/L
0,0050
1
09/28/09 23:21
78-87-5
cis- 1,3-Dich loropropene
NO mg/L
0.0050
1
0912810923:21
1D061-01-5
trans-1,3-Dichloropropene
NO mg/L
0.0050
1
09/28/0923:21
10061-02-6,
Ethylbenzene
NO mg/L
0.0050
1
09/28/09 23:21
100-41-4
Methylene Chloride
NO mg/L
0.0050
1
09/28/09 23:21
75-09-2
1,1,2,2-Tetrachloroethane
NO mg1L
0.0050
1
09/28/09 23:21
79-34-5
Tetrachloroethene
NO mg1L
0,0050
1
09/28/09 23:21
127-18-4
Toluene
0.0065 mg/L
0.0050
1
09/28/09 23:21
108-88-3
1,1,1-Trichooroethane
NO mg/L
0.0050
1
09/28/09 23:21
71-55-6
1,1,2-Trichloroethane
NO mglL
0.0050
1
09/28/09 23:21
79-00-5
Trichloroethene
ND mg/L
0,0050
1
09/28/09 23:21
79-01-6
Trichlorofluoromethane
NO mg/L
0.010
1
09/28/09 2321
75-69-4
Vinyl chloride
NO mg/L
0.0050
1
09/28/09 23:21
75-01-4
Dibromofluoromethane (S)
106 %
88-113
1
09/28/09 23:21
1868-53-7
4-Bromofluorobenzene (S)
98 %
86-111
1
09/28/09 23:21
460-00-4
Toluene-d8 (S)
104 %
92-105
1
09/28/09 23:21
2037-26-5
1,2-Dichloroethane-d4(S)
104 %
70-130
1
09/28/0923.21
17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 2.5 1 09/24/09 16:11
9640 pH Analytical Method: EPA 9040
pH 7.5 Std. Units 0.10 1 09/25/09 17:30 H6
Date: 1011412009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 7 of 22
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
wtmtpecalabs.com
Pace Analytical services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Stormwater Testing
Pace Project No.: 9253627
QUALITY CONTROL DATA
QC Batch: OEXT/8088 Analysis Method: EPA 625
QC Batch Method: EPA 625
Associated Lab Samples: 9253627001
Analysis Description: 625 MSS
METHOD BLANK: 340126 Matrix: Water
Associated Lab Samples: 9253627001
Blank
Reporting
Parameter
Units Result
Limit
Analyzed Qualifiers
1,2,4-Trichlorobenzene
mg/L
ND
0.0050
09/24/09 07.13
2,4,6-Trichlorophenol
mg/L
ND
0.010
09/24/09 07:13
2,4-Dichlorophenol
mg/L
ND
0.0050
09/24/09 07:13
2,4-Dimethylphenol
mg/L
ND
0.010
09/24/09 07:13
2,4-Dtnitrophenol
mg/L
ND
0.050
09/24/09 07:13
2,4-Dinitrotoluene
mg/L
ND
0.0050
09/24/09 07:13
2,6-Dinitrotoluene
mg/L
ND
0.0050
09/24/09 07:13
2-Chloronaphthalene
mg/L
ND
0.0050
09/24/09 07:13
2-Chlorophenol
mg/L
ND
0.0050
09/24/09 07:13
2-Nilrophenol
mg/L
ND
0.0050
09/24/09 07:13
3,3'-Dichlorobenzidine
mg/L
ND
..0.0050
09/24/09 07:13
4,6-Dinitro-2-methylphenol
mgA-
ND
0.020
09/24/09 07:13
4-Bromophenylphenyi ether
mg/L
ND
0.0050
09/24/09 07:13
4-Chloro-3-methyiphenoi
mg/L
ND
0.0050
09/24/09 07:13
4-Chlorophenylphenyl ether
mg/L
ND
0.0050
09/24/09 07:13
4-Nitrophenoi
mg/L
ND
0.050
09/24/09 07:13
Acenaphthene
mg/L
ND
0,0050
09/24/09 07:13
Acenaphthylene
mg/L
ND
0.0050
09/24/09 07:13
Anthracene
mg/L
ND
0.0050
09/24/09 07:13
Benzo(a)anthracene
mg/L
ND
0.0050
09/24/09 07:13
Benzo(a)pyrene
mg/L
ND
0.0050
09/24/09 07:13
Benzo(b)fluoranthene
mg/L
ND
0.0050
09/24/09 07:13
Benzo(g,h,i)peryiene
mg/L
ND
0.0050
09/24/09 07:13
Benzo(k)fluoranthene
mg/L
ND
0.0050
09/24/09 07:13
bis(2-Chloroethoxy)methane
mg/L
ND
0.010
09/24/09 07:13
bls(2-Chloroethyl) ether
mg/L
ND
0.0050
09/24/09 07:13
bis(2-Chioroisopropyl) ether
mg/L
ND
0.0050
09/24/09 07:13
bis(2-Ethylhexyl)phthalate
mg/L
ND
0,0050
09/24/09 07:13
Butylbenzyiphthalate
mg/L
ND
0.0050
09/24/09 07:13
Chrysene
mg/L
ND
0.0050
09/24/09 07:13
Di-n-butytphthalate
mg1L
ND
0.0050
09/24/09 07:13
Di-n-octylphthalate
mg/L
ND
0.0050
09/24/09 07:13
Dibenz(a,h)anthracene
mg/L
ND
0.0050
09/24/09 07:13
Diethytphthalate
mg/L
ND
0.0050
09/24/09 07:13
Dimethylphthalate
mg/L
ND
0.0050
09/24/09 07:13
Fluoranthene
mg/L
ND
0,0050
09/24/09 07:13
Fluorene
mg/L
ND
0.0050
09/24/09 07:13
Hexachloro-1,3-butadiene
mg/L
ND
0.0050
09/24/09 07:13
Hexachlorobenzene
mg/L
ND
0.0050
09/24/09 07:13
Hexachlorocyclopentadiene
mg/L
ND
0.010
09/24/09 07:13
Hexachloroethane
mg/L
ND
0.0050
09/24/09 07:13
Indeno(1,2,3-cd)pyrene
mg/L
ND
0.0050
09124/0907:13
Isophorone
mg/L
ND
0.010
09124/09 07:13
Date: 10/14/2009 04:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent
of Pace Analytical Services, Inc..
a ,N •OCORo
c
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 22

Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
aceAnalytical o
www.patel8ba,pp�n
Project: Stormwater Testing
Pace Project No.: 9253627
QUALITY CONTROL DATA
[phone]
METHOD BLANK: 340126
Associated Lab Samples:
Parameter
9253627001
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
N-Nitroso-di-n-propylamtne
mg/L
ND
0.0050
09/24/09 07:13
N-Nitrosodimethylamine
mg/L
ND
0,0050
09/24/09 07:13
N-Nitrosodiphenylamine
mg/L
ND
0.010
09/24/09 07:13
Naphthalene
mg/L
ND
0.0050
09/24/09 07:13
Nitrobenzene
mg1L
NO
0.0050
09/24/09 07:13
Pentachlorophenol
mg/L
ND
0.025
09/24/09 07:13
Phenanthrene
mg/L
ND
0.0050
09/24/09 07:13
Phenol
mg/L
NO
0.0050
09/24/09 07:13
Pyrene
mg/L
ND
0.0050
09/24/09 07:13
2,4,6-Tribromophenol (S)
%
92
10-137
09/24/09 07:13
2-Fluorobiphenyl (S)
%
87
15-120
09/24/09 07:13
2-Fluorophenol (S)
%
46
10-120
09/24/09 07:13
Nitrobenzene-d5 (S)
%
81
10-120
09/24/09 07:13
Phenol-d6 (S)
%
28
10-120
09/24/09 07:13
Terphenyl-d14 (S)
%
99
11-131
09/24/09 07:13
LABORATORY CONTROL SAMPLE: 340127
Qualifiers
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/L
.05
0.033
67
44-142
2,4,6-Trichlorophenol
mg/L
.05
0.050
100
37-144
2,4-Dichlorophenol
mg/L
.05
0.040
81
1-191
2,4-Dimethylphenol
mg/L
.05
0.045
90
32-119
2,4-Dinitrophenol
mg/L
.05
ND
14
1-161
2,4-Dinitrotoluene
mg/L
.05
0.042
84
39-139
2,6-Dinitrotoluene
mg/L
.05
0.046
92
50-158
2-Chloronaphthalene
mg/L
.05
0.043
85
60-118
2-Chlorophenol
mg/L
.05
0.033
65
23-134
2-Nitrophenol
mg/L
.05
0.036
71
29-182
3,3'-Dichlorobenzidine
mgA-
.05
0.050
100
1-262
4,6-Dinitro-2-methyfphenol
mg/L'
.05
.0091J
18
1-181
4-Bromophenylphenyt ether
mg/L
.05
0.042
83
53-127
4-Chloro-3-methylphenol
mg/L
.05
0.044
88
22-147
4-Chlorophenylphenyl ether
mg/L
.05
0.042
84
25-158
4-Nitrophenol
mg/L
.05
.0151
29
1-132
Acenaphthene
mg/L
.05
0,042
84
47-145
Acenaphthylene
mg/L
.05
0.046
92
33-145
Anthracene
mg/L
.05
0.041
83
1-166
Benzo(a)anthracene
mg/L
.05
0.040
80
33-143
Benzo(a)pyrene
mg1L
.05
0.040
80
17-163
Benzo(b)fluoranthene
mg/L
.05
0.039
77
24-159
Benzo(g,h,i)peryiene
mg/L
.05
0.027
54
1-219
Benzo(k)fluoranthene
mg/L
.05
0,053
107
11-162
bis(2-Chloroethoxy)methane
mg/L
.05
0.040
80
33-184
bis(2-Chloroothyl) ether
mg/L
.05
0.039
77
12-158
[phone]
Date: 1011412009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 9 of 22
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
r

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
• 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalytical Asheville, NO 28804 Huntersville, NO 28078
www.pacoafttan
[phone] [phone]
QUALITY CONTROL DATA
Project: Stormwater Testing
Pace Project No.: 9253627
LABORATORY CONTROL SAMPLE: 340127
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Oualiiiers
bis(2-Chloroisopropyt) ether
mg/L
.05
0.0066
13
36-166
bis(2-Ethylhexyl)phthalate
mg/L
.05
0.053
106
8-158
Butytbenzylphthalate
mg/L
.05
0.054
107
1-152
Chrysene
mg/L
.05
0.039
78
17-168
Di-n-butylphthalate
mg/L
.05
0.040
81
1-118
Di-n-octylphthalate
mg/L
.05
0.049
99
4-146
Dibenz(a,h)anthracene
mg/L
.05
0.031
62
1-227
Diethylphthalate
mg/L
.05
0.042
84
1-114
Dimethylphthalate
mg/L
.05
0.041
82
1-112
Fluoranthene
mg/L
.05
0.039
78
26-137
Fluorene
mg/L
.05
0.043
87
59-121
Hexachloro-1,3-butadiene
mg/L
.05
0.035
70
24-116
Hexachlorobenzene
mg/L
.05
0.043
85
1-152
Hexachlorocyclopentadiene
mg/L
.05
0.017
33
25-150
Hexachloroethane
mg/L
.05
0.025
50
40-113
Indeno(1,2,3-cd)pyrene
mg/L
.05
0.028
55
1-171
Isophorone
mg/L
.05
0.041
81
21-196
N-Nitroso-di-n-propylamine
mg/L
.05
0.049
98
1-230
N-Nitrosodimethylamine
mg/L
.05
0,027
53
25-150
N-Nitrosodiphenylamine
mg/L
.05
0.039
79
25-150
Naphthalene
mg/L
.05
0.035
69
21-133
Nitrobenzene
mg/L
.05
0.034
68
35-180
Pentachlorophenol
mg/L
.05
0.033
65
14-176
Phenanthrene
mg/L
.05
0.039
78
54-120
Phenol
mg/L
.05
0.015
30
5-112
Pyrene
mg/L
.05
0.060
119
52-115 Li
2,4,6-Tribromophenol (S)
%
95
10-137
2-Fluorobiphenyl (S)
%
87
15-120
2-Fluorophenol(S)
%
43
10-120
Nitrobenzene-d5 (S)
%
73
10-120
Phenol-d6 (S) -
%
29
10-120
Terphenyt-d14 (S)
%
133
11-131 SO
JAN 2 R ?RIf1
1 ``J;
Date: 10/14/2009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 10 of 22
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
' ,w ♦aca,�e

aceAnalytical
www.pncelana,com
I
Project: Stormwater Testing
Pace Project No.: 9253627
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
QUALITY CONTROL DATA
QC Batch: OEXT/8107 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 9253627002
[phone]
METHOD BLANK: 340897
Matrix: Water
Associated Lab Samples: 9253627002
Blank
Reporting
Parameter
Units Result
Limit
Analyzed Qualifiers
1,2,4-Trichlorobenzene
mg/L
ND
0.0050
10/13/09 02:12
2,4,6-Trichlorophenol
mg/L
ND
0.010
10/13/09 02:12
2,4-Dichlorophenol
mg/L
ND
0.0050
10/13/09 02:12
2,4-Dimethylphenol
mg/L
ND
0.010
10/13/09 02:12
2,4-Dinitrophenof
mg1L
ND
0.050
10/13/09 02:12
2,4-Dinifrotoluene
mg/L
ND
0,0050
10/13/09 02:12
2,6-Dinitrotoluene
mg/L
ND
0.0050
10/13/09 02:12
2-Chloronaphthalene
mg/L
ND
0.0050
10/13/09 02:12
2-Chlorophenol
mg/L
ND
0.0050
10/13/09 02:12
2-Nitrophenol
mg/L
ND
0.0050
10/13/09 02:12
3,3'-Dichlorobenzidine
mg/L
ND
0.0050
10/13/09 02:12
4,6-Dinitro-2-methyiphenol
mg/L
ND
0.020
10/13/09 02:12
4-Bromophenylphenyl ether
mg/L
ND
0.0050
10/13/09 02:12
4-Chloro-3-methylphenol
mg/L
ND
0.0050
10/13/09 02:12
4-Chlorophenylphenyl ether
mg/L
ND
0.0050
10/13/09 02:12
4-Nitrophenol
mg/L
ND
0.050
10/13/09 02:12
Acenaphthene
mg/L
ND
0.0050
10/13/09 02:12
Acenaphthyfene
mg/L
ND
0.0050
10/13/09 02:12
Anthracene
mg/L
ND
0,0050
10/13/09 02:12
Benzo(a)anthracene
mg/L
ND
0.D050
10/13/09 02:12
Benzo(a)pyrene
mg/L
ND
0.0050
10/13/09 02:12
Benzo(b)fluoranthene
mg/L
ND
0.0050
10/13/09 02:12
Benzo(g,h,l)perylene
mg/L
ND
0.0050
10/13/09 02:12
Benzo(k)fluoranthene
mg/L
ND
0.0050
10/13/09 02:12
bis(2-Chloroethoxy)methane
mg/L
ND
0.010
10/13/09 02:12
bis(2-Chioroethyl) ether
mg/L
ND
0.0050
10/13/09 02:12
bis(2-Chloroisopropyl) ether
mg/L
ND
0.0050
10/i 3/09 02:12
bis(2-Ethyfhexyl)phthafate
mg/L
ND
0.0050
10/13/09 02:12
Butytbenzylphthalate
mg/L
ND
0.0050
10/13/D9 02:12
Chrysene
mg/L
ND
0.0050
10/13/09 02:12
Di-n-butylphthalate
mg/L
ND
0.0050
10/13/09 02:12
Di-n-octylphthatate
mg/L
ND
0.0050
10/13/09 02:12
Dibenz(a,h)anthracene
mg/L
ND
0.0050
10/13/09 02:12
Diethylphthalate
mg/L
ND
0,0050
10/13/09 02:12
Dimethylphthalate
mg/L
ND
0.0050
10/13/09 02:12
Fluoranthene
mg/L
ND
0.0050
10/13/09 02:12
Fluorene
mg/L
ND
0.0050
10/13/09 02:12
Hexachloro-1,3-butadiene
mg/L
ND
0.0050
10/13109 02:12
Hexachlorobenzene
mg/L
ND
0.0050
10/13/09 02:12
Hexachlorocyclopentadiene
mg1L
ND
0.010
10/13/09 02:12
Hexachloroethane
mg/L
ND
.0.0050
10/13/09 02:12
Indeno(1,2,3-od)pyrene
mg/L
ND
0,0050
10/13/09 02:12
isophorone
mg/L
ND
0.010
10/13/D9 02:12
Date: 10/14/2009 04:55 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of
Pace Analytical
Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 22

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
m 2225 Riverside Dr, 9600 Kincey Ave. Suite 100
(!;acmnaly4ical Asheville, NC 28804 Huntersville, NC 28078
wwwpaWaba.cnm [phone] [phone]
QUALITY CONTROL DATA
Project: Stormwater Testing
Pace Project No.: 9253627
METHOD BLANK: 340897 Matrix: Water
Associated Lab Samples: 9253627002
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
N-Nitroso-di-n-propylamine
mg/L
ND
0.0050
10/13/09 02:12
N-Nitrosodimethylamine
mg/L
ND
0.0050
10/13/09 02:12
N-Nitrosodiphenylamine
mg/L
ND
0.010
10/13/09 02:12
Naphthalene
mg/L
ND
0.0050
10/04/09 00:50
Nitrobenzene
mg/L
ND
0.0050
10/13/09 02:12
Pentachlorophenol
mg/L
ND
0.025
10/13/09 02:12
Phenanthrene
mg/L
ND
0,0050
1Ott 3/09 02:12
Phenol
mg/L
ND
0,0050
10/13/09 02:12
Pyrene
mg/L
ND
0.0050
10/13/09 02:12
2,4,6-Tribromophenol (S)
%
70
10-137
10/13/09 02:12
2-Fiuorobiphenyi (S)
%
68
15-120
10/13/09 02.12
2-Fluorophenol (S)
%
37
10-120
10/13/09 02:12
Nitrobenzene-d5 (S)
%
73
10-120
10/13/09 02:12
Phenol-d6 (S)
%
30
10-120
10/13/09 02:12
Terphenyl-d14 (S)
%
66
11-131
10/13/09 02:12
LABORATORY CONTROL SAMPLE:
Parameter
340898
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg1L
.05
0.030
59
44-142
2,4,6-Trichlorophenol
mg/L
.05
0.035
70
37-144
2,4-Dichlorophenot
mg/L
.05
0,034
67
1-191
2,4-Dimethylphenol
mg/L
.05
0.031
61
32-119
2,4-Dinitrophenol
mg/L
.05
.025J
49
1-181
2,4-Dinitrotoiuene
mg/L
.05
.0.038
75
39-139
2,6-Dinitrotoluene
mg/L
.05
0.038
76
50-158
2-Chloronaphthalene
mg/L
.05
0.033
66
60-118
2-Chlorophenol
mg/L
.05
0.032
65
23-134
2-Nitrophenol
mg/L
.05
0.037
73
29-182
3,3'-Dichlorobenzidine
mg/L
.05
0.043
86
1-262
4,6-Dinitro-2-methylphenol
mg/L
.05
0.031
62
1-181
4-Bromophenylphenyl ether
mg1L
.05
0.035
69
53-127
4-Chloro-3-methylphenol
mg/L
.05
0.034
69
22-147
4-Chlorophenylphenyl ether
mg/L
.05
0.033
65
25-158
4-Nitrophenol
mg/L
.05
.0161
32
1-132
Acenaphthene
mg/L
.05
0.035
71
47-145
Acenaphthylene
mg/L
.05
0.035
69
33-145
Anthracene
mg/L
.05
0.036
72
1-166
Senzo(a)anthracene
mg/L
.05
0.037
74
33-143
Benzo(a)pyrene
mg/L
.05
0.035
70
17-163
Benzo(b)fluoranthene
mg/L
.05
0.038
77
24-159
Benzo(g,h,i)perylene
mg/L
.05
0.030
59
1-219
Benzo(k)fluoranthene
mg/L
.05
0.032
64
11-162
bis(2-Chloroethoxy)methane
mg/L
.05
0.037
74
33-184
bis(2-Chloroethyl) ether
mg/L
.05
0.035
70
12-158
Date: 10114/2009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 12 of 22
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ca ,w roco�e

Pace Analytical Services, Inc.
• 2225 Riverside Dr.
aceAnalXical Asheville, NC 288N
_.. www.pacelaha.cam
[phone]
DUALITY CONTROL DATA
Project: Stormwater Testing
Pace Project No.: 9253627
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
340898
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
bis(2-Chloroisopropyl) ether
mg/L
.05
0.033
67
36-166
bis(2-Ethyihexyl)phthalate
mg/L
.05
0.032
64
8-158
Butylbenzyiphthalate
mg/L
.05
0,036
71
1-152
Chrysene
mg/L
.05
0.036
72
17-168
Di-n-butylphthalate
mg/L
.05
0.032
63
1-118
Di-n-octylphthalate
mg/L
.05
0.040
79
4-146
Dibenz(a,h)anthracene
mg/L
.05
0.031
63
1-227
Diethylphthalate
mg/L
.05
0.031
63
1-114
Dimethylphthalate
mg/L
.05
0.032
63
1-112
Fluoranthene
mg/L
.05
0.038
76
26-137
Fluorene
mg/L
.05
0.033
66
59-121
Hexachloro-1,3-butadiene
mg/L
.05
0.030
60
24-116
Hexachlorobenzene
mg/L
.05
0.033
65
1-152
Hexachlorocyclopentadiene
mg/L
.05
0.033
67
25-150
Hexachloroethane
mg/L
.05
0.027
54
40-113
lndeno(1,2,3-cd)pyrene
mg/L
.05
0.031
62
1-171
Isophorone
mg/L
.05
0.035
70
21-196
Naphthalene
mg/L
.05
0.029
58
21-133
Nitrobenzene
mg/L
.05
0.035
71
35-180
Pentachlorophenol
mg/L
.05
0.040
80
14-176
Phenanthrene
mg/L
.05
0.035
71
54-120
Phenol
mg/L
.05
0.016
30
5-112
Pyrene
mg/L
.05
0.033
66
52-115
2,4,6-Tribromophenol (S)
%
70
10-137
2-Fluorobiphenyl (S)
%
67
15-120
2-Fluorophenol(S)
%
20
10-120
Nitrobenzene-d5 (S)
%
52
10-120 1 g
Phenol-& (S)
%
25
10-120
Terphenyl-d14 (S)
%
57
11-131
Date: 10/1412009 04:55 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
y •0[oTe
Page 13 of 22

ace Analytical
www.pacele6s.00m
Project: Stormwater Testing
Pace Project No.: 9253627
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
(,QUALITY CONTROL DATA
QC Batch: WET/9890 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 9253627001, 9253627002
SAMPLE DUPLICATE: 341901
9253552001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 7.5 7.5 0 H6
Date: 10/14/2009 04:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
`q M FOGOIO
c
u�
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 22

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalyiical Asheville, NC 28804 Huntersville, NC 28078
(B28)254-7176 [phone]
f
QUALITY CONTROL DATA
Project: Stormwater Testing
Pace Project No.: 9253627
QC Batch: MPRP/5115 Analysis Method-. EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9253627001, 9253627002
METHOD BLANK: 340859 Matrix: Water
Associated Lab Samples: 9253627001, 9253627002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead mg/L ND 0.0050 09/25/09 21:00
LABORATORY CONTROL SAMPLE: 340860
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Lead mg/L .5 0.49 98 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 340861 340862
MS MSD
9253573001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead mg/L ND .5 .5 0.49 0.49 98 98 70-130 1
SAMPLE DUPLICATE: 340863
Parameter
Lead
Date: i0/14/2009 04:55 PM
9253593002 Dup
Units Result Result RPD Qualifiers
mg/L ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 15 of 22

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr. 98M Kincey Ave. Suite 100
aceAnalyftal Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
i
QUALITY CONTROL DATA
Project: Stormwater Testing
Pace Project No.: 9253627
QC Batch: GCSV/6310 Analysis Method: EPA 1664A
QC Batch Method: EPA 1664A Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 9253627001, 9253627002
METHOD BLANK: 340905 Matrix: Water
Associated Lab Samples: 9253627001, 9253627002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease MA NO 5.0 09/24/09 10:39
LABORATORY CONTROL SAMPLE: 340906
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 40 37.5 94 78-114
MATRIX SPIKE SAMPLE: 340907
9253688004 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 5.7 40 42.5 92 78-114
Date: 1011412009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 16 of 22
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services. Inc
S

�;ZeAnalyficale
/ WWW.pawfabsxom
Project: Stormwater Testing
Pace Project No.: 9253627
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WET/9876 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 25400 Total Suspended Solids
Associated Lab Samples: 9253627001, 9253627002
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 341277
Matrix: Water
Associated Lab Samples: 9253627001, 9253627002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5
09/24/0916:07
LABORATORY CONTROL SAMPLE:
341278
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 274
110 80-120
SAMPLE DUPLICATE: 341279
9253597001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 880 950 8
Date: 10114/2009 04:55 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
O R �C C0�0
Page 17 of 22

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr. 9800 Kinoey Ave. Suite 100
aceAnafytica! Asheville, NC 28804 Huntersville, NC 28078
Ia.ca� [phone] [phone]
i
QUALITY CONTROL DATA
Project: Stormwater Testing
Pace Project No.: 9253627
QC Batch: MSV/8453
OC Batch Method: EPA 624
Associated lab Samples: 9253627001, 9253627002
Analysis Method: EPA 624
Analysis Description: 624 MSV
METHOD BLANK: 342352
Matrix: Water
Associated Lab Samples: 9253627001, 9253627002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
1,1.1-Trichloroethane
mg/L
ND
0.0050
09/28/09 22:10
1,1,2,2-Tetrachloroethane
mg/L
ND
0.0050
09/28/09 22:10
1, 1,2-Trich loroethane
mg/L
NO
0.0050
09/28/09 22:10
1,1-Diehl oroethane
mg/L
ND
0.0050
09/28/09 22:10
1,1-Dichloroethene
mg/L
ND
0.0050
0912810922:10
1,2-Dichlorobenzene
mg/L
NO
0.0050
09/28/09 22:10
1,2-Dichloroethane
mg1L
ND
0.0050
09/28/09 22:10
1,2-Dichloropropane
mg/L
NO
0.0050
09/28/09 22:10
1,3-Dichlorobenzene
mg/L
ND
0.0050
09/28/09 22:10
1,4-Dichlorobenzene
mg/L
NO
0.0050
09/28/09 22:10
Benzene
mg/L
ND.
0.0050
09/28/09 22:10
Bromodichloromethane
mg/L
NO
0.0050
09/28/09 22:10
Bromoform
mg/L
NO
0.0050
09/28/09 22:10
Bromomethane
mg/L
ND
0.010
09/28/09 22.10
Carbon tetrachloride
mglL
NO
0.0050
09/28/09 22:10
Chlorobenzene
mg/L
NO
0.0050
09/28/09 22:10
Chloroethane
mg/L
NO
0.010
09/28/09 22:10
Chloroform
mg/L
NO
0.0050
09/28/09 22:10
Chloromethane
mg/L
NO
0.0050
09/28/09 22:10
cis-1,2-Dichloroethene
mg/L
NO
0.0050
09128/0922:10
cis-1,3-Dichloropropene
mg/L
NO
0,0050
09/28/09 22:10
Dibromochloromethane
mg/L
ND
0.0050
09/28/09 22:10
Ethylbenzene
mg/L
NO
0.0050
09/28/09 22:10
Methylene Chloride
mg/L
NO
0.0050
09/28/09 22:10
Tetrachloroethene
mg/L
NO
0.0050
09/28/09 22:10
Toluene
mg/L
ND
0.0050
09/28/09 22:10
trans-1 ,2-Dichloroethene
mg/L
NO
0.0050
09/28/09 22:10
trans- l,3-Dichloropropene
mg/L
NO
0.0050
09/28/09 22:10
Trichloroethene
mg/L
NO
0.0050
09/28/09 22:10
Trichlorofiuoromethane
mglL
NO
0.010
09/28/09 22:10
Vinyl chloride
mg/L
NO
0.0050
09/28/09 22:10
1,2-Dichloroethane-d4 (S)
%
101
70-130
09/28/09 22:10
4-Bromofluorobenzene (S)
%
101
86-111
09/28/09 22:10
Dibromofluoromethane (S)
%
107
88-113
09/28/09 22:10
Toluene-d8 (S)
%
102
92-105
09/28/09 22:10
Qualifiers
LABORATORY CONTROL SAMPLE: 342353
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rae Limits Qualifiers
1,1,1-Trichloroethane mg/L .02 0.023 116 52-162
1,1,2,2-Tetrachloroethane mg/L .02 0.021 107 46-157
Date: 10/14/2009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 18 of 22
This report shall not be reproduced, except in full,
withoet the written consent of Pace Analytical Services, Inc..
J

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalytical Asheville, NC 28804 Huntersville, NC 28078
w�pacOab&cam
[phone] [phone]
F
QUALITY CONTROL DATA
Project: Stormwater Testing
Pace Project No.: 9253627
LABORATORY CONTROL SAMPLE: 342353
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits
Qualifiers
1,1,2-Trichloroethane
mg/L
.02
0.024
121
52-150
1,1-Dichloroethane
mg/L
.02
0.024
119
59-155
1,1-Dichloroethene
mg/L
.02
0.025
127
1-234
1,2-Dichlorobenzene
mg/L
.02
0.021
105
18-190
1,2-Dichloroethane
mg/L
.02
0.024
118
49-155
1,2-Dichloropropane
mg/L
.02
0.025
124
1-210
1,3-Dichlorobenzene
mg/L
.02
0.021
105
59-156
1,4-Dichlorobenzene
mg/L
.02
0.020
101
18-190
Benzene
mg/L
.02
0.024
118
37-151
Bromodichloromethane
mg/L
.02
0.023
114
35-155
Bromoform
mg/L
.02
0.022
109
45-169
Bromomethane
mg/L
.02
0.029
145
1-242
Carbon tetrachloride
mg/L
.02
0.024
121
70-140
Chlorobenzene
mg/L
.02
0.021
107
37-160
Chloroethane
mg/L
.02
0.025
125
14-230
Chloroform
mg/L
.02
0.024
118
51-138
Chloromethane
mg/L
.02
0.024
118
1-273
cis-1,2-Dichloroethene
mg/L
.02
0.025
124
68-146
cis-1,3-Dichloropropene
mg/L
.02
0.025
127
1-227
Dibromochloromethane
mg1L
.02
0.020
102
53-149
Ethylbenzene
mg/L
.02
0.022
109
37-162
Methylene Chloride
mg/L
.02
0.025
126
1-221
Tetrachloroethene
mg/L
.02
0.022
109
64-148
Toluene
mg/L
.02
0.024
119
47-150
trans- 1,2-Dichloroethene
mg/L
.02
0.023
115
54-156
trans- 1 3- Dich loropropene
mg/L
.02
0.025
124
17-183
Trichloroethene
mg/L
.02
0.024
121
71-157
Trichlorofluoromethane
mg/L
.02
0.024.
118
17-181
Vinyl chloride
mg/L
.02
0.026
130
1-251
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
114
86-111 SO
Dibromofluoromethane (S)
%
97
88-113
Toluene-d8 (S)
%
102
92-105
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 342354
342355
MS
MSD
9253627002
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units Result
Cone.
Cone.
Result
Result
% Rec % Rec Limits RPD Qual
1,1,1-Trichloroothane
mg/L
ND
.02
.02
0.026
0.025
129
123 46-171 4
1,1,2,2-Tetrachloroethane
mg/L
ND
.02
.02
0.022
0.022
112
111 73-159 2
1,1,2-Trichloroethane
mg/L
ND
.02
.02
0.025
0.024
125
118 64-152 6
1,1-Dichloroethane
mg/L
ND
.02
.02
0.026
0.025
130
125 43-172 4
1,1-Dichloroethene
mg/L
ND
.02
.02
0.028
0.027
138
134 48-189 3
1,2-Dichlorobenzene
mg1L
ND
.02
.02
0.021
0.021
103
103 54-154 1
1,2-Dichloroethane
mglL
ND
.02
.02
0.026
0,024
128
122 42-171 5
1,2-Dichloropropane
mg/L
ND
.02
.02
0.026
0.025
129
125 55-157 3
1,3-Dichlorobenzene
mg/L
ND
.02
.02
0.021
0.020
106
102 57-148 3
Date: 10/14/2009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 19 of 22
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
` yn •QCq�pi
�\ C

Pace Analytical Services, Inc.
e 2225 Riverside Dr.
aceAnalytical Asheville, NC 28804
www.pacef4Gs,00m
E [phone]
QUALITY CONTROL DATA
Project: Stormwater Testing
Pace Project No.: 9253627
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 342354
342355
MS
MSD
9253627002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
1,4-Dichlorobenzene
mg/L
ND
.02
.02
0.020
0.020
100
99
58-149
1
Benzene
mg/L
ND
.02
.02
0.025
0.024
127
121
54-163
5
Bromodichlorom ethane
mg/L
ND
.02
.02
0,024
0.023
121
115
56-152
5
Bromoform
mg/L
ND
.02
.02
0.023
0.022
115
111
53-151
4
Bromomethane
mg/L
ND
.02
.02
0.028
0.027
139
134
10-200
4
Carbon tetrachloride
mg/L
ND
.02
.02
0.026
0.025
128
124
41-175
3
Chlorobenzene
mg/L
ND
.02
.02
0.022
0.021
111
106
67-152
5
Chloroethane
mg/L
ND
.02
.02
0.027
0.025
135
125
23-200
7
Chloroform
mg/L
ND
.02
.02
0.026
0.025
129
123
51-166
5
Chloromethane
mg/L
ND
.02
.02
0.027
0.025
133
123
40-175
7
cis-1,2-Dichloroethene
mg/L
ND
.02
.02
0.027
0.026
135
130
45-174
4
cis- 1,3-Dichloropropene
MA
ND
.02
.02
0.026
0.024
128
122
38-146
4
Dibromochloromethane
mg/L
ND
.02
.02
0,022
0,021
108
106
65-144
2
Ethylbenzene
mg/L
ND
.02
.02
0.022
0.021
111
106
57-152
5
Methylene Chloride
mg1L
ND
.02
.02
0.026
0.025
130
125
40-167
4
Tetrachloroethene
mg/L
ND
.02
.02
0.023
0.022
113
111
59-155
3
Toluene
mg/L
0.0065
.02
.02
0.030
0.029
120
113
47-162
4
trans-1,2-Dichloroethene
mg/L
ND
.02
.02
0.026
0.024
130
122
47-178
6
trans-1,3-Dichloropropene
mg/L
ND
.02
.02
0.025
0.024
124
121
39-148
2
Trichloroethene
mg/L
ND
.02
.02
0.026
0.026
130
125
60-153
4
Trichlorofluoromethane
mg/L
ND
.02
.02
0.025
0.024
126
118
42-199
6
Vinyl chloride
mg/L
ND
.02
.02
0.029
0.027
147
133
46-176
10
1,2-Dichloroethane-d4 (S)
%
92
91
70-130
4-Bromofluorobenzene (S)
%
110
108
86-111
Dibromofluoromethane (S)
%
101
100
88-113
Toluene-d8 (S)
%
100
100
92-105
Date: 10/14/2009 04:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 20 of 22

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalytical Asheville, NC 28504 Huntersville, NC 28078
www.pacoiab3.com [phone] [phone]
QUALIFIERS
Project: Stormwater Testing
Pace Project No.: 9253627
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
BATCH QUALIFIERS
Batch: MSSV/3123
�1) The DFTPP tune failed method criteria for ion 275 (greater than 30% of mass 198 (30.09)), Ion 442 (greater than 110% of
mass 198 (192.23)), and the tailing factor for pentachlorophenol was greater than 2.000 (2-34375). The Internal standard
response for the points In the ical was also outside method control limits. Results reported as preliminary qualified data.
ANALYTE QUALIFIERS
1 g Intemal standard concentration was above the qc limit, the results may be biased low.
H6 Analysis initiated more than 15 minutes after sample collection.
L1 Analyle recovery In the laboratory control sample (LCS) was above OC limits. Results for this analyte in associated
samples may be biased high.
SO Surrogate recovery outside laboratory control limits.
Date: 10/14/2009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 21 of 22
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

• aceAnalgical -
' *ww.pacolgh.com
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
e
Section A Section B . Section C
Pa9e- of
Required Gient IMarmation:. Required Project Information: Invoice Information:
I
Cote Report To: Attention:
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Copy l
Company Name:
RfGULA70fiY AGENCY
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Address:
r NPDES GROUND WATER r` DRINKING WATER
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EmdIJ To: Purchase
Order No.: I
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'Important Note: By signing this form you are accepting Paces NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invokes ro paid within 30 days. F-ALL-Q-020rev.07, 15-May-2007

c x
10 . f
��q�T MAN 0 F pG-tO
August 31, 2009
Division of Water Quality
Attn: Central Files
1617 Mail Service -Center
Raleigh, NC 27699-1617
To Whom It May Concern:
ACLU-FAB, INC.
801 BEACON LAKE DR. • RALEIGH, NC 27610-1377
919.212.6400 - FAX [phone]
SalesgAccuFabNC.cam " [e-mail]
www.Acc uFa bN G.c om
Enclosed you will find a copy of the Storm Water Discharge Outfall Monitoring Report, Analytical
Results for the TTO that was not included in the last report due to the fact that the sample bottles were
not available at the time of the rain event that occurred on 4/6/09, and the Chain of Custody for the
period of January of 2009 thru June of 2009. These TTO analytical results are not to be substituted for
the period of July of 2009 thru December of 2009.
This report is in reference to General Permit Number CG 030000 which became effective on
November 1, 2007.
Please advise us on any additional activity that is required to remain in full compliance of our permit.
If you have any quesl<ions, please notify me via.
son ale
Environment Safety Manager
[e-mail]
919-212-6400 x155
919-215-3244
919-212-2333 Fax
Ft: OCT ?- 8 26M
v
to
0 rn
-tiail
An ISO 9001:2000 Registered Company

1�55'neAnaljtcal m
wwwwCatziftcum
I
September 01, 2009
Ms. Sonya Walsh
ACCU FAB
801 Beacon Lake Dr.
Raleigh, NC 27610
RE: Project: OUTFALL SAMPLING 816109
Pace Project No.: 9250333
Dear Ms. Walsh:
Pace Analytical Services, Inc.
2225 Riverside a.
Asheville, NC 28804
[phone]
Pace Analytical Servlces, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on August 06, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page for
Tammie Easter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Servioes, Inc..
[phone]
Page 1 of 20

aceAnalytical o
r wmpscersbscom
i
Project: OUTFALL SAMPLING 8l6/09
Pace Project No.: 9250333
Pace Analytical Services, Inc.
2225 Riverside Dr.
Ashevii1e, NC 28804
CERTIFICATIONS
[phone]
Charlotte Certification IDs
West Virginia Certification #: 357
North Carolina Field Services Certification #: 5342
Virginia Certification #: 00213
North Carolina Drinking Water Certification #: 37706
Tennessee Certification #: 04010
Now Jersey Certification #: NC012
South Carolina Drinking Water Cori. #: 990060003
LouisianafLELAP Certification #: 04034
South Carolina Certification #: 99006D001
Kentucky UST Certification #: 84
Pennsylvania Certification #: 68-00784
Florida/NELAP Certification #; E87627
Connecticut Certification #: PH-0104
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
wittwut the written consent of PaceAnaytical Services, Inc..
Pace Ana"cal Services. Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 20

aceAnalytical®
wrwpar elabacw
Project: OUTFALL SAMPLING 816/D9
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
98DO Kincey Ave. Suite 100
Huntersville, NC 28078
Pace Project No.: 9250333
Sample: OL ITFALL #1 Lab ID: 9250333001 Collected: 08f06109 07:10 Received: 0810610913:25 Matrix: Water
[phone]
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
608 GCS Pesticides and PCBs Analytical Method: EPA608 Preparation Method: EPA3535
Aldrin
ND mg/L
0.000050
1
08/07/09 10:00 08/11/09 13:44
309-00-2
alpha-BHC
ND mg/L
0.000050
1
0810710910.00 08/1110913:44
319-84-6
beta-BHC
NO mg1L
0.000050
1
OW0710910:00 0811110913:44
319-85-7
delta-BHC
NO mg/L
0.000D50
1
08I07/09I0:00 08111/0913!44
319-86-8
gamma-BHC (Lindane)
NO mg/L
0.000050
1
08/07/09 10:00 08/11/09 13:44
58-69-9
Chlordane (Technical)
ND mg/L
0.00050
1
08/07/09 10:00 08/11/09 13:44
57-74-9
4,4'-DDD
ND mg/L
0.000050
1
0810710910.00 0811110913:44
72-54-8
4,4'-DDE
ND mg/L
0.00D050
1
08/07/0910.00 08/1110913:44
72-55-9
4,4'-DDT
NO mg/L
D.000050
1
0810710910:00 08/1110913.44
50-29-3
Dieldrin
NO mg/L
0.000050
1
08/07/09 10:00 08/11109 13:44
60-57-1
Endosulfan I
ND mg/L
0.000050
1
08/0710910-00 08/11/09 13:44
959-98-8
Endosulfan 11
ND mg/L
0.000050
1
08/07/09 101)0 08/1110913:44
33213-65-9
Endosuffan sulfate
ND mg/L
0.00D050
1
08/07/09 10:00 0811110913:44
1031-07-8
Endrin
NO nVIL
0.000050
1
08107/0910:00 0811110913:44
72-20-8
Endrin aldehyde
NO mg/L
0.000050
1
08107/091000 0811110913:44
7421-93-4
Heptachlor
NO mg/L.
0.000050
1
08107/0910:00 08/11/0913:44
7644-8
Heptachlor apoxide
NO mg/L
0.000050
1
08/0710910:00 08/11/0913:44
1024-57-3
PCB-1016 (Arodor 1016)
ND mg/L
0.00050
1
08/07/09 10 )0 08/11109 13:44
12674-11-2
PCB-1221 (Arodor 1221)
NO mg1L
0.00050
1
08/07/09 10:00 08/11/09 13:44
11104-28-2
PCB-1232 (Arodor 1232)
NO mg/L
0.00050
1
08/07/09 10,00 08/11109 13:44
11141-16 5
PCB-1242 (Arodor 1242)
ND mg/L
0.00050
1
08/07/09 10:00 08/11/09 13:44
53469.21-9
PCB-1248 (Aroctor 1248)
ND mg/L
0.00050
1
0af07109 10:00 08/11/09 13:44
12672-29-6
PCB-1254 (Arodor 1254)
ND mg/L
0.00050
1
08/07/09 10:00 08/11109 13:44
110.97-69-1
PCB-1260 (Arodor 1260)
NO mg/L
0.00050
1
08/07/09 10:00 08111/0913:44
11096-82-5
Toxaphene
NO mg/L
0.00050
1
08107/0910:00 08/11/09 13:44
8001-35-2
Tetrachloro-nrxyleno (S)
23 %
20-110
1
08/07/09 10 00 08/11/09 13:44
877-09'
Decachlorobiphenyl (S)
37 %
20-138
1
08/07109 10:00 08/11/09 13:44
2051-243
625 MSSV
Analytical Method: EPA625
Preparation Method: EPA625
Aoenaphtheno
NO mg/L
0,0053
1
08/1210910.30 08/1810911:11
83-32-9
Acenaphthylene
NO mg/L
0.0053
1
0811210910:30 08/1810911:11
208-96-8
Anthracene
ND mg/L
0,0053
1
0811210910:30 08/1810911:11
120-12-7
Benzo(a)anthracene
ND mg1L
0.0053
1
08/1210910:30 0811810911:11
56-55-3
Benzo(a)pyrene
ND mg1L
0.0053
1
00/121091030 08/1810911:11
5032-8
Benzo(b)fluoranthene
ND mg1L
0.0053
1
08112/091030 0811810811:11
205-99-2
Bonzo(g,h,l)perylene
ND mg/L
0.0053
1
08112/0910:30 08118/0911:11
191-24-2
Benzo(k)fluoranthene
ND mg/L
0.0053
1
08/12/09 10:30 08/18109 11:11
207-08-9
4-Bromophenylphenyl ether
ND mglL
0.0053
1
08/12/09 10:30 0811509 11,11
101-55-3
Butylbenzytphthalato
NO mg/L
0,0053
1
0811210910:30 08118/0911:11
85-M7
4-Chloro-3-mothylphenol
NO mg/L
0.D053
1
08/1210910:30 08/18/0911:11
59-50-7
bis(2-Chloroethoxy)methane
ND mg/L
0.011
1
0811210910:30 0811810911:11
111-91-1
bis(2-Chloroothyl)other
NO mg/L
0.D053
1
0811210910:30 0811810911:11
111-44-4
bis(2-Chloroisopropyl) ether
NO mg/L
0.0053
1
08/12/09 10:30 08/18109 11.11
108-60-1
2-Chloronaphthalone
ND mg1L
0.0053
1
08/1210910:30 08118/0911:11
91-58-7
2-Chlorophenol
NO mg1L
0.0053
1
08112/0910:30 081181D911:11
95-57-8
4-Chlorophenylphenyl ether
NO mg1L
0.0053
1
08112/09 10:30 08/18/09 11:11
7005-72-3
Chrysone
NO mglL
0.0053
1
08112/0910:30 08/1810911:11
218-01-9
Date: 09/01/2009 04:38 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
without the written consent of Pace Analytical Services, Ina.
tears.
Page 3 of 20

o Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceMalytrcal 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wrmcPbsaxe Asheville, NC28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: OUTFALL SAMPLING 816109
Pace Project No.: 9250333
Sample: 0UTFALL#1 Lab ID: 9250333001 Collected: 08106/0907:10 Received: 0810610913:25 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quat
625 MSSV Analytical Method: EPA625 Preparation Method: EPA625
Dibenz(a,h)anthracone
NO mg/L
0.0053
1
08/1210910:30 0811810911:11
53-70-3
3,3'-Dichforobenzidine
NO mg1L
0.0053
1
08/1210910:30 08/1810911:11
91-94-1
2,4-Dichlorophenol
ND mg1L
0.0053
1
0811210910.30 08118/0911.11
120-83-2
Diethylphthalate
ND mg/L
0.0053
1
0811210910:30 08/1010911:11
84-66-2
2,4-Dimothyfphenof
ND mglL
0.011
1
08112/0910:30 08/1810911:11
105-67-9
Dimethylphthalate
NO mg/L
0.0053
1
08/12/0910.30 00/18/0911:11
131-11-3
01-n-butylphthabto
ND mg/L
0.0053
1
08/12/0910:30 0811810911:11
84-74-2
4,6-Dinkro-2-methylphenol
ND mg1L
0.021
1
08/1210910:30 08/1810911:11
534-52-1
2,4-Dinitrophenol
NO mg/L
0.053
1
08112/0910:30 08118/0911:11
51-28-5
2,4-Dinitrotoluene
N0 mg/L
0.0053
1
08112/0910:30 08118/0911:11
121-14-2
2,6-Dinitrotoluene
ND mg/L
0.0053
1
0811210910:30 06/1810911:11
606-20-2
Di-n-octylphthalate
NO mg1L
0.0053
1
08112/0910:30 0811810911.11
117-"0
bis(2-Ethylhexyl)phthafate
ND mg/L
0.0053
1
=1210910:30 08/1810911:11
117-01-7
FluoraMhene
NO mg/L
0.0053
1
08/1210910:30 08/18/0911:11
206-44-0
Fluorene
NO nV/L
0.0053
1
0811210910:30 08118/0911:11
86-73-7
Hexachloro-1,3-butadione
NO mg/L
0.0053
1
08/12109 10:30 08/18/0911:11
87-68-3
Hoxachlorobenzene
NO mg/L
0.0053
1
08/1210910:30 08118/D9I1:11
118-74-1
Hexachlorocyclopentadiene
ND mg/L
0.011
1
0811210910:30 0811810911:11
77-47-4
Hexachloroothane
ND mg/L
0.0053
1
08/1210910:30 0811810911:11
67-72-1
Indeno(1,2,3-cd)pyrone
NO mg/L
0.0053
1
0811210910.30 0811810911:11
193-395
Isophorone
NO mg/L
0.011
1
08112/0910:30 08/18/D911:11
78-59-1
Naphthalene
NO mg/L
0.0053
1
08/12/0910:30 D8/18/0911:11
91-20-3
Nitrobonzene
NO mglL
0.0053
1
08/1210910.30 08/1810911:11
98-95-3
2-Nitrophenol
ND mg/L
0.0053
1
08/1210910:30 08/1810911:11
88-75-5
4-Nitrophenol
NO mg/L
0.053
1
08112/0910:30 08/1810911:11
100-02-7,
N-Nitrosod(methylamine
NO mg/L
0.0053
1
0811210910:30 08/18= 11:11
62-75-9
N-Nitroso-clk"ropylamino
ND mg1L
0.0053
1
08/1210910:30 08/18f0911:11
621-04-7
N-Nitrosodiphenylamine
NO mg/L
0.011
1
08/1210910:30 08/1810911:11
86-30.6
Pentachlorophenol
NO mg/L
0.027
1
08/12/09 10:30 0811810911.11
87486-5
Phenanthrene
NO mglL
0.DD53
1
0811210910:30 08118/0911:11
85-01-8
Phenol
ND mg/L
0.0053
1
08/12109 10:30 08/111W 11:11
108-95-2
Pyrene
ND mg/L
0.0053
1
08/1210910.30 08/18/0911:11
129400-0
1,2,4-Trichlorobenzene
NO mg/L
0.0053
1
08/121D910.30 0811810911:11
120-82-1
2,4,6-Trichlorophenol
NO ng/L
0.011
1
08/121091030 0811810911:11
88-M2
Nitrobenzene-0 (S)
48 %
10-120
1
0811210910:30 08/18/09 11:11
4165-60-0
2-Fluorobiphenyl (S)
65 %
15-120
1
08112/0910:30 08/18/09 11:11
321460$
Terphenyl-c!114 (S)
69 %
11-131
1
08/12/09 10:30 08/18/09 11:11
171851-0
Phenol-cl6 (S)
25 %
10-120
1
08/12/09 10:30 08/18109 11:11
131274M-3
2-Fluorophenol (S)
32 %
10-120
1'
08/12/09 10:30 08/10/09 11:11
367-12-4
2,4,6-Tribromophenol (S)
64 %
10-137
1
138/1210910:30 08/18/09 11:11
118-7"
624 Volatile Organics Analytical Method: EPA624
Benzene-
NO mg1L 0.0050 1
08109/0915A2 71-43-2
Bromodlchloromethane
ND mg/L 0.0050 1
08/09MS I1 :42 75-27-4
Bromoform
NO mg/L 0.0050 1
08/0910915:12 75-25-2
13romomethane
NO mg/L 0.010 1
081091091 :42 74-03-9
Carbon tetrachloride
ND rrg/L 0.0050 1.
08/09/09 1:42 56-23-5
Date: 09/01/2009 04:38 PM
REPORT OF LABORATORY ANALYSIS
Page 4 of 20
This report shalt not be reproduced, except in full.
withal the writbm oonsent of Pace Analytical Services, Inc..
1 41,

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical ® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwpacd'ahs.00m Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: OUTFALL SAMPLING 816109
Pace Project No.: 9250333
Sample: OUTFALL #1 Lab ID: 9250333001 Collected: 08/06/09 07:10 Recehred: 08/06/09 13:25 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
624 Volatile Organics Analytical Method: EPA 624
Chlorobenzeno
NO mg1L
0.0050
1
08/D910915:42 108-90-7
Chloroethane
ND mg1L
0.010
1
08/09/09 15A2 75-M3
Chloroform
ND mg/L
0.0050
1
08/0910915:42 67-66-3
Chloromethane
ND mg/L
0.0050
1
08/0910915A2 74-07-3
Dibromochloromethane
ND mg/L
0.0050
1
08/0910915:42 124-48-1
1,2-Dichlorobenzene
NO mg/L
0.0050
1
08/0910915:42 95-50-1
1,3-Dichlorobenzene
ND mg/L
0,0050
1
08/0910915:42 541-73-1
1,4-Dichlorobenzene
NO mg/L
0.0050
1
0810910915:42 106-46-7
1,1-Dichloroethane
NO mg1L
0.0050
1
08109/0915:42 75-34-3
1,2-Dichloroethane
ND mg/L
0.0050
1
OW09/0915:42 107-06-2
1,1-Dichloroethene
ND mg1L
0.0050
1
081OW0915:42 75-35-4
cis- 1,2-Dichloroothene
NO mg1L
0.0050
1
08/09/0915:42 156-59-2
trans-1,2-Dichloroethene
NO mg/L
0.0050
1
08/0910915:42 156-60-5
1,2-Dichloropropane
ND mg/L
0.0050
1
08/09/0915:42 78-87-5
cis-1,3-Dichloropropene
NO mg/L
0.0050
1
0810910915:42 10061-01-5
trans-1,3-Dichtoropropene
NO mg/L
0,0050
1
08/0910915.42 10061-02-6
Ethylbonzeno
NO mg/L
0.0050
1
08/0910915A2 100-41-4
Methylene Chloride
ND mg/L
0.0050
1
08/09109 15:42 75-09.2
1,1,2,2-Tetrachloroothane
ND mg/L
0.0050
1
08/0910915:42 79-04-5
Tetrachloroethene
NO mg/L
0.0050
1
08/0910915:42 127-18-4
Toluene
ND mg/L
0.0050
1
08/09(0915:42 108-88-
1,1,1-Trichloroethane
NO mg/L
0.0050
1
DB10910915A2 71-55-6
1,1,2-Trichloroethane
ND mg1L
0.0050
1
08/0910915:42 79-00-5
Trichloroethene
ND mg/L
0.0050
1
08/09/0915:42 79-01-6
Trichlorofluoromethans
ND mg/L
0.010
1
08/09/09 15:42 75-69-4
Vinyl chloride
ND mg/L
0.0050
1
08/09/09 15:42 75-014
Dibromofluoromethane (S)
100 %
88-113
1
08/09/09 15:42 1868-53-7
4-Bromofluorobenzene (S)
95 %
86-111
1
08/09109 15:42 460-00-4
Toluene-d8 (S)
103 %
92-105
1
08/09/09 15:42 2037-26-5
1,2-Dichloroethane-d4 (6)
101 %
70-130
1
08109/0915A2 17060-07-0
Sample: OUTFALL #2 Lab ID: 9250333002 Collected: 08/06/09 07:25 Received: 0810610913:25 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
608 GCS Pesticides and PCBs Analytical Method: EPA608 Preparation Method: EPA3535
Aldrin
NO mg1L
0.000050
1 0810710910:00
08/11/0914:00
309-OD-2
alpha-BHC
ND n'rg/L
0.000050
1 08107/0910:00
08/1110914:00
319-84-6
beta-BHC
ND mg1L
0.000050
1 08107/0910.00
08/1110914:00
319-85-7
delta-BHC
NO mg/L
0.000050
1 0010710910-00
OB/1110914:00
319-86-8
gamma-BHC (Lindane)
ND mg/L
0.000050
1 08/07/09 10.W
08111/09 14:00
5849-9
Chlordane (Technical)
ND mg/L
0.00050
1 08107/0910-D0
08/11/0914:00
57-74-9
4,4'-DDD
NO mgfL
0.000050
1 0810710910:00
Ball 1/09 14:00
72-54-8
4,4'-DDE
ND mg/L
0.000050
1 0810710910:00
08111/0914:00
72-55-9
4X-DDT
ND mg/L
0.000050
1 08107/0910.00
08/1110914:00
50-29-3
Dieldrin
ND mg/L
0.000050
1 08/07/09 10:00
=11/09 14:00
60 57-1 .
Date: 09/01/2009 04:38 PM
REPORT OF LABORATORY
ANALYSIS
Page 5 of 20
This report shall not be reproduced, except in full,
without the written
consent of Pace Analytical Services. Inc_.

Q /{�,� r to Pace Analytical Services, Inc. Pace Analytical Services, Inc.
'dCG1`'ll ij 't,r�t` I 2225 Riverside Dr. 9804 Kincey Ave. Suite 100
www,pxebbs.com Asheville. NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: OUTFALL SAMPLING 8/6109
Pace Project No.: 9250333
Sample: OUTFALL #2
Parameters
Lab ID: 9250333002
Resutts Units
Collected: 08/06/09 07:25
Report Limit OF
Received: 08/06/09 13:25 Matrix: Water
Prepared Analyzed CAS No. Qual
608 GCS Pesticides and PCBs
Analytical Method: EPA608 Preparation Method: EPA 3535
Endosulfan I
NO mg/L
0.000050
1
08/07/09 10:00 08111/09 14:00
959-98-8
Endosulfan 11
NO mg1L
0.000050
1
08/07109 10100 0811110914:00
33213-65-9
Endosulfan subte
NO mg/L
0.000050
1
08/07/09 10:00 08/1110914:00
1031-07-8
Endrin
NO mg/L
0.000050
1
0810710910.00 08/1110914:00
72-20-8
Endrin aldehyde
NO mg1L
0.000050
1
08/07/09 10,00 08/11/09 14:00
7421-93-4
Heptachlor
NO mg/L
0.000050
1
08/07/09 10:00 08/11/09 14:00
76-44-6
Hoptachlorepoxide
NO mg/L
0.000050
1
08/0710910:00 08111/0914:00
1024-57-3
PCB-1016 (Arodor 1016)
NO mg/L
0.00050
1
D8107109 10:00 0811110914:00
12674-11-2
PCB-1221 (Arodor 1221)
NO mg/L
0.00050
1
08/07/0910.00 08111/0914:00
11104-28-2
PCB-1232 (Arodor 1232)
NO mg/L
0.00050
1
08/07/09 10:00 08/11/0914:00
11141-16-5
PCB-1242 (Arodor 1242)
NO mg1L
0.00050
1
08/0710910:D0 08/11/09 14:00
53469-21-9
PCB-1248 (Arodor 1248)
NO mg/L
0.00050
1
08/07/09 10:00 08/11/09 14:00
12672-29-6
PCB-1254 (Arodor 1254)
NO mg/L
0.00050
1
08/07/09 10:00 08/11/09 14:00
11097-69-1
PCB-1260 (Arodor 1260)
NO mg/L
0.00050
1
08/07/09 10-00 08/11/09 14:00
11096-82-5
Toxaphene
NO mg1L
0.00050
1
0810710910:00 08/1110914:00
8001-35-2
Tetra chloro-m-xylene (S)
25 %
2D-110
1
08107/09 1000 08/11/09 14:00
877-09-8
Decachlorobiphenyl (S)
48 %
2D-138
1
08/07/09 10:00 08/1110914:00
2051-243
625 MSSV
Analytical Method: EPA 625 Preparation Method:
EPA 625
Acenaphthene
NO mg/L
0.0050
1
08)1210910:30 08/1810911:36
83-32-9
Acenaphthylene
NO mg/L
0.0050
1
08112t0910:30 0811810911:36
208-96-8
Anthracene
NO mg/L
0.0050
1
08/12/0910:30 0811810911:36
120-12-7
Benzo(a)anthracene
NO mg/L
0.0050
1
08/1210910:30 08118/0911:36
56-55.3 .
Benzo(a)pyrene
NO mglL
0.0050
1
08/12/0910:30 0811810911:36
50-32-8
Benzo(b)fluoranthene
NO mg/L
0.0050
1
08112/0910:30 0811810911:36
205-99-2
Benzo(g,h,)perylene
NO mg/L
0.0050
1
08/1210910:30 08/1810911:36
191-24-2
Benzo(k)fluoranthene
NO mg/L
0.0050
1
08/12/09 10:30 08/18/09 11:36
207-08-9
4-Bromophenylphenyl ether
NO mg/L
0.0050
1
08/121091030 08/18/09 11:36
101-553
Butyibenzyiphthalate
ND mg1L
0.0050
1
08/1210910,30 08/18/09 11:36
85.68-7
4-Chloro-3-methylphenol
NO mg/L
0.D050
1
08112M91030 D8/1810911:36
59-50-7
bis(2-Chloroothoxy)methane
ND mg/L
0.010
1
08112/0910:30 0811810911:36
111-91-1
bis(2-Chloroethyl) ether
NO mg/L
0.D050
1
08/12/09 10:30 08/18/09 11:36
111 444
bis(2-Chloroisopropy) ether
ND mg/L
0.0050
1
08/12/09 10:30 08/18/09 11:36
108-60-1
2-Chloronaphthalene
NO mg/L
0.005D
1
0811210910:30 0811&0911:36
91-58-7
2-Chlorophenol
ND mg/L
0.0050
1
08112JOS 10:30 08/18109 11:36
95-57.8
4-Chlorophenylphenyl ether
NO mg/L
0.0050
1
0811210910,30 08/18/09 11:36
7D05-723
Chrysene
NO mg/L
0.0050
1
081121091030 08/1810911:36
218-01-9
Dibenz(a,h)anthracene
ND mg/L
0.D050
1
0811210910.30 0811810911:36
53-70-3
3,3'-Dichlorobenzidine
ND mg1L
0,0050
1
081121091030 08/1810911:36
91-94-1
2,4-Dichlorophenol
ND mg/L
0.0050
1
0811210910:30 0811810911:36
120-83-2
Diethylphthalate.
ND mg/L
0.0050
1
08/1210910:30 0811810911.36
84-66-2
2,4-Dimethylphenol
ND mg/L
0.010
1
08/1210910:30 08/1810911:36
105-67-9
Dimethylphthalate
ND mg1L
0.0050
1
08/1210910:30 08/1810911:36
131-11-3
Di-n-butylphthabte
ND mg/L
0.0050
1
0811210910:30 0811810911:36
84-74-2
4,6-Dinitro-2-mothylphenol
ND mg/L
0,020
1
08/1210910:30 0811810911:36
534-52-1
2,4-Dinitrophenol
ND mg/L
0.050
1
0811210910:30 0811810911:36
51-28-5
2,4-Dlnitrotoluene
NO mg/L
0.0050
1
08/1210910:30 08118/0911:36
121-14-2
Date: 09/01/2009 04:38 PM
REPORT OF LABORATORY ANALYSIS
Page 6 of 20
This report shall not be reproduced, except in full,
without the written
consent of Pace Analytical
Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acmnal yt 'a f ® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwPw ta6scarrr Asheville. NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: OUTFALL SAMPLING 816109
Pace Project No.: 9250333
Sample: OUTFALL #2
Parameters
Lab ID: 9260333002
Results Units
Collected: 08/06/09 07:25
Report Limit DF
Received: 08/06/09 13:25 Matrix: Water
Prepared Analyzed CAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
2,6-Dinitrotoluene
ND mg/L
0.0050
1
0811210910:30 08/18/0911:36
606-20-2
Di-n-octylphtholate
NO mg1L
0,0050
1
08112/0910:30 08/18/0911:36
117-84-0
bis(2-Ethylhoxy0phthaiate
NO rnWL
0.0050
1
08/12/09 10:30 08/18109 11:36
117-81-7
Fluoranthen_ a
NO mg1L
0.0050
1
08/12/09 10:30 08/18/09 11:36
206-44-0
Fluorene
NO mg1L
0.0050
1
08/1210910:30 0811010911:36
86-73-7
Hexachloro-1,3-butadiene
NO mg/L
0.0050
1
08/12109 10:30 0811810911.36
87.68-3
Hexachlorobenzene
NO mg/L
0.0050
1
08/12/0910:30 0811810911:36
118-74-1
Hexachlorocyclopentadiene
NO mg/L
0.010
1
00112/0910:30 0811810911:36
77-47-4
Hexachloroethano
NO mg/L
0.0050
1
08/12/09 10:30 08/18/09 11:36
67-72-1
Indeno(1,2,3-cd)pyreno
NO mglL
0.0050
1
0811210910:30 08/18/0911:36
193-39-5
Isophorone
NO mg/L
0.010
1
0811210910:30 0811810911:36
7859-1
Naphthalene
NO mg/L
0.0050
1
08112109'10:30 08/18/0911:36
91-20-3
Nitrobenzene
NO mg1L
0,0050
1
0811210910:30 08/18/0911:36
98-95-3
2-Ndrophenol
NO mg1L
0.0050
1
0811210910.30 08/1810911:36
88-75-5
4-Nitrophenol
NO mg1L
0.050
1
0&12/091030 08/18/0911:36
100-02-7
N-Nitrosodimethylamine
NO mg/L
0.0050
1
08/1210910:30 08118/0911:36
62-75-9
N-Nitroso-di-n-propylamine
NO nrg1L
0.0050
1
M1210910:30 0811810911:36
621-64-7
N-Nitrosodiphenylamine
ND nVIL
0.010
1
08/1210910:30 08/1810911:36
86-30-6
Pentachlorophenot
ND rrgli-
0.025
1
08/1210910:30 08/1810911:36
87-86-5
Phenanthrene
ND rrg/L
0.0050
1
08112/091030 08118/0911:36
85-01-8
Phenol
ND mg/L
0.0050
1
08/1210910:30 0811810911:36
108-95-2
Pyrene
NO mg/L
0.0050
1
08/1210910:30 08/18/09 11:36
129-00-0
1,2,4-Trichlorobenzene
NO nV/L
0.0050
1
08/1210910:30 0811810911:36
120-82-1
2,4,6-Trichlorophenol
NO mg1L
0,010
1
08/1210910:30 .08/18/0911:36
88-06-2
Nitrobenzene-d5 (S)
57 %
10-120
1
08/12109 10:30 08/18/09 11:36
4165-60-0
2-Fluorobiphenyl (S)
69 %
15-120
1
08112 OS 10.30 08/18/0911:36
321-M-8
Torphonyl-d14 (S)
72 %
11-131
1
08/12/09 10:30 08118/0911:36
1718-01-0
Phenol-d6 (S)
27 %
10-120
1
08112 O910.30 OB/18/0911:36
13127488-3
2-Fluorophenol (S)
31 %
10-120
1
08/12/09 10:30 08/1810911:36
367-12-4
2,4,6-Tribromophonol (S)
68 %
10-137
1
=12109 10:30 =18/09 11:36
118-79-6
624 Volatile Organics
Analytical Method: EPA624
Benzene
NO mg/L
0.0050
1
08/09/0916.01
71-43-2
Bromodichloromathane
NO rrglL
0.0050
1
08/09/09 16:01
75-274
Bromoform
ND mg/L
0.0050
1
08/09/0916.01
75-25-2
Bromomethane
NO mg/L
0.010
1
08109/0916:01
74-83-9 '
Carbon tetrachloride
NO mg/L
0.0050
1
08/09/09 16:01
56-23-5
Chlorobenzene
NO mg/L
0.0050
1
08/09/09 16:01
108-90-7
Chloroethane
NO mg1L
0.010
1
08109/09 16:01
75-00-3
Chloroform
NO mg/L
0.0050
1
011/09/0916.01
67-66-3
Chloromethane
NO mg/L
0,0050
1
08109/0916.01
7"7-3
Dibromochloromethane
NO nglL
0.0050
1
08109/0916:01
12448 1
1,2-Dichlorobenzene
NO mg/L
0.0050
1
08/0910916.01
95-50-1
1,3-Dichlorobenzene
NO mg1L
0.0050
1
=09/0916:01
541-73-1
1,4-Dichlorobenzene
NO mg/L
0.0050
1
08109/0916:01
106-46-7
1,1-Dichloroethano
NO wG&
0,0050
.1
08/09/091601
75-34-3
1,2-Dichloroethane
NO mg/L
0.0050
1
08/0910916,01
107-06-2
Date: 09/01/2009 04:38 PM
REPORT OF LABORATORY
ANALYSIS
Page 7 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalXkal
WWWcx cr la6sca n
1
Project: OUTFALL SAMPLING 816/09
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
98W KinceyAve. Suite 100
Huntersville, NC 28078
Pace Project No.: 9250333
Sample: OUTFALL #2 Lab ID: 9260333002 Collected: 08106/09 07.25 Received: 08/06/09 13:25 Matrix: Mter
[phone]
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff
624 Volatile Organics Ana tykal Method: EPA624
1,1-Dichloroethene
ND mg/L
0.0050
1
08/09/0916.01
75-35-4
cis- 1,2-Dichloroothono
ND rrkA
0.0050
1
08/09/0916.01
156-59-2
trans-1,2-Dichloroethene
ND mg/L
0.0050
1
OS/09/091"1
156-60-5
1,2-Dichloropropane
ND mg/L
0.0050
1
08109/0916:01
78-87-5
cis-1,3-Dichloropropene
ND mg/L
0.0050
1
0810910916:01
10061-01-5
trans-1.3-Dichloropropene
ND mg/L
0,0050
1
08/0910916.01
10061-02-6
Ethylbenzene
ND mg/L
0.0050
1
0810A/0916:01
100-41-4
Methylene Chloride
ND mg/L
0.0050
1
08/09/09 16:01
75-09-2
1,1,2,2-Tetrachtoroothane
ND mg/L
0.0050
1
08/09/0916:01
79-34-5
Tetrachloroethene
ND mg/L
0.0050
1
08/0910916:01
127-184
Toluene
ND mgfL
0.0050
1
08109/091601
108-88-3
1,1,1-Trichloroethane
ND mg/L
0.0050
1
08/0910916:01
71-55-6
1,1,2-Trichloroethane
ND mg/L
0.0050
1
0810910916:01
79-00.5
Trichloroethene
ND mg/L
0.0050
1
08/0910916:01
79-01-6
Trichlorofluoromethane
ND mg/L
0.010
1
0810910916.01
75-69-4
Vinyl chloride
ND mg1L
0.0050
1
08109109 16:01
75-014
Dibromofluoromethane (S)
101 %
88-113
1
0810910916:01
1868-53-7
4-Bromofluorobenzone (S)
97 %
86-111
1
08/09/09 16:01
460-00-4
Tolueno-c!8 (S)
102 %
92-105
1
08/09/09 16:01
2037-26-5
1,2-Dichloroethane-04 (S)
99 %
713-130
1
08/09/09 16:01
17060-07-0
Date: 09/01/2009 04:38 PM REPORT OF LABORATORY ANALYSIS Page 8 of 20
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, Inc..
e,

aceAnalXitcal
-PaGehD&COM
1
f
Project: OUTFALL SAMPLING 8/6109
Pace Project No.: 9250333
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV17910
QC Batch Method: EPA624
Associated Lab Samples: 9250333001, 9250333002
Analysis Method: EPA624
Analysis Description: 624 MSV
METHOD BLANK: 319916
Matra: Water
Associated Lab Samples:
9250333001, 9250333002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
1,1,1-Trick loroetha ne
mg/L
NO
0.0050
08/09/09 09:03
1,1,2,2-Tetrachloroethane
mg/L
NO
0.0050
08/0910909.03
1,1,2-Trichloroethane
mg/L
NO
0.0050
0810910909.03
1,1-Dichloroethane
mg/L
ND
0.0050
08/09/0909:03
1,1-Dichloroethene
mg1L
ND
0.0050
08109/09 09:03
1,2-Dichlorobenzene
mg/L
ND
0.0050
08/09/09 09:03
1,2-Dichloroethano
mglL
ND
0.0050
08/09/09 09,03
1,2-Dichloropropane
mg/L
ND
0,0050
08/0910909U3
1,3-Dichlorobenzene
mg/L
NO
0.0050
0810910909:03
1,4-Dichtorobenzene
mg/L
NO
0.0050
08109/0909.03
Benzene
mg/L
NO
0.0050
08109M 09Z3
Brornodichtoromothane.
mg/L
NO
0.0050
08109/0909.03
Bromoform
mg/L
NO
0.0050
0810910909:03
Bromomethane
mg/L
NO
0.010
08109/0909:03
Carbon tetrachloride
mg1L
N D
0.0050
08/09/09 09-03
Chlorobenzene
mg/L
NO
0.0050
D8/09109 09:03
Chloroethane
mg/L
NO
0.010
08/09/09 09,03
Chloroform
mg/L
ND
0.0050
08/09/09 09:03
Chloromethane
mg/L
ND
0.0050
08/0910909:03
cis-1,2-Dichloroetheno
mg/L
NO
0.0050
08/09/0909.03
cis- 1,3-DicMoropropene
mg/L
NO
0.0050
0810910909:03
Dibromochloromethane
mg/L
ND
0.0050
08109/0909:03
Ethylbenzene
mg/L
ND
0.0050
08/09/0909:03
Methylene Chloride
mg/L
0,0052
0.0050
08/09/09 09:03 C9
Tetrachloroethene
mg/L
ND
0.0050
08/09109 09:03
Toluene
mgfL
ND
0.0050
08/09/09 09.03
trans-1 ,2-Dichloroethene
mg/L
ND
0.0050
08/09/09 09:03
trans-1,3-Dichloropropene
mg/L
ND
0.0050
08109/0909:03
Trichioroethene
mg/L
N D
0.0050
08109/09 09 03
Trichlorofluoromethane
mg/L
ND
0.010
08/09/09 09:03
Vinyl chloride
mglL
ND
0.0050
08109/0909:03
1,2-Dichloroethane-d4(S)
%
99
713-130
0810910909-.03
4-Bromofluorobenzone (S)
%
97
86-111
DS/09109 09:03
Dibromofluoromethane (S)
%
100
88-113
08109/09 09.03
Toluene-d8 (S)
%
105
92-105
08109/09 09.03
Qualifiers
LABORATORY CONTROL SAMPLE: 319917
Spike LCS LCS % Roe
Parameter Units Conc. Result % Rec Limits
1,1,1-Trichloroethane mg/L .02 0.021 107 52-162
1,1,2,2-Tetrachloroethane mg/L .02 0.024 119 46-157
Date: 09/01/2009 04:38 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Ina.
<<a
oa.e*
Pace Analytical Services, Inc.
9800KinceyAve, Suite100
Huntersville, NC 28078
(704)875.9W2
Qualifiers
Page 9 of 20

Pace Analytical Services, Inc.
1�55neMalXical" 2225 Riverside Dr.
K,wwpWd3bs,com Asheville, NC 288N
1 [phone]
QUALITY CONTROL DATA
Project: OUTFALL SAMPLING 8/6109
Pace Project No.: 9250333
LABORATORY CONTROL SAMPLE: 319917
Parameter
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,2-Trichloroethane
rrtg/L
.02
0.022
110
52-150
1,1-Dichloroethane
mg/L
.02
0.022
109
59-155
1,1-Dichloroethene
mg1L
.02
0.025
125
1-234
1,2-Dichlorobenzene
mg/L
.02
0.021
105
18-190
1,2-Dichloroethane
mg/L
.02
0.022
108
49-155
1,2-Dichloroprepane
mg/L
.02
0.023
113
1-210
1,3-Dichlorobenzene
mg/L
.02
0.021
106
59-156
1,4-Dichlorobenzene
mg/L
.02
0.021
104
18-190
Benzene
mg1L
.02
0.021
104
37-151
Bromodichloromethane
mg/L
.02
0.020
100
35-155
Bromoform
mg/L
.02
0.019
97
45-169
Bromomethane
mg1L
.02
0.023
116
1-242
Carbon tetrachloride
mg/L
.02
0.022
112
70-140
Chlorobenzone
mg/L
.02
0.021
105
37-160
Chloroethane
mg1L
02
0.022
110
14-230
Chloroform
mg/L
.02
0.020
101
51-138
Chloromethane
mg/L
.02
0.022
112
1-273
cis-1,2-Dichloroethene
mg/L
.02
0.023
115
68-146
cis-1,3-Dichloropropene
mg/L
.02
0.023
114
1-227
Dibromoch lo rometha no
mg1L
.02
0.020
99
53-149
Ethylbenzene
mg/L
.02
0.022
108
37-162
Methylene Chloride
mg/L
.02
0.026
128
1-221
Tetrachloroethene
mg/L
.02
0,022
111
64-148
Toluene
mg/L
.02
0.021
107
47-150
trans-1,2-Dichloroethene
mg/L
.02
0.022
108
54-156
trans-1,3-Dichloropropene
mg/L
.02
0.023
114
17-183
Trichloroethene
mgtL
_02
0.021
104
71-157
Trichlorofluoromethane
mg/L
.02
0.025
124
17-181
Vinyl chloride
mg/L
.02
0.021
104
1-251
1,2-Dichloroethane-d4 (S)
%
94
70-130
4-Bromofluorobenzeno (S)
%
101
86-111
Dibromotluoromethane (S)
%
99
88-113
Toluene-d8 ($)
%
101
92-105
MATRIX SPIKE 8, MATRIX SPIKE DUPLICATE: 319918 319919
Pace Analytical Services, Inc.
9800 KfnceyAve. Suite iD0
Huntersvilfe, NC 28078
[phone]
Qualifiers
Parameter
Units
9250410002
Result
MS
Spike
Cone.
MSD
Spike MS
Cone. Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
1,1,1-Trichioroethane
mg/L
ND
.02
.02 0.024
0.024
122
122
46-171
0
1,1,2,2-Tetrachloroethane
mg/L
ND
.02
.02 0.025
0.025
126
125
73-159
1
1,1,2-Trichloroethane
mg/L
ND
02
.02 0.024
0.023
120
117
64-152
2
1,1-Dichloroethane
mg/L
ND
.02
.02 0.024
0.024
122
119
43-172
3
1,1-Dichloroothene
mg/L
ND
.02
.02 0.028
0.028
142
142
48-189
0
1,2-Dichlorobenzone
mg/L
ND
.02
.02 0.022
0,022
110
111
54-154
1
1,2-Dichloroethane
mg/L
ND
.02
.02 0.023
0.023
115
117
42-171
1
1,2-Dichloropropane
mg/L
ND
.02
.02 0.026
0.025
129
123
55-157
5
1,3-Dichlorobenzene
rrtg/L
ND
.02
.02 0.022
0.022
110
112
57-148
2
Date: 09/01/2009 04:38 PM
REPORT
OF
LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wfthout
the written consent of Pace Analytical
Services. Inc..
V
Qual
Pago 10 of 20

aceAnalXical
f wex:pacefa8scavrr
Project: OUTFALL SAMPLING 816109
Pace Project No.: 9250333
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
kuntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 319918
9250410002
Parameter Units Result
MS
Spike
Cone.
MSD
Spike
Conc.
319919
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzone
mg1L
ND
.02
.02
0.021
0.022
107
109
58-149
1
Benzene
mg/L
ND
.02
.02
0.023
0.023
117
115
54-163
1
Bromodichlorornethane
mgtL
ND
.02
.02
0.023
0.023
114
113
56-152
1
Bromoform
mg/L
NO
.02
.02
0.021
0,020
103
102
53-151
1
Bromomothane
mg/L
ND
.02
.02
0,034
0.031
170
153
10-200
10
Carbon tetrachloride
mg1L
ND
.02
.02
0.026
0.025
130
123
41-175
6
Chlorobonzene
mg[L
ND
.02
.02
0.022
0.022
112
112
67-152
0
Chloroethane
mg/L
NO
.02
.D2
0.024
0.024
122
122
23-200
0
Chloroform
mg/L
ND
.02
.02
0.023
0.023
115
116
51-166
1
Chloromethane
mg/L
ND
.02
.02
0.022
0.023
112
115
40-175
2
cis-1,2-Dichioroethene
mg/L
ND
.02
.02
0.025
0.025
123
123
45-174
1
cis-1,3-Dichloropropeno
mg/L
ND
.02
.02
0.024
0.024
122
121
38A46
1
Dibromochloromethane
mg/L
ND
.02
.02
0.021
0.022
104
108
65-144
3
Ethylbenzene
nig/L
ND
.02
.02
0.023
0.023
115
116
57-152
0
Methylene Chloride
mg/L
NO
.02
.02
0.025
0.024
127
121
40-167
5
Tetrachloroethene
mg/L
NO
.02
.02
0.024
0.024
119
118
59-155
1
Toluene
mg/L
NO
.02
.02
0.024
0.024
121
118
47-162
3
trans-1,2-Dichloroethene
mg/L
NO
.02
.02
0.025
0.025
124
124
47-178
0
trans-1,3-Dichloropropene
mg1L
NO
.02
.02
0.025
0.024
124
121
39-148
2
Trichloroetheno
mg/L
NO
.02
.02
0.023
0,022
117
112
60-153
4
Trichlorofluoromethane
mg1L
NO
.02
.02
0.029
0.029
143
145
42-199
1
Vinyl chloride
mg/L
NO
.02
.02
0.024
0.024
122
118
46-176
4
1,2-Dichloroethane-d4 (S)
%
96
98
70-130
4-Bromofluorobenzone (S)
%
102
100
66-111
Dibromofluoromethane (S)
%
100
102
88-113
Toluene-d8 (S)
%
104
103
92-105
Date: 09/01/2009 04:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent at PamAnaytical Services, Inc..
aye
5. :
Page 11 of 20

aceAnalytrcal
wwAioorn
1
Project: OUTFALL SAMPLING 816/09
Pace Project No.: 9250333
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/7676 Analysis Method:
QC Batch Method: EPA625 Analysis Description:
Associated Lab Samples; 9250333001, 9250333002
EPA625
625 MSS
METHOD BLANK: 321084
Matrix: Water
Associated Lab Samples:
9250333001, 9250333002
Blank Reporting
Parameter
Units Result Limit
Analyzed
1,2,4-Trichlorobenzene
mg1L
NO
0.0050
08/13(0914:44
2,4,6-Trichlorophonot
mg1L
NO
0.010
08113/0914A4
2,4-Dichlorophenol
mg/L
NO
0.0050
08/1310914:44
2,4-Dimethylphenol
mg1L
ND
0.010
0811310914:44
2,4-Dinitrophenol
mg1L
ND
0.050
08113/0914:44
2,4-Dinitrotoluene
mg/L
ND
0.0050
08113/0914:44
2,6-Dinitrotoluene
mg1L
NO
0,0050
0811310914:44
2-Chloronaphthatene
mg/L
NO
0.0050
0811310914A4
2-Chlorophenol
mg/L
ND
0.0050
08113/0914A4
2-Nilrophenol
mg/L
NO
0.0050
08/1310914:44
3,3'-Dichlorobenzidine
mg/L
ND
0.0050
08/1310914:44
4,6-Dinitro-2-methylphenol
mg/L
ND
0.020
08/1310914:44
4-Bromophenylphenyl ether
mg/L
NO
0.0050
08/13/09 14:44
4-Chloro-3-methylphenol
mg1L
NO
0.0050
08113M 14A4
4-Chlorophenylphenytether
mg/L
NO
0.0050
08113/0914A4
4-Nitrophenol
rrg1L
NO
0.050
08/13/0914:44
Acenaphthene
mg/L
NO
0.0050
0811310914:44
Acenaphthylene
mg1L
ND
0.0050
0611310914:44
Anthracene
mg1L
ND
0.0050
08/1310914:44
Benzo(a)anthracene
mg1L
ND
0.0050
08113/0914:44
Benzo(a)pyrene
mg/L
NO
0,0050
0811310914:44
Benzo(b)fluoranthene
mg/L
ND
0.0050
08/13f0914*44
Benzo(g,h,)perylene
rng/L
ND
0.0050
0811310914:44
Benzo(k)fluoranthene
mg/L
ND
0.0050
0811310914:44
bis(2-Chloroethoxy)methane
mg[L
ND
0.010
0811310914:44
bis(2-Chloroethy) ether
mg/L
ND
0.0050
08/13/09 14A4
bis(2-ChloroisopropyQ ether
mg1L
ND
0.0050
08/13/09 14:44
bis(2-Ethylhexy)phthalate
mg1L
ND
0.0050
0011310914:44
Butylbenzylphthalate
mg/L
NO
0.0050
0811310914A4
Chryseno
mg/L
ND
0.0050
08/1310914:44
Di-n-butylphthalate
trg1L
ND
0-0050
0811310914:44
Di-n-adytphthalate
mg/L
NO
0.0050
08/13/0914A4
Dibonz(a,h)anthracene
mg1L
NO
0,0050
0811310914:44
Dlethylphthatate
mg/L
ND
0.0050
08/1310914:44
Dimethylphthalate
mg1L
ND
0.0050
0811310914:44
Fluorantheno
mg1L
ND
0.0050
08113/0914:44
Fluorene
mg1L
ND
0.0050
0811310914:44
Hexachloro-1,34 utadiene
mg/L
ND
0.0050
0811310914:44
Hoxachlorobenzene
mg1L
ND
0,0050
08/13t0914:44
Hexachlorocyclopentadiene
mg/L
NO
0.010
08113/0914:44
Hexachloroethane
mg/L
NO
0.0050
0811310914:44
Indono(1,2.3-cd)pyrene
m9/L
NO
0,0050
08/1310914:44
Isophorone
mg/L
ND
0.010
0811310914A4
Date: 09/0112009 04:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc..
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 20
� �� : l t14

Pace Analytical Services, Inc, Pace Analytical Services, Inc.
acEAnalytical ® 2225 Riverside Or. 9600 Kinney Ave. Suite 100
J wxwpa0%db&mm Asheville. NC 28804 Hurdersvilte, NC 28078
j [phone] (704)875-9W2
QUALITY CONTROL DATA
Project: OUTFALL SAMPLING 8/6109
Pace Project No.: 9250333
METHOD BLANK: 321084
Matrix: Water
Associated Lab Samples:
9250333001, 9250333002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
N-Nitroso-di-n-propylamine
mg/L
ND
0.0050
08113/0914:44
N-Nitrosodimethylamine
mg1L
ND
0.0050
0811310914:44
N-Nitrosodiphenylamine
mg/L
ND
0.010
0811310914:44
Naphthalene
mg/L
ND
0.0050
08/1310914:44
Nitrobenzene
mg/L
ND
0.0050
0811310914:44
Ponta chlorophenol
mg1L
ND
0.025
0811310914A4
Phenanthrone
mg/L
ND
0.0050
08/13/0914:44
Phenol
mglL
ND
0.0050
08/13/0914:44
Pyrone
mg1L
ND
0.0050
0811310914:44
2,4,6-Tribromophenol (S)
%
38
10-137
08/13/09 14:44
2-Fluorobiphenyt (S)
%
56
15-120
08113/09 14:44
2-Fluorophenol (S)
%
28
10-120
0811310914A4
Nitrobenzene-d5 (S)
%
69
10-120
0811310914A4
Phenol-d6 (S)
%
27
10-120
08/13/09 14A4
Terphenyl-dl4 (S)
%
55
11-131
08/13/09 14A4
LABORATORY CONTROL SAMPLE:
Parameter
321085
Units
Spike
Conc.
LCS
Rosult
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg1L
.05
0.025
50
44-142
2,4,6-Trichiorophenol
mg1L
.05
0.027
53
37-144
2,4-Dichlorophenol
mg1L
.05
0.026
52
1-191
2,4-Dimethylphenol
mg1L
.05
0.026
51
32-119
2,4-Dinitrophonol
mg/L
.05
.035J
70
1-181
2,4-Dinitrotoluene
mg/L
.05
0.033
66
39-139
2,6-Dinitrotoluene
mg/L
.05
0.028
56
50-158
2-Chloronaphthatene
rrg1L
.05
0.026
53
60-118 LO
2-Chtorophenol
mg/L
.05
0.028
55
23-134
2-Nitrophenol
rrg/L
.05
0.030
60
29-182
3,3'-Dichlorobenzidine
rg/L
.05
0.025
50
1-262
4,6-Dinitro-2-methylphenol
rrg/L
.05
0.031
62
1-181
4-Bromophenytphenyl ether
nV/L
.05
0.029
58
53-127
4-Chtoro-3-methytphenol
mgfL
05
0.029
59
22-147
4-Chlorophenylphenyl ether
mg/L
.05
0,031
63
25-158
4-Nitrophenot
mglL
.05
.044J
87
1-132
Acenaphthone
nV/L
.05
0,025
51
47-145
Acenaphthytene
mglL
.05
0.040
79
33-145
Anthracene
mg/L
.05
0.027
54
1-166
Benzo(a)anthrecene
mg/L
.05
0.029
58
33-143
Benzo(a)pyrene
mg/L
.05
0.039
79
17-163
Benzo(b)fiuoranthene
mg/L
.05
0.031
62
24-159
Benzo(g,h,l)perylene
mg/L
.05
0.028
55
1-219
Benzo(k)fiuoranthene
mg/L
.05
0.032
63
11-162
bis(2-Chtoroethoxy)methane
mg1L
.05
0.030
60
33-164
bis(2-Chbroethyl) ether
mg/L
05
0.026
52
12-158
Date: 09/01/2009 04:38 PM REPORT OF LABORATORY ANALYSIS Page 13 of 20
This report shall not be reproduced, except in full,
without the written consent of PaoeAnalytical Services, Inc..
cee.e-
r
:ice

aceAnaiXical
- www.pmebbs.com
Project: OUTFALL SAMPLING 8/6/09
Pace Project No.: 9250333
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 321085
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
tus(2-ChloroisopropA ether
mg/L
.05
0.031
62
36-166
bis(2-Ethylhexyl)phthalate
mg1L
.05
0.034
67
8-158
Butylbe nzylphtha late
mg1L
.05
0.034
69
1-152
Chrysene
mg1L
.05
0.031
62
17-168
Di-n-butylphthalate
mg/L
.05
0.031
63
1-118
Di-n-octylphthalate
mg/L
.05
0.033
66
4-146
Dibenz(a,h)anthraceno
rM/L
.05
0.030
59
1-227
Diethylphtha late
mg1L
.05
0.031
62
1-114
Dimethylphthelate
mg/L
.05
0.029
57
1-112
Fluorenthene
mg/L
.05
0.029
58
26-137
Fluorene
mg1L
.05
0.031
62
59-121
Hexachloro-1,3-butodiene
mg/L
.05
0.028
56
24-116
Hexachlorobenzene
mg/L
.05
0,026
53
1-152
Hexachlorocyclopentadiene
mg/L
.05
0.025
51
25-150
Hexachloroethane
mg/L
.05
0.032
63
40-113
Indeno(1,2,3-cftyrene
mg/L
.05
0.033
66
1-171
Isophorone
mg/L
.05
0.026
52
21-196
N-Nitroso-di-n-propylamine
mg/L
.05
0.032
64
1-230
N-Nitrosodimethylamino
mg/L
.05
0.027
53
25-150
N-Nhrosodiphenylamino
mg1L
.05
0.038
76
25-150
Naphthalene
rng1L
.05
0.027
53
21-133
Nitrobenzene
mg1L
.05
0.042
84
35-180
Ponta chlorophe nol
mg1L
.05
0.040
81
14-176
Phenanthrene
mg/L
.05
0.029
57
54-120
Phenol
mg/L
.05
0.030
60
5-112
Pyrene
mg/L
.05
0.030
59
52-115
2,4,6-Tribromophenol (S)
%
47
10-137
2-Fluorobiphenyl (S)
%
57
15-120
2-Fluorophonol (S)
%
27
10-120
Nitrobenzone-d5 (S)
%
50
10-120
Phenol-d6 (S)
%
29
10-120
Terphenyl-c!14 (S)
%
60
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
321086
321087
MS
MSD
9250359001
Spike
Spike MS
MSD
MS MSD % Rec
Parameter
Units
Result
Conc.
Conc. Result
Result % Rec % Rec Limits RPD
1,2,4-Trichlorobenzene
mg/L
ND
.14
.14 0.090
0.079
65
57 44-142 14
2,4,6-Trichlorcphenol
mg/L
ND
.14
.14 0.11
0.092
77
66 37-144 15
2,4-Dichlorophenol
mg/L
ND
.14
.14 0.098
0.089
71
64 1-191 10
2,4-Dimethylphonol
mg/L
ND
.14
.14 0.099
0.074
71
54 32-119 28
2,4-Dinitrophenol
mg/L
ND
.14
.14 .03J
ND
22
19 1-181
2,4-Dinitrotoluene
mg1L
ND
.14
.14 0.D83
0.076
59
55 39-139 8
2,6-Dinitrotoluene
mg/L
ND
.14
.14 0.076
0.073
55
52 50-158 5
2-Chloronsphthalene
mg/L
ND
.14
.14 0.097
0.084
70
61 60-118 14
2-Chtorophenol
mg/L
ND
.14
.14 0.087
0.080
62
58 23-134 8
2-Nitrophonol ,
mg1L
ND
.14
.14 0.086
0.080
62
58 29-182 6
Date: =01/200904:38 PM
REPORT OF LABORATORY ANALYSIS
This report Mail not be reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc..
co,
Qua[
Page 14 of 20

m Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acemalxical 2225 Riverside Dr. 9800 Kinsey Ave. Suite 100
wM .pa akftmm Asheville, NC 20804 HuntersAlle, NC 28078
l [phone] (704)8755092
1
QUALITY CONTROL DATA
Project: OUTFALL SAMPLING 8/6109
Pace Project No.: 9250333
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
321086
321087
MS
MSD
9250359001
Spike
Spike
MS
MSD
MS
MSD
% Roc
Parameter
Units
Result
Conc.
Conc,
Result
Result
% Roo
% Rec
Limits
RPD Qual
3,3'-Dichlorobenzidine
mg/L
NO
14
.14
0.098
0.064
71
46
1-262
42 R1
4,6-Dinitro-2-methyiphenol
mg1L
NO
14
.14
.031J
.026J
23
19
1-181
4-Bromophonylphenyl ether
mg/L
NO
.14
.14
0.11
0.099
80
71
53-127
12
4-Chloro-3-methylphenol
mg/L
NO
.14
.14
0.10
0.089
73
64
22-147
14
4-Chlorophonylphenyl ether
mg/L
NO
.14
.14
0.11
0.10
83
75
25-158
10
4-Nitrophenol
mg/L
NO
.14
.14
.061J
.049J
44
35
1-132
Acenaphthene
mg/L
NO
.14
.14
0.096
0.091
67
63
47-145
5
Acenaphthylene
mg/L
NO
.14
.14
0.10
0.090
72
65
33-145
11
Anthracene
mg/L
ND
.14
.14
0.11
0.098
79
71
1-166
11
Benzo(a)anthracone
mg1L
ND
.14
.14
0.10
0.093
72
67
33-143
7
Benzo(a)pyrene
mg/L
NO
.14
.14
0.11
0,093
76
67
17-163
12
Senzo(b)tluorantthene
mg1L
NO
.14
.14
0.19
0.12
138
84
24-159
49 R1
Benzo(g,h,)perylene
mg/L
NO
A4
.14
0.064
0.054
46
39
1-219
18
Benzo(k)fluoranthene
mg/L
NO
.14
.14
0.20
0.12
141
85
11-162
49 R1
bis(2-Chloroethoxy)methane
mg/L
NO
.14
-14
0.11
0.096
76
69
33-184
9
bis(2-Chloroethyl) ether
mg/L
NO
.14
.14
0,097
0.087
70
62
12-158
11
bis(2-Chlorolsopropyl) ether
mg/L
NO
.14
.14
0.099
0.096
72
69
36-166
4
bis(2-EthylhexyQphthalato
mg/L
NO
.14
.14
0.12
0.12
88
84
8-158
5
Butylbenzylphthalate
mg/L
ND
.14
.14
0.12
0.12
87
83
1-152
5
Chrysone
mg/L
ND
.14
.14
0.11
0.099
82
71
17-168
14
Di-n-butylphthalate
mg/L
ND
.14
.14
0.11
0.099
80
71
1-118
12
Di-n-octylphthalate
mg/L
NO
.14
.14
0.12
0.11
87
81
4-146
7
Dibenz(a,h)anthracene
mg/L
NO
.14
.14
0.073
0.064
52
46
1-227
13
Diethylphthalate
mg/L
NO
.14
.14
0.10
0.093
76
67
1-114
12
Dimethylphthalate
mg/L
NO
.14
.14
0.094
0.086
68
62
1-112
9
Ftuoranthono
mg/L
NO
.14
.14
0.11
0.095
76
69
26-137
11
Fluorene
mg/L
4.3.1
.14
.14
0.11
0.096
77
66
59-121
14
ug/L
Hexachloro-1,3-butadier►e
mg/L
NO
.14
.14
0.091
0.083
66
60
24-116
10
Hexachlofobenzene
mg/L
ND
.14
.14
0.092
0.084
66
61
1-152
9
Hexachlorocyclopentadiene
mg/L
ND
.14
-14
0.044
0.039
32
28
25-150
13
Hexachloroethane
mg/L
NO
.14
.14
0.077
0.072
55
52
40-113
7
Indeno(1,2,3-cd)pyreno
mg/L
NO
.14
.14
0.071
0.D61
51
44
1-171
15
Isophorone
mg/L
ND
.14'
.14
0.090
0.D85
65
61
21-196
6
N-Nitroso-di-n-propylamine
mg/L
NO
.14
.14
0.044
0,10
32
72
1-230
78 R1
N-Nitrosodirnethylamine
mg/L
NO
.14
.14
0.049
0.048
36
34
25-150
3
N-Nitrosodiphenylamine
rng/L
NO
.14
.14
0.12
0.10
83
75
25-150
11
Naphthalene
mg1L
76.3
.14
.14
0.18
0,16
77
60
21-133
14
ug1L
Nitrobenzene
mg/L
NO
.14
.14
0,086
0.079
62
57
35-180
6
Pentachlorophenol
mg/L
NO
.14
.14
0.10
0.0%
72
69
14-176
5
Phenanthrone
mg/L
4.1J
.14
.14
0.12
0.10
83
71
54-120
16
ug/L
Phenol
mg/L
ND
.14
.14
0.D63
0.059
46
43
5-112
7
Pyrene
mg/L
ND
14
.14
0.11
0.11
80
76
52-115
5
2,4,6-Tribromophenol (S)
%
68
59
10-137
2-Fiuorobiphenyt (S)
%
72
63
15-120
2-Fluorophenol (S)
%
47
46
10-120
Date: 09/01/2009 04:38 PM
REPORT OF
LABORATORY ANALYSIS
Page 15 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace AnaVical Services, Inc..

1�55'oeAnalytica(
r www.pace~abtcem
I
Project: OUTFALL SAMPLING 8/6109
Pace Project No.: 9250333
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HuntersMile, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE; 321086
321087
MS
MSD
9250359001 Spike
Spike MS MSD MS
MSD
% Rec
Parameter Units Result Cone.
Conc. Result Result % Roe
% Roe
Limits RPD Qua[
Nitrobenzene-dS(S) %
61
57
10-120
Phenol-d6 (S) %
46
43
10-120
Terphenyl-cI14 (S) %
71
67
11-131
Date: 09/01/2009 04:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, exoept in full,
wMxxA the written consent of Pats Analytical Services, Inc..
Page 16 of 20

_ aceAnalytrcal
www.pacdabscam
Project: OUTFALL SAMPLING 816109
Paco Project No.: 9250333
QC Batch: OEXTf7630
QC Batch Method: EPA 3535
Associated Lab Samples: 9250333001, 9250333D02
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA608
Analysis Description: 608 GCS Pest PCB
METHOD BLANK: 319263
Associated Lab Samples:
Parameter
9250333001, 9250333002
Units
Matra: Water
Blank Reporting
Result Limit
Analyzed
4,4'-DDD
mg/L
NO
0.000050
0811110911:43
4A'-DDE
mg/L
NO
0.000050
0811110911:43
4,4'-DDT
mg/L
NO
0.000050
0811110911:43
Aldrin
mg/L
NO
0.000050
08/1110911:43
alpha-BHC
mg/L
NO
0,000050
08/1110911:43
beta-BHC
rng/L
NO
0.000050
08/1110911:43
Chlordane (Technical)
mg1L
NO
0.00050
0811110911:43
delta-BHC
mgfL
NO
0.00D050
08111Mg 11:43
Dieidrin
mg/L
NO
0.000050
0811110911:43
Endosulfan I
mg/L
ND
0.000050
08/11109 11:43
Endosulfan It
mg/L
NO
0.000050
08111/0911:43
Endosulfen sulfate
mg1L
NO
0.000050
08/11109 11:43
Endrin
mg/L
NO
0.000050
0811110911:43
Endrinaldehyde
mg/L
NO
0.000050
0811110911:43
gamma-BHC (Lindane)
mg/L
NO
0.000050
08/1110911:43
HeptacWr
mg/L
NO
0,000050
08/1110911:43
Heptachlor epoxide
mg/L
NO
0.D00050
08/11/09 11:43
PCB-1016 (Aroclor 1016)
mg1L
NO
0.00050
06111/0911:43
PCB-1221 (Arodor 1221)
mg/L
NO
0.00050
08/11/09 11:43
PCB-1232 (Arodor 1232)
mg/L
ND
0.00050
08/11/09 11:43
PCB-1242 (Arodor 1242)
mg/L
NO
0.00050
0811110911:43
PCB-1248 (Arodor 1248)
mg/L
NO
0.00050
08111/0911:43
PCB-1254 (Arodor 1254)
mg/L
NO
0.D0050
08111/0911:43
PCB-1260 (Arodor 1260)
mg/L
NO
0.00050
08111/0911:43
Toxaphene
mglL
NO
0.D0050
0811110911:43
Decachlorobiphenyl (S)
%
52
20-138
08/11/09 11:43
Tetrachioro-m-xylene (S)
%
31
20-110
08/11/09 11:43
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
319264
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
4,4'-DDD
mg/L
.00008
0.000051
64
31-141
4,4'-DDE
mg/L
.00008
NO
54
30-145
4,4'-DDT
mg/L
_00008
0.000072
91
25-160
Aldrin
mg/L
.00008
NO
54
42-122
alpha-BHC
mg/L
.00008
NO
56
37-134
beta-BHC
mg1L.
.00008
0.000068
86
17-147
delta-BHC
mg/L
.00008
NO
46
19-140
Dieldrin
mg/L
.00008
0.000D52
64
36-146
Endosulfan I
mg/L
.00008
0.000052
65
45-153
Endosulfan II
mg/L
.00008
NO
50
1-202
Date: 09/0112009 04:38 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fuii,
without the written consent of Pace Ana"[ Services, Inc -
Pace Analytical Services, Inc.
9800KinceyAve. Suite100
Huntersville, NC 28078
[phone]
Qualifiers
Page 17 of 20

acmnalytical
( www.pacelabscorn
Project: OUTFALL SAMPLING 8!8l09
Pace Project No,: 9250333
LABORATORY CONTROL SAMPLE: 319264
Parameter
Units
Endosul(an sulfate
mg1L
Endrin
mg/L
Endrin aldehyde
mg/L
gamma-BHC (Lindane)
mglL
Heptachlor
mg/L
Heptachlor epoxide
mg1L
Docachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
Pace Analyttcat Services, Inc.
2225 Riverside Or,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike
Cone,
LCS
Result
LCS
% Rec
% Rec
Limits
.00008
0.000062
78
26-144
.00008
0.000072
91
30-147
.00008
0.000082
103
50-150
.00008
ND
60
32-127
.00008
0.000065
81
34-111
.00008
ND
55
41-126
66
20-138
101
20-110
Pace Analytical Services, Inc.
98M Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
319265
319266
MS
MSD
9250333002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
4,4'-DDT
mg/L
NO
.00008
00008
0.000058
0.000061
73
76
25-160
4
Aidrin
mg/L
NO
00008
.00008
0.000066
0.000053
83
66
42-122
23
Dieldrin
mg[L
ND
.00008
.00W8
0.000058
O.D00064
73
79
36-146
8
Endrin
rng/L
ND
.00008
.00008
0.000056
0.000064
69
80
30-147
14
gamma-BHC (Lindane)
nV/L
NO
OWW
.00008
O.D00078
0.000062
98
78
32-127
23
Heptachlor
mg/L
ND
_00008
DD008
ND
ND
53
48
34-111
Dec:achlorobiphenyt (6)
%
59
78
20-138
Tetmchloro-m xylene (8)
%
75
71
20-110
Date: 09/01/2009 04:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall rat be reproduced, except in full.
without the written consent of PaoeAnalytical Services, Inc,.
oe,a
Page 18 of 20

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