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NCG030392_MONITORING INFO_20180213 (FIX)
PERMIT NO. DOC TYPE DOC DATE STORMWATER DIVISION CODING SHEET NCG PERMITS --- � Ivo3b31a HISTORICAL FILE MONITORING REPORTS YYYYMMDD Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Q 3 D 2 D,rt bmitted I- 8 CERTIFICATE OF COVERAGE NO. NCG03 O O !7 SAMPLE COLLECTION YEAR Zo { 8 FACILITY NAME Ornte1A 1 'necrr_Spt�.�,kwS SAMPLE PERIOD 5q Jan -June ❑ July -Dec COUNTY �jafs,� or Monthly' month PERSON COLLECTING SAMPLES Z�,;n„,,o RE@SGIAii�6�T0 CLASS ❑ORW :HOW ❑Trout ❑PNA .J ❑Zero -flow ❑Water Supply ❑SA LABORATORY cc. Lab Cert. # FEB I � '� [:]OtherComments on sample cof ection or analysis: Part A: Stormwater Benchmarks and Monitoring Results CENTRAL t=i, OWR 8PE— ."!-hEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 .� ❑ No discharge this period?z Outfall No. [)ate Sample Collected) (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics] Benchmarks =__> _ 100 mg/L or 50 mg/L° 6.o -- 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L of apl rd O .S�.3.1 m11L f4 6 M 0 300 V.Y% 20Z .8 23_1L,_ 1 :& L 21zo 141 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date. 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions ofthe solvent management plan included in the Stormwater Pollution Prevention Plan." i-d Name (Print name) Aa f- MSG- - - Title f Pri t title) a- 91 (Signature) (Odle) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: i Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?` Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B " See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: 11 you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER Z REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR_, inclu_d_ing all No Discharqe" reports within 30 days of receipt of the lab results (or at end of monitoring period ` in the case o "No Discharge' reports) to: Division of Water Quality Attm DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED; "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations." (Signature of Permittee) Permit Date: 11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report ror yrridorrce of filling out this form, please visit: l / car I.ncd nr,r ru vre b we titi s i /r1 I s - %0it ti -4 Permit No.: ur' Certificate of Coverage No.: Facility Name: CQdtec+—� T ca(�Solu+tis County: 10"C Phone No. gt9SS1'7.56a Inspector: ay— r�,naiuf:eo� Date of Inspection: 130 ( b Time of Inspection: fc)'.00A"%A Total Event Precipitation (inches): 0.5- Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must he per fiu-med during a "representative storm event" or "measureable storm et Brat" (requirerrrerrts vary, depending on the permit). Qualitative monitoring; requirements vary. Most permits require qualitative monitoring to he performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a sturm event that measures greater than 0.1 inches of rainfail and that is preceded by at least 72 Hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the perrnittee is able to document that a shorter interval is representative for local storm events during the sarnpling period, and the permittee obtains approval from the local DWQ Regional Office. Ry this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Pernlittee or Designee) Page I of Z SwU-"L42, Last madihed 10/"-5/2112 r 1. Outfall Description: Outfall No. �Structure (pipe, ditch, etc.) /J, OC Receiving Stream: Describe the industrial activities that e7ccur within the outfall drainage area: 2, Color: Describe the color of the discharge using basic colors (red, brawn, blue, etc.) and tint (light, medium, dark) as descriptors: rlan(- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weals chlorine odor, etc.): n-e— 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 0 2 3 4 5 S. Floating Solids: Choose the rrurnber which hest describes the amount of Floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 10 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes Vo 8. Is there an oil sheen in the stormwater discharge? Yes c 9. Is there evidence of erosion or deposition at the outfall? Yes l) 10. Other Obvious Indicators of Stornrwater Pollution: List and describe Llon(- Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erasion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SW-242, Last moditied t 0/25/2012 �r NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report [,oryuidunc'e oil filling out this form, please visit: http//uartal.ncdenr. rr;/web/�vn/tvs/su!rinLie ss_ b-I Permit No,: N/C/ L!/ o / 3/ 0/ a/ o/o / Facility Name: E ee County: iJ CL" Inspector: Let 6agmi-c- Date of Inspection: l' 3&ob Time of Inspection; r ®.OcAm or Certificate of Coverage No.: Phone No. G f4'vSV• IbtD Total Event Precipitation (inches): -! __ Was this a "Representative Storm Event" or "Measureahle Storm Event" as defined by the permit"? (See information below.) � } Yes ❑ No Pleuse verify whether Qualitative Monitoring must be per forrrred during a "representative .storm event" or "nreusureuble storm event" (requirements vary, depending on the perrnit). Qualitative nionitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureahle storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicahle. A "representative storm event" is n storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 clays) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a stor ,in event that results in an actual discharge from the pernnitted site outfall, The previous nieasurahle storm event must have been at least 72 hours prior. The 72-hour storrii interval does not apply if the permittee is able to doctnnent that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of illy knowledge: (Signature of Permittee or Designee) Page 1 42 SWIJ-212, r,ast modiried I U/25/2012 1. Outfall Description: Outfall No. — Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: f�&V.-L 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc,): K&11� 4. Clarity: Choose the nurnber- which hest describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 S. Floating Solids: Choose the number whit;h best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 & Suspended Solids: Choose the number which hest describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: n 2 3 4 5 7. Is there any foam in the .stormwater discharge-? Yes H. Is there an oil sheen in the stormwater discharge? Yes Tf�c 9. Is there evidence of erosion or deposition at the outl-all? Yes jSP 10. Other Obvious Indicators of Stormwater Pollution: List and describe h1.c5ti^y Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. I'age 2 of 2 SWU-242, Last mudiried 10/25/2012 aceAnayrca!m / - www pacelab s, cam February 07, 2018 Jennifer Chaltain Contech 6115 Chapel Hill Road Raleigh, NC 27607 RE: Project: Outfalls 1 &2 Pace Project No.: 92371337 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Jennifer Chaltain: Enclosed are the analytical results for sample(s) received by the laboratory on January 30, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except:n full, without the written consent of Pace Analytical Services, LLC. page 1 of 14 �IceAnalXicala i t w*W parelabS com Project: Outfalls 1 &2 Pace Project No.: 92371337 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Hunlefsville, NC 28079 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification Ws 2225 Riverside Drive, Asheville, NC 28804 FioridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Certification #: 99006001 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification M 40 South Carolina Certification #: 9903DD01 VirginiafVELAP Certification #: 460222 North Carolina Wastewater Certification #'. 633 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 2 of 14 _ . ac e Analytical rwwwpacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 6701 Conference Dnve Raleigh, NC 27607 (919)834-4984 Projecc Pace Project NO.; Outfalls 1 &2 92371337 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92371337001 Outfall 1 SM 2540D SAM1 1 PASt-E EPA 1664E JMS 1 PASI-C EPA 200.7 SH1 3 PASI-A 92371337002 Outfall 2 SM 2540D SAM1 1 PASi-E SM 4500-H+8 WCP 1 PASI-E EPA 1664B JMS 1 PASI-C EPA 200.7 SH1 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC_ Page 3 of 14 aceAnalyiical A www paceiabs. corn ANALYTICAL RESULTS Pace Analytical services, LLC 6701 Conference Drive Raleigh, NC 27607 (919y834-49B4 Project: Outfalls 1&2 Pace Project No.: 92371337 Sample: Outfail 1 LabID: 92371337001 Collected: 01/30118 07:30 Received: 0113008 10:26 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Sotids 3.1 mg/L 2.5 1 02/02/18 1149 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 5.0 1 02/07/18 D4:50 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200 7 Copper ND ug/L 5.0 1 02/03/18 03:00 02/06/18 18:48 7440-50-8 Lead ND ug1L 5.0 1 02/03/18 03:00 02/06/18 18:48 7439-92-1 Zinc 1090 ug1L 10.0 1 02103/1803:00 02106/1818A8 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Lull. Date: 02/07/2018 03',40 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 172ceAnalyfical wi wpacxlalmcom ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27507 (919 )834-4 984 Project Outfalls 1&2 Pace Project No.: 92371337 Sample: Outfall 2 Lab ID: 92371337002 Collected: 01/30/18 07:45 Received: 01/30/18 10:26 Matr4: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual 2540D Total Suspended Solids Analytical Method SM 2540D Total Suspended Solids 202 mg1L 11.9 1 02/02/18 10.50 4500H+ pH, Electrometric EDN Analytical Method: SM 4500-H+B pH at 25 Degrees C 6.8 Std. Units 1.0 1 02/05/18 10:13 H1,H6 1664 SGT-HEM, TPH Analytical Method'. EPA 1664E Total Petroleum Hydrocarbons ND mglL 5.0 1 02/07/18 04:50 200.7 MET ICP Analytica! Method EPA 200.7 Preparation Melhod: EPA 200.7 Copper 23.7 ug1L 5.0 1 02/03/18 03:00 02106118 18:51 7440-50-8 Lead 15.8 ug/L 5.0 1 02/03/18 03:00 02/06/18 18:51 7439-92-1 Zinc 3320 ug/L 10.0 1 02/03/18 03:00 02/06/18 18:51 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 02/07/2018 0140 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 ZI ace Analytical www pacelabs, com QUALITY CONTROL DATA Project: Outfalls 1 &2 Pace Project No.: 92371337 QC Batch: 396472 Analysis Method. SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92371337001, 92371337002 METHOD BLANK: 2198129 _ Matrix: Water — Associated Lab Samples: 92371337001, 92371337002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 02/02/18 10:47 LABORATORY CONTROL SAMPLE: 2198130 Spike LCS Parameter Units Conc. Result Total Suspended Solids mg[L 250 248 SAMPLE DUPLICATE: 2198131 92371384001 Dup Parameter Units Result Result Total Suspended Solids mg/L 147 201 SAMPLE DUPLICATE: 2198132 92371585001 Dup Parameter Units Result Result Total Suspended Solids mg/L 151 187 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LCS % Rec % Rec Limits Qualifiers 99 90-110 RPD Qualifiers 31 D6 RPD Qualifiers 21 D6 Results presented on this page are in the units indicated by the"Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/07/2018 03:40 PM without the written consent of Pace Analytical Services. LLC Page 6 of 14 aceAnalyiical wwwpace?abs com QUALITY CONTROL DATA Project Outfalls 1&2 Pace Project No.'. 92371337 QC Batch: 396702 Analysis Method: SM 4500-H+B QC Batch Method: SM 4500-H+B Analysis Description: 4500H+B pH EDEN Associated Lab Samples'. 92371337002 SAMPLE DUPLICATE: 2199481 92371337002 Dup Parameter Units Result Result RPD Qualifiers PH at 25 Degrees C Sid. Units 6.8 7.0 3 H1,1-16 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date' 02/0712018 03:40 PM without the written consent of Pace Analytical Services. Li Page 7 of 14 aceAnalytical iF www paceiabs. com QUALITY CONTROL DATA Project: Outfalls 1&2 Pace Project No.: 92371337 QC Batch: 396988 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description- 1664 SGT-HEM, TPH Associated Lab Samples'. 92371337001, 92371337002 METHOD BLANK: 2201373 Matrix: Water Associated Lab Samples: 92371337001, 92371337002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 02/07/18 04:34 LABORATORY CONTROL SAMPLE: 2201374 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sp)ke LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 17.9 90 64-132 MATRIX SPIKE SAMPLE: 2201375 92371544001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mgtL ND 20 19.0 93 64-132 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 02/0712018 03:40 PM without the written consent of Pace Analytical Services. LLC. Page B of 14 TaceAnalytical J W^.paceiabscom QUALITY CONTROL DATA Project: Outtalls 1&2 Pace Project No.: 92371337 CC Batch: 396571 Analysis Method: EPA 200.7 CC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92371337001, 92371337002 METHOD BLANK: 2198965 Associated Lab Sampfes: 92371337001, 92371337002 Parameter Units Copper ug1L Lead ug1L Zinc ug1L Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 02/06/1816:33 ND 5.0 0210611816:33 NO 10.0 02/06/1816:33 Qualifiers Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE: 2198966 Spike LCS LCS % Rec Parameter Units Cone Result % Rec Limits Qualifiers Copper uglL� 500 496 99 85-115 Lead uglL 500 468 94 85-115 Zinc ug1L 500 463 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2198967 2198968 MS MSD 92371596013 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Copper uglL NO 500 500 484 477 97 95 70-130 1 Lead ug1L NO 500 500 459 451 92 90 70-130 2 Zinc ug1L NO 500 500 456 448 91 89 70-130 2 Qual MATRIX SPIKE & MATRIX SPIKE DUPLICATE. 2198969 2198970 MS MSD 92371622010 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Resutt Result % Rec °% Rec Limits RPD Qual Copper uglL NO 500 500 483 486 96 97 70-130 1 Lead uglL ND 500 500 458 458 91 92 70-130 0 Zinc ug1L 3 01 500 500 478 482 95 96 70-130 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full. Date: 02107/2018 03:40 PM without the written consent of Pace Analytical Services, LLC Page 9 of 14 1�20Analyfica( www.pacelabs com QUALIFIERS Project: Outfalls 1&2 Pace Project No.: 92371337 DEFINITIONS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834�4964 DP - Dilution Factor. if reported. represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL- Practical Quantitalion Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodipheny lam ine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits Hi Analysis conducted outside the EPA method holding time H6 Analysis initiated outside of the 15 minute EPA required holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02107/2018 03:40 PM without the written consent of Pace Analytical Services, LLC Page 10 of 14 7 aceAnalytica! fwww pacelabs cam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Pace Project No.: Outfalls 1&2 92371337 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92371337001 Outfall f SM 2540D 396472 92371337002 Outfall 2 SM 2540D 396472 92371337002 Outfall 2 SM 4500-H+B 396702 92371337001 Outfall 1 EPA 16645 396988 92371337002 Outfall 2 EPA 1664E 396988 92371337001 Outfall 1 EPA 200.7 396571 EPA 200.7 396631 92371337002 Outfall 2 EPA 200.7 396571 EPA 200.7 396631 Date: 02/07/2018 0140 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 r n2,I Z Jr""" • Document Name: Sample Condition U Receipt(SCUR) Document Revlsed: January 16, 2018 Page 1 of 2 Issuing Authority: Document No.: F•CAR-CS-033-Rev, us Pace Carolinas Quality Office Laboratory ► eiving samples: As eville i ❑ Eden❑ Greenwood Huntersullle Raleigh Mechanicsville(] LilentNarrte: 611-Fe.c WO# : 92371337 k Project q: Courier: ❑FadUPS USPS ❑Ciient i I ❑ Commercial ace 00ther. Custodv Seal Pros ❑Yes Intact? 92371337 nt? Seals ❑Yes No Dale/lnkiihPeron ExamSning[ententsr: c �3 Packing Material: Thermortf,eat.er: ❑Bubble Wrap PK-6bi Bags []None ❑ othor BialogiCal Tissue Fro Dyes ❑Nq IaJ IR Gu 10: type of Ice: of ❑gtue N/A ❑None Conor (1,U4 r[15amptes Cooler Temp Corrected ('CI Temp should be above freezing to 6'C out of temp criteria Samples an iu, cooling process ! `�^ I has beg -in USDA Regulated L oil I A, water sample} Did samples origins quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples onginale from a foreign source (internati rhees 1—r ...VNn Camments/til Chain of Custoi IV Present? res No N/A i. Samples Arriv I within Hold rime? No N/A 2. ShonHold Tin* Mal B(c72hr. ? Dyes o N A 3. Rusin Turn Am nd Time R uested7 Yes G3<0 JZ)N/A a. Sufficient Volui ie7 es QND N A S. Correct ContAit iets Used? -Pace Contal°�oers Used? rS es ❑Np No ❑N/A N A G. Containers QND N A 7. Dissolved anaiy is: Samples Field Filtered? FIVOS No /A B. Sample Labels latth COO -includes Da me/10/Analysis Matrix: s ■ e []NO []NIA 9. Head ace In V A Vials (>5-6mm)? es MP40 ++/A 10. Trip Blank Prase t? Trip Blank Cult y Seals Present?[]Yes Dyes ONO No N/A N A 11. CLIENT Person contacted; Project Project Menage Note: Whenever the Out of hotd, incorrect DISCREPANCY Date/Time; Lot ID of split containers: Fieia pate RequottC / LJYes LjNe SCURFRenrlew: r:�� - Date:'�-- r SRF Review; Pate: 4 a discrepancy affecting North Carolina compliance samples, a copy of this form wilt be sent to the North Carolina DEHNR Certification OffRe (i-e. reservative, out of temp, incorrect containers) o_ a b R s �a = v w a re o n Q � d 19 a . t^ 3 � ro v w Items BP411.125 ml Plastic Unpreserrmd (N/A1(0-1 BPW-250 mL Plastic Unpreserved (N/A) 6P2U-500 mL Plastic Unpreser ed (NIA) $PIU-1 hter Plastic Unpreserved {N/A) - 9POS-125 mL Ptastk H$50a (pH < 2J (CI-) 6a3N-250 mL plastic HNO3 (pH < 21 6P42-125 mL Plastic ZN Acetate & NaOH (>9) $W-125 mt Plastic NaOH (PH > 1,11 (a -I WGFU-Wide-mouthed Glass Jar Unprrssurved AGI -1 liter Amber Unpresmved (NfA) (C-) AGIN-1 titer Amber HCI Jpk < 2) AG3U-250 mL Amber Unpreserved (N/Af JG-1 AGIS-1 Mer Amber H2504 (pH < 21 A153�,250 ml. Amber H2504 (PH < 2) AG3A(1>63A)•ZSA mL Amber NH4p (N/A)(O-) UGSH-40 mL VOA HO (NIA) VG9i40 m L VOA Nut 5203 (N jA) VG9W0 mL VOA Unp (N/A1 DG9P.40mL VOA H3PO4 (N/A) Vanat (6 vkk per kit)-5035 kit (N/Al W69 13 Willis Pur kit)-VPHJGas kit (N/AJ SPST•125 mt 5terlie Plesuc (NIA —tab) SPIT-2S0 mL Sterile Plaoc (N/A —lab) tlP3A-250 mL Ptaslk (N H2)2504 (9.3-9.7) Culdtalner VSGU-20 K SOMIllation vials (N/A) GN o � a: n v r a 8 M Q a 2 m ♦.a J 0 � � w n w S j N0 9 !f 3 0. Y O c b � W o m A + _ N t+ fJ Oo CHAIN -OF -CUSTODY I Analytical Request DocumaM Tne Chew -a -Cw>aM Is LEGAL DOCUAtEWT. Om rwov" rlwh ".0 the wmpWim --slay f4 44er CYwq 1A(WI SUOn' aw �a Wvpa �onrat�on hh[ Whom. Muwm 2— 6115 Ctwipei HID Raved To Dan AleOdy'dmoo6�recri�mm" r ro: a a%Ccontachm.tarn pwomage OrrbrNO: WA, one 91V BSI -DIED Pax- NWWL !!!A pares ow dywtAT: wtm anaar. NurtWr WA D vaud Rttrk Celia 2 aver+c.a.v rnrr.ru. W AW C94E o yd� COLLECTED 9.• roan : f �y d � D —Tm 6 mlk VfF wn PPOMCT P 74f U �] Co murc 6T.wT 00WO rT{ 040"s Fes' y� 6OlAttO % a SAMPLE: ID vm (o MUST n oT Tr-su ` $Qrprr'Do Wi157 BEE L1HtOufi � O U Ir ¢ U W G OetY6 TW@ MTE 3MIf OutfaEll wT 6 n M 4 1 + Outfail 2 tivT o1 i/10 9 -NCC PNWT the of AAIPPLEfe UOIMT1111@ of A+lMPI.IR: �� Ipow W ... In OVP a*Ch EroksweFed $akdmakrs - Npms r- a%ouw wkTv f DR1NKwa vwkT6R (- UST 1 RCRA r OTHER A B10rM }Yi NC woosIN N N pi � pAEp pr t Na.) Lob iL. I � i 0 v c a :• 0 Semi-annual Stormwater Discharge Monitoriniz Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 1 /- 13- 1-7 CERTIFICATE OF COVERAGE NO. NCG030 ,� 9 FACILITYNAME C,,Jech cn r COUNTY Wa t1C R_ PERSON COLLECTING SAMPLES G r c LABORATORY Joa ce Aoq !„ f: ra; Lab Cert. # 1.Z06 —C/1 -7 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR a 0' 1 —7 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ©monthly' (month) DISCHAR61NG TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA o P ❑Zero -flow [:]Watersupply ❑SA �`► �,�41T ❑Other G W � -MEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 D fNo discharge this period?2 Outfal! No. bate Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks =__> _ - 100 mg/L or 50 mg/0 6.0 — 9.0 0.007 mg/L 0.033 mg/l. 0.067 mg/L 15 mg/L 1 mg/L ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. f4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent'Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 I,1 • Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit.hor those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." C� a/les wolTe Name (Print name) 1 IRr,~f gart a Title (Print title) 11-13_l-7 (Signature (Date) i I Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. s. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. 'i Part B: •Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. I n No discharge this period?z I x; Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies_ Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar o&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 -- 9.0 SU 7,} I Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 0 0 0 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ } REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMIi including all "No Discharge" reports, within 30 days of receipt of the lab results tor at end of monitoring eriod in the case o "No Discharge" reports) to: . Division of Water Quality Attn:;DWQCentral Files _., 1617 Mail Service Center f Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." /// 49!� _ (Signature of Permittee) _y-13-t7 (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 e NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit. bttp://portal.ncdenr.or-/web/�ws/sub nndessw#tab-ii Permit No.: N/C/_/_/_/_/_/_/^/ or Certificate of Coverage No.: Facility Name: C'a_ C& ICA County: —IA.Aa ,� ` Phone No. Inspector: Date of Inspection: REGFIVED Time of Inspection: oEp 0 a nr Total Event Precipitation (incgfi§]TRAI CIF c!� DWR SEC p Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A `representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no i precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the ipermitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. ' By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature,oermittee or Designee) Page l of 2 SWll-242, Lak rT oMJ&d io/25/2012 1. Outfall Description: Outfali No. I Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. -,Page 2 of 2 SM-242, Lastmodified 10/25/2012 -" ��A NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: I-itp://12ort ii.ncdenr.or /� web/wq/ws/su/npde�sw#lib—,t Permit No.:/�/_/_/_/ ,/_/_/_/ or Certificate of Coverage No.: Facility Name: So County: Phone No. 11 q , 8,5-j'" ZBo Inspector: Date of Inspection: Time of Inspection: Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ❑ Yes 0 No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no j precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Sign atur�ermittee or Designee) Page 1 of 2 SWU-242, Last modified 10/25/2012 .— _- 1. Outfall Description: Outfall No. ..5 Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of Floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. - Page 2 of 2 5WU-Z42, LastmodiNi d 10/25/201Z r Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted — 17 CERTIFICATE OF COVERAGE NO. NCG03_O 3 q Z FACILITY NAME Ct;,lkcl�_ F ne?ram _-5 ut&� COUNTY _ LL a.i►-.C.. PERSON COLLECTING SAMPLES LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2-o ( -7 SAMPLE PERIOD ❑ 1 -June July -Dec or onthly' Si' month � �Iftllo {GING TO CLASS ❑ORW HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA SEP 4 6 2017 [-]Other CENTRAL CTiON PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -a �o discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids ,pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks ===> _ 100 mg/L or 50 mg/L 6.6 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 3 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. Tfie solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for totai toxic organics (TTU), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." I've —Name (Print name) lM 4t.ti.a ¢{r.._- Title (Print title) (Signatur (Dare) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format, When results are below the applicable limits, they must be reported In the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: 1f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected, (mo/dd/yr) 2446ur rainfall amount,. Inches"_;.. _. Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or So mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mailon oriainal and one copy of this DMR, includina all "No Discharae" reports, within. 30 days of receipt of the lab results or at end of monitoring period in the case of Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Pe 9 -s-1 7 (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 A A� NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit.' http://porL-,il,uQdenr.u-rg/-w—eb/wQ/ws/sLi/ni2de.ssw4tzib-4 Permit No.: N&/_/_/_/_/_/_/_/ or Certificate of Coverage No.: Facility Name: Ooj Mck-i of 6o1`o,-_S County: _ kJa ke Phone No. Inspector: Date of Inspection: Time of Inspection: Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ❑ Yes No RECEIVE, SEP 0 6 Please verify whether Qualitative Monitoring must be performed during a "rep?W ntative storm event" or "measureable storm event" (requirements vary, depend'.�� p 1 lttlf' Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Piease refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office._ By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature ofiittee or Designee) Page 1 of Z SWU-242,.Lastm'odified 10/25/2.012 1. Outfall Description: Outfall No. i Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No B. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 - —� Semi-annual Stor_mwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 9 - ;- - I T CERTIFICATE OF CO ERAGE NO. NCG03 ® J ? Z FACILITY NAME I -�eG1, COUNTY PERSON COLLECTING SAMPLES LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2-01-7 SAMPLE PERIOD ❑ J -June ❑ July -Dec or [�Monthly' month DISCHARGING TO CLASS ❑ORW ❑H W [-]Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other RECEIVED PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -i SEP 06 Z011 CINTiP1L FILEF,MNo discharge this eriod?z n�ni'� �f=a^�'inni 9 P Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids - pH, ' Standard units - Copper - Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L Z ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Cha-le- s (,J'.i -'- Name (Print name) _ Pja*_ —. Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mjz/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note, If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Y§,,1io discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) ' 24-hour rainfall amount,. Inches; :. ,:. Non -polar O&G/TPH by EPA .1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 5.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES [-]NO[-] REGIONAL OFFICE CONTACT NAME: Mail an original and one copy o this DMR includin oll "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MIDST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 'FOO200'r (Signature of (Date) Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 3 of 3 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: h r -i.l.n nr. r w w w n w#t-1 -4 Permit No.: N/C/_/_/_/�/_/_/_/ or Certificate of Coverage No.: N/C/G/Q/ 3/ 0/ Z/ Facility Name: Lor]-C-4 �rlgfnee,-ed SolL KF-J County: f,Uakp-- Phone No. Inspector: Date of Inspection: Time of Inspection: Total Event Precipitation (inches): } Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ❑ Yes *No V t i �p ! �fl Please verify whether Qualitative Monrtdri4r))neotl pe"pperformed during a "representative storm event" or "measureable storm even rf iqq irements vary, depending on the permit). Qualitative monitoring requirements vary. MoMermits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of rmittee or Designee) Page 1 of 2 5wi1-242,Last modified 10/25/2012 1. Outfall Description: Outfall No. Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4, Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWll-242,Last modified to/25/2012 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 9 - / —7 CERTIFICATE OF COVERAGE NO. NCG03D (). 0 G Q 3M(7 3 FACILITY NAME Cnd ecA» S 4r en s COUNTY Wa I< 2 PERSON COLLECTING SAMPLES Choe/tS t lol0P•f LABORATORY PQce AnitU.ra1 Lab Cert. #!A(36-O!!-7 Comments on sample collection or analysis: Neso _Q-ttwls-re/rdeol 6y NcD%A/Rg read Wenl--e Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR v-L' / SAMPLE PERIOD ❑ Jan -June ® July -Dec � O''fF'll '� 3 or © Monthly' jr<4 �t02 9 cr (month) C "tf.,110 � DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [:]WaterSupply [:]SA RECEIVED ❑Other SEP 2 5 2017 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTI`P.I_ FiI-ES GWR SECTION ❑ No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L I a y /06//7 0. s- , . 3 INS N io ! . a a. A/ D A/ A t 09 06/1 0.5- 33 -7.9 0.037 0•0z9 !- 6 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement, ' See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22;.and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: ,"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." l C h Rr/P.S 1�h r'Q i Name (Print name) of i Plant ,/'ran4�9tr' o Title (Print title) 9-ate-/ -7 (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, NO, or other similar non -numerical format. When results are below the applicable limits, ihey must be reported in the format "<XX mg/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. !Vote: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===a _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 5U Footnotes from Part A also apply to this Part EI * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART Ii SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO f IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copv of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case o "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files I 1617 Mail Service Center I � Raleigh, North Carolina 27699-1617 4f YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: € "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to ' assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm' ee) (Date) I 7 ' t j 'k Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Arja NCDENR 40 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report • Forguidance on filling out this form, please visit: -1 . r, r w w w d w# a -4 Permit No.: N/C/�/�/,/�/_/_/_/ or Certificate of Coverage No.: N Facility Name: Co nfe vi r r So/vI J&r7 I County: VVft k G Phone No. % 19' S.SI - $ TO Inspector: Gh Ic K h✓� ��'�_ _ _ Date of [nspection: Time of Inspection: N Total Event Precipitation (inches): %' f Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "meosureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, i some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains anproval from the local DWp Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature oi�Xmittee or Designee) SWU-242, Last modified 10/r)/2012 Page i of 2 1. Outfall Description: le Outfali No. I Structure (pipe, ditch, etc.) TP Receiving Stream: S Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium; dark) as descriptors: C / Qo(r 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 110 sl 2 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 01 & 3 4 5 6. " Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 O2 3 4 5 7. Is there any foam in the stormwater discharge? Yes (DO 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. • • Page 2 of 2 SWU-242, Last modified 10/25/2012 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out thisform, please visit. >iLp-/j. portal.ncdenr.org/web/wgjwsjsu jnpdessw#tab-4 Permit No.: N%�/_/_/_/_/_/_/�/ or Certificate of Coverage No.: N/-C/G FacilityName: o ec ; n S Ic, -, County: Wak t- „Phone No. 9/9- S`-f- Qet C Inspector: G .tr_ we lee _ Date of Inspection: .- 6- /7 Time of Inspection: Total Event Precipitation (inches): 0- f- " Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) -Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). eQualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. • A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at:least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from'the local DWQ Regional Office. By this signature, I certiN-that this report is accurate and complete to the best of my knowledge: (Signatur �ermittee or Designee) 5WU-242, Last modified 10/25/2012 Page 1 of 2 1. Outfall Description: Outfall No. 3 _ Structure (pipe, ditch, etc.) 'e Receiving Stream: • Describe the industrial activities that occur within the outfall drainage area: 2, Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: & ro %W ✓n 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ✓1 o n e _ 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3D 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: O' 2 2 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 O 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes D 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and) describe Se Ui med ter tm GGr-'yr /y arr_f f' Co-n"gz C Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. 0 Page 2 of 2 SWU-242, Last modified 10/25/2012 4PAnalytical www.pacelabs.com September 21, 2017 Mr. Chuck Wolfe Contech 6115 Chapel Hill Road Raleigh, NC 27607 RE: Project: Outfall Sampling Pace Project No.: 92354285 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834.4984 Dear Mr. Wolfe: Enclosed are the analytical results for sample(s) received by the laboratory on September 07, 2017. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. -- Pagel of 15 __ ace Analytical www.parelabs eom Project: Outfall Sampling Pace Project No.: 92354285 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 LouisianalNELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Dnve, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Certification 9: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #, 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 North Carolina Wastewater Certification #, 633 VirginialVELAP Certification #: 460025 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, - -_ without the written consent of Pace Analytical Services, LLC. , Page 2 of 15 aceAnalytical www pacelabs. can SAMPLE ANALYTE COUNT Project: Outfall Sampling Pace Project No.: 92354285 Lab ID Sample ID Method 92354285001 Outfall 1 SM 2540D SM 4500-H+B _ EPA 1664B EPA 200.7 92354285002 Outfall 3 SM 2540D SM 4500-H+B EPA 1664E EPA 200.7 REPORT OF LABORATORY.ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. LLC. Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Analysts Analytes Reported Laboratory CTB 1 PASI-E NMH 1 PASI-E JMS 1 PASI-C SH1 3 PASI-A CTB 1 PASI-E NMH 1 PASI-E JMS 1 PASI-C SH1 3 PASI-A _Page_3 of 15_ __ aceAnalytical www.parerab&=n ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919?834-4984 Project: Outfall Sampling Pace Project No.: 92354285 Sample: Outfall 1 Lab ID: 92364285001 Collected: 09/06/17 16:00 Received: 09/07/17 08:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Total Suspended Solids 4500H+ pH, Electrometric EDN pH at 25 Degrees C 1664 SGT-HEM, TPH Total Petroleum Hydrocarbons 200.7 MET ICP Copper Lead Zinc Analytical Method: SM 2540D 6.3 mg1L 2.7 1 0911211713.08 Analytical Method: SM 4500-H+B 6.7 Std. Units 1.0 1 09/08/17 16.03 H1,H6 Analytical Method: EPA 1664B ND mg1L 5.0 1 09/20/17 0537 Analytical Method: EPA200.7 Preparation Method: EPA200.7 ND ug1L 5.0 1 09118/1718:45 09/20/1718:12 7440-50-8 ND uglL 5.0 1 09/1811718:45 09120/1718:12 7439-92-1 1220 uglL 10.0 1 09/18/1718:45 09120/1718:12 7440-66-6 _. ._ REPORT OF LABORATORY ANALYSIS _ This report shall not be reproduced, except in full, ' Date: 09121/2017 03:44 PM without the written consent of Pace Analyticai Services, LLC. _ _ Page 4 of 15 aceAnalytical www,pacelabs.00m ANALYTICAL RESULTS Project: Outfall Sampling Pace Project No.: 92354285 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Outfall 3 Lab ID: 92354285002 Collected: 09106/17 16:00 Received: 09/07/17 08:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Oual 2540D Total Suspended Solids Analytical Method: SM 254017 Total Suspended Solids 332 mg/L 16.7 1 09112/17 13:09 4500H+ pH, Electrometric EDN Analytical Method: SM 4500-H+B pH at 25 Degrees C 7.9 Sid. Units 1.0 1 09/08/17 16:03 H1,H6 1664 SGT-HEM, TPH Analytical Method: EPA 16648 Total Petroleum Hydrocarbons ND mg1L 5.0 1 09/20/17 05:37 200.7 MET IC Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 37.0 ug1L 5.0 1 09/18/1718:45 09/20/1718:24 7440-50-8 Lead 29.6 ug1L 5.0 1 09/18/1718:45 09120/1718:24 7439-92-1 Zinc 1620 ug1L 10.0 1 09118/1718:45 09120/1718:24 7440-66-6 _ Date: 09/21/2017 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. x. __ _ _Page 5-,0f 15 __ acmnalytical www pacelabs mm QUALITY CONTROL DATA Project: Outfall Sampling Pace Project No.: 92354285 QC Batch; 377329 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92354285001. 92354285002 METHOD BLANK: 2090572 Matrix: Water Associated Lab Samples: 92354285001, 92354285002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 09/12/17 13:07 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-49B4 LABORATORY CONTROL SAMPLE: 2090573 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 262 105 90-110 SAMPLE DUPLICATE: 2090574 Parameter Total Suspended Solids SAMPLE DUPLICATE: 2090575 Parameter Total Suspended Solids Units 92354285002 Result Dup Result mglL 332 330 Units 92354394001 Result Dup Result mg1L 464 497 RPD Qualifiers 1 RPD Qualifiers 7 D6 Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS -This report shall not be reproduced, except in full, Date: 09/21 /2017 03A4 PM without the written consent of Pace Analytical Services, LLC. _ Page 6 of 15 aceAnalytrcal www.pacefabs.com QUALITY CONTROL DATA Project: Outfall Sampling Pace Project No.: 92354285 QC Batch: 376971 Analysis Method: SM 4500-H+B QC Batch Method: SM 4500-H+B Analysis Description: 4500H+B pH EDEN Associated Lab Samples: 92354285001, 92354285002 SAMPLE DUPLICATE: 2088568 92354285001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.7 6.7 0 H1,H6 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY -ANALYSIS T This report shall not be reproduced, except in full, Date_09121/2017 03:44 PM without the written consent of Pace Analytical Services, LLC. Page, 7 of 15_ aceAnalyfical www pacelab ccm Project: Outfall Sampling Pace Project No.: 92354285 QC Batch: 378467 QC Batch Method: EPA 1664B Associated Lab Samples: 92354285001, 92354285002 METHOD BLANK: 2097011 Associated Lab Samples: 92354285001, 92354285002 Parameter Units Total Petroleum Hydrocarbons mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 09/20/17 05:25 Pace Analytical Services, LLC 6701 Conference drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE & LCSD: 2097012 2097013 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Cone. Result Result % Rec % Rec Limits RPD RPD Qualifiers Total Petroleum Hydrocarbons mg/L 20 18.9 19.5 94 98 64-132 3 30 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. — REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/21/2017 03:44 PM without the written consent of Pace Analytical Services, LLC.--_ _ 4 W Page 8 of 15 Y � acmnalytical www,pacelabs.com QUALITY CONTROL DATA Project: Outfall Sampling Pace Project No.: 92354285 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QC Batch: 378210 Analysis Method: EPA 200.7 OC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92354285001, 92354285002 _ .. METHOD BLANK: 2095650 Matrix: Water Associated Lab Samples: 92354285001, 92354285002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 09120/1717:50 Lead ug/L NO 5.0 09/20/1717:50 Zinc ug/L ND 10.0 09/20/1717:50 LABORATORY CONTROL SAMPLE: 2095651 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L Soo 499 100 85-115 Lead ug/L 500 494 99 85-115 Zinc ug/L 500 494 99 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2095652 2095653 MS MSD 92354257001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug1L ND 500 500 492 494 98 98 70-130 0 Lead ug1L ND 500 500 496 486 99 97 70-130 2 Zinc ug/L 125 500 500 618 603 99 96 70-130 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE-. 2095654 MS 92354314001 Spike Parameter Units Result Conc. Copper ug/L 20.0 500 Lead ug/L ND 500 Zinc ug/L 73.3 500 2095656 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 539 517 104 99 70-130 4 500 493 478 98 95 70-130 3 500 577 547 101 95 70-130 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY_ ANALYSIS This repoo shall not be reproduced, except in full. Date: 0912112017'03:44 PM without the written consent of Pace Analytical Services, LLCJr 777 Qual __ Page 9_of 15 ._� _ axAnalXical ® www,pacoobs mn QUALIFIERS Project: Outfall Sampling Pace Project No.: 92354285 DEFINITIONS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)a34-4984 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. - MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI•E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. —REPORT OF LABORATORY ANALYSIS " 'This report shall not be reproduced, except in full, Date: 09/21/2017 03:44 PM - -t - without the wntten consent of Pace Analytical Services, LLC. _-- T Page 10 of 15 acMnalytical www.pacelabs aom QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Outfall Sampling Pace Project No.: 92354285 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834A984 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92354285001 Outfall 1 SM 2540D 377329 92354285002 Outfall 3 SM 2540D 377329 92354285001 Outfall 1 SM 4500-1-1+13 376971 J 92354285002 Outfall 3 SM 4500-H+B 376971 92354285001 Outfall 1 EPA 1664B 378467 92354285002 Outfall 3 EPA 1664B 378467 92354285001 Outfall 1 EPA 200.7 378210 EPA 200.7 92354285002 Outfall 3 EPA 200.7 378210 EPA 200.7 - REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, Date: 09/21/2017 03:44 PM without the written consent of Pace Analytical Service-s, LLC. _ �_: — Analytical Batch 378267 378267 Page .11_of 15 Document Name: • Document Revised: August 4, 2017 Sample Condition Upon Rece' t(SCUR) Page 1 of 2 Document No.: Issuing Authority: . F-CAR-CS-033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ . Eden . GreepWQgd �. _._Hs�nit:rslrills ❑ ftalslgb '-_—. Naecttani uill�❑.. Upon ReCeipt Client Name: Project A: WOW 92354285 Caur[er: Fade K ❑UPS ❑ Commercial ❑Other. ❑tlient I� I II I II+I I �I� �'� ❑ 92354289 Custody Seal Present? ❑Yes Xo Seals Intact? Des]�Jnlo '�" �T (late/IIfta[s Person Examirkft Contenls:��-_____ Packing Material: []Bubble Wrap []Bubble Bags []None ❑ Other Biological Tissue Frozen? Thermometer. ❑Yes ❑No GOIA PLIR Gun ID: L type of Ice. ewet ❑Blue ©None Correction Factor: Cooler Temp Corrected (ICY 1.3 Temp should be above freezing to G'C .• d , ❑Samples out of temp criteria. Samples on Ice, cooling process hasbegun USDA Regulated Sall ( NJA, water sample) Did samples grlglpate in a uarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a fordan source (Ilonally, r1vns 11U. Comments/1131w n ; Chain of Custody Present? es NoCINIA 1. Samples Arrived within Hold Time? es []No EWA 2. Short Hold Time Ana s 42 hr.)? ove, N N/A 3. Rusty Turn Around Time Requested? Yes Ho N/A 4. Sufficient Volume? No UNIA S. Correct Containers Used? -Pace Containers Used? Y!K ❑No ONO []N/A QNJA 6. Containers Intact? 13f,ON- N/A 7. Dissolved ana sis: Sam es Field Filtered? No N/A 9. Sample tabs h Match CDC? -includes Date/Ttme/ID/Ana is Matrix; IfYes 4/1011/ []NO CjN/A 9. Neadspace in VOA Vials >5 6mm)? []Yes ❑No N A lo. Trip Blank Present? Trip Blank Cusco Seats Present? [3Yes Ely&& ONO ONO N/A NIA ll. CLIENT NOTIFICATION/RESOLUTION �, rt L Person Contacted: f a� Date/Time: CI—]— f FIeWRetaRequtred? []Yes ❑No Comments/Sample Discrepancy: cto �4- /()/e —Zm- ,— — Ny io�i l_�_-:!r&,wL A-'-4dcl �Cl @ 11 c,Lc) �(���1"1 CU, Cn GoC� Lot ID of split containers: [� Project: Manager SCURF Wow: i_J Date: Project Manager SRF Review: (11 Y F� _ Date: — 0 Nate: Whenever there is a discrepancy affecting North Carolina romptarice: samples, a cmpy of this form wilt be sent to the North Carolina DEHNR Cerllilcatlon Office (i.e. Out of hold, Incorrect preservative, out of temp incorrect oorrtalners) �. - Page 12 of 15 L' i I m CD rn � ro ,k r s C �a 8 Y rL A ro 3 a 3 O lQ fC h v 6 . l N �+ O ItarrHl � d1 < BP4U•12S mL PI25CtC Unpreserved (N/A);Q-) a OID �—� rL 3 610311.1-250 mL Plastic Unpreserved (N/A) T O al MU-506 mL Plastic Unpreserved (N/A) t I G 0 ti `-` 9&PfU-Miter PI35ttc Unpreserved (N/A) 'd A v, eMS-125 mL Plastic H2SO4 1pH < 21(Cy p � � r BP3r&250 mL plastic HNO3 IpH < 21 o_ n ` x J� BM-125 mL Plastic ZH Acetate & NaOH (>91 ! C Oil _ zzz ISM-125, ML Plastic NaOH (pH > 12) (0-) tv f0 WGPLFWide-mouthed Glass Jar Unpreserved o lT eDD p, AGIU-1 liter Amber Unpreserved (N/A) {CI-) 0 CD l 3 AGm-1 liter Amber HCl (pH < 2) H 0 T AG3U-250 mt Amber Unpreserved (N/A) (CI-) d aAo� aOn AGMI liter Amber H2504 (pH < 2) fj 3 rb w ^ AG35.250 mL Amber H2SO4 (pH < 2) AG3A(DGUA 250 mi.Amber NH4C1 (N/A)CCI-) i ro UG9H-40 mL VOA H Cl {N/A) a n V09i-40 mL VOA iva2S203 (N/A) y VGiSUiO nIL VOA Unp (N/A) C7 � DGSP-AD mL VOA H3PO4 IN/A) r~a 3 m VOAK (6 vials per klt).5035 kit (N/A) 1 3 W ro V/GK 13 vlela per kl*VPH/Gas ktt (N/A) N SP5T-125 mL Sterile Plastic (N/A - tab) n o SP2T-250 mL Sterile Plastic (N/A— lab) 3 / _ � ] y s v W+T. NW n r /� A r^ S 4 Vl o A HP3Jk-250 rnL Plastic (NH2)2SU4 {9.3-9.7) m �+ o Cub)hiner 4 ♦ o VSGt} 20 mL SCtntlRation vials (NIA) IUD �i 1 N ' GN ►+ r+ Page 1 of 1 Angela Baioni - RE: Collection date? From: "Wolfe, Charles" <CWolfe@conteches.com> To: Angela Baioni <Angela.Baioni cr pacelabs.com> Date: 9/7/2017 10:30 AM Subject: RE: Collection date? Yes — we collected 4PM yesterday evening 9/6/17 and put in fridge last night. Thanks for double checking From: Angela Baioni [Angela.Baioni@pacelabs.coml Sent: Thursday, September 07, 2017 10:22 AM To: Wolfe, Charles <CWolfe@conteches.com> Subject: Collection date? Hi Chuck, I hope you're doing well today! I have your samples in house, and the sample date on the COC says 9/7/17. The collection time on the containers is 1600, so I know one of those is not correct. We haven't hit 4pm today yet.:-) Can you confirm the date/time for collection? Thanks! Angela Angela M. Baioni Project Manager Pace Analytical Services, Inc. -Carolina Lab 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Direct Dial: 704-977-0939 Office: 704-875-9092 an ela.baioni acelabs. om www.pacelabs.cQm This email may contain confidential and/or privileged information. If you are not the intended recipient, you are hereby notified that retention, dissemination, or copying of this communication is prohibited. If you have received this email in error, please notify the sender by reply email and _ permanently delete this email and any attachments. Thank you. - -- - Page 14 of 15 '" file:///C:/Users/abaioni/AppData/Local/3'e'mp/XPgrpwise/59BI I B4PACE_DOMAINCHR... 9/7/2017 ' /!Zr-� � . AW"1ca nwwdwra..� ae.. Section A Reomlra (:hem Itifixn rerorr. I f CHAIN OF-CU—,, 7DY f Analytical Request Document The Chun-d-CU bdY is a LEGAL OOCUMENT. AG Iebrddd 48W must os aampewd amunaey. as rn IL I Section 9 secam c CumPa1T Contech Engineered Solutions P-PW TO: GtmrlaS Wolfe `CWotfeCjContadl9S.Gor Ra Wgh AIP Aaaesa 8115 Chapel Hill Road Coorlo: pen Moody "dmoody*oarYa0p.0Is1' Owpim Nome- Contach Engineered Sotubons AdINOW APC xft-rhRak40@corteChes.corn Ernd To Cwolfe@wnft0ws.=n RIIdM* Omw No,; NIA am" WA F%a1n�1Ea: Pnma. 919-851-261 PrwctName, WA NgCteBlorw hussm Due oade/TAT.' ISM IIme G-a d•Y Pryrd Nunwrr. MIA PauPw"fil 5628-1(LH) a RaquhW Chwd hamraalon MIN= am fl COLLECTED n•+.or�e+ua. cw 0 S . WATER KI O �-MmM T11 vWY FfRlAST P y y OOMOiR 4rAn1 COUPOe TE END126" sac-�aw 4 OL OL s SAMPLE ID {A-Z, 69I -) WrER OTIL O Semple IN MUST BE u1IlOUE c» u C) a s ?S IDATE TIME DATE TIME Outfali 1 %- Wr G rq na 4 s Outfail2 vVT c ra A 3 ❑ulFall i A— —2— I i wr r A e-- IY1-17 pwff 1, of elute+-,* C MMTURE of LW`LM- 7e1164M NOW 9T 5% rer w*M w arw j*OW not paid OM 71) dwfL "'Pik`•.%s%r'�rr•':,',��i�- :`Y,,�ii ■ Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 7- /Y- /? CERTIFICATE OF COVERAGE NO. NCG030 Q a _Q 03D3�_ SAMPLE COLLECTION YEAR a0 r —7 FACILITY NAME a Jam. �v C,i1s COUNTY (Al.,k e PERSON COLLECTING SAMPLES LABORATORY 20 C—e liqWzra Lab Cert. # 2,0 — a 7 Comments on sample collection or analysis: e&W ! selede&Z 6X A1C19,FJVA -Thqd V.1ed.-ie- Part A: Stormwater Benchmarks and Monitoring Results SAMPLE PERIOD © Jan -June ❑ July -Dec or ❑ Monthly' !month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA RECEIVED ❑Zero -flow ❑Water Supply ❑SA JUL 18 2017 ❑other CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 � DWR SECTION ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 061zi r r-7 0-Zs IU 0 Alp Al o 17 Al V A114 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." C A Qrl e-5 CJa/fie fir, Name (Print name) Title (Print title) 7— (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. !Vote: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfal[ No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, lnches3 !Von -polar O&G/TPH by- EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 Su Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 ' 0 0 0 s •. • Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART Il SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this AMR including all "No Discharge" reports, within 30 days s of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) %— (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 0 r-I • ��A A�=�� NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: hU11://nortaLncdenr.org/web/wq /ws/su/npdes5w#tab-4 Permit No.: N/-C/�- Facility Name: LG County: Inspector: Date of Inspection: Time of Inspection: a Total Event Precipitation (inches): o. as Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) EV�Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatuye, I certify t4at this report is accurate and complete to the best of my knowledge: (Sigv ture of PV ittWor Designee) 5WU-242, Last modified 10/25/2012 Page 1 of 2 1. Outfall Description: Outfall No. I Structure (pipe, ditch, etc.) �- Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the di2?26r rge using basic colors (red, brown, blue, etc.] and tint (light, medium, dark) as descriptors: L _ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _/)/�/7e1 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids: O2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may he indicative of pollutant exposure. These conditions warrant further investigation. Cl Page 2 of 2 SWU-242, last modified 10/25/2012 H Ai lacie Analytical wiw.pacelabscom July 03, 2017 Mr. Chuck Wolfe Contech 6115 Chapel Hill Road Raleigh, NC 27607 RE: Project: Outfall 1 (6/21/17) Pace Project No.: 92345094 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Mr. Wolfe: Enclosed are the analytical results for sample(s) received by the laboratory on June 21, 2017. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 aceAnalytical www.pwWabscom Project: Outfall 1 (6121/17) Pace Project No.: 92345094 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #. E87627 Kentucky UST Certification #: 84 VrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VrginiaNELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 VrginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in NIL without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 2 of 13 aceAnalytical wwwpacsMbs.com SAMPLE ANALYTE COUNT Project: Outfall 1 (6/21117) Pace Project No.: 92345094 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92345094001 Outfall 1 6121117 SM 2540D CTB 1 PASI-E SM 4500-H+B NMH 1 PASI-E EPA 1664E JMS 1 PASI-C EPA200.7 SH1 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 Pace Analytical Services, LLC aceMalytical ® 670t Conference 70 Raleigh, NC 27607 rnrwpaCVbbs.com (919)834-4984 ANALYTICAL RESULTS Project: Outfall 1 (6/21/17) Pace Project No.: 92345094 Sample: Outfall 1 6121/17 Lab ID: 92345094001 Collected: 06/21/17 07:00 Received: 06/21/17 13:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg1L 2.5 1 06/23/17 11:43 4500H+ pH, Electrometric EDN Analytical Method: SM 4500-H+B pH at 25 Degrees C 6.6 Std. Units 1.0 1 06/22117 14:45 H1,H6 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 06/23117 06:45 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND ug/L 5.0 1 06/27/1717:05 06/29/1716:27 7440-50-8 Lead ND ug/L 5.0 1 06/27/1717:05 06/29/1716:27 7439-92-1 Zinc 917 ug/L 10.0 1 06127/1717:05 06/29/1716:27 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/03/2017 07:00 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnalytical wwwpacalab.00m QUALITY CONTROL DATA Project: Outfali 1 (6/21/17) Pace Project No.: 92345094 QC Batch: 366270 Analysis Method: SM 25400 QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples? 92345094001 METHOD BLANK: 2030405 Associated Lab Samples: 92345094001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 2030406 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2030407 Parameter Units Total Suspended Solids mg/L Pace AnalyticaI Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 06123/1711:40 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 266 106 90-110 92345198001 Dup Result Result RPD Qualifiers 6.1 213 189 D6 SAMPLE DUPLICATE: 20304C8 92345150001 Dup Parameter Units Result Result Total Suspended Solids mg]L 600 600 RPD Qualifiers 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 07103/2017 07:00 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 (�Iacmnalytical wwwpacwabscom Project: Outfall 1 (6/21/17) Pace Project No.: 92345094 QC Batch: 366107 QC Batch Method: SM 4500-H+B Associated Lab Samples: 92345094001 SAMPLE DUPLICATE: 2029542 Parameter Units pH at 25 Degrees C Std. Units QUALITY CONTROL DATA Analysis Method: SM 4500-H+B Analysis Description: 4500H+B pH EDEN 92345094001 Dup Result Result RPD Qualifiers 6.6 5.6 1 H1,H6 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Date: 07/03/2017 07:00 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalytical" wwwpacdabs.com Project: Outfall 1 (6121/17) Pace Project No.: 92345094 QC Batch: 366181 QC Batch Method: EPA 1664B Associated Lab Samples: 92345094001 METHOD BLANK: 2029870 Associated Lab Samples: 92345094001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 2029871 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 5.0 06/23/17 06:32 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 20 19.5 98 64-132 MATRIX SPIKE SAMPLE: 2029872 92345060001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L NO 20 19.7 98 64-132 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/03/2017 07:00 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnalytical e www.pacefabs com QUALITY CONTROL DATA Project: Outfall 1 (6/21/17) Pace Project No.: 92345094 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QC Batch: 366578 QC Batch Method: EPA 200.7 Associated Lab Samples: 92345094001 Analysis Method: Analysis Description: EPA 200.7 200.7 MET METHOD BLANK: 2031983 Matrix: Water Associated Lab Samples: 92345094001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 06129/1715:05 Lead ug/L ND 5.0 06129/1715:05 Zinc ug/L ND 10.0 07/01/1716:19 LABORATORY CONTROL SAMPLE: 2031984 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper ug/L 500 501 100 85-115 Lead ug/L 500 495 99 85-115 Zinc ug/L 500 508 102 85-115 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2031985 MS 92345355002 Spike Parameter Units Result Cone. Copper ug/L 0.77 500 mg1L Lead ug1L 0.086 500 mg/L Zinc ug/L 8.6 500 mg/L 2031986 MSD Spike MS MSD MS MSD % Rec Cone. Result Result % Rec % Rec Limits RPD Qua{ 500 1270 1330 100 112 70-130 4 500 566 598 96 102 70-130 6 500 8940 9500 68 182 70-130 6 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2031987 2031988 MS MSD 92345596008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 494 523 99 105 70-130 6 Lead ug/L ND 500 500 509 526 102 105 70-130 3 Zinc ug/L ND 500 500 511 537 100 105 70-130 5 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except m full, Date: 07/03/2017 07:00 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 (�15'ne Analytical WWpacWabs.com QUALIFIERS Project: Outfall 1 (6121117) Pace Project No.: 92345094 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. POL - Practical Ouantitation Limit. RL - Reporting Limit. Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. M6 Matrix spike and Matrix spike duplicate recovery not evacuated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/03/2017 07:00 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 acemamical wwwpacefabacvm QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Pace Project No.: Outfall 1 (6/21117) 92345094 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92345094001 Outfall 1 6121117 SM 2540D 366270 92345094001 Outfall 1 6/21117 SM 4500-H+B 366107 92345094001 Outfall 1 6121117 EPA 1664B 366181 92345094001 Outfall 1 6/21117 EPA 200.7 366578 EPA 200.7 366958 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07103/2017 07:00 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 uacument Name: t,SI Iecn bpec uocument Kevlseo_ Sept. eL, ZULo 8C81 male Sample Condition Upon Recel t(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-QA-003-Rev.02 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Sample Condition Upcil Client Name: Pt Rerofi Project N. Courier: Eed Ex []UPS❑USPS Client ❑ Commercial Pace ❑Other: Custody Seal Present? ❑Yes 06 Seals Intact? ❑Yes io Raleigh® Mechanicsville❑ WO#:92345094 III III 111111111111111 92345094 Oate/Initials Pawn Examining Contents: Packing; Material: Bubble Wrap []Bubble Bags ❑None ❑Other Thermometer: YJ ® IR Gun ID: _IS-3492 — Type of Ice; et ©Blue ❑None ❑Samples on ice, cooling process has begun Correction Factor: sub -a I Cooler Temp Corrected ('C): d , f Biological Tissue Frozen? []Yes ❑No /A Temp should be above Wfe ezingtoVCUSDA Regulated Soil (NIA, water sample) Didsample��s[PrtgtnateInuarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, ❑Yes Mo Including Hawaii and Puerto Rico)? ©Yes ILV10 Comme nts/Olscrepancy: Chain of Custody Present? i. Samples Arrived within Hold Time? 0 El2. Short (fold Time Analysis (c02 hrJ? 3. Rush Turn Arwnd Tlme Requested? Z D 4. Sufficient Volume? © 11 5. Correct Containers Used? -Pace Containers Used? ❑ 6- Containers I ntact? �8. 7. Samples Field Filtered? LJ ET Note if sediment is visible In the dissolved container Sample Labels Match COC7 -Includes Date/rime/ID/Analysis .- 4. Headspace in VOA Vials >5-6mm)? Yes No N A 10. Trip Blank Present? Trip Blank Custody Seals Present? Yes No ❑ ❑ Yes No N A N 11. CLIENT NOTIRCATION/RESOIUTION Field Oats Required? UYes UNo Person Contacted: I Date/Time: Comments/Sample Discrepancy: Project Manager SCURF Review: Date: f % Project Manager 5RF Review: 111 j Date: -- None: whenever there Is a dLtcrepancy Wading North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i,e. Out of hold, incorrect pseservative, out oftemp, incorrect container) Page 11 of 13 rV O W e x 7 x i o � is o � � 3 D a R n O V n � LSD • a o 7 m � 3� 6 s C a • a N O W m -Q a, w a w N Iterna BR4U-125 mL Flastic Unpreserved (N/A) (Ct-) MU-250 ml Plastic Unpreserved IN/A) BPZU-SW mL Plastic Unpreserved ( N/A) BPIU-t liter Plastic Unpreserved (N/A) BP°-5-250 mi. Plastic H2SO4 (pH <2) iCi-) BP3N-250 mi. plastic HNO3 (pH < 21 BP32-250 ml Plastic ZN Acetate & NaOH (>% zzBP3C 250 mL Plastic N20H (pH > 12) (Cl-) LVGFU•VJlde-mouthed Glass jar Unpreserved AGiU-1 liter Amber Unpreserved (N/A) (CI-) -r AG1H•1 liter Amber MCI ipH c 2} AG31.0-250 mL Amber Unpreserved (N/A) (CI-) AGIS-1 liter Amber H2504 (pH < 2) AG3S-250 mL Amber H2504 (pH < 2) AG3A(OGUA -250 m L Am ber NH4Cl (N/A)(CI-) 069H-40 mL VOA MCI (N/A) VGST-40 m L VOA Na2.S203 (N/A) VG9U-40 mL VOA Unp (N/A) DG4P-40 rnL VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per ldt)•VPH/Gas kit tN/A) SPST-225 ml. Sterile Plastic (N/A — lab) SPIT 250 mL Sierlle Plastic (N/A —tab) BA3A-250 mL Plastic (NH2)2SO4 (9.3-9.7) Cubitaln r VSGU-20 rnL Scintillation vials (NIA} GN O � O -ft 3 v X 4A 3 �. O fP g 3 a 3 2 A ro 0 p li g A a M K p � � � S H 0 d O 2 V n m 0 3 v 06 C z � w C 0 ,. z � = N Z r C a dDC-0E-CUb )DY ! Analytical Request Document / o ce d"4kW " .c tueeouy h a LEGAL DOCUMENT. AN mbv" fWib "M be —00W roars"e . � s!1 Ca I. i ORlNKfNG WATER S7 riyy � ,'srrJ.t'� S r � /ii�.,%l"-%S' %' Yam i� //ir � --ls�. y� jay ``!,✓ i✓ Sk SAMPLE 1 Adt APO i MUST TZ So on •- BE UhkQLJE i'i11V1�a� rr e..�wr�wrr�er.r.r.� w�.aw.r�..aw•�•�•��r���� ,ff���f�rl��� ���;a� /.•A Il.�f�'s[II��'`.J�'�C��*�i'ii ©F� --------- - ----------------- �npaur. tract Bl .�nt,0 0da fartse you .n erupYq P•n'. NET y] aY P.Y�y NM. &W ogre" [o fm aM11..lw 1,5% W mm rxvvftwd0wpNww*30 a". F-ALL-0-02OMV-08, 12-0t1-2007 • • 9 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 / 3q DDe submitted NC& 03 CERTIFICATE OF COVERAGE NO. NCG03 Q �VCV �� SAMPLE COLLECTION YEAR FACILITY NAME_ Co i fcc� S SAMPLE PERIOD X❑ Jan -June ❑ July -Dec COUNTY a or ❑ Monthly' month PERSON COLLECTING SAMPLES na� f'ca 1 DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout ❑PNA a2 LABORATORY face o., Cd Lab Cert. # I;L06 []Zero -flow ❑Water Supply [:]SA Comments on sample collection or analysis: ❑Other pace Rcsulls ojlartieilAt COA EASEREMEMBERTO SIGN ON PAGES2AND/OR3 Part A: Stormwater Benchmarks and Monitoring Results ❑ Na discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks 100 mg/L or 50 mg/L' 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. for those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." GkQ.-/es W-I e Name (Print name) P�qn! /] ar)a���� Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX mg/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 0 0 Page 2 of 3 0 0 0 0 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AAND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO Q IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of recei t of the lab results or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date: 11/1/2012-10/31/2017 3 -4-14 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 • ff-j';'Av .� .NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: ]ittp;//VQrtal.ncdeiir.oi-g/wawa/wsfujtipdQSsw�, 4ttab_4 Permit No.: IV/C/_/_/_/_/_/_/_/ or Certificate of Coverage No.: Facility Name: Go n)ee r n �, i » e ercd .5 County: o,,P=-e- Phone No. 919 - FS/-_a-$SG_ _ Inspector: P ace _ ,na1�a _ Date of Inspection: Time of Inspection: Total Event Precipitation {inches): 1- 0 �a f MAY 10 Z016 Was this a "Representative Storm Event" or "Measureable Storm Event"" VVRI SECTlQN permit? (See information below.) W SECTION ® Yes ❑ No Please verify whether Qualitative Monitoring must he performed during a "representative storm event" or "measureahle storm event" (requirements vary, depending on the permit). 'I Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Per1e or Designee) Page 1 of 2 SWU-242, Last modified 10/2S/2012 1. Outfall Description: Outfall No. _. I Structure (pipe, ditch, etc.) �� ��h Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 16KOW" f /�7 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Ah n 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 (D 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1@ 2 3 4 5 h. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 02) 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes N� 10. Other Obvious Indicators of Stormwater Pollution: List and describe N ° +I e Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 9 SWU-242, Last modified ] 0/25/2012 Semi-annual Stormwater ni? Re Discharge Monitoring Report lII ,p .gyp for North Carolina Division of Water Quality General Permit No. NCG030000' Date submitted 3 a 3q CERTIFICATE OF COVERAGE lNO. NCGO3� Q 0/ SAMPLE COLLECTION YEAR a r FACILITY NAME GQ i tech )57n i; efreO� .So /v T ; SAMPLE PERIOD ❑ Jan -June [g July -Dec COUNTY 4a1R k --e- or ❑ Monthly" (month} PERSON COLLECTING SAMPLES DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY Lab Cert. # RECEIVED ❑zero -flow [:]Water Supply ❑SA Comments on sample collection or analysis: ❑Other DEC 2 8 2016 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL ALES Part A: Stormwater Benchmarks and Monitoring Results DWR SECTION FANo discharge this period: Outfall No. Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For.purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." C,� at WO Name (Print name) P/anlAn�o��r Title (Print title) /Q_OC_ /L (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?Z Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, lnches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B , 4 * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:ll/1/2012-10/31/2017 0 SWU-245, last revised 10/25/2012 Page 2 of 3 0 0 0 0 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. A �s FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one coDV of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitorinaperiod in the case of "No Discharge" reports) to: Division of Water Quality Attm DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of iaw, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permi /-2 --2 0 (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 • • • Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 C& 6 3 03q ?_Date submitted y CERTIFICATE OF COVERAGE NO. NCG03D OL a SAMPLE COLLECTION YEAR 0 .S FACILITY NAME C n „iee f= n g; .i efra ¢ / / La rl S SAMPLE PERIOD ❑ Jan -June ® July -Dec COUNTY tiLa.k R_ J or ❑ Monthly month PERSON COLLECTING SAMPLES Po.c a Anal'. T;C Q t DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY Ra cr ��. r a l Lab Cert. 06 ^ 0/1 I LI ❑Zero -flow ❑Water Supply ❑SA Comments on sample collection � or analysis: ❑Other _ r QCQ Rey Uc oa�Tach4 _ PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -i Part A: Stormwater Benchmarks and Monitoring Results No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks =__> - - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L off/ / G S .. C. 00-a IVP 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 • Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." *des LyolF-e Name (Print name) a j t 14Rr7a Rip" Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, lnches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 0 0 0 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copy of this DMR, including all "No Discharge" reports. within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) ,�q - (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 aceAnalytical - wwwPa�fabs.com September 15, 2015 Mr. Chuck Wolfe Contech 6115 Chapel dill Road Raleigh, NC 27607 RE: Project: WT Pace Project No.: 92265584 Dear Mr. Wolfe: Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Enclosed are the analytical results for sample(s) received by the laboratory on August 31, 2015. The results relate only to the samples included in this report, Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, �1rC"�— CCY�`J4j�a�_ Liamm Carrubba liamm.carrubba@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc., Page 1 of 12 aceAnalytical www.pwWabs.mn Project: WT Pace Project No.: 92265584 Raleigh Certification Ill 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Charlotte Certification Ill 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 - South Carolina Certification #: 99006001 Asheville Certification Ill 2225 Riverside Drive, Asheville, INC 28804 Florida/NELAP Certification M E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Cerlification #: 37712 CERTIFICATIONS North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the wrltten consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 2 of 12 aceAnalytical - wwwpacefaps.mm SAMPLE ANALYTE COUNT Project: WT Pace Project No.: 92265584 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92265584001 WT EPA 1664B JMS 1 PASI-C EPA 200.7 JDA 3 PASI-A SM 2540D RC 1 PASI-R REPORT OF LABORATORY ANALYSIS This report shall not t>e reproduced, except in full, without the written consent of Pace Analytical Services, Inc,. Page 3 of 12 Pace Analytical Services, Inc. ® 6701 Conference Drive aceAnalytical Raleigh, NC 27607 wwwpacelabs com (919)834-4964 ANALYTICAL RESULTS Project: WT Pace Project No : 92265584 Sample: WT Lab ID: 92265584001 Collected: 08/31115 08 15 Received: 08/31/15 11:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg1L 5.0 1 09/10115 08:29 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 11.2 ug1L 5.0 1 09/02115 18:15 09/03/15 23:44 7440-50-8 Lead ND ug1L 5.0 1 09/02/15 18:15 09/03/15 23:44 7439-92-1 Zinc 254 ug1L 10.0 1 09/02/15 18:15 09/03/15 23:44 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 50.0 1 09/01/15 13:15 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date- 09M 512015 08:20 AM without the wntten consent of Pace Analytical services, Inc . Page 4 of 12 e aceAnalyircal www.pacerabs.txun QUALITY CONTROL DATA Project: WT Pace Project No.: 92265584 QC Batch: GCSV122540 Analysis Method: EPA 1664B OC Batch Method: EPA 16646 Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92265584001 METHOD BLANK: 1552171 Matrix: Water Associated Lab Samples: 92265584001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 09110/15 08:13 LABORATORY CONTROL SAMPLE: 1552172 Parameter Units Total Petroleum Hydrocarbons mg1L MATRIX SPIKE SAMPLE: 1552173 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 13.8 69 64-132 92266290001 Spike MS MS % Rec Result Conc Result % Rec Limits Qualifiers ND 2D 14.1 71 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/15/2015 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 aceAnalylical. tvrrw.pacelabs cam Project: WT Pace Project No.: 92265584 QC Batch: MPRP119397 QC Batch Method: EPA 200.7 Associated Lab Samples. 92265584001 METHOD BLANK: 1547087 Associated Lab Samples: 92265584001 Parameter Copper Lead Zinc QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Units Result Limit Analyzed ug/L ND 5.0 09103/15 23:01 uglL ND 5.0 09103/15 23:01 uglL ND 10.0 09104/1518:07 Qualifiers Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-49B4 LABORATORY CONTROL SAMPLE: 1547088 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper uglL 416 377 90 85-115 Lead uglL 416 395 95 85-115 Zinc ug1L 416 404 97 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1547089 1547090 MS MSD 92265719006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc Conc. Result Result % Rec % Rec Limits RPD Copper ug/L 4.6J 416 416 386 443 92 105 70-130 14 Lead ug/L 5.2 416 416 394 449 93 107 70-130 13 Zinc uglL 108 416 416 523 585 100 114 70-130 11 Qual MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1547091 1547092 MS MSD 92265600003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug1L ND 416 416 368 420 88 101 70-130 13 Lead uglL ND 416 416 384 440 92 105 70-130 13 Zinc ug/L ND 416 416 403 462 96 110 70-130 14 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0911512015 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceAnalytical _ tnvw.pacefabs.com QUALITY CONTROL DATA Project: WT Pace Project No.'. 92265584 QC Batch: RWET18629 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples. 92265584001 METHOD BLANK: 1545997 Matrix: Water Associated Lab Samples: 92265584001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 09/01/15 13:13 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE: 1545998 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 258 103 90-110 SAMPLE DUPLICATE: 1545999 92265584001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/15/2015 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 aceAnalytical www pacelabs c= QUALIFIERS Project: WT Pace Project No.: 92265584 DEFINITIONS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. POL - Practical Quantitation Limit_ RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SIS - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chtoroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonilrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-R Pace Analytical Services - Raleigh REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09115/2015 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 aceAnalXical www.pacetabs corn QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 6701 Conference [)rive Raleigh, NC 27607 (919)834-4984 Project: Pace Project No.: WT 92265584 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92265584001 WT EPA 1664B GCSV122540 92265584001 WT EPA200.7 MPRPI19397 EPA200.7 ICP117436 92265584001 WT SM 2540D RWET18629 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/15/2015 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 . �acoAnalylical` Document Name: Sample Condition Upon Recel t SCUR Document Revised: May 15, 2015 Page 1 of 2" Document No.: F-RAL-CS-001-rev.03 Issuing Authorities: Pace Raleigh Quality Offlce 'Page 2 of 2 is for Inlemal Use Only Client Name: Courier (Circle): Fed Ex UPS USPS Client Commercial Pace Other Custody Seal on CooledBox Present: C yes /J no Seals Intact: 1P yes ❑ no Packing Material 0 Bubble Wrap gs None Other Circle Thermometer Used: ER Gun S�12�206538 a of Ice jet;) Blue None Sempiesan Iw, cooirnQ process has begun1R Gun Sackt Temp Correction Factor: Add I btract C Data and Initials of po eon xamining Corrected Cooler Tomp.: C Biological Tissue Is Frozen: Yes No c 1 P to _ chock Temp should be above freezing to M Comments: Chain of Custody Present: Yea ❑ o ONIA 1. Chain of Custody Filled Out: XJYos No ONIA 2. Chain of Custod Ralln uished: se No OWA 3. Sam tar Name & Si nature on CDC: Yes L7No ❑NIA 4, Samples Arrived wlthtn Hold Time: OY. ON. ❑ndA 5. Short Hold Time Anal is a72hr : ❑Yes LKI No ❑NrA 6. Rush Turn Around Time Requested: ❑Yee No ONIA 7. Sufficient volume: j2Yes ❑No ONIA 8, Correct Containers Used: �i cs CNo OWA 9. -Pace Containers Used: Yes ❑No ONIA Containers Intact: Yes ❑No OWA 10. Filtered volume received for Dissolved tests ❑Yea ❑No 16NfA 11. Sample Labels match COC: Y ❑No ❑NrA 12. -Includes dale/time/ID/Analysis Matrix: All contalners needing preservation have been checked. Yes []No1]N!A 13. All containers needing preservation are found to be InjYea ❑Nn ❑NrA compilancovAth EPA recommendation. exwDtlons: VOA, cordonn, TOG, Odp. WI•DRO (water) . ON. Samples checked for dechiorinatlnn: Yes []No ONIA 14. Headspace In VOA Vials (>6mm): Dyes Ono WA IS. Trip Blank Present: ❑Yes 1)NotfA IA 16. Trip Blank Custody Seals Present ❑Yes ❑No race Trip Blank Lot�Jif_purchased . Client Notification/ Resolutions: Field Dole Required? Y ) N Poison Contacted: Commenls! Resolution: DateRme: SCURF 1SRF Woom Review:: Data:Wo#;9226566Nose; Whana co y of hi a orsa vIll be of t to t g North arince u ��� samples, a copy of this form Yrlll be sent to the North Carolina DE:HNR Certification Office (I.e out of hold, Incorrect preservative. out of temp, 1I incorrect conialnera)—92263584 age o 2 CHAIN-OF-CUS DY 1 Analytical Request Document ?17;eeArratXka' 1 The Cna"f-Custody is a LEGAL DOCUMENT. m relevant fiekts musf oe tamperea accvratey ioetionA SOC&M 9 Sectsonc t ar ;egukred C►sn1 frdOrtnotioY Requlrad Pr"C:' Wonr�alen- Papa: InvOioe IfGarnsOt,ort: �baperr�: _ Repot To x1e+,lan �S Cozy ( To. commnr Name. REGULATORY AGENCY � a, Ts F,-6 6' / OGraa. NPOES J( GROUNDWATER DRINKING WATER I : - f UST r RCRA OTHER :mad Tn /+Q e,n use Order Np .e Ouse T GC H eehe s. a Project Nartw: Liamm Carrubba Site Locrtlon $TA7� / c J vaf ieque6 Due DE WTAT: 3 Drr tam Prolfia Nu w. • Prvl+e r. Requested Analysis Filtered (YIN) Swakon D Valld Brats Caws a x ffagUIndCaa,ltefcr er. uAra £ ,c ii COLLECTED Preservatives P V ATM _ 3 y 2 W 4STt: W�TEF WW aa�� 11 CJrf99TE CC-40S G �wucf n � m � STAAT GNQK;F" yV„, spvsorD a 0 SAMPLE ID W AR3 A4ta (A•LD•81;i 0T.ca ar O w 4 ur 4 m F r Sample Ipe htUSl• BE UNIOU_E T; O i m ~ Z An C] Xrc a �U ai6,5 � O m {Tp 1 CCC ~ O1TE TIME DATE TIME w a i S Z Z �x O a PaCP Q 8Ct NO J Lab I.D. T (A, T r ..f V c 'ls FAA 3�rt iQ ! 1 I 4 S $ I 7 I 8 ! 9 I 10 ,2 ! AD0=KAL COMMENTS R"Q WSNED BY l AFF1UATlON DATE TIME A E?PTED BY l AFFI TION DATE 71ME SAMPLE CONDITIONS I f •�' N SAMPLER NAME AND SIGNATURE PRINT SAMPLED- Nava of F Y r DATE Slyned & '—' U `' SIGNATURE of SAM PLEB: (MIAfDWYY}. m in m m a rivpoamr NCH BY s,grinT the fan rev air ac:e Paee'a NET 30 dc/ GOY.'Iierli ttmrs a rieeinC :o rY.e c.5arpes c1 t 5%der n`onlh fp anY nweea M rom w h-r 30 owns F-ALL-0020rrr.07. 75-1`e�-2007 • L` Aga RECEIVED �.� P NCDENR 5E 16 2015 Stormwater Discharge Outfall (SDO) CENTRAL FILES Qualitative Monitoring Report DWR SECTION For guidance on filling out this form, please visit: littp:.//poi,tal.ncdeni-.org/web/wq/Ws/su/nPdQs5w#tab-4 Permit No.: N/C/_/,/_/_/_/`/_/ or Certificate of Coverage No.: Facility Name: CcnJeAi✓v j is n S County: 1A I,1., k f_ _ _ Phone No. ?1-9- Kr 1- a '??O Inspector: P u- c e A n a c a. _ Date of Inspection: - 31- /S _ Time of Inspection: `r A / 1 Total Event Precipitation (inches]: G- S Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, I' some permits do not have this requirement. Please refer to these definitions, if applicable. i A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no 1 precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permor Designee) SWU-242, East modified 10/25/2012 Page 1 of 2 • 1. Outfall Description: Outfall No. I Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: - 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 0 h 2 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: ' 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 © 3 4 5 . 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes B. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe /V on • Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 N ,, r 0 2 O3 q � Date submitted CERTIFICATE OF COVERAGE NO. NCG03fz 0 O SAMPLE COLLECTION YEAR Zd / FACILITY NAME SAMPLE PERIOD ®Jan -June ❑July -Dec COUNTY y or ❑Monthly" (month) PERSON COLLECTING SAMPLES Pa,e nR ; Ca DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY Pace A-1, ALCa 1 Lab Cert. # i ;a d (— o %/ 7 ❑Zero -flow [:]WaterSupply [:]SA 0 C nments on sample collection analysis: ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 Part A: Stormwater Benchmarks and Monitoring Results ❑ No discharge this period?Z [ Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rain#all amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks =__> _ - 100 mg/L or SO mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L ND N ND ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfail. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may ble waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." (�,_ h *,, les Uld!& Name (Print name) Ilan ' 10onopier' Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, the must be reported in the format "<XX m L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L IOD mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NOp] IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" resorts) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 aceAnalytical wwwpacefabxc= June 23, 2015 Mr. Chuck Wolfe Contech 6115 Chapel Hill Road Raleigh, NC 27607 RE: Project: WEEKLY WASTEWATER Pace Project No.: 92253686 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Mr. Wolfe: Enclosed are the analytical results for sample(s) received by the laboratory on June 10, 2015. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely,/ Liamm Carrubba liamm.carrubba@pacelabs.com Project Manager Enclosures e REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 (�15'neAnalytical www.pacelabs.com Project: WEEKLY WASTEWATER Pace Project No.: 92253686 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, tiuntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 Florida]NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginta/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceAnalytrcal wwwpacslabs.corn SAMPLE ANALYTE COUNT Project: WEEKLY WASTEWATER Pace Project No.: 92253686 Pace Analytical Services, Inc. 6701 Conference [Yve Raleigh, NC 27607 (919)834-4984 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92253686001 STORM WATER EPA 1664B JMS 1 PASI-C EPA 2007 JMW 1 PASI-A SM 2540D RC 1 PASI-R REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 laneAnalytical" www.pacelabs c= ANALYTICAL RESULTS Project: WEEKLY WASTEWATER Pace Project No.: 92253686 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NG 27607 (919)834-4984 Sample: STORM WATER Lab ID: 92253686001 Collected: 06/09/15 07:50 Received: 06/10/15 08:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mglL 5.0 1 06123/15 10:00 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Lead ND ug/L 5.0 1 06/15/15 17:20 06/17/15 04:56 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mglL 1250 1 06/11/15 09:15 REPORT OF LABORATORY ANALYSIS 'Ns report shall not be reproduced, except in full, Date: 06/2312015 04:47 PM without the written consent of Pace Analytical Services, Inc,. Page 4 of 11 laceAnalytical" www.pacelabs.aom QUALITY CONTROL DATA Project: WEEKLY WASTEWATER Pace Project No.: 92253686 QC Batch: GCSV121741 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92253686001 METHOD BLANK: 1491767 Associated Lab Samples: 92253686001 Parameter Units Oil and Grease mg1L LABORATORY CONTROL SAMPLE: 1491768 Parameter Units Oil and Grease mg/L MATRIX SPIKE SAMPLE: 1491769 Parameter Units Oil and Grease mg/L Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 06/23/15 09:53 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 36.8 92 78-114 92253799001 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers ND 40 37.3 91 78.114 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/2312015 04:47 PM without the written consent of Pace Analytical Services, Inc. Page 5 of 11 aceAnalytical www.pamialts.ccm QUALITY CONTROL DATA Project: WEEKLY WASTEWATER Pace Project No.: 92253686 QC Batch: MPRP118714 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92253686001 METHOD BLANK: 1484841 Associated Lab Samples: 92253686001 Parameter Units Lead ug1L LABORATORY CONTROL SAMPLE: 1484842 Parameter Units Lead ug/L Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 06/17/15 04:04 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 500 456 91 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1484843 1484844 MS MSD 92254122002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 439 486 88 97 70-130 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1484845 1484846 MS MSD 92254234004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 497 453 99 91 70-130 9 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS ThiS report Shall not be reproduced, except in full, Date: 06123/2015 04:47 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 (�IacleAnalAcal" www.pacalabsoom Project: WEEKLY WASTEWATER Pace Project No.: 92253686 QC Batch: RWET18397 QC Batch Method: SM 2540D Associated Lab Samples: 92253686001 METHOD BLANK: 1481756 Associated Lab Samples: 92253686001 Parameter Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 1481757 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 06/11/1509:15 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 254 102 90-110 SAMPLE DUPLICATE: 1481758 92253686001 Dup Parameter Units Result Result Total Suspended Solids mg/L ND ND RPD Qualifiers Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06123/2015 04:47 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnalytical Kww.pacWabs com QUALIFIERS Project: WEEKLY WASTEWATER Pace Project No.: 92253686 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit, MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-R Pace Analytical Services - Raleigh REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/23/2015 04:47 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalXical wwwpacefabacam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Pace Project No.: WEEKLY WASTEWATER 92253686 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92253686001 STORM WATER EPA 1664B GCSV121741 92253686001 STORM WATER EPA 200.7 MPRP118714 EPA 200.7 ICP116791 92253686001 STORM WATER SM 2540D RWETI8397 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 06/23/2015 04:47 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 2-C'Aflc?iC�1- Document Name: Sample Condition Upon Document Revised: May 15, 2015 �•-ww+opncele .,,,,,. Recel t (SCUR) Page 1 of 2' Document No.: Issuing Authorilles: F-RAL-CS-001-rev,03 Pace Ralel h Quality Office `Page 2 of 2 Is for Internal Use Only Client Name: - Cav)�& Courier (Circle): Fed Ex UPS USPS Cilant Commercial P OthCustodySeal on Cooler/Box Present: yes Zno Seals Intact: no Packing Matarlal: ❑ Bubble Wrap Bubble Begs None n Other Circle Thermometer Used: IR G SN:122065387T If Ie Wet tug None ❑ Samples on ice, cooling process hes begun lR Gun g :1220t;5371 Temp Correction Factor: Add btract C Date and initials of porson oxernintng cotee", r e all Corrected Cooler Temp.: C BlologieaI Tissue is Frozen: Yes No NIA check: 2 Temp should be above rroeOng to WC Comments: Chain of Custody Present: - Was iONO DIVA 1, Chain of Custody Filled Out: Re, ONO DNA 2. Chain of Custody Relinquished: as ONO ©N/A 3. Sam ter Name S Signature on COG: Ye.. ❑No ❑NIA 4. Samples Arrived within Hold Time: )Yes ON. QNIA 5. Short Hold Time Analysis c72hr : ❑Yes o ❑WA 6. Rush Turn Around Time Requested: ❑Ya, No ❑wA 7. Sufficient Volume: ee ❑Na ❑WA B. Correct Containers Used: )e)Ye, ONO ❑wA 9. -Pace Containers Used: Yes 014- ❑NtA Containers Intact: (Y„ ONO ❑NIA 10. Filtered volume received for Dissolved tests 0Y., ❑l.a rA 11. Sample Labels match COG: Ye ❑No ❑wA 12. -Includes date/timal10/Anal sis Matrix: All containers needing preservation have been checked, rr,Yes ONO ❑NIA 13. All containers needing prosorvation are found to be In (jr� oa ONO ❑NIA compliance with EPA recommendagon, � exceptions: VDA, coSform, TDE, OSG, MORO iwater} Vy...ONO Samples checked for dechlorination: e, ❑No ❑NIA 14. Headspace In VOA Vials >Smm : ❑Yea ONO rA 15. Trip Blank Present: ❑Yee ONO YNJA 16, Trip Blank Custody Seats Present ❑Yea ❑NouA Pace Trip Blank Lot # (if urchased)i Client Notlflcallonf Resolution: Field Data Required? Y / N Person Contacted: DateMme: Comments/ Resolution: SCURF ISRF Date: " r 1J Review:; 1 C'} - Or Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Cerbf-calion Once (i.o out of hold. incorrect prasorvalivo, out of temp, Incorrect containers) Place label hero OR uon:saasasss 92283686Ilpl�llll�l911 Page 10 of 11 CHAIN -OF -CUSTODY 1 Analytical Request Docitmcint- - The C min-of-Cuc=y Is a LEGAL DOCUMENT. AS re*vanl Odds must be wmpW" acnaatay- Section A Becd*n B SOcilon C . Page: of Requtred Qwd WarrmUom Required PMen k0ortnacati - lrnvlce Inkemetkm '- �n TQ o,: 1902783 � i 15 L Lfr (e CfL� Ta L' D � QS' CaMPo+y Name: ftMULlTORY'ACaENGY :'. t • ti.`:.: ri _ , G f'I N, C V� dress F NPDES ;r . GROUND WATER r ORINKING WATER UST r RCRA OTHER E W TO: Pratlusa Orden No-, pme 010. afworca: Prraf� Fac Provo« I,bnte: Z• �� u Pr ��� re.rosg.gr p sts. Loes • STA 3 - .. .. _ _ ReQuraled Due oat.lfAr: Pmj= Number PamP s• �p \ I� RBgi�estnd.Arraiysia Flkerod jYMj. _ '->:+i 9ecf bn Omovu rr+vwnacawxrkbnrrson iMT f ag a COLLECTED FieservativeS :y.: ". wowWarr w< a osrrs n 0 waxewaaar Ww 1 a oorr soar fnnow SoilS,osd SL UJ r! SAMPLE ID °F o • ' m WtDo (A•Z."I:) Air AR G W 2 v . ' mob 03 MVST BE UNIOI.'E Tcsue TS O 4 m Odlwr OT Pam'r0�^ -St4, OlRE 17ss@ oars TIME n 3 = z z z O Pace Project NoJ Lab LD. -Y -71-T. I I x %mi I I I I I 1Z i 2 .3. :4 T .e 0 4b t1 i2 I F-1-FFI-L-31 rIDOiT10NAL CObU4i>TS "'`�;-1iELJN04JtSFIE6 'l7 Giia'[ls, - ,'QgTE :� - t�".TLeE, • • - - ActCE7'I;EU.BTYAf�BlA:l01{" - 9ATp'. " .;i1:14 . ' SAMPLE CONDITONS G-ra d�sa �— 6 •� � .o N ORIGINALSAMPLER NAME AND SIGRATURE. U pqS� ��C.7Z CZL PRINT wrae er sAssPLk72r V ,3 � n $ : SIGNATIIAE d SlWPLER DATE Signed ftJA11O01YY): C � W T � e e O a '}:oorwt N AL By qw-m ft form reu :m aoccpanq Pains 67e r :ie ery pereunf mmu and 30 tax dw9" of 1.5% w mao W any rrre> -s ins pata wdwu pa ttys. .. F-ALL• -01�+9Y.0T,,1�•dr[3y-ZS797 . ���� NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this farm, please visit: http://portal.ncdenr.org/web/wq/ws/suInpdessw#tab-4 Permit No.: Fad IityName: G.%jer4 99iaPer County: wxk<. Inspector:- 8xfe Ao-.4 ;ca Date of Inspection: Time of Inspection: 7`S0 A1*1 or Certificate of Coverage No.: Phone No. Total Event Precipitation (inches): 0. 31 CENTRAL FILES DWR SECTION Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) © Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. i A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall j and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature,p6ermittee or Designee) Pagel of 2 SWU-242, Last modified 10/25/2012 1. Outfail Description: } Outfall No. l Structure (pipe, ditch, etc.) r/ - /c4 Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: BrOU10 d 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 61- ri e 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3� 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 33 4 5 7. is there any foam in the stormwater discharge? Yesl 8. Is there an oil sheen in the stormwater discharge? Yes ON) 9. Is there evidence of erosion or deposition at the outfall? Yes CN 10. Other Obvious Indicators of Stormwater Pollution: List and describe IVo n t Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may he indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 Wolfe, Charles From: Wolfe, Charles Sent: Wednesday, June 24, 201S 10:42 AM To: john.holley@ncdenr.gov' Subject: Contech permit certificate request John, Per our discussion, can you provide me with a certificate that shows my facility is in compliance with our General Permit No. NCG030000. I spoke with Mitch Hayes at the State division of water quality earlier today. I explained to him that pace analytical that has been doing our testing was unaware that there were recent revisions to our general permit. He said to note this with the paperwork I am submitting today and that it should not be a problem as long as we get this corrected moving forward. I have contacted pace analytical and updated the COC form so that the testing complies to the revisions of our permit. If we do not have a certificate on file, please contact me so we can move forward with the application process. Thanks, Chuck Wolfe Plant Manager Contech Engineered Solutions LLC 6115 Chapel Hill Road I Raleigh, NC 27607 Off: 919-851-2880 Mob: 217-993-1511 Fax: 919-851-2883 cwolfe@conteches.com www.ContechES.com 1 QED DEC 2 9 2014 cErvr Stormwater Discharge Outfall (SDO) °WR �crroN Qualitative Monitoring Report '17P For guidance on Iling out 111is orm, please visit: http:1/li2o.enr.stat6.ne.us/su/Forrns Documen ts.htni#miscforms Permit No.: N, Facility Name: County: Inspector• c)/0/C)/ or Certificate of Coverage No.: NICIGI 1__I 1_I_I_I c �! _ Date of Inspection: / Time of Inspection: Phone No. -?-gP a Total Event Precipitation (inches): 6 - -3 d � Was this a Representative Storm Event? (See information below) 2/yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 fours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee 1. OutfalI Description: Outfall No. Structure (pipe, ditch, etc.) D r f C P Recciving Stream: C e,R/3 7-466: tt-6-&k-- Desc ibe the industrial activities that occur within the outfall drainage area:_ 4 N >l-- 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: G T 9 (L.o t,v nl 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weals chlorine odor, etc.): h, Page 1 of 2 SwU-242.1 I2608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 � 3 4 S 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: bi 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 10 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes (DNo S. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe 1V a Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. . Page 2of2 SWU-242-112608 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number: NCS or SAMPLES COLLECTED DURING CALENDAR YEAR: 01 Certificate of Coverage Number: NCG.�� _��)� (tin (This monitoring report shall be received by the Division'no later than 30 days -from the date the facility receives the sampling results from the laboratory.) FACILITY NAME _ CU.c) TE�-J _ COUNTY W A)LC PERSON COLLECTING SAMPLE S) // PHONE NO. CERTIFIED LABORATORY(S} c G� Lab #(i—O// I T J Lab # (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. Part A: Specific Monitoring Requirements Outfall Date' 50050 �. No. Sample Total Total .. Oil &Grease.; Total Total Lead. pH Collected Flow (if app.) Rainfall Suspended' Solids (TSS) ' ,- .mio/dd/ r MG • inches h,911 m m Units Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no (if yes, complete Part B) ?art B: Vehicle Maintenance Activity MonitorinLy Requirements <-0 ffalI No: Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches m nigA Units al/me Form SWU-246-112608 Page 1 of 2 GERM EVENT CHARACTERISTICS: Date % Y r Total Event recipitation (inches): Q,.3.;. Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files - 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Z % (Signature of Permittee) (Date) Form SWU-246-112608 Page 2 of 2 aceAnalytical. , www.pWftWh'5.WM December 24, 2014 Mr. Greg Demerjian Contech 6115 Chapel Hill Road Raleigh, NC 27607 RE: Project: Stormwater 12/17 Pace Project No.: 92230147 Pace Analytical Services, Inc. 6701 conference Drive Raleigh, NC 27607 (919)834-4984 Dear Mr. Demerjian: Enclosed are the analytical results for sample(s) received by the laboratory on December 17, 2014. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, i> Laura J Cooper laura.cooper@pacelabs_com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 aceAnalytrcal wwwpacelabs,com CERTIFICATIONS Project: Stormwater 12117 Pace Project No.: 92230147 Pace Analytical Services, Inc. 6701 Conference Drit<e Raleigh, NC 27607 (919)834-4984 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certification #: 16 North Carolina Wastewater Certification #: 67 North Carolina Drinking Water Certification #: 37731 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Flodda/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification ibs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FloridalNELAP Certification #: E87648 South Carolina Certification #. 99030001 Massachusetts Certification #: M-NCO30 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaA/ELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 ace'Analytical wMm.Paael3b&0DM SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Stormwater 12117 Pace Project No.: 92230147 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92230147001 Stormwater EPA 1664E CLW 1 PASI-C EPA 200.7 JMW 1 PASI-A TNM 3 PASI-R SM 2540D RC 1 PASI-R REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalXical , wwwpaceta &cw ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Stormwater 12/17 Pace Project No.: 92230147 Sample: Stormwater LabID: 92230147001 Collected: 12/17/14 08:00 Received: 12117114 15:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mgll. 5.0 1 12/19/14 09:18 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Lead 5.4 ug1L 5.0 1 12/19/14 15:15 12/19/14 23:40 7439-92-1 Field Data Raleigh Analytical Method; Collected By Daniel K. 1 12/17/14 08:00 Spencer Field pH 7A Std. Units 0.10 1 12/17/14 08:00 Field Temperature 14.6 deg C 0.50 1 12/17/14 08:00 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 67.3 mg1L 16.7 1 12/23/14 08:29 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 12/24/2014 09:38 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 aceAnalytical" , wwwpaoalab&com Project: Stormwater 12117 Pace Project No.: 92230147 QC Batch: GCSV/19852 QC Batch Method: EPA'1664B Associated Lab Samples: 92230147001 METHOD BLANK: 1356164 Associated Lab Samples: 92230147001 Parameter Units Oil and Grease mg1L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/19/14 09:12 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-0984 LABORATORY CONTROL SAMPLE: 1356165 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 35.6 89 78-114 MATRIX SPIKE SAMPLE: 1356166 92230OW04 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 37.7 94 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/24/2014 09:38 AM without the Written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalytrca! wwwpnoafabs txxn Pace Anatytical Services, Inc, 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QUALITY CONTROL DATA Project: Stormwater 12I17 Pace Project No.: 92230147 QC Batch: MPRP117592 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92230147001 METHOD BLANK: 1356521 Associated Lab Samples: 92230147001 Parameter Units Lead ug1L LABORATORY CONTROL SAMPLE: 1356522 Parameter Units Lead uglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/19/14 22:26 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 500 494 99 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1366523 1356524 MS MSD 92230378001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead uWL ND 500 500 489 489 98 98 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1356525 1356526 MS MSD 92230067003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug1L 6.1 500 500 485 477 96 94 70-130 2 Results presented an this page are in the units Indicated by the "Units" column except where an alternate unli it presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12l24l2014 09:38 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 s aceAnalytrcal www.paostabs.com QUALITY CONTROL DATA Project. Stormwater 12117 Pace Project No.: 92230147 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QC Batch: RWET17764 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92230147001 METHOD BLANK: 1358301 Matrix: Water Associated Lab Samples: 92230147001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 12/23/14 08:26 LABORATORY CONTROL SAMPLE: 1358302 Spike LCS LCS e% Rec Parameter Units Conc. Result e% Rec Limits Qualifiers Total Suspended Solids mg/L 250 246 98 90-110 SAMPLE DUPLICATE: 1358303 92230022003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 144 153 6 SAMPLE DUPLICATE: 1358304 92230161001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 121 123 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 12/24/2014 09:38 AM without the mitten consent of Pace Analytical Services, Inc.. Page 7 of 11 acuftlytical Nnrx p3cebbs com QUALIFIERS Project: Stormwater 12l17 Pace Project No.: 92230147 DEFINITIONS Pace Analytical Services, Inc. 8701 Conference Drive Raleigh, NC 27607 (919)8344984 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MOL -Adjusted Method Detection Limit. POL - Practical Quantitalion Limit. RL - Reporting Limit. S. - Surrogate 1,2-Diphenylhydrazine (8270 listed anatyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 6270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-R Pace Analytical Services - Raleigh REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 12/24/2014 09:38 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 ceAnalytical www.pacelahs wm QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 6701 Conferenoe Drive Raleigh, NC 27607 (919)634-4984 Project: Stormwater 12117 Pace Project No.: 92230147 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92230147001 Stormwater EPA 1664B GCSV/19852 92230147001 Stormwater EPA 200.7 MPRP/17592 EPA 200.7 ICP/15846 92230147001 Stormwater RFLDI 92230147001 Stormwater SM 2540D R1NET17764 Date: 12/24/2014 09:38 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 Document Nalne: Sample Cc ;,XZeAwVical Recel rt SCUR' Document No.: F-RAL-CS-001-rev Client Name: �,iA ndition Upon Document Revised: April 04. 2013 page 1 of 2 Issuing Authorities: 02 Pace Asheville QualftyOffice Whore Received: Hunlersvrlle 0 Asheville Eden Raleigh Courier (Circle): - Fed Ex UPS USPS Client Commercial Pace ether Custody Seal on Cooler/Box Present: yes Q1no Seals Intact: yes no Packing Material: 0 Bubble Wrap ❑ Bubble Bags None Other Circle Thermometer Used: IR Sun S : 22065387T of Ice: et Blue None Samples on Ice, cooling process has begun IR Gun Saak.Up , 2206ti37'L Temp Correction Factor: Ad a act C xaning Date and fnitiats of persiT, Corrected Cooler Temp.: C Biological Tissue Is Frozen: Yos No A zOn n P ese n check: Temp should be above freezing to VC Comments: Chain of Custody Present: ! ❑No • ❑WA T. Chain of Cu5todyF1led Out: 26.3 ©No ❑WA 2. Chain of Custody Relinquished: Yes ONO ❑NIA 3. Sampler Name & Si nature an COC: Yes ONO ❑WA 4. Samples Arrived within Hold Time: Yos ONO ❑WA 5. Short Hold Time Analysis t72hr : ❑Yes VN. OWA 6. Rush Turn Around Time Requested: -Dyes ❑WA 7. Sufficient Volume: AYes ONO ❑WA S. Correct Containers Used: Yes ONO ❑WA 9. -Pace Containers used: Yes nNo ❑WA Containers Intact: Yes ON. ❑NIA 10. Filtered volume -received for Dissolved tests ❑Yes GNo ON/A 11. Sample Labols match COC: Yes QNo ❑WA 12. -Includes datellimellD/Anai is Matrix: All containers needing preservation have been checked, Yee ❑No ❑WA 13. AA containers needing preservation are found to be In i(� fas ❑No ❑WA compliance vrith EPA recommendation. T 8xoopliow VOA, Colifarm, TOG, O&G, WWRO (water) es ❑No Samples chocked for dechlorination: Yea ONO ❑N/A 14. Heedspaco in VOA Vials >6mm : Dyes ❑No N!A 15. Trip Blank Present: ❑Ye's ©No WA 1fi. Trip Blank Custody Seals Present Dyes DNo 94A Pace Trip Blank Lot # if urchased : Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: DatelTime. Comments/ Resolutlon: samples, a copy of M form will be sent to the North Carolina. DF;HNR Certification Office (1-e outof hold, Inoarfed preaervattve, out of temp, k►correct oontainers) Una: 23 11111111111111111 92230147 w M Page W oi. I I ;ceAna1j&ca1- www.98culabs,com 6701 Corderenoe Drive• Ralelgh, NC 27607 ph: 1919) 834-4984. tax; (919) 834-6497 NCVVW CenN7, NCDW Ceri#37731 Report Results To: Company: Address: Attn: Phone: - -- Fax: Sampled by (signature): Chain of Custody Wo.# 0zZ?� j��1? Bill To: Project Reference: Project Number: Purchase Order #: 0 Standard Report Delivery 0 Rush Report Delivery (wlsu(charge) "Rush pmjects are subject to prior approval by the laboratory Requested Rue Date: u n �¢,y t. df ,��F,�i. �' �?�� YC'+�F ,t _i�,. k7' 1� A•; i.�i�.��Y r• 1��� �I a 7f '. '_t .'.n: 3�:(b.: '���� .: '.i •Sj 4; t� ��f'1 S� �i.q�✓;k:�e_rtl�s't.t'rr�..•C..��i�l �iIY f4 � rii,`•.M.� 1.;F" r "ram •L 1 J..�. �ii .: ili5l r'! �(t' ,� �;e; !a,,�{e � .:.}�T!?..Ic..F J�+�! : ,+?'• 3; n are5� 7.�'i..�t Y *�.;'C-;r,.af•lq .�3�1/ �it+�yr .N f' �t ��a? ` ; �., ..��r il�{1� ''i .M;yjl •.ti%/'�sILL!i•Li{t7� k' .n r � �s. �. IIr Y. ., +rr y:• or =,: �`.� ;� �� x rr + � i s.;• 1 r }'�'+ � t { it S'•� '+�'�'�,. Y.��f,:�,�4++ �' '�F�x,,fi J.i,z� ri _r4 gel si<'� ��'%1 f i`4�a{%_ni 54;-t�z.7.i1,�i..r:-'�r}�1�+�1`!-y-. �I.{cf 1 ? :� �4j,, t' , d;.,.i. ;. ! ^:.r ! tl I { 3•= � . �# s'l1 •�1, ::� :ti r'J� �.,511 i ,.,;,t f �-�1 a�. i�' -{.�i i t �•�rY,L: ..a�'�_ t ,� 1,n. � -r .S:•e, C.• 7z; r,•;.t:°: .� e,,+ r y}}y .r � 1 ��• 4�.'�+PP i tg��a1r7� r} i eta 1 t" ;3 � f ,rP ! :. .■,. j Mia, Res. Chlorine: 0 Yes tr E. Base• a 1 • 1 1 1' If - -� RECEIVED DEC 10 2014 CENTRAL FILES Stormwater Discharge Outfall (SDO) DWR SECTION Qualitative Monitoring Report For gfddance on filling out this form, please visit: littp:l/h2o.enr.state.nc.us/su/Forms_ Documents.httiiMuiscforms Permit No.: NICI(�IOl l�la I o IQI or Certificate of Coverage No.: NICIGIOjiQl ggA Facility Name: County:. y-,j.p UE CO- Phone No. Inspector: _ Date of Inspection: 6 �' 11LI,._.._,.____...._.W� Time of Inspection: �,,,_Or),p b& Total Event Precipitation (inches):.- O Lf 3 Was this a Representative Storm Event? (See information below) 9/yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative stomp event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or 1. Outfall Description: Outfall No. - Structure (pipe, ditch, etc.) = H Receiving Stream: "-.A.aul_,'-- C— ri- _ - Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: W rJ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): no o L>r- In _. Page 1 of 2 S WU-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: { 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: (1 � 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the otttfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe a Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosionldeposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-1 t2608 STORr-J VATER DISCHARGE OUTFALL (SDO) MONITORING REPORT ' ,rmit Number: NCS or SAMPLES COLLECTED DURING CALENDAR YEAR: o Certificate of Coverage Number: NCGQ ?� r2 �c� _ /VCC7'o3C) (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITYNAME PERSON COLLECTING SAMPLE(S) _'po <<= p N a L-" -t + c [\ L CERTIFIED LABORATORY(S) C-hcr— ti.� j�; �u trt c_nt _ _Lab # Lab # Part A: Specific Monitoring Requirements COUNTY {N a izz PHONE NO. (q/ y } 8 S/ — a (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. Outfall Date' .50050 No. Sample Total Total Oil & Grease.: Total Total Lead. pH Collected . Flow (if app.) Rainfall Suspended Solids (TSS) nib/jdd/yr MG inches m mom, mgl .. Units Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —yes -Xno (if yes, complete Part B) =art B: Vehicle Maintenance Activitv Monitoring• Requirements 'utfall No. Date Sample Collected 50050 ' 00556 00530 00400. . Total Flow (if applicable) Total Rainfall Oil & Grease Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches mgfl rho Units al/mo Form SWU-246-112608 Page 1 of 2 S T C-2M- EVENT CHARACTERISTICS: Date I IS 1 Y Total Event recipitation (inches): 6 . �s Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours); (only if applicable — see permit.) iblail Original and one copy to: Division of Water Quality Attn: Central Files 16I7 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the hest of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Pernvttee) (Date) Form SWU-246-112608 Page 2 of 2 I6YAna"cal W&WPaaVW&Ccm December 05, 2014 Mr. Greg Demerjian Contech 6115 Chapel Hill Road Raleigh, NC 27607 RE: Project: SAMPLING 11/18 Pace Project No.: 92226008 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)934.4984 Dear Mr. Demedian: Enclosed are the analytical results for sample(s) received by the laboratory on November 18, 2014. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Laura J Cooper laura.cooper@pacelabs.com Project Manager Endosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page i of 11 • aceAnalytrcal rww.pacelsb&cafn CERTIFICATIONS Project: SAMPLING 11118 Pace Project No.: 92226008 Raleigh Certification IDs 6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certification #: 16 North Carolina Wastewater Certification #: 67 North Carolina Drinking Water Certification #: 37731 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Feld Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Florida/NEt.AP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 VirginialVELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginialVEtAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Anatydcal Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)8344984 Page 2 of 11 PaceAnalytical Services, Inc. aceAnalyiical • 6701 Conference Drive Raleigh, NC 27607 WWWC0M (919)834A984 SAMPLE ANALYTE COUNT Project: SAMPLING 11118 Pace Project No.: 92226008 Lab 10 Sample ID Method Analysts Analyses Reported Laboratory 92226008001 GRAB EPA 1664B CLW 1 PASI-C EPA 2003 JMW 1 PASI-A TNM 2 PASI-R SM 2540D LJI 1 PASI-R REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 1C, Analytical wWP&cMbbscom ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)B34-4984 Project: SAMPLING 11118 Pace Project No.; 92226008 Sample: GRAB Lab ID: 92226008001 Collected: 11/18/14 12:57 Received: 11/18/14 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 11/22/14 07:10 200.7 MET ICP Analytical Method: EPA 2003 Preparation Method: EPA 200.7 Lead ND ug/L 5.0 1 11/20/14 15:05 11/21/14 05:10 7439-92-1 Field Data Raleigh Analytical Method: Field pH 6.97 Std, Units 0.10 1 11/18/14 12:57 Field Temperature 14.2 deg C 0.50 1 11/18/14 12:57 2546D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 28.7 mg/L 4.2 1 11/21/14 10:04 Date: 12105/2014 12;25 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Servioes, Inc.. Page 4 of 11 ceAnalXical. wwwwwwa4cam QUALITY CONTROL DATA Project. SAMPLING 11118 Pace Project No.: 92226008 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QC Batch: GCSV119575 Analysis Method: EPA 1664E QC Batch Method: EPA 16646 Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92226008001 METHOD BLANK: 1336328 Matrix: Water _ Associated Lab Samples: 92226008001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease _ mg1L ND 5.0 11/22/14 07:07 LABORATORY CONTROL SAMPLE: 1336329 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 36.4 91 78-114 MATRIX SPIKE SAMPLE: 1336330 92226287001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 35.2 88 78-114 Resutts presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/05/2014 12:25 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 ceAnalytical e WWWpaCekb&com Project: SAMPLING 11118 Pace Project No.: 92226008 QC Batch: MPRPl17390 QC Batch Method: EPA 200.7 Associated Lab Samples: 92226008001 METHOD BLANK: 1334955 Associated Lab Samples: 92226008001 Parameter Units LtWL Lead QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 11/21/14 04:52 LABORATORY CONTROL SAMPLE: 1334956 Spike Parameter Units Conc. Lead ug1L 500 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)8344984 LCS LCS % Rec Result % Rec Limits Qualifiers 463 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1334957 1334958 MS MSD 92225974001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug1L ND 500 500 456 460 91 91 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1334959 1334960 MS MSD 92226090001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead 4L ND 500 500 447 449 89 89 70-130 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/05/2014 12:25 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 IaceAnalytical ...paaala6scom QUALITY CONTROL DATA Project; SAMPLING 11118 Pace Project No.: 92226008 QC Batch: RWET17585 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92226008001 METHOD BLANK: 1335584 Associated Lab Samples: 92226008001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: Parameter 1335585 Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1335586 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE; 1335587 Parameter Units Total Suspended Solids mg1L Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4964 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 11/21/14 09:59 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 250 234 94 90-110 92226096001 Dup Result Result 6530 6780 92226096002 Dup Result Result 6520 6680 RPD Qualifiers 4 RPD Qualifiers 2 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT Of LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 12/05/2014 12:25 PM witltout the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnaIXica!s wwwp3csk6&=n Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QUALIFIERS Project: SAMPLING 11f18 Pace Project No.: 92226008 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MOIL - Adjusted Method Detection Limit. PQL - Practical Quanfitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenytamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyi ether, Styrene, and Vinyl chloride. LABORATORIES PAST -A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-R Pace Analytical Services - Raleigh REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1210512014 12:25 PM without the written consent of Pace Analytical Services, Inc-. Page 8 of 11 aceAnalytical wwwpacalaba.00m QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 6701 Conferenoe Drive Raleigh, NC 27807 (919)8344984 Project: SAMPLING 11118 Paoe Project No.: 92226008 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92226008001 GRAB EPA 1664B GCSV119575 92226008001 GRAB EPA 200.7 MPRP117390 EPA 200.7 ICP115670 92226008001 GRAB RFLD1 92226008001 GRAB SM 2540D RWET17585 REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 12/05/2014 1126 PM without the written consent of Pace Analyticai Services, Inc.. Page 9 of 11 Document Name: Sample Condition Upon Document Revised: April 04, 2013 -PaceAnafytical Receipt (SCUR) Page 1 of 2 Document No.: issuing Authorities:. ww..,pnr»inoa cam ' F-RAL-CS-001-rev,02 Pace Asheville Quality Offlce Client Name: Where Received: Huntersville ❑ Asheville Eden Raleigh Courier (Circle): Fed Ex UPS LISPS Client Commercial Pace Other Custody Seal on Cooler/Box Present: Q yes [7 no . Seals intact: �ff yes no Packing Material: ❑ Bubble Wrap _Bubble Bags EJ None M Other Circle Thermornetor Used: IR G< SN'12206538 of Ice. Wet Blue None Samples on toe, cooling process has begun 1R Gun sac 5N:122095371 Temp Correction Factor: Add f ubtract, C Date and Inl1ols of parson examining Corrected Cooler Temp.: C Biological Tissue Is Frozen. Yes NtA' co re a o aherk: Temp. should be above freezing to 6140 Comments: Chain of Custody Present: Yes ©No - OWA 1: Chain of Custody Filled Out: es ONO OWA 2. Chain of Custody Relin ulshad: es ONO ❑WA 3. Sam for Name & Si nature on COC: Yes ONO OwA 4. Samples Arrived within Hold Time: j6Y. ©No ❑NIA 6. Short Hold Tim Ana is' <72hr : Dyes j6NO ❑WA 6, Rush Turn Around Time Requested: OYas No OWA 7. Sufflclent Volume: Yes ONO OWA S. Correct Containers Used: vas ONO ONZA 9. -Pace Containers Usod: es ❑No OWA Containers Intact: Yes [IN. tON1A 10. Filtered volume -received for Dissolved tests ❑Yes ONO &A 11. Sample Labels match COC: Oho ❑N!A 12. -Includes dateltimellDlAnalysis Matrix: a All containers needing'preservatlon have been checked. y�,Yes ONO ❑WA 13. All containers needing preservation are found to be in ZYes ONO ❑NIA compliance with EPA recommendation. y woWknis: VOA, poilform, TOC, OdG, W!-Olio (water) Yes f]No Samples checked for dechlorinstlon: 06yes ONO ©WA 14. Heads ace In VOA Vials y6mm): Oyes OW NIA 15. Trip Stank Present: C7Yea ONO NIA 16, Trip Blank Custody Seals Present }=Oyes ONO PNrA Pace Trip Blank Lot # (if purchased Client Notification/ Resolution: F)eld Data Required? Y ! N Person Contacted: D1at"ef'Time: Cornmenis/ Resolution: _DUS ^U�i Cir�� �. ltlts5 U1 e-�L �iS t« �kP-Id SCURF ISRF j--Q' `�.`."`_" bate: Review:: 11,k Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification -Office t Le out of hold, incorrect preservative, out of temp. Incorrect containers) uo#:92226008 IIIIAIBIIIIIIV Page 10 of 11 alceAnalytical` ynvw,paselatis.rnm 6701 Cordarenca Mve, Raleigh, NC 27607 ph: (919) 834-4984, fax: (919) 634-6497 NCWW Cert#67, NCOW Cen#37731 Report ResuNs To: Company: Address: Attn: Phone: Fax: Sampled by (signature): Chain of Custody t Bill To: r Project Reference: Project Number: Purchase Order #: ❑ Standard Report Delivery ❑ Rush Report Delivery (wlsurcharge) —Rush proje= are to prk3r epprwal by the wwabuy Ron11AQT�1� [lien rSalo- Reiinquby (signature) R s to ) D Tmle Reiinquished by ( re) Received by (signatu ) Dane 'Time k Refinqufshad by (signature) Reo*M by (signature) Date Ztm9 ReooipI CondRlon8 (L b only) © 4±TC ❑ Temp°C Res. Chiodne: ❑ Absent ❑ Pmsent ❑ n/a Acid pressor <2? ❑ Yes ❑ No ❑ nla Base preseN, >12? ❑ Yes ❑ No ❑ n/a Page 11 of 11