NCG030260_MONITORING INFO_20100715 (FIX)

PERMIT N
DOC TYPE
DOC DATI
STORMWATER DIVISION CODING SF
NCG PERMITS
HISTORICAL FILE
MONITORING REPORTS
an)D o-� )S
YYYYMMDD

SIEMENS
r
JUL i 5 20l0
July 9, 2010
Danny Smith
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Surface Water Protection
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Re: Siemens Energy, Inc.
Wendell, NC Facility
NPDES Permit No. NCG030260 Analytical Monitoring results
CERTIFIED MAIL: 7004 2890 0001 5483 1080
Dear Mr. Smith:
Enclosed arc Analytical Monitoring results required under the General Permit No.
NCG030000 Certificate of Coverage No NCG030260 for the Siemens Energy, Inc.
facility located in Wendell. NC. The results included are for the two storm water outfalls
located on the property for the Monitoring Period of Year 3 — Period 1, Sample Number
5.
If you need any additional information regarding our analytical monitoring
results, please give me a call at 704-551-5339.
Sincerely,
Amy . Gray
Enclosure

STO_ RMWATER DISCHARGE OUTFALL (SDO)
' MONITORING REPORT
GENERAL PERMIT NO. NCG030000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2010
CERTIFICATE OF COVERAGE NO. NCGO30260 (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Siemens Energy, Inc. COUNTY Wake Count
PERSON COLLECTING SAMPLES Michelle L. Logut PHONE NO. [phone]
CERTIFIED LABORATORY Environmental Conservation Laboratories, Inc. Lab # 591
Lab # PLEASE SIGN ON THE REVERSE 4
Part A: Specific Monitoring Requirements
Outfall
Date
. 00530
00400
01051
00556
78141
No.
Sample Collected,
Total Suspended Solids,
Ph,
Lead, mg/L
Oil and Grease,
Total Toxic Organics', mg/L
mo/dd/ r
m
Standard units
m
Benchmark
-
100
Within 6.0 — 9.0
0.033
30
1
Chloroform — 0.0012
Outfall 001
6/16/2010
<1.0
7.16
0.0022
CIA
All Other Constituents Below
LaboratoryDetection Limits
Below Laboratory Detection
Outfall 002
6/16/2010
9.5
6.38
0.0038
<3,0
Limits
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample Collected,
mo/dd/ r
00556
00530
00400
Oil and Grease,
m
Total Suspended Solids,
m
pH,
Standard units
New Motor Oil Usage,
Annual averse al/mo
Benchmark
-
30
100
6.0 — 9.0
-
NA
NA
NA
NA
NA
NA
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier I or Tier 2 responses.
See General Permit text.
STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
Division of Water Quality
Date 6/16/2010 (first event sampled) Attn: DWQ Central Files
Total Event Precipitation (inches): 0.11 1617 Mail Service Center
Raleigh, North Carolina 27699-1617
l r-- n n ,17 l�
Date (list each additional event sampled this reporting period,rand�rainfall amount)' i
Total Event Precipitation (inches):
t: JUL 15 2010 1
E SWU-245-031308
Page I of 2

1 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or
manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject
to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for
electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The
solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ
the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I
certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater
runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management
plan included in the Stormwater Pollution Prevention Plan."
NA
Name (Print name)
NA
Title (Print title)
(Signature)
NA
(Date)
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee) `3 (Date)
4DJIr";tw, 16YAIC.2
S WU-245-0313 08
Page 2 of 2

Environmental Conservation Laboratories, Inc.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Wednesday, June 30, 2010
S&ME, Inc. (SM001)
Attn: Ed Woloszyn
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Siemens Stormwater
ENCO Workorder: C006718
Dear Ed Woloszyn,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, June 17, 2010.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
The total number of pages in this report, including this page is 28,
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www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: Outfall002
Lab ID: C006718-01
Sampled: 06/16/10 15:45 Received: 06/17/10 13:10
Parameter
--------------------------------------------
Hold Date/Time(s)
Prep Date/Time(s)
-------------------------------------
----
Analysis Date/Time(s)
- -------------------------------------------
EPA 1664A
07/14/10
06/24/10
11:12
6/28/2010 14:59
EPA 200.7
12/13/10
06/18/10
10:19
6/21/2010 14:26
EPA 608
06/23/10
08/02/10 06/23/10
09:05
6/28/2010 12:16
EPA 624
06/30/10
06/19/10
08:01
6/19/2010 21:30
EPA 625
06/23/10
07/28/10 06/18/10
10:25
6/21/2010 21:14
SM 2540D 06/23/10 06/21/10 10:05 6/21/2010 10:05
Client ID: Outfall001
Lab ID: C006718-02
Sampled:.06116110
16:00
Received: 06/17/10 13:10"
Parameter
.................................
Hold Date/Time(s)
....--....
Prep Date/Time(s)
.. - -- -- ................
Analysis Date)Time(s)
--.... --... ---------------------
EPA 1664A
07/14/10
06/24/10
11:12
6/28/2010
14:59
EPA 200.7
12/13/10
06/18/10
10:19
6/21/2010
14:29
EPA 6D8
06/23/10
08/02/10 06/23/10
09:05
6/28/2010
12:30
EPA 624
06/30/10
06/19/10
08:01
6/19/2010
21:59
EPA 625
06/23/10
07/28/10 06/18/10
10:25
6/21/2010
21:44
SM 2540D
06/23/10
06/21/10
10:05
6/21/2010
10:05
Page 2 of 28

ce00
www.encolabs.com
SAMPLE DETECTION SUMMARY
lient TO: Outfall 002 Lab ID: C006718.01
Analyte Results Flag MDL PQL Units Method Notes
Lead - Total 3.8 3 1.9 10.0 vg/L EPA 200.7
Total Suspended Solids 9.5 1.0 1.0 mg/L SM 2540D
lient ID: Outfall 001 Lab ID; C006718-02
Analyte Results Flag MDL PQL Units Method Notes
. ------I .................................. I ................ --.................... .............. ................. --
Chloroform 1.2 0.083 1.0 ug/L EPA 624
Lead - Total
Page 3 of 28
2.2 ) 1.9 10.0 ug/L EPA 200.7

co
www.encolabs.com
ANALYTICAL RESULTS
Description: Outfall 002 Lab Sample ID: C006718-01 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 15:45 Work Order: C006718
Project: Siemens Stormwater Sampled By: Michelle Logut
Volatile Organic Compounds by GCMS
^ - ENCO Cary cetVA-d analyte (NC 5911
Analvte [GAS Number]
Results
FI g
yDiu
PIE
M"
nu
Batch
Method
AnalyZ&d
By Note
1,1,1-Trichloroethane [71-55-6] ^
0.15
u
ug/L
1
0.15
1.0
OF19GOi
EPA 624
06/19/10 21:30
JKG
1,1,2,2-Tetrachlorcethane [79-34-51 ^
0.085
U
ug/L
1
0.085
1.0
OF19001
EPA 624
06/19110 21:30
JKG
1,1,2-Trlchloroethane [79-00-5] ^
0.068
u
ug/L
1
0.068
1.0
OF19COl
EPA 624
06/19/10 21:30
JKG
1,1-Dichloroethane [75-34-31 ^
0.050
u
ug1L
I
0.050
1.0
OF19C01
EPA 624
06/19/10 21:30
JKG
I J-Dichlproethene [75-35-4] ^
0.15
u
ug1L
1
0.15
1.0
OF19001
EPA 624
06/19/10 21:30
]KG
1,2-Dichlorobenzene [95-50-1]^
0.052
u
ug/L
1
0.052
t.0
OF19001
EPA 624
106/19/1021:30
JKG
1,2-Dichloroethane [107-06-2] ^
0.082
u
ugJL
1
0.062
1.O
OF19001
EPA 624
06/19/10 21 30
JKG
1,2-Dichloropropane [78-87-5] ^
0.098
U
ug/L
1
0.098
Lo
OF19001
EPA 624
06/19/10 21:30
JKG
1,3-Dichloroltenzene [541-73-1] ^
0.092
a
ug/L
1
0.092
1.0
OF19001
EPA 624
06/19/10 21:30
JKG
1,4Dichlorobenzene [106-46-7] ^
0.10
U
ugJL
1
0.10
1.0
OF19001
EPA 624
06/19/10 21:30
JKG
2-Chloroethyl Vinyl Ether [110-75-8] ^
0,94
U
ugJL
1
0.94
5.0
OF19001
EPA 624
06/19/10 21:30
JKG
Acrolein 1107-02-81 ^
3.0
u
ugJL
1
3.0
10
OF19001
EPA 624
06/19/10 21:30
JKG
AcrylOnitrile [107-13-11 ^
2.1
a
ugJL
1
2A
10
GF19001
EPA 624
06/19/10 21:30
JKG
Benzene [71-43-2] ^
0.050
u
ug/L
1
C.050
1.0
OF19001
EPA 624
06/19/10 21:30
JKG
Bromodichloromethane [75-27-4] ^
0.10
u
ug/L
1
0.10
1.0
OF19001
EPA 624
D5119/10 21 30
JKG
Bromoform [75-25-2] ^
0.20
U
ug/L
1
0.20
1.0
OF19001
EPA 624
06/19/10 21:30
3KG
Bromomethane [74-83-9] ^
0.26
u
ug/L
1
0.28
1.0
OF19001
EPA 624
06/19/10 21:30
JKG
Carbon Tetrachloride [56-23-5] ^
0.092
U
ugJL
1
0.082
1.0
01`19001
EPA 624
06/19/40 21:30
JKG
Chlorobenzene [108-90-71 ^
0.069
u
ug/L
1
0.069
1.0
CF19001
EPA 624
06/19/10 71:30
JKG
ChWoethane [75-00-3] ^
0.18
a
ugJL
1
0.18
1.0
OF19001
EPA 624
06/19/10 21:30
JKG
Chloroform [67-6rr3] ^
0.083
U
ugJL
1
0.083
1.0
OF19001
EPA 624
06/19/10 21:30
JKG
Chloromethane [74-87-31 ^
0.050
u
ug/L
1
0.050
1.0
OF19001
EPA 624
06/19/10 21:30
JKG
cis-1,3-Dichloropropene [10061-01-5] ^
0.073
u
ug/L
1
0.073
1.0
OF19001
EPA 624
05/1911021:30
JKG
Dibromochloromethane [124-48-11 ^
0.067
u
ug/L
1
0.067
1.0
OF19001
EPA 624
06/1911021:30
JKG
Ethylbenzene [100-414]^
0.10
u
ug/L
1
0.10
1.0
OF19001
EPA 624
06/19/10 21:30
JKG
Methylene Chloride [75-09-21 ^
0.070
u
uglt
1
0.071)
1.0
OF19001
EPA 624
06119/10 21:30
JKG
Tetrachloroethene [127-18.4]^
0.099
U
ugJL
1
0.099
1.0
OF19001
EPA 624
06/19/1021:30
]KG
Toluene [108-88.31 ^
0.053
U
ug/L
1
0.053
1.0
OF19001
EPA 624
06/19110 21:30
JKG
trans-1,2-Dichloroethene [156-60-51 ^
O.11
U
ugJL
1
0.11
1.0
OF19001
EPA 624
06/19/10 21:30
JKG
trans-1,3-Dichloropropene [10061-02-61 ^
IWO
U
ug1L
1
O.C80
t.0
OF19001
EPA 624
C6119/10 21:30
JKG
Trichloroethene [79-01-61 ^
0.13
u
ugJL
1
0.13
1.0
OF19001
EPA 624
06/19/10 21:10
JKG
Vinyl chloride [75-01-41 ^
0.083
u
ugJL
1
0.083
1.0
OF19001
EPA 624
06/19/10 21:30
JKG
Surrogates
Results
OF
Spike L vt
% Rer
0/a Rec limits
Ratch
memod
Analyzed
By Notts
4-8romafuorodenzene
42
1
50.0
84%
51-122
OF19DOI
EPA624
0611911021:3D
3K6
Dibromotluorornethane
38
1
500
7796
68.117
0F19001
EPA 624
0611911011:30
JKG
Toluerx-d8
43
1
50.0
8796
69-JIO
OF19001
EPA 624
0611911011:30
MG
Page 4 of 28

Description: Outfa II 002
Matrix: Surface Water
Project: Siemens Stormwater
Lab Sample ID. C006718-01
Sampled: 06/16/10 15:45
Sampled By: Michelle Logut
��J9
www.encolabs.com
Received: 06/ 17/10 13:10
Work Order: C006718
Semivolatile Organic Compounds by GCMS
................ ............. ........ -- --............ ............ ...........
^ ENCO Cary certrfr9d analyte (NC 591)
Analvte ICAS Numberl
Results
fig
units
RE
I+IDD6
MU
Batch
Method
A4sIlyge
1}y Note5
1,2,4-TrlChlorDbenzene (120-82-1] ^
1.3
u
ug/L
1
1.3
10
OFIBU16
EPA 625
06121110 2 1; 14
DFM
1,2-Dichlorobenzene (95-50-1] ^
1.1
u
ug/L
1
1.l
10
OF18016
EPA 625
06/21/10 21:14
DFM
1,3-Dicnbrobenzene (S41-73-1)^
1.1
u
ug/L
1
LL
LO
OF18016
EPA 625
06/2111021:14
DFM
1,4-Dichlorobenzene (106-46-7] ^
1.2
u
ug/L
1
1.2
LO
OF18016
EPA 625
05/21/1021:14
DFM
1-Methylnaphthalene [90-12-0] ^
1.4
u
ug/L
1
1.4
10
OF18016
EPA 625
06/21/10 21:14
DFM
2,4,5-Trichlorophenol [93-95-4] ^
1.1
u
ug/L
1
1.1
10
OF18016
EPA 625
05/21/10 21:14
DFM
2,4,6-Trichlorophenol [88-06-2] ^
1.5
u
ug/L
1
1.5
10
OF18016
EPA 625
06/21/10 21:14
DFM
2,4-Dichbrophenol (120-83-2)^
2.0
u
ug/L
1
2.0
LO
OFISO16
EPA 625
06/21/1021:14
DFM
2,4-Dimethylphenol [105-67-9]^
2,6
u
ug/L
t
2.6
10
OF18016
EPA 625
06121/1021:14
DFM
2,4-Dinitmphenol [51.28-5]^
2.6
u
ug/L
t
2.6
10
OF18016
EPA 625
06121/102L14
DFM
2,4-Diniaotoluene [121-14-2) ^
1.1
u
ug/L
1
1.1
10
OF18016
EPA 625
O6/21110 21:14
DFM
2,6-DinitnAoluene [606-20-2) ^
1.0
U
uglL
1
1.0
10
OF18016
EPA 625
06/21/10 21:14
DFM
2-Chloronaphthalene (91-58-71 ^
1.1
U
ug/L
1
1.1
10
CF18016
EPA 625
06/21/10 21:14
DFM
2-Chlorophenol (95.57-8] ^
l.9
u
ug/L
1
1.9
10
OF18016
EPA 625
06/21/10 21:14
DFM
2-Methyl-4,6-dinitropheml [534-52-1] ^
L9
u
ug/L
1
19
10
OF18016
EPA 625
06121I10 21:14
DFM
2-Methylnaphthalene (91-57-6]^
1.3
u
ug/L
1
1.3
10
OFISO16
EPA 625
06121/1021:14
DFM
2-Noophenol (98-75-51^
2.3
u
ug/L
1
2.3
10
OF18016
EPA 625
06/2L/LO21:14
DFM
3,T-Dichlorobenzidine [91-94-L] ^
1.7
U
ug/L
1
1.7
10
OF18016
EPA 625
06RI/10 21:L4
DFM
4-Sromophenyl-phenylether [101-55-3] ^
1.0
U
ug/L
1
1.0
to
OF18016
EPA 625
06/21/10 21:14
DFM
4-Chloro-3-methylphenol [59-50-7] ^
1.6
U
ug/L
1
1.6
10
OF18016
EPA 625
06/21/10 21:14
DFM
4-Chlorophenyl-phenylether [7005-72-3] ^
1.1
u
ug/L
1
1.1
10
OF18015
EPA 625
06/21/10 21:14
DFM
4-Namphenol [f00-02-7] ^
II
u
ugR
1
1.2
10
OFIBO16
EPA 625
06121/1021:14
DFM
Acenaphthene (83-32-9]^
L1
u
ug/L
1
1.1
10
OF1B016
EPA 625
06/2111021A4
DFM
Acenaphthylere (208-96-8]^
1.1
u
ug/L
1
1.1
10
OF18016
EPA 625
06/211102L14
DFM
Anthraoene [120-12-7] ^
0,64
u
ug/L
1
0.64
10
OF18016
EPA 625
06/21/10 21:14
DFM
Oenzldine [92-87-51 ^
1.2
u
ug/L
1
1.2
10
OF18016
EPA 625
M/21/10 2L:14
DFM
Benzo(a)anthracene [55-55-3] ^
0.76
u
ug/L
1
0.76
10
OF18016
EPA 625
06/21/10 21:14
DFM
Benzo(a)pyrem [50-32-81 ^
1.6
u
ug/L
1
Lo
10
OFISO16
EPA 625
06/21/10 21:14
DFM
Benzo(b)fluaranthene [205-99-2] ^
0.78
u
ug/L
1
0.78
10
OF18016
EPA 625
06/21/10 21:14
DFM
Benzo(g,h,i)perylene [191-24-2) ^
1.9
a
ug/L
L
L9
10
OF18016
EPA 62S
06/21/10 21:14
DFM
Benzo(k)fluoranthene [202-08-9] ^
0.77
U
ug/L
L
0.77
10
OF18016
EPA 625
06/21/10 21:14
DFM
Benzoic add [65-65-0] ^
3.6
u
ug/L
1
3.6
10
OF16016
EPA 625
06/21/10 21:14
DFM
Bis(2-chlor0eth0ay)methane [111-91-I] ^
L9
U
ug/L
l
1.9
10
OF18016
EPA 625
06/21/10 21:14
DFM
Bis(2-chloroethyl)eUw [111-44-4] ^
1.9
u
ug/L
1
1.9
10
OFISO16
EPA 625
06/21/10 21:14
DFM
Bis(2-chbroisWopyllether (108-6D-1]^
1.8
u
ugR
1
1.8
10
OFISO16
EPA 625
D612111021:14
DFM
Bis(2-ethylhexyl)phthalate [117-81-7] ^
2.6
u
ug/L
1
2.6
10
OF18016
EPA 625
06/21/10 21:14
DFM
ButylbenzyIMLhalate [85-68-7] ^
1.4
u
uglL
1
1.4
10
OF18016
EPA 625
06/21/10 21:14
DFM
Chrysene [216-OL9] ^
0.92
U
ug/L
1
0.92
10
OF18016
EPA 625
06/21/10 21:14
DFM
Dibenzo(a,h)anthramne (53-70-3] ^
1.8
U
ug/L
1
1.8
10
OF18016
EPA 625
06/21/10 21:14
DFM
Diethylphthalate ]84.66.2) ^
0.51
u
ug/L
1
0.61
10
OFISO16
EPA 625
06/21/10 21:14
DFM
Dimethylphthalate [131-11-3] ^
0.79
u
uglL
1
0.79
10
OF18016
EPA 625
06/21/10 21:14
DFM
Di-n-butylphthalate [84-74-2] ^
1.4
u
ug/L
1
1.4
I0
OF18016
EPA 625
06/21/10 21:14
DFM
Di-n-octylphthalate (117.84-0] ^
1.4
u
ug/L
1
1.4
10
OF18016
EPA 625
06/21/10 21: 14
DFM
DPH (as Awbenzene) [103-33-3]
1.4
u
ug/L
1
1.4
10
OF18016
EPA 625
06/21/10 21:14
DFM
Fluoranthene [2D6-44-0] ^
1.2
a
ug/L
t
1.2
10
OF18016
EPA 625
06/21/10 21:14
DFM
Fluorene [86.73-7] ^
1.1
u
ug/L
1
1.1
10
OF18016
EPA 625
06/21/10 21:14
DFM
Hexachlorobenzene [116-74-1]^
1.2
u
uglL
t
1.2
10
OFISO16
EPA 625
06/21/1021:14
DFM
Hexachlorotlutadiem [87-68-3] ^
1.2
u
ug/i
1
1.2
10
OF18016
EPA 625
06/21/10 21:14
DFM
Hexachlorocyclopentadiene [77-47-4] ^
1.0
u
ug/L
1
1.0
10
CFIOO16
EPA 625
O6/21/10 21:14
DFM
Hexachlcmethane [57.72-1] ^
0.97
U
ug/L
1
0.97
le
OF18o16
EPA 625
06/21/10 21:14
DFM
Indeno(1,2,3-cd)pyrene (193-39-51 ^
1.7
u
ug/L
1
1.7
10
OF38616
EPA 625
06/21/10 21:14
DFM
Page 5 of 28

k �
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Description: Outfall 002 Lab Sample ID: C006718-01 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 15:45 Work Order: C006718
Project: Siemens Stormwater Sampled By: Michelle l.ogut
Semivolatile Organic Compounds by GCMS
........................................ ..........
...............
---------
...............
...........
-- .......... --------
.......
^ - ENCO Cary certified analyte [NC 591]
Analvte [CAS Numberl
Results
aw
Unils
p�
MDL HU
Batch
ethod
Analyzed
gt Notes
Isophorone [78.59.1] ^
1.6
U
ug/L
1
1.6
10
OF18016
EPA 625
06/21/10 21:14
DFM
Naphthalene [91-20-3] ^
1.4
U
ug/L
1
1.4
10
OF18016
EPA 625
05/21/1D 21:14
DFM
Nitrobenzene [98-95-3] ^
1.9
U
u91L
1
1.9
10
OF18016
EPA 625
05/21110 21:14
DFM
N-Nitrosodimethylamine [62-75-9] ^
1.4
U
ug/L
1
1.4
10
OF18016
EPA 625
05/21110 21:14
DFM
N-Nitrm-di-n-propylamine [621-64-7] ^
1.5
U
ug/L
1
1.8
10
OF18016
EPA 625
06/21/1021:14
DFM
N-Nitrosodiphenylamine/Diphenylamine
1.1
U
ug/L
1
1.1
10
OF18016
EPA 625
06/21/10 21:14
DFM
[86-30-6/122-39-4]
Pentachlorcphenol [87-86-5] ^
1.0
U
ug/L
1
1.0
10
OF18016
EPA 625
06121/1021:14
DFM
Phenanthrene [85-01-8] ^
0.74
U
ug/L
1
0.74
10
OF18016
EPA 625
06/21110 21:14
DFM
Phenol [108-95-2] ^
1.2
U
ug1L
1
1.2
10
OF18016
EPA 625
06/21/1021:14
DFM
Pyrene [129-00-0] ^
1.3
U
ug1L
1
1.3
10
OF18016
EPA 625
06/21/10 21:14
DFM
Surmgates
Results
DF
Spike Lvt
0.6 Rec
% Rec Limits
Batch
Method
Analyzed
By Notes
7,4,6-Trrbromopheso1
93
1
100
93 %
18-157
OF18016
EPA 625
0612111021:14
DFM
2-FlrmrL6phen)4
33
1
55.0
67 %
15.139
OF18016
FPA 625
05121110 21:14
DFM
Z-FIUDMAhwl
43
1
100
4396
10-104
OF18016
EPA 625
06121110 21:14
DFM
mrrobenzene-d5
32
1
50.0
6396
16.140
OF18016
EPA 625
06121110 21:14
DFM
Phenold5
40
1
100
40 %
10-83
OF18016
EPA 625
06121110 21:14
DFM
Terphenyl,di4
48
1
50.0
97%
23-164
OF18016
EPA 625
D912111021:14
OFM
Page 6 of 28

CS..0E0
www.encolabs.com
Description: Outfall 002 Lab Sample ID: C006718-01 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 15:45 Work Order: C006718
Project: Siemens Stormwater Sampled By: Michelle Logut
Semivolatile Organic Compounds by GC
^ - EAU0 Cary Certirled analyte (AIC 591)
AM= ICAS Numberl
Results
Flag
Units
p�
Im
Batch
l
nA alvzed
fy
No
4,4-DDD (72-54-8] A
0.013
u
uglL
1
0.013
0.050
OF23001
EPA 608
06128j1012:16
JHH
4,4'-DDE [72-55-9] ^
0.012
u
ug1L
1
0.012
0.050
OF23001
EPA 608
06/28/10 12:16
JHH
4,4-DDT 150-29-31 ^
0,015
u
uglL
1
0.015
0.050
OF23001
EPA 608
06/28/10 1116
JHH
Aldrin [309-00.2] ^
0.012
u
uglL
1
0.012
0.050
OF23001
EPA 608
06128/10 1116
JHH
alpha-BHC [319-64.61 ^
0.015
u
uglL
1
0.015
0.050
OF23001
EPA 608
06/28/10 12:16
JHH
beta-BHC [319-85-7) A
0.012
u
uglL
1
0.012
0.050
OF23001
EPA 608
06f28110 12A6
JHH
Chlordane (n.o.s.) [57.74-9)
0,020
U
uglL
1
0.020
1,0
OF23001
EPA 508
06/28/10 1216
JHH
Chlordane (tech) [12769-03-5] ^
0.20
u
ug/L
1
0.20
0,50
OF23001
EPA 508
06128/1012:16
JHH
delta-BHC [319.85.8] ^
0.014
u
ugIL
1
0.014
0.050
OF23001
EPA 608
06/28/10 12:16
JHH
Dleldrin (60.57-1] ^
0.0089
u
ug/L
1
0.0089
0.050
OF23001
EPA609
0612811012:16
JHH
Endosuifan 1 [9$9-96-8] ^
0.016
u
uglL
1
0.016
0,050
OF23001
EPA 608
06/28/10 12A6
JHH
Endosulfan 11 133213-65-9] ^
0.012
u
ug/L
1
0.012
0.050
OF23DOI
EPA 608
C6128/10 12:16
JHH
EndOsulfan sulfate [1031-07-8] ^
0.012
u
ug/L
1
0.012
0.050
OF23001
EPA 608
06126/10 12:16
JHH
Endrin [72-20-81 ^
0.013
u
u911
1
0.013
0.050
OF23001
EPA 608
06/28/10 12:16
JHH
Endrin aldehyde 17421-93-4] ^
0.012
u
ug/L
1
0.012
0,050
OF23001
EPA 608
06/28/10 12:16
JHH
gamma-BHC 158-89-91 ^
0.016
u
ug1L
1
0,016
0.050
OF23001
EPA 608
06/28/10 12:16
IHH
Heptachlor [76-44-0]A
0,012
u
uglL
1
0.012
0.050
OF23D01
EPA 608
06/28/10 12:16
JHH
Heptachlor epoxide [1024.57.3] ^
0.DO89
U
uglL
1
0.0089
0.050
OF23001
EPA 608
06/28/10 12:16
JHH
PCB-1016/1242 [12674-11-2/53469-21.9] ^
0.19
u
uglL
1
0.19
0.50
OF23002
EPA 608
06/28/10 12:16
JHH
PCB-1221 [11104-28.2] ^
0.046
U
uglL
1
0.046
0.50
OF23002
EPA 6D8
06/28/10 12:16
JHH
PCB-1232 [1114L-L6-5] ^
0,028
U
ug1L
1
0.028
0.50
OF23002
EPA 609
06/28/10 12:16
JHH
PCB-1248 [12672-29.61 ^
0.014
U
u91L
t
0.014
0.50
OF23002
EPA 608
06/28/10 12:16
JHH
PCB-1254 111097-69-11 A
0.015
u
uglL
1
0.015
0.50
OF23002
EPA 608
06/28/10 12:16
JHH
PCB-1260 (11095-82-5] A
0,13
u
uglL
L
0.13
0.50
OF23002
EPA 608
06/28/10 12:16
JHH
QV-01
Toxaphene [8001-35-2] ^
0.22
u
uglL
t
0.22
1.0
0F23001
EPA 608
06/28/10 12:16
JHH
Surrogates
Results
OF
Spike Lvl
% Rec
% Rec Limits
Ratch
Method
Analyzed
Ry
Notes
1,4,S,6-TCMX
0.60
1
1.00
60 %
45-151
OF13DO2
EPA 608
D612811D 12:16
JHH
2,4,5,6.7C'MX
0.67
1
1.00
6? %
44-134
0123001
IIPA 608
0612811012:15
JHH
Dccachlorobi Aenyl
0.62
1
1.00
62 %,
37-149
OF23001
EPA 608
0612811012:16
JHH
1kCd ft-to4enyl
0.80
1
1.00
80 %
42-159
OF23002
EPA 608
96128110 12:15
JHH
Page 7 oi'219

(��Eo
www.encolabs.com
Description: Outfall 002 Lab Sample ID: C006718-01 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 15:45 Work Order: C006718
Project: Siemens Stormwater Sampled By: Michelle Logut
Metals by EPA 200 Series Methods
................................................................ ........ ................
I - ENCO Cary certified anaVe INC 591)
Analvte_ CASNumberl Results flag Units DF MDL Mn Batch Method Analvxed ]ly Notes
Lead [7439-92-1] ^ 3.8 1 ug1L 1 1.9 10,0 OF18015 EPA 200.7 06121/10 14:26 ]DH
Page 9 ul'29

(F.-
www.encolabs.com
Description: Outfall 002 Lab Sample ID: C006718-01 Received: 06/17/10 13:10
Matrix: Surface Water sampled: 06/16/10 15:45 Work Order: C006718
Project: Siemens Stormwater Sampled By: Michelle Logut
Classical Chemistry Parameters
-- -- - -- -- -------- --- ------....1.................... . . . . -- -- -- ... ..........................
^ - ENCO Cary certified anelyte [NC 591]
Analyte [CAS Numberl Results EI9 1JD& PF MDL MRL Batch Meth Analyzed By Notes
Total Suspended Solids [ECL-0159] ^ 9.5 mg/L 1 1.0 1.0 OF21004 SM 2540D C6/21/10 10:05 FLT
Page 9 of 28

www.encolabs.com
Description: Outfall 002 Lab Sample ID: C006718-01 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 15:45 Work Order: 0006718
Project: Siemens Stormwater Sampled By: Michelle Logut
Classical Chemistry Parameters
.............. .
- £NCO Jacksonville certifed analyte [AC 442J
Analyte rCAS Ntir l Results Flag Units PF NDL kM Batch Mrs Analyz ly Note�
Oil & Grease (HEM) (C-0007] ^ 3.00 U mglL 1 3.00 5.00 OF23013 EPA 1664A 06128/10 14:59 M]F
This report relates only to the Sample as received by the IaWratory, and may Only he reproduced in full.
I'age 10 of 28

Ce Nih 1,
hi;: 99)
www.encolabs.com
Description: Outfall 001 Lab Sample ID: C006718-02 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 16:00 Work Order: C006718
Project: Siemens 5tormwater Sampled By: Michelle Logut
Volatile Organic Compounds by GCMS
-- --------- - ..............
^ - ENCO Cary -ItIrfred dnalyte INC 591)
Analyte ICA5 Numbe[]
Results
Flao
vita
U
DLDL
MRI
§D=
Method
Analyzed
J_Iy Note
1,1,1-7richloroethane [71-55-61 ^
0.15
u
ug/L
1
0.15
1.0
OF1900i
EPA 624
U6119/10 21:59
JKG
1,1,2,2-Tetrachloroethane [79-34-5] ^
0.085
U
ug/L
1
0,085
1.0
OF19CGI
EPA 624
06/19/10 21:59
JKG
1,1,2-Trichlorcethane [79-00-5] ^
0.068
u
ug/L
1
0.068
1.0
OF19COI
EPA 624
06/19/1C 21:59
JKG
I,I-Dichloroethane [75-34-3] ^
0.050
U
ug/L
1
0.C50
1.0
OF19001
EPA 624
06119/1021:59
JKG
1,1-Dichloroethene [75-35.4] ^
0.15
u
ug/L
1
0.15
1.0
OF1900i
EPA 624
0611911021:59
JKG
1,2-Dichlorobenzene [95-50-1] ^
0.052
u
ug/L
1
0.052
1.0
OF19001
EPA 624
06119/1021:59
JKG
1,2-Dichloroethane [107-06-2] ^
0.082
U
ug/L
1
0.082
1.0
OF190C1
EPA 624
0611911021:59
JKG
1,2-Dichloropropane [78-87-5] ^
0.098
U
ug/L
1
0.D98
1.0
OF19001
EPA 624
06/19/10 21:59
JKG
1,3-Dichlorobenzene [541-73-1] ^
0,092
U
ug/L
1
0.092
1.0
OF19001
EPA 624
06/19/10 21:59
JKG
1,4-Dichlarobenzene [106-46-71 ^
0A0
U
uglL
1
C.10
10
CF19001
EPA 624
06/19/10 21;59
JKG
2-Chloroethyl Vinyl Ether [110-75-8] ^
0.94
U
ug/L
1
C.94
50
OF19001
CPA 624
C6/19/10 21:59
]KG
Acrolein [107-02-8] ^
3,0
u
ug/L
t
3.0
10
OF19001
EPA 524
06/19/10 21:59
JKG
Acrylonitrile [107-13-11 ^
2.1
U
ug/L
1
2.1
10
OF19001
EPA 624
06/19/10 21i59
JKG
Benzene [71-43-2] ^
0.050
U
ug/L
1
0.050
1.0
OF19001
EPA 624
06/19/10 21:59
JKG
Bromodichloromethane [75.27-4] ^
0.10
U
ug1L
1
0.10
1.0
OF19001
EPA 624
06/19/10 21:59
JKG
Bromoform [75-25-2] ^
0,20
U
ug/L
1
0.20
1.0
OF19001
EPA 524
06/19/10 21:59
JKG
Bromomethane [74-63-91 ^
C.28
u
ug/L
1
0.28
1.0
OF19001
EPA 624
06/19/10 21:59
JKG
Carbon Tetrachloride [56-23-5] ^
0.082
U
ug/L
1
0,082
LID
OF19001
EPA 624
06/19/10 21:59
JKG
Chlorobenzene [108-90-7] ^
0.069
u
ug/L
1
0.069
1.0
OF19001
EPA 624
06/19/10 21:59
JKG
ChloroeUlane [75-00-3] ^
0.18
u
ugll-
1
0.18
1.0
OF19001
EPA 624
06/19/10 21:59
]KG
Chloroform [67.66.3] ^
1.2
ug/L
1
0.083
1.0
OF19001
EPA 624
06/I9/10 21:59
JKG
Chloromethare [7487-3] ^
Use
U
ug/L
1
0.050
1.0
OF19001
EPA 624
06/19/10 21:59
JKG
cis-1,3-Dichloropropene [10061-01-51 ^
0.073
u
ug/L
1
0.073
1.0
CF19001
EPA 624
06/19/10 21:59
JKG
Dibromochloromethane [124-48-1]^
0,%7
U
ug/L
1
0.067
1.0
CF19001
EPA 624
06119/1021:59
JKG
Ethylbenzene [100-41-4] ^
0,10
u
ug/L
1
0.10
1,0
CF19001
EPA 624
06/19/10 21:59
JKG
Methylene Chloride [75-09-2] ^
0.070
U
ug/L
1
0.070
1.0
OF19001
EPA 624
06/19/10 21:59
JKG
Tetrachloroethene [127-18-41 ^
0.099
U
ug/L
1
0099
1.0
OF19001
EPA 624
05/19/10 21:59
JKG
Toluene [108-88-3] ^
0.053
U
ug/L
1
0,053
1.0
OF19001
EPA 624
05/19/10 21:59
JKG
trans-1,2-Dichloroethene [156-50-5] ^
0.11
U
ug/L
1
0.11
1.0
OF19001
EPA 624
06/19/10 21:59
JKG
trans-1,3-1)ichloropropene [10061-02-6] ^
0.080
U
ug/L
1
C.O80
I.6
OF19001
EPA 624
06/19/10 21:59
JKG
Trkhloroethene [79-01-6] ^
0,13
U
ug/L
1
013
1.0
orI9001
EPA 624
06/19/10 71:59
JKG
Vinyl chloride [75-01-4] ^
0.083
U
ug/L
1
0.083
1.0
OF19001
EPA 624
06/19/10 21:59
JKG
Surrwates
Results
DF
Spike Lv/
% Rec
% Rae Limits
&arch
Method
Analyzed
By Notes
4-8romaf7uorabienzene
41
1
500
82%
51-122
OF19001
EPA 624
06/19/1021:59
)KG
Dibrpmof ioromethane
39
1
50.0
77 %
68-117
OF19001
EPA 6Z4
06119119 21:59
JKG
Toluen d8
44
I
50.0
8796
59-110
OF19001
EPA 624
06119110 21:59
JKG
Page I [ of 28

www.encolabs.com
Description: Outfall 001 Lab Sample ID: 006718-02 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 16:00 Work Order: C006718
Project: Siemens Stormwater Sampled By: Michelle Logut
Semivolatile Organic Compounds by GCMS
-------------------------------------------
^ - ENCO Cary certified anolyte [NC 591]
Analvte fCAs Numbed
Results
Flaa
Units
DF
M6L
MRL
Batch
Method
Analyzed
py Note
1,2,4-Trichlorobenzene [120.82-11 ^
1.3
U
ug/L
1
1.3
10
OF18016
EPA 625
06/21/10 21:44
DFM
1,2-Dichbrobenzene (95-50-1] ^
1.1
u
ug/L
1
1.1
10
OFISO15
EPA 625
06/21/10 21:44
DFM
1,3-Dichbrobenzene [511-73-1] ^
1.1
u
ug/L
1
1.1
10
OF18015
EPA 62S
06/21/10 21:44
DFM
1,4-DiWorobenzene [106-46-7] ^
1.2
u
ug/L
1
1.2
10
orlsois
EPA 625
06/21/10 21:44
DFM
1-Methylnaphthalene [90-12-0] ^
1.4
u
ug/L
1
1.4
10
OF18016
EPA 625
06/21/10 21:44
DFM
2,4,5-Trichlorophenol [95-95-41 ^
1.1
U
ug/L
1
1.1
le
OF18016
EPA 625
06/2111C 21:44
DFM
2,4,5-Trichlorophenol [88-06-21 ^
1.5
u
ug/L
1
1.5
10
OF16O15
EPA 625
06/21/10 21:44
DFM
2,4-Dichbrophenol [120-83-2] ^
2.0
u
ug/L
1
2.0
Lc
OF16016
EPA 625
05/21/1021:44
DFM
2,4-Dimethylphenal [105-67-9] ^
2.6
u
ug/L
1
2.6
10
OF18016
EPA 625
06/21/10 21:44
DFM
2,4-Dinitrophenol [51-28-51^
2.6
U
ug/L
1
2.6
t0
OF18016
EPA 625
06121/1021:44
DFM
2,4-Dinitrotoluene [121-14-2] ^
1.1
u
ug/L
1
1.1
10
OF18016
EPA 625
06/21/10 21:44
DFM
2,6-Dinitrotoluene [606-20-2) ^
1.0
u
ug/L
1
1.0
IO
OF18016
EPA 625
06/21/10 21:44
DFM
2-Chloronaphthalene [91-58-71 ^
1.1
u
ug/L
1
1.1
10
OF18016
EPA 625
06/21/10 21:44
DFM
2-Chlorophenol [95-57-5) ^
1.9
u
ug/L
1
1.9
10
OFIS016
EPA 625
06/21/10 21:44
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]^
1.9
u
ug/L
1
IS
10
OF18016
EPA 625
06/21/10 21:44
DFM
2-Methylnaphthalene (91-57-6] ^
1.3
u
ug/L
1
1.3
10
OF18016
EPA 625
06/21/10 21:44
DFM
2-Nitrophenol [88-75-51^
2.3
U
ug/L
1
2.3
10
OF18016
EPA 625
06/2111021A4
DFM
3J-Dichloraberzidine [91-94-1]^
1.7
U
ug/L
1
1.7
LO
OFIB016
EPA 625
06/21/1021:44
DFM
4-6romophenyl-phenylether [101-55-3] ^
1.0
U
ug/L
L
1.0
LO
OFISO16
EPA 625
06/71/10 21:44
DFM
4-Chbro-3-methylphencl [59-50-71 ^
1.6
a
ug/L
L
1.6
10
OFIS016
EPA 625
06/71/10 21:44
DFM
4-Chlorophenyl-phenylether [7005-72-3] ^
1.1
U
ug/L
1
1.1
10
OF18016
EPA 625
06/21/10 21:44
DFM
4-Nitrophenol (100-02-7] ^
1.2
u
ug/L
1
1.2
10
OFIB016
EPA 625
06/21/10 21:44
DFM
Acenaphthene [83-32-9] ^
1.1
u
ug/L
1
1.1
10
OF18016
EPA 625
06/21/10 21:44
DFM
Acenaphthylene [208-96-8] ^
1.1
a
ug/L
1
1.1
10
OFIBO16
EPA 625
06/21/10 21:44
DFM
Anthracene (120-12-71 ^
0,64
U
ug/L
1
054
i0
OFIPO16
EPA 625
06/2111C 21:44
DFM
Benzidine [92-87-5] ^
1.2
U
ug/L
1
1.2
10
OFISO16
EPA 625
06/21/10 21:44
DFM
Benzo(a)anthracene (56-55-3] ^
0.76
u
ug/L
1
0.76
to
OF18015
EPA 625
06/21/10 21:44
DFM
Benzo(a)pyrene (50-32-8] ^
1.0
u
ug/L
1
1.0
to
6F18015
EPA 625
06/21/10 21:44
DFM
Benzo(b)fluoranthene [205-99-21 ^
0.78
u
ug/L
1
0.78
10
OF18016
EPA 625
06/21/10 21:44
DFM
Senzo(g h,i)perylene L191-29-2] ^
1.9
u
ug/L
1
1.9
10
OF18016
EPA 625
0612L/10 21:44
DFM
Benzo(k)Noranthene [207-08.9] ^
0.77
u
ug/L
1
0.77
10
OF18016
EPA 625
06/2L/LO 21:44
DFM
Benzoic acid [65.85.0] ^
3.6
It
ug/L
1
3.6
10
OF18016
EPA 625
06/21/10 21t44
DFM
Bis(2-ch1oroethoxy)methane [111-91-1] ^
1.9
u
ug/L
1
1.9
10
OF18016
EPA 625
06/21/102L44
DFM
Bis(2-chloroethygether [111-44-4] ^
1.9
u
ug/L
1
1.9
10
OF18016
EPA 625
06121/10 2L:44
DFM
Sis(2-chloroisopropyl)ether [108-60-1] ^
1.8
a
ug/L
1
1.8
10
OF18016
EPA 625
06i21/1021:44
DFM
Bis(2-ethy1hexy1)phtha1ate [117-81-7] ^
2.6
u
ug/L
1
2.6
10
OF18016
EPA 625
06/21/10 21:44
DFM
Butylbenzylphthalate [85-68-7] ^
1.4
u
ug/L
1
1.4
10
OFISO16
EPA 625
06/21/10 21:44
DFM
Chry5ene [218-01-9] ^
0.92
u
ug/L
1
0.92
I0
Or18016
EPA 625
06/21/10 21:44
DFM
Dibenzo(a,h)anthracene (53-70-3) ^
1.8
U
ug/L
1
1.8
10
OF18016
EPA 625
06/21/10 21:44
DFM
Diethylphthalate [84-66-2] ^
0.61
a
ug/L
1
0.61
10
OF18016
EPA 625
06/21/10 21:44
DFM
Dimethylphthalate [131-11-3] ^
0,79
u
ug/L
1
0.79
10
OFIS016
EPA 625
06/21/10 21:44
DFM
Di-n-butylphthalate (84-74.2] ^
1A
u
ug/L
1
1.4
10
OF18015
EPA 625
06/21/10 21:44
DFM
Di-r-cctylphthalate [117-54-01 ^
1.4
U
ug/L
1
1.4
10
OF18016
EPA 675
05/21/10 21:44
DFM
DPH (as Azobenzene) [103-33-3]
1.4
u
ug/L
1
1.4
10
OFISO16
EPA 625
06/21/10 21:49
DFM
Fluorarthene [206-44-0]^
1.2
U
ug/L
1
1.2
10
OF18016
EPA 625
06121/1021:44
DFM
!`Wren [86-73-71 ^
1.1
u
ug/L
1
1.1
10
OF18016
EPA 625
06121/1021:41
DFM
Hexachlorobenzene [118-74-1] ^
1.2
u
ug/L
1
1.2
10
OF18016
EPA 625
06/21110 21:41
DFM
Hexachlorobutadiene [87-68-3] ^
1.2
U
ugR
1
1.2
LO
OF18016
EPA 625
06/2l/tO21:44
DFM
Hexachlerocyclopentadiene [77-47-4]^
1.0
U
ug/L
1
1.0
l0
OF18016
EPA 625
06/21/10 21:44
DFM
Hexachlorcethane [67-72-1] ^
0.97
U
ug/L
1
0.97
10
OFIBU16
EPA 625
06/2111021:44
DFM
Indeno(1,2,3-cd)pyrene [193-39-51 ^
1.7
u
uglL
1
1.7
10
0F18016
EPA 625
06/21/10 21:44
DFM
Page 12 of' 28

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Description: Outfall 001 Lab Sample ID: C006718-02 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 16:00 Work Order: C006718
Project: Siemens Stormwater Sampled By: Michelle Logut
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certiEed anal4e [NC 591]
Analvte [CAS Numberl
Results
BIG!
units
RE
MDl
RL
UA=
Method
Analyzed
ft Notes
lsophorone [78-59-11 ^
1.6
U
uglL
1
1,6
10
OF18016
EPA 625
06/21/10 21:44
DFM
Naphthalene [91-20-3] A
1.4
u
ug/L
1
1.4
10
OF18016
EPA 625
06/21/10 21:44
DFM
Nitrobenzene [98-95-3] ^
1.9
U
UgX
1
1.9
10
OF18016
EPA 625
06/21/10 21:44
DFM
N•NiLrosodimethylamine 162-75-9] ^
1,4
U
U9/L
1
114
10
OF18016
EPA 625
06/21/10 21:44
DFM
N-Nitrm-dm-propylamine [621-64-7] ^
1.8
U
ug/L
1
1,8
10
OF18016
EPA 625
06/21/10 21:44
DFM
N-Nitrp5041iphenylamine/Dphenylamine
1.1
L
ug1L
1
1.1
10
OF18016
EPA 625
06/21/10 21:44
DFM
[86.30-6/122-39-41
Pentachlorophenol [67-86-5] ^
1.0
U
ug/L
1
1,0
10
OF18016
EPA 625
06/21/10 21:44
DFM
Phenan[hrene [854ll-8]^
0.74
U
Ug1L
1
0,74
to
OF18016
EPA 625
06/21/10 21:44
DFM
Phend [108-95-2]^
1.2
u
ug1L
1
1.2
10
OF1B016
EPA 625
06121/1021:44
DFM
Pymne [129-00-01^
1.3
u
vg1L
1
1.3
10
OF1B016
EPA 625
06121/1021:44
DFM
Surrogates
Results
DF
Spike L vl
% Rec
% Rec Limits
Batch
Method
Analyzed
By Notes
1, 4,6-Tnbmiwphenol
8B
1
100
88 %
16-157
OF18016
EPA 6Z5
06121110 21: 44
DFM
7-Fluorobwpheno
37
1
50.0
74 %
15-139
OF18016
EPA 625
06121110I1: 44
DFM
2-Fiuorop6awl
50
1
100
50 %
10-104
OF18016
EPA 625
D6121110 21:44
DFM
Nitrobenzene-dS
35
1
50.0
71 %
16-140
OF18016
EPA 625
0612111D 21:44
DFM
Phenol-U5
4S
1
100
46 96
10-B3
OF18015
EPA 625
06121110 21:44
DFM
Terph87yl d14
47
1
50.0
95 %
73-164
OFJBO16
EPA 625
06121110 21:44
DFM
Page 13 of 28

(� �Go
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Description: Outfall 001 Lab Sample ID: C006718-02 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 16:00 Work Order: C006718
Project: Siemens Stormwater Sampled By: Michelle Logut
Semivolatile Organic Compounds by GC
^ - £NCO Cary certified -Oe (NC 5911
Analvte I"CAS Numberl
Results
Hag
Units
pf
MD
1�RL
Batch
Meth
Anal
By Notes
4,4'-DDO 172-54-81 ^
0.013
u
ug1L
1
0.013
0.050
OF23001
EPA 608
06/28/10 17:30
JHH
9,4'-ODE 172-55.91 ^
0,012
u
uglL
1
0.012
0.950
OF23001
EPA 608
06/28/10 12:30
JHH
4,4'-DDT [50-29-3] ^
0.015
u
ug/L
1
0.015
0.95E
OF23001
EPA 608
06/28/10 12:30
JHH
Aldbn [309-042] ^
OAl2
u
ug/L
1
0.012
0.050
OF23001
EPA 60B
06/28/10 12:30
JHH
alpha-BHC (319-84-6) ^
0015
U
ug/L
1
0.015
0.050
CF23001
EPA 6CS
06/78/10 12:30
JHH
beta-BHC [319-85-7] ^
0,012
u
ug/L
1
0.012
0.050
CF23001
EPA 608
06/28/10 12:30
1HH
Chlordane(n.o.s.) [57.74.9]
0020
U
ug/L
1
C.020
1.0
CF23001
EPA 6CS
06/2B/10 12:30
3HH
Chlordane (tech) [12789-03-61 ^
0.20
u
ug/L
1
0,20
0.50
CF23001
EPA 6C8
06/2B/10 12:30
JHH
delta-BHC (319-86-8] ^
01014
u
uglL
1
0.014
0.050
OF23001
EPA 608
06/2B/10 12:30
3HH
[leldrin 160-57-1] ^
0.0089
U
uga
1
0.0089
0.050
OF23001
EPA 608
06/28/10 12:30
JHH
Endosulfan 1 [959-98-8] ^
0.016
U
ug/L
1
0,016
0.050
OF23001
EPA 608
05/28/10 12:30
JHH
Endosulfan 11 [33213-65-9] ^
0.012
u
ug/L
1
0,012
0.050
OF23001
EPA 608
06/28/10 12:30
JHH
Endosulfan sulfate (1031-07-8] ^
0.012
u
ug/L
1
0,012
0.050
OF23001
EPA 608
05/28/10 12:30
JHH
Enddn [72-20-8]^
0.013
u
ug/L
1
0,013
0.05E
OF23001
EPA 608
0612811012:30
JHH
Endrin aldehyde [7421-93-41 ^
0.012
U
ug/L
1
0012
0.050
OF23001
EPA 608
06/29/1012:30
3HH
gamma-BHC [58-89-9] ^
0.016
U
ug/L
1
0016
0.050
OF23001
EPA 608
06/28/10 12:30
JHH
Heptachlar [76-44-8]^
0.012
U
ug/L
1
0.012
O.C50
OF23001
EPA 608
06/28/10 12:30
JHH
Heptachiorepoxide [1024-57.3] ^
0.0089
u
ug/L
1
0.0089
0.050
OF23001
EPA 609
06/28/10 12:30
JHH
PCB•1016/1242 [12674-11-2153469-21-91 ^
0.19
u
ug/L
1
0.19
0.50
OF23002
EPA 608
06/28/10 12:30
3HH
PCB-1221 111104-28-2] ^
0.045
u
ug&
1
0.046
0.50
OF23002
EPA 608
06/28/10 12:30
3HH
PCB-1232 [11141-16-5] ^
0.028
U
ug/L
1
0.028
0.50
CF23002
EPA 608
06/28/10 12:30
JHH
PCB-1248 [12572-29-5] ^ _
0,014
u
ug/L
1
0.014
0.5E
OF23002
EPA 608
05/28/10 12:30
JHH
PCB-1254 [11097-69-1] ^
0,015
u
ug/L
1
0,015
0.50
OF23002
EPA 608
06/28/10 12:30
JHH
PCB-1260 [11096-82-5] ^
0.13
u
ug/L
1
0.13
0.5E
OF23002
EPA 608
06/28/10 12:30
JHH QV-01
Toxaphene [8001-35-2] ^
0.22
u
ug/L
1
0.22
1.0
OF23001
EPA 608
06/28/10 12:30
JHH
Surrogates
Results
OF
Spike Lvl
a/oRec
%RecLimits
Batch
Method
Analyzed
By Notes
2,4,5,E-TOIX
0.50
1
1.00
50 %
45-151
OF23002
EPA 608
05121VJO 12.•30
JHH
2,4,5,6-704Y
0.65
1
1.00
65 %
44-134
OF23001
EPA 608
061281101230
JHH
Deavh1orobrpheny1
a69
1
1.00
69 %
37-149
OF23001
EPA 6M
0612811011:30
JHH
Decachbmbiphenyl
0.90
1
1.00
90 %
42-159
OF23002
EPA 608
061281101220
JHH
Page 14 of28

(E-
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Description: Outfall 001 Lab Sample ID: C006718-02 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 16:00 Work Order: C006718
Project: Slemens Stormwater Sampled By: Michelle Logut
Metals by EPA 200 Series Methods
......................
^ - ENCO Cary certified a -We ANC 591J
Analyte ICAS Numberl Results Fjig Units pf HDI MRL Batch Method nA alVed §y Notes
Lead [7439-92-1] ^ 2.2 ] ug/L 1 1.9 100 OF18015 EPA200.7 06121/1014.29 ]OH
Page 15 of28

0
NCO
www.encolabs.com
Description: Dutfall 001 Lab Sample ID: C006718-02 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 16:00 Work Order: C006718
Project: Siemens Stormwater Sampled By: Michelle Logut
Classical Chemistry Parameters
.......................................................................................................
^ - ENCO Cary reriifed analyte INC 5911
Analvte ICAS Numberl Results Flag Units p_ 1MOL M& Batch Method Analyzed gy Notes
Total Suspended Solids {ECL-0169] ^ 1.0 u mg/L 1 1.0 1.c OF21004 SM 2540D 06/21/10 10:05 FLT
Page 16 al' 28

Ce== �Go
www.encolabs.com
Description: Outfall 001 Lab Sample ID: C006718-02 Received: 06/17/10 13:10
Matrix: Surface Water Sampled: 06/16/10 16:00 Work Order: C006718
Project: Siemens Stormwater Sampled By: Michelle Logut
Classical Chemistry Parameters
........................... ---- ...—-------- I...... ................ --- ------------ --...............
^-ENCOlacksonLi&-CertlrAedanalyte[NC 442]
Analvte ICAS Numberl Results fW Units PE MPL RLRl Batch Medtod Analyzed )}y Note:
Oil & Grease (HEM) [C-0007i ^ 3.00 u mg/L 1 3.00 5.00 OF23013 EPA 1664A 06/26/10 14:59 MY
71rts report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page I7 of 28

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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch OF19001 - EPA 50308 MS
Blank (OF39001-BLK1) Prepared: 06/19/2010 08:01 Analyzed: 06/19/2010 10:09
Spike Source %REC RPD
Analyte
Result
Flag
MRL
Units Level Result %REC Limits RPD Limit Notes
1,1, i-Trichlorcethane
0.15
U
1.0
ug/L
1, 1, 2,2 -Tetrach lo roethane
0.085
U
1.0
ug/L
1, 1, 2-Trich I oroethane
0.068
U
1.0
ug/L
1,1-Dkhloroethane
0.850
u
1.0
ug/L
1,1-Dichluroelhene
0.15
u
1.0
ug/L
1,2-Dichlorobenzene
0.052
U
1.0
ug/L
1,2-Dichloroethane
0.082
U
1.0
ug/L
1,2-Dichlaropropane
0.098
U
1.0
ug/L
1,3-Dichlarobenzene
O.D92
U
1.0
ug/L
1,4-Dichlorobenzene
0.10
U
1.0
ug/L
2-Chloroethyl Vinyl Ether
0.94
U
5.0
ug/L
Acrolein
3.0
u
10
uglL
AcryiGnitrile
2.1
u
10
ug/L
Benzene
0.050
U
1.0
ug/L
Bromodichloromethane
0.10
U
1.0
ug/L
Bromoform
0.20
U
1.0
ug/L
Bromomethane
0.28
U
1.0
ug/L
Carbon Tetrachloride
0.082
U
1.0
ug/L
Chlorobenzene
0,069
U
1.0
ug/L
Chloroethane
0,18
U
1.0
ug/L
Chloroform
0.083
U
1.0
ug/L
Chloromethane
0.051)
U
1.0
ug/L
cis-1,3-Dichloropropene
0.073
u
1.0
ug/L
Dibromochlommethare
0.067
U
1.0
ug/L
Ethylbenzene
0.10
U
1.0
ug/L
Methylene Chloride
0.070
U
1.0
ug/L
TWachloroethene
0.099
u
1.0
ug/L
Toluene
0.053
U
LO
ug/L
vans-1,2-Dchloroethene
0.11
U
1,0
ug/L
trans-1,3-Dichlaropropene
0.080
L
1.0
ug/L
Trichloroethene
0,13
U
1.0
ug/L
Vinyl chloride
0.083
U
1.0
ug/L
Surrogrte:4-Bronaofruorobenzem 4Z WA 50.9 85 51-122
Surroyete: LibmnbRuoroaethane 37 W4 50.0 74 68-117
Surrogate: Toluene-d8 44 WIL 50.0 88 59-110
LCS (OF19001-BS1)
Prepared: 06/19/2010 08:01 Analyzed: 06/19/2010 10:39
Spike Source %REC RPD
Analyte
Result,_ _. Flag
MRL
Units
Level Result %REC. Limits. RPD Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0 94 75-133
Benzene
21
1.0
ug/L
200 106 81-139
Chlorobenzene
19
1.0
ug/L
20.0 96 83-117
Toluene
19
1.0
ug/L
20.0 97 71-118
Trichloroelhene
19
1.0
ug/L
20.0 95 75-115
51r1ogafe:4-1311111W,170benzene 43 » 50.0 85 51-127
Surrogate: DVbmfwl7commethanO 37 u94 50.0 74 58-117
Surrogate: Toluene-d8 43 ug/1 S0.0 87 69-110
Page ISol'28

QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch OF19001 - EPA 50308 MS
ENCa
www.encolabs.com
Matrix spike (OF19001-MS3)
Prepared: 06/19/2010 08:01 Analyzed; 06/19/2010 11:08
Source: 0007248-05
Spike
Source
%REC
RPD
Analyte
Result
Flag
MRL
Units
Level
Result
%REC
Limits RPD
Limit Notes
l,l-Dichloroethene
19
1.0
ug/L
20.0
0.15 U
94
75-133
Benzene
22
1.0
ug/L
20.0
0.050 U
111
81-134
Chlorobenzene
20
1.0
ug/L
20.0
0.069 U
98
83-117
Toluene
20
1.0
Ug/L
20.0
0.053 U
98
71-118
Trichloroethene
19
1.0
ug/L
20.0
0.13 U
97
75-115
5urm9ate:4-8romathvrobenzene
43
ug/L
50.0
85
51-122
Sutmgate: L4hvarnoet.nratn YAane
36
L+94
50.0
71
58-117
Surrogate: Toluene -Ow
43
U91L
50.0
86
69-110
Matrix Spike Dup (OF19001-MSD1)
Prepared: 06/19/2010 08:01 Analyzed: 06/19/2010 11:37
Source: 0007248-05
Spike
Source
%REC
RPD
Analyte
Result
Flag
MRL,
Units
Level
Result
%REC
Limits RPD
Limit Notes
l,i-Dichloroethene
19
1.0
ug/1
20.0
0,isU
54
75-133 0.4
20
Benzene
21
1.0
ug/L
20.0
0.050 U
106
81-134 5
17
Chlorobenzere
19
1.0
ug/L
20.0
0.069 U
95
83-117 3
16
Toluene
19
1.0
uglL
20.0
0,053 U
97
71-118 0.9
17
Trkhloroethene
19
1.0
ug/L
20.0
0.13 U
97
75-11S 0.3
1B
5urnoate.• 4-8mmo17wmbenzene
44
LVA
50.0
88
51-122
Surrogate .• Dibmm fluommethane
36
UO
50.0
71
68-117
Surrogate: Tolmned8
............ ................... .................................
43
U91Z
...............
5D.D
--'-----
87
........ ....---.......
69-110
..--................
--
Semirrolatile Organic Compounds by GCMS - Quality Control
Batch OF18016 - EPA 3510C MS
81ank (OF18016-BLK1)
Prepared: 06/18/2010 10:25 Analyzed: 06/19/2010 01:36
lAnalyte
Spike
'Source
%REC
RPD
Result
Flag
MRL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,2,4-Trichlorobenzene
1.3
U
10
uglL
1,2-Dichbrobenzene
1.1
U
10
ug/L
1,3-Dichlorobenzene
1.1
U
10
ug/L
1,4-Dkhbrobenzene
1.2
U
10
ug/L
1-Methylnaphthalene
1.4
U
10
ug/L
2,4,5-Trichlorophenol
1.1
U
10
ug/L
2,4,6-Trichlorophenol
1.5
U
10
ug/L
2,4-Dichlorophend
2.0
U
10
ug/L
2,4-Dirrethylpheiol
2.6
U
10
ug/L
2,4-Dinitrophenol
2.6
U
10
ug/L
2,4-131nitrotoluene
1.1
U
10
ug/L
2,6-DnlrotDluene
1.0
U
10
ug/L
2-Chbronaphthalene
1.1
U
10
ug/L
2-Chlorophenol
1.9
U
10
ug/L
2-Methyl-4," nitrophenol
1.9
U
10
ug/L
2-Methylnaphthalene
1.3
U
10
ug/L
2-Nitrophewl
2.3
U
10
ug/L
3,3'-Oichlorobenzidine
1.7
U
10
ug/L
Page 19 of 28

QUALITY CONTROL
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OF18016 - EPA 3510C MS
(��C-O
www.encolabs.com
Blank (01`18016-01-Kl) Continued Prepared: 06/18/2010 10:25 Analyzed: 06/19/2010 01:36
Spike Source %AEC RPD
Analyte
Result
Flag _
TU
MRLUnits
Level Result %REC Limits RPD Limit Notes
4-11m=phenyl-phenylether
1.0
10
u91L
4-Chloro-3-methylphen6
1.6
U
10
Lg/L
4-Chlorophenyl-phenylether
1.1
U
10
ug/L
4-Nitropheno9
1.2
U
10
ug/L
Acenaphthene
1.1
U
10
ug/L
Acenaphthylene
1.1
U
10
ug/L
Anthracene
0.64
U
10
ug/L
Benzidine
L2
U
10
u9/1-
BenzO(a)anthraCene
0.76
U
10
ug/L
Benzo(a)pyrene
1.0
U
10
ug/L
Benzo(b)flucranthene
0.76
U
10
ug/L
Benzo(g,h,i)perylene
1.9
U
10
uglL
Benzo(k)lluoranthene
0.77
U
10
ug/L
Benzoic add
3.6
U
10
ug/L
Bis(2-chloroethoxy)methane
1.9
U
10
Lg/L
Bi5(2-Chlomethyl)ether
1.9
U
10
ug/L
Bis(2-chlor0i50propyl)ether
1.8
U
10
Lg/L
BiS(2-eL"hexyi)phthalate
2.6
u
10
ug/L
BUtylbenzylphthalate
LA
U
10
ug/L
Chrysene
0.92
a
10
ug/t
Dibenz0(a,h)anthracene
1,8
U
10
ug/L
Diethylphthalate
0.61
U
10
ug/L
Dimethylphthalate
0.79
U
10
ug/L
Di-n-hutylphthalate
1,4
U
10
ug/L
Di-n-Ottylphthalate
1.4
U
10
ug/L
DPH (as Azobenzene)
1.4
U
10
ug/L
Fluoranthene
1.2
U
10
ug/L
Fluorene
1.1
U
10
u9/L
Hexachlorobemene
1.2
U
10
ug/L
Hexachlorobutadiene
1.2
U
10
ug/L
Hexachlorocydopentadiene
1.0
U
10
u911-
Hexachloroethane
0.97
U
10
ug/L
Indelo(1,2,3-cdlpyrene
1.7
U
10
ug/L
Iwphorone
1.6
U
10
ug/L
Naphthalene
1.4
U
10
ug/L
Nitrobenzene
1.9
U
10
ug/L
N-Nitro500imethylamine
1.4
U
10
ug/L
N-Nitroso-di-n-propylamine
LB
U
10
ug/L
N-Nitrowdiphenylamine/Diphenylamine
III
U
10
ug/L
Pentachbrophenol
1.0
U
10
ug/L
Phenanthrene
0.74
U
10
Ug/L
Phend
1.2
U
10
ug/L
Pyrene
1.3
U
10
u9/L
Surrogate: 14,6-7nbiwwph-W
82
LVA
100
82
I8-167
Surrogate.' 2-FILOobiphenyl
33
U91L
50.0
67
15-139
Sunngate:2-Fluorapheno/
45
LVA
IM
45
10-104
Surrogate: Nitrobenzene-dS
32
U91L
5V a
64
16-140
Surrogate: Phenol-05
41
U91L
160
41
10-83
Page 20 of 28

QUALITY CONTROL
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OF18016 - EPA 3510C MS
www.encolabs.com
Blank (OF18016-BLKI) Continued Prepared: 06/18/2010 10:25 Analyzed: 06/19/2010 01:36
Spike Source %REC RPD
141-alyte Result Flag MRL Units. Level Result o/nREC Limits RPD Limit Notes
Surrogate: Terpheny1-dI4 49 uq/L 50.0 97 23-164
LCS (OF18016-BS1)
Prepared: 06/18/2010 10:25 Analyzed: 06/19/2010 02:05
IAnalyte
Spike
Source
°/DREG RPD
Result Flag
MRL
Units
Level
Result %REC
Limits RPD Limit Notes
1,2,4-Trichlorobenzene
29
10
uglL
50.0
58
27-90
1,4-Dichlerohen2ene
27
10
41L
50.0
54
23.84
2,4-Dinitrotoluene
51
10
ug/L
50,0
102
67-132
2-Chlorophenol
31
10
uglL
5o.0
62
40.109
4-Chloro-3-melhylphenol
43
10
uglL
50.0
85
58-121
4-Nitrophenol
39
10
ug1L
50.0
78
33-105
Acenaphthene
39
10
uglL
50.0
77
43-118
N-NiVoso-di-n-propylamine
34
10
ug/L
50.0
69
48-126
Pentachlorophenol
43
10
ug1L
50.0
86
51-135
Phenol
22
10
ug/L
30.0
43
19-78
Pyrene
47
10
ug1L
50.0
94
65-134
5unugate:2,4,6-Tnbromophen01
93
u91L
100
93
18-157
Surragate.• 2-Fh+nrobrpheny4
36
irq/L
50.0
72
IS-139
Surrogate:2-FLuorophenol
46
u91L
100
46
10404
Surrogate.' Nitro�S
33
L91L
50.0
55
16-140
Sunngate: Phen01-d5
41
u91L
100
41
10-63
Sum:9ate: Terpheno-d14
48
eg/L
50.0
96
23-164
Matrix Spike (OF18016-MSi)
Prepared: 06/18/2010 10:25 Analyzed: 06/19/2010 03:05
Source: C007248-06
�Analyte
Spike
Source
%REC RPD
Result Flag
MRL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,2,4-Tnchlorobenzene
27
10
uglL
50.0
1.3 u
55
27-90
1,4-Dichbrohenzene
26
10
uglL
50.0
1.2 U
51
23-81
2,4-Dinitrctoluene
49
10
ug/L
50.0
1.1 U
98
67432
2-Chbrophenol
29
to
uglL
50.0
1.9 U
58
40-109
4-Chloro-3-methylphenal
40
10
uglL
50.0
1.6 U
81
58.121
4-Nitrophenol
40
10
ug/L
50.0
1.2 U
60
33-105
Acenaphthene
37
10
uglL
50.0
L1 U
74
43-118
N-Nitroso-di-n-propytamine
33
10
ug/L
50.0
1.8 U
65
48-176
Penta[hlorophenol
43
10
uglL
50.0
1.0 U
87
51-135
Phenol
21
10
uglt
50.0
1.2 u
41
19-78
Pyrene
46
10
uglL
50.0
1.3 U
93
65-134
Sumlgate.'2,4,6-TnAwWheno!
90
ug/L
100
90
18.157
5urrogate:2-FlcmrobipAenyl
34
WIL
50.0
69
IS-139
Surroiyate:2-FB.nroph&0/
44
u34
100
44
10-104
Surrogate; Nitrobemmge-dS
30
ug/L
S0.0
61
16-140
Surnwte.' PheWld5
39
ug/L
100
39
I0-83
Surrogate: Terphenyl-dl4
48
WIL
50.6
96
23-164
Matrix Spike Dup (OF38016-MSDi)
Source: 0007248-06
Page 21 of 28
Prepared: 06/18/2010 10:25 Analyzed: 06/ 19/2010 03:35

QUALITY CONTROL
Semivolatile Organic Compounds by GCNIS - Quality Control
Batch DF18D16 - EPA 3510C MS
QF.
www,encolabs.com
Matrix Spike Dup (OF18016-MSD1) Continued
Prepared: 06/18/2010 10:25 Analyzed: 06/19/2010 03:35
Source:0007248-06
IAnalyte
Spike-
Source...
%REC.
RPD.
Result Flag
MRL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,2,4-Trichlorobenzene
27
10
ug/L
50.0
1.3 U
54
27-90
0.8
43
1,4-Dichlorobenzene
25
10
ug/L
5C.0
1.2 U
50
23-84
2
39
2,4-oinitrataluene
48
10
ug/L
50.0
1.1 U
97
67-132
1
17
2-Chlorophenol
28
10
ug/L
50.0
1.9 U
56
40-109
3
22
4-Chlo o-3-nnethylphenol
40
10
ug/L
50.0
1.6 U
81
58-121
0.3
22
4-Nitrophenol
40
10
ug/L
50.0
1.2 u
79
33-105
2
27
Acenaphthene
36
10
ug/L
50.0
1.1 U
73
43-118
2
21
N-Nitroso-dl-n-propylamine
32
10
ug/L
50.0
1.8 U
63
48-125
3
23
Pentachlorophenal
45
10
ug/L
50.0
1.0 U
90
51-135
3
11
Phenol
20
1n
ug/L
50.0
1.2 U
40
19-75
2
18
Pyrene
46
10
ug/L
50.0
L3 U
92
65-134
0.5
16
Surrogate.' 1,4,6-Trrbromophen01
89
ug/L
100
89
18-157
5uhWare.' 2-F1ua]Nph-4
34
ug/1
50.0
68
15-139
Surnagate.' 2-Fluomphenal
43
U91L
100
43
10-104
51umgate: Mtmdemmn"S
31
LVA
50.0
61
16-140
Surrogate: Phenol-d5
38
U91L
100
38
10-83
Surrogate: Terph&70-dl4
48
ug/L
50.0
96
13-164
Semivolatile Organic Compounds by GC - Quality Control
Batch OF23001 - EPA 3510C
Blank (OF23001-BLK1) Prepared: 06/23/2010 09:05 Analyzed: 06/28/2010 10:30
Spike Source %REC RPD
Analyte
Result
Flag.
MRL
Units Level Result %REC .- Limits RPD Limit Notes
4,4'-DDD
0.013
U
0.050
ug/L
4,4'-DDE
0.012
U
0050
ug/L
4,4-DOT
0.015
U
0.050
uglL
Aldrin
0.012
U
0.05C
ugIL
alpha-BHC
0,015
U
0.050
ug/L
beta-BHC
0.012
U
0.090
ug/L
Chlordane (n.o.s.)
0.020
U
1.0
ug/L
Chlordane (tech)
0.20
U
0.50
ug/L
delta-BHC
0.014
U
0.050
ug/L
Deldrin
0.0089
U
0.050
ug/L
Endosulfan 1
O.C16
U
0.050
ug/L
Endosulfan 11
0.012
U
0.050
ug/L
Endosuifan sulfate
0.012
U
C.050
ug/L
Endrin
0.013
U
0.050
ug/L
Endrin aldehyde
0.012
U
0A50
ug/L
gamma-BHC
0.016
U
0.050
ug/L
Heptachlor
0.012
U
0,050
ug/L
Heptachlor epoxide
0.0089
U
0.050
ug/L
Toxaphene
C.22
U
1.0
ug/L
Surragate.•1,4,5,6-TCW 0.89 DO 1.00 89 44-124
Surrogare: &--cachbrobipheny! a92 ug/L 1.00 92 37-149
Page 22 of 28

QUALM CONTROL
Semivolatile Organic Compounds by GC - Quality Control
Batch OF23001 - EPA 3510C
(� �Eo
..encolabs.com
LCS (OF23001-BSI)
Prepared: 06/23/2010 09:05 Analyzed: 06/28/2010 1013
Spike
Source
%REC
RPD
Analyte
Result
Flag
MRL
Units
Level
Result
°/.REC
Limits
RPD
Limit Notes
4,4'-DDT
0.94
0.050
ug/L
1.00
94
37-139
Aldrin
0.91
0.050
ug/L
1.D0
91
47-123
Dieldrin
0.95
0.050
ug/L
1.00
95
46-132
Endnn
0.95
0.050
ug/L
1.00
95
43-133
gamma-BHC
0.92
0.050
Ug/L
1.00
92
52-117
Heptachtor
0.93
0.050
ug/L
1.00
93
45-122
Swrngat-- 2,4,5,6-TCMX
0.99
ugn
1.00
69
44-134
Surrogate: f-raehlorobphenyl
0.76
uy/1
1.90
76
37-149
-....
-- --'................. "--'-------...........
Matrix Spike (OF23001-MSS)
...........................
.......... ............ -... ......... ......----...........
Prepared: 06/23/2010 09:05 Analyzed: 06/28/2010 10:57
Source:0007248-10
�Analyte
Spike
Source
%REC
RPD
Result
Flag
MRL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
4,4'-DDT
0.97
0.050
ug/L
1,00
0.015 U
97
37-139
Aldnn
0.90
0.050
ug/L
1.00
0.012 V
90
47-123
Deldnn
0.96
0.050
ug/L
1.00
0.0089 U
96
46-132
Endrin
0.96
0.050
ug/L
1.00
0.013 U
96
43-133
gamma-BHC
0.91
0.050
Ug/L
1.00
0.016 U
91
52-117
Heptachlor
0.93
0.050
ug/L
1.00
0,012 U
93
45-122
Sutmgate.•2,4,5,6.7CAA'
0.66
V9A
1.00
66
44-134
Surrogate: Decechlorobiphenyl
0.74
ugA
1.00
74
37-149
Matrix Spike Dup (OF23001-MSD1)
Prepared; 06/23/2010 D9:05 Analyzed: 06/280010 11:10
Source: C007248-10
Spike
Source
%. REC
RPD
Analyte
Result
Flag
MRL
units
'Level
Result
°/.REC
Limits
RPD
Limit Notes
4,4'-DDT
1.0
0.050
Ug/L
1.00
0.015 U
104
37-139
7
26
Aldnn
1.0
0,050
ug/L
1.00
0.012 U
101
47-123
11
32
Dieldnn
1.1
0,05C
ug/L
1.00
0.0089 U
106
46-132
10
27
Endnn
1.1
0.050
ug/L
1.00
0,013 U
106
43-133
10
26
gamma-BHC
1.0
0.050
ug1L
1.00
0.016 U
102
52-117
12
28
Heptachlor
1.0
0.050
ug/L
1.00
0,012 U
104
45-122
11
32
Surrogate: 2,4,5,E-rCmx
0.75
u9/1
1,00 75 44-134
Surrogate- DeCach/orobpheny!
0.32
u9/1
1.00 82 37449
Batch OF23002 - EPA 3510C
Blank (OF23002-BLKI)
Prepared: 06/23/2010 09:05 Analyzed: 06/28/2010 10:30
Spike Source %REC RPD
Analyte
Result
Flag
MRL
Units
Level Result %REC Limits RPD Limit Notes
PCB-1016/1242
0.19
U
0.50
ug/L
PCB-1221
0.046
U
0.50
ug/L
PCB-1232
0.028
U
0.50
ug/L
PCB-1248
0.014
U
0.50
ug/L
PCB-1254
0.015
U
0.50
ug/L
PCB-1260
0.13
U
0.50
ug/L
QV-01
Page 23 0l' 28

QUALITY CONTROL
Semivolatile Organic Compounds by GC - Quality Control
Batch OF23002 - EPA 3510C
Ce
�19
www.encolabs.com
Blank (OF23002-BLK1) Continued Prepared: 06/23/2010 09;05 Analyzed: 06/28/2010 10:30
Spike Source 'L:: "/nREC RPD:
Analyte Result Flag ' MRL Units Level Result %REC Limits IRPD Limit Notes
Surragate:2,4,5,6-TCMX 0.60 ug/1 1.00 60 45--151
Surrogate. Lecwhkvoblphenyl 1.0 U91L 1.00 100 42-159
LCS (OF23002-BS1) Prepared: 06/23/2010 09:05 Analyzed: 06/28/2010 11:23
Spike Source %REC RPD_
Analyte .. Result Flag MRL Units ... Level Result %REC . Limits RPD Limit, Notes
PCB-101611242 12 0.50 uglL 10.0 119 66-149
PCB-1260 11 0.50 uglL 10.0 115 64-150
Surrogate:2,4,5,6-TCMX 0.60 Wi 1.00 60 45-151
Surrzvale--De-chlorobrp/tenyl 1.1 U91L 1.00 110 42-159
Matrix Spike (OF23002-MS1)
Prepared: 06/23/2010 09:05 Analyzed: 06/28/2010 11:36
Source: C007248-11
Spike
Source
%REC RPD:'
Analyte
Result Flag MRL Units Level .
Result
%REC Limits RPD .: Limit Notes
PCB-1016/1242
8.8 0.50 ug/L iC.0
019 U
88 66d49
PCB-1260
8.8 0.50 ug/L 10.0
0.13 U
88 64-150
5urrogate:2,4,5,6-7CMX 040 ug/L 1.00 40 45--151 QS-03
Surrogate: DecXhloroblphenyt ago U91L 1.00 90 42-159
Matrix Spike Dup (OF23002-MSD1) Prepared; 06/73/2010 09:05 Analyzed: 06/28/2010 11:50
Source: C007248-11
, Spike Source 9ruREC RPD
IAnalyte Result Flag MRL Units Level Result .%REC Limits RPD Limit Notes
PCB-1016/1242 10 0.50 Ug/L 10.0 OA9 U 105 66-149 18 21
PCB-1260 11 C.50 ug/L 10'0 0.13 U 110 64.15C 23 18 QR-02
5urrogiate:2,4,5,6-TCMX 0.50 ag/L 1.00 50 45-151
Surrogate: Dmachlorobiphenyl 1.0 ug/L 1.00 100 42-159
Metals by EPA 200 Series Methods - Quality Control
Batch OF18015 - EPA 3005A
Blank (OF18015-BLK1) Prepared; 06/18/2010 10:19 Analyzed: 06/21/2010 13:25
Spike Source %REC RPD
IAnalyte - Result Flag MRL Units Level Result , %REC ;. Limits .. RPD Limit Notes
Lead 1.9 U 10.0 uglL
LCS (OF18015-BSI) Prepared: 06/18/2010 10:19 Analyzed: 06/21/2010 13:29
Spike Source %REC RPD
Analyte Result Flag MRL" Units Level>. Result <%REC Limits . _ RPD : Limit Notes.
Lead 1080 10.0 ug/L 1000 108 65-115
Matrix Spike (OF18015-MS1)
Source: C006698-01
Page 24 of 28
Prepared: 06/18/2010 10:19 Analyzed: 06/21/2010 13:44

(E�0
www.encolabs.com
QUALM CONTROL
Metals by EPA 200 Series Methods - Quality Control
Batch OF18015 - EPA 3005A
Matrix Spike (OF18015-MS3) Continued Prepared: 06/18/2010 10:19 Analyzed: 06/21/2010 13:44
Source: C006698-01
Spike . Source %REC RPD
Analyte Result Flag MRL Units Level Result 0/aREC .:iLimits RPD "LIm1t Notes'
Lead 1060 10.0 ug/L 1000 1.9 U 106 75-125
Matrix Spike Dup (OF18015-MSD1) Prepared: 06/18/2010 10:19 Analyzed: 06/21/2010 13:47
Source: C006698-01
Spike - , Source �". P/oREC ., 4 R PD .°.
Analyte :Result . .. Flag :: MRL Units Level .,. Result.., a/DREG,Limits RpD ` ,",' Limit' Notes
Lead 1070 10.0 ug/L 1000 1.9 U 107 75-125 0.2 25
Classical Chemistry Parameters - Quality Control
Batch OF21004 - NO PREP
Blank (OF21004-BLK1) Prepared & Analyzed: 06/21/2010 10:05
Spike _ Source %REC"':, RPD
Analyte Atesult Flag MRL Units Level Result a/o EC 'Limits' RPD Limit. =' Notes
Total Suspended Solids LO U 1.0 mg/L
LCS (OF21004-B51) Prepared & Analyzed: 06/21/2010 10:05
So Spike' urce %REC RPD`:
Analyte Result Flag MRL Units Lever Result %REC ` Limits RPD '" Limit :Notes
Total Suspended Solids 87 1.0 mg/L 80.0 109 90-122
Duplicate (OF21004-DUPS) Prepared & Analyzed: 06/21/2010 10:05
Source: C006482-01
Spike Source :! %REC : RpD
Analyte Result Flag MRL Units Levef Result - %REC Limits RPD Limit Notes
Total Suspended Solids 110 1.0 mg/L 110 0 25
QUALM CONTROL
Classical Chemistry Parameters - Quality Control
Batch OF23013 - EPA 1664A
Blank (OF23013-BLKl) Prepared: 06/24/2010 11:12 Analyzed: 06/28/2010 14:59
Spike °Source' , %REC RPD :;,
Analyte Result =' % . Flag MRL ' m " `Units Level Result %REC Limits ` ° RPD Limit Notes
Oil & Grease (HEM) 3.00 U 5.00 m91L
LCS (OF23013-BS3) Prepared: 06/24/2010 11:12 Analyzed: 06/28/2010 14:59
Spike ^,Sourte-, %AEC
" .
Analyte Result Flag MRL Units Level Result %REC imits RPD Limit Notes
Oil & Grease (HEM) 36.1 5.00 mg/L 10.6 89 78-114
Matrix Spike (OF23013-MS3)
Source: 8002862-03
Paige 25 of 28
Prepared: 06/24/2010 11:12 Analyzed: 06/28/2010 14:59

QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch OF23013 - EPA 1564A
Matrix Spike (OF23013-MS1) Continued
www.encolabs.com
Prepared: 06/24/2010 11:12 Analyzed: 06/28/2010 14:59
Source: B002862-03
Spike Source. n.REC RPD :.
Analyte:. - Result. Flag MRL - Units Level Result . .%REC Limits'__ RPD Limit: Notes
Oil & Grease (HEM) 37.1 5.00 mg/L 40.8 3,00 U 91 78-114
Matrix Spike Dup (OF23013-MSD1)
Prepared: 06/24/2010 11:12 Analyzed: 06/28/2010 14:59
Source: 0002862-03
Spike Source %REC RPD
�Afialyte.Result. Flag ... MRL Units Level Result %DREG Limits RPD Limit Notes
Oil & Grease (HEM) 37.3 5.00 mgIL 40.8 3,00 U 92 78-114 0.7 18
Page 26 of 28

��O
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
lJ The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
F The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were
acceptable. Sample results for the QC batch were accepted based on percent recoveries and
completeness of QC data.
QS-03 Surrogate recovery outside acceptance limits
QV-Ol The associated continuing calibration verification standard exhibited high bias; since the result is
ND, the impact on data quality is minimal.
Page 27 of 29

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30

Table — Summary of Stormwater Analytical Results

SUMMARY OF STORMWATER ANALYTICAL RESULTS
JUNE 2010 MONITORING EVENT
SIEMENS ENERGY, INC.
7000 SIEMENS ROAD
WENDELL, NORTH CAROLINA
S&ME PROJECT NO. 1054-10-183
*Field
EPA Method
EPA Method
SW 846
VOCs by
SVOCs by
Measurement
1664A,
2540D;_
Method 6010B
EPA' 624
EPA 625 .
Analvtical Method
c,
ontaminant of Concern
pH
{TPH
.'
Total.
, Total Lead ,
- Chloroform
Constituent-.
o-�
(standard unit s)
,Oil & Grease
:
Snspended
(ntg/L) ,
(mg/L)
Specific
(mglL)
Solids (mg/L)
.--(mg/L)
Sample 1D
Date Collected
Outrann 001
6/16/2010
7.16
<3.0
<1.0
0.0022J
0,0012
ALL BDL
Outfall 002
1 6/16/2010
6.39
<3.0
9.5
0.0038.1
<0.000083
ALI, 13DL
Permit No. NCG030000'Benchmark Values
14'" 6.0 - 9.0
30
100
0.'033
1.0
1.0
Notes:
1. *p1-1 measurements collected in the field with 15 minutes of sample collection using calibrated Hanna Combo Meter,
2. VOCs = Volatile Organic Compounds
3. SVOCs = Semi -Volatile Organic Compounds
4. TPfi = Total Petroleum Hydrocarbons
5. mglL = milligrams per I iter
6. Constituents not shown were not detected.
7. J = The reported value is between the laboratory method detection limit and the laboratory method reporting limit.
S. ALL BDL = all constituents below laboratory detection limits �
9. Permit No. NCG030000 Benchmark: Values for Analytical Monitoring Requirements. '[T&E'is rently
.,,.-permitted under General Permit No. NCG030000. Certificate of Coverage NCG030013.