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HomeMy WebLinkAboutNCG030027_MONITORING INFO_20141010 (FIX)STORMWATER DIVISION CODING NCG PERMITS PERMIT NO. /V C& bJ0 0a"-� DOC TYPE ❑HISTORICAL FILE iZl MONITORING REPORTS DOC DATE o aol q I oI o YYYYM M DD Mr. Danny Smith DWQ Regional Supervisor North Carolina Department of Environment and Natural Resources 1628 Mail Service Center Raleigh, NC 27699-162$ a OCT 10 2014 RE: Eaton Corporation i General Permit No. NCG030000 NC DENR Raleigh Regional Office Dear Mr. Smith: Eaton Corporation operates automotive component metal fabrication plant in Roxboro, NC. The facility operates under the North Carolina Stormwater Industrial General Permit (IGP) No. NCG030000 for establishments engaged in Metal Fabrication. The facility's permit tracking number is NCG030027. The effective date of the current IGP is 11/01/2012, and the expiration date is 10/31/2017. Beginning in 2013 the facility began sampling the stormwater and comparing the analytical results to the benchmark values as required by the Permit. The facility has had four exceedances of the benchmark values at Outfall-OOS. As required by the Tier Three response actions in the Permit, Eaton is providing notification of benchmark value exceedances. This Tier Three notification is for Outfall-OOS related to sample result exceedances for copper. A copy of the submitted DMRs with results and the laboratory reports are attached. As a result of the exceedances of the benchmark values, Eaton initiated the response actions for Tier One and Tier Two required in the permit to limit the impact to stormwater. These actions include: • Remediation project changing drainage pattern, water flow, and overall characteristics of this outfall. • Changing the covering and lining material of a swarf dumpster to prevent possible leakage and runoff to the trench. • Standardization of the process for mopping floors and trained all operators on the proper methodology. A remediation project changing drainage pattern, water flow, and overall characteristics of this outfall was undergone at the facility in December 2013. These changes have included: Grading the area draining into the outfall, directing roof drainage water into the outfall and increasing overall water through the outfall and total drainage area. The swarf at the facility is stored in a dumpster prior to recycling the material at an offsite recycler. To prevent any stormwater contributions, the plant changed the material used to line the dumpster to a thicker grade polyethylene (plastic material). A solid cover was also placed on this dumpster to prevent rainwater entrance and migration. Eaton has also reviewed the manufacturing activities to identify potential sources of copper. The facility operates an enclosed fabrication area which utilizes copper wires. It is possible that residue is carried out of the shop on footware. As a result of this finding, a standard approach to mopping was implemented and all operators on all shifts were trained on the proper mopping technique. Furthermore, a floor scrubber is utilized to clean the floors to prevent transport of this material on lift trucks. Y l The potential sources of copper include a possible presence in swarf stored onsite prior to recycling. af'ys During our investigation, historical. practices at the site were also reviewed. It was revealed that historically brass chips3and tailings were stored in enclosed bins near to Outfall 005. These metal chips were then loaded onto trucks in the adjacent loading dock to be taken off -site. We discussed the potential impactforcopper presence in the immediate area due to these historical practices. Eaton has also carefully reviewed the analytical data and the sampling activities and completed and submitted DMRs. according to the permit. Samples results were received on November 12, 2013, July 7, 2014, July 21, 2014 and September 11, 2014. See the attached spreadsheet of the sampling dates and analytical results. Eaton believes additional stormwater sampling should be conducted to collect more representative data to compare with the benchmark values to further evaluate the impacts of the response actions that have been taken at the facility before concluding the response actions have had not result on the stormwater impacts. While Eaton has promptly responded with follow-up actions and continues to inspect the drainage area and evaluate to facility conditions for opportunities to reduce impacts to stormwater, Eaton believes that more sampling is needed to further evaluate the conditions and actions taken. We propose collecting of additional representative samples for four months and then submitting an update to this letter. Pleased contact me at 336-503-6449 if you have any questions or need additional information. Sincerely, Katie Holbrook dy- OCT 10 20% NC Storm Water Tier Response Actions NIC CENR RaN99 + Regio W Off@ l -R A�.tionc Complete inspection must be performed within 2 weeks of receiving sampling results. 2) Identify possible causes of the exceedance. 31 Idenitfy control measures to red Lice the concentration of the exceeded parameter(s). 4) Implement selected controls within 2 months. 51 Record Tier One responses in SWPPP Person(s) Benchmark value Inspection conducting Date Actions Date exceeded date inspection Corrective actions Implemented Sample Location; 004 Behind Supply Corrective actions will take place in two phases. Phase 1: • Stop parking in areas off the pavement, this is leading to increased erosion 12/18/2013 • Stop forktruck maintenance outside 12/2/2013 • Place straw/haybailes to stop the erosion from entering stormwater runoff from the area where no grass is present to filter or reduce erasion 12/18/2013 Phase 2: Phase 2 to be performed (Spring 20141: Sample Received 11/12/2013 Above limits for TSS, Cooper, Lead and Zinc. 11/12/ 2013 and 12/2/2013 K. Holbrook, K. Witkowski, K. Stetcher • Perform grading in the area to disperse water, effectively removing the outfall, preventing water draining from the area to enter "waters of the state" and preventing erosion. The outfall will no longer exist, as stormwater will not leave the site, but rather be dispersed across 6/9/14- the site. 6/13/14 6/9/14- - Move topsoil to the area to prevent ersosion/sediment load 6/13/14 6/9/14- Plant grass in the eroded area 6/13/14 Sample Location: 005 Next to Houghton Area Remediation project changing drainage pattern, water flow, and Sample Received 11/12/2013 Above the limits for copper and zinc. 11/12/2013 and 12/2/2013 K. Holbrook, K. Witkowski, K. Stetcher overall characteristics of this outfall. These changes have included: November 21, 2013-Jan. 2014 • Grading the area draining into the outfall ' Directing roof drainage water into the outfall • Increasing overall water through the outfall and total drainage area. Sample Location: 001 Pond Cover the heat treat dumpster K. Holbrook, K. Sample taken Witkowski and 6/25/14 Sample results Received Above the limits for copper and zinc. 7/14/14 and 8/26/14 8/26 with Holbrook, Witkowski, Improve the heat treat parking area by laying gravel gravel laid 9/3/14 7/7/14 Scripps, Schick and Fesko I R A11t— Complete inspection must be performed within 2 weeks of receiving sampling results. 2) Identify possible causes of the exceedance. 3) Id enitfy control measures to reduce the concentration of the exceeded parameter(s). 4) Implement selected controls within 2 months. S) Record Tier One responses in SWPPP. 6) Immeidately implement monthly monitoring for all parameters at each outfall where a sampling result exceeded a benchmark value for two consecutive samples. Monthly monitoiring (qualitative and quantitative) shall continue anti! 3 consecutive samples are below the values or within the benchmark parameters.7) Submit a No Flow report in no discharge is present during the month, 8) Benchmark exceedances for a different parameter trigger a seperate Tier response. 9) Maitain a record of the Tier responses and monitoring results in the SWPP Person(s) Benchmark valu[date spection conducting Date Actions Date exceeded inspection Corrective actions Implemented Sample Location: 005 Next to Houghton Area K. Holbrook, K. Improve the swarf dumpster by providing a different cover and Witkowski and removal of exisiting clumsier 9/5/2014 7/14/14 and 8/26 with Holbrook, Sample Taken 8/26/14 Witkowski, Provide different liner as an improved barriar for leak resistance 6/25 results Scripps, Schick received Above the limit and Fesko 7/7/14 for copper 9/5/2014 Note- Part of inspection included a review with Kay Stetcher on historical practices at the site which included material storage in the Dock 4 area of brass chips and tailings. We discussed the potential impact for copper pressence in the immediate area due to these historical practices. IER A tion Notify Agency in writing within 30 days of 4th exceedance Sample location: 005 Next to Houghton Area Person(s) Benchmark value Inspection conducting Date Actions Date exceeded date inspection Corrective actions Implemented Require that painting operations at the Tool Room have a plastic liner down prior to beginning painting 9/20/2014 K. Holbrook, K. Witkowski and Implement SS at the aluminum dumspter and provide materials to do Results received 7/21/14 Above limit for copper 7/24/2014 and 8/26/14 8/26 with Holbrook, Witkowski, Scripps, Schick and Fesko so 9/9/2014 Standard work created for mopping in all areas of the plant 8/28/2014 Investigating the potential to fill in Dock 4 and provide containment for inbound/recycled petroleum products will be obtained by above grade containment berm installation Notify Agency In writing within 30 days of 4th exceedance ' Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 12 10 2013_ CERTIFICATE OF COVERAGE NO. N00030027 FACILITY NAME Eaton Corporation —Engine Components Division COUNTY Person PERSON COLLECTING SAMPLES Katie Holbrook LABORATORY ESC Lab Cert. #i ENV375/DW21704/B10041 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2013 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' (month? DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply []SA ❑Other WS-III; NSW PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 Part A. Stormwater Benchmarks and Monitoring Results ❑ No discharge this period?2 outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 004 11/1/13 .25 1400 7.4 3.8 0.19 2.3 <5.6 0.023 005 11/1/13 .25 52.0 7.1 0.048 <0.005 0.085 <5.3 0.002 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. ' Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic c . s se, . e_definition as found in 40 CFR 469.22; and for cathode ray A% tube manufacture use the definition found in 40 CFR 469.31). OCT 10 204 NC DENR Rakigh R egiom Permit Date: 11/1/2012-10/31/2017 f OffiCQ SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver4Hd•`d cha ge shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with.the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certif- t at'this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution PreveritiorS.P,lan.' Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 No&! if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results Tor at end of monitoring, period in the case o "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date: 11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/2S/2012 Page 3 of 3 OESC t Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Report Summary Tuesday November 12, 2013 Report Number: L666370 Samples Received: 11/02/13 Client Project: 28091-R 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fa (615) 75B-5859 Tax I.D. 62-0814269 Est. 1970 Description: Eaton Corp Semi -Annual Stormwater The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Entire Report Reviewed By: A44— JiM4Hunt , ESC Representative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT -- PH-0197, FL - E87467, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-7, TX - T104704245-11-3, 0K - 9915, PA - 68-02979, 1A Lab #364 Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lot> Sciences. Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA FLAP. This report may not be reproduced, except in full, wiChout written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standaid operating procedures: 060302, 060303, and 060 04. R: 2D�y Page 1 of 13 OCT 10 NC DENR Raleigh Regional ors ce T REPORT OF ANALYSIS Katie Holbrook. Eaton Corporation 2564 Durham Road Roxboro, NC 27573 November 12, 2013 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 753-585B 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 ESC Sample # L666370-01 Date Received November 02, 2013 Description Eaton Corp Semi -Annual Stormwater Site ID ROXBORO, NC Sample ID STORMWATER SAMPLE PT-001 Project # 28091-R Collected By Katie Holbrook Collection Date 11/01/13 14:45 Parameter Result MDL RDL Units Qualifier Method Date Dil. U = ND (Not Detected) MDL = Minimum Detection Limit = LOU = TRRP SUL RDL = Reported Detection Limit - LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 11/12/13 15:51 Printed: 11/12/13 15:51 Page 2 of 13 REPORT OF ANALYSIS Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 November 12, 2013 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5B58 1-600-767-5859 Fax (615) 758-5859 Tar. I.D. 62-0814229 ESL. 1970 ESC Sample 4 : L666370-02 Date Received November 02, 2013 Description Eaton Corp Semi -Annual Stormwater Site ID ROXBORO, NC Sample ID STORMWATER SAMPLE PT-002 Project 9 : 28091-R Collected By Katie Holbrook Collection Date 11/01/13 14:30 Parameter Result MDL RDL Units Qualifier Method Date Dil. U = ND (Not Detected) MDL Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 11/12/13 15:51 Printed: 11/12/13 15:51 Page 3 of 13 Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS November 02, 2013 Eaton Corp Semi -Annual Stormwater STORMWATER SAMPLE PT-004 Katie Holbrook 11/01/13 14:15 12065 Lebanon Rd. Mr. Juliet, TN 37122 I615) 758-5858 1-800-767-5859 Far (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 November 12, 2013 ESC Sample # : L666370-03 Site ID Project 0 ROXBORO, NC 28091-R Parameter Result MDL RDL Units Qualifier Method Date Dil. Suspended Solids 1400 0.35 2.5 mg/1 2540 0- 11/08/13 1 TPN - Oil 6 Grease U 0.72 5.6 mg/1 1664A 11/08/13 1 Copper 3.8 0.0070 0.020 mg/1 200.7 11/12/13 1 Lead 0.19 0.0020 0.0050 mg/1 200.1 11/12/13 1 zinc 2.3 0.0034 0.030 mg/l 200.7 11/12/13 1 TTO Volatile Organics Acrylonitrile U 0.0019 0.010 mg/l J4 624 11/03/13 1 Benzene U 0.00033 0.0c10 mg/1 624 11/03/13 1 Bromodichloromethane U 0.00038 0.0010 mg/l 624 11/03/13 1 Bromoform U 0.00047 0.0010 mg/l 624 11/03/13 1 Bromomethane U 0.00007 0.0050 mg/1 624 11/03/13 1 Carbon tetrachloride U 0.00038 0.0010 mg/1 624 11/03/13 1 Chlorobenzene U 0.00035 0.0010 mg/1 624 11/03/13 1 Chlorodibromomethane U 0.00033 0.0010 mg/l 624 11/03/13 1 Chlorcethane U 0.00045 0.0050 mg/1 624 11/03/13 1 2-Chloroethyl vinyl ether U 0,0030 0.050 mg/l 624 11/03/13 1 Chloroform U 0,00032 0.0050 mg/l 624 11/03/13 1 Chloromethane U 0.00028 0.0025 mg/1 624 11/03/13 1 1,2-Dichlorobenzene U 0.00035 0.0010 mg/l 624 11/03/13 1 1,3-Dichlorobenzene U 0.00022 0.0010 mg/l 624 11/03/13 1 1,4-Dichlorobenzene U 0.00027 0.0010 mg/l 624 11/03/13 1 Dichlorcdifluoromethane U 0.00055 0,0050 mg/1 624 11/03/13 1 1,1-Dichloroethane U 0.00026 0.0010 mg/1 624 11/03/13 1 1,2-Dichloroethane U 0.00036 0.0010 mg/1 624 11/03/13 1 1,1-Dichlorcethene U 0.00040 0.0010 mg/1 624 11/03/13 1 trans-1,2-Dichloroethene U 0.00040 0,0010 mg/1 624 11/03/13 1 1,2-Dichloropropane U 0.00031 0.0010 mg/1 624 11/03/13 1 ci3-1,3-Dichloropropene U 0.00042 0.0010 mg/1 624 11/03/13 1 trans-1,3-Dichloropropene U 0.00042 0.0010 mg/1 624 11/03/13 1 Ethylbenzene U 0.00038 0.0010 mg/1 624 11/03/13 1 Methylene Chloride U 0.0010 0.0050 mg/1 J4 624 11/03/13 1 1,1,2,2-Tetrachlorcethane U 0.00059 0.0010 mg/l 624 11/03/13 1 Tetrachloroethene U 0,00037 0.0010 mg/1 624 11/03/13 1 Toluene U 0.0007B 0.0050 mg/1 624 11/03/13 1 1,1,1-Trichloroethane U 0.00032 0.0010 mg/1 624 11/03/13 1 1,1,2-Trichloroethane U 0.00038 0.0010 mg/1 624 12/03/23 1 Trichloroethene U 0.00040 0.0010 111g/1 624 11/03/13 1 Trichlorofluoromethane U 0.0012 0.0050 mg/l 624 11/03/13 1 Vinyl chloride U 0.00026 0.0010 mg/l 624 11/03/13 1 Surrogate Recovery U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = SQL - TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 11/12/13 15:51 Printed: 11/12/13 15:51 Page 4 of 13 JOESC L•A-6 S•C•I•E-N-C-E-S Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS November 02, 2013 Eaton Corp Semi -Annual Stormwater STORMWATER SAMPLE PT-004 Katie Holbrook 11/01/13 14:15 12065 Lebanon Rd. Mt. Juliet, TN 37122 1615) 758-5858 1-800-767-5859 Fax (615) 758-5659 Tax I.D. 52-0814289 Est. 1970 November 12, 2013 ESC Sample # : L666370-03 Site ID Project # ROXBORO, NC 28091-R Parameter Result MDL ROL Units Qualifier Method Date Dil. Toluene-d8 98.6 % Rec. 624 11/03/13 1 Dibromofluoromethane 103. % Rec. 624 11/03/13 1 a,a,a-Trifluorotoluene 97.8 % Rec. 624 11/03/13 1 4-Bromofluorobenzene 92.0 % Rec. 624 11/03/13 1 TTO Volatile Organics Acrolein U 0.0099 0.050 mg/1 624 11/04/13 1 Surrogate Recovery Pesticide/PCBs Aldrin U 0.0000081 0.000050 mg/1 608 11/07/13 1 Alpha BHC U 0.000017 0.00c050 mg/l 608 11/07/13 1 Beta BHC U 0.000018 0.000050 mg/l 608 11/07/13 1 Delta BHC U 0.000020 0,000050 mg/l 608 11/07/13 1 Gamma BHC U 0.000018 0,000050 mg/l 608 21/07/13 1 Chlordane U 0.000098 0.00050 mg/l 608 11/07/13 1 4,4-DDD U 0.000017 0.000050 mg/1 608 ll/07/13 1 4,4-DDE U 0.000016 0.000050 mg/1 608 ll/07/13 1 4,4-DDT U 0.000018 0.000050 mg/l 608 11/07/13 1 Dieldrin U 0.000018 0.000050 mg/l 608 11/07/13 1 Endosulfan I U 0.000016 0.000050 mg/l 608 11/07/13 1 Endosulfan II U 0.000018 0.000050 mg/l 608 11/07/13 1 Endosulfan sulfate U 0.000020 0.000050 mg/1 608 11/07/13 1 Endrin U 0.000019 0.000050 mg/1 608 11/07/13 1 Endrin aldehyde U 0.000014 0.000050 mg/l 608 11/07/13 1 Endrin ketone U 0.000017 0.000050 mg/1 608 11/07/13 1 Heptachlor U 0.000011 0.000050 mg/1 608 11/07/13 1 Heptachlcr epoxide U 0.000018 0.000050 mg/1 608 11/07/13 1 Hexachlorobenzene U 0.000013 0.000050 mg/l 608 11/07/13 1 Methoxychlor U 0.000019 0,000050 mg/1 608 11/07/13 1 Toxaphene U 0.00017 0.00050 mg/1 608 11/07/13 1 PCB 1016 U 0.000020 0.00050 mg/1 608 11/07/13 1 PCB 1221 U 0.000024 0.00050 mg/1 608 11/07/13 1 PCB 1232 U 0.000021 0,00050 mg/1 608 11/07/13 1 PCB 1242 U 0.000024 0.00050 mg/1 608 11/07/13 1 PCB 1248 U 0.000014 0.00030 mg/1 608 11/07/13 1 PCB 1254 U D.000018 0.00050 mg/l 608 11/07/13 1 PCB 1260 U 0.000015 0.00050 mg/1 608 11/07/13 1 Pest/PCBs Surrogates Decachlorobiphenyl 74.1 % Rec. 608 11/07/13 1 Tetrachloro-m-xylene 68.5 % Rec. 608 11/07/13 1 TTO Base/Neutral Extractables U = NO (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 11/12/13 15:51 Printed: 11/12/13 15:51 Page 5 of 13 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 158-5958 1-900-767-5e59 OESC Fax (015) 758-5859 t-.A• B 5•C• I•E•N•C,E•S Tax I.D. 62-0819389 Est. 1570 REPORT OF ANALYSIS Katie Holbrook November 12, 2013 Eaton Corporation 2564 Durham Road Roxboro, NC 27573 ESC Sample # L666370-03 Date Received November 02, 2013 Description Eaton Corp Semi -Annual Stormwater Site ID ROXBORO, NC Sample ID STORMWATER SAMPLE PT-004 Project # 28091-R Collected By Katie Holbrook Collection Date 11/01/13 14:15 Parameter Result MDL RDL Units Qualifier Method Date Dil. Acenaphthene U 0,00032 0.0010 mg/l 625 11/07/13 1 Acenaphthylene U 0.00031 0.0010 mg/1 625 11/07/13 1 Anthracene U 0.00029 0.0010 mg/l 625 11/07/13 1 Benzidine U 0.0043 0.010 mg/l 625 11/07/13 1 Benzo(a)anthracene U 0.00032 0.0010 mg/1 625 11/07/13 1 Benzo{b)fluoranthene U 0,00027 0.0010 mg/l 625 11/07/13 1 Benzo(k)fluoranthene U 0.00036 0.0010 mg/1 625 11/07/13 1 Benzo(q,h,i)perylene U 0.00033 0.0010 mg/1 625 11/07/13 1 Benzo(a)pyrene U 0.00034 0.0010 mg/l 625 11/07/13 1 Bis(2-chlorethoxy)methane U 0,00033 0.010 mg/l 625 11/07/13 1 Bis(2-chlorcethyl)ether U 0.0016 0.010 mg/1 625 11/07/13 1 Bis(2-chloroisopropyl)ether U 0.00044 0.010 mg/1 625 11/07/13 1 4-Bromophenyl-phenylether U 0.00034 0.010 mg/l. 625 11/07/13 1 2-Chloronaphthalene U 0.00033 0.0010 mg/l 625 11/07/13 1 4-Chlorophenyl-phenylether U 0.00030 0.010 mg/l 625 11/07/13 1 Chrysene U 0.00033 0.0010 mg/1 625 11/07/13 1 Dibenz(a,h)anthracene U 0.00028 0.0010 mg/l 625 11/07/13 1 3,3-Dichlorobenzidine U 0.0020 0.010 mg/1 625 11/07/13 1 2,4-Dinitrotoluene U 0.0016 0.010 mg/1 625 11/07/13 1 2,6-Dinitrotoluene U 0.00028 0.010 mg/l 625 11/07/13 1 1,2-Diphenylhydrazine U 0.00016 0.010 mg/1 625 11/07/13 1 Fluoranthene U 0.00031 0.0010 mg/1 625 11/07/13 1 Fluorene U 0.00032 0.0010 mg/1 625 11/07/13 1 Hexachlorobenzene U 0.00034 0.0010 mg/l 625 11/07/13 1 Hexachloro-1,3-butadiene U 0.00033 0.C10 mg/1 625 11/07/13 1 Hexachlorocyclopentadiene U 0,0023 0.010 mg/1 625 11/07/13 1 Hexachl.oroethane U 0,00037 0.010 mg/1 625 11/07/13 1 Indeno(1,2,3-cd)pyrene U 0.00028 0.0010 mg/l 625 11/07/13 1 Isophorone U 0.00027 0,010 mg/l 625 11/07/13 1 Naphthalene U 0.00037 0.0010 mg/l 625 11/07/13 1 Nitrobenzene U 0.00037 0.010 mg/1 625 11/07/13 1 n-Nitrosodimethylamine U 0.0013 0.010 mg/1 625 11/07/13 1 n-Nitrosodiphenylaruine U 0.00030 0.010 mg/l 625 11/07/13 1 n-Nitrosodi-n-propylamine U 0.00040 0.010 mg/1 625 11/07/13 1 Phenanthrene U 0.00037 0.0010 mg/1 625 11/07/13 1 Benzylbutyl phthalate U 0,00028 0.0030 mg/1 625 11/07/13 1 Bis(2-ethylhexyl)phthalate 0.0012 0.00071 0.0030 mg/1 J 625 11/07/13 1 Di-n-butyl phthalate 0.00037 0.00027 0.0030 mg/l J 625 11/07/13 1 Diethyl phthalate U 0.00028 C.0030 mg/l 625 11/07/13 1 Dimethyl phthalate U 0.00028 C.0030 mg/l 625 11/07/.13 1 Di-n-octyl phthalate U 0.00028 0.0030 mg/1 625 11/0?/13 1 Pyrene U 0.00033 0.0010 mg/l 625 11/07/13 1 1,2,4-Trichlorobenzene U 0.00036 0.010 mg/1 625 11/07/13 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 11/12/13 15:51 Printed: 21/12/13 15:51 Page 6 of 13 REPORT OF ANALYSIS Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received November 02, 2013 Description Eaton Corp Semi -Annual Stcrmwater Sample ID STORMWATER SAMPLE PT-004 Collected By Katie Holbrook Collection Date 11/01/13 14:15 Parameter Result MDL TTO Acid Extractables 4-Chloro-3-methylplenol U 0,00026 2-Chlorophenol U 0.00028 2,4-Dichlorophenol U 0.00028 2,4-Dimethylphenol U 0.00062 4,6-Di.nitro-2-methylphenol U 0.0026 2,4-Dinitrophenol U 0.0032 2-Nitrophenol U 0,00032 4-Nitropheno2, U 0,0020 Pentachlorophenol U 0.00031 Phenol 0.021 0.00033 2,4,6-Trichlorophenol U 0.00030 Surrogate Recovery 2-Fluorophenol 25.2 Phenol-d5 26.4 Nitrobenzene-d5 77.0 2-Fluorobiphenyl 82.1 2,4,6-Tribromophenol 21.0 p-Terphenyl-d14 81.6 12065 Lek)azion Rd. ME. Juliet, TN 37122 (615) 758-5B55 1-800-767-5859 :ax (615) 158-5859 Tar. I.D. 62-0814289 Est. 1970 November 12, 2013 ESC Sample # = L666370-03 Site ID ROXBORO, NC Project 4 : 28091-R RDL Units Qualifier Method Date Dil. 0.010 mg/l 625 11/07/13 1 0.010 mg/1 625 11/07/13 1 0.010 mg/l 625 11/07/13 1 0.010 mg/1 625 11/07/13 1 0,010 mg/l 625 11/07/13 1 0.010 mg/l 625 11/06/13 1 0.010 mg/1 625 11/07/13 1 0.010 mg/1 625 11/07/13 1 0.010 mg/l 625 11/07/13 1 0.010 mg/1 625 11/07/13 1 0,010 mg/l 625 11/07/13 1 % Rec. 625 11/07/13 1 % Rec. 625 11/07/13 1 % Rec. 625 11/07/13 1 % Rec. 625 11/07/13 1 % Rec. 625 11/07/13 1 % Rec. 625 11/07/13 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SOL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported_ 11/12/13 15:51 Printed: 11/12/13 15:51 Page 7 of 13 Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS November 02, 2013 Eaton Corp Semi -Annual Stormwater STORMWATER SAMPLE PT-005 Katie Holbrook 11/01/13 14:00 12065 Lebanon Rd. ML. Juliet, '1'0 37122 (615) 758-5658 1-800-767-5859 Fax (615) 758-5659 Tax I.D. 62-0814289 ESL. 1970 November 12, 2013 ESC Sample � : L666370-04 Site ID Project 4 ROXBORO, NC 28091-R Parameter Result MDL RDL Units Qualifier Method Date Dil. Suspended Solids 52. 0.35 2.5 mg/l 2540 D- 11/09/13 1 TPH - Oil & Grease U 0.72 5.3 mg/l 1664A ll/Oa/13 1 Copper 0.048 0.0070 0.020 mg/l 200.7 11/12/13 1 Lead U 0.0020 0.0050 mg/l 200.7 11/12/13 1 Zinc 0.085 0.0034 0.030 mg/l 200.7 11/12/13 1 TTO Volatile Organics Acrylonitrile U 0.0019 0.010 mg/l J4 624 11/03/13 1 Benzene U 0.00033 0.0010 mg/l 624 1l/03/13 I Bromodichloromethane U 0.00036 0.0010 mg/1 624 11/03/13 1 Bromoform U 0.00047 0.0010 mg/l 624 11/03/13 1 Bromomethane U 0.00087 0.0050 mg/1 624 11/03/13 1 Carbon tetrachloride U 0.00038 0.0010 mg/l 624 11/03/13 1 Chlorobenzene U 0.00035 0.0010 mg/1 624 11/03/13 1 Chlorodibromomethane U 0.00033 0.0010 mg/l 624 11/03/13 1 Chloroethane U 0.00045 0.0050 mg/l 624 11/03/13 1 2-Chloroethyl vinyl ether U 0.0030 0.050 mg/1 624 11/03/13 1 Chloroform U 0.00032 0.0050 mg/1 624 11/03/13 1 Chloromethane U 0.00028 0.0025 mg/1, 624 11/03/13 1 1,2-Dichlorobenzene U 0.00035 0.0010 mg/l 624 11/03/13 1 1,3-Dichlorobenzene U 0.00022 0.0010 mg/l 624 11/03/13 1 1,4-Dichlorobenzene U 0.00027 0.0010 mg/l 624 11/03/13 1 Dichlorodiflucromethane U 0.00035 0.0050 mg/l 624 11/03/13 1 1,1-Dichloroethane U 0.00026 0.0010 mg/1 624 11/03/13 1 1,2-Dichloroethane U 0.00036 0.0010 mg/l 624 11/03/13 1 1,1-Dichloroethene U 0.00040 0.0010 mg/1 624 11/03/13 1 trans-1,2-Dichloroethene U 0.00040 0.0010 mg/1 624 11/03/13 1 1,2-Dichloropropane U 0.00031 0.0010 mg/l 624 11/03/13 1 cis-1,3-Dichloropr.opene U 0.00042 0.0010 mg/l 624 11/03/13 1 trans-1,3-Dichloropropene U 0.00042 0.0010 mg/l 624 11/03/13 1 Ethylbenzene U 0,00038 0.0010 mg/l 624 11/03/13 1 Methylene Chloride U 0.0010 0.0050 mg/l J4 624 11/03/13 1 1,1,2,2-Tetrachlorcethane U 0.00059 0.0010 mg/1 624 11/03/23 1 Tetrachloroethene U 0.00037 0.0010 mg/l 624 11/03/13 1 Toluene U 0.00078 0.0050 mg/l 624 11/03/13 1 1,1,1-Trichloroethane U 0.00032 0.0010 mg/1 624 11/03/13 1 1,1,2-Trichloroethane U 0.00038 0.0010 mg/1 624 11/03/13 1 Trichloroethene U 0.00040 0.0010 mg/1 624 11/03/13 1 Trichlorofluoromethane U 0.0012 0.0050 rng/l 624 11/03/13 1 Vinyl chloride U 0.00026 0.0010 mg/1 624 11/03/13 1 Surrogate Recovery U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full., without the written approval from ESC. Reported: 11/12/13 15:51 Printed: 11/12/13 15:51 Page B of 13 JOESC L•A,8 5•C• I•E•N'C'E•S Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS November 02, 2013 Eaton Corp Semi -Annual Stormwater STORMWATER SAMPLE PT-005 Katie Holbrook 11/01/13 14:00 12065 Lehanon Rd. Mt. Julie[, TN 37122 (615) 758-5B58 1-800-767-5859 Fax (615) 758-5659 Tax I.D. 62-0814289 Est. 1970 November 12, 2013 ESC Sample # : L666370-04 Site ID ROXBORO, NC Project # : 28091-R Parameter Result MDL RDL units Qualifier Method Date Dil. Toluene -dB 99.5 % Rec. 624 11/03/13 1 Dibromofluoromethane 102. % Rec. 624 11/03/13 1 a,a,a-Triflucrotoluene 97.1 % Rec. 624 11/03/13 1 4--9romofluorobenaene 90.8 % Rec. 624 11/03/13 1 TTO Volatile Organics Acrolein Surrogate Recovery Pesticide/PCBs Aldrin Alpha BHC Beta BHC Delta BHC Gamma BHC Chlordane 4,4-DDD 4,4-DD£ 4,4-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachl,cr Heptachlor epoxide Hexachlorobenzene Methoxychlor Toxaphene PCB 1016 PCB 1221 PCB 1232 PCB 1242 PCB 1249 PCB 1254 PCB 1260 Pest/PCBs Surrogates Decachlorobiphenyl Tetrachloro-m-xylene TTO Base/Neutral Extractables U 0.0089 0.050 mg/l 624 11/04/13 1 79.0 65.0 0.0000081 0.000030 mg/l 608 11/07/13 1 0.000017 0.000050 mg/I 608 11/07/13 1 0.000018 0.000050 mg/l 608 11/07/13 1 0.000020 0.000050 mg/l 608 11/07/13 1 0.000016 0.000050 mg/l 608 11/07/13 1 0.000098 0.00050 mg/l 608 11/07/13 1 0,000017 0.000050 mg/l 608 11/07/13 1 0.000016 0.000050 mg/l 608 11/07/13 1 0,000018 0.000050 mg/l 608 11/07/13 1 0.000018 0.000050 mg/1 608 11/07/13 1 0.000018 0.000050 mg/l 608 11/07/13 1 0.000018 0.000050 mg/1 608 11/07/13 1 0.000020 0.000050 mg/I 608 12/07/13 1 0.000019 0.000030 mg/l 608 11/07/13 1 0.000014 0.000050 mg/l 608 11/07/13 1 0.000017 0.000050 mg/l 608 11/07/13 1 0.000011 0.000050 mg/1 608 11/07/13 1 0.000018 0.000050 mg/l 608 12/07/13 1 0.000013 0.000050 mg/l 608 11/07/13 1 0.000019 0,000050 mg/l 608 11/07/13 1 0.00017 0.00050 mg/I. 608 12/07/13 1 0.000020 0.00050 mg/i 608 11/07/13 1 0.000024 0.00050 mg/l 608 11/07/13 1 0.000021 0.00050 mg/1 608 11/07/13 1 0.000024 0.00050 mg/l 608 11/0-1/13 1 0.000014 0.00050 mg/1 608 11/07/13 1 0.090018 0.00050 mg/1 608 21/07/13 1 0.000015 0,00050 mg/l 608 11/07/13 1 % Rec. 608 11/07/13 1 % Rec. 608 11/07/13 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shaI,l not be reproduced, except in full, without the written approval from ESC. Reported: 11/12/13 15:51 Printed: 11/12/13 15:51 Page 9 of. 13 12065 Lebanon Rd. Mc. Juliet, TN 37122 1615) 756-585B 1-800-767-5659 *ESC Fax (615) 758-5859 L. S•G•I•E•N•C•E•S Tax I.D. 62-OE14289 EsL. 1970 REPORT OF ANALYSIS Katie Holbrook November 12, 2013 Eaton Corporation 2564 Durham Road Roxboro, NC 27573 ESC Sample L666370-04 Date Received November 02, 2013 Description Eaton Corp Semi -Annual Stormwater Site ID ROXBORO, NC Sample ID STORMWATER SAMPLE PT-005 Project f 2809I-R Collected By Katie Holbrook Collection Date 11/01/13 14:00 Parameter Result MDL RDL Units Qualifier Method Date Dil. Acenaphthene U 0.00032 0.0010 mg/1 625 11/07/13 1 Acenaphthylene U 0.00031 0.0010 mg/1 625 11/07/13 1 Anthracene U 0.00029 0.0010 mg/1 625 11/07/13 1 Benzidine U 0.0043 0,010 mg/l 625 11/07/13 1 Benzo(a)anthracene U 0,00032 0.0010 mg/l 625 11/07/13 1 Benzo(k)fluoranthene U 0.00027 0.0010 mg/l 625 11/07/13 1 Benzo(k)fluoranthene U 0.00036 0.0010 mg/1 625 11/07/13 1 Benzo(g,h,i)perylene U 0.00033 0.0010 mg/l 625 11/07/13 1 Benzo(a)pyrene U 0.00034 0.0010 mg/l 625 11/07/13 1 Bis(2-chlorethoxy)methane U 0.00033 0,010 mg/1 625 11/07/13 1 Bis(2-chloroethyl)ether U 0.0016 0.010 mg/l 625 11/07/13 1 Sis(2-chloroisopropyl)ether U 0,00044 0.010 mg/l 625 ll/07/13 1 4-Bromophenyl-phenylether U 0.00034 0.010 mg/l 625 11/01/13 1 2-Chloronaphthalene U 0.00033 0.0010 mg/1 625 11/07/13 1 4-Chlorophenyl-phenylether U 0.00030 0.010 mg/l 625 11/07/13 1 Chrysene U 0.00033 0.0010 mg/l 625 11/07/13 1 Dibenz(a,h)anthracene U 0,00028 0.0010 mg/l 625 11/07/13 1 3,3-Dichlorobenzidine U 0.0020 0.010 mg/l. 625 1I/07/13 1 2,4-Dinitrotoluene U 0.0016 0.010 mg/l 625 11/07/13 1 2,6-Dinitrotoluene U 0.00028 0.010 mg/l 625 11/07/13 1 1,2-Diphenylhydrazine U 0.00016 0.010 mg/1 625 11/07/13 1 Fluoranthene U 0.00031 0.0010 mg/l 625 11/07/13 1 Fluorene U 0.00032 0.0010 mg/1 625 11/07/13 1 Hexachlorobenzene U 0,00034 0.0010 mg/l 625 11/07/13 1 Hexachloro-1,3-butadiene U 0.00033 0.010 mg/l 625 11/07/13 1 Hexachlorocyclopentadiene U 0.0023 0.010 Ong/l 625 11/07/13 1 Hexachloroethane U 0.00037 0.010 mg/1 625 11/07/13 1 lndeno(1,2,3-cd)pyrene U 0.00028 0.0010 mg/1 625 11/07/13 I Isophorone U 0.00027 0.010 mg/l 625 11/07/13 1 Naphthalene U 0.00037 0.0010 mg/1 625 11/07/13 1 Nitrobenzene U 0.00037 0.010 mg/l 625 21/07/13 1 n-Nitrosodimethylamine U 0,0013 0,010 mg/l 625 11/07/13 1 n-Nitrosodiphenylamine U 0.00030 0.010 mg/l 625 ll/07/13 I n-Nitrosodi-n-propylamine U 0.80040 0.010 mg/1 625 11/07/13 1 Phenanthrene U 0.00037 0.0010 mg/l 625 11/07/13 1 Benzylbutyl phthalate U 0,00028 0.0030 mg/l 625 11/07/13 1 Bis(2-ethylhexyl)phthalate 0,0012 0.00071 0.0030 mg/1 J 625 11/07/13 I Di-n-butyl phthalate 0.00039 0.00027 0.0030 mg/1 J 625 11/07/13 1 Diethyl phthalate U 0-00028 0.0030 mg/l 625 11/07/13 1 Dimethyl phthalate U 0.00028 0.0030 mg/l 625 11/07/13 1 Di-n-octyl phthalate U 0.00028 0.0030 mg/1 625 11/07/13 1 Pyrene U 0.00033 0.0010 mg/l 625 11/07/13 1 1,2,4-Trichlorobenzene U 0.00036 0.010 mg/l 625 11/07/13 1 U = NO (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL ROL = Reported Detection Limit = LOQ = PQL - EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 11/12/13 15:51 Printed: 11/12/13 15:51 Page 10 of 13 REPORT OF ANALYSIS Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received November 02, 2013 Description Eaton Corp Semi -Annual Stormwater Sample TD STORMWATER SAMPLE PT-005 Collected By Katie Holbrook Collection Date 11/01/13 14:00 Parameter TTO Acid Extractables 4-Chloro-3-methylphenol 2-Chlorophencl 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol Surrogate Recovery 2-Fluorophenol Phenol-d5 Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol p-Terphenyl-d14 U = ND (Not Detected) Result MDL 12065 Lebanon Rd, Mt. JUIieC, TN 37122 t615) 758-5858 1-800-767-5859 Fax (615) 756-5B59 Tax I.D. 62-0814289 f Est. 1910 November 12, 2013 ESC Sample # : L666370-04 Site ID ROXBORO, NC Project # 28091-R RDL Units Qualifier Method Date Dil, U 0.00026 0.010 mg/l 625 11/07/13 1 U 0.00028 0.010 mq/1 625 11/07/23 1 U 0.00028 0.010 mg/l 625 11/07/13 1 U O.00062 0.010 mg/l 625 11/07/13 1 U 0.0026 0.010 mg/l. 625 11/07/13 1 U 0.0032 0,010 mg/l 625 11/OB/13 1 U O.00032 0.010 mg/1 625 11/07/13 1 U 0.0020 0.010 mg/l 625 11/07/13 1 U 0.00031 0.010 mg/l 625 11/07/13 1 0,00088 0.00033 0.010 mg/l J 625 11/07/13 1 U 0.00030 0.010 mg/l 625 11/07/13 1 34.5 % Rec. 625 11/07/13 1 27.6 % Rec. 625 11/07/13 1 76.8 % Rec. 625 11/07/13 1 80.3 % Rec. 625 11/07/13 1 38.9 % Rec. 625 11/07/13 1 84.7 % Rec. 625 11/07/13 1 MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit - LQQ - PQL = EQL = TRAP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 11/12/13 15:51 Printed: 11/12/13 15:51 Page 11 of 13 Attachment A List of Analytes with QC Qualifiers Sample Work Sample Run Number Group Type Analyte ID Qualifier L666370-03 WG690400 SAMP Acrylon.itrile R2848421 J4 WG690400 SAMP Methylene Chloride R2848421 J4 WG690885 SAMP Bis(2-ethylhexyl)phthalate R2850143 J WG690685 SAMP ni-n-butyl phthalate R2850143 J L666370-04 WG690400 SAMP Acrylonitrile R2846421 J4 WG690400 SAMP Methylene Chloride R2848421 J4 WG690885 SAMP Bis{2-ethylhexyl)phthalate R2850143 J WG690885 SAMP Di-n-butyl phthalate R2850143 J WG690865 SAMP Phenol R2850143 J Page 12 of 13 Attachment B Explanation of QC Qualifier Codes Qualifier Meaning J (EPA) - Estimated value below the lowest calibration point. Confidence correlates with concentration. J4 The associated batch QC was outside the established quality control range for accuracy. Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable "unless qualified as 'R' (Rejected)." Definitions Accuracy - The relationship of the observed value of a }mown sample to the true value of a }mown sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence_ Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. Page 13 of 13 Summary of Remarks For Samples Printed 11/12/13 at 15:51:53 TSR Signing Reports: 350 R5 - Desired TAT MDL/RDL; Accounting - pending credit app Sample: L666370-01 Account: EATONRNC Received: 11/02/13 07:00 Due Date: 11/08/13 00:00 RPT Date: 11/12/13 15:51 Do not report; MISC = Extraction for 602 and 625; Deleted metals, 608 and 625TTO per JH. AV 11/6 Sample: L666370-02 Account: EATONRNC Received: 11/02/13 07:OD Due Date: 11/08/13 00:00 RPT Date: 11/12/13 15:51 Do not report; MISC = Extraction for 608 and 625; Deleted metals,TSS,OGHEx, 608 and 625TTO per JH. AV 11/6 Sample: L666370-03 Account: EATONRNC Received: 11/02/13 07:00 Due Date: 11/08/13 00:00 RPT Date: 11/12/13 13:51 Sample: L666370-04 Account: EATONRNC Received: 11/02/13 07:00 Due ❑ate: 11/08/13 00:00 RPT Date: 11/12/13 15:51 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 9 16 14 CERTIFICATE OF COVERAGE NO. NCG030027 FACILITY NAME EaLqn Corporation -nine Con]Ronents Division COUNTY _ Person PERSON COLLECTING SAMPLES datie Holbrook LABORATORY ESC Lab Cert. i# ENV375/DW21704/810041 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2014 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly'. August_ _ !month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA ❑Other IRIS -Ill fJ5W PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -) No discharge this period?? Outfall No. Date Sample Collected' {mo/dd/ r) 24-hour rainfall amount, Inches$5 Total Suspended Solids pH, standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ===> - - 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L Tool Room Trench 005) 8/19/14 0.625 3.6 6.8 0.017 Not Detected 0.018 1.5 0.003 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to s efinition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for ele efinition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). MAUNM Permit Date:31/1/2012-10/31/2017 OCT 10 2M NC DENR Raleigh R99WW OR* 5WU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BOL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No, Date Sample Collected' (mo/dd/ rj 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (5GT-HEM) Total Suspended Solids pH Benchmarks -__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Nate: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AAND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART fl SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART it SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Danny Smith, ThS Tier III notification and supporting documentation will be sent to the DWQ Regional Office Su ervisor in accordance with the General Stormwater Permit. Mail an original and one copy of this QMii. includinrf all "NO Dischgrae" reports, within 30 days of receipt of the lah results (or at end of monitoring Period in the se gf "No Discharge" e s Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPQRTED: "i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date-,11/1/2012-10/31/2017 912 r�/ (Da e) SWU-245, last revised 10/25/2012 Page 3 of 3 1. 1 40ESC L-A,B 5-C•I-E-N-C•E•5 Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Report Summary Tuesday August 26, 2014 12065 Lebanon Rd. Mt. Juliet, TH 37122 (615) 758-5858 1-600-767-5859 Pax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 Report Number: L716808 Samples Received: 08/19/14 Client Project: Description: Eaton Corp, Semi Annual Stormwater The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. if you have any questions regarding this data package, please do not hesitate to call. Entire Report Reviewed By: Ji Hunt ESC Representative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, A7, - 0612, MN - 047-999-395, NY - 11742, WT - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 Accreditation is only applicable to Ole Lest methods specified on each scope of accreditation held by ESC Lab Sciences. This report may noc be reproduced, except in full, without written approval from ESC Lah Sciences. Where applicable, sampling coriducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Page 1 of 15 OCT 10 20% NC DENR h Regk)'W Office V O U R L A B op C H O I C E REPORT OF ANALYSTS Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 August 26, 2014 ESC Sample # 12055 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-B00-767-5855 Fay. (615) 755-5855 Tar. I.D. 62-06152B9 Est. ID70 L716808-01 Date Received August 19, 2014 Description Eaton Corp, Semi Annual Stormwater Site ID Sample ID TOOL ROOM TRENCH Project # . Collected By Katie Holbrook � Collection Date 08/18/14 13:30 Parameter Result MDL RDL Units Qualifier Method Date Dil. pH (On Site} 6.8 su Temperature (on -site) 27. Deg. C Suspended Solids 3.6 0.35 2.5 mg/l 2540 D- 08/21/14 1 TPH - Oil s Grease 1.5 0.72 5.6 mg/l J 1664A 06/26/14 1 Copper 0.017 0.0053 0.020 mg/l J 6010C 08/20/14 1 Lead U 0.0019 0.0050 mg/1 6010C 08/20/14 1 Zinc 0.018 0.0059 0.050 mg/l J 6010C 08/20/14 1 TTO Volatile Organics Acrolein U 0.0089 0.050 mg/1 624 06/21/14 1 Acrylonitrile U 0.0019 0.010 mg/l 624 08/21/14 1 Benzene U 0.00033 0.0016 mg/l 624 06/21/14 1 Bromodichloromethane U D.00038 0.0010 mg/1 624 08/21/14 1 Bromoform U 0.00047 0.0010 mg/l 624 08/21/14 1 Bromomethane U 0.00087 0.0050 mg/1 624 08/21/14 1 Carbon tetrachloride U 0.00039 0.0010 mg/l 624 06/21/14 1 Chlorobenzene U 0.00035 0.0010 mg/l 624 08/21/14 1 Chlorodibromomethane U 0.00033 0.0010 mg/1 624 08/22/14 1 Chloroethane U 0.00045 0.0050 mg/l 624 OB/21/14 1 2-Chloroethyl vinyl ether U 0.0030 0.050 mg/1 624 08/21/14 1 Chloroform U 0.00032 0.0050 mg/l 624 08/21/14 1 Chloromethane U 0.00028 0.0025 mg/1 624 08/21/14 1 1,2-Dichlorobenzene U 0.00035 0.0010 mg/l 624 08/21/14 1 1,3-Dichlorobenzene U 0.00022 0.0010 mg/l 624 08/21/14 1 1,4-Dichlorobenzene U 0.00027 0.0010 mg/1 624 08/21/14 1 Dichlorodifluoromethane U 0.00055 0.0050 mg/1 624 OB/21/14 1 1,1-Dichloroethane U 0.00026 0.0010 mg/l 624 08/21/14 1 1,2-Dichloroethane U 0,00036 0.0010 mg/l 624 08/21/14 1 1,1-Dichloroethene U 0.00040 0,0010 mg/1 624 08/21/14 1 trans-1,2-Dichloroethene U 0.00040 0.0010 mg/l 624 08/21/14 1 1,2-Dichloropropane U 0.00031 0.0010 mg/1 624 08/21/14 1 ci3-1,3-Dichloropropene U 0,00042 0.0010 mg/1 624 08/21/14 1 trans-1,3-Dichloropropene U 0.00042 0,0010 mg/l 624 08/21/14 1 Ethylbenzene U 0.00038 0.0010 mg/l 624 08/21/14 1 Methylene Chloride U 0.0010 0.0050 mg/1 624 08/21/14 1 1,1,2,2-Tetrachloroethane U 0.00058 0.0010 mg/l 624 OB/21/14 I Tetrachloroethene U 0.00037 0.0010 mg/l 624 08/21/14 1 Toluene U 0.00078 0.0050 mg/l 624 08/21/14 1 1,1,1-Trichloroethane U 0.00032 0.0010 mg/1, 624 OB/21/14 I 1,1,2-Trichloroethane U 0,00036 0.0010 mg/l 624 OB/21/14 1 U = ND (Not Detected} MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not he reproduced, except in full, without the written approval from £SC. Reported: 08/26/14 17:59 Printed: 08/26/14 18:00 Page 2 of 15 OESC 1 Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS August 19, 2014 Eaton Corp, Semi Annual Stormwater TOOL ROOM TRENCH Katie Holbrook 08/16/14 13:30 12065 Lebanon Rd. Mt. Joliet, Tt" 37122 (615) 756-5858 1-800-767-5859 Fax {615) 758-5859 'Pax I.D. 62-0614289 Est. 1970 August 26, 2014 ESC Sample 4 L716806-01 Site ID Project (I . Parameter Result MDL RDL Units Qualifier Method Date Dil. Trichloroethene U 0.00040 0.0010 mg/1 624 03/21/14 1 Trichlorofluoromethane U 0.0012 0.0050 mg/1 624 08/21/14 1 Vinyl chloride U 0.00026 0.0010 mg/1 624 08/21/14 1 Surrogate Recovery Toluene-d6 100. % Rec. 624 08/21/14 1 Dibrcmoflucromethane 95.6 % Rec. 624 08/21/14 1 a,a,a-Trifluorotoluene 101. % Rec. 624 08/21/14 1 4-Bromofiuorobenzene 99.1 % Rec. 624 08/21/14 1 Pesticide/PCBs PCB 1016 U 0.000020 0.00050 m9/1 EPA-608 08/21/14 1 PCB 1221 U 0,000024 0,00050 mg/1 EPA-606 08/22/14 1 PCB 1232 U 0.000021 0.00050 mg/l EPA-608 06/21/14 1 PCB 1242 U 0.000024 0.00050 mg/1 EPA-608 0B/21/14 1 PCB 1248 U 0.000014 0.00050 mg/l EPA-608 08/21/14 1 PCB 1254 U 0,000018 0.00050 mg/l EPA-608 08/21/14 1 PCB 1260 U 0.000015 0.00050 mg/l EPA-608 08/21/14 1 Pest/PCBs Surrogates Decachlorobiphenyl 95.5 % Rec. EPA 608 OB/21/14 1 Tetrachloro-m-xylene 82.2 % Rec. EPA 608 08/21/14 1 TTO Base/Neutral Extractables Acenaphthene U 0.00032 0.0010 mg/1 625 08/22/14 1 Acenaphthylene U 0.00031 0.0010 mg/1 625 06/22/14 1 Anthracene U 0.00029 0.0010 mg/1 625 08/22/14 1 Benzidine U 0.0043 0.010 mg/l J3 625 08/22/14 1 Benzo(a)anthracene U 0.00032 0.0010 mg/1 625 08/22/14 1 Benzo(b)fluoranthene U 0.00027 0.0010 mg/l 625 08/22/14 1 Benzc(k)fiuoranthene U 0.00036 O.0010 mg/1 625 08/22/14 1 Benzo(g,h,i)perylene U 0.00033 0.0010 mg/1 625 08/22/14 1 Benzo(a)pyrene U 0.00034 0.0010 mg/l 625 C8/22/14 1 Bis(2-chlorethoxy)methane U 0.00033 0.010 mg/l 625 09/22/14 1 Bis(2-chloroethyl)ether U 0.0016 O.C10 mg/1 625 06/22/14 1 Bis(2-chloroisopropyl)ether U O.00044 0.010 mg/1 625 08/22/14 1 4-Bromophenyl-phenylether U 0,00034 0.010 mg/l 625 08/22/14 1 2-Chloronaphthalene U C.00033 0.0010 mg/1 625 08/22/14 1 4-Chlorophenyl-phenylether U 0.00030 0.010 mg/1 625 08/22/14 1 Chrysene U 0.00033 0.0010 mg/l 625 08/22/14 1 Dibenz(a,h)anthracene U 0.00028 0.0010 mg/1 625 08/22/14 1 3,3-Dichlorobenzidine U 0.0020 0.010 mg/1 625 08/22/14 1 2,4-Dinitrotoluene U 0.0016 0.010 mg/1 J4 625 08/22/14 1 2,6-Dinitrotoluene U 0.00028 0.010 mg/l 625 08/22/14 1 1,2-Dipheny1hydrazine U 0.00016 0.010 mg/1 625 08/22/14 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit - LOQ = PQL = EQL - TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/26/14 17:59 Printed: 08/26/14 18:00 Page 3 of 15 Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS August 19, 2014 Eaton Corp, Semi Annual Stormwater TOOL ROOM TRENCH Katie Holbrook 08/18/14 13:30 12065 Lebanon Rd. Mt. Juliet, 7N 31122 1615) 758-5858 1-8D0-767-5859 Fax 1615) 758-5859 Tax I.D. 62-0814289 Est. 1970 August 26, 2014 ESC Sample # L7168OB-01 Site ID Project H . Parameter Result MDL RDL Units Qualifier Method Date Dil. Fluoranthene Fluorene Hexachlorobenzene Hexachloro-1,3-butadiene Hexachlorocyclopentadiene Hexachloroethane 1ndeno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethylamine n-Nitrosodiphenylamine n-Nitrosodi-n-propylamine Phenanthrene Benzylbutyl phthalate Bis(2-ethylhexyl)phthalate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene TTO Acid Extractables 4-Chloro-3-methylphenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol Surrogate Recovery 2-Fluorophenol Phenol-d5 Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol p-Terphenyl-d14 U 0,00031 0.0010 mg/l 625 06/22/14 1 U 0.00032 0.0010 mg/1 625 08/22/14 1 U 0.00034 0.0010 mg/1 625 08/22/14 1 U 0.00033 0.010 mg/1 625 C8/22/14 I U 0,0023 0.010 mg/l 625 08/22/14 1 U 0.00037 0.010 mg/l 625 08/22/14 1 U 0.00028 0.0010 mg/1 625 OB/22/14 1 U 0.00027 0.C10 mg/1 625 08/22/14 1 U 0.0003-1 0.0010 mg/1 625 08/22/14 1 U 0.00037 C.010 mg/1 625 08/22/14 1 U 0.0013 0.01C mg/1 625 CS/22/14 I U 0.00030 0.010 mg/1 625 06/22/14 1 U 0.00040 0.010 mg/1 625 08/22/14 1 U 0.00037 0,0010 mg/l 625 08/22/14 1 U 0.00028 0.0030 mg/l 625 08/22/14 1 0.0012 0.00071 0.0030 mg/l J 625 08/22/14 1 0.00054 0.00027 0.0030 mg/l J 625 06/22/14 1 0.0011 0.00028 0.003C mg/1 J 625 08/22/14 1 U 0.00028 0,0030 mg/1 625 08/22/14 1 U 0.00028 0.0030 mg/1 625 08/22/14 1 U 0.00033 0.0010 mg/1 625 C8/22/14 1 U 0.00036 C.010 mg/1 625 08/22/14 1 U 0.00026 0,010 mg/1 625 08/22/14 1 U 0.00028 C.01C mg/l 625 06/22/14 1 U 0,00028 0.010 mg/1 625 08/22/14 1 U 0.00062 0.010 mg/l 625 08/22/14 1 U 0.0026 0,010 mg/1 625 08/22/14 l U 0.0032 0.010 mg/l 625 08/22/14 1 U 0.00032 0.010 mg/1 625 C8/22/14 1 U 0,0020 0.010 mg/1 625 08/22/14 1 U 0.00031 0,010 mg/1 625 08/22/14 1 U 0.00033 0.010 mg/1 625 08/22/14 1 U 0.00030 0.010 mg/l 625 08/22/14 1 42.4 % Rec. 625 08/22/14 1 33.2 % Rec. 625 08/22/14 1 56.4 % Rec. 625 06/22/14 1 62.5 % Rec. 625 08/22/14 1 73.5 % Rec. 625 08/22/14 1 57.8 % Rec. 625 08/22/14 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/26/14 17:59 Printed: 08/26/24 16:00 Page 4 of 15 Attachment A List cf Analytes with QC Qualifiers Sample Work Sample Run Number Group Type Analyte ID L716808-01 WG738310 SAMP Benzidine R298004B WG738310 SAMP 2,4-Dinitrotoluene R2980048 WG738310 SAMP Bis(2-ethylhexyl)phthalate R2980046 WG738310 SAMP Di-n-butyl phthalate R2980048 WG738310 SAMP Diethyl phthalate R2980048 WG738628 SAMP PCB 1016 R2979207 WG738219 SAMP Copper R2978645 WG738219 SAMP zinc R2978645 WG739395 SAMP TPH - Oil & Grease R2981365 Qualifier Page 5 of 15 Attachment B Explanation of QC Qualifier Codes Qualifier Meaning J (EPA) - Estimated value below the lowest calibration point. Confidence correlates with concentration. J3 The associated batch QC was outside the established quality control range for precision. J9 The associated batch QC was outside the established quality control range for accuracy. Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either. EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all. reported data is valid and useable "unless qualified as 'R' (Rejected)." Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. Page 6 of 15 Summary of Remarks For Samples Printed 08/26/14 at 18:00:10 TSR Signing Reports: 350 R5 - Desired TAT MDL/RDL; PO = 79918 Sample: L716B08-01 Account: NATONRNC Received: 08/19/14 09:00 Due Date: 08/26/14 00:00 RPT Date: 08/26/14 17:59 12OG5 Lebanon Rd. Mt, Juliet, TN 37122 (615) 758-5858 1-800-767-5859 OESC Fax (615) 758-5859 L•A•8 S•C•I E•N C•E•5 Tax I.D. 62-0814289 Est. 1970 Eaton Corporation Katie Holbrook 2564 Durham Road nuality Assurance Report Level II Roxboro, NC 27573 August 26, 2014 L716808 Laboratory Blank Analyte Result Units % Rec Limit Batch Date Analyzed Copper < .02 mg/1 WG738219 08/20/14 12:52 Lead < .005 mg/1 WG738219 08/20/14 12:52 Zinc < .05 mg/I WG738219 08/20/14 12:52 Suspended Solids < 2.5 nig/l WG733332 05/21/14 09:18 1,1,1-Trichloroethane < .001 mg/1 WG738552 08/20/14 23:45 1,1,2,2-Tetrachloroethane < .001 ma/l WG73B552 08/20/14 23:4G 1,1,2-Trichloroethane < .001 mg/1 WG738552 08/20/14 23:46 1,1-Dichloroethene < .001 ma/l WG738552 08/20/14 23:46 1,1-Dichloroethene < .001 mg/1 WG736552 02/20/14 23:16 1,2-Dichlorobenzene < .001 mg/1 WG738552 C8/20/14 23:46 1,2--Dichloroethane < .001 mg/1 WG738552 08/20/14 23:46 1,2-Dichloropropene < .001 mg/l WG736552 08/20/14 23:46 1,3-Dichlorobenzene < .001 Trig/1 WG738552 O8/20/14 23:46 1,4-Dichlorobenzene < .001 mg/1 WG738552 08/20/14 23:46 2-Chloroethyl vinyl eLlier. < .05 mg/1 WG738552 08/20/14 233:46 Acrolein < .025 mg/1 WG738552 08/20/14 23:46 Acrylonitrile < .01 mg/1 WG738552 08/20/14 23:46 Benzene < .001 ma/1 WG733552 08/20/14 23:46 Bromodichloromethane < .001 mg/l WG738552 06/20/14 23:46 Bromoform < .001 mg/l WG738552 08/20/14 23:46 Bromomethane < .005 my/1 WG738552 08/20/14 23:46 Carbon tetrachloride < .001 mg/1 WG738552 06/20/14 23:46 Chlorobenzene < .001 mg/1 WG738552 08/20/14 23:46 Chlorodibromomethane < .001 ma/1 WG738552 08/2D/14 23:46 Chloroethane < .005 mg/1 WG738552 05/20/14 23:46 Chloroform < .005 mg/l WG738552 06/20/14 23:46 Chlorometharre < .0025 mg/1 WG738552 OB/20/14 23:46 cis-1,3-Dichloropropene < .001 mg/1 WG738552 08/20/14 23:46 Dichlorodifluoromethane < .005 mg/l W073B552 08/20/14 23:46 Ethylbenzene < .007 ma/1 WG738552 08/20/14 23:46 Methylene Chloride < .005 Ilia/1 WG738552 06/20/14 23:46 Tetrachloroethene < .001 mg/1 WG738552 09/20/14 23:46 Toluene < .005 nig/1 WG738552 08/20/14 23:46 trans-1,2-Dichloroethene < .001 mg/1 WG736552 08/20/14 23:46 trans•-1,3-Dichloropropene < .001 mg/1 wG738552 08/20/14 23:46 Trichlorcethene < .001 mg/1 WG738552 08/20/14 23:46 Trichlorofluoromethane < .005 mg/I WG738552 08/20/14 23:46 vinyl chloride < .001 mg/1 WG738552 39/20/14 22:46 4-Bromofluorobenzene % Rec. 99.40 71-126 WG738552 OB/20/14 23:46 Dibromofluoromethane 8 Rec. 97.00 78.3-121 WG738552 08/20/14 23:46 Toluene-d8 % Rec. 201.0 88.5-111 WG738552 08/2C/14 23:46 a,a,a-Trifluorotoluerie 8 Rec. 97.60 85-114 WG738552 08/20/14 23:46 PCB 1016 < .0005 mg/1 WG738628 08/21/14 13:10 PCB 1221 < .0005 nia/1 WG73862B 08/21/14 13:10 PCB 1232 < .0005 mg/1 WG738628 08/21/14 ia:10 PCB 2242 < .0005 mg/1 WG738628 08/21/14 13:10 PCB 1248 . .0005 mg/l WG738628 08/21/14 13:10 PCB 1254 < .DD05 mg/1 WG738628 08/21/14 13:10 PCB 1260 < .0005 mg/1 WG738628 08/21/14 13:10 Decachlorobiphenyl % Rec. 147,0 10-156 WG738628 08/21/14 13:10 Tetrachloro-m-xylene % Rec. 69.70 13.9-127 WG738628 08/21/14 13:10 Performance of this Ana Iyte is outside cf establislied criteria. For additional information, please see Attachment A 'List of Anal ytes with OC Qua liliers.' Page 7 of 15 12065 Lebanon Rd. Mt. Jaliet, TN 37122 1615) 758-5B58 1-800-767-5a59 *ESC Paz (615) 758-5859 L•A•6 5•C•I,E•N,C E5 Tax I.D. 62-0814289 Est. 1970 Eaton Corporation Katie Holbrook 2564 Durham Road ;luality Assurance Report Level lI Roxboro, NC 27573 August 26, 2014 L716808 Laboratory Blank Analyte Result Units 8 Rec Limit Batch Date Analyzed 1,2,4-Trichlorobenzene < .01 mg/1 WG738310 08/21/14 23:25 2,4,6-Trichlorophenol < .01 n19/1 WG738310 08/21/14 23:25 2,4-Dic)llorophenpl < .01 mg/1 WG738310 08/21/14 23:25 2,4-Dimethylphenol < .01 mg/1 W0738310 08/21/14 23:25 2,4-Dinitrophenol < .01 mg/1 WG738310 06/21/14 23:25 2,4-Dinitrotoluene < .01 mg/1 WG73831D 08/21/14 23:25 2,6-Dinitrotoluenp < .01 mg/1 WG738310 08/21/14 23:25 2-Chloronaphthalene < .001 mg/1 WG738310 08/21/14 23:25 2-Chloraphenol < .01 mg/1 WG738310 08/21/14 23:25 2-Nitrophenol < .01 mg/1 WG738310 08/21/14 23:25 3,3-Dichlorobenzidine < .01 mg/l WG738310 08/21/14 23:25 4,6-Dinitro-2-methy2phenol < .01 mg/l WG738310 08/21/14 23:25 4-Bromophenyl-phenylether < .01 mg/I WG738310 08/21/14 23:25 4-Chloro-3-methylphenol < .01 mg/I WG738310 OB/21/14 23:25 4-Ch1oronhenyI-phenylether < .01 mg/l WG738310 08/21/14 23:25 4-Nitrophenol < .01 mg/1 WG738310 OB/21/14 23:25 Acenaphthene < .001 mg/1 WG738310 06/21/14 23:25 Acenaphthylene < .001 mg/l W(738310 08/21/14 23:25 Anthracene < .001 mq/1 WG738310 08/21/14 23:25 1,2-Diphenylhydrazine < .01 Man WG738320 08/22/14 23:25 Benzidine < .01 mg/1 WG73V310 08/21/14 23:25 Benzola)anchracene < .001 mg/1 WC738310 08/21/14 23:25 Senzola)pyrene < .001 71g/1 WG738310 08/21/14 23:25 Benzo(b)fluoranthene < .001 mg/l WG13a310 08/21/14 23:25 Benzo(g,h,i)perylene < .001 mg/1 WG738310 06/21/14 23:25 Senzo(k)fluoranthene < .001 mg/l WG738310 08/21/14 23:25 Senzylbutyl phthalate < .003 mg/I WG736310 OB/21/14 23:25 Bis(2-chlorethoxy)methane < .01 mg/l WG738310 08/21/14 23:25 Bis(2-chloroethyl)ether < .01 mg/1 WG738310 OB/21/14 23:25 Bis(2-chloroisopropyl)ether < .01 mg/l WG733310 08/21/14 23:25 Bis{2-ethylhexyl)phthalate < .003 mg/l WG738310 08/21/14 22:25 Chrysene < .001 ma/1 WG73831C 08/21/14 23:25 Di-n-butyl phthalate < .003 mg/1 WG73B310 08/21/14 23:25 Di-n-octyl phthalate < .003 mg/1 WG738310 06/21/14 23:25 Dibenz(a,h)anthracene < .001 mg/l WG738310 06/21/14 23:25 Diethyl phthalate < .003 mg/l WG738310 OB/21/14 23:25 Dimethyl phthalate < .003 mg/l WG738310 08/21/14 23:25 Fluoranthene < .001 me/1 WG738310 08/21/14 23:25 Fluorene < .001 mg/1 wG738310 08/21/14 23:25 Hexachloro-1,3-butadiene < .01 mg/l WG739310 08/21/14 23:25 Herachlorobenzene < .001 ma/1 WG738310 08/21/14 23:25 Hexac)iIorocyclopentadiene < .01 me/i WG738310 08/21/14 23:25 Hexachloroethane < .01 mg/1 WG738310 08/21/14 23:25 Indenol1,2,3-cd)pyrene < .001 mg/1 wG738310 06/21/14 23:25 Isophorone < .01 nig/1 WG738310 08/21/14 23:25 n-Nitrosodi-n-pxopylamine < .01 mg/l WG738310 OB/21/14 23:25 n-Nitrosodimethylamine < .01 mg/1 WG738310 08/21/14 23:25 n-Nitrosodiphenylamirte < .01 ma/1 WG738310 06/21/14 23:25 Naphthalene < .001 mg/l WG738310 08/21/14 23:25 Nitrobenzene < .01 mg/1 WG738310 08/21/14 23:25 Pentachlorophenol < .001 Mg/.I W0738310 OB/21/14 23:25 Phenanthrene < .001 mg/i WG138310 08/21/14 23:25 Phenol < .01 mg/1 WG736110 08/21/14 23:25 Pyrene < .001 mg/1 WG738320 05/21/14 23:25 2,4,6-Tribromophenol % Rec. 88.70 11.2-130 WG738310 OB/21/14 23:25 2-Fluorobinhenyl 9 Rec. 79.30 29.5-131 WG736310 08/21/14 23:25 2-Fluoroohenol % Rec. 51.60 10-77.9 WG73831D 08/21/14 23:25 Nitrobenzene-d5 8 Rec. 66.50 21.8-123 WG735310 08/21/14 23:25 Phenol-d5 8 Rec. 38.50 5-70.1 WG739310 08/21/14 23:25 Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with 4C Qualifiers.' Page 8 of 15 12065 Lebanon Rd. Mt. 3ulie, T;d 37122 JOESC i6151 756-5838 1-B00-767-5859 Fax (615) 758-5559 L•A 9 5• C• I• E• N C• E•S Ta>: I.D. 62-0814289 ` Est. 1970 Eaton CorporeLicn Katie Holbrook• 2564 Durham Road Quality Assurance ReporL Level II Roxboro, NC 27573 August 26, 2014 L716808 Laboratory Blank Analyte Result Units Rec Limit Batch Pate Analyzed p-Terphenyl-d14 % Rec. 90.60 29.3-137 08/21/14 23:25 TPH - Oil d Grease < 5 mq/l WG739395 08/26/14 17:23 Duplicate Analyte Units Result Duplicate RPD LimiL Ref Samp Baton Suspended Solids mg/1 31.8 31.3 1.41 5 L716802-01 WG738332 Laboratory Control Sample Analyte Units Known Val Result 8 Rec Limit Batch Copper mg/1 1 I.04 104. 80-120 WG738219 Lead ma/1 1 1.06 106. BO-120 WG736219 Zinc mg/1 1 1.03 103. 60-120 WG736219 Suspended Solids mg/1 773 830. 114. 85-115 WG738332 1,1,1-Trichloroethane mg/1 .025 0.0232 92.7 73.2-123 WG738552 1,1,2,2-TetrachloroeLhane mg/1 .025 0.0257 103. 70.7-122 WG738552 1,1,2-Trichloroethane mg/1 .025 C.0257 103. 77.7-118 WG738552 1,1-Dichloroethane mg/1 .025 0.0227 90.9 70.7-126 WG738552 1,1-Dichloroethene mg/1 .025 0.0206 62.5 67.8-129 WG738552 1,2-Dichlorobenzene mg/1 .025 0,0255 102. 78.4-117 WG738552 1,2-Dichloroethane mg/1 .025 0.0227 90.9 68.2-124 WG736552 1,2-Dichloropropane mg/1 .D25 9.0249 99.8 76.5-119 WG738552 1,3-Dichlorobenzene mg/1 .025 0,0239 95.6 70.8-128 WG738552 1,4-Dichlorobenzene mo/I .025 0,0250 100. 78.6-115 WG738552 2-Chloroethyl vinyl ether mg/1 .125 0.124 99.3 43.E-150 WG738552 Acrolein mg/1 .125 0.113 90.8 10-190 WG738552 Acrylonitrile ma/1 .125 0.128 102. 55.2-130 WG738552 Benzene mg/1 .025 0.0234 93.6 74.6-121 WG738552 Bromodichloromethane mu/1 .025 0,0259 104, 75.1-116 WG738552 Bromoform mg/1 .025 0.0264 106. 67,5-130 WG738552 Bromomethane Pie/1 .025 0.0242 96.8 49.9-362 WG738552 Carbon tetrachloride ma/1 .025 0.0236 94.4 70.2-123 WG738552 Chiorobenzene mg/1 .025 0.0265 106, 78.1-119 WG738552 Chlorodibromcmethane mg/1 .025 0.0252 I01. 74-121 WG738552 Chloroethane mg/1 .025 0.020E 93.0 61.7-135 WG738552 Chloroform mg/1 .025 0,0238 95.1 76-121 WG738552 Chloromethane RIg/l .025 0,0205 82.2 51.5-129 WG738552 cis-1,3-Dichloropropene mg/1 .025 0.0275 113. 76.2-120 WG738552 Dichlorodifluoromethane mg/1 .025 0.0203 81.0 54.8-135 WG738552 Fthylbenzene mg/1 .025 0.0267 107. 78.8-122 WG738552 Methylene Chloride mg/1 .023 0.0216 66.2 70.3-120 WG738552 Tetrachloroethene mg/l .025 0.0274 109. 72.6-126 WG736552 Toluene mg/l .025 0,0249 99.4 79.7-116 WG738552 trans-1,2-Dichloroethene mg/1 '025 0.0223 89.0 72.G-121 WG738552 trans-1,3-Dichloropropene mg/1 .025 0.0279 112. 74.3-123 WG736552 Trichloroethene ma/1 .025 0.0248 99.3 77.7-118 WG738552 Trichlorofluoromethane mg/1 .025 0.0233 93.3 63.5-135 WG738552 Vinyl chloride mg/1 .025 0.0215 85.9 65.9-128 WG738552 4-Bromofluorobenzene 87.9p 71-126 WG738552 Dibrcmof1uoromet]�ane 92.90 7E.3-121 WG738552 Toluene-d8 100.0 88.5-111 WG738552 a, a, a-Trifluorotoluene 101.0 85-114 WG738552 Performance of this Analyte is outside of established criteria. For additional information, Please see Attachment A 'List of Arialytes with X Qualifiers.' Page 9 of 15 12065 Lehancrj Rd. Mt- Juliet, TN 37122 (615) 758-5858 1-800-767-5859 OESC Fax (615) 758-5659 L•A•a S•C•i•E•N•C•E•S Tax T.D. 62-0814289 Est. 1970 Eaton Corporation Katie Holbrook 2564 Durham Rosa Quality Assurance Report Level I1 Roxboro, NC 27573 August 26, 2014 1,716808 Laboratory Control Sample Analyte Units Known Val Result Rec Limit Batch PCB 1016 mg/1 .0005 0.000434 86.9 24.7-129 WG738626 PCB 1260 mg/l .0005 0.000562 112. 47.7-149 WG738626 Decachlorobiphenyl 915.60 10-156 WG738628 Tetrachloro-m-xylene 90.60 13.9-137 WG738628 1,2,4-Trichloronenzene uig/1 .C25 0.0160 7i.8 22.9-96.1 WG738310 2,4,6-Trichlorophenol mg/1 .025 0.0211 84.3 29.8-107 WG73B310 2,4-Dichlorephenol mg/l .025 0.0217 86.6 31.4-103 WG73B310 2,4-Dimethylphenol mg/1 .025 0.0214 85.5 31.9-107 WG738310 2,4-DinitroplienoI mg/l .025 0.0158 63.1 24.2-128 WG73631C 2,4-Dinitrot oluene mg/1 .025 0.0266 107.* 31.2-105 WG738310 2,6-Dinitrotoluene nig/l .025 0,0259 104. 30.5-206 WG738310 2-Chloronaphthalene mg/l .D25 0.0207 82.7 33.6-205 WG738310 2-Chlorophenol mg/1 .025 0.0186 74.3 26.2-91.5 WG738310 2-Nitrophenol mg/l .025 0.0220 87.8 25.9-106 WG736310 3,3-DichIorobenzidine mg/1 .025 0.0229 91.6 27.2-142 WG738310 4,6-Di nitro-2- met hyIpheno1 mg/1 .025 0.0251 100. 18.4-148 WG738310 4-Bromophenyl-phenylether mg/1 .025 0,0248 99.1 40.7-116 WG738310 4-Chloro-3-methylphenol mg/l .025 0.0240 96.1 35.7-100 WG73831D 4-Chlorophenyl-phenylether mg/l .025 0.0242 96.9 39-113 WG733320 4-Nitrophenol mg/1 .025 0.0113 45.1 10-52.1 WG738310 Acenaphthene mg/l .025 0,0212 84.8 36.7-109 WG736310 Acenaphthylene mg/1 .025 0.0199 79.6 36-106 W0738310 Anthracene mg/1 .025 0.0222 51.2 43.6-1I3 WG736310 1,2-Diphenylhydrazine mg/1 .025 0.0212 84.9 37.6-111 WG738310 Benzidine m(J/l .025 0.0101 40.4 10-165.2 WG738320 Benno{a)anthracene mg/1 025 0.0220 87.9 51.2-112 WG738310 Benzo(a)pyrene mg/l .025 0.0212 95.0 45.6-106 WG738310 Benzo(b)fluoranthene mg/1 .025 0.0229 91.7 47.6-111 WG738310 Benzo(g,h,i)perylene mg/1 .025 0.0239 95.7 45.2-117 WG738310 Benzo(k)fluoranthene ma/1 .025 0.0219 87.7 49.4-114 WG73631U Benzylbutyl phthalate mg/1 .025 0.0261 104. 31.6-123 WG738310 Bis(2-chlore thoxy)methane mg/l .025 0.0192 77.0 37.2-111 WG738310 Bis(2-chloroethyl)ether mg/1 .025 0.0151 60.3 22.6-108 WG738310 Bis(2-ch2oroisonropyl)ether mg/l .025 0.0193 77.2 32.9-100 WG738313 Bis(2-ethyIheY.yI)phthaIaCe mg/1 .025 0.0264 105. 36.9-134 WG738310 Chrysene mg/1 .025 0.0221 85.3 54.6-120 WG738310 Di-n-butyl phthalate mg/1 .025 0.0242 96.6 41.6-120 WG738310 Di-n-octyl phthalate mg/1 .025 0.0241 96.5 39.7-112 WG738310 Dibenz(a,h)anthracene mg/l '025 0,0242 96.9 42.8-118 WG738310 Diethyl phthalate mq/1 .025 0.0248 99.1 36.5-129 KG738310 Dimethyl phthalate ma/1 .025 0.0247 98.3 35.3-128 WG738310 Fluoranthene mg/1 .025 0.0214 65.5 45.9-115 WG738310 Fluorene mg/1 .025 0.0228 91.1 41-112 WG738320 Hexachlorc-I,3-butadiene mg/1 .025 0.0178 71.2 16.1-104 WG738310 Hexachlorobenzene mg/l .025 0.0244 97.E 38.5-116 WG736310 Hexachlerocyclopentadiene ma/1 .025 0.0113 45.1 10-121 WG718310 Hexachloroethane mg/1 .025 0.0160 64.0 16.5-a9.8 WG738310 Indeno(1,2,3-cd1pyrene mg/1 .025 0.0244 97.5 45-116 WG738310 Isophorone mg/1 .025 0.0209 83.3 35.4-112 WG738310 n-Nitresadi-n-propyIamine mg/1 .025 0.0188 75.1 33.2-106 WG135310 n-Nitrosodimethylamine ma/1 .025 0.0108 43.2 10-80.1 WG738310 n-Nitrosodipheny.lamine mg/l .025 0.0235 94.0 44.4-111 WG738310 Naphthalene mg/1 .025 0.0173 69.2 32.2-101 WG738310 Nitrobenzene mg/l .D25 0.0197 78.8 31.4-106 WG738310 Pentachlorophenol mg/1 .025 0.0160 64.0 10-97.4 WG738310 Phenanthrene mg/1 .025 0.0214 85.8 46.4-113 WG736310 Phenol mg/l .025 0.0111 44.5 10-57.9 WG738310 Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analyzes with QC Qualifiers.' Page 10 of 15 Eaton Corporation Katie Holbrook 2564 Durham Road Roxboro, NC 27573 Quality Assurance Report Level II L7168 08 12065 Lebanon Rd. Mt. JulieL, TN 31122 1615) 758-5858 1- BOO -767-5659 Fax (615) 758-5859 Tax I.D. 62-0814269 Est. 1970 August 26, 2014 Analyte Laboratory Control Sample Units Known Val Result $ Rec Limn Batch Pyrene mg/l .025 0.0222 88.6 46.3-117 WG738310 2,4,6-Tribromophenol 104.0 11.2-130 WG738310 2-Fluorcbipnenyl 62.70 29.5-131 WG738310 2-Fluorcphenol 53.40 10-77.9 WG738310 Nitrobenzene-d5 66.20 21.8-123 WG738310 Phenol-d5 43.60 5-70.1 WG736310 p-Terphenyl-d14 83.50 29.3-137 WG738310 TPH - Oil & Grease /1 20 17.3 56.5 78-114 KG739395 Laboratory Control Sample Duplicate Analyte Units Result Ref $Rec Limit RPD Limit Batch Copper mg/1 1.04 1.04 104. 80-120 0.0 20 WG73B215 Lead mg/l 1.07 1.06 107. 80-120 1.00 20 WG738219 Zinc mg/I 1,04 1.03 104. 80-120 1.00 20 WG738219 Suspended Solids mg/1 868. 880. 112. 85-115 1.37 5 WG738332 1,1,1-Trichloroetiiane mg/I 0,0230 0.0232 92.0 73.2-123 0.910 20 WG738552 1,1,2,2-Tetrachlorcethane mg/1 0.0256 0.0257 102. 70.7-122 0.510 20 WG738352 1,1,2-Trichloroethane mg/1 0.025E 0.0257 103. 77,7-116 0.340 20 WG738552 1,1-Dichloroethane mg/1 0,0218 0,0227 87.0 70.7-126 4.03 20 WG738552 I,1-Di chloroethene mg/1 0.0197 0.0206 79.0 67.8-129 4.73 20 WG738552 1,2-Dichlorobenzene mg/1 0.0254 0.0255 102. 78,4-117 0.290 20 WG736552 1,2-Dichloroethane mg/1 0.0223 0.0227 89.0 68.8-124 1.80 20 WG738552 2,2-Dichloropropane mg/l 0,0244 0,0249 98.0 76.5-119 2.26 20 WG738552 1,3-Dichlorobenzene mg/1 0,0232 0.0239 93.0 70.8-128 3.10 20 WG738552 1,4-1)ichlorobenzene mg/1 0.0248 0.0250 99.0 78.8-215 1.13 20 WG738552 2-Chloroethyl vinyl ether mg/1 0.129 0.124 103. 43.8-150 4.08 20 WG738552 Acrolein mg/1 0.123 0.113 98.0 10-190 7.89 28.1 WG738552 Acrylonitrile mg/l 0.132 0.128 106. 55.2-130 3,38 20 WG738552 Benzene mg/1 0,0228 0.0234 silo 74.8-121 2.70 20 WG738552 Bromodichloromethane mg/1 0.0255 0.0259 102. 75.1-116 1.66 20 WG738552 Bromoform mg/1 0,0264 0.0264 106. 67.5-130 0.110 20 WG738552 Bromomethane mg/1 0.0229 0.0242 92.0 49.9-162 5.45 20 WG738552 Carbon tetrachloride mg/] 0.0230 0.0236 92.0 70.2-123 2,56 20 WG738552 Chlorobenzene mg/1 0.0260 0,0265 104. 78.1-119 1.97 20 WG738552 Chlorodibromomethane mg/l 0.0247 0.0252 99.0 74-121 1.93 20 WG738552 ChloroeL'hane mg/1 0.0206 0.0208 82.0 61.7-135 0.970 20 WG738552 Chloroform mg/l 0.0231 0.0238 92.0 76-121 3.00 20 WG738552 Chloromethane mg/1 0,0197 0.0205 79.0 61.5-129 4.19 20 WG735552 cis-1,3-Dichloropropene mg/1 0.0265 0.0275 106. 78,2-120 3,78 20 WG738552 Dichlorodifluoromethane mg/I 0.0190 0.0203 76.0 54.8-135 6,46 20 WG739552 ELhylhenzene mg/1 0,0258 0.0267 103, 78.E-122 3.55 20 WG738552 Methylene Chloride mg/1 0.0208 0.0216 83.0 70.3-12D 3.73 20 WG73B552 Tetrachloroethene mg/1 0.0262 0.0274 105. 72.6-126 4,33 20 WG738552 Toluene mg/1 0.0246 0.0249 98-0 79.7-116 0.910 20 WG738552 trans-1,2-Dichloroethene mg/1 '0.0211 0.0223 84.0 72.6-121 3.33 20 WG736552 trans-1,3-Dichloropropene mg/1 0.0280 0.0279 112. 74.3-123 0.220 20 WG738552 Tfichloroethene mg/I 0.0238 0.0248 95.0 77.7-118 4.18 20 WG738552 TrLchlorofluorOmethane mg/1 0.0227 0.0233 91.0 63.5-135 2,79 20 WG738552 Vinyl chloride mg/1 0.0202 0.0215 81.0 65.9-128 5.97 20 WG738552 4-Sromofluorobenzene 86.60 71-126 WG738552 D i br Omo fl u o roffie tha rle 92.10 78.3-121 WG738552 Toluene-d8 101.0 86.5-111 WG738552 ' Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of An aIytes wieh OC Qualifiers.' Page 11 of 25 12065 Lebanon Rd. Mt. Juliet, TN 37122 1615) 758-5858 1- ODD -767-5859 OESC Fax (615) 758-5859 4•A B 5•C,I-E•N C E•S Tax 1.1). 62-0814285 Esc. 1970 Eaton Corporation Katie Holbrook 2564 Durham Road Quality Assurance Report Level 11 Roxboro, NC 27573 August 26, 2014 L716808 Laboratory Control Sample Duplicate Analyte Units Result _ Ref %Rec Limit RPD Limit Batch a,a,a-Trifluorctoluene 101.0 85-114 PCB 1D16 mg/1 0.000481 0.000434 96.0 24.7-128 10.3 34.9 wG73662B PCB 1260 mg/1 0.000569 0.000562 118. 47.7-149 4.64 28.8 WG738628 Decachlorobiphenyl 104.0 10-156 WG738628 Tetrachlor'o-m-xylene 90.30 13.9-131 WG738628 1,2,4-Triciilorobenzene mg/1 0.0192 0.0160 77.0 22.9-96.1 6.74 27.5 WG738310 2,4,6-Trichlorophenel ma/l 0.0210 0.0211 84.0 29.8-107 C.500 24.1 WG738310 2,4-Dichlcrophenol mg/1 0.0216 0.0217 86.0 31.4-103 0.410 24.9 WG73B310 2,4-Dimethvlphenol mg/1 0.0218 0,0214 87.0 31.9-107 1.76 25.7 WG738310 2,4-Dinitrophenol Mg/1 0.0168 0.0158 67.0 24.2-128 6.14 20.5 WG73B310 2,4-Dinitrotoluene mg/1 0.0263 0.026fi 105. 31.2-105 1.33 22 WG73a310 2,6-Dinitrotoluene mg/1 0,0260 0.0259 104. 30.6-106 D.420 23.1 WG738310 2-Chloronaphthalene me/1 0.C220 0.0207 68.0 33.6-105 6.17 23 WG738310 2-Chlorophenol 1110/1 0.0194 0.0186 78.0 26.2-91.5 4.40 26.5 WG138310 2-Nitrophenol DWI 0.0230 0.0220 92.0 25.9-106 4.76 26.9 WG738310 3,3-Dichloroben7idine mg/1 0.0245 0.0229 98.0 27.2-142 6.63 22.3 WG736310 4,6-Dinitro-2-methylphenol mg/1 0,0248 0.0251 99.0 19.4-148 0.850 24.4 WG733310 4-Bromopheny]-phenyiether mg/1 0.0255 0.024E 102. 40.7-116 2.73 21 WG738310 4-Chloro-3-met}lylphencl 111a/1 0.0243 0.0240 97.0 35.7-100 1.18 22.9 WG739310 4-Chlorophenyl-phenylether ❑ia/l 0.0256 0.0242 102. 39-113 5.69 20.9 WG738310 4-Nitrophenol mg/l 0.0121 0.0113 48.0 10-52.7 6.79 40 WG738310 AcenaphUiene ma/1 0.0212 0.0212 85.0 38.7-109 0.170 21.5 WG738310 Acenaphthylene mg/i 0.0215 0.0i99 86.0 36-1DG 7.69 21 WG738310 Anthracene mg/1 0.0227 0.0228 91.0 43.6-113 0.400 18.8 WG738310 1,2-Diphenylhydrazine mg/l 0.0222 0.02I2 89.0 37.6-111 4.47 21.1 WG736310 Ben zidiIle mg/1 0,00562 0.0201 22.0 10-165.2 57.0- 40 WG736310 Benzo(a)anthracene mg/l 0,0224 0.0220 89.0 51.2-112 1.65 20 WG736310 Benzola)pyrene mg/1 0.0201 DAM 83.0 45.6-106 2.42 20 WG738310 Benzo(b)fluoranthene mg/1 0.0228 0.0229 91.0 47.6-111 0.640 20 WG738310 Benzo(g,h,i)perylene mg/1 0.0240 0.0239 96.0 45.2-117 0.280 20 WG738310 Benzo(Y,)fluoranthene mg/1 0.0223 0.0229 99.0 49.4-114 1.87 20 WG736310 Henzylbutyl phthalate mg/1 0.0261 0.0261 104. 31.8-123 0.100 20.7 WG73B310 Bis(2-chlcrethoxy)methane mg/1 0.0197 0.0192 79.0 37.2-111 2.29 24.1 WG738310 Bis(2-chloroethyl)ether my/1 0.0162 0.0151 65.0 22.6-103 7.35 27.9 WG738310 2is(2-chloroisopropyl)ether mg/1 0.0183 0.0193 73.0 32.9-100 5.29 25.1 WG736310 Bis(2-ethylhexyllphthalate mg/1 0.0269 0.0264 107. 36.9-134 1,84 23.6 WG736310 Chrysene mg/1 0,0224 0.0221 50.0 54.5-120 2,30 20 WG738310 Di-n-butyl phtlalate mg/1 0.0251 0.0242 100. 42.8-120 3.76 20.2 WG738310 Di-n-octyl phthalate mg/1 0.0244 0.0241 98.0 39.7-112 1.32 21.1 WG738310 Dihenz(a,h)anthracene mg/1 0.0244 0.0242 97.0 42.E-1i8 0.570 20 WG738310 Diethyl phthalate mg/l 0.0250 0.0248 100. 36.5-129 1.03 20 WG738310 Dimethyl phthalate mg/1 0.0250 0,0247 ]Co. 35.3-128 1,25 20.8 WG738310 Flucranthene my/1 0.0220 0.0214 88.0 45.9-115 2.89 20 WG738310 Fluorene mg/1 0.0236 0.0229 95.0 41-112 4.30 20.2 WG738310 Hexachloro-1,3-butadiene mg/l 0.0199 0.0178 80.0 16.1-104 11.2 31.2 WG73B310 Heyachlorobenzene mall 0.025B 0.0244 103. 39.5-116 5.71 20.1 WG738310 Hexachlorocyclopentadiene mg/1 0.0116 0.0113 46.D 10-121 3.09 27.9 WG738310 Hexachloroethane mg/1 0.0176 DAM 70.0 16.5-89.8 9.52 30.7 WG738310 lndeno(1,2,3-cd)pyrene ma/1 0.0242 0,0244 97.0 45-116 0.61D 20 WG735310 isophorone mg/] 0.0225 0.0209 90.0 35.4-112 7.36 21.5 WG738310 n-Nitrosodi-n-propylamine mg/1 0.02C3 0.0188 61.0 33.2-]06 7.69 23.7 WG738320 n-Nitrosodimethylamine mg/l 0.0111 D.0108 44.0 10-80.1 2.69 37.5 WG738310 n-Nitrosodiphenyiamirie ma/1 0,0239 0.0235 95.0 44.4-113 1.58 20 WG738320 Naphthalene mg/l 0.0185 0.0173 74.0 32.2-101 6.96 23.8 WG738310 Nitrobenzene mg/l D.0199 0.0197 80.0 31.4-106 0.520 25.7 WG738310 Pentachlcrophenol mg/1 0.0173 0.0160 69.0 10-97.4 9.04 35.1 WG738310 Phenanthrene mg/l 0,0217 0.0214 87.0 46.4-113 1.17 20 WG738310 Performance of this Analyte is outside of established Criteria. For additional inror'mation, please see Attachment A 'List of Analytes with pC Qualifiers.' Page 12 of 15 JOESC L-A•B 5•C•1•E•N,C-E•S Eaton Corporation Katie Holbrook 2564 Durham Road Roxboro, NC 27573 Quality Assurance Report Level II 1,716808 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 August 26, 2014 Laboratory Control Sample Duplicate Analyte Units Result Ref `kec Limit RPD Limit Batch Phenol ma/l C.0116 0.0111 46.0 10-57.9 4.02 35 WG738310 Pyrene mg/1 0.0229 0.0222 91.0 46.3-117 3.19 20 SdG738310 2,4,6-Tri1>romophenol 99.60 11.2-130 wG738310 2-Fluorobiphenyl 82.40 29.5-131 WG738310 2-Fluoroohenol 56.60 10-77.9 WG738310 Nitrobenzene-d5 87.40 21.8-123 WG738310 Phenol-d5 44.50 5-70.1 WG738310 o-Terphenyl-d14 94.30 29.3-137 WG738310 TPH - Oil & Grease mg/1 16.9 17.3 84.0 78-114 2.34 18 WG739395 Matrix Spike Analyte Units MS Res Ref Res TV 9 Rec Limit Ref Samp Batch 1,1,1-Trichloroethane mg/1 0.0214 0.0 .025 66.0 58.7-134 1,716460-02 WG738552 1,1,2,2-Tetrachloroethane mg/l 0.0262 0.0 .025 100. 56-132 L716460-02 WG738552 1,1,2-Trichloroethane mg/1 0.0242 0.0 .025 97.0 66.3-125 11716460-02 WG738552 1,1-nichloroethane mg/1 0.0198 0.0 .025 79.0 58.5-132 L716460-02 WG738552 1,1-Dichloreethene ma/l 0.0168 0.0 .025 67.0 51.1-140 L716460-02 WG738552 1,2-Dichlorobenzene mg/l 0.0237 0.0 .C25 95.0 68.2-123 L716460-02 WG738552 1,2-Dichloroethane mg/1 0.019B 0.0 .025 79.0 50-126 L716460-02 WG738552 1,2-Dichloropropane mg/I 0.0?18 0.0 .025 87.0 64.2-123 L716460-02 WG738552 1,3-Dichlorobenzene mg/1 0.0224 0.0 .025 90.0 63.1-131 L716460-02 WG738552 1,4-Dichlorobenzene mg/1 0.0234 0.0 .025 94.0 68.6-123 L716460-02 WG738552 2-Chloroethyl vinyl ether mg/1 0.0184 0.0 .125 15.0 10-155 L716460-02 WG738552 Acrolein mg/l 0.106 C.0 .125 85.0 10-200 L716460-02 WG738552 Acrylonitrile mg/l 0.120 0.0 .125 96.0 49.4-I33 L716460-02 WG738552 Benzene mg/i 0.020C 0.0 .025 80.0 54.3-133 L716460-C2 WG738552 Bromodichlorometharne mg/1 0.0234 0.0 .025 94.0 63.9-121 L716460-02 WG738552 Hromoform mg/1 0.0253 0.0 .025 160. 59.5-134 L716460-02 WG738552 Sromcmethane mg/l 0.0183 0.0 .025 73.0 41.7-155 L716460-02 WG738552 Carbon tetrachloride nig/1 0.0211 0.0 .025 84.0 55.7-134 L716460-02 WG738552 Chlorobenzene mg/l 0.0239 0.0 .025 96.0 67-125 L716460-02 WG738552 Chlorodibromomethane mg/1 0.0234 0.0 .C25 94.0 64.3-125 L716460-02 WG73B552 Chloroethane mg/1 0.0171 0.0 .025 68.0 51.5-136 L716460-02 WG738552 Chloroform rng/l 0.0207 0.0 .025 83.0 63-129 L716460-02 WG738552 Chloromethane mg/l 0.0152 0.0 .025 61.0 42.4-135 1,716460-02 WG738552 cis-1,3-Dichloropropene mg/l 0.0226 0.0 .C25 90.0 66.4-125 L716460-02 WG73B552 Dichlorodifluoromethane mg/1 0.0169 0.0 .025 68.0 40.6-144 L716460-02 WG738552 Fthylbenzene mg/l 0.D239 0.0 .025 95.0 61.4-133 L716460-02 WG738552 Methylene Chloride mg/1 0.0178 0.0 .025 71.0 58.1-122 L716460-02 WG138552 Tetrachloroetherie mg/l 0.0233 0.0 .025 93.0 53-139 L716460-02 WG738552 Toluene mg/l 0.0216 0.0 .025 B6.0 61.4-130 L716460-02 WG738552 trans-1,2-Dichloroethene mg/1 0.0179 0.0 .025 72.0 56.5-129 L716460-02 WG738552 trans-1,3-Dichloropropene mg/l 0.0260 0.0 .025 100. 64.1-128 1,726460-02 WG738552 Trichloroethene mg/1 0.0206 0.0 .025 82.0 44.1-149 L716460-02 WG738552 Trichlorofluoromethane mg/1 0.0202 0.0 .025 81.0 49.6-145 L716460-02 WG738552 Vinyl chloride mg/1 0.0162 0.0 .025 65.0 47.8-137 L716460-02 WG738552 4-Sromofluorobenzene 91.20 71-126 WG736552 Dibrcmofluoromethane 93,90 78.3-121 WG738552 Toluene -dB 99,20 88.5-111 WG738552 a,a,a-Trifluorotoluene 102.0 65-114 WG738552 Matrix Spike Duplicate Analyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch I,1,1-Trichloroethane mg/l 0.0206 0,0214 82.5 58.7-134 3.84 20 L716460-02 WG736552 1,1,2,2-TetrachloroeLhane mg/I 0.0271 0.0262 108. 56-132 3.24 22.2 L716460-02 WG73B552 ' Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes wzth QC Qualifiers.' Page 13 of 15 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5856 1-800-767-5859 OESC Fax (615) 758-5859 L-A•B 5-C•FE•N•C•E•5 Tax I.D. 62-0914285 ` Est. 1970 Eaton Corporation Katie Holbrook 2564 Durham Road duality Assurance Report Level II Roxboro, NC 27573 August 26, 2014 L716808 Analyte Units Matrix Spike MS❑ Ref Duplicate 4Rec Li in it RPD Limit Ref Samp Batch 1,1,2-Trichlorcethdne mg/1 0.0246 0,0242 98.2 66.3-125 1.62 20 L716460-02 WG738552 1,1-Dichloroethane mg/1 0.0196 0.0188 78.3 58.5-132 1.18 20 L716460-D2 WG738552 1,1-Dichloroethene mg/l 0.0163 0.0168 65.1 51.1-140 3.26 20.2 L716460-02 WG738552 1,2-Dich.lorobenzene mg/1 0,0239 0,0237 95.5 66.2-123 0.620 20 L716460-02 WG738552 1,2-Dichloroethane mg/I 0.0202 C.0198 80.E 60-126 2,09 20 L716460-02 WG73B552 1,2-Dichloropropane mg/1 0.0221 0.021E B8.3 64.2-123 1.46 20 L716450-02 WG738552 1,3-Dichlorobenzene mg/1 0.0224 0.0224 89.4 63.1-131 0.0700 20 1,716460-02 WG736552 1,4-Dich2orobenzene mg/1 0-0232 0.0234 92-7 68.6-123 0.930 20 L716460-02 WG738552 2-ChlorceChyl vinyl ether mg/1 0.0055E 0.0164 4.46, 10-155 107.' 20 L'116460-02 WG738552 AcroIei❑ mg/1 0.112 0.106 89.4 10-200 4.86 27.7 L716460-02 WG738552 Acrylonitrlle mg/I 0.126 0.120 101. 49.4-133 4.71 25.3 L716460-02 WG738552 Benzene mg/1 0.0204 0.0200 B1.6 34.3-133 1.94 20 L716460-02 WG738552 Bromodichlorcmethane mg/1 0-0229 0.0234 91.7 63.9-121 2.07 20 L716460-02 WG738552 Bromoform mg/1 C.0258 0.0253 103, 59.5-134 2.01 20.5 L716460-02 WG738552 Bromomethane mg/1 0.0177 0.0183 70.6 41.7-155 3.72 21.9 L716460-02 WGI3n552 Carbon tetrachloride mg/1 0.0208 0.0231 83.4 55.7-134 1.19 20 L716460-02 WG738552 Chlorobenzene mg/1 0.0244 0-0239 97,4 67-125 1.87 20 L716460-02 WG738552 Chlorodibromomethane mg/1 0.0235 0.0234 94.2 64.3-125 0.710 20.8 L716460-02 WG738552 C)ilorcethane mg/1 0.0160 0.0171 64.1 .91.5--136 6.34 40 L716460-02 WG738552 Chloroform mg/l 0.026E 0-0207 53.3 63-129 0.540 20 L716460-02 WG738552 Chloromethane mg/1 0.0149 0,0152 59.5 42.4-135 2,05 20 L716460-02 WG736552 cis-1,3-Dichloropropene mg/1 0.0229 0.0226 91.5 66.4-125 1.08 20 L716460-02 WG738552 Dichlorodifluoramethane ma/1 0.0160 0.0169 64.1 40.6-144 5.46 20.2 L716460-02 WG738552 ELhylbenzens uig/1 0.0240 0.0238 96.2 61.4-133 1.03 20 L716460-02 WG738552 Methylene Chloride mg/1 0.0176 0,0178 71.1 56.1-122 0.270 20 L716460-02 WG736552 Tetrachloroethene mg/1 0.0238 0.0233 95.3 53-139 2.04 20 L716460-02 WG738552 Toluene ma/1 0.0221 0.0216 88.3 61.4-130 2.04 20 L716460-02 WG738552 trans-1,2-Dichloroethene mg/1 0.0175 0.0179 70.3 56.5-129 2.05 20 L316460-02 WG738552 trans-1,3-Dichloropropene ma/1 0.0260 0.0260 104. 64.1-128 0.0400 20 L716460-02 WG738552 Tli ChloLoethene mg/l 0.0208 0-0206 83.3 44.1-349 1.31 2D L71646D-02 WG738552 Trichloroflucromethane mg/1 0.0193 0,0202 77.1 49-6-145 4.91 21.2 L716460-02 WG738552 Vinyl chloride mg/1 0.0155 0.0162 63.4 47.8-137 2.20 20 L716460-02 WG738552 4-Brc7icfIuorobenzene 90.00 71-126 WG738552 Dibromofluoromethane 90.70 76.3-121 WG73B552 Toluene-d8 98.60 88.5-111 WG738552 a, a, a-Trif1u0rot01uene 99.30 85-114 WG738552 Batch number /Run number / Sample number cross reference WG738219: R2978645: 1,716608-01 WG738332: R2978973: L716608-01 WG738552: R2179021: L716808-01 WG738528: R2979207; L716808-01 WG738310: R2980048 R2960776 R2980848: L116808-01 WG739395: R2981365: L716808-01 Calculations are performed prior to rounding of reported values. Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 14 of 15 OESCL•A•B 5•C•I•E•IV•C•E•S Eaton Corporation Katie Holbrook 2564 Dui..-h�jni Roau Roxboro, NC 27573 12065 Lebanon Rd. Mt. Juliet, Th 37122 1615) 756-5858 1-800-767-5859 Fax (615) 758-5859 Tar. I.D. 62-D814289 Est. 1970 nualily Assurance Report Level II AuquSL 26, 2014 L716808 The data package includes a summary of the analytic results or the quality control samples required by the SW-646 or CwA methods. The quality control samples include a method blank, a laboratory control sample, and the matrix spike/matrix spike duplicate analysis. If a target parameter is outside the method limits, every sample that is effected is flagged with the appropriate qualifier in Appendix 8 of the analytic report. Method Blank - an aliquot or reagent water carried through Che entire analytic process. The method blank results indicate it' any possible contamination exposure during the sample handling, digestion or extraction process, and analysis. Concentrations of target analytes above the repertiny limit in the method blaf7k are qualified with the "B" qualil'ief-. Laboratory Control Sample - is a samole of known concenLration that is carried through the digestion/extraction and analysis process. The percent recovery, expressed as a percentage of the theoretical concenLration, has statistical control limits indicating that the analytic process is "in control". If a target ana2yte is outside the control limits for the laboratory control sample or any other control sample, the parameter is flagged with a "014- qualifier for all effected samples. Matrix Spike and Matrix Spike Duplicate - is two aliquots of an environmental sample that is spiked with known concentrations of target analytes. The percent recovery of the target analytes also has statistical control limits. If any recoveries that are outside the method control limits, the sample that was selected rof matrix spi$e/matrix spiF:e duplicate analysis is flagged with either a "J3" or a "J6'•. The relative percent difference (%RPD) between the maLiix spike and the matrix spike duplicate recoveries is all calculated. If the RPD is above the method limit, the effected samples are flagged with a "J3" qualifier. Page 15 of 15 Semi-annual Stormwater D'Ischaae Monitorinir Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 7 21 14 CERTIFICATE OF COVERAGE NO. NCG030027 FACILITY NAME Eaton Corporation—Eneine Comoonents Division COUNTY Person PERSON COLLECTING SAMPLES Katie Holbrook LABORATORY_ ESC Lab Cert. #i ENV37VDW21724LB10041 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2014 _ SAMPLE PERIOD [] Jan -June ❑ July -Dec or ® Monthly'_ _ July _ _ „ (monthl DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA ❑Other WS-I11• NSW PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inche? Total Suspended Solids PH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ==-> - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L Tool Room Trench (005) 7/10/14 0,25 7.6 7.5 0.034 Not Detected 0.037 1.2 0.003 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For pu of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement s i e definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for c crystal manufa the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). OCT 10 2014 NC DENR RaWO R900r l Oi(ioe Permit Date: 11/1/2012-10/31/2017 SWO-245, last revised 10/25/2012 Page 1 of 3 racmoes Lnat incorporate a solvent management plan into the stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), i certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) 7L'/ (Signature) Kate) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, t ey must be_reported-in the format,_'<XX me/L". where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?? Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches) Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks == > _ -1 15 mg/L 100 mg/L or 50 mg/L' 6.0 — 910 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date; 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2of3 , .1..j ruu , cr,rur t u sumpre varue in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART Il SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. + TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one cagy of this DIVLR,_includinQal! "No_Dischardre"reports, within 30 dates of receipt of the lob results (or at end of moni_tnrina period in the case of Discharge" reuortsjto: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted_ Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 7 1 ,' (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 0 *ESC I Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Report Summary Monday July 21, 2014 Report Number: L709644 Samples Received: 07/11/14 Client Project: 12065 Lebanon Rd. Mt, Juliet, TN 37122 1615) 758 585E 1-800-767-5B59 Fan (615) 758-5859 Tax I.D. 62-CB14289 Est. 1970 Description: Eaton Corp Semi -Annual. Stormwater The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Entire Report Reviewed By: Ji Hunt , ESC Representative Laboratori, Certification Numbers A2LA - 1461-01, ATHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BT0041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN400032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 Accreditation is oniy applicable to the test methods specified on each scone of accreditation held by ESC Lab Sciences. This report may noL be reproduced, except in full, without written approval from ESC Lai) Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Paoe 1 of 15 Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NO 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS July 11, 2014 Eaton Corp Semi -Annual Stcrmwater TOOL ROOM TRENCH Katie Holbrook 07/10/14 12:30 12065 Lebanon Re. Mt. Juliet TN 37122 1615) 758-5658 1-800-767-5859 Fax (615) ?58-5859 Tax S.D. 62-0814289 Est. 1910 July 21, 2014 ESC Sample N L709644-01 Site ID ROXBORO, NO Project # Parameter Result MDL RDL Units Qualifier Method Date Dil. PH (On Site) 7.5 su Temperature (on -site) 27.8 Deg C Suspended Solids 7.6 0.35 2.5 mg/1 2540 D- 07/15/14 1 TPH - Oil & Grease 1.2 0.72 5.6 mg/l J 1664A 07/18/14 1 Copper 0.034 0.0053 0.020 mg/1 6010C 07/15/14 1 Lead U 0.0019 0.0050 mg/l 6010C 07/13/14 1 Zinc 0.037 0.0059 0.050 mg/l J 6010C 07/15/14 1 TTO volatile Organics Acrolein U 0.0089 0.050 mg/l 624 07/13/14 1 Acrylonitrile U 0.0019 0.010 mg/1 624 07/13/14 1 Benzene U 0.00033 0.0010 mg/l 624 07/13/14 1 Bromodichloromethane U 0.00038 0.0010 mg/l 624 07/13/24 1 Bromoform U 0,00047 0.0010 mg/l 624 07/23/14 1 Bromomethane U 0.00087 0.0050 mg/l 624 07/13/14 1 Carbon tetrachloride U 0.00038 0.0010 mg/l 624 07/13/14 1 Chlorobenzene U 0,00035 0.0010 mg/1 624 07/13/14 1 Chlorodibromomethane U 0.00033 0.0010 mg/1 624 07/13/14 1 Chloroethane U 0.00045 0.0050 mg/1 624 07/13/14 1 2-Chlorcethyl vinyl ether U 0,0030 0.050 mg/l 624 07/13/14 1 Chloroform U 0.00032 0.0050 mg/l 624 07/13/14 1 Chloromethane U 0.00028 0.0025 mg/l 624 07/13/14 1 1,2-Dichlorobenzene U 0.00035 0.0010 mg/l 624 07/13/14 1 1,3-Dichlorobenzene U 0,00022 0.0010 mg/1 624 07/13/14 1 1,4-Dichlorobenzene Ti 0.00023 0.0010 mg/l 624 07/13/14 1 Dichlorodiflucromethane U 0.00055 0.0050 mg/l 624 07/13/14 1 1,1-Dichloroethane U 0.00026 0.0010 mg/l 624 07/13/14 1 1,2-Dichloroethane U 0.00036 0.0010 mg/l 624 07/13/14 1 1,1-Dichloroethene U 0.00040 0.0010 mg/l 624 07/13/14 1 trans-1,2-Dichloroethene U 0.00040 0.0010 mg/l 624 07/13/14 1 1,2-Dichloropropane U 0.00031 0.0010 mg/1 624 07/13/14 1 cis-1,3-Dichloropropene U 0.00042 0.0010 mg/l 624 07/13/14 1 trans-1,3-Dichloropropene U 0.00042 0.0010 mg/1 624 07/13/14 1 Ethylbenzene U 0.00038 0.0010 mg/l 624 07/13/14 1 Methylene Chloride U 0.0010 0.0050 mg/l 624 07/13/14 1 1,1,2,2-Tetrachloroethane U 0.00058 0.0010 mg/l 624 07/13/14 1 Tetrachloroethene U 0.00037 0.0010 mg/1 624 07/13/14 1 Toluene U 0.00078 0.0050 mg/l 624 07/13/14 1 1,1,1-Trichloroethane U 0.00032 0.0010 mg/l 624 07/13/14 1 1,1,2-Trichloroethane U 0,00038 D.0010 mg/l 624 07/13/14 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/21/14 10:52 Printed: 07/21/14 10:53 Page 2 of 15 12065 Lebanon Rd. Mt. Juliet, TN 3712^- (615) 758-5858 1-800-767-5859 *ESC Fax (615) 75B-5859 l•A-8 5•C•I,E•N•C E•s Ta:_ I.D. 62-0814285 Est. 1970 REPORT OF ANALYSIS Katie Holbrook July 21, 2014 Eaton Corporation 2564 Durham Road Roxboro, NC 27573 ESC Sample # L709644-01 Date Received July 11, 2014 Description Eaton Corp Semi -Annual. Stormwater Site ID ROXBORO, NC Sample ID TOOL ROOM TRENCH Project # Collected By Katie Holbrook Collection Date 07/10/14 12:30 Parameter Result MDL RDL Units Qualifier Method Date Dil. Trichloroethene U 0.00040 0.0010 mg/1 624 07/13/14 1 Trichlorcfluoromethane U 0,0012 0.0050 mg/l 624 07/13/14 1 Vinyl chloride U 0.00026 0.0010 mg/1 624 07/13/14 1 Surrogate Recovery Toluene-d8 104, % Rec. 624 07/13/14 1 Dibromofluoromethane 109, % Rec. 624 07/13/14 1 a,a,a-Trifluorotoluene 97.4 % Rec. 624 07/13/14 1 4-Bromofluorobenzene 98.4 % Rec. 624 07/13/14 1 Pesticide/PCBs Aldrin U 0.0000081 0,000050 Trig/1 608 07/15/14 1 Alpha BHC U 0.000017 0.000050 mg/1 608 07/15/14 1 Beta HHC U 0,000018 0.000050 mg/l 608 07/15/14 1 Delta BHC U 0,000020 0.000050 mg/l 608 07/15/14 1 Gamma BHC U 0.000018 0.000050 mg/l 608 07/15/14 1 Chlordane U 0.000098 0,00050 mg/1 608 07/15/14 1 4,4-DDD U 0.000017 0.000050 mg/l 608 07/15/14 1 4,4-DDE U 0.000016 0.000050 mg/1 608 07/15/14 1 4,4-DDT U 0.000018 0.000050 mg/1 608 07/15/14 1 Dieldrin U 0.000018 0.000050 mg/1 L1 608 07/15/14 1 Endosulfan I U 0.000018 0.000050 mg/1 LI 608 07/15/14 1 Endosulfan II U 0,000018 0.000050 mg/1 60B 07/13/14 1 Endosulfan sulfate U 0.000020 0.000050 mg/1 608 07/15/I4 1 Endrin U 0.000019 0,000050 mg/1 L1 608 07/15/14 1 Endrin aldehyde U 0.000014 0.000050 mg/l 608 07/15/14 1 Endrin ketone U 0.000017 0.000050 mg/l 608 07/15/14 1 Heptachlor U 0.000011 0.000050 mg/1 608 07/15/14 1 Heptachlor epoxide U 0.000018 0.000050 mg/l Ll 606 07/15/14 1 Hexachlorobenzene U 0.000013 0.000050 mg/l 608 07/15/14 1 Methoxychlor U 0.000019 0.000050 mg/1 L1 608 07/15/14 1 Toxaphene U 0,00017 0.00050 mg/1 608 07/15/14 1 PCs 1016 U 0.000020 0,00050 mg/1 608 07/15/14 1 PCB 1221 U 0.000024 0.00050 mg/l 608 07/15/14 1 PCB 1232 U 0.000021 0,00050 mg/1 608 07/15/14 1 PCB 1242 U 0.000024 0.00050 mg/l 608 07/15/14 1 PCB 1248 U 0,000014 0.00050 mg/1 608 07/15/14 1 PCB 1254 U 0.000018 0.00050 mg/l 608 07/15/14 1 PCB 1260 U 0.000015 0,00050 mg/1 608 07/15/14 1 Pest/PCBs Surrogates Decachlorobiphenyl 73.0 % Rec. 608 07/15/14 1 Tetrachloro-m-xylene 79.6 % Rec. 608 07/15/14 1 TTO Base/Neutral Extractables U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/21/14 10:52 Printed: 07/21/14 10:53 Page 3 of 15 12065 Lebanon Rd, Mt. Juliet, TH 37122 JOESC (615) 756-5858 1-800-767-5859 Fay: (615) 756-5859 L-A 9 S•C•I•E•N C•E-S Tax T.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Katie Holbrook July 21, 2014 Eaton Corporation 2564 Durham Road Roxboro, NC 27573 ESC Sample 4 L709644-01 Date Received July 11, 2014 Description Eaton Corp Semi -Annual Stormwater Site ID ROXBORO, NC Sample ID TOOL ROOM TRENCH Project . Collected By Katie Holbrook Collection Date 07/10/14 12:30 Parameter Result MDL RDL Units Qualifier Method Date Dil. Acenaphthene U 0.00032 0.0010 mg/1 625 07/15/14 1 Acenaphthylene U 0.00031 0.0010 mg/1 625 07/15/14 1 Anthracene U 0.00029 0.0010 mg/l 625 07/15/14 1 Benzidine U 0.0043 0.010 mg/l 625 07/15/14 1 Benzo(a)anthracene U 0.00032 0.0010 mg/l 625 07/15/14 1 Benzo{b)fluoranthene U 0.00027 0,0010 mg/1 625 07/15/14 1 Benzo(k)f2uoranthene U 0.00036 0.0010 mg/1 625 07/15/14 1 Benzo(g,h,i)perylene U 0.00033 0.0010 mg/l 625 07/25/14 1 Benzo(a)pyrene U U.o0034 0.0010 mg/l 625 07/15/24 1 Bis(2-chlorethoxy)methane U 0.00033 0.010 mg/l 625 07/15/14 1 Bis(2-chlorcethyl)ether U 0.0016 0,010 mg/1 625 07/15/14 1 Bis(2-chloroisopropyl)ether U 0,00044 0,010 mg/1 625 07/15/14 1 4-Bromophenyl-phenylether U 0.00034 0.010 mg/1 625 07/15/14 1 2-Chloronaphthalene U 0.00033 0.0010 mg/1 625 07/15/14 1 4-Chlorophenyl-phenylether U 0.00030 0.010 mg/l 625 07/15/14 1 Chrysene U 0.00033 0.0010 mg/1 625 07/15/14 1 Dibenz(a,h)anthracene U 0.00028 0.0010 mg/l 625 07/15/14 1 3,3-Dichlorobenzidine U 0.0020 0.010 mg/l 625 07/15/14 1 2,4-Dinitrotoluene U 0.0016 0.010 mg/1 625 07/15/14 1 2,6-Dinitrotoluene U 0.00028 0.010 mg/l 625 07/13/14 1 1,2-Diphenylhydraxine U 0.00016 0,010 mg/l 625 07/15/14 1 Fluoranthene U 0,00031 0.0010 mg/l 625 07/15/14 1 Fluorene U 0.00032 0.0010 mg/1 625 07/15/14 1 Hexachlorobenzene U 0.00034 0.0010 mg/l 625 07/15/14 1 Hexachloro-1,3-butadiene U 0.00033 0.010 mg/l 625 07/15/14 1 Hexachlorocyclopentadiene U 0.0023 0.010 mg/1 625 07/15/14 1 Hexachloroethane U 0.00037 0.010 mg/l 625 07/15/14 1 Indeno(1,2,3-cd)pyrene U 0.00028 0.0010 mg/l 625 07/15/14 1 Isophorone U 0.00027 0.010 mg/l 625 07/15/14 1 Naphthalene U 0,00037 0.0010 mg/l 625 07/15/14 1 Nitrobenzene U 0.00037 0.010 mg/1 625 07/13/14 1 n-Nitrosodimethylamine U 0.0013 0.010 mg/l 625 07/15/14 1 n-Nitrosodiphenylamine U 0.00030 0.010 mg/l 625 07/15/14 1 n-Nitrosodi-n-propylamine U 0.00040 0.010 mg/l 625 07/15/14 1 Phenanthrene U 0.00037 0.0010 mg/1 625 07/15/14 1 Henzylbutyl phthalate U 0.00028 0.0030 mg/l 625 07/15/14 1 Bis(2-ethy1hexyl)phthalate 0.00091 G.00071 0.0030 mg/l J 625 07/15/14 1 Di-n-butyl phthalate 0.00070 0.00027 0.0030 mg/1 J 625 07/15/14 1 Diethyl phthalate 0.00044 0.00028 0.0030 mg/1 J 625 07/15/14 1 Dimethyl phthalate 0.00048 0.00028 0.0030 mg/1 J 625 07/15/14 1 Di-n-octyl phthalate U 0.00028 0.0030 mg/l 625 07/15/24 1 Pyrene U 0.00033 0.0010 mg/l 625 07/15/14 1 1,2,4-Trichlorobenzene U 0.00036 0.010 mg/1 625 07/15/14 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = SQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/21/14 10:52 Printed: 07/21/14 10:53 Page 4 of 15 REPORT OF ANALYSIS Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received July 11, 2014 Description Eaton Corp Semi -Annual Stormwater Sample ID TOOL ROOM TRENCH Collected By Katie Holbrook Collection Date 07/10/14 12:30 12065 Lebanon Rd. Mt. Juliet, TH 37122 (615) 758-5858 1-600-767-5859 Fax (615) 753-5859 Tax I.D. 62-Q814289 Est. 1970 July 21, 2014 ESC Sample 4 : 1,709644-01 Site ID ROXBORO, NC Project Parameter Result MDL RDL Units Qualifier Method Date Dil. TTO Acid Extractables 4-Chlorc-3-methylphenol U 0.00026 0.010 mg/l 625 07/15/14 1 2-Chloxophenol U 0.00028 0.010 mg/l 625 07/15/14 1 2,4-Dichlorophenol Ti 0.0002B 0.010 mg/1 625 07/15/14 1 2,4-Dimethylphenol U 0.00062 0.010 mg/1 625 07/15/14 1 4,6-Dinitro-2-methylphenol U 0,0026 0,010 mg/1 625 07/15/14 1 2,4-Dinitrophenol U 0.0032 0.010 mg/1 625 07/15/14 1 2-Nitrophenol U 0.00032 0,010 mg/l 625 07/15/14 1 4-Nitrophenol U 0.0020 0.010 mg/1 625 07/15/14 1 Pentachlorophenol U 0.00031 0.010 mg/l 625 07/15/14 1 Phenol U 0.00033 0.010 mg/1 625 07/15/14 1 2,4,6-Trichlorophenol U 0.00030 0.010 mg/1 625 07/15/14 1 Surrogate Recovery 2-Fluorophenol 37.8 % Rec. 625 07/15/14 1 Phenol-d5 23.5 % Rec. 625 07/15/14 1 Nitrobenzene-d5 55.6 % Rec. 625 07/15/14 1 2-Fluorobiphenyl 76.8 % Rec. 625 07/15/14 1 2,4,6-Tribromophenol 72.9 % Rec. 625 07/15/14 1 p-Terphenyl-d14 85.7 % Rec. 625 07/15/14 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/21/14 10:52 Printed: 07/21/14 10:53 Page 5 of 15 Attachment A List of Analytes with QC Qualifiers Sample work Sample Run Number Group Type Analyte ID Qualifier L709644-01 WG731497 SAMP Dieldrin R2962145 L1 WG731497 SAMP Endosulfan I R2962145 L1 WG731497 SAMP Endrin R2962145 L1 WG731497 SAMP Heptachlor epoxide R2962145 L1 WG731497 SAMP Methoxychlor R2962145 L1 WG731499 SAMP Bis(2-ethylhexy1)phthalate R2962252 i WG731499 SAMP Di-n-butyl phthalate R2962252 J WG731499 SAMP Diethyl phthalate R2962252 i WG731499 SAMP Dimethyl phthalate R2962252 i wG732206 SAMP TPH - oil & Grease R2964692 J wG731528 SAMP Zinc R2962153 J Page 6 of 15 Attachment B Explanation of QC Qualifier Codes Qualifier Meaning (EPA) - Estimated value below the lowest calibration point. Confidence correlates with concentration. L1 (ESC) The associated batch LCS exceeded the upper control limit, which indicates a high bias; The sample analyte was "not detected" and is therefore unaffected. Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fail outside of established ranges. These exceptions are evaluated and all reported data is valid and useable "unless qualified as 'R' (Rejected)." Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. Page 7 of 15 Summary of Remarks For Samples Printed C7/21/14 at 10:53:31 TSR Signing Reports: 350 R5 - Desired TAT MDL/RDL; PO = 79918 Sample: L709644-Cl Account: EATONRNC Received: 07/11/14 09:00 Due Date: 07/18/14 00:00 RPT Date: 07/21/14 10:52 12065 Lebanon Rd. Mt. Juliet, TN 37122 1 615 1 758-5858 1-800-767-5859 E S C Fay: (615) 758-5859 L•A•B S•C•E•E•N-C•E•S Tare 1,D. 62-0834299 Est. 1970 Eaton Corporation Katie Hclbrook 2564 Durham Road nuality Assurance Reoort Level I1 Roxboro, NC 27513 July 21, 2014 I,709644 Laboratory Blank Analyte ReSUIL Units $ Rec Limit Batch Date Analyzed 1,1,l-Trichlorcethane < .CC] mg/1 WG731467 07/13/14 06:11 1,1,2,2-Tetrachloroeth6ne < .001 mg/1 WG731467 01/13/14 06:11 1,1,2-Tricliloroethane < .001 mg/1 WG731467 07/13/14 06:11 1,1-Dichloroethane < .001 mg/l WG731467 07/13/14 06:11 1,1-❑ichloioethene < .Dol mg/l WG731467 D7/13/14 06:11 1,2-Dichlorobenzene < .col mg/I wG731467 07/13/14 06:11 1,2-Dichloroethane < .001 ma/l WG731467 07/13/14 06:11 1,2-Dichloropropane < .001 me/1 WG731467 07/13/14 06:11 1,3-Dichlorobenzene < .001 me/l WG731467 07/13/14 06:11 1,4-Dichlorobenzene < .001 mg/1 WG731467 07/13/14 06:11 2-Chlor'oethyl vinyl ether < .05 mg/1 WG131467 07/13/i4 06:11 Acrolein < .025 mg/l WG731467 07/13/14 06:11 Acrylonitriie < .01 ma/l WG731467 07/13/14 06:11 Benzene < .001 mg/1 WG731467 07/13/14 06:11 Bromodichloromethane < .001 ma/l WG731467 07/13/14 06:11 Bromoform < .001 mg/l WG731467 07/I3/14 D6:11 Bromomethane < .005 mg/1 WG731467 07/13/14 06:11 Carbon tetrachloride < .001 mg/1 WG1314G7 07/13/14 06:11 Chlorobenzene < .001 mg/l WG731467 07/13/14 06:11 Chlorcdibromamethane < .001 mg/I WG731467 07/13/14 06:11 ChloroeLhane < .005 ma/1 WG731467 07/13/14 06:11 Chloroform < .005 mg/l WG731467 07/13/14 06:11 Chloromethane < .0025 mo/1 WG731467 07/13/14 06:11 cis-1,3-Dichloropropene < .001 1110/1 WC731467 07/13/14 06:11 Dichiorodifluoromethane < .005 mg/I WG731461 07/13/I4 06:11 Ethylbenzene < .001 mg/1 WG731467 07/13/14 06:11 Methylene Chloride < .005 mg/1 WG731467 07/13/14 DG:11 Tetrachloroethane < .001 mg/1 WG731467 07/13/14 06:11 Toluene < .005 mg/l WG732467 07/13/14 06:11 trans-1,2-Dichloroethene < .001 mg/1 WG731467 C7/13/14 06:11 trans-1,3-Dichloropropene < .001 mg/1 WG731467 07/13/14 D6:11 Trichloroethene < .001 mg/l WG731467 07/13/14 06:11 Trichloro£luoromethane < .005 mg/1 WG731467 07/13/14 06:11 vinyl chloride < .001 mg/I WG731467 07/13/14 06:11 4-Bromofluorobenzene % Rec. 97.10 71-126 WG731467 07/13/14 06:11 Dibromofluorometliane % Rec. 207.0 78.3-121 WG731467 07/13/14 06:11 Toluene-d8 % Rec. 203.0 88.5-111 WG731467 07/13/14 06:ll a,a,a-Trifluorotoluene $ Rec. 99.00 85-114 KG731467 07/13/14 06:11 Suspended Solids < 2.5 mg/l WG731508 07/15/14 12:53 4,4-DUD < .00005 Trig/l WG731497 07/15/14 10:12 4,4-DUE < .00005 mg/1 WG721497 07/15/14 10:12 4,4-DDT < .00005 mg/l WG731497 07/15/14 10:12 Aldrin < .00005 mg/1 WG731497 07/15/14 10:12 Alpha BHC < .00005 mg/l WG731497 07/15/14 10:12 Beta BHC . .D0005 mg/l WG731497 07/15/14 10:12 Chlordane < .005 mg/1 WG731497 07/15/14 10:12 Delta BHC < .H005 mo/1 WG731497 07/15/14 10:12 Die,Idiin < .00005 mg/] WG731497 07/15/14 10:12 Endosulfan I < .00005 mg/l WG731497 01/15/14 10:12 Endosulfan II < .00005 mg/1 WG731497 07/15/14 10:12 Endosulfan sulfate < .00005 ma/l WG731497 07/15/14 10:12 Endrin < .00005 mg/1 WG731497 07/15/14 10:12 Endrin aldehyde < .00005 rng/l WG731497 07/15/14 10:14- Endrin ketone < .00005 mg/1 WG731497 07/15/14 10:72 Gamma BHC < .00D05 mg/1 WG731497 07/15/14 10i12 Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 8 of 15 12065 Lebanon Rd. MC. 7ulie[, TN 37122 (615} 758-s85a i-B00-767-5859 OESC Fax (615) 75e-5859 L•A•B 5•C•r•E•N•C-E•5 Tar: I.D. 62-0814289 Est. 1970 Eaton Corporation Katie Holbrook 2564 Durham Road OualiLy Assurance Report Level II Roxboro, NC 27573 July 21, 2011 L709644 Laboratory Blank Analyte Result Units % Rec Limit batch Date Analyzed Heptachlor < .00005 mg/l WG737497 07/15/14 10:12 Heptachlor epoxide < .00005 mg/1 WGI31497 07/15/14 10:12 Herachlorobenzene < .00005 mg/1 WG731497 07/15/14 ]0:12 Methoxychlor < .00005 ma/1 WG731497 07/15/14 10:12 Toxaphene < .0005 nig/1 WG731497 01/15/14 10:12 Decachlorobiphenyl % Rec. 96.60 10-156 IRG731497 07/15/14 10:12 Teti achlora-m--xylene % Rec. 89.50 13.9-137 WG731494 07/15/14 20:12 Leaci < .005 mg/1 WG731528 07/15/14 08:54 Zinc < .05 mg/1 WG731528 07/15/14 08:54 1,2,4-Tr.ichlorcbenzene < .01 mg/1 WG731499 07/15/14 00:55 2,4,5-Trichloraphenol < .01 mg/1 WG731499 07/15/14 00:55 2,4-Dichloraphenol < .01 mg/1 WG731499 07/15/14 00:55 2,4-Dimethylphenol < .01 mg/1 WG731499 07/15/14 00:55 2,4-Dinitrophenol < .01 mg/1 WG731499 07/15/14 00:55 2,4-DiniLrOLOluene < .01 mg/1 WG731499 07/15/14 00:55 2,6-Dinitrotoluene < Al mg/l WG731499 07/15/14 00:55 2-Chloronaphthalene < .001 mg/l WG731499 07/15/14 00:55 2-Chloropheriol < .01 11[0/1 WG731499 07/15/14 00:55 2-Nitrophenol < .01 mg/l WG731499 07/15/14 00:55 3,3-Dichlorobenzidine < .01 mg/l WG731499 07/15/14 00:55 4,6-Dinitro-2-methylphenol < .01 mg/1 WG731499 07/15/14 00:55 4-Bromoplienyl-phenylether < .01 mg/1 WG731499 07/15/14 00:55 4-Chloro-3-methylphenol < .01 mg/1 WG731499 07/15/14 00:55 4-Chlorophenyl-phenylether < .01 mg/l WG731499 07/13/14 00:55 4-Nitrophenol < .01 1110/1 WG731499 07/15/14 00:55 AcenaphLhene < .001 mg/I WG731499 07/15/14 00:55 Acenaphthylene < .001 mg/1 wG731499 07/15/14 00:55 Anthracene .001 tug/l WG731459 07/15/14 00:55 1,2-Diphenylhydrazine < .01 mg/1 WG731499 07/15/14 00:55 Benzidine < .01 ma/1 WG731499 07/15/14 00:55 Benzo(a)anthracene < .001 mg/1 WG731499 07/15/14 00:55 Benzofa)pyrene < .001 mg/1 WG731499 07/15/14 00:55 Benzo(blfluoranthene < .001 mg/l WG731499 07/15/14 00:55 Benzo(g,h,i)perylene < .001 mg/1 WG731499 07/15/14 00:55 Benzo(k)fluoranthene < .001 mg/l WG731499 07/15/14 00:55 Benzylbutyl phthalate < .003 mg/l WG731499 07/15/14 00:55 Bis(2-ch1erethoxy)methane < .01 mg/1 WG731499 07/25/14 00:55 Bis(2-chlorcethyl)ether < .01 mg/1 WG731499 07/15/14 00:55 Bis(2-chloroisopropyl)ether < .01 ma/l WG731499 07/15/14 00:55 Ris(2-ethylhexyl)phthaIate < .003 mg/1 WG731499 07/15/14 00:55 Chrysene < .001 mg/1 WG731499 07/15/14 00:55 Di-n-butyl phthalate _ .003 mg/1 WG731499 07/15/14 00:55 Di-n-octyl phthalate < .003 rng/l WG721499 07/15/14 00:55 Dibenz(a,h)anthracene < .001 mg/1 WG731499 07/15/14 00:55 Diethyl phthalate < .003 mg/l WG731499 07/15/14 00:55 Dimethyl phthalate < .003 mg/l WG731499 07/15/14 00:55 Fluoranthene < .001 mg/1 WG73149D 07/15/14 00:55 Fluorene < .001 rng/l WG731499 07/15/14 00:55 Hexachloro-1,3-butadiene < .01 mg/l WG731499 07/15/14 00:55 Hexachlorobenzene < .001 mg/1 WG731499 07/15/14 00:55 Hexachlorocyclopentadiene < .01 nig/l WG731499 07/15/14 00:55 Ilexachloroethane < .01 mg/l WG731499 07/25/14 00:55 Indeno{1,2,3-cd)pyrene < .001 mg/l WG731499 07/15/14 00:55 Isophorone < .01 mg/l WG731499 07/15/14 00:55 n-Nitrosodi-n-propylamine < .01 mg/1 WG731499 07/15/14 00:55 Performance of this Analyte is outside of esLablis},ed criteria. For additional irntormation, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 9 of 15 JOESC L• A• 6 5- C• I• E- N, C- E, S Eaton Corporation Katie Holbrook 2561 Durham Road Roxboro, 14C :7573 Q.uality Assurance Report Level TI L709644 12065 Lebanon Rd. Mt. Juliet, TN 37122 1615) 756-5858 1-800-767-5859 Fax {615) 758-5859 Tax I.D. 62-08142B9 Est. 1910 July 21, 2014 Analyte Resu1L Laboratory Units Blank % Rec Limit Batch Date Analyzed n-Nitrosodimethylamine < .01 mg/l WG731499 07/15/14 00:55 n-Nitrosodiphenylarnine < .01 me/1 wG731499 07/15/14 0 0 : 5 3 Naphthalene < .001 mg/1 WG731499 07/15/14 0c:55 Nitrobenzene < .01 mg/1 WG731499 07/15/14 00:55 Pentaclilorophenol < .001 mg/1 WG731499 07/15/14 00:55 Phenanthrene < .001 1110/1 WG731499 07/15/14 00:55 Phenol - .01 ma/l WG731499 07/15/14 00:55 Pyrene < .001 mg/1 WG731499 07/15/14 00:55 2,4,6-TribtomophenoI 6 Rec. 92.70 11.2-130 WG731499 07/15/14 OD:55 2-Fluorobiphenyl % Rec. 100.0 29.5-131 WG731499 07/15/14 00:55 2-Fluorophenol % Rec. 53.90 10-77.9 WG731499 07/15/14 00:55 Nitrobenzene-d5 W Rec. 67.40 21,8-123 WG731499 07/15/24 00:55 Phenol-d5 8 Rec, 36.40 5-70.1 WG731499 07/15/24 00:55 p-Terphenyl-d14 % Rec. 89.60 29.3-137 WG731499 07/15/14 00:55 PCB 1016 < .0005 mg/1 WG731497 07/15/14 13:02 PCB 1221 < .ODD5 mg/1 WG731497 07/15/14 13:02 PCB 1232 < .0005 mg/1 WG731497 07/15/14 13:02 PCB 1242 < .00D5 mg/l WG731497 07/15/14 13:02 PCB 1248 < .000G mg/1 WG731497 07/15/14 13:02 PCS 1254 < .0005 rna/1 WG731497 07/15/14 13:02 PCB 1260 < .0005 mg/1 WG731497 07/15/14 13:02 Decachlorobiphenyl i Rec. 61.20 10-156 WG731497 07/15/14 13:02 Tetrachloro-m-xylene 8 Rec. 75.10 13.9-137 WG7.1497 07/15/14 13.02 TPH - Oil & Grease < 5 mg/l WG732206 07/18/14 13:42 Copper < .02 mg/1 WG731528 07/15/14 05:13 Duplicate Analyte Units Result Duplicate RPD Limit Ref Samp Batch Suspended Solids mg/1 197. 214. 8.46' 5 L709507-01 WG731508 Laboratory Control Sample Analyte Units Known Val Result 8 Rec Limit Batch 1,1,1-Trichloroethane mg/1 .025 0.0257 103. 73.2-)23 WG731467 1,1,2,2-TetrachloroeLhane mg/l .025 0.0255 102. 70.7-122 WG731467 1, 1, 2-Trichloroethane mg/1 .025 0.0232 92.6 77.7-118 WG731467 I,]-Dichloroethane mg/l .025 0.0247 95.6 70.7-126 wG731467 1,1-❑ichloroethene mg/l .025 0,0251 100. 67.6-129 WG731467 1,2-DichIcrobenzene mg/1 .025 0.0254 102. 78.4-227 WG731467 1,2-Dichloroethane mg/1 .025 0.0296 118. 68.8-124 WG731467 1,2-Dichloropropane mg/1 .025 0,0263 105. 76.5-119 WG731467 1,3-Dichlorchenzene mg/1 025 0.0256 103. 70.8-126 WG731467 2,4-Dichlorobenzene mg/l .025 0.0247 99.7 78.8-115 WG731467 2--Chloroethyl vinyl ether. mg/1 .125 0.134 108. 43.B-150 wG731467 Acrolein mg/1 .125 0.117 93.4 10-190 WG731467 Acrylonitrile mg/1 .125 0.223 98.6 55.2-130 WG731467 Benzene [rig /1 .025 0.0269 106. 74.9-121 WG731467 Bromodichlorometharle mg/1 .025 0.0271 108. 75.1-116 WG731467 Bromoform mg/l .025 0.0232 92.7 67.5-130 WG731467 BrOMOITIethaile mq/l .025 0.0264 306. 49.9-162 WG73I467 Carbon tetrachloride mg/1 .025 0.0260 104. 70.2-123 WG731467 Chlorobenzene mg/1 .025 0.0254 102. 76.1-119 WG731467 Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with OC Qualifiers.' Page 10 of 15 12065 Lebanon Rd. - Mt. Juliet, TH 37122 (615) 758-5858 1-800-767-5859 OESC Fax (615) 758-5859 L•A 0 S•C•I•E•N•C•E•S Tao I.D. 62-0814259 Est. 1970 Eaton COroorati077 Katie Holbrook 2564 Durham Road Quality Assurance Report Level II Roxboro, NC 27573 July 21, 2014 T.709644 Laboratory Control Sample Analyte Units Known Val Result 8 Rec Limit Batch Chlorodibromomethane mg/1 .025 0.0257 103. 74-121 WG731467 Ctiloroethane mg/1 .025 0.0289 f15. 61.7-135 WG731467 Chloroform mg/1 .025 0.0257 103. 76-121 WG131467 Chloromethane mg/l .025 0.0221 88.3 61.5-129 WG731467 cis-1,3-Dichloronropene me/1 .025 0,0267 107. 78.2-120 WG731467 Dichlorodifluoromethane mg/L .025 0.0222 89.0 54.8-135 WG731467 Ethylbenzene rng/l .025 0.0253 101. 78.8-122 WG731467 Methylene Chloride mg/1 .025 0.0230 92.1 70.3-120 WC,731467 TeLrachloroethene mg/1 .025 0.0240 96.1 72.6-126 WG731467 Toluene mg/l .025 C_0267 107• 79.7-116 WG731467 trans-1,2-DichlcrOethene mg/l .025 C.0226 90.3 72.6-121 WG731467 trans-1,3-Dichloropropene mg/1 .025 0.0260 104. 74.3-123 WG731461 Trichlorcethene mg/1 .025 0,0265 196. 77.7-118 WG731467 Trichloroflucromethane mg/1 .025 0.0238 95.0 63.5-135 WG731467 Vinyl chloride mg/1 .025 0.0217 86.8 65.9-128 WG751467 4-Bromofluorobe n_ene 98.30 71-126 WG731467 Dibromofluoromethane 98.40 78.3-121 WG731467 Toluene-d8 109.0 88.5-111 WG731467 a, a, a-TrifluorotcIuene 101.0 85-114 WG731467 Suspended Solids mg/l 773 758. 102. 85-115 WG731508 4,4-DDD mg/1 .0002 0.000270 135, 47,6-144 WG731497 4,4-DDE mg/1 .ECO2 0.000216 119. 45-124 WG732497 4,4-DDT mg/1 .0002 0.000260 130. 49.8-130 WG732497 Aldrin mg/1 .0002 0.0000631 31.5 10-120 WG731497 Alpha BHC mg/l .0002 C.0002I0 105, 53.6-125 WG731497 Beta BAC mg/l .0002 0.000248 124. 35.8-130 WG731497 Delta BHC mg/1 .0002 0.000235 117. 42.2-135 WG731497 Dieldrin mg/1 .0002 0,000261 130.• 55-127 WG731491 Endosulfan I mg/1 .0002 0.000265 132.' 54.7-127 WG732497 Endosulfan 11 mg/l .0002 0.000262 1-,1. 53.1-135 WG731497 Endosulfan sulfate mg/l PD02 0.000265 1-.2. 51.5-132 WG731497 Endrin mg/1 .0002 0.000264 132.' 50.1-131 WG731497 Endrin aldehyde mg/l .0002 0,000256 128. 39.5-137 WG731497 Endrin ketone mg/1 .0002 0/000265 132. 53.5-139 WG73:497 Gamma BHC mg/1 .0002 0.000217 109. 54.7-125 WG731497 Heptachlor mg/1 .0002 0.000115 57.5 20.7-127 WG731497 Heptachlor epoxide mg/1 .0002 0.000250 125.- 56.4-124 WG73I497 Hexachlorobenzene mg/1 .0002 0.0000884 44.2 26.7-114 WG731497 Methoxychlor mg/1 .0002 0.000290 145.' 49.2-144 W0731497 Decachlorobiphenyl 102.0 10-156 WG731497 TetrachlOro-m-xylene 88.10 13.9-137 WG731497 Lead pia/1 1 1.04 104. 85-115 WG731528 Zinc ma/1 1 1.05 105. 85-115 WG731526 1,2,4-Trichlorobenzene mg/1 .025 0.0175 70.1 22.5-96.1 WG73149D 2,4,6-Trichlorophenol mn/l .025 0.0227 90.8 29.5-107 WG731499 2,4-DiChlarop}ienol mg/1 .025 0.0199 79.5 31.4-103 WG731495 2,4-DimeLhyIphenoI mg/1 .025 0.020C 60.1 31.9-101 UG331499 2,4-Dinitropheno2 mg/1 .025 0.0115 46.2 24.2-128 WG731499 2,4-Dinitrotoluene mg/1 .325 0.0213 85.2 31.2-105 WG731499 2,6-Dinitrotoluene mg/l C25 0.0228 91.0 30.6-106 WG731499 2-Chloronaphthalene mg/1 .025 0.0225 50.1 33.6-105 WG731499 Performance of this Analyte is outside of estahlis}jed criteria. For additional information, please see Attachment A 'List of Ana Iytes wi tli QC Qua if ier s.' Pane 11 of 15 12065 Lebanon Rd. Mt. Jvliet, TN 37122 (615) 758-5856 1-800--76'7-5859 OESC Fax (615} 758-5859 L•A B 5• C• I• E• N• C• E•5 Tax I.R. 62-0814289 Est. 1970 Eaton Corporation 5atie Holbroo): 2564 Durham Road Quality Assurance Reocrt Level Il Roxboro, NC 27573 Ji:ly 21, 2014 I,709644 Laboratory Control Sample Analyte Units Known Val Result Red Limit Batch 2-Chloroplienol mg/1 .025 0.0176 70.4 26.2-91.5 WG731499 2-Nitranhell o] mg/1 .025 ❑.0217 86.9 25.9-106 WG731499 3,3-Dichloroben idine mg/1 .025 0.0231 92.4 27.2-142 WG731499 4,6-Dinitro-2-methylphenol mg/1 .025 0.0214 85.5 18.4-148 WG731499 4-13rcmophenyl-atienylether mg/l .025 0.0734 93.7 40.7-116 WG731499 4-ChIoro-3-me thylphenol pig/l .025 0.0175 70.0 35.7-1D0 WG731499 4-Chlorophenyl-phenylether mg/1 .025 0.0226 90.4 39-113 WG731499 4-Nitrophenol mg/1 .025 0.00707 28.3 10-52.7 WG731499 Acenaphthene mg/1 .025 0.0211 84.3 39.7-109 WG731499 Acenaphthylene mg/1 .C25 0,0207 82.9 36-206 WG731499 Anthracene mg/1 C25 0.0214 85.6 43.6-113 WG731499 1,2-DiphenyIhydrazine mg/1 .025 0.0267 107. 37.6-111 WG731499 Penzidine mg/i .025 0.0164 73.5 10-165.2 WG731499 Benzo(a)anthracene rag .025 0.0218 87.0 52.2-112 WG732499 Benzo(alpyrene mg/1 .025 0.0195 71.9 45.6-106 SVG731495 Benzo(b)fluoranthene mg/1 .025 0.0219 87.6 47.6-111 WG731499 Benzc(g,h,i)perylene mg/1 .025 0.0230 92.0 45.2-117 WG731499 Benzo(k)fIuoranthen e mg/1 .025 0.0206 63.2 49.4-114 WG731499 Benzylbutyl phthalate mg/1 .025 0.0194 77.6 31.9-123 WG731499 Bis(2-chlorethoxy)methane mg/1 .025 0.0168 67.2 27.2-111 WG731499 Bis(2-chlorcethy1)ethe r mg/l .025 0.0156 63.1 22.6-108 WG731499 Bis(2-Chloroisoprcpyl)ether mg/1 .025 0.0178 71.3 32.9-100 WG731499 Bis(2-ethylhexy1)phthaIate mg/l .025 0.0197 78.7 36.9-134 WG731499 Chrysene mg/1 .025 0,0207 82.6 54.6-170 WG733499 Di-n-butyl phthalate mg/1 .025 0,0202 B1.0 41.B-120 WG731499 Di-n-octyl phthalate mg/1 .025 0.0204 81.5 39.7-112 WG732499 Dibenz(a,h)anthracene mg/1 .025 0.0246 98.6 42.8-118 WG731499 Diethyl phthalate mg/1 .025 0.0220 87.9 36.5-129 WG721499 Dimethyl phthalate mg/l D25 0.0235 93.B 35.3-120 WG731499 F'luoranthene mg/1 .025 0,0211 B4.5 45.9-125 WG731499 Fluorene mg/I .025 0,0214 85.4 41-112 WG731499 Hexachlcro-1,3-butadiene mg/l .025 0.0172 68.6 16.1-104 WG731199 Hexachlerebenzene mg/1 .025 0.0214 85.5 39.5-116 WG731499 Hexachlorocyclopentadiene mg/l D25 0.0133 53.3 10-121 WG731499 Hexachloroethane mg/i .025 0.0155 62.2 16.5-89.9 WG731499 Indeno(1,2,3-c(I)pyrene mg/1 .025 0.0241 96.3 45-116 WG731499 Isophorone mg/1 .025 0.0209 83.8 35.4-112 WG731499 n-Nitrosodi-n-propylamine ma/1 .025 0.0183 73.4 33.2-106 WG731499 n-Nitrosodimethylamine mg/l .025 0.0101 40.6 10-80.1 WG731499 n-Nitrosodiphenylamine mg/1 .025 0.0242 96.6 44.4-113 WG731499 Naphthalene mg/1 .025 0.0164 73.5 32.2-101 WG731499 Nitrobenzene mg/1 .025 0.0213 65.1 31.4-106 wG731499 Pentachlorophenol mg/1 .025 0.0154 61.6 10-97.4 WG731499 Phenanthrene ma/I .025 0.0206 82.4 46.4-113 WG721499 Phenol m0/1 .025 0.00887 35.5 10-57.9 WG731499 Pyrene mg/1 .025 0.0220 87.9 46.3-117 WG731499 2,4,6-Tribrcmophencl 87.90 11.2-130 WG731499 2-Fluorobiuhenyl 94.B0 29.5-131 wG731499 2-Fluorophenol 46.00 10-77.9 VJG731499 Nitrobenzene-d5 76.40 21.8-123 WG731499 Phenol-d5 3:'.70 5-70.1 WGI31499 p-Terpiienyl-d14 82.10 29.3-137 WG731499 PCS 1016 frig/.1 .0005 0.000603 121. 24.7-125 WG731497 PCB 1260 mg/1 .0005 0.000716 143. 47.7-149 WG731497 DecactiIorobiphenyl 97.10 70-256 WG731497 Tetrachlorc-m-xylene 62.10 13.9-137 WC731497 Performance of this Analyte is outside of established Criteria. For additional information, please see Attachment A 'List of Analytes with QC QualiEiers.' Page 12 of 15 12065 Lebanon Rd. Mt, Juliet, TN 37122 (615) 758-5858 1-800-767-5859 OESC Fax (615) 758-5859 L-A•B S•C•I•E•N•C,E•5 Tax I.D. 62-0814289 Est. 1970 Eaton Corporation Katie Holbrook 2564 Durham Road Quality Assurance Report Level it Roxboro, NC 27373 July 21, 2014 L709644 Laboratory Control Sample Analyte UniLs Known Val ReSolt % Rec Limit Batch PPH - Oil 6 Grease mg/l 20 16.8 84.0 78-114 WG732206 Copper ma/1 1 1.13 113. 80-220 WG731528 Laboratory Control Sample Duplicate Analyte Units Result Ref %Rec Limit RPD Limit Batch 1,1,1-Trichloroethane mg/1 0.0263 0.0257 105. 73.2-123 2.33 20 WG731467 1,1,2,2-Tetrachl0r0ethane mg/l 0.025B 0.0255 103. 70.7-122 1.18 20 wG731467 1,1,2-Trichlaroethane mg/l 0.0234 0.0232 94.0 77,7-118 0.870 20 WG731467 1,1-Dichlorcethane mg/1 0.0252 0.0247 101. 70.7-126 2.09 20 WG731467 1,1-Dichlorcethene mn/2 0.0251 0.0251 100. 67.B-129 0.320 2D WG731467 1,2-Dichlorobenzene mg/2 0.0261 0.0251 104. 78.4-117 2.69 2C wG731467 1,2-Dichlcroethane mg/1 0.0296 0.0296 118. 68.8-124 0.230 20 WG731467 1,2-Dichloropronane mg/1 0.0262 0.0263 105. 76.5-119 0.650 20 WG731467 1,3-Dichlorobenzene mg/l 0.0267 0.0256 107. 70.6-126 4.21 20 WG731467 1,4-Dichlorobenzene mg/1 0,0254 0.0247 102. 78.8-115 2.74 20 WG731467 2-Chloroethyl vinyl etlier mg/1 0.130 0.134 104. 43.8-150 3.33 20 WG731467 Acrolein mg/1 0.117 0.117 93.0 10-190 0.110 28.1 WG731467 Acrylonitrile mg/1 0.123 0.123 S48.0 55.2-130 0.260 20 WG731467 Benzene mg/1 0,0269 0.0269 108. 74.8-121 0,0600 20 WG731467 Bromodichloromethane mg/1 0.0263 0.0271 105. 75,1-116 2.96 20 WG731467 Bromoform mg/1 0.0233 0.0232 93.0 61.5-130 0.670 20 WG731467 Bromomethane mg/1 0.0267 0.0264 107. 49.9-162 1.20 20 WG731467 Carbon tetrachloride mg/] 0,0262 0.0260 105. 70.2-123 0.100 20 WG7.1461 Chlorobenzene mg/1 0.0262 0.0254 105. 78.1-119 2.77 20 WG731467 Chlorodibrcmomethane mg/l 0.0262 0.0257 105, 74-122 2.21 20 WG73]467 Chloroethane mg/1 0.0299 0,0289 120. 61.7-135 3.69 20 WG731467 Chloroform mg/l 0,0261 0,0257 104. 76-121 1.54 20 WG731467 Chloromethane mg/1 0.0227 0.0221 91.0 61.5-129 2.58 20 WG731467 cis-1,3-Dichlaropropene mg/1 0.0262 0.0267 105. 78.2-120 2.81 20 WG731467 Dichlorodifluoromethane mg/l 0.0229 0.0222 92.0 54.8-135 2.89 20 WG731467 ELhylbenzene mg/1 0.0253 0.0253 101, 78.8-122 0,0400 20 WG731467 Muthylene Chloride mg/1 0,0235 0,0230 94.0 70.3-120 2.24 20 WG731467 Tetrachioroethene mg/1 0.0237 0.0240 95.0 72.6-126 1.57 20 WG731467 Toluene mg/1 0.0266 0.0267 106. 79.7-116 0.250 20 WG732467 trans-1,2-Dichloroethene mg/1 0.0233 0.0226 93.0 72.6-221 3.28 20 WG731467 Craps-1,3-Dichloropropene mg/1 0.0266 0.0260 106. 74.3-123 2,46 20 WG731467 TrichlGroeLhene mg/1 0.0269 0.0265 208. 77.7-118 1.63 20 WG731467 Trichlorofluorometnane mg/1 0.0240 0.023E 96.0 63.5-135 0.960 20 WG732467 Vinyl chloride mg/l 0.0222 0.0217 89.0 65.9-128 2.17 20 WG731467 4-Bromofluorobenzene 100.0 71-126 WG731467 Dibromo£luoromethane 99.60 78.3-121 WG731467 Toluene-d8 105.0 86.5-111 WG731467 a,a,a-Trifluorotoluene 98.20 e5-114 WG731467 Suspended Solids mg/1 788. 788. 102. 65-115 0.00 5 WG731508 4,4-DDD mg/1 0.OD0262 0.000270 231. 47.6-144 2.70 24.3 WG731497 4,4-LDE mg/l 0,000224 0.000238 112. 45-124 5.80 25.7 WG731497 4,4-DDT mg/l 0,000251 O.000260 126. 45.8-130 3.51 25.4 W0731497 Aldrin mg/l 0.0000507 0.0000631 23.0 10-120 21.7 33.9 WG731497 Alpha BHC mg/1 0.000202 0.000210 101, 53.6-125 3.94 22.3 WG731497 Beta T314C mg/l 0.000234 0.000248 117, 55.E-130 6.07 20.6 WG731497 Delta BHC mg/1 0.000225 0.000235 112. 42.2-135 1.45 23.3 WG731497 Performance of tnis Analyte is outside of established criteria. For additional information, please see Attachment A 'List of AnaIytes uit'� OC Qualifiers.' Page 13 of 15 12065 Lebanon Rd. Mt. Juliet, TN 37122 JOESC (6151 758-5858 1-800-767-5859 Fax (615) 758-5859 L•A-B S•C•I-E•N•C E'S Tax I.D. 62-08142$9 Est. 1970 Eaton Corporation Katie Holbrook 2564 Durham Road Quality Assurance Report Level II Roxboro, NC 27573 July 21, 2014 L709644 i,aboratory Control Sample Duplicate Analyze Units Result Ref %Rec Limit RPD Limit Batch Dieldrin mg/1 0,000250 0.000261 125. 55-127 4.26 22.9 WG731497 Enciosulfan I mg/1 0.000251 0.000265 125. 54.7-127 5,38 24.3 WG731497 Endosul£an 11 mg/1 0.000259 0.000261 129. 53.1-1v5 1.00 23.5 WG731497 Endosulfan sulfate mg/1 0.000259 0.000265 130. 51.5-132 2.00 26.3 WG731497 Endrin mg/1 0.000243 0.000264 122. 50.1-131 9.00 29.1 WG721497 Endrin aldehyde mg/1 0.000252 0.000256 126. 39.5-137 1.51 28.4 WG731497 End[ -in ketone rug/1 0.D00265 0.000265 132. 53.5-139 0.0400 28.4 WG731497 Gamma EHC mg/1 0.000206 0.000217 103. 54.7-125 5,28 21.1 WG731497 Heptachlor mg/1 0.0000933 0.000115 47.0 20.7-127 21.0 3 0. 5 WG731497 Heptachlor epoxide ma/1 0.000240 0.000250 120. 56.4-124 4.34 23.1 WG731497 Hexachlorobenzene mg/1 0.0000832 0.0000884 42,0 26.7-114 6.07 27.6 WG731497 Methoxychlor mg/l 0.000285 0.000290 143. 48.2-144 1.58 27.8 WG731497 ➢ecachlorobiphenyl 106.0 10-156 WG731497 Tetracnlero-m-xylene 92.80 13.9-137 WG731497 Lead mg/l 1.03 1,04 103. 85-115 0.434 20 WG731523 Zinc ma/1 1.05 1.05 105. 85-115 0.00a64 20 WG731528 1,2,4-Trichlorobenzene mg/1 0.0178 0.0175 71.0 22.9-96.1 1.35 27,5 WG731499 2,4,6-Trichlorophenol mg/1 0.0229 0.0227 92.0 29.8-107 0.980 24.1 WG731499 2,4-❑ichlorophenoI me/1 0.0199 0.0199 80.0 31.4-103 0.160 24.9 WG731499 2,4-Dimethylphenol mg/1 0.0212 0.0200 85.0 31.9-107 5.66 25.7 WG731499 2,4-Dinitrophenol mg/1 0.0116 0.0115 46.0 24.2-128 0.700 20.5 WG731499 2,4-Dinitrot01Lzene ma/1 0.0214 0.0213 85.0 31.2-105 D.290 22 WG731499 2,6-Dinitrotoluene mg/1 0.0216 0.0228 86.0 30.6-106 5.25 23.1 WG731499 2-Chloronaphthalene mg/1 0.0211 0.0225 84,0 33.6-105 6.29 23 WG731499 2-Chloronhenol mo/1 0.0174 0.0176 70.0 26.2-91.5 1.14 26.5 WG731499 2-Nitrophenol mg/1 0.0220 0.0217 88.0 25.9-106 1.12 26.9 WG731499 3,3-Dichlorobenzidine mg/1 0.0216 0.0231 B6.0 27.2-i42 6.63 22.3 WG731499 4,6-Dinitro-2-methylphenol mg/1 O.D219 0.0214 88.0 18.4-146 2.44 24.4 wG731499 4-Bromophenyl-phenylether mg/1 0.0224 0.0234 90.0 40.7-I16 4,52 21 WG731499 4-Chlorc-3-methylphenol mg/1 0.0185 0.0175 74.0 35.7-100 5.51 22.9 WG731499 4-Chlorophenyl-phenylether mg/l 0.0225 0,0226 90.0 39-113 0.530 20.9 WG731499 4-Nitrophenol mg/1 0.00739 0.00707 30.0 1C-52.7 4.35 40 WG731499 Acenaphthene mg/1 0.0214 0.0211 86.0 38.7-109 1.58 21,5 WG731499 Acenaphthylene mg/1 0.0204 0.0207 02.0 36-106 3.64 21 WC; 73a499 Anthracene Mgt] 0.0210 0.0214 84.0 43.6-113 i.89 18.8 WG731499 1,2-Dip1heny1hydrazine mg/1 0.0262 0.0267 105. 37.6-111 2.13 21.1 WG731499 Ben2idine mg/1 0.0220 0.0184 86.0 10-165.2 17.8 4C WG731499 Benzo(a)anthracene mg/1 0.0217 0.0218 97.0 51.2-112 0.180 20 WG731499 Benzo(a)pyrene mg/] 0.0205 D.0195 82.0 45.6-106 5.21 20 WG731499 Benzo(b)fluoranthene mg/1 0.0224 0.0219 90.0 47.6-111 2.50 20 WG731499 Benzo(g,h,ilperylene mg/l 0.0241 0,0230 96.0 45.2-117 4.55 20 W2731499 Benzo(k)fluoranthene mg/l 0.0226 0.0208 90.0 49.4-114 8.43 20 WG731499 Benzylbutyl phthalate mg/l 0.0212 0.D194 B5.0 31.8-123 8.66 20.7 WG731499 Bis(2-chlorethoxy)nIeUiane mg/l 0.0171 0.0166 71.0 37.2-111 5,02 24.1 WG731499 Bis(2-ch1oroethyl)ether my/1 0.0155 0.0158 62.0 22.6-10E 2.03 27.9 WG737499 Bis(2-chloroisopropyllether mg/l 0.0157 0.0178 G3.0 32.9-100 12.9 25.1 WG731499 Bisi2-ethylhexyl)phthalate mg/1 0.0202 0.0197 81.0 36.9-134 2.56 23.6 WG731499 Chrysene mg/1 0.0226 0.0207 90.0 54.6-120 9.20 20 WG731499 Di-n-butyl phthalate mg/l 0.0196 0,0202 78.0 41.E-120 3.30 20.2 WG731499 Di-n-octyl phthalate mg/1 0.0204 0,0204 82.0 39.7-112 0.110 21.1 WG731499 Dibenz(a,'n)anthracene mg/l 0.0249 0.0246 100. 42.6-118 1.09 20 WG731499 Diethyl phthalate mg/l 0.0218 0.0220 37.0 36.5-129 0.910 20 WG731199 ➢imethyl phthalate mg/1 0.0236 0.0235 94.0 35.3-128 0.4B0 20.8 WG731499 Flucranthene mg/1 0.0209 0.0211 84.0 45.9-115 0.970 20 WG731499 Fluorene mg/l 0.0205 0.0214 62.0 41-112 4.03 20.2 WG731499 Performance of this Ana2yte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 14 of 15 *ESC 1 Eaton Corporation Katie Holbrcck 2564 Durham Road Roxboro, NC 27573 Quality Assurance Report Level II L709644 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-600-767-5859 Fax (615) 758-5859 I'ax I.D. 62-0814289 Est. 1970 July 21, 2014 Laboratory Control Sample Duplicate Analyte Units Resu'_t Ref %Rec Limit RPD Limit Batch Hexachlore-1,3-butadiene mg/1 0.0172 0.0172 69.0 16.1-104 0.510 31.2 wG731499 Hexachlorobenzene mg/l 0.0213 0.0214 85.0 39.5-116 0.360 20.1 WG731499 Herachlorocyclopentadiene mg/1 0,0128 0,013, 51.0 10-121 3.50 27.9 wG731499 Hexachloroethane ma/I 0.0141 0,0155 36.0 16.5-89.8 9.52 3D.7 WG731499 Indenoi1,2,3-cdlpy[ene mg/1 0.0245 0.0241 98.0 45-116 1.37 20 WG731499 Isophorone mg/1 0.0216 0.0209 86.0 35.4-112 3.10 21.5 WG731499 n-Nitrosodi-n-propylamine mg/l 0.0193 C-0183 77.0 33.2-106 5.32 23.7 WG731499 n-Nitrosodimethylamine mg/l 0.0116 0.0101 46.0 10-80.1 13.7 37.5 wG731499 n-Nitrosodiphenylamine mo/1 0.0239 0.0242 96.0 44.4-113 O.E80 20 WG731499 Naphthalene mg/l 0.0189 0.0184 76.0 32.2-101 2.90 23.8 WG731499 Nitrobenzene mg/l 0.0216 0.0213 67.0 31.4-106 2.35 25.7 W0731499 Rentachlorophenol mg/l O.C144 0.0154 58.0 10-97.4 6,71 35.1 WG731499 Phenanthrene mg/1 0.0203 0.0206 81.0 46.4-113 1.67 20 WG731499 Phenol mg/1 0-00893 0.00887 36.0 10-57.9 0.580 35 WG731499 Pyrene mg/l 0.0223 0.0220 89.0 46.3-117 1.56 20 WG731499 2,4,6-Tribromophenol 96.00 11.2-130 WG731499 2-Fluorobiphenyl 95.20 29.5-231 WG731499 2-Fluorcphenol 45.40 10-77.9 wG731499 Nitrobenzene-d5 71.60 21.8-123 WC732499 Plienol-d5 34.50 5-70.i WG731499 p-Terphenyl-d14 90.40 29.3-137 WG731499 PCB 1016 ma/l 0.000555 0.000603 Ill, 24.7-228 8.21 34.9 WG731497 PCB 1260 mg/l 0.000631 0.3GC716 126. 47.7-149 12.6 28.6 WG731497 Decachlorobiphenyl 107.0 10-156 WG731497 Tetracl,lorc-m-xylene 100.0 13.9-137 WG731497 TPH - Oil ti Grease mg/l 16.8 16.8 84.0 78-114 0.00 18 WG732206 Copper mq/1 1.11 1.13 Ill. 80-120 2.00 20 WG731528 Matrix Spike Analyte Units MS Res Ref Res TV 8 Rec Limit Ref Samp Batch 1,1,1-Trichloroethane mg/1 0,0276 0.0 .025 110. 58.7-134 L709814-04 WG731467 1,1,2,2-Tetracliloroethane mg/l O.D265 0.0 .025 110. 56-232 L709814-04 WG731467 1,1,2-Trichloroethane rn0/1 0.0236 0.0 .025 94.0 66.3-125 L709614-04 WG731467 1,1-Dichloroethane mg/1 0.0275 0.0 .025 110. 58.5-132 L709814-04 WG731467 1,1-Dichloroethene mg/1 0.0283 0.0 .023 110. 51.1-140 L709824-04 WG731467 1,2-Dichlorobenzene mg/l 0.0259 0.0 .025 100. 68.2-123 L709814-04 WG731467 1,2-Dichloroethane mg/l 0.0297 0.0 .025 120. 60-126 1,709614-04 WG731467 1,2-Dichloropropane mg/l 0.0266 0.0 .025 310, 64.2-123 L709814-04 WG731467 1,3-Diclilerooenzene mg/1 0.0264 0.0 .025 110. 63.1-231 L709814-04 WG731467 1,4-Dichlorobenzene mg/l 0.0251 0.0 .025 100, 68.6-123 L709814-04 WG721467 2-Chlorcethyl vinyl ether ma/l 0.134 0.0 .125 110. 10-155 L709614-04 WG731467 Acrolein mg/l 0.139 0.0 .225 110, 10-200 L709514-04 WG731467 Acrylonitrile mg/1 C.143 0.0 .125 110. 49.4-133 L709814-04 WG731467 Benzene mg/1 0.0269 0.0 .025 110. 54.3-133 L709814-D4 WG731467 Bromodichloromethane rua/1 0,0265 0.0 .025 110. 63.9-121 L709614-04 WG731467 Bromoform mg/l 0.0237 0.0 .025 95-0 59.5-134 1,709814-04 WG731467 Bromomethane mg/1 0.0310 0.0 .025 120. 41.7-155 L709814-04 wG731467 Carbon tetrachloride mg/1 0.0281 0.0 .025 lie. 55.7-134 L709814-04 WG731467 Chlorobenzene mg/1 0.026C 0.0 .025 100. 67-225 L709814-04 WG731467 Chlorodibromomethane mg/1 D.0257 0.0 .025 ]00. 64.3-125 L709814-04 WG731467 Chloroethane rrig/1 0,0337 0.0 .025 140. 51.5-136 L709814-04 WG732467 Chloroform mg/1 0.0278 0.0 .025 120. 63-129 L709814-04 wG731467 Performance of this Analyte is outside of established criteria. For additional information, p ease see ACtacnment A 'List of Analytes with QC Qualifiers.' Page 15 of 15 OESC I Eaton Corporation K,) tie Holbrook 2564 Durham Road Roxboro, HC 27513 (Duality Assurance Report Level II L709644 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5855 Tar. I.D. 62-0814289 Est. 1970 July 21, 2014 Analyze Units MS Res Matrix Ref Spike Res TV 8 Rec Limit Re` Samp Batch Chloromethane mg/l 0.0264 0.0 .025 110. 42.4-135 L709814-04 WG731467 cis-1,3-Dichloropropene mg/1 0.0265 0.0 .D25 110. 66.4-125 L709614-04 WG731467 Dichlorodifluoromethane mg/1 0.02EI 0.0 .025 110. 40.6-144 L709614-04 WG731467 Ethylbenzene ma/1 0.0257 0.0 .025 100. 61.4-133 L709814-04 WG731467 Methylene Chloride n1g/I 0.0260 0.0 .025 100. 58.1-122 L709814-04 WG731467 Tetrachloroethene mg/1 0.0235 0.0 .025 94.0 53-139 L709814-04 WG731457 Toluene mg/1 0.0257 D.0 .025 100. 61.4-130 L709814-04 WG731467 trans-1,2-Dichloroethene mg/1 0.0256 0.0 .025 100. 56.5-129 L709814-04 WG731467 trans-1,3-Dichloropropene mg/1 0.0255 0.0 .025 100. 64.1-12B L709814-04 WG731467 Trichloroethene mg/l 0.0265 0.0 .025 110. 44.1-149 L709814-04 WG731467 Trichlorofluoromethane mo/1 0.027I 0.D .025 110, 49.6-145 L709814-04 WG731467 Vinyl chloride ma/1 0.0247 0.0 .025 99.0 47.8-137 L709814-04 wG731467 4-8romofluorobenzene 100.0 71-126 WG731467 Dibromofluoramethane 108.0 78.3-121 WG731467 Toluene-d8 105.0 88.5-111 WG731467 a,a,a-TrifluaroLoluene 98.10 85-114 WG731467 Lead rnq/1 1,03 0.0 1 i00. 15-125 L709775-09 WG731528 Matrix Spike Duplicate Analyte Units MSD Ref %Rec Limit RpD Limit Ref Samn Batch 1,1,1-Trichloroethane Semi-annual Stormwater Discharge Monitoring Report _ for North Carolina Division of Water Quality General Permit No. NCGO30000 Date submitted 7/.t4114 CERTIFICATE OF COVERAGE NO. NCG030027 FACILITY NAME Eaton Corporation—Eneine Comoonents Division COUNTY Person _ PERSON COLLECTING SAMPLES Kim Witkowski_ LABORATORY ESC Lab Cert. # ENV375LW21704/810041 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2014 SAMPLE PERIOD ® Jan -June [❑ July -Dec or ❑ Monthly' month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow ❑Water supply E]SA ❑Other WS-111: NSW PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --> [] No discharge this period?' Date Sample 24-hour rainfall pH, Non -Polar O&G/Total Toxic Outfall No. Collected' amount, Total Suspended Solids Standard units Copper Lead Zinc Total Petroleum Organics (mo/dd/yr) Inches3 Hydrocarbons Benchmarks ===> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0-03 mg/L 0.067 mg/L 15 mg/L 1 mg/L Pond (001) 6/25/14 1.375 32 8.3 0,0096 <0.005 0.083 2.0 Not Detected Tool Room Trench 6/25/14 1.375 49 7.2 0.025 0.0025 OA50 <5.6 Not (0051 Detected 9 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page i of 3 NC DENR Raleigh RegiorW oftce racuaties that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Sao/i: Name (Print name) 6 , Pr - Title (Print title) (Signature) ( rate) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported ir3 the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier I, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > S5 gal of new oil per month. n No discharge this period?2 Outfall No. Date Sample Collected) (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L' 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B " See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 mute: q you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES [] No ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one coyv of this DMR including all "No Discharge" reports, within 30 days of receivt of the !ab results (or at end of monitoring period in the case of "No Discharge" reports)_to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Pe 7 Date] Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 *ESC I Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Report Summary Monday .duly 07, 2014 Report Number: L707275 Samples Received: 06/27/14 Client Project: 28091-R 12065 Lebanon Rd. Mt. JUlieL, TH 7129 (615) 758-5858 1-800-767-5B59 Fax (615) 758-5859 Tax I.D, 62-0814289 Est. 1970 Description: Eaton Corp Semi -Annual Stormwater The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Entire Report Reviewed By: JiM4 Hunt ESC Representative Laboratory Certifrcatio1l NuMbers A2LA - 1461-01, AIRA - 100769, AL - 10660, CA - 01157CA, CT - PH-0197, FL - S87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, W1 - 998093910, NV - TN000032011-1, TX - T1047C4245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, extent in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Page 1 of 22 r YOUR LAB OF CMOICS Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS June 27, 2014 Eaton Corp Semi -Annual Stormwater POND Katie Holbrook 06/25/14 19:25 July 07, 2014 ESC Sample # 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 158-5656 1-800-767-5859 Fax f615) 758-5859 Tax I.D. 62-0814269 Est. 1970 L707275-01 Site ID ROXBORO, NC Project # 28091-R Parameter Result MDL RDL Units Qualifier Method Date Dil. pH {On Site) 8.3 su Temperature (on -site) 25.1 Deg. C Suspended Solids 32. 0.35 2.5 mg/1 2540 D- 06/30/14 1 TPH - Oil & Grease 2.0 0.72 5.4 mg/l J 1664A 06/30/14 1 Copper 0.0096 0.0070 0.020 mg/l J 200.7 07/02/14 1 Lead U 0.0020 0.0050 mg/1 200.7 07/07/14 1 Zinc 0,083 0.0034 0,030 mg/1, 200.7 07/02/14 1 TTO Volatile Organics Acrolein U 0.0089 0.050 mg/l 624 06/28/14 1 Acrylonitrile U 0.0019 0.010 mg/l 624 06/28/14 1 Benzene U 0.00033 0.0010 mg/1 624 06/28/14 1 Bromodichloromethane U 0.00038 0.0010 mg/1 624 06/28/14 1 Bromoform U 0.00047 0.0010 mg/l 624 06/28/14 1 Bromomethane U 0.00087 0.0050 mg/1 624 06/28/14 1 Carbon tetrachloride U 0.00038 0.0010 mg/1 624 06/28/14 1 Chlorobenzene U 0.00035 0.0010 mg/1 624 06/28/24 1 Chlorodibromomethane U 0.00033 0.0010 mg/1 624 06/28/14 1 Chloroethane U 0.00045 0.0050 mg/1 624 06/28/14 1 2-Chloroethyl vinyl ether U 0.0030 0.050 mg/l 624 06/28/14 1 Chloroform U 0.00032 0.0050 mg/1 624 06/28/14 1 Chlcromethane U 0.00028 0.0025 mg/l 624 06/28/14 1 1,2-Dichlorobenzene U 0.00035 0.0010 mg/1 624 06/28/14 1 1,3-Dichlorobenzene U 0.00022 0.0010 mg/l 624 06/28/14 1 1,4-Dichlorobenzene U 0.00027 0.0010 mg/1 624 06/2a/14 1 Dichlorodiflucromethane U 0.00055 0.0050 mg/l 624 06/28/14 1 1,1-Dichloroethane U 0.00026 0.0010 mg/l 624 06/28/14 1 1,2-Dichlorcethane U 0,00036 0.0010 mg/1. 624 06/28/14 1 1,1-Dichloroethene U 0.00040 0.0010 mg/l 624 06/28/14 1 trans-1,2-Dichloroethene U 0.00040 0.0010 mg/1 624 06/28/14 1 1,2-Dichloropropane U 0.00031 0.0010 mg/l 624 06/28/14 1 cis-1,3-Dichloropropene U 0.00042 0.0010 mg/1 624 06/28/14 1 trans-1,3-Dichloropropene U 0.00042 0.0010 mg/l 624 06/26/14 1 Ethylbenzene U 0.00038 0.0010 mg/1 624 06/28/14 1 Methylene Chloride U 0.0010 0.0050 mg/1 624 06/28/14 1 1,1,2,2--Tetrachlorcethane U 0.00058 0,0010 mg/1 624 06/28/14 1 Tetrachloroethene U 0.00037 0.0010 mg/1 624 06/28/14 1 Toluene U 0.00078 0.0050 mg/l 624 06/28/14 1 1,1,1-Trichloroethane U 0,00032 0,0010 mg/1 624 06/28/14 1 1,1,2-Trichloroethane U 0.00038 0.0010 mg/l 624 06/28/14 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 17:36 Printed: 07/07/14 17:36 Page 2 of 22 OESC 4 Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS June 27, 2014 Eaton Corp Semi -Annual Stormwater POND Katie Holbrook 06/25/14 19:25 12065 Lebanon Rd. W. JUlieL, TN 37122 (615) 756-5658 1-800-761-5659 Fax (615) 758-5859 Tay. I.D. 62-0814289 Est. 1970 July 07, 2014 ESC Sample # : L707275-01 Site ID ROXBORO, NC Project # 28091-R Parameter Result MDL RDL Units Qualifier Method Date Dil. Trichloroethene U 0.00040 0.0029 mg/l 624 06/28/14 1 Trichloroflucromethane U 0.0012 0.0050 mg/l 624 06/28/14 1 Vinyl chloride U 0.00026 0.0010 mg/l 624 06/28/14 1 Surrogate Recovery Toluene-d8 98.9 % Per-. 624 06/28/14 1 Dibromoflucromethane 100. % RLc. 624 06/28/14 1 a,a,a-Trifluorotoluene 100. % Rec. 624 06/28/14 1 4-Bromofluorobenzene 98.4 % Rec. 624 06/28/14 1 Pesticide/PCBs Aldrin U 0.0000081 0.000050 mg/1 608 07/03/14 1 Alpha BHC U 0.000017 0.000050 mg/1 608 07/03/14 1 Beta BHC U 0.000018 0.000050 mg/1 608 07/03/14 1 Delta BHC U 0.000020 0.000050 mg/1 608 07/03/14 1 Gamma BHC U 0.000018 0.000050 mg/l 608 07/03/14 1 Chlordane U 0.000098 0.00030 mg/1 608 07/03/14 1 4,4-ODD U 0,000017 0.000050 mg/1 608 07/03/14 1 4,4-ODE U 0.000016 0.000050 mg/l 608 07/03/14 1 4,4-DDT U 0.000018 0.000050 mg/1 608 07/03/14 1 Dieldrin Ti 0.000018 0.000050 mg/1 608 07/03/14 1 Endosui€an I U 0.000018 0.000050 mg/1 608 07/03/14 1 Endosulfan II U 0.000018 0.000050 mg/1 608 07/03/14 1 Endosulfan sulfate U 0.000020 0.000050 mg/l 608 07/03/14 1 Endrin U 0.000019 0.000050 mg/l 608 07/03/14 1 Endrin aldehyde U 0.000014 0.000050 mg/1 608 07/03/14 1 Endrin ketone U 0.000017 0,000050 mg/l 608 07/03/14 1 Heptachlor U 0.000011 0.000050 mg/l 608 07/03/24 1 Heptachlor epoxide U 0.000018 0.000050 mg/l 608 07/03/14 1 Hexachlorobenzene U 0.000013 0.000050 mg/1 608 07/03/14 1 Methoxychior U 0.000019 0,000050 mg/1 609 07/03/14 1 Toxaphene U 0.00017 0.00030 mg/1 608 07/03/14 1 PCB 1016 U 0.000020 0.00050 mg/l 608 07/02/14 1 PCB 1221 U 0.000024 0.00050 mg/l 608 07/02/14 1 PCB 1232 U 0.000021 0.00050 mg/1 608 07/02/14 1 PCB 1242 U 0.000024 0.00050 mg/l 608 07/02/14 1 PCB 1248 U 0.000014 0.00030 mg/1 608 07/02/14 1 PCB 1234 U 0.000018 0.00050 mg/l 608 07/02/14 1 PCB 1260 U 0.000015 0.00050 mg/1 608 07/02/14 1 Pest/PCBs Surrogates Decachlorobiphenyi 42.8 % Rec. 608 07/02/14 1 Tetrachloro-m-xylene 67.1 % Rec. 608 07/02/14 1 TTO Base/Neutral Extractabl.es U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL - EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 17:36 Printed: 0-1/07/14 17:36 Page 3 of 22 12065 Lebanon Rd. Mt. Juliet, TN 31122 1615) 758-5856 1-B00-76_�-5859 OESC Fax 1615) 758-5859 L•A•B B•G•i•E•N-C•E,5 Tax I.D. 62-0814285 Est, 1970 REPORT OF ANALYSIS Katie Holbrook July 07, 2014 Eaton Corporation 2564 Durham Road Roxboro, NC 27573 ESC Sample # L707275-01 Date Received June 27, 2014 Description Eaton Corp Semi -Annual Stormwater Site ID ROXBORO, NC Sample ID POND Project # 28091-R Collected By Katie Holbrook Collection Date 06/25/14 19:25 Parameter Result MDL RDL Units Qualifier Method Date Dil. Acenaphthene Ti 0.00032 0.0010 mg/l 625 06/30/14 1 Acenaphthylene U 0.00031 0.0010 mg/1 625 06/30/14 1 Anthracene U 0.00029 0.0010 mg/l 625 06/30/14 1 Benzidine U C.0043 0.010 mg/l 625 06/30/14 1 Benzo(a)anthracene U 0.00032 0.0010 mg/1 625 06/30/14 1 Benzo(b)fluoranthene U 0.00027 0.0010 mg/1 625 06/30/14 1 Benzo(k)fluoranthene U 0.00036 0.0010 mg/1 625 06/30/14 1 Benzo(g,h,i)perylene U C.00033 0,0010 mg/1 625 06/30/14 1 Benzo(a)pyrene U 0,00034 0.0010 mg/1 625 06/30/14 1 Bis(2-chlorethoxy)methane U 0.00033 0.010 mg/l 625 06/3C/14 1 Bis(2-chloroethyl)ether U 0.0016 0.010 mg/l 625 C6/30/14 1 Bis(2-chloroisopropyl)ether Ti 0.00044 0.01C mg/l 625 06/30/14 1 4-Bromophenyl-phenylether U 0.00034 0,010 mg/1 625 06/30/14 1 2-Chloronaphthalene U 0.00033 0.0010 mg/l 625 06/30/14 1 4-Chlorophenyl-phenylether U 0.00030 0.010 mg/1 625 06/30/14 1 Chrysene U 0.00033 0.0010 mg/1 625 06/30/14 1 Dibenz(a,h)anthracene U 0.00028 0.0010 mg/l 625 06/30/14 1 3,3-Dichlorobenzidine U 0.0020 0.010 mg/l 625 06/30/14 1 2,4-Dinitrotoluene U 0.0016 0,010 mg/l 625 06/30/14 1 2,6-Dinitrotoluene U 0.00028 0.010 mg/1 625 06/30/14 1 1,2-Diphenylhydrazine U 0.00016 0.010 mg/1 625 06/3C/14 1 Fluoranthene U 0.00031 0.0010 mg/1 625 06/30/14 1 Fluorene U 0.00032 0.0010 mg/1 625 06/30/14 1 Hexachlorobenzene U 0.00034 0.0010 mg/1 625 06/30/14 1 Hexachloro-1,3-butadiene U 0.00033 0.010 mg/1 625 06/30/14 1 Hexachlcrocyclopentadiene U 0.0023 0.010 mg/1 625 06/30/14 1 Hexachlorcethane U 0.00037 0.010 mg/1 625 06/30/14 1 Indeno(1,2,3-cd)pyrene U 0.00028 0.0010 mg/l 625 06/30/14 1 Isophorone U 0.00027 0.010 mg/l 625 06/30/14 1 Naphthalene U 0.00037 0.0010 mg/1 625 06/30/24 1 Nitrobenzene U 0.00037 0.010 mg/1 625 06/30/14 1 n-Nitrosodimethylamine U 0.0013 0.010 mg/1 625 06/30/14 1 n-Nitrosodiphenylamirie U 0.00030 0.010 mg/1 625 06/30/14 1 n-Nitrosodi-n-propylamine U 0.00040 0.010 mg/l 625 06/30/24 1 Phenanthrene U 0.00037 C.0010 mg/1 625 06/30/14 1 Benzylbutyl phthalate U 0.00028 0.0030 mg/1 625 06/30/14 1 bis(2-ethylhexyl)phthalate U 0.00071 0.0030 mg/l 625 06/30/14 1 Di-n-butyl phthalate U 0.00027 0.0030 mg/l 625 06/30/14 1 Diethyl phthalate U 0.00028 0.0030 mg/1 625 06/30/14 1 Dimethyl phthalate U 0,00028 0.0030 mg/l 625 06/30/14 1 Di-n-octyl phthalate U 0.00028 0.0030 mg/1 625 06/30/14 1 Pyrene U 0.00033 C.0010 mg/1 625 06/30/14 1 1,2,4-Trichlorobenzene U 0.00036 0.010 mg/I 625 06/30/14 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: C7/07/14 17:36 Printed: 07/07/14 17:36 Page 4 of 22 Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS June 27, 2014 Eaton Corp Semi -Annual Stormwater POND Katie Holbrook 06/25/14 19:25 12065 Lebanon Rd. Mt, Juliet, TN 37122 1615) 758-5858 1-800-767-5859 Fax (6151 758-5859 Tax I.D. 62-0814289 Est. 1970 July 07, 2014 ESC Sample # L707275-01 Site ID ROXBORO, NC Project # 28091-R Parameter Result MDL RDL Units Qualifier Method Date Dil. TTO Acid Extractables 4-Chloro-3-methylphenol U 0,00026 0.010 mg/l 625 06/30/14 1 2-Chlorophenol U 0.00028 0.010 mg/l 625 06/30/14 1 2,4-Dichlorophenol U 0.00626 0.010 mg/l 625 06/30/14 1 2,4-Dimethylphenol U 0,00062 0,010 mg/l 625 06/30/14 1 4,6-Dinitro-2-methylphenol U 0.0026 0.010 mg/l 625 06/30/14 1 2,4-Dinitrophenol U 0.0032 0.010 mg/1 625 06/30/14 1 2-Nitrophenol U 0.00032 0.010 mg/1 625 06/30/14 1 4-Nitrophenol U 0.0020 0.010 mg/l 625 06/30/14 1 Pentachlcrophenol U 0.00031 0.010 mg/1 625 06/30/14 1 Phenol U 0.00033 0.010 mg/l 625 06/30/14 1 2,4,6-Trichlorophenol U 0.00030 0.010 mg/1 625 06/30/14 1 Surrogate Recovery 2-Fluorophenol 39.7 % Rec. 625 06/30/14 1 Phenol-d5 26.B % Rec. 625 06/30/14 1 Nitrobenzene-d5 50.6 $ Rec. 625 06/30/14 1 2-Fluorobiphenyl 60.1 % Rec. 625 06/30/14 1 2,4,6-Tribromophenol 64.4 % Rec. 625 06/30/14 I p-Terphenyl-d14 62.4 % Rec. 625 06/30/14 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 17:36 Printed: 07/07/14 17:36 Page 5 of 22 OESC i REPORT OF ANALYSIS Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NO 27573 July 07, 2014 12065 Lebanon Rd. Mt. iuiiet, TN 37122 I615) 758-5858 1-600-767-5855 Fa:: (615) 758-5855 Tar. I.D. 62-0811289 Est. 1910 ESC Sample # : L707275-02 Date Received June 27, 2014 Description Eaton Corp Semi -Annual Stormwater Site ID ROXBORO, NC Sample ID TOOL ROOM TRENCH Project # 28091-R Collected By Katie Holbrook Collection Date 06/25/14 18:45 Parameter Result MDL RDL Units Qualifier Method Date Dil. PH (On Site) 7.2 su Temperature (on -site) 23.4 Deg. C Suspended Solids 49. 0.35 2.5 mg/l 2540 D- 06/30/14 1 TPH - Oil & Grease U 0.72 5.6 mg/1 1664A 06/30/14 1 Copper 0.025 0.007C 0.020 mg/l 200.7 07/02/14 1 Lead 0.0025 0.0020 0.0050 mg/l J 200.7 07/07/24 1 Zinc 0.050 0.0034 0.030 mg/1 200.7 07/02/14 1 TTO Volatile Organics Acrolein U 0.0089 0.050 mg/l 624 06/28/14 1 Acrylonitrile U 0.0019 0.010 mg/1 624 06/2B/14 1 Benzene U 0.00033 0,0010 mg/1 624 06/28/14 1 Bromodichloromethane U 0.00038 0.0010 mg/l 624 06/28/14 1 Bromoform U 0.00047 0,0010 mg/1 624 06/28/14 1 Bromomethane U 0.00087 0.0050 mg/l 624 06/2B/14 1 Carbon tetrachloride U 0.00038 O.0010 mg/l 624 06/26/24 1 Chlorobenzene U 0.00035 0.0010 mg/l 624 06/28/14 1 Chlorodibromomethane U 0.00033 0.0010 mg/1 624 06/28/14 1 Chlorcethane Ti 0.00045 0.0056 mg/l 624 06/28/14 1 2-Chloraethyl vinyl ether U 0.0030 0.050 mg/l 624 06/2B/14 I Chloroform U 0.00032 0.0050 mg/1 624 06/2B/14 1 Chlorcmethane U 0.00028 0,0025 mg/l 624 06/28/14 1 1,2-Dichlorobenzene U 0.00035 0.0010 mg/1 624 06/28/14 1 1,3-Dichlorobenzene U 0,00022 0.0010 mg/1 624 06/28/14 1 1,4-Dichlorobenzene U 0.00027 0.0010 mg/l 624 06/28/14 1 Dichlorodifluoromethane U 0.00055 0.0050 mg/l 624 06/28/14 1 1,1-Dichloroethane U 0.00026 0.0010 mg/l 624 06/28/14 1 1,2-Dichloroethane U 0.00036 0.0010 mg/l 624 06/28/14 1 1,1-Dichloroethene U 0.00040 O.0010 mg/l 624 06/28/14 1 trans-1,2-Dichloroethene U 0.00040 0,0010 mg/l 624 06/28/14 1 1,2-Dichloropropane U C.00031 0.0010 mg/1 624 06/28/14 1 cis-1,3-Dichloropropene U 0.00042 0.0010 mg/l 624 06/28/14 1 trans-1,3-Dichloropropene U 0.00042 0.0010 mg/1 624 06/26/14 1 Ethylbenzene U C.00038 0.0010 mg/1 624 06/28/14 1 Methylene Chloride U 0.0010 0.0050 mg/1 624 06/28/14 1 1,1,2,2-Tetrachloroethane U 0.00058 0,0010 mg/1 624 06/28/14 1 Tetrachloroethene 0 0.00037 0.0010 mg/1 624 06/28/14 1 Toluene U 0.00076 0.0050 mg/l 624 06/28/14 1 1,1,1-Trichloroethane U 0.00032 0.0010 mg/l 624 06/29/14 1 1,1,2-Trichloroethane U 0.00038 0.0010 mg/1 624 06/28/14 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 17:36 Printed: 07/07/14 17:36 Page 6 of 22 *ESC I Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received Description Sample ID Collected By Collection Date REPORT OF ANALYSIS June 27, 2014 Eaton Corp Semi -Annual Stormwater TOOL ROOM TRENCH Katie Holbrook 06/25/14 18:45 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 July 07, 2014 ESC Sample # : 1,707275-02 Site ID ROXBORO, NC Project 28091-R Parameter Result MDL ROL Units Qualifier Method Date Dil, Trichloroethene U 0.00040 0.0010 mg/1 624 06/28/14 1 Trichlorofluoromethane U 0.0012 0,0050 mg/1 624 06/26/14 1 Vinyl chloride U 0,00026 0.0010 mg/1 624 06/28/14 1 Surrogate Recovery Toluene-d8 96.1 % Rec. 624 06/28/14 1 Dibromofluoromethane 99.3 % Rec. 624 06/28/14 1 a,a,a-Triflucrotoluene 99.4 % Rec. 624 06/28/14 1 4-Bromofluorobenzene 94.8 % Rec. 624 06/28/14 1 Pesticide/PCBs Aldrin U 0.0000081 0.000050 mg/1 608 07/03/14 1 Alpha BHC U 0.000017 0.000050 mg/l 608 07/03/14 1 Beta BHC U 0.000018 0.000050 mg/l 608 07/03/14 1 Delta BHC U 0.000020 0,000050 mg/l 606 07/03/14 1 Gamma BHC U 0.000018 0.000050 nag/1 608 07/03/14 1 Chlordane U 0.000096 0.00050 mg/l 608 07/03/14 1 4,4-DDD U 0.000017 0.000050 mg/1 608 07/03/14 1 4,4-DDE U 0.000016 0.000050 mg/1 608 07/03/14 1 4,4-DDT U 0.000018 0.000050 mg/l 608 07/03/14 1 Dieldrin U 0.000018 0.000050 mg/1 608 07/03/24 1 Endosulfan I U 0.000018 0.000050 mg/1 608 07/03/14 1 Endosulfan II U 0.000018 0.000050 mg/l 608 07/03/14 1 Endosulfan sulfate U 0.000020 0.000050 mg/1 608 07/03/14 1 Endrin U 0.000019 0.000050 mg/l 608 07/03/24 1 Endrin aldehyde U 0.000014 0.000050 mg/1 608 07/03/14 1 Endrin ketone U 0.000017 0.000050 mg/1 608 07/03/14 1 Heptachlor U 0.000011 0.000050 mg/l 608 07/03/14 1 Heptachlor epoxide U 0.000018 0.000050 mg/l 606 07/03/14 1 Hexachlorobenzene U 0.000013 0.000050 mg/l 608 07/03/14 1 Methoxychlor U 0.000019 0.000050 mg/1 608 07/03/14 1 Toxaphene U 0.00017 0.00050 mg/l 608 07/03/14 1 PCB 1016 U 0.000020 0,00050 mg/l 608 07/02/14 1 PCB 1221 U 0.000024 0.00050 mg/l 608 07/62/14 1 PCB 1232 U 0.000021 0.00050 mg/l 608 07/02/14 1 PCB 1242 U 0.000024 0.00050 mg/l 608 07/02/14 1 PCB 1248 U 0.000014 0.00050 mg/1 608 07/02/14 1 PCB 1254 U 0.000018 0.00050 mg/1 608 07/02/14 1 PCB 1260 U 0.000015 0,00050 mg/l 608 07/02/14 1 Pest/PCBs Surrogates Decachlorobiphenyl 44.0 % Rec. 608 07/02/24 1 Tetrachloro-m-xylene 78.5 % Rec. 608 07/02/14 1 TTO Base/Neutral Extractables U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SOL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 17:36 Printed: 07/07/14 17:36 Page 7 of 22 12065 Lebanon R6. Mt. Juliet, TN 37122 (615) 755-585B 1-60D-767-5859 *ESC rax f615) 758-5959 L•A,B S-C•f•E-N-C,E•5 Tam I.D. 62-0814285 ` Est. 1970 REPORT OF ANALYSIS Katie Holbrook July 07, 2014 Eaton Corporation 2564 Durham Road Roxboro, NC 27573 ESC Sample 4 L707275-02 Date Received June 27, 2014 Description Eaton Corp Semi -Annual Stormwater Site ID ROXBORQ, NC Sample ID TCOL ROOM TRENCH Project 4 28091-R Collected By Katie Holbrook Collection Date 06/25/14 16:45 Parameter Result MDL RDL Units Qualifier Method Date Dil. Acenaphthene U 0.00032 0.0010 mg/1 625 06/30/14 1 Acenaphthylene U 0,00031 0.0010 mg/1 625 06/30/14 1 Anthracene U 0.00029 0.0010 mg/l 625 06/30/24 1 Benzidine Ti 0.0043 0.010 mg/1 625 06/30/14 1 Benzo(a)anthracene U 0.D0032 0.0010 mg/l 625 06/30/14 1 Benzo(b)£luoranthene U 0.00027 0.0010 mg/1 625 06/30/14 1 Benzc(k)fluoranthene U 0.00036 0,0010 mg/1 625 06/30/14 1 Benzo(g,h,i)perylene U 0.00033 0.0010 mg/1 625 06/30/14 1 Benzo(a)pyrene U 0.00034 0.0010 mg/l 625 06/30/14 1 Bi5(2-chlorethoxy)methane U 0.00033 0.010 rng/l 625 06/30/14 1 Bis(2-chloroethyl)ether U 0.0016 0.010 mg/1 625 06/30/14 1 Bis(2-chlorci5opropyl)ether U 0.00044 0.010 mg/l 625 06/30/14 1 4-Bromophenyl-phenylether U 0,00034 0.010 mg/l 625 06/30/14 1 2-Chloronaphthalene U 0,00033 0.0010 mg/l 625 06/30/14 1 4-Chlorophenyl-phenylether U 0.00030 0.010 mg/1 625 06/30/14 1 Chrysene U 0.00033 0.0010 mg/l 625 06/30/14 1 Dibenz(a,h)anthracene U 0.00028 0-0010 mg/l 625 06/30/14 1 3,3-Dichlorobenzidine U 0,0020 0.010 mg/l 625 06/30/14 1 2,4-Dinitrotoluene U 0,0016 0.010 mg/l 625 06/30/14 1 2,6-Dinitrotoluene U 0.00028 0.010 mg/l 625 06/30/14 1 1,2-Diphenylhydrazine U 0,00016 0.010 mg/1 625 06/30/14 1 Fluoranthene Ti 0.00031 0.0010 mg/1 625 06/30/14 1 Fluorene U 0.00032 0.0010 mg/1 625 06/30/14 1 Hexachlorobenzene U 0.00034 0.0010 mg/l 625 06/30/14 1 Hexachloro-1,3-butadiene U 0.00033 0.010 mg/l 625 06/30/14 1 Hexachlorocyclopentadiene U 0.0023 0.010 mg/1 625 06/30/14 1 Hexachloroethane U 0,00037 0.010 mg/l 625 06/30/14 1 Indeno(1,2,3-cd)pyrene U 0.00028 0.0010 mg/l 625 06/30/24 1 Isophorone U 0.00027 0.010 mg/1 625 06/30/14 1 Naphthalene U 0.00037 0.0010 mg/l 625 06/30/14 1 Nitrobenzene U 0.00037 0.010 mg/l 625 06/30/14 1 n-Nitrosodimethylamine U 0.0013 0.010 mg/l 625 06/30/14 1 n-Nitrosodiphenylamine U 0.00030 0.010 mg/1 625 06/30/14 1 n-Nitrosodi-n-propylamine U 0.00040 0.010 mg/l 625 06/30/14 1 Phenanthrene U 0.00037 0.0010 mg/l 625 06/30/14 1 Benzylbutyl phthalate U 0.00028 0.0030 mg/1 625 06/30/14 1 Bis(2-ethylhexy.l)phtha1ate U 0.00071 0.0030 mg/1 625 06/30/14 1 Di-n-butyl phthalate U 0.00027 0.0030 mg/l 625 06/30/14 1 Diethyl phthalate U 0.00028 0,0030 mg/l 625 06/30/14 1 Dimethyl phthalate U 0,00028 0.0030 mg/l 625 06/30/14 1 Di-n-octyl phthalate U 0.00028 0.0030 mg/l 625 06/30/14 1 Pyrene U 0.00033 0.0010 mg/1 625 06/30/14 1 1,2,4-Trichlorobenzene U 0.00036 0.010 mg/l 625 06/30/14 1 U - NO (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SOL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 17:36 Printed: 07/07/14 17:36 Page 8 of 22 REPORT OF ANALYSIS Katie Holbrook Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Date Received June 27, 2014 Description Eaton Corp Semi -Annual Stormwater Sample 1D TOOL ROOM TRENCH Collected By Katie Holbrook Collection Date 06/25/14 1B:45 July 07, 2014 ESC Sample # 12065 Lebanon Rd. Mt. Juliet, TYd 37122 )6151 158-5E58 1-800-767-5859 Fax )615) 758-5859 Tax T.D. 62-CB14289 ESE. 1970 L707275-02 Site ID ROXBORO, NC Project # 28091-R Parameter Result MDL RDL Units Qualifier Method Date Dil. TTO Acid Extractables 4-Chloro-3-methylphenol U 0.00026 0.010 mg/1 625 06/30/14 1 2-Chlorophenol U 0.00028 0.010 mg/l 625 06/30/14 1 2,4-Dichlorophenol U 0.00028 0.010 mg/1 625 06/30/14 1 2,4-Dimethylphenol U 0.00062 0.010 mg/1 625 06/30/14 1 4,6-Dinitro-2-methy1phenol U 0.0026 0.010 mg/1 625 06/30/14 1 2,4-Dinitrophencl U 0.0032 0.010 mg/l 625 06/30/14 1 2-Nitrophenol U 0.00032 0.010 mg/l 625 06/30/14 1 4-Nitrophenol U 0.0020 0.010 mg/l 625 06/30/14 1 Pentachlorophenol U 0.00031 0.010 mg/1 625 06/30/14 1 Phenol U 0.00033 0.010 mg/1 625 06/30/14 1 2,4,6-Trichlorophenol U 0.00030 0.010 mg/1 625 06/30/14 1 Surrogate Recovery 2-Fluorophencl 39.5 % Rec. 625 06/30/14 1 Phenol-d5 25.8 8 Rec. 625 06/30/14 1 Nitrobenmene-d5 41.1 % Rec. 625 06/30/14 1 2-Fluorobiphenyl 48.3 % Rec. 625 06/30/14 1 2,4,6-Tribromcphenol 53.1 % Rec. 625 06/30/14 1 p-Terphenyl-d14 46.6 % Rec. 625 06/30/14 1 U = ND (Not Detected) MDL = Minimum Detection Limit = LOD = TRRP SDL RDL = Reported Detection Limit = LOQ = PQL = EQL = TRRP MQL Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 17:36 Printed: 07/07/14 17:36 Page 9 of 22 Attachment A List of Analytes with QC Qualifiers Sample Work Sample Number Group Type Analyte L707275-01 WG729742 SAMP Copper WG729422 SAMP TPH - Oil & Grease L707275-02 WG730173 SAMP Lead Run ID Qualifier R2954625 i R2952266 J R2956667i Page 10 of 22 Attachment B Explanation of QC Qualifier Codes Qualifier Meaning (EPA( - Estimated value below the lowest calibration point. Confidence correlates with concentration. Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable "unless qualified as 'R' (Rejected(." Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through ail stages of preparation and analyses. TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. Page 11 of 22 Summary of Remarks For Samples Printed 07/07/14 at 17:36:56 TSR Signing Reports: 350 R5 - Desired TAT MDL/RDL; PO = 79918 Sample: L707275-01 Account: EATONRNC Received: 06/27/24 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 17:36 PO - 79918 Sample: L707275-02 Account: EATONRNC Received: 06/27/14 09:00 Due ❑ate: 07/07/14 00:00 RPT Date: 07/07/14 17:36 12065 Lebanon Rd. Mc. Juliet, TN 37122 (615) 75B-585B 2-800-167-5859 *ESC Fax (615) 758-5859 L•A-6 S•C•i•E-N-C•E•S Tax I.D. 62-0814289 Est. 1970 Eaton Corporation Katie Holbrook: 2564 Durham Road Quality Assurance Report Level Ii Roxboro, NC 27573 July 07, 2014 L707275 Laboratory Blank Analyte Result Units Rec Limit Batch pate Analyzed 1,1,1-Trichloroethane < .001 mg/1 WG729149 06/28/14 06:17 1,1,2,2-Tetrachloroethane < .001 mg/1 WG729149 06/23/14 06:17 1,1,2-Trichloroethane < .001 mg/1 WG729149 06/28/14 06:17 1,1-Dichloroethane < .001 ma/1 WG729149 06/28/14 06:17 1,1-Dichloroethene < .001 ma/1 WG729149 06/28/14 06:17 1,2-Dich1orobenzene < .001 mg/1 WG729149 06/28/14 06:17 1,2-Dichloroethane < .001 mg/l WG729149 06/2R/14 06:17 1,2-Dichloropropane < .001 mg/l WG729149 06/28/14 06:17 1,3-Dichlorobenzene < .001 mg/1 wG729149 06/26/14 06:17 1,4-Dichlorobenzene < .001 mg/1 WG729149 O0/28/14 06c17 2-Chloroethyl vinyl ether < .05 ma/1 WG729149 06/2R/14 06:17 Acrolein < .025 111g/1 WG729149 06/26/14 06:17 Acrylonitrile < .01 mg/1 WG729149 06/26/14 o6:17 Benzene < .001 mg/l WG729149 06/28/14 06:17 Bromodichloremethane < .001 mg/1 WG729149 06/2Q/14 06:11 Bromoform < _001 mg/l WG729149 C6/28/14 06:17 Bromomethane < .005 mg/1 WG729149 06/28/14 06:17 Carbon tetrachloride < .001 mp/1 WG729149 OG/28/14 06:17 Chlorobenzene < .001 mg/l WG729149 06/28/14 06:17 Chlorodibromomethane < .001 ma/1 WG729149 06/28/14 06:17 Chloroet}lane < .005 mg/1 IXG729149 06/28/14 06:17 Chloroform < .005 mg/1 WG729149 C6/28/14 06:17 Chloromethane < .0025 mg/1 WG729149 06/26/14 06:17 cis-1,3-Dichloropropene < .001 mg/1 WG729149 06/28/14 06:17 Dichlorodifiuoromethane < .005 mg/1 WG729149 06/28/14 06:17 Ethylbenzene < .001 mg/1 WG729149 06/2b/I4 06:17 Methylene Chloride < .DD5 mg/1 WG729149 06/28/24 06:17 Tetrachlorcethene < .001 mg/1 WG729149 06/28/14 06t17 Toluene < .005 mg/1 WG729149 06/28/14 06:17 trans-1,2-1)ichloroethene < .001 mg/1 WG729149 06/28/14 06:17 trans-1,3-DiChloropropene < .001 mg/1 WG729149 06/28/14 06:17 Trichloroethene < .001 mg/1 WG729149 D6/28/14 06:17 T'richlorofluoromethane < .005 mg/1 WG729249 D6/28/14 D6:17 Vinyl chloride < .001 mg/1 WG729149 06/28/14 06:17 4-Brom01luorobenzene % Rec. 96.70 71-126 WG729149 06/28/14 06:17 Dibromofluoromethane 9 Rec. 99,60 7B.3-121 WG729149 06/26/14 06:17 Toluene -dB % Rec. 100.0 88.5-111 WG729149 06/28/14 0G:17 a,a,a-Trlflucrotoluene B Rec. 100.0 85-114 WG729149 06/28/14 06:17 TPH - 011 6 Grease < 5 mg/1 WG729422 06/30/14 01:59 Suspended Solids < 2.5 mg/1 WG729296 06/30/34 09:11 1,2,4-Trichlorobenzene < .01 mg/1 WG729093 06/29/14 23:10 2,4,6-Trichloroohenol < .01 rag/1 WG729093 06/29/14 23:10 2,4-Dichlorophenol < .01 mg/1 WG729093 06/29/14 23:10 2,4-Dimet}iyIohenoI < .01 mg/1 WG729093 06/29/14 23:10 2,4-Dinitrophenol < .01 mg/1 WG729093 06/29/14 23:10 2,4-Dinitrotoluene < .01 mg/1 WG729093 06/29/14 23:10 2,6-Dinit1'0t01uene < .01 mg/l WG729093 06/29/14 2--- :I0 2-Ch10ronaphthaIene < .001 mg/1 WG729093 06/29/14 23:10 2-Chlorophenol < .01 mg/l WG72K93 06/29/14 23:10 2-Nitrophenol < .01 mg/1 WG729093 06/29/14 23:10 3,3-Dichlorobenzidine < .01 mg/l WG729093 06/29/14 23:1D 4,6-Dinitro-2-methylphenol < .01 mg/1 WG729093 06/29/14 23:10 4-BromophenyI-phenyIether < .01 mg/1 WG729093 06/29/14 23:10 Per£O1"IiianCe of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with OC Qualifiers.' Page 12 of 22 12065 Lebanon Rd. Mt. Juliet, TN 37122 (6151 758-5858 1-800-767-5859 OESC Fax (6151 758-5859 L-A-B 5•C•I•E•N•C•E'S Tax I.D. 62-0814289 Est, 1970 Eaton Corporation Katie Holbxcok 2564 Durham Road Quality Assurance Report Level II Roxboro, NC 27573 July 07, 2024 L707275 LaboraLory Blank Analyte Result Units 8 ReC Limit Ratcli Date Analyzed 4-Ch1cro-3-methyiphenol < .01 mg/l WG729093 06/29/14 23:10 4-Chlorophenyl-phenylether < .01 mg/l WG729093 06/29/14 23:10 4-Nitrophenol < .01 mg/I WG729093 06/29/14 23:10 Acenaphthene < .001 m71/1 WG729093 06/29/14 23:10 Acenaphthylene < .001 me/1 WG729093 06/29/14 23:10 Anthracene < .001 me/l WG729093 06/29/14 23:10 1,2-Diphenylhydrazine < .01 ma/1 WG729093 06/29/14 23:10 Benzidine < .01 mg/1 WG729D93 06/29/14 23:10 Benzo(a)anthracene < .001 mg/l WG729093 06/29/14 23:10 Benzo(a)pyrene < .001 mg/l WG729093 06/29/14 23:10 Benzo(b)fluoranthene < .001 nIg/l WG729093 06/29/14 23:10 Benzo(9,h,i)perylene < .002 Ina/1 WG729093 06/29/14 23:10 Benzo(k)fluoranthene < .001 mg/l WG729D93 06/29/14 23:10 Benzylbutyl phthalate < .003 mg/1 WG729093 06/29/14 22:10 Ris{2-ch2orethoxylmethane < .01 mg/1 WG729093 06/29/14 23:10 Bis(2-chloroethyl)ether < .01 mg/l WG729093 06/29/24 23:10 Bisf2-chloroisonropylpether < .01 ma/1 WG729093 06/29/14 23:10 Eis(2-ethylhexyl)phthalate < .003 mg/1 WG729093 06/29/14 23:10 Chrysene < .001 mg/1 WG729093 06/29/14 23:10 Di-n-butyl phthalate < .003 mg/1 WG729093 06/29/14 23:10 Di-n-octyl phthalate < .003 mg/l WC729093 06/29/14 23:10 Dibenz(a,h)anthracene < .001 mg/l WG729093 06/29/14 23:10 Diethyl phthalate < .003 ma/1 WG729093 06/29/14 23:10 Dimethyl phthalate < .003 me/l WG729093 06/29/14 23:10 Fluoranthene < .001 mg/1 WG729093 06/29/14 23:10 Fluorene < .001 mg/1 WG729093 06/29/14 23u10 Hexachloro-1,3-butadiene < .03 MU/1 WG729093 06/29/14 23:10 Haxachlorobenzene < .001 mg/l WG729093 06/29/14 23:10 Hexachlorocyclopentadiene < .01 mg/1 WG729093 06/29/14 23:10 Hexachloreethane < .01 mg/1 WG729093 06/29/14 23:10 Indeno(1,2,3-cd)pyrene < .001 mg/1 WG729093 06/29/14 2 :10 Isophorone < .02 mg/1 WG729093 06/29/14 23:10 n-Nitrosodi-n-prooylamine < .01 mg/1 WC729093 06/29/24 23=10 n-Nitrosodimethylamifie < .01 mg/1 WG729093 O6/29/14 23:10 n-Nitrosodiphenylamine < .01 mg/1 WG729053 06/29/14 23:10 Naphthalene < .001 mg/1 WG729093 06/29/14 23:10 Nitrobenzene < .01 mg/l WC729093 06/29/14 23:10 Pentachloraphnnol < .001 mg/1 WG729093 06/29/14 23:10 Phenanthrene < .001 mg/1 WG729093 06/29/14 23:10 Phenol < .01 mg/1 WG729093 06/29/14 23:10 Pyrene < .Col mg/I WG729093 06/29/14 23:20 2,4,6-Tribromophenol 8 Rec. 63.80 11.2-130 WG729093 06/29/14 23:10 2-Fluorobiphenyl 6 Rec. 59.80 29.5-131 WG729093 06/29/14 23:10 2-Fluorophenol 6 Rec, 48.20 10-77.9 WG729093 06/29/14 23:10 Nitrobenzene-d5 8 Rec, 47.50 21.8-123 WG129093 06/29/14 23:10 Phenol-d5 9 Rec. 31.80 5-70.1 WG729C93 06/29/14 23:10 p-Terphenyl-d14 % Rec. 59,90 29.3-137 WG729093 06/29/14 23:10 Copper < .02 mg/1 WG129742 07/02/14 24:32 Zinc < .03 1119/1 WG729742 07/02/14 14:32 PCB 1016 < .0005 ma/l WG729545 07/02/24 16:02 PCB 1221 < .0005 m9/1 WG729545 D7/02/14 16:02 PCB 1232 < .0005 mg/1 WG729545 07/02/14 16:02 PCB 1242 < .0005 mg/1 WG729545 07/02/14 16:02 PCB 1248 < .0005 ma/1 WG729545 D7/02/14 16:02 PCE 1254 < .0005 mg/1 WG729545 07/02/14 16:02 Performance of this Analyte is outside of established criteria. For addiLional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 13 of 22 *ESC I 12065 Lebanon Rd. Mt, Juliet, Ti\ 37122 (615) 758-5858 1-800-761-5859 Fax (615) 758-5859 'Pax I.D. 62-0814269 Est. 1970 Eaton Corporation Katie Holbrook 2561 Durham Road Quality Assurance Report Level II Roxboro, PC 27573 July 07, 20I4 L707275 Laboratory Blank Analyte Result Units Rec Limit Batch Date Analyzed PCB 1260 DD05 Mull WG729545 07/02/14 16:02 Decachlorobiphenyl 8 Rec. 65.30 10-i56 wG729545 07/02/14 16:02 TeLrachloro-m-xylene % Rec. 60.00 13.9-137 WG729545 07/02/14 16:02 Lead < .005 1110/1 WG730173 07/05/14 2D:45 4,4-DUD < .00005 ma/1 WG729545 07/03/14 10:10 4,4-DDE < .00005 mg/1 WG729545 07/03/14 10:10 4,4-DDT < .00005 trig/1 WG729545 07/03/14 10:1D Aldrin < .00005 mg/l WG729545 07/03/14 10:10 Alpha BHC < .00005 mg/l W0729545 07/03/14 10:10 Beta BHC < .00005 my/I WG729545 07/03/24 1D:10 Chlordane < .005 mg/l WG729545 07/03/14 10:10 Delta BHC < .00005 my/1 WG729545 07/03/14 10:10 Dieldrin < .00005 mg/l WG729545 07/03/14 10:10 Endosulfan I < .00005 mg/l WG729545 07/03/14 10:10 Endosulfan 17 < .00005 1119/1 WG729545 07/03/14 10:10 Endosulfan sulfate < .00005 mg/1 WG729545 07/03/14 10c10 Endrin < .00005 mg/1 WG729545 07/03/14 10:10 Endrin aldehycie < .00005 mg/1 WG729545 07/03/14 1D:10 Endrin ketone < .00005 mg/1 WG729545 07/03/14 10:10 Gamma BHC < .00005 mg/1 WG729545 07/03/14 10:10 Heptachlor. < .00005 mg/1 WC729545 07/03/14 10:10 Heptachlor epoxide < .00005 mg/1 WG729545 07/03/14 10:10 Hexachiorobenzene < ,00005 mg/1 WG729545 07/03/14 10:10 Methoxychlor < ,00005 mg/1 WG729545 07/03/14 10:10 Toxaphene < .0005 mg/l WG729545 07/03/14 10:10 Decachlorobiphenyl % Rec. 77.50 10-156 WG729545 07/03/14 10:10 TeLrachloro-m-xylene % Rec. 90.20 13.9-137 WG729545 01/03/14 10:10 Duplicate Analyte Units Result Duplicate RPD Limit Ref samp Batch Suspended Solids mg/1 614. 568. 7,78' 5 L707091-01 WG729296 Suspended Solids mg/1 1110 1070 3.67 5 L7D7353-02 WG729296 Laboratory Control Sample Analyte Ur.1ts Known Val Result % Rec Limit Batch 1,1,1-Trichloroethane mg/l .025 0.0250 100. 73.2-123 WG729149 1,1,2,2-TetrachloroeLPiane mg/l .025 0.0297 119. 70.7-122 WG729149 1,1,2-Trichloroethane mu/l .025 0.0272 106. 77.7-118 WG729149 1,1-Dichloroethane ma/1 .025 0.0247 98.9 70.7-126 WG729149 1,1-Dichloroethene mg/l .025 0.0222 88.9 67.P-129 WG729149 1,2-Dichlorobenzene ma/1 .025 D.0264 I06. 78.4-117 WG729149 1,2-Dichloroethane mg/1 .025 0,0229 91.6 68.8-124 WG729149 1,2-Dichloropropane mg/l 0^_5 0.0243 97.2 76.5-119 WG729149 1,3-Dichlorobenzene mg/l .025 0.0268 107. 7G.8-128 WG729149 1,4-Dichlorobenzene mg/l .025 0.0254 201. 78.8-115 WG729149 2-Chloroethyl vinyl ether Mg/1 .125 0,115 92.2 43.3-150 WG729149 Acrolein mg/1 .125 0.140 i12, 10-190 WG729149 Acrylonitrile mg/l .125 0.129 103. 55.2-130 WG729149 Benzene mg/1 .025 0.0252 100. 74.8-121 wG729149 Bromodichloromethane mg/1 .025 0.0247 98.9 75.1-116 WG729149 Bromoform mg/1 .025 D.0297 115. 67.5-130 WG729149 Bromomethane mg/1 .025 D.0219 a7,8 49.9-162 WG729149 Carbon tetrachloride my/l .025 0.0274 109. 70.2-123 WG729149 Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with pC nualiliers.' Page 14 of 22 OESC t Eaton Corporation Katie Holbrook 2564 Durham Road Roxboro, NC 27573 Quality Assurance Reoort Level II L707275 12065 Lebanon Rd. ML. Juliet, TN 37122 (615) 758-5656 1-800-767-5859 Fax (615) 758-5659 Tax I.D. 62-0814289 rst. 197C July 07, 2014 LaboraLory Control Sample Analyte Units Known Val Result % Rec Limit Batch Chlorobenzene mq/1 .025 0.0260 104. 78.1-119 WG729149 ChlorodibromomeLhane mg/1 .025 0.0266 106. 74-121 WG729149 Chloroetirane mg/1 .025 0,0207 82.6 61.7-135 W0729149 Chloroform mg/1 .025 0.0250 100. 76-121 WG729:49 Chloromethane mg/1 .025 0.0221 88.3 61.5-129 WG729149 cis-1,3-Dichloropropene mg/1 .025 0.0258 103. 78.2-120 WG729149 Dichlorodifluoromethane mg/l .025 0.D232 92.9 54.8-135 WG729149 Elhylbenzene mg/1 .025 0.0261 105. 7818-222 WG729149 Methylene Chloride mg/1 .025 0.0251 100. 70.3-120 WG729149 TetraChIoroethene mg/1 .025 0.0260 104. 72.6-126 WC729149 Toluene mg/1 .025 0.0250 99.8 79.7-116 WG729149 trans- 1,2-DichloxoeLliene mg/1 .025 0.0264 106. 72.6-121 WG729149 trans-1,3-Dichloropropene mg/1 .025 0.0266 106. 74.3-123 WG729149 Trichloroethene MG/1 .025 0.0257 I03. 77.7-11? WG729149 Trichlorofluororriethane ma/1 .025 0,0239 95.4 63.5-135 WG729149 Vinyl chloride mg/1 .025 0,0206 83.2 65.5-128 WG729149 4-BromofIuorobenzene 95.40 71-126 WG729149 Dibromoflucromet.hane 99.10 78.3-121 WG729149 Toluene-d8 97.50 88.5-111 WG729149 a,a,a-Trifluorotoluene 96.80 85-114 WG729149 TPH - Oil & Grease mg/1 20 17.0 85.0 76-114 WG729422 Suspended Solids ng/1 773 609. 105, 85-115 WG729296 1,2,4-Trichlorobenzene mg/1 .025 0,0114 45.7 22.9-96.1 WG729093 2,4,6-Trichlorophenol mg/1 .025 0.0156 62.5 29.8-107 WG729093 2,4-Dichlorophenol mg/l .025 0.0137 54.3 31.4-103 WG729093 2,4-Dimethylphenol mg/1 .025 0.0149 59.6 31.9-107 WG729093 2,4-Dinitrophenol mg/1 .025 0.0166 66.6 24.2-128 WG729093 2,4-Dinitrotoluene mg/1 .025 0,0170 67.B 31.2-105 WG729093 2,6-Dinitrotoluene mg/1 .023 0,0167 66.n 30.6-106 WG729093 2-Chlcronaphthalene mg/1 .025 0.0157 62,7 33.6-105 WG729093 2-Chlorcphenol mg/1 .025 0.0137 54.6 26.2-91.5 WG729093 2-Hitrophenol mg/1 .025 0.0153 61.4 25.9-706 WG729093 3,3-Dichlorobenzidine mg/l .025 0.0160 63.9 27.2-142 WG729093 4,6-Dinitro-2-methylphenol mg/l .025 0.0159 63.6 18.4-148 WG729093 4-Brorncphenyl-phenylether mg/l .025 0.0153 611.3 40.7-116 WG729093 4-Ch2oro-3-mel}ry1phernol mg/1 .025 0.0152 60.6 35.7-100 WG729093 4-Chlorophenyl-phenylether mg/1 .025 0.0172 68.6 39-113 WG729093 4-Ni tz'oplienol mg/1 .025 0.00741 29.6 10-52.7 WG729093 Acenanhthene mg/1 .025 0.0158 63.0 38.7-109 WG729093 Acenaphthylene mg/1 .025 0.0153 61.3 36-106 WG729093 Anthracene mg/1 .025 0.0149 59.5 43.6-113 WG729093 1,2-Di phenyl hydrazine ma/1 .025 0.0181 72.6 37.6--211 WG729093 Benzidine mg/1 .025 0.0146 58.2 10-165.2 WG729093 Benzo(a)anthracene mg/1 .025 0.0154 61.6 51.2-112 WG729093 Benzolalpyrene mg/1 .025 0.0137 54.9 45.6-106 WG729093 Benzo(b)fluoranthene MU/1 .025 0.0156 62.3 47.6-111 WG729093 Benzo(g,h,i)perylene ma/1 .025 0.0162 64.6 45.2-117 WG729D93 Benzo(k)fluoranthene mg/1 .025 0.0156 62.6 49.4-114 WG729093 Benzylbutyl phthalate mg/1 .025 0.0155 62.0 31.8-123 WG729093 Sis(2-chlorethoxy)methane mg/1 .025 0.0127 51.0 37.2-111 WG729093 Bis(2-chloroethyl)ether mg/1 .025 0.0116 46.3 22.6-108 WG729093 Bis(2-chloroisopropyl)ether mg/1 .025 0.0133 53.1 32.9-100 WG729093 Bis(2-ethylhexyl)nhthalate mg/l .025 0.0159 63.5 36.9-134 WG729093 Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Ana lytes with QC Qualifiers.' Page 15 of 22 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 75B-5858 1-800-767-5859 OESC Fax (615) 758-5859 L,A•H 5•C•f• E•N• GE•S Tax I.D. 62-0814289 Est. 1910 Eaton Corporation Katie Hclbroo}: 2564 Durham Road Quality Assurance Report Level II Roxboro, NC 27573 July 07, 2014 L707275 Laboratory Control Sample Analyte Units Known Val Result Rec Limit Batch Chrysane mg/1 .025 0,0159 63.8 54.6-120 WG729093 Di-n-butyl phthalate mg/1 .025 0.0155 62.2 41.8-120 WG729093 Di-n-octyl phthalate ma/1 .025 0.0156 62.3 39.7-112 WG729093 Dibenz(a,hlanthracene mg/1 .025 0.0162 64.7 42.8-118 WG729093 Diethyl phthalate mu/1 .025 0.0164 65.8 36.5-129 WG729093 Dimethyl phthalate m(J/l .025 0.0171 68.4 35.3-128 WG729093 Fluoranthene mg/1 .025 0.0152 60.9 45.9-115 WG729093 Fltic! ene mg/l .025 0.3164 65.7 41-112 WG729093 Hexachloxo-i,3-butadiene mg/1 .025 0.0109 43.5 16.1-104 WG729093 Hexachlorobenzene mg/1 .025 0.0146 58.5 38.5-116 WS729093 Hexachlorocyclopentadiene mg/1 .025 0.00762 30.5 10-121 WG729093 Hexachloroethane ma/1 .025 0.00963 3B.5 16.5-89.8 WG729092 Indencf1,2,3-cd)pyrene mg/1 .025 0.0166 66.5 45-116 WG729093 Isophorone mg/l .025 0.0154 61.4 35.4-112 WG729053 n-Nitrosodi-n-propylamine mg/1 .025 0.0146 58.5 33.2-106 WG729093 n-Nitrosodimethylamine mg/1 .025 0.00904 36.2 10-80.1 WG729093 n-Nitrosodiphenylamine mg/1 .025 0.0169 67.7 44.4-113 WG729093 Naphthalene mg/1 .025 0.0131 52.6 32.2-101 WG729093 Nitrobenzene mg/1 .025 0.0144 57.5 31.4-106 WG729095 Pentachlor.ophenol mg/1 .025 0,0131 52.5 10-97.4 WG729093 Phenanthrene mg/1 .025 0,0149 59.7 46.4-113 WG729093 Phenol mg/1 .025 0.00873 34.9 10-57.9 WG729093 Pyrene mg/1 .025 0.0159 63.5 46.3-117 WG729095 2,4,6-Tribromopheno). 62.20 11.2-130 wG729093 2-Fluorobiphenyl 66.40 29.5-131 WG729093 2-Fluorophenol 46.G0 10-77.9 WG729093 Nitrobenzene-d5 54.40 21.8-123 WG729093 Phenol-d5 30.60 5-70.1 WG729093 p-Terphenyl-d]4 60.50 29.3-137 WG729093 Copper mg/1 1 1.01 101. 85-113 WG729742 Zinc mg/1 1 1.01 101. 85-115 WG729742 PCB 1016 mg/1 .0005 0.000401 B0.3 24.7-128 WG729545 PCB 1260 my/1 .0005 0.000363 72.6 47.7-149 WG729545 Decachlorobiphenyl 67,20 10-156 WG729545 Tetrachloro-m-xylene 85.20 13.9-137 WG729545 Lead ma/I 1 1.12 112. 85-115 WG730173 4,4-DDD mg/1 .0002 0.000177 88.3 47.6-144 WG729545 4,4-DDE mg/i .0002 0.000175 87.3 45-124 WG729545 4,4-DDT mg/I .0002 0.000188 93.9 49.8-130 WG729545 A.16rin mg/1 .0002 0.000179 89.7 10-120 WG729545 Alpha BHC mg/l .0002 0.000173 86.7 53.6-125 WG729545 Beta BHC mg/1 .0002 0.000199 99.7 55.8-130 WC729545 Delta BHC rria/l .0002 0.000176 R7.9 42.2-135 WG729545 Dieldrin ma/1 .0002 0.000187 93.4 55-127 WG729545 Endosulfan I mg/i .0002 0.000192 95.9 54.7-127 WG729545 Endosulfan I1 trig/l .0002 0.000200 100. 53.1-135 WG729545 Endosulfan sulfate me/1 .0002 0.000192 95.8 51.5-132 WG729545 Endrin mg/l .0002 0.000192 96.0 50.1-131 WG729545 Endrin aldehyde mg/1 .0002 0.000180 90.0 39.5-137 WG729545 Endrin ketone ma/1 .0002 0.000189 94.4 53.5-139 WG729545 Gamma BHC ma/1 .0002 0.000172 86.2 54.7-125 WG729545 Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analyzes with 4C Qualifiers.' Page 16 of 22 JOESC L•A•9 5•C.1•E•N•C•E•5 Eaton Corporation Katie Holbrook. 2564 Durham Road Roxboro, NC 27573 Quality Assurance Report Level II L707275 12065 Lebanon R6. Mt. Juliet, TN 37122 (615) 758-5856 1-600-767-5859 Fax (615) 758-5859 Tax l.D. 62-0814289 Est. 1970 July 07, 2014 Analyte Units Laboratory Known Val Control Sample Result 4 Rec Limit Batch Heptachlor mg/i .0002 0.000193 96.5 20.7-127 WG729545 Heptachlor epoxide mg/1 .0002 0.000187 93.4 56.4-124 WG729545 Hexachlorobenzene my/1 .1002 0.000180 90.0 26.7-114 WG729545 Methoxychlor mg/1 .0002 0.000219 110. 48.2-144 WG729545 Decachlorobiphenyl 86.3C 10-156 WG729545 Tetrachloro-m-xvlene 93.30 13.9-137 WG729545 Analyte Units Laboratory Result Control Ref Sample Duplicate %Rec Limit RPD Limit Batch 1,1,1-1'richloroethane mg/1 0.0250 0.0250 300. 73.2-121 0,130 20 WG729149 3, 1, 2, 2-Tetrachlorcethane mg/l 0.0274 0.0291 110. 70.7-122 8.16 20 WG729149 1,1,2-Trichloroethane mg/1 0.0259 0.0271 304, 77.1-118 4.45 20 WG729149 1,1-Dichloroethane mg/l 0.0248 0.0241 99.0 70.7-126 0,260 20 WG729149 1,1-Di chIoroe tliene mg/1 0.0222 0.0222 89.0 67.8-129 D.320 20 WG729149 I,2-DichIarobeRzene ` mg/1 0.0255 0.0264 102. 78.4-117 3.40 20 WG729149 1,2-Dichloroethane mg/l 0,0227 0.0229 91.0 68.8-124 1.02 20 WG729149 1,2-Dichloropropane mg/1 0.0247 0.0243 99.0 7G.5-119 1.43 20 WG729149 1,3-Dichlorobenzene ma/1 0.0256 0.0268 102. 70.8-128 4.76 20 WG729149 1,4-Dichlorobenzene mg/l 0.0247 0.0254 99.0 78.8-115 2.47 20 WG729149 2-Ch2orcethyl vinyl ether mg/1 0.113 0.115 90.0 47.8-150 2,01 20 WG729149 Acrolein mg/1 0.135 0.140 108. 10-190 3.10 28.1 WG729149 Acrylonitrile mg/l D.124 0.129 99.0 55.2-130 4.04 20 WG729149 Benzene mg/1 0.0251 0.0251 100. 74.E-121 0.250 20 WG729149 Brcmodichloromethane mg/1 0,0249 0.0247 99.0 75.1-116 0,510 20 WG729149 Promoform mg/1 0.0266 0.0287 106, 67.5-130 7.59 20 WG729149 Bromomethane mg/l 0.022) 0.0219 88.0 49.9-162 0.590 20 WG729149 Carbon tetrachloride mg/1 0.0277 0.0274 Ill, 70.2-123 1.22 20 WG729149 Chlcrobenzerie mg/1 0.0251 0.0260 100. 78.1-119 3.47 20 WG725149 Chlorodib:omomethane mg/1 0.0259 0.0266 104. 74-12I 2,36 20 WG729149 Chloroetiiane mg/l 0,0202 0.0207 80.0 61.7-135 2.58 20 WG729149 Chloroform mg/l 0.0251 0.0250 100. 76-121 0.190 20 WG729149 Chloromethane mg/l 0.0219 0.0221 68.0 61.5-129 0.820 20 WG729149 cis-1,3-Dichloropr.opene mg/l C.0257 0.0258 103, 78.2-120 0.260 20 WG729149 Dichlorodifluoromethane mg/1 0.0231 0.0232 92.0 54.8-135 0.650 20 WG729149 Ethylhenzene mg/l 0,0252 0.0262 101. 78.8-122 3,73 20 WG729149 Methylene Chloride mg/l 0.0254 0.0251 101. 70. -120 1.19 20 WG729149 TetrachloroeLhene rng/l 0.0249 0.0260 100. 72.6-126 4.54 20 WG729119 Toluene mg/1 0.0254 0.0250 102. 79.7-1I6 1.66 20 WG729149 trans-1,2-Dichloroethene mg/1 0,0263 0.0264 105. 72.6-121 0.230 20 WG729149 trans-1,3-Dichloropropene mg/1 0.0271 0.0266 100. 74.3-123 1.94 20 WG729149 Trichloroethene mg/1 0.0262 0.0257 105, 77.1-118 1.87 20 WG729i49 Trich2orofluoromethane ma/1 0.0244 0.0239 98.0 63.5-135 2.23 20 WG729149 Vinyl chloride mg/1 0.0209 0,0206 84.0 65.9-128 0.340 20 WG729149 4-Bromofluorobenzene 94.50 71-I26 WG729149 Dibromofluorcmethane 99.40 78.3-121 WG729149 Toluene-d8 99.90 88.5-111 WG729149 a,a,a-Trifluorotoluene 700.0 85-1i4 WG729149 TPH - Dil h Grease mg/1 18.2 17.0 91.0 78-114 6.82 18 WG729422 Suspended Solids my/1 836. 808. 108. 85-215 3.41 5 WG729296 1,2,4-Trichlorobenzene mg/l 0.00890 0.0114 36.0 22.9-96.1 24.9 27.5 WG729093 2,4,6-Trichlorophenol mg/1 0.0154 0.0156 G2.0 29.E-107 1.33 24.1 WG729093 2,4-Dichlorophenol mg/1 0.0122 0.0137 49.0 31.4-103 11.2 24.9 WG729093 • Performance or this Analyte is outside of established criteria. For addiLional information, please see Attachment A 'List of AnalyLes With QC Cualifiers.' Page 17 of 22 12065 Lebanon Rd, ML. Juliet, TN 37122 t615) 758-5858 1-800-761-5859 OESC Fax (615) 75B-5859 L•AB 5•C•4•E•N•G•E•5 Tax I.D. 62-0E14289 Est. 1970 Eaton Corocration Katie Holbrook 2564 Durham Road Quality Assurance Reoert Level Ii Roxboro, NC 27573 July 07, 2014 L707275 Laboratory Control Sample Duplicate Analyte units Result Ref BRec LimiL RPD Limit Batch 2,4-Dimethylphenol mg/1 0.0131 0. 014 9 52.0 31.9-107 12.8 25.7 WG729093 2,4-Dinitfophenol mg/1 0.0140 0.0166 56.0 24.2-128 17.1 20.5 WG729093 2,4-Dinitrotoluene mg/1 0.0147 0.0170 59.0 32.2-105 14.4 22 WG729093 2,6-Dinitrotoluene mg/1 0.0138 0,0167 55.0 30.6-106 19.3 23.1 WG729093 2-Chlcronaphthalene mo/I 0.0127 0.0157 51.0 33.6-105 20.6 23 WG729093 2-Chlorcphenol mg/1 0.D121 0.0137 48.0 26.2-91.5 11.9 26.5 WG729093 2-Nitrophenol mg/1 0.0124 0.0153 50.0 25.9-106 20.8 26.9 WG729093 3,3-Dichlorobenzidine mg/1 0.0142 0.Di60 57.0 27.2-142 11.5 22.3 WG729093 4,6-Dinitro-2-methylphenol mg/1 0.0165 0.0159 66.0 18.4-148 3.63 24.4 WG729093 4-Bromophenyl-phenyl etiier mg/l 0.0139 0,0153 56.0 40.7-116 9.89 21 WG72SO93 4-Chloro-3-methylphenol ma/l 0.0114 0.0152 58.0 35.7-10D 4.94 22.9 WG729093 4-Ch2orcphenyl-phenylether mg/1 0.0145 0.0172 58.0 39-113 16.8 20.9 WG729093 4-Nitrophenol mg/1 0.00681 0.00741 27.0 10-52.7 8.47 40 WG729093 AcenaphChene nig/l 0.0139 0.0158 56.0 38.7-109 12.6 21.5 WG729093 Acenaphthylene mg/1 0.0136 0,0153 55.0 36-106 10.4 21 WG729093 AnLhracene mg/1 0,0143 0.0149 57.0 43.6-113 4,22 1B.9 WG729093 1,2-Dipheny1hydrazine ma/l 0.0163 0.0181 65.0 37.6-111 10.E 21.1 WG729093 Benzidine mg/1 0.0140 0.0146 56.0 10-165.2 3.98 40 WG729093 Benzo(a)anthracene mg/1 0,0140 0.D154 56.0 51.2-112 9.31 20 WG729093 Benzo(a)pyrene mg/1 0.0128 0.0137 51.0 45.6-206 6.63 20 WG729093 Benzo(b)fluoranthene mg/1 0.0140 0.015G 56.0 47.6-111 10.7 20 WG729C93 Benzo(g,h,i)perylene mg/l 0.0139 0.0162 56.0 45.2-117 15.0 20 WG729093 Benzo M fluoranthene mg/l 0.0144 0,0156 57.0 49.4-114 8.47 20 WG729093 Senzylbutyl phthalate mg/1 0.0146 0.0155 58.0 31.9-123 6.04 20.7 WG729093 Bis(2-chlorethoxy)methane mg/1 0.0110 0.0127 44.0 37.2-111 19.9 24.1 WG729093 13is(2-chlorcethyl)ether ❑ig/l 0.0104 0,0116 42.0 22.G-108 10.7 27.9 WG729093 Sis(2-chloroisopropyl)ether mg/1 0.0120 0,0133 43.0 32.9-100 9,71 25.1 WG729093 8is(2-ethylhexyl}phthaIate mg/1 0.0154 0.0159 61.0 36.9-134 3.35 23.6 WG729093 Chrysene mg/1 0.0147 0.0159 59.0 54.6-12D 8.OE 20 WG729093 Di-n-butyl phthalate mg/1 0.0140 0.0155 56.0 41.8-120 10.8 20.2 WG729093 Di-n-octyl phthalate mg/1 0.0149 0.0156 60.0 39.7-112 4.26 21.1 WG729093 Dibenz(a,h)antliracene my/1 0.0138 0.0162 55.0 42.E-118 16.0 20 WGIZ9093 Diethyl phthalate mg/1 0.0154 0.0164 62.0 36.5-129 6.46 20 WG729093 Dimethyl phthalate mg/1 0.01513 0.0171 62.0 35.3-128 9.09 20.8 WG729093 Fluoranthene mg/1 0.0133 0.0152 53.D 45.9-115 13.6 20 WG729093 Fluorene mg/1 0.0142 0.0164 57.0 41-112 14.6 20.2 WG729093 Hexachloro-2,3-butadiene mg/1 0.00797 0.0109 32.0 16.1-104 30.9 31.2 WG729093 Hexachlorobenzene mg/1 0,0135 0.0146 54.0 3E.5-116 8.29 20.1 WG729093 Hexachlorocyclopentadiene mg/l 0.00637 0.00762 25.0 10-121 18.0 27.9 WG729093 Hexachloroethane mg/1 0.00788 0.00963 32.0 16.5-89.8 20.1 30.7 WG729093 Indeno(1,2,3-cd)pyrene mg/1 0.0143 0.0166 57.0 45-116 14.7 20 WG729093 Isophorone my/1 0.0138 0.0154 55.0 35.4-I12 10.4 21.5 WG729093 n-Nitrosodi-n-propylamine mg/1 0.0120 0.0146 48.0 33.2-106 20.1 23.7 WG729093 n-NiLrosodimethylamine mg/1 0100768 0.00904 31.0 10-80.1 16.4 37.5 WG729093 n-Nitrosodiphenylamine mg/1 0.0152 0.0169 61.0 41.4-113 1D•5 20 WG729093 Naphthalene mg/1 C.0106 0.0131 42.0 32.2-101 21.1 23.8 WG729093 Nitrobenzene me/1 0.0124 0.0144 49.0 31.4-106 15.1 25.7 KG729093 Pentachlorophenol mg/1 0.0120 0.0131 48.0 10-97.4 8.87 35.i WG724093 Phenanthrene mg/1 0.0137 0,0149 55.0 46.4-113 6.22 20 WC729093 Phenol nig/1 0.00767 0,00873 31.0 10-57.9 13.0 35 WG729093 Pyrene ma/l 0.0197 0.0159 59.0 46.3-117 7.88 20 WG729093 2,4,6-Tribromophencl 59.20 11.2-130 WG729093 2-Fluorobiphenyl 58.20 29.5-131 WG729093 2-Fluoropnenol 40.60 10-77.9 WG729093 Nitrobenzene-d5 44,00 21.8-123 WG729093 Phenol-d5 30.00 5-70.1 WG729093 p-Terphenyl-d14 57.80 29.3-137 WG725093 Performance of this Analyte is ouLside of established criteria. For additional information, please see Attachment A 'List of Analytes with nC Qualifiers.' Pace 19 of 22 OESC I Eaton Corporation Katie Holbrook 2564 Durham Road Roxboro, NC 27573 nuality Assurance Report bevel lI L707275 12065 Lebanon Rd. Mt, Juliet, TN 37122 (615) 756-5858 1-800-7G7-5859 Fax (615) 756-5859 Tax. I.D. 62-0814289 Est. 1970 July 07, 2014 Laboratory Control Sample Duplicate Analyze Units Result Ref %Rec Li- ITIit RFD Limit Batcli Copper mg/l 1.00 1.01 100. 85-115 0.0 20 WG729742 Zinc mg/l 1.01 1.01 101. 85-'.15 0.0 20 WG729742 PCB 1016 mg/1 0.D00366 0.000401 73.0 24.7-128 9.20 34.9 WG729545 PCB 1260 mg/l 0.000401 0.DC0363 8D.0 47.7-149 9.99 28.E WG729545 Dec5chlorabipheny1 63.10 10-156 WG729545 Tetrachloro-m-xylene 76.40 13.9-137 WG729545 Lead ma/1 1.10 1.12 110. 85-115 2.CC 20 WG730173 4,4-DDD ma/1 0,000166 0.000177 83.0 43.6-144 6.31 24.3 WG729545 4,4-DDE mg/l 0.000160 0.000175 80.0 45-124 8.93 25.7 WG729545 4,4-DDT mg/1 0.000167 0.000186 83.0 49.8-130 11.9 25.4 WG729545 Aldrin mg/1 0,000159 0,000179 80.0 10-120 11.9 33.9 WG729545 Alpha BHC mg/l 0.DOU153 0.000173 76.0 53.6-125 12.7 22.3 WG729545 Beta BHC mg/l 0.000179 0.000I99 89.0 55.R-130 10.8 20.6 WG729545 Delta BHC ma/1 0.000156 0.000176 78.0 42.2-135 12.0 23.3 wG729545 Dieldrin 1110/1 0,000170 0.000187 85.0 55-127 9.37 22.9 WG729545 Endosulfan 1 mg/1 0.000173 0.000192 86.0 54.7-127 10.5 24.3 WG729545 Endosulfan II ma/1 0.000274 D.000200 87.0 53.1-135 13.9 23.5 WG729545 Endosulfan sulfate mq/1 0.000173 0.000192 86.0 51.5-132 10.3 26.3 WG729545 Endrin mg/1 0.000177 0.000192 88.0 50.1-131 8.20 29.1 WG729545 Endrin aldehyde mg/l 0.000277 0.000180 88.0 39.5-137 1.7E 28.4 WG729545 Endrin ketone mg/l 0.000i71 0.000169 86.0 53.5-139 9.71 28.4 WG729545 Gamma BHC mg/l 0.000154 0.000172 77.0 54.7-125 10.9 21.1 WG729545 Heptachlor mg/l D.000IG8 0.000193 84.0 20.7-127 13.5 30.5 WG729545 Heptachlor epoxide mg/l 0,000272 D.000187 86.0 56.4-124 8.46 23.1 WG729545 Hexar_hlorcbenzerie mg/l 0.000159 0.000160 80.0 26.7-114 12.2 27.6 WG729545 Methoxychlor nia/l 0.000205 0.000219 102, 48.2-144 6.92 27.8 WG729545 Decachlorobiphenyl 77.40 10-156 WG729545 Tetrachloro-m-xylene 77.90 13.9-137 WG729545 Anal to Units MS Res Matrix Spike Ref Res TV 9 Rec Limit Ref Samo Batch 1,1,1-Trichloroethane mg/l 0,0264 0.0 .025 110, 58.7-134 L706786-01 WG729149 1,1,2,2-Tetrachloroethane mg/1 0.0294 0.0 .025 120. 56-132 L706786-01 WG729145 1,1,2-Trichloroethane mg/l 0.0211 0.0 .025 110. 66.3-125 L706786-01 WG729149 1,1-Dichloroethane mg/l 0.0263 0.0 .025 100. 58.5-132 L706786-01 WG729149 1,1-Dichloroethene mg/l 0,0240 0.000802 .C25 93.0 51.1-140 L706786-01 WC729149 1,2-Dichlorobenzene mg/l 0.0272 0.0 .C25 110. 68.2-123 L706786-01 wG729149 1,2-Dichleroethane mg/l 0.0237 0.0 .025 95.0 60-126 1,706786-01 WG729149 1,2-M chloroprcpane mg/l 0.0248 0.0 .025 99.0 64.2-123 L706786-01 WG729149 1,3-Dichlorobenzene mg/1 0,0275 0.0 .025 110. 63.1-131 L706786-01 WG729149 1,4-Dichlorobenzene mg/l 0.0266 0.0 .025 110, 68.6-123 L706786-01 WG729149 2-Chlorcethyl vinyl ether mg/l 0.119 0.0 .125 95.0 10-155 L7067E6-01 WG729149 Acrolein nig/I 0.149 0.0 .125 120. 10-200 1,706786-01 WG729149 Acrylonitrile mg/l 0.139 0.0 .125 110. 49.4-133 L706786-01 WG729149 Benzene mg/1 0.0262 0.0 .025 100. 54.3-133 L706796-01 WG729149 Bromodichlor.omethane mg/l 0.0252 0.0 .025 100. 63.9-121 L7D6786-01 WG729149 Bromoform mg/1 0.0283 0.0 .025 116. 59.5-134 L706786-01 WG729149 Brcmcmethane mg/l C.0233 0.0 .025 93.0 41.7-155 L706786-01 WG729149 Carbon tetrachloride mg/l 0.0295 0.0 .025 120, 55.7-134 L706786-01 W0729149 Chlorobenzene mg/1 0,0271 0.0 .025 i10. 67-125 L706786-01 WG729149 Chlorodibromomethane nig/I 0.0270 0.0 .025 110. 64.3-125 L706786-01 WG729149 Chloroethane mg/1 0.0217 0.0 .025 87.0 51.5-136 L706786-01 WG729149 Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 19 of 22 12065 Lebanon Rd, Mt. Juliet, TN 37122 (615) 756-585B 1-800-767-5859 OESC Fax (615) 758-5859 L-A-6 S-C•I•E-N,C E-S Tax S.D. 62-0814289 Est. 1970 Eaton Corporation Katie Holbrook 2564 Durham Road Quality Assurance Report Level II Roxboro, NC 27573 July 07, 2014 1.707275 Matrix Spike Analyte Units N,S Res Ref Res TV % Rec Limit Ref Samo Batch Chloroform ma/l 0.0262 0.0 .025 100. 63-129 L706786-01 WG729149 Chloromethane ma/1 O.D230 0.0 .025 92.0 42.4-135 L106796-01 WG729149 cis-1,3-Dichloropropene m9/1 0,0263 0.0 .025 100. 66.4-125 1,706786-01 WG729149 Dichlorodifluoromethane ma/1 0.0254 0.000576 .025 99.0 40.6-144 L706786-01 WG729149 Ethylbenzene ma/1 0.0269 0.0 .025 110. 61.4-133 L706786-01 WG729149 Methylene Chloride ttia/1 0.0265 0.D .025 110. 58.1-122 L706786-01 WG729149 Tetrachloroethene mg/l 0.0267 0.0 .025 110. 53-139 L7067EG-01 WG729149 Toluene 1110/1 0.0258 0.0 .025 i00. 61,4-130 L706786-01 WG729149 trans-1,2-Dichloroethene m0/1 0.0279 0.0 .025 110. 56.5-129 L106786-01 WG729149 trans-1,3-Dichloropropene mg/1 0.0269 0.0 .025 110. 64.1-128 1706786-01 WS729149 Trichloroethene mq/1 0.0357 0.00969 .025 100. 44.1-149 L706786-01 WG729149 Trichlorofluoromethane nig/1 0.0258 0.0 .025 100. 49.6-145 L706766-01 WG729249 Vinyl chloride mg/1 0.0225 0.0 .025 50.0 47.8-137 1,706786-01 WG729149 4-Bromofluorobenzene 93.50 71-126 WG729149 DibromofIuoromethane 97.60 78.1-121 WG729249 Toluene-d8 96.50 88.5-122 WG729149 a,a,a-Trifluorotoluene 97.70 85-114 WG729149 Lead mq/1 1.09 0.000848 1 110. 75-125 L707942-01 WG730173 Matrix Spike Duplicate Analyte Units MSD Ref %Rec Limit RPD Limit Ref Samo Batch 1,1,1-Trichloroethene mg/1 0.0269 0.0264 108. 58.7-134 1.87 20 L706786-01 WG729145 1,1,2,2-Tetrachloroethane mg/l 0.0306 0.0294 122. 56-132 4.23 22.2 L706786-01 WC729149 1,1,2-Trichloroethane mg/l 0.0273 0.0271 109. 66.3-125 0.540 20 L706786-01 WG729149 l,l-Dichloroethane mg/1 0.0266 0.0263 106. 58.5-132 1.06 20 L706786-01 WG729149 ],I-Dichloroethene my/1 0,0247 0.0240 95.6 51.1-140 2.85 20.2 1,706786-01 WG129149 1,2-Dichlorobenzene mg/1 0.0274 0.0272 110. 68.2-123 0,840 20 L706786-01 WG729149 1,2-Dichloroethane mg/f 0.0243 0.0237 97.1 60-126 2.19 20 L70678b-01 WG729149 1,2-❑iChloropropane mg/1 0.0249 0.0248 99.7 64.2-123 0.350 20 L706786-01 WG729149 1,3-Dichlorobenzene mg/1 0.0270 0.0275 106. 63.1-131 1.70 20 L706786-01 WG729149 1,4-Dichlorobenzene mg/l 0.0266 0.0266 106. GB.6-123 0.270 20 L7C6786-01 WG729149 2-Chloroethyl vinyl ether mg/1 0.122 0.119 97.3 10-155 2.29 20 L706786-01 WG729149 Acrolein 1110/1 0.159 0,149 127, 10-20D 6.51 27,7 L706786-01 WG729149 AcryloniLrile m0/1 0.149 0.139 119. 49.4-133 6.59 25.3 L706796-01 WG729149 Benzene mg/1 0.0268 0.026-1 I07. 54.3-133 2.37 20 L706786-01 WG729149 Bromodichloremethane mq/1 0.0258 0.D252 103. 63.9-121 2.19 2D L7067B6-01 WG729149 Bromoform mg/1 0,0294 0.0283 118, 59.5-134 3,93 20.5 L706766-01 WG729149 Bromomethane mg/l 0.0240 0.0233 93.8 41.7-155 2.71 21.9 L706786-01 WG729149 Carbon tetrachloride mg/1 0.0302 0.0295 121. 55.7-134 2.41 20 L706766-01 WG729149 Chlorohenzene mg/1 M269 0.0271 I09. 67-125 0.660 20 1,7D6786-01 WG729149 Chlorodibromomethane mg/1 0.0271 0.0270 108. 64.3-125 0.240 20.8 L706786-01 WG729149 Chloroeihane mg/l 0.0222 0.0217 38.8 51.5-136 2.13 40 i,706786-oi WG729149 Chloroform mg/1 0.0265 0.0262 106. 63-129 1.27 20 L706786-01 WG729149 Chloromethane mg/l 0.0241 0.0230 96.3 42.4-135 4.37 20 L70678G-01 WG729149 cis-1,3-Dichloropropene mg/1 0.0265 0.0263 106. 66.4-125 0.650 20 L706786-01 WG729I49 Dichlorodifluoromethane mg/1 0,0255 0.0254 99.6 40.6-144 0.350 20.2 L706786-01 WG729149 Ethylbenzene ma/1 0.0269 0.0269 108. 61.4-133 0.140 20 L706786-01 WG729149 Methylene Chloride mg/1 0,0272 0.0265 109. 58.1-122 2.68 20 L706786-01 WG729149 Tetrachloroethene mg/l 0.0273 0.0267 109. 53-139 2.22 20 L706786-01 WG729149 Toluene mg/1 0.0263 0.0258 105. 61.4-130 I.B5 20 L706786-Oi WG729149 trans-2,2-Dichloroethene mg/l 0.0281 0.0279 112. 56.5-129 0.660 20 L706786-01 WG729149 trans-I,3-Dichloropropene mg/l 0.0281 0.0269 112. 64.1-128 4.27 20 L706786-01 WG729149 Trichloroethene mg/1 0.0364 D.0357 107. 44.1-149 1.80 20 L706786-01 WG729149 Trichlorofluoromethane mg/1 0.0266 0.0258 107. 49.6-145 3.66 21.2 1,706786-01 WG729149 Vinyl chloride mg/1 0.0228 0.0225 91.1 47.6-137 1.25 20 L706786-01 WG729149 4-Bromofluorobenzene 95.10 71-126 WG729149 ' Performance of this Analyte is outside of established criteria. For additional information, olease see Attachment A 'List of Analytes With QC Qualifiers.' Page 20 of 22 *ESC I Eaton Corporation Katie Holbrook 2564 Durham Road Roxboro, NC 27573 Quality Assurance Report Level II L707275 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5B58 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 July 07, 2014 Matrix Spike Duplicate Asia lyte Units MSD Ref BRec Limit RPD Limit Ref Samp Patch Dibromofluorometharje 101.0 78.3-121 Toluene-d8 99.00 88.5-ill a,a,a-Tr'flucrotoluene 98.40 85-114 Lead ma/l 1.10 1.09 110. 75-125 1.00 20 L707942-01 WG730173 Post Spike Serial Dilution Ratch number /Run number / Sample number cross reference wG129149: R2951472: L707275-01 02 WG729422: R2952266: I,707215-01 02 WG729296: R2952411: L707275-01 02 WG729093: R2952529: L707275-0] 02 wG729742: R2954825 R2954931: L707275-01 02 wG729545: R295512B R2956545: L707275-01 02 WGI30173: R2956186 R2956667: L707275-01 02 Calculations are performed prior to rounding of reported values. Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with N (qualifiers. Page 21 of 22 Eaton Corporation Katie Holbrook 2564 Durham Road Roxboro, NC 27573 12065 Lebanon Rd, Mt. Juliet, TN 37122 (615) 756-585B 1-800-767-5859 Fax (6151 756-5859 Tax I.D. 62-0814289 Est. 19'10 Quality Assuzance Report Level 71 L707275 The data package includes a summary of the analytic results of the quality control samples required by the SW-846 or CWA methods. The quality control samples include a method blank, a laboratory control sample, and the matri-•- spike/matrix spike duplicate analysis. If a target parameter is outside the method limits, every sample that is effected is flagged with the appropriate qualifier in Appendix: B of the analytic report. Metaled Blank - an aliquot of reagent water carried through the entire analytic process. The method blank results indicate if any possible contamination exposure during the sample handling, digestion or extraction process, and analysis. Concentrations Of target analytes above the reporting limit in the method blank az'e qualified with tiie "E" qualifier. Laboratory Control Sample - is a sample of known concentration that is carried through the digestion/extraction and analysis process. The percent recovery, (}:pressed as a percentage of the theoretical concentration, has statistical control limits indicating that the analytic process is "in control". If a target analyte is outside the control limits for the laboratory control sample or any other control sample, the parameter is .lagged with a "J4" qualifier for all effected samples. Matrix Spi,:e and Matrix Spike Duplicate - is two aliquots of an environmental sample that is spired with known concentrations of target analytes. The percent recovery of the target analytes also has statistical control limits. if any recoveries that are outside the method control limits, the sample that was selected ibr matrix spike/matrix spike duplicate analysis is flagged with either a "J5" or a "J611. The relative percent difference (%RPD) between the matrix spike and the matrix spike duplicate recoveries is all calculated. If the RPD is above the method limit, the effected samples are flagged with a "J3" qualifier. Page 22 of 22 July 07, 2014 STORMWATER POLLUTION PREVENTION PLAN E:7•N Powering Business Worldwide Roxboro Manufacturing Facility Stormwater Pollution Prevention Plan (SWPPP) MESH 3.0 — Stormwater Management 1/01/2014 REVISION Table of Contents 1.0 Facility Information...............................................................................................................................1 2.0 Stormwater Pollution Prevention Team...............................................................................................1 3.0 Facility Description...............................................................................................................................2 4.0 Site Map............................................................................................................................................... 3 5.0 Description of Potential Pollutant Sources and Applicable Control Measures....................................4 6.0 Measures and Controls......................................................................................................................11 6.1 Minimize Exposure...........................................................................................I.......................11 6.2 Good Housekeeping.................................................................................................................11 6.3 Preventive Maintenance...........................................................................................................11 6A Spill Prevention and Response Procedure..............................................................................11 6.5 Employee Training...................................................................................................................12 6.6 Erosion and Sediment Controls...............................................................................................13 6.7 Management of Run-on and Runoff.........................................................................................13 7.0 Prohibited Activities. ................................................................................................................... ....... 13 8.0 Allowable Discharges.........................................................................................................................13 9.0 Documentation of Permit Eligibility Related to the 303(d) List of Impaired Water Bodies.................14 10.0 Identification and Elimination of Illicit Discharges..............................................................................14 11.0 Inspections, Evaluations, Monitoring, Reporting, Corrective Action and Recordkeeping .................15 11.1 Qualitative Monitoring..................................................................................................... .........15 11.2 Analytical Monitoring................................................................................................................15 11.3 Reporting Requirements........................................................................ .................... ..............16 12.0 SWPPP Certification..........................................................................................................................17 Figure 1. Topographic Map Figure 2. Site Map FIGURES (following text) ATTACHMENTS (following figures) Attachment 1. Training Logs Attachment 2. Blank Forms Attachment 3. Completed Qualitative Monitoring Forms Attachment 4. Completed Analytical Monitoring Forms Em,.ToN Powering Business Worldwide 1.0 Facility Information Roxboro MESH Document 3.0 Water Management Stormwater Pollution Prevention Plan (SWPPP) This document establishes a Stormwater Pollution Prevention Plan (SWPPP) for Eaton Corporation's manufacturing facility located at 2564 Durham Road (US 501 South), Roxboro, Person County, North Carolina. Maintenance of a SWPPP to manage Stormwater discharges is required by North Carolina Stormwater Industrial General Permit (IGP) No. NCG030000 for establishments engaged in Metal Fabrication, and the North Carolina General Statute 143-215.1. The facility's permit tracking number is NCG030027. The effective date of the current IGP is 11/01/2012, and the expiration date is 10/31/2017. The Standard Industrial Classification (SIC) code for the Roxboro facility is 3714, and the North American Industry Classification System (NAICS) code is 336312. The facility employs several hundred people and conducts the following operations related to the manufacture of motor vehicle parts and accessories: • Receipt and storage of raw materials • Heat treat • Metal machining and fabrication • Testing of finished product • Maintenance activities to support manufacturing operations • Packaging and storage of finished products • Shipping of finished products This document will be maintained at the facility and will be made available to the North Carolina Department of Environment and Natural Resources (NCDENR), or the City of Roxboro upon request. 2.0 Stormwater Pollution Prevention Team The pollution prevention team is the group of individuals responsible for developing and revising the facility's SWPPP; implementing and maintaining Best Management Practices (BMPs) and other control measures; training personnel in proper Stormwater management practices; conducting inspections and water quality sampling; and taking corrective actions where required. Each member of the stormwater pollution prevention team should have ready access to either an electronic or paper copy of the IGP and the SWPPP. Facility Manager The facility manager is responsible for overall operations at the facility and is responsible for reviewing and approving this SWPPP and providing the necessary human and financial resources required to execute the SWPPP. Name: Glenn McLean Office Phone: 336-503-6536 Environmental Health & Safety Manager The Environmental Health & Safety Manager is the primary emergency coordinator for the Roxboro facility. This individual is responsible for maintaining and deploying the facility's SWPPP and has full authority to make necessary decisions to ensure success of the plan. The 1 /01/2014 Page 1 of 19 FAI.T*N Powering Business Worldwide Roxboro MESH Document 3.0 Water Management Stormwater Pollution Prevention Plan (SWPPP) Environmental Health & Safety Manager is authorized to amend the plan and is authorized to halt any operation at the facility where there is a potential to violate any provision outlined in the plan. This person will maintain all records outlined in the SWPPP. Employees responding to spills or releases of materials that could result in stormwater pollution will work under the direction of the Environmental Health & Safety Manager. Name: Kim Witkowski Office Phone: 336-503-6538 Environmental Health & Safety Assistant The Environmental Health & Safety Assistant is the designated back-up person for the Environmental Health & Safety Manager in matters related to stormwater pollution prevention. This individual will assume SWPPP responsibilities assigned to the Environmental Health & Safety Manager in their absence. Name: Katie Holbrook Office Phone: 336-503-6449 Facility Engineer The Facility Engineer has responsibility for planning, design and implementation of manufacturing, maintenance and other processes and activities at the facility. As a pollution prevention team member, the Facility Engineer will help to ensure that stormwater is adequately protected during the conduct of facility operations. Name: Mike Riley Office Phone: 336-503-6631 3.o Facility Description Eaton Corporation's Roxboro facility consists of manufacturing operations housed in a roughly 300,000 square foot (sq ft) industrial building and several ancillary buildings. The facility is located on approximately 50 acres of land in the City of Roxboro, Person County, North Carolina. The facility is serviced by municipal water and sanitary sewer systems. The central portion of the property is situated on a relatively flat area, generally sloping to the west and south. Elevations of the property range between approximately 660 feet above sea level at the northern portions of the property, to about 640 feet above sea level to the south of the property. A topographic map showing the property location and surrounding areas is presented in Figure 1. Runoff from the east portion of the property, including the eastern portion of the building roof, drains south by both overland flow and on -site storm sewers to a stormwater detention pond located along the south-central property line. The detention pond outlets to a drainage ditch (Outfall #001) which empties into a southwest -flowing stream, eventually joining the North Flat River. Paved parking lots along the east portion of the facility flow south via overland flow and on -site storm sewers to a drainage ditch along the southeastern property line. This drainage is not associated with any industrial activities. 110 112o14 Page 2 of 19 F mT* N Powering Business Worldwide Roxboro MESH Document 3.0 Water Management Stormwater Pollution Prevention Plan (SWPPP) Surface water runoff from the southwest portion of the property is conveyed by overland flow to a south -flowing drainage ditch located just east of the asphalt drive at the southwest property corner. This ditch connects with a southwest -flowing stream, eventually joining the North Flat River. This drainage is not associated with any industrial activities. Surface water runoff from the southwest and west portion of the property is conveyed by overland flow to a south -flowing drainage ditch located along the west property line (Outfall #004). This ditch connects with a southwest -flowing stream, eventually joining the North Flat River. This drainage appears to be associated with industrial activities on the west side of the plant but steps are being made to modify the grading so that the drainage will not be associated with any industrial activities. After completion, this work will be documented in site records and Outfall #004 will be removed from the sampling locations. The northern portion of the property drains to the west via overland flow and on -site storm sewers to a ditch (Outfall #005) that flows west to an unnamed tributary of the North Flat River. The Flat River flows to Lake Michie, a source of drinking water for the City of Durham. The main manufacturing building measures approximately 600 feet by 600 feet and houses manufacturing operations including raw material receipt, metal machining and fabrication, testing of finished product and maintenance activities to support manufacturing operations. Paved vehicle parking areas are located along the southeast and north portions of the property. Asphalt access drives extend along the south and west portions of the facility. There are a total of five paved receiving/shipping loading docks located along the west and east sides of the facility. To the west and south of the building, there are several pad -mounted transformers. A backup generator is located on the south side of the facility. Also in this area is a pad -mounted chiller system with a reservoir containing coolant. The facility is classified as a conditionally exempt small quantity generator (CESOG) of hazardous waste. The site's EPA ID number is NCD004520136. The hazardous wastes are contained in 55-gallon drums and stored in the hazardous waste storage building located along the west side of the facility. The fire storage tank is located in the northwest corner of the facility. An oil and chip recovery area (termed "chip truck") is located in the west portion of the facility. Dumpsters for collection and storage of solid waste and other materials for recycling (e.g., cardboard and metal scrap) are located in the northwest paved area. A solid waste compactor is also located in this paved area. A diked aboveground storage tank (AST) farm for synthetic oil products, along with aboveground piping for transfer of oil from the ASTs into the building, is located along the north side of the facility. Two large air conditioning units are located along the northeast side of the facility. Several cooing tower units are located on the roof in the southeast corner of the facility. No significant spills or leaks of pollutants have occurred at the facility in the past three (3) years. Significant materials and activities present at the facility are listed in Section 5.0 of this document. 4.0 Site Map A site map is provided in Figure 2. The map outlines the following information: • Locations of impervious surfaces such as parking lots and access roads • Direction of stormwater flow indicated by arrows 1101 /2014 Page 3 of 19 U ITAN Roxboro MESH Document 3.0 Water Management Powering Business Worldwide Stormwater Pollution Prevention Plan (SW PPP) ■ Location of potential stormwater pollutant sources ■ Location of Best Management Practices (BMP) and other control measures • Location of parameter benchmark monitoring locations and stormwater outfalls 5.0 Description of Potential Pollutant Sources and Applicable Control Measures This section of the SWPPP describes industrial activities and materials that may be potential sources of stormwater pollutants. Best Management Practices (BMPs) and other applicable control measures designed to minimize these pollutant sources are also described in this section. Additional descriptions of BMPs and other control measures are included in Section 6.0. 1 /01/2014 Page 4 of 19 E:T•N Powering Business Worldwide Roxboro MESH Document 3.0 Water Management Stormwater Pollution Prevention Plan (SWPPP) Category & Description Activity: Truck Loading/Unloading (Docks #1, #2, #3, #3A, #4 and Houghton Area) Potential Pollutants New & Used Hydraulic Oils, Raw Materials, Liquid Chemicals Description of Best Management Practices Minimize Exposure Truck loading and unloading operations will take place only at appropriate facilities and following standard practices that minimize exposure outside covered and contained areas. Housekeeping Accumulations of residues will be promptly removed by sweeping or vacuuming. Bulk trailers will be cleaned frequently to remove residues from the trailers. Preventive Maintenance Standard practice and care will be employed when loading and unloading to prevent exposures during loading and unloading operations. Training, Inspections & Corrective Action Personnel associated with the operation will be trained in proper stormwater management procedures. The area will be inspected during the semi-annual SWPPP inspections, and more frequently as needed. Corrective actions will be tracked to completion through the corrective action module of MESH Suite. 1 /01 /2014 Page 5 of 19 Fm,ToN Powering Business Worldwide Roxboro MESH Document 3.0 Water Management Stormwater Pollution Prevention Plan (SWPPP) Category & Description Activity: Fuel filling operations at the backup -power generator Potential Pollutants Constituents associated with diesel fuel Description of Best Management Practices Minimize Exposure When filling operations take place, standard practices will be employed to dripping, leaks and spills. Preventive Maintenance The 660-gallon fuel storage tank is double -walled, with the outer container designed to allow pressure or vacuum testing to verify integrity of the inner and outer vessels. Standard practice and care will be employed during filling operations. Training, Inspections & Corrective Action Personnel associated with the operation will be trained in proper stormwater management procedures. The area will be inspected during the semi-annual SWPPP inspections, and more frequently as needed. Corrective actions will be tracked to completion through the corrective action module of MESH Suite. 1 /01 /2014 Page 6 of 19 U mT* N Powering Business Worldwide Roxboro MESH Document 3.0 Water Management Stormwater Pollution Prevention Plan (SWPPP) Category & Description Activity: Trash Collection and Solid Waste Compaction Potential Pollutants Solid debris; oily residues Description of Best Management Practices Minimize Exposure Solid wastes and oil residues will be handled and disposed in accordance with standard care and practices to minimize exposures from dumpsters, waste bins and compactors. Housekeepinq Areas surrounding each solid waste compactor and waste bin will be cleaned as needed to remove any accumulations of residues. Preventive Maintenance Waste compactors will be inspected, cleaned and replaced as needed to prevent releases of residues. Spill Prevention and Response Employees will implement provisions of the facility's oil Spill Prevention, Control and Countermeasures (SPCC) Plan, incorporated herein by reference, to address any oil releases. Training, Inspections & Corrective Action As appropriate, personnel associated with the operation will be trained in proper stormwater management procedures. The area will be inspected during the semi-annual SWPPP inspections, and more frequently as needed. Corrective actions will be tracked to completion through the corrective action module of MESH Suite. 1 /01/2014 Page 7 of 19 EAIaTeN Powering Business Worldwide Roxboro MESH Document 3.0 Water Management Stormwater Pollution Prevention Plan (SWPPP) Category $ Description Activity: Bulk tank unloading, storage and transfer of products Potential Pollutants Oil residues Description of Best Management Practices Minimize Exposure Truck loading and unloading operations will take place only at appropriate facilities and following standard practices that minimize exposure outside covered and contained areas. Containment area will be inspected and accumulated stormwater will be verified to be free of oil prior to discharge. Equipment and the transfer will be continuously monitored during transfer operations. Housekeeping The containment areas surrounding the truck unloading area and aboveground storage tanks will be cleaned whenever oily residues are present. Preventive Maintenance Tanks, piping, fittings, seals, over -fill protection devices and other components associated with the system will be inspected, cleaned and replaced as needed to prevent releases. Spill Prevention and Response Employees will implement provisions of the facility's oil Spill Prevention, Control and Countermeasures (SPCC) Plan, incorporated herein by reference, to address any oil releases. Training, Inspections & Corrective Action Personnel associated with the operation will be trained in proper stormwater management procedures. The area will be inspected during the semi-annual SWPPP inspections, and more frequently as needed. Corrective actions will be tracked to completion through the corrective action module of MESH Suite. 1/01/2014 Page 8 of 19 F AIRTO N Powering Business Worldwide Roxboro MESH Document 3.0 Water Management Stormwater Pollution Prevention Plan (SWPPP) Category & Description Activity: Outside Storage of Equipment and Materials (Houghton Area) Potential Pollutants Suspended solids; oily residues Description of Best Management Practices Minimize Exposure Equipment and materials will only be stored inside the building or under a covered area. No maintenance activities (such as pressure washing, cleaning, painting, lubrication) will be performed outdoors in areas exposed to precipitation and stormwater runoff. Housekeeping Accumulations of residues will be removed by sweeping or vacuuming. Training, Inspections & Corrective Action Personnel responsible for maintenance activities and transfer/storage of equipment and materials will be trained in proper stormwater management procedures. The area will be inspected during the semi-annual SWPPP inspections, and more frequently as needed. Corrective actions will be tracked to completion through the corrective action module of MESH Suite. 1 /01/2014 Page 9 of 19 U MITS N Powering Business Worldwide Roxboro MESH Document 3.0 Water Management Stormwater Pollution Prevention Plan (SWPPP) Category & Description Activity: Operation of Cooling Towers and Chilled Water Systems Potential Pollutants Water with chemical treatment additives Description of Best Management Practices Minimize Exposure No water from cooling towers, chillers or other systems, which contains any water treatment chemicals or other contaminants, will be drained or otherwise discharged onto the ground or into storm sewers. Provisions will be maintained to ensure that any such discharges are routed to the City sanitary sewer. Preventive Maintenance Piping, fittings, seals and other components associated with cooling water system will be inspected, cleaned and replaced as needed to prevent leaks and other releases. Training,_Inspections & Corrective Action Personnel responsible for operation and maintenance of cooling systems will be trained in proper stormwater management procedures. Areas surrounding cooling towers, chillers and other cooling systems will be inspected during the semi-annual SWPPP inspections, and more frequently as needed. Corrective actions will be tracked to completion through the corrective action module of MESH Suite. 1 /01 /2014 Page 10 of 19 FAInToN Powering Business Worldwide 6.0 Measures and Controls Roxboro MESH Document 3.0 Water Management Stormwater Pollution Prevention Plan (SWPPP) The following Best Management Practices (BMPs) and other stormwater management controls are appropriate for use at the facility in order to reduce stormwater pollutants and ensure compliance with the Industrial General Permit, 6.1 Minimize Exposure Minimize exposure of all potential pollutant sources to rain, snow, snowmelt, and surface water runoff. Such sources include material loading, unloading and storage areas; waste handling areas and waste storage bins; and equipment cleaning, maintenance and storage activities. Exposure is minimized by locating these materials and activities inside or protecting them with storm resistant coverings. 6.2 Good Housekeeping Maintain all areas where potential sources of stormwater pollutants are present in a clean and orderly fashion. Check these areas regularly and promptly clean up any spills or other residues. 6.3 Preventive Maintenance Inspection and preventative maintenance measures will be implemented which will help ensure that stormwater controls and management devices are functioning properly, and prevent breakdowns or failures resulting in discharges of pollutants to surface water. These measures are described by activity in Section 5.0. 6.4 Spill Prevention and Response Procedure The following measures will be implemented to minimize the potential for leaks, spills and other releases of oil and other potential pollutants: Labeling of Containers: Clearly label all containers (e.g., "Used Oil," "Spent Solvents," "Fertilizers and Pesticides," etc.) that could be susceptible to spillage or leakage to encourage proper handling and facilitate rapid response if spills or leaks occur. Barriers Spill Containment & Other Protections: Maximize the use of preventative measures such as barriers between material storage and traffic areas; secondary containment provisions; and safe procedures for material storage and handling. As stated in the IGP, secondary containment is required for bulk storage of liquid materials. Bulk storage is defined as a single above -ground container with greater than 660 gallons of capacity, or multiple above -ground containers in close proximity to each other with a total combined storage capacity of 1,320 gallons. Spill Prevention & Response Measures: Ensure that proper procedures are in place for expeditiously stopping, containing, and cleaning up leaks, spills, or other releases. In the case of the Roxboro facility, this will involve implementation of the facility's Spill Prevention, Control and Countermeasure (SPCC) Plan, incorporated herein by reference. The SPCC Plan is intended to minimize the potential for the facility to adversely impact the environment and to attain and maintain compliance with U.S. EPA standards for oil pollution prevention and response. Spill Notification Procedures: Ensure that proper procedures are in place for notification of appropriate facility personnel, emergency response agencies, and regulatory agencies in the event of a leak, spill, and other release. The SPCC Plan defines detailed 1 /01 /2014 Page 11 of 19 Um,aT*N Roxboro MESH Document 3.0 Water Management Powering Business Worldwide Stormwater Pollution Prevention Plan (SWPPP) procedures for notification in the event of a release. Those procedures are summarized below. For leaks, spill, or other releases involving either: discharges of oil if they "cause a film or sheen upon or discoloration of the surface of the water or adjoining shorelines or cause a sludge or emulsion to be deposited beneath the surface of the water or upon adjoining shorelines." (40 CFR 110.3(b)); or releases of a hazardous substance to the environment (i.e., navigable waters, any other surface water, ground water, drinking water supply, land surface or subsurface strata, or ambient air) in an amount equal to or greater than a reportable quantity (RQ) established under 40 CFR Part 110, 40 CFR Part 117, or 40 CFR Part 302, and occurring during a 24-hour period; the following organizations are to be notified immediately: Organization Phone Number National Response Center (800) 424-8802 North Carolina Department of Environment and Natural Resources, Land Quality Section - Raleigh Regional Office (919) 791-4200 Eaton Emergency Hotline (215) 942-8216 The following information should be provided to the extent possible: • Name, address, and telephone number of the facility and the person reporting; • Specific location of the incident; • Date and time the incident occurred or was discovered; • Name of the chemicallmaterial released; • Source and cause of the release; • Total quantity discharged, • Medium into which the substance was discharged; • Amount spilled into water; Weather conditions; • Name of the carrier or vessel, the railcar/truck number, or other identifying information; • Number and type of injuries or fatalities; Whether an evacuation has occurred; • Estimation of the dollar amount of property damage; • Description of current and future cleanup actions; and • Other agencies notified or about to be notified. 6.5 Employee Training Train all employees who work in areas where industrial materials or activities are exposed to stormwater, or who are responsible for implementing activities necessary to meet the conditions of the Industrial General Permit, including all members of the Pollution Prevention Team. The training should address the following topics: • Overview of applicable permit requirements; • Contents and goals of the stormwater pollution prevention plan; 1 /01/2014 Page 12 of 19 =�.� Roxboro MESH Document 3.0 Water Management Powering Business Worldwide Stormwater Pollution Prevention Plan (SWPPP) • Pollution prevention techniques, including good housekeeping, management of materials, minimization of outdoor exposure and other BMPs; • Spill reporting and response procedures. Training is to be conducted annually, and records will be kept with this SWPPP in Attachment 1. 6.6 Erosion and Sediment Controls Identify areas that, due to topography, activities, or other factors, have a high potential for significant soil erosion, and identify structural, vegetative, and/or stabilization measures to be used to limit erosion. 6.7 Management of Run-on and Runoff In addition to stormwater management practices which control the source of pollutants, consideration should be given to "traditional" stormwater management practices which are sometimes used to divert, infiltrate, reuse, or otherwise manage stormwater runoff in a manner that reduces pollutants in stormwater discharges from the site. Implement and maintain such measures where they are determined to be reasonable and appropriate. Appropriate measures may include: • vegetated swales; • reuse of collected stormwater (such as for a process or as an irrigation source); • inlet controls (such as oil/water separators); • snow management activities; • infiltration devices; and • wet detention/retention devices. The facility currently maintains vegetated drainage swales along the north, west and south portions of the property, and a stormwater detention basin in the northeast portion of the property. 7.0 Prohibited Activities Outdoor Manufacturing Operations: The facility does not perform any manufacturing operations outdoors. Outdoor Storage of Materials: To the extent practicable, uncovered materials will not be stored outdoors. Outdoor Maintenance Activities: To the extent practicable, maintenance activities by employees and contractors will not be performed outdoors. 8.0 Allowable Discharges Stormwater discharges associated with industrial activity that are mixed with sources of non- stormwater are prohibited, except for the following non-stormwater discharges identified in the IGP, provided the non-stormwater component of such discharges meets all requirements of the permit: • discharges from emergency fire fighting activities; • fire hydrant flushing; • potable water sources including water line flushing; 1 /01 /2014 Page 13 of 19 Uml,,T*N Roxboro MESH Document 3.0 Water Management Powering Business Worldwide Stormwater Pollution Prevention Plan (SWPPP) • runoff from irrigation using non -process water; • landscape watering provided all pesticides, herbicides, and fertilizers have been applied in accordance with the approved labeling; • routine external building washdown which does not use detergents; • pavement wash waters where spills or leaks of toxic or hazardous materials have not occurred (unless all spilled material has been removed) and where detergents are not used; • air compressor condensate; • steam condensate; • uncontaminated condensate from air conditioners, coolers, and other compressors and from the outside storage of refrigerated gases or liquids (such as the discharge of thawed condensate from the surface of liquid nitrogen tanks stored outdoors); • incidental windblown mist from cooling towers that collects on rooftops or adjacent portions of the facility, but not intentional discharges from the cooling tower (e.g., "piped' cooling tower blowdown or drains); • uncontaminated ground water or spring water (See Note Below); • foundation or footing drains where flows are not contaminated with process materials such as solvents (See Note Below); • excavation dewatering (See Note Below); and • non -process water used for dust suppression on roads. Note: There shall be no turbid discharges to surface waters of the state resulting from dewatering activities (see permit for additional details). 9.0 Documentation of Permit Eligibility Related to the 303(d) List of Impaired Water Bodies The Industrial General Permit requires that SWPPPs include information on whether or not the stormwater discharges from the facility enter a water body that is impaired or subject to an approved Total Maximum Daily Load (TMDL). If either of these situations is applicable, various actions may be required to document that surface water quality is adequately protected. The 2012 North Carolina List of Impaired Water Bodies (303(d) list) indicates that the North Flat River which flows to Lake Michie, which receives stormwater runoff from the facility, is not an impaired stream. 10.0 Identification and Elimination of Illicit Discharges The following measures will be implemented at the facility to identify and eliminate the discharge of process wastewater, domestic wastewater, non -contact cooling water, and other illicit discharges to stormwater drainage systems or to Waters of the State: Observations during visual site inspections and comprehensive site evaluations (Section 11) will include checks for flow in stormwater channels, storm sewers and other conveyances during dry weather conditions. Such flows may indicate the possible presence of a prohibited discharge. If observed, the origin will be identified, and appropriate corrective actions taken and documented. The facility will maintain drawings and other information to document that all discharges of wastewater, cooling water and similar discharges are properly routed to the city sanitary sewer. Where uncertainty or a lack of information is indicated, additional evaluation will be completed, and may include: flow testing; dye testing; or tracing of lines. Before any new discharge of wastewater, cooling water or similar source is implemented, an evaluation will be completed to confirm that the tie-in will not result in discharge to the stormwater conveyance system. 1/01/2014 Page 14 of 19 E M, TO N Roxboro MESH Document 3.0 Water Management Powering Business Worldwide Stormwater Pollution Prevention Plan (SWPPP) 11.0 Inspections, Evaluations, Monitoring, Reporting, Corrective Action and Recordkeeping Following is a summary of permit requirements for stormwater inspections, site evaluations and water quality monitoring, along with reporting to the Division of Water Quality/Land Quality Section (DWQ/LQS), internal recordkeeping, and other items. Blank forms can be found in Attachment 2. • Conduct qualitative monitoring (twice yearly). • Conduct analytical monitoring (twice yearly). • Submit Discharge Monitoring Reports to DWQ/LQS. • Implement a corrective action plan if parameter benchmark values are exceeded. • Modify the SWPPP at least annually and as needed based on inspections, evaluations or monitoring results. • Maintain all permit -related records for five (5) years from date of permit expiration. Additional information pertaining to these requirements is included below and in the IGP. 11.1 Qualitative Monitoring Complete routine inspections of all potential stormwater pollutant areas, all stormwater control measures and all stormwater outfalls. A minimum of two (2) qualitative monitoring events are required each year, to be completed concurrent with analytical monitoring. Qualitative monitoring is to be performed during a measurable storm event (i.e. one that results in an actual discharge) and documented on Form SWU-242 (found in Attachment 1). During each inspection, observe areas for indications that pollutants may be exposed to or entering stormwater conveyances. When flow is occurring, look for indications of possible concern, such as floating solids, oily sheen, odor, discoloration or excess turbidity. Inspections are to be conducted by qualified individual (i.e., members of the pollution prevention team and/or other individuals who have been trained). Document the following information for facility records: date; personnel; observations; and a summary of any required actions. Corrective actions, where identified as necessary, will be tracked to completion through the corrective action module of MESH Suite, and documented for facility records in Attachment 3. 11.2 Analytical Monitoring Conduct analytical monitoring of stormwater discharges from the facility. Requirements are summarized below and detailed in the IGP. Frequency: Two (2) times per calendar year, with one event between January and June, and a second event between July and December. The sampling events are to be separated by a minimum of 60 days. Locations: Qutfalls #001, #004 and #005 (see Figure 2). IT SHOULD BE NOTED THAT OUTFALL #001 AS OF JANUARY 1, 2014 IS COVERED BY INDIVIDUAL NPDES PERMIT # NC0003379. UNDER AN AGREEMENT WITH THE STATE, THIS INDIVIDUAL PERMIT WILL BE RESCINDED AND OUTFALL # 001 WILL BE COVERED UNDER THIS GENERAL PERMIT AFTER COMPLETION OF THE STORM SEWER PROJECT AT THE SITE. V0112014 Page 15 of 19 MIT* N Roxboro MESH Document F3.0 Water Management Powering Business Worldwide Stormwater Pollution Prevention Plan (SWPPP) Qualif in Event: Sample stormwater runoff from a "measurable storm event" — i.e., one that results in an actual discharge from the site — and which follows the preceding measurable storm event by at least 72 hours. Sample Type: Collect a minimum of one grab sample from each outfall within the first 30 minutes after discharge resulting from the storm event begins. If this is not possible, collect the sample as soon as practicable after the first 30 minutes and document the reason for delay. Sample Anal Complete the following field and laboratory analyses for each sample, using methods described in 40 CFR Part 136 or the latest revision of Standard Methods for the Examination of Water and Wastewater: • pH • Total Suspended Solids (TSS) • Non -Polar Oil & Grease/TPH (EPA Method 1664) • Total Recoverable Copper • Total Recoverable Lead • Total Recoverable Zinc • Total Toxic Organics (TTO), only if the facility's Solvent Management Plan has lapsed • Total Rainfall (in inches) Report: For each monitoring event, record and report the date and duration (in hours) of the storm event; rainfall measurements or estimates (in inches); the duration between the sampled storm event and the end of the previous measurable storm event; and an estimate of the total volume (in gallons) of the discharge. Evaluation & Corrective Action: Compare sample analytical results to the parameter benchmark values listed below. If any exceedances are indicated, investigate the cause of the elevated reading(s), and perform Tier 1, Tier 2 or Tier 3 corrective actions, as described in Part II, Section B of the IGP. Parameter Benchmark Comparison Values Parameter Units Parameter Benchmark Value Minimum Maximum H s.u. 6.0 9.0 Total Suspended Solids TSS m IL - - 100 Non -Polar Oil & GreaseiTPH m IL - - 15 Total Recoverable Copper m IL - - 0.007 Total Recoverable Lead m IL - - 0.030 Total Recoverable Zinc m IL - - 0.067 Total Toxic Or anics TTO m IL - - 1 11.3 Reporting Requirements A Discharge Monitoring Report (DMR) must be prepared and submitted to Division of Water Quality/Land Quality Section within 30 days of receiving laboratory results. The DMR Forms are to be signed in accordance with Part III, Section B.5 of the IGP. Each submission is to include two (2) signed copies of the DMR Forms (refer to the IGP for details). A copy of the submittal can be filed in Attachment 4. 1101 /2014 Page 16 of 19 =T•N Roxboro MESH Document 3.0 Water Management Powering Business Worldwide Stormwater Pollution Prevention Plan (SWPPP) In addition, an annual review of the SWPPP and an annual summary of data monitoring reports shall be conducted and documented on Form SW U-264 (found in Attachment 1). The purpose of this report is to provide an opportunity to review the SWPPP and to summarize the monitoring results for the calendar year. This form does not require submittal, but rather, should be kept on file in the SWPPP. 12.0 SWPPP Certification certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name: Glenn McLean Title: Facility Manager Signature: e Date: 5 F2b 2- 1 /01 /2014 Page 17 of 19 Figure 1 — Topographic Map (Attached) EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC 625 HUNTSMAN COURT GASTONIA, NC 28054 (704) 853-08000 FIGURE 2 -- SITE TOPOGRAPHICAL MAP AND ONE MILE RADIUS Excel Proiect No. 28091 Source: USGS N3615 — W7852 Timberlake NC, 1981 Figure 2 — Site Map (Attached) FF PAKD PARKING LEGEND . ' North BULK M TANKS — — APPROXIMATE PROPERTY LINE STORM SEWER GAp _� N M � -' STORMWATER DRAINAGE SWALE STORM WATER OU TFALL ao rI ROUG/TGN AREA POTENTIAL STORM WA TER 14 POLLUTANT AREA l ❑ WATER FLOW SURFACE J Nw � � / — — — DRAINAGE AREA AP PRO ( ) 4 X. ACING • - ` LOADING DOCK --- - l.>'.I.J.J TREE LINE GENERATOR 1} CHILLER UNIT TRASH UUMPSTERS LOADING DOCK EXISTING UANUFACTURWG I TRANSFORMER CHIP TRUCi( ❑ Hw HAZARDOUS WASTE STORAGE LOADING OOCK - PA Y£D PARKNC �I � I ` ® ' Oro +.. n. >v ,r a.. +a. •s a I 1 A \ u+rArm rinan�w. \ FIGURE 2- SITE PLAN TO NCR1N MT M�EA STORM WATER Pg14770N PREVENTION PLAN (SAPPP) l ap, EATON CORPORATION. ROkSORO. NC S AS u1