HomeMy WebLinkAboutWQ0039053_Modification_20191213Initial Review
INITIAL REVIEW
Reviewer Thornburg, Nathaniel
Is this submital an
application?*
r Yes r No
Is this a complete
application?* Complete App Date
r Yes r No 12/03/2019
Project Number* WQ0039053
Applicant/Permittee Bio-Nomic Services, Inc.
Applicant/Permittee 530 Woodlawn Street, Belmont, NC 28012
Address
Is the owner in BIMS? Is the facility in BIMS?
r Yes r No r Yes r No
Owner Type
Facility Name George L. Bernhardt, Sr. Lake Rhodhiss WTP
County
Fee Category Fee Amount
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if
non -application)
Email Notifications
Does this need O Yes
review by the r No
hydrogeologist? *
Regional Office Mooresville
CO Reviewer Poonam Giri: eads\pagiri
Admin Reviewer Kendall.Williams@ncdenr.gov
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notification
Comments for Kendall
Comments for RO
Comments for Reviewer
Comments for Applicant
Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
........................................................................................................................................................................................................................................................................................................................................................................
Name * Martin Mabe
Email Address*
martin@Wllcoxmabesoil.com
Project Information
.........................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number WQ0039053
currently has project
Applicant\Permittee * Bio-Nomic Services, Inc.
Phone Number*
3363121396
Applicant/Permittee 530 Woodlawn Street, Belmont, NC 28012
Address*
r Modification (Major or Minor)
r Additional Information
r Other
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Facility Name * George L. Bernhardt, Sr. Lake Rhodhiss WTP
Please provide comments/notes on your current submittal below.
One hardcopy and the modification fee will be mailed to NCDEQ on 12/3/19. Please contact Martin Mabe at Willcox &
Mabe Soil Solutions, PLLC with any questions regarding this permit modification.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
WQ0039053 Permit Modification.pdf 9.83MB
upload only 1 RDF document. NL@iple documents must be combined into one RDF file.
For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper --polka*-ion is required,
be advised, applications accepted' far pre -review until both the paper and eIect-c-,i_ co1)ies nave been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments (calcs, soils report, specs, etc.)
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
MallinE address:
❑iuision of Water Resources1 Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center 1 Aft: Nathaniel Thornburg, 91° Floor, Cfice #942W
----------------------------------------------------------- -----------------------------------------
Raleih, NC 27699-1617 512 N. Salisbury St.
Far questions or problems contact Tessa Monday attessa.monday@ncdenr.Qov or 919.707.3560.
* W By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 12/2/2019
APPLICATION FOR
DISTRIBUTION OF CLASS A RESIDUALS
PERMIT MODIFICATION
BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. W00039053
Willcox & Mabe Soil Solutions, PLLC Project No. 15-18
Prepared for:
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Prepared by:
Willcox & Mabe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
willcox&mabe
SO I L SO LUT I ON S
December, 2019
TABLE OF CONTENTS
APPENDIX TITLE
DISTRIBUTION OF CLASS A RESIDUALS
APPLICATION FORM
(FORM: DCAR 06-16)
H FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION)
III FORM DCAR 06-16 (ITEM H. OPERATION AND MAINTENANCE
PLAN)
IV RESIDUALS SOURCE CERTIFICATION
APPLICATION FORM
CITY OF LENOIR WTP
(FORM: RSC 06-16)
December 3, 2019
NCDEQ/DWR
Water Quality Permitting Section
512 N. Salisbury Street
9s' Floor, Office #942W
Raleigh, North Carolina 27604
Attention: Non -Discharge Permitting Unit
4� a !
willcox&mabe
SO I L SOL U T I ON S
Reference: Modification for Distribution of Class A Residuals
Bio-Nomic Services, Inc. W00039053
Willcox & Mabe Soil Solutions, PLLC Project No. 15-18, Phase: 14
Non -Discharge Permitting Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting the enclosed application to
modify the existing Distribution of Class A Residuals permit WQ0039053 for Bio-Nomic
Services, Inc. (BNS) on behalf of BNS. The application package includes information for
adding one Class A source at this time: City of Lenoir WTP - 2,000 Dry Tons.
It should be noted that City of Lenoir WTP is an municipal water treatment plant with no
domestic contribution to the waste stream. Fecal coliform sampling has demonstrated that
the residuals meet Class A requirements (all 7 individual samples were below 1,000
MPN/g). Per 15A NCAC 02T .1106.d and .1107.c vector attraction reduction should not
be required for this source.
If there is any further information required or questions regarding this application please do
not hesitate to contact Bio-Nomic's, Mr. Vaughn "Buck" Stevenson at (704) 529-0000 or
WMSS's Mr. Martin Mabe at 336-312-1396 for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
1
Martin Mabe
Agronomist
cc: Bio-Nomic Services, Inc.
Rob Willcox, L.S.S.
Licensed Soil Scientist
SharaMWMSS PmJecta12MM18-18 Bio•Norn!=Thase 09 • Class A Perntm2819 Penn Modification (Lenoir WTP)M-18 Bionomirs
Distribution of Class A Residuals Application Package.doc
Willcox & Mabe Soil Solutions, PLLC /7231 B Summedield Road /Summedield. NC 27368 / Rob 336.339.9128 or
Martin 336.312.1396 / Wmmillcownabesoil.com
APPENDIX 1
DISTRIBUTION OF CLASS A RESIDUALS
APPLICATION FORM (DCAR 06-16)
DWR -
`61sion of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
15A NCAC 02T A 100 — DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted. the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website
General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residuals under 15A NCAC 02T A 100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 06-16):
( Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
The project name should be consistent on the plans, specifications, etc.
The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T 0106(b). An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T .0106(b).
❑ If this project is for a modification of an existing permit, submit one copy of the existing permit.
❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
9 Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification
New Permit
Major Modification'
Major (residuals permitted for distribution a 3,000 dry tons/year)
$1,310
$395
Minor (residuals permitted for distribution < 3,000 dry tons/year)
$810
$245
' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
® List all items included in the application package, as well as a brief description of the requested permitting action.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 1 of 3
D. Program Information (All Application Packages)
Provide a narrative explaining the following:
How the materials will be handled and transported from where the residuals were produced to where it will be treated.
® How the residuals will be processed/treated (attach process flow diagram).
® How leachate collection will be handled.
Where the residuals will be stored until processed.
® How the final product will be distributed (packaging, bulk, etc.)
® What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed..
Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
® Name and address of the person who prepared the residual that is sold or given away.
® A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
® A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
® A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
® Information on all applicable setbacks in accordance with 15A NCAC 02T 1108(b).
® A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A
NCAC 02T 1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1108(a) on the plans.
❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the final product in accordance with 15A NCAC 02T. 1104(a)(2)(B), including leakage and pressure testing as appropriate.
❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and
specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T
. I I G4(a)..
G. Environmental Assessments (May be Required — See 15A NCAC 1 C .0300)
❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3
H. Operation and Maintenance Plan (New and Renewal Application Packages)
For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
[ Submit the O&M Plan in accordance with 15A NCAC 02T .l 110 and include at a minimum:
Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
Safety measures; may include safety training program, manuals, signs, etc.
Spill response plan; including control, containment, remediation, emergency contact information, etc.
Inspection plan including the following information;
Names and titles of personnel responsible for conducting the inspections.
® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
Sampling and monitoring plan including the following information;
® Names and titles of personnel responsible for conducting the sampling and monitoring.
Detailed description of monitoring procedures including parameters to be monitored.
® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: (919) 807-6464
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: (919) 807-6496
INSTRUCTIONS FOR FORM: DCAR 06-16
Page 3 of 3
D I "Wit
Division of Water Resources
I. APPLICANT INFORMATION:
State of North Carolina
Department of Environmental Quality
Division of Water Resources
15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
1. Applicant's name: Bio-Nomic Services, Inc
Applicant type: ❑ Individual Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
El Federal Q State ❑ Municipal M County
Signature authority's name per 15A NCAC 02T .0106: Mr. Vaughn Stevenson Title: Vice President
Applicant's mailing address: 530 Woodlawn Street
City: Belmont State: NC Zip: 28012
Telephone number: (7U) 529- 000 Email Address: vstevenson@bio-nomic.com
2. Consultant's name: Martin Mabe License Number (for P.E.): _
Affiliation: El On Staff ® Retained (Firm: Willcox & Mabe Soil Solutions, PLLCI
Consultant's mailing address: 7231B Summerfield Road
City: Summerfield State: NC Zip: 27358
Telephone number: (336) 312-1396 Email Address: martin@willcoxmabesoil.com
3. Fee submitted: $395.00 (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, E9 modified, ❑ renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00039053
Date of most -recently issued permit: March 22, 2017
Date of most -recently certified Attachment A (if different than the permit): April 16, 2019
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Bio-Nomic Services. Inc.
City: Belmont State: NC Zip: 28012 -�6d
Coordinates: Latitude: 35016' 32" Longitude: Slo3' 7"
Datum: NAD 83 Level of accuracy: Nearest Second
Method of measurement: MAP
County where facility is located: Gaston
2. Facility contact (person familiar with residuals preparation):
Name: Vaughn "Buck" Stevenson Title: Vice President
Mailing address: 530 Woodlawn Street
City: Belmont State: NC Zip: 28012- "' " �j
Telephone number: 704 529-0000 E-mail address: vstevenson@bio-nomic.com
FORM: DCAR 06-16 Page 1 of 3
3. Is the residual process facility also the generator? ❑ Yes; 0 No
If No, please specify delivery frequency and quantity of residual to be processed: N/A
4. Length of residuals storage at facility: N/A days (Note: the Division requires minimum 30 days storage in units that are separate
from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
Q sold or given away in bags or other containers; ❑ lawn (bulk); [] home garden (bulk);
[, other (explain); Land Application
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
I Complete the following if residuals are to be mixed with other materials:
Type of Materials
Amounts to be added
3. Approximate amounts of the residuals received and processed at the facility: N/A dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: N/A dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): N/A
6. Does the facility have a stormwater management plan? ❑ Yes; ® No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: N/A
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
Residuals Source
Certification
FORM: DCAR 06-16 Page 2 of 3
Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
Yes ❑ No, Explain;
I, Vaughn Stevenson Vice President
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Bio-Nomic Services. Inc. — Distribution of Class A Residuals
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature:y Date:
FORM: DCAR 06-16 Page 3 of 3
APPENDIX 11
FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION
FORM DCAR 06-16 (ITEM D. PROGRAM INFORMATION)
D. Program Information (Bio-Nomic Services Class A Residuals)
Currently, Bio-Nomic Services is proposing to add one source: George L. Bernhardt, Sr.
Lake Rhodhiss WTP (in association with dewatering WTP residuals on an as -needed
basis.)
How the materials will be handled and transported from where the residuals
were produced to where it will be treated.
The operational functions of this program involve removing Class A Residuals from the
respective WTP and beneficially recycling the biosolids to land application sites which
meet NCDEQ-DWR regulatory requirements. Class A Residuals will be land applied at
or below agronomic rates.
• How the residuals will be processed/treated (attach process flow diagram).
The Class A Residuals will be tested at the respective treatment plants prior to hauling for
land application.
• How leachate collection will be handled.
Leachate will not be generated
• Where the residuals will be stored until processed.
Class A Residuals will be stored at the respective treatment plants
• How the final product will be distributed (packaging, bulk, etc.)
Class A Residuals will be land applied, not distributed
What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum,
calcium, etc.) are used or recommended as the limiting parameter for
determination of residuals loading rate to ensure that it does not overload the
soil and cause contravention of surface water or groundwater standards, limit
crop growth, or adversely impact soil quality.
Product Information Labels and Application Information Sheets are Attached.
Attach a marketability statement detailing destinations and approximate
amounts of the final product to be distributed.
D. Program Information (Bio-Nomic Services Class A Residuals) Page 2
Product Information Labels and Application Information Sheets are Attached
Provide either a label that shall be affixed to the bagged processed residual or an
information sheet that shall be provided to the person who receives the
processed residual. The label or information sheet shall contain, at a minimum,
the following information:
• Name and address of the person who prepared the residual that is sold or given
away.
• A statement that application of the residuals to the land shall be in accordance
with the instructions on the label or information sheet.
• A statement that the residuals shall not be applied to any site that is flooded,
frozen or snow-covered.
• A statement that adequate procedures shall be provided to prevent surface runoff
from carrying any disposed or stored residuals into any surface waters.
• Information on all applicable setbacks in accordance with 15A NCAC 02T
.1108(b).
• A statement that the residuals shall be applied at agronomic or recommended rates
for intended uses.
Product Information Labels and Application Information Sheets are Attached
APPENDIX III
FORM DCAR 06-16 (ITEM H. - OPERATION AND MAINTENANCE PLAN)
BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
I. Purpose
To put into place a plan that implements the requirements of North Carolina Department
of Environmental Quality — Division of Water Resources (NCDEQ-DWR) Permit No.
WQ0039053 for Bio-Nomic Services, Inc. (Bio-Nomic Services). Requirements are
included for the Class A source(s) (WWTP's and WTP's) and Bio-Nomic Services (land
application contractor). Class A source(s) are listed within the permit.
II. Operational Functions
The operational functions of this program involve hauling Class A Residuals from the
respective WWTP's and WTP's to land application sites which meet NCDEQ-DWR
regulatory requirements. Class A Residuals will be land applied at or below agronomic
rates. Bio-Nomic Services will also account for any nutrient sources the
landowner/lessee has applied. Some source(s) may be land applied as either a liquid or
cake material utilizing either pumper trucks, vacuum trucks, tractor trailer, tractor and
cake spreader and/or tractor and pull tank. Class A Residuals will be spread evenly and
at consistent rates. Class A Residuals will be land applied on fields that are used for hay
production, grazing, or row crop production harvested for animal feed. In the case where
Class A Residuals are land applied on fields utilized for grazing, applications rates will
be reduced by 25% in accordance with USDA-NRCS 590 Nutrient Management
Standards. Grazed fields will be determined by Bio-Nomic Services Operations Manager
on site.
The Bio-Nomic Services Class A Residuals will be monitored to confirm its compliance
with conditions in Non -Discharge Permit No. WQ0039053 to include:
• 15A NCAC 02T .1105 Pollutant Limits and nutrient analysis,
• Toxicity Characteristics Leaching Procedure (TCLP), and
• Reactivity, Ignitability and Corrosivity
III. Maintenance Schedules
Bio-Nomic Services will follow the maintenance schedule as recommended by the
manufacturer for the equipment utilized to complete the job within the limits of the permit.
IV. Safety Measures
Bio-Nomic Services takes pride in operating in a safety conscious manner. Employees
participate in regular safety training that is designed to help employees recognize safety
issues and take steps to prevent potential accidents from occurring. Bio-Nomic Services
employees have the authority to stop operations if they think any aspect of the operation
is going to lead to the cause of an environmental or personal accident.
C9UsersWartin\Willcox and Mabe Soil Solutions\Rob Willcox - Shared\WMSS Projects\2015\15-19 Bio-Nomics\Phase 09 - Class A Permit\2019 Permit
Modification (Lenoir WTP)\Bio-Nomic Services Class A C&M Plan 201 B.doc 11-21-19
BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
V. Spill Response Plan
• Halt the source of the spill: Such as a ruptured line or valve, or damaged transportation
unit.
• Contain spill: Use straw bales to form a barrier. Straw or hay bales can be obtained
from several sources for this purpose. Soil near the site can also be used to form a barrier
for containment.
• Clean up: Use Class A Residuals application equipment to recover as much of the
material as possible. After the application equipment has recovered as much material as
possible, it will be land applied as per the management plan. A temporary sump pit may
be dug in the containment area and spilled material washed into it to enhance recovery.
• Final Clean up: The ultimate goal will be to restore the spill area to its original
condition if possible.
• Notification: As soon as possible after a spill occurs notify:
• Bio-Nomic Services —Home Office
704-529-0000
Andy Taylor
704-907-7933
Joel Coert
704-904-9704
Buck Stevenson
704-930-8886
• Department of Environmental Quality
Division of Water Resources
Applicable Regional Office (See Permit)
Management of clean-up efforts: The field superintendent shall take immediate charge
of the clean-up activities. Additional labor will be requested from Bio-Nomic Services as
needed.
VI. Reporting
Within 24 hours of a spill the field superintendent shall present a written report detailing the
cause of the spill and all action taken in response to the spill. Bio-Nomic Services will notify
the appropriate Regional Office as soon as possible, but not more than 24 hours after, or on the
next working day following the occurrence
VII. Inspection Plan
Inspections for the land application of Class A Residuals will be conducted at a minimum of
daily at the land application site during land application events. Inspections will consist of
inspecting the current field(s) that are being applied on, as well as inspecting random fields
that have previously received Class A Residuals applications. Inspections will be performed
by Bio-Nomic Services personnel on a rotational basis to ensure that all employees are
familiar with the inspection processes. At a minimum, these inspections will consist of the
following:
CAUsensWartin\Wlllcox and Mabe Soil Solutlons\Rob Willcox - Shared\WMSS Projects\2015\15-18 Bio-Nomics\Phase 09 - Class A Permlt\2019 Permit
Modification (Lenoir WTP)\Bio-Nomic Services Class 0&M Plan 2018.doc 11-21-19
BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
• Verify that a residuals analysis has been collected prior to land application
activities being performed and that it meets the criteria for land application.
• Verify that pathogen reduction data has been collected for the source to be land
applied and that it meets the criteria for land application.
• Verify the crop that is planted or is to be planted on the respective field(s).
• Confirm that the correct amount of Class A Residuals are being land applied.
• Confirm that transport and application vehicles have a copy of the spill control plan.
• Confirm that a copy of the permit and the operations and maintenance plan are
maintained at the land application sites during land application activities.
• Check that the field has been properly flagged and that buffers are adhered to.
• Confirm that records are turned in at the end of each business day.
Inspections will also be conducted by the respective employees of the Class A Residuals
generating facilities (at the source generating facility). Bio-Nomic Services is not
responsible for inspections at the source generating facilities. These inspections
should be conducted by the respective ORC of each facility and should fall under
their own Operations and Maintenance Plans.
VIII. Sampling and Monitoring Plan
All sampling and monitoring shall be performed in accordance with current Permit No.
WQ0039053, Bio-Nomic Services Class A Residuals.
Pollutant concentrations for Class A Residuals shall not exceed the following Ceiling
Concentrations or Monthly Average Concentrations (i.e., dry weight basis):
Parameter
Ceiling Concentration
(milligrams per
kilogram)
Monthly Average
Concentration
(milligrams per kilogram)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
n/a
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
SIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
Class A Residuals shall be analyzed to demonstrate it is non -hazardous under the Resource
Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity,
and toxicity characteristic leaching procedure (I'CLP)] shall be performed prior to land
application of Class A Residuals.
TCLP analysis of Class A Residuals shall include the following parameters (the regulatory level in
milligrams per liter is in parentheses):
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol(100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Chlorobenzene 100.0
( )
Heptachlor (and its
hydroxide) (0.008)
Toxaphene(0.5)
Chloroform 6.0
( )(0.5)
Hexachloro-1,3-butadiene
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol(200.0)
Lindane (0.4)
2,4,5-TP (Silvex)(1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor(10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
An analysis shall be conducted on the Class A Residuals based on conditions set forth in Permit No.
W00039053. The analysis shall include the following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
Pathoeen Reduction: Per 15A NCAC 02T.1106
For Distribudon/Land Application of Class A or Enuivalent.
M A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids
BIO-NOMIC SERVICES PRODUCT INFORMATION LABEL
Produced/Land Applied By: Preparer:
Bio-Nomic Services, Inc. Respective WWTP's and WTP's
530 Woodlawn Street
Belmont, North Carolina 28012
For information on these products contact Bio-Nomic Services, Inc.
Vaughn "Buck" Stevenson, Vice President (704) 529-0000
The Bio-Nomic Services Class A Residuals are WTP Plant Residuals and WWTP Biosolids that
meet NCDEQ-DWR Class A land application requirements. The Bio-Nomic Services Class A
Residuals and Biosolids contain varying values of Nitrogen, Phosphorus and Potassium. Each
permitted Source will have a laboratory sample analyzed, with current nutrient values made
available prior to land application of the product.
Provisions for Application
Application of the Bio Nomic Services Class A Residuals are prohibited except in accordance with
the provisions specified in the Application Information Sheet. Application must conform to
standards identified in Permit WQ0039053 and include but are not limited to:
Setback Description
Setback
(feet)
Private or public water supply sources
100
Surface waters (streams — intermittent and perennial, perennial waterbodies,
and wetlands)
25
Surface water diversions (ephemeral streams, waterways, ditches)
0
Groundwater lowering ditches (where the bottom intersects the SHWT)
0
Wells with exception to monitoring wells
100
Bedrock outcrops
0
Bio-Nomic services Class A Residual Product Information Label
Application Information Sheet
1. Bio-Nomic Services Class A Residuals are intended for use as a fertilizer product.
Applications of Bio-Nomic Services Class A Residual should be made in accordance with
approved application standards and WQ0039053 permit conditions.
2. Bio-Nomic Services Class A Residuals shall not be applied to flooded, frozen, or snow
covered areas.
3. Application and storage of Bio-Nomic Services Class A Residuals must be conducted in
such a way as to prevent runoff from the application or storage site to any surface water.
4. Applications and loading rates of Bio-Nomic Services CIass A Residuals shall be
applied at agronomic or recommended rates.
Contact Bio-Nomic Services for a copy of the most recent Class A Residuals analysis and
loading rates.
Bio-Nomic services Class A Residual Product Information Label
BIO-NONIIC SERVICES CLASS A RESIDUALS RECEIPT FORM
name) have received
pounds and/or gallons of the Bio-Nomic Services Class A Residuals, a copy of the Bio-Nomic
Services Class A Residual product information label, and a copy of the most recent analysis of
the product (if requested). I have read these documents and agree to adhere to the directions
specified on the Application Information Sheet and the Product Information Label.
Signature of Receiver Date of Receipt
Address of Receiver
Bio-Nomic services Class A Residual Product Information Label
APPENDIX IV
RESIDUALS SOURCE CERTIFICATION
APPLICATION FORM
CITY OF LENOIR WTP
(FORM: RSC 06-16)
State of North Carolina
Department of Environmental Quality R-DW
Division of Water Resources
"Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one on final and two conies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permittine Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item, to which they refer.
® For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Man Guidance for
Residuals Land Application Permits".
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. S.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
® For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of I
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State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: George L. Bernhardt Sr Lake Rhodhiss WTP
2. Facility permit holder is: Federal, ❑ State, 0. Local Government, or [] Private.
Facility permit issued by: ® Div. of Water Resources, 0 Div. of Environmental Health,
or ❑ Other (explain: _).
3. Facility contact person and title: Kevin Matheson. WTP Superintendent
Complete mailing address: 5474 Waterworks Road
City: Granite Falls State: NC Zip: 28630
Telephone number: 828 757-4460 E-mail address: kmatheson@ci.lenoir.nc.us
4. Facility physical address: 5474 Waterworks Road
City: Granite Falls State: NC Zip: 28630
Coordinates: Latitude; 35o47' 8.38" Longitude: 81028' 54_5V
Datum: NAD83 Level of accuracy: Nearest hundredths of second
Method of measurement: MAP
5. Purpose of the facility:
treatment of municipal wastewater, R treatment of 100% domestic wastewater,
treatment of potable water, jj treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: I % industrial and RM % domestic)
other (explain: ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 12 MGD and facility average daily flow: 6_4 MGD
8. Average amount of residuals being generated at this facility 2000 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: N/A
Type and volume of residuals storage (i.e., outside of residuals treatment units): 0.75 acres with an average depth of 8 feet
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
Specify if residuals are regulated under:
_. 40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T 1102(6) as:
[ Biological Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: Ej yes no.
If yes, list the number(s): 1
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: I yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Blue Ridge Labs and Date of analysis: I0B/19
Passed corrosivity test: yes N no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: yes Of no. Flashpoint: > 140 OF (> 140°F)
Passed reactivity test: W yes no. HCN: I mg/kg (<250) & HzS: 5 mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(mg/1)
Result
(mg/9
Arsenic
5.0
<0.500
Hexachlorobenzene
0.13
<0.1
Barium
100.0
<5
Hexachloro-1,3-Butadiene
0.5
<0.04
Benzene
0.5
<0.25
Hexachloroethane
3.0
<0.2
Cadmium
1.0
<0.1
Lead
5.0
<0.5
Carbon Tetrachloride
0.5
<0.25
Lindane
0.4
<0.005
Chlordane
0.03
<0.025
Mercury
0.2
<0.002
Chlorobenzene
100.0
<2.5
Methoxychlor
10.0
<0.005
Chloroform
6.0
<0.25
Methyl Ethyl Ketone
200.0
< 5
Chromium
5.0
<0.2
Nitrobenzene
2.0
<0.2
m-Cresol
200.0
< 10
Pentachlorophenol
100.0
<0.5
o-Cresol
200.0
< 10
Pyridine
5.0
<0.5
p-Cresol
200.0
< 10
Selenium
1.0
<0.05
Cresol
200.0
< 10
Silver
5.0
<0.5
2,4-D
10.0
<0.5
Tetrachloroethylene
0.7
<0.25
1,4-Dichlorobenzene
7.5
<0.2
Toxaphene
0.5
<0.05
1,2-Dichloroethane
0.5
<0.25
Trichloroethylene
0.5
<0.25
I,1-Dichloroethylene
0.7
<0.25
2,4,5-Trichlorophenol
400.0
<0.5
2,4-Dinitrotoluene
0.13
<0.1
2,4,6-Trichlorophenol
2.0
<0.5
Endrin
0.02
<0.005
2,4,5-TP (Silvex)
1.0
<0.5
Heptachlor and its Hydroxide
0.008
<0.005
Vinyl Chloride
0.2
<0.1
FORM: RSC 06-16 Page 2 of 5
4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under ISA NCAC 02T .1105.
a. For Distribution/Land Application. Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Blue Ridge Labs and Date of analysis: 10/8/19
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
0.46
Cadmium
85
39
<0.0618
Copper
4,300
1,500
33.8
Lead
840
300
<3.09
Mercury
57
17
0.0822
Molybdenum
75
n/a
<0.309
Nickel
420
420
<0.309
Selenium
100
100
0.0822
Zinc
7,500
2,800
314
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but <25
30
200
210
❑ >_ 25 but < 50
34
220
240
50 but < 75
39
260
270
>_ 75 but < 100
46
300
320
❑ >_ 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5
5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 31.3 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Blue Ridge Labs and Date of analysis: 10/8119
Parameter
Result
(mg/kg)
Aluminum
2,686
Ammonia -Nitrogen
3,738
Calcium
1,463
Magnesium
2,130
Nitrate -Nitrite Nitrogen
325
pH (Standard Unit)
6.3
Phosphorus
2,686
Potassium
1,594
Sodium
1,035
Total Kjeldahl Nitrogen
9,220
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 2.25
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 20 %. This
rate is a (check one): H default value, or JJ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1") Year PAN
Five -Year
(M91k9)
Maximum Adjusted PAN
(mg/kg)
Surface
3,290
4,134
Injection/Incorporation
5,159
6,003
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: N/A
FORM: RSC 06-16 Page 4 of 5
7. Pathoeen Reduction: Per 15A NCAC 02T.1106 specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
IM Alternative 1 [15A NCAC 02T.I106(b)(3)(A)] - Time/Temperature Compliance.
Rg Alternative 2 [15A NCAC 02T. I 106(b)(3)(B)] - Alkaline Treatment.
Jffl Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: composting, ❑ heat drying, ❑ heat treatment,
thermophilic aerobic digestion, Q beta ray irradiation,
gamma ray irradiation, or 0 pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T. 1 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, air drying, Q anaerobic digestion,
composting, or lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
IM Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item Il. 7b. above.
Exempt -If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
0. Alternative I [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T,1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Q Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
0 Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
Q Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Q Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals.
[Q Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection.
EJ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
0 Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)].
EJ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5
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BI0-NONIC SERVICES 1:: (704) 529-00
F: (704) 529-1648
A Carylon Company www.bio-nomic.com
CITY OF LENIOR
GEORGE BERNHARDT LAKE RHODHISS WATER TREATMENT PLANT
Residuals Source- Generating Facility Information
- Process Flow Narrative
The City of Lenoir operates an existing water treatment plant at 5474 Waterworks Road, which
produces drinking water for the local community. The source of raw water originates from Lake
Rhodhiss, the second impoundment on the Catawba River.
The George Bernhardt Lake Rhodhiss Water Treatment Plant has been operational since 1956
and has a capacity of 12 MGD. The average daily flow is 6.5 million gallons per day.
Raw water from Lake Rhodhiss is pumped to a dual train Acti-flo mechanical pretreatment unit
capable of processing up to 9 MG on each side. Then the introduction of alum coagulant and an
anionic polymer causes particles to clump together allowing additional sedimentation to occur
with the aid of flocculators and a sedimentation basin.
Upon the completion of settled water, the treated water is gravity fed through 12 mixed media
filtration units. The filtrate is then disinfected using Sodium Hypochlorite, fluoridated, and finally
pH adjusted to produce clear, sediment free finished water. The finished water is then pumped
into clear wells and remote storage tanks ready for distribution. The collected alum sludge and
sediment from the treatment process is discharged into 2 holding tanks in series and
subsequently may be diverted into the original holding lagoon that is to be cleaned out.
The lagoon will hold the sediment until removal is necessary. A portable hydraulic dredge is
placed in the lagoon to pump the materials out of the basin. The floating hydraulic dredge is
advantageous as it allows the lagoon to remain in service during the process. The sediment is
pumped in slurry form to a 20,000-gallon receiving tank. The tank is fitted with mixers to
homogenize the materials for mechanical dewatering.
The mechanical dewatering process is accomplished with a mobile belt filter press system. An
anionic or catanionic polymer is introduced to concentrate the slurry during the dewatering
process. The belt filter press further removes water by compressing the residuals between filter
belts generating a filter cake. The filtrate water resulting from the process can be returned to the
lagoon.
The filter cake, is now suitable for either onsite land application or for loading into dump trucks
for transportation to a secondary application site as a soil amendment.
- Quantitative Justification for Residuals Production Rate
A minimum of 2,000 dry tons may be removed and land applied annually.
A Carylon Company
SAMPLING PLAN
Sampling Procedures
Accurate sampling is essential for valid laboratory test results. All samples collected at the respective
Water Treatment Plant's (WTP) are grab samples, which are samples taken at selected intervals to
represent conditions at a given location at a particular point in time.
Grab samples of residuals are stored in a manner that will not alter sample characteristics. Proper
preservatives are used for specific parameters. The samples are kept under refrigeration at 4° C until
delivered to laboratory for analysis.
Sampling Log
Sampling information is recorded on a chain of custody (COC) form by Bio-Nomic Services personnel
provided by the respective laboratory that is performing the required testing required by the permit. Log
book entries include, at a minimum:
• Purpose of sampling
• Location of sampling point
• Type of sample (grab or composite)
• Name of person collecting samples
• Type of residuals sampled (undigested, post -digestion, post -storage)
• Number and volume of sample(s) collected
• Description of sampling point
• Date and time of collection
The residual solids analysis will be conducted for, but not limited to, the following parameters, percent total
solids, phosphorus, lead, copper, cadmium, sodium, total Kjeldahl nitrogen, nitrate nitrogen, nitrite nitrogen,
magnesium, potassium, zinc, nickel, arsenic, mercury, selenium, molybdenum, calcium, ammonia nitrogen,
aluminum and pH on an Annual Basis, or as required by Permit Conditions based upon annual tons land
applied.
Prepared By:
Lake Rhodhiss WTP
FIELD LOADINGS
DATE SPD: 2019
FARM:
CAKE ACRES:
150.00
SITE:
Plant Site RESIDUALS WET TONS
6,000.0
FIELD:
Wl
WT/ACRE
40.00
CROP:
Bermuda
%TS
31.30
Site Cond
G/D
DT/ACRE:
12.52
a, �a
I)-T45 jk
x 1 so _
�, ��� 6-7"'5
willcox&mabe
SOIL SOLUTIONS
BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 8, 2019
Lake Rhodhiss WTP
31.30 % Solids
6.3 off
Permit No. W00039053
Parameter
%
Mg/Kg Dry Weight
(% x .10,000)
Pounds/Dry Ton
(M /K x 0.hall
Nitrogen (TKN)
0.922
9,220.000
18.440
Phosphorus
0.269
2,686.000
5.372
Potassium
0.159
1,594.000
3.188
PAN (injected)*
0.516
3,869.500
7.739
PAN (surface)*
0.329
3,777.000
7.554
Ammonia Nitrogen
0.374
3,738.000
7.476
Calcium
0.146
1,463.000
2.926
Calcium Carbonate E .
0.000
0.000
0.000
Magnesium
0.213
2,130.000
4.260
Sodium
0.104
1,035.000
2.070
Sulfur
---
---
___
Nitrate N / Nitrite N
---
325.000
0.650
Barium
---
---
Chloride
---
---
---
Iron
---
---
Aluminum
---
2,686.00
5.372
Arsenic
0.46
0.001
Cadmium
---
0.062
0.000
Chromium
---
0.639
0.001
Copper
33.80
0.068
Lead
---
3.09
0.006
Mercury
0.0822
0.000
Molybdenum
0.31
0.001
Nickel
0.31
0.001
Selenium
0.08
0.000
Zinc
---
314.00
0.628
Blue Ridge Labs # LSID-2019-03188
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
SAR
Ceiling Concen.
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or � detection limits are listed as detection limits
for calculation purposes.
s !
Willcox&mabe
Prepared By: S O I L S O L U T I O N S
Willcox & Mahe Soil Solutions, PLLC
Greensboro, North Carolina
RESIDUAL PAN CALCULATION
George L. Bernhardt, Sr. Lake Rhodhiss WTP
TKN=
9,220
mg/kg
NH3=
3,738
mg/kg
NO3-NO2-N=
325
mg/kg
Min Rate=
0.20
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO21
0.20 5,482 1,869 325.00
PAN= 3290.40 mg/kg
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N]
0.10 5,482 1,096
PAN= 438.56 mg/kg remaining from 1st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N]
0.05 4,386 439
PAN= 210.51 mg/kg remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - NJ
0.03 3,947 211
PAN= 124.55 mg/kg remaining from 1st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N]
0.02 3,737 125
PAN= 70.00 mg/kg remaining from 1st year application
Residual PAN from years 2 thru 5 after the initial application = 843.62
Application
Method
First Year PAN
(mg/kg)
Five Year Maximum
Adiusted PAN
Surface
3,290
4,134
Incorporation
5,159
6,003
mg/kg
WN
SAR Calculation
Na m /I
Cam /I
Mg m /I
323.955
457.919
666.69
Na
Ca
Mg
SAR
14.085
22.896
55.558
2.249
Na mil eq
Ca mil eq
Mg mil eq
14.085
22.896
55.558
Enter
Enter .% TS
31.3
Data
Nam /kg
1035
Ca m /k
1463
M m /k
2130
Job Name:
George L. Bernhardt, Sr. Lake Rhodhiss WTP
Page 2
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149 blueridgelabslenoir@gmail.com
Client :
City of Lenoir Water Plant
P. 0. Box 958
Lenoir, NC 228645
Attention:
Mr. Kevin Matheson
Date Received:
08-Oct-19
Report Date:
19-Nov-19
Sample Date:
08.Oct-19
BRL a:
BRL-2019-0839
Reissued
due to
typographical
error.
Lab Sample ID:
LSID-2019-03188
Client Sample ID:
Lenoir Alum Lagoon (Sludge)
Analysis
Anal Vsls
Parameter
Result MQL
Unit
Method
Time
Date
Analyst
%Solids
31.3 0.1
%
%Solids
14:53
10/30/2019
KCJ
Corrosivity as pH
63 0.1
su
9045C SW-8
10:35
10/9/2019
KCJ
pit
63 0.1
SU
SW-846-9040
10:35
10/9!2019
KCJ
lnnitability
>140 70
Deg. F.
SW846-1030
10:15
10/9R019
KCJ
Reported By
S.,1. doh son. D.R. Wessinger
• Concentrations are belwv Minimmn Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page I of I
Blue Ridge Labs
Po Box 2940
Lenoir, NC 28645
828-728-0149 blueridgelabslenoir@gmaii.com
Client :
City of Lenoir Water Plant
P. O. Box 958
Lenoir, NC 28645
Attention:
Mr. Kevin Matheson
Date Received:
08-Oct-19
Report Date:
19-Nov-19
Sample Date:
08-Oct-19
BRL #:
BRL-2019-0839
Reissued due to
typographical error.
Lab Sample ID:
LSID-2019-03196
Client Sample ID:
Lenoir Alum Lagoon
(Sludge)
Analysis Analysis
Parameter
Result
M Q L
Unit
Method
Time Date
Analyst
'rCLPSemi-VOCExtraction extracted
SW-846-1311
Summit
2,4,5-TP(SiNre.o
» O.i
mg.1
SW-846-8080
10/16<2019
Summit
2,4-1)
+ 0.5
mg/l
SW-846-8080
10/10019
Summit
Chlordane
• 0.025
mg/t
SW-846-8080
1011,7,12019
Summit
Endtin
• 0.005
mg4
SW-846-8080
1011V2019
Summit
Heptachlor
* 0.005
mg11
SW-846-8080
10/17l2O19
Summit
Heptachlor Epoxide
* 0,005
mg/l
SW-846-9080
10/17/2019
Summit.
Lindane
* 0.005
mg/l
SW-846-8080
10/1712019
Summit
Methoxvchlor
• 0.005
mg(I
SW-846-8080
10117:2019
Summit
'roxaphene
• 0.05
mg(I
SW-846-8080
1Or17,2019
Summit
Reported By
S. J. hnson, D.R. Wessinger
" Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 1 of I
.,.-..v'..., -_, ,. S'nnenrfl F.imrrmmrnlal ltelnmh>¢idr. lire
WM
19100989
.. E:nvhogul•ald<ohm aa3?3
Datc Repbrtcd:
11/1912019
- - - •- TU.' 13301 '53-6711 R-LY.r (330) 253-4489
Company:
Blue Ridge Labs, Inc.
Address:
P U Box 2940
•
Lenoir NC 28645
Received:
I Oil 112019
ProjeCO:
w'asle Gtaracete
TCLP eY1'etals Analysis (SW1311/6010)
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
3190.3191.3192.3195001
1002019 TCLP Arsenic(As)
0.500
• NO mg/L
Sludge
EPA 6010
1
5.00
10/1512019
EAM
D
^.1U£?lO!'9'la^liar m1
!nl917A7a +. ql Pft=ri=i,rftar
SAn
NO m„n
,.
91:1nc
- ..
PP6 FI)t❑
.
t
lore
wviTS nw
pave
D
3190.3191,3192.3196 001
IOIM019 TCLP Cadmium(Cd)
0.100
NO mg1L
Sludge
EPA 6010
1
1.00
101151201g
FAN
D
3190,3191,3192,3196 001
10/812019 TCLP Chmmlum(Cr)
0,200
NO mg1L
Sludge
EPA S010
1
5.00
1011&2019
EAM
0
3190.3191,3192.3196 001
10192019 TCLP Lead(PC)
0.500
NO mg)L
Sludge
EPA 6010
1
5.00
10/1512019
EAM
D
3190,3191;3192.3196 001
10!812019 TCLP SelenlLrni(Se)
0.0500
NO mgiL
Sludge
EPA5010
1
1.06
1011wola
EAM
r
3 ri,;..r rv1,31 :i.i 9u Gia
iu,ctZo:a rvLr armeriA91
a.pvu
1•)0 Mg'L
aelage
LrA w10
t
6.00
i6r1514rs
L-nrd
D
TCLP Mercury .Analysis (SIVI311(7.470)
Client ID# Lab ID# Collected Analyte
Rep Lent Result Units
Matrix
Method
DF
RegLvl
Ran
Analyst
3190.3191,3192,3196 001
10/812019 TCLP Martyry
0.00200 NO mg/L
Sludge
EPA 7470 A
1
0.200
10/15/2019
MJM
4a .w.w MILV: 11
:1289:
Client ID# Lab ID# Collected Aoalyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
3190.3191,3192,3196 Cal
10IN2019 Chlordane; total
0.0250 NO mgiL
Sludge
EPA 80818
10
0.0300
1011712019
MES
3190.3191,3192,3196 001
101812019 Toxaphene
09500 NO mglL
Sludge
EPA 8081E
10
0.500
1&1712019
MES
3190.3191,3192,3196 001
1018)2019 Enddn
0.00500 NO mglL
Sludge
EPA80818
10
0.0200
1011712019
MES
3190,3191,3192.3196001
10)812019 gamma•SHC
0.00500 NO mglL
Sludge
EPA 80818
10
9.400
10117/2019
MES
3190.3191.3192,319E 001
10IW2019 Heptachlar
0.00500 NO mglL
Sludge
EFIA8081B
10
0.00800
19/1712019
MES
3t90,3t01,3192,3196001
10LO8/2019 HepLchlorepe7ide
0100599 NO mg/L
fudge
EPA. 60818
10
0.00a00
10/172ols
[,DEs
n10-119
�5,.,..,.,..
3190.3191,3192.3196001
1002019 SUm TCMK
66.5 %Rae
Sludge
EPA 8081B
10
1011712019
MES
3190,3191,3f9213196001
101&2019 Sum DC.B
A-119 95.2 %Rea
Sludge
EPA.8081B
10.
10/172019,
MES
Page 5 of 23
wiga Tullf ,S iYlkf
Post Office Box 1056 • Granite FaIls, North Carolina 28630
Phone (828) 396.4444 • EMAIL: tonygragg@watertcchlabs,com
OCTOBER 1 T 2019
CITY OF LENOIR
P. O, BOX 968
LENOIR, NC 28645
SAMPLE I.D.: ALUM LAGOON SLUDGE (WATERTRT PLT)
COLLECTED: 10/08/191420
COLLECTED BY: KEVIN MATHESON
..: FECAL-"COLIFORM BACTERIA (METHOD SM 9223B-MULTIPLE WELL @ 44.5 C)
01 13.2 MPN COLONIES/GRAM
#2 11.8
93 10.8
#4 9.5 "
#5 13.2 °
#6 16.9 "
#7 12.0 °
ANALYSIS BEGIN: 101081191630
ANALYSIS END; 10109119 1630
ANALYZEZYY
DRE Y,
MRAG
NOTE: REVISED REPORT TO INCLUDE ANALYSIS METHOD
W 't �' ? , Inc 9A-
5 Plnewodti Pleiq Dtivo r 1? 0. $ox 9056
Granite Fags, Np 286d0
. .Phone (828) 3.1�8-4444 r Fax (828J 398-6761„ -. -
CLIENT: City of Lenoir " PHONE NUM13ER: 820-S06.1006
P.0.6ox988 TYPE SAMPLE: FilterBacicvlash
Lonolr, NC 28645 No, LOCATIONS: 1
PERPJIITf1: NC0044104. SAMPLER NAME: `Girl U76Y p{�
- Sam-fe'Collection
Infonnatlon
TYPE •
CONTAINERS
1.
ANALYSIS REQUIF
Suniple Location
FacHi Namo..
DATE
TIME
TEMP.°C
Grabl
Composite
Nq'
Plastlal
Glass
Efttt:entj2lttNFltF,j
Grab
1
Plaglla
Tudsldlty.
— Effj=l (Q (3, y
Grab
1
Pfastic
Flo,irld'e'
'�
,,
i's.=',_ui�•
.rk h:
,iti tiirl w
5
%:.; ..
i
OW
tt
1
t2Tab
l
+I
_i
tir W �
RellnquI hed 6y:
TZ
Dater ;
b1gliq
The:
l5:rio
Reclov d , • — .
Date::.
Relinquished By;
pate:
T[mot
Recoiled B :
Date:
ITIme;
PRESERVATION;
ff boQ140C
[JH2SO4
[INp0l4
(JHNO3
(]DochlornatIng Agent
pOther _
SAMPLE TEMP, @JAB yIC
Chlorine Residual
NO CERTIFIED LAB P 60
City of Lenoir
1905 Broadland Road
Lenoir, NC 28633
Receive Date:
Reported:
For:
Comments:
Analytical Results
01/10/2019
01/27/2019
STATESYILLE
ANACYTiCAL
t,
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
190110-25-01
Arsenic - Solid
Lagoon Inf
0.46
mg/kg
SM3113 31004
01/17/2019
MD
190110-25-01
Percent Solids
Lagoon Inf
21
%
SM25408,2011
01/11/2019
MD
190110-25-01
Selenium Solid
Lagoon Inf
<0.003
mg/kg
sm'13B
01/25/2019
MD
190110-25-02
Arsenic - Solid
Lagoon Eff
0.57
mg/kg
SM3113 5-2004
Ot/1712019
MD
190110-25-02
Percent Solids
Lagoon Eff
17.1 -
%
BM3UM2011
01/11/2019
MD
190110-25-02
Selenium Solid
Lagoon Eff
0.95
mg/kg
SM3113B
01/25/2019
MD
Respectfully submitted,
'Ow- ' J'Y'J'Vn
Dena Myers
NC Cert#440,
NCDW Cart #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 3
Condition of Receipt
Sample Number 190110-25-01 Temp on Arrival: 3.2
pH on Arrival: <2 Parameter Schedule:
Nitric Acid Received on Ice
Chemicals in containers, lab
pH on Arrival: <2 Parameter Schedule:
Received on Ice
Chemicals in containers, lab
pH on Arrival: <2 Parameter Schedule:
Received on Ice
Chemicals in containers, lab
pH on Arrival: <2 Parameter Schedule: Arsenic -Solid
Nitric Acid Received on Ice
Chemicals in containers, lab
pH on Arrival: <2 Parameter Schedule: Percent Solids
Nitric Acid Received on Ice
Chemicals in containers, lab
Sample Number 190110-25-02 Temp on Arrival: 3:2
pH on Arrival: <2 Parameter Schedule:
Nitric Acid Received on Ice
Chemicals in containers, lab
pH on Arrival: <2
Parameter Schedule:
Received on Ice
Chemicals in containers, lab
pH on Arrival: <2
Parameter Schedule: Arsenic - Solid
Nitric Acid Received on Ice
Chemicals in containers, lab
pH on Arrival: <2
Parameter Schedule: Percent Solids
Nitric Acid Received on Ice
Chemicals in containers, lab
pH on Arrival: <2 Parameter Schedule:
Nitric Acid Received an Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/87214697
Page 2 of 3
S Jo E OBed
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¢ a: ¢ '¢ ti F F F F
INVOICE
Blue Ridge Labs, Inc. Invoice # 2019- 0869
Date: 10/30/2019
P.O. Box 2940
Lenoir. NC 28645
Phone: 8287280149 Fax: 8287280131
Client: City of Lenoir Water Plant Bill To: City of Lenoir
P. O. Box 958 P. O. Box 958
Lenoir, NC 28645 Lenoir, NC 28645
PO NUMBER LAB REF. ID TERMS LAB CONTACT PROJECT NAME
839 Net 10 Days Steve Johnson Lenoir Alum Lagoon
Sample Name Lenoir Alum Lagoon
TARGET NAME
% Solids
Ammonia Nitrogen
CERTIFIED 200.7 Metals Scan
Corrosivity as pH
Ignitability
pH
SW-846-808018150 TCLP Herb. & Pest.
SW846-7471 B/7470 Hg
SW846-8260B TCLP VOC
SW846-82700 TCLP Semi VOC
SW846-Reactivity
TCLP RCRA Metals
Total Nitrogen
Total Phosphorus
QUANTITY UNIT PRICE EXTENDED PRICE
1
$5.00
$5.00
1
$25.00
$25.00
1
$169.00
$169.00
1
$5.00
$5.00
1
$30.00
$30.00
1
$5.00
$5.00
1
$300.00
$300.00
1
$35.00
$35.00
1
$220.00
$220.00
1
$245.00
$245.00
1
$45.00
$45.00
1
$165.00
$165.00
1
$40.00
$40.00
1
$20.00
$20.00
Please Remit: $1,309.00
Upon submission of samples, buyer agrees that invoices are due at time of delivery. Open accounts are due 20 days following
the invoice date. A finance charge of 1.5 % per month will be imposed on all past -due accounts. When relinquishing samples to
Blue Ridge Labs, buyer agrees to pay all collection and attorneys fees if the account becomes deliquent. Blue Ridge Labs
reserves the right to deny all QC and support documentation for all open accounts which are greater than 60 days. Additionally,
Blue Ridge Labs also reserves the right to inform the appropriate local, state or federal agency that all support documentation
is not available due to the failure to the above Invoice terms. Data used for compliance purposes will be rendered invalid for
reporting until the account is cleared.
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
blueridgelabslenoir@gmail.com
Client : City of Lenoir Water Plant
P. O. Box 958
Lenoir, NC 28645
Attention: Mr. Kevin Matheson
Date Received: 08-Oct-19
Report Date: 30-Oct-19
Sample Date: 08-Oct-19
BRL4: BRL-2019-0839
Lab Sample Ill: LSID-2019-03186
Client Sample ID: Lenoir Alum Lagoon (Sludge)
Analysis Analysis
Parameter Result MQL
Unit Method Time Date Analyst
Ammonia Nitrogen 3738 607
dry mg/kg SM4500 199 15:25 10/18/2019 KCJ
Reported By
011�f
S. J. boson, D.R. Wessinger
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page I of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
blueridgelabslenoir@gmaii.com
Client :
City of Lenoir Water Plant
P. O. Box 958
Lenoir, NC 28645
Attention:
Mr. Kevin Matheson
Date Received:
08-Oct-19
Report Date:
30-Oct-19
Sample Date:
08-Oct-19
BRI. tt:
BRL-2019-0839
Lab Sample ID:
LSID-2019-03187
Client Sample ID:
Lenoir Alum Lagoon (Sludge)
Analysis
Analysis
Parameter
Result MQL
Unit Method
Time
Date
N2+N3
325 47.4
dry mg/kg SM 19 4500-N
15:42
10/16/2019
TKN
9220 588
drying/kg SM194500-N
8:15
10/17/2019
Reported By:
Wessinger
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 2 of 9
Analyst
KCJ
KCJ
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client : City of Lenoir Water Plant
P. O. Box 958
Lenoir. NC 28645
Attention: Mr. Kevin Matheson
Date Received:
08-Oct-19
Report Date:
30-Oct-19
Sample Date:
08-Oct-19
BRL 4:
BRL-2019-0839
Lab Sample Ill:
LSID-2019-03188
Client Sample ID:
Lenoir Alum Lagoon (Sludge)
blueridgelabslenoir@gmail.com
Analysis
Analysis
Parameter
Result MQL Unit Method
Time
Date
Analyst
%Solids
31.3 0.1 % %Solids
14:53
1060/2019
KCJ
Corrosivity as pH
6.3 0.1 su 9045C SW-8
10:35
10/9/2019
KCJ
PH
6.3 0.1 SU SW-846-9040
10:35
10/9/2019
KCJ
Ignitability
Not Ignitable 70 Deg. P. SW846-1030
I0:15
10/9/2019
KCJ
Reported By:
Flinson,
S. D.R. Wessinger
* Concentrations are below Minimum Quantification'L anit except where noted.
NC Laboratory Certificate No. 275
Page 3 of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
blueridgelabslenoir@gmail.com
Client :
City of Lenoir Water Plant
P. O. Box 958
Lenoir, NC 28645
Attention:
Mr. Kevin Matheson
Date Received:
08-Oct-19
Report Date:
30-Oct-19
Sample Date:
08-Oct-19
BRL p:
BRL-2019-0839
Lab Sample ID:
LSID-2019-03189
Client Sample ID:
Lenoir Alum Lagoon (Sludge)
Parameter
Result MQL Unit Method
Reactivity as CN
+ I mg/kg SW-846-7.3.3
Reactivity as Sulfide
* 5 mg/kg SW-846-7.3.3
Analysis
Analysis
Time
Date
Analyst
16:10
10/11/2019
KCJ
15:42
10/11/2019
KCJ
Reported By:
S. J. hnson, D.R. Wessinger
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Pagc 4 of 9
Blue Ridge Labs
PO Boa 2940
Lenoir, NC 28645
828-728-0149 blueridgelabslenoir@gmail.com
Client :
City of Lenoir Water Plant
P. O. Box 958
Lenoir, NC 28645
Attention:
Mr. Kevin Matheson
Date Received:
08-Oct-19
Report Date:
30-Oct-19
Sample Date:
08-Oct-19
BRL #:
BRL-2019-0839
Lab Sample Ill:
LSID-2019-03190
Client Sample ID:
Lenoir Alum Lagoon (Sludge)
Analysis Analysis
Parameter
Result MQL
Unit
Method
Time Date
Analyst
Hg by Cold Vapor AAS * 0.002
mg/I
7470A 1994
10/16/2019
Summit
TCLP Extraction Metals
extracted
SW-846-1311
Summit
A;
0.5
mu/I
SW-846-6010
I015/2019
Summit
As
0.5
mg/I
SW-846-6010
l0il5'2019
Sunvnir
Da
* 5
mg/I
SW-846-6010
10/15/2019
Surnmit
Cd
* 0.1
mg/I
SW-846-6010
10/15/2019
Summit
Cr
* 0.2
mg/l
SW-846-6010
10/15/2019
Summit
Pb
* 0.5
mg/I
SW-846-6010
10/15/2019
Summit
Se
* 0.05
mg/I
SW-846-6010
10/15/2019
Summit
Reported By:
StJsont .R. Wessinger
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 5 of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
blueridgelabslenoir@gmail.com
Client:
City of Lenoir Water Plant
P. O. Box 958
Lenoir, NC 28645
Attention:
Mr. Kevin Matheson
Date Received:
08-Oct-19
Report Date:
30-Oct-19
Sample Date:
08-Oct-19
BRL u:
BRL-2019-0839
Lab Sample ID:
LSID-2019-03191
Client Sample ID:
Lenoir Alum Lagoon (Sludge)
Analysis Analysis
Parameter
Result
MQL
Unit
-
Method
----------- - - -. _._
Time Date
..
Analyst
TCLP ZHE Volatiles Extraction extracted
SW-846-1311
Summit
Benzene
*
0.25
mg/l
SW846-8260
10/14/2019
Summit
Carbon Tetrachloride
*
0.25
mg/l
SW846.8260
10/14/2019
Summit
Chlorobenzene
k
2.5
mg/l
SW846-8260
10/14/2019
Summit
Chloroform
*
0.25
mg/l
SW846-8260
10/142019
Summit
Dichloroethane, 1,2-
*
0.25
mg/l
SW846-8260
10/14/2019
Summit
Dichloroethene, 1,1-
*
0.25
mg/l
SW846-8260
10/14/2019
Summit
MEK
*
5
mg/l
SW846-8260
10/142019
Summit
Tetrachloroethene
0.25
mg/l
SW846-8260
10/142019
Summit
Trichloroethene
*
0.25
mg/l
SW846-8260
10/14/2019
Summit
Vinyl Chloride
0.1
mg/l
SW846-8260
10/14/2019
Summit
Reported By
014;�r
S.:I. tson, D.R. Wessinger
" Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 6 of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149 blueridgelabslenoir@gmail.com
Client:
City of Lenoir Water Plant
P. O. Box 958
Lenoir, NC 28645
Attention:
Mr. Kevin Matheson
Date Received:
08-Oct-19
Report Date:
30-Oct-19
Sample Date:
08-Oct-19
BRI,ii:
BRI, 2019-0839
Lab Sample 1D:
LSID-2019-03192
Client Sample ID:
Lenoir Alum Lagoon (Sludge)
Analysis Analysis
Parameter
Result
MQL
Unit
Method
Time Date
Analyst
TCLP Semi-VOC Extraction extracted
SW-846-1311
Summit
Cresols (Total)
* 10
mg/l
SW-846-8270
10/17/2019
Summit
Dichlorobenzene, 1,4
* 0.2
mg/l
SW-846.8270
10/17/2019
Summit
Dinitrotoluene, 2,4-
* 0.1
m.-/I
SW-846-8270
10/17/2019
SUITtnlit
Hexachloro-1,3-Butadiene
* 0.04
mg/I
SW-846-8270
10/17/2019
Summit
Hexachlorobenzene
* 0.1
mg/l
SW-846-8270
10/17/2019
Summit
Hexachloroethane
* 0.2
mg/l
SW-846-8270
10/1712019
Summit
Nitrobenzene
+ 0.2
mg/l
SW-846-8270
10/17/2019
Summit
Pentachlorophenol
* 0.5
mg/I
SW-846-8270
10/17/2019
Summit
Pyridine
* 0.5
mg/l
SW-846-8270
10/17/2019
Summit
Trichlorophenol,2,4,5-
* 0.5
mg/l
SW-846-8270
10/17/2019
Summit
Trichlorophenol,2,4,6-
* 0.5
mg/1
SW-846-8270
10/17/2019
Summi[
Reported By:
tJ,iso,,
i
•
D.R. Wessinger
* Concentrations are
below Minimum Quantification Limit except
where noted.
NC Laboratory
Certificate No. 275
Page 7 of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client: City of Lenoir Water Plant
P. O. Box 958
Lenoir, NC 28645
Attention: Mr. Kevin Matheson
blueridgelabsienoir@gmail.com
Date Received:
08-Oct-19
Report Date:
30-Oct-19
Sample Date:
08-Oct-19
BRL #:
BRL-2019-0839
Lab Sample ID:
LSID-2019-03193
Client Sample ID:
Lenoir Alum Lagoon (Sludge)
Analysis
Analysis
Parameter _ _
_ Result
MQL
Unit
Method
Time
Date
Analyst
Total Phosphorus
2686
6.18
dry mg/kg
200.7 1994
17:01
10/17/2019
KCJ
Al by ICP-AES
59453
1.54
dry mg/kg
200.7 1994
17:01
10/17/2019
KCJ
Ca by ICP-AES
1463
7.72
dry mg/kg
200.7 1994
17:01
10/17/2019
KCJ
Cd by ICP-AES
*
0-0618
dry mg/kg
200.7 1994
17:01
10/172019
KCJ
Cr by ICP-AES
.r7.3
0.309
dry mg/kg
200.7 1994
17:01
10,' 17/2019
KCJ
Cu by ICP-AES
33.8
0.309
dry mg/kg
200.7 1994
17:01
10/172019
KCJ
K by ICP-AES
1594
149
dry mg/kg
200.7 1994
12:28
10;17/2019
Summit
Mg by ICP-AES
2130
1.54
dry mg/kg
200.7 1994
17:01
10/17/2019
KCJ
Mo by ICP-AES
*
0.309
dry mg/kg
200.7 1994
17:01
10/17/2019
KCJ
Na by ICP-AES
1035
149
dry mg/kg
200.7 1994
12:28
10/17/2019
Summit
Ni by ICP-AES
•
0.309
dry mg/kg
200.7 1994
17:01
10/17/2019
KCJ
Pb by ICP-AES
•
3.09
dry mg/k,
200.7 1994
17:01
10172019
KCJ
Zn by ICP-AES
314
0.309
dry mg/kg
200.7 1994
17:01
10/17/2019
KCl
Hg by Cold Vapor AAS 0.0822
0.0432
dry mg/kg.
7470A 1994
l 1:37
10/24/2019
KCJ
Reported By:
Wessinger
" Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No, 275
Page 8 of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client: City of Lenoir Water Plant
P. O. Box 958
Lenoir, NC 28645
Attention: Mr. Kevin Matheson
blueridgelabslenoir@gmail.com
Date Received:
08-Oct-19
Report Date:
30-Oct- l9
Sample Date:
08-Oct-19
BRL#:
BRL-2019-0839
Lab Sample ID:
LSID-2019-03196
Client Sample ID:
Lenoir Alum Lagoon (Sludge)
Analysis Analysis
Parameter
Result
MQL
Unit
Method
Time Date
Analyst
TCLP Semi-VOC Extraction extracted
SW-846-1311
Summit
2,4,5-TP(Silvex)
•
0.5
mg/I
SW-846-8080
10/16/2019
Summit
2,4-D
*
0.5
mg/I
SW-846-8080
10/16/2019
Summit
Chlordane
*
0.25
m /I
g
SW-846-8080
10/17I20I9
Summit
Endrin
•
0.025
mg/I
SW-846-8080
10/17/2019
Summit
Heptachlor
*
0,025
mg/1
SW-846-8080
10/17/2019
Summit
HeptachlorLpoxide
*
0.025
mg/I
SW-846-8080
10/17/2019
Summit
Lindane
*
0.025
mg/1
SW-846-8080
10/17/2019
Summit
Methoxychlor
+
0.025
mg/1
SW-846-8080
10/17/2019
Summit
Toxaphene
*
0.5
mg/I
SW-846-8080
10/17/2019
Summit
Reported By
.. _ _......---------
5. J. J son, D.R. Wessinger
" Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No.275
Page 9 of 9
E .
t�, - „yy ;� w h'_ ,3E
57wunil h"n-Ironlrrenlal;zclmol3gl s. Inc
A»nisi:nnll �nnn>rF
wnl� .001
Ca,3f 14
Ctvydaga Falls Ohio 44213
(consolidated)
- - ....
M: (330) 253-8211 F.41" (330) 253-4489
14'O#: 19100987
Websile: hllu:!ntmar se//ek cam
Dale Reported: 101ISY1019
I.LtE l:
Blue Rlilae Labs. hic.
C oNction Date:
i0420l 12:02:00 YNI
Project:
Lab Analysis
r ab ln,
19(tvnog;t_003
:t2:trix:
SL'„DUE
Client Sample 1D
3193
Analyses Result PQL Qua] Units DF Date Analyzed
g;erni S AaIALverc MI
Potassium(K)
ODUiui33t1` o)
sWSQ?^ emnnenc n..otr,or oAM
499 46.7 mo/Ka
jz4 4u 7 In9IK9
i G11712G1912:28.01 PIM
lon (2G19 1G:[t}:Gi YM
(1aRl{RIPS: N hloWo�¢tWxs lmprepmnonararolya¢eeeae¢d --. ... _....
N Nadaal lnty/p3tDn Wed to de@rmmearm t6ppBe
Na Not DeNcld p� eMIklhk
R RP6out}idno<¢ptallcuven lma3 RL Repwting Do3Mvn 4rort
\l' Sanlyia Wlg4utll leniµraEu�oeomorruyt as ipa:ifiul u33utwde
Original
Summit Enwail orrnl Technologies, hw• WO8; 191$99$9
rP 3310 Win 51.
- ; r •' ' I> r - Cuyahoga rails, Ohio 44223 pate Reported: 10/21/2019
TEL: (330) 253-8211 FAX: (330) 253— 489 Company: Blue Ridge Labs, Inc.
a'ehai r; httnt.-irrenta'uuak cam
Address: P O Bus 2940
Lenoir NC 28645
Received:. 1011 U2019
Project#: Waste Characete
TCLP Volatiles Analysis
Client ID# Lab W# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
3190,3191,3192,3196 001
10/812019 11-Dichloroethene
0.250
ND mg/L
Sludge
EPA 82601)
50
0.700
10/1412019
SKM
3190,3191,3192.3198 001
10/812019 1,2-Dichloroethane
0,250
NO moll.
Sludge
EPA 82600
50
0.500
10/14/2019
SKM
3 1 Lv,a, 9 i. 3i D25156 VUj
.v,&Lu iu iwEK
5.6Z
NF mq,L
Siuugl'
Er-6260D
50
260
1Ui i42V iJ
JfVN
3190,3191,3192,3196001
101812019 Benzene
0250
NO mg/L
Sludge
EPA 8260D
50
0.500
10/14/2019
SKM
3190,3191,3192,3196 001
10/82019 Carbon tetrachloride
0.260
ND mg/L
Sludge
EPA 82600
50
0.500
10/14/2019
SKM
3190,319l,3i92,3106001
10/8/2019 Chlorobenzene
2.50
ND mg1L
Sludge
EPA 8260D
50
100
10/14/2019
SKM
3190,3191,3192,3196 001
10182019 Chloroform
0.250
NO mg/L
Sludge
EPA 8260D
5o
6,00
10N42019
SKM
3190,3191.3192,3196 001
10/8/2019 Tetrachlemethene
0.250
NO mg/L
Sludge
EPA 82600
50
0.700
10/142019
SKM
3190,3191,3192,3198 001
10/82019 Trichloroethene
0.250
NO mglL
Sludge
EPA 8260D
5o
0.500
10/1412019
SKM
3190,3191,3192,3196 001
10/812019 Vinyl chloride
0.100
NO mg/L
Sludge
EPA 82600
50
0.200
10/14/2019
SKM
� � .,eve uvrSi
1JIxh201J Guf:i
M1-U ,-.
v,
�P rt,uwul
Bromofluorobenzene
3190,3191,3192,3196 001
IOIWO19 Surr:
70.130
86.8 %Rec
Sludge
EPA 8260D
50
10/142019
SKM
Dibromofluoromethane
3190.3191,3192,3196 001
10/82019 Sum., Toluened8
70.130
96.5 %Rea
Sludge
EPA 82600
50
10/14/2019
SKM
TCLP Semi-Volatiles Analysis (SW1311l8270)
Client illlk Lacs lllk Collected Anylyfe Ilan l,me R"Hif baits hinfrir \dnthn,t DF PeaLvl Ran Anayst
3190.3191,3192,3196 001
10182019 14-Dichlombenzene
0.200
ND mg/L
Sludge
EPA 8270E
2
7.50
totl72019
SFG
3190,3191,3192,3196 001
10/8/2019 2,4,5-Trlchlorophenol
0.500
NO mg1L
Sludge
EPA 8270E
2
400
IM7/2019
SFG
3190,3191,3192,3196 001
10/82019 2,4,6 Tdchlorophenol
0.500
NO mg/L
Sludge
EPA 8270E
2
2.00
10/172019
SFG
3190,3191.3192,3196 001
lo/82019 2,4-Dinitmtaluene
0,100
ND mg/L
Sludge
EPA 8270E
2
0.130
10/172019
SFG
3190,3191,3192,3196 001
10/8/2019 Cresols, Total
10.0
ND mg/L
Sludge
EPA 8270E
2
200
10/17/2019
SFG
3190,3191,3192,3196 001
10/812019 Hexachloro-1.3-
0.0400
ND mg/L
Sludge
EPA 8270E
2
0.500
10/17/2019
SFG
butadiene
3190.3191.3192.3196 001
10/8/2019 Hexachlorobenzene
0.100
ND mo/L
Sludoe
EPA 8270E
2
0.130
10117/2019
SFG
J iau,3 /57,51yG,3lfiia vu'1
iuroi2i;iu rlexacriiuwetiiarrt
4.2iw
ND mgrL
Siudye
try: o270c
2
3,U0
ICU 1714i-9
6twG
3190,3191,3192.3196 001
10/8/2019 Nitrobenzene
0.200
ND mg1L
Sludge
EPA 8270E
2
2.00
10/17/2019
SFG
3190,3191,3192,3196 001
10/812019 Pentachlomphenol
0.500
ND mg/L
Sludge
EPA 8270E
2
100
10/17/2019
SFG
3190,3191,3192,3196 001
1018/2019 Pyridine
0,500
ND mg/L
Sludge
EPA 8270E
2
5.00
10/17/2019
SFG
3190,3191,3192,3196 001
10/82019 Sum 2-Fluorophenoi
10-to9
48.4 %Rea
Sludge
EPA 8270E
2
1011712019
SFG
3190,3191,3192,3195 001
10/8/2019 Sun: Phenold6
10-109
54.1 %Rea
Sludge
EPA 8270E
2
10/172019
SFG
3190,3191,3192.3196 001
10IM019 Sun: Nitrobenzene-
19-120
52.7 %Rea
Sludge
EPA 6270E
2
10/17/2019
SFG
as
3190.319'1,3192.3196 OU'I
'1002019 SUIT: 2,48-
lo-120
664 %ilec
S'ludoe
EPA B270F
1.
10117tZ019
SFG
Tribramophenol
3190,3191,3192,3196 001
101812019 Sum. 2-
22-117
48.0 %Rec
Sludge
EPA B270E
2
101172019
SFG
Fluarobiphenyl
3190,3191,3192,3196 001
10/8/2019 Sum. p•Terphenyl-
34-116
79,3 %Rec
Sludge
EPA 8270E
2
10/172019
SFG
d14
f
Page 5 of 21
X„ -- _ _ .S'mnma Kmurornuen/al Technologies. /nc,
µ'p#;
19100989
I. 3310 Win 5r.
Cacahoga Falls, Ohio 44223
Date Reported:
1012112019
-�- •--- - - TEL: (33Q) 253-821 h FAX.• r330) 253-4489
Company:
Blue Ridge Labs, Inc.
1Cehsire, hvn-Ar,t-w setrek o nn
Address:
P O Box 2940
Lenoir NC 29645
Received:
10/11/2019
Project#:
Waste Characete
TCLP Metals Analysis (SW1311/6010)
Client [D# Lab ID# Collected Analyso
Rep Lunt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
31K3191,3192,3196001
10/8/2019 TCLPArsenic(As)
0.500 ND mgIL
Sludge
EPA6010
1
5.00
10/16/2019
EAM
D
Rtan nlni 3102 `iiw; nn1
1nmr2nao Trl a npd,.imtnal
5.on nln �n
.ey,d;,<
nnc Rr11n
r
inn
Intl srpnI9
Fc[n
D
3190.3191.3192,319E 001
10/8/2019 TCLP Cadmlum(Cd)
0.100 NO mgIL
Sludge
EPA 6010
1
1,00
10/15/2019
EAM
D
3190,31131,3192,3196 001
1018/2019 TCLP Chmmium(Cr)
0.200 ND mg/L
Sludge
EPA 6010
1
5.00
10/15/2019
EAM
D
3190.3191,3192,3196 001
10/512019 TCLP Lead(Pb)
0.500 ND mg/L
Sludge
EPAS010
1
6.00
10/15/2019
EAM
D
3190,3191,3192,3196 001
10/8/2019 TCLP Selenium(Se)
0.0500 NO mg1L
Sludge
EPA 6010
1
1.00
10/15/2019
EAM
D
Jieu,Jii".3192,3196 uui
1Ut6t2Uiy ri,LP bnyer(Ag1
0.5uu NU mg/L
oluage
LrAoulu
1
5.W
10n6Qu iS
LAiA
D
TCLP Mercury Analysis (S W 1311/7470)
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run Analyst
3190,3191,3192,3196 001
10/8/2019 TCLP Mercury
0.00200 NO mglL
Sludge
EPA 7470 A
1
0.200
10/1612019
MJM
TC'r.P Pectieiape A naivsie(SW 1311/80811
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
3190,3191,3192,3196 001
10/812019 Chlordane, total
0.250
ND mgIL
Sludge
EPA 80618
10
0.0300 10/1712012
MES
3190,3191,3192,3196 001
1002019 Tomphene
0.500
ND mg/L
Sludge
EPA 6081E
10.
0.500 10117/2019
MES
3190,3191,3192,3196 001
10/8/2079 Enddn
0.0260
NO mgIL
Sludge
EPA 8081E
10
0.0200 10/17/2019
MES
3190,3191,3192,3196 001
10/8/2019 gamma-BHC
0.0250
NO mg/L
Sludge
EPA 8081a
10
0.400 10/1712019
MES
3190,3191,3192,3196 001
10/8/2019 Heptachlor
0.0250
ND mg&
Sludge
EPA 8081E
10
0.00e00 10(1712019
MES
3190,3191,3192,3196 001
10/8-12019 Heptachlor epoxide
0.0250
ND mg1L
Sludge
EPA 8081B
10
0.008001011712019
MES
3190,3191,3192.3196 001
10/8I2019 Sum: TCMX
10-119
66.5 %Reo
Sludge
EPA 8081E
10
10/17/2019
MES
3190,3191,3192,3196 001
10/8/2019 Sum DCB
10-119
95.2 %Rec
Sludge
EPA 60819
10
10117/2019
MES
Page 4 of 21
S'trmmff Em4ronmenral Ttchnoragres, hie.
3910 WM Sr,
Cgvahoga l ults. Ohio 44223
TEL: (330) 253-8211 F4X: (330) 253-4489
(Mnlrer hr1n.> dau wsenzk.cnne
WOO:
19100989
Date Reported:
10212019
Company:
Blue Ridge Labs, Inc.
Address:
P O Box 2940
Lenoir \C 28645
Received:
I Oil 1i2019
Projected:
Waste Characete
SVOC SW-846: 8321 Herbicides-TCLP
Client ID# Lab lD# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl Run Analyst
3190,3191,3192,3196 001 1018/2019 2,4-6
0.500 NO mg!L
Sludge
EPA 8321 A
50
10.0 10/1612019 BJH
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