Loading...
HomeMy WebLinkAboutWQ0035595_Modification_20191209Initial Review INITIAL REVIEW Reviewer Thornburg, Nathaniel Is this submital an application?* r Yes r No Is this a complete application?* r Yes r No Project Number* WQ0035595 Applicant/Permittee Granville Farms, Inc. Applicant/Permittee PO Box 1396 Oxford, NC 27565 Address Is the owner in BIMS? r Yes r No Owner Type Organization Facility Name Granville Farms RLAP County Edgecombe Complete App Date 12/09/2019 Is the facility in BIMS? r Yes r No Fee Category Fee Amount Major $395 Signature Authority Jason Smith Signature Authority Title Vice President Signature Authority Email jsmith@granvillefarmsinc.com Document Type (if non -application) Email Notifications Does this need O Yes review by the r No hydrogeologist? * Regional Office Raleigh CO Reviewer Ranveer Katyal: eads\rkatyal Admin Reviewer KendalI.Williams@ncdenr.gov Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notification Comments for Kendall Comments for RO Comments for Reviewer Comments for Applicant Submitted Form Project Contact Information Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues. ........................................................................................................................................................................................................................................................................................................................................................................ Name * Drew Matthews Email Address* dmatthevvs@soilplus.net Project Information Submittal Type* r New Permit Application r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number WQ0035595 currently has project Applicant\Permittee * Granville Farms, Inc. Applicant/Permittee PO Box 1396 Oxford, NC 27565 Address* Facility Name * Granville Farms RLAP Phone Number* 2528839301 r Modification (Major or Minor) r Additional Information r Other r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) GFI WQ0035595 Permit Mod Dec 19.pdf 79.75MB Upload only 1 RDF document. Maniple documents must be combined into one RDF file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contactthe reviewer or Tessa Monday. If a paper --polka*-ion is required, be advised, applications accepted' far pre -review until both the paper and eIect-c-,i_ co1)ies nave been received. The paper copy shall include the following: o Application Form o All relevant attachments (calcs, soils report, specs, etc.) o One full-size engineering plan set o One 11x17" engineering plan set o One extra set of specifications o Fee (if required) MallinE address: ❑iuision of Water Resources1 Division of Water Resources Non -Discharge Branch I Non -Discharge Branch 1617 Mail Service Center 1 Aft: Nathaniel Thornburg, 91° Floor, Cfice #942W ----------------------------------------------------------- ----------------------------------------- Raleih, NC 27699-1617 512 N. Salisbury St. Far questions or problems contact Tessa Monday attessa.monday@ncdenr.Qov or 919.707.3560. * W By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature 0- � Submission Date 12/9/2019 GRANVILLE FARMS, INC. PERMIT MODIFICATION CLASS B PROGRAM WQ0035595 Submitted by: Soil Plus PO Box 1396 Oxford, North Carolina 27565 December 9, 2019 SOIL PLUS SOIL PLUS December 9, 2019 NCDEQ-DWR Non -Discharge Branch 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Mr. Nathaniel Thornburg Reference: PERMIT MODIFICATION Granville Farms, Inc. Residual Biosolids "Class B" Program Permit # WQ0035595 Soil Plus Project No. 200705.D10 Mr. Thornburg: Soil Plus, LLC (Soil Plus) is submitting one paper copy and one electronic copy of this permit modification application package for Granville Farms, Inc. (WQ0035595). This package includes: 1. Completed Residual Land Application Program Application 2. Completed Residual Source Certification Attachment a. Arbor Hills MHP (New) b. Birchwood RV Park (New) c. Chapel Ridge WWTP (New) d. Cottonwood/Baywood WWTP (New) e. Lake Royale WWTP (New) f. Lewiston Woodville WWTP (New) g. Hominy Creek WRF (Modified) h. Perdue WWTP (Modified) 3. Completed Land Application Site Certification Attachment a. Eddie Brown (EB) This package is designed to add (6) new facilities, increase the permitted dry tonnage for (2) facilities, and add (4) fields in Martin County totaling approximately 68 acres. A check for $395 is enclosed with this package per the Division of Water Resources Land Application Unit's fee schedule for a major modification to a major non -discharge permit. Soil Plus will be responsible for completing this permit application for the Granville Farms, Inc. If there is any further information required or questions regarding this permit application, please do not hesitate to contact me for assistance. PO Box 1396 Oxford, NC 27565 Respectfully, (252) 883-9301 dmatthews@soilplus.net wwwsoilplus.net Drew Matthews, Soil Plus LLC Jason Smith, Granville Farms Inc. Residual Land Application Program Application Weighted Source PAN Calculations Revised O&M Plan Residual Source Certification Attachment Arbor Hills MHP Analytical/Field Loading Calculations Residual Source Certification Attachment Granville Birchwood RV Park Analytical/Field Loading Calculations Farms, Inc. Residual Source Certification Attachment Chapel Ridge WWTP Permit Analytical/Field Loading Calculations Modification Residual Source Certification Attachment Cottonwood/Baywood WWTP Analytical/Field Loading Calculations WQ0035595 Residual Source Certification Attachment Lake Royale WWTP E dge c o mb e Analytical/Field Loading Calculations County, NC Residual Source Certification Attachment Lewiston Woodville WWTP Analytical/Field Loading Calculations Residual Source Certification Attachment Hominy Creek WRF Analytical/Field Loading Calculations Residual Source Certification Attachment Perdue WWTP Analytical/Field Loading Calculations Land Application Site Certification Attachment Site EB Land Owner Agreement Form Martin County Board of Commissioners Notification / Maps Soil Scientist Certification and Borings Biosohd Utilization Calculations / Sod Samples APPENDIX 1 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Land Application Program Application RLAP Weighted Source PAN Calculations Revised O&M Plan State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 03-15 I. APPLICANT INFORMATION: 1. Applicant's name: Granville Farms, Inc. Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State ❑ Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Jason Smith Title: Vice President Applicant's mailing address: P.O. Box 1396 City: Oxford State: NC Zip: 27565- Telephone number: (919) 690-8000 Email Address: jsmithkgranvillefarmsinc.com 2. Consultant's name: Drew Matthews License Number (for P.E.): Affiliation: ❑ On Staff ® Retained (Firm: Soil Plus, LLC) Consultant's mailing address: PO Box 1396 City: Oxford State: NC Zip: 27565- Telephone number: (252) 883-9301 Email Address: dmatthewsksoilplus.net 3. Agronomist's name: License Number: Affiliation: ❑ N/A ❑ On Staff 0 Retained (Firm: ) Agronomist's mailing address: City: State: Zip: - Telephone number: (_) _- Email Address: 4. Soil Scientist's name: License Number: ME Affiliation: 0 N/A ❑ On Staff N Retained (Firm: _) Soil Scientist's mailing address: _ City: = State: Zip: �- Telephone number: O - Email Address: 5. Fee submitted: $395.00 (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): M new, ® modified, ❑ renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: WQ0035595 Date of most -recently issued permit: October 10, 2016 Date of most -recently certified Attachment A (if different than the permit): April 17, 2019 Date of most -recently certified Attachment B (if different than the permit): April 17, 2019 FORM: RLAP 03-15 Page 1 of 5 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: NA City: State: Zip: - Coordinates: Latitude: _° Longitude: Datum: -M Level of accuracy: Method of measurement: County where residuals land application program is headquartered: _ 1. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Jason Smith Granville Farms, Inc. 13266 Back -Up ORC Bryan A. Smith Granville Farms, Inc. 13265 Additional Back -Up ORCs if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 2. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 8,701 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 33.58 48.05 292,221 418,057 Five -Year Maximum Adjusted 47.69 58.48 414,991 508,872 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation Row Crops 415.21 Hay 181.14 Pasture Total: 596.35 Methods Surface 596.35 Incorporation or Injection Total: 596.35 FORM: RLAP 03-15 Page 2 of 4 c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Application Rate (lbs PAN/ac yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 5,844.43 8,361.13 8,299.81 10,177.43 100 2,922.21 4,180.57 4,149.91 5,088.72 150 1,948.14 2,787.04 2,766.60 3,392.48 200 1,461.11 2,090.28 2,074.95 2,544.36 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): Many of these sources will also maintain their current land application program in coniunction with this one. Basicallv for most sources this Dermit will not serve as an exclusive land application moeram. but rather as a supplement. 7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated If Dedicated, specify the following (check all that apply): ❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; I ❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; -A IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. IR Land Application Siite Certification.doc FORM: RLAP 03-15 Page 3 of 4 Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. Yes No, Explain; . I, Jason Smith Vice President (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for Granville Farms. Inc. (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. JSignature: qoCir1 � .��1� Date: FORM: RLAP 03-15 Page 4 of 4 Q a 4 4 O� 0 0 M O E; ' .m. c, a a I 0 0 o O N, O c O ti A O n 8 M o 4 N L r � 0 0 0 0 0 0 0 0 0 �D a o 0 0 0 0 pnp .� .� o N r GNi N a O N Ni N C I a r o N o o M e mr a w n 0 0 N f o ll�M 0 g M M M M M N M N M 0 0 0 0 .M+ M a c 0 0 0 0 0 0 0 cr�l .. N O a O N N 0 0 0 cat O O O O O O b cV G C G O G O C O C O .+ O C O G O G C C O G M...... C a a c a 1a� � M r N 1 V" -F NS a" r P r IV' m 1, M r M W O S 1,1. 4V 9 & 1,S N 'n M M O . C. M r M . N .� O M M . .� 1� cVi ? yy a �'. . M M a r r . .. G p N N V .• �O .. �O N . M oD If C � .+ rN M N a0 1� W vi O o G,� a 'V .+ N O O C O C O 0 0 0 .� O O C 0 0 0 0 0 0 .+ ..-� C O O O O O O O C C M Ni O O O O O C O a W i O r O Q ~ ~ a P z U O C/11814/1 & Mm 1.1 O"^218 iM1 O M& N W rrI11 M W a� 11 r C r m m m E. F4� N 0N KO oo s C a M o2 Nr,NSNM M r -..1 Ca N N r ONO Y C O If O M TA 14,16 OM N�N w N W rr M T 1 Y O M� — N N N N N - M — N N — — — — N N N N — — - N .- � N N � — N — — - — N — N N — .. — — a N P. 1 O O S O MO O O� O O N O O MO O O O� N M r O 0 0 0 0 0 0 S 2 O N M~ W N 8 .� M a .n. S N O .n+ .-. . . . N . O .-� O O r 0 0 0 0 0 C\ (V 0 0 0 0 0 0 0 0 C\ O N 0 0 0 0 0 0 0 0 vMi N N N N N r m d O O N . . . O O m ~V' MV' m O r .-� N C C .-C` C` . .� C` O � . rl � V (V . . . O c0 0o a N rl O G M Ih 0 0 0 0 0 0 0 0 0 0 o M o 0 0 0 0 0 0 0 0 0 o vi o C S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S S O Q U A, `" v w° vQ� o o q T B '� '° v '3 U > ""a ra r o g c '� o 'a 'a n, v❑ o z, C A A 3 q o � U u o 00 0 0 a .-�N GRANVILLE FARMS, INC. OPERATION AND MAINTENANCE PLAN LAND APPLICATION OF CLASS B RESIDUAL BIOSOLIDS WQ#0035595 Revised October 2019 1.0 SUMMARY Granville Farms, Inc. (GFI) is a privately owned company that is contracted to haul and land apply nutrient enriched by-products such as Biosolids from Wastewater Treatment Plants, Residuals from Water Treatment Plants, Animal Waste from Animal Production Facilities, and certain Construction Debris from Road Work (i.e. slurry water from diamond cutting of concrete). GFI is unique in that it does not participate in the generation or treatment of the by- products generated by any of the source types listed above. At times GFI is requested to provide lime stabilization of Biosolids by smaller operating facilities, but this quantity is normally very small. GFI's main role is to provide transportation and operational equipment to spread the nutrient enriched by-products listed above. Another unique characteristic about GFI is that it owns and maintains permits to land apply these by-products. Given that most generators are issued their own land application permit, they have direct oversight of the preparation, removal, and application of their by-products. This creates some operational and permit challenges for GFI since standard, state issued permits are typically issued to generators not land application companies. This Operation and Maintenance Plan (O&M) addresses how GFI is able to manage by-products produced by multiple, independent generators and land applies under their own land application permit. Revised 10/19 ©Granville Farms, Inc. Operation and Maintenance Plan GRANVILLE FARMS O&M PLAN SAMPLING & ANALYTICAL 2.0 ANALYTICAL REQUIREMENTS Prior to the hauling and land application event being schedule the generator must provide analytical results documenting that all parameters listed in Condition IV. 2 — 4 and at the frequency listed in most recent copy of this permit. If GFI does not collect the sample then it DOES NOT own the responsibility of the integrity of the sample and the method it was collected, transported, submitted, and analyzed. Should the generating source elect to have GFI collect the sample prior to land application, then it will be done in the following manner: Four factors that may ultimately affect the integrity of reported data include: 1) obtaining a representative sample, 2) preventing contamination of the sample, 3) providing legal documentation of the sampling event, and 4) protecting the sample from chemical, physical or biological change prior to analysis. A sample will be collected according to the schedule provided in the most recent copy of the Attachment of this permit and prior to land application one composite sample should be pulled from a designated location from the generating source. GFI has identified Meritech, Inc. out of Reidsville, NC to be used as the Certified Laboratory. The composite sample should be analyzed for: • % Solids, • Nitrogen Series (TKN, Ammonia, Nitrate, Nitrite, and Organic Nitrogen), • Phosphorus, • Potassium, • Sulfur, • Calcium, • Magnesium, • Sodium, • Iron, • Aluminum, • Manganese, • Copper, • Zinc, • and Remaining 503 Metals (i.e. Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium) Approximately 2 quarts of residual should be collected. The sample containers should be clean and sterile. They should also be labeled so that they are easily identifiable in the lab. The samples should be pulled using the method listed below: ❖ Collect one sample from each digester(s) from which the material will be land applied using a "swing sampler" o The swing sampler must be used with a sterile, plastic 960 ml container ❖ Combine each sample in a stainless steel bucket ❖ Mix thoroughly using a fiberglass rod ❖ Collect each sample from the top of the access point at each digester. This access point is obtained by climbing the installed ladder on the side of the digester. Revised 10/19 ©Granville Farms, Inc. Operation and Maintenance Plan Once the sample is pulled, it should be placed in medium size cooler packed with ice. The sample should be collected with an enough time so that it can be delivered to the laboratory. Once per calendar year (if applicable) a sample should be collected and submitted to Meritech, Inc. in Reidsville, NC. This sample should be analyzed for: • Full TCLP • Ignitability, Corrositivity, and Reactivity • Requires 5 Liters (In Opac Glass Bottles) If required, a third should be submitted to Meritech, Inc. for a 30-Day Scale Bench test and Fecal Colifom Density. The 30-Day Scale Bench Test also requires 1 quart of "clear" water from the Clarifier for Dilution if necessary. This sample would be analyzed for: • 30-Day Scale Bench Test (4 Quarts of Residuals and 1 Quart of Clarifier water) • Fecal Coliform Density Test (seven pint samples) The contact information for the lab is: Mailing Address Meritech, Inc. 642 Tamco Rd Reidsville, NC 27320 (336) 342-4748 Sampling frequency will be conducted in accordance with the Table listed in the most recent Attachment A of this permit. The sample will be collected by a representative of Soil Plus, LLC. For further information please contact: Drew Matthews PO Box 1396 Oxford, NC 27565 252-883-9301 Revised 10/19 ©Granville Farms, Inc. Operation and Maintenance Plan GRANVILLE FARMS O&M PLAN OPERATION, SPILL CONTROLL, & TRAINING 3.0 BIOSOLIDS REMOVAL, TRANSPORT, AND APPLICATION Biosolids will be transported from the generators to suitable, permitted land application sites. Transport equipment will be inspected, licensed and appropriately marked, as required, for the purpose of transporting biosolids. Biosolids will be delivered to the application sites between sunrise to sunset. Both liquid and dewatered biosolids distribution on the land application sites will be uniform throughout the application area. To ensure adequate control of the application rate for each site, the equipment used for spreading the sludge will be calibrated by measuring the amount handled on a known square footage. While the rate of discharge from the application vehicle is fixed, the speed of the equipment can be adjusted to maintain the flow rate needed to achieve specific application rates. Spreading operations will be discontinued during periods of inclement weather and will not be resumed until sufficient drying of the fields has occurred. This allows equipment access without causing excessive soil compaction or rutting. To prevent adherence of the biosolids, transport vehicles will be equipped with rear mud flaps, thereby preventing biosolids from being tracked onto roadways. Biosolids adhering to the mud flap will be scraped off in the field before the truck returns to the roadway. Examples of our application tracking and summary form/reports can be provided upon request. 4.0 SITE OPERATION Biosolids will be surface applied at the properly -calculated agronomic rate and in strict accordance with any state and federal regulations for the land application of the biosolids. Buffer zone distances will be observed in accordance with applicable state and federal regulations. Buffer zones will be flagged and no biosolids will be applied within those areas. The most restrictive buffer will apply in combined situations. Operational provisions will be taken to prevent soil loss through erosion. Provisions will include contour application and avoidance of areas where surface drainage patterns result in concentrated flow of runoff from rainfall. In accordance with sound, industry standard agronomic practice, areas which are unseasonably wet (and would produce rutting or damage to the field) will not be utilized for biosolids application operations during those periods. Operations will be discontinued when soils are saturated and will not be resumed until the field has sufficient dried. The amount of biosolids applied will not exceed the hydraulic capacity of the soil at the time of each application. If a subsequent pass across a field is necessary to achieve the desired application rate, sufficient drying time will be allowed between passes. 5.0 PROJECT CONTROL To ensure biosolids are continuously applied at the correct application rate and in a manner consistent with the Operations Plan, a GFI Project/Field Manager will be in direct charge of the field operations, controlling the amount of biosolids delivered to each field, and conducting daily field inspections. Field inspections will include ensuring that flags are in place, biosolids are applied uniformly at the designated application rate, setbacks are observed, trucks are unloading at best location, trucks are not driving over biosolids, trucks are cleaned before leaving the field and the land application equipment is maintained in working condition. 6.0 TRANSPORTATION SYSTEM ROUTING Per the specifications, GFI transportation vehicles will be equipped with GPS devices that will guide drivers to the land application sites. Transportation routes will follow primary highways and avoid residential areas where possible. Designated routes are followed unless a detour is specified. In the event of a detour route, it shall be taken as specified by the detour authority. There shall be no unscheduled stops when loaded. Transportation vehicles will be inspected, licensed and appropriately marked as required with identification numbers for the purpose of this contract. All units will be equipped with spill guards and full mud flaps. This will prevent the biosolids from adhering to the tires and undercarriage of the transport vehicle, thereby preventing biosolids from being tracked onto roadways. Biosolids adhering to the mud flap will be scraped off in the field before the truck returns to the roadway. All federal OSHA Revised 10/19 ©Granville Farms, Inc. Operation and Maintenance Plan and DOT laws and regulations are complied with for the protection of our clients, the community and our drivers. Examples of vehicle and driver transportation logs and inspection forms can be provided upon request. 7.0 DEWATERED BIOSOLIDS Dewatered biosolids will be transported in standard end dump trailers with a capacity of 22 wet tons. The tankers will be loaded per the generator's specifications and standard protocols. The aluminum dump trailers used for transportation of dewatered cake biosolids will be equipped with sealed tailgates and will be completely sealed to prevent leakage. All trucks will be fully covered and will be fitted with positive lock tailgates. 8.0 LIQUID BIOSOLIDS Liquid biosolids will be transported using 6,500 gallon capacity liquid tankers, pulled by standard road tractors, for liquid biosolids transportation. The tankers will be loaded per the generator's specifications and standard protocols. The tractor/tanker unit will transport its load to a designated staging area inside the buffered area of a permitted land application site. 9.0 APPLICATION (SPREADING) — DEWATERED BIOSOLIDS At the staging area each load will be unloaded in.a designated area within the land application site. Biosolids will be loaded into our Side Slinger cake box by a GFI employee using a front-end loader. This unit is capable of delivering an accurate, calibrated application of dewatered biosolids over the application site. The uniform spread pattern ensures that biosolids are applied at proper agronomic (nutrient) and hydraulic loading rates. The application rates for each site, and its corresponding crop, will be determined based on the Plant Available Nitrogen (PAN) content of the biosolids, or other limiting factors. Typical applications will deliver between 75 and 100 percent of a crop's annual PAN requirement. 10.0 APPLICATION (SPREADING) — LIQUID BIOSOLIDS At the staging area each load will be transferred into a 4,000 gallon capacity pull behind subsequent land application. This unit is capable of delivering an accurate, calibrated application of liquid biosolids over the application site. The uniform spread pattern ensures that biosolids are applied at proper agronomic (nutrient) and hydraulic loading rates. The application rates for each site, and its corresponding crop, will be determined based on the Plant Available Nitrogen (PAN) content of the biosolids, or other limiting factors. Typical applications will deliver between 75 and 100 percent of a crop's annual PAN requirement. 11.0 SPILL AND EMERGENCY RESPONSE PROGRAM In the unlikely event of a spill, GFI will take the following actions immediately. • Halt Source of Spill. Use of any leaking or damaged unit which is causing the spill will cease immediately. The unit will be repaired before resuming its use. • Contain Spill. In the event large quantities of biosolids have been spilled, straw bales will be used where available and as necessary to either form a barrier or absorb biosolids. • Clean -Up. Depending on the type and amount of biosolids spilled, a variety of equipment may be used to remove the biosolids: front-end loader, shovels and brooms and vacuum equipment of a liquid biosolids applicator. Any biosolids removed from the spill site will be spread on an approved application site, returned to the WWTP, or disposed of in an approved landfill. Revised 10/19 ©Granville Farms, Inc. Operation and Maintenance Plan • Final Clean -Up. Flush roadways with water or sweep as necessary to clean. Allow to dry and incorporate if spill occurs on non -paved and tillable area. In the event a spill occurs on private property, final clean-up should be completed immediately to the satisfaction of the owner. • Management of Clean -Up Efforts. The Operations Manager will take immediate charge and initiate clean-up activities. GFI labor will be used, with additional labor secured as needed. The Operations Manager will also communicate with the public on the scene, answering questions and advising of clean-up activities. • Reporting. All spills will be reported immediately to GFI offices and the client. State and local agencies will be notified in accordance with their notification requirements. Within 24 hours of the spill, the Operations Manager will send GFI office a written report detailing how the spill occurred and remedial action taken. This report will be provided using the enclosed Spill Report form. • Spill Prevention. The Operations Manager will implement the following spill prevention measures: o Ensure truck drivers watch trailer while loading and do not overload; o Ensure trailer hatches are closed and latched while transporting; o Ensure trailer seals are inspected on a daily basis and replaced as necessary; and o Ensure unloading operations in the field are conducted to minimize any potential runoff or tracking. All employees receive safety and spill response training as part to their new hire training and thereafter participate in our monthly safety and spill response training program. In addition to our internal training and protocols, we also contract with a regional emergency response firm - HEPACO - available to respond to an incident in the Central and Eastern North Carolina area within two hours. A copy of our agreement with HEPACO can be provided upon request. Names and Titles of Inspection Personnel Andy Smith, Area Supervisor Jason Smith, Area Supervisor JT Bryant, Regional Supervisor Jay Bryant, Project Supervisor Matt Foster Project Supervisor BJ Bryant, Field operator Jeff Bumpass, Field operator Tammy Walston, Field operator 12.0 PREVENTION The goal of a compliance assurance system is to prevent compliance issues from occurring. Prevention involves: • Ensuring personnel understand their role in assuring compliance; • Identifying compliance requirements at the federal, state and local levels; • Implementing a system where compliance tasks are scheduled, assigned and tracked to completion; • Developing standard operating procedures where appropriate; and • Reviewing the compliance task list and standard operating procedures on an ongoing basis and modifying them as appropriate to account for changes in regulations/requirements and operating methods, and to address compliance deficiencies. Revised 10/19 ©Granville Farms, Inc. Operation and Maintenance Plan GFI ensures employees understand their role in assuring compliance through new employee orientation programs and on the job training. 13.0 Standard Operating Procedures (SOP's) GFI develops and implements SOPs to ensure compliance tasks are completed consistently across the company. The SOP provides standard forms to use, approved biosolids analytical methods, frequency of monitoring information, etc. Another key SOP relative to preventing compliance issues from occurring is the use of a "Pre - Operating and Buffer Checklist". The Pre -Operating and Buffer Checklist ensures federal, state and local regulations and permit requirements are met prior to initiating biosolids applications at field sites. Compliance items on the Checklist include: • The field is permitted and suitable for the biosolids/residuals type being applied; • Pre -application requirements are met; • Farmer and landowner agreements are current and the crop to be grown has been verified; • The field is flagged to prevent applications in buffer zones and restricted areas; • The appropriate application rate and field capacity is calculated; and • Any special permit or local requirements are met. • A listing of the buffer zones and restricted areas where biosolids/residuals cannot be applied • A listing of operating requirements including notification requirements, • application method requirements, and inclement weather operating requirements 14.0 ASSESMENT To help ensure compliance requirements are being met and the compliance assurance system is implemented and working, periodic, consistent, objective and documented assessments of a project/facility's compliance status are conducted. GFI personnel have clearly -defined compliance assessment responsibilities and time to conduct such assessments. GFI conducts informal site inspections and formal audits on an ongoing basis. 15.0 CORRECTIVE ACTION Once compliance issues have been identified during the course of day to day business and through internal audits and inspections a system must be in place which ensures that appropriate and timely corrective action is taken, the cause of the compliance issue is identified and actions are taken to prevent recurrence of the issue. GFI's goal is to have no instances of non-compliance. However, issues and incidents may occur and when this happens employees work to correct the incident in a timely and thorough manner. When compliance issues are identified, the situation is examined to determine the root cause of the problem and the corrective and preventive action that must be taken. The preventive action must address the root cause with the goal of preventing a recurrence. Depending on the nature of the compliance issue, it is assigned to one or more responsible parties to ensure that the corrective and preventive actions are implemented. A deadline for completion of the task is assigned and the issue is tracked to completion by regional and corporate compliance personnel. 16.0 TRAINING An effective compliance training program involves: • Identifying training needs and requirements; Revised 10/19 ©Granville Farms, Inc. Operation and Maintenance Plan • Assigning personnel to provide training and providing them the resources they need to conduct training; • Documenting and tracking that mandatory t raining has occurred; and • An employee's training needs and requirements, as well as their training responsibilities, are based on his/her position within the company. Revised 10/19 ©Granville Farms, Inc. Operation and Maintenance Plan GRANVILLE FARMS O&M PLAN PROCESS FLOW DIAGRAM GRANVILLE FARMS CLASS B WWTP SOURCES Ahoskie WWTP Amherst WWTP Arbor Hills MHP Ashley Hills WWTP Avocet Barclay Downs WWTP Beachwood WWTP Birchwood RV Park Briar Chapel WWTP Briarwood Farms WWTP Carolina Meadows WWTP Chapel Ridge WWTP Cole Park Plaza Colvard Farms Contentnea MSD Cottonwood/Baywood WWTP Crooked Creek WWTP Cross Creek WWTP Deerchase WWTP Govenor's Club WWTP Hasentree Golf Community Hawthorn Subdivision WWTP Hominy Creek WRF Kenly Regional WWTP Kings Grant Subdivision Knightdale Mobile Home Park Lake Ridge WWTP Lake Royale WWTP Legacy at Jordan Lake Lewiston Woodville WWTP Mallard Crossing WWTP Nature Trails MHP WWTP Neuse Colony WWTP Neuse River RRF Neuse River Village Perdue WWTP Pikeville WTF Plymouth WWTP Preserve at Jordan Lake River Mill WWTP Robersonville WWTP Rock Bridge WWTP Snow Hill WWTP Stantonsburg WWTP Tar River Regional WWTP Tarboro WWTP Tradewinds WWTP Westfall WWTP Williamston WWTP Whippoorwill Valley WWTP Wildwood Green WWTP Willowbrook WWTP These sources coorespond to the attached flow diagram provided below. m L co U U U a 0) LU N 2 L ot V Y� L! yn Cr LL b J � L Q aD � L co Q o U J Q a LU c 0 Un a � Uod abpnlS palenllOV ua nja�{ cu mL W Q a ) Q �.± O O J od N Q 40 LU J Y L LE a a J �y J O V X O m C O C GRANVILLE FARMS CLASS B WTP SOURCES Martin County WTP Sunset WTP Tar River WTP These sources coorespond to the attached flow diagram provided below. 70 _ m 1 i i2 Q Q)_ Q c c a •� W co CO 0 V ood O �_ (0 CID J LL J •i� r'n C U) > m _0 O E cu 0 i) a) U) 0 N m o o U) 0 J � a U � U N 0 O c0 LL 0) V/ cu U � �y O m N a cu c ii = � o JFL V N--V,l/11i a/ U a E L W U J J_ Z aD cu a� U 0 cu 3 c0 GRANVILLE FARMS O&M PLAN MAXIMUM PRODUCTION QUANTIFICATION & JUSTIFICATION AVERAGE Nof Forecasted Requested Gallons Dry Tons WWTP Years Counted Production DT 1,452,660 166.81 Ahoskie WWTP 5 AhoskieWWTP 333.62 280 45,390 2.87 Amherst WWTP 5 Amherst WWTP 5.74 10.00 - - Arbor Hills MHP 1 Arbor Hills MHP 0.00 10.00 - - Ashley Hills WWTP 1 Ashley Hills WWTP 0.00 20.00 48,950 4.18 Avocet 2 Avocet 8.35 10.00 24,030 0.66 Barclay Downs WWTP 5 Barclay Downs WWTP 1.31 10.00 25,588 1.94 Beachwood WWTP 4 Beachwood WWTP 3.68 10.00 - - Birchwood RV Park 1 Birchwood RV Park 0.00 10.00 119,575 10.55 Briar Chapel Development 2 Briar Chapel Development 21.10 30.00 70,310 3.92 Briarwood Farms W WTP 5 Briarwood Farms WWTP 7.85 30.00 321,530 36.34 Carolina Meadows WWTP 5 Carolina Meadows WWTP 72.67 50.00 - - Chapel Ridge 1 Chapel Ridge 0.00 10.00 80,990 8.39 Cole Park Plaza 5 Cole Park Plaza 16.78 10.00 23,950 1.13 Colvard Farms 3 Colvard Farms 2.26 10.00 - - Cottonwood/Baywood 1 Cottonwood/Baywood 0.00 10.00 196,000 12.72 CMSD 2 CMSD 25.44 319.00 121,940 11.24 Crooked Creek WWTP 5 Crooked Creek WWTP 22.47 25.00 51,620 2.25 Cross Creek Mobile Estates 5 Cross Creek Mobile Estates 4.50 10.00 64,720 3.63 Deerchase WWTP 5 Deerchase WWTP 7.26 10.00 207,720 9.68 Govenor's Club WWTP 5 Govenor's Club WWTP 19.36 20.00 40,050 3.91 Hasentree Golf Community 1 Hasentree Golf Community 7.82 30.00 308,460 28.28 Hawthorne Subdivision WWTP 5 Hawthorne Subdivision WWTP 56.55 100.00 1,862 491.25 Hominy Creek WRF 2 Hominy Creek WRF 982.49 1500.00 855,760 76.14 Kenly Regional WWTP 5 Kenly Regional WWTP 152.28 318.00 27,590 1.38 Kings Grant Subdivision 5 Kings Grant Subdivision 2.76 10.00 73,870 6.04 Knightdale Mobile Home Park 5 Knightdale Mobile Home Park 12.09 15.00 18,913 1.52 Lake Ridge WWTP 4 Lake Ridge WWTP 3.04 10.00 - - Lake Royale WWTP 1 Lake Royale WWTP 0.00 10.00 - - Legacy at Jordan Lake 1 Legacy at Jordan Lake 0.00 20.00 - - Lewsiton Woodville WWTP 1 Lewsiton Woodville WWTP 0.00 25.00 100,570 7.51 Mallard Crossing WWTP 5 Mallard Crossing WWTP 15.02 15.00 288,167 18.44 Martin County WTP 3 Martin County WTP 36.87 319.00 144,180 6.34 Nature Trails MHP WWTP 5 Nature Trails MHP WWTP 12.67 20.00 1,106,690 81.47 Neuse Colony WWTP 5 Neuse Colony WWTP 162.94 100.00 85,440 4.07 Neuse River Village 5 Neuse River Village 8.14 15.00 978,820 132.37 Neuse River WWTP 3 Neuse River WWTP 264.73 1500.00 1,620,467 228.89 PerdueWWTP 3 Perdue WWTP 457.79 800.00 53,625 6.23 Pikeville WTF 4 Pikeville WTF 12.46 75.00 417,200 34.80 Plymouth WWTP 5 Plymouth WWTP 69.60 85.00 116,400 5.97 Preserve at Jordan Lake 2 Preserve at Jordan Lake 11.94 20.00 - - River Mill WWTP 1 River Mill WWTP 0.00 10.00 378,850 64.12 Robersonville WWTP 4 Robersonville WWTP 128.23 80.00 46,725 3.12 Rock Bridge WWTP 4 Rock Bridge WWTP 6.24 10.00 200,250 31.01 Snow Hill WWTP 3 Snow Hill WWTP 62.01 50.00 110,600 10.40 Stantonsburg WWTP 5 Stantonsburg WWTP 20.81 50.00 2,627,333 418.47 Sunset WTP 3 Sunset WTP 836.94 318.00 12,373,833 1,152.88 Tar River Regional WWTP 3 Tar River Regional WWTP 2305.76 800.00 4,627,000 654.11 Tar River WTP 3 Tar River WTP 1308.21 318.00 3,411,800 492.90 Tarboro WWTP 5 Tarboro WWTP 985.81 829.00 81,120 3.89 Tradewinds WWTP 5 Tradewinds WWTP 7.78 10.00 13,350 0.81 Westfall WWTP 1 Westfall WWTP 1.62 10.00 41,450 2.17 Whippoorwill Valley WWTP 5 Whippoorwill Valley WWTP 4.34 10.00 79,720 6.84 Wildwood Green WWTP 5 Wildwood Green WWTP 13.67 15.00 628,620 60.09 Williamston WWTP 5 Williamston WWTP 120.19 300.00 81,880 3.60 Willowbrook WWTP 5 WillowbrookWWTP 7.20 10.00 8,630.40 8,701.00 33,795,567 4,315 GRANVILLE FARMS O&M PLAN SOURCE VICINITY MAPS SOURCE FIGURE Ahoskie WWTP 1 Amherst WWTP 2 Arbor Hills MHP 36 Ashley Hills WWTP 30 Avocet 3 Barclay Downs WWTP 4 Beachwood WWTP 4 Birchwood RV Park 36 Briar Chapel Development 7 Briarwood Farms WWTP 5 Carolina Meadows WWTP 6 Chapel Ridge WWTP 37 Cole Park Plaza 7 Colvard Farms 8 Contentnea MSD 9 Cottonwood/Baywood WWTP 30 Crooked Creek WWTP 2 Cross Creek WWTP 4 Deerchase WWTP 10 Governor's Club 6 Hasentree Golf Community 11 Hawthorne Subdivision WWTP 12 Hominy Creek WRF 13 Kenly Regional WWTP 31 Kings Grant Subdivision 14 Knightdale Mobile Home Park 4 Lake Ridge WWTP 15 Lake Royale WWTP 38 Legacy at Jordan Lake 16 Lewiston Woodville WWTP 29 Mallard Crossing WWTP 17 Martin County WTP 26 Nature Trails MHP WWTP 6 Neuse Colony WWTP 18 Neuse River RRF 14 Neuse River Village 4 Perdue WWTP 29 Pikeville WTF 19 Plymouth WWTP 20 Preserve at Jordan Lake 16 River Mill WWTP 21 Robersonville WWTP 22 Rock Bridge WWTP 14 Snow Hill WWTP 23 Stantonsburg WWTP 24 Sunset WTP 33 Tar River Regional WWTP 34 Tar River WTP 35 Tarboro WWTP 25 Tradewinds WWTP 10 Westfall WWTP 32 Williamston WWTP 26 Whippoorwill WWTP 27 Wildwood Green WWTP 12 Willowbrook WWTP 28 N W E S 2 �G�j 4 Pinewood Manor Rest Home Ahoskie WWTP HERTFORD .I Ahoskier3 Legend ❑ NC Sources — Road ❑ County Boundary BERTIE ❑ Municipal Boundary ❑ River Ahoskie 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Ahoskie, North Carolina 1 Date: January'17 Soil Plus Project # 200705.C10 � N / SR- CAWEi083 SR- SR- Cary a Springs IX"N 1568-- FSR- SR 1 w SR-3942 w FUgU7 A� SszO S l467 SR�1391 �j � m N SR-1Sp3 I l v � � SR-1504 7 o c +.� � ti JIQ g uquay- SR-473, SR-39� 2811 I � I dle o iSg� NP Cr eek SR-2724 M SR-5006 5733 ( ^ JJ Fuquay-Varina SR-3952 �s SR '1595t' �1� 13"3 Fuquay-VaAna S SR 39 � m M SR-3959 SR_4038� � v � Boa Oti it �}5� N SR-2752 S Fuquay-Varina Legend I SR-3730 Source Location Terrible Creek Fuquay-Varina — Road s�R,-3�56 s' R y Stream sR-41615 r County F L_JounY Boundary SR-4813 L Municipal Boundary N 0.5 0.25 0 0.5 39 Miles SA-488i Scale: 1 inch = 0.5 miles SOIL PLUS LOCATION MAP Figure 2 Drawn by: CSC GFI Land Application Permit (WQ0035595) Reviewed by: CSC Fuquay-Varina, North Carolina Date: Sept'16 Soil Plus Project # 200705.G10 Y N L a) W E S Y O S �C� m 1 Y — v a) a> U Y a3 o'o Shearon Ha ris uclear Power Plant( S-� 27 W wee o I 12 �J 115 1394 I� K 17 Ott o i s TP 1395 lllg 4 4024 1 96 s �~ 1 01 1126 1113 ei o 1 11 v I11,2S 1112 Twin L ke T o I. N 242 25 24 a 1 J 1110 c� II 2Q Q I 1123 1104 N Q 1274 n 1103 /L IQ JIJB � 1122 Jl � CHATHAM i915 tip° 0 22 1120 o t �ti ti J 140.-) � ~ 1 14 c w 1451 Legend 68 0 Source ee �5 Water — Stream Road e� Gte �eC� Sent rs t o 0 0 County Boundary �� 0 Municipal Boundary , Ago 1 0.5 0 1 141a Miles 141 Scale: 1 inch = 1 miles SOURCE LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Pen -nit (WQ0035595) Reviewed by: Holly Springs, North Carolina 3 Date: Nov'17 Soil Plus Project # 200705.D10 N W E S 6 SR-2680 SR-2625 a �P A WAKE Raleigh Carolina Lak 0 1Wvvu h h �\ SR-2946 `Lbti^ N Sh':ZS90 ry' �54 SR� SR 2592 SR -4164 SR-2593 `SR-4188 SR_4102 r SR �` SR-2671 N Q 08 6,31 < Neuse River Village j °n-1007 Knightdale MHP Cross Creek 0 Legend Source Location h 6 — Road • Stream J, IL _J County Boundary SR-z67s L Municipal Boundary 0.5 0.25 0 0.5 Miles r3- Scale: 1 inch = 0.5 miles SOIL PLUS LOCATION MAP Figure 4 Drawn by: CSC GFI Land Application Permit (WQ0035595) Reviewed by: CSC Raleigh, North Carolina Date: Sept'16 Soil Plus Project # 200705.G10 N \W E S � Cary V a SR-1010 Cam � co n � �ra�cli SR -so ^MO � SR-1448 542q v. SR SR-5098 WAKE s� ti p' SR-4017 Briarwood SR-5845 ❑ SR-4797 1 C� Sk3939 SR-3951 SR-3934 � m I �o SR-I122 0� SR_ 5832 SR-3937 5830 n u w \S AC)" J SR-1484 fir, N Legend .Source Location Holly Springs Sti53 s — Road r Stream Sg9 I SR-1390 aCounty Boundary ❑ Municipal Boundary o 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC Cary, North Carolina 5 Date: Sept'16 Soil Plus Project # 200705.G10 N w E Ste" ORANGE s --------------- <---- ---- SR-2001 SR�1'116 S-1811 SR 1832R S� CHATHAM Morgan Creek N r Trail Morgan O� y Chatham WRF of Jordan Lake Legend SR-1753 Source Location — Road New Hope Rv Arm of B. Everett Jord Stream New Hope River Arm of B�Evgrptt [--_]County Boundary L Municipal Boundary c r Surface Water 40.5 0.25 0 0.5 Miles It Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Durham, North Carolina 6 Date: Sept'16 Soil Plus Project # 200705.G10 va N Q 1602 ^�0� 1575 ~ W ELn ` ►�` Cole Park Plaza _I a 1532 ell tih4i r13g� � .� I � 15800 Ln 4 �' IgGs 0 o 1530 ON M~ 1�� a 1721 o ti� `� cn 1606 Briar Chapel Development D 0 1634 r 1719 Dogwood Veterinary Hospital CHATHAM 1717 Legend 1618 E) NC Sources ~ ��T �� Fearrington Village 3 — Stream NN 1 1❑, 1�6� 1779 — Road � 1803 4^ 9 NHDWaterbody ❑ <all other values> o 1 1805 I8 1718� q Oq FType 16 1802 ���15�7 0 1836 ❑ Estuary ti ❑ Ice Mass ❑ LakePond ❑ Playa ❑ Reservoir 0 ❑ SwampMarsh 0 j J! CountyBoundary ❑ MunicipalBoundaries_polys 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn hy: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed hy: CSC Chapel Hill, North Carolina 7 Date: April'17 Soil Plus Project # 200705.G10 DURHAM 1103 Colvard Farms 0 Durham Durh IDurham SR I �I Legend Cary 8c, ❑Source Location — Road Cary Stream aCounty Boundary Northeast Creek ❑ Municipal Boundary 7"1 �_ - - M rgan C►►reek Arm o New Hope River Arm of B. Everett Jo:0.5 0.25 0 0.5 Surface Water _ ^ � I I Milest y Morgan ree me u ing the Morgan Creek Arm of New Hope River Arm of B. Everett Jordan Lake Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595 Reviewed by: CSC Durham, North Carolina 8 Date: Sept'16 Soil Plus Project # 200705.G10 N �W E 1801 lJ r. Contentnea 190� 1911 PITT 19og 1910 District WWTP LENOIR District WWTP Legend Neuse Rive_ ' ' Neuse River NC Sources-� — Road ❑ County Boundary CRAVEN Municipal Boundary ❑ River 0.5 0.25 0 0.5 Jos Miles 5 Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC 442WGrifton, North Carolina 9 Date: January Soil Plus Project # 200705.C10 N \ Wake Forest] W E / S Wake Forest o� v �Sl� SR\2045 I v Wake Forest SR-2043 Forest Deer Chase Me Forest ' s 5R-3564 T� Creek Raleigh SR-3509 Raleigh 4 SR-44601 Legend 11'\ Source Location SR-2930 Q SR-2982 — Road Stream County Boundary tititi� 54���� Municipal Boundary 54 0.5 0.25 0 0.5 Surface Water sR-2223 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Wake Forest, North Carolina 10 Date: Sept'16 Soil Plus Project # 200705.G10 N U1 N [� � N W E S � r J � M A 00 N 1909 x N Neuse River (Falls Lake below normal pool elevation) �I8 7t O N Phase 1 & 2A Hasentree Golf N N � WAKE 98 451 V \Io 1<0� h~ Legend \ 'l `--� / � NC Sources River (Falls/Lake below normal pool elevation) c N — Road County Boundary Raleigh Municipal Boundary 0.5 0.25 0 0.5 River Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Wake Forest, North Carolina 11 Date: January '17 Soil Plus Project # 200705.C10 ^N / 3J SR-4281 s,�c Jf�cs/ SR-4633 J¢A J� J�g2 JR.1g4 SR-4230 w E SR 1899 1�0� 4 00 I s � SR-4483 SR-4984 S ' s� et •N � sR,s � �' SR-4976 n 5619 M Ak P SR r SR 60R� Cn sf A�n SR 4689 Sg s� SR-5686 oo X� T awt ornu • vis e Ln s SR-4989 SR-49 90 / �9 �0 SR-1 \rI2 SR-3382 LSD SAS g9�J GAG M —M 8 SR 3452 t� �scp3 v S CP n N N MSR-3286 1 y SR-3591 SR 3 W CP00 C SR-469q 4�ofi Cn �ro 3379 w lL.�r, J �,�;• c SR-1839 � Raleigh s cc SR-1898 �2 I-540 5� SR 3354 SR-4276 RMP4201 SR-1836 41�9a SR-3225 S�p2° 0$ WildWo— d- reen � SR-3447 1540 Raleigh S4 . �M SR-3445 s� Raleigh N M 4209 SR 1 SR-3289� No Raleigh sR 1s29 S4 5^ s cJ ? R-3236 SR—_3221 � ~� c cP� S � SR-3450 Sh, SR-3256 � . N R '•'>M 7 �(� SR-3241 Legend .Source Location — RoadM) �� y Raleigh — Stream �� of SR-3305 OCounty Boundary SR-3363 SR-3303 ❑ Boundary Raleigh COMunicipal o'�� Surface Water h lei g p M 0.5 0.25 0 0.5 ��54 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC Raleigh, North Carolina 12 Date: Sept'16 rS0i;lus Project # 200705.G10 N S �c 264 1613 1695 1615 1614 264 `0C ~� 2G57 ti 301 167 5 Wilson, NC -Processing Facility E3 1608 Wilson Reclaimed Water -Distribution System 4692 Wilson WWTP WIL�ON 1696 1697 Legend 1616 . NC Sources Road 1617 1623 ❑ County Boundary ❑Municipal Boundary �titi Black Creek 0.5 0.25 0 0.5 ❑ River q— _,Jack Creek 0 Miles 7 22 Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Wilson, North Carolina 13 Date: January'17 Soil Plus Project # 200705.C10 114 SR,4j 11 SR-21 Rock Bridge 's 1 �� SR-2511 WAKE " s � 0 Kings/ Grant SR-4198 13p Neuse River 0 Y 5230 SR-524 N � SR - N iw SR-2507 SR-2508 01' �� Legend EDSource Location — Road Stream — Count Boundar %� JOHNSTON Clayton �_J Y Y L Municipal Boundary 1�rE Usk 0.5 0.25 0 0.5 Surface Water R Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Clayton, North Carolina 14 Date: Sept'16 Soil Plus Project # 200705.G10 SR-1221414 N W E S M O V r C, Cn Cn C Cn SR_1g1 SR1 SNS 1 S� ��3� s� I�8 8 ja�tbe^xee�"' WE s�S03 ory pool e le �7va attion) AKEEV Legend • �/ `� Source Location — Road SR-1895 Stream s� N QCounty Boundary ❑ Municipal Boundary �a c SR-1893� F Surface Water 0.5 0.25 0 0.5 ur am Miles u'rham Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC Durham, North Carolina 15 Date: Sept'16 Soil Plus Project # 200705.G10 N Ne Hope River Arm of W E \S 1782 Legend NC Sources — Road County Boundary Municipal Boundary River The Preserve at E) / The Legacy af J New Hope Rv New 8544 Lake Park � 85 1 749 8584 ja�2 40.5 0.25 0 0.5 Miles- Y V I .• 1 / ti Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Chapel Hill, North Carolina 16 Date: January'17 Soil Plus Project # 200705.C10 N �j � /W E0 1"i SA4-62 S Raleigh Raleigh N N 0 , �224 14 � N iA 'W-2982 SR-2223 S. SR 295� SR 4 08 SR-2296 Od�.es � SR,3g M\ Creek S9,2959 Mallard Raleigh 1 LJ 43g0 SR/ SR-4313 \x Raleigh SR-2217 0 0 N I N P4 Legend �V Source Location — Road Stream r i_J County Boundary Municipal Boundary Rr Surface Water 0.5 0.25 0 0.5 ti Miles ightdale nnigntaate Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Raleigh, North Carolina 17 Date: Sept'16 Soil Plus Project # 200705.G10 N SR-2641 w E Archer Lodge o i S Sj� 323 SR=2693 c w 4 ti� SR'3215 SR 2669�'~� cG �� Clayton Clayton o zG s A9 Clayton SR 5� x NC-42 w� Meuse-9-- ro Clayton JOHNSTON \2g2G Clayton `, 903 Legend 1NIZ Source Location R�0�Road laytonStream o r J County Boundary o o SR-1913 p� L Municipal Boundary Surface Water 0.5 0.25 0 0.5 Miles -0 US-70 R� Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Clayton, North Carolina 1 g Date: Sept'16 Soil Plus Project # 200705.G10 M ' r N /W E S 1363 v 1� Ss. cc � `PS L Ln en 00 ss�s 1O02 U` _J Pikcv ills 1322 1-42 1,534 Pikeville Wastewater Treatment WANE 1'4 Legend 2304 NC Sources — Road County Boundary ❑ Municipal Boundary River 0.5 0.25 0 0.5 1614 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC s o IL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Pikeville, North Carolina 19 Date: January'17 Soil Plus Project # 200705.C10 N W E S R auth WWTP River WASHINGTO rrs 13�� 1328 "s Legend 1325 NC Sources �J Road Plymouth w I County Boundary ❑ Municipal Boundary -' 0.5 0.25 0 0.5 River Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Plymouth, North Carolina 20 Date: January'17 Soil Plus Project # 200705.C10 V (N W E S O N SR-362'4 Neuse River S� 1 ennys M �i I River' Mill nal pool elevation) v v /110 o � U WAKE Raleigh Wake Forest NC-98 n—� i �3 M � O Wake1Forest Sl2 SR-5107 n S�, SR-2045 230 21 JS 2 � ti 5�-3691, Legend Source Location Wake Forest — Road Stream [_-_—],County Boundary L Municipal Boundary 0.5 0.25 0 0.5 Surface Water Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC4949swpw— Raleigh, North Carolina 21 Date: Sept'16 1 Soil Plus Project # 200705.G10 N / S 64 l/ / MARTIN 118� Robersonville WWTP )1438 � 1145 N A3 a A3 I BSI 1148 Legend NC Sources PITT — Road County Boundary Municipal Boundary River 0.5 0.25 0 0.5 zls� Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC 442WRobersonville, North Carolina 22 Date: January Soil Plus Project # 200705.C10 N S 1247 1� Hill I 11 I ti Snow Hill WWTP 903 Legend v NC Sources — Road County Boundary a ~ do I Municipal Boundary ti~ I�3 s8 0.5 0.25 0 0.5 River IIo� Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Snow Hill, North Carolina 23 Date: January'17 Soil Plus Project # 200705.C10 N W E ,G dl JG V- 1ti% WILSON Stantonsburg WWTP GREENE 1235 1230 1232 N� Legend ❑ NC Sources JA223 Road County Boundary ❑ Municipal Boundary��❑ River 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC 44owrs tantonsburg, North Carolina 24 Date: January'17 oil Plus Project # 200705.C10 N —W E �J 9 iZ1� 1212 �1 J� 1� Orp Tarboro 1Z2 1351 !�19g! A�� 1344 10i 25S 'I'ar.River. P-rinc.vi e 111 iro WWTP E 1539 M \ 10 0 45- JN tK Legend NC Sources — Road County Boundary ❑ Municipal Boundary River 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC 442spw- FS arboro, North Carolina 25 Date: January oil Plus Project # 200705.C10 N W E s ROANO f RIVER BERTIE 1450 ~ Williamston WWTP tih 1581 Williamston b, 1 ti� 1 u 1598 1� c 37 O J 1123 M C ~ b ti ti Martin County WTP MARTIN 1124 1208 N 119a 0 ti moo° 454 0 7125 465-5zi Legend ❑ NC Sources — Road ❑ County Boundary ❑ Municipal Boundary jr ❑ River 11�8 1501 0.5 0.25 0 � 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC 442WFso illiamston, North Carolina 26 Date: January'177 il Plus Project # 200705.C10 i N S 1a1a00 W E 19 6 1 co SR-1715 J FRANKLIN S4/ Sg SR_2447 �9I y SR-1724 SR,23�1 WAKE SR-2313 W O Legend Source Location 1I25 Sg — Road Stream N �e SR-2309 ce, J County Boundary 9�k L Municipal Boundary r 0.5 0.25 0 0.5 Surface Water Miles SR-2315 Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Zebulon, North Carolina 27 Date: Sept'16 Soil Plus Project # 200705.G10 \ N. W E S N � N G � ^� N 0 SR-417R ' tihh� � N SR-52041 ,ela Gtieek '" n-265g Beadin� M WAKE W N N SR-1771 N SR-3224 Willowbrook w N� _,1 0� SR SR-1779 ti JOHI S NN �0, s U SR-1615 SR-1639 M SR -1677 Clayton � SR-1632 Legend Cn w P Source Location N o� — Road s�'ssJ Stream SR-1550 r �_J County Boundary s L Municipal Boundary r hN Surface Water 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Garner, North Carolina 28 Date: Sept'16 Soil Plus Project # 200705.G10 1 N ( W E S SR�1 Perdue WWTP HALIFAX _ SR-1 S¢i Lewiston -'Woodville WWTP ,2 0 11 �J ti~ o BERNIE SR 1 �Wlston W00 'He SR-1119 l� z� 1108 Legend 0 Sources Stream Road 0 County Boundary 0.95 0.475 0 0.95 N Municipal Boundary Miles z Scale: 1 inch = 1 miles SOURCE LOCATION MAP Figure Drawn by: CSC SDIL PLUS WQ0035595 O&M PLAN Reviewed by: Lewiston -Woodville, North Carolina 29 Date: Aug'17 Soil Plus Project # 200705.C10 N W E S WAKE Knig le e Cottonwood/Baywood 0 Ashley Hills WWTP Wendell Legend I e Sources — Road 0 County Boundary 0.5 0.25 0 0.5 Municipal Boundary Kings Gra Subdivision W Miles Scale: 1 inch = 1 miles SOURCE LOCATION MAP Drawn by: DM ;OIL PU GFI Land Application Permit (WQ0035595) Figure Reviewed by: Knightdale, North Carolina 30 Date: June'18 Soil Plus Project # 200705.D10 N 2�qS S� _W E SR-2147 S S aC � v '''o U 0 w w SR-2146 N z 4 / �R-2143 Kenly Mill Creek S4 Kenly Kenly S� N SR-2343 1b Sg� r �R�2385 Legend �„�'�`� 7Source Location SR-2341 a — Road Qofi Stream ���� SR-2,414 County Boundary S4 s� L Municipal Boundary Surface Water 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Kenly, North Carolina 31 Date: Sept'16 Soil Plus Project # 200705.G10 p W EV $ Gv XAGE f 198 CHA N N DURHAM CD o n 1103 h N `°° O N N 1 C o ' a Meado s WW a k Nature Trail obile Home Par WWTP 1 6 l 1832 1 eiCc � Y n U tfall WWTP n I m 1753 r� c 1795 F°lk Gr ner ce' e 1� C Creek Ira. 1740 41 N 1801 Legend 1j49 1 C, L . Source m� 761 m 2 Water �� CD1,05 — Stream 1,4 L 1WAKE Road Y' o p� 0 County Boundary � 0 1 0.5 0 1 Municipal Boundary Miles n 174 Scale: 1 inch = 1 miles SOURCE LOCATION MAP Figure Drawn by: CSC SOIL PL. Us GFI Land Application Permit (WQ0035595) Reviewed by: Chapel Hill, North Carolina 32 Date: Nov'17 Soil Plus Project # 200705.D10 RMP-172 H Rocky Mount Maple CreeJ M sR Horn B 1 S� SR-1599 v� p1 SR;1542 tiS3 O� o, G„ LOCi915 y US-64P_1 WTP � o O U O \�f RUP_16j O G� C: C G � Lc end LOC-914 cq o Source Location — Road M Swami' Stream 1,;ttle C°key [_JCounty Boundary L Municipal Boundary SR-1'27 0.5 0.25 0 0.5 Surface Water Miles u Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Rocky Mount, North Carolina 33 Date: Sept'16 Soil Plus Project # 200705.G10 N W E s SR-1404 00 Tar River U i Rocky Mount Legend Source Location — Road Stream _IR J County Boundary L Municipal Boundary Surface Water N 0 �ek WWTP SR-1414 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC Rocky Mount, North Carolina 34 Date: Sept'16 Soil Plus Project # 200705.G10 Z1707��t 460 CIOard SR-1710 rah � SR-1709 c!l a Tar River WTP s u SR-1749f NASH ti Sg ranch 233`� Rocky wK sR,l N� 8G3 1 �0 SR-1733 I V � Legend G - .Source Location — Road 7� Stream QCounty Boundary ❑ Municipal Boundary s�I��o 0.5 0.25 0 0.5 Surface Water Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC Rocky Mount, North Carolina 35 Date: Sept'16 Soil Plus Project # 200705.G10 61 N '1449 a= ti � w e16 9 ti- �� 486 ti � S FtN �7 1510 1556 o 1404 c\7 o / 5 N f 1�42 7402 II3 h� ti c� IS r_ G8 Ar r s e Ho P 1888 ^titi ee �� I87j tic�G� 8728 85 St to P WTP �58 1494 140� 812 1710 � �tiN l oaf tiS 1721 �I3 4-5 erbe Cree 911 ORANGE 720 1, '9 8 78 19 32 1874 x ^ DURHAM 2p'12 Ne 0 e 1718 0 w CP 84 b n � g C ro I a�•e`a 90 227 � od Mobil me k ^ in 2219 z2o` " 1880^ N 172 illtop Mob e P k N2 1731 o � � � 136 Bran 1303 e� w ti N 2 35 4 z Legend 0 Source �q. 904 � 0 Water d~� N o1/1 `V 1146 — Stream Road OI �J 0 County Boundary N 0 Municipal Boundary 1 0.5 0 1 o 5` Miles 38 2220 ti Scale: 1 inch = 1 miles SOURCE LOCATION MAP Figure Drawn by: DM SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: Durham, North Carolina 36 Date: June '19 Soil Plus Project # 200705.G10 N 1547 �MN W E s � Creek Cry Creek Lo 9 Branch 10°� c Chapel Ridge N E 1680 160 �s ittsbo 1523 871 �rarorl Ig 1346 eel Gtoae 4 yr CHATHAM 159 1659 o dj0 2059 v N 0% IS M � Q mo �p3 f 159 1 1649 1648 1,564 N m N F �n N N f 1967 01 I \s`s 1824 206 2p �� 91 1943 P' sboro TP �� g 19 N N 2159 N 116 O es cue Legend J N �12 0 Source ° 0 Water goti eA — Stream Road 0 County Boundary Municipal Boundary 1 0.5 0 1 N Miles N Scale: 1 inch = 1 miles SOURCE LOCATION MAP Figure Drawn by: DM SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: Pittsboro, North Carolina 37 Date: June '19 Soil Plus Project # 200705.G10 N —W E\ s Cron /re 7755 aC Lrek do JJ r 98 Cana s po,v 1 7\'FRANI-CLIN � I> 1652 1633 ,cs A �c o� 1608 16i I c4 1638 0 0 ID ,6 U ke Royale P IS ti ti 1316 I �- 9 �O NASH .ga Al n Legend 1738 00, 0 Source Q` 0 Water a � — Stream Road ey T a' ~h TrCr ti 0 County Boundary I�S9 eel 1 0.5 0 M 1' Municipal Boundary 1747 Miles I�gB "sue 11,n Scale: 1 inch = 1 miles SOURCE LOCATION MAP Figure Drawn by: DM SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: Bunn, North Carolina 3 8 Date: June '19 Soil Plus Project # 200705.G10 APPENDIX 2 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RS CA Arbor Hills MHP Field Loading Calculations Analytical a y C O H A C O U s. z z 3 z z z z z a, U O O U w W H 72 a� a H o Z o3 w o zzzz z z r/1 U III Ml RE 73 C z State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water KesoUFces RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Arbor Hills Mobile Home Park WWTP 2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or 0 Private. Facility permit issued by: ® Div. of Water Resources, Div. of Environmental Health, or ❑ Other (explain: M. 3. Facility contact person and title: Mr. Luther Thomas Harden III Complete mailing address: k228 US Highway City: Durham State: NC Zip: 27705- Telephone number: (919) 768-2921 E-mail address: ltharden319540)gmail.com 4. Facility physical address: *28 US Highway 0 City: ur State: LC Zip: 705- Coordinates: Latitude: 36' 02' 57.0" Longitude: 79' 01' 26.0" Datum: NAD 83 Level of accuracy: Sub -Meter Method of measurement: 5. Purpose of the facility: [] treatment of municipal wastewater, treatment of 100% domestic wastewater, Ej treatment of potable water, treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: 0.006 MGD and facility average daily flow: M MGD 8. Average amount of residuals being generated at this facility < 5 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 6,000 Galldweration Basin Type and volume of residuals storage (i.e., outside of residuals treatment units): 5,000 Gallon Sludge Holding Tank II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: Biological 0 Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 11-13 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: _ and Date of analysis: _ Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes no. Flashpoint: _ °F (> 140°F) Passed reactivity test: Eyes Ono. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500) TCLP Parameter Limit (mg/1) Result (Mg/1) TCLP Parameter Limit (Mg/1) Result (Mg/1) Arsenic 5.0 Hexachlorobenzene 0.13 Barium 100.0 Hexachloro-1,3-Butadiene 0.5 Benzene 0.5 Hexachloroethane 3.0 Cadmium 1.0 Lead 5.0 Carbon Tetrachloride 0.5 Lindane 0.4 Chlordane 0.03 Mercury 0.2 Chlorobenzene 100.0 Methoxychlor 10.0 Chloroform 6.0 Methyl Ethyl Ketone 200.0 Chromium 5.0 Nitrobenzene 2.0 m-Cresol 200.0 Pentachlorophenol 100.0 o-Cresol 200.0 Pyridine 5.0 p-Cresol 200.0 Selenium 1.0 Cresol 200.0 Silver 5.0 2,4-D 10.0 Tetrachloroethylene 0.7 1,4-Dichlorobenzene 7.5 Toxaphene 0.5 1,2-Dichloroethane 0.5 Trichloroethylene 0.5 1,1-Dichloroethylene 0.7 2,4,5-Trichlorophenol 400.0 2,4-Dinitrotoluene 0.13 2,4,6-Trichlorophenol 2.0 Endrin 0.02 2,4,5-TP (Silvex) 1.0 Heptachlor and its Hydroxide 0.008 Vinyl Chloride 0.2 FORM: RSC 11-13 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: eritech Inc. and Date of analysis: - Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <2.45 Cadmium 85 39 1.59 Copper 4,300 1,500 288 Lead 840 300 7.94 Mercury 57 17 0.123 Molybdenum 75 n/a 5.25 Nickel 420 420 5.88 Selenium 100 100 24.6 Zinc 7,500 2,800 598 b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) I > 0 but < 25 30 200 210 Ej > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 j > 100 but < 125 53 360 390 El > 125 62 450 420 Result (mg/kg) FORM: RSC 11-13 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: a %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Meritech Inc. and Date of analysis: - Parameter Result (mg1kP) Aluminum 3,180 Ammonia -Nitrogen 9,020 Calcium 36,200 Magnesium 2,820 Nitrate -Nitrite Nitrogen <490 pH (Standard Unit) 6.7 Phosphorus 12,000 Potassium 2,320 Sodium 2,990 Total Kjeldahl Nitrogen 53,400 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.58 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): E default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex Iain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: ii e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (m91k9) (mg/kg) Surface 18,314 27,346 Injection/Incorporation 22,824 30,695 6. Other Pollutants Determination: SpecifX whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: None lleM FORM: RSC 11-13 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, 4 heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, or I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item Il. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. 1 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 11-13 Page 5 of 5 it, Facility Arbor Hills MHP FIELD LOADING ESTIMATES Sampling Date 5/24/2019 % Solids 2.04 Mineralization Rate 0.3 Gallons per DT 11,755.30 pH 6.7 Sodium Absorpotion 0.58 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 53,400 lbs./1,000 gal 9.09 Ammonia Nitrogen (mg/Kg) 9,020.00 lbs./1,000 gal 1.53 Nitrate -Nitrite (mg/Kg) 490.00 lbs./1,000 gal 0.08 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 18,314 lbs./1,000 gal 3.12 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 22,824 lbs./1,000 gal 3.88 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 0.39 Phosphorus lbs./1,000 gal 2.04 Calcium lbs./1,000 gal 6.16 Magnesium lbs./1,000 gal 0.48 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 2.45 Arsenic lbs./1,000 gal 0.00 Cadmium (mg/Kg) 1.59 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 288.00 Copper lbs./1,000 gal 0.05 Lead (mg/Kg) 7.94 Lead lbs./1,000 gal 0.00 Mercury (mg/Kg) 0.12 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 5.88 Nickel lbs./1,000 gal 0.00 Selenium (mg/Kg) 24.60 Selenium lbs./1,000 gal 0.00 Zinc (mg/Kg) 598.00 Zinc lbs./1,000 gal 0.10 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) 53,400 18,314 36.63 35,086 53,400 22,824 45.65 30,576 35,086 5,263 10.53 29,823 30,576 4,586 9.17 25,990 29,823 2,237 4.47 27,586 25,990 1,949 3.90 24,040 27,586 1,034 2.07 26,552 24,040 902 1.80 23,139 26,552 498 1.00 26,054 23,139 434 0.87 22,705 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Total 27,346 54.69 Total 30,695 61.39 Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Meritech Work Order # 0524d949 Parameters Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Sample: AR052419 Grab Results Analysis Date Report Date: 6/11/2019 Project: Arbor Hills Date Sample Rcvd: 5/24/2019 5/24/19 Reporting Limit Method %Total Solids 2.04 % 5/29/19 0-100 % SM 2540B Ammonia, Nitrogen 9020 mg/kg 6/3/19 10 mg/kg EPA 350A TKN 53,400 mg/kg 6/3/19 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <490 mg/kg 5/29/19 490 mg/lcg EPA 353.2 Aluminum, total 3,180 mg/kg 5/31/19 2.50 mg/kg EPA 200.7 Arsenic, total <2.45 mg/kg 5/31/19 2.45 mg/kg EPA 2003 Cadmium, total 1.59 mg/kg 5/31/19 0.20 mg/kg EPA 2003 Calcium, total 36,200 mg/kg 5/31/19 10.0 mg/kg EPA 200.7 Copper, total 288 mg/kg 5/31/19 1.00 mg/kg EPA 2003 Lead, total 7.94 mg/kg 5/31/19 0.500 mg/kg EPA 2003 Magnesium, total 2,820 mg/kg 5/31/19 10.0 mg/k9 EPA 2003 Mercury, total 0.123 mg/kg 6/10/19 0.053 mg/kg EPA 245.1 Molybdenum, total 5.25 mg/kg 5/31/19 0.500 mg/kg EPA 200.7 Nickel, total 5.88 mg/kg 5/31/19 2.0 mg/kg EPA 2003 Phosphorus, total 12,000 mg/kg 5/31/19 2.00 mg/kg EPA 200.7 Potassium, total 2,320 mg/kg 5/31/19 20.0 mg/kg EPA 200.7 Selenium, total 24.6 mg/kg 5/31/19 2.63 mg/kg EPA 200.7 Sodium, total 2,990 mg/kg 5/31/19 20.0 mg/kg EPA 200.7 Zinc, total 598 mg/kg 5/31/19 0.500 mg/kg EPA 200.7 pH 6.7 S.U. 5/29/19 1.0 - 14.0 S.U. SM 4500-HB I hereby certify thatl have reviewed and approve these data. (�(� 4(� Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 ? Y Y a O Ik` = 0 0 aJ a y 0 Q V vLn n LJ m £ 1 as hi a O E u }(1`_ = E E _ v N r= OFF- 0 U 7 �y Q LJ'': CY) Lo N x. ti U E ig N a Y q o N O N O) N �'• N � U a c V) a N o w -w U_ o ,. E a t x O F: Q IU- w Z a w a` n: n, 0 Z w v0 C O O MOMS C MIFF&W 0 MMMMEMMMM MUW E z FIFO w OF_y .0 �� Q N -o i N wLf) O - ti `� Q 4MJ NFIFO t0 >% .N. Z L 0 N _ O. w Z N c N o d) Z U) X 0 O 'O a- m 3 S E 0 E Z O x 3 a p o v m cc ri O OF. 'CFFMd y .. MOMP F'.. V a N m U a cD z U Q Q u o Y w v E E E I= i= F N E v c o N a Y £ > CA N N @ N v,V , « i= roWw o« QNOCL p Z E Fib E . m C c }y m R o Q N o U O = QJ c w E U x 'O 0 m y C �a ~ !Y G N V .J N Mt V � v OFF,a Ou L� E 'm cu z @Ej °` g o 49 F' 0 -� Ln @ 0 E Y T C U — '6 Z NdMMM� N O N N d N E -F— o U W j 0 u w .i d d s w E 0 0 0 ^` Vl N a �. 51 N.MdF,N 0 a a t -o E - - - um E 0 0 - — - — - — G O O� w G' / a� .. 0 x> 3 J N N Ln w 0 w vi 0 E a -o .0 Mc M.0 m U, rLLlx r'i,. APPENDIX 3 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RS CA Birchwood RV Park Field Loading Calculations Analytical State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources DiivisIon of Water ResoUKes RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Mchwood RV Park 2. Facility permit holder is: Federal, 0 State, 0 Local Government, or ® Private. Facility permit issued by: Div. of Water Resources, Div. of Environmental Health, or Other (explain: �. 3. Facility contact person and title: Jay Murray Complete mailing address: F901 Wilkins Dr City: Durham State: NC Zip: 27705- Telephone number: (919) 493-1557 E-mail address: birchwoodrvparkgyahoo.com 4. Facility physical address: 5901 Wilkins Dr City: - State: NC Zip: 705- Coordinates: Latitude: 35' 59' 06.0" Longitude: 79' 00' 00.4" Datum: NAD 83 Level of accuracy: Sub -Meter Method of measurement: 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water, treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: .018 MGD and facility average daily flow: M MGD 8. Average amount of residuals being generated at this facility < 5 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 18,000 Gallons Extended Aeration Type and volume of residuals storage (i.e., outside of residuals treatment units): 5,000 Gallon Primary Sludge Storage Tank & 10,000 Gallon Secondary Sludge Storage Tank II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ® Biological 0 Non -Biological FORM: RSC 11-13 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: E yes M no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: _ and Date of analysis: _ Passed corrosivity test: el yes 0 no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: L] yes A no. Flashpoint: _ OF (> 140°F) Passed reactivity test: Eyes Ono. HCN: 11" mg/kg (<250) & HZS: _ mg/kg (<500) TCLP Parameter Limit (Mg/1) Result (Mg/1) TCLP Parameter Limit (mg/l) Result (mg/1) Arsenic 5.0 Hexachlorobenzene 0.13 Barium 100.0 Hexachloro-1,3-Butadiene 0.5 Benzene 0.5 Hexachloroethane 3.0 Cadmium 1.0 Lead 5.0 Carbon Tetrachloride 0.5 Lindane 0.4 Chlordane 0.03 Mercury 0.2 Chlorobenzene 100.0 Methoxychlor 10.0 Chloroform 6.0 Methyl Ethyl Ketone 200.0 Chromium 5.0 Nitrobenzene 2.0 m-Cresol 200.0 Pentachlorophenol 100.0 o-Cresol 200.0 Pyridine 5.0 p-Cresol 200.0 Selenium 1.0 Cresol 200.0 Silver 5.0 2,4-D 10.0 Tetrachloroethylene 0.7 1,4-Dichlorobenzene 7.5 Toxaphene 0.5 1,2-Dichloroethane 0.5 Trichloroethylene 0.5 1,1-Dichloroethylene 0.7 2,4,5-Trichlorophenol 400.0 2,4-Dinitrotoluene 0.13 2,4,6-Trichlorophenol 2.0 Endrin 0.02 2,4,5-TP (Silvex) 1.0 Heptachlor and its Hydroxide 0.008 Vinyl Chloride 0.2 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: eritech Inc and Date of analysis: Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <4.13 Cadmium 85 39 1.95 Copper 4,300 1,500 181 Lead 840 300 4.42 Mercury 57 17 0.372 Molybdenum 75 n/a 4.42 Nickel 420 420 7.25 Selenium 100 100 10.7 Zinc 7,500 2,800 740 b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) > 0 but < 25 30 200 210 0 > 25 but < 50 34 220 240 > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: a %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory:lkeritech Inc. and Date of analysis: 05/29/19 Parameter Result (mg/kg) Aluminum 2,790 Ammonia -Nitrogen 5,240 Calcium 13,700 Magnesium 3,140 Nitrate -Nitrite Nitrogen <826 pH (Standard Unit) 6.5 Phosphorus 9,420 Potassium 3,540 Sodium 4,260 Total Kjeldahl Nitrogen 75,000 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.94 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: ii e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 24,374 37,406 Injection/Incorporation 26,994 39,352 6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106 i 3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, oi I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. it, Facility Birchwood FIELD LOADING ESTIMATES Sampling Date 5/29/2019 % Solids 1.21 Mineralization Rate 0.3 Gallons per DT 19,818.86 pH 6.5 Sodium Absorpotion 0.94 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 75,000 lbs./1,000 gal 7.57 Ammonia Nitrogen (mg/Kg) 5,240.00 lbs./1,000 gal 0.53 Nitrate -Nitrite (mg/Kg) 826.00 lbs./1,000 gal 0.08 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 24,374 lbs./1,000 gal 2.46 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 26,994 lbs./1,000 gal 2.72 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 0.36 Phosphorus lbs./1,000 gal 0.95 Calcium lbs./1,000 gal 1.38 Magnesium lbs./1,000 gal 0.32 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 4.13 Arsenic lbs./1,000 gal 0.00 Cadmium (mg/Kg) 1.95 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 181.00 Copper lbs./1,000 gal 0.02 Lead (mg/Kg) 4.42 Lead lbs./1,000 gal 0.00 Mercury (mg/Kg) 0.37 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 7.25 Nickel lbs./1,000 gal 0.00 Selenium (mg/Kg) 10.70 Selenium lbs./1,000 gal 0.00 Zinc (mg/Kg) 740.00 Zinc lbs./1,000 gal 0.07 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) 75,000 24,374 48.75 50,626 75,000 26,994 53.99 48,006 50,626 7,594 15.19 43,032 48,006 7,201 14.40 40,805 43,032 3,227 6.45 39,805 40,805 3,060 6.12 37,745 39,805 1,493 2.99 38,312 37,745 1,415 2.83 36,329 38,312 718 1.44 37,594 36,329 681 1.36 35,648 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Total 37,406 74.81 Total 39,352 78.70 Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Meritech Worlc Order # 05291978 Parameters Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Sample: TP052919 Grab Results Analysis Date Report Date: 6/11/2019 Project: Triangle RV Park Date Sample Rcvd: 5/29/2019 5/29/19 Reporting Limit Method %Total Solids 1.21 % 5/30/19 0-100 % SM 2540B Ammonia, Nitrogen 5,240 mg/kg 6/3/19 10 mg/kg EPA 350A TKN 75,000 mg/kg 6/3/19 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <826 mg/kg 5/30/19 826 mg/kg EPA 353.2 Aluminum, total 2,790 mg/kg 6/5/19 2,50 mg/kg EPA 200.7 Arsenic, total <4.13 mg/kg 6/5/19 4.13 mg/kg EPA 200.7 Cadmium, total 1.95 mg/kg 6/5/19 0.20 mg/kg EPA 2003 Calcium, total 131700 mg/kg 6/5/19 10.0 mg/kg EPA 2003 Copper, total 181 mg/kg 6/5/19 1.00 mg/kg EPA 200.7 Lead, total 4.42 mg/kg 6/5/19 0.500 mg/kg EPA 200.7 Magnesium, total 3,140 mg/kg 6/5/19 10.0 mg/kg EPA 2003 Mercury, total 0.372 mg/kg 6/10/19 0.053 mg/kg EPA 245A Molybdenum, total 4.42 mg/kg 6/5/19 0.500 mg/kg EPA 2003 Nickel, total 7.25 mg/kg 6/5/19 2.0 mg/kg EPA 2003 Phosphorus, total 9,420 mg/kg 6/5/19 2.00 mg/kg EPA 2003 Potassium, total 3,540 mg/kg 6/5/19 20.0 mg/kg EPA 200.7 Selenium, total 10.7 mg/kg 6/5/19 2.63 mg/kg EPA 200.7 Sodium, total 4,260 mg/kg 6/5/19 20.0 mg/kg EPA 200.7 Zinc, total 740 mg/kg 6/5/19 0.500 mg/kg EPA 2003 PH 6.5 S.U. 5/30/19 1.0 - 14.0 S.U. SM 4500-HB /hereby certify that I have reviewed and approve these data. � ''�?`} �(�, ��(�(`(� (�i (�� Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 x Y Y C O n y 0 2 O CL O ~ ~ F O ¢ c m ° u co I� O Chi (3) L N co W N o X CN O 1_ LO `O o) E E- co a N M : Ul #6 w 0) U a o O < O O cr x c6 Z a 0 E zUM) a v ti n 4J T r .Y W c W Z C a) CO N lU O co U a` r Q 2 N a >> z a na m Z n > Lt m O 3 t E � � O rc 3 - - 0 a O ° m E c = U # o at y v° `-' a [j a a v n � O a o c7 Y ° Z U Q Q u o E v E ° E 6 ° J O \ • W C U N fq v g E Q O m N a a o E > n o aQ Na !� f° o m p >. O ^V = cmw m" OA E r Sl E a V � •Q. 75 O F d ''�- BTM o � N N c W m z U o o T _LPU (D o m cu Lu •� E O W m ;� v> .> a a u � U � O i 3 u O j 3 JO 0) Lnwa o" a v c � D C� C APPENDIX 4 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RS CA Chapel Ridge WWTP Field Loading Calculations Analytical State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water ResoUKes RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: 2. Facility permit holder is: Federal, 0 State, 0 Local Government, or ® Private. Facility permit issued by: Div. of Water Resources, Div. of Environmental Health, or Other (explain: M. 3. Facility contact person and title: Roger Tupps, Area Manager Complete mailing address: F02 MacKenan Court City: = State: NC Zip: 27597- Telephone number: (919) 632-6120 E-mail address: RBTupTskaquaamerica.com 4. Facility physical address: Hardwood Forest Trail City: - State: NC Zip: 7� 312- Coordinates: Latitude: 35' 47' 7.4" Longitude: M° J4' 10.7" Datum: NAD 83 Level of accuracy: Sub -Meter Method of measurement: 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water, treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: 0 MGD and facility average daily flow: 0.07 MGD 8. Average amount of residuals being generated at this facility E dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 70,000 gallon Aeration; Type and volume of residuals storage (i.e., outside of residuals treatment units): 90,000 gallon Sludge Storage Tank II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ® Biological 0 Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 11-13 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no. If yes, list the number(s): = b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: _ and Date of analysis: _ Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes no. Flashpoint: _ °F (> 140°F) Passed reactivity test: Eyes Ono. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500) TCLP Parameter Limit (mg/1) Result (Mg/1) TCLP Parameter Limit (Mg/1) Result (Mg/1) Arsenic 5.0 Hexachlorobenzene 0.13 Barium 100.0 Hexachloro-1,3-Butadiene 0.5 Benzene 0.5 Hexachloroethane 3.0 Cadmium 1.0 Lead 5.0 Carbon Tetrachloride 0.5 Lindane 0.4 Chlordane 0.03 Mercury 0.2 Chlorobenzene 100.0 Methoxychlor 10.0 Chloroform 6.0 Methyl Ethyl Ketone 200.0 Chromium 5.0 Nitrobenzene 2.0 m-Cresol 200.0 Pentachlorophenol 100.0 o-Cresol 200.0 Pyridine 5.0 p-Cresol 200.0 Selenium 1.0 Cresol 200.0 Silver 5.0 2,4-D 10.0 Tetrachloroethylene 0.7 1,4-Dichlorobenzene 7.5 Toxaphene 0.5 1,2-Dichloroethane 0.5 Trichloroethylene 0.5 1,1-Dichloroethylene 0.7 2,4,5-Trichlorophenol 400.0 2,4-Dinitrotoluene 0.13 2,4,6-Trichlorophenol 2.0 Endrin 0.02 2,4,5-TP (Silvex) 1.0 Heptachlor and its Hydroxide 0.008 Vinyl Chloride 0.2 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Peritech Inc. and Date of analysis: 06/19/19 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <0.963 Cadmium 85 39 1.89 Copper 4,300 1,500 717 Lead 840 300 29.5 Mercury 57 17 0.125 Molybdenum 75 n/a 1.95 Nickel 420 420 18.1 Selenium 100 100 1.38 Zinc 7,500 2,800 2,470 b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) 11 > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: a %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory:lkeritech Inc. and Date of analysis: 06/19/19 Parameter Result (mg/kg) Aluminum 19,500 Ammonia -Nitrogen 320 Calcium 25,600 Magnesium 3,240 Nitrate -Nitrite Nitrogen 102 pH (Standard Unit) 6.6 Phosphorus 20,200 Potassium 1,500 Sodium 3,510 Total Kjeldahl Nitrogen 16,600 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1.25 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: ii e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 5,146 8,095 Injection/Incorporation 5,306 8,213 6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106 i 3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, oi I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. it, FIELD LOADING ESTIMATES Facility Chapel Ridge WWTP Sampling Date 6/19/2019 % Solids 5.19 Mineralization Rate 0.30 Gallons per DT 4,620.58 pH 6.6 Sodium Absorpotion 1.25 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 16,600 lbs./1,000 gal 7.19 Ammonia Nitrogen (mg/Kg) 320.00 lbs./1,000 gal 0.14 Nitrate -Nitrite (mg/Kg) 102.00 lbs./1,000 gal 0.04 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 5,146 lbs./1,000 gal 2.23 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 5,306 lbs./1,000 gal 2.30 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 0.65 Phosphorus lbs./1,000 gal 8.74 Calcium lbs./1,000 gal 11.08 Magnesium lbs./1,000 gal 1.40 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 0.96 Arsenic lbs./1,000 gal 0.00 Cadmium (mg/Kg) 1.89 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 717.00 Copper lbs./1,000 gal 0.31 Lead (mg/Kg) 29.50 Lead lbs./1,000 gal 0.01 Mercury (mg/Kg) 0.13 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 18.10 Nickel lbs./1,000 gal 0.01 Selenium (mg/Kg) 1.38 Selenium lbs./1,000 gal 0.00 Zinc (mg/Kg) 2470.00 Zinc lbs./1,000 gal 1.07 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) 16,600 5,146 10.29 11,454 16,600 5,306 10.61 11,294 11,454 1,718 3.44 9,736 11,294 1,694 3.39 9,600 9,736 730 1.46 9,006 9,600 720 1.44 8,880 9,006 338 0.68 8,668 8,880 333 0.67 8,547 8,668 163 0.33 8,505 8,547 160 0.32 8,387 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Total 8,095 16.19 Total 8,213 16.43 Meritech, Inc. x;Environmental Laboratory Laboratory Certification No. 165 Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Date Report Date: Project: Sample Rcvd: 7/2/2019 Chapel Ridge 6/19/2019 Meritech Work Order # 061919114 Sample: CR061919 Grab 6/19/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 5.19 % 6/21/19 0-100 % SM 2540B Ammonia, Nitrogen 320 mg/kg 6/25/19 10 mg/kg EPA 350.1 TKN 16,600 mg/kg 6/27/19 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen 102 mg/kg 6/21/19 31.3 mg/kg EPA 353.2 Aluminum, total 19,500 mg/kg 6/27/19 2.50 mg/kg EPA 2003 Arsenic, total <0.963 mg/kg 6/27/19 0.963 mg/kg EPA 2003 Cadmium, total 1.89 mg/kg 6/27/19 0.20 mg/kg EPA 2003 Calcium, total 25,600 mg/kg 6/27/19 10.0 mg/kg EPA 2003 Copper, total 717 mg/kg 6/27/19 1.00 mg/kg EPA 2003 Lead, total 29.5 mg/kg 6/27/19 0.500 mg/kg EPA 200.7 Magnesium, total 3,240 mg/kg 6/27/19 10.0 mg/kg EPA 2003 Mercury, total 0.125 mg/kg 6/25/19 0.02 mg/kg EPA 245A Molybdenum, total 1.95 mg/kg 6/27/19 0.500 mg/kg EPA 2003 Nickel, total 18.1 mg/kg 6/27/19 2.0 mg/kg EPA 2003 Phosphorus, total 20,200 mg/kg 6/27/19 2.00 mg/kg EPA 2003 Potassium, total 1,500 mg/kg 6/27/19 20.0 mg/kg EPA 200.7 Selenium, total 1.38 mg/kg 6/27/19 0.50 mg/kg EPA 2003 Sodium, total 3,510 mg/kg 6/27/19 20.0 mg/kg EPA 2003 Zinc, total 2,470 mg/kg 6/27/19 0.500 mg/kg EPA 2003 pH 6.6 S.U. 6/20/19 1.0 - 14.0 S.U. SM 4500-HB I hereby certi/y that 1 have reviewed and approve these data. � (� �� Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336]342-1522 T Y Y ° O M a C Q v D'' E � 1 5 z a v j 0 u E E F i= _ � m tf c Y �0` M V H = y..; o Q 0 O N M c6 -1- N ..• m w - v L c11 •F it AT E Z a LL w a` 2• T v Y CD H LL _ W a N L LO E CD = Z aLw1Ut 3 � O x 0 o co O Li 14 mo {l0vdy'l� a-Ee 0 a i=v _ ~gyOHNEE E EF- cis 0oE O mNO Eo . a @ ° �m °M c `U m wm uN Ep 1�-U7UN1i— o o -Np N uL.I E U sLR E uw o EU vs; ° U WW c G a ry N 0 y - u O 0 - _ - C p U O AdoL_L LL c Q i Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Report Date: Project: Date Sample Rcvd: Page 1 9/10/2019 Chapel Ridge 8/21/2019 Meritech Work Order # 08211990 Sample: CRO82119 Grab 8/21/2019 1311- TCLP Metals Parameter Results Analysis Date Det. Limit Reg. Limit Method Arsenic <0.100 mg/L 8/28/2019 0.100 5.0 EPA 2003 Barium 0.685 mg/L 8/28/2019 0.050 100.0 EPA 2003 Cadmium <0.020 mg/L 8/28/2019 0.020 1.0 EPA 2003 Chromium 0.061 mg/L 8/28/2019 0.050 5.0 EPA 200.7 Lead <0.100 mg/L 8/28/2019 0.100 5.0 EPA 200.7 Mercury <0.02 mg/L 8/28/2019 0.02 0.2 EPA 245A Selenium <0.100 mg/L 8/28/2019 0.100 1.0 EPA 200.7 Silver <0.050 mg/L 8/28/2019 0.050 5.0 EPA 200.7 TCLP Organics Parameter Results Analysis Date Reporting Limit Method Volatiles 8260 Attached 8/26/2019 8260 Semi Vol. 8270 Attached 8/29/2019 8270 Other Tests Parameter Results Anal�is Date Reporting Limit Method %Total Solids 6.25 % 8/22/2019 0-100 % SM 2540B Cyanide, total <0.500 mg/lcg 9/3/2019 0.500 mg/kg EPA 335.4 Sulfide <10.0 mg/kg 8/27/2019 10.0 mg/kg SM4500S2D Ignitability >140 OF 8/28/2019 EPA 1030 Corrositivity (pH) 6.5 S.U. 8/22/2019 1.0 - 14.0 S.U. SM 4500 HB 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 2 Contact: Drew Matthews Report Date: 9/10/2019 Client: Soil Plus P.O. Box 1396 Project: Chapel Ridge Oxford, NC 27565 Date Sample Rcvd: 8/21/2019 Meritech Work Order # 08211990 Sample: CR082119 Grab 8/21/2019 1311 - TCLP Pesticides & Herbicides Pesticide - SW-846 8081A Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor Endrin Attached - - Chlordane Attached Toxaphene Attached Methoxychlor Attached Heptachlor Attached Lindane Attached Herbicides - SW-846 8151A Parameter 2,4-D 2,4,5-TP (Silvex) Results Analysis Date Det. Limit Reg. Limit Dilution Factor Attached Attached I hereby certify that 1 have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)3424522 MERI TECH, INC. Environmental Laboratories Laboratory Certificate #165 Client: Project: Client Sample ID: Sample Collection: Meritech Sample 1D: Volatiles: SW-846 8260 Analysis: 08/26/19 Analyst: V W V Parameter Soil Plus Chapel Ridge CR082119 08/21/19 08211990 1311 - TCLP Organics Extraction: 08/22/19 Report Date: 09/02/19 Result Units Det. Limit Re¢. Limit Dilution Factor Benzene < 0.0100 mg/L 0.0100 0.50 10 CarbonTetrachloride <0,0100 mg/L 0,0100 0,50 10 Chlorobenzene < 0,0100 mg/L 0,0100 100 10 Chloroform <0,0100 mg/L 0,0100 6.0 10 1,2-Dichloroethane < 0,0100 mg/L 0,0100 0,50 10 1,1-Dichloroethene <0,0100 re 0,0100 0,70 10 Methyl Ethyl Ketone <0,100 mg/L 0,100 200 10 Tetrachloroethylene < 0.0100 mg/L 0,0100 0,70 10 Trichloroethene < 0,0100 mg/L 0,0100 0,50 10 Vinyl Chloride <0,0200 mg/L 0,020 0,20 10 Semi-Volatiles: SW-8468270 Analysis: 08/29/19 Extraction: 08/22/19 Analyst: PM Report Date: 09/04/19 Parameter Result Units Det. Limit Ree. Limit Dilution Factor 1,4-Dichlorobenzene <0,100 mg/L 0.100 7.5 10 Hexachlorobenzene <0.100 me 0,100 0,13 10 Hexachloro-1,3-butadiene <0.100 mg/L 0,100 0.5 10 Hexachloroethane <0.100 mg/L 0,100 3,00 10 o-cresol <0.100 re 0,100 200 10 m&p-cresol <0.200 mg/L 0,200 200 10 Total cresols <0.300 mg/l. 0,300 200 10 Nitrobenzene <0.100 me 0,100 2,00 10 Pentachlorophenol <0.500 mg/L 0.500 100 10 Pyridine <0.100 mg/L 0,100 5.0 10 2,4,5-Trichlorophenol <0.100 mg/L 0,100 400 10 _.. _... 2,4,6-Trichlorophenol_ <0.100 __.mg/L 0.100 __. 2,00.. 10 _. 2,4-Dinihotoluene <0.100 mg/L 0.100 0,13 10 I hereby certify that I have reviewed and approve these data. YYL n---.--�bk , Laboratory Representative 642 Tamco Road *Reidsville, NC 27320 (336) 342-4748 *info@meritechlabs.com < , . . . . .. . . . .. .. . . . .. . . . . ... . . : . . . . � { . m § § e (\ ) } ) \ } \ \ { ° u \ \ / ` a = ; w _ = a / e= e= e s e= \ \ \ _ = m = m m = m \ \ \ ) k o d U O ad o F �`p I.Q�p y O C W C N 3 a- a E _ Sol LF Coo)rollO Sol W O N s= Q as K �l c a `vyyy,,..,. SolN _M N W o W •o 'Sol a s x w O m v E Z a LL a` a � � � (,• � � a y u SO O CIS LIB O v (C �� U m a v3 � LO o a O milln T 0 NCu a w K N ° CD ~ Cf)U a Z a' � O "6 o - - d coO 3 Sol Y E LL O iC o d O o m m y = u Y iA a Sol Lf' M O U u a a P r i= ti N E a } p O low N p O W @ G fl O O Q vNi ZJim u d M N G m M t u u m e N s - � SO V a n v fl g H v io E @ r E o cu z o W Imm CA N 42 � U Z r o N 0IS o v N� _ n' N c N W N N SON W N E -i— o a a 3 u > g u w •� yx N O z z w a p v; `E ° Q v G G INN 0 O � O \ ESYS _ i U z E @ O - - - = U cY ¢ O V- u O � J N � O1 x w ai N � O a So L a +�+ a LL O U Sol N = APPENDIX 5 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RS CA Cottonwood/Baywood WWTP Field Loading Calculations Analytical DWR Division of Water ResoUKes State of North Carolina Department of Environment and Natural Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Cottonwood/Baywood WWI 2. Facility permit holder is: ❑ Federal, A State, 0 Local Government, or ® Private. Facility permit issued by: ■ Div. of Water Resources, Div. of Environmental Health, or ❑ Other (explain: �. 3. Facility contact person and title: Lucille C. Ginsbere Complete mailing address: 7536 NC HWY 39 City: Zebulon State: NC Zip: 27597 Telephone number: (919) 404-1668 E-mail address: crosbywater@bellsouth.net 4. Facility physical address: Bethlehem Road City: m State: NC Zip: 545- Coordinates: Latitude: 35' 45' 42.9" Longitude: 78' 28' 24.6" Datum: NAD 83 Level of accuracy: Sub -Meter Method of measurement: 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water, treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: Q95A MGD and facility average daily flow: = MGD 8. Average amount of residuals being generated at this facility E dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 0.0575 MG Extended Aeration' Type and volume of residuals storage (i.e., outside of residuals treatment units): 13,000 Gallon Sludge Holding Tank II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ® Biological 0 Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 11-13 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no. If yes, list the number(s): = b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: _ and Date of analysis: _ Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes no. Flashpoint: _ °F (> 140°F) Passed reactivity test: Eyes Ono. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500) TCLP Parameter Limit (mg/1) Result (Mg/1) TCLP Parameter Limit (Mg/1) Result (Mg/1) Arsenic 5.0 Hexachlorobenzene 0.13 Barium 100.0 Hexachloro-1,3-Butadiene 0.5 Benzene 0.5 Hexachloroethane 3.0 Cadmium 1.0 Lead 5.0 Carbon Tetrachloride 0.5 Lindane 0.4 Chlordane 0.03 Mercury 0.2 Chlorobenzene 100.0 Methoxychlor 10.0 Chloroform 6.0 Methyl Ethyl Ketone 200.0 Chromium 5.0 Nitrobenzene 2.0 m-Cresol 200.0 Pentachlorophenol 100.0 o-Cresol 200.0 Pyridine 5.0 p-Cresol 200.0 Selenium 1.0 Cresol 200.0 Silver 5.0 2,4-D 10.0 Tetrachloroethylene 0.7 1,4-Dichlorobenzene 7.5 Toxaphene 0.5 1,2-Dichloroethane 0.5 Trichloroethylene 0.5 1,1-Dichloroethylene 0.7 2,4,5-Trichlorophenol 400.0 2,4-Dinitrotoluene 0.13 2,4,6-Trichlorophenol 2.0 Endrin 0.02 2,4,5-TP (Silvex) 1.0 Heptachlor and its Hydroxide 0.008 Vinyl Chloride 0.2 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: environment 1, A and Date of analysis: 3/26/2019 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <2.5 Cadmium 85 39 1.3 Copper 4,300 1,500 208 Lead 840 300 11 Mercury 57 17 0.57 Molybdenum 75 n/a 13 Nickel 420 420 8 Selenium 100 100 <5.0 Zinc 7,500 2,800 1,166 b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) 11 > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: a %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: environment 1, Ir>♦ and Date of analysis: 03/26/2019 Parameter Result (mg/kg) Aluminum 3,157 Ammonia -Nitrogen 509.1 Calcium 16,306 Magnesium 3,008 Nitrate -Nitrite Nitrogen 113.4 pH (Standard Unit) 6.8 Phosphorus 25,610 Potassium 6,585 Sodium 21,932 Total Kjeldahl Nitrogen 46,270 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): - [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: ii e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 14,096 22,379 Injection/Incorporation 14,351 22,568 6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106 i 3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, oi I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. it, Facility Cottonwood/Baywood WWTP FIELD LOADING ESTIMATES Sampling Date 3/26/2019 % Solids 0.49 Mineralization Rate 0.3 Gallons per DT 48,940.44 pH 6.8 Sodium Absorpotion 2.89 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 46,270 lbs./1,000 gal 1.89 Ammonia Nitrogen (mg/Kg) 509.10 lbs./1,000 gal 0.02 Nitrate -Nitrite (mg/Kg) 113.40 lbs./1,000 gal 0.00 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 14,096 lbs./1,000 gal 0.58 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 14,351 lbs./1,000 gal 0.59 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 0.27 Phosphorus lbs./1,000 gal 1.05 Calcium lbs./1,000 gal 0.67 Magnesium lbs./1,000 gal 0.12 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 2.50 Arsenic lbs./1,000 gal 0.00 Cadmium (mg/Kg) 1.30 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 208.00 Copper lbs./1,000 gal 0.01 Lead (mg/Kg) 11.00 Lead lbs./1,000 gal 0.00 Mercury (mg/Kg) 0.57 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 8.00 Nickel lbs./1,000 gal 0.00 Selenium (mg/Kg) 5.00 Selenium lbs./1,000 gal 0.00 Zinc (mg/Kg) 1166.00 Zinc lbs./1,000 gal 0.05 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) 46,270 14,096 28.19 32,174 46,270 14,351 28.70 31,919 32,174 4,826 9.65 27,348 31,919 4,788 9.58 27,131 27,348 2,051 4.10 25,297 27,131 2,035 4.07 25,096 25,297 949 1.90 24,348 25,096 941 1.88 24,155 24,348 457 0.91 23,891 24,155 453 0.91 23,702 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Total 22,379 44.76 Total 22,568 45.14 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 COTTONWOOD ATTN: LUCI CROSBY CROSBY WATER & SEWER 7536 NC HWY 39 SOUTH ZEBULON ,NC 27807 PARAMETERS PH (not to be used for reporting) Aluminum, (dry wt. basis), mglkg Arsenic (dry wt. basis), mglkg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mglkg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 6.8 03/26/19 TCW 4500HB-11 3157 04/04/19 LFJ EPA200.7 2.5 04/04/19 MTM 3113B-04 16306 04/04/19 LFJ EPA200.7 1.3 04/08/19 MTM 3113B-04 208 04/04/19 LFJ EPA200.7 6 04/04/19 LFJ EPA200.7 11 04/05/19 MTM 3113B-04 3008 04/04/19 LFJ EPA200.7 0.57 04/17/19 MTM EPA7471B 8 04/04/19 LFJ EPA200.7 6585 04/04/19 LFJ EPA200.7 C5.0 04/10/19 MTM 3113B-04 21932 04/18/19 AKS 3111B-11 1166 04/04/19 LFJ EPA200.7 0.49 03/28/19 KDS 254OG-11 c 46270 03/29/19 TLH 351.2 R2-93 c 509.1 04/01/19 CLO 350.1 R2-93 c 25610 04/02/19 CLO 365.4-74 c 113.4 04/02/19 DTL 353.2 R2-93 14096 04/05/19 SEJ 13 04/04/19 LFJ EPA200.7 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 339 C DATE COLLECTED: 03/26/19 DATE REPORTED : 04/22/19 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. APPENDIX 6 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RS CA Lake Royale WWTP Field Loading Calculations Analytical State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water ResoUKes RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: 2. Facility permit holder is: Federal, 0 State, 11 Local Government, or ® Private. Facility permit issued by: Div. of Water Resources, IN Div. of Environmental Health, or Other (explain: `). 3. Facility contact person and title: Total Environmental Solutions, Inc. Complete mailing address: P.O. Box 14059 City: Baton Rouge State: Zip: 70898-4059 Telephone number: 52) 478-4704 E-mail address: dhartgtesi-usa.com 4. Facility physical address: NCSR 1611 City: � State: NC Zip: 7549- Coordinates: Latitude: 35' 57' 0111" Longitude: 78' 11' 27.0" Datum: NAD 83 Level of accuracy: Sub -Meter Method of measurement: 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water, treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes ® No 7. Facility permitted/design flow: 0.080 MGD and facility average daily flow: 0.0027 MGD 8. Average amount of residuals being generated at this facility < 5 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 0.08 MG Aeration Tank(s) Type and volume of residuals storage (i.e., outside of residuals treatment units): 5,000 Gallon Sludge Holding Tank II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ® Biological 0 Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 11-13 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no. If yes, list the number(s): = b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: _ and Date of analysis: _ Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes no. Flashpoint: _ °F (> 140°F) Passed reactivity test: Eyes Ono. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500) TCLP Parameter Limit (mg/1) Result (Mg/1) TCLP Parameter Limit (Mg/1) Result (Mg/1) Arsenic 5.0 Hexachlorobenzene 0.13 Barium 100.0 Hexachloro-1,3-Butadiene 0.5 Benzene 0.5 Hexachloroethane 3.0 Cadmium 1.0 Lead 5.0 Carbon Tetrachloride 0.5 Lindane 0.4 Chlordane 0.03 Mercury 0.2 Chlorobenzene 100.0 Methoxychlor 10.0 Chloroform 6.0 Methyl Ethyl Ketone 200.0 Chromium 5.0 Nitrobenzene 2.0 m-Cresol 200.0 Pentachlorophenol 100.0 o-Cresol 200.0 Pyridine 5.0 p-Cresol 200.0 Selenium 1.0 Cresol 200.0 Silver 5.0 2,4-D 10.0 Tetrachloroethylene 0.7 1,4-Dichlorobenzene 7.5 Toxaphene 0.5 1,2-Dichloroethane 0.5 Trichloroethylene 0.5 1,1-Dichloroethylene 0.7 2,4,5-Trichlorophenol 400.0 2,4-Dinitrotoluene 0.13 2,4,6-Trichlorophenol 2.0 Endrin 0.02 2,4,5-TP (Silvex) 1.0 Heptachlor and its Hydroxide 0.008 Vinyl Chloride 0.2 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Peritech Inc. and Date of analysis: - Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <1.81 Cadmium 85 39 3.97 Copper 4,300 1,500 750 Lead 840 300 42.8 Mercury 57 17 0.217 Molybdenum 75 n/a 5.29 Nickel 420 420 10.4 Selenium 100 100 2.22 Zinc 7,500 2,800 1,880 b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) 11 > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: a %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory:lkeritech Inc. and Date of analysis: - Parameter Result (mg/kg) Aluminum 10,500 Ammonia -Nitrogen 2,620 Calcium 11,500 Magnesium 1,440 Nitrate -Nitrite Nitrogen <361 pH (Standard Unit) 6.7 Phosphorus 10,300 Potassium 1,780 Sodium 2,380 Total Kjeldahl Nitrogen 20,600 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.92 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: ii e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 7,065 10,549 Injection/Incorporation 8,375 11,522 6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106 i 3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, oi I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. it, FIELD LOADING ESTIMATES Facility Lake Royale Sampling Date 5/31/2019 % Solids 2.77 Mineralization Rate 0.30 Gallons per DT 8,657.33 pH 6.7 Sodium Absorpotion 0.92 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 20,600 lbs./1,000 gal 4.76 Ammonia Nitrogen (mg/Kg) 2,620.00 lbs./1,000 gal 0.61 Nitrate -Nitrite (mg/Kg) 361.00 lbs./1,000 gal 0.08 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 7,065 lbs./1,000 gal 1.63 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 8,375 lbs./1,000 gal 1.93 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 0.41 Phosphorus lbs./1,000 gal 2.38 Calcium lbs./1,000 gal 2.66 Magnesium lbs./1,000 gal 0.33 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 1.81 Arsenic lbs./1,000 gal 0.00 Cadmium (mg/Kg) 3.97 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 750.00 Copper lbs./1,000 gal 0.17 Lead (mg/Kg) 42.80 Lead lbs./1,000 gal 0.01 Mercury (mg/Kg) 0.22 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 10.40 Nickel lbs./1,000 gal 0.00 Selenium (mg/Kg) 2.22 Selenium lbs./1,000 gal 0.00 Zinc (mg/Kg) 1880.00 Zinc lbs./1,000 gal 0.43 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) 20,600 7,065 14.13 13,535 20,600 8,375 16.75 12,225 13,535 2,030 4.06 11,505 12,225 1,834 3.67 10,391 11,505 863 1.73 10,642 10,391 779 1.56 9,612 10,642 399 0.80 10,243 9,612 360 0.72 9,251 10,243 192 0.38 10,051 9,251 173 0.35 9,078 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Total 10,549 21.10 Total 11,522 23.04 Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Meritech Work Order # 05311923 Parameters Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Sample: LR053119 Grab Results Analysis Date Report Date: Project: Date Sample Rcvd: 6/12/2019 Lake Royale 5/31/2019 5/31/19 RenortingLimit Method %Total Solids 2.77 % 6/5/19 0-100 % SM 2540B Ammonia, Nitrogen 2620 mg/kg 6/6/19 10 mg/kg EPA 350.1 TKN 20,600 mg/kg 6/7/19 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <361 mg/kg 6/4/19 361 mg/kg EPA 353.2 Aluminum, total 10,500 mg/kg 6/5/19 2,50 mg/kg EPA 200.7 Arsenic, total <1.81 mg/kg 6/5/19 1.81 mg/kg EPA 200.7 Cadmium, total 3.97 mg/kg 6/5/19 0.20 mg/kg EPA 200.7 Calcium, total 11,500 mg/kg 6/5/19 10.0 mg/kg EPA 200.7 Copper, total 750 mg/kg 6/5/19 1.00 mg/kg EPA 200.7 Lead, total 42.8 mg/kg 6/5/19 0.500 mg/kg EPA 200.7 Magnesium, total 1,440 mg/kg 6/5/19 10.0 mg/kg EPA 200.7 Mercury, total 0.217 mg/kg 6/10/19 0.02 mg/kg EPA 245.1 Molybdenum, total 5.29 mg/kg 6/5/19 0.500 mg/kg EPA 200.7 Nickel, total 10.4 mg/kg 6/5/19 2.0 mg/kg EPA 200.7 Phosphorus, total 10,300 mg/kg 6/5/19 2.00 mg/kg EPA 200.7 Potassium, total 1,780 mg/kg 6/5/19 20.0 mg/kg EPA 2003 Selenium, total 2.22 mg/kg 6/5/19 2.63 mg/kg EPA 200.7 Sodium, total 2,380 mg/kg 6/5/19 20.0 mg/kg EPA 200.7 Zinc, total 1,880 mg/kg 6/5/19 0.500 mg/kg EPA 2003 pH 6.7 S.U. 6/4/19 1.0 - 14.0 S.U. SM 4500-HB I hereby certify that 1 have reviewed and approve these data. �, (�(' �) Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 0 C :c00 °£e(\\, _ `E \ • ; ! / ) 2, k w � /} / k / aCL }; § ®k \ } %ail . \ § 7 © \ S 0) 3 0._ _ in CO } < . c * � � § . \ \ \ E - . ® ` ! \ ) _? § ` ® \ \CL \ ® $ / Co \ \ ) & n o / _ \ § \ a \ r ƒ # - \ \ \ / \ / / .2 \ . / eƒ a\ r ° \ ) E e / 2 ) / ! r \ } # i= i= / ® } ) \ ,. \ \ § t Q _ 2 \ ( a 3 \ U 7 C9 , » u § ) j E © \ r - _ $ / O ) \ V < t « 0 a)} \ ® \ - {) 14 z . \ / 2 \ 0 e O kn E \ - - ) � $ t 0 E- , - _ 3 0 Q ` ƒ % = E 3 ) , / \ \ \ 2� k \ 2 �. ®/DS APPENDIX 7 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RS CA Lewiston Woodville WWTP Field Loading Calculations Analytical State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water KesoUFces RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Lewiston Woodville WWTP 2. Facility permit holder is: ❑ Federal, A State, N Local Government, or 0 Private. Facility permit issued by: ® Div. of Water Resources, Div. of Environmental Health, or ❑ Other (explain: �. 3. Facility contact person and title: James Pujzh Complete mailing address: 103 W. Church Stree'i City: Lewiston Woodville State: NC Zip: 27849- Telephone number: (252) 348-2824 E-mail address: lewistonwoodville(a�gmail.com 4. Facility physical address: 346 NC Highway 11 City: Lewiston Woodville State: Zip: 27849- Coordinates: Latitude: 36' 8' 35" Longitude: id' /' 53" Datum: NAD 83 Level of accuracy: Sub -Meter Method of measurement: 5. Purpose of the facility: ®' treatment of municipal wastewater, treatment of 100% domestic wastewater, ❑ treatment of potable water, treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: E MGD and facility average daily flow: = MGD 8. Average amount of residuals being generated at this facility - dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 0.64 MG Aeration Basin Type and volume of residuals storage (i.e., outside of residuals treatment units): 15,000 Gallon Aerobic Digester II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: Biological 0 Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 11-13 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Meritech, Inc and Date of analysis: MMW2 Passed corrosivity test: yes no. pH: 6.4 s.u. (2 < pH < 12.5) Passed ignitability test: yes no. Flashpoint: � OF (> 140°F) Passed reactivity test: Oyes Ono. HCN: _ mg/kg (<250) & H2S: 10.0 mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (Mg/1) Result (Mg/1) Arsenic 5.0 <0.100 Hexachlorobenzene 0.13 <0.100 Barium 100.0 0.102 Hexachloro-1,3-Butadiene 0.5 <0.100 Benzene 0.5 <0.0100 Hexachloroethane 3.0 <0.100 Cadmium 1.0 <0.020 Lead 5.0 <0.100 Carbon Tetrachloride 0.5 <0.0100 Lindane 0.4 <0.040 Chlordane 0.03 <0.003 Mercury 0.2 <0.02 Chlorobenzene 100.0 <0.0100 Methoxychlor 10.0 <1.000 Chloroform 6.0 <0.0100 Methyl Ethyl Ketone 200.0 <0.100 Chromium 5.0 <0.050 Nitrobenzene 2.0 <0.100 m-Cresol 200.0 <0.200 Pentachlorophenol 100.0 <0.500 o-Cresol 200.0 <0.100 Pyridine 5.0 <0.100 p-Cresol 200.0 <0.200 Selenium 1.0 <0.100 Cresol 200.0 <0.300 Silver 5.0 <0.050 2,4-D 10.0 <1.000 Tetrachloroethylene 0.7 <0.0100 1,4-Dichlorobenzene 7.5 <0.100 Toxaphene 0.5 <0.05 1,2-Dichloroethane 0.5 <0.0100 Trichloroethylene 0.5 <0.0100 1,1-Dichloroethylene 0.7 <0.0100 2,4,5-Trichlorophenol 400.0 <0.100 2,4-Dinitrotoluene 0.13 <0.100 2,4,6-Trichlorophenol 2.0 <0.100 Endrin 0.02 <0.002 2,4,5-TP (Silvex) 1.0 <0.100 Heptachlor and its Hydroxide 0.008 <0.0008 Vinyl Chloride 0.2 <0.0200 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: [jeriteM and Date of analysis: - Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <2.29 Cadmium 85 39 1.76 Copper 4,300 1,500 195 Lead 840 300 52.8 Mercury 57 17 0.069 Molybdenum 75 n/a 4.28 Nickel 420 420 9.77 Selenium 100 100 <2.29 Zinc 7,500 2,800 541 b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) I > 0 but < 25 30 200 210 Ej > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 j > 100 but < 125 53 360 390 El > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: a %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: keriteM M and Date of analysis: - Parameter Result (mg1kP) Aluminum 19,000 Ammonia -Nitrogen <459 Calcium 7,750 Magnesium 1,630 Nitrate -Nitrite Nitrogen 2,640 pH (Standard Unit) 6 Phosphorus 6,560 Potassium 2,090 Sodium 5,700 Total Kjeldahl Nitrogen 13,400 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 2.26 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): E default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex Iain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: ii e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (m91k9) (mg/kg) Surface 6,752 8,463 Injection/Incorporation 6,981 8,634 6. Other Pollutants Determination: SpecifX whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: None 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, 4 heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, or I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item Il. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. 0 Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. 1 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FIELD LOADING ESTIMATES Facility Lewiston -Woodville WWTP Sampling Date 7/11/2019 % Solids 2.18 Mineralization Rate 0.30 Gallons per DT 11,000.37 PH 6 Sodium Absorpotion 2.26 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 13,400 lbs./1,000 gal 2.44 Ammonia Nitrogen (mg/Kg) 459.00 lbs./1,000 gal 0.08 Nitrate -Nitrite (mg/Kg) 2,640.00 lbs./1,000 gal 0.48 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 6,752 lbs./1,000 gal 1.23 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 6,981 lbs./1,000 gal 1.27 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 0.38 Phosphorus lbs./1,000 gal 1.19 Calcium lbs./1,000 gal 1.41 Magnesium lbs./1,000 gal 0.30 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 2.29 Arsenic lbs./1,000 gal 0.00 Cadmium (mg/Kg) 1.76 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 195.00 Copper lbs./1,000 gal 0.04 Lead (mg/Kg) 52.80 Lead lbs./1,000 gal 0.01 Mercury (mg/Kg) 0.07 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 9.77 Nickel lbs./1,000 gal 0.00 Selenium (mg/Kg) 2.29 Selenium lbs./1,000 gal 0.00 Zinc (mg/Kg) 541.00 Zinc lbs./1,000 gal 0.10 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) T (mg/kg) (lbs/DT) (mg/Kg) 13,400 6,752 13.50 6,648 13,400 6,981 13.96 6,419 6,648 997 1.99 5,651 6,419 963 1.93 5,456 5,651 424 0.85 5,227 5,456 409 0.82 5,047 5,227 196 0.39 5,031 5,047 189 0.38 4,857 5,031 94 0.19 4,937 4,857 91 0.18 4,766 Equations 1 st Yr. PAN (mg/I0=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Total 8,463 16.93 Total 8,634 17.27 Meritech, Inc. rk Environmental Laboratory Laboratory Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Revised Date, Report Date: Project: Date Sample Rcvd: 8/5/2019 7/23/2019 Lewiston 7/11/2019 Meritech Work Order # 071119129 Sample: LW071119 Grab 7/11/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 2,18 % 7/12/19 0-100 % SM 2540B Ammonia, Nitrogen <459 mg/kg 7/16/19 459 mg/kg EPA 350A TKN 13,400 mg/kg 8/2/19 20 mg/kg EPA 351A Nitrate/Nitrite, Nitrogen 2,640 mg/kg 7/17/19 31.3 mg/kg EPA 353.2 Aluminum, total 19,000 mg/kg 7/17/19 2,50 mg/kg EPA 200.7 Arsenic, total <2.29 mg/kg 7/17/19 2.29 mg/kg EPA 2003 Cadmium, total 1.76 mg/kg 7/17/19 0.20 mg/kg EPA 2003 Calcium, total 7,750 mg/kg 7/17/19 10.0 mg/kg EPA 200.7 Copper, total 195 mg/kg 7/17/19 1.00 mg/kg EPA 200.7 Lead, total 52.8 mg/kg 7/17/19 0.500 mg/kg EPA 200.7 Magnesium, total 1,630 mg/kg 7/17/19 10.0 mg/kg EPA 200.7 Mercury, total 0.069 mg/kg 7/16/19 0.02 mg/kg EPA 245A Molybdenum, total 4.28 mg/kg 7/17/19 0.500 mg/kg EPA 200.7 Nickel, total 9.77 mg/kg 7/17/19 2.0 mg/kg EPA 200.7 Phosphorus, total 6,560 mg/kg 7/17/19 2.00 mg/kg EPA 200.7 Potassium, total 2,090 mg/kg 7/17/19 20.0 mg/kg EPA 200.7 Selenium, total <2.29 mg/kg 7/17/19 2.29 mg/kg EPA 2003 Sodium, total 5,700 mg/kg 7/17/19 20.0 mg/kg EPA 200.7 Zinc, total 541 mg/kg 7/17/19 0.500 mg/kg EPA 200.7 pH 6.0 S.U. 7/12/19 1.0 - 14.0 S.U. SM 4500-HB I hereby certify that I have reviewed and approve these data. AP mi� Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Z .a °. o °' E .ti--. a Yk m �♦ E E a co _ ce) V a e z N Q Y o o N M co a cp U d cr N c Z a L T V] N «o a E Z ` v - LO > N Z O LO Y �. CL Z W Z N Z ca V) X '6 m Y O a ~ ° m U � F u 0 s U Q Q o ;ZT t E N }- i= CN E co O N N O Z (0VN U T� co v m ^ E E m u + o m .n W = .ca o z UaE a o 2 C U m wo z _ o OC & W a "m �J o U w •L 3t Y C W O G C u c o ` � T' O CU E v S N Ln El 0eCll Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Contact: Drew Matthews Report Date: 8/16/2019 Client: Soil Plus P.O. Box 1396 Project: Lewiston Oxford, NC 27565 Date Sample Rcvd: 7/26/2019 Meritech Work Order # 07261946 Sample: LW072619 Grab 7/26/2019 1311- TCLP Metals Parameter Results Analysis Date Det. Limit Reg. Limit Method Arsenic <0.100 mg/L 8/7/2019 0,100 5.0 EPA 200.7 Barium 0,102 mg/L 8/7/2019 0,050 100.0 EPA 2003 Cadmium <0.020 mg/L 8/7/2019 0,020 1.0 EPA 2003 Chromium <0.050 mg/L 8/7/2019 0,050 5.0 EPA 200.7 Lead <0.100 mg/L 8/7/2019 0,100 5.0 EPA 200.7 Mercury <0.02 mg/L 7/30/2019 0,02 0.2 EPA 245A Selenium <0.100 mg/L 8/7/2019 0,100 1.0 EPA 2003 Silver <0.050 mg/L 8/7/2019 0,050 5.0 EPA 2003 TCLP Organics Parameter Results Analysis Date Reporting Limit Method Volatiles 8260 Attached 8/1/2019 8260 Semi Vol. 8270 Attached 8/8/2019 8270 Other Tests Parameter Results Analysis Date Reporting Limit Method %Total Solids 0,55 % 7/31/2019 0-100 % SM 2540B Cyanide, total <0.500 mg/kg 8/6/2019 0.500 mg/kg EPA 335A Sulfide <10.0 mg/kg 8/1/2019 10.0 mg/kg SM4500S2D Ignitability >140 °F 8/1/2019 EPA 1030 Corrositivity (pH) 6A S.U. 7/31/2019 1.0 - 14.0 S.U. SM 4500 HB 642 Tamco Road, Reidsville, North Carolina 27320 teL(336)342-4748 fax,(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: Drew Matthews Client: Soil Plus Page 2 Report Date: 8/16/2019 P.O. Box 1396 Project: Lewiston Oxford, NC 27565 Date Sample Rcvd: 7/26/2019 Meritech Work Order # 07261946 Sample: LW072619 Grab 7/26/2019 1311 - I LLP Pesticides & Herbicides Pesticide - SW-846 8081A Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor Endrin Attached - - - Chlordane Attached Toxaphene Attached Methoxychlor Attached Heptachlor Attached Lindane Attached Herbicides - SW-846 8151A Parameter Results Analvsis Date Det. Limit Ree. Limit Dilution Factor 2,4-D Attached - - - 2,4,5-TP (Silvex) Attached - - - I hereby certify thatl have reviewed and approve these data, ., ;� �(� � } Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 teL(336)342-4748 fax.(336)342-1522 MERITECH, INC. Environmental Laboratories Laboratory Certificate #165 Client: Soil Plus Project: Lewiston Client Sample ID: LW072619 Sample Collection: 07/26/19 Meritech Sample ID: 07261946 1311 - TCLP Oraanics Volatiles: SW-846 8260 Analysis: 08/01/19 Extraction: 07/29/19 Analyst: VWV Report Date: 08/12/19 Parameter Result Units Det. Limit Rea, Limit Dilution Factor Benzene <0,0100 mg/L 0.0100 0.50 10 Carbon Tetrachloride <0,0100 mg/L 0.0100 0.50 10 Chlorobenzene < 0.0100 mg/L 0.0100 100 10 Chloroform <0.0100 mg/L 0,0100 6.0 10 1,2-Dichloroethane < 0,0100 mg/L 0.0100 0,50 10 1,1-Dichloroethene < 0.0100 mg/L 0.0100 0.70 10 Methyl Ethyl Ketone <0,100 mg/L 0.100 200 10 Tetrachloroethylene < 0.0100 mg/L 0.0100 0.70 10 Trichloroethene < 0.0100 mg/L 0.0100 0.50 10 Vinyl Chloride < 0.0200 mg/L 0.020 0.20 10 Semi-Volatiles: SW-846 8270 Analysis: 08/OS/19 Extraction: 08/OS/19 Analyst: PM Report Date: 08/09/19 Parameter Result Units Det. Limit Rea. Limit Dilution Factor 1,4-Dichlorobenzene <0.100 mg/L 0,100 7.5 10 Hexachlorobenzene <0.100 mg/L 0.100 0.13 10 Hexachloro-1,3-butadiene <0.100 mg/L 0.100 0.5 10 Hexachloroethane <0.100 mg/L 0.100 3.00 10 o-cresol <0.100 mg/L 0.100 200 10 m&p-cresol <0.200 mg/L 0.200 200 10 Total cresols <0.300 mg/L 0,300 200 10 Nitrobenzene <0.100 mg/L 0.100 2.00 10 Pentachlorophenol <0.500 mg/L 0.500 100 10 Pyridine <0.100 mg/L 0.100 5.0 10 2,4,5-Trichlorophenol <0.100 mg/L 0.100 400 10 2,4,6-Trichlorophenol <0.100 mg/L 0.100 2,00 10 2,4-Dinitrotoluene <0.100 mg/L 0.100 0.13 10 I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road *Reidsville, NC 27320 (336) 342-4748 *info@meritechlabs.com 4 m ) e - m ) j § } Y C O tN CoO v C •� Ul # N « Q z O O _ •� � � E o_ Z LL E ti cr , A W O cd O y _ a+ +JCD a. CL V LO Y E U o > 1 a to>< O °' E m 3 N o E 0 o '°co m .. N •C U N d r Z II,IMIIIIIIIIII O v N ! E E E IT i= w rn r• w ^ Vu E u� d N N ti O O Y O w M o E c a o It Z OM a m v m o N w U m M V^i OU m M c E m = Q ii 11 = a d a�i f� _ > a m O LIJ N K W N \ d N nl t N N N W Ljj U w a s u' > 0 it O 5 w w 12 �✓ C Q v O u U K E O O C U ay O 3 w u O Z O N a w N 0 H o N / a 3 a 0 6 t O Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Contact: Drew Matthews Report Date: 8/7/2019 Client: Soil Plus P.O. Box 1396 Project: Lewiston Oxford, NC 27565 Date Sample Rcvd: 7/26/2019 Meritech Work Order # 07261939 Sample: LW072619 (001) Grab 7/26/19 Parameters Results Analysis Date Reporting Limit Method %Total Solids 0.94 % 7/31/19 0-100 % SM 2540B Fecal Coliform (Sludge) 2,901 col/g dry wt 7/26/19 208 col/g dry wt SM 9222D Meritech Work Order # 07261940 Sample: LW072619 (002) Grab 7/23/19 Parameters %Total Solids Fecal Coliform (Sludge) Results Analysis Date Reporting Limit Method 0.96 % 7/31/19 0-100 % SM 2540B 947 col/g dry wt 7/26/19 208 col/g dry wt SM 9222D Meritech Work Order # 07261941 Sample: LW072619 (003) Grab Parameters Results Analysis Date Reporting Limit %Total Solids 0.90 % 7/31/19 0-100 % Fecal Coliform (Sludge) 1,010 col/g dry wt 7/26/19 208 col/g dry wt Meritech Worlc Order # 07261942 Sample: LW072619 (004) Grab 7/23/19 Method SM 2540B SM 9222D 7/23/19 Parameters Results Analysis Date Reporting Limit Method %Total Solids 1.01 % 7/31/19 0-100 % SM 2540B Fecal Coliform (Sludge) 2,700 col/g dry wt 7/26/19 208 col/g dry wt SM 9222D Meritech Work Order # 07261943 Sample: LW072619 (005) Grab 7/23/19 Parameters Results Analysis Date Reporting Limit Method %Total Solids 0.99 % 7/31/19 0400 % SM 2540B Fecal Coliform (Sludge) 2,755 col/g dry wt 7/26/19 208 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Page 2 Report Date: 8/7/2019 Project: Lewiston Date Sample Rcvd: 7/26/2019 Meritech Work Order # 07261944 Sample: LW072619 (006) Grab Parameters 7/26/19 Results Analysis Date Reporting Limit Method %Total Solids 0.96 % 7/31/19 0-100 % SM 2540B Fecal Coliform (Sludge) 2,841 col/g dry wt 7/26/19 208 col/g dry wt SM 9222D Meritech Work Order # 07261945 Sample: LW072619 (007) Grab Parameters Results Analysis Date Reporting Limit %Total Solids 0.88 % 7/31/19 0-100 % Fecal Coliform(Sludge) 2,583 col/gdrywt 7/26/19 208 col/gdrywt 7/26/19 Method SM 2540B SM 9222D I hereby certify that! have reviewed and approve these data. �`�(� �'��� (� �(( Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 uz - E P E E N E to M I� a CA Lo s Ch '.� is rn� oo CA Cl CV u' C° E N 0) N Ul w c v # X O w E Z a LL w a a w S a O l0 N a 3 G Vi i 3 v o h [--aI-p F I-p I-p lf) p' °' O 4J 1- o 0 0 0 0 o Y O � o s CL Y E E E E E E E m r '= w E 0 - _ rn N o 0 0 o 0 o Q O T ."O- .0 .0 •0 0 O O N � Z -p a- U U U U U U U a N x o m m m m m O ti N E _ _ _ d m E N N N N aUi w ti w w w U. w w Oc 3 m n 0 d Q 0 N « m = u Y r z n a v w o C7 C9 C9 C9 C7 C9 C9 z r a O c U Q Q UCOO c .. .. .. t M Lo �xJ w `E o, �. a, o, rn o� V O O 7 Y N N N N N O O VN E W N Q m o e o o T V p Kt V Q Z O N N N N N N N E E O_ H m a /` d r !` n r r r t` Q (6 nAOmm t.i O O O O 1/1 6 O $ Z m zaaaaaaa4 OU = c N E Q x S J O a o a v° V ¢ a t 0 LJJ E ,— o N K ° H c / , m U m _ N c t• N_ p Z O M \ 0 .0 V N 3 � J > o w } o _N a u CN.� �L s z E v p ` s = � U cal m %at to o E UO ro O O O O O O p O C O O O 1 O CDp U O cu O 3 Q\ Q, Q\ a, 01 ON 01 C xv N E a L N N N N N N v O O O O Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: Drew Matthews Report Date: 9/6/2019 Client: Soil Plus P.O. Box 1396 Project: Lewiston Oxford, NC 27565 Date Sample Rcvd: 7/26/2019 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test) Meritech Worlc Order # 07261947 Week 1 Weelc 2 Week 3 Week 4 Week 5 Total Solids 0.840 0.740 0.710 0.760 0.620 Sample: LW072619 Grab Volatile Solids 0.350 0.310 0.280 0.290 0.250 7/26/19 Volatile Solids 0.419 0.425 0.395 0.380 0.396 Mass Balance Equation = 5.39%Volatile Solids Reduction as per EPA Part 503 Biosolids Rule I hereby certify that /have reviewed and approve these data. ���. A('A � �)C' C� .� ) Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)3424748 fax.(336)342-1522 cu M h N 0)� EY 3 ^ ti °P cn N W O j X no 4 N O) Q z 0 Nco N M N � Yk i; �✓ o � •� off- � X � � � w £ m c x a vai ci C cC ` N r v v 0 LO 0 a h s `o v C.0 >1 Y N o 0 c a Ci a m a Z u m to n Inw o a p o Y _ Y °44 g F Z F• v E U m a z �Ac� w N E E E c F y E N a o VYJCO 0 Q 0 N H 0 £ a o ZO m v u f\ y co 0 Q < ` U OU m05 Sl E a o x W LL • c �-- J 5 -6 V a N O, t c d v Q o W E i s o W o L co W s U C E 3 O U a i _ .v G O\ ci c O 3 O J l� O a -O t W 3 -o .. D_ Q li 0 APPENDIX 8 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RS CA Hominy Creek WRF Field Loading Calculations Analytical State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water KesoUFces RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: k WW 2. Facility permit holder is: ❑ Federal, 0 State, N Local Government, or 0 Private. Facility permit issued by: ® Div. of Water Resources, Div. of Environmental Health, or ❑ Other (explain: �. 3. Facility contact person and title: Jimmy Pridgen Complete mailing address: PO Box 10 City: Wilson State: Zip: 27894-0010 Telephone number: (252) 399-2491 E-mail address: jpridgengwilsonnc.org 4. Facility physical address: 3100 Old Stantonsburg Rd� City: ffilson State: NC Zip: 7894- Coordinates: Latitude: 35' 41' 15.4" Longitude: A° 5533' 40.3" Datum: NAD 83 Level of accuracy: Sub -Meter Method of measurement: 5. Purpose of the facility: ®' treatment of municipal wastewater, treatment of 100% domestic wastewater, ❑ treatment of potable water, treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: E MGD and facility average daily flow: 4.14 MGD 8. Average amount of residuals being generated at this facility = dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: conventional activated sludge with biological nutrient removal and tertiary treatment Type and volume of residuals storage (i.e., outside of residuals treatment units): 4 anaerobic digesters with a total volume of 2,346,500; belt press with a covered 32,000 square ft storage pad holding annroximately 216,000 cubic ft II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: Biological 0 Non -Biological FORM: RSC 11-13 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: U yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Tmerican Testing Technologies, Inc. and Date of analysis: 2/7/18 Passed corrosivity test: ® yes ❑ no. pH: 6.8 s_u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: _ OF (> 140°F) Passed reactivity test: 19yes Eno. HCN: " mg/kg (<250) & HZS: W mg/kg (<500) TCLP Parameter Limit (Mg/1) Result (Mg/1) TCLP Parameter Limit (mg/l) Result (mg/1) Arsenic 5.0 < 1.0 Hexachlorobenzene 0.13 < 0.05 Barium 100.0 < 10 Hexachloro-1,3-Butadiene 0.5 < 0.05 Benzene 0.5 < 0.1 Hexachloroethane 3.0 < 0.05 Cadmium 1.0 < 0.5 Lead 5.0 < 1.0 Carbon Tetrachloride 0.5 < 0.1 Lindane 0.4 < 0.005 Chlordane 0.03 < 0.005 Mercury 0.2 < 0.02 Chlorobenzene 100.0 < 0.1 Methoxychlor 10.0 < 0.1 Chloroform 6.0 < 0.1 Methyl Ethyl Ketone 200.0 < 2.0 Chromium 5.0 < 1.0 Nitrobenzene 2.0 < 0.05 m-Cresol 200.0 < 0.5 Pentachlorophenol 100.0 < 0.5 o-Cresol 200.0 < 0.5 Pyridine 5.0 < 0.05 p-Cresol 200.0 < 0.5 Selenium 1.0 < 0.5 Cresol 200.0 < 0.5 Silver 5.0 < 1.0 2,4-D 10.0 < 1.0 Tetrachloroethylene 0.7 < 0.1 1,4-Dichlorobenzene 7.5 < 0.05 Toxaphene 0.5 < 0.1 1,2-Dichloroethane 0.5 < 0.1 Trichloroethylene 0.5 < 0.1 1,1-Dichloroethylene 0.7 < 0.1 2,4,5-Trichlorophenol 400.0 < 0.5 2,4-Dinitrotoluene 0.13 < 0.05 2,4,6-Trichlorophenol 2.0 < 0.5 Endrin 0.02 < 0.005 2,4,5-TP (Silvex) 1.0 < 1.0 Heptachlor and its Hydroxide 0.008 < 0.005 Vinyl Chloride 0.2 < 0.2 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Meritech, Inc. and Date of analysis: Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <0.829 Cadmium 85 39 0.307 Copper 4,300 1,500 124 Lead 840 300 16.3 Mercury 57 17 0.041 Molybdenum 75 n/a 2.13 Nickel 420 420 10.4 Selenium 100 100 <0.829 Zinc 7,500 2,800 510 b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mglkg) Chromium (mg/kg) Nickel (mg/kg) > 0 but < 25 30 200 210 0 > 25 but < 50 34 220 240 > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 d > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: a %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Meritech, Inc. and Date of analysis: _ Parameter Result (mg1kP) Aluminum 3,550 Ammonia -Nitrogen 3,850 Calcium 7,060 Magnesium 752 Nitrate -Nitrite Nitrogen 20.7 pH (Standard Unit) 5.4 Phosphorus 15,700 Potassium 561 Sodium 348 Total Kjeldahl Nitrogen 5,040 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): - [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This rate is a (check one): M default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: ii e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (m91k9) (mg/kg) Surface 2,184 2,689 Injection/Incorporation 4,109 4,273 6. Other Pollutants Determination: SpecifX whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: None 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, 4 heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, or I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item Il. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. 0 Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. 1 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. NGMAN FIELD LOADING ESTIMATES Facility Hominy Creek WWTP Sampling Date 7/17/2019 Solids 60.3 Mineralization Rate 0.20 Wet Tons per DT 1.66 PH 5.4 Sodium Absorpotion 0.81 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 5,040 lbs./WT 6.08 Ammonia Nitrogen (mg/Kg) 3,850.00 lbs./WT 4.64 Nitrate -Nitrite (mg/Kg) 20.70 lbs./WT 0.02 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 2,184 lbs./WT 2.63 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 4,109 lbs./WT 4.96 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./WT 0.68 Phosphorus lbs./WT 18.93 Calcium lbs./WT 8.51 Magnesium lbs./WT 0.91 Manganese lbs./WT 0.57 Sulfur lbs./WT 20.02 Molybdenum lbs./WT 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 0.83 Cadmium (mg/Kg) 0.31 Copper (mg/Kg) 124.00 Lead (mg/Kg) 16.30 Mercury (mg/Kg) 0.04 Nickel (mg/Kg) 10.40 Selenium (mg/Kg) 0.83 Zinc (mg/Kg) 510.00 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) 5,040 2,184 4.37 2,856 5,040 4,109 8.22 931 2,856 286 0.57 2,571 931 93 0.19 838 2,571 129 0.26 2,442 838 42 0.08 796 2,442 61 0.12 2,381 796 20 0.04 776 2,381 30 0.06 2,351 776 10 0.02 767 Arsenic lbs./WT 0.00 Cadmium lbs./WT 0.00 Copper lbs./WT 0.15 Lead lbs./WT 0.02 Mercury lbs./WT 0.00 Nickel lbs./WT 0.00 Selenium lbs./WT 0.00 Zinc lbs./WT 0.11 Equations 1st Yr. PAN (mg/I g)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Total 2,689 5.38 Total 4,273 8.55 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Contact: Andrew Mlot Report Date: 8/1/2019 Client: City of Wilson NPDES #: NC0023906 3100 Old Stantonsburg Rd Project: Hominy Creek Class B Sludge Wilson, NC 27893 Date Sample Rcvd: 7/17/2019 Meritech Work Order # 071719109 Sample: Hominy Creek Class B (A-181-1) Grab 7/17/19 Parameters Results Analysis Date Reoortine Limit Method %Total Solids 66.3 % 7/19/19 0-100 % SM 2540B Fecal Coliform (Sludge) 2,331 col/g dry wt 7/17/19 134 col/g dry wt SM 9222D Meritech Work Order # 071719110 Sample: Hominy Creels Class B (A-181-2) Grab 7/17/19 Parameters Results Analysis Date Reporting Limit Method %Total Solids 66.5 % 7/19/19 0-100 % SM 2540B Fecal Coliform (Sludge) 19,549 col/g drywt 7/17/19 134 col/g dry wt SM 9222D Meritech Work Order # 071719111 Sample: Hominy Creek Class B (A-181-3) Grab 7/17/19 Parameters Results Analysis Date Reporting Limit Method %Total Solids 49.9 % 7/19/19 0-100 % SM 2540B Fecal Coliform (Sludge) 1,640 col/g dry wt 7/17/19 134 col/g dry wt SM 9222D Meritech Work Order # 071719112 Sample: Hominy Creek Class B (A-181-4) Grab 7/17/19 Parameters Results Analysis Date Reporting Limit Method %Total Solids 68.0 % 7/19/19 0-100 % SM 2540B Fecal Coliform (Sludge) 55,882 col/g dry wt 7/17/19 134 col/g dry wt SM 9222D Meritech Work Order # 071719113 Sample: Hominy Creek Class B (A-181-5) Grab 7/17/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 47.2 % 7/19/19 0-100 % SM 2540B Fecal Coliform (Sludge) 190,678 cal/g dry wt 7/17/19 134 cal/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Page 2 Contact: Andrew Mlot Report Date: 8/1/2019 Client: City of Wilson NPDES #: NC0023906 3100 Old Stantonsburg Rd Project: Hominy Creek Class B Sludge Wilson, NC 27893 Date Sample Rcvd: 7/17/2019 Meritech Worlc Order # 071719114 Sample: Hominy Creels Class B (A-181-6) Grab 5/16/19 Parameters Results Analysis Date Reporting Limit Method %Total Solids 52A % 7/19/19 0-100 % SM 2540B Fecal Coliform (Sludge) 178,503 col/g dry wt 7/17/19 134 col/g dry wt SM 9222D Meritech Work Order # 071719115 Sample: Hominy Creek Class B (A-181-7) Grab 7/17/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 64.1 % 7/19/19 0-100 % SM 2540B Fecal Coliform (Sludge) 24,961 col/g dry wt 7/17/19 134 col/g dry wt SM 9222D Meritech Work Order # 071719116 Sample: Hominy Creek Class B (A-182) Grab 7/17/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 60.3 % 7/19/19 0-100 % SM 2540B Ammonia, Nitrogen 3,850 mg/kg 7/23/19 0.1 mg/kg EPA 350A TKN 5,040 mg/kg 7/23/19 0.20 mg/kg EPA 351.1 Nitrate, Nitrogen 20.7 mg/kg 7/19/19 27.2 mg/kg EPA 353.2 Aluminum, total 3,550 mg/kg 7/19/19 0.050 mg/kg EPA 2003 Arsenic, total <0.829 mg/kg 7/19/19 0.829 mg/kg EPA 2003 Cadmium, total 0.307 mg/kg 7/19/19 0.272 mg/kg EPA 2003 Calcium, total 7,060 mg/kg 7/19/19 0.100 mg/kg EPA 2003 Chromium, total 12.4 mg/kg 7/19/19 0.005 mg/kg EPA 200.7 Copper, total 124 mg/kg 7/19/19 0.002 mg/kg EPA 2003 Iron, total 121,200 mg/kg 7/31/19 0.025 mg/kg EPA 200.7 Lead, total 16.3 mg/kg 7/19/19 0.010 mg/kg EPA 2003 Magnesium, total 752 mg/kg 7/19/19 0.005 mg/kg EPA 2003 Manganese, total 474 mg/kg 7/19/19 0.005 mg/kg EPA 2003 Mercury, total 0.041 mg/kg 7/23/19 0.0002 mg/kg EPA 245A Molybdenum, total 2.13 mg/kg 7/19/19 0.679 mg/kg EPA 200.7 Nickel, total 10.4 mg/kg 7/19/19 0.010 mg/kg EPA 2003 Phosphorus, total 15,700 mg/kg 7/19/19 0.020 mg/kg EPA 2003 Potassium, total 561 mg/kg 7/19/19 1.00 mg/kg EPA 2003 Selenium, total <0.829 mg/kg 7/19/19 0.829 mg/kg EPA 2003 Sodium, total 348 mg/kg 7/19/19 0.100 mg/kg EPA 2003 Sulfur, total* 16,600 mg/kg 7/31/19 0.1 mg/kg EPA 200.7 Zinc, total 510 mg/kg 7/19/19 0.010 mg/kg EPA 2003 pH 5.4 S.U. 7/19/19 1.0 - 14.0 S.U. SM 4500-HB * Results not for regulatory purposes I hereby certify that I have reviewed and approve these data. �I I ►Q� 0(1� Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)3424522 a m bq 'o d = O O a a d O n u c m o 0 = J E r F'�•• .) C Y a c O' nx y E u m m 0 O v Y ro F , U 3 O 3 -• M � � ? 1? � w •• y o c m t Q 'c Q ❑ v o c S^� cr c N - E m❑ C u �A\ vl a m m V Oj I.,fn LL j N E E i+ lL lY Ll LL Ll Il t N co q$ o2S o2f oZ$ oif of = - a o a c Y`+� c c u E =_ °' O K c H H vi +n H H 'n u O m O c "O C ❑. pp VI N N V7 N Vl VI N m a � O p a � m m m m '� � "3 w N •3 0 a3i � Y � y v°'i 0 U 3N 0 1 ~ 9 H c V o- U m s Q \ \ \' \ N i 0 z o a 3— o\° o\' o\° a° v''i E t O c .. N Q •� l.J ~ to ❑ "'i r F ,(� U Q Q uLD Z o v" E EN E H E a a v � c • W _ Z Oco H m m o � _ Gl ^ f6 OU > O o v to 'O CL v a v o W £ z u r. �'- 0� � W O � N N v �O � o O } U m z 3 � N W Qi � ❑ N Wc-1 rl ail ci ei ci M N > o a •,� �� c a a a a a a v � � m __ V c m m m m m m m U s z rc •y, U U U U U U U Y 2, J W N U U U U U U U T 0 V) p v C a a t 'SE; C LL= E E E E E E E E o t c N❑❑ 2 2 2 2 2 2 M G ❑' ❑ lF4 Waypoint ANALYTICAL 02/12/2018 14:50:18 Export Batch Report Export Batch Id : 1995EXP To: and e an Testing. TOO-, 1350 Hone Ave. Akron, OH 44310 330-634-9906 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 W rn+W. W aypolnta na lydca l.com Page 1 of 1 Created, 2/12/2018 14:S0:04 Computer: RVADESK001 User: Morgan Tichacek From: Waypoint Analytical Virginia, Inc. 7621 Whitepine Rd. Richmond, VA 23237 804-743-9401 Report No Sample Date Rush Lab No Method No Fee Code Description 18-043-0205 02/08/2018 11:18 58572 ASTM D93-80 Ignitability/Flashpoint (ASTM D93-80) 18-043-0205 02/08/2018 11:18 58572 SW-7.3.3 Cyanide Reactivity 18-043-0205 02/08/2018 11:18 58572 SW-7.3.4 Sulfide Reactivity 18-043-0205 02/08/2018 11:18 58572 SW-9045C Corrosivity (pH) 18-043-0205 02/08/2018 11:18 58573 SW-1311 TCLP Extraction Method 1311 18-043-0205 02/08/2018 11:18 58573 SW-1311 (ZHE) TCLP Extraction Method 1311 18-043-0205 02/08/2018 11:18 58573 SW-6010C (TCLP) TCLP Metals (8 RCRA Metals) 18-043-0205 02/08/2018 11:18 58573 SW-7470A (TCLP) TCLP Metals (8 RCRA Metals) 18-043-0205 02/08/2018 11:18 58573 SW-8081A (TCLP) TCLP Pesticides (Pest) 18-043-0205 02/08/2018 11:18 58573 SW-8151A (TCLP) TCLP Herbicides (Herbs) 18-043-0205 02/08/2018 11:18 58573 SW-8260B (TCLP) TCLP VOCs (Volatiles) 18-043-0205 02/08/2018 11:18 58573 SW-8270C (TCLP) LCLP SVOCs(BNAs) 18-043-0206 02/08/2018 12:23 58574 ASTM D913-80 Ignitability/Flashpoint (ASTM D93-80) 18-043-0206 02/08/2018 12:23 58574 SW-7.3.3'l Cyanide Reactivity 18-043-0206 02/08/2018 12:23 58574 SW-7.3.4 Sulfide Reactivity 18-043-0206 02/08/2018 12:23 58574 SW-9045r Corrosivity (pH) 18-043-0206 02/08/2018 12:23 58575 SW-1311 TCLP Extraction Method 1311 18-043-0206 02/08/2018 12:23 58575 SW-1311I (ZHE) TCLP Extraction Method 1311 18-043-0206 02/08/2018 12:23 58575 SW-6010C (TCLP) TCLP Metals (8 RCRA Metals) 18-043-0206 02/08/2018 12:23 58575 SW-7470A (TCLP) TCLP Metals (8 RCRA Metals) 18-0,13-0206 02/08/2018 12:23 58575 SW-8081A (TCLP) TCLP Pesticides (Pest) 18-043-0206 02/08/2018 12:23 58575 SW-8151A (TCLP) TCLP Herbicides (Herbs) 18-043-0206 02/08/2018 12:23 58575 SW-8260B (TCLP) TCLP VOCs (Volatiles) 18-043-0206 02/08/2018 12:23 58575 SW-8270C(TCLP) TCLP SVOCs(BNAs) Sampled By Method of Shipment Blank / Cooler Temp. y / iX r ( C Remarks ReI wished By (sign) ' Date / Time / Q n Received By (sign) Date / Time Relinquished By (sig Date / Time Reseiv�d y (sign) Date /Time r V B Waypoint- ANALYTICAL 02/08/2018 14:17:20 Export Batch Report Export Batch Id : 1987EXP To: I American Testing Technologies �1350 Hone Ave. Akron, CH 44310 330-634-9906 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypoi nta n a lytica l.com Page 1 of 1 Created: 2/8/2018 14:16:56 Computer: RVADESK001 User: Morgan Tichacek From: Waypoint Analytical Virginia, Inc. 7621 Whitepine Rd. Richmond, VA 23237 804-743-9401 Report No Sample Date Rush Lab No Method No Fee Code Description 18-039-0203 02/07/2018 11:57 58513 ASTM D93-80 Ignitability/Flashpoint (ASTM D93-80) 18-039-0203 02/07/2018 11:57 58513 SW-7.3.3 Cyanide Reactivity 18-039-0203 02/07/2018 11:57 58513 SW-7.3.4 Sulfide Reactivity 18-039-0203 02/07/2018 11:57 58513 SW-9045C Corrosivity (pH) 18-039-0203 02/07/2018 11:57 58514 SW-1311 TCLP Extraction Method 1311 18-039-0203 02/07/2018 11:57 58514 SW-1311 (ZHE) TCLP Extraction Method 1311 18-039-0203 02/07/2018 11:57 58514 SW-6010C (TCLP) TCLP Metals (8 RCRA Metals) 18-039-0203 02/07/2018 11:57 58514 SW-7470A (TCLP) TCLP Metals (8 RCRA Metals) 18-039-0203 02/07/2018 11:57 58514 SW-8081A (TCLP) TCLP Pesticides (Pest) 18-039-0203 02/07/2018 11:57 58514 SW-8151A (TCLP) TCLP Herbicides (Herbs) 18-039-0203 02/07/2018 11:57 58514 SW-8260B (TCLP) TCLP 'VOCs (Volatiles) 18-039-0203 02/07/2018.11:S7 58514 SW-8270C (TCLP) TCLP SVOCs (BNAs) Sampled By Method of Shipment Blank / Cooler Temp. t C Remarks Relinquished By (sign) TimeEReceiv (sign) Date / Timei Z ' l�f�®;3t HTime Re mquished By (s n) sign) Dpte / Ti 0 i (31 t3'_c % 02/28/2018 American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Report No.: 021318-02 04 Enclosed are the results of the sample(s) submitted to our laboratory on 02/13/2018. All analyses were performed according to our laboratory's quality assurance program. All sample results are reported on an "as -received" wet basis unless otherwise noted. The test results meet requirements of the NELAP standards for methods listed on the laboratory's current fields of accreditation (EPA 8260, 8082, 8081, 8151, 8270, 6010, 6020, 1010, 9045, 7471, 1010, 1311, 150.1, 200.7, 200.8, and 245.1) except as noted. Results apply only to the items submitted to the laboratory for analysis. Pursuant to NELAP, this report may not be reproduced except in full, and with written approval from the laboratory. If you have any questions please contact the laboratory manager at 330-634-9906 or via email at samy@atnericantestinptechnolo2ies.com nager ATT is NELAP-accredited by the State of Florida, #E871084. Other state accreditations include: North Carolina, #670; Pennsylvania #68-05167; West Virginia, #372. The results relate only to the items tested. ATT shall have no liability to the client or client's customer with respect to decisions or recommendations made, actions taken or courses of conduct implemented by either the client or the client's customer as a result of or based upon the Test Results. In no event shall ATT's liability with respect to the Test Results exceed the amount paid to ATT by the client therefor. 1350 Home Avenue Akron, OH 44310 Page 1 of 19 Toll Free: 877.634 9906 Phone: (330) 6349906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.com %W American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 11:18 Client ID #: 58573 Laboratory ID #: 021318-02 Date of Analysis: 02/15/2018 Certificate of Analysis Metals-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010C Barium <10 mg/L 100.0 6010C Cadmium <0.5 mg/L 1.0 6010C Chromium <1.0 mg/L 5.0 6010C Lead <1.0 mg/L 5.0 6010C Mercury <0.02 mg/L 0.2 7470A Selenium <0.5 mg/L 1.0 6010C Silver <1.0 mg/L 5.0 6010C reviewed by: 1350 Home Avenue Akron, OH 44310 Page 2 of 19 ToJI Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website:www.AmericanTes>tingTechnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 11:18 Client ID #: 58573 Laboratory ID #: 021318-02 Date of Analysis: 02/16/2018 Certificate of Analysis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260B Carbon tetrachloride <0.1 mg/L 0.5 8260B Chlorobenzene <0.1 mg/L 100 8260B Chloroform <0.1 mg/L 6.0 8260B 1,2-Dichloroethane <0.1 mg/L 0.5 8260B 1,1-Dichloroethene <0.1 mg/L 0.7 8260B Methyl ethyl ketone <2.0 mg/L 200 8260B Tetrachloroethene <0.1 mg/L 0.7 8260B Trichloroethene <0.1 mg/L 0.5 8260B Vinyl chloride <0.2 mg/L 0.2 8260B 1350 Home Avenue Akron, OH 44310 Page 3 of 19 Tall Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.corm American Testing Technologies, Inc. WayPoint Analytical 7621 Wbitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 11:18 Client ID #: 58573 Laboratory ID #: 021318-02 Date of Analysis: 02/17/2018 Certificate of Analvsis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 24-Dinitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 mg/L 0.13 8270C Hexachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C Page 4 of 19 1350 Home Avenue Akron, OH 44310 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.com s American Testing Technologies, Inc. WayPomt Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 11:18 Client ID #: 58573 Laboratory ID #: 021318-02 Date of Analysis: 02/17/2018 Certificate of Analysis Pesticides-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081B Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 8081B Heptachlor epoxide <0.005 mg/L 0.008 8081B Lindane <0.005 mg/L 0.4 8081B Methoxychlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0.5 8081B 1350 Home Avenue Akron, 0H 44310 Page 5 of 19 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 WVebsite: www.AmericariTestindTechnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 11:18 Client ID #: 58573 Laboratory ID #: 021318-02 Date of Analysis: 02/27/2018 Certificate of Analysis Herbicides-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A 1350 Home Avenue Akron, OH 44310 Page 6of19 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.com WayPoint Analytical 7621Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 11:18 Client ID #: 58572 Laboratory ID #: 021318-02 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Units Method Date of Number Analysis Reactive Cyanides <0.5 mg/kg 7.3.3.2 02/23/2018 Reactive Sulfides <25 mg/kg 7.3.4.1 02/23/2018 pH (Lab) 3.29 S.U. 9045D . 02/13/2018 Flash point >140 °F 1010A 02/16/2018 1350 Home Avenue Akron, OH 44310 Page 7 of 19 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 12:23 Client ID #: 58575 Laboratory ID #: 021318-03 Date of Analysis: 02/15/2018 Certificate of Analysis Metals-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010C Barium <10 mg/L 100.0 6010C Cadmium <0.5 mg/L 1.0 6010C Chromium <1.0 mg/L 5.0 6010C Lead <1.0 mg/L 5.0 6010C Mercury <0.02 mg/L 0.2 7470A Selenium <0.5 mg/L 1.0 6010C Silver <1.0 mg/L 5.0 6010C 1350 Home Avenue Akron, OH 44310 Page 8 of 19 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologes.com Ing American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 12:23 Client ID #: 58575 Laboratory ID #: 021318-03 Date of Analysis: 02/16/2018 Certificate of Analvsis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260B Carbon tetrachloride <0.1 mg/L 0.5 8260B Chlorobenzene <0.1 mg/L 100 8260B Chloroform <0.1 mg/L 6.0 8260B 1,2-Dicbloroethane <0.1 mg/L 0.5 8260B 1,1-Dichloroethene <0.1 mg/L 0.7 8260B Methyl ethyl ketone <2.0 mg/L 200 8260B Tetrachloroethene <0.1 mg/L 0.7 8260B Trichloroethene <0.1 mg/L 0.5 8260B Vinyl chloride <0.2 mg/L 0.2 8260B reviewed by: Manager 1350 home Avenue Akron, OH 44310 Page 9 of 19 Tall Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingfechnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 12:23 Client ID #: 58575 Laboratory ID #: 021318-03 Date of Analysis: 02/17/2018 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 mg/L 0.13 8270C Hexachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C 1350 Home Avenue Akron, OH 44310 Page 10 of 19 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 4Vebsite: wmv.AmericanTestingTechnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 12:23 Client ID #: 58575 Laboratory ID #: 021318-03 Date of Analysis: 02/17/2018 Certificate of Analvsis Pesticides-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081B Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 8081B Heptachlor epoxide <0.005 mg/L 0.008 8081E Lindane <0.005 mg/L 0.4 8081B Methoxychlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0.5 8081B Toll Free: 877-634-9906 1350komeAvenue Akron. OH 44310 Page 11 of 19 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 12:23 Client ID #: 58575 Laboratory ID #: 021318-03 Date of Analysis: 02/27/2018 Certificate of Analvsis Herbicides-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A 1350 Home Avenue Akron, OH 44310 Page 12 of 19 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.com WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 12:23 Client ID #: 58574 Laboratory ID #: 021318-03 a WASW American Testing Technologies, Inc. Certificate of Analvsis Parameter Results Units Method Number Reactive Cyanides <0.5 mg/kg 7.3.3.2 Reactive Sulfides <25 mg/kg 7.3.4.1 pH (Lab) 3.68 S.U. 9045D Flash point >140 °F 1010A Date of Analvsis 02/23/2018 02/23/2018 02/13/2018 02/16/2018 Page 13 of 19 1350 Horne Avenaae Akron, 0H 44310 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 12:23 Client ID #: 58575 Laboratory ID #: 021318-03 Date of Analysis: 02/15/2018 Certificate of Analysis Metals-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010C Barium <10 mg/L 100.0 6010C Cadmium <0.5 mg/L 1.0 6010C Chromium <1.0 mg/L 5.0 6010C Lead <1.0 mg/L 5.0 6010C Mercury <0.02 mg/L 0.2 7470A Selenium <0.5 mg/L 1.0 6010C Silver <1.0 mg/L 5.0 6010C 1350 Home Avenue Akron, OH 44310 Page 14 of 19 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericarTestin,- echnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/07/2018 Time Collected: 11:57 Client ID #: 58514 Laboratory ID #: 021318-04 Date of Analysis: 02/16/2018 Certificate of Analysis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260B Carbon tetrachloride <0.1 mg/L 0.5 8260B Chlorobenzene <0.1 mg/L 100 8260B Chloroform <0.1 mg/L 6.0 8260B 1,2-Dichloroethane <0.1 mg/L 0.5 8260B 1,1-Dichloroethene <0.1 mg/L 0.7 8260B Methyl ethyl ketone <2.0 mg/L 200 8260B Tetrachloroethene <0.1 mg/L 0.7 8260B Trichloroethene <0.1 mg/L 0.5 8260B Vinyl chloride <0.2 mg/L 0.2 8260B Page 15 of 19 1350 Home Avenue Akron. OH 44310 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.com Amerls n Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/07/2018 Time Collected: 11:57 Client ID #: 58514 Laboratory ID #: 021318-04 Date of Analysis: 02/17/2018 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4-Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 mg/L 0.13 8270C Hexachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o-Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5-Trichlorophenol <0.5 mg/L 400 8270C 2,4,6-Trichlorophenol <0.5 mg/L 2.0 8270C 1350 Home Avencae Akron, OH 44310 Page 16 of 19 Tall Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: ww v.AmericanTestingTechnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/07/2018 Time Collected: 11:57 Client ID #: 58514 Laboratory ID #: 021318-04 Date of Analysis: 02/17/2018 Certiff'icate of Analysis Pesticides-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081B Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 8081B Heptacblor epoxide <0.005 mg/L 0.008 8081B Lmdane <0.005 mg/L 0.4 8081B Methoxychlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0:5 8081B 1350 Home Avenue Akron, 0H 44310 Page 17 of 19 Toll Free; 877-634-9906 Phone: (330) 634-9906 Fax (330) 634-9907 Website: wv✓w.AmericanTestingTechnologies.com s American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/07/2018 Time Collected: 11:57 Client ID #: 58514 Laboratory ID #: 021318-04 Date of Analysis: 02/27/2018 Certificate of Analvsis Herbicides-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A reviewed by: Manager 1350 Hame Avenue Akron,OH 44310 Page 18 of 19 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 4vebsite: www.AmericanTestingTechnologies.com WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/07/2018 Time Collected: 11:57 Client ID #: 58513 Laboratory ID #: 021318-04 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Unfits Method Date of Number Analvsis Reactive Cyanides <0.5 mg/kg 7.3.3.2 02/23/2018 Reactive Sulfides <25 mg/kg 7.3.4.1 02/23/2018 pH (Lab) 6.80 S.U. 9045D 02/13/2018 Flash point >140 °F 1010A 02/16/2018 Toll Free: 877-634-9906 1380 Home Avenue Akron, OH 44310 Page 19of19 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.ArnericarTestingTechnologies.com Waypointo ANALYTICAL 02/08/2018 14:17:11 Export Batch Report Export Batch Id : 1987EXP To: American Testing Technologies 1350 Hone Ave. Akron, OH 44310 330-634-9906 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Page 1 of 1 Created: 2/8/2018 14:16: 56 Computer: RVADESK001 User: Morgan Tichacek From: Waypoint Analytical Virginia, Inc. 7621 Whitepine Rd. Richmond, VA 23237 804-743-9401 Report No Sample Date Rush Lab No Method No Fee Code Description 18-039-0203 02/07/2018 11:57 58513 ASTM D93-80 Ignitability/Flashpoint (ASTM D93-80) 18-039-0203 02/07/2018 11:57 58513 SW-7.3.3 Cyanide Reactivity 18-039-0203 02/07/2018 11:57 58513 SW-7.3.4 Sulfide Reactivity 18-039-0203 02/07/2018 11:57 58513 SW-9045C Corrosivity (pH) 18-039-0203 02/07/2018 11:57 58514 SW-1311 TCLP Extraction Method 1311 18-039-0203 02/07/2018 11:57 58514 SW-1311 (ZHE) TCLP Extraction Method 1311 18-039-0203 02/07/2018 11:57 58514 SW-6010C (TCLP) TCLP Metals (8 RCRA Metals) 18-039-0203 02/07/2018 11:57 58514 SW-7470A (TCLP) TCLP Metals (8 RCRA Metals) 18-039-0203 02/07/2018 11:57 58514 SW-8081A (TCLP) TCLP Pesticides (Pest) 18-039-0203 02/07/2018 11:57 58514 SW-8151A (TCLP) TCLP Herbicides (Herbs) 18-039-0203 02/07/2018 11:57 58514 SW-8260B (TCLP) TCLP VOCs (Volatiles) 18-039-0203 02/07/2018 11:57 58514 SW-8270C (TCLP) TCLP SVOCs (BNAs) Sampled By I Method of Shipment I Blank / Cooler Temp. Remarks Relinquished By (sign) Date / Time Received By (sign) Date / Time Relinquished By (sign) Date / Time Received By (sign) Date / Time M C O E T a U O V r C O as O O tp N O �ON r W TO p t C _ LL � � t r r ,c —sue ~ � c e o _ Q w v t- O Z r+ � v � U y N M (0 N N O Q > Y X M Q LL U X w ,n U O N F- U =a X c aLi O a) O 3 C) X ) z `n U)- J Ln NW X � o m E N X o U) o w c O c _ J >N X O N > .0 ..+ N C .l N C T a o 0 I `' a O O I I I� I� v Y�F coo 0 p U N U U) N U N U ` c a) m@ Jl m 0 u) inn T ca N N R r� 4 T C� a C5 a 0 a CD a N � � _ o C OE ` `C) -C (a O p Lq _ d N z o Qr, 3 E F- N 1 tJ c — c y o O f0 E U a3 ,7 0 is C C Q o m �1 — a N N 00- J m a -0a cu E -E 0m E aE ns �E IT (7 U U C� U O n`. ` T :3 Z .n -0 Q'o mco J J � Z JL T m (D 3 N u (n J N �9 O C U C C IV C: iu m LL m 0 U a a O U °0' a0i E c m 0 m cci co m E E m � � C Y U cn E Z N �0 O Q m c O J O _ m - E ( 0 Z 2 E aci u O L o fl C m m a o to 0 o, O N Z a) c' aci a� m N o c Y Z E U co t E � m �_ ' L) E o o E Y F, co N U U Q c U) H = J n1 E m m Y N a U a) U O U H � c 3 _ � to a� V/ C mil_ p (D Q 61 d U) a1 � 0 N f6 o i0- m CY CV � p Ul oLO Z PLL PROMPT•ACCURATE-RELIABLE LABORATORIES, INC W W W.PARLABS.COM REPORT OF ANALYSES Attn: ANDREW MLOT CITY OF WILSON PO BOX 10 WILSON, NC 27894-0010 PROJECT NAME: JUL 19 DATE: 08/27/19 SAMPLE NUMBER- 136439 SAMPLE ID- HOMINY CREEK A-169 SAMPLE MATRIX- SO DATE SAMPLED- 07/09/19 TIME SAMPLED- 0754 DATE RECEIVED- 07/10/19 SAMPLER- NH RECEIVED BY- DJ TIME RECEIVED- 0930 DELIVERED BY- FEDEX TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS 40 DAY BENCHTOP DIGESTION EPA625R 07/10/19 1315 RE 5.25 LABORATORY DIRECTOR f 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 R. I-AHORA7'ORKES, INC 40 Day Bench Scale Extended Aeration Test for Anearobically Digested Solids Percent Volatile Solids Reduction pay 0 - Start of Test Empty Dish 24.2891 19.2a31 212200 21,9416 2230at 21 A064 B Initial Sam Wl • EmptyDVeh W[ 78.8772 29-5293 31.WaB 35.5956 339719 33.9630 c Dried $ern 9Yt+Em Dch V. 296006 23,0230 251614 27.0018 26.5339 26.2641 D Ashed &anad Sam a lrlt • Dish V9t 25.8819 20.9560 22 9*4 24.2253 24.2072 23,8134 L • A U d 5 e Wt 14.5981 10.2462 10.5208 13.0540 11.60R 12-t546 $ • C-A Dried Siud a 4Vt 5.3115 3.7399 39444 5, 0802 4.2258 4.4558 V C-D Vdatde s(Ads WI 2.9187 2.0570 2,1650 2.T765 2.3267 2A508 F= D-A Fored Solid. WE 2-3928 1,6729 1.7764 2.2837 1.6981 2.0050 V%. fS'100 PercenlVdetMe Solids % 54.951 55.269 54.930 54.869 55,059 65.0156 !L Mass Fraction of Yolatila 8o4ds m L uid (Feed Sludge at Stan d Test 0.2000740 0.2017333 0.2038453 0.2033470 0.1994864 0 2017 = FfL Mass Fraction of Fixed 9o5da Feed Slud a[ Sled o1 Teat 0.1$40241 0.1832703 0.1672567 0.1672550 0.1... 0.1649 Day 20 - Mil -Pant of Tnt (« Ch.crll nA A tea. Em Dish 24206 - ---19 2e48 21.220E 21.9436 22.3088 21.608 B Initial Sam M Empty Dish M 338125 290575 32.0557 34.0211 32.7215 32.3397 C Dried Sam Wt • Em U'sh 9y1 277443 22.6960 252144 26.4326 260949 25.6755 D ABW Burned Sem Y4k * D®h Yet 25.8704 20.9276 230514 24.0454 2t 0470 23.5902 L • &A uqw swgeWl 9.5217 9.8029 10.8351 12.0775 10.4127 10.5300 $ • c-A Dried WI 3.4535 36114 3.9938 4.4992 37861 3.8668 V •IC-D) Voletie Solids fA'1 1 A649 1,9682 2.1630 2.3874 2-0479 2.0863 F • p-A Fixed Soli Wit 1.5886 1.6432 1.8308 2.1010 17382 1.7B05 V%. f5).too Parcem Volatile solids % 54, 54,500 54.159 53.181 54.090 5339880 20 V% < 0 QC Check.f Ana . 1.20 de V%"s then 0 di V%7 Yee Yee yes Yes Yea Day 40 - End o1 Test Av M. WI -21.5187 227077 21.0370 19,3M 21.a72d 21268t B Initial Sam M I Em Dish W[ 3a.0450 33,0201 32,154a 30 7490 37.2156 32.7989 c Drted Sam yyt+Ern Drh Wr 24.6334 208304 25.0753 23.5187 27 l58a 25.5033 p Burned Sem AWt Dkh WI 229916 24.6730 229586 213322 24.5653 23.3054 L • B-Ad Md S lNl 6.5263 11.1124 tt1278 11.4440 15.3438 11.5108 5 • GA Doled S VJt 3.1147 4,1227 4,0383 4.2137 5 Sass 4.2152 V • ClJ Volatile Soids Wt 1.6356 2.1574 2.1165 2.1865 29933 2.1979 F- (D-All Fixed SaitdsM 1.4789 1,9653 1,9218 2.0272 2.6933 2.0173 Percent Volatiie Soids % 52.519 52.330 52-411 51 �e90 51790 52.1880 b = n Mass Fraction or Volaele scadsm u4(Bono-)SI al Endof Test 0.191B534 0.1941435 0.1901993 O.t9f0808 0,1885672 0.1972 = FIL Mass Fraction o}Fixed Solids in id BaBom e! End o1 Teat 0.1734516 0.1768565 0.372T028 0.17T1409 0.1755325 0.1751 40 < 0 QC Check ar Ane7 .. N 40 d. V%lesa then 0 de V%1 Yee Yee Yee Yes Yee VSR Smb) = See Belay Fractional Volatile Solids Reduction (Mass Balance Method) 3.93% 2.84% 7.90% 6 40% 5.20% Average FVSR (mb) of all vaild replicate results 5.25% Is Average FVSR (mb) less than or equal to 17%? YES - Sample Passes Requirement 'Calculation: FVSR (mb) _ y = mass fraction of volatile solids in the liquid sludge x = mass fraction of fixed solids in the liquid sludge f = indicates feed sludge at start of the test to = indicates "bottoms" sludge at and of the test fy(fl " (1 - x(b))l - [y(b) ` ('E-x{f})l Ly(i ` ('I-x(b)-y(b))l P.O. 9oa 4114.1. (:h dl . NC M1-1-14e3 Ph- (7n4) W-9333. F.. (704) 5e&033.1 �f618f� CHAIN OF CUSTODY F A- RREI_iABLE Phone (704) 588-8333 Fax (704) 588-8335 LABORATORIES, INC Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Chartotte, NC 28273 Chartotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc- and the North Caroiina Depamnent of Environmental and Natural Resources. Company Na (billing) Comments/ Special Instructions Address Lo City, state zip code jau ,(1 c,2 -7b43 0 0 , r Point Con & ct Teiephone Number sy Sample Taken By: SIGNATURE � PRINTED NAME � ARE SAMPLES FOR STATE or fl PA REPORTING YES NO 'Sample Type: oW ww_ GWMW HW Soli other ° C Sample Temp upon receipt: ° C Sample Temp at time of sTaiMe *"Field Preserved: Yes LinerlZero Headspace: Yes No _ n/a _Teflon Residual Chlorine checkeof sampling (YIN): Dechlodnation Necessary (Y/N): Bent Sample I.D. Sample Location I Number) Comp Grab Preserv. Set Up Date rime Cofte ion Data(rme iyseb RequesW ` �10 ' C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Wel HW=Hazardous Waste 0 APPENDIX 9 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RS CA Perdue WWTP Field Loading Calculations Analytical DWR Division of Water ResoUKes State of North Carolina Department of Environment and Natural Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: - 2. Facility permit holder is: Federal, 0 State, 0 Local Government, or 0 Private. Facility permit issued by: ® Div. of Water Resources, Div. of Environmental Health, or ❑ Other (explain: �. 3. Facility contact person and title: K Mizzell Complete mailing address: 1539 Governors Rd City: Lewiston Woodville State: NC Zip: 27849- Telephone number: (252) 287-8839 E-mail address: Timothy.Mizelle(a&Perdue.com 4. Facility physical address: 3539 Governors R� City: Lewiston Woodville State: ` Zip: 27849- Coordinates: Latitude: 36' 8' 33.11" Longitude: 77° 13' 3.07" Datum: NAD 83 Level of accuracy: Sub -Meter Method of measurement: 5. Purpose of the facility: [] treatment of municipal wastewater, treatment of 100% domestic wastewater, Ej treatment of potable water, treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: 0 MGD and facility average daily flow: 2.36 MGD 8. Average amount of residuals being generated at this facility = dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Aeration 14 Md Type and volume of residuals storage (i.e., outside of residuals treatment units): 46 MG Anaerobic II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: Biological 0 Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 11-13 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: 41eritech, Inc. and Date of analysis: Passed corrosivity test: yes no. pH: 6.9 s_u. (2 < pH < 12.5) Passed ignitability test: yes no. Flashpoint: � OF (> 140°F) Passed reactivity test: Oyes Ono. HCN: _ mg/kg (<250) & H2S: mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (Mg/1) Result (Mg/1) Arsenic 5.0 <0.100 Hexachlorobenzene 0.13 <0.100 Barium 100.0 <0.050 Hexachloro-1,3-Butadiene 0.5 <0.100 Benzene 0.5 <0.0100 Hexachloroethane 3.0 <0.100 Cadmium 1.0 <0.020 Lead 5.0 <0.100 Carbon Tetrachloride 0.5 <0.0100 Lindane 0.4 <0.040 Chlordane 0.03 <0.003 Mercury 0.2 <0.02 Chlorobenzene 100.0 <0.0100 Methoxychlor 10.0 <1.000 Chloroform 6.0 <0.0100 Methyl Ethyl Ketone 200.0 <0.100 Chromium 5.0 <0.050 Nitrobenzene 2.0 <0.100 m-Cresol 200.0 <0.200 Pentachlorophenol 100.0 <0.500 o-Cresol 200.0 <0.100 Pyridine 5.0 <0.100 p-Cresol 200.0 <0.200 Selenium 1.0 <0.100 Cresol 200.0 <0.300 Silver 5.0 <0.050 2,4-D 10.0 <1.000 Tetrachloroethylene 0.7 <0.0100 1,4-Dichlorobenzene 7.5 <0.100 Toxaphene 0.5 <0.05 1,2-Dichloroethane 0.5 <0.0100 Trichloroethylene 0.5 <0.0100 1,1-Dichloroethylene 0.7 <0.0100 2,4,5-Trichlorophenol 400.0 <0.100 2,4-Dinitrotoluene 0.13 <0.100 2,4,6-Trichlorophenol 2.0 <0.100 Endrin 0.02 <0.002 2,4,5-TP (Silvex) 1.0 <0.100 Heptachlor and its Hydroxide 0.008 <0.0008 Vinyl Chloride 0.2 <0.0200 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: eritech and Date of analysis: _ Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <1.13 Cadmium 85 39 0.633 Copper 4,300 1,500 240 Lead 840 300 <1.13 Mercury 57 17 <0.023 Molybdenum 75 n/a 7.26 Nickel 420 420 13.9 Selenium 100 100 4.67 Zinc 7,500 2,800 596 b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) I > 0 but < 25 30 200 210 Ej > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 j > 100 but < 125 53 360 390 El > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: a %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Meritech, Inc. and Date of analysis: _ Parameter Result (mg1kP) Aluminum 54,200 Ammonia -Nitrogen 8,340 Calcium 26,800 Magnesium 3,360 Nitrate -Nitrite Nitrogen <227 pH (Standard Unit) 6.7 Phosphorus 49,000 Potassium 10,800 Sodium 14,100 Total Kjeldahl Nitrogen 51,500 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 152 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This rate is a (check one): M default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: ii e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (m91k9) (mg/kg) Surface 17,345 26,137 Injection/Incorporation 21,515 29,234 6. Other Pollutants Determination: SpecifX whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: None 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, 4 heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, or I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item Il. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. 0 Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. 1 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FIELD LOADING ESTIMATES Facility Perdue Farms - Lewiston Sampling Date 7/11/2019 % Solids 4.41 Mineralization Rate 0.30 Gallons per DT 5,437.83 pH 6.7 Sodium Absorpotion 4.52 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 51,500 lbs./1,000 gal 18.94 Ammonia Nitrogen (mg/Kg) 8,340.00 lbs./1,000 gal 3.07 Nitrate -Nitrite (mg/Kg) 227.00 lbs./1,000 gal 0.08 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 17,345 lbs./1,000 gal 6.38 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 21,515 lbs./1,000 gal 7.91 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 3.97 Phosphorus lbs./1,000 gal 18.02 Calcium lbs./1,000 gal 9.86 Magnesium lbs./1,000 gal 1.24 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 1.13 Arsenic lbs./1,000 gal 0.00 Cadmium (mg/Kg) 0.63 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 240.00 Copper lbs./1,000 gal 0.09 Lead (mg/Kg) 1.13 Lead lbs./1,000 gal 0.00 Mercury (mg/Kg) 0.02 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 13.90 Nickel lbs./1,000 gal 0.01 Selenium (mg/Kg) 4.67 Selenium lbs./1,000 gal 0.00 Zinc (mg/Kg) 596.00 Zinc lbs./1,000 gal 0.22 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) 51,500 17,345 34.69 34,155 51,500 21,515 43.03 29,985 34,155 5,123 10.25 29,032 29,985 4,498 9.00 25,487 29,032 2,177 4.35 26,854 25,487 1,912 3.82 23,576 26,854 1,007 2.01 25,847 23,576 884 1.77 22,692 25,847 485 0.97 25,363 22,692 425 0.85 22,266 Equations I st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Total 26,137 52.27 Total 29,234 58.47 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Date Report Date: Project: Sample Rcvd: 7/24/2019 Perdue Q3 7/11/2019 Meritech Work Order # 071119128 Sample: PD071119 Grab 7/11/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 4,41 % 7/12/19 0-100 % SM 2540B Ammonia, Nitrogen 8,340 mg/kg 7/16/19 10 mg/kg EPA 350A TKN 51,500 mg/kg 7/15/19 20 mg/kg EPA 351A Nitrate/Nitrite, Nitrogen <227 mg/kg 7/17/19 227 mg/kg EPA 353.2 Aluminum, total 54,200 mg/kg 7/23/19 2,50 mg/kg EPA 200.7 Arsenic, total <1.13 mg/Icg 7/17/19 1.13 mg/kg EPA 2003 Cadmium, total 0.633 mg/kg 7/17/19 0.20 mg/kg EPA 2003 Calcium, total 26,800 mg/kg 7/17/19 10.0 mg/kg EPA 200.7 Copper, total 240 mg/Icg 7/17/19 1.00 mg/kg EPA 2003 Lead, total <1.13 mg/kg 7/17/19 1.13 mg/kg EPA 2003 Magnesium, total 3,360 mg/kg 7/17/19 10.0 mg/kg EPA 2003 Mercury, total <0.023 mg/lcg 7/16/19 0.023 mg/kg EPA 245.1 Molybdenum, total 7.26 mg/kg 7/17/19 0.500 mg/kg EPA 2003 Nickel, total 13.9 mg/kg 7/17/19 2.0 mg/kg EPA 2003 Phosphorus, total 49,000 mg/kg 7/23/19 2.00 mg/kg EPA 2003 Potassium, total 10,800 mg/kg 7/17/19 20.0 mg/kg EPA 200.7 Selenium, total 4.67 mg/kg 7/17/19 0.50 mg/kg EPA 2003 Sodium, total 14,100 mg/kg 7/17/19 20.0 mg/kg EPA 2003 Zinc, total 596 mg/kg 7/17/19 0.500 mg/kg EPA 2003 PH 6.7 S.U. 7/12/19 1.0 - 14.0 S.U. SM 4500-HB 1 hereby certify that I have reviewed and approve these data � � (,�" ,� L- dboratoryRepresentative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 d � O p. U M M 4 m O) LON E o 1) co OMO CD'C3 j X. U Q z NUD Y fir. Cl) xk N' L- U a q o X m 'o O m z d LL w a` L: Rf E Mow � 4 n. E Z Q N N v 3 IE O io w ,m N Zo MMMMN � N W c c o Z m Y N x0 ? 'O C) �- CO a) O E Z m O 3 q d OX E U) G 2 �° o a M H ri O Y u Y hhh IMMMM v #i MW v a� MU m0 °c as U o m z U Q Q o Y C! m — O O EO W O\ N �Ni O N E a O ZO F m N U y m N `o U m m ..c T u u dD w E j w E v d� MW N v a Q W E ;� o 'm oMM z a, o E � - a 0 ��// 1.1. u W> W 41 o (co D °' D xx a .0 N h - V o c U O X 3 (U h a t _u fa A4 N ❑ r`f LJ'. Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Report Date: 2/12/2019 Project: Perdue 1st Quarter Date Sample Rcvd: 1/24/2019 Meritech Work Order # 01241979 Sample: P012419 Grab 1/24/2019 1311- TCLP Metals Parameter Results Analysis Date Det. Limit Reg. Limit Method Arsenic <0.100 mg/L 1/31/2019 0.100 5.0 EPA 200.7 Barium <0.050 mg/L 1/31/2019 0.050 100.0 EPA 2003 Cadmium <0.020 mg/L 1/31/2019 0.020 1.0 EPA 2003 Chromium <0.050 mg/L 1/31/2019 0.050 5.0 EPA 200.7 Lead <0.100 mg/L 1/31/2019 0.100 5.0 EPA 200.7 Mercury <0.02 mg/L 1/31/2019 0.02 0.2 EPA 245.1 Selenium <0.100 mg/L 1/31/2019 0.100 1.0 EPA 200.7 Silver <0.050 mg/L 1/31/2019 0.050 5.0 EPA 2003 TCLP Organics Parameter Results Analysis Date Reporting Limit Method Volatiles 8260 Attached 2/4/2019 8260 Semi Vol. 8270 Attached 2/8/2019 8270 Other Tests Parameter Results Analvsis Date Reporting Limit Method %Total Solids 4.05 % 1/31/2019 0-100 % SM 2540B Cyanide, total <0.500 mg/lcg 2/5/2019 0.500 mg/kg EPA 335.4 Sulfide 4.33 mg/kg 1/29/2019 10.0 mg/kg SW 846 9038 Ignitability >140 °F 2/1/2019 EPA 1030 Corrositivity (pH) 6.9 S.U. 1/31/2019 1.0 - 14.0 S.U. SM 4500 HB 642 Tamco Road, Reidsville, North Carolina 27320 te1.(336)342-4748 fax.(336)342-1522 Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 2 Report Date: 2/12/2019 Project: Perdue 1st Quarter Date Sample Rcvd: 1/24/2019 Meritech Work Order # 01241979 Sample: P012419 Grab 1/24/2019 1311 - TCLP Pesticides & Herbicides Pesticide - SW-846 8O81A Parameter Endrin Chlordane Toxaphene Methoxychlor Heptachlor Lindane Herbicides - SW-846 8151A Parameter 2,4-D 2,4,5-TP [Silvex) Results Anal�is Date Det. Limit Re�Limit Dilution Factor Attached Attached Attached Attached Attached Attached Results Attached Attached Analysis Date Det. Limit Reg. Limit Dilution Factor 1 hereby certify that I have reviewed and approve these data. �Lti Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 MERITECH, INC. Environmental Laboratories Laboratory Certificate #165 Client: Project: Client Sample ID: Sample Collection: vleritech Sample ID: Volatiles: SW-846 8260 Analysis: 02/04/19 Analyst: V W V Parameter Soil Plus Perdue 1st Quarter P0124198 O1/24/19 01241979 1311 - TCLP Organics Extraction: 01 /28/ 19 Report Date: 02/05/19 Result Units Det. Limit Ree. Limit DiluUoo Factor Benzene <0.0100 mg/L 0.0100 0.50 10 CarbonTetrachloride <0,0100 mg/L 0.0100 0,50 - 10 Chlorobenzene < 0,0100 mg/L 0,0100 100 10 Chloroform <0.0100 mg/L 0,0100 6.0 10 1,2-Dichloroethane <0,0100 mg/L 0,0100 0,50 10 1,I-Dichloroethene < 0,0100 mg/L 0,0100 0.70 10 Methyl Ethyl Ketone <0,100 mg/L 0,100 200 10 Tetrachlmnethylene <0,0100 mg/L 0,0100 0,70 10 Trichloroethene < 0,0100 mg/L 0,0100 0,50 10 Vinyl Chloride <0,0200 mg/L 0,020 0.20 10 Semi-Volatiles: SW-8468270 Analysis: 02/08/19 Extraction: Ol/28/19 Analyst: PM Report Date: 02/II/19 Parameter Result Units Det. Limit Reg. Limit Dilution Factor 1,4-Dichlorobenzene <0.100 mg/L 0,100 7.5 10 Hexachlorobenzene <0.100 mg/L 0,100 0.13 10 Hexachloro-1,3-butadiene <0.100 mg/L 0,100 0.5 10 Hexachloroethane <0.100 mg/L 0,100 3,00 10 o-cresol <0.100 mg/L 0,100 200 10 m&p-cresol <0.200 mg/L 0,200 200 10 Total cresols <0.300 mg/L 0,300 200 10 Nitrobenzene <0.100 mg/L 0,100 2,00 10 Pentachlorophenol <0.500 mg/L 0,500 100 10 Pyridine <0.100 mg/L 0.100 5.0 10 2,4,5-Trichlorophenol <0.100 mg/L 0,100 400 10 2,4,6-Trichlorophenol <0.100 mg/L 0,100 2.00 10 2,4-Dinitrotoluene <0.100 mg/L 0,100 0,13 10 I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road *Reidsville, NC 27320 (336) 342-4748 *info@meritechlabs.com LAbORATORIESP INC. nalytical/Process consultations EPA HW Quantitnton Number Contaminant Llrait(mt:/L) 1. TCLP PESTICIDES/HERBIC►DES D-020 Chlordane D-016 2,4-13 D-012 lindrin D-031 Heptachlor D-013 Lindane D-014 Methoxychlor D-015 Toxaphene D-017 2,4,5-TP(Silvex) Sample Number Sample Date Sample Time (hrs) .Sample Mat ix Date Analyzed 2A J 12esnits Characteristic m r/L Levei(me/L) EPA Method Anal st 0.003 l3QL 0.030 3081 MG 1,000 13QL 10.0 8151 MG 0.002 BQL 0.020 8081 MG 0.0008 BQL U08 8081 MG 0.040 BQL 0,400 8081 MG 1.000 BQL 10.0 8081 MG 0.05 13QL U00 8081 MG 0.100 BQL 1,00 8151 MG 620)t7.04 01124/19 Sludge 02106-02/07/19 mEJl:g=>iiiilligrams per kilogrnm=puns per million (Ppm) HQL = Hclow Qumitilnfiaii Limitti _ _ E n' M1• 'o e Y Y O c a)fi o = o w e - .. z a mE �� �..-� .2 = E E�, a N F m F F k QC1 0 J O} v _ O 4a m O Y O Lo W .°. co LJ O = B Y .. W N X E o (D 0 (° E LO a N •• a)- O) m o I _ w v it O � d X •O �� E w Z a O Y Oco a Y `w V) m 2 (D L %Wamm� _ - s T _ o V) N ' c O C. � ^ C K O = c W rn c N O a o a Z cn -° - U X 'O 'O ~ O m E - - - �- m O 3 E °' o � Y 3 = ti a O 2 ( n v O Y V Y .. m C w Y v w o O CJ Q Q a V c ° .. .. E .. E v E N N p F i- VI � w V W ^ V �- ✓6 \ y NIF Y E N 0 6 O c O r Z g tO, � Q m � O U m V) M O E O ca w u a m d � .Q o f V a v W i o o ° z o W O CA N `� N N ISN_ Z a O ix C) •N O N N d n W �' 0 _ N E —F— FL d N u W It Z Z W m w v i O Q O y N O •w O Ow - 0 u w oi rn w O c > Z O N X / O a o s LL a c O 01I,,pIII = Irk N �� Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Contact: Drew Matthews Report Date: 7/23/2019 Client: Soil Plus P.O. Box 1396 Project: Perdue Q3 Oxford, NC 27565 Date Sample Rcvd: 7/11/2019 Meritech Work Order # 071119120 Sample: PD071119 (001) Grab 7/11/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 4.28 % 7/12/19 0-100 % SM 2540B Fecal Coliform (Sludge) 1,488 col/g dry wt 7/10/19 208 col/g dry wt SM 9222D Meritech Work Order # 071119121 Sample: PD071119 (002) Grab 7/10/19 Parameters Results Analysis Date Reporting Limit Method %Total Solids 4.34 % 7/12/19 0-100 % SM 2540B Fecal Coliform (Sludge) 1,047 col/gdry wt 7/10/19 208 col/gdry wt SM 9222D Meritech Work Order # 071119122 Sample: PD071119 (003) Grab 7/10/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 4.30 % 7/12/19 0-100 % SM 2540B Fecal Coliform (Sludge) 846 col/g dry wt 7/10/19 208 col/g dry wt SM 9222D Meritech Work Order # 071119123 Sample: PD071119 (004) Grab 7/10/19 Parameters Results Analysis Date Reporting Limit Method %Total Solids 4.39 % 7/12/19 0-100 % SM 2540B Fecal Coliform (Sludge) 1,450 col/g dry wt 7/10/19 208 col/gdrywt SM 9222D Meritech Work Order # 071119124 Sample: PD071119 (005) Grab 7/10/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 4.35 % 7/12/19 0-100 % SM 2540B Fecal Coliform (Sludge) 1,045 col/g dry wt 7/10/19 208 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 3: Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 2 Contact: Drew Matthews Report Date: 7/23/2019 Client: Soil Plus P.O. Box 1396 Project: Perdue Q3 Oxford, NC 27565 Date Sample Rcvd: 7/11/2019 Meritech Work Order # 071119125 Sample: PD071119 (006) Grab 7/10/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 4.29 % 7/12/19 0-100 % SM 2540B Fecal Coliform (Sludge) 1,059 col/g dry wt 7/10/19 208 col/g dry wt SM 9222D Meritech Work Order # 071119126 Sample: PD071119 (007) Grab 7/10/19 Parameters Results Analysis Date Reporting Limit Method % Total Solids 4.30 % 7/12/19 0-100 % SM 2540B Fecal Coliform (Sludge) 1,057 col/g drywt 7/10/19 208 col/g dry wt SM 9222D hereby certify that /have reviewed and approve these data. � �%�(' �_J Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 Fax.(336)342-1522 E 'T7 O k O n O # _ 10 au m w E o � o Y' -0 `\ 01 f6 F� E pp ~ h o 1 � O Q c M r� N c Y 07 Ln M00 o o o a Y 000 aNi x, LO en to .. C j O N •� E Z a LL w w a` M1, cr w X N tll N N N N 6 LL W � �� N O O o U) (u F v V) wa O yb O O O O O m L1 tV 3 ..� o r r h LO j, p 4mJ ~ o o o r o \ cCL O LO Y E E E E E E E v N - W Y ,....... �- o o O o Z w o U UUj U y x '0 - m O 3 Y E ii LL uL 1� ti LL W — O x 3 = E 0 o- O c = c U Z v O U F Y w v o O U CD C7 0 U I I I E K'O C� HtF> cI` f cf a a v Q� O� O� °� O� O� O� • a �y U W N V O O V l�• ui` ai� ai �N11 ��y Y N N N O p �� O OC E W v�i O 7$ u N O T m m U txo v E w u i o x v T�! (� a V a LL= @, 0 z 1 w `n W (D t� U o v O N W W o w -�— V a _N o UI u z E Sz W O N 0 Q v h V �O, E O O O O O�D O _w _= _ C O O O O 0 3 0 u O O rn rn rn rn o, rn� x v y O E a v 9 s Y. Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: Project: Date Sample Rcvd: 8/15/2019 Perdue Q3 7/11/2019 Vector Attraction Reduction /Aerobically Digested Sludge (3Q Day. Test) Meritech Worlc Order # 071119127 Week 1 Week 2 Week 3 Week4 Week 5 Total Solids 1.33 1.29 1.30 1.39 1.45 Sample: PD071119 Grab Volatile Solids 0.760 0.770 0.760 0.810 0.820 7/11/19 %Volatile Solids 0.573 0.600 0.580 0.585 0.566 Mass Balance Equation = 1.26%Volatile Solids Reduction as per EPA Part 503 Biosolids Rule /here by certify that t have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)3424522 T Y o d = O 0 a u .. E� E� E E wa o N 'C = o_ 000 O� o o Q a3 C, W 0 O O Q = • +� E Z c ux.•. Y v ^c v� u o = NW arm Cd O :3LO v jO N w `/ .✓ ce) V T m a Z a a N X @ o -o o v o - - - m O e = 3 = o a p o ri Omo # U Z v U Q Q a U o Z E E N n c uj u i= r F N w O _ a } cr' E c U N V a o p N 0 N a ok m N^ o V m m s 40 aj E m u o x a"i 11 > > Q cr v o L� F E E _ o ui C z v 0 lima zo D V > o u w •i # Y O C W VJ a C G N .> v \ E _ V c 2 m O = v �I U v- O Ao. pajj O O a v L 61V N APPENDIX 10 2018 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Land Application Site Certification Attachment LAS CA e � ° ° a z � a y `Cd o U PQ L y b w w w b w C O tz :�+ •M�y 1 1 MMY MMom" z z w w y� uJ U z z z z x x x x H PC a rz 'z 'z a �U d r U C C o •� z C J)����� 'O N (-A N N La 3 71 7� 71 n n n cn ) c M UN z N z N z 0 z N z N z N z N z ° a O U b 0 UO v) on v) A A A A d d d d C 0 O O � CO 0q0 0q0 0q0 0q0 00 0 A A A A A AW A q0 A cA a d z z z z z z z z 00 Nil I O O ONow O a N N N id ill m m �o ^O 006 0 loom _ vi On kn O) Q\ kn loom01 ° a o 0 v� 0 0loom M M M M A 1 v1 ca a APPENDIX 11 2018 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Eddie Brown (EB) County Manager Notification Land Owner Agreement Maps Soil Boring & Certification Soil Samples and Biosolid Utilization County Manager Notification SOIL PLUS October 31, 2019 Tommy Bowen, Chairman Martin County Board of Commissioners PO Box 668 Williamston, NC 27892 Reference: COUNTY BOARD NOTIFICATION ATTACHMENT Granville Farms, Inc. "Class B" Program Soil Plus Project No. 200705.D10 Mr. Bowen: Soil Plus, LLC (Soil Plus) is submitting these completed forms and maps as part of a permit application to the North Carolina Department of Environmental Quality— Division of Water Resources (DWR) on behalf of Granville Farms, Inc. These attachments are part of a larger application to modify their existing permit through DWR. This is a routine process that is frequently preformed by Soil Plus across North Carolina for various permit holders/land appliers. We understand that those individuals who do not use these forms on a daily basis have a difficult time understanding the information which is provided. If you or anyone in your county has questions about this application or Land Application of Residual Biosolids in general please do not hesitate to call us at (252) 883-9301 or send us an email at dmatthewsnsoilplus.net. Please also feel free to visit our website (www.soilplus.net) for more information about our programs. Respectfully, Drew Matthews PO Box 1396 Oxford, NC 27565 (252) 883-9301 dmatthews @s oilplus. net www.soilplus.net NCDENR North Carolina Department of Environment and Natural Resources Pat McCrory Donald R. van der Vaart Governor Secretary Date: 10/31/2019 To: Name of Chairman to the Board of County Commissioners: Tommy Bowen Complete mailing address: PO Box 668 City: Williamston State: NC Zip: 27892- County where land application sites are located: Martin From: Applicant's name: (on behalf of the Division of Water Resources in accordance with Session Law 2013-340) Contact person and title: lason Smith Complete mailing address: PO Box I A City: _ State: Zip: 27565- Telephone number: (919) 690-8000 E-mail address: lsmithggranvillefarmsinc.com Subject: Notification of residual land application site proposal This is to notify you that the Applicant listed above will be submitting an application to the Division of Water Resources for the land application of residual solids to site(s) located in your county. During this review, the Division will ensure that all federal and state regulations are enforced. Attached to this form is information regarding residuals - generating sources and locations of the proposed land application sites. Please forward this letter and its associated attachments to the appropriate Department within your County (i.e., Health or Environmental Health Department and Planning Department) if applicable. More information of the land application sites included in this application will be available at the following Division of Water Resources Regional Office: Name of appropriate regional office: Raleigh Regional Office Complete mailing address: T=arrett Drive City: Raleigh State: NC Zip: Telephone number: M) 7�91-4200 Expected date of application submission: - Should you desire to comment on this application, please do so no later than 30 calendar days following the expected application submission date. If you have any questions or comments about this notification, or if you would like more information, please contact the appropriate regional office at the telephone number provided above. Thank you in advance for your attention to this matter. Enclosures: Source Facility Summary Land Application Site Summary Maps Non -Discharge Permitting Unit 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Phone: 919-807-6464 \ Internet: htto://i)ortal.ncdenr.ora/web/wo An Equal Opportunity \ Affirmative Action Employer- Made in part with recycled paper FORM: CBN 1 1-13 e � ° ° a z � a y `Cd o U PQ L y b w w w b w C O tz :�+ •M�y 1 1 MMY MMom" z z w w y� uJ U z z z z x x x x H PC a rz 'z 'z a �U d r U C C o •� z C J)����� 'O N (-A N N La 3 71 7� 71 n n n cn ) c M UN z N z N z 0 z N z N z N z N z ° a O U b 0 UO v) on v) A A A A d d d d C 0 O O � CO 0q0 0q0 0q0 0q0 00 0 A A A A A AW A q0 A cA a d z z z z z z z z 00 Nil I O O ONow O a N N N id ill m m �o ^O 006 0 loom _ vi On kn O) Q\ kn loom01 ° a o 0 v� 0 0loom M M M M A 1 v1 ca a N E s Tar River( arboro) Legend — Road Stream ❑ County Boundary ❑ Field Boundary ❑ Municipal Boundary ❑ Water Supply Watershed SITE EB a 1 0.5 0 1 Miles Scale: 1 inch = 1 mile TT LOCATION MAP Figure Drawn by: DM SOIL. PLUS Granville Farms Inc. Class B Land App Reviewed by: Oak City, North Carolina 1 Date: October'19 Soil Plus Project # 200705.D10 a. C 0 d � •N M M ri Ci Cl! N O m M In m M M m M M In M M M M M m M O O O O O O O O O O O O O O O O O O O O O O d .S C rUw e o 0 0 0 0 0 Qi CQ �Q -119 -a -a -C� C C ti+' id of c� c•� ed iC 7d "C� cC a id cC ..p. O C. L O C C P Q Q * � sE py +c+ w Q x to to to to on to o o 0 0 0 0 0 C W O T T N T N 4W T N 0 (� N CQ N W T T T T T .��+ T Las 78 a "a ' c� a ' c; ' c� a a a c'� � rA a; L' 7 �+ L ❑ Q � C C ❑ � cC C Q � cC O C .D cd � cd � ed � cd ? G 7 C O O t7 ate+ 7 q 7 Q '� q C C C C Q '� q C Q aC 7 G /-• /y w C/] Cn Vi Vi Vi U] N Y bDw o L, L y W •L ¢°' ld co wz� U o 7 L E Fa O kn O O O O O C � In tn O O O O O O O O O 'k N 00 m N 00 O 00 M .-, �-. �-. N �-. .-. N .-. �-. .-� cn CO L L A •--� .�-i Qr L� co ", Vi Vl N V1 y y y y yy VJ V1 y VI VI h N V] V1 N Vi f/ Vi V] S 00 00 OC. N �n O N ID O N :t to m m m t� oo �D 'O O n In N �o � N Ul 00 t- 01 _m O y O O O O O O �D O oo O ON M O �o oo 00 O Cll m CD O N t- 00 N O �o CD N �c ON m M_ O Y1 N �o M �o �D D t- E O N N N N N N N N M M M "It ""I It d' W) h W) W) cn v1 h 7 O Cl O O O O O Cl O O O O O O O O O Cl O O O O O O O O O O O O O O O O O O O O O O O O O O O O p" Z U U U U U U U U U U U U U U U U U U U U U U U z z z z z' z z z z z z z z z z z z z z z z z z •i.w OU N U fV Y v 3 3 as 3 3 3 3 3 3 3 3 3 v 3 W W oAl '> $ E~ 3 W 3 E m o 3 x �$ Q tea, �z E 0 3 a> Y rx a, U U U cn a cd o o > 3 o p v ccF cd ° •� cd cd v C ar 's o o O 'T' o p N �•• m ;; o .0 G C Z c .� o U 4, o `� o ° U P. Q U U °w3 U U U U p as aWi .UC 4. yo L' A o w ° S y o c� }' o � o z 0 z w z z z f. O U ❑ U y z z c� N z c� 09 N Cd T M 0 0 It N C% H w C u' M M M M M M M Cl! M M cn M M M fn M M M rM M M M c o 0 0 0 o 0 o c o 0 0 0 o c o o 0 o c o o ' 0 0 � o 0 ❑ o a o a C � � a o a ❑ o C q� q0 q❑ q� q0 qo q� 0 0 �y C�.,' qC C qC C C C C C �y C C 0 ❑❑ C �j K C �Cy ..fl a a a a a a v U q � U C � U C .� .-. 0 •--� 0 ^' Wn N o m wl� •--� o .-. o ^� °O 0 '� °,° N N 0 �n o 0 N 0 — 0 N a` m M M M M N N N d N N N o N O o 0 V1 O C% C1 lh l- 00 M C\ Vl O 4 �_ �O 00 r , l0 +� In N_ en M_ 00 •--� 7O V"> M 4 d• C1 �' M O N 00 .--� �p V1 M Y1 oo O C� WA o :O .-. N N t- N [- N �D m [- M m � V1 Id,� 00 [- N N M M in 00 � C1 00 C� O1 M 00 M M 00 C1 W) O W) O �c O �c O �D O 110 O IC O 110 O �O O 10 o �O O W O %O O l- O l- O l- O 00 Cl 00 Cl "" N N p N p I- 00 00 0 o O O O O C. o 0 o O O O CD Cl O O O O O z z z z z z z z z z z z z z z z z z 3 3 3 3 3 z z z le �a 3 •° > �a v, x � � 3 3 0 3 � 3 3 � 3 3 �• .° � �w 3 � � � � 0 o b �' w C7 o 0bp o d o b 3 C on a� o u' U� o °o :' c C o x c o N 11 F-I ts � N 1-N I--1 IH Fti �••, (.. F--I I--� Q ° 0 V1 y°� •� •p •� .O •0 •p .� .O y •0 � rn U U U U U U c U o o w U U w U C 33 ° o o a3i ub o o ° c3i �b Z z-+ z w Z..z z z w z z O - tO cd Cd c0 Cd () c0 ca () F [-. (� [ s. U U"' ¢ d d u d d 3¢ ¢ ¢ Ud¢¢ M O N 91 R, Q N Q WA '!f N O ai U M M M M M M M M O O O O O O O O O O O 7 7 O O O O O 'a "J• 7 O O N O kn O N O O CD N n In y y y �D O\ �r O d• N d0 \D OO N N N N N en O O O O O O O O 3 3 3 3 3 3 3 3 3 3 3 u u 3 42 1• � ti �• P O O m N a, H 2 T N N rr U v a U v U U 15 O 0 0 O zz�z O p O O z H b E, Q Q Q O Q Q 9 W .-4 cV tri 4 vi F+ o _ Wkn U O p Vi R y p R v 0. d R w a � K U 0� O O O L m y O O O kn d a v v in rii m M O YO .fir F„ ++ Al L M O A s. Al nl S =' o O y v O o Al At = 0 Al Al F L A I G U d N r� U.S. Postal Service' CERTIFIED MAIL@ RECEIPT Domestic Mail Only For delivery information. visit our website at www.usps.com Certified Mail Fee $ Extra Services & Fees (check boy add tee'' _apjtlgpdate) rq [I Return Receipt (hardcopy) $ 11 .. I i i i E] Return Receipt (electronic) $ f-1 l'; 1-i Postmark El E] Certified Mail Restricted Delivery $ Here 0 E]Adult Signature Required $ Q Q E] Adult Signature Restricted Delivery $ Postage M _r $ Total Postage and Fees M $ U') r-q Sent To martin o!;� ....... Street and Apt. No., or P Sok 'T - ------ .--- - OF -- ff ED,ti --------------------------- ----------------------------- CitK State, ZIP+4 JVC d 7tf 9,Z- LISPS Trackim, Intranet Page I of I He,p . I , T t Product Tracking & Reporting flcLIPl-"�D s�tA-V"-t J P "' Por 'u- P .nual i rit"Y LISPS Tracking Intranet 7"M Delivery Signature and Address DEC 0 5 2019 Tracking Number: 7015 3430 0000 1846 5692 1 M, W, This item was delivered on 11104/2019 at 10:12:00 1ARM-MM , Return to Trackino Number View Select Search Type, ;Quick Search Submit Product Tracking & Reporting, All Rights Reserved Version: 20.1.1.0.5 https:llpts-2.usps.gov/pts2-web/tclntranetTrackingNui-nResponse/deliverySignattireAndAd... 12/5/2019 Land Owner Agreement State of North Carolina DWR Department of Environmental Quality Division of Water Resources DIvision of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting nit. General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ❑ A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Granville Farms, Inc. hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) EB 7-9 Yes Row Crop/Small Grains Animal Consumption No -Till EB 10 Yes Bermuda Hay Animal Consumption Over -Seed The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page 1 of 3 I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section Il) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. H. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h) allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ❑ A re -defined compliance boundary is needed for field(s) ID: (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ❑ A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: NELLIE BUNTING BROWN Address: 205 NC 1 l City: Oak City State: NC Zip: 27857 Phone: E-mail address: Signature: � 1%� ' Jt� �� / h r Date: 020l NORTH CAROLINA. Gra nu lf_ COUNTY I, the undersigned Notary Public do hereby certify that N e i l i e— bunt I Yt 4, E r'D ij h personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the i h- day of ��H P rn f 1 20 Signature and seal: b My commission expires: 7—S — oLd of-� K_ - Lessee's/Operator's Certification: �J E-° I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Eddie Brown Address: 409 NC 11 City: Oak City State: 1►`[y Phone: , 2 — `� iD f E-mail address: Signature: Date: Permittee's Certification: Zip: 27857 I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official Signature: vP Date: �? —/ % 1/ FORM: LOA 06-16 Page 3 of 3 Location Map Soil Map Buffer Map N E s Tar River( arboro) Legend — Road Stream ❑ County Boundary ❑ Field Boundary ❑ Municipal Boundary ❑ Water Supply Watershed SITE EB a 1 0.5 0 1 Miles Scale: 1 inch = 1 mile TT LOCATION MAP Figure Drawn by: DM SOIL. PLUS Granville Farms Inc. Class B Land App Reviewed by: Oak City, North Carolina 1 Date: October'19 Soil Plus Project # 200705.D10 FIELD 3 ism FIELD NET ACRES 5 7.89 7 23.20 8 20.48 9 12.71 10 11.78 FIELD 2 Legend A Structure Well I Ditch r- Property Boundary Field Boundary QApplication Area FIELD 1 FIELD 9 FIELD 8 FIELD 10 FIELD 7 FIELD 5 AL kA Buffer The Compliance Boundary is established either 250 feet from the residuals application area or 50 feet within within the Soil Boundary property boundary, whichever is closest to the application area. I Stream The Review Boundary is established midway between the Pond Compliance Boundary and the perimeter of the residuals 400 200 0 400 application area. Feet Scale: 1 inch = 400 feet EB FIELDS 5 & 7-10 SOIL MAP Figure Drawn by: DM SOIL PLUS Granville Farms, Inc. (WQ0035595) Reviewed by: DM Oak City, North Carolina Date: August'19 Soil Plus Project # 200705.C10 '48 Oro FIELD NET ACREJ Y 'i 11.78 FIELD 9 FIELD 8 FIELD 10 FIELD 5 Legend A Structure �I Well �► I Ditch 40- Stream Application Area Buffer The Compliance Boundary is established either 250 feet from Field Boundary the residuals application area or 50 feet within within the property boundary, whichever is closest to the application area. Pond The Review Boundary is established midway between the Property Boundary Compliance Boundary and the perimeter of the residuals 400 200 0 400 application area. I Feet Scale: 1 inch = 400 feet SOIL PLUS EB FIELDS 5 & 7-10 BUFFER MAP Figure Drawn by: DM Granville Farms, Inc. (WQ0035595) Reviewed by: DM Oak City, North Carolina Date: August'19 1 Soil Plus Project # 200705.C10 Soil Boring & Certifications willcoX&I'l abe SOIL SOLUTIONS October 7, 2019 Granville Farms, Inc. P.O. Box 1396 Oxford, North Carolina 27565 Attention: Mr. Jason Smith Article I. Reference: Soil Scientist Services for Permit Application Granville Farms — Permit No. WQ0035595 Martin County Site — Eddie Brown WMSS Project No. 19-06, Phase: 01 Dear Mr. Smith: Willcox & Mabe Soil Solutions, PLLC (WMSS) has conducted a Soil Scientist Evaluation per WMSS Proposal No. 2019-P11 dated October 3, 2019. The evaluation was performed to provide information for submitting a modification to a non -discharge permit to the North Carolina Department of Environmental Quality (NCDEQ) — Division of Water Resources (DWR), Non -Discharge Permitting Unit (NDPU) in accordance with 15A NCAC 2T .1104(c)(2)(A). The evaluation was conducted to assess the soil properties of the proposed acreage and to determine suitability for land application activities in the referenced permit application. WMSS has included our findings in Appendix I and II in order for this information to be incorporated into the permit modification package being prepared by Granville Farms, Inc. (Granville Farms). The Appendices summarize our evaluations, findings, and recommendations. Should you have any questions or comments about this report please feel free to contact us at (336) 339-9128. Sincerely, Willcox & Mabe Soil Solutions, PLLC Martin Mabe Agronomist Rob Willcox, L.S.S. Soil Scientist Attachments: Appendix I — Summary Table Appendix II — Maps, Soil Profile Description Sheets Shared\WMSS Projects\2019\19-06 Granville Farms\Phase 01 - Martin County Site\Phase 01 Soil Scientist Report - Granville Farms (WQ0035595) - Martin County.doc Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summerfield, INC 27358 / Rob 336.339.9128 or Martin 336.312.1396 / www.willcoxmabesoil.com APPENDIX I - SUMMARY TABLE On October 1, 2019, a Willcox & Mabe Soil Solutions, PLLC (WMSS) licensed soil scientist performed hand auger borings (denoted on the attached maps by red circles) on the following sites and determined that the noted predominant soil series was present for each of the following fields: Project/Permit County Farm Name Field Predominant Soil Series / Site No. No. Mapping Unit 7 Goldsboro / GoA 8 Goldsboro / GoA Granville Farms, Inc. Martin Eddie Brown / WQ0035595 9 Lynchburg / Ly 10 Rains / Ra The hand auger borings were performed to determine if the proposed land application sites were suitable for land application activities in accordance with 15A NCAC 2T .1104(c)(2)(A) and to be incorporated into a permit modification package for Granville Farms, Inc. All fields evaluated were found to be suitable for land application activities. Please reference the attached maps for hand auger boring locations and subsequent soil profile descriptions. SOIL SC� 5 w It - �� 108 Ago NO RSH I ZF41 � E Z � Rob Willcox NC Licensed Soil Scientist # 1098 APPENDIX II - MAPS, SOIL PROFILE DESCRIPTION SHEETS N V � > FIELD NET ACRES 5 7.89 7 23.20 FIELD 1 7-1 7-2 8 20.48 9 12.71 FIELD 7 10 11.78 FIELD 2 FIELD 8 AL ////�'8 -1 FIELD 5� FIELD 9 O 9-1 FIELD 3 FIELD 10 Legend 10-2 A Structure ,I 10-1 Well DitchAj 'I Property Boundary Field Boundary T „ QApplication Area Buffer The Compliance Boundary is established either 250 feet from the residuals application area or 50 feet within within the Soil Boundary property boundary, whichever is closest to the application area. I Stream The Review Boundary is established midway between the Pond Compliance Boundary and the perimeter of the residuals 400 200 0 400 application area. Feet Scale: 1 inch = 400 feet EB FIELDS 5 & 7-10 SOIL MAP Figure Drawn by: DM SOIL PLUS Granville Farms, Inc. (WQ0035595) Reviewed by: DM Oak City, North Carolina Date: August'19 1 1 Soil Plus Project # 200705.C10 WILLCOX & MABE SOIL SOLUTIONS, PLLC After J aF 4 SITE/SOIL EVALUATION Project No. lq- 06 ' Ptt: 01 Phone No. Location �prFO geep//�/Pin County: FEL-05 r7- lb Proposed Facility: 1_.9n/D APP21L470n/ Water Supply: DF ,�tFs�Durt-z5 Described By: ';C206 A/lLl10 lc Weather: SUMA)yy ;WARM Antecedent Moisture n ra- Date: /D l 1 �1 7-/A/ Property Size On -Site Well ❑ Evaluation: Community ❑ Public ❑ Publ Surface Water: rJ- Auger Boring X Pit ❑ Cut ❑ FACTORS PROFILE 2-0n1+ PROFILE PROFILE r1— I PROFILE -1 Landscape Position% A11,1L. N/q Horizon Depth I d — O _ Color Mansell 311 Q /� S - Texture s Structure Consistence s 11 A5 nj2 V Fi' Boundary Horizon Depth II (o _ /Q 2 } - f Z - 52 t Color -Mansell , 5' S.4 Id2 2 L 3 & Texture Mottles e/ I !� ¢ _ ,� L - 5 Structure le4 k, k' Consistence S S SS S Boundary Horizon Depth III 12 _ Z Color —Mansell , S S ¢ 57A, Texture Mottles . / /y >^ Structure Consistence $S Boundary Horizon Depth IV l 11 Color —Mansell fo1 /p Texture Mottles - Structure S L S Consistence 5 5 55 S c - 6 U f0 3 Boundary Soil Wetness I/!} Restrictive Horizon Saprolite LTAR Classification AId ff0 j2& O pS 136 M r! 2EDQ,vI�,v/+nlr SE2r� � s o�2 LEGEND LANDSCAPE POSITION R Ridge Interfluve S Shoulder L Linear Slope FS Foot Slope N Nose Slope H Head Slope Cc Concave Slope Cv Convex Slope T Terrace P Flood Plain TEXTURE s and Is loamy sand sl sandy loam I loam si sat sa silt loam sicl silty clay loam el clay loam scl sandy clay loam sc sandy clay sic silty clay c clay Ns non -sticky Ss slightly sticky S sticky Vs very sticky Np non -plastic Sp slightly plastic P plastic Vp very plastic MOIST vfr Very friable fr friable it firm vfi Very firm STRUCTURE sg single grain m massive cr crumb gr granular sbk subangular blocky abk angular blocky pl platy pr prismatic WILLCOX & MABE SOIL SOLUTIONS, PLLC A6 r 2 of SITE/SOIL EVALUATION Project No. lq-4Z ' IQFI; Q / Phone No. Date: /Q Location CD&F P Ally Pin County: /YlA.QTiN Property Size Proposed Facility: ZAAZ APAtU p v Water Supph vF s�9uRLS Described By: 2K`Wzz-e0z Weather: $uNN� bj�fcm Antecedent Moisture n R On -Site Well ❑ Evaluation: Auger Boring ,� Community ❑ Pit ❑ Public ElCut ElM /' Ibl S 7-Ok Surface Water: N I A FACTORS PROFILE PROFILE PROFILE PROFILE GDn1+ Landscape Position % A// A �Pr Horizon Depth I `S Color Munsell / Z ..3 1 Texture Structure Consistence ✓ AS Fr Boundary Horizon Depth (� - I'Z `L t 'u12(0 Color —Munsell (o / 2 6 /D 2 Texture C 5 Mottles Structure 1L S lL /L Consistence 5 S i S C S c , 1D Boundary Horizon Depth IH / _ I r7 Color — Munsell (p $ Texture Mottles -F'_ /ae (- _ !� Structure W) be G Consistence 5 Boundary Horizon Depth IV Color —Mansell to (0 2 Texture G/ G Mottles C- &)YAL 2 G hl- & Structure xl Consistence 55 S Boundary Soil Wetness 2 4, 11 r7 It Restrictive Horizon Saprolite LTAR Classification 5 De0 NG "AP FIE - FDQMINA 7 SDIL- S-FOLS IS 1.)LDS95eD LEGEND LANDSCAPE POSITION R Ridge Interfluve S Shoulder L Linear Slope FS Foot Slope N Nose Slope H Head Slope Cc Concave Slope Cv Convex Slope T Terrace P Flood Plain TEXTURE s sand Is loamy sand sl sandy loam I loam si silt sil silt loam sicl silty clay loam cl clay loam scl sandy clay loam sc sandy clay sic silty clay c clay Ns non -sticky Ss slightly sticky S sticky Vs very sticky Np non -plastic Sp slightly plastic P plastic Vp very plastic MOIST vfr Very friable IT friable fi fimt vfi Very turn STRUCTURE sg single grain an massive cr crumb gr granular sbk subangular blocky abk angular blocky pl platy pr prismatic WILLCOX & MABE SOIL SOLUTIONS, PLLC ?A(" SITE/SOIL EVALUATION Project No. /9—t`)6,' Aq, Q/ Phone No. Date: lD / Location E&&r I&ODWNPin County: Property Size Proposed Facility: .L y�,Op�tCp t?Dt✓ Water Supply: On -Site Well ❑ Evaluation: Auger Boring Described By: Z-7vF ESt.D4AL5 AI/LLLDIC Community ❑ Pit ❑ 's Public ❑ Cut ❑ Weather: Nt Antecedent Moisture SliN��� Ut5 T �2 Surface Water: Nllaj A q FACTORS PROFILE PROFILE l 9-( �D PROFILE PROFILE Landscape Position % n/ 4 Horizon Depth I — Color Munsell Texture Structure Consistence ns y A - Boundary Horizon Depth II — l 2r]2 Color—Munsell ,S S 1Pka Texture Mottles 1 Q- Z /fig 6 Structure L Consistence SS 5 rn- 6 Boundary Horizon Depth Color—MunsellTexture MottlesStructureConsistence A_/'/0 Boundary Horizon Depth IV 9 Color—Munsell /p Texture SG Mottles C 3 Structure /L Consistence SS C Al — Boundary Soil Wetness 11 Restrictive Horizon Saprolite LTAR Classification LyN D WfY?1NAa SD/L SE21C-S 15ZVV1,qSj911b1 LEGEND LANDSCAPE POSITION R Ridge Intertluve S Shoulder L Linear Slope FS Foot Slope N Nose Slope H Head Slope Cc Concave Slope Cv Convex Slope T Terrace P Flood Plain TEXTURE s sand Is loamy sand d sandy loam I loam si silt sil silt loam sicl silty clay loam cl clay loam scl sandy clay In= so sandy clay sic silty clay c clay Ns non -sticky Ss slightly sticky S sticky Vs very sticky Np non -plastic Sp slightly plastic P plastic Vp very plastic MOIST vfr Very friable fir friable fi ram vfi Very firth STRUCTURE sg single grain m massive cr crumb gr granular sbk subangular blocky abk angular blocky pl platy pr prismatic WILLCOX & MABE SOIL SOLUTIONS, PLLC f q'r 4 L)F 4 SITE/SOIL EVALUATION Project No. I Q-ofp pff! ©I Phone No. Location Ew)IZ 13emiA/ Pin Proposed Facility: N PkieA-noai Water Suppl, OF 140MA-1-S Described By: ,38/LG[pL/ Weather: Antecedent Moisture t ci n /A County: Date: m b 141— Property Siz On -Site Well ❑ Evaluation: Auger Boring A Community ❑ Pit ❑ �Public ❑ Cut ❑ /r lN37 Surface Water: MIA c,n I/\ FACTORS PROFILE /6- PROFILE I -1 con PROFILE - 2 PROFILE -2 cant Landscape Position% ofl)q� N A Horizon Depth I _ r] Y Color Mansell 3 5 2 Texture Structure MIA r Consistence Boundary Horizon Depth II rf— / _ 5 k _ 12— —S?- Color — Mansell R $ Z Q $ C, (0)2 Texture $ G1 S < G Mottles — ( 2 _ - /U 2 (o/ Structure I/�. S bt Consistence S 5 S 5 Boundary Horizon Depth III (o Color —Mansell / /a (o Texture Mottles /0 le _ (p Structure Consistence SS S Boundary Horizon Depth IV —4 Color — Mansell 6 I jo 6 Texture C% Mottles (p 2 -'C 2 Structure bX Consistence 5 S S 4 4- Boundary Soil Wetness 2 q Restrictive Horizon Saprolite LTAR Classification / D De ! D lb— / MlA)rw-r. d!L S elFS lS RAW LEGEND LANDSCAPE POSITION R Ridge Intertluve S Shoulder L Linear Slope FS Foot Slope N Nose Slope H Head Slope Cc Concave Slope Cv Convex Slope T Terrace P Flood Plain TEXTURE s send Is loamy sand sl sandy loam I loam si silt sil silt loam sicl silty clay loam cl clay loam scl sandy clay loam se sandy clay sic silty clay c clay Ns non -sticky Ss slightly sticky S sticky Vs very sticky Np non -plastic Sp slightly plastic P plastic Vp very plastic MOIST vfr Very friable fir friable fi firm vfi Very finn STRUCTURE as single grain m massive cr crumb gr granular sbk subangular blocky abk angularblocky PI platy pr prismatic WIN G I ctr S HAV& 27tCtj4LW LotdEB O .EI[K?/A16 q� z 7ABLES Soil Samples Biosolid Utilization 00 00U 0 (n o Z ON LO 00 C a>'iUco N J 0)N J � U co Z O a N 00 M E a cu = o cn cn coO N L 0 0 O m co E N o o Z Z M Z — c co a cn lJJ N CD o E 7 4).0 O m co E o o Z Z M Z cn cn a W o 0 E = Z d m O co L m O m O a) OQ O O 3: X CO d = L U U O p- L E 0 Z _4) a) cn Z a) cn a) p 0 N Q U O = O N > O C o CL 0 U — O U — > 'a U 0 — o = 00 CO 00 = c, 00 00 r ui U m riun v E Tm N O Lo d N CD R 00 d O N J N J U 0 C N L N L U) aa) . O 4? E nz — — a6 .o o �O c LO o � N 00 v Q N V)LO O M O N CD U (D a) u) Ecm N y y cm ` LO = Q m a U Q E ci Q E ui L U) -- E L co O —_ .O 7 •E coo .O E 8 N _ 76 •2 O O c m c 2 E L O U 0 0 U_ a) o .N L-0� a) O s 0) O s E a) X Z O .- -O Lo N O >, a3 Co > a) z 01 0 Q I� M U Z CD 0 Q 0 M U o p C m p E� = 3 w c 0 U) E p X a3 O L N - 3 (D 0 U) m0 E rn > N (06 >, O 0 LO O O O O - N - N � Q C (V co COY N O _ N O Y L U U 0 0 4? c 0 0 — d Y m Y m 0 p O 0 N CV Z - cn 00 ITZ cn c0 Z U m V) c 00 W- N 0 O N C O uoi p cu a> LL M" �� s E CDE O U) v+ U rtt x w m E o E p UI Q L Q �Y CD: Z� o CDCDV Z� cc c0 N R LO = R W U.BUD ��_ c V _ c VLO = M E z Z E Z E L >.E cn > cu M m M N U o c s° m O— U m O— L U cn c� w o E m a s ui ._ .( m L u o o Z M_ Y rn m L u o Z M_ Y LO �_ > �, J�,�O E JN�O E 0 c c c`1 M — m > a) U 0 w CL — — O Lq — — 0 O U')cn M -a a 06 N s a CDs a o c NE E o O E c; E �1 o as c c cc000 L U E co E o 6 R Q Qr c •Lo ZO • c; Q s d 5 m r Z-0 .� o m R m R w o ccv a�cl c c cC A/ x CD a) c� L E V E V �+ c O. V O a UO E c U) Q U O 0 � N — J N O � v c co c co _O E > 0p _ c 0Sc: Q_ E rn E c c O o U � U r O 0 CDO E ns cop 0 r- Q a0 Q 0 n Q s ry til O ;a � X Q� d � w � M w �' w � N aLO te+ z Q a) 0 y y s k O N !ECN y N N q Ta+4 Q- p — C N N M 16 p V aq UL Q. > R E y+ d x N E �+ d= _ Z ig5x. y Q cn J H Cl) J H c >, p .+ c cn cu E Z ocn c � U m � E •V = o a a LL cn Q cn 0 O O N O C OL N CO ,O -0 cu .O L 0 cn N c O Y o v) U s = O w o E Z E E CO o 0 E u) � O U N � O N U) p� U = E 0 0 .� � 0 O O N C � C 0 = cu p o M s O O Y co w co 0 0 ~ c E N 0 O a a) \ \ \ y U- 0 \ I § o m n E 6 os 7z z z _ ( Cl) a- w g o ( § E- o M E 6 os 7z z 0 z (n m o- w 6 ( z m/ i mo i E z\ n z\ n � 3C 3C) k \ I--k \ o a a NCD p $ �� �_ ) ~ N 5 5 �0 3 & 0 3 \ _ m N _ m 04 2 Q _ ( n = U) \ U) E 0 2 2 U) I 0 7 } _ § Cl) § \ � _ 2 & 0 o o o G\ � �C) �cy) / � z � z 3 U $ § N o qo k a o a CD' CD z\ cm a \ �\ = cm a E � 2 ¢ Em S ¢ / E / \ § ® �uco E 2 a a �uoo E) a a w c u n c u A p 8 _ CDo \ ƒ _ _ Lo (.0 G I » ) m I 0-)) c £ % \ z 0 a 2 2 z 2 = 2 - E { w 2 E w 2© E § 2 0 \ u 7 E § CL 2 f u # @ , u a® @ E P , u^ k// / F m E F m E a § § ° / U o ® 0 / U n ® 0 0 2 2 U § c � ' 3 0 ' 3 aE _ _ Cl) — 2 _ w E m m § 2 § � - a § ® � \ $ / $ / Q b 2 & I I E b � E 2 I I z m n 0 O O Cn Op N � p p Q fU 0 Cl) N C O ++ •R� Q Q N C O E m C U C1 C1 U E a) U .0 T i C to .0 U +•-Q cuN -0 CO m E E a- x x x _ a o co - -0 a) a) a s o E x a : m cn a) x .c co a) a) <n E cn a cn a a) .Q c � cu 2 c a 7 7 N x Eco 0) U C2 ' O— U U C) a co 7 U O U y 0 0 i .0. 0 (m L Cm O O x ,C - O cn ,� O C •� U O O Cm O Q '(p m C W W C a) m a) w w W 0) CU CU 0 0) E C- C L - N x a) O- mmO C C O OxO x 0 0 c O(m <n -0 U U a)Cl Cl cL E E 2 2 E E pm ) UC aa) O O a7t tN 7C 0 U c O U Q Q U U 2i 'N •C C N CV Z V to N W 3 to 'L Z C: C C C 0i N O �' 2— O fn C C Z Z Z O O. d d fn fn N N C 0 Cm >, Co i +- L U) .(n w O O O O N a) M ;- °° 0- cmO 0 C m co o§ C E `) U) U� C:im .0� ~ a) m �� Q U) =5 a Lo LO a) L U o 0 ° a) o= S a) n aa)i Q o a �C) 0 a)� o ° �C� 0zo L m N fn = N E i O Z'§ c Ego Lo o ° m 0 oo u 40 '-� Za a) o E U '- 0 O� C -O E a U > a) tm CU> a Cm C 0- y C Cp p O a i O L C L m O m O a) N a) a •C U)= E U O) C = a) Lo a) in Ein v� C cm 'p C O .N ° Z -a p C U cm N N y R o E m' > CD o c ai U co L) L C � o 0 o E ^�' CD ` � Cm E m CO L3 3Q iC . E E E L a)a oa°oo m m O O U m 0- E m cm m Q m O YC y C NNyO C,° N a E Q) a) a L C a) cm G a) O C 73 fV 0 °(D a) 4)a) ELL cn d O =a Zu)-E m U N NEO� 6. � `~ a 0- W NQ ta C n Cn u 1 C0 o�CV Q M N O C a U o >, _° m°N O ° v CL E oE i,.� UUoQ N a)O WQ C ° C � 7 m -Z LL O D — c Z a)to r- o R !E L E O 0 Z 0O U 0 O ) °a°A)a)o x 0 — a) a o D to a) -0 U) °E_o 0) a a) —c a E m 8-0U) C: U 'EE o° OLO LO E m m C Q E a) c0N� O U CL w QUC E ) 0 cc p U °An 0 v) _ 0_ v: N LO C t) O 0 p O C Ncn -- y cn _0 ay u> Y m CD U) U O NO -0 cn � N U) C-C °n-cn OC O n>Er a 70 � o ° � () CL C C 0 .' .E U)m L0 O =) -O a)0 V2- U! U °i i E O O N E U p 0 0 °, E L C vcn U C2 0- a) O O OU x a) N "a U .O. C L O m � 0 A m i a) a)> \ E m C Cm a) >' N m N a) a) E Cm L Z O 0 .. E LL L C C Q' O m m 0 O a) U LL C C �' E H > m Waypointo ANALYTICAL 10/14/2019 Soil Plus, LLC Joyce Barrett P.O. Box 1396 Oxford, NC, 27565 Ref: Analytical Testing Report Number: 19-282-0001 Project Description: Granville Farms Inc (EB) 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Joyce Barrett: Waypoint Analytical Virginia, Inc. received sample(s) on 10/9/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, �a f• 6-7' Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 (2) Waypoint, 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 19-282-0001 Client Project Description: Granville Farms Inc (EB) Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 68538 EB-007 Solids 10/09/2019 6010D WTN 68538 EB-007 Solids 10/09/2019 SW-7471B WTN 68539 EB-008 Solids 10/09/2019 SW-7471B WTN 68539 EB-008 Solids 10/09/2019 6010D WTN 68540 EB-009 Solids 10/09/2019 SW-7471B WTN 68540 EB-009 Solids 10/09/2019 6010D WTN 68541 EB-010 Solids 10/09/2019 6010D WTN 68541 EB-010 Solids 10/09/2019 SW-7471B WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia Page 2 of 8 :)Z•Z a) Ma % y N v D'0 ME Q -y m en N O C) V d 0 CD `l PV T U) Q 00 L) w c 00 = i l6 C� = o CL C� r-I 7• °C 3 .Q o a 00 N n J Q J Q Q m w LO �— Cfl U LO C N to J U li J N Z i 7 m O N m co > y U O E o0OX = 0o Z Z O , H d 0 N 3 O CO O M 'O Q CV C1 LO C d Q 0 U) _o J Z Q LJL °a ui a) Q E R cn a) m 0 m O n g O >1 O O O U) .0 .w C C a) a� L L O U U w @ •'= LO M O -O 'O y E ww c J Oo Ci a co Cl) 3 ui O O L L N � 75 70- CU_ CU_ Y O a) a) y o U U o U U .U) U � d ui w N U)U) m co -a a U) in 0)0) � c .70, m m ww `o 0 cn cn O O L L N � 00 o Y cn cn a) a) � m O O E O w Y It CO 00 E a) C m w U) U E y �, OcLrL E Z mU t ma c6 C a) O d U) O7 O J Q 2 Z) Z) U co nLo� "aMa § / q ME a a ) 2 § r 0 > r t 2 C c 00 k §k j � _0 CL / R 7 � Eo 00 k k 2 / e � � � � � 3 u \ 2 G—� (\ }\0 2 :5 0 3 E =co 5 . \ o ) E m \�$/ o { \ 7 C.0 9 k E3 SLO \ k \ co � � 7 Q LJL O � � O W 1% � ƒ 2 ) a k \ R }\CD §§ � 77 \\ E E \\ § /7 CO �/ dj \ « 2 2 m i 22 k\ // §2/ 27 \\ J\j v �>1 EE ƒƒ \\ \\ �70, m co \\ k\ as ƒ/ ƒ\ 2 / 2j E / It CO 00 \ —a)m f } } \ \ k }E \ \i 0ƒƒ& ° e \ @ ms 2//o « 2 ==Q � � co j } / nLo� "aMa § / q ME a a ) 2 § r 0 > r t 2 C c 00 k §k j � _0 CL / R 7 � Eo 00 k k 2 / e � � � � � 3 u \ 2 G—� (\ }\0 2 :5 0 3 E =co 5 . \ o ) E m \�$/ o { \ 7 C.0 9 k E3 SLO \ k \ co � � 7 Q LJL O � � O W 1% � ƒ 2 ) a k \ R }\CD §§ � 77 \\ E E \\ § /7 CO �/ dj \ « 2 2 m i 22 k\ // j§/ kk @g J/v EE ƒƒ \\ \\ �70, m co \\ k\ as ƒ/ \\ 2 �// 2j E / It CO 00 \ —a)m f } } \ \ k }E \ \i 0ƒƒ& ° e \ @ ms 2//o « 2 ==Q � � OD j } / nLo� "aMa § / q ME a a ) 2 § r 0 > r t 2 C c 00 k §k j � _0 CL / R 7 � Eo 00 k k 2 / e � � � � � 3 u \ 2 G—� (\ }\0 2 \j§� ° E =co \ . \ o ) E m \�$/ o { \ 7 C.0 9 k E3 SLO \ k \ co � � 7 Q LJL O � � O W 1% � ƒ 2 ) a k \ R }\CD §§ � 77 \\ E E \\ § /7 �/ dj \ « 2 2 m i \\ » // j\/ kk @g J/v EE ƒƒ \\ \\ �70, m co \\ k\ as ƒ/ o = y« /9 2j E / It CO 00 \ —a)m f } } \ \ k }E \ \i 0ƒƒ& ° e \ @ ms 2//o « 2 ==Q � � co j \ a WayPAoint. NALYTICAL Customer Number: 04596 Customer Name: Soil Plus, LLC Report Number: 19-282-0001 0 Fed Ex 0 US Postal 0 UPS 0 Client 7621 Whitepine Road, Richmond, VA 2-4237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Cooler Receipt Form Shipping Method 0 Lab 0 Other: 0 Courier Thermometer ID: Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers received Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required Custody seals intact on sample bottles? 0 Yes 0 No Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? ® Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No ® N/A F High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: Brandi Watson Date & Time: I10/09/2019 14:23:41 Page 7 of 8 LQ Q7 LO C 0 C ra d 2 R/ cz 0 tj w 4 N � C O � C T5 N LO c N 21 CD LS7 00 CO ❑ m m 0 � [a N G p y-- � N U o o LL } W U) x Z � a w c Q a p C CL o CO CV u7 a. ¢ -0 D — -0 F 0 d N a o ❑ 7+ vj p p W a x v } C7 c o 0 ° c 2 � 0 .. _v a a � �,C U- R C4 u C Cl L p N io N .Z v' y Q — 2 � ' N N Q US N (3 (} E a- aw m x w x a� � m �to o > z c m CI] M � o m rV C N yy ca C] O E U] .� o a :0O p � U ❑ � N m m CY C U3 U N y O 47 6 U) LL [6 Em w C V .7 7 E (13 Fc) E O C C p N y F.. N � N E m�� m ❑ c No co a = E 73_ Q 3 coo [] m d ° ❑ N T �L � ooCL In L) 2 m 0 a a) cu mr 0 v� i W m x a m a CLLI [❑v 0 ` CtJ cm U7 DD QJ N .Q 76 E U LU O_ � o Q r U N E o a CDa U N M 00 M T- .- M V 00 O r GD M O oo co Lr) G1 00 GG1 ; M O G1 00 a O H C1 CN O is U O O On 0000 C7 a � U 00 00 to F+1 M Ln z� ~ c� O U U V V v 4-4 d' � � � C7 C7 C7 -d Lr) o V � C N � n 00 y z N O N N -i' "0 -" o c� .v � oo c, w U U � O y H a a H c7 H A in �4 00 GN l- 00 N :1 C+1 M O "t tr' M h 00 Z 9 U v� Q sa 0 0 U � Ln Ln �o b a 7 H u Q °z O 00 U n w (� U U o c