WQ0037094_Residual Annual Report 2014_20150512

F
L l�
2014 ANNUAL REPORT
HOWARD FERTILIZER COMPANY, INC.
DISTRIBUTION OF CLASS A MUNICIPAL
WASTEWATER TREATMENT PLANT RESIDUALS
NON -DISCHARGE PERMIT #WQ0037094
Prepared For:
Howard Fertilizer Company, Inc.
8306 South Orange Avenue
Orlando, Florida 32809
Compiled By:
S&ME, Inc.
8646 West Market Street, Suite 105
Greensboro, North Carolina 27409
May 2015

May 8, 2015
NCDENR-DWR / Non -Discharge Permitting Unit
512 North Salisbury Street, 6 h Floor
J
Raleigh, North Carolina 27604
Attention: Mr. Ed Hardee
Non -Discharge Permitting Unit
Reference: 2014 ANNUAL REPORT
Howard Fertilizer Company, Inc.
Non -Discharge Permit No. WQ0037094
S&ME, Inc. Project No. 4358-14-025, Phase: 02
S&ME, Inc. (S&ME) is submitting all monitoring and reporting requirements as specified in
the above referenced permit for Howard Fertilizer Company, Inc. (Howard Fertilizer) on
behalf of Howard Fertilizer. S&ME compiled this report using data provided by Howard
Fertilizer. This data includes: 1) Class A Annual Distribution of Marketing / Surface
Disposal Certification and Summary Form, 2) Annual Residual Sampling Summary Form, 3)
Annual Pathogen and Vector Attraction Reduction Form (02T), and 4) Analytical Data.
Howard Fertilizer distributed 128.75 Dry Tons of residual solids in North Carolina under
Permit No. WQ0037094 during the 2014 calendar year.
If there is any further information required or questions regarding this distribution program
please do not hesitate to contact Mr. Michael Brooks, Corporate Compliance Officer (407)
466-2960 for further assistance.
Sincerely,
S&ME, Inc.
Rob Willcox, L.S.S.
Senior Project Manager
Enclosure(s)
cc: Howard Fertilizer Company, Inc.
T:\Projects\2014\EN\A4358-14-025 Howard Fertilizer\Phase 02 - 2014 Annual Report\2014 ANNUAL REPORT.doc
S&ME, INC. / 8646 W. Market Street, Suite 105 / Greensboro, NC 27409 / p 336.288.7180 f 336.288.8980 / www.smeinc.com

i
Li TABLE OF CONTENTS
Jj SECTION NO. TITLE
a
I Class A Distribution and Marketing / Surface Disposal
Certification Summary Form
Form DMSDF
II Annual Residual Sampling Summary Form
Form RSSF
III Annual Pathogen and Vector Attraction Reduction Form
(02T Rules)
Form PVRF 02T
IV Lab Sheets
Analytical Data

Class A Distribution and Marketing / Surface Disposal Certification
Summary Form
FORM DMSDF

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: W00037094 FACILITY NAME: _ Howard Fertilizer Company, Inc. / South Cross Bgou WRF Pelletizing Facility
PHONE:[phone] COUNTY: Statewide OPERATOR: N/A
FACILITY TYPE (please check one): ❑ Surface Disposal,(complete Part A (Source(s) and "Residual In" Volume only) and Part C)
El Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the oast calendar ven r? VAR fri Nn f-1 IfNaskin nnrts A_ R. r and certifv farm hrinw
Part A*•
Part B*•
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons
i
Recipient Information
Amendment/
Bulki Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
JanuarySouth
Cross Bayou WRF Pelletizing Facility
128.75
128.75
Class A Residuals utilized
128.75
Fertilizer
February
for Distribution during 2014
March
April
May
June
Jul
August
September
October
November
December
Total ,from FORM DMSDF(sup
0.
0
0
0
Totals: I Annual (dry tons :
0
128.75
1 128.75
128.75
Amendments used:
Bulking Agent(s) used:
u muro space is mquireu, anaca aamnonai mrormauon snecis kruKM liMbur (Sapp)): Total Number of Form DMSDF (Supp)1_ _ 1
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit ` El yes
(including but not limited to items 1 3 below) issued by the Division of Water Resources: ❑ No -► If No, Explain in,Narritive
L All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
r
I li L s �01V ` N/A N /A
Signaturof e Permittee _ a Signature ofPreparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (1212006)

Annual Residual Sampling Summary Form
FORM RSSF

1
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B .
WQ Permit Number: WQ0037094 Laboratory: 1) A&L Eastern Laboratories, Inc.
Facility Name: Howard Fertilizer Company, Inc. (Permittee) 2)
Residual Source WQ # or WQ0037094 3)
NPDES #: 4)
WWTP Name: South Cross Bayou WRF Pelletizing Facility 5)
Residual-AnaIvAs Data
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sam le or Composite Date
3/5/14
Percent Solids (%)
NA
91.83
Arsenic
75
17.0
Cadmium
85
13.0
Copper
4,300
552
Chromium
NA
- -
Lead
840
188
Mercury
57
0.5
Molybdenum
75
10
Nickel
420 '
26
Selenium
100
5.0
Zinc
7,500
1640
Total Phosphorus
NA
31800
TKN
NA
-a
5.85
Ammonia -Nitrogen
NA
5160
Nitrate and Nitrite
NA
4.57
ror surrace aisposai racemes the ceding concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under, my direction or supervision in accordance with a system designed
to assure: that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penaltiesfor submitting false information, including the possibility of fines and imprisonment for knowing violations."
* Permitte (Howard Fertilizer)
Signature of Preparer * `eve Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
i

_1 Annual Pathogen and Vector Attraction Redaction Form - (02T Rules)
FORM PVRF 02T

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Howard Fertilzer Company, Inc. (Permittee) WQ Permit Number: WQ0037094
WWTP Name: South Cross Bayou WRF Pelletizing Facility NPDES Number:
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)[]............
Alt.D (No Prior Test) ®
Process to Further Reduce Pathogengs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying El
Heat Treatment ❑
Thermo hilic ❑
Beta Ra ❑
Y
Gamma Ra ®
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
All. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying 0
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
Frequency
of Analysis
Sample
Type
a ica
Tech-
nioue
Minim
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
wei ht
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ®
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization ®
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) El
Alt. 9 (Injection) ®
Alt. 10 (Incorporation) ®
No vector attraction reduction alternatives were performed ❑
r I
CERTIFICATION STATEMENT (please check the appropriate statement)
CI "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
N/A N/A
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
N/A
Signature of Preparer*
Date
N/A
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Lab Sheets
ANALYTICAL DATA

Page: 1 of
Report -Number: 14-065-0207
A.&L Eastern Labocatones, Mc.
Account Number: 02537
Pit -
7621 Whitepine Road Richmond, Virginia 23237 (s04) 743.9401 :Fax [phone]. '
Submitted By: JUSTIN MANNING
wwKaleastern:com
Send.To:`SYNAGRO FL" (29-0750)
Project :PELLETS
MATTHEW BUSCH
5.900 74TH ST NORTH
ST PETERSBURG , FL 33709
'REPORT OF ANALYSIS
Date Sampled: 3/5/201413:00:00
Lab Number: 98246
Date Received: 03/06/2014 00:00.
-Sample-Id: PELLET
RESULT
RESULT
QUANTITATION
Date Reported: 03113/2.014
PARAMETER
Total Solids, *
91.83�
918300
100.'0.
ANALYST
JM
.•
03106/201414:35
•.
SM-2540G
Moisture A
8.17
100:0
JM
03106/2014'14:35
SM 2540G.
Total Kjeldahl Nitrogen
5.85
58500
. 10.0
JM
03/07/2014 08:05 SM-4500-NH3C-TKN
Total Phosphorus
3.18
31800 `
100
KM
03/071201413:23
SW 601 OC
Total Potassium
0.28
2800
100
KM
03/07/201413:23 _
SW 601 OC
Total Sulfur
1.26
12600
100
KM
03/07/201413.2
SW 601 OC:
Total Calcium
3.77
37700.
100 .
KM
03/07/2014 13:23
SW 6010C
Total Magnesium nesium
0.54'
5380
100
KM
03/07/2014 13:23
SW"6010C
Total Sodium
0:17 :
16.90
100
KM. -03107/201
413:23
SW 601 OC '-
Total Iron
8220
.100
KM
03/07/2014 13:23
SW 60100
Total Aluminum
30800
:100, .
KMM
03/07/2014 13:23
SW 6010C
Total Manganese
204
5.
KM.
03/07/2014 13:23
SW 6010C
- Total"Copper
552
= 5 -- .
XM
03/07/2014 13:2.3
SW 601 OC
Total Zinc
1640
5
KM
03107/201413:23
SW 6010C .
Ammonia Nitrogen, -
0.52
5160 , ::
-10.0 :
JM
03/07/2014 08:05
SM-4500-NH3C
OrganicN ..
5.33
53340 .
10.0
03/07/20.14.-08:05 "
CALCULATION . .
Nitrate+Nitrite-N ..
4.57:.
a 2:00
= JM .
03/07/2014 08:05.
SM-4500NO3F
Total Cadmium ..
13.0 .
-2.0
KM
03/07/201413:23
SW 601 OC
All -values are on -a dry weight basis except as noted.by-asterisk: Detection limit on all N
series is on- a wet basis.
our reports and letters are for the exclusive and confidential use
of our clients,
and may not be reproduced in' whole or part, nor may any reference.be-made
to the work. the results; or the company:in any advertising, news
release.: or other public announcements
without obtaining our prior written authorization:
Debbie Holt

Page: 2 of:2
Report Number:. 14-065=0207 AL catorias lnc.
A &L: eastern- :LabO
Account Number: .02537 Mi.whitephte Road: RieWand; Virginia 23W [phone] paX,MW) 271,E+346
Submitted By: JUSTIN MANNING www.awastem.com
Send To: SYNAGRO.FL (29-0750) - Project : PELLETS
MATTHEW. BUSCH.
5900 74TH ST NORTH
ST PETERSBURG , FL 33709
'REPORT OF ANALYSIS Date Sampled: 3/5/201413:00:00
Lab Number : 9824E Date Received: 03✓06/2014 00:00.
Sample Id: PELLET Date Reported: 03/1312014
RESULT RESULT QUANTITATION
DATEITIME METHOD
Total'Nickel.. 26 .5 KM . 03/07/201413:23 SW 6010C
Total Lead 188 5 KM 03107/2014 13:23 SW 6010C
Total Arsenic 17.0 3.0 KM 03/07/201413:23 SW:6010C .
'Total Mercury 0.5 0.4 KM 03/10/2014 09,00 SW-7471B
Total Selenium 5.0 5.0 KM 63107/2.01413:23 SW 601CC:
pH"(Standard Units) " 6.93 2.00 - JM- 03/07/2014 08:05 SW-9045D- -
Calcium.Carbonate Equivalent 3.93 39300 100 JM 03/07/2014 13:09 AOAC.955.01
Total Volatile Solids 70.'03 700300 100:0 . JM : 03/11/2014 13:00 SM-2540G.;'
Total Molybdenum. 10 5 :KM. 03/07/201413:23 SW 601'0C
Total-Borori 62 3 KM 03/07/2014 13:23 SW 6010C -
Specific Gravity (standard units)1.2060 JM 03/07/2014 1159 ASTM DA298-85:
Comments:
NELAP ACCREDITED: VA NEI AC LAB: # 460014. PA NELAC_ LAB # 68-03109,_ FL NELAC. LAB #- E871087; NJ NELAC-LAB #•VA011..RESULTS REPORTED
MEET ALL REQUIREMENTS OF THE CURRENT:NELAC STANDARDS:. SPECIFIC, GRAVITY, SULFUR AND. ORGANIC -NITROGEN NOT. FOR COMPLIANCE
PURPOSES. - CCE FOR COMPLIANCE IN VIRGINIA AND PENNSYLVANIA ONLY.
:QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "K". ALL OTHER QC DATA IS ACCEPTABLE.
CUSTOMER REQUESTED TOTAL ALADDED-3111/14
All values are on a dry weight basis except as noted .by asterisk: Detection limit on all N series is on a wet basis.. .
Our re orts and letters are for the exclusive and confidential use'of our clients, and ma not be, reproduced in whole or part, nor may any reference.be made
P Y P _
toahe, work, the results, orthe companyin any advertising, news release, :or other public announcements without obtaining our prior written authorization:'
Debbie Holt-

CERTIFICATION
"I certify, under penalty of law, that the information that will be used todetermine compliance with. the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s). South Cross Bayou WRF Pelletizing Facility
Reporting Period: November 2014
Name: Mathew Busch4 Synagro
Signature: �� Date:01-December-2014
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The.temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503,33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process, shall.be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

TestAmerica �
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Tampa
6712 Benjamin Road
Suite 100
Tampa, FL 33634
Tel: [phone]
TestAmerica Job ID: 660-59272-1
Client Project/Site: Pinellas County Pelletizer
For:
Synagro Technologies, Inc.
Pinellas Pelletizer
5900 74th St. N.
St. Petersburg, Florida 33709
Attn: Matthew Busch
_d am
Authorized for release by:
212812014 3:46:23 PM
Amy Atkins, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

;;lent; Syriagro.Technofogies Inc:TestAinerica Job iD:-660-59272-1
roj6ctISite: Pinellas' County. Pelletizer .'
.,Ta,bIe,'.df Contefits:,
Cover Page • a .. ... .. :. ... ' ' ....... • o
�. Table of Contents :.
. y
2•
Fry .
Sample Summ ..y : :..
W f , _
..:....: • .. .
Case Narrative ; .. .... .... ...... .. .... . .
4
Definitions/Glossary . .:. .. .:..
:5 .
Detection Summary . • • .......• ..
6
. .
_Client Sample Results. ::
i
• . • • . ... •
..'
QC Sample Results : .... ::......:..: .:.
12
QC Association' Summary ...... - : •. • :.
18.'
Lab Chronicle'.. .. ....... .. ...... .......:.
21
IVlethod Summary:;
24
Certification Summary.:
:..
.
Chain of Custody : :.
27
• .. , ..:.:.
Receipt Checklists .: ....: .:. .. :.: ..
28.
.
.
� •.
Te Pa,
" 2
Page of 30
•
S�2128/2014 '

..,Sample Summary
Client: Synagro Technologies, Inc.
Project/Site: Pinellas County Pelletizer
Lob Sample W
Client Sample ID
Matrlx
660-59272-1
Synagro-1
Solid
660-59272-2
Synagro-2
Solid
660-59272-3
Synagro-3
Solid
660-59272-4
Synagro-4
Solid
660-59272-5
Synagro-5
Solid
TestAmenca Job ID: 660-59272-1
. IM
Collected
Received
/1408:53
02/21M 10:47
02/21/14 08:51
02121114 10:47
02/21/14 08:52
02/2t/14 10:47
02/21/14 08:50
02121/44 16:47
02/21/14 08:50
02/21/14 10:47
t.
TestAmerica Tampa
Page 3 of 30 .2/28/20.14

Case Narrative
Client: Synagro Technologies, Inc. TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
Job ID: 660-59272-1
Laboratory: TestAmerica Tampa
Narrative
Job Narrative
660-59272-1
Receipt
The samples were received on 2/21/2014 10:47 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 4.91 C.
GC/MS Semi VOA
Method 8270D: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for batch 107872 recovered
outside control limits for the following analyte: pyridine. This analyte was biased high in the LCS and was not detected in the associated
samples; therefore, the data have been reported.
Method 8270D: The matrix spike / matrix spike duplicate 660-59272-1(MS/MSD) recoveries for batch 107872 were below the lower control
limits for pyridine. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery was within
acceptance limits.
Method 8270D: Surrogate recovery for the following sample(s) was outside control limits: (660-59272-1 MS), (660-59272-1 MSD),
Synagro-4 (660-59272-4). Evidence of matrix interference is present; therefore, re -extraction and/or re -analysis was not performed.
Method 8270D: One of the surrogates, nitrobenzene-d5, in the method blank (MB) batch 107872 recovered below the lower control limit.
The surrogate recoveries for the lechate blank (LB) passed criteria.
GC Semi VOA
Method(s) 8082: The following sample(s) required a dilution due to the nature of the sample matrix: Synagro-2 (660-59272-2), Synagro-3
(660-59272-3), Synagro-4 (660-59272-4), Synagro-5 (660-59272-5). Because of this dilution, the surrogate spike concentration in the
sample was reduced to a level where the recovery calculation does not provide useful information.
Method(s) 8082: The following sample(s) was diluted due to the nature of the sample matrix: Synagro-2 (660-59272-2), Synagro-3
(660-59272-3), Synagro-4 (660-59272-4), Synagro-5 (660-59272-5). Elevated reporting limits (RLs) are provided.
No other analytical or quality issues were noted.
TestAmerica Tampa
Page 4 of 30 2/28/2014

Definitions/Glossary
Client: Synagro Technologies, Inc.
Project/Site: Pinellas County Pelletizer
Qualifiers
GUMS Semi VOA
Qualifier Qualifier Description
U Indicates that the compound was analyzed for but not detected.
J3 Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.
A Estimated value; value may not be accurate. Surrogate recovery outside of criteria.
The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
GC Semi VOA
Qualifier Qualifier Description
U Indicates that the compound was analyzed for but not detected.
D1 Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis
Metals
Qualifier Qualifier Description
U Indicates that the compound was analyzed for but not detected.
The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
Glossary
Abbrevilatton These commonly used abbreviations may or may not be present in this report.
■ Listed under the "D" column to designate that the result Is reported on a dry weight basis
°/aR Percent Recovery
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
oil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Job ID: 660-59272-1
Page 5 of 30
TestAmerica Tampa
2/28/2014

:.
Detection .
s
p
Client: Synagro Technologies, Inc.
.
TestAmerica Job 1p:'660-59272-1'
Project/Site: Pinellas County Pelletiaer
i
Client Sample ID: Synagr9=.1
Lab Sample I®: 660-59272=1-
Analyte
Result Qualifier
RL
PIDL Unit.
Dil Fee D Method Prep Type
_ Methyl Phenois,Total
0.71
0.050
0.020 mg/L
•1 . 8270D TCLP
3 & 4 Methylphenol
0.65
0.650
0.020 'mg/L
1 8270D TCLP
Barium
0.13 1.
6.50
0.030 mg/L
1 6010B TCLP
;
-;• Client Salnpie.ID: Synagro.-2.
Lab 'Sarnple. ID: 66.0=59272-2
Analyte
Result 'Qualifier
RL
MDL' Unit
Dil Fee D Method 'PrepType
Methyl Phenols,Toial
0.73
0.050
0.020 mg/L
1 82700 TCLP
-3 & 4 Methyiphenol
0.67
0.050
0.020 mg/L
1 8270D TCLP
Barium
0.23 1
0.50
0.030 mg/L
1 6010B TCLP
Client SaiTiple ID: Synagro,�3--------
---- -
T --
----- Lab Sample ID: 660-59272-3.
Analyte
Result Qualifier-
RL
MDL Unit
Dil Fac D Method Prep Type
Methyl Phenols,Total
0.72
0.050,
0.026. mg/L,
1 8270D TCLP,
3 & 4 Methylphenol
0.66
0.050
0.020 mg/L
1 8270D TCLP
Barium
0.099 I
0.50
0.030. mg/L
1 6010B TCLP
_
- .
Client Sample ID Synagr9-4
Lab.Sarnole ID: 66.0=59272-4
t
Anaiyte'
Result Qualifier
RL
MDL. Unit.
Dil Fab D Method Prep Type
Methyl Phenols,Total
0.75,
0.050.
0.020 mg/L
1 6270D TCLP
3 & 4 Methylphenol
0.69
0.050
0.020 . mg/L .
1 8270D TCLP
Barium
0.20 I ,
0.50
0.030 nig%L
1 - 60108. TCLP
Lead
0.21 1
1.0
0.040 mg/L
1 60106 TCLP
Client Sarnple ID: Synagro-5
--
------
Lab Sarnple ID::660-59272�5
Analyte
Result Qualifier
RL
MDL Unit
Dil Fac D Method Prep Type
Methyl Phenols,Total
0.73 T
0.050
0,020 mg/L
1 6270D TCLP
3 & 4 Methylphenol
0.67
0.050
0.020 mg/L
1 8270D TCLP .
Barium
0.10 1
0.50
0.030 mg/L
1 6010B TCLP
Lead
0,063 1
1:0 ..
0.040 mg/L
1 6010B TCLP •

Client Sample Results
Client: Synagro Technologies, Inc.
TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
-
- Client Sample ID: Synagro-1
Lab Sample ID: 660-59272-1
Date Collected: 02/21/14 08:53
Matrix: Solid
Date Received: 02/2111410:47
Method: 8270D - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
DO Fac
1,4-Dichlorobenzene
0.0085
U
0.050
0.0085
mg/L
02/26/14 10:00
02/27/14 23:19
1
2,4-Dinitrotoluene
0.0063
U
0.050
0.0063
mg/L
02/26/14 10:00
02/27/14 23:19
1
Hexachlorobenzene
0.015
U
0.050
0.015
mg/L
02/26/14 10:00
02/27/14 23:19
1
Hexachlorobutadiene
0.0085
U
0.050
0.0085
mg/L
02/26/14 10:00
02/27/14 23:19
1
Hexachioroethane
0.010
U
0,050
0.010
mg/L
02/26/14 10:00
02/27/14 23:19
1
Nitrobenzene
0.021
U
0.050
0.021
mg/L
02/26/14 10:00
02/27/14 23:19
1
Pentachlorophenol
0.017
U
0.25
0.017
mg/L
02/26/14 10:00
02/27/14 23:19
1
Pyridine
0.065
J3 U
0.25
0.065
mg/L
02/26/14 10:00
02/27/14 23:19
1
2,4,5-Trichlorophenol
0.024
U
0.050
0.024
mg/L
02/26/14 10:00
02/27114 23:19
1
2,4,6-Trichlorophenol
0,013
U
0.050
0.013
mg/L
02/26/14 10:00
02/27/14 23:19
1
Methyl Phenols,Total
0.71
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 23:19
1
2-Methylphenol
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 23:19
1
3 & 4 Methylphenol
0.65
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 23:19
1
Surrogate
%.Recovery
Qualifier
Limits
Prepared
Analyzed
Dif Fac
Nitrobenzene-d5 (Surr)
84
32 - 146
02126114 10:00
02127114 23:19
1
2-Fluorobiphenyl
82
34 - 141
02/26/14 10:00
02/27/14 23:19
1
Terphenyl-d14 (Surr)
43
10 - 160
0226114 10:00
02/27/14 23:19
1
Phenol-d5 (Surr)
105
18 - 110
02126114 10:00
0227114 23:19
1
2-Fluorophenol (Surr)
79
17 - 110
02/26/14 10:00
0227/14 23:19
1
2,4,6-Tribromophenol(Surr)
97
37-118
02/26/14 10:00
02/27/14 23:19
1
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
PCB-1016 - -
3.2 U
37
3.2
ug/Kg
-
02/24/14 12:39
02/28/14 05:34
1
PCB-1221
5.3 U
74
5.3
ug/Kg
02/24/14 12:39
02/28/14 05:34
1
PCB-1232
3.7 U
37
3.7
ug/Kg
02/24/14 12:39
02/28/14 05:34
1
PCB-1242
3.1 U
37
3.1
ug/Kg
02/24/14 12:39
02/28/14 05:34
1
PCB-1248
8.0 U
37
8.0
ug/Kg
02/24/14 12:39
02/28/14 05:34
1
PCB-1254
2.6 U
37
2.6
ug/Kg
02/24114 12:39
02/28/14 05:34
1
PCB-1260
7.4 U
37
7.4
ug/Kg
02/24/14 12:39
02/28/14 05:34
1
PCB-1268
1.9 U
37
1.9
ug/Kg
02/24/14 12:39
02/28114 05:34
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
11711 Fac
DCB Decachlorobiphenyl
61
54 - 133
0224114 12:39
02/28/14 05:34
1
Tetrachloro-m-xylene
90
46 - 130
02124114 12:39
0228/14 05:34
1
Method: 6010B - Metals (ICP) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
0.050 U
0.50
0.050
mg/L
02/25/14 11:30
02/26/14 08:54
1
Arsenic
0.12 U
1.0
0.12
mg/L
02/25/14 11:30
02/26/14 08:54
1
Barium
0.13 1
0.50
0.030
mg/L
02/25/14 11:30
02/26/14 08:54
1
Cadmium
0.018 U
0.50
0.018
mg/L
02/25/14 11:30
02/26/14 08:54
1
Chromium
0.050 U
1.0
0.050
mg/L
02/25/14 11:30
02/26/14 08:54
1
Lead
0.040 U
1.0
0.040
mg/L
02/25114 11:30
02/26/14 08:54
1
Selenium
0.15 U
0.50
0.15
mg/L
02/25/14 11:30
02/26/14 08:54
1
Method: 7470A - Mercury (CVAA) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
DII Fac
Mercury
0.00050 U
0.00070
0.00050
mg/L
02/26/14 09:26
02/26/14 13:36
1
TestAmerica Tampa
Page 7 of 30 2/28/2014

Client Sample Results
Client: Synagro Technologies, Inc.
TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
Client Sample ID: Synagro-2
Lab Sample ID: 660-59272-2
Date Collected: 112121114 08:51
Matrix: Solid
Date Received: 02/21/1410:47
-
Method: 8270D - Semivolatile Organic Compounds
(GC/MS) - TCLP
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,4-Dichlorobenzene
0.0085
U
0.050
0.0085
mg/L
62/26/14 10:00
02/27/14 23:47
1
2,4-Dinitrotoluene
0.0063
U
0.050
0.0063
mg/L
02/26/14 10:00
02/27/14 23:47
1
Hexachlorobenzene
0.015
U
0.050
0.015
mg/L
02/26/14 10:00
02/27/14 23:47
1
Hexachlorobutadiene
0.0085
U
0.050
0.0085
mg/L
02/26/14 10:00
02/27/14 23:47
1
Hexachloroethane
0.010
U
0.050
0.010
mg/L
02/26/14 10:00
02t27/14 23:47
1
Nitrobenzene
0.021
U
0.050
&021
mg/L
02/26/14 10:00
02/27/14 23:47
1
Pentachlorophenol
0.017
U
0.25
0.017
mg/L
02/26/14 10:00
02/27/14 23:47
1
Pyridine
0.065
J3 U
0.25
0.065
mg/L
02/26/14 10:00
02/27/14 23:47
1
2,4,5-Trichlorophenol
0.024
U
0,050
0.024
mg/L
02/26/14 10:00
02/27/14 23:47
1
2,4,6-Trichlorophenol
0.013
U
0.050
0.013
mg/L
02/26/14 10:00
02/27/14 23:47
1
Methyl Phenols,Total
0.73
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 23:47
1
2-Methylphenol
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 23:47
1
3 & 4 Methylphenol
0.67
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 23:47
1
Surrogate
1Y..Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
Nitrobenzene-d5 (Surr)
68
32 - 146
02126114 10:00
02/27/14 23:47
1
2-Fluorobiphenyl
69
34 - 141
02126114 10:00
02127114 23:47
1
Terphenyl-d M (Surr)
49
10 - 160
02126114 10:00
02127114 23:47
1
Phenol-d5 (Surr)
101
18 - 110
02/26/14 10:00
02127114 23:47
1
2-Fluorophenol (Surr)
71
17 - 110
02126114 10:00
02/27/14 23:47
1
2,4,6-Tribromophenol (Surr)
91
37- 118
02/26/14 10:00
02/27/14 23:47
1
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Anafyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
PCB-1016
32 U
360
32
ug/Kg
02/24/14 12:39
02/28/14 07:51
10
PCB-1221
53 U
740
53
ug/Kg
02/24/14 12:39
02/28/14 07:51
10
PCB-1232
36 U
360
36
ug/Kg
02/24/14 12:39
02/28/14 07:51
10
PCB-1242
31 U
360
31
ug/Kg
02/24/14 12:39
02/28/14 07:51
10
PCB-1248
80 U
360
80
ug/Kg
02124/14 12:39
02/28/14 07:51
10
PCB-1254
25 U
360
25
ug/Kg
02/24/14 12:39
02/28/14 07:51
10
PCB-1260
74 U
360
74
ug/Kg
02/24/14 12:39
02/28/14 07:51
10
PCB-1268
19 U
360
19
ug/Kg
02/24/14 12:39
02/28/14 07:51
10
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
DU Fac
DCB Decachlorobiphenyl
0 D1
54 - 133
02124114 12:39
02128114 07:51
10
Tetrachloro-m-xylene
0 D1
46 - 130
02/24/14 12:39
02128114 07:51
10
Method: 6010B - Metals (ICP) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Silver
0.050 U
0.50
0.050
mg/L
02/25/14 11:30
02/26/14 08:58
1
Arsenic
0.12 U
1.0
0.12
mg/L
02/25/14 11:30
02/26/14 08:58
1
Barium
0.23 1
0.50
0.030
mg/L
02/25/14 11:30
02/26/14 08:58
1
Cadmium
0.018 U
0.50
0.018
mg/L
02/25/14 11:30
02/26/14 08:58
1
Chromium
0.050 U
1.0
0.050
mg/L
02/25/14 11:30
02/26/14 08:58
1
Lead
0.040 U
1.0
0.040
mg/L
02/25/14 11:30
02/26/14 08:58
1
Selenium
0.15 U
0.50
0.15
mg/L
02/25/14 11:30
02/26/14 08:58
1
Method: 7470A - Mercury (CVAA) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Mercury0.00050 U
0.00070
0.00050
mg/L
02/26/14 09:26
02/26/14 13:37
1
TestAmerica Tampa
Page 8 of 30 2/28/2014

Client Sample Results
Client: Synagro Technologies, Inc. TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
Client Sample ID: Synagro-3 Lab Sample ID: 660-59272-3
Date Collected: 02/21/14 08:52 Matrix: Solid
Date Received: 02/21/1410:47
Method: 8270D - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
DU Fac ,
1,4-Dichlorobenzene
0.0085
U
0.050
0.0085
mg/L
02/26/14 10:00
02/28/14 00:17
1
2,4-Dinitrotoluene
0.0063
U
0.050
0.0063
mg/L
02/26/14 10:00
02/28/14 D0:17
1
Hexachlorobenzene
0.015
U
0.050
0.015
mg/L
02/26/14 10:00
02/28/14 DO:17
1
Hexachlorobutadiene
0.0085
U
0.050
0.0085
mg/L
02/26114 10:00
02/28/14 00:17
1
Hexachloroethane
0.010
U
0.050
0.010
mg/L
02/26/14 10:00
02/28/14 00:17
1
Nitrobenzene
0.021
U
0.050
0.021
mg/L
02/26/14 10:00
02128/14 00:17
1
Pentachlorophenol
0.017
U
0.25
0.017
mg/L
02/26/14 10:00
02/28/14 00:17
1
Pyridine
0.065
J3 U
0.25
0.065
mg/L
02/26/14 10:00
02/28/14 00:17
1
2,4,5-Trichlorophenol
0.024
U
0.050
0.024
mg/L
02126/14 10:00
02/28/14 00:17
1
2,4,6-Trichlorophenol
0.013
U
0.050
0.013
mg/L
02/26/14 10:00
02/28/14 00:17
1
Methyl Phenols,Total
0.72
0.050
0,020
mg/L
02/26/14 10:00
02/28/14 00:17
1
2-Methylphenol
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/28/14 00:17
1
3 & 4 Methylphenol
0.66
0.050
0.020
mg/L
02/26/14 10:00
02/28/14 00:17
1
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
Nitrobenzene-d5 (Surr)
74
32 - 146
D 6/14 10:00
ODQ /14 00:17
1
2-Fluorobiphenyl
67
34 - 141
02/26/14 10:00
02128114 00:17
1
Terphenyl-d 14 (Surr)
40
10 - 160
02126114 10:00
02/28/14 00:17
1
Phenol-d5 (Surr)
105
18 - 110
02126,114 10:00
02/28/14 00:17
1
2-Fluorophenol (Surr)
77
17 - 110
02/26/14 10:00
02/28/14 00:17
1
2,4,6-Tribromophenol (Surr)
88
37 - 118
02/26/14 10:00
021128114 00:17
1
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Ana"
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
PCB-1016
32 U
360
32
ug/Kg
02/24/14 12:39
02/28/14 08:14
10
PCB-1221
53 U
740
53
ug/Kg
02t24/14 12:39
02/28/14 08:14
10
PCB-1232
36 U
360
36
ug/Kg
02/24/14 12:39
02/28/14 08:14
10
PCB-1242
31 U
360
31
ug/Kg
02/24/14 12:39
02/28/14 08:14
10
PCB-1248
80 U
360
80
ug/Kg
02/24/14 12:39
02/28/14 08:14
10
PCB-1254
25 U
360
25
ug/Kg
02/24114 12:39
02/28/14 08:14
10
PCB-1260
74 U
360
74
ug/Kg
02/24/14 12:39
02/28/14 08:14
10
PCB-1268
19 U
360
19
ug/Kg
02/24/14 12:39
02/28/14 08:14
10
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
0 D1
54 - 133
02124114 12:39
02128114 08:14
10
Tetrachloro-m-xylene
0 D1
46 - 130
02124114 12:39
02,28/14 08:14
10
Method: 6010E - Metals (ICP) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Silver
0.050 U
0.50
0.050
mg/L
02/25/14 11:30
02/26/14 09:01
1
Arsenic
0.12 U
1.0
0.12
mg/L
02/25/14 11:30
02/26/14 09:01
1
Barium
0.099 1
0.50
0.030
mg/L
02/25/14 11:30
02/26/14 09:01
1
Cadmium
0.018 U
0.50
0,018
mg/L
02/25/14 11:30
02/26/14 09:01
1
Chromium
0.050 U
1.0
0.050
mg/L
02125/14 11:30
02/26/14 09:01
1
Lead
0.040 U
1.0
0.040
mg/L
02/25/14 11:30
02/26114 09:01
1
Selenium
0.15 U
0.50
0.15
mg/L
02/25/14 11:30
02/26/14 09:01
1
Method: 7470A - Mercury
(CVAA) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Mercury
0.00050 U
0.00070
0.00050
mg/L
02/26/14 09:26
02/26/14 13:43
1
TestAmerica Tampa
Page 9 of 30 2/28/2014

Client Sample Results
Client: Synagro Technologies, Inc.
TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
Client Sample ID: Synagro-4
Lab Sample ID: 660-59272-4
Date Collected: 02/21/14 08:50
Matrix: Solid
Date Received: 02/21/14 10:47
Method: 8270D - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,4-Dichlorobenzene
0.0085
U
0.050
0.0085
mg/L
02/2611410:00
02/2811400:45
1
2,4-Dinitrotoluene
0.0063
U
0.050
0,0063
mg/L
02/26/14 10:00
02/28/14 00:45
1
Hexachlorobenzene
0.015
U
0.050
0.015
mg/L
02t26/14 10:00
02/28/14 00:45
1
Hexachlorobutadiene
0.0085
U
0.050
0.0085
mg/L
02/26/14 10:00
02/28/14 00:45
1
Hexachloroethane
0.010
U
0.050
0.010
mg/L
02/26/14 10:00
02128/14 00:45
1
Nitrobenzene
0.021
U
0.050
0.021
mg/L
02/26/14 10:00
02/28/14 00:45
1
Pentachlorophenol
0.017
U
0.25
0.017
mg/L
02/26/14 10:00
02/28/14 00:45
1
Pyridine
0,065
J3 U
0.25
0.065
mg/L
02/26/14 10:00
02/28/14 00:45
1
2,4,5-Trichlorophenol
0.024
U
0.050
0.024
mg/L
02/26/14 10:00
02/28/14 00:45
1
2,4,6-Trichlorophenol
0.013
U
0.050
0.013
mg/L
02/26/14 10:00
02/28/14 00:45
1
Methyl Phenols,Total
0.75
0.050
0.020
mg/L
02/26/14 10:00
02/28/14 00:45
1
2-Methylphenol
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/28/14 00:45
1
3 & 4 Methylphenol
0.69
0.050
0.020
mg/L
02/26114 10:00
02/28/14 00:45
1
Surrogate
%Recovery
QuaIIHer
Limits
Prepared
Analyzed
Dil Fac
Nitrobenzene-d5 (Surr)
80
32- 146
02126114 10:00
02/28H4 00:45
1
2-Fluorobiphenyl
76
34 - 141
02/26/14 10:00
02128114 00:45
1
Terphenyl-d14 (Surr)
45
10 - 160
02/26/14 10:00
02128114 00:45
1
Phenol-d5 (Surr)
126
Jl
18 - 110
02126114 10:00
02128114 00:45
1
2-Fluorophenot (Surr)
84
17.110
02/26/14 10:00
02/28/14 00:45
1
2,4, 6-Tribromophenol (Surr)
92
37 - 118
02/26/14 10:00
02/28/l4 00:45
1
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
PCB-1016
32 U
360
32
ug/Kg
02/24/14 12:39
02/28/14 08:37
10
PCB-1221
53 U
740
53
ug/Kg
02/24/14 12:39
02/28/14 08:37
10
PCB-1232
36 U
360
36
ug/Kg
02/24/14 12:39
02/28/14 08:37
10
PCB-1242
31 U
360
31
ug/Kg
02/24/14 12:39
02/28/14 08:37
10
PCB-1248
79 U
360
79
ug/Kg
02/24/14 12:39
02/28/14 08:37
10
PCB-1254
25 U
360
25
ug/Kg
02124/14 12:39
02/28/14 08:37
10
PCB-1260
74 U
360
74
ug/Kg
02t24114 12:39
02/28/14 08:37
10
PCB-1268
19 U
360
19
ug/Kg
02/24/14 12:39
02/28/14 08:37
10
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
0 D1
54 - 133
02124114 12:39
02/28/14 08:37
10
Tetrachloro-m-xylene
0 D1
46 - 130
02124114 12:39
02/28/14 08:37
10
Method: 6010E - Metals (ICP) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Silver
0.050 U
0.50
0.050
mg/L
02/25/14 11:30
02/26114 09:05
1
Arsenic
0,12 U
1.0
0.12
mg/L
02/25/14 11:30
02/26/14 09:05
1
Barium
0.20 1
0.50
0.030
mg/L
02125/14 11:30
02/26/14 09:05
1
Cadmium
0.018 U
0.50
0.018
mg/L
02t25/14 11:30
02/26/14 09:05
1
Chromium
0.050 U
1.0
0.050
mg/L
02/25/14 11:30
02/26/14 09:05
1
Lead
0.21 1
1.0
0,040
mg/L
02/25/14 11:30
02/26/14 09:05
1
Selenium
0.15 U
0.50
0.15
mg/L
02/25/14 11:30
02/26/14 09:05
1
Method: 7470A - Mercury
(CVAA) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Mercury
0.00050 U
0.00070
0.00050
mg/L
02126/14 09:26
02126/14 13:44
1
TestAmerica Tampa
Page 10 of 30 2/28/2014

Client Sample Results
Client: Synagro Technologies, Inc.
TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
Client Sample ID: Synagro 5
---- --.._- ..
Lab Sample ID: 660-59272-5
Date Collected: 02/21/14 08:50
Matrix: Solid
Date Received: 02/21/14 10:47
--------------- ..._..__
Method: 8270D - Semivolatile Organic
Compounds
(GC/MS) - TCLP
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,4-Dichlorobenzene
0.0085
U
0.050
0.0085
mg/L
02/26114 10:00
02/28/14 01:15
1
2,4-Dinitrotoluene
0.0063
U
0.050
0.0063
mg/L
02/26/14 10:00
02/28/14 01:15
1
Hexachlorobenzene
0.015
U
0.050
0.015
mg/L
02/26/14 10:00
02/28/14 01:15
1
Hexachlorobutadiene
0.0085
U
0.050
0.0085
mg/L
02126/14 10:00
02/28/14 01:15
1
Hexachloroethane
0.010
U
0.050
0.010
mg/L
02/26/14 10:00
02/28/14 01:15
1
Nitrobenzene
0.021
U
0.050
0,021
mg/L
02/26/14 10:00
02/28/14 01:15
1
Pentachlorophenol
0.017
U
0.25
0.017
mg/L
02/26/14 10:00
02/28/14 01:15
1
Pyridine
0.065
J3 U
0.25
0.065
mg/L
02/26/14 10:00
02/28/14 01:15
1
2,4,5-Trichlorophenol
0.024
U
0.050
0.024
mg/L
02/26114 10:00
02/28/14 01:15
1
2,4,6-Trichlorophenol
0.013
U
0.050
0.013
mg/L
02/26/14 10:00
02/28/14 01:15
1
Methyl Phenols,Total
0.73
0.050
0.020
mg/L
02/26/14 10:00
02/28/14 01:15
1
2-Methylphenol
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/28/14 01:15
1
3 & 4 Methylphenol
0.67
0.050
0.020
mg/L
02/26/14 10:00
02/28/14 01:15
1
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
DU Fac
Nitrobenzene-d5 (Surr)
79
32 - 146
0226/14 10.00
02/28/14 01:15
1
2-Fluorobiphenyl
73
34 - 141
02126,114 10:00
02/28/14 01:15
1
Terphenyl-d14 (Surr)
43
10- 160
02126114 10:00
02128114 01:15
1
Phenol-d5 (Surr)
108
18 - 110
02126114 10:00
02/28/14 01:15
1
2-Fluorophenol (Surr)
78
17 - 110
02126114 10:00
02/28✓14 01:15
1
2,4,6-Tribromophenol (Sun')
94
37 - 118
02126114 10:00
02128114 01:15
1
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
PCBA016
32 U
360
32
ug/Kg
*
02/2411412:39
02/2811409:00
10
PCB-1221
53 U
740
53
ug/Kg
*
02/24/14 12:39
02/28/14 09:00
10
PCB-1232
36 U
360
36
ug/Kg
0
02/24/14 12:39
02/28/14 09:00
10
PCB-1242
31 U
360
31
ug/Kg
*
02/24/14 12:39
02/28/14 09:00
10
PCB-1248
80 U
360
80
ug/Kg
02/24/14 12:39
02/28/14 09:00
10
PCB-1254
25 U
360
25
ug/Kg
0
02/24/14 12:39
02/28/14 09:00
10
PCB-1260
74 U
360
74
ug/Kg
*
02/24/14 12:39
02/28/14 09:00
10
PCB-1268
19 U
360
19
ug/Kg
0
02/24/14 12:39
02/28/14 09:00
10
Surrogate
%Recovery Qualifier
Llmlts
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
0 D1
54 - i33
0224/14 12:39
0228/14 09:00
10
Tetrachloro-m-xylene
0 D1
46.130
0224114 12:39
02/28/14 09:00
10
Method: 6010B - Metals (ICP) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
0.050 U
0.50
0.050
mg/L
02/25/14 11:30
02/26/14 09:15
1
Arsenic
0.12 U
1.0
0.12
mg/L
02/25/14 11:30
02/26/14 09:15
1
Barium
0,10 1
0.50
0.030
mg/L
02/25/14 11:30
02/26/14 09:15
1
Cadmium
0.018 U
0.50
0.018
mg/L
02/25/14 11:30
02/26/14 09:15
1
Chromium
0.050 U
1.0
0.050
mg/L
02/25/14 11:30
02/26/14 09:15
1
Lead
0.063 1
1.0
0.040
mg/L
02/25/14 11:30
02/26/14 09:15
1
Selenium
0.15 U
0.50
0.15
mg/L
02/25/14 11:30
02/26/14 09:15
1
Method: 7470A - Mercury (CVAA) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.00050 U
0.00070
0.00050
mg/L
02/26/14 09:26
02r26/14 13:46
1
TestAmerica Tampa
Page 11 of 30 2/28/2014

QC Sample Results
Client: Synagro Technologies, Inc.
Project/Site: Pinellas County Pelletizer
Method 8270D - Semivolatile Organic Compounds (GC/MS)
TestAmerica Job ID: 660-59272-1
Lab Samp!e ID: MB 640-10787211-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 107920
Prep Batch:
107872
MB
MB
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,4-Dichlorobenzene
0.0085
U
0,050
0.0085
mg/L
02126/1410:00
02/27/14 20:21
1
2,4-Dinitrotoluene
0.0063
U
0.050
0.0063
mg/L
02/26/14 10:00
02/27/14 20:21
1
Hexachlorobenzene
0,015
U
0.050
0.015
mg/L
02/26/14 10:00
02/27/14 20:21
1
Hexachlorobutadiene
0,0085
U
0.050
0.0085
mg/L
02/26/14 10:00
02/27/14 20:21
1
Hexachloroethane
0.010
U
0.050
0.010
mg/L
02/26/14 10:00
02/27/14 20:21
1
Nitrobenzene
0.021
U
0.050
0.021
mg/L
02/26/14 10:00
02127/14 20:21
1
Pentachlorophenol
0.017
U
0.25
0.017
mg/L
02/26/14 10:00
02127114 20:21
1
Pyridine
0.065
U
0.25
0.065
mg/L
02/26/14 10:00
02/27/14 20:21
1
2,4,5-Trichlorophenol
0.024
U
0.050
0.024
mg/L
02/26/14 10:00
02/27/14 20:21
1
2,4,6-Trichlorophenol
0.013
U
0.050
0.013
mg/L
02/26/14 10:00
02/27/14 20:21
1
Methyl Phenols,Total
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 20:21
1
2-Methylphenol
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 20:21
1
3 & 4 Methylphenol
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 20:21
1
MB
MB
Surrogate
Y.Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
Nitrobenzene-i:15 (Surr)
22
J1
32 - 146
02126114 10:00
02127114 20:21
1
2-Fluorobiphenyl
79
34 - 141
02126114 10:00
02127114 20:21
1
Terphenyl-d 14 (Surr)
86
10 - 160
02126114 10:00
02,27114 20:21
1
Phenol-d5 (Surr)
69
18 - 110
02/26/14 10:00
02127114 20:21
1
2-Fluorophenol (Surr)
82
17 - 110
02126114 10:00
02127114 20:21
1
2,4,6-Tribromophenol (Surr)
79
37- 118
02126114 10.00
02127114 20:21
1
Lab Sample ID: LCS 640-107872/3-A
Client Sample ID: Lab Control
Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 107920
Prep Batch:
107872
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,4-Dichlorobenzene
0.250
0.220
mg/L
88
21 - 100
2,4-Dinitrotoluene
0.250
0.240
mg/L
96
72 - 118
Hexachlorobenzene
0.250
0.235
mg/L
94
71.109
Hexachlorobutadiene
0.250
0.225
mg/L
90
10 - 100
Hexachloroethane
0,250
0.210
mg/L
84
10 - 100
Nitrobenzene
0.250
0.233
mg/L
93
58 - 119
Pentachlorophenol
0.500
0,416
mg/L
83
22 - 138
Pyridine
0.250
0.195 1
mg/L
78
10 - 100
2,4,5-Trichlorophenol
0.250
0.244
mg/L
98
60 - 115
2,4,6-Trichlorophenol
0.250
0.231
mg/L
92
57 - 115
2-Methylphenol
0.250
0.205
mg/L
82
46 - 101
3 & 4 Methylphenol
0.250
0.205
mg/L
82
23.138
LCS LCS
Surrogate Y.Recovery Qualifier
Limits
Nitrobenzene-d5 (Surr)
102
32 - 146
2-Fluorobiphenyl
84
34 - 141
Terphenyl-d14 (Surr)
84
10- 160
Phenol-d5 (Surr)
99
18 - 110
2-Fluorophenol (Surr)
83
17 - 110
2,4,6-Tribromophenol (Surr)
89
37- 118
TestAmerica Tampa
Page 12 of 30 2/28/2014

QC Sample Results
Client: Synagro Technologies, Inc.
Project/Site: Pinellas County Pelletizer
Method 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 640-10787214-A
Matrix: Solid
Analysis Batch: 107920
Analyte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2-Methylphenol
3 & 4 Methylphenol
Surrogate
Nitrobenzene-d5 (Surr)
2-Fluorobiphenyl
Terphenyl-d14 (Surr)
Phenol-d5 (Surr)
2-Fluorophenol (Surr)
2,4,6-Tribromophenol (Surr)
LCSD LCSD
%Recovery Qualifier
84
83
84
91
86
88
Spike
Added
0.250
0.250
0.250
0.250
0.250
0.250
0.500
0.250
0.250
0.250
0.250
0.250
Limits
32 - 146
34 - 141
10-160
18 - 110
17 - 110
37 - 118
LCSD LCSD
Result Qualifier
0.216
0.248
0.235
0.208
0.222
0.201
0.438
0.262 J3
0.233
0.235
0.207
0.205
TestAmerica Job ID: 660-59272-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 107872
%Rec.
RPD
Unit
D %Rec
Limits
RPD
Limit
mg/L
87
21 - 100
2
33
mg/L
99
72 - 118
3
32
mg/L
94
71 - 109
0
20
mg/L
83
10-100
8
30
mg/L
89
10-100
5
50
mg/L
81
58 - 119
15
25
mg/L
88
22 - 138
5
40
mg/L
105
10 - 100
29
40
mg/L
93
60 - 115
5
37
mg/L
94
57 - 115
2
35
mg/L
83
46 - 101
1
40
mg/L
82
23. 138
0
44
Lab Sample ID: LB 640-10785511-B
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 107920
Prep Batch:
107872
LB
LB
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
-
1,4-Dichlorobenzene
0.0085
U
0.050
--
0.0085
-
mg/L
-
02r16/1410:00
02/27/1420:52
1
2,4-Dinitrotoluene
0.0063
U
0.050
0.0063
mg/L
02/26/14 10:00
02/27/14 20:52
1
Hexachlorobenzene
0.015
U
0.050
0.015
mg/L
02/26/14 10:00
02/27/14 20:52
1
Hexachlorobutadiene
0.0085
U
0.050
0.0085
mg/L
02/26/14 10:00
02/27/14 20:52
1
Hexachloroethane
0.010
U
0.050
0.010
mg/L
02/26/14 10:00
02/27/14 20:52
1
Nitrobenzene
0.021
U
0.050
0.021
mg/L
02/26/14 10:00
02/27/14 20:52
1
Pentachlorophenol
0.017
U
0.25
0.017
mg/L
02/26/14 10:00
02/27/14 20:52
1
Pyridine
0.065
U
0.25
0.065
mg/L
02/26/14 10:00
02/27/14 20:52
1
2,4,5-Trichlorophenol
0.024
U
0.050
0.024
mg/L
02/26/14 10:00
02/27/14 20:52
1
2,4,6-Trichlorophenol
0.013
U
0.050
0.013
mg/L
02/26/14 10:00
02/27/14 20:52
1
Methyl Phenols,Total
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 20:52
1
2-Methylphenol
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 20:52
1
3 & 4 Methylphenol
0.020
U
0.050
0.020
mg/L
02/26/14 10:00
02/27/14 20:52
1
LB
LB
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
Ntrobenzene-d5 (Surr)
63
32 - 146
02/26/14 10:00
02/27/14 20:52
1
2-Fluorobiphenyl
78
34 - 141
02/26/14 10:00
02127114 20:52
1
Terphenyi-d14 (Surr)
88
10- 160
02/26/14 10:00
02/27/14 20.52
1
Phenol-d5 (Surr)
71
18 - 110
02126114 10:00
02/27/14 20:52
1
2-Fluorophenol (Surr)
62
17 - 110
02126114 10:00
02127114 20:52
1
2,4,6-Tribromophenol (Surr)
83
37 - 116
02126114 10:00
02/27/14 20:52
1
Page 13 of 30
TestAmerica Tampa
2/28/2014

QC Sample Results
Client: Synagro Technologies, Inc. TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 660-59272-1 MS
Client Sample ID: Synagro-1
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 107920
Prep Batch: 107872
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
1,4-Dichlorobenzene
0.0085 U
0.250
0.196
mg/L
78
27 - 135
2,4-Dinitrotoluene
0.0063 U
0.250
0.257
mg/L
103
38 - 135
Hexachiorobenzene
0.015 U
0.250
0.230
mg/L
92
45 - 135
Hexachlorobutadiene
0.0085 u
0.250
0.228
mg/L
91
27.135
Hexachloroethane
0.010 U
0.250
0.199
mg/L
80
26.135
Nitrobenzene
0.021 U
0.250
0.225
mg/L
90
45.135
Pentachlorophenol
0.017 U
0.500
0.521
mg/L
104
24 - 135
Pyridine
0.065 J3 U
0.250
0.065 J3 U
mg/L
0
45 - 135
2,4,5-Trichlorophenol
0.024 U
0.250
0.279
mg/L
111
45 - 135
2,4,6-Trichlorophenol
0.013 U
0.250
0.266
mg/L
107
45 - 135
2-Methylphenol
0.020 U
0.250
0.229
mg/L
91
34 - 135
3 & 4 Methylphenol
0.65
0.250
0.932
mg/L
113
30 - 135
MS MS
Surrogate
%Recovery Qualifter
Limits
Nitrobenzene-d5 (Surr)
94
32.146
2-Fluorobiphenyl
88
34 - 141
Terphenyl-04 (Surr)
43
10- 160
Phenol-d5 (Surr)
115 Jl
18 - 110
2-Fluorophenol (Surr)
90
17 - 110
2,4,6-Tribromophenol (Surr)
105
37.118
Lab Sample ID: 660-59272-1 MSD
Client Sample ID: Synagro-1
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 107920
Prep Batch: 107872
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D SGRec
Limits RPD Limit
1,4-Dichlorobenzene
0.0085 U
0.250
0.201
mg/L
60
27 - 135 2 40
2,4-Dinitrotoluene
0.0063 U
0.250
0.235
mg/L
94
38 - 135 9 40
Hexachlorobenzene
0.015 U
0.250
0.220
mg/L
88
45 - 135 4 40
Hexachlorobutadiene
0.0085 U
0.250
0.217
mg/L
87
27 - 135 5 40
Hexachloroethane
0,010 U
0.250
0.188
mg/L
75
26 - 135 5 40
Nitrobenzene
0.021 U
0,250
0.211
mg/L
84
45 - 135 7 40
Pentachlorophenol
0.017 U
0,500
0.477
mg/L
95
24 - 135 9 40
Pyridine
0.065 J3 U
0.250
0.065 J3 U
mg/L
0
45 - 135 NC 40
2,4,5-Trichlorophenol
0.024 U
0.250
0.271
mg/L
109
45 - 135 3 40
2,4,6-Trichlorophenol
0.013 U
0.250
0.263
mg/L
105
45 - 135 1 40
2-Methylphenol
0.020 U
0.250
0.235
mg/L
94
34 - 135 3 40
3 & 4 Methylphenol
0.65
0,250
0.938
mg/L
115
30 - 135 1 40
MSD MSD
Surrogate
'/.Recovery Qua/Ker
UnI is
Nitrobenzene-d5 (Surr)
86
32 - 146
2-Fluorobiphenyl
91
34 - 141
Terphenyl-d 14 (Surr)
41
10 - 160
Phenol-d5 (Surr)
118 J1
18 - 110
2-Fluorophenol (Surr)
89
17 - 110
2,4,6-Tribromophenol (Surr)
103
37- 118
TestAmerica Tampa
Page 14 of 30 2/28/2014

QC Sample Results
Client: Synagro Technologies, Inc.
TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: MB 680-316932113-A
Client Sample
ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 317335
Prep Batch: 316932
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
PCB-1016
2.9 U
33
2.9 ug/Kg
02/24/14 12:39
02/26/14 16:27 1
PCB-1221
4.8 U
67
4.8 ug/Kg
02/24/14 12:39
02/2611416:27 1
PCB-1232
3.3 U
33
3.3 ug/Kg
0212411412:39
02/26/1416:27 1
PCB-1242
2.8 U
33
2.8 ug/Kg
02/2411412:39
02/26/1416:27 1
PCB-1248
7.2 U
33
7.2 ug/Kg
02124/1412:39
02/26/1416:27 1
PCB-1254
2.3 U
33
2.3 ug/Kg
02/24/14 12:39
02/26/14 16:27 1
PCB-1260
6.7 U
33
6.7 ug/Kg
02/2411412:39
02/26/1416:27 1
PCB-1268
1.7 U
33
1.7 ug/Kg
02/24/14 12:39
02/26/1416:27 1
MB MB
Surrogate %.Recovery Qualifier
Limits
Prepared
Analyzed DU Fac
DCB Decachlorobiphenyl
100
54 - 133
02/24/14 12:39
02/26/14 16:27 1
Tetrachloro-m-xylene
95
46- 130
02124114 12:39
02/26/14 16:27 1
Lab Sample ID: LCS 680-316932114-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 317335
Prep Batch: 316932
Spike
LCS
LCS
•kRec.
Analyte
Added
Result
Qualifier
Unit
D •kRec
Limits
PCBA 016
332
282
ug/Kg
85
43 - 130
PCB-1260
332
303
ug/Kg
91
45 - 130
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
DCB Decachlorobiphenyl 101
54 - 133
Tetrachloro-m-xylene 92
46 - 130
Method: 6010B - Metals (ICP)
Lab Sample ID: LCS 660-14646912-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 146501
Prep Batch: 146469
Spike
LCS
LCS
XRec.
Analyte
Added
Result
Qualifier
Unit
D XRec
Limits
Silver
5.00
5.25
mg/L
105
75.125
Arsenic
5.00
5.21
mg/L
104
75 - 125
Barium
5.00
5.03
mg/L
101
75 - 125
Cadmium
5.00
5.14
mg/L
103
75 - 125
Chromium
5.00
5.16
mg/L
103
75 - 125
Lead
5.00
4.96
mg/L
99
75 - 125
Selenium
5.00
5.15
mg/L
103
75 - 125
Lab Sample ID: LCSD 660-146469/3-A
Client
Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 146501
Prep Batch: 146469
Spike
LCSD
LCSD
XRec. RPD
Analyte
Added
Result
Qualifier
Unit
D `kRec
Limits RPD Limit
Silver
5.00
5.24
mg/L
105
75.125 0 20
Arsenic
5.00
5.21
mg/L
104
75- 125 0 20
TestAmerica Tampa
Page 15 of 30
2/28/2014

QC Sample Results
Client: Synagro Technologies, Inc.
Project/Site: Pinellas County Pelletizer
Method: 6010B - Metals (ICP) (Continued)
Lab Sample ID: LCSD 660-14646913-A
Matrix: Solid
Analysis Batch: 146501
Spike
Analyte
Added
Barium
5.00
Cadmium
5.00
Chromium
5.00
Lead
5.00
Selenium
5.00
Lab Sample ID: LB 660-146460/1-B
Matrix: Solid
Analysis Batch: 146501
Analyte
Silver
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Lab Sample ID: 640-46879-A-1-C MS
Matrix: Solid
Analysis Batch: 146501
TestAmerica Job ID: 660-59272-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 146469
LCSD LCSD
%Rec. RPD
Result Qualifier
Unit
D %Rec
Limits RPD Limit
5.00
mg/L
100
75 - 125 1 20
5.14
mg/L
103
75 - 125 0 20
5A7
mg/L
103
75 _ 125 0 20
4.97
mg/L
99
75. 125 0 20
5.19
mg/L
104
75 - 125 1 20
LB
LB
Result
Qualifier
RL
MDL
Unit
0.050
U
0.50
0.050
mg/L
0.12
U
1.0
0.12
mg/L
0.030
U
0.50
0.030
mg/L
0.018
U
0.50
0.018
mg/L
0.050
U
1.0
0.050
mg/L
0.040
U
1.0
0.040
mg/L
0.15
U
0.50
0.15
mg/L
Sample Sample
Analyte
Result Qualifier
Silver
0.050 U
Arsenic
0.12 U
Barium
0.20 1
Cadmium
0.018 U
Chromium
0.050 U
Lead
0.048 1
Selenium
0.15 U
Lab Sample ID: 640-46879-A-1-D MSD
Matrix: Solid
Analysis Batch: 146501
Sample Sample
Analyte
Result Qualifier
Silver
0.050 U
Arsenic
0.12 U
Barium
0.20 1
Cadmium
0.018 U
Chromium
0.050 U
Lead
0.048 1
Selenium
0.15 U
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 146469
D Prepared
Analyzed
Dil Fac
02/25/14 11.30
02/26/14 08:17
1
02/25/14 11:30
02/26/14 08:17
1
02/25/14 11:30
02/26/14 08:17
1
02/25/14 11:30
02/26/14 08:17
1
02/25/14 11:30
02/26/14 08:17
1
02/25/14 11:30
02/26/14 08:17
1
02/25/14 11:30
02/26/14 08:17
1
Client Sample ID: Matrix Spike
Prep Type: TCLP
Prep Batch: 146469
Spike
MS MS
%Rec.
Added
Result Qualifier
Unit
D %Rec
Limits
5.00
5.26
mg/L
105
75 - 125
5.00
5.16
mg/L
103
75. 125
5.00
5.28
mg/L
102
75. 125
5.00
5.04
mg/L
101
75 - 125
5.00
5.12
mg/L
102
75 - 125
5.00
4.95
mg/L
98
75 - 125
5.00
5.11
mg/L
102
75 - 125
Client Sample ID: Matrix Spike Duplicate
Prep Type: TCLP
Prep Batch: 146469
Spike
MSD MSD
%Rec.
RPD
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
5.00
5.27
mg/L
105
75 - 125
0
20
5.00
5.20
mg/L
104
75 - 125
1
20
5.00
5.24
mg/L
101
75 - 125
1
20
5.00
5.12
mg/L
102
75 - 125
1
20
5.00
5.19
mg/L
104
75.125
1
20
5.00
5.01
mglL
99
75. 125
1
20
5.00
5.17
mg/L
103
75. 125
1
20
Page 16 of 30
TestAmerica Tampa
2/28/2014

QC Sample Results
Client: Synagro Technologies, Inc.
Project/Site: Pinellas County Pelletizer
Method: 7470A - Mercury (CVAA)
Lab Sample ID: LCS 660-146506/14-A
Matrix: Solid
Analysis Batch: 146511
Analyte
Mercury
Lab Sample ID: LCSD 660-146506/15-A
Matrix: Solid
Analysis Batch: 146511
Analyte
Mercury —
Lab Sample ID: LB 660-14646011-C
Matrix: Solid
Analysis Batch: 146511
LB LB
Analyte
Result Qualifier
Mercury
0.00050 U
Lab Sample ID: 640-46879-A-1-F MS
Matrix: Solid
Analysis Batch: 146511
Sample Sample
Analyte
Result Qualifier
Mercury
0.00050 U
Lab Sample ID: 640-46879-A-1-G MSD
Matrix: Solid
Analysis Batch: 146511
Sample Sample
Analyte
Result Qualifier
Mercury
0.00050 U
TestAmerica Job ID: 660-59272-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 146506
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
0.00140 0.00141 mg/L 101 60 -120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 146506
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
0.00140 0.00137 mg/L 98 80 -120 3 20
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 146506
RL MDL Unit D Prepared Analyzed Oil Fac
0.00070 0.00050 mg/L 02/26/14 09:26 02/26/14 13:22 1
Spike MS MS
Added Result Qualifier Unit
0.00140 0.00128 mg/L
Spike MSD MSD
Added Result Qualifier Unit
0.00140 0.00129 mg/L
Client Sample ID: Matrix Spike
Prep Type: TCLP
Prep Batch: 146506
%Rec.
D %Rec Limits
Client Sample ID: Matrix Spike Duplicate
Prep Type: TCLP
Prep Batch: 146506
%Rec. RPD
D %Rec Limits RPD Limit
92 80.120 1 20
Page 17 of 30
TestAmerica Tampa
2/28/2014

QC Association Summary
Client: Synagro Technologies, Inc.
TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
GUMS Semi VOA
Leach Batch: 107855
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
660-59272-1
Synagro-1
TCLP
Solid
1311
660-59272-1 MS
Synagro-1
TCLP
Solid
1311
660-59272-1 MSD
Synagro-1
TCLP
Solid
1311
660-59272-2
Synagro-2
TCLP
Solid
1311
660-59272-3
Synagro-3
TCLP
Solid
1311
660-59272-4
Synagro-4
TCLP
Solid
1311
660-59272-5
Synagro-5
TCLP
Solid
1311
LB 640-107855/1-B
Method Blank
TCLP
Solid
1311
Prep Batch: 107872
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
660-59272-1
Synagro-1
TCLP
Solid
3520C
107855
660-59272-1 MS
Synagro-1
TCLP
Solid
3520C
107855
660-59272-1 MSD
Synagro-1
TCLP
Solid
3520C
107855
660-59272-2
Synagro-2
TCLP
Solid
3520C
107855
660-59272-3
Synagro-3
TCLP
Solid
3520C
107855
660-59272-4
Synagro-4
TCLP
Solid
3520C
107855
660-59272-5
Synagro-5
TCLP
Solid
3520C
107855
LB 640-107855/1-B
Method Blank
TCLP
Solid
3520C
107855
LCS 640-107872/3-A
Lab Control Sample
Total/NA
Solid
3520C
LCSD 640-107872/4-A
Lab Control Sample Dup
Total/NA
Solid
3520C
MB 640-107872/1-A
Method Blank
Total/NA
Solid
3520C
Analysis Batch: 107920
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
660-59272-1
Synagro-1
TCLP
Solid
8270D
107872
660-59272-1 MS
Synagro-1
TCLP
Solid
8270D
107872
660-59272-1 MSD
Synagro-1
TCLP
Solid
8270D
107872
660-59272-2
Synagro-2
TCLP
Solid
8270D
107872
660-59272-3
Synagro-3
TCLP
Solid
8270D
107872
660-59272-4
Synagro-4
TCLP
Solid
8270D
107872
660-59272-5
Synagro-5
TCLP
Solid
8270D
107872
LB 640-107855/1-B
Method Blank
TCLP
Solid
8270D
107872
LCS 640-107872/3-A
Lab Control Sample
Total/NA
Solid
8270D
107872
LCSD 640-107872/4-A
Lab Control Sample Dup
Total/NA
Solid
8270D
107872
MB 640-10787211-A
Method Blank
Total/NA
Solid
8270D
107872
----- .. - . -
GC Semi VOA
... --
---- - - ---
- ........_-
.....
Prep Batch: 316932
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
660-59272-1
Synagro-1
Total/NA
Solid
3546
660-59272-2
Synagro-2
Total/NA
Solid
3546
660-59272-3
Synagro-3
Total/NA
Solid
3546
660-59272-4
Synagro-4
Total/NA
Solid
3546
660-59272-5
Synagro-5
Total/NA
Solid
3546
LCS 680-316932/14-A
Lab Control Sample
Total/NA
Solid
3546
MB 680-316932/13-A
Method Blank
Total/NA
Solid
3546
TestAmerica Tampa
Page 18 of 30 2/28/2014

QC Association Summary
Client: Synagro Technologies, Inc.
Project/Site: Pinellas County Pelletizer
GC Semi VOA (Continued)
Analysis Batch: 317335
Lab Sample ID
Client Sample ID
LCS 680-316932/14-A
Lab Control Sample
MB 680-316932/13-A
Method Blank
Analysis Batch: 317675
Lab Sample ID
Client Sample ID
660-59272-1 —
Synagro-1
660-59272-2
Synagro-2
660-59272-3
Synagro-3
660-59272-4
Synagro-4
660-59272-5
Synagro-5
Metals
Leach Batch: 146460
Lab Sample ID
Client Sample ID
640-46879-A-1-C MS
Matrix Spike
640-46879-A-1-D MSD
Matrix Spike Duplicate
640-46879-A-1-F MS
Matrix Spike
640-46879-A-1-G MSD
Matrix Spike Duplicate
660-59272-1
Synagro-1
660-59272-2
Synagro-2
660-59272-3
Synagro-3
660-59272-4
Synagro-4
660-59272-5
Synagro-5
LB 660-146460/1-B
Method Blank
LB 660-146460/1-C
Method Blank
Prep Batch: 146469
Lab Sample ID
Client Sample ID
640-46879-A-1-C MS
Matrix Spike
640-46879-A-1-D MSD
Matrix Spike Duplicate
660-59272-1
Synagro-1
660-59272-2
Synagro-2
660-59272-3
Synagro-3
660-59272-4
Synagro-4
660-59272-5
Synagro-5
LB 660-146460/1-B
Method Blank
LCS 660-146469/2-A
Lab Control Sample
LCSD 660-146469/3-A
Lab Control Sample Dup
Analysis Batch: 146501
Lab Sample ID Client Sample ID
640-46879-A-1-C MS
640-46879-A-1-D MSD
660-59272-1
660-59272-2
660-59272-3
660-59272-4
660-59272-5
LB 660-146460/1-B
Matrix Spike
Matrix Spike Duplicate
Synagro-1
Synagro-2
Synagro-3
Synagro-4
Synagro-5
Method Blank
TestAmerica Job ID: 660-59272-1
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
8082
316932
Total/NA
Solid
8082
316932
Prep Type
Matrix
Method
Prep Batch
TOtal/NA
Solid
8082
316932
Total/NA
Solid
8082
316932
Total/NA
Solid
8082
316932
Total/NA
Solid
8082
316932
Total/NA
Solid
8082
316932
Prep Type
Matrix
Method
Prep Batch
TCLP
Solid
1311
TCLP
Solid
1311
TCLP
Solid
1311
TCLP
Solid
1311
TCLP
Solid
1311
TCLP
Solid
1311
TCLP
Solid
1311
TCLP
Solid
1311
TCLP
Solid
1311
TCLP
Solid
1311
TCLP
Solid
1311
Prep Type
Matrix
Method
Prep Batch
TCLP
Solid
3010A
146460
TCLP
Solid
3010A
146460
TCLP
Solid
3010A
146460
TCLP
Solid
3010A
146460
TCLP
Solid
3010A
146460
TCLP
Solid
3010A
146460
TCLP
Solid
3010A
146460
TCLP
Solid
3010A
146460
Total/NA
Solid
3010A
Total/NA
Solid
3010A
Prep Type
Matrix
Method
Prep Batch
TCLP
Solid
6010B
146469
TCLP
Solid
6010B
146469
TCLP
Solid
6010E
146469
TCLP
Solid
6010B
146469
TCLP
Solid
6010B
146469
TCLP
Solid
6010B
146469
TCLP
Solid
6010E
146469
TCLP
Solid
6010B
146469
TestAmerica Tampa
Page 19 of 30 2/28/2014

QC Association Summary
Client: Synagro Technologies, Inc.
Project/Site: Pinellas County Pe►letizer
Metals (Continued)
Analysis Batch: 146501 (Continued)
Lab Sample ID Client Sample ID
LCS 660-146469/2-A Lab Control Sample
LCSD 660-146469/3-A Lab Control Sample Dup
Prep Batch: 146506
Lab Sample ID Client Sample ID
640-46879-A-1-F MS
Matrix Spike
640-46879-A-1-G MSD
Matrix Spike Duplicate
660-59272-1
Synagro-1
660-59272-2
Synagro-2
660-59272-3
Synagro-3
660-59272-4
Synagro-4
660-59272-5
Synagro-5
LB 660-146460/1-C
Method Blank
LCS 660-146506/14-A
Lab Control Sample
LCSD 660-146506/15-A
Lab Control Sample Dup
Analysis Batch: 146511
Lab Sample ID
Client Sample ID
640-46879-A-1-F MS
Matrix Spike
640-46879-A-1-G MSD
Matrix Spike Duplicate
660-59272-1
Synagro-1
660-59272-2
Synagro-2
660-59272-3
Synagro-3
660-59272-4
Synagro-4
660-59272-5
Synagro-5
LB 660-146460/1-C
Method Blank
LCS 660-146506/14-A
Lab Control Sample
LCSD 660-146506/15-A
Lab Control Sample Dup
General Chemistry
Analysis Batch: 146429
Lab Sample ID
Client Sample ID
640-46876-A-1 DU
Duplicate
660-59272-1
Synagro-1
660-59272-2
Synagro-2
660-59272-3
Synagro-3
660-59272-4
Synagro-4
660-59272-5
Synagro-5
TestAmerica Job ID: 660-59272-1
Prep Type
Matrix
Method
Total/NA
S Wd
601DB
Total/NA
Solid
6010B
Prep Type
Matrix
Method
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
Total/NA
Solid
7470A
Total/NA
Solid
7470A
Prep Type
Matrix
Method
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
TCLP
Solid
7470A
Total/NA
Solid
7470A
Total/NA
Solid
7470A
Prep Type
Matrix
Total/NA
Solid
Total/NA
Solid
Total/NA
Solid
Total/NA
Solid
Total/NA
Solid
Total/NA
Solid
Method
Moisture
Moisture
Moisture
Moisture
Moisture
Moisture
Prep Batch
146469
146469
Prep Batch
146460
146460
146460
146460
146460
146460
146460
Prep Batch
146506
146506
146506
146506
146506
146506
146506
146506
146506
Prep Batch
Page 20 of 30
TestAmerica Tampa
2/28/2014

Lab Chronicle
Client: Synagro Technologies, Inc.
Project/Site: Pinellas County Pelletizer
Client Sample ID: Synagro-1
Date Collected:
02/21/14 08:53
Date Received: 0212111410:47
Batch
Batch
Prep Type
Type
Method
TCLP
Leach
1311
TCLP
Prep
3520C
TCLP
Analysis
6270D
Total/NA
Prep
3546
Total/NA
Analysis
8082
TCLP
Leach
1311
TCLP
Prep
3010A
TCLP
Analysis
6010E
TCLP
Leach
1311
TCLP
Prep
7470A
TCLP
Analysis
7470A
Total/NA
Analysis
Moisture
Client Sample
ID: Synagro-2
Date Collected:
02/21/14 08:51
Date Received: 02121/1410:47
Batch
Batch
Prep Type
Type
Method
TCLP
Leach
1311
TCLP
Prep
3520C
TCLP
Analysis
8270D
Total/NA
Prep
3546
Total/NA
Analysis
8082
TCLP
Leach
1311
TCLP
Prep
3010A
TCLP
Analysis
6010E
TCLP
Leach
1311
TCLP
Prep
7470A
TCLP
Analysis
7470A
Total/NA
Analysis
Moisture
- -- ---............. ............ ........... -
Client Sample ID: Synagro-3
Date Collected: 02/21/14 08:52
Date Received: 02121/1410:47
Batch
Batch
Prep Type
Type
Method
TCLP
Leach
1311
TCLP
Prep
3520C
TCLP
Analysis
8270D
Total/NA
Prep
3546
Total/NA
Analysis
8082
TCLP
Leach
1311
TCLP
Prep
3010A
TCLP
Analysis
6010B
TestAmerica Job ID: 660-59272-1
Lab Sample ID: 660-59272-1
Matrix: Solid
Dilution
Batch
Prepared
Run Factor
Number
or Analyzed
Analyst
Lab
107855
02/24/14 16:30
TJW
TAL TAL
107872
02/26/14 10:00
JCS
TAL TAL
1
107920
02/27/14 23:19
VHW
TAL TAL
316932
02/24/14 12:39
JMV
TAL SAV
1
317675
02/28/14 05:34
JCK
TAL SAV
146460
02/24/14 16:30
RAG
TAL TAM
146469
02/25/14 11:30
RAG
TAL TAM
1
146501
02/26/14 08:54
GAF
TAL TAM
146460
02/24/14 16:30
RAG
TAL TAM
146506
02/26/14 09:26
RAG
TAL TAM
1
146511
02/26/14 13:36
RAG
TAL TAM
1
146429
02/24/14 06:32
AJG
TAL TAM
Lab Sample ID: 660-59272-2
Matrix: Solid
Dilution
Batch
Prepared
Run Factor
Number
or Analyzed
Analyst
Lab
107855
02/24/14 16:30
TJW
TAL TAL
107872
02/26/14 10:00
JCS
TAL TAL
1
107920
02/27/14 23:47
VHW
TAL TAL
316932
02/24/14 12:39
JMV
TAL SAV
10
317675
02/28/14 07:51
JCK
TAL SAV
146460
02/24/14 16:30
RAG
TAL TAM
146469
02/25/14 11:30
RAG
TAL TAM
1
146501
02/26/14 08:58
GAF
TAL TAM
146460
02/24/14 16:30
RAG
TAL TAM
146506
02/26/14 09:26
RAG
TAL TAM
1
146511
02/26/14 13:37
RAG
TAL TAM
1
146429
02/24/14 06:48
AJG
TAL TAM
Lab Sample ID: 660-59272-3
Matrix: Solid
Dilution
Batch
Prepared
Run Factor
Number
or Analyzed
Analyst
Lab
107855
02/24/14 16:30
TJW
TAL TAL
107872
02/26/14 10:00
JCS
TAL TAL
1
107920
02/28/14 00:17
VHW
TAL TAL
316932
02/24/14 12:39
JMV
TAL SAV
10
317675
02/28/14 08:14
JCK
TAL SAV
146460
02/24/14 16:30
RAG
TAL TAM
146469
02/25/14 11:30
RAG
TAL TAM
1
146501
02/26/14 09:01
GAF
TAL TAM
Page 21 of 30
TestAmerica Tampa
2/28/2014

Lab Chronicle
Client: Synagro Technologies, Inc.
TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
Client Sample ID: Synagro-3
Lab Sample ID: 660-59272-3
Date Collected: 02/21/14 08:52
Matrix: Solid
Date Received: 0212111410:47
Batch Batch
Dilution Batch
Prepared
Prep Type Type Method
Run Factor Number
or Analyzed
Analyst
Lab
TCLP Leach 1311
146460
02/24/14 16:30
RAG
TAL TAM
TCLP Prep 7470A
146506
02/26/14 09:26
RAG
TAL TAM
TCLP Analysis 7470A
1 146511
02/26/14 13:43
RAG
TAL TAM
Total/NA Analysis Moisture
1 146429
02/24/14 06:46
AJG
TAL TAM
Client Sample ID: Synagro-4
Date Collected: 02/21114 08:50
Date Received: 02/2111410:47
Batch
Batch
Prep Type
Type
Method Run
TCLP
Leach
1311
TCLP
Prep
3520C
TCLP
Analysis
8270D
Total/NA
Prep
3546
Total/NA
Analysis
8082
TCLP
Leach
1311
TCLP
Prep
3010A
TCLP
Analysis
6010E
TCLP
Leach
1311
TCLP
Prep
7470A
TCLP
Analysis
7470A
Total/NA
Analysis
Moisture
Client Sample ID: Synagro-5
Date Collected: 02/21/14 08:50
Date Received: 0212111410:47
Batch
Batch
Prep Type
Type
Method
TCLP
Leach
1311
TCLP
Prep
3520C
TCLP
Analysis
8270D
Total/NA
Prep
3546
Total/NA
Analysis
8082
TCLP
Leach
1311
TCLP
Prep
3010A
TCLP
Analysis
6010E
TCLP
Leach
1311
TCLP
Prep
7470A
TCLP
Analysis
7470A
Total/NA
Analysis
Moisture
Run
Lab Sample ID: 660-59272-4
Matrix: Solid
Dilution
Factor
Batch
Number
Prepared
or Analyzed
Analyst
Lab
107855
02/24/14 16:30
TJW
TAL TAL
107872
02/26/14 10:00
JCS
TAL TAL
1
107920
02/28/14 00:45
VHW
TAL TAL
316932
02/24/14 12:39
JMV
TAL SAV
10
317675
02/28/14 08:37
JCK
TAL SAV
146460
02/24/14 16:30
RAG
TAL TAM
146469
02/25/14 11:30
RAG
TAL TAM
1
146501
02/26/14 09:05
GAF
TAL TAM
146460
02/24/14 16:30
RAG
TAL TAM
146506
02/26/14 09:26
RAG
TAL TAM
1
146511
02/26/14 13:44
RAG
TAL TAM
1
146429
02/24/14 07:07
AJG
TAL TAM
Lab Sample ID: 660-59272-5
Matrix: Solid
Dilution
Batch
Prepared
Factor
Number
or Analyzed
Analyst
Lab
107855
02/24/14 16:30
TJW
TAL TAL
107872
02/26/14 10:00
JCS
TAL TAL
1
107920
02/28/14 01:15
VHW
TAL TAL
316932
02/24/14 12:39
JMV
TAL SAV
10
317675
02/28/14 09:00
JCK
TAL SAV
146460
02/24/14 16:30
RAG
TAL TAM
146469
02/25/14 11:30
RAG
TAL TAM
1
146501
02/26/14 09:15
GAF
TAL TAM
146460
02/24/14 16:30
RAG
TAL TAM
146506
02/26/14 09:26
RAG
TAL TAM
1
146511
02/26/14 13:46
RAG
TAL TAM
1
146429
02/24/14 06:59
AJG
TAL TAM
Page 22 of 30
TestAmerica Tampa
2/28/2014

Lab Chronicle
Client: Synagro Technologies, Inc.
r Project/Site: Pinellas County Pelletizer
j
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TAL TAL = TestAmedca Tallahassee, 2846 Industrial Plaza Drive, Tallahassee, FL 32301, TEL [phone]
TAL TAM = TestAmerica Tampa, 6712 Benjamin Road, Suite 100, Tampa, FL 33634, TEL [phone].
1
Page 23 of 30
TestAmerica Tampa
2/28/2014

Method 'Sur>nmary
.
JA
Client: Synagro Technologies, Inc.
TestAmerica Job ID: 660-59272-1
Project/Site: Pinellas County Pelletizer
-
----= - --------------= --- - — — - - — = — -- ---
Method Method Description
-
Protocol
— --- -
Laboratory
i''.
8270D Semivolatile Organic Compounds (GC/MS) -
sW846
TAL TAL,
6082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography,
SW846
TAL SAV
6010E Metals (ICP) _
SW846
TAL TAM.
7470A Mercury (CVAA)
5W846
TAL TAM.:
t;
Moisture Percent Moisture . -
EPA .
TAL TAM
f.�
Protocol References:
EPA =US Environmental Protection Agency'.-
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And
Its Updates.
;t •
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404; TEL [phone]
"
TAL TAL,= TestAmerica Tallahassee, 2846 Industrial Plaza Drive, Tallahassee, FL 32301, TEL [phone] .
TAL TAM = TestAmedca Tampa, 6712 Benjamin Road, Suite 100, Tampa, FL 33634, TEL [phone]
F,t},
k
i
j •.
i
TestAmerica Tampa
Page 24. of 30
"; 2/28/2014

;:.
Certification Summalry.
Client: Synagro-Technologieis, Inc.
TestAmerica Job ID: 660-69272-1
'I
ProjecMte: Pinellas County Pelletizer
Laboratory:. TestArnerica Tampa,
t.
All certifications held by this laboratory ate listed. Not -all certifications are applicable. to this.report.,
— - —
- - ----- — -----
'•
--.
. ----.
--- -
I
Authority Program
EPA, Region _
Certification ID
Expiration,Date
r
Alabama State Program,
4
40610
06-30-14
k
Florida NELAP
4
E84282
06-30714 :,
L
Georgia State Program
4 ;
905 :
06 30 14
.
-
USDA Federal
P330-11-00177
04-20-14
taborato ..
ry: Test�.rrserica Savannah
AII'certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program
EPA Region' .'
' Certification ID
Expiration Date.
;
AFCEE ...
SAVLAB
9LA DoD ELAP
399.01
02-28-15
A2LA ISO/IEC' 17025
399.01
02-28-15
Alabama State Program
4
41450
06-30=14
r:
k /
l
Arkansas DEQ State Program
6 ..
88-0692
01 31.15
I
California NELAP
9 :
3217CA
07-31.-14
Colorado State Program
8 .•
N/A
12-31-14
I +
Connecticut State'Program
1
PH-0161
03-31-15 „
Florida NELAP
4 :
E87052
06-30-14.. .
GA Dept. of Agriculture State Program
4-
N/A
06-30-14
Georgia State Program
4
N/A
06-30-14
i -
Georgia' State -Program
4
803
66-30-14. •
c•
Guam State Program
9
09-005r
04-17-14.
Hawaii State Program
.9 -
N/A
06-30-14
Illinois NELAP
.5. .
200022
11-30-14
Indiana State Program
5'
N/A-
06-30-14
Iowa State Program
7
353:
07-01-15
Kentucky (DW) State Program
4
90084
12-31-14
Kentucky (UST) State Program
4
18
06-30-14
Louisiana NELAP,
6
LA100015
12731-14 .
Maine State Program
1
GA00006
08-16-14
Maryland State Program
3
250
12-31-14
Massachusetts State Program
9
M-GA006
06730714
Michigan State Program
5
9925
06-30-14
Mississippi State Program
4
N/A
06-30-14 .
Montana State Program,
6
CERT0081
01701-15
:Nebraska. State Program
7
TestAmerica-Savannah
06-30-14 -.
New Jersey NELAP
2
GA769
06-30-14
i
New Mexico State Program
6
N/A
06-30-14
New York NELAP
2
10842.
03-31-14
North Carolina DENR State Program
4
269
12-31-14'
North Carolina DHHS State Program
4
13701
07-31-14
Oklahoma State Program
6
9984
08-31-14
Pennsylvania ..NELAP.
3
68-00474
06-30-14
Puerto Rico State Program
2
GA00006
12-31-14
South Carolina State Program
4
98001
06-30-14
Tennessee State Program
4
TN02961
06-30714
Texas NELAP.
6
T1.D4704185-OB-TX
11-30-14
i
USDA Federal
SAV 3=04
04-07714
Virginia NELAP
3
460161
06-14714
Washington State Program
10,
C179.4
06-10=14
estAmerica Tampa
Page 25 of30
2/28 2014

Certification Summary
Client: Synagro Technologies, Inc.
Project/Site: Pinellas County Pelletizer
Laboratory: TestAmerica Savannah (Continued)
Ali certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region
Certification ID
TestAmerica Job ID: 660-59272-1
Expiration Date
West Virginia DEP State Program
3
94
06-30-14
West Virginia DHHR State Program
3
9950C
12-31-14
Wisconsin State Program
5
999819810
08-31-14
Wyoming State Program
I
8TMS-L
06-30-14
Laboratory: TestAmerica Tallahassee
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.
F
Authority Program
EPA Region
CoMfleation ID
Expira*m Date
Florida NELAP
4
E81005
06-30-14
Georgia State Program
4
06-30-14
Louisiana NELAP
6
30663
06-30-14
New Jersey NELAP
2
FLO12
06-30-14
Texas NELAP
6
T104704459-11-2
03-31-14
USDA Federal
P330-08-00158
08-05-14
i�
TestAmerica Tampa
Page 26 of 30 2/28/2014

Login Sample Receipt Checklist
Client: Synagro Techriologies,,lnc:
:.
Job Number: 660-59272-1 F?
Login Number: 59272,
: List Source: TestAmerica Tampa
List Number:11
Creator: ,MMulty, Carol
Question
Answer Comment "
t•
Radioactivity wasn't; checked or is <I= background as measured by a. survey " :
NIA
meter.
The cooler's custody. seat; .if present, is Intact.
True
,
Sample custody seals, If present, are intact.
True :
The cooler or samples "do riot appear to have been comprorrilsed or
True
tampered with.
.. .
Samples were,received on ice.. " . .
True
Cooler Temperature: is acceptable:.
True'
Cooler Temperature is recorded. "
True'
-
' COC is present.
True
y COC Is frlledout in'ink and.iegibte:.
True
COC-is,'filled out with all pertinent Information.
True
`
Is the Field Sampler's name present on COC?
True
There are no discrepancies, between the'containers received and 'the COC.
• True
Samples ere receivedwithin Holding Time.
True
Sample containers have.legible.labels:
True :
! Containers are not broken or leaking.
"
True -
Sample collection dateitimes are provided.
True
Appropriate sample containers are used.
True
1 Sample bottles are completely filled.
True, . .
Sample'Preservation Verified:
True
There is sufficient vol. for all requested analyses; Incl. any requested ' .
True.
MS/MSDs
Containers requiring zero headspaoe have no headspace or bubble Is
NIA
6mm.(1I4"). .
Muitiphas'rc samples.are not present..
True'
Samples do not require splitting or compositing:
True
:
Residual Chlorine Checked.
NIA.
,
f �
1
TestAmerica Tampa :.
_.
Page 28.
of 30..
2/28/2014

53
Logirn SaMple Receipt Checklist
x
Client: Synagro Technologies, Inc.
-
.,lob Number: 660 59272-1
x
irr$
Login Number: 59272
List Source: TestAmerica Savannah.
List Number. 4 _
List Creation: 02/22/14 09:46'AM
I
Creator: Conner, Keaton , '
Question,
Answer Comment:.
_
Radioactivity wasn't checked or Is </='background as measured by a survey
N/A
`
meter.
i
. The cooler's custody seal, if present, is intact: ..
True
Sample custody seats; lf.present, are Intact.
True
(
Tfte cooler or samples do riot appear to have been compromised or
True^
.
f
tampered with.. -
Samples were received on fce...
True
Coder.Temperature is acceptable.
True ._
Cooler Temperature is recorded.
True
COG Is present.. - ' ..
True_. '
COC'is filled out in ink and legible.
True.
GOC is filled out with: all pertinent information:.
True.
Is theIeldSampler'sname present onCOC?'
NIA:.
'
There are no discrepancies between the containers received and the COC.
True
k"
Samples are received- within holding Time.
True,
Sample containers -have legible labels.
True
r
Containers are not .broken or leaking. ..
True. -
_k
Sample collection dateAimes are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filed:
True.
Sample Preservation Verified.
True
There Is sufficient Vol. for all requested, analysesincl. any requested
True
MSIMSDs .
Containers requiring zero headspace have no headspace or bubble Is
True
Multiphasic samples are not present.
True
Samples do not require splitting or co siting.
8 P 9 ►hPo
True ,
Residual Chlorine Checked.
N/A.
4,
T i tA Tesmerca Tampa
Page 29
p
of 30 . ' . :
/201
2128 4

Login Sample Receipt Checklist
-?
•5
Client: Synagro Technologies, Inc,
:
Job Number: 6M 59272-1
Ye .
Login Number: 59272,
List Source: TestAmerica Tallahassee
List Number: 2
List Creation: 02126114 09:03 AM
Creator: Savoie, Joseph.L
_,.. Question,
Answer Comment
r; .
Radioactivity wasn't checked or Is </= background as measured bya:survey
N/A
meter,
The cooler's custody seal; if present, is intact.
True
Sample custody seats,'if present, are intact.
True
The tooter or samples do not appear to have been compromised or
True
tampered with.
Samples were received on Ice..
T r ue
1 Cooier.7emperature Is acceptable.
'True .
l Gooier Temperature is recorded.
True
COC is present.
True
COC'is filled out in ink and legible:
True
COC is filled out with all pertinent Information.
True
Is the Field Sampler's name present on-COC?
True
i I - There are no discrepancies.between.the containers.re.ceived and the-COC.
True
Samples are,ieceived:within Holding Time
True
Sample containers have legible labels:"
True"
Containers are not broken or leaking.
True .. '.
I "Sample collection date/times are provided. a ..
True
Appropriate sample containers are used.
True
Sample bottles are •completely filled.
'True.
Sample Preservation Verified:
NIA
There is sufficient vol. for all requested analyses, Incl. any requested
True
MS/MSDs
Containers requiring zero headspace, have no headspace or`bubble Is
NIA
<6mm (1/4") ..
"
..
Multiphasic samples, are not present.:.
True '
Samples do not require s littin or corn siti
1t P q' p . 9 i�
N/A
.
" Residual Chlorine Checked. .: '
N/A .
TestAmerica Tampa
Pa a 30
g
of'30 ...
2J28/2014 ,

Summit Environmental Technologies, Inc.
3310 Win St.
a EPdIrI?IK?adk1E yitiLl Okr6It3113 s� , 3t Cuyahoga Falls, Ohio 44223
AhallrlicalLaliotal'orfet; :TEL: [phone] FAX.- [phone]
Website: h1tp:1Avivt'v.settek.corir
l March ' 17, 2014
Matt Busch
Synagro
m 5900 744L Street North
St. Petersbutg,.FL 33789
TEL: [phone]
FAX: '[phone] . .
RE: Pinellas
Dear Matt Busch: Order No.: 1403.1'194
Summit Environmental Technologies, Inc. received I sample(s) on 3/13/2014 for the. analyses
presented in.the -following report:
f "
There .were no problems with the analytical events associated with this reportunless noted in the
Case Narrative.
1 Quaiity:control data is within laboratory defined_or method specified' acceptance limits except:.
,t where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman ..
Project Manager _.
3310 Win St..
Cuyahoga Fa'lls', .Ohio 442'23
A2LA 0724-01, Alabaina 41600,, Arkansas 88-0735, California 07256CA; Colorado, Connecticut PH-0105, Delaware; Florida'NELAC E87688; Georgia
E87688'and 943, Idaho OH00923, Illinois 200061 and Reg.5; Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky'
90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey 01-1006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CLA052, Oklahoma 9940, Oregon
OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8T ' S-,
..L; USDA/APHIS P330-11-00244, Utah OH00923201 1 -1, Vermont VT-87688, Virginia 00440 and .1581, Washington C891, West Virginia 248 and 9957C
l i• and E87688, Wisconsin 199013010
f .

ri ��'
." a: F
i x I.
Summit Environmental Technologies, Inc.
3310 Win St.
Workorder
E •.
b.hio
Sa' le
t%s'IRCr
jiaiE:>+'rAL.T_rCHfdOLOGIZ$,.I,C
Cuyahoga Falls, 44223
*summary
An_gly!Ycs$
tobbaa.fprios
TEL: [phone] FAX: [phone]
WO#: 14031194
Website: hjW,,1Avww,settek.com
17-Mar-14
CLIENT:
Synagro
Project:
Pinellas
tab SampleID
Client Sample ID Tag No Date Collected
Date Received Matrix
14031194-001
SYN-PIN 3-12
3/12/2014
3/13/2014 9:40:60 AM Solid

Summit Environmental Technologies, Inc. �T
3310Win St, Case Narrative
FIll�VI-3Ot4►iIEN'rALTk--CHh.OLaC.d4S, 1,14C Cuyahoga Falls, Ohio 44223 WO#: 14031194
-Anajytlral l.ohoratorles TEL: [phone] FAX: [phone]
Website: haw/Amhaw/Ammseftek,com Date: 3/17/2014
CLgENT: Synagro
Project: Pinellas
This report in its entirety consists of the documentslisted below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual. field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request. . .
Any comments or problems with the analytical events associated with this report are noted below.
Original

Summit Environmental Technologies, Inc.
St.
WO#: '14031194
1:1
P{4P��k7tdpslt�TsL.Cttl+9t CsC, y, BtO
3310.Win
Cuyahoga Falls, Ohio 44223.
.Date Reported: 3/17/2014
a1 1 r 1 •l tic retvrl TU: [phone] FAJL (330) 25374489
Company: Synagro
websire: hrrn:ih�wvwseuek.com .
Address: 5900 744L Street North
St. Petersburg FL 33789
Deceived: 3/13/2014
Project#: Pinellas
Client IDW
Lab ID# Collected Analyte
Result Units
Matrix Method. '.DF RL 'Run
Analyst
SYN-PIN 3-12
001 3/12/2014 Flaehpoint (140T)
>140 `F
Solid EPA 1040 1 3/14/2014
TJR
SYN-PIN 3-12
001 3/12/2014 Cyanide, Reactive
AID ppm_
Solid EPA 9014 1 0.50 3/14/2014
TIR
SYN-PIN 3-12
001 3/12/2014 pH
6.9 S:u.
Solid EPA 9045 D 1 : 3/14/2014
AYS
SYN-PIN 3-12
001 3/12/2014 Sulfide, Reactive
ND ppm
Solid EPA 9034 1 25 3/1412014
TIR

Sumumit ED�viromnentai "Teelirimlogies; Inc.
/� q�
NY111 SICCCD
®®]]•��QQ c
l.adl(,8��1� s
t
33 1V
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:.'Cuyahoga Falls, O]rio.44223
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Logged 01 by,
G:1QC SHAR€DiDocument Control Templates -
Tra6kingtooler receipt form Rev. 12 07-27-i 3.doc
Rage 1 of 2

i n virenmentai
aboratoriea, Inc.
The difference is service
AIR I SOIL I WATER I MARINE CHEMISTRY
Analytical Report For
Client: Synagro Technologies, Inc.
Client Project Name: Synagro - Pinellas
Attention: Mathew Busch
5900 74th Street North
St. Petersburg, FL 33709-1374
EM
Approved for release on 02/27/2014 by:
- Stephen Nowak
IeaW nk t Project Manager
Ernail your PM t
Calscience Environmental Laboratories, Inc. (Calscience) certifies that the test results provided in this report meet all NELAC requirements for parameters for which
accreditation is required or available. Any exceptions to NELAC requirements are noted in the case narrative. The original report of subcontracted analyses, if any,
is attached to this report The results in this report are limited to the sample(s) tested and any reproduction thereof must be made in its entirety. The client or
recipient of this report is specifically prohibited from making material changes to said report and, to the extent that such changes are made, Caisclence is not
responsible, legally or otherwise The client or recipient agrees to indemnify Caiscience for any defense to any litigation which may arise.
s,. I-. cr t,,P ID OS,..:0"A 3 L?t_I YE(AP ID 1.}n^+� t1ii3`a f (qr

I Page 2 of 38
a/sclence.
{
nvlronmental-
• aboratorles, Inc.. ..Contents
client Project Name: Synagro - PineHas
Work Orde'r Number. 14-02.1588
1 Work_Order-Narrative.... .. .. ... .. :..
3
2 Sample Summary•. •.. • . ..... .. .... ::..... .:.:...
4
3 Client Sample :Data...: ............
3:1 SM 2540 B, (M) Total Solids (Solid).. .......... .. .: .... ... :.
.5
- . 3.2 'EPA 601'OBR471 A CAC. Title 22 Metals (Solid)... ; ..........::.... .. ...
6 .
3:3 . EPA 7471 A Mercury (Solid). .. ..:. :.:...... :: • ........• • ....
9
3.4 EPA 8682 PCB Aroclors (Solid)....:, .......
3.5 EPA '8270C Semi -Volatile Organics .(Solid)...... .. ... .... .. ..
11
3.6 EPA 8260B TCLP Volatile Organics (Aqueous):.: :
20
4 Quality Control Sample Data:. .......::...
24 _
4.. MS/M,SD.. • .. .... .. .. :..:. •:.... .::. :
..24. .
4.2 Sarrtple ©.uplicate. .. • .. • ....... ::. , .. • : • .:
28 .
4.3 LCSlLCSD. :: ..... . :.
29.
5 Sample Analysis Sum:mary............. .. • .W.
6 Glossaryaf:Terms and Qualifiers. .: ..:... :.
- 35
7�.: .Chain ofi.CustodytSampie Receipt Form.. . , ... .. , , . .....
36
7440 Lincoln WayGarden Grove, CA ®2841-1427 ..• TEL'. [phone] • FAX: (714),894-7501

Page 3 of 38
"alscience
nvlronmental
aboratories, Inc.
Work Order Narrative
Work Order: 14-02-1588 Page 1 of 1
Condition Upon Receipt:
Samples were received under Chain of Custody (COC) on 02/22/14. They were assigned to Work Order 14-02-1588.
Unless otherwise noted on the Sample Receiving forms all samples were received in good condition and within the
recommended EPA temperature criteria for the methods noted on the COC. The COC and Sample Receiving Documents are
integral elements of the analytical report and are presented at the back of the report.
All samples were analyzed within prescribed holding times (HT) and/or in accordance with the Calscience Sample Acceptance
Policy unless otherwise noted in the analytical report and/or comprehensive case narrative, if required.
Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of — 15
minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being
received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time.
Quality Control:
All quality control parameters (QC) were within established control limits except where noted in the QC summary forms or
described further within this report.
Additional Comments:
Air - Sorbent-extracted air methods (EPA TO-4A, EPA TO-10, EPA TO-13A, EPA TO-17): Analytical results are converted from
mass/sample basis to mass/volume basis using client -supplied air volumes.
New York NELAP air certification does not certify for all reported methods and analytes, reference the accredited items here:
//www.calscience.com/PDF/New York.pdf
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC
results are always reported on a wet weight basis.
Subcontractor Information:
Unless otherwise noted below (or on the subcontract form), no samples were subcontracted.
7440 Lincoln Way, Garden Grove, CA 92841-1427 . TEL: [phone] • FAX: [phone]

Page 4 of 38
alscience
Environmental
Sample Summary
Z. aboratories, Inc.
Client: Synagro Technologies, Inc.
Work Order:
14-02-1588
5900 74th Street North
Project Name:
Synagro - Pinellas
St. Petersburg, FL 33709-1374
PO Number:
Date/Time
02/22/14 09:30
Received:
Number of
5
Containers:
Attn: Mathew Busch
Sample Identification
Lab Plumber
Collection Date and Time
Plumber of
Matrix
Containers
Syn-1
14-02-1588-1
02/21/14 12:17
1
Solid
Syn-2
14-02-1588-2
02121/14 12:16
1
Solid
Syn-3
14-02-1588-3
02/21/14 12:19
1
Solid
Syn-4
14-02-1588-4
02/21/14 12:20
1
Solid
Syn-5
14-02-1588-5
02/21/14 12:21
1
Solid
7440 Lincoln way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]

Page 5 of 38
alsc%nce
nvironmenta/
Analytical Report
aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
N/A
Method:
SM 2540 B (M)
Units:
%
Project: Synagro - Pinellas
Page 1 of 1
Client Sample Number
Lab Sample Date/Time
Matrix Instrument
Date
Date/Time QC Batch ID
Number Collected
Prepared
Analyzed
Syn-1
14-02-1588-1-A 02/21/14
Solid N/A
02122/14
02/22/14 E0222TSBI
12:17
17:15
Parameter
Result
EL
PF
Quglifiers
Solids, Total
91.2
0.100
1.00
Method Blank 099-05-019-2487 NIA Solid NIA 02/22/14 02/22/14 E0222TSB1
f 17:15
Parameter Result —LL DFF Qualifiers
Solids, Total ND 0.100 1.00
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 6 of 38
alscience
Environmental
Analytical Report
aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3050B
Method:
EPA 6010B
Units:
mg/kg
Project: Synagro - Pinellas
Page 1 of 3
Client Sample Number
Lab Sample Date/Time
Matrix Instrument
Date
Date/Time QC Batch ID
Number Collected
Prepared
Analyzed
Syn-3
14-02-1588-3-A 02/21114
Solid ICP 7300
02121114
02/22114 140221L0I
12:19
16:31
Parameter
Resul
Qualifier
Antimony
41.5
0.721
0.962
Arsenic
18.8
0.721
0.962
Barium
199
0.481
0.962
Beryllium
ND
0.240
0.962
Cadmium
16.2
0.481
0.962
Chromium
43.3
0.240
0.962
Cobalt
4.63
0,240
0.962
Copper
549
0.481
0.962
Lead
232
0.481
0.962
Molybdenum
8.52
0.240
0.962
d
Nickel
21.6
0.240
0.962
0
Selenium
4.79
0.721
0.962
U
s
Silver
3.60
0.240
0.962
a
Thallium
ND
0.721
0.962
Vanadium
9.30
0.240
0.962
Zinc
1620
0.962
0.962
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] - FAX: [phone]

Page 7 of 38
E alscience
Analytical Report
nvironmenta/
Laboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3050B
Method:
EPA 6010B
Units:
mg/kg
Project: Synagro - Pinellas
Page 2 of 3
Client Sample Number
Lab Sample Date(Time
Matrix Instrument
Date
Date/Time QC Batch ID
Number Collected
Prepared
Analyzed
Syn-4
14-02-1588-4-A 02/21/14
Solid ICP 7300
02/21/14
02/22/14 140221L09
12:20
16:32
Parameter
Result
QUalifiers
Antimony
46.6
0.769
1.03
Arsenic
20.8
0.769
1.03
Barium
217
0.513
1.03
Beryllium
ND
0.256
1.03
Cadmium
17.9
0.513
1.03
Chromium
48.0
0.256
1.03
Cobalt
5.06
0.256
1.03
Copper
599
0.513
1.03
Lead
253
0.513
1.03
Molybdenum
9.39
0.256
1.03
Nickel
23.5
0.256
1.03
d
0
Selenium
4.58
0.769
1.03
U
a
E
Silver
4.02
0.256
1.03
Thallium
ND
0.769
1.03
Vanadium
10.2
0.256
1.03
Zinc
1770
1.03
1.03
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 8 of 38
alscience
Environmental
Analytical
Report
aboratorles, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3050B
Method:
EPA 6010B
Units:
mglkg
Project: Synagro - Pinellas
Page 3 of 3
Client Sample Number
Lab Sample Daterrime
Matrix Instrument
Date
Date/Time QC Batch ID
Number Collected
Prepared
Analyzed
Method Blank
097-01-002-18047 NIA
Solid ICP 7300
02/21/14
02/21114 1402211-09
23:47
Parameter
Result
EL
DF
Qualifiern
Antimony
ND
0.750
1.00
Arseni-c
ND
0,750
1.00
Barium
ND
0.500
1.00
Beryllium
ND
0.250
1.00
Cadmium
ND
0.500
1.00
Chromium
ND
0.250
1.00
Cobalt
ND
0.250
1.00
Copper
ND
0.500
1.00
Lead
ND
0.500
1.00
Molybdenum
ND
0.250
1.00
Nickel
ND
0.250
1.00
Selenium
ND
0.750
1.00
Silver
ND
0.250
1.00
Thallium
ND
0.750
1.00
Vanadium
ND
0.250
1.00
Zinc
ND
1.00
1.00
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 9 of 38
alscience
Environmental
aboratories, Inc.
Analytical Report
Synagro Technologies, Inc. Date Received: 02/22/14
5900 74th Street North Work Order: 14-02-1588
St. Petersburg, FL 33709-1374 Preparation: EPA 7471A Total
Method: EPA 7471A
Units: mg/kg
Project: Synagro - Pinellas Page 1 of 1
Client Sample Number
Lab Sample
Date/Time
Matrix
Instrument
Date
Date/Time QC Batch ID
Number
Collected
Prepared
Analyzed
Syn-3
14-02-1588-3-A
02/21/14
Solid
Mercury
02/22/14
02/22/14 140222L03
12:19
14:13
Parameter
Result
pF
Qualifiers
Mercury
0.650
0.0794
1.00
Syn-4
14-02-1588-4-A
02/21/14
Solid
Mercury
02/22/14
02/22/14 140222L03
12:20
14:15
parameter
Result
$L
DF
Qualifiers
Mercury
0.554
0.0794
1.00
Method Blank
099-16-272-41
N/A
Solid
Mercury
02/22/14
02/22/14 1402221-03
11:15
Parameter
Result
EL
-E
QualifierE
Mercury
ND
0.0820
1.00
0
U
0
c
a
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]

Page 10 of 38
alscience
Environmental
Analytical Report
aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3545
Method:
EPA 8082
Units:
ug/kg
Project: Synagro - Pinellas
Page 1 of 1
Client Sample Number
Lab Sample
Date/Time
Matrix Instrument
Date
Date/Time QC Batch ID
Number
Collected
Prepared
Analyzed
Syn-2
14-02-1588-2-A
02/21/14
Solid GC 66
02/22/14
02/25/14 1402221-02
12:18
02:34
Paramete
Result
El
12E
Qualifiers
Arodor-1016
ND
50
0.996
Arodor-1221
ND
50
0.996
Aroclor-1232
ND
50
0.996
Arodor-1242
ND
50
0.996
Arodor-1248
ND
50
0.996
Arodor-1254
ND
50
0.996
Arodor-1260
ND
50
0.996
Arodor-1262
ND
50
0.996
Surrogate
Rec. I%)
Control Limits
Qualifiers
Decachlorobiphenyl
92
24-168
2,4,5,6-Tetrachloro-m-Xylene
81
25-145
Method Blank
099-12-535-2494
N/A
Solid GC 66
021M14
02/25/14 140222102
00:46
Parameter
Result
EL
DF
Qualifierfi
Arodor-1016
ND
50
1.00
Arodor-1221
ND
50
1.00
Arodor-1232
ND
50
1.00
Aroclor-1242
ND
50
1.00
Arodor-1248
ND
50
1.00
Arodor-1254
ND
50
1.00
Aroclor-1260
ND
50
1.00
Aroclor-1262
ND
50
1.00
Surrogate
Rec. 1%1
Control Limits
Qualifiers
Decachlorobiphenyl
125
24-168
2,4,5,6-Tetrachloro-m-Xylene
115
25-145
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]
t
io
0
U
E

Page 11 of 38
alscience
Environmental
Analytical Report
aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3545
Method:
EPA 8270C
Units:
mg/kg
Project: Synagro - Pinellas
Page 1 of 9
Client Sample Number
Lab Sample Date/Time
Number Collected
Matrix Instrument
Date
Prepared
Date/Time QC Batch ID
Analyzed
Syn-3
14-02.1588-3-A 02/21114
Solid GC/MS TT
02/22/14
02/24/14 140222L01A
12:19
16:41
Parameter
Result
RL
12E
Qualifiers
Acenaphthene
ND
5.0
10.0
Acenaphthylene
ND
5.0
10.0
Aniline
ND
5.0
10.0
Anthracene
ND
5.0
10.0
Azobenzene
ND
5.0
10.0
Benzidine
ND
100
10.0
Benzo (a) Anthracene
ND
5.0
10.0
Benzo (a) Pyrene
ND
5.0
10.0
Benzo (b) Fluoranthene
ND
5.0
10.0
Benzo (g,h,i) Perylene
ND
5.0
10.0
Benzo (k) Flvoranthene
ND
5.0
10.0
Benzoic Acid
ND
25
10.0
Benzyi Alcohol
ND
5.0
10.0
Bis(2-Chioroethoxy) Methane
ND
5.0
10.0
Bis(2-Chloroethyl) Ether
ND
25
10.0
Bis(2-Chloroisopropyl) Ether
ND
5.0
10.0
Bis(2-Ethyihexyl) Phthalate
12
5.0
10.0
4-Bromophenyl-Phenyl Ether
ND
5.0
10.0
Butyl Benzyl Phthalate
ND
5.0
10.0
4-Chloro-3-Methylphenol
ND
5.0
10.0
4-Chloroaniline
ND
5.0
10.0
2-Chloronaphthalene
ND
5.0
10.0
2-Chlorophenol
ND
5.0
10.0
4-Chlorophenyl-Phenyl Ether
ND
5.0
10.0
Chrysene
ND
5.0
10.0
Di-n-Butyl Phthalate
ND
5.0
10.0
Di-n-Octyl Phthalate
ND
5.0
10.0
Dibenz (a,h) Anthracene
ND
5.0
10.0
Dibenzofuran
ND
5.0
10.0
1,2-Dichlorobenzene
ND
5.0
10.0
1,3-Dichlorobenzene
ND
5.0
10.0
1,4-Dichlorobenzene
ND
5.0
10.0
3,3'-Dichlorobenzidine
ND
100
10.0
2,4-Dichlorophenoi
ND
5.0
10.0
Diethyl Phthalate
ND
5.0
10.0
RL: Reporting Limit. DF: Dilution Factor, MDL: Method Detection Limit
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]

Page 12 of 38
- alscience
Analytical Report
Environmental
16 aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3545
Method:
EPA 8270C
Units:
mg/kg
Project: Synagro - Pinellas
Page 2 of 9
Parameter
Result
El
L
Qualifiers
Dimethyl Phthalate
ND
5.0
10.0
2,4-Dimethylphenol
ND
5.0
10.0
4,6-Dinitro-2-Methylphenol
ND
25
10.0
2,4-Dinitrophenol
ND
25
10.0
2,4-Dinitrotoluene
ND
5.0
10.0
2,6-Dinitrotoluene
ND
5.0
10.0
Fluoranthene
ND
5.0
10.0
Fluorene
ND
5.0
10.0
Hexachloro-1,3-Butadiene
ND
5.0
10.0
Hexachlorobenzene
ND
5.0
10.0
Hexachlorocyclopentadiene
ND
25
10.0
Hexachloroethane
ND
5.0
10.0
Indeno (1,2,3-c,d) Pyrene
ND
5.0
10.0
Isophorone
ND
5.0
10.0
2-Methylnaphthalene
ND
5.0
10.0
1-Methylnaphthalene
ND
5.0
10.0
2-Methylphenol
ND
5.0
10.0
3/4-Methylphenol
18
5.0
10.0
N-Nitroso-di-n-propylamine
ND
5.0
10.0
N-Nitrosodimethylamine
ND
5.0
10.0
N-Nitrosodiphenylamine
ND
5.0
10.0
Naphthalene
ND
5.0
10.0
4-Nitroaniline
ND
5.0
10.0
3-Nitroaniline
ND
5.0
10.0
2-Nitroaniline
ND
5.0
10.0
Nitrobenzene
ND
25
10.0
4-Nitrophenol
ND
5.0
10.0
2-Nitrophenol
ND
5.0
10.0
Pentachlorophenol
ND
25
10.0
Phenanthrene
ND
5.0
10.0
Phenol
ND
5.0
10.0
Pyrene
ND
5.0
10.0
Pyridine
ND
5.0
10.0
1,2,4-Trichlorobenzene
ND
5.0
10.0
2,4,6-Trichlorophenol
ND
5.0
10.0
2,4,5-Trichlorophenol
ND
5.0
10.0
Surrogate
Rec. (%)
Control Limits
Qualifiers,
2-Fluorobiphenyl
82
27-120
RL: Reporting Limit. DF: Dilution Factor.
MDL: Method Detection Limit.
7440 Lincoln Way Garden Grove CA 92841-1427 • TEL: [phone] • FAX: [phone]
t
0
U
0
a

Page 13 of 38
alscience
nvironmenta/
Analytical Report
Iff
aboratories, Inc.
Synagro Technologies, Inc.
Date Received: 02/22/14
5900 74th Street North
Work Order: 14-02-1588
St. Petersburg, FL 33709-1374
Preparation: EPA 3545
Method: EPA 8270C
Units: mg/kg
Project: Synagro - Pinellas Page 3 of 9
Surrooate Rec. M Control Limits Qualifiers
2-Fluorophenol 66 25-120
Nitrobenzene-d5 86 33-123
p-Terphenyl-d 14 82 27-159
Phenol-d6 65 26-122
2,4,6-Tribromophenol 80 18-138
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 14 of 38
alscience
Environmental
Analytical Report
r aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3545
Method:
EPA 8270C
Units:
mg/kg
Project: Synagro - Pinellas
Page 4 of 9
Client Sample Number
Lab Sample DatefTime
Matrix Instrument
Date
DatefTime QC Batch ID
Analyzed
Number Collected
Prepared
Syn-4
14-02.1588-4-A 02/21/14
Solid GC/MS TT
02/22/14
02/24/14 140222LOIA
12:20
17:00
Parameter
Besult
EL
lii r
Acenaphthene
ND
5.0
10.0
Acenaphthylene
ND
5.0
10.0
Aniline
ND
5.0
10.0
Anthracene
ND
5.0
10.0
Azobenzene
ND
5.0
10.0
Benzidine
ND
100
10.0
Benzo (a) Anthracene
ND
5.0
10.0
Benzo (a) Pyrene
ND
5.0
10.0
Benzo (b) Fluoranthene
ND
5.0
10.0
Benzo (g,h,i) Perylene
ND
5.0
10.0
Benzo (k) Fluoranthene
ND
5.0
10.0
Benzoic Acid
ND
25
10.0
Benzyl Alcohol
ND
5.0
10.0
Bis(2-Chloroethoxy) Methane
ND
5.0
10.0
Bis(2-Chloroethyl) Ether
ND
25
10.0
Bis(2-Chloroisopropyl) Ether
ND
5.0
10.0
Bis(2-Ethylhexyl) Phthalate
10
5.0
10.0
4-Bromophenyl-Phenyl Ether
ND
5.0
10.0
Butyl Benzyl Phthalate
ND
5.0
10.0
4-Chloro-3-Methylphenol
ND
5.0
10.0
4-Chloroaniline
ND
5.0
10.0
2-Chloronaphthalene
ND
5.0
10.0
2-Chlorophenol
ND
5.0
10.0
4-Chlorophenyl-Phenyl Ether
ND
5.0
10.0
Chrysene
ND
5.0
10.0
Di-n-Butyl Phthalate
ND
5.0
10.0
Di-n-Octyl Phthalate
ND
5.0
10.0
Dibenz (a,h) Anthracene
ND
5.0
10.0
Dibenzol'uran
ND
5.0
10.0
1,2-Dichlorobenzene
ND
5.0
10.0
1,3-Dichlorobenzene
ND
5.0
10.0
1,4-Dichlorobenzene
ND
5.0
10.0
3,3'-Dichlorobenzidine
ND
100
10.0
2,4-Dichlorophenol
ND
5.0
10.0
Diethyl Phthalate
ND
5.0
10.0
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]
d
3
E

Page 15 of 38
alsc%nce
nvironmenta/
Analytical Report
aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3545
Method:
EPA 8270C
Units:
mg/kg
Project: Synagro - Pinellas
Page 5 of 9
Parameter
&11111
EL
2E Qualifiers
D rnethyi Phthalate
ND
5.0
10.0
2,4-Dimethylphenol
ND
5.0
10.0
4,6-Din4tro-2-Methylphenol
ND
25
10.0
2,4-DiNtrophenol
ND
25
10.0
2,4-Dinitrotoluene
ND
5.0
10.0
2,6-Dinitrotoluene
ND
5.0
10.0
Fluoranthene
ND
5.0
10.0
Fluorene
ND
5.0
10.0
Hexechloro-1,3-Butadiene
ND
5.0
10.0
Hexachlorobenzene
ND
5.0
10.0
Hexachlorocyctopentadiene
ND
25
10.0
Hexachloroethane
ND
5.0
10.0
Indeno (1,2,3-c,d) Pyrene
ND
5.0
10.0
Isophorone
ND
5.0
10.0
2-Methylnaphthatene
ND
5.0
10.0
1-Methyinaphthalene
ND
5.0
10.0
2-Methylphenol
ND
5.0
10.0
3/4-Methylphenot
16
5.0
10.0
N-Nitroso-di-n-propylamine
ND
5.0
10.0
N-Nitrosodirnethylamine
ND
5.0
10.0
N-Nitrosodiphenyiamine
ND
5.0
10.0
Naphthalene
ND
5.0
10.0
4-Nitroaniline
ND
5.0
10.0
3-Nitroaniline
ND
5.0
10.0
2-Nitroaniline
ND
5.0
10.0
Nitrobenzene
ND
25
10.0
4-Nitrophenol
ND
5.0
10.0
2-Nitrophenol
ND
5.0
10.0
Pentachlorophenol
ND
25
10.0
Phenanthrene
ND
5.0
10.0
Phenol
ND
5.0
10.0
Pyrene
ND
5.0
10.0
Pyridine
ND
5.0
10.0
1,2,4-Trichlorobenzene
ND
5.0
10.0
2,4,6-Trichlorophenol
ND
5.0
10.0
2,4,5-Trichlorophenol
ND
5.0
10.0
Surrogate
Rec. M
Control Limits
Qualifiers
2-Fluorobiphenyl
73
27-120
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 16 of 38
a/science
Analytical Report
Environmental
aboratories, Inc.
Synagro Technologies, Inc. Date Received: 02/22/14
5900 74th Street North Work Order: 14-02-1588
St. Petersburg, FL 33709-1374 Preparation: EPA 3545
Method: EPA 8270C
Units: mg/kg
Project: Synagro - Pinellas Page 6 of 9
Surrowte
Rec. (%1
Control Limits Qualifers
2-Fluorophenol
54
25-120
Nitrobenzene-d5
72
33-123
p-Terphenyl-d14
73
27-159
Phenol-d6
55
26-122
2,4,6-Tribromophenol
70
18-138
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 17 of 38
alscience
nvironmental Analytical Report
aboratories, Inc.
Synagro Technologies, Inc. Date Received: 02/22/14
5900 74th Street North Work Order: 14-02-1588
St. Petersburg, FL 33709-1374 Preparation: EPA 3545
Method: EPA 8270C
Units: mg/kg
Project: Synagro - Pinellas Page 7 of 9
Client Sample Number Lab Sample Date/Time Matrix Instrument Date Daterrime QC Batch ID
Number Collected Prepared Analyzed
Method Blank 099-12549-2858 N/A Solid GC/MS TT 02/22/14 02/24/14 140222L01A
11:45
Parameter
Result
EL
PFF
Qualifiers
Acenaphthene
ND
0.50
1.00
Acenaphthylene
ND
0.50
1.00
Aniline
ND
0.50
1.00
Anthracene
ND
0.50
1.00
Azobenzene
ND
0.50
1.00
Benzidine
ND
10
1.00
Benzo (a) Anthracene
ND
0.50
1.00
Benzo (a) Pyrene
ND
0.50
1.00
Benzo (b) Fluoranthene
ND
0.50
1.00
Benzo (g,h,i) Perylene
ND
0.50
1.00
d
Benzo (k) Fluoranthene
ND
0.50
1.00
o
Benzoic Acid
ND
2.5
1.00
U
a
Benzyl Alcohol
ND
0.50
1.00
Bis(2-Chloroethoxy) Methane
ND
0.50
1.00
Bis(2-Chloroethyl) Ether
ND
2.5
1.00
Bis(2-Chloroisopropyl) Ether
ND
0.50
1.00
Bis(2-Ethylhexyl) Phthalate
ND
0.50
1.00
4-Bromophenyl-Phenyl Ether
ND
0.50
1.00
Butyl Benzyl Phthalate
ND
0.50
1.00
4-Chloro-3-Methylphenol
ND
0.50
1.00
4-Chloroaniline
ND
0.50
1.00
2-Chloronaphthalene
ND
0.50
1.00
2-Chlorophenol
ND
0.50
1.00
4-Chlorophenyl-Phenyl Ether
ND
0.50
1.00
Chrysene
ND
0.50
1.00
Di-n-Butyl Phthalate
ND
0.50
1.00
Di-n-Octyl Phthalate
ND
0.50
1.00
Dibenz (a,h) Anthracene
ND
0.50
1.00
Dibenzofuran
ND
0.50
1.00
1,2-Dichlorobenzene
ND
0.50
1.00
1,3-Dichlorobenzene
ND
0.50
1.00
1,4-Dichlorobenzene
ND
0.50
1.00
3,3'-Dichlorobenzidine
ND
10
1.00
2,4-Dichlorophenol
ND
0.50
1.00
Diethyl Phthalate
ND
0.50
1.00
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 18 of 38
a/science
Environmental
Analytical Report
aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3545
Method:
EPA 8270C
Units:
mg/kg
Project: Synagro - Pinellas
Page 8 of 9
Pararnete
Result
F-L
PIE Qualifiers
Dimethyl Phthalate
ND
0.50
1.00
2,4-Dimethylphenot
ND
0.50
1.00
4,6-Dinitro-2-Methylphenol
ND
2.5
1.00
2,4-Dinitrophenol
ND
2.5
1.00
2,4-Dinitrotoluene
ND
0.50
1.00
2,6-Dinitrotoluene
ND
0.50
1.00
Fluoranthene
ND
0.50
1.00
Fluorene
ND
0.50
1,00
Hexachloro-1,3-Butadiene
ND
0.50
1.00
Hexachlorobenzene
ND
0.50
1.00
Hexachlorocyclopentadiene
ND
2.5
1.00
Hexachloroethane
ND
0.50
1.00
Indeno (1,2,3-c,d) Pyrene
ND
0.50
1.00
Isophorone
ND
0.50
1.00
2-Methytnaphthalene
ND
0.50
1.00
1-Methytnaphthalene
ND
0.50
1.00
2-Methylphenol
ND
0.50
1.00
3/4-Methylphenol
ND
0.50
1.00
N-Nitroso-di-n-propylamine
ND
0.50
1.00
N-Nitrosodimethylamine
ND
0.50
1.00
N-Nitrosodiphenylamine
ND
0.50
1.00
Naphthalene
ND
0.50
1.00
4-Nitroaniline
ND
0.50
1.00
3-Nitroaniline
ND
0.50
1.00
2-Nitroaniline
ND
0.50
1.00
Nitrobenzene
ND
2.5
1.00
4-Nitrophenol
ND
0.50
1.00
2-Nitrophenol
ND
0.50
1.00
Pentachlorophenol
ND
2.5
1.00
Phenanthrene
ND
0.50
1.00
Phenol
ND
0.50
1.00
Pyrene
ND
0.50
1.00
Pyridine
ND
0.50
1.00
1,2,4-Trichlorobenzene
ND
0.50
1.00
2,4,6-Trichlorophenol
ND
0.50
1.00
2,4,5-Trichlorophenol
ND
0.50
1.00
Surrogate
Rec. (%)
Control Limits
Qualifiers
2-Fluorobiphenyl
92
27-120
RL: Reporting Limit. DF: Dilution Factor.
MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]
0
U
0
E
d

Page 19 of 38
alscience
Environmental Analytical Report
aboratories, Inc.
Synagro Technologies, Inc. Date Received: 02/22/14
5900 74th Street North Work Order: 14-02-1588
St. Petersburg, FL 33709-1374 Preparation: EPA 3545
Method: EPA 8270C
Units: mg/kg
Project: Synagro - Pinellas Page 9 of 9
Surrogate
Rec. (%)
Control Limits Qualifiers
2-Fluorophenol
90
25-120
Nitrobenzene-d5
98
33-123
p-Terphenyl-d 14
92
27-159
Phenol-d6
90
26-122
2,4,6-Tribromophenol
96
18-138
t
d
0
U
0
c
d
K
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 20 of 38
aISC%enCe
Analytical Report
nvironmenta/
aborator%s, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 1311
Method:
EPA 8260E
Units:
ug/L
Project: Synagro - Pinellas
Page 1 of 4
Client Sample Number
Lab Sample Date/Time
Number Collected
Matrix Instrument
Date
Prepared
Date/Time QC Batch ID
Analyzed
Syn-5
14-02-1588-5-A 02121/14
Solid GC/MS JJ
02/21/14
02/25/14 1402251-02
12:21
16:12
Parameter
Result
EL
PFF
Qualifiers
Acetone
ND
2000
1.00
Benzene
ND
50
1.00
Bromobenzene
ND
100
1.00
Bromochloromethane
ND
100
1.00
Bromodichloromethane
ND
100
1.00
Bromoform
ND
100
1.00
Bromomethane
ND
1000
1.00
2-Butanone
ND
1000
1.00
n-Butylbenzene
ND
100
1.00
sec-Butylbenzene
ND
100
1.00
tert-Butylbenzene
ND
100
1.00
Carbon Disulfide
ND
1000
1.00
Carbon Tetrachloride
ND
50
1.00
Chlorobenzene
ND
100
1.00
Chlorcethane
ND
200
1.00
Chloroform
ND
100
1.00
Chloromethane
ND
1000
1.00
2-Chlorotoluene
ND
100
1.00
4-Chlorotoluene
ND
100
1.00
Dibromochloromethane
ND
100
1.00
1,2-Dibromo-3-Chloropropane
ND
500
1.00
1,2-Dibromoethane
N D
100
1.00
Dibromomethane
ND
100
1.00
1,2-Dichlorobenzene
ND
100
1.00
1,3-Dichlorobenzene
ND
100
1.00
1,4-Dichlorobenzene
ND
100
1.00
Dichlorodifluoromethane
ND
100
1.00
1,1-Dichloroethane
ND
100
1.00
1,2-Dichloroethane
ND
50
1.00
1,1-Dichloroethene
ND
100
1.00
c-1,2-Dichloroethene
ND
100
1.00
t-1,2-Dichloroethene
ND
100
1.00
1,2-Dichloropropane
ND
100
1.00
1,3-Dichloropropane
ND
100
1.00
2,2-Dichloropropane
ND
100
1.00
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] • FAX: [phone]

Page 21 of 38
alscience
nvironmentai
Analytical Report
aboratories, inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 1311
Method:
EPA 8260B
Units:
ug/L
Project: Synagro - Pinellas
Page 2 of 4
Parameter
Result
RL
DF
Qualifiers
1,1-Dichloropropene
ND
100
1.00
c-1,3-Dichloropropene
ND
50
1.00
t-1,3-Dichbropropene
ND
50
1.00
Ethytbenzene
ND
100
1.00
2-Hexanone
ND
1000
1.00
tsopropylbenzene
ND
100
1.00
p-Isopropyltoluene
ND
100
1.00
Methylene Chloride
ND
1000
1.00
4-Methyl-2-Pentanone
ND
1000
1.00
Naphthalene
ND
1000
1.00
n-Propylbenzene
ND
100
1.00
Styrene
ND
100
1.00
1,1,1,2-Tetrachloroethane
ND
100
1.00
1,1,2,2-Tetrachloroethane
ND
100
1.00
Tetrachloroethene
ND
100
1.00
Toluene
ND
100
1.00
1,2,3-Trichlorobenzene
ND
100
1.00
1,2,4-Trichlorobenzene
ND
100
1.00
1,1,1-Trichloroethane
ND
100
1.00
1,1,2-Trichloroethane
ND
100
1.00
Trichloroethene
ND
100
1.00
Trichlorofluoromethane
ND
1000
1.00
1,2,3-Trichloropropane
ND
500
1.00
1,2,4-Trimethylbenzene
ND
100
1.00
1, 3, 5-Trimethylbenzene
ND
100
1.00
Vinyl Acetate
ND
1000
1.00
Vinyl Chloride
ND
50
1.00
p/m-Xylene
ND
100
1.00
o-Xyiene
ND
100
1.00
Methyl-t-Butyl Ether (MTBE)
ND
100
1.00
Surroaale
Rec. (%)
Control Limits
Qualifiers
1,4-Bromofluorobenzene
96
80-120
Dibromonuoromethane
105
80-126
1,2-Dichloroethane-d4
105
80-134
Toluene-d8
95
80-120
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]
FF,
lJ

Page 22 of 38
alscience
nvironmenta/
Analytical
Report
iff
aboratorfes, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 1311
Method:
EPA 8260E
Units:
ug/L
Project: Synagro - Pinellas
Page 3 of 4
Client Sample Number Lab Sample
Date/Time
Matrix Instrument
Date
Date/Time QC Batch ID
Number
Collected
Prepared
Analyzed
Method Blank 099-14-519-571 N/A
Aqueous GC/MS JJ
02/21/14
02/25/14 140225E
15:13
Parameter
Result
EL
PFF
li r
Acetone
ND
2000
1.00
Benzene
ND
50
1.00
Bromobenzene
ND
100
1.00
Bromochloromethane
ND
100
1.00
Bromodichloromethane
ND
100
1.00
Bromoform
ND
100
1.00
Bromomethane
ND
1000
1.00
2-Butanone
ND
1000
1.00
n-Butylbenzene
ND
100
1.00
sec-Butylbenzene
ND
100
1.00
tert-Butylbenzene
ND
100
1.00
Carbon Disulfide
ND
1000
1.00
Carbon Tetrachloride
ND
50
1.00
Chlorobenzene
ND
100
1.00
Chloroethane
ND
200
1.00
Chloroform
ND
100
1.00
Chloromethane
ND
1000
1.00
2-Chlorotoluene
ND
100
1.00
4-Chlorotoluene
ND
100
1.00
Dibromochloromethane
ND
100
1.00
1,2-Dibromo-3-Chloropropane
ND
500
1.00
1,2-Dibromoethane
ND
100
1.00
Dibromomethane
ND
100
1.00
1,2-Dichlorobenzene
ND
100
1.00
1,3-Dichlorobenzene
ND
100
1.00
1,4-Dichlorobenzene
ND
100
1.00
Dichlorodifluoromethane
ND
100
1.00
1,1-Dichloroethane
ND
100
1.00
1,2-Dichloroethane
ND
50
1.00
1,1-Dichloroethene
ND
100
1.00
c-1,2-Dichloroethene
ND
100
1.00
t-1,2-Dichloroethene
ND
100
1.00
1,2-Dichloropropane
ND
100
1.00
1,3-Dichloropropane
ND
100
1.00
2,2-Dichloropropane
ND
100
1.00
RL: Reporting Limit. DF: Dilution Factor.
MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 23 of 38
alscience
Environmental
Analytical Report
aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 1311
Method:
EPA 8260E
Units:
ug/L
Project: Synagro - Pinellas
Page 4 of 4
Parameter
Result
EL
PF Qualifiers
1,1-Dichloropropene
ND
100
1.00
c-1,3-Dichloropropene
ND
50
1.00
t-1,3-Dichloropropene
ND
50
1.00
Ethylbenzene
ND
100
1.00
2-Hexanone
ND
1000
1.00
Isopropylbenzene
N D
100
1.00
p-Isopropyttoluene
ND
100
1.00
Methylene Chloride
ND
1000
1.00
4-Methyl-2-Pentanone
ND
1000
1.00
Naphthalene
ND
1000
1.00
n-Propylbenzene
ND
100
1.00
Styrene
ND
100
1.00
1,1,1, 2-Tetrachloroethane
ND
100
1.00
1,1,2, 2-Tetrachloroethane
ND
100
1.00
Tetrachloroethene
ND
100
1.00
Toluene
ND
100
1.00
1,2,3-Trichlorobenzene
ND
100
1.0o
1,2,4-Trichlorobenzene
ND
100
1.00
1, 1, 1 -Trichforoethane
ND
100
1.00
1,1,2-Trichloroethane
ND
100
1.00
Trichloroethene
ND
100
1.00
Trichlorofluoromethane
ND
1000
1.00
1,2,3-Trichloropropane
N D
500
1.00
1,2,4-Trimethylbenzene
ND
100
1.00
1,3,5-Trimethylbenzene
ND
100
1.00
Vinyl Acetate
ND
1000
1.00
Vinyl Chloride
ND
50
1.00
plm-Xylene
ND
100
1.00
o-Xylene
ND
100
1.00
Methyl-t-Butyl Ether (MTBE)
ND
100
1.00
Surrogate
Rec.
('/ol Control Limits
Qualifiers
1,4-Bromofluorobenzene
95
80-120
Dibromofluoromethane
108
80-126
1,2-Dichloroethane-d4
105
80-134
Toluene-d8
100
80-120
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 24 of 38
I
alsc%nce
nvlronmenta/ Quality Control -Spike/Spike Duplicate
aborator/es, Inc.
Synagro Technologies, Inc. Date Received: 02/22/14
5900 74th Street North Work Order: 14-02-1588
St. Petersburg, FL 33709-1374 Preparation: EPA 3050E
Method: EPA 6010B
Project: Synagro - Pinellas Page 1 of 4
luality Control Sample ID
Type
Matrix
Instrument
Date Prepared
Date Analyzed MSIMSD Batch Numbei
4-02-1562-3
Sample
Solid
ICP 7300
02/211/4
02/21/14 23:55 140221S09
4-02-1562-3
Matrix Spike
Solid
ICP 7300
02/21/14
02121114 23:51 140221S09
4-02-1562-3
Matrix Spike Duplicate
Solid
ICP 7300
02121/14
02121/14 23:52 140221S09
Parameter
amole
SDjke
i
7.
%gec. CL
$PQ
RPD CL
lifi em
Conc.
Added
Conc•
�
Conc•
Antimony
ND
25.00
7.195
29
7.827
31
50-115
8
0-20
3
Arsenic
ND
25.00
23.47
94
24.42
98
75-125
4
0-20
Barium
76.84
25.00
85.21
34
87.72
44
75-125
3
0-20
3
Beryllium
0.4836
25.00
26.60
104
26.81
105
75-125
1
0-20
Cadmium
ND
25.00
25.39
102
25.47
102
75-125
0
0-20
Chromium
42.86
25.00
69.13
105
76.87
136
75-125
11
0-20
3
Cobalt
Copper
16.06
22.55
25.00
25.00
43.00
47.04
100
98
46.78
49.54
115
108
75-125
75-125
8
5
0-20
0-20
Lead
2.640
25.00
27.47
99
28.69
104
75-125
4
0-20
Molybdenum
ND
25.00
22.12
68
21.54
86
75-125
3
0-20
Nickel
61.54
25.00
64.86
13
76.18
59
75-125
16
0-20
3
Selenium
ND
25.00
22.75
91
21.34
85
75-125
6
0-20
0
Silver
ND
12.50
13.59
109
13.60
109
75-125
0
0-20
Thallium
ND
25.00
14.68
59
14.42
58
75-125
2
0-20
3
Vanadium
40.30
25.00
67.80
110
76.15
143
75-125
12
0-20
3
Zinc
44.17
25.00
63.96
79
70.61
106
75-125
10
0-20
RPD: Relative Percent Difference. CL: Control Limits
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]

Page 25 of 38
I
alsc%nce
Environmental
Quality Control - Spike/Spike Duplicate
aborator/es, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 7471A Total
Method:
EPA 7471A
Project: Synagro - Pinellas
Page 2 of 4
Quality Control Sample ID
Type
Matrix
Instrument
Date Prepared
Date Analyzeo mzwm5u tsatcn rvumoer
Sample
Solid
Mercury
02/22/14
0212211411:21 140222503
E14-002-1534-2
-1534-2
Matrix Spike
Solid
Mercury
02/22/14
02122/1411:28 140222503
-1534-2
Matrix Spike Duplicate
Solid
Mercury
02122/14
02i22/1411:30 140222503
Parameter Sample aa& fM A�%L %oRec. CL RPD RPD CLQualifiers
Conc. Added Conc' 1sRec 9gm lsRec.
Mercury ND 0.8350 0.6508 78 0.6439 77 71-137 1 0-14
RPD: Relative Percent Difference. CL: Control Limits
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]
0
o
0
E
s

Page 26 of 38
alscience
Quality Control -Spike/Spike Duplicate
Environmental
aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3545
Method:
EPA 8082
Project: Synagro - Pinellas
Page 3 of 4
Quality Control Sample ID
Type
Matrix
Instrument
Date Prepared
Date Analyzed MS/MSD Batch Number
Sample
Sediment
GC 66
02/22/14
02/25/14 01:40 140222502
F14-002-1389-1
-1389-1
Matrix Spike
Sediment
GC 66
02/22/14
02/25/14 01:04 140222S02
-1389-1
Matrix Spike Duplicate
Sediment
GC 66
02/22/14
02/25/14 01:22 140222502
Parameter Samole Spike
IVIS
n
Map MD %R . CL B� > ' 1� if
.0 . Added
Conc.
° R -
-Q 1;7e-c
Aroclor-1016 ND 100.0
72.54
73
114.3 114 50-135 45 0-20 4
Aroclor-1260 249.3 100.0
341.4
92
336.3 87 50-135 1 0-25
RPD: Relative Percent Difference. CL: Control Limits
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]

Page 27 of 38
alscience
Quality Control -Spike/Spike Duplicate
Environmentalim
aboratories, Inc.
Synagro Technologies, Inc. Date Received: 02/22/14
5900 74th Street North Work Order: 14-02-1588
St. Petersburg, FL 33709-1374 Preparation: EPA 1311
Method: EPA 8260E
Project: Synagro - Pinellas Page 4 of 4
2uality Control Sample ID
Type
Matrix
Instrument
Date Prepared
Date Analyzed MS/MSD Batch Number
lyn-5
Sample
Solid
GUMS JJ
02/21/14
02/25/1416:12 140225S02
lyn-5
Matrix Spike
Solid
GUMS JJ
02121/14
02/2511418:11 140225S02
lyn-5
Matrix Spike Duplicate
Solid
GC/MS JJ
02/21114
02125/1418:41 140225S02
Parameter
Sample
Scike
M
MS
°/°Rec. CL
RPD
RPD CL
ualifi r
Conc.
Added
Conc.
�
Benzene
ND
5000
5066
101
5093
102
78-120
1
0-20
Carbon Tetrachloride
ND
5000
5176
104
5097
102
67-139
2
0-20
Chiorobenzene
ND
5000
5191
104
5264
105
M120
1
0-20
1,2-Dibromoethane
ND
5000
5257
105
5359
107
80-123
2
0-20
1,2-Dichlorobenzene
ND
5000
5369
107
5497
110
76-120
2
0-20
1,2-Dichioroethane
ND
5000
4697
94
4703
94
76-130
0
0-20
1,1-Dichloroethene
Ethylbenzene
ND
ND
5000
5000
4935
5136
99
103
4994
5192
100
104
70-130
73-127
1
1
0-27
0-20
Toluene
ND
50M
5163
103
5147
103
72-126
0
0-20
Trichloroethene
ND
5000
4950
99
4926
99
74-122
0
0-20
v
Vinyl Chloride
ND
5000
4728
95
4818
96
65-131
2
0-24
01
p/m-Xylene
ND
10000
10880
109
11010
110
70-130
1
0-30
O
o-Xylene
ND
5000
5682
114
5775
115
70-130
2
0-30
Methyl-t-Butyl Ether (MTBE)
ND
5000
5286
106
5116
102
69-123
3
0-20
RPD: Relative Percent Difference. CL: Control Limits
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]

Page 28 of 38
alscience
k-pWronmental
Quality Control -Sample Duplicate
1. aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
N/A
Method:
SM 2540 B (M)
Project: Synagro - Pinellas
Page 1 of 1
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed Duplicate Batch Number
r-1 Sample Solid NIA 02/22/14 00:00 02/22114 17:15 E0222TSDI
n-1 Sample Duplicate Solid NIA 02/22/14 00:00 02/2211417:15 E0222TSDI
Parameter Samole Conc. DUP Conc. RPD RPD CL Qualifiers
Solids, Total 91.20 91.30 0 0-10
RPD: Relative Percent Difference. CL: Control Limits
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 29 of 38
1
alscience
Environmental
aboratories, Inc.
Quality Control - LCS
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3050E
Method:
EPA 6010E
Project: Synagro - Pinellas
Page 1 of 5
Quality Control Sample ID
Type Matrix
Instrument
Date Prepared Date Analyzed LCS Batch Number
097-01-002-18047
LCS Solid
ICP7300
02/21/14 02121/1423:49 140221L09
Parameter
Soike Added
Conc.
LCS %°Rec. %Rec. CL
ME CL Qualifiers
vered
Antimony
25.00
24.69
99
80-120
73-127
Arsenic
25.00
24.55
98
80-120
73-127
Barium
25.00
25.70
103
80-120
73-127
Beryllium
25.00
24.32
97
80-120
73-127
Cadmium
25.00
26.18
105
80-120
73-127
Chromium
25.00
25.80
103
80-120
73-127
Cobalt
25.00
28.23
113
80-120
73-127
Copper
25.00
26.37
105
80-120
73-127
Lead
25.00
26.34
105
80-120
73-127
Molybdenum
25.00
25.65
103
80-120
73-127
Nickel
25.00
27.29
109
80-120
73-127
Selenium
25.00
24.08
96
80-120
73-127
Silver
12.50
13.31
107
80-120
73-127
Thallium
25.00
27.31
109
80-120
73-127
Vanadium
25.00
24.67
99
80-120
73-127
Zinc
25.00
25.77
103
80-120
73-127
Total number of LCS compounds: 16
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
RPD: Relative Percent Difference. CL: Control Limits
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]

Page 30 of 38
alscience
Quality Control -LCS
Environmental
aboratories, Inc.
Synagro Technologies, Inc. Date Received: 02/22/14
5900 74th Street North Work Order: 14-02-1588
St. Petersburg, FL 33709-1374 Preparation: EPA 7471A Total
Method: EPA 7471A
Project: Synagro - Pinellas Page 2 of 5
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number
U99-16-272-41 LCS Solid Mercury 02122114 02/2211411:17 140222L03
1 ram Spike Added Conc. Recovered LCS %Rea %Rec. CL Qualifiers
Mercury 0.8350 0.7268 87 85-121
RPD: Relative Percent Difference. CL: Control Limits
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]

Page 31 of 38
alscience
environmental
Quality Control
-LCS
1. aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3545
Method:
EPA 8082
Project: Synagro - Pinellas
Page 3 of 5
Quality Control Sample ID Type
Matrix
Instrument Date Prepared Date Analyzed
LCS Batch Number
099-12-535-2494 LCS
Solid
GC 66 02/22114 02/25114 00:29 1402221-02
Parameter
Spike Added
Conc, Recovered LCS %Rec. %Rec.
CL Qualifiers
Aroclor-1016
100.0
94.86 95 50-135
Aroclor-1260
100.0
102.6 103 50-135
RPD: Relative Percent Difference. CL: Control Limits
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] • FAX: [phone]

Page 32 of 38
alscience
nvironmenta/
Quality Control -LCS
aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 3545
Method:
EPA 8270C
Project: Synagro - Pinellas
Page 4 of 5
Quality Control Sample ID
Type Matrix
Instrument
Date Prepared Date Analyzed LCS Batch Number
0 99-12-549-2858
LCS Solid
GC/MS TT
02/22/14 02/24114 12:03 140222L01A
Parameter
Spike Added
Conc.
LCS %Rec. %Rec. CL
ME CL Qualifier§
Recovered
Acenaphthene
10.00
9,048
90
51-123
39-135
Acenaphthylene
10.00
8.994
90
52-120
41-131
Butyl Benzyl Phthalate
10.00
8.906
89
43-139
27-155
4-Chloro-3-Methylphenol
10.00
9.124
91
55-121
44-132
2-Chlorophenol
10.00
9.093
91
58-124
47-135
1,4-Dichlorobenzene
10.00
8.922
69
42-132
27-147
Dimethyl Phthalate
10.00
8.641
86
51-123
39-135
2,4-Dinitrotoluene
10.00
10.15
101
51-129
38-142
Fluorene
10.00
9.316
93
54-126
42-138
N-Nitroso-di-n-propylamine
10.00
8.774
68
40-136
24-152
Naphthalene
10.00
8,831
88
32-146
13-165
4-Nitrophenol
10.00
10.02
100
24-126
7-143
Pentachlorophenol
10.00
8.837
88
23-131
5-149
Phenol
10.00
8.946
69
40-130
25-145
Pyrene
10.00
9.427
94
47-143
31-159
1,2,4-Trichlorobenzene
10.00
8.961
90
45-129
31-143
Total number of LCS compounds: 16
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
RPD: Relative Percent Difference. CL: Control Limits
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]
0
U
o
E

Page 33 of 38
a/science
nvironmenta!
Quality Control -LCS
1. aboratories, Inc.
Synagro Technologies, Inc.
Date Received:
02/22/14
5900 74th Street North
Work Order:
14-02-1588
St. Petersburg, FL 33709-1374
Preparation:
EPA 5030C
Method:
EPA 8260E
Project: Synagro - Pinellas
Page 5 of 5
Quality Control Sample ID Type
Matrix Instrument
Date Prepared Date Analyzed LCS Batch Number
099-14-519-571 LCS
Aqueous GC/MS JJ
02/25/14 02/25/1413:12 140225L02
arm ter
Spike Added Conc.
vered
LCS %Rec. %Rec. CL
ME CL Qualifiers
Benzene
50.00
52.97
106
80-120
73-127
Carbon Tetrachloride
50.00
53.27
107
66-138
54-150
Chlorobenzene
50.00
54.52
109
80-120
73-127
1,2-Dibromoethane
50.00
53.95
108
80-120
73-127
1,2-Dichlorobenzene
50.00
55.22
110
80-120
73-127
1,2-Dichloroethane
50.00
48.47
97
80-129
72-137
1,1-Dichloroethene
50.00
51.95
104
71-131
61-141
Ethylbenzene
50.00
54.50
109
80-123
73-130
Toluene
50.00
53.15
106
79-121
72-128
Trichloroethene
50.00
52.25
105
80-120
73-127
Vinyl Chloride
50.00
49.97
100
70-136
59-147
p/m-Xylene
100.0
114.4
114
75-125
67-133
i'
d
o-Xylene
50.00
59.50
119
75-125
67-133
10
Methyl-t-Butyl Ether (MTBE)
50.00
53.50
107
72-126
63-135
°
Total number of LCS compounds: 14
u
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
RPD: Relative Percent Difference. CL: Control Limits
7440 Lincoln Way, Garden Grove, CA 92841-1427 - TEL: [phone] - FAX: [phone]

Page 34 of 38
aiscience
Environmental
Sample Analysis Summary Report
aboratories, Inc.
Work Order: 14-02-1588
Page 1 of 1
Method
Extraction
Chemist ID
instrument
Analytical Location
EPA 6010B
EPA 3050B
469
ICP 7300
1
EPA 7471A
EPA 7471A Total
769
Mercury
1
EPA 8082
EPA 3545
669
GC 66
1
EPA 8260B
EPA 1311
876
GC/MS JJ
2
EPA 8270C
EPA 3545
449
GC/MS TT
1
SM 2540 B (M)
N/A
689
NIA
1
0
U
0
m
Location 1: 7440 Lincoln Way, Garden Grove, CA 92841
Location 2: 7445 Lampson Avenue, Garden Grove, CA 92841
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: [phone] • FAX: [phone]

Page 35 of 38
a/science
nWronmenta/ Glossary of Terms and Qualifiers
Au-iff
LF aboratories, Inc.
Work Order: 14-02-1588 Page 1 of 1
Qualifiers Definition
* See applicable analysis comment.
< Less than the indicated value.
> Greater than the indicated value.
1 Surrogate compound recovery was out of control due to a required sample dilution. Therefore, the sample data was reported without further
clarification.
2 Surrogate compound recovery was out of control due to matrix interference. The associated method blank surrogate spike compound was
in control and, therefore, the sample data was reported without further clarification.
3 Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The
associated LCS recovery was in control.
4 The MS/MSD RPD was out of control due to suspected matrix interference.
5 The PDS/PDSD or PES/PESD associated with this batch of samples was out of control due to suspected matrix interference.
6 Surrogate recovery below the acceptance limit.
7 Surrogate recovery above the acceptance limit.
B Analyte was present In the associated method blank.
BU Sample analyzed after holding time expired.
BV Sample received after holding time expired.
E Concentration exceeds the calibration range.
ET Sample was extracted past end of recommended max. holding time.
HD The chromatographic pattern was inconsistent with the profile of the reference fuel standard.
HDH The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but heavier hydrocarbons
were also present (or detected).
HDL The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but tighter hydrocarbons were
also present (or detected).
J Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value is
estimated.
JA Analyte positively identified but quantitation is an estimate.
ME LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean).
ND Parameter not detected at the indicated reporting limit.
Q Spike recovery and RPD control limits do not apply resulting from the parameter concentration in the sample exceeding the spike
concentration by a factor of four or greater.
SG The sample extract was subjected to Silica Gel treatment prior to analysis.
X % Recovery and/or RPD out -of -range.
Z Analyte presence was not confirmed by second column or GC/MS analysis.
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are
reported on a wet weight basis.
Any parameter identified in 40CFR Part 136.3 Table it that is designated as "analyze immediately" with a holding time of — 15 minutes
(40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the
stated holding time unless received at the laboratory within 15 minutes of the collection time.
A calculated total result (Example: Total Pesticides) is the summation of each component concentration and/or, if "J" flags are reported,
estimated concentration. Component concentrations showing not detected (ND) are summed into the calculated total result as zero
concentrations.
7440 Lincoln Way, Garden Grove, CA 92841-1427 * TEL: [phone] * FAX: [phone]

clisclenca
AS vironment<TI
Zboratortes, Inc.
7440 LINCOLN WAY
GARDEN GROVE, CA 92841-1432
TEL: [phone] . FAX: [phone]
CHAIN OF CUSTODY RECORD
DATE:
PAGE
OF
LABORATORY CLIENT:
Synagro Technologies
�. c r 0 _ 'po
••
ADDRESS:
5900 74th Street North
PROJECT COtrr
I'( 177 6USCH
QUOTE NO.:
CITY:
St. PetersbuEq, FL
SAMPLER(S): (SIGNATURE)
J � Mcmn;nq
TEL:
727-386-7931
FAX:
727-646.7432
E-MAIL
ftynagro.com
mbusch
SAME DAY 24 HR ❑ 48HR ❑ 72 HR ❑ 5 DAYS ❑10 DAYS
REQUESTED ANALYSIS
SPECIAL REQUIREMENTS (ADDITIONAL. COSTS MAY APPLY)
❑ RWQCB REPORTING ARCHIVE SAMPLES UNTIL 3 if r ,
R
J
SPECIAL INSTRUCTIONS
Present results in both wet and dry weight basis for metals (WET).
Run STLC if any metal parameter wet concentration is >1Ox STLC
RUSHI RUSHI RUSHI please.
u
In
CD
>
m
'
se
SAMPLEro
LOCATION/ �W
DIESCR► MON
SAMPLING
DATE
TIME
,
H
/
p
Q
n
Y rl `
Nk
a
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P��vrS.
Re�ttgilimhed by: (S
Received by (Signature)
Date:
Time:
ReHnquiahed by: (Sgnature
Received by: (Signature)
Dr/
Time:O v
_
Z
Re*xruished by: (Signature)
Received by: (Signature)
Date:
Time:
d
0
(D
W
0)
O
W
00
Return to Contents N*

Page 37 of 38
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Page 38 of 38
WORK ORDER M U-02"D DOE-
0
ler - of
CLIENT: �� ��` DATE 02 1Z -2-1 14
TEMPERATURE: Thermometer ID: SC1 (Criteria: 0.0 °C — 6.0 °C, not frozen except sediment/tissue)
Temperature 3- - 0 OC - 0.3°C (CF) = 2 .1—°C ❑ Blank` [Sample
❑ Sample(s) outside temperature criteria (PM/APM contacted by: )
❑ Sample(s) outside temperature criteria but received on ice/chilled on same day of sampling.
❑ Received at ambient temperature, placed on ice for transport by Courier.
Ambient Temperature: ❑ Air ❑ Filter
Checked by:
-L.
CUSTODY SEALS INTACT:
❑ Cooler ❑ ❑ No (Not Intact) 2 Not Present
❑ N/A
Checked by:
❑ Sample ❑ ❑ No (Not Intact) Not Present
Checked by: 000
SAMPLE CONDITION: Yes
Chain -Of -Custody (COC) document(s) received with samples ...................
No
❑
NIA
❑
t
COC document(s) received complete ...................................................
❑
❑
v
C�7I Collection date/time, matrix, and/or # of containers togged in based on sample labels.
❑ No analysis requested. ❑ Not relinquished. 0 No date/time relinquished.
0
E
Sampler's name indicated on COC ................................. ....................l
❑
❑
Sample container label(s) consistent with COC.....................................
/¢'
❑
❑
Sample container(s) intact and good condition ......................................
//a.
❑
❑
Proper containers and sufficient volume for analyses requested ...............
❑
❑
Analyses received within holding time .................................................
❑
❑
Aqueous samples received within 15-minute holding time
❑ pH ❑ Residual Chlorine ❑ Dissolved Sulfides ❑ Dissolved Oxygen...........
❑
❑
jd
Proper preservation noted on COC or sample container .......................... ❑ ❑ A
❑ Unpreserved vials received for Volatiles analysis
Volatile analysis container(s) free of headspace..................................... ❑ ❑
Tediar bag(s) free of condensation...................................................... ❑ ❑
CONTAINER TYPE:
Solid: 04ozCGJ 08ozCGJ 016ozCGJ ❑Sleeve ❑EnCoree ❑TerraCoree C2f
Aqueous: ❑VOA ❑VOAh 0V0Ana2 0125AGB 0125AGBh 0125AGBp ❑1AGB01AGBna2 01AGBs
0500AGB 0500AGJ ❑500AGJs 0250AGB 0250CGB 0250CGBs 01PB 01PBna 0500PB
0250PB ❑250PBn 0125PB 0125PBznna 0100PJ 0100PJna2 ❑ ❑.` ❑
Air: ❑Tediare ❑Canister Other: ❑ Trip Blank Lot#: Lab led(Checked by: 'Q-
Container: C: Clear A: Amber P: Plastic G: Glass J: Jar B: Bottle Z: Ziploc/Resealable Bag E: Envelope-keviewed by:
Preservative: h: HCL n: HNO3 na2:Na2S203 na: NaOH p: H3PO4 s: H2SO4 u: Ultra -pure znna: ZnAc2+NaOH f: Fitenlf Scanned by:.
SOP T100 090 (07131113)

ANALYTICAL TEST REPORT-_
I 'THESE RESULTS MEET NELAC STANDARDS
Submission Number. 14030132
Synagro., Project Name: PINELLAS COUNTY PELLETIZER ..
P.O. Box -3227. .
Pinellas. Park, F.I. 33780 Date Received: 03/05/2014
Time,Received: 093.0
submission. Number 14030132
:. .
j
,
Sample Number: 001Sample Description: Pellets"
Sample Date: "03/05/201.4 Sample Method: Grab
Sample Tlm®:: •0723
Parameter Result.. Units tin: Procedure Analyst
.Detects . Analysis .
Limit' Date: _ Time
PH 7.07 Q UNITS 9045 : 0310512014. 13:11 _ TN/KR
TOTAL SOLIDS - 92.5 %DRY WT 0,1 'SM2546G 03/07/20'14 40:05 JA
FECAL COLIFORM: BY MPN., 0..195 U WGRAM . 0'.195 SM9221 E ' 03105h014 '09:48 KU
03111/2014 '
Dale D& J Laboratory` Director Date
Tillay :Tanrtsever/Jessica Sierra Medina:- QC Of
DATA'QUALIFIERS TNAT MAY APPLY: -
I = Reported Value Is lbetween theiaboratory MDL and the PQL . NOTES. 1: (PQL = U MDL).
J2 = Est. Value. No control criteria exists for, this component 2. SOUR calculations are based on total solids
J3 = Est: value qualky control cviterie for predslcn or accuracy iioi met: J2 = Per client request, analysis conducted without method blank
L Off scale high', Value Is known tobe> the valve reported:: A4 Est. value.: Sample matrix Interference suspected.
! Q =Sample held. beyond.the accepted holding time. X = Value exceed MCL.
U = Analyte not detected at the -value Indicated NOTES;
1 V =;Anaiyte detected'in sample and method blank.
Z = Too many colonies were present (TFITC). The numeric value represents the 1ptrailon .
volume.. .
6rauestions and comments regarding these results: please contact Bettina lieilfuss at [phone].'
Results relate only to the sampres.
{ All'.solid ;values are.reported on a dry weight basis
14030132 PAGE :1. OF 2
1711 12th Street Bast *.Palmetto, FL 34221 * Plione [phone] *.Fax [phone]

Summit Environmental Technologies, Inc.
3310 Win St.
�itl eO.aiF1Ft1`P�L 1C�ZQI lta#� 4, t€d Cuyahoga Falls Ohio 44223
i AAWkii0'AJ t0oWeasi TEL: [phone] FAX. [phone]
Website:-hKy,1Av tvv.settek.com
March 24, 2014 .
Matt Busch
Synagro ,
5900 744L Street North .
St. Petersburg; FL 33789
F. TEL: [phone]
FAX: [phone]
RE: Pinellas
a
Dear Matt Busch:. Order No.: 14031194
Summit Environmental Technologies; Inc. received 1 sample(s)'on 3/13/2014 for the analyses
presented in the following report.
There were no problems. with the analytical events associated with this report.unless noted in the
Case Narrative.
Quality control data is within laboratory defined or, method s .ecified. acce tance limits except
Q. tY ry P P P
where.noted.. .
If you have any questions regarding these 'tests results; please feel free to call the laboratory.
,
Sincerely,
Dr. Mo Osman
Project Manager ..
3310 Win St.
Cuyahoga Falls, Ohio 44223
-A2LA 0724.01, Alabama 41600, Arkansas 88-.0735; California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida, NELAC E87688, Georgia, .
_ E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
901461. Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M,01`1`1923,,Minnesota 4097.111 Montana CERT0099, New
Hampshire 2996; New Jersey OH006, New York 11777, North Carolina 39705 end 631, Ohio 4170; Ohio, VAP CL0052, Oklahoma 9940, Oregon
OH200001; Pennsylvania.68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TNO4018, Texas TI04704466-11=5; Region 8 8TMS-
L, USDA/APHIS MCA I-00244, Utah OH00923201171, Vermont VT-87688, Vi-rginia 00440 and 1581; Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page. I of 4
rr '
I ..

Summit Enyironmental Technologies, Inc,
.., `
l®rk®rder
.
..
_ 3316 Win St.
��mph Sumpi.ary
r94'IFlC1#�&41
AlTA I ^3$PIiJCOwS�
,,iP, .-' Cuyahoga Falls,:Ohio 44223
T
4n'
alyffli--gi Labdtaibr es -
TEL: [phone] FAX.•- [phone]
WO#: 14031194
Website: httn Nhsnlseltek.com
24-Mar-14
CLIENT:
Synagro
j Project:
Pinellas
�. Y.ali SampleYD .
Client Sample ID
Tag No Date Collected
Date Received Matrix
14031194001
SYN-PIN 3-12
3/12/2014
3/13/2014 9:40:00 AM Solid
4

SO
Summit 'Etivironmental Technologies, Inc. •
M11",
.bi 3310 Win St Case Narrative
r . 3 It Cuyahoga Falls, Ohio 44223
Fra� i c a�it_ r i r eHcit a€:�fi ., �r�cw0#: 14031104
1a1#i ?1 t�4CYt?tli 9 TEL: [phone] FAX.- [phone]
Website: hHoMliviviv.seitek.com Date: 3/24/2014
— CLIENT:. Synagro
Project:. Pinellas.
This, report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies- Inc. Work Order Number assigned to this report.
Paginated Reportincluding:' Cover Letter, -Case Narrative, Analytical results, Applicable Quality.
Control Summary reports and copies of the Chain of Custody Documents supplied with this sample
set.
.Concentrations reported with a J flag in the Qtial field are values below the Limit of Quantitation
LO but greater than the established Limit of Detection.' OD There is eater certaintv
associated with these results and data should be considered as estimated.
Method numbers; unless specified as SM "(Standard Methods) or ASJ. M- , are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report. are noted below.
Tclp pest & herb were added per client 's.reauest on 3/18/2014.: .
"
,I
Revision V.I.
Page 3 of 4
i.

1
Summit Environmental Technologies, Inc.WO#:
_
14031194
4
mviRbtAIr.N`
i +.
AL TECH
0Wr.7;-s, #OC
3310 Win St.
Cuyahoga Falls, Ohio 44223
Date Reported: 3/24/2014
— Analyllc-4l•l.abwarodes
TEL: [phone] FAX: [phone]
Company: .Synagro
Tlebsite: hnn:/hvwtivsettek.com
Address: 5900 744L
Street North
{ a
St Petersburg
3 3789
Received: 3/13/2014
�l
Project#: Pinellas
SVOC SW-846: 80814CLP Pesticides .
Client ID#.
Lab IID#
Collected Analyte
Rep.Lmt Result Units
Matrix Method
DF
Reglwl .
Itun
Analyst.
SYN=PIN 3A2
001
3/12/2014 Chlordane, total
.0.010 ND mg/L
Solid EPA 8081 B
1
0.630
3/22/2014
JBN'
SYN-PIN 3-12
001
3/12/2014 Toxaphene
0.10 ND mg/L
Solid EPA 8081 B
1•
0.50..
3/22/2014
- JRN
SYN-PINS-12
001
9112/2014 Endrin
0.0020 '.AID mg/L
Solid EPA8081 B.'.
1
0:020
3/22/2014
JBN
SYN-PIN 3-12
.001
3/1212014- gamma-BHC
0.0020 ND- ring/L
Solid EPA 8081 B
1
0.40
3/22/2014
JBN
SYN-PIN 3-12
001 .
3/12/2014 .Heptachlor
.-0.0020 - ND- mg/L
Solid EPA 8081 B
1
0.0080
3/22/2014,
_ JBN
SYWPIN 3-12
001,
3/1. /2014 Heptachlot epoxide
0.0020 ND mg/L
Solid EPA 8081 B
1
0.0080
3/22/2014
JBN.
SYN=PIN 3-12
001
3/12%2014 P/lethoxychlor
0.0020 ND mg/L
Solid. EPA 8081 B
1
10
3/22/2014
JBN .
SVOC SW-846: 8321'Herbicides-TCLP .
Ghent ID#•
Lab ID# Collected Analyse..
Rep Lint'Result Units
Matrix Method
DF
RegLv1
Run
Analyst
SYN-PIN 3-1.2
00.1
3/12/2614 2,4-D
5.0 ND .rngiL
Solid EPA 8321 A,
1.
90
3/20Y2014
AMZ
SYN-PIN 3-12
001
3/12/2014 2,4,5-TP .
0.50, ND rhg/L
Solid EPA 8321 A
1
1.0
3/20/2014
. AMZ
y
-
T
Page 4 of 4 . .

! Sunin t` mjrtDnmentfil �cfth6l®gies; Inc-,®..
.0.
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331
Win. Street f .:
Odyahtiga Falls, Ohio 44223
F&SuirrimitEnidr6ttimental,techttaloote Ina:,useonly .
Tel: [phone] .Fax: [phone].
r
Page of 5ET Ate.
Cntnpany stele'.' {Please Print)
Pr6ject'Name
iat� d: aHi e ® S
L.
Ctmtpany'A ess .. ` /_
Protect rtddtess
r
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Report to
9�
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Contact Parson.
✓L9s�i�:�Lf3G�i%
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White andyeHow pages should accompany satnpiat to the tebom;ory: The elienXJeAftiae me pink page.

Rev. 12 . .
Dife; 07/27113
i 6 Pt1 i EnvirtSFrG3'1'tental'Tisch E01dgi S, g@f :
- Cooleo ipceipt F®rrs
Initials of pemon-inspecting cooterand sarriptes _ r
i
`t
- Clent. 1 (
- Order Number:
Oate RecFived:'� v 1 timeke ceined. Cate cooler(s) opened and samples inspected.
Number or Co ierslFto s; NIA
Shipper: Ft=P CX lop DKL Airborne US Postal Walk-in Pickup Other,
Packaging. Peanuts' Bubb(® Wrap Paper Foam 1463'e Other: .
Tape on'coolerlboz. N :. N'A
�✓
Custody Seals intact to
t1;A
C-Q•C in. p)2slic Y fa
-
Pa1A
Ice _- Btue'ice �prese tt (absent 1 melted IVfH
SaSiple Temperature IR .Gun 0 020458 CF
ld1A.
Radioiogi¢at,Testing ' Instrument serial #35127, Y Ia
h1tA
(gee page 2'for scan results)
`"Us@.4 sti63t per sarnpPe'fov RedPologicGf Feststti�c. If santpte is HOT, tttE.Radiologioal Barely
. . .
4ii rcer.inust 6= riotifi4d
drnPnediately.
c-O-C filled.out properly -
l.r
NIA
Samples in separate bags H
PJ1A
Snple containers intact' t f!
fdlq
'If no. Iist broken samplefs)i
Sample label(s) compiele (ID, date, etc:) N
L�1
talk
..Labegs)'agree *ith C-0.0 fr
Pd1A
Corroct containers used; Pi
►UfA
Suffigient sampie reoeivetl. ty
NIA
Bu:)bles'absent from 46 nnL veals".. y
" Samples with bubbles <Gmm ere acceptable. Indicate bubble size If >6mm.
Weis client contacted about samples Y N
Wip client sand neu sample's Y N
Client contact:
Date�me:
f i Lagged in by.
comments:.
G:iQC'SPiARE00ocumentCoatrol, Templates - TrackinglCtiolerreceipt form Rev. 12 07-27-13.doc
. Page 1 of 2