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HomeMy WebLinkAboutNCG060040_MONITORING INFO_20181026STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V U&UG DD�iV DOC TYPE El HISTORICAL FILE 9-"MONITORING REPORTS DOC DATE ❑ 3W I D 3 YYYYMMDD MounrrVERN®N CHEMICALS . L L C 2001 Willow Springs Lane, Burlington, North Carolina 27215, PHONE 336-506-0524 FAX 336-228-6963 October 23, 2018 Central Files RECEIVED Division of Water Quality 1617 Mail Service Center OCT 2 Raleigh, NC 27699-1617 CENTRI--'L FILE3 Re: 2018 Semi -Annual NPDES Stormwater Report UPJR St'C rloni General Permit: NCG060000 COC No: NCGO60040 Mount Vernon Chemicals, LLC 1 Apollo Chemical — Burlington Facility 2001 Willow Springs Lane Burlington, NC 27215 Enclosed are the original and a copy of the stormwater monitoring results for the second -half of 2018 for our Willow Springs Lane facility. Our four stormwater outfalls were sampled during a significant rain event (documentation is attached). On -site measurement of pH was conducted at Apollo Chemical at the time of sampling. The samples were sent to Meritech, Inc. (Lab Certification No: 165) for analysis. The samples were tested for TSS, COD, and Oil & Grease. The Meritech report is appended. Our "Stormwater discharge outfall monitoring report" which includes pH results, is also appended. If you need additional information, please contact me. Sincerely, Mount Vernon Chemicals, LLCIApollo Chemical Gary S. Dagenhart, Ph.D. Vice -President — Chemical Technology Custom Manufacturing 1 R&D 1 Regulatory Compliance gdaQenhart(o)apoll ochemica1. cam Phone 336-506-0524 Copy: Vice -President — Chemical Technology, Plant Managers, Regulatory File, Corporate Director Environmental Affairs Apollo Chemical 2001 Willow Springs Lane, Burlington, North Carolina 27215 Tel: 336-226-1161 Fax: 336-228-6963 www.apollochemical.com MOUNT'VERNON Apollo Chemical GARY S. DAGENHART, Ph.D. Technical Director Bus: {336) 506-0524 Mount Vernon Chemicals, LLC Fax: (336) 228-6963 2001 Willow Springs Lane Mobile: (864) 323-2172 Burlington, NC 27215 gdagenhart+illapollochemical.com (10". fAli�tr- SF�� ) SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 10/23/2018 CERTIFICATE OF COVERAGE NO. NCG060040 SAMPLE COLLECTION YEAR July -December 2018 FACILITY NAME Mount Vernon Chemicals LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Alamance ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Shawn Rudison DISCHARGING TO SALTWATERS? ❑YES X NO LABORATORY Meritech, Inc Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall 20.12 inches or ❑ No discharge this period Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 500 SDO-1 10/09/18 < 2.5 6.0 15 < 5 N/A N/A SDO-2 10/09/18 49 6.3 28 < 5 N/A N/A SDO-3 10/09/18 9 6.6 < 15 < 5 N/A N/A 5DO-4 10/09/18 5 6.7 < 15 < 5 N/A N/A 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at Lny outfails. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504 6.0 — 9.0 - (if yes, complete Part B) 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any. outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the mare protective benchmark applies. SWU-249 Last Revised: October 1$, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days ot receipt of the lab results or at end o monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." r's ' W'11111111111 (Signature of Permittee) October 23, 2018 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wgZws/su/npdessw#tabb4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Shawn Rudison Report Date: 10/19/2018 Client: Apollo Chemical 2001 Willow Spings Ln Burlington, NC 27216 Date Sample Rcvd: 10/10/2018 Meritech Work Order # 10101869 Sample: SD01 Grab 10/9/18 3:15 Parameters Resul Analysis Date Reporting Litni Metho COD 15 mg/L 10/17/18 15 mg/L EPA 410.4 Total Suspended Solids <2.5 mg/L 10/10/18 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 10/16/18 5 mg/L EPA 1664B Meritech Work Order # 10101870 Sample: SD02 Grab 10/9/18 3:20 Parameters Resin AAn&sis Date Reporting Lim Method COD 28 mg/L 10/17/18 15 mg/L EPA 410.4 Total Suspended Solids 49 mg/L 10/10/18 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 10/16/18 5 mg/L EPA 1664E Meritech Work Order # 10101871 Sample: SD03 Grab 10/9/18 3:25 Paramete Result Analysis Date Reporting► Limi Metho COD <15 mg/L 10/17/18 15 mg/L EPA 410.4 Total Suspended Solids 9 mg/L 10/10/18 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 10/16/18 5 mg/L EPA 1664B Meritech Work Order # 10101872 Sample: SD04 Grab 10/9/18 3:30 Parameters tern Res-t An*sis Date Reporting Limit Method COD <15 mg/L 10/17/18 15 mg/L EPA 410.4 Total Suspended Solids 5 mg/L 10/10/18 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 10/16/18 5 mg/L EPA 1664B I hereby certify that I have reviewed and approve this data. -1)),9 Laboratory Representative —_---.------_--_______-642 Tamco Xoad,lteids—V ill -,-North Caro).i tel.(336)342-4748 fax.(336)342-1522 Chain of Custody Record COC► Client: Address: Attention: Apollo Chemical 2001 Willow Springs Ln Burlington, NC 27216 Shawn Rudison NPDES #: I Phone: 336-506-0532 Fax: Email: srudisonrQaDollochemical.ccm Project: PO #: MERITECH INC. 4 Environmental Laboratories A Division of Water Tcchnology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclabp_bellsouth.net Web Site: www.meritech-labs.com Turn Around Time* Std (10 days) X 3 -6 Day 24 -46 Hr Sample Location/lD # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only!' START END Comp? Grab? #of Conts. Tests Required On Ice? c Oo? Date Ttme Date nme SDO1 1019118 3:15p,m 3 Oii+Grease, COD, TSS Yes,T SD02 1019118 3:20pm 3 011+Grease, COD, TSS Yes SDO3 1019118 3:25pm 3 Oil+Grease, COD, TSS Yes S004 1019118 3:30pm 3 OiI+Grease, COD, TSS Yes i I I j I Method of Shipment: Comments: i i j UPS Fed Ex [] Hand Delivery Other Will these results be used for regulatory purposes? Yes X No *RUSH work must be approved prior to submitting samples. Tim: Reli ulsh by: Date: ;��L Received by: Date: Time: , Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: R!!!l b rr� Rat :} G �V iV �! e I 4�V e: � 1 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http://h2o.enr.state.ne.us/su/Forms Documents.htm#miscforms Permit No.: NIC/ GAO / 6/ 0 / 0/ 0/ 0/ or Certificate of Coverage No.: N/CIG/ 0/ 6/ 0 /4 /0 /0 Facility Name: Mount Vernon Mills Inc 1 Mount Vemon Chemiga[s LLC 1 Apollo Chemical County: Alamance Phone (336) 506-0524 No. Inspector: Shawn Rudison Date of Inspection: 10/09t2018 Time of Inspection: 3:15 - 3:30 PM Total Event Precipitation (inches): 0.12 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: G5D (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. 5Do1 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR. COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Pagel of 2 S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 -5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 7. Is there any foam in the storrnwater discharge? No 8. Is there an oil sheen in the stormwater discharge? No 9. Is there evidence of erosion or deposition at the outfall? No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of poilutarrt exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 . STA7g a Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform, please visit: http://h2o.enr.state.nc.us/su/Forms Documents.htm#miscforms Permit No.: N/C/ G/O / 6/ 0 / 0/ 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0/6l 0 l4 /0 A l Facility Name: Mount Vemon Mills, Inc t Mount Vemon Chemicals, LLC t Apollo Chemical County: Alamance Phone (336) 506-0524 No. Inspector. Shawn Rudison Date of Inspection: 10/09/2018 Time of Inspection: 3:15 - 3:30 PM Total Event Precipitation (inches): 0.12 Was this a Representative Storm Event? (See information below) Itl Yes n No Please check your permit to verb if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0,1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: G5D (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SD02 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 S W U-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwatcr discharge, where I is no solids and 5 is the surface covered with floating solids: l 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 7. Is there any foam in the stormwater discharge? No 8. Is there an oil sheen in the stormwater discharge? No 9. Is there evidence of erosion or deposition at the outfall? No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These condilions warrant further invcstigatioll. Page 2 of 2 S W U-242-1 12608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out thisform, please visit: http://h2o.enr.state.nc.us/su/Forms_Documents_htm#miscforms Permit No.: N/C/ G/0 / 6/ 0 / 0/ 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/0/4/0/0/ Facility Name: Mount Vemon Mills. Inc 1 Mount Vemon Chemicals, LLC 1 Apollo Chemical County: Alamance Phone (336) 506-0524 No. Inspector: 5nawn ru Date of Inspection: Time of Inspection: 1010912018 3:15 - 3:30 PM Total Event Precipitation (inches): 0-12 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verb if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: G5 D (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SD03 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page l of 2 S W U-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 7. Is there any foam in the stormwater discharge? No S. Is there an oil sheen in the stormwater discharge? No 9. Is there evidence of erosion or deposition at the outfall? No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. 'These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12608 Stormwater Discharge 4utfall (SDQ) Qualitative Monitoring Report For guidance on filling out thisform, please visit: http://h2o.enr.state.nc.us/su/Forms_Documents.htm#miscforms Permit No.: NIC/GA I sl 0l 0l 0l 0l or Certificate of Coverage No.: NICIGI 0/ fi/ 0 /4 /0 /0 / Facility Name: Mount Vernon Mills. Inc t Mount Vemon Chemicals, LLC t Apollo Chemical County: Alamance Phone (336)_506-0524 No. Inspector: Shawn Rudison Date of Inspection: 10/09/2018 Time of Inspection: 3:15 - 3:30 PM Total Event Precipitation (inches): 0.12 Was this a Representative Storm Event? (See information below) Yes No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: ret r (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. S1304 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 SWU-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 5. Floating Solids: Choose the number which best describes the amount of floating solids in the storrnwater discharge, where I is no solids and 5 is the surface covered with floating solids: 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the storrnwater discharge, where I is no solids and 5 is extremely muddy: 7. is there any foam in the storrnwater discharge? No 8. Is there an oil sheen in the stormwater discharge? No 9. Is there evidence of erosion or deposition at the outfall? No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242- l 12608 Attached is the Rainfall record for the Burlington Airport for the Storm Water Monitoring Sample collected on October 9, 2018, collected from 3:15pm—3:30pm. The rain gauge at the Apollo Chemical Burlington Facility measured the even to be 0.12 inches at the time of collection. The pH of each sample was measured using a calibrated electrode using buffer 4, buffer 7, and buffer 10. The samples were equilibrated to a temperature of 20.3°C prior to sampling. SDO-1: pH 6.0 SDO-2: pH 6.3 SDO-3: pH 6.6 SDO-4: pH 6.7 Mount Vernon Chemicals, LLC Shown Rudison Chemical Regulatory Manager Research and Development / Regulatory Compliance Group Apollo Chemical 336.506.0532 srudison@apollochemical.com National Weather Service : Observed Weather for past 3 Days : Burlington... Pagel of 3 G Enter Your "City, 5T" or zip code 0 o metric en espariol Precipitation D Temperature (°F) Wind lleat Pressure (in.) a Time Wind Vis. Weather Sky Relative Chill Index t edt ( ) (mph) ( p) mi. ( ) Cond. 6 hour Humidi ty (on (on altimeter sea hr Air Dwpt level 1 3 hr 6 hr e Max. Min. (in) (mb) 10 06:54 E 3 10.00 Overcast BKN021 70 68 93% NA NA 30.08 1017.9 BKN027 OVC065 10 05:54 NE 3 10.00 Mostly BKN024 70 68 93% NA NA 30.08 1017.8 Cloudy 10 04:54 NE 3 10.00 Mostly FEW021 69 67 93% NA NA 30.09 1018.2 Cloudy SCT028 BKN075 10 03:54 N 3 10.00 Mostly BKN023 69 67 93% NA NA 30.10 1018.5 Cloudy 10 02:54 Calm 10.00 Fair CLR 69 67 93% -NA NA 30.11 I018.9 10 01:54 NE 3 10.00 Mostly BKN050 69 67 74 69 93% NA NA 30.12 I019.3 0.01 Cloudy 10 00:54 NE 3 10.00 Fair CLR 69 67 93% NA NA 30.14 1020.0 09 23:54 Calm 10.00 Fair CLR 70 68 93% NA NA 30.16 1020.5 09 22:54 E 3 10.00 Fair CLR 71 69 94% NA NA 30.16 1020.6 0.01 09 21:54 Calm 10.00 Fair CLR 72 70 94% NA NA 30.17 1021.0 09 20:54 NE 3 10.00 Light FEW013 74 71 91 % NA NA 30.16 1020.8 0.01 Rain BKN030 OVC050 09 19:54 NE 5 10.00 A Few FEW043 74 70 81 74 88% NA NA 30.15 1020.4 0.16 Clouds FEW070 09 18:54 Calm 10.00 Fair CLR 75 71 88% NA NA 30.15 1020.3 09 17:54 NE 6 10.00 A Few FEW020 77 71 - 82% NA 79 30-15 1020.5 Clouds FEW025 09 16:54 NE 6 10.00 A Few FEW021 78 71 79% NA 80 30.16 1020.6 0.16 Clouds 09 15:54 E 6 10.00 Partly FEW075 78 71 79% NA 80 30.18 1021.3 0.14 Cloudy SCTI10 09 14:54 E 10 10.00 Light FEW023 77 70 79% NA 79 30.20 1022.0 0.02 G 17 Rain BKN029 OVC060 09 13:54 E 6 10.00 Mostly FEW031 80 70 80 70 71 % NA 83 30.21 1022.3 0.01 0.01 Cloudy BKN065 09 12:54 E 6 10.00 Overcast FEW031 79 69 72% NA 82 30.24 1023.5 BKN046 OVC070 09 11:54 E 10 10.00 Mostly BKN020 79 69 72% NA 82 30.26 1024.0 Cloudy BKN028 09 I0:54 NE 8 10.00 Mostly BKNO15 77 70 79% NA 79 30.27 1024.5 Cloudy BKN024 BKN030 http://wI.weather.gov/data/obhistory/KBLTY.htmi 10/ 10/2018 National Weather Service : Observed Weather for past 3 Days: Burlington... Page 2 of 3 09 09:54 E 8 10.00 Mostly BKNO09 73 69 Cloudy 09 08:54 NE 5 10.00 Partly SCI'007 71 68 Cloudy SCT050 09 07:54 NE 6 10.00 Fair CLR 70 68 70 67 09 06:54 NE 3 10.00 A Few FEW034 70 68 Clouds 09 05:54 NE 5 10.00 Mostly BKN046 70 68 Cloudy 09 04:54 NE 3 10.00 Overcast OVC046 70 68 09 03:54 Calm 10.00 Fair CLR 69 67 09 02:54 E 3 10.00 Fair CLR 68 67 09 01:54 Calm 10.00 Fair CLR 69 66 76 68 09 00:54 Calm 10.00 Fair CLR 69 67 08 23:54 E 3 10.00 Fair CLR 72 68 08 22:54 Calm 10,00 Fair CLR 73 68 08 21:54 E 5 10.00 Fair CLR 73 67 08 20:54 NE 5 10,00 Fair CLR 74 68 08 19:54 NE 3 10.00 Fair CLR 76 69 86 75 08 18:54 E 5 10.00 A Few FEW035 77 70 Clouds 08 17:54 E 6 10.00 A Few FEW070 80 71 Clouds 08 16:54 E 7 10.00 Fair CLR 84 70 08 15:54 R 7 10.00 Fair CLR 83 69 08 14:54 SE 6 10.00 Partly FEW022 83 71 Cloudy SCT047 SCT075 08 13:54 E 7 10.00 Mostly SCT022 81 71 83 72 Cloudy BKN026 BKN070 08 12:54 Vrbl 5 10.00 Overcast FEW019 81 72 BKN034 OVC065 08 11:54 E 3 10,00 Overcast 13KNO13 80 72 BKNO19 OVC035 08 10:54 SE 5 10.00 Overcast BKNO07 77 72 OVCO15 08 09:54 E 6 10.00 Overcast OVC004 74 72 08 08:54 E 6 10.00 Overcast OVC002 73 72 08 07:54 NE 3 10.00 Overcast OVC002 72 71 72 68 08 06:54 E 6 10.00 Overcast OVC002 72 71 08 05:54 Calm 10.00 Overcast OVC002 71 70 08 04:54 E 3 10.00 Mostly BKNO03 71 69 Cloudy 08 03:54 NE 3 10.00 Mostly BKN030 70 68 Cloudy 08 02:54 N 3 10.00 Fair CLR 68 66 08 01:54 Calm 10.00 Fair CLR 69 67 76 68 87% NA NA 30.28 1024.9 90% NA NA 30.27 1024.5 93% NA NA 30.26 1024.2 # 93% NA NA 30.26 1024.0 ! 93% NA NA 30.26 1023.9 93% NA NA 30.25 1023.8 93% NA NA 30.26 10239 96% NA NA 30.27 1024.4 90% NA NA 30.28 1024.8 93% NA NA 30.29 1025.0 87% NA NA 30.29 1025.1 84% NA NA 30.29 1025.0 81% NA NA 30.27 1024.5 82% NA NA 30.26 1024.0 79% NA 77 30.25 1023.7 79% NA 79 30.24 1023.3 74% NA 83 30.23 1023.1 63% NA 88 30.23 1023.1 63% NA 87 30,24 1023.4 67% NA 88 30.25 1023.7 72% NA 85 30.27 1024.4 74% NA 85 30.29 1025.1 76% NA 84 30.31 1025.6 85% NA 78 30.31 1025.8 94% NA NA 30.29 1025.2 96% NA NA 30.29 1025.0 97% NA NA 30.27 1024.E 97% NA NA 30.26 1023.9 96% NA NA 30.25 1023.8 94% NA NA 30.25 1023.7 93% NA NA 30.25 1023.5 93% NA NA 30.25 1023.6 93% NA NA 30,25 1023.6 http://wl.weather.gov/data/obhistory/KBUY.html 10/10/2018 National Weather Service : Observed Weather for past 3 Days : Burlington... Page 3 of 3 08 00:54 Calm 10.00 Fair CLR 70 68 93% NA NA 30.24 1023.3 07 23:54 Calm 10.00 Fair CLR 71 68 90% NA NA 30.24 1023.4 07 22:54 Calm 10.00 Fair CLR 71 68 90% NA NA 30.23 1023.1 07 21:54 Calm 10.00 Fair CLR 71 69 94% NA NA 30.22 1022.8 07 20:54 Calm 10.00 Fair CLR 73 70 90% NA NA 30.21 1022.4 07 19:54 Calm 10.00 Fair CLR 75 70 88 74 84% NA NA 30.20 1022.1 07 18:54 Calm 10.00 Fair CLR 79 69 72% NA 82 30.19 102I.8 07 17:54 E 5 10.00 Fair CLR 84 70 63% NA 88 30.19 1021.5 07 16:54 E 5 10.00 Mostly BKN036 84 70 63% NA 88 30.18 1021.4 Cloudy 07 15:54 Calm 10.00 A Few FEW055 85 69 59% NA 89 30.19 1021.6 Clouds 07 14:54 Calm 10.00 Partly SCT032 88 70 55% NA 93 30.20 1022.0 Cloudy SCl'048 07 13:54 Calm 10.00 A Few FEW035 85 69 85 69 59% NA 89 30.22 1022.6 Clouds 07 12:54 Vrb] 5 10.00 Partly SCI`027 84 71 65% NA 89 30.24 1023.4 Cloudy 07 11:54 Calm 10.00 Mostly SCT017 82 70 67% NA 86 30.25 1023.7 Cloudy BKN024 07 10:54 Calm 10.00 Partly FEW006 78 70 76% NA 80 30.25 1023.8 Cloudy SCT0I0 07 09:54 Calm 10.00 Overcast OVC001 72 71 97% NA NA 30.25 1023.7 07 08:54 Calm 10.00 Overcast OVC002 70 69 97% NA NA 30.24 1023.5 07 07:54 Calm 10.00 Overcast OVC002 69 67 69 66 93% NA NA 30.22 1022.7 H Max. Min. altimeter sea Time Wind Vis. Air Dwpt 6 Relative Wind Heat (in.) level I hr 3 hr 6 hr level a weather Sky hour Chill Index t (edt) (mph) (mi.) Cond. Humidity a (F) a (IF) Precipitation e Temperature ff) Pressure (in.) National Weather Service Back to previous page Last Modified: Febuary, 7 2012 Southern Region Headquarters Privacy Policy Fort Worth, Texas Disclaimer http://wI.weather.gov/data/obhistory/KBUY.htmi 10/10/2018 NC Department of STORMWATER DISCHARGE OUTFACE (SDO) Environmental QualityReceived ANNUAL SUMMARY DATA MONITORING REPORT (DMR) OCT 15 2018 Calendar Year 2018 Individual NPDES Permit No. NCS❑❑❑❑❑❑ or Certificate of Coverage (COC) No. NCG060040 VV1ncfnn-Cajam Regional Office This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March I" of the following year. Facility Name: Mount Vernon Chemicals LLC dba Apollo Chemical County: Alamance Phone Number: (336)506-0524 Total no. of SDOs monitored 4 Outfall No. SDO1 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Total Rainfall, inches TSS, m91L pH, Standard units COD, mglL Oil and Grease, mglL Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 — 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy - 03/06/18 0.14 28 7.6 60 < 5 NIA NIA 10/09/18 0.12 < 2.5 6.0 15 < 5 NIA NIA Additional Outfall Attachment SWU-264-Generic-251VIay2010 Outfall No. S1302 Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes❑ No® Yes ❑ No Yes ❑ No Total Rainfall, inches TSS, m g 1L pH, Standard units COD, m IL g Oil and Grease, mg/L Fecal Coiiform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 — 9.0 120 30 1000 1000 Date Sample Collected, mmldd/yy MMMMM 03/06/18 0.14 74 7.3 92 < 5 NIA NIA 10/09/18 0.12 49 6.3 28 < 5 NIA NIA Outfall No. SDO3 Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Yes ❑ No Yes ❑ No SWU-264-Generic-25May2010 Total Rainfall, inches TSS, m 1L g pH, Standard units COD, m 1L 9 Oil and Grease, mglL Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 — 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy MMMMM 03/06/18 0.14 24 7.3 41 < 5 NIA N/A 10/09/18 0.12 9 6.6 < 15 < 5 NIA NIA Outfall No. SD04 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Total Rainfall, inches TSS, mg1L pH, Standard units COD, mg1L Oil and Grease, mglL Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 — 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy MMMMM 03/06/18 0.14 11 7.4 41 < 5 NIA NIA 10109/18 0.12 5 6.7 < 15 < 5 NIA NIA SWU-264-Generic-25May2010 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature G D Date: October 23, 2017 Mail Annual DMR Summary Reports to: DWQ Regional Office Contact Information: ASHEVILLE REGIONAL OFFICE FAYETTEVILLE REGIONAL OFFICE M_ OORESVILLE REGIONAL OFFICE 2090 US Highway 70 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 296-4500 Favetteville, NC 28301-5043 (704) 663-1699 (910) 433-3300 RALEIGH REGIONAL OFFICE WASHINGTON REGIONAL OFFICE WILMINGTON REGIONAL OFFICE 3800 Barrett Drive 943 Washington Square Mall 127 Cardinal Drive Extension Raleigh, NC 27609 Washington, NC 27889 Wilmington, NC 28405-2845 (919) 791-4200 (252) 946-6481 (910) 796-7215 WINSTON-SALEM REGIONAL OFFICE CENTRAL OFFICE 1617 Mail Service Center i" "TO preserve, protect 585 Waughtown Street Winston-Salem, NC 27107 (336) 771-5000 Raleigh, NC 27699-1617 (919) 807-6300 and enhance tVorth Cerotina's wafer..." SW U-264-Generic-25May2010 iPA95110 N FOR PERF`ECT10M 2001 Willow Springs Lane, Burlington, North Carolina 27215, PHONE 336-506-0524 FAX 336-228-6963 March 15, 2018 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 MA ,R Re: 2018 Semi -Annual NPDBS Stormwater Report 7IpN General Permit: NCG060000 COC No: NCG060040 Mount Vernon Chemicals, LLC 1 Apollo Chemical — Burlington Facility 2001 Willow Springs Lane Burlington, NC 27215 Enclosed are the original and a copy of the stormwater monitoring results for the first half of 2018 for our Willow Springs Lane facility. Our four stormwater outfalls were sampled during a significant rain event (documentation is attached). On -site measurement of pH was conducted at Apollo Chemical at the time of sampling. The samples were sent to Meritech, fnc. (Lab Certification No: 165) for analysis. The samples were tested for TSS, COD, and Oil & Grease. The Meritech report is appended. Our "Stormwater discharge outfall monitoring report" which includes pH results, is also appended. If you need additional information, please contact me. Sincerely, Mount Vernon Chemicals, LLCIApollo Chemical Css Gary S. Dagenhart, Ph.D. Vice -President — Chemical Technology Custom Manufacturing 1 R&D 1 Regulatory Compliance gdagenhart@apollochemical.com Phone 336-506-0524 Copy: Plant Managers, Regulatory File, Corporate Director Environmental Affairs Apollo Chemical 2001 Willow springs Lane, Burlington, North Carolina 27215 Tel: 336-226-1161 Fax: 336-228-6963 www.apollochemical.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 3/15/2018 CERTIFICATE OF COVERAGE NO. NCG060040 SAMPLE COLLECTION YEAR January -June 2018 FACILITY NAME Mount Vernon Chemicals LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check a[[ that apply): ^ COUNTY Alamance ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Shawn Rudison DISCHARGING TO SALTWATERS? ❑YES X NO LABORATORY Meritech, Inc Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall 20.14 inches or ❑ No discharge this period' Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform', Colonies per 100.ml Enterococcil, Coloniesiper100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 500 SDO-1 03/06/18 28 7.6 60 < 5 N/A N/A SDO-2 03/06/18 74 7.3 92 < 5 N/A N/A SDO-3 03/06/18 24 7.3 41 < 5 N/A N/A SDO-4 03/06/18 11 7.4 22 < 5 N/A N/A 1 Only applies to facilities that use/process meats. zThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504 6.0 —9.0 - (if_yes, complete Part B) 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. `See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case o "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) March 15, 2018 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.og/web/wq/ws/su/npdessw#tab-4 S WU-249 Last Revised: October 18, 2012 Page 2 of 2 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://h2o.erlr.state.nc.us/su/Forms Documents.htm#miscforms Permit No.: N/C/ G/O / 6/ O / O/ O/ O/ or Certificate of Coverage No.: N/C/G/ O/ 6 / O / 4 /O /0 / Facility Name: Mount Vernon Mills. Inc 1 Mount Vemon Chemicals. LLC / Apollo Chemical County: Alamance Phone (3361506-0524 No. Inspector: Shawn Rudison Date of Inspection: 03/06/2018 Time of Inspection: 2:30 - 2:45 PM Total Event Precipitation (inches): 0.14 Was this a Representative Storm Event? (See information below) ✓ Yes [] No Please check your permit to verb if Qualitative Monitoring must be performed during a representative storm event (requirements vary). _..... ..... .....,.... ..............__................_..............................,.....�...... ..-....-..........._...._-_................_........................................._.......__......._.........._... ............................ ._......................... __._............._........._._.... A "Representative Storm Event"is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature,) certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SDO1 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page I of 2 S W U-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1. S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1_ 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 7. Is there any foam in the stormwater discharge? No 8. Is there an oil sheen in the stormwater discharge? No 9. Is there evidence of erosion or deposition at the outfall? No 1.0. Other Obvious indicators of Storrnwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of'2 S WU-242-112608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance onfrllingout thisform, please visit: http.//h2o.enr.state.nc.us/su/Forms Documents.htm#misefonns Permit No.: NICI G/O / 6/ 0 / 0l 0/ 0l or Certificate of Coverage No.: NIC/G/ 0/ 6/ 0 /4 /0 /0 / Facility Name: Mount Vernon Mills. Inc 1 Mount Vernon Chemicals. LLC t Apollo Chemical County: Alamance Phone (336) 506-0524 _ No. Inspector: Shawn Rudison Date of Inspection: 03/06/2018 Time of Inspection: 2:30 - 2:45 PM Total Event Precipitation (inches): 0.14 Was this a Representative Storm Event? (See information below) Wes ❑ No Please check your permit to verb if Qualitative Monitoring must he performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to I0 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: G5 D (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SD02 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL. MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 S W U-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 7. Is there any foam in the stormwater discharge? No 8. Is there an oil sheen in the stormwater discharge? No 9. Is there evidence of erosion or deposition at the outfall? No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. `these conditions warrant further investigation. Page 2 of 2 SWU-242-112608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http://h2o.enr.state.nc.us/su/For7ms Documents.iitm##miscforms Permit No.: N1Cl GIO l 61 a 1 0l 0l 0l or Certificate of Coverage No.: N/C1Gl 0l 61 0 14 l0 10 I Facility Name: Mount Vemon Mills. Inc 1 Mount Vernon Chemicals, LLC,t Apollo Chemical County: Alamance Phone (3361506-0524 No. Inspector: Shawn Rudison Date of Inspection: 03106/2018 Time of Inspection: 2:30 - 2:45 PM Total Event Precipitation (inches): 0.14 Was this a Representative Storm Event? (See information below) Yes R No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: G5 D (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SD03 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page I of 2 SWU-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 7. Is there any foams in the stormwater discharge? No S. Is there an oil sheen in the stormwater discharge? No 9. Is there evidence of erosion or deposition at the outfall? No la. Other Obvious Indicators of Stormnwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or crosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Paget oft S W U-242-112608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform, please visit: http://h2o.enr.state.nc.us/su/Fonns Documents.htm#miscforms Permit No.: N/C/G10 / 610 / 0/ 0/ 0/ or Certificate of Coverage No.: N/C/Gl 0161014 /0 10 1 Facility Name: Mount Vernon Mills, Inc t Mouni Vernon Chemicals, LLC 1 Apollo Chemical County: Alamance phone (336) 5OM524 No. Inspector: Shawn Rudison Date of Inspection: 03/06/2018 Time of Inspection: 2:3o - 2:45 PM 'total Event Precipitation (inches): 0.14 Was this a Representative Storm Event? (See information below) 1✓ Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: G5 b (Signature of Pcrmittee or Designee) 1. Outfall Description: Outfall No. sp04 Structure (pipe, ditch, etc.) PIPE Receiving Stream: CUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Pagel of 2 SWIJ-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1 6. Suspended Solids: Choose the number winch best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 11 7. Is there any foam in the stormwater discharge? No S. Is there an oil sheen in the stormwater discharge? No 9. Is there evidence of erosion or deposition at the outfall? No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242- l 12608 Meritech, Inc. Environmental Laboratory A.-.Oj Laboratory Certification No.165 Contact: Shawn Rudison Report Date: 3/14/2018 Client: Apollo Chemical 2001 Willow Spings Ln Burlington, NC 27216 Date Sample Rcvd: 3/7/2018 Meritech Work Order #1 03071865 Sample: SD01 Grab 3/6/18 2:30 Parameters _ Result Analysis Date Roorting limit Method COD 60 mg/L 3/8/18 15 mg/L EPA 410.4 Total Suspended Solids 28 mg/L 3/8/18 IS mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 3/12/18 5 mg/L EPA 1664B Meritech Work Order # 03071866 Sample: SD02 Grab 3/6/18 2:35 Parameters Result Analysis Date Reporting Limit Method COD 92 mg/L 3/B/18 15 mg/L EPA 410.4 Total Suspended Solids 74 mg/L 3/B/18 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 3/12/18 5 mg/L EPA 1664B Meritech Work Order # 03071867 Sample: SD03 Grab 3/6/18 2:40 Parameters Result Analysis Date Reporting Limit Method COD 41 mg/L 3/8/18 15 mg/L EPA 410.4 Total Suspended Solids 24 mg/L 3/8/18 2.5 mg/l, SM 2540 D Oil & Grease (HEM) <5 mg/L 3/12/18 5 mg/L EPA 1664E Meritech Work Order # 03071868 Sample: SD04 Grab 3/6/18 2AS Parameters Result Analysis Date Reporting Limit Method COD 22 mg/L 3/8/18 15 mg/L EPA 410.4 Total Suspended Solids 11 mg/L 3/8/18 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 3/12/18 5 mg/L EPA 1664B I hereby certify thatl have reviewed and approve this data. 6' 00'-� - Laboratory Representative 642 Tameo Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Attached is the Rainfall record for the Burlington Airport for the Storm Water Monitoring Sample collected on March 6, 2018, collected from 2:30pm—2:45pm. The rain gauge at the Apollo Chemical Burlington Facility measured the even to be 0.14 inches at the time of collection. The pH of each sample was measured using a calibrated electrode using buffer 4, buffer 7, and buffer 10. The samples were equilibrated to a temperature of 20.3'C prior to sampling. SDO-1: pH 7.6 SDO-2: pH 7.3 SDO-3: pH 7.3 SDO-4: pH 7.4 Mount Vernon Chemicals, LLC Shown Rudison Chemical Regulatory Manager Research and Development/ Regulatory Compliance Group Apollo Chemical 336.506.OS32 srudison@apollochemical.com National Weather Service : Observed Weather for past 3 Days : Burlington... Page 1 of 3 Burlington Alamance Regional Airport ®Enter Your "City, ST" or zip code Go metric en esoanol Precipitation D Temperature (°F) Wind Heat Pressure (in.) a Time Wind Vis. Slcy Weather 6 hour Relative Chill Index sea I t (est) (mph) (mi.) Cond. Air Dwpt Humidity o (� a (�'i altimeter level 1 hr 3 hr 6 hr, e Max. Min. (in) (mb) 06 14:54 Calm 4.00 Light FEW030 40 38 93% NA NA 29.87 1011.7 0.12 Rain 13KN035 Fog/Mist OVC075 06 13:54 Calm 5.00 Rain FEW020 41 37 86% NA NA 29.92 1013.4 0.07 Fog/Mist BKN030 OVC042 06 12:54 Calm 10,00 Light BKNO50 41 35 43 40 79% NA NA 29.94 10139 0.02 0.06 Rain OVC080 06 11:54 Vrbl 3 10.00 Overcast OVC050 41 35 79% NA NA 29.96 1014.8 06 10:54 Calm 10.00 Overcast OVC050 40 32 73% NA NA 29.99 1015.7 0.02 06 09:54 Calm 8.00 Light BKN080 40 29 65% NA NA 29,99 1015.9 0.02 0.02 Rain OVC095 06 08:54 SE 6 10.00 Overcast BKN065 42 21 43% 38 NA 29.99 1015.6 OVC090 06 07:54 E 6 10.00 Overcast BKN065 4I 20 43% 37 NA 30.01 1016.2 OVC085 06 06:54 E 3 10.00 Overcast OVC065 40 20 42 38 45% NA NA 30.00 1016,0 06 05:54 E 3 10.00 Overcast FEW075 40 20 45% NA NA 30.01 1016.2 OVC095 06 04:54 Calm 10.00 overcast OVC080 39 21 48% NA NA 30.00 1015.9 j 06 03:54 Calm 10.00 Mostly BKN080 38 18 44% NA NA 30,00 1016.0 Cloudy 06 02:54 Calm 10.00 Mostly SCT090 40 18 41% NA NA 30.02 1016.7 Cloudy BKN1.20 06 01:54 Calm 10.00 Overcast OVC100 41 19 41% NA NA 30.05 1017.5 06 00:54 Calm 10.00 Overcast OVCI10 41 18 51 40 39% NA NA 30.05 1017.5 05 23.54 Calm 10.00 Fair CLR 43 16 34% NA NA 30.05 1017.7 } 05 22:54 Calm 10.00 Fair CLR 42 15 33% NA NA 30.06 1017.9 05 21:54 E 3 10.00 Fair CLR 41 18 39% NA NA 30.05 1017.8 05 20:54 Cahn 10.00 Fair CLR 44 16 32% NA NA 30,04 1017.4 05 19:54 E 6 10.00 Fair CLR 47 18 31% 44 NA 30.03 1017.0 05 18:54 E 3 10.00 Fair CLR 50 16 58 50 26% NA NA 30.01 1016.6 i 05 17:54 E 3 10.00 Fair CLR 55 14 20% NA NA 30.01 1016.5 05 16:54 N 5 10.00 Fair CLR 58 13 17% NA NA 30.01 1016.3 05 15:54 N 3 10.00 Fair CLR 56 12 17% NA NA 30.02 1016,8 05 14:54 Vrb13 10.00 Fair CLR 55 10 16% NA NA 30.04 1017.3 05 13:54 NA 10.00 Fair CLR 57 11 16% NA NA 30.05 1017.7 05 12:54 Vrb17 10.00 Fair CLR 53 10 55 30 18% NA NA 30.09 1019.0 05 11:54 N 7 10.00 Fair CLR 51 13 22% NA NA 30.12 1020.1 http://wI.weather.gov/data/obhistory/l,,'-BUY.html 3/6/2018 National Weather Service : Observed Weather for past 3 Days : Burlington- Page 2 of 3 05 10:54 NW 7 10.00 Fair CLR 48 15 27% 45 NA 30.14 1020.7 05 09:54 N 8 10.00 Fair CLR 47 17 30% 43 NA 30.15 1021.0 05 08:54 NE 8 10.00 Fair CLR 43 18 37% 38 NA 30.16 1021.6 05 07.54 NE 3 10.00 Fair CLR 38 26 620/a NA NA 30.15 1021.2 05 06:54 Calm 10.00 Fair CLR 31 25 44 28 79% NA NA 30.14 1020.7 05 05:54 Calm 10.00 Fair CLR 31 25 79% NA NA 30.12 1020.0 05 04:54 Calm 10.00 Fair CLR 34 25 70% NA NA 30.13 1020.3 05 03:54 Calm 10.00 Fair CLR 34 23 64% NA NA 30.13 1020.5 05 02:54 Calm 10.00 Fair CLR 36 21 55% NA NA 30.14 1020.6 05 01:54 Calm 10.00 Fair CLR 42 19 40% NA NA 30.15 1021.0 05 00:54 N 7 10.00 Fair CLR 43 20 52 38 40% 39 NA 30.16 1021.2 04 23:54 N 6 10.00 Fair CLR 45 20 37% 42 NA 30.17 1021.5 04 22:54 NW 9 10.00 Fair CLR 48 21 34% 44 NA 30.16 1021.3 04 21:54 W 5 10.00 Fair CLR 40 26 58% 36 NA 30.15 1021.0 04 20:54 Calm 10.00 Fair CLR 42 24 49% NA NA 30.13 1020.4 04 19:54 Calm 10.00 Fair CLR 47 23 39% NA NA 30.13 1020.3 04 19:54 Calm 10.00 Fair CLR 51 17 60 51 26% NA NA 30.13 1020.4 04 17:54 N 6 10.00 Fair CLR 55 15 21% NA NA 30.13 1020.6 04 16:54 N 6 10.00 Fair CLR 59 13 16% NA NA 30.13 1020.2 04 15:54 N 13 10.00 Fair CLR 59 16 18% NA NA 30.14 1020.7 G 20 04 14:54 N 10 10.00 Fair CLR 58 15 18% NA NA 30.16 1021.3 04 13:54 N 14 10.00 Fair CLR 57 15 19% NA NA 30.19 1022.2 G 22 04 12:54 N 15 10.00 Fair CLR 55 18 56 35 23% NA NA 30.21 1023.0 G 24 04 11:54 N 12 10,00 Fair CLR 53 19 26% NA NA 30.24 1023.9 G 23 04 10:54 N 13 10.00 Fair CLR 50 19 29% 45 NA 30.25 1024.5 04 09:54 N I5 10.00 Fair CLR 47 18 31% 41 NA 30.26 1024.7 G21 04 08:54 N 13 10.00 Fair CLR 43 17 35% 36 NA 30.27 1025.0 G21 04 07:54 N 9 10.00 Fair CLR 40 17 40% 34 NA 30.26 1024.7 04 06:54 NW 6 10.00 Fair CLR 35 17 42 35 48% 30 NA 30.24 10241 04 05:54 Calm 10.00 Fair CLR 37 16 42% NA NA 30.23 1023.8 04 04:54 NW 6 10.00 Fair CLR 37 16 42% 32 NA 30.22 1023.3 04 03:54 NW 5 10.00 Fair CLR 38 16 41% 34 NA 30.20 1022,8 04 02:54 NW 7 10.00 Fair CLR 40 16 38% 35 NA 30.19 1022.5 04 01:54 NW 9 10.00 Fair CLR 41 17 38% 35 NA 30.19 1022.4 04 00:54 NW 8 10.00 Fair CLR 42 17 52 42 36% 37 NA 30.19 1022.3 03 23:54 NW 7 10.00 Fair CLR 43 16 34% 39 NA 30.19 1022.3 03 22:54 N 13 10.00 Fair CLR 46 15 29% 40 NA 30.18 1022.1 G21 03 21:54 NW 10.00 Fair CLR 47 14 26% 41 NA 30.18 1022.1 16G 24 03 20:54 10.00 Fair CLR 49 13 23% 44 NA 30.18 1022.2 http://wI.weather.gov/data/obhistory/KBUY.htrnl 3/6/2018 National Weather Service : Observed Weather for past 3 Days : BurIington— Page 3 of 3 NW 14G 23 03 19:54 NW 10.00 Fair 16G 24 03 18:54 N 9 10.00 Fair 03 17:54 N 9 G 10.00 Fair 18 03 16:54 NW 10.00 Pair 13 G 26 CLR 51 12 21 % NA NA 30.16 1021.6 CLR 52 10 60 52 I8% NA NA 30.I5 1021.2 CLR 55 8 15% NA NA 30.12 1020.1 CLR 58 5 12% NA NA 30.10 1019.2 03 15:54 N 16 10.00 Pair CLR 60 7 12% NA NA 30.09 1019.0 G 24 D Max. Min. altimeter Sea Time Air Dwpt slcy 6 hour Wind Heat Relative level a hr 3 hr 6 hr (in•) a Wind Vis. Weather Chill (mb) t (est) (mph) (mi.) Cond. Humidity )Index F (0(cF) Precipitation e Temperature CF) Pressure (in.) National Weather Service Back to previous page Last Modified: Febuary, 7 2012 Southern Region Headquarters Privau Policy Fort Worth, Texas Disclaimer http-.//wI.weather.gov/data/obhistory/KBUY.htmi 3/6/2018 MoUrArr'VERNON CHEMICALS , L L C 2001 Willow Springs Lane, Burlington, North Carolina 27215, PHONE 336-506-0524 FAX 336-228-6963 September 5, 2017 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2017 Semi -Annual NPDES Stormwater Report for Second Half General Permit: NCG060000 COC No: NCG060040 Mount Vernon Chemicals, LLC 1 Apollo Chemical — Burlington Facility 2001 Willow Springs Lane Burlington, NC 27215 Enclosed are the original and a copy of the stormwater monitoring results for the second half of 2017 for our Willow Springs Lane facility. Our stormwater outfalls were sampled during a significant rain event (documentation is attached). On -site measurement of pH was conducted at Apollo Chemical at the time of sampling. The samples were sent to Meritech, Inc. (Lab Certification No: 165) for analysis. The samples were tested for TSS, COD, and Oil & Grease. The Meritech report is appended. Our "Stormwater discharge outfall monitoring report" which includes pH results, is also appended. If you need additional information, please contact me. Sincerely, Mount Vernon Chemicals, LLCIApollo Chemical RECEIVED G5 b €� a 6 2017 Gary S. Dagenhart, Ph.D. CENTRAL FILESEN Vice President - Technology CEN SECTION gdagenhart(cbapollochemical.com DVVR Phone 336-506-0524 Copy: Plant Managers, Regulatory File, Corporate Director Environmental Affairs Apollo Chemical 2001 Willow Springs Lane, Burlington, North Carolina 27215 TeL 336-226-1161 Fax: 336-228-6963 www.apollochemical.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality Genera! Permit No. NCG060000 Date submitted 9/5/2017 CERTIFICATE OF COVERAGE NO. NCG060040 SAMPLE COLLECTION YEAR July -December 2017 FACILITY NAME Mount Vernon Chemicals, LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Alamance ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Shawn Rudison DISCHARGING TO SALTWATERS? ❑YES X NO LABORATORY Meritech, Inc Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Totol event rainfall 20.21 inches or ❑ No discharge this period3 Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L_ Fecal Coliforml, Colonies per 100 ml Enterococci;, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 500 SDO-1 08/23/17 4 6.4 31 < 5 N/A N/A 5DO-2 08/23/17 24 6.8 59 < 5 I N/A N/A SDO-3 08/23/17 8 6.6 85 < 5 N/A N/A SDO-4 08/23/17 8 7.0 54 < 5 N/A N/A 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50° 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at outfalls, you must still submit this discharge monitoring report with a checkmark here. (if yes, complete Part B) 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No _Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) September 5, 2017 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 S W U-249 East Revised: October 18, 2412 Page 2 of 2 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Shawn Rudison Report Date: 9/1/2017 Client: Apollo Chernical 2001 Willow Spings Ln Burlington, NC 27216 Date Sample Rcvd: 8/24/2017 Meritech Work Order # 08241729 Sample: SDO1 Grab 8/23/17 3:00 Parameters Result Analysiste Reporting Limit Method COD 31 mg/L 8/25/17 15 mg/L EPA 410.4 Total Suspended Solids 4 mg/l. 8/25/17 2.5 mg/L SM 2540 D Oil & Grease (HF,M) <5 mg/l. 8/28/17 5 mg/L IPA 1.664B Meritech Work Order # 08241730 Sample: SD02 Grab 8/23/17 3:05 Parameters Result Analysis Date Reporting; Limi Method COD 59 mg/L 8/25/17 15 mg/L E,*PA 410.4 Total Suspended Solids 24 mg/L 8/25/17 2.5 rng/L SM 2540 D Oil & Grease (HEM) <5 mg/L 8/28/17 5 mg/L EPA 1664E Meritech Work Order # 08241731 Sample: SD03 Grab 8/23/17 3:10 Parameters ROSE It Analysis Date Reporting Limit Method COD 85 mg/L 8/25/1.7 15 mg/l. EPA 410.4 Total Suspended Solids 8 mg/L 8/25/17 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 nag/L 8/28/17 5 mg/L EPA 1664B Meritech Work Order # 08241732 Sample: SD04 Grab 8/23/17 3:15 Parameters Result Analysis Date Reporting Limit Method COD 54 mg/l. 8/25/1.7 15 mg/L EPA 410.4 Total Suspended Solids 8 mg/L 8/25/17 2.5 rng/L SM 2540 D Oil & Grease (HEM) <5 mg/L 8/28/1.7 5 mg/L EPA 1664B I hereby certify that 1 have reviewed and approve this data. tt, Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Chain of Custody Record(COC Client: Address: Attention: Apollo Chemical 2001 Willow Springs Ln Burlin ton, NC 27216 Shawn Rudison NPDES#: Phone: 336-506-0532 Fax: Email: srudisarirCu)apollochemical-cam Project: PO #: MERITECHINC. Environmental Laboratories } A Division of Water Technology and Control, Inc. 642 Tamco Rd Prone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclabgDbelisouth.net Web Site: www.meritech-labs.com Turn Around Time* Std (10 days) X 3 - 5 Day 24 -48 Fir Sample LocationllD # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? #of conts. Tests Required uired On lee? pHaK? C12 OK? ❑ale Time Date Time SD01 8123117 3:00pm 3 Oil+Grease, COD, TSS Yes SD02 8/23117 3:05pm 3 Oil+Grease, COD, TSS 30 Yes SD03 8123117 3.10pm 3 10il+Grease, COD, TSS 3 Yes SD04 8123117 3:15pm 3 Oil+Grease, COD, TSS Yes Method of Shipment: Comments: ❑ UPS ❑ Fed Ex Hand Delivery '❑Other Will these results be used for regulatory purposes? Yes x No RUSH work must be approved prior to submitting samples. Reli ui5hep L Date: Time: V24MV `! Received by: Date: Time: Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Rec z (� ❑ ei Tim: Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out this form, please visit: http://l12o,enr.state.nc.us/su/Forms_ Documents.htm#miscforms Permit No.: NICI G/d / 6/ 0 / 0/ 0/ 0l or Certificate of Coverage No.: NICIGI al 6/ 0 /4 /0 /0 Facility Name: Mount Vernon Mills. Inc! Mount Vernon Chemicals. LLC t Apollo Chemical County: Alamance Phone (336) 506-0524 No. Inspector: Shawn Rudison Date of Inspection: 08/23/2017 Time of Inspection: 3:00 - 3:15 PM Total Event Precipitation (inches): 0_21 Was this a Representative Storm Event? (See information below) Ft/ Yes 0 No Please check your permit to verify If Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. ---------------- By this signature, I certify that this report is accurate and complete to the best of my knowledge: G5D (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. soot Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: l 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: ] 7. Is there any foam in the stormwater discharge? No S. Is there an oil sheen in the stormwater discharge? No 4. Is there evidence of erosion or deposition at the outfall? No l(). Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12608 x `'TATE w i Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://h2o.enr.state.nc.us/su/Forms_Documcnis.htm#miseforms Permit No.: NICI C'I0 1$/ 0 / 0l 010/ or Certificate of Coverage No.: N/C/G/ 0/6 / 0 /4 /0 /0 / Facility Name: Mount Vernon Mills. Inc 1 Mount Vemon Chemicals, LLC 1 Apollo Chemical County: Alamance Phone 336 506-0524 No. Inspector: Shawn Rudison Date of Inspection: 0812312017 Time of Inspection: 3:00 - 3:15 PM Total Event Precipitation (inches): 0_21 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A Representative Storm Event a stop "Representative " ' is n event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: GD (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SD02 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak Chlorine odor, etc.): NONE Page I of 2 S W U-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is veI}V cloudy: 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with Iloating solids: b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 7. Is there any foam in the stormwater discharge? No 8. Is there an oil sheen in the stormwater discharge`? No 9. Is there evidence of erosion or deposition at the outfall? No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform, please visit: http:l/h2o,enr.state.ne.us/su/Forms_Documents.htm#miscforms Permit No.: NIC/ G/O / 6/ 0 / 0/ 0/ 01 or Certificate of Coverage No.: NICIG/ 0/ 6/ 0 /4 /0 /0 I Facility Name: Mount Vernon Mills. Incl Mount Vemon Chemicals, LLC 1 Apollo Chemical County: Alamance Phone (336) 506-0524 No. Inspector: Shawn Rudison Date of Inspection: 0812312017 Time of Inspection: 3:00 - 3:15 PM Total Event Precipitation (inches): 0_21 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). --..................P.__... ._.............._.....................................................--.........----.........--.---- -.----._..........._._._......_._._._._._._........_..._._._._..---- ----- -- - ---------------- - A "Representative Stonn Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: C5 D (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SD03 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors. CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page] of 2 S W U-242- l 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 5. Floating Solids: Choose the number which best describes the amount offloating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where l is no solids and 5 is extremely muddy: 1 7. Is there any foam in the stormwater discharge? No 8. Is there an oil sheen in the stormwater discharge? No 9. Is there evidence of erosion or deposition at the MICA? No 1f1. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen. or erosion/deposition may be indicative of pollutant exposure. 'these conditions warrant further investigation. Page 2 of 2 S W U-242-1 I2608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http_//h2o.enr.state,nc.us/su/Forms Documents.htm#miscforms Permit No.: NIC/ G/O / 6/ 0 / 0/ 0/ 0/ or Certificate of Coverage No.: N/C/GI 0l - 6/0/4/0/0/ Facility Name: Mount Vernon Mills Inc t Mount Vemon Chemicals LLC 1 Apollo Chemical County: Alamance Phone (336) 5g6-0524 No. Inspector: Shawn Rudison Date of Inspection: 08/23/2017 Time of Inspection: 3:00 - 3:15 PM Total Event Precipitation (inches): 0-21 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: GD (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. 5DO4 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page E of 2 S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 7. Is there any foam in the stormwater discharge'? No 8. Is there an oil sheen in the stormwater discharge? No 9. Is there evidence of erosion or deposition at the outfall? No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids; and/or the presence of foam. oil sheen, or erosion/deposition may be indicative of pollutant exposure. "These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12608 Attached is the Rainfall record for the Burlington Airport for the Storm Water Monitoring Sample collected on August 23, 2017, collected from 3:00pm—3:15pm. The rain gauge at the Apollo Chemical Burlington Facility measured the even to be 0.21 inches at the time of collection. The pH of each sample was measured using a calibrated electrode using buffer 4, buffer 7, and buffer 10. The samples were equilibrated to a temperature of 20.3'C prior to sampling. SDO-1: pH 6.4 SDO-2: pH 6.8 SDO-3: pH 6.6 SDO-4: pH 7.0 Shown Rudison Chemical Regulatory Specialist Research and Development / Regulatory Compliance Group Mount Vernon Chemicals, LLC / Apollo Chemical 336.506.0532 srudison@apollochemical.com National Weather Service : Observed Weather for past 3 Days : Burlington Alamance Regional Airport 24 ,06:54 N 8 10.00 Overcast 24 05:54 NE 6 10.00 Mostly Cloudy 24, 04:54 N 5 10.00, Mostly Cloudy 24 03:54 N 6 10.00 Overcast 24 02:54 N 7 ,10.00 Mostly Cloudy OVC012 72 FEW008 72 BKN095 FEW017 72 BKN036 BKN050 OVC010 74 FEW010 75 BKN018 BKN026 69 70 91% 94% NA NA NA NA 70 94% NA NA 71 91% NA NA 72 90% NA NA 24 01:54 N 6 10.00 Overcast OVC013 76 72 82 76 88% NA 76 24, 00:54 NE 5 10.00 Overcast OVC014 76 72 88% NA 76 23 23:54 NE 6 10.00 Mostly BKNO15 76 73 91% NA 76 Cloudy 23, 22:54 NE 6, 10.00 Partly Cloudy SCT100 77 73 88% NA 78 23 21:54 E 5 10.00 Fair CLR 78 74 87% NA 80 23, 20:54 Calm 10.00 Overcast OVC085 81 74 79% NA 86 23 19:54 Calm 10.00 Overcast OVC080 81 73 90 77 77% NA 86 23 18:54 SW 3 10.00 Mostly BKN075 83 73 72% NA 89 Cloudy 23 17:54 W 6 10.00 A Few FEW085 83 71 67% NA 88 Clouds 23 16:54 SW 8 10.00 Partly Cloudy FEW035 82 75 79% NA 89 SCT095 23 15:54 S 5 6.00 Thunderstorm 13KN100 80 74 82% NA 85 in Vicinity Light Rain 23 14:54 NW 10.00 Thunderstorm BKN042 83 71 67% NA 88 18 G in Vicinity 25 23 13:54 SE 5 10.00 Light Rain SCT043 82 73 92 75 74% NA 87 BKN070 OVC100 23 12:54 NW 3 10.00 Mostly SCT044 89 70 53% NA 94 Cloudy BKN055' B KN090 23 11:54 Vrbl6 10.00 Fair CLR 90 71 54% NA 96 23 10:54 Calm 10.00 Fair CLR 87 70 57% NA 92 29.92 -1012.5= _ _ 29.92 =1012.4= 2990 r 101 1.9- 29.91 =1012.0= _ = 29.90 =101 1.8= _ 29.90 101 1.6= _ 29.90 = 101 1.8: 29.90 =1011.8= 29.88 1011.2= 29.88 1011.0= _ 29.84 ' 1009.8= - _ 29.84 =1009.7= =0.03= 29.82 1009.1: _ 29.82 =1009.2= _ - 29.84 = t009.8=_0.02g0.03€ _ 29.86 '_ 1010.3=0.01 29.88 = 1010.9= 29.88 =101 1.1= 29.89 101 1.2= 29.90 =101 1.7= 29.91 =_ 101 1.9' http://wl.%ti'cather.govldata/obhistory/Kl3UY.html[g124/2017 8:01;54 AM] National Weather Service '. Observed Weather for past 3 Days : Buriinglon Alamance Regional Airport 23 09:54 NW 5 10.00 Fair CLR 84 73 23 08:54 W 7 . 10.00 Fair CLR 79 73 23 07:54 Calm 10.00 Fair CLR 75 73 23-06:54: S 5 10.00 Fair CLR 73 71 23 05:54 SW 5 10.00 Fair CLR 73 71 23 04:54 SW 3 10.00 Fair CLR 73 71 23 03:54 S W 3 10.00 Fair CLR 74 71 23, 02:54 SW 5' 10.00: Fair CLR 75 71 23 01:54 SW 3 10.00 Fair CLR 76 71 23 00:54 Vrb13 10.00 Fair CLR 77 70 22 23:54 S W 5 10.00 Fair CLR 78 70 22 22:54 S W 3 10.00' Fair CLIZ 79 69 22 21:54 SW 5 10.00 Fair CLR 81 70 22 20:54 SW 6; 10.00 Fair CLR 84 70 22 19:54 S 6 10.00 Partly Cloudy SCT060 88 67 22 18:54 S W 9 10.00 Fair CLR 91 66 22 17:54 SW 8 10.00 Fair CLR 94 63 22 16:54 S 10 10.00 Fair CLR 95 61 22 15:54 S 8 10.00 Fair CLIZ 95 60 22 14:54 NA 10.00 fair CLR 92 63 22 13:54 S W 5 10.00 Fair CLR 90 67 22 12:54 SW 10.00 A Few F) W047 92 69 10 Clouds 22 11:54 SW 8 10.00 A Few FLW036 89 71 Clouds 22 10:54 W 7 10.00 Fair CLR 85 72 22 09:54 SW 6 10.00 Fair CLR 82 74 22 08:54 S W 6 10.00 Fair CLR 77 73 22 07:54 Calm 6.00 Fog/Mist CLR 73 71 22 06:54 Calm 2.00 Fog/Mist CLR 68 68 22 05:54 Calm 6.00 Fog/Mist CLR 68 68 22 04:54 Calm 8.00 Fair CLR 68 67 22 03:54 Calm 10.00 Fair CLR 69 68 22 02:54 Calm 10.00 Fair CLR 68' 67 22 01:54 Calm 10.00 Fair CLR 72 69 22 00:54 Calm 10.00 Fair CLR 71 69 21 23:54 Calm 10.00 Fair CLIZ 71 70 21 22:54 Calm 10.00 Fair CLR 72 • 70 21 21:54 Calm 10.00 Fair CLR 75 70 21 20:54 Calm 10.00 Fair CLIZ 77 71 21 19:54 SE 3 10.00 Fair CLR 82 71 21 18:54 S171 6 10.00 Fair CLR 87 69 21 17:54 SFa3 10.00 Mostly BKN120 86 69 Cloudy 70% NA 90 82% NA 82 76 72 94% NA NA 94% NA NA 94% NA NA 94% NA NA 91% NA NA 88% NA NA 87 76 85% NA 77 79% NA 79 76% NA 80 72% NA 82 69% NA 84 63% NA 88 95 88 50% NA 91 44% NA 94 36% NA 95 32% NA 95 31 % NA 95 38% NA 93 93 73 47% NA 93 47% NA 97 55% NA 95 65% NA 91 77% NA 88 88% NA 78 73 67 94% NA NA 100% NA NA 100% NA NA 96% NA NA 96% NA NA 96% NA NA 82 69 91 % NA NA 94% NA NA 96% NA NA 94% NA NA 84% NA NA 82% NA 79 93 82 69% NA 86 55% NA 91 57% NA 90 29.91 = 101 1.9_ 29.90 ' ] 01 1.8= 29.90 = 101 1.7- 29.89 1011.51 - - 29.89 _' 101 1.3 - 29,88 = 101 1.1= 29,89 =101 1.3= = - 29,91 =1012.0 29.92 29.93 29.94 = 1012.4 = 10 12.5= =1013.0=. 29.96 =1013.6 = - E - 29.95 =1013.3= 29.94 =1012.9 ` _ - 29.94 =_1013.1= 2994 21013.0 = - 29.94 "__ 1013.2 _ 29.95 €1013 A Z= _ _ 29.98 ° 1014.4 _ - 30.01 1015.6_ = - 30.06 `-1017.0' 30.07 =1017.5 30.09 r 30.11 =1018,1= = =1018.7 _ C - 30.11 =:1018.91 = = _ 30.12 11019.3_ 30.13 =1019.5= - = 30.12 10 19.2 zz_ 30.11 =1018.9= = - 30.11 1018.7= 30.12 1019.3= 30.14 E 1019.9 30.16 '_ ]020.5= 30.17 =1021.0= _ 30.18 1021.3= - _ _ 30.18 1021.4= 30.18 :1021.1 _ - _ 30.16 1020.7= 30.15 =1020.4= 30.15 =1020.2= E 30.15 =1020.1 "__ hllp://wl.weuther.gov/ciata/oblaistory/KliUY.htm[IS/24/2017 8:01:54 AM] National Weather Service : Observed Weather for past 3 Days : Burlington Alamance Regional Airport 21 16:54 SE 7 10.00 A Few FEW 110 89 68 Clouds 21 15:54 Vrbl6 10.00 Overcast OVCI 10 87 67 21 14:54 SE 5 10.00 Mostly BKN 120 87 67 Cloudy 21 13:54 Vrbl7 10.00 lair CLR 93 68 93 74 21 12:54 SE 6 10.00 A Few FEW040 91 70 Clouds 21 l 1:54 Calm 10.00 Partly Cloudy SCT036 88 72 21 10:54 Vrbl5 10.00 Fair CLR 87 74 21 09:54 Vrbl 3 10.00 A Few FEW 120 82 74 Clouds 21 08:54 E 3 10.00 Mostly BKN 120 79 73 Cloudy 21 07:54 Calm 9.00 Fair CLR 74 71 74 70 a Time' t (edt) e 50% NA 93 30.17 =1020.8- _ 51 % NA 90 30.16 :1020.5= 51 % NA 90 30.18 1021.3 44% NA 97 30.19 `_ 1021.5= 50% NA 97 30.21 `=1022.2= _ 59% NA 95 30.22 = 1022.6 = _ 65% NA 95 30.23 -1022.8- 77% NA 88 30.23 = 1022.8= - - - 82% NA 82 30.23 =1022.7 _ T� 91 % NA NA 30.22 ` 1022.4 �Vlnd� F- ' Vis. Weather Sky [ ,'i'x Min: Air i)wpt� G hour �:Relatrve kR ^' a1'timeter, sell n 5w V1'ind lleat level I hrF 3hr 6lir �- Chill Bidet (mb) (mph) i (mi.) Cond: llum�dit} o o (Ft) (')Prccipit>ttan :1,r '1 ressur�f' Temperature( F}_ National Weather Service Southern Region Headquarters Fort Worth. Texas Disclaimer ,,,ck t, vre.;uu, rage Last Modified: I-ebuary, 7 2012 Privacy Policy http:l/ivl,%veather.Rovldata/obhistory/K[iUY_hunl[8124/2017 8:01:54 AM] MOUW-VERNON CHEMICALS, ILILC 2001 Willow Springs Lane, Burlington, North Carolina 27215, PHONE 336-506-0524 FAX 336-228-6963 March 28, 2017 Central Files Division of Water Quality 1617 Mail Service Center p Raleigh, NC 27699-1617 �C1vCD Re: 2017 Semi -Annual NPDES Stormwater Report MAP 3 0 2011 Ce'" COC No: GeneralNCG060040060000 pwR �eTj� S Mount Vernon Chemicals, LLC 1 Apollo Chemical — Burlington Facility 2001 Willow Springs Lane Burlington, NC 27215 Enclosed are the original and a copy of the stormwater monitoring results for the first half of 2017 for our Willow Springs Lane facility. Our four stormwater outfalls were sampled during a significant rain event (documentation is attached). On -site measurement of pH was conducted at Apollo Chemical at the time of sampling. The samples were sent to Meritech, Inc. (Lab Certification No: 165) for analysis. The samples were tested for TSS, COD, and Oil & Grease. The Meritech report is appended. Our "Stormwater discharge outfall monitoring report" which includes pH results, is also appended. If you need additional information, please contact me. Sincerely, Mount Vernon Chemicals, LLCIApollo Chemical Css D�tc—h�� Gary S. Dagenhart, Ph.D. Vice -President - Technology Custom Manufacturing 1 R&D 1 Regulatory Compliance gdagenhart(cD-apollochemical. com Phone 336-506-0524 Copy: Plant Managers, Regulatory File, Corporate Director Environmental Affairs Apollo Chemical 2001 Willow Springs Lane, Burlington, North Carolina 27215 Tel: 336-226-1161 Fax: 336-228-6963 www.apollochemical.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 03/28/2017 CERTIFICATE OF COVERAGE NO. NCG060040 SAMPLE COLLECTION YEAR JanuarV-June 2017 FACILITY NAME Mount Vernon Chemicals, LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Alamance ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Shawn Rudison DISCHARGING TO SALTWATERS? ❑YES X NO LABORATORY Meritech Inc Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall 20.13 inches or ❑ No discharge this perioo3 Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 500 SDO-1 03/13/2017 11 6.6 191 < 5 N/A N/A SDO-2 03/13/2017 37 7.7 120 < 5 N/A N/A SDO-3 03/13/2017 27 7.5 69 < 5 N/A N/A SDO-4 03/13/2017 < 2.5 7.1 17 < 5 N/A N/A 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504 6.0 -- 9.0 - 1 Only applies to facilities that use/process meats. 2 The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. cifyes, complete Part B) 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SWU-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy o f this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Q> (Signature of Permittee) 3 iz0[Iq- (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr,org/web/wq/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 Meritech, Inc. Environmental Laboratory _ Laboratory Cextificalion No. 165 Contact: Shawn Rudison Report Date: 3/22/2017 Client: Apollo Chemical 2001 Willow Spings Ln Burlington, NC 27216 Date Sample Rcvd: 3/14/2017 Meritech Work Order # 031417SS Sample: SD01 Crab 3/13/17 5:00pm Parameters Result Anaiysis Date Reporting Limit Met COD 191 mg/L 3/15/1.7 15 mg/L 11PA 410.4 Total Suspended Solids 1.1 mg/1. 3/1.5/1.7 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 nig/L 3/21/17 5 mg/L EPA 1.66413 Meritech Work Order If 03141756 Sample: SD02 Grab 3/13/17 5:05pm Parameters Result Analysis Date Reporting Hinit Method COD 120 mg/L 3/15/17 15 mg/L C-PA 410.4 Total Suspended Solids 37 mg/L 3/15/17 2.5 rng/L SM 2540 D Oil & Grease (HEM) <5 mg/L 3/20/17 5 mg/L EPA 1664E Meritech Work Order # 03141757 Sample: SD03 Grab 3/13/17 5:10pm Parameters Result Analysis Date Reporting Limit Method COD 69 mg/L 3/15/17 1.5 mg/L RPA 410.4 Total Suspended Solids 27 mg/L 3/15/17 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 3/20/1.7 5 mg/L l?i'A 1664B Meritech Work Order # 03141758 Sample. SD04 Grab 3/13/17 5:15pm Parameters Result Analysis Date Reporting Limit Method COD 17 mg/L 3/15/1.7 15 rng/L CPA 410.4 Total Suspended Solids <2.5 mg/L 3/15/17 2.5 rng/L SM 2540 D Oil & Grease (HEM <5 mg/L 3/20/1.7 5 mg/L EPA 1664E I hereby certify that I have reviewed and approve this data. 2_ &V Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Chain of Custody Record CCC Client; Address: Attention: Apollo Chemical 2001 Willow Springs Ln Burlington, NC 27216 Shawn Rudison NPOES #: Phone: 336-506-0532 Fax: Email: srudisonr(c)apollochemical.com Project: PO #: MERITECH INC. Environmental Laboratories A Division of Water Technology and Control., Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab(cObellsouth.net Web Site: www.meritech-labs.com Turn Around Timex Std (10 days) X 3 - 5 Day 24 -48 Hr Sample P LocationllD # Sampling Dates & Times P g Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? # of conts. Tests Required On lee? pH OK? C12OK? Date Time Date Time SD01 3/13/17 5:00pm 3 Oil+Grease, COD, TSS Yes S002 3113117 5:05pm 3 Oil+Grease, COD, TSS �' Yes SDO3 3113117 5:10pm 3 Oil+Grease, COD, TSS i Yes SD04 3/13117 5:15pm 3 Oil+Grease, COD, TSS Yes •c L Method of Shipment: Comments: ❑ UPS ❑ Fed Ex ❑ Hand Delivery ❑Other Will these results be used for regulatory purposes? Yes I X No *RUSH work must be approved prior to submitting samples. Relin fished Date: 1 Ti 7 .� 3i�2017 �f 1 r Received by: Date: Time: Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: lime: Rq2er 7er b by: i e: Time: ,_ y� Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling oral this forrrr, please visit: http://h2o.enr.state.nc.us/su/Forms DOCUInentshtnl#miscforms Permit No.: NIC/Glo 16l O / OI OI 0/ or Certificate of Coverage No.: NICIGI O/ 6101410/0/ Facility Dame: Mount Vernon Mills, Inc 1 Mount Vernon Chemicals, LLC / Apollo Chemical County: Alamance phone No. (336) 506-0524 InSDeetor: Shawn Rudison Date of Inspection: 03/1312017 '['ime of Inspection: 5:15-5:30 PM Total Event Precipitation (inches): 0_13 Was this a Representative Storm Event? (See information below) 7Yes ❑ No Please check your permit to verify if Qualitative Monitoring must he peafortned during a representative storni event (requii-ements vary). A "Representative Stone Event" is it storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permi4e or Designee) 1. Outfall Description: Outfall No. SDO1 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNK CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page I of 2 5 WU-242- l 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: G2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where l is no solids and 5 is extremely muddy: (D 2 3 4 5 7. is there any foam in the stormwater discharge? Yes 05 S. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes Q 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. "These conditions warrant further investigation. Page 2of2 S W U-242-1 r 2608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this fonn, please visit: http://h2o.enr.state.nc.us/su/Foriiis Documents.htm#miscforms Permit No.: NICIGIO 10/ 0/ 0I 0/ 0/ or Certificate of Coverage No.: NIC/G/ 0/ 610 /4 /0/0/ Facility Name: Mount Vernon Mills, Inc t Mount Vernon Chemicals, LLC / Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Dale of Inspection: 03/13/2017 Time of Inspection: 5:15 - 5:30 PM Total Esvent Precipitation (inches): 0_13 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Moniioring must be perfonned daring a representali ve storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at Feast 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive Hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittce or Designee) I. Outfall Description: Outfall No. SDO2 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the Outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page l of 2 SWU-242- l } 2608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: (D 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: Cl 2 3 4 5 J 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes vo 9. is there evidence of erosion or deposition at the outfall? Yes D Ill. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition m-ay be indicative ot' pollutant exposure. These conditions warrant further investigation. ["age 2 of 2 SWU-242-1 12608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling ow this form, please visit: http://h2o.enr.statC.nC.uslsu/Forms_D0atments.htm#tniscforins Permit No.: N/C/Glo 16l 0l 0l 4l 0l or Certificate of Coverage No.: NICIG/ 0/6/ - 0/4/0l0/ Facil ICv Name: Mount Vernon Mills, Inc 1 Mount Vernon Chemicals, LLC t Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: 03113/2017 Time of Inspection: 5:15 - 5:30 PM Total Event Precipitation (inches): 0.33 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check yaxr permit to verrfj if Qualitative Monitoring must be perforrrred during a rel�re,serztative storm event (requirements vary), A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. Sy this signature, I certify that this report is accurate and complete to the best of my knowledge: &D (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. 3003 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR. COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly Of oil, weak chlorine odor, etc.): NONE Page t of 2 5 W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: Ol 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: lJ 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: \J 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes G 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes (D 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12609 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfitlling ow this form, please visit: http:/lh2a.enr.state,nc.us/su/Fornis Documents.htm#miscforms Permit No.: NICI G/O 16l 0/ 0l 01 ()l or Certificate of Coverage No.: N/C/GI 0/ 6l0/4 /0 /0 I l'acil Itv Name: Mount Vernon Mills, Inc ! Mount Vernon Chemicals, LLC t Apollo Chemical County: Atamance Phone No. (336) 506-0524 Inwector: Shawn Rudison Date of Inspection: 03/13/2017 "Time of Inspection: 5:15 - 5:30 PM "Total Event Precipitation (inches): 0.13 Was this a Representative Storm Event? (See information below) RV( Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. 13y this signature, 1 certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittffe or Designee) 1. Outfall Description: Outfall No. So04 Structure (pipe, ditch, etc.) PIPE Deceiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page I of 2 S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity o17 the discharge, where I is clear and 5 is very cloudy: [ l} 2 3 4 5 5. bloating Solids: Choose the number which best describes the amount of- floating solids in the stormwater discharge, where I is no noo solids and 5 is the surface covered with floating solids: ( 1) 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: ,) 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes CN 9. Is there evidence of erosion or deposition at the outfall? Yes o Itl. Other Obvious Indicators or Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of Foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242- l 12608 Attached is the Rainfall record for the Burlington Airport for the Storm Water Monitoring Sample collected on March 13, 2017, collected from 5:15pm—5:30pm. The rain gauge at the Apollo Chemical Burlington Facility measured the even to be 0.13 inches at the time of collection. The pH of each sample was measured using a calibrated electrode using buffer 4, buffer 7, and buffer 10. The samples were equilibrated to a temperature of 20.4°C prior to sampling. SDO-1: pH 6.6 SDO-2: pH 7.7 SDO-3: pH 7.5 SDO-4: pH 7.1 Shown Rudison Chemical Regulatory Specialist Research and Development / Regulatory Compliance Group Mount Vernon Chemicals, LLC / Apollo Chemical 336.506.0532 srudison@apollochemicaI-corn National Weather Service: Observed Weather for past 3 Days : Burlington... Page 1 of 3 weather.gov KE.,T" gton 7Your Aiamance Regional Airport or zip code Go metric en espanol Precipitation D Temperature ff) Wind Heat Pressure a Time t (edt) Wind (mph) Vis. (mi.) Weather Sky Cond. 6 hour Relative Humidity Chill Index all sea Air Dwpt (°F) (°F) (in) level 1 hr 3 hr 6 hr e Max. Min. (mb) 14 06:54 NW 9 10.00 Unknown OVC007 36 35 97% 29 NA 29.66 1004.6 0.01 Precip 14 05:54 N 6 10.00 Overcast FEW008 36 34 93% 31 NA 29.64 1003.9 0.02 OVC042 14 04:54 NW 8 10.00 Light OVC009 35 33 93% 28 NA 29.68 1005.4 0.04 0.08 Rain 14 03:54 NW 6,00 Light BKNO08 34 33 97% 25 NA 29.71 1006.5 0.04 12 Rain OVC014 Fog/Mist 14 02:54 NW 6.00 Fog/Mist OVC006 34 33 97% 25 NA 29.75 1007.7 14 G 21 14 01:54 N 9 G 6.00 Light OVC005 34 33 36 34 97% 27 NA 29.77 1008.4 0.01 0.07 20 Rain Fog/Mist 14 00:54 N 13 7.00 Overcast OVC007 35 33 93% 26 NA 29,82 I009.9 0.01 G21 13 23:54 N 13 6.00 Light OVC007 35 33 93% 26 NA 29,88 1012.0 0.01 Rain Fog/Mist 13 22:54 N 13 7.00 Light OVC007 36 34 93% 27 NA 29.94 1014.0 0.01 0.04 G 20 Rain 0 21:54 N 13 8.00 Light OVC008 36 35 97% 27 NA 29.98 1015.4 0.01 G 22 Rain 13 20:54 NE 9 6.00 Light 13KN007 36 35 97% 29 NA 30.00 1016.4 0.02 Rain OVC012 Fog/Mist 13 19:54 NE 7 4.00 Light BKNO07 36 35 41 36 97% 30 NA 30.05 1018.1 0.06 0.16 Rain OVC014 Fog/Mist 13 18:53 N 10 5.00 Light SCT009 36 35 97% 29 NA 30.08 1019.1 0.03 Rain OVC016 Fog/Mist 13 17:54 NE 9 6.00 Light SCT011 37 34 89% 30 NA 30.11 1020.2 Rain BKN015 Fog/Mist OVCO27 13 16:54 NE 8 10.00 Overcast OVC016 37 35 93% 31 NA 30.14 1021.1 0.03 0.07 13 15:54 NE 8 10.00 Overcast BKNO15 39 34 82% 33 NA 30.17 1022.1 0.01 OVCO28 13 14:54 NE 9 TOO Light OVCO29 39 36 89% 33 NA 30.21 1023.5 0.03 Rain 13 12:54 E 8 10.00 Overcast BKN032 44 22 OVC046 41 % 39 NA 30.28 1025.8 http://w1.weather.gov/data/obhistory/KBLTY.html 3/14/2017 National Weather Service: Observed Weather for past 3 Days: Burlington... Page 2 of 3 13 11:54 E 10 10.00 Mostly BICN050 44 23 43% 39 NA 30.30 1026.3 G 20 Cloudy BKN065 13 10:54 NE 10 10.00 A Few FEW060 41 23 49% 35 NA 30.32 1027.2 Clouds 13 09:54 NE 7 10.00 Fair CLR 38 27 65% 33 NA 30.37 1028.8 13 08:54 NE 5 10.00 Fair CLR 33 27 78% 28 NA 30.38 1029.1 13 07:54 NE 5 10.00 Fair CLR 28 25 31 25 88% 22 NA 30.36 1028.3 13 06:54 NE 5 10.00 Fair CLR 27 25 92% 21 NA 30.34 1027.9 13 05:54 NE 5 10.00 Fair CLR 25 22 88% 19 NA 30.34 1027.7 13 04:54 Calm 10.00 Fair CLR 27 24 89% NA NA 30.33 1027.2 13 03:54 Calm 10.00 Fair CLR 30 26 85% NA NA 30.31 1026.8 13 02:54 Calm 10.00 Fair CLR 29 24 92% NA NA 30.32 1027.2 13 01:54 Calm 10.00 Fair CLR 31 25 44 29 79% NA NA 30.33 1027.4 13 00:54 Calm 10.00 Fair CLR 33 27 78% NA NA 30.33 1027A 12 23:54 Calm 10.00 Fair CLR 35 26 70% NA NA 30.33 1027.4 12 22:54 Calm 10A0 Fair CLR 33 24 70% NA NA 30.33 1027.4 12 21:54 SE 3 10.00 Fair CLR 39 24 55% NA NA 30.32 1027.0 12 20:54 E 3 10.00 Fair CLR 41 22 47% NA NA 30.31 1026.E 12 19:54 SE 3 10.00 Fair CLR 44 19 50 43 37% NA NA 30.30 1026.2 12 18:54 S 3 10A0 Fair CLR 47 18 31% NA NA 30.26 1025.0 12 17:54 N 5 10.00 Fair CLR 50 13 22% 48 NA 30.24 1024.3 12 16:54 NA 10.00 Fair CLR 49 15 26% NA NA 30.25 1024.4 12 15:54 NW 6 10.00 Fair CLR 49 17 28% 46 NA 30.26 1024.9 12 14:54 Calm 10.00 Fair CLR 46 20 35% NA NA 30.29 1025.7 12 13:54 NA 10.00 Fair CLR 43 20 44 30 40% NA NA 30.31 1026.5 12 12:54 Vrbl 3 10.00 Fair CLR 41 23 49% NA NA 30.34 1027.5 12 11:54 Vrbl 5 10.00 Mostly BKN025 39 25 57% 35 NA 30.37 1028.5 Cloudy 12 10:54 Vrbl 3 10.00 Partly SCT013 35 28 76% NA NA 30.39 1029.3 Cloudy 12 09:54 Calm 2.00 Light BKN038 31 28 89% NA NA 30.38 1029.3 Snow BKN055 Fog/Mist OVC070 12 08:54 Calm 0.75 Light VV019 31 28 89% NA NA 30.38 1029.0 Snow Fog/Mist 12 07:54 NE 5 5.00 Light OVCO28 33 22 40 33 64% 28 NA 30.36 1028.5 Snow 12 06:54 Vrbl 7 8.00 Light OVC044 35 17 48% 29 NA 30.33 1027.4 Snow 12 05:54 N 8 10.00 Overcast BKNO70 37 8 30% 31 NA 30.31 1026.4 OVC080 12 04:54 N 8 10.00 Overcast OVC070 37 8 30% 31 NA 30.27 1025.3 12 03:54 N 8 10.00 Overcast OVC060 38 6 26% 32 NA 30.29 1025.7 12 02:54 N 7 10.00 Overcast BKN075 39 6 25% 34 NA 30.30 1026.1 OVC090 12 01:54 N 10 10.00 Overcast OVC095 40 7 46 39 25% 34 NA 30.28 1025.6 12 00:54 N 9 10.00 Mostly BKN095 41 7 24% 35 NA 30.26 1025.0 Cloudy http://wImeather.gov/data/obhistory/KBUY.html 3/14/2017 National Weather Service : Observed Weather for past 3 Days : Burlington... Page 3 of 3 11 23:54 N 6 10.00 Fair CLR 40 11 22:54 N 5 10.00 Fair CLR 41 11 21:54 N 6 10.00 Fair CLR 39 11 20:54 W 3 10.00 Fair CLR 40 11 19:54 Calm 10.00 Fair CLR 46 11 18:54 SW 7 10.00 Fair CLR 48 11 17:54 SW 6 10.00 Fair CLR 49 11 16:54 W 10 10.00 Fair CLR 50 11 15:54 W 10 10.00 Fair CLR 49 11 14:54 W 10 10.00 Fair CLR 48 11 13:54 W 9 10.00 Fair CLR 44 11 12:54 SW 8 10.00 Fair CLR 43 11 11:54 W 8 10.00 Overcast OVC110 40 11 10:54 N 13 10.00 Mostly BKN 120 40 Cloudy 109:54 NW 10.00 Fair CLR 40 10 11 08:54 NW 9 10.00 Fair CLR 37 13 33% 36 NA 30.25 1024.6 15 35% 38 NA 30.25 1024.7 17 41% 35 NA 30.24 1024.3 19 43% NA NA 30.21 1023.5 13 50 44 26% NA NA 30.20 1022.8 11 22% 45 NA 30.20 1022.8 7 18% 46 NA 30.20 1022.9 6 17% 46 NA 30.21 1023.1 3 15% 45 NA 30.23 1023.8 8 19% 44 NA 30.25 1024.4 11 45 34 26% 39 NA 30.28 1025.5 10 26% 38 NA 30.29 1025.8 10 29% 35 NA 30.31 1026.6 10 29% 32 NA 30.29 1026.0 14 35% 34 NA 30.29 1025.9 16 11 07:54 Calm 10.00 Fair CLR 34 18 39 32 Max. Min. 42% 30 NA 30.28 1025.5 52% NA NA 30.25 1024.5 altimeter sea D Air Drvpt Wind Heat level I hr 3 hr 6 hr a Time Wind Vis. Weather Sky 6 hour Relative Chill Index (in.) (mb) t (edt) (mph) (mi.) Cond. Humidity (.F) (OF) Precipitation e Temperature (°F) Pressure (in.) National Weather Service Back to previous page I Last Modified: Febuary, 7 2012 Southern Region Headquarters Privacy Policy Fort Worth, Texas Disclaimer http://wI.weather.gov/data/obhistoi-y/KBUY.htmi 3/14/2017 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted _12/27/2016 CERTIFICATE OF COVERAGE NO. NCG060040 SAMPLE COLLECTION YEAR July -December 2016 FACILITY NAME Mount Vernon Chemicals, LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Alamance PERSON COLLECTING SAMPLES Shawn Rudison LABORATORY Meritech, Inc Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results ❑ use/process meats ❑ use animal fats/byproducts DISCHARGING TO SALTWATERS? ❑YES X NO RECEIVED QED. 3 Q 2016 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 CENTRAL FII F; Total event rainfall 20.17 inches or ❑ No discharge this period Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, 0'^JR Standard units 5eoD,ION mg/L Oil and Grease, mg/L Fecal Coliform', Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 S00 SDO-1 12/6/16 15 8.6 38 < 5 N/A N/A SDO-2 12/6/16 6.6 8.7 26 < 5 N/A N/A SDO-3 12/6/16 23.3 8.1 24 < 5 N/A N/A SDO-4 12/6/16 3.3 7.7 78 < 5 N/A N/A ' Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50' 6.0 — 9.0 - (if yes, corn plete Part B) ' Only applies to facilities that use/process meats. 2 The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. S W U-249 Last Revised: October I S. 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: _Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" rep arts) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." G (Signature of Permittee) r z I z +--( 16 (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 ,VCc;ro 0 C/a d,., Q NC Department of ' Environmental Quality :K;;.;; • Received STORMWATER DISCHARGE OUTFALL (SDO) _• DEC 2 8 2016 ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year 2016 Winston-Salem �1:-• „. Individual NPDES Permit No. NCS❑❑❑❑❑❑ or T Certificate of Coverage (COC) No. NCG060040 This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March 1" of the following year, Facility Name: Mount Vernon Chemicals, LLC dba Apollo Chemical County: Alamance Phone Number: (336 5�0524 Total no. of SDOs monitored 4 Outfall No. SDO1 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No TotalTSS, Rainfall, inches glL mg/ rd units Standard a COD, mglL Oil and Grease, mg/L Fecal Coliform Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 — 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy 4/22/16 0.22 25 6.6 97 < 5 NIA NIA 12/6116 0.17 1 15 8.6 38 < 5 NIA NIA Additional Outfall Attachment SWU-264-Generic-25May2010 .. ;� y,., .� Ltd �.' W. �.ii ��r : C • 5 •7 • 1 �. 1_ � i.r•; 41 Lr Ci .ry � ._r W f,r L.a �._ � Z I� '� i �, Outfall No. SD02 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Total Rainfall, inches TSS, mglL Standard rd units a COD, mglL Oil and Grease, mg1L Fecal Coliform, Colonies per 100 ml Dnterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 — 9.0 120 30 1000 1000 Date Sample Collected, mm/ddtyy 4/22/16 0.22 53 7.3 115 < 5 NIA NIA 1216/16 0.17 6.6 8.7 26 < 5 N/A NIA Outfall No. SDO3 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No SW U-264-Generic-25May2010 Total Rainfall, inches TSS, m g 1L pH, Standard units COD, m IL g Oil and Grease, mglL Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 - 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy MMMMM 4/22116 0.22 118 7.5 150 12 NIA NIA 12/6116 0.17 23.3 8.1 24 ¢ 5 NIA NIA Outfall No. SD04 Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes No® Yes ❑ No Yes ❑ No Total Rainfall, inches TSS, mglL ard units Standard COD, mg1L Oil and Grease, mglL Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 - 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy 4/22/16 0.22 12 7.3 83 < 5 NIA NIA 1216/16 0.17 3.3 7.7 78 < 5 NIA NIA SW U-264-Generic-25 May2010 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature Date I2r' 2� I I,( - Mail Annual DMR Summary Reports to: DWQ Regional Office Contact Information: 'ASHEVILLE REGIONAL OFFICE FAYETTEVILLE REGIONAL OFFICE MOORESVILL_E_REGIONA_L OFFICE 2090 US Highway 70 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 (704) 663-1699 (910) 433-3300 RALEIG_H REGIONAL OFFICE_ W_AS_HI_NGT_ON_REGIONAL _OFFICE WILMINGTON REGIONAL OFFICE 3800 Barrett Drive 943 Washington Square Mall 127 Cardinal Drive Extension Raleigh, NC 27609 Washington, NC 27889 Wilmington, NC 28405-2845 (919) 791-4200 (252) 946-6481 (910) 796-7215 WINSTON_SALEM REGIONAL OFFICE CENTRAL OFFICE I 585 Waughtown Street 1617 Mail Service Center "To preserve, protect Winston-Salem, NC 27107 Raleigh, NC 27699-1617 and enhance _(336) 771-5000) 807-6300 North Carot;nas water... SWU-264-Generic-25May2010 r SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 05/18/2016 SAMPLE COLLECTION -Jun 2 1 CERTIFICATE OF COVERAGE NO. NCG060040 CO C ION YEAR January -June 0 6 FACILITY NAME Mount Vernon Chemicals LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Alamance ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Shawn Rudison DISCHARGING TO SALTWATERS? ❑YES X NO LABORATORY Meritech, Inc Lab Cert. # 165 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfoll 20.22 inches or ❑ No discharge this period' Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 500 SDO-1 04/22/2016 25 6.6 97 < 5 N/A N/A SDO-2 04/22/2016 53 7.3 115 < 5 N/A N/A SDO-3 04/22/2016 118 7.5 150 12 N/A N/A SDO-4 04/22/2016 12 7.3 83 < 5 N/A N/A 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at a� outfalls. You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfal! No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark 30 100 or 504 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at qny outfalls, you must still submit this discharge monitoring report with a checkmark here. (if yes, complete Part B) 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SWU-249 East Revised: October 18, 2012 Page l of 2 *FOR ?AR'rA AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Per ittee) (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year 2015 F7LI& RECEIVED—� N.C. Dept. of ENR JAN 1 1 2016 wINSiON-sALEM REGIONAL OFFICE Individual NPDES Permit No. NCS❑❑❑❑❑❑ or Certificate of Coverage (COC) No. NCG060040 This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March I" of the following year. Facility Name: Mount Vernon Chemicals, LLC dba Apollo Chemical County: Alamance Phone Number: (336)506-0524 Total no. of SDOs monitored 4 Outfail No. SDO1 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Total Rainfall, inches TSS, mglL pH, Standard units COD, mg1L Oil and Grease, mg1L Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 — 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy Emmmm 611115 0.56 3 6.4 62 < 5 NIA N/A 12/14115 0.12 11 8.9 80 < 5 NIA NIA Additional Outfall Attachment SWU-264-Generic-25May2010 Outfall No. S1302 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Total Rainfall, inches mg/L glrd Standard aunits mglL COD, Oil and Grease, mg/L Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 — 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy MMMMM 611115 0.56 28 6.8 94 < 5 NIA NIA 12/14/15 0.12 8 8.6 106 < 5 NIA NIA Outfall No. SD03 Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Yes ❑ No Yes ❑ No SWU-264-Generic-25May201 0 Total Rainfall, inches TSS, mglL pH, Standard units COD, mglL Oil and Grease, mglL Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 — 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy 611115 0.56 319 6.7 69 < 5 NIA NIA 12/14/15 0.12 15 8.0 67 7 NIA NIA Outfall No. SD04 Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes❑ No® Yes ❑ No Yes ❑ No Total Rainfall, inches TSS, mglL ard units Standard COD, mglL Oil and Grease, mglL Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 -- 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy M M 611115 0.56 12 6.0 87 <5 NIA NIA 12/14/15 0.12 4 8.7 39 <5 NIA NIA SW U-264-Generic-25 May2010 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature Date Mail Annual DMR Summary Reports to: DWQ Regional Office Contact Information: ASHEVILLE REGIONAL OFFICE FAYETTEVILLE REGIONAL OFFICE MOORESV_ ILLE,REGIONAL,OFFICE 2090 US Highway 70 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 (704) 663-1699 910 433-3300 RALEIGH REGIONAL OFFICE WASHINGTON REGIONAL OFFICE WILMINGTON REGIONAL OFFICE 3800 Barrett Drive 943 Washington Square Mall 127 Cardinal Drive Extension Raleigh, NC 27609 Washington, NC 27999 Wilmington, NC 28405-2845 (919) 791-4200 (252) 946-6481 (910) 796-7215 WINSTON-SAL'EM REGIONAL OFFICE CENTRAL OFFICE 585 Waughtown Street 1617 Mail Service Center 7opreserve, protect Winston-Salem, NC 27107 Raleigh, NC 27699-1617 and enhance i North- Carolinas water..." 336 771-5000 919 807-6300 SWU-264-Generic-25May2010 ITO fi,!� P A 8 8 1 0 N F. O R P E R VE C T I O N CHEMICALS. LLC 2001 Willow Springs Lane, Burlington, North Carolina 27215, PHONE 336-506-0524 FAX 336-228-6963 December 29, 2015 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2015 Semi -Annual NPDES Stormwater Report General Permit: NCG060000 COC No: NCG060040 Mount Vernon Chemicals, LLC 1 Apollo Chemical — Burlington Facility 2001 Willow Springs Lane Burlington, NC 27215 RECEIVED JAN 0 4 2016 CENTRAL RILES DWR SECTION Enclosed are the original and a copy of the stormwater monitoring results for the second half of 2015 for our Willow Springs Lane facility. Our stormwater outfalls were sampled during a significant rain event (documentation is attached). On -site measurement of pH was conducted at Apollo Chemical at the time of sampling. The samples were sent to Meritech, Inc. (Lab Certification No: 165) for analysis. The samples were tested for TSS, COD, and Oil & Grease. The Meritech report is appended. Our "Stormwater discharge outfall monitoring report" which includes pH results, is also appended. If you need additional information, please contact me. Sincerely, Mount Vernon Chemicals, LLCIApollo Chemical V\ Gary S. Dagenhart, Ph.D. Technical Director gdagenhart@apoilochemical.com Phone 336-506-0524 Copy: Plant Managers, Regulatory File, Corporate Director Environmental Affairs Apollo Chemical 2001 Willow Springs Lane, Burlington, North Carolina 27215 Tei: 336-226-1161 Fax: 336-228-6963 www.apollochemical.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 12/29/2015 CERTIFICATE OF COVERAGE NO. NCG060040 SAMPLE COLLECTION YEAR July -December 2015 FACILITY NAME Mount Vernon Chemicals, LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Alamance ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Shawn Rudison DISCHARGING TO SALTWATERS? ❑YES X NO LABORATORY Meritech, Inc Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE —> Total event rainfall 20.12 inches or ❑ No discharge this period Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 -120 30 1000 500 SDO-1 12/14/15 11 8.9 80 < 5 N/A N/A SDO-2 12/14/15 8 8.6 124 < 5 N/A N/A SDO-3 12/14/15 1s 8.0 67 7 N/A N/A SDO-4 12/14/15 4 8.7 39 < 5 N/A N/A 1 Only applies to facilities that use/process meats. zThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50' 6.0 — 9.0 - I Only applies to facilities that use/process meats. zThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. (ifyes, complete Part B) 4,ee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies SWU-249 I,ast Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER i REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." rAw IMAnj (Signature of Permittee) I Zr2.9120 f E (Date) Additional copies of this form may be downloaded at: http://"portal.ncdenr.org/webLw _qZws su n dessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT • for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 12/29/2015 CERTIFICATE OF COVERAGE NO. NCG060040 SAMPLE COLLECTION YEAR JuIV-December 2015 FACILITY NAME Mount Vernon Chemicals LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Alamance ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Shawn Rudison DISCHARGING TO SALTWATERS? ❑YES X NO LABORATORY Meritech, Inc Lab Cert. # 165 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: 5tormwater Benchmarks and Monitoring Results Total event rainfall 20. 12 inches or n No discharge this period Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 500 SDO-1 12/14/15 11 8.9 80 < 5 N/A N/A SDO-2 12/14/15 8 8.6 106 < 5 N/A N/A S DO-3 12/14/15 15 8.0 67 7 N/A N /A SDO-4 12/14/15 4 8.7 1 39 < 5 N/A N/A Only applies to facilities that use/process meats - The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504 6.0 — 9.0 - (ifyes, complete Part B) 1 Only applies to facilities that use/process meats. The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective bench mark applies. - SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • 'A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 11 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 116 k6 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wp/ws/su/npdessw4tab-4 SWU-249 Last Reprised: October 18, 2012 Page 2 of 2 0 SrATt Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this fawn, please visit: hat JIh2o.enr.siate.ne.us/su/Forms Docwnenls.hnn#miscforms Permit No.: N/C/ G/416l 0I 0l al 0l o, Certificate of Coverage No.: N/C/Gl 016l014/0/0/ Facility Name: Mount Vernon Mills, Inc t Mount Vernon Chemicals, LLC t Apollo Chernica4 County: Alamance. Phone No. (336) 566.0524 Inspector: Shawn Rudison Date of Inspection: 1211412M Time of Inspection: 2:45 - 3:0o PM Total Event Precipitation (inches): 0_12 Was this a Representative Storm Event? (See information below) W1Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed clueing a represenlative slorn? event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. 5DO1 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that Occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc,): NONE Page 1 of 2 S W U-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: l�L 3 4 5 5. Floating Solids, Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 0,140 8. Is there an oil sheen in the stormwater discharge? Yes 0 9. Is there evidence of erosion or deposition at the outfall? Yes (0) 1.0. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foarn, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions watTant further investigation. Page 2 of 2 S WU-242-1126CO Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://h2o.enr.state.ne.us/sufForrns_Doetiments.htrn#lmiscforms Permit No.: NICI G/0 16/ 0 / 0/ Ol Ol or Certificate of Coverage No.; NICIGI 0/6/0/4/0/0 I Facility Name: Mount Vernon Mills, Inc t Mount Vernon Chemicals, LLC t Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: 12/14/2015 Time of Inspection: 2:45 - 3:00 PM Total Event Precipitation (inches): 0_12 Was this a Representative Storm Event? (See information below) W1Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be pet formed during a representative slorrn event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SD02 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNK CREFK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR. COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., stills strongly of oil, weak chlorine odor, etc.): NONE Page I of 2 S WU-242-t 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 0 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is noossolids and 5 is the surface covered with floating solids: (1 } 2 3 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes (Lo 8. is there an oil sheen in the stormwater discharge? Yes No 9. is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SI U-242-lt2608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this forin, please visit: Itlty:/Ar2n.enr.state.nc.tts/su/Farms Documcnt_s,htuz#miscfornrs Permit No.: NICI G!O 1610I 0l 0l 0l or Cet-tificate of Coverage No.: NICIGI Of 6/ 01 l0 l0 I T acil itv Name: Mount Vernon Mills, Inc 1 Mount Vernon Chemicals, LLC ! Apoiio Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: 12/14/2015 Time of Inspection: 2:45 - 3:00 PM Total Event Precipitation (inches): 012 Was this a Representative Storm Event? (See information below) ZYes ❑ No Please check your permit to verify if Qualitative Monitoi•iiig ni.tisi Ise per foriiied cliiring a representative storm event (requirements vniy). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SD03 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, me(lium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smelIs strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 S W U-2,12-112608 4. Clarity: Choose the number which best describes the clai�ity of the discharge, where I is clear and 5 is very cloudy: (D 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is rio solids and 5 is the surface covered with floating solids: (D 2 3 4 5 C. Suspended Solids: Choose the number which best describes the amount of' suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes Na 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the oulfall? Yes Q 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2of2 S w u-24 z-112Gos Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisfornr, please visit, htip:Mi2o.enr.state.ne.iislsu/Forms Documents.lit m$miscforms Permit No.: NICI Glo l 610I QI 01 01 or Certificate of Coverage No.: NICIGI 016/ 0 /4 /O /0 Facility Name: Mount Vernon Mills, Inc 1 Mount Vernon Chemicals, LLC 1 Apollo Chemical County. Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: 12/1412015 Time of Inspection: 2.45 - 3:00 PM Total Event Precipitation (inches): 0.12 Was this a Representative Storm Event? (See information below) zYes ❑ No Please check your permit to verify if Qualitative Monitoring must be petforined daring a representative stoma event (requirements vaiy). A "Representative Storm Event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in wluch no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of PerTnittee 1. Outfall Description: Outfall No. 5°04 Structure (pipe, ditch, etc.) PIPE Deceiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3, Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2. SNVU-242-1t2608 4. ChWit.y: Choose the number which hest describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: (D 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 C. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: C1) 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfail? Yes Q M. Other Obvious Indicators of Storznwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion deposition may be indicative of pollutant exposure. These conditions warrant further investigation, Page 2 of 2 S WU-242-112b08 Meritech, .Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Shawn Rudison Client: Apollo Chemical 2001 Willow Spings Ln Burlington, NC 27216 Revised Date: 1213012015 Report Date: 12/28/2015 Date Sample Rcvd: 1.2/1.5/2015 Meritech Work Order # 12151569 Sample: SD01 Grab 1.2/14/15 2:45pm Parameters Result Analysis Date, Reporting Limit Method COD 80 mg/L 12/16/15 15 mg/L EPA 410.4 Total Suspended Solids 11 mg/L 12/17/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 12/16/15 5 mg/L EPA 1664A Meritech Work Order # 12151570 Sample: SD02 Grab 12/14/15 2:50pm Parameters Result Analysis Date Reporting Limit Method COD 87 mg/L 12/29/15 15 mg/L EPA 410.4 Total Suspended Solids 8 mg/L 12/17/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 12/16/15 5 mg/L EPA 1664A Meritech Work Order #t 121.51571 Sample: SD03 Grab 1.2/14/15 2:55pm Parameters Result Analysis Date Reporting Limit Method COD 67 mg/l, 12/16/15 15 mg/L EPA 410.4 Total Suspended Solids 15 mg/L 12/17/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) 7 mg/[, 12/19/15 5 mg/L EPA 1664A Meritech Work Order # 12151572 Sample: SD04 Grab 12/14/15 3:00pm Parameters Result Analysis Date Reporting_Limi Method COD 39 mg/l. 12/16/15 15 mg/L EPA 410.4 Total Suspended Solids 4 mg/L 12/17/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/l. 12/19/15 5 mg/L CPA 1664A I hereby certify that I have reviewed and approve this data. Laboratory Representative 642 Tantco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 From: won To- Shawn Rudison Subject: Storm water Sampling 12,14.2015 Date: Tuesday, December 15, 2015 9:49:43 AM Attached is the Rainfall record for the Burlington Airport for the Storm Water Monitoring Sample collected on 14-December-2015, collected from 2:45 — 3:00pm. The rain gauge at the Apollo Chemical - Burlington Facility measured 0.12 inches at the time of collection. I have measured the pH of each sample using a calibrated electrode using buffer 4 (Reagents Lot:7402048 EXP 2/2016), buffer 7 (Reagents Lot: 7403278 EXP 3/2016), and buffer 10 (Reagents Lot: 7403301 EXP 4/2014). The samples were equilibrated to a temperature of 18.9°C prior to sampling. SDO-1: pH 8.9 SDO-2: pH 8.6 SDO-3: pH 8.0 SDO-4: pH 8.7 Shawn Rudison Chemical Regulatory Specialist Research and Development / Regulatory Compliance Group Mount Vernon Chemicals, LLC / Apollo Chemical 336,506.0532 srudison@apoliochemical.com National Weather• Service : Observed Weather for past 3 Days : Burlington... Page 1 of 3 weather.gov • • r r �EAIj14 Burlington, Burlington Alamance Regional p Airport �; •�''' , Enter Your "City, ST" or zip code Go metric en espahol D Temperature (OF) Pressure Precipitation (in.) a Time t (est) Wind (mph) Vis. Sky Weather (mi.) Cond. Air Dwpt 6 flour Relative Humidity Wind Chill Heat Index altimeter sea level 1 to 3 hr 6 hr (,F) ('F) in () e Max. Min. (m5) 15 06:54 SW 7 10.00 Fair CLR 51 50 59 50 96% NA NA 29.75 1007.2 15 05:54 SW 5 10.00 Fair CLR 52 51 97% NA NA 29.73 1006.4 15 04:54 SW 3 10.00 Fair CLR 54 52 93% NA NA 29.72 1006.1 15 03:54 SW 6 10.00 Fair CLR 56 54 93% NA NA 29.71 1005.8 15 02:54 SW 7 10.00 Fair CLR 57 54 90% NA NA 29.72 1005.8 15 01:54 SW 9 10.00 Fair CLR 58 55 90% NA NA 29.70 1006.4 15 00:54 SW 9 10.00 Partly SGT017 59 55 69 59 87% NA NA 29.69 1004.9 Cloudy 14 23:64 SW 10.00 Mostly BKNO19 60 56 86% NA NA 29.68 1004.6 12 Cloudy 14 22:54 SW 10.00 Fair CLR 61 55 81% NA NA 29.67 1004.3 12 14 21:54 SW 9 10.00 Fair CLR 62 57 84% NA NA 29.66 1003.9 14 20:54 313 10.00 Fair CLR 65 59 81% NA NA 29.66 1003.9 G 20 14 19:54 SW 10.00 Mostly FEW023 67 60 79% NA NA 29.67 1004.1 13 G Cloudy BKN043 24 BKN060 14 18:54 SW 10.00 Overcast BKN039 69 64 69 66 84% NA NA 29.66 1004.1 0.08 12 G OVG095 21 14 17:54 812 10.00 Overcast BKNO21 69 66 90% NA NA 29.66 1003.9 OVCO26 14 16:54 S 9 10.00 Overcast FEW016 69 66 90% NA NA 29.6E 1004.5 OVCO25 14 15:54 87 10A0 Overcast FEW012 68 66 93% NA NA 29.69 1005.0 0.08 BKN016 OVC037 14 14:64 S 10 10.00 Overcast OVC013 68 66 93% NA NA 29.71 1005.7 0.03 14 13:54 S 8 1.75 Light BKNO06 67 66 97% NA NA 29.74 1005.5 0.05 Rain BKNO12 Fog/Mist OVC018 14 12:54 S 9 6.00 Light SKNO17 67 64 71 60 91% NA NA 29.77 1007.5 Rain OVCO21 Fog/Mist 14 11:84 S 16 10.00 Overcast FEW035 71 61 71 % NA NA 29.80 1008.8 G 24 BKN044 OVC095 14 10:54 S 9 G 10.00 Overcast OVC065 67 60 79% NA NA 29.86 1010.7 18 14 09:54 10.00 Overcast 66 60 81% NA NA 29.89 1012.0 _ http://wl.weather.gov/data/obhistoiy/KBUY.btinl 12/15/2015 National Weather Service : Observed Weather -k- past 3 pays :.Burlington... Page 2 of3 S 12_ BKN055 C 22 DVC070 14 08:54 Vrhl 5 10.00 Mostly SC-i 007 63 60 90% NA NA 20,91 1012.4 Cloudy SKN027 R KN070 14 07:64 SF 5 10.00 overcast .OVC005 62 60 93% NA NA 2.9.91 1012..E 14 06:54 S 6 10.00 Mostly BKNO08 60 59 61 59 96% NA NA 29,93 1013.3 Cloudy 14 05:54 Calm 10,00 Paiily SC-f 026 60 59 96% NA NA 29.94 1013.6 Cloudy 14 04:54 SF 7 8.D0 Overcast OVC002 61 60 97% NA NA 29.96 1014.3 14 03:54 S 5 0.75 Fog/Mist VV002 60 60 100a/6 NA NA 90.01 1015.7 14 02:54 S 6 5.00 FogliVist CVC003 60 59 96% NA NA 30.03 1016.6 14 01:54 83 10.00 A Few FEW055 59 58 96% NA NA 30.05 1D17.0 Clouds 14 00:54 S 3 1D,00 Partly SCT055 59 57 63 53 93% NA NA 30.05 1017.3 Cloudy 13 23:54 85 10.00 overcast OVC055 59 56 90% NA NA 30.08 1D18.3 13 22:54 Calm 10.00 Fair CLR 54 52 93% NA NA 30.09 1018.7 13 21:54 Calm 10.00 Parity SCT050 55 53 93% NA NA 30.10 1019.1 Cloudy 13 20:54 Calm 10.00 Partly SCTD34 58 54 87% NA NA 30.12 1019.7 Cloudy 13 19:54 Calm 10.00 Fair CLR 60 55 84% NA NA 30.12 1019.7 13 18.54 S 3 10.00 Fair CI_R 63 55 72 63 76% NA NA 30.13 1020.1 13 17:54 S 3 10.00 Fair CLR 64 54 70a/a NA NA 30.12 1019.7 13 16:54 S 6 10.00 Fair CLR 67 54 63% NA NA 30,13 1020.0 13 16:64 S 5 10.00 Fair CLR 69 53 57% NA NA 30,12 1019.8 13 14:54 S 9 10,00 Fair CLR 72 53 52.a/a NA NA 3012 1019.8 13 13:54 SW 10,00 Fair CLR 72 55 55% NA NA 30.14 1020.3 10 13 12:54 SW 6 10.00 Fair CLR 70 56 70 44 61% NA NA 30.17 1021.2 13 11:54 Calm 10.00 Fair CLR 67 58 73% NA NA 30A9 1022.0 13 10:64 S 3 10,00 Fair CLR 62 58 863% NA NA 30.23 1023A 13 09:54 Calm 6,0C Fog/Mist CLR 56 55 97% NA NA 30.24 1023.9 13 08:54 Calm 0.75 Fog/Mist W001 60 50 100% NA NA 20.23 1023.5 13 07:54 Calm 0.25 Fog VV001 46 46 100% NA NA 30.23 1023.4 13 06:54 Calm 0,25 Fog W001 45 45 49 44 100% NA NA 30.22 1023.4 13 05:54 Calm 0.25 Fog W001 46 46 100% NA NA 30.21 1023.0 13 04:54 Calm 0.50 Fog W001 47 47 1DO% NA NA 30.20 1022.6 13 03:54 Calm 0.25 Fog VV001 49 40 97% NA NA 30,20 1022.5 13 02:54 Calm 0.25 Fog VV001 47 47 100% NA NA X21 1022.7 13 01:54 Calm 0.25 Fog W001 48 48 100% NA NA 30.22 1023.1 13 00:54 Calm 0.25 Fog VV001 48 48 63 48 100% NA NA 30,22. 1023.1 12 23:54 Calm 6.00 Fog/Mist CLR 50 49 96% NA NA 3C.23 1023.4 12 22:54 Calm 0.25 Fog VV002 50 49 06% NA NA 30.23 1023.4 12 21:54 Calm 0.50 Fog CLR 53 53 100% NA NA 30.22 1023.3 http-//wI.weatlier.gov/data/obhistoryjTOUY.litml 12115/2M It National Weather Service: Observed Weather for past 3 Days : Burlington... Page 3 of 3 12 20:54 Calm 8.00 Fair CLR 54 54 100% NA NA 30.23 1023,5 12 19:54 Calm 10.00 Fair CLR 56 54 93% NA NA 30.23 1023.6 12 18:54 S 5 10.00 Fair CLR 63 57 72 63 81% NA NA 30.22 1023.2 12 17:54 S 6 10.00 Fair CLR 65 57 76% NA NA 30.20 1022,5 12 16:54 S 5 10.00 Fair CLR 68 58 70% NA NA 30.19 1022.1 12 15:54 Vrbf6 10.00 Fair CLR 70 57 64% NA, NA 30.19 1022.0 12 14:54 S 7 10.00 Fair CLR 71 58 63% NA NA 30.17 1021.5 12 13.54 SW 8 10.00 Fair CLR 71 58 63% NA NA 30.18 1021.8 12 12:54 SW 8 10.00 Fair CLR 69 58 69 50 68% NA NA 30.20 1022A 12 11:54 Vrbl5 10.00 Fair CLR 65 59 81% NA NA 30.22 1023.1 12 10:54 SW 6 10.00 overcast OVC006 63 59 87% NA NA 30.24 1023-9 12 09:54 SW 6.00 Fog/Mist OVC004 61 59 93% NA NA 30.25 1024.1 10 12 08:54 SW 6 2.00 Fog/Mist OVC002 58 58' 100% NA NA 30.23 1023.5 12 07:54 S 3 0.50 Fog VV003 55 55 100% NA NA 30.21 1022.9 D Vis. Sky Air Max. Min. Dw t p Relative Wind Heat altimeter (in.) Sea level 1 hr 3 hr 6 hr a Time t (est) Wind (mph) (mi.) Weather Cond. 6 hour Humidity Chill (•F) Index (,F) (mb) e Temperature (OF) Pressure Precipitation (in.) Last Modified: Febuary, 7 2012 Privacy Policy !National Weather Service eVlois BaGI( to I le e P 9 Southern Region Headquarters Fort Worth. Texas Disclaimer http://w l .weather-gov/data/obhistoiy/l�BUY.htinl 12/15/20J5 P.A.8.8 IONFOR P_E.R F E C,Tii.O;N. 2001 Willow Springs Lane, Burlington, North Carolina 27215, PHONE 336-506-0524 FAX 336-228-6963 January 7, 2016 _ RECE Vf_-u Central Files JAIL 12 2016 Division of Water Quality CENTRAL. FILES 1617 Mail Service Center DWR SECTION Raleigh, NC 27699-1617 Re: 2015 Semi -Annual NPDES Stormwater Report for Second Half REVISION OF ORIGINAL REPORT DATED DECEMBER 29, 2015 General Permit: NCG060000 COC No: NCG060040 Mount Vernon Chemicals, LLC 1 Apollo Chemical - Burlington Facility 2001 Willow Springs Lane Burlington, NC 27215 Enclosed are the original and a copy of the stormwater monitoring results for the second half of 2015 for our Willow Springs Lane facility. Our stormwater outfalls were sampled during a significant rain event (documentation is attached). On -site measurement of pH was conducted at Apollo Chemical at the time of sampling. The samples were sent to Meritech, Inc. (Lab Certification No: 165) for analysis. The samples were tested for TSS, COD, and Oil & Grease. The Meritech report is appended. Our "Stormwater discharge outfail monitoring report" which includes pH results, is also appended. The original report included data for COD for SDO-2 that was slightly above the benchmark (124 vs 120). The same sample was retested by Meritech, with a value of 87 determined. The two results (124 and 87) were averaged, and the average 106 is below the benchmark. That data is reported in this revised report. If you need additional information, please contact me. Sincerely, Mount Vernon Chemicals, LLCIApollo Chemical Gary S. Dag art, Ph.D. Technical Director da enhari a ollochemical.com Phone 336-506-0524 Copy: Plant Managers, Regulatory file, Corporate Director Environmental Affairs Apollo Chemical 2001 Willow Springs Lane, Burlington, North Carolina 27215 Tel: 336-226-1161 Fax: 336-228-6963 www, apollochemical.com r Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report �� d D /-/d For guid nace on filling out This farm, please visil: Permit No.: NICI i / 6/ 0/ 01 0/ 0/ or Certificate of Coverage No.: NICIGI OF6TOI�Pl Facility blame: T Mount Vernon Mills, Inc ! Mount Vernon Chemicals, LLC 1 Apollo Chemical County: Alamance Phone No, (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: 12/14/2015 Time of inspection: 2:45 - 3:00 PM Total Invent Precipitation (inches): 0_12 Was this a Representative Storm Event? (See information below) 7Yes ❑ No Please check your permit to verify if'Qualitative M017it0t-ill,� must he performed ditring a representative Storm event (requirements vary), A "Representative Storm Lvent" is a storm event that treasures greater than 0. l inches of rainfall and that is preceded by at. least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: GIN A, -- (Signature of Pertittee or Designee) 1. Outfall Description: Outfall No. Soot Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using hasic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page l of 2 r�ji.+nrvurr��. i� JrXils S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: lQ 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes oNo S. Is there an oil sheen in the stormwater discharge? Yes Q 9. Is there evidence of erosion or deposition at the outfall? Yes lob 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12GD8 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For l;rridwice onfilling orrt this form, please visit: http://h20.enr.state.nc.us/su/Forms DOCLI]nentS.11l[11#nliscforms Permit No.: NICI G/0 / 6/ 0/ 01 0I 0I or Certificate of Coverage No.: NICIGI 0I 6l 0l4 /0 l0 1 Facility Name: Mount Vernon Mills, Inc 1 Mount Vernon Chemicals, LLC / Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspcdor: Shawn Rudison Date of Inspecticm: 12114/2015 'I'fine of Inspection: 2:45 - 3:00 PM Total Event Precipitation (inches): 0_12 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if'Quctlitatitve Monitoring must be petformed during a representative storm event (requirements val'1'). A "Representative Storm lvent" is a storm event that measures greater than 0. l inches of rainfall and that is preceded by at least 72 hours Q days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1� (Signature of Pernlittee or Designee) 1. Outfall Description: Outfall No. SD02 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area. CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, ulcdiunl, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page I of 2 54vU-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: D 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: Ol 2 3 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspended solids in (lie stormwater discharge, where I is no solids and 5 is extremely muddy: D 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes (NOj S. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No Itl. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 42 S wU-242-112608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling ow ibis form. please visit: http://h2o-enr,state.tic.us/su/Foriiis DOCuillents,lltnl#nliscforms Permit No.: NICI i 1 6101 0/ 0/ O/ or Certificate of Coverage No.: NICIGI 0/ 6l 0 /4 /0 /0 I Facility Name: Mount Vernon Mills, Inc! Mount Vernon Chemicals, LLC t Apollo Chemical County: Alamance Phone No. (336) 506-0524 1115DeCtOr: Shawn Rudison Date of Inspection: 12114/2015 Tinge of Inspection: 2:45 - 3:0o PM Total Event Precipitation (inches): 0_12 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permil to verify if Qualitative Monitoring must be petformed during a representative storm eveltt (requ relncllts vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours Q days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. I3y this signature, E certify that this report is accurate and complete to the best of my knowledge: v (Signature of Pernlittee or Designee) 1. Outfall Description: Outfall No. S003 Structure (pipe, ditch, etc.) PIPE IZeCeiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page l of 2 swu-242-1t 26aa 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where l is no solids and 5 is the surface covered with floating solids: O 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where l is no solids and 5 is extremely muddy: D 2 3 4 5 7. Is (here any foam in the stormwater discharge? Yes i o R. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes No I11. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or crosionldeposilion may be indicative of pollutant exposure. These conditions warrant further investigation. ['acre 2 of 2 SwU-242- t t 260E Stormwater Discharge Out#'all (SDO) Qualitative Monitoring Report 1�olglddance on.filling Out this form, please visit: httf)://l12o.enr.sl ite.nc.us/silt)'orrns_Documents.hln]#miscforms Permit No.: NIC/ G/O 1610/ 0/ 01 01 or Certificate of Coverage No.: N/C/GI 01 6/0/4 /0 /0 1 hacililV Name: Mount Vernon Mills, Inc 1 Mount Vernon Chemicals, LLC / Apollo Chemical Courtly: Alamance Phone No. (336) 506-0524 Inspector. Shawn Rudison Date of Inspection: 12114/2015 'Time o1' Inspection: 2:45-3:00 PM Total Event Precipitation (inches): 0.12 Was this a Represeruative Storm Event? (See information below) ZYes ❑ No Please check your permit to ver-ify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Invent" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: cs> P- (Signature of PCI'nlitteC Designee) 1. Outlall Description: Out[all No. SDO4 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, wean chlorine odor, etc.): NONE Page I of 2 S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: /r'� [ l} 2 3 4 5 5. Floating Solids: Choose the ninrrber which best describes the amount of floating solids in the storrnwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the arrrourlt of suspended solids in the storrnwater discharge, where l is no solids and 5 is extremely muddy: I) 2 3 4 5 7. Is there any foam in the storrnwater discharge? Yes e S. is there an oil sheen in the storrnwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes o 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of I'o tirr, oil sheen, or erosionldeposition may be indicative of pollutant exposure. "These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12608 Meritech., Inc. Environmental Laboratory Laboratory Certification No.165 i _ F Contact: Shawn Rudison Report Date: 12/28/2015 Client: Apollo Chemical 2001 Willow Spings Ln Burlington, NC 2721.6 Date Sample Rcvd: 12/15/2015 Meritech Worlc Order # 12151569 Sample: SD01 Grab 12/14./15 2:45pm Parameters Result Analysis Date Reporting; Limit Method COD 80 mg/L 12/16/15 15 mg/L EPA 410.4 Total SUspended Solids 1.1 mg/l, 12/17/15 2.5 mg/L SM 2540 D Oil & Grease (11EM) <5 mg/L 12/16/15 5 mg;/L EPA 1664A Meritech Worl( Order it 12151570 Sample: SD02 Grab 12/14/1.5 2:50pm Parameters Result Analysis Date Reporting Limit Method COD 1.24 mg/L 1.2/16/1.5 1S mg/L EPA 410.4 Total Suspended Solids 8 mg/L 12/17/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) <S mg/1, 1.2/16/15 5 mg/L EPA 1664A Meritech Work Order it 121S1571 Sample: SI)03 Grab 12/14/15 2:55pm Parameters Result Analysis Date Reporting; Limit Method COD 67 mg/I, 12/16/15 15 mg/I, EPA 410.4 Total Suspended Solids 15 mg/L 12/17/15 2,5 mg/L SM 2540 D Oil & Grease (HEM) 7 mg/L 12/19/15 5 mg/L EPA 1664A Meritech Work Order It 12151572 Sample: SD011 Grab 12/14/15 3:00pm Pai ameters Result Analysis Date Reporting; Limit Method COD 39 mg/L 12/16/15 15 mg/L EPA 410.4 Total Suspended Solids 4 mg/L 12/17/15 2.5 mg/L SM 2 540 D Oil & Grease (1-1FM) <S mg/L 12/19/15 5 mg/L EPA 1664A I hereby certify thati have reviewed and approve this data. '619 Lahm-atoty Representative 642 'ramco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax,(336)342-1522 Chain of Custody Record CQC Client: Address. Attention. Apollo Chemical 2001 Willow Springs Ln Burlington, NC 27216 Shawn Rudison NPDES #: Phone: 336-506-0532 Fax: Email: srudisonr(oapollochemical.com Project: PO #: ERITECH INC. Environmental Laboratories A Division of Water Tecbnology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab@belisouth.net Web Site: www.meritech-labs.corn Turn Around Time* Std (10 days) x 3 - 5 Day o 24 - 48 Fir Sample p Location/lD # Sampling Dates & Ti � g es Times Person Taking Sample (Signature): Lab Use Only START END comp? Grab? #of costs. Tests Required On Ice? `:. pH OK? C12 OK? Date Time Date Time SDO1 12/14/15 2:45pm 3 Oil+Grease, COD. TSS Yes SD02 12/14/15 2:50pm 3 Oil+Grease, COD, TSS Yes SD03 12/14/15 2:55pm 3 Oil+Grease, COD, TSS w� Yes I SDO4 12/14/15 3:00pm 3 Oil+Grease, COD, TSS Yes ., Method of Shipment: Comments: UPS Fed Ex Hand Delivery Other Will these results be used for regulatory purposes? Yes X No *RUSH work must be approved prior to submitting samples. Relinquished} Date: Tom: -' J' *- — 1211512015 ?; . Received by: Date: Time: Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Dale: Time: JR rved at b y- Date: Time: -. From: Shawn Rudison To: Shawn Rudison Subject: storm Water Sampling 12.14.2015 Date: Tuesday, December 15, 2015 9:49:43 AM Attached is the Rainfall record for the Burlington Airport for the Storm Water Monitoring Sample collected on 14-December-2015, collected from 2:45 — 3:OOpm. The rain gauge at the Apollo Chemical - Burlington Facility measured 0.12 inches at the time of collection. I have measured the pH of each sample using a calibrated electrode using buffer 4 (Reagents Lot:7402048 EXP 2/2016), buffer 7 (Reagents Lot: 7403278 EXP 3/2016), and buffer 10 (Reagents Lot: 7403301 EXP 4/2014). The samples were equilibrated to a temperature of 18.9°C prior to sampling. SDO-1: pH 8.9 SDO-2: pH 8.6 SDQ-3: pH 8.0 SD0-4: pH 8.7 Shown Hudson Chemical Regulatory Specialist Research and Development / Regulatory Compliance Group Mount Vernon Chemicals, LLC / Apollo Chemical 336.506.0532 srudison@apollochemical.com , • National Weather Service : Observed Weather- for past 3 Days : Burlington... Page 1 of 3 weather,gov s • 4 �tAIIjt9 Burlington, Burlington Alarnance Regional •r m Airport,.,° .. Entor Your "City, ST" or zip code Go metric en espariol p Temperature (°F) Pressure Precipitation (in.) a Time Wind Vis. Weather Sky 6 hour Relative Wind Chili Heat Index altimeter 5ea t (as() (mph) (mi.) Cond. Air ❑wpt Humidity ('F) ('F) (in) level 1 hr 3 hr 6 hr e Max. Min. (mh) 15 06:54 SW 7 10.00 Fair CLR 51 50 59 50 96% NA NA 29.75 1007.2 15 05:54 SW 5 10.00 Fair CLR 52 51 97% NA NA 29.73 1006.4 15 04:54 SW 3 10.00 Fair CLR 54 52 93% NA NA 29.72 1006.1 15 03:54 SW 6 10,00 Fair CLR 56 54 93% NA NA 29.71 1005.8 15 02:54 SW 7 10.00 Fair CLR 57 54 90% NA NA 29.72 1005.8 15 01:54 SW 9 10.00 Fair CLR 58 55 90% NA NA 29.70 1005.4 15 00:54 SW 9 10.00 Partly SCT017 59 55 69 59 87% NA NA 29.69 1004.9 Cloudy 14 23:54 SW 10.00 Mostly BKNO19 60 56 86% NA NA 29.68 1004.6 12 Cloudy 14 22:54 SW 10.00 Fair CLR 61 55 81% NA NA 29.67 1004.3 12 14 21.54 SW 9 10.00 Fair CLR 62 57 84% NA NA 29.66 1003.9 14 20:54 S 13 10.00 Fair CLR 65 59 81% NA NA 29.66 1003.9 G 20 14 19:54 SW 10.00 Mostly FEW023 67 60 79% NA NA 29,67 1004.1 13 G Cloudy BKN043 24 BKN060 14 18:54 SW 10.00 Overcast BKN039 69 64 69 66 84% NA NA 29.66 1004.1 0.08 12 G OVC095 21 14 17:54 S 12 10.00 Overcast BKN021 69 66 90% NA NA 29.66 1003.9 OVCO26 14 16:54 S 9 10.00 Overcast FEW016 69 66 90% NA NA 29.68 1004.5 OVCO25 14 15:54 S 7 10.00 Overcast FEW012 68 66 93% NA NA 29.69 1005.0 0.08 BKNO16 OVC037 14 14:54 S 10 10.00 Overcast OVC013 68 66 93% NA NA 29.71 1005.7 0.03 14 13:54 S 8 1.75 Light BKNO06 67 66 97% NA NA 29.74 1006.5 0.05 Rain BKNO12 Fog/Mist OVC018 14 12:54 S 9 6.00 Light BKNO17 67 64 71 60 91% NA NA 29.77 1007.5 Rain OVCO21 Fog/Mist 14 11:54 S 16 10.00 Overcast FEW035 71 61 71% NA NA 29.80 1008.8 G 24 BKN044 OVC095 14 10:54 S 9 G 10.00 Overcast OVC065 67 60 79% NA NA 29.86 1010.7 18 14 09:54 10.00 Overcast 66 60 81% NA NA 29.89 1012.0 http://wI.weather.gov/data/obhistory/KBUY.html 12/15/2015 . National Weather Service : Observed Weather for past 3 Days : Burlington... Page 2 of 3 S 12 BKN055 G 22 OVC070 14 08:54 Vrbl5 10.00 Mostly SCT007 63 60 90% NA NA 29.91 1012.4 Cloudy BKN027 BKN070 14 07:54 SE 5 10.00 Overcast OVC005 62 60 93% NA NA 29.91 1012.6 14 06:54 S 6 10.00 Mostly BKNO08 60 59 61 59 96% NA NA 29.93 1013.3 Cloudy 14 05:54 Calm 10.00 Partly SCf026 60 59 96% NA NA 29.94 1013.6 Cloudy 14 04:54 SE 7 8.00 Overcast OVC002 61 60 97% NA NA 29.96 1014.3 14 03:54 S 5 0.75 Fog/Nisi VV002 60 60 100% NA NA 30.01 1015.7 14 02:54 S 6 5.00 Fog/Mist OVC003 60 59 96% NA NA 30.03 1016.6 14 01:54 S 3 10,00 A Few FEW055 59 58 96% NA NA 30.05 1017.0 Clouds 14 00:54 S 3 10.00 Partly SCT055 59 57 63 53 93% NA NA 30.05 1017.3 Cloudy 13 23:54 S 5 10.00 Overcast OVC055 59 56 90% NA NA 30.08 1018.3 13 22:54 Calm 10.00 Falr Ct_R 54 52 93% NA NA 30.09 1018.7 13 21:54 Calm 10.00 Partly SCl'050 55 53 93% NA NA 30.10 1019.1 Cloudy 13 20:54 Calm 10.00 Parfly SCT034 58 54 87% NA NA 30.12 1019.7 Cloudy 13 19:54 Calm 10.00 Fair CLR 60 55 84% NA NA 30,12 1019.7 13 18:54 S 3 10.00 Fair CI_R 63 55 72 63 76% NA NA 30.13 1020.1 13 17:54 S 3 10.00 Fair CLR 64 54 70% NA NA 30.12 1019.7 13 16:54 S 6 10.00 Fair CLR 67 54 63% NA NA 30,13 1020.0 13 15:54 S 5 10.00 Fair CLR 69 53 57% NA NA 30.12 1019.8 13 14,54 89 10.00 Fair CLR 72 53 52% NA NA 30.12 1019.8 13 13:54 SW 10,00 Fair CLR 72 55 55% NA NA 30A4 1020.3 10 13 12:54 SW6 10.00 Fair CLR 70 56 70 44 61% NA NA 30,17 1021.2 13 11:54 Calm 10.00 Fair CLR 67 58 73% NA NA 30.19 1022.0 13 10:54 S 3 10,00 Fair CLR 62 58 86% NA NA 30.23 1023.4 13 09:54 Calm 6.00 Fog/Mist CLR 56 55 97% NA NA 30.24 1023.9 13 08:54 Calm 0.75 Fog/Mist VV001 50 50 100% NA NA 30.23 1023.5 13 07:54 Calm 0.25 Fog VV001 46 46 100% NA NA 30.23 1023.4 13 06:54 Calm 0.25 Fog VV001 45 45 49 44 100% NA NA 30.22 1023.4 13 05:54 Calm 0.25 Fog W001 46 46 100% NA NA 30.21 1023.0 13 04:54 Calm 0.50 Fog VV001 47 47 100% NA NA 30,20 1022.6 13 03:54 Calm 0.25 Fog VV001 49 48 97% NA NA 30.20 1022.5 13 02:54 Calm 0,25 Fog VV001 47 47 100% NA NA 30.21 1022.7 13 01:54 Calm 0.25 Fog VV001 48 48 100% NA NA 30.22 1023.1 13 00:54 Calm 0.26 Fog VV001 48 48 63 48 100% NA NA 30.22 1023.1 12 23;54 Calm 5.00 Fog/Mist CLR 50 49 96% NA NA 30.23 1023.4 12 22:54 Calm 0.25 Fog VV002 50 49 06% NA NA 30.23 1023.4 12 21:54 Calm 0.50 Fog CLR 53 53 100% NA NA 30,22 1023.3 http://w l .weather,gov/data/oblhistory/KBUY.htm1 12/15/2015 National Weather Service : Observed Weather for past 3 Days : Burlington... Page 3 of 3 12 20:54 Calm 8.00 Fair CLR 54 54 100% NA NA 30.23 1023.5 12 19:54 Calm 10.00 Fair CLR 56 54 93% NA NA 30.23 1023.6 12 18:54 S 5 10.00 Fair CLR 63 57 72 63 81% NA NA 30,22 1023.2 12 17:54 S 6 10.00 Fair CLR 65 57 76% NA NA 30.20 1022.5 12 16:54 S 5 10.00 Fair CLR 68 58 70% NA NA 30.19 1022.1 12 15:54 Vrbl 6 10.00 Fair CLR 70 57 64% NA- NA 30.19 1022.0 12 14:54 S 7 10.00 Fair CLR 71 58 63% NA NA 30.17 1021.5 12 13:54 SW 8 10.00 Fair CLR 71 58 63% NA NA 30.18 1021.8 12 12:54 SW 8 10,00 Fair CLR 69 58 69 50 68% NA NA 30.20 1022.4 12 11:54 Vrbl5 10.00 Fair CLR 65 59 81% NA NA 30.22 1023.1 12 10:54 SW 6 10.00 Overcast OVC006 63 59 87% NA NA 30.24 1023.9 12 09:54 SW 6.00 Fog/Mist OVC004 61 59 93% NA NA 30.25 1024.1 10 12 08:54 SW 6 2.00 Fog/Mist OVC002 58 58 100% NA NA 30.23 1023.5 12 07:54 S 3 0.50 Fog VV003 55 55 100% NA NA 30.21 1022.9 D a Time Wind Vis. Sky Air Max. Min. Dry t p Relative Wind Heal alti peter ) sea level 1 hr 3 hr 6 hr t (est) (mph) (mi.) Weather Cond. 6 hour Humidity Chi)] Index (mb) (7) ('F) e Temperature (IF) Pressure Precipitation (in.) National Weather Service Back to Last Modified: Febuary, 7 2012 Southern Region Headquarters previous page Privacy Policy Fort Worth, Texas Disclaimer http://w 1.weather.gov/data/obhistory/KBLTY.htm1 12/15/2015 4- a MOUNT'INRNON CHEMICALS, LLC 2001 Willow Springs Lane, Burlington, North Carolina 27215, PHONE 336-506-0524 FAX 336-228-6963 June 25, 2015 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2015 Semi -Annual NPDES Stormwater Report lREt V ED JUN 2 9 2015 CENTRAL FILES DWR SECTION General Permit: NCG060000 COC No: NCG060040 Mount Vernon Chemicals, LLC 1 Apollo Chemical — Burlington Facility 2001 Willow Springs Lane Burlington, NC 27215 Enclosed are the original and a copy of the stormwater monitoring results for the first half of 2015 for our Willow Springs Lane facility. Our four stormwater outfalls were sampled during a significant rain event (documentation is attached). On -site measurement of pH was conducted at Apollo Chemical at the time of sampling. The samples were sent to Meritech, Inc. (Lab Certification No: 165) for analysis. The samples were tested for TSS, COD, and Oil & Grease. The Meritech report is appended. Our "Stormwater discharge outfall monitoring report" which includes pH results, is also appended. If you need additional information, please contact me. Sincerely, Mount Vernon Chemicals, LLC/Apollo Chemical C5 D Gary S. Dagenhart, Ph.D. Technical Director gdagenhart@apollochemical.com Phone 336-506-0524 Copy: Plant Managers, Regulatory File, Corporate Director Environmental Affairs Apollo Chemical 2001 Willow Springs Lane, Burlington, North Carolina 27215 Tel: 336-226-1161 Fax: 336-228-6963 www.apollochemical.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 6/25/2015 CERTIFICATE OF COVERAGE NO. NCGO60040 SAMPLE COLLECTION YEAR January -June 2015 FACILITY NAME Mount Vernon Chemicals LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Alamance ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Shawn Rudison DISCHARGING TO SALTWATERS? ❑YES X NO LABORATORY Meritech, Inc Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall 20.18 inches or ❑ No discharge this period] Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml _ Enterococcil, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 Soo SDO-1 6/1/2015 3 6.4 62 < 5 N/A N/A SDO-2 6/1/2015 28 6.8 94 < 5 N/A N/A SDO-3 6/1/2015 319 6.7 69 < 5 N/A N/A SDO-4 6/1/2015 12 6.0 87 < 5 N/A N/A 1 Only applies to facilities that use/process meats. zThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at an_y outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504 6.0 — 9.0 - 1 Only applies to facilities that Use/process meats. zThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. (if yes, complete Part B) 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies SWU-249 Last Revised: October 18, 2012 Page 1 of 2 .r *FOR PART A AND PART S MONITORING RESULTS: • A,BENCiAMARK EXCEEDANCE TRIGGERS TIER I REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including_ all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to. - Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of PermWtee) 6125 /2* 15 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 S- Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: httR://h2o.enr.state.ne.us/su/Forms Documents.htm#miseforms Permit No.: NICI G1O / 6l 01 0/ 0l 0l or Certificate of Coverage No.: N/C/Gl 0/ 6/0/4 /0 /0 Facility Name: Mount Vernon Mills, Inc! Mount Vernon Chemicals, LLC t Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison > Date of tnspect.ion: 6/1/2015 Time of Inspection: 5:30 - 5:45 PM Total Event Precipitation (inches): 1.67 Was this a Representative Storm Event? (See information below) ZYes ❑ No PIease check your permit to verify' if Qualitative Monitoring must be petfornted during a representative stone event (requirements vary). ........... _.-_ __-------------- -. _ _----- _-...--.._--.---.._--_.----. _ ._ __.-__._-_-. _ _— ----- A A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event treasuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: f WIS' (Signature of PermittYe or Designee) I. Outfall Description: Outfall No. 5D01 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear - and 5 is very cloudy: D 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where l is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where l is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes CNOD S. is there an oil sheen in the stormwater discharge? Yes No 9. is there evidence of erosion or deposition at the outfalI? Yes Rio 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosionldeposition may be indicative of pollutant exposure. "These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12609 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: httpa/h2o.enr. state. nc.uslsu/Forms_Documents.htm#miscforms Permit No.: NICI G/O / 6/ 0l 0/ 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0l 6l 0l4 /0 /0 Fact I Ily Name: Mount Vernon Mills, Inc r Mount Vernon Chemicals, LLC 1 Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: Time of Inspection: 6/1/2015 5:30-5:45PM Total Evcnt Precipitation (inches): 1_67 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must he performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0. l inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of PerMi tee or Designee) 1. Outfall Description: Outfali No. Soot Structure (pipe, ditch, etc.) PIPE Rcceiving stream: GUNN CREEK Describe the industrial activities that occur within the out.fall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: C 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes UtN l(). Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For ifidance on filling out this foam, please visit: http://h2o.enr.state,nc.us/su/Forms_Docutnent.0triAniscforms Permit No.: NICI G/O 16/ 0/ 0/ OI 41 or Certificate of Coverage No.: NICIGI 0/ 610/4/0/0/ I'aci I i I v Name: Mount Vernon Mills, Inc t Mount Vernon Chemicals, LLC 1 Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: 6/1/2015 Time of Inspection: 5:30 - 5:45 PM Total Event Precipitation (inches): 167 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed daring a representative storm event (requirements vary), — — -- -- -- .._. - -- ...----... — -- - ..---.-- .._-... _-_-----------_----_-_. A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. I3y this signature, I certify that this re ort is accurate and complete to the best of my knowledge: C. &i2y(-.,s (Signature of Permittee orYesignee) 1. Outfall Description: Outfall No. S003 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Light Brown 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page I of 2 S W U-242- 11260 S 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: l 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes N 8. is there an oil sheen in the stormwater discharge? Yes No 9. is there evidence of erosion or deposition at the outfall? Yes No to. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. `These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onji'lling oul this form, please visit: htti)://li2o.enr.state.nc.us/su/Forms_ Documents.htm#miscforms Permit No.: NICI G/O / 6101 0/ 0/ 01 or Certificate of Coverage No.: NICIGI 0/ 6/ 014 /0 /0 I Facility Name: Mount Vernon Mills, Inc! Mount Vernon Chemicals, LLC / Apollo Chemical County. Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: 6/1/2015 Time of Inspection: 5:30 - 5:45 PM Total Event Precipitation (inches): 1_67 Was this a Representative Storm Event? (See information below) zYes ❑ No Please check your permit to verify if Qualitative Monitoring must be petfonned daring a representative storm event (requirements vary). A `Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: GS GJ� ,� b I-L51 TO (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. So04 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: C"EMICAI_ MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Clear, colorless 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page l of 2 5WU 242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: I 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where l is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foarn in the stormwater discharge? Yes i\io S. Is there an oil sheen in the stormwater discharge? Yes D 9. Is there evidence of erosion or deposition at the outfalI? Yes Q I(). Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 Attached is the Rainfall record for the Burlington Airport for the Storm Water Monitoring Sample collected on June 1, 2015, collected from 5:30—5:45pm. The rain gauge at the Apollo Chemical Burlington Facility measured the even to be 0.56 inches at the time of collection. The pH of each sample was measured using a calibrated electrode using buffer 4, buffer 7, and buffer 10. The samples were equilibrated to a temperature of 22.1°C prior to sampling. SDO-1: pH 6.4 SDO-2: pH 6.8 SDO-3: pH 6.7 SDO-4: pH 6.0 Shown Rudison Chemical Regulatory Specialist Mount Vernon Chemicals, LLC / Apollo Chemical 336.506.0532 srudison@apollochemical.com Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 .ti Contact: Shawn Rudison Report Date: 6/1.0/2015 Client: Apollo Chemical 2001 Willow Spings Ln Burlington, NC 27216 Date Sample Rcvd: 6/2/2015 Meritech Work Order It 06021593 Parameters Result Sample: SDO1 Grab 6/1/15 Analysis Date Reporting limit 5:30 Method COD 62 rng/L 6/4/15 15 mg/L EPA 410.4 Total Suspended Solids 3 rng/€, 6/4/15 2.5 mg/l, SM 2540 D Oil & Grease (ITEM) <5 rng/L 6/8/15 5 mg/L EPA 1664A Meritech Work Order # 06021594. Sample: SD02 Grab 6/1/15 5:35 Parameters Result Analysis Date Reporting Limit Method COD 94 nag/l, 6/4/15 15 mg/L EPA 410.4 Total Suspended Solids 28 mg/I, 6/4/15 2.5 mg/I., SM 2540 D Oil & Grease (HEM) <5 rng/L 6/8/15 5 mg/L EPA 1664A Meritech Work Order # 06021595 Sample: SD03 Grab 6/1/15 5:40 Parameters Res rl Analysis Date Reporting Win it Method COD 69 mg/I, 6/4/15 15 mg/L EPA 410.4 Total Suspended Solids 319 rng/1. 6/4/15 2.5 mg/L SM 2540 D Oil & Grease (DIEM) <5 mg/1, 6/8/15 5 mg/L EPA 1664A Meritech Work Order # 06021596 Sample: SD04 Grab 6/1/15 5:45 Parameters Result Analysis Date Reporting Limit Method. COD 87 mg/I, 6/4/15 15 mg/L EPA 410.4 Total Suspended Solids 12 mg/L 6/4/15 2.5 mg/L SM 2540 1) Oil & Grease (ITEM) <5 rng/I, 6/8/15 5 mg/L 1,11A 1664A I hereby certify that I have reviewed and approve this data, c Kl� Lahoratory Representative 642 Tainco Road, Reidsville, North Carolina 27320 tel. (336)342-4748 f ax. (33 6)342-1522 Chain of Custody Rre+■ccordCOC Client: Address. Attention: Apollo Chemical 2001 Willow Springs Ln Burlington, NC 27216 Shawn Rudison NPDES #: Phone: 336-506-0532 Fax: ^ Email: sr;3disonr(c7apoliechemical_corn Project: PO#: M`-'RI .!k ECH INC. Environmental Laboratories A. IDivision of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtcla ba hellsouth. net Web Site: www.ineritech-labs.com Turn Around Time* Std (10 days) 3-5 Day I 24-48 Hr Sample LOCationllD # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? #or Conts. Tests Required on Ice? i pH OK? C12 OK? Date Time Date T me cool 611115 5:30pm 3 Oil+Grease, COD, TSS C Yes S SD02 611115 5:35pm 3 Oil+Grease, G'OD, TSS Cj Yes SDO3 611115 5:40pm 3 Oil+Grease, Coo, TSS q Yes SD04 611115 5:45pm 3 J Oil+Grease, COD TSSi Yes T Method of Shipment: Comments: ❑ UPS ❑ Fed Ex ❑ Hand Delivery ❑Other Will these results be used for regulatory purposes? Yes � No * RUSH work must be approved prior to submitting samples. Relr dished by: Date: Timo: , i� .__ tiD Received by: Date: Time: Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Received at i ! e` j TiR195 National Weather Service: Observed Weather for past 3 Days: Burlington, Burlington Al... Page 1 of 3 1: weather.gov . . rfAT//�, , A Burlington, 9 Burlington Alamance Regional 9 g Airport Enter Your "City, ST" or zip code rGoj metric en espanol Temperature (OF) Pressure Precipitation (in.) aTime Wind Vis, Weather Sky 6 hour Relative Wind Chill Heat Index t (edt) (mph) (mi.) Cond. Air dwpt Humidity (F) (°F) altimeter sea level 1 hr 3 hr 6 e Max. Min. (in) (mb) hr 01 17:54 W 6 0.25 Thunderstorm VV013 68 66 93% NA NA 30.05 1017.0 1.67 Heavy Rain Fog 01 16:54 SW 3 10.00 Thunderstorm FEW080 87 67 51% NA 90 29.97 1014.1 0.02 in Vicinity 01 15:54 W 6 6.00 Light Rain FEW080 79 69 72% NA 82 29.98 1014.5 0.02 SCT110 01 14:54 S 8 10.00 Thunderstorm FEW049 90 65 44% NA 92 30.00 1015.2 in Vicinity 01 13:54 S 8 10.00 Mostly BKNO50 86 64 90 73 48% NA 87 30.03 1016.3 Cloudy BKN065 01 12:54 Vrbl 10.00 Fair CLR 88 64 45% NA 89 30.06 1017.0 7 01 11:54 S 8 10,00 Fair CLR 86 66 51% NA 88 30.07 1017.3 01 10:54 SW 9 10.00 Fair CLR 84 66 55% NA 86 30.07 1017.5 01 09:54 Vrbl 10.00 Fair CLR 79 68 69% NA 81 30.08 1017.9 6 01 08:54 S 8 10.00 Partly Cloudy FEW080 76 67 74% NA 77 30.09 1018.2 SCT110 01 07:54 55 10.00 Partly Cloudy SCT100 73 67 74 68 81% NA NA 30.08 1017.9 01 06:54 Calm 9.00 Fair CLR 69 66 90% NA NA 30.07 1017.6 01 05:54 S 5 10.00 Fair CLR 69 65 87% NA NA 30.06 1017.3 01 04:54 SW 3 10,00 Fair CLR 70 66 87% NA NA 30.06 1017.1 01 03:54 S 3 10.00 Mostly BKN120 71 65 81% NA NA 30.06 1017.1 Cloudy 01 02:54 S 3 10.00 A Few Clouds FEW095 72 65 79% NA NA 30.07 1017.4 01 01:54 S 3 10.00 Partly Cloudy SCT075 74 64 82 71 71% NA NA 30.07 1017.4 SCT090 01 00:54 Calm 10.00 Partly Cloudy SCT070 72 64 76% NA NA 30.07 1017.4 31 23:54 Calm 10.00 Overcast FEW060 73 66 79% NA NA 30.06 1017.2 FEW075 OVC110 31 22:54 Calm 10.00 Mostly BKN060 74 64 71% NA NA 30.06 1017.2 Cloudy 31 21:54 Calm 10.00 Partly Cloudy FEW070 77 64 64% NA 79 30.04 1016.7 SCT095 31 20.54 Calm 10.00 A Few Clouds FEW075 79 63 58% NA 81 30.02 1015.9 31 18:54 S 5 10.00 Fair CLR 84 62 48% NA 85 30.01 1015.5 http://w1.weather.gov/data/obhistory/KBUY.html 611I2015 National Weather Service : Observed Weather for past 3 Days: Burlington, Burlington Al... Page 2 of 3 31 17:54 S 7 10.00 A Few Clouds FEW090 87 62 43% NA 87 30.01 1015.4 G16 31 1&54 S 6 10.00 Mostly BKN100 85 62 46% NA 86 30.02 1015.9 G 16 Cloudy 31 15:54 S 8 10,00 Partly Cloudy F'EW055 86 62 45% NA 87 30.04 1016.5 SCT100 31 14:54 S 12 10.00 A Few Clouds FEW048 87 64 46% NA 88 30.05 1016.9 31 13:54 S 10 10.00 A Few Clouds FEW047 87 64 87 71 46% NA 88 30.08 1017.7 G 18 31 12:54 S 7 10.00 Fair CLR 86 63 46% NA 87 30.10 1018.4 31 11:54 S 8 10.00 Fair CLR 84 64 51% NA 85 30.12 1019.1 31 10:54 SW 10.00 A Few Clouds FEW110 81 66 61% NA 83 30.13 1019.5 10 31 09:54 SW 10.00 A Few Clouds FEW070 77 65 66% NA 79 30.14 1019.8 10 31 08:54 S 6 10.00 Mostly SCT048 71 64 79% NA NA 30.14 1020.0 Cloudy BKNO65 BKN100 31 07:54 S 5 10.00 Overcast BKN046 71 65 72 68 81 % NA NA 30.13 1019.7 OVC060 31 0&54 SW 5 10.00 Overcast OVC043 69 64 84% NA NA 30.13 1019.5 31 05:54 SW3 10.00 Overcast OVC046 69 64 84% NA NA 30,12 1019.2 31 04:54 Calm 10.00 Overcast OVC095 68 64 87% NA NA 30.11 1018.9 31 03 54 S 3 10.00 Mostly BKN090 69 63 81% NA NA 30.11 1018.8 Cloudy 31 02:54 85 10.00 Fair CI_R 70 64 82% NA NA 30.11 1018.9 31 01:54 S 3 10.00 Fair CLR 72 64 81 72 76% NA NA 30.12 1019.1 31 ❑0:54 S 6 10.00 Fair CLR 74 64 71% NA NA 30.12 1019.0 30 23:54 S 7 10.00 Fair CLR 75 65 71% NA NA 30.11 1019.0 30 22:54 SE 5 10.00 Overcast BKN060 74 65 74% NA NA 30.10 1018.6 OVC090 30 21:54 Calm 10.00 Mostly SCT070 74 65 74% NA NA 30,09 1018.1 Cloudy BKNO85 30 20:54 Calm 10.00 Partly Cloudy SCT080 77 65 66% NA 79 30.08 1018.0 30 19:54 SE 3 10.00 Fair CLR 81 64 87 81 57% NA 83 30.09 1018.3 30 18:54 S 5 10.00 Mostly 13KNO85 83 64 53% NA 84 30.09 1018.4 Cloudy 30 17:54 S 7 10.00 Fair CLR 85 63 48% NA 86 30.10 1018.8 30 16:54 S 8 10.00 A Few Clouds FEW049 86 63 46% NA B7 30.11 1019.1 30 15:54 Vrbl 10.00 Fair CLR 86 63 46% NA 87 30.14 1019.8 3 30 14:54 SE 9 10.00 Fair CLR 86 64 48% NA 87 30.16 1020.5 30 13:54 SS 10.00 Partly Cloudy FEW041 83 64 85 68 53% NA 84 30.19 1021.5 SCT085 30 12:54 Vrbl 10.00 Partly Cloudy SCT075 83 64 53% NA 84 30.21 1022.2 6 30 11:54 Vrbl 10,00 Mostly SCT031 80 66 62% NA 82 30.22 1022.8 7 Cloudy SCT039 BKN048 30 10:54 S 6 10.00 A Few Clouds FEW024 78 65 64% NA 80 30,23 1023.0 http://wl .weather.gov/data/obhistoly/KB UY.litnil 6/1/2015 National Weather Service: Observed Weather for past 3 Days : Burlington, Burlington Al... Page 3 of 3 30 09:54 Vrbl 10.00 Fair CLR 77 66 69% NA 79 30.23 1023.1 3 30 08:54 S 6 10.00 A Few Clouds FEW065 73 66 79% NA NA 30.24 1023.3 30 07:54 Calm 10.00 Fair CLR 68 64 68 61 87% NA NA 30.24 1023.2 30 06:54 Calm 10.00 Fair CLR 61 59 93% NA NA 30.23 1022.9 30 05:54 Calm 10.00 Fair CLR 61 59 93% NA NA 30.20 1022.2 30 04:54 Calm 9.00 Fair CLR 62 60 93% NA NA 30.19 1021.8 30 03:54 Calm 10.00 Fair CLR 63 60 90% NA NA 30.19 1021.6 30 02:54 Calm 10.00 Fair CLR 63 60 90% NA NA 30.19 1021.6 30 01:54 Calm 10.00 Fair CLR 66 61 81 63 84% NA NA 30.19 1021.6 30 00:54 SE 5 10.00 Fair CLR 68 60 76% NA NA 30.19 1021.6 29 23,54 Calm 10.00 Fair CLR 66 60 81% NA NA 30.19 1021.8 29 22:54 Calm 10.00 Fair CLR 67 61 81% NA NA 30.20 1022.0 29 21:54 Calm 10.00 Fair CLR 72 61 68% NA NA 30.19 1021.9 29 20:54 SE 3 10.00 Fair CLR 77 59 54% NA 79 30.18 1021.5 29 19:54 SE 5 10.00 Fair CLR 81 63 88 81 54% NA 82 30.17 1020.9 29 18:54 Vrbl 10.00 Fair CLR 84 64 51% NA 85 30,16 1020.6 7 D Max. Min. altimeter sea 6 a Time Wind Vis. Sky Air Dwpt 6 hour Relative Wind Heat ( in.) level (mb) i hr 3 hr hr t (edt) (mph) (mi.) Weather Cond. Humidity Chill .F Index e Temperature (°F) ( (`F) Pressure Precipitation (in.) National Weather Service Back to revious. a e p p- 9- Last Modified: Febuary, 7 2012 Southern Region Headquarters -' Privacy Policy Fort Worth, Texas Disclaimer http://wl.wcather.gov/data/obhistory/KBUY.htmi 6/1/2015 f � w C H E M I C A L S, L L C 2001 Willow Springs Lane, Burlington, North Carolina 27215, PHONE 336-506-0524 FAX 336-228-6963 November 26, 2014 RECEIVED Central Files DEC 4 4 2014 Division of Water Quality CENTRAL FILES 1617 Mail Service Center DWR SECTION Raleigh, NC 27699-1617 Re: 2014 Semi -Annual NPDES Stormwater Report General Permit: NCG060000 COC No: NCG060040 Mount Vernon Chemicals, LLC 1 Apollo Chemical — Burlington Facility 2001 Willow Springs Lane Burlington, NC 27215 Enclosed are the original and a copy of the stormwater monitoring results for the second half of 2014 for our Willow Springs Lane facility. Our stormwater outfalls were sampled during a significant rain event (documentation is attached). On -site measurement of pH was conducted at Apollo Chemical at the time of sampling. The samples were sent to Meritech, Inc. (Lab Certification No: 165) for analysis. The samples were tested for TSS, COD, and Oil & Grease. The Meritech report is appended. Our °Stormwater discharge outfall monitoring report" which includes pH results, is also appended. If you need additional information, please contact me. Sincerely, Mount Vernon Chemicals, LLCIApollo Chemical Gary S. Dagenhart, Ph.D. Technical Director gdag enhart-.apollochemical.com Phone 336-506-0524 Copy: Plant Managers, Regulatory File, Corporate Director Environmental Affairs Apollo Chemical 2001 Willow Springs Lane, Burlington, North Carolina 27215 Tel: 336-226-1161 Fax: 336-228-6963 www.apollochemical.com Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: Shawn Rudison Report Date: 11/19/2014 Client: Apolio Chemical 2001 Willow Spings Ln Burlington, NC 27216 Date Sample Rcvd: 11/7/2014 Meritech Work Order # 11071416 Sample: SDO1 Grab 11/6/14 Parameters Result Analysi� Date Reporting Limit Method COD S7 mg/L 11/10/14 15 mg/L EPA 410.4 Total Suspended Solids 26 mg/l. 11/12/14 2.5 mg/L SM 2S40 D Oil & Grease (HEM) < 5 mg/L 11/13/14 5 mg/L EPA 1664A Meritech Work Order # 11071717 Sample: SD02 Grab 11/6/14 Parameters Result AnalysJ2 Date Reporting limit Method COD 43 mg/L 11/10/14 15 mg/L EPA 41.0.4 Total Suspended Solids 36 mg/L 11/1.2/14 2.5 mg/L SM 2540 D Oil & Grease (HEM) < 5 mg/l, 11/13/14 5 mg/L EPA 1664A Meritech Work Order# 11071418 Sample: SD04 Grab 11/6/14 Parameters Result Analysis Date Reporting Limit Method COD 27 mg/L 11/10/14 15 mg/L EPA 410.4 Total Suspended Solids 7 mg/L 11/12/14 2.5 mg/L SM 2540 D Oil & Grease (HEM) < 5 mg/L 1.1/17/14 5 mg/L EPA 1664A I hereby certify that I have reviewed and approve this data. Laboratory Representative 642 Tamco Road, Reidsville, North. Carolina 27320 tel_(336)342-4748 fax.(336)342-1522 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 11 6 2014 CERTIFICATE OF COVERAGE NO. NCG060040 SAMPLE COLLECTION YEAR July -December 2014 FACILITY NAME Mount Vernon Chemicals, LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Alamance ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Shawn Rudison DISCHARGING TO SALTWATERS? ❑YES X NO LABORATORY Meritech, Inc Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall20.18 inches or ❑ No discharge this period3 Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 S00 SDO-1 11/6/14 26 7.6 57 < 5 N/A N/A SDO-2 11/6/14 36 7.5 43 < 5 N/A N/A SDO-4 11/6/14 7 8.2 27 < 5 N/A N/A 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at �ny outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504 6.0 — 9.0 - (ifyes, complete Part B) 1 Only applies to facilities that use/process meats. z The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SWU-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. * 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK FXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy ot this DMR includin all "No Discharge" reports, within 30 days of receipt of the lab results or at end o monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Cc5Jw-.1�,�— it I 2-11 I Iff (Signature of P (Date) Additional copies of this form may be downloaded at: http:/Iportal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidtuace on filling out this form, please visit: http://h2o.enr.state.ne.us/su/Forms Documents.htm#miscforms Permit No.: NICI G/O / 610I 01 0/ 0l or Certificate of Coverage No.: NICIGI 0/ 61014 /0 /0 I Facility Name: Mouni Vernon Mills, Inc t Mount Vernon Chemicals, LLC / Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: 111612014 Time of lnspeetion: 12:00 - 12:15 PM Total Event Precipitation (inches): 0_11 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be perfortned daring a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SDO1 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 5 WU-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: lO 2 3 4 5 6. Suspended Solids: Choose the number which best describes the arnount of' suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 0 2 3 4 5 7. is there any foam in the stormwater discharge? Yes No S. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or (lie presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 s wU-242-1 12608 Stormwater Discharge Outfall (SDQ) Qualitative Monitoring Report For guidwice on filling out this form, please visit: http://h2o.enr.state.ne.us/su/Forms_Documents.htm#miseforms Permit No.: NI_G GIO / 610 / 01 0/ 01 or Certificate of Coverage No.: NICIGI 0/ 6101410/0/ Facility Name: Mount Vernon Mills, Inc / Mount Vernon Chemicals, LLC 1 Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date ol' Inspection: 11/6/2014 Time of Inspection: 12:00 -12:15 PM Total Event Precipitation (inches):_111 Was this a Representative Storm Event? (See information below)121 Yes ❑ No Please check your permit to verify if Qualitative Monitoring must he petfornzed (luring a representative .storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SDO2 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNK CREEL( Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page l of 2 S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 0 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the arnount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 0 2 3 4 5 7. 1s there any foam in the stormwater discharge? Yes G o 8. Is there an oil sheen in the stormwater discharge? Yes Q 9. Is there evidence of erosion or deposition at the outfall? Yes 0Nq 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://h2o.enr.state.nc.us/su/Forms_ Documents.htm#miscforrrrs Permit No.: NICI Gf0 f 6/ 0/ Of 0f 0f or Certificate of Coverage No.: NICIGI Of 6f 0 f4 f0/0/ Facility Name: Mount Vernon Mills, Inc 1 Mount Vernon Chemicals, LLC 1 Apollo Chemical County: Alamance Phone No. (336) 506-0524 1nwector: Shawn Rudison Date of Inspection: 1 1/612014 Time of Inspection: 12:00- 12:15 PM Total Event Precipitation (inches): 0_17 Was this a Representative Storm Event? (See information below) W]Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during cr representative storm event (requirements vary). A '`Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event rneasuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of' no precipitation. By this signature, 1 certify that this report is accurate and complete to the best of my knowledge: A (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SDO3 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: NONE 1 NO FLOW 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weals chlorine odor, etc.): NONE I NO FLOW Page l oi'2 S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of' suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? 8. Is there an oil sheen in the stormwater discharge? 9. Is there evidence of erosion or deposition at the outfall? 10. Other Obvious Indicators of Stormwater Pollution: List and describe Yes No jVp 1�0 iti.J Yes No Yes No Iv0 �o aJ Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 Swt1-242-1126as Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For gctidcurce on filling out this form, plectse visit: http://h2o.enr.state.nc.us/su/Forms Documents. htm#miscforms Permit No.: NICI GIO / 6101 0/ 0/ 0/ or Certificate of Coverage No.: NICIGI 0/6/0/4/0 /0 / Facility Name: Mount Vernon Mills, Inc! Mount Vernon Chemicals, LLC t Apollo Chemical County: Alamance Phone No. (336) 506-0524 InSUector: Shawn Rudison Date of Inspection: 11/6/2014 Time of Inspection: 12:00 - 12:15 PM Total Event Precipitation (inches): 0_11 Was this a Representative Storm Event? (See information below) FV1Yes ❑ No Please check your permit to verify if Qualitative Monitoring must he petformed daring a representative storm event (requirements var),). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: oUtfall No. SD04 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page I ol'2 S W U-242-1 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: Q 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: [D 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: lO 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes e 8. Is there an oil sheen in the stormwater discharge? Yes UJ 9. Is there evidence of erosion or deposition at the outfall? Yes Io I(}. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242- l 12608 From: Shawn Rudison To: Shawn Rudison Subject: Stormwater Sample collection far 6-November-2014 Date: Friday, November 07, 2014 8:07:57 AM Attached is the Rainfall record for the Burlington Airport for the Storm Water Monitoring Sample collected on 6-November-2014, collected from 12:00 — 12:15pm. The rain gauge at the Apollo Chemical Burlington Facility measured the even to be 0.13 inches at the time of collection. I have measured the pH of each sample using a calibrated electrode using buffer 4 (Reagents Lot:1231NCA EXP 1/2015), buffer 7 (Reagents Lot: 0124PCA EXP 2/2015), and buffer 10 (Reagents Lot: 0107PCA EXP 1/2015). The samples were equilibrated to a temperature of 22.1°C prior to sampling. SDO-1: pH 7.6 SDO-2: pH 7.5 SDO-4: pH 8.2 Shown Rudison Chemical Regulatory Specialist Mount Vernon Chemicals, LLC / Apollo Chemical 336.506.0532 srud ison@a pol lochem ical.com National Weather Service : Observed Weather for past 3 Days : Greensbor... Page 1 of 4 weather.gov rrte Greensboro, Piedmont Triad International Airport .� Enter Your "City, ST" or zip code Go metric en espanol p Temperature (OF) Pressure Precipitation (in.) a Time Wind Vis. Weather Sky Cond. Relative Wind Heat f� e (est) (mph) (mi.) 6 hour Humidity Ff}I F) altimeter sea 3 Air Dwpt (in} level 1 hr 6 hr hr Max. Min. (mb) 07 06:54 NW 10.00 Fair CLR 44 32 47 40 63% 37 NA 29.94 1013.9 14 07 05:54 W 9 10.00 Fair CLR 44 32 63°% 39 NA 29.92 1012.8 07 04:54 NW 10.00 Fair CLR 47 32 56% 42 NA 29.90 1012.3 10G 24 07 03:54 NW 9 10.00 Fair CLR 42 33 71% 37 NA 29.89 1011.8 07 02:54 Calm 10.00 Fair CLR 45 33 63% NA NA 29.88 1011.5 07 01:54 W 7 10.00 Fair CLR 43 33 68% 39 NA 29.87 1011.2 07 00:54 NW 9 10.00 Fair CLR 44 33 56 44 65% 39 NA 29.87 1011.4 06 23:54 NW 10.00 Fair CLR 49 33 55% 43 NA 29.88 1011.4 16G 25 06 22:54 NW 10.00 Fair and CLR 50 32 50% 43 NA 29.88 1011.3 21 G Breezy 24 06 21:54 NW 10.00 A Few FEW090 52 32 47% NA NA 29.86 1010.8 20 G Clouds 36 06 20:54 NW 10.00 Partly SCT090 54 36 51 % NA NA 29.83 1009.7 18 G Cloudy 32 06 19:54 NW 10.00 Mostly BKN070 56 40 55% NA NA 29.80 1008.5 22 G Cloudy BKN110 29 and Breezy 06 18:54 NW 10.00 Light SCT030 55 45 65 55 69% NA NA 29.79 1008.4 0.05 0.10 16 Rain BKN050 OVC070 06 17:54 W 17 7.00 Light SCT020 62 55 78% NA NA 29.76 1007.0 0.05 G 24 Rain BKN045 BKN065 06 16:54 SW 8 10.00 Mostly FEW020TCU 63 57 81% NA NA 29.74 1006.5 Cloudy SCT035 B KN 085 06 15:54 SW 10.00 Partly FEW017 65 58 78% NA NA 29.74 1006.3 13 G Cloudy SCT035 22 06 14:54 SW 10.00 Mostly BKN012 63 59 12 Cloudy 06 13:54 SW 4.00 Fog/Mist BKNO06 61 59 12 OVC011 87% NA NA 29.77 1007.5 93% NA NA 29.81 1008.8 httn•//wi _wenther.gov/data/obhistoi-v/KGSO.html 11/7/2014 National Weather Service : Observed Weather for Fast 3 Days : Greensbor... .Page 2 of 4 06 12:54 W 17 3.00 Light BKNO06 60 58 64 60 93% NA NA 29.85 1010,2 0.C2 0.11 G 23 Rain OVC011 Fog/Mist 06 11:54 SW 3.00 Rain BKNO09 60 59 96% NA NA 29.88 1011.3 0.07 10 Fog/Mist OVC014 06 10:54 SW 5.00 Light BKN022 61 58 90% NA NA 29.92 1012.5 0.02 13 Rain OV0048 Fog/Mist 06 09:54 SW 10.00 Overcast BKN024 63 56 78% NA NA 29.95 1013,E 14 G OVC050 20 06 08:54 SW 10.00 Overcast BKNO34 62 56 80% NA NA 29.97 1014.5 10 OVC050 06 07:54 SW 7 10.00 Overcast BKN032 61 56 84% NA NA 29.99 1015.0 BKN040 OVC050 06 06:54 SW 10.00 Overcast SCr037 60 55 62 59 84% NA NA 29.99 1015.2 12 G BKN049 18 OVC070 06 05:54 SW 10.00 Light BKN075 60 55 84% NA NA 30.00 1015.2 14 G Rain OVC110 20 06 04:54 SW 10.00 Light BKNO90 60 54 80% NA NA 30.02 1015.9 10 Rain OVC120 06 03:54 SW 10.00 Overcast FEW075 61 54 78% NA NA 30.02 1016.0 13 O VC 095 06 02:54 SW 10.00 Overcast BKN100 60 53 78% NA NA 30,05 1016.7 13 OVC120 06 01:54 SW 10.00 Overcast BKN110 59 52 78% NA NA 30.08 1017.9 10 OVC250 06 00:54 SW 9 10,00 Overcast SCT035 59 51 60 54 75% NA NA 30.11 1018.9 BKN150 OVC250 05 23:54 SW 7 10.00 Overcast SCT120 57 51 81% NA NA 30.11 1019.1 OVC250 05 22:54 SW 8 i0.00 Mostly BKN250 57 50 78% NA NA 30.15 1020A Cloudy 05 21:54 SW 6 10.00 Mostly BKN250 55 48 77% NA NA 30.17 1021.3 Cloudy 05 20:54 SW 3 10.00 Mostly BKN250 55 48 77% NA NA 30.18 1021.6 Cloudy 05 19:54 S 3 10.00 Mostly FEW180 58 48 70% NA NA 30.18 1021.7 Cloudy BKN250 05 18:54 SW 3 10.00 Mostly SCT180 60 48 67 59 65% NA NA 30.17 1021.5 Cloudy BKN250 05 17:54 SW 7 10.00 Mostly SCT180 61 47 60% NA NA 30.18 1021.7 Cloudy BKN250 05 16:54 SW 5 10.00 Mostly SCT180 63 42 47% NA NA 30.18 1021.5 Cloudy BKN250 05 15:54 SW 5 10.00 Overcast FEW200 65 41 42% NA NA 30.18 1021.7 OVC250 05 14:54 SW 7 10.00 Overcast FEW200 67 40 37% NA NA 30.18 1021.7 OVC250 05 13:54 S 8 10.00 Overcast 67 42 41 % NA NA 30.20 1022.2 http://wI.weatlier.gov/data/obhistory/KGSO.litnil ] 1/7/20l4 National Weather Service: Observed Weather for past 3 Days : Greensbor... Page 3 of 4 SCT200 OVC250 05 12:54 S 5 10.00 Overcast SCT200 65 41 66 48 42% NA NA 30.23 1023.2 OVC250 05 11:54 SW 3 10.00 Overcast FEW180 64 41 43% NA NA 30.25 1024.0 OVC250 05 10:54 W 8 10.00 Overcast FEW180 62 40 44% NA NA 30.28 1025.1 OVC250 05 09:54 SW 9 10.00 Overcast OVC250 59 39 48% NA NA 30,29 1025.2 05 08:54 SW 8 10.00 Overcast BKN200 56 39 53% NA NA 30.27 1024.8 OVC250 05 07:54 SW 7 10.00 Overcast BKN200 51 38 61% NA NA 30.27 1024.9 OVC250 05 06:54 SW 7 10.00 Overcast OVC200 48 38 55 48 68% 45 NA 30.24 1024.1 05 05:54 W 5 10.00 Overcast OVC200 51 36 56% NA NA 30.24 1023.6 05 04:54 SW 6 10.00 Overcast OVC250 50 37 61% 48 NA 30.23 1023.4 05 03:54 SW 7 10,00 Overcast OVC250 51 36 56% NA NA 30.22 1023.1 05 02:54 SW 7 10.00 Overcast OV0220 52 37 57% NA NA 3022 1022.8 05 01:54 SW9 10.00 Overcast OV0220 54 36 51% NA NA 30.21 1022.7 05 C0:54 SW 9 10.00 Overcast OVC220 55 36 57 53 49% NA NA 30,22 1022.9 04 23:54 SW 9 10.00 Overcast OVC200 56 36 47% NA NA 30.22 1023.0 04 22:54 SW 6 10.00 Overcast OVC190 53 37 55% NA NA 30.23 1023.5 04 21:54 S 7 10.00 Overcast OVC200 54 37 53% NA NA 30.24 1023.7 04 20:54 SW 8 10,00 Mostly BKN200 56 36 47% NA NA 30.23 1023.5 Cloudy 04 19:54 SW 8 10.00 Overcast OVC200 56 35 46% NA NA 30.24 1023.9 04 18:54 SW 6 10.00 Overcast CVC200 56 33 67 56 42% NA NA 30.24 1023.8 04 17:54 SW 6 10.00 Overcast OV0200 58 31 36% NA NA 30.22 1023.2 04 16:54 SW 8 10.00 Overcast OVC200 62 30 30% NA NA 30.21 1022.9 04 15:54 SW 8 10.00 Overcast OVC240 63 28 27% NA NA 30.22 1023.2 04 14:54 SW 10,00 Overcast FEW180 65 26 23% NA NA 30.22 1023.1 10 OVC250 04 13:54 SW 10.00 Overcast FEW180 66 30 26% NA NA 30.24 1023.6 12 OVC250 04 12:54 SW 10,00 Overcast FEW180 65 32 65 42 29% NA NA 30.26 1024.3 12 OVC250 04 11:54 SW 10.00 Overcast FEW180 63 33 33% NA NA 30.29 1025.6 12 OVC250 04 10:54 SW 9 10.00 Overcast FEW140 60 35 39% NA NA 30.31 1026.2 OVC250 04 09:54 SW 7 10.00 Mostly BKN250 56 35 46% NA NA 30.32 1026.5 Cloudy 04 08:54 W 10 10.00 Mostly FEW140 52 34 50% NA NA 30.31 1026.3 Cloudy SKN250 04 07:54 SW 6 10.00 Overcast FEW130 47 33 59% 44 NA 30.32 1026,E OVC250 D Time Wind Vis. Weather Sky Cond. Max. Min. Relative Wind Heat altimeter sea 3 a (est) (mph) (mi.) Air Dwpt Humidity Chill Index (in ) level 1 hr hr 6 hr t 6 hour (7) CF) (mb) e Temperature (OF) Pressure lit.tn-Hwl.weatlher.gov/data/obhistorv/`KGSO.html I l/7/20I 4 National Weather Service : Observed Weather for past 3 Days : G•eensbor... Page 4 of 4 Precipitation (in.) National Weather Service Back to previous page Last ModiCed: Febuary, 7 2012 Southern Region Headquarters Privacy Policy Fort Worth, Texas Disclaimer http://wl .weather.gov/data/obhistoiy/KGS0.htm1 11/7/2014 ti MOUNT-VERNON CHEMI.GALS LLC 2001 Willow Springs Lane, Burlington, North Carolina 27215, PHONE 336-506-0524 FAX 336-228-6963 May 28, 2014 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 201+Semi-Annual NPDES Stormwater Report RECEIVED MAY 3 0 2014 CENTRAL FILES DWO/BOG General Permit: NCG060000 COC No: NCG060040 Mount Vernon Chemicals, LLC 1 Apollo Chemical — Burlington Facility 2001 Willow Springs Lane Burlington, NC 27215 Enclosed are the original and a copy of the stormwater monitoring results for the first half of 2014 for our Willow Springs Lane facility. Our four stormwater outfalls were sampled during a significant rain event (documentation is attached). On -site measurement of pH was conducted at Apollo Chemical at the time of sampling. The samples were sent to Meritech, Inc. (Lab Certification No: 165) for analysis. The samples were tested for TSS, COD, and Oil & Grease. The Meritech report is appended. Our "Stormwater discharge outfall monitoring report" which includes pH results, is also appended. If you need additional information, please contact me. Sincerely, Mount Vernon Chemicals, LLCIApollo Chemical Os Gary S. Dagenhart, Ph.D. Technical Director gdagenhartCcDapollochemical.com Phone 336-506-0524 Copy: Plant Managers, Regulatory File, Corporate Director Environmental Affairs Apollo Chemical 2001 Willow Springs Lane, Burlington, North Carolina 27215 Tel: 336-226-1161 Fax: 336-228-6963 www.apollochemical.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 5/15/2014 CERTIFICATE OF COVERAGE NO. NCG060040 SAMPLE COLLECTION YEAR January -June 2014 FACILITY NAME Mount „Vernon Chemicals, LLC dba Apollo Chemical FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Alamance ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Shawn Rudison DISCHARGING TO SALTWATERS? ❑YES X NO LABORATORY Meritech, Inc Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall 20.18 inches or ❑ No discharge this period3 Outfall No. Sample Collected, mo/dd/yn TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark - 100 or 50 Within 6.0 — 9.0 120 30 1000 500 SDO-1 5/15/14 8 8.3 28 7 N/A N/A SDO-2 5/15/14 99 8.7 107 < 5 N/A N/A SDO-3 5/15/14 25 7.9 73 < 5 N/A N/A SDO-4 5/15/14 3 8.3 41 < 5 N/A N/A 1 Only applies to facilities that use/process meats. 2 The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes X no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50 6.0 — 9.0 - (ifyes, complete Part B) 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SWU-249 Last Revised: October 18, 2012 Pagel of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO D4 IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports] to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Per (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 Shawn Rudison From: Shawn Rudison Sent: Thursday, May 15, 2014 3:37 PM To: Shawn Rudison Subject: FW: Storm Water Sample Collection for 15-May-2015 Attached is the Rainfall record for the Burlington Airport for the Storm Water Monitoring Sample collected on 15-May- 2014, collected from 11:30—11:45am. The rain gauge at the Apollo Chemical Burlington Facility measured the even to be 0.44 inches at the time of collection. I have measured the pH of each sample using a calibrated electrode using buffer 4 (Reagents Lot:1231NCA EXP 1/2014), buffer 7 (Reagents Lot: 0124PCA EXP 2/2015), and buffer 10 (Reagents Lot: 0107PCA EXP 1/2015). The samples were equilibrated to a temperature of 21.7°C prior to sampling. SDO-1: pH 8.3 SDO-2: pH 8.7 SDO-3: pH 7.8 SDO-4: pH 8.3 Shawn Rudison Chemical Regulatory Specialist Mount Vernon Chemicals, LLC / Apollo Chemical 336.506.0532 srudison@apollachemical.com 1 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://h2o.enr.state.nc,us/su/Forms Documents.htm#miscforms Permit No.: N/C/G/O 16/0/ 0/ 0/ 0/ or Certificate of Coverage No.: N/CIG/ 0/6/0/4/0 /O Facility Name: Mount Vernon Mills, Inc / Mount Vernon Chemicals, LLC 1 Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: 05/15/2014 Time of Inspection: 11:30 -11:45 AM Total Event Precipitation (inches): 0.44 Was this a Representative Storm Event? (See information below) F7Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). -- _ —.. --- - ------------ _- -.-.. - .... -- - ...._-. __ _----...---..-------....-.._ _ _..--... -... --...-.._-.._-.._. _. _ ..._. A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours Q days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SDO1 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR. COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page I of 2 S W U-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: G) 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 issnno solids and 5 is extremely muddy: ( 1) 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes (0 8. Is there an oil sheen in the stormwater discharge? Yes ON 9. Is there evidence of erosion or deposition at the outfall? Yes No to. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-112608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://h2o.enr.state.nc.us/su/Forms Documents.htrn#miscforms Permit No.: NIC/ G/0 / 6/0/ 0/ 0l 0l or Certificate of Coverage No.: NIC/G/ 0/6/0/4/0 /0 I Facilitv Name: Mount Vemon Mills, Inc! Mount Vemon Chemicals, LLC !Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector: Shawn Rudison Date of Inspection: 0511512014 Time of Inspection: 11:30 -11:45 AM Total Event Precipitation (inches): 0.44 Was this a Representative Storm Event? (See information below) � Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours Q days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: Do (Signature of PermitteeWr Designee) 1. Outfall Description: Outfall No. SDd2 Structure (pipe, ditch, etc.) RIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, LIGHT 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 S W U-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2O 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: (D 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 2D 3 4 5 7. Is there any foam in the stormwater discharge? Yes oNo S. Is there an oil sheen in the stormwater discharge? Yes 100 9. Is there evidence of erosion or deposition at the outfall? Yes 10 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242- I t 2608 �. s<ATE Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: hit p_//h2o.enr. state. nc.uslsu/Forms_ Documents.htm#miscforms Permit No.: N/C/ G/O / 6/ 0/ 0/ 0/ 0/ or Certificate of Coverage No.: NIGGI 0/ 6/ 0/4/0/0/ Facility Name: Mount Vemon Mills, Inc 1 Mount Vemon Chemicals, LLC t Apollo Chemical County: Alamance Phone No. (336) 506-0524 Inspector. Shawn Rudison Date of Inspection: 05/15/2014 Time of Inspection: 11:30 - 11:45 AM Total Event Precipitation (inches): 0.44 Was this a Representative Storm Event? (See information below) W1Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: la L (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. SD03 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, LIGHT 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 S W U-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: D 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: (D 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes e 8. Is there an oil sheen in the stormwater discharge? Yes CN)o 9. Is there evidence of erosion or deposition at the out€all? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2of2 5 WU-242- 112608 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit; htt ://h2o.enr.state,ne,us/sti[Forms Documents. htm#miseforms Permit No.: NICI G/O / 6/ 0/ 0/ 0l 0l or Certificate of Coverage No.. N/C/G/ 0l 6/ 0/4/0/0/ Facility Name: Mount Vernon Mills, Inc! Mount Vernon Chemicals, LLC t Apollo Chemical County: Alamance Phone No. (336) 506-0524 Insnector: Shawn Rudison Date of Inspection: 05/15/2014 Time of Inspection: 11:30 - 11:45 AM Total Event Precipitation (inches): 0.44 Was this a Representative Storm Event? (See information below) 7Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. so04 Structure (pipe, ditch, etc.) PIPE Receiving Stream: GUNN CREEK Describe the industrial activities that occur within the outfall drainage area: CHEMICAL MANUFACTURING 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLEAR, COLORLESS 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NONE Page 1 of 2 5WU-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: CID 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: ( 1 j 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I�iss no solids and 5 is extremely muddy: rc lj 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes oNo S. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S WU-242-1 12608 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 wJ Contact: Shawn Rudison Report Date: 5/22/2014 Client: Apollo Chemical 2001 Willow Spings Ln Burlington, NC 27216 Date Sample JIM: 5/16/2014 Meritech Work Order # 05161416 Sample: SDO1 Grab 5/15/14 Parameters Result Analysis Date Reporting Limit Method_ COD 28 mg/L 5/21/14 15 mg/L EPA 410.4 Total Suspended Solids 8 mg/L 5/19/14 2.5 mg/L SM 2540 D Oil & Grease (HEM) 7 mg/L 5/20/14 5 mg/L EPA 1664A Meritech .Work Order # 05161417 Sample: SD02 Grab 5/15/14 Parameters Result Analysis Date Reporting Limit Method COD 107 mg/L 5/21/14 15 mg/L EPA 410.4 Total Suspended Solids 99 mg/L 5/20/14 2.5 mg/L SM 2540 D Oil & Grease (HEM) < 5 mg/L 5/20/14 5 mg/L EPA 1664A Meritech Work Order # 05161418 Sample: SD03 Grab 5/15/14 Parameters Result Analysis Date R rtin Limit Method COD 73 mg/L 5/21/14 15 mg/L EPA 410.4 Total Suspended Solids 25 mg/L 5/19/14 2.5 mg/L SM 2540 D Oil & Grease (HEM) < 5 mg/L 5/20/14 5 mg/L EPA 1664A Meritech Work Order # 05161419 Sample: SD04 Grab 5/15/14 Parameters Result Ana1�i Date Reporting Limit Method COD 41 mg/L 5/21/14 15 mg/L EPA 410.4 Total Suspended Solids 3 mg/L 5/19/14 2.5 mg/L SM 2540 D Oil & Grease (HEM) < 5 mg/L 5/20/14 5 mg/L EPA 1664A I hereby certify that I have reviewed and approve this data. Lg Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Chain of Custody Record COC Client: Apollo Chemical Address: 2001 Willow Springs Ln Burlington, NC 27216 Attention: Shawn Rudison NPDES#: Phone: 336-506.0532 Fax: Email: srudisonr@apollochomical.com Project: PO#: INC.MERITECH I - ` Environmental Laboratories A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab@bellsouth.net Web Site: www.meritech-labs.com Turn Around Time' Std (10 days) 3 - 5 Day o 24 - 48 Hr Sample Location/lD # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? riot Conis. Tests Required , n }`� pH 7 C 20 Date Time Date Time SDO1 5/15/14 11:30am 3 OII+Grease, COD, TSS r Yes C _ SD023 5115114 11:35am 3 Oil+Grease, COD"TS n - Yes l SD03 5/15/14 11:40am 3 Oil+Grease, COD, TSS 1 Yes SD04 5/15114 11:45am 3 Oil+Grease, COD, TSS r Yes � �-� Method of Shipment: Comments: A , r lt�a ❑ UPS ❑ Fed Ex ❑ Hand Delivery ❑Other Will these results be used for regulatory purposes? Yes I X No RUSH work must be approved prior to submitting samples. Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Received by: Date: Time: Re nquishe Dat Ttma: Received tab by: Date: Time: National Weather Service : Observed Weather for past 3 Days: Burlington Alamance Regional Airport weather.gov �f 4Ta� 0 P � { �� J. D TemperatureEF] Pressure Precipitation a Time Wind ems. Sky-! Relative Wind Heat (in.) Weather Chill Index t (edt) (mph) (mQ Cond.. 6 hour Humidity altimeter seaE 3 e RH ❑❑ ('F) (*F) level E6h..L'(m5)hr '15 � 13:54 SE 6' 5.00 ] Rain SCT014 69l 65 75 67 87% NA NA 29.99 11015.0.10:11 ' i0.99 Fog/Mist SCT060 OVC090 15 12:54 Vrbl 2,50 Thunderstorm SCT060 68 65 90% NA NA 30.00 1015.2 0.56 6 Rain BKN075 Fog/Mist OVC090 15 11.54 S 13 0.75 'Thunderstorm OVC015 70, 65 84% NA NA 30.03 1016.2 0.32 G in Vicinity 25 Heavy. Rain 15 10:54 SE 10.00 Overcast BKN015 74 67 79% NA NA 30.00 1015.3 10 OVCO20 G 17 15 '09:54 Vrbl 10.00. Overcast OVC010 72 65 79% NA NA 30.01 1015.7 7 15 08:54 SE 7 10:00 Overcast OVC011 70 64 82% NA NA 30.03 1016.2 15 07:54 SE 7 10.00. Overcast OVC012 68 64 68 66 87% NA NA 30.03 1016.2 15 06:54 SE 5 10.00 Mostly FEW012 67 63 87% NA NA 30.04 1016.4 Cloudy BKN020 , BKN026 15 05:54 SE 5 10.00! Overcast SCT025 67 62 OVC100 15 04:54 SE 5 10.00 Mostly BKN022 66 62 Cloudy 15 03:54 E 5 10.00 Mostly BKN026 .66 62 Cloudy 15 02:54 SE 5 10.00 Partly Cloudy FEW019 68 62 SCT024 15 01:54 SE 6 10.00" A Few Clouds FEW023 69 61 15 00:54 SE 7 10.00 Fair CLR 70 61 14 23:54' S 7 10.00 Fair CLR 72 59 14 22:54 S 8 10.00 Fair CLR 74 58 14 21:54 S 10 10,00, Fair CLR 76 56 G 17 14 20:54 SE 6 10.00 Mostly BKN060 77 59 Cloudy 14 19:54 SE 5 10.00 A Few Clouds FEW060 80 60 84% NA NA 30.04 1016.4 87% NA NA 30.05 1016.7 87% NA NA 30.05 1017.0 81 % NA NA 30.07 1017.4 80 69 76% NA NA 30.07 1017.6 73% NA NA 30.10 1018.5 64% NA NA 30.12 1019.1 57% NA NA 30.11 1019.1 50% NA 78 30.10 1018.7 54% NA 79 30.08 1018,0 87 80 51 % NA 81 30.07 1017.5 hitp:NwI.weather.gov/data/obhistory/KBUY.html[5/15/2014 2:37:56 PM] National Weather Service : Observed Weather for past 3 Days: Burlington Alamance Regional Airport 14 18:54 SE 8 10.00 Partly Cloudy SCT060 84 58 41% NA 83 30.06 1017.2 14. 17:54 S 10 10.00: Fair CLR 86, 56 36% NA 85 30.06 1017.1 G 17 14 16:54 SE 10.00 A Few Clouds FEW060 86 59 40% NA 85 30.07 1017.6 10 14 15:54 Vrbl .10.00! A"Few Clouds 'FEW050" 85', 60 43% NA 85 30.09 '1018.0 7 14 14:54 SE 8 10.00 A Few Clouds FEW048 85 63 48% NA 86 30.12 1019.1 14 13:54, S 10 10.00 .Partly Cloudy SCT044 '84 63 86 70 49% NA 85 30.14 1019.7 14 12:54 SE 10.00 Fair CLR 84 64 51 % NA 85 30.15 1020.1 10 14 11:54 SW 10.001 Mostly SCT035 [84 65 53% NA 86 30.17 1020.9 8 Cloudy BKN075 14 10:54 S 6 10.00 Fair CLR 81 65 58% NA 83 30.16 1020.6 14 09:54 Vrbl 10.001 Fair CLR • 78i 65 64% NA 80 30.16 i1020.7 5 14 08:54 SW 10:00 Fair CLR 74 65 74% NA NA 30.17 1020.8 7 14 07:54 Calm' 9.00 A Few Clouds 'FEW055 170 64 . 73 68 82% NA NA 30.16 1020.8. 14 06:54 SW 9.00 Mostly BKN060 69 64 84% NA NA 30.15 1020.3 5 Cloudy 14.05:54, SW .10.06-Fair CLR 69' 64 84% NA NA 30.13 1019.6 3 14 04:54 SW 10.00 Fair CLR 70 64 82% NA NA 30.13 1019.4 3 14 03:54 S 3 10.00 Overcast OVC070 72 64 76% NA NA 30.13 '1019.6 14 02:54 Calm 10.00 Fair CLR 69 63 81 % NA NA 30.13 1019.4 14 01:54 Calm 10.00 A Few Clouds 'FEW080, 73 64 83 71 74% NA NA 30.13 .1019.6 14 00:54 S 5 10.00 Partly Cloudy SCT065 74 64 71 % NA NA 30.14 1019.8 13 23:54 Calm; 10.00] iM _..... , ostly BKN060 _. ._.. 72:' 65 79/o NA NA, 30.15 ... i1020.0', Cloudy BKN080, 13 22:54 Calm %00 Mostly BKN065 75 65 71 % NA NA 30.14 1019.7 Cloudy BKN080 13 21:54 Calm 10.00 Fair CLR .77 , 64 64% NA 79 30.12 P1019.3 13 20:54 SE 5 10.00 A Few Clouds FEW065 80 63 56% NA 81 30.10 1018.7 13 19:54 SE 3' 10.00i Fair CLR 83 63 91 $3 51% NA 84 30.09 1018.2 13 18:54 S 5 10.00 Fair CLR 87 60 40% NA 87 X08 1017.9 13 17:54 Vrbl 10.0& A Few Clouds FEW060 89 60 38% NA 89 30.08 1018.1 7 13 16:54 S 8 10.00 A Few Clouds FEW060 90 61 38% NA 90 30.09 1018.2 FEW110 13 15:54 S 8 10.00; Partly Cloudy SCT060 90 61 38% NA 90 30.09 1018.4 SCT075 13 14:54 W 8 10.00 A Few Clouds FEW065 90 61 38% NA 90 30.11 1019.1 13 13:54 SW 10.00 A Few Clouds 'FEW055 89 62 90 69 41 % NA 90 30.13 '1019.6 9 http://wl.weather.gov/data/obh i story/ K BU Y,htm 1[5 /15/2014 2:37:56 PM] National Weather Service : Observed Weather for past 3 Days : Burlington Alamance Regional Airport 13 12$4 W 8 10.00 Partly Cloudy SCT050 89 64 43% NA 90 30.14 1020.1 13 11:54 W 8 10.00..!Fair CLR Z5 65 51% NA 87 30.15 1020.2 13 10:54 W 6 10.00 Fair CLR 83 67 69% NA 86 30.16 1020.5 13 09:54 SW 10.00! Fair. CLR 80;', 66 62% NA 82 30.16 1020.6 6 13 08:54 SW 10.00 Fair CLR 76 66 72% NA 78 30.15 1020.4 7 13 07:54 Calmi 8:00 Fain CLR 69 64 69 61 84% NA NA 30.14 1020.1' 13 06:54 Calm 6.00 Fog/Mist CLR 63 60 90% NA NA 30.13 1019.6 13 05:54 Calm 10.00 Fair CLR 64; 60 87% NA NA 30'.12 1019.3 13 04:54 Calm 8.00 Fair CLR 62 59 90% NA NA 30.12 1019.3 13: 03:54' Calm: 7.00. Fair CLR .63 59 87% NA NA 30.12 .1019.4 13 0154 Calm 10.00 Fair CLR 65 60 84% NA NA 30.11 1019.1 '13 01:54, S 3 • 10:001 Fair CLR '661 62 B2 65 : 87% NA NA 30.12 1019.3 13 00:54 Calm 10.00 Fair CLR 66 62 87% NA NA 30.12 1019.3 12, 23:54' Calm; 10:001 Fair CLR 67' 62 84% NA NA 30;13 1019.6 12 22:54 Calm 10.00 Fair CLR 70 63 79% NA NA 30.14 1019.8 12 21:54. Calml 10.00 Fair CLR i72 63 73% NA NA 30.14 '1019.9 12 20:54 Calm 10.00 Fair CLR 74 61 64% NA NA 30.12 1019.5 12..19:54 Calm. 10.00, Fair CLR 83 60 . 89 82 46% NA 83 30.12 1019.2 12 18:54 SW 10.00 Fair CLR 86 59 40% NA 85 30.11 1019.0 5 121 17:54 S 6 '10.00' Fair CLR '88 58 36% NA 87 30.11 1019.2 12 16:54 SW 10.00 Fair CLR 89 55 31 % NA 87 30.12 1019.4 8 12 15:54 S 7 10.00 'Fair CLR 88 55 33% NA 86 30.14 1019.9 12 14:54 SW 10.00 Fair CLR 88 56 34% NA 86 30.16 1020.7 8 DF a t e ,. Wind Vis. Weather '.� Sky� -Max. Min. • . •- .. - sea altimeter Hh Wind Hea! level1 hrTime 6 ho�ur Relative i t__.J Chill Index (mb) (edt) (mph) , (mi:), Cohd. Humidity (°F) ff) Precipitation, Temperature ('IF) p (in.) - National Weather Service Southern Region Headquarters Fort Worth, Texas Disclaimer BaG m provou. w9• Last Modified: Febuary, 7 2012 Privacy Policy htip://w].weather.gov/data/obhistory/KBUY.htm1[5/15/2014 2:37:56 PM] STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) Calendar Year 2013 Individual NPDES Permit No. NCS❑❑❑❑❑❑ or Certificate of Coverage (COC) No. NCG060040 This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March 1" of the following year. Facility Name: Mount Vernon Chemicals, LLC dba Apollo Chemical County: Alamance Phone Number: (336)506-0524 Total no. of SDOs monitored 4 Outfall No. SD01 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Additional Outfall Attachment SW U-264-Generic-25May2010 OutFall No. SDO2 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Totai Rainfall, inches TSS, m g IL pH, Standard units COD, m IL g Oil and Grease, mg/L . Fecal Coliform, Colonies per 100 ml Enteracocci, Colonies per 100 ml Benchmark NIA 100 or 504 Within 6.0 - 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy 4/4/2013 0.14 42 8.3 35 < 5 NIA NIA 11/26/2013 0.18 119 8.6 80 < 5 NIA NIA Outfall No. SDO3 Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No Yes ❑ No Yes ❑ No SW U-264-Generic-25May2010 Total Rainfall, inches TSS, m $ IL pH, Standard units COD, m/L g Oil and Grease, mg1L Fecal Coliform, Colonies per 100 ml En#erococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 - 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy 4/4/2013 0.14 7 7.0 21 <5 NIA NIA 11/26/2013 0.18 14 8.4 < 15 <5 N/A NIA Outfall No. SD04 Is this outfall currently in Tier 2 (monitored monthly)? Was this outfall ever in Tier 2 (monitored monthly) during the past year? If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes❑ No® Yes ❑ No Yes ❑ No Total Rainfall, inches TSS, mg/L pH' Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform; Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark N/A 100 or 504 Within 6.0 -- 9.0 120 30 1000 1000 Date Sample Collected, mmlddlyy 4/412013 0.14 3 7.9 < 15 <5 NIA N/A 11/2612013 0.18 8 1 8.3 44 <5 NIA NIA SW U-264-Generic-25May2010 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature Date 12,L 1 2 Mail Annual DMR Summary Reports to: DWO Regional Office Contact Information: N.C.Dept. of ENR DEC 18 2013 Winston-Salem ASHEVILLE REGIONA ,:OFFICE FAYET_ TEVILLE REGIONAL OFFICE MOORESVILLE REGIONAL OFFICE 1 2090 US Highway 70 225 Green Street 610 East Center Avenue/Suite 301 Swannanoa, NC 28778 Systel Building Suite 714 Mooresville, NC 28115 (828) 296-4500 Fayetteville, NC 28301-5043 (704) 663-1699 (910) 433-3300 RALEIGH REGIONAL OFFICE 3800 Barrett Drive Raleigh, NC 27609 (919) 791-4200 585 Waughtown Street Winston-Salem, NC 27107 (336) 771-5000 943 Washington Square Mall Washington, NC 27889 (252) 946-6481 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 807-6300 127 Cardinal Drive Extension Wilmington, NC 28405-2845 (910) 796-7215 To preserve, protect and enhance North Cardin s wafer... SW U-264-Generic-25May2010