NCG020537_MONITORING INFO_20160815

i
STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V Oa 65M
DOC TYPE
El HISTORICAL FILE
E�,'MONITORING REPORTS
DOC DATE
❑
YYYYMMDD

N ANNUAL f UAL SUMMARY DMR - WASTEWATER
ASTE . T ATER
11 SEND TO CENTRAL OFFICE
PROCESS MINEIDEWATER.ING WASTEWATER
GENERAL PERMIT NO. NCG020000
`r Report All Wasteirater- discharge monitoring data on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH I of each year. If
Jyou have limit violations, you must also have turned in a Limit Violation DMR to your local Regional Office within 30 days of receiving sample results from a lab.
CERTIFICATE OF COVERAGE NO. NCG42,f�.3 2
FACILITY NAME:
PERSON COLLECTING SAMPLES:
CERTIFIED LABORATORY: C Lab # //_ -11)-3131;
Lab #
LIMIT VIOLATIONS? YES ❑ NO
Part A: Wastewater Monitoring Requirements
SAMPLE COLLECTION[ YEAR: 2p/�
COUNTY:d%SGdLJ
PHONE NO. (z,�z)
ADD TO LISTSERVE? YES ❑ NO❑ EMAIL:
INDUSTRIAL SAND'? ❑ DISCHARGING TO SA W `AU,!,R v? []
Outfail No.
Date Sample
CoIlectedi
Total Flow
Total Suspended
Solids'
T
Settleable Solids
pH
Fecal Coltforms
-
mnVdd/yr
MG
mg/1'''
NTU2'3
m1/I2
Standard'
v `03 /
�
� �• l
0 a7
7 pcol/ml2,4
orO
RECEIVE
f IOITRAI •11
W,q
DV` R SECTION
1 Allmines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
2 If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term,
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Outfall. Alternatively, the pernuttee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
4 Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Pernut Date: 1/112010-12/31/2014 Last Revised 0 1 -21 -11
Page 1 of 2

Part A Continued: Wastewater Monitoring Requirements
Outfall No.
Date Sample
Collected
Total Flow
Total Suspended
Solids
Turbidity
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
MG
mg/l'
NTU�
mlll'
Standard
collml'"'4
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH 1 OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
( gnature of Permittee) (Da e)
Permit Date: 1/l/2010-12/31/2014 Last Revised 01-21-11
Page 2 of 2

I LIMIT VIOLATION DMR - WASTEWATER I
u SEND TO YOUR LOCAL REGIONAL OFFICE*
PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000 (MIMNG)
* Use'this form if you have Exceeded Wastewater Limits for any parameters. Send sample results to your local DWQ Regional Office within 30 days of receipt from lab.
CERTIFICATE OF COVERAGE NO. NCGO%5 f-3 :7
FACILITY NAME: l-1 n �_,�_ra r-ci1 �P + 44 _
PERSON COLLECTING SAMPLES: '
CERTIFIED LABORATORY: Jgr= r ab #
C L�nssrs. Z e, • Lab # ^
LIMIT VIOLATIONS? YES ❑ NO ❑
Part A: Wastewater Monitorina Reauirements
2016
SAMPLE COLLECTION QUARTER: 1 ❑ 2 ❑ 3 ❑ 4
MONTHLY MONIOTORING? YES ❑ NO ® MONTH: t 5
COUNTY: ©AJ'a[-(:? ra )
PHONE NO. (2S 21 -� .� - e o2.li
ADD TO LISTSERVE? YES ❑ NOD EMAIL:
INDUSTRIAL SAND? ❑ DISCHARGING TO SA WATERS°? ❑
Qutfall No
Date:Sample
t°°
:. Collected :
r
Total Flow .
Total Suspended r
= Solids:
Turbidtty3
Settleable Sotrds
pH
F
Fecal ColFform, .'
Ymmldd/yr; ::
MG
mg/l
NTU _
- ml/1
Standard
col/raal.
��
rz
• 3!
7.;i'
' All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
2 If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the Stormwater
Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the SDO.
° Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Permit Date: 1/112010-12/31/2014 Last Revised 01-2:1-1 l
Page I of 2

USE THIS FORM IF YOU HAVE EXCEEDED WASTEWATER LIMITS FOR ANY PARAMETERS.
SEND TLHS DMR TO YOUR DWO REGIONAL OFFICE WITHIN 30 DAYS OF RECEIPT OF SAMPLE RESULTS FROM THE LAB.
DWQ REGIONAL OFFICES:
Asheville Regional Office (ARO)
Roger Edwards, Surface Water Protection
Supervisor
2090 US Highway 70
Swannanoa, NC 28778
COURIER 12-59-01
Phone: (828) 296A500
Fax:[phone]
Fayetteville Regional Office (FRO)
Belinda Henson, Surface Water Protection
Supervisor
225 Green Street
Systel Building Suite 714
Fayetteville, NC 28301-5043'
COURIER 14-56-25
Phone: [phone]
Fax: [phone]
Mooresville Regional Office (MRO)
Rob Krebs, Surface Water Protection
Supervisor
610 East Center Avenue, Suite 301
Mooresville, NC 28115
COURIER 09-08-06
Phone: [phone]
Fax: [phone]
Raleigh Regional Office (RRO)
Danny Smith, Surface Water Protection
Supervisor
3800 Barrett Drive
Raleigh, NC 27609
COURIER 52-01-00
Phone: [phone]
Fax: [phone]
Washington Regional Office (WaRO
Al Hodege, Surface Water Protection
Supervisor
943 Washington Square Mall
Washington, NC 27889
COURIER 16-04-01
Phone: [phone]
Fax: [phone] or [phone]
Wilmington Regional Office (WRO)
Rick Shiver, Surface Water Protection
Supervisor
127 Cardinal Drive Extension
Wilmington, NC 28405-2845
COURIER 04-16-33
Phone: [phone]
Fax: [phone]
Winston-Salem Regional Office (WSRO)
Steve Tedder, Surface Water Protection
Supervisor
585 Waughtown Street
Winston-Salem, NC 27107
COURIER 13-15-01
Phone: [phone]
Fax: [phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
of Permittee)
(bate)
Permit Date: 1/1/2010-12/3112014 Last Revised 0 1 -2 1 -11
Page 2of2

Environmental Chemists, Inc.
envirochem 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Bogue Sound Septic Date of Report: Dec 28, 2015
325 Barrington Ridge Customer PO #:
Newport NC 28570 Customer ID: 15010004
Attention: Owner Report #: 2015-17017
Project ID: Sand Mine
Lab ID Sample ID: Collect Date/Time Matrix Sam pied by
15-40516 Site: sand mine effluent 12/21/2015 10:35 AM Water Will Coggins
Test Method Results Date Analyzed
Turbidity
SM 2130 B
231 NTU
12/22/2015
Residue Suspended (TSS)
SM2540D
251 mg/L
12/2212015
Residue Settleable (SS)
SM2540F
0.1 ml/L
12/22/2015
Temperature
SM 2550 B
18.1 C
12/21/2015
pH
SM4500H8
7.26 units
12/21/2015
Fecal Coliform
SM e222D MF
55 Colonies/100ml-
12/21/2015
Corn rnent:
Reviewed by:
Reporl #:: 2015-17017 Page 1 of 1

Environmental Chemists, Inc.
env7rochem
ANALYTICAL & CONSULTING CHEMISTS
Bogue Sound Septic
325 Barrington Ridge
Newport NC
Attention:
Lab ID Sample ID:
16-01753 Site:Outfall
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info cci cnvironmentalchemists.com
Date of Report: Jan 21, 2016
Customer PO #:
28570 Customer ID: 15010004
Report #: 2016-00702
Project ID: Sand Mine
Test Method
Turbidity
SM 2130 H
Residue Suspended (TSS)
SM 2540 D
Residue Settleable (SS)
SM 2540 F
Temperature
SM 2550 a
PH
SM 4500 H s
Fecal CoVorm
SM 0222D MF
Comment:
Reviewed by:
Collect Date/Time Matrix Sampled by
1/18/2016 2:30 PM Water Will C000ins
Results Date Analyzed
49.4 NTU
01 /19/2016
56.7 mg/L
01119/2016
<0.1 ml/L
01/19/2016
12.1 C
01/18/2016
6.52 units
01/18/2016
19 Colonies/100mL 01/18/20%
0
Report*: 2016-00702 Page 1 of 1

ANNUAL SUMMARY DMR -WASTEWATER
,SEND TO CENTRAL OFFICE*
PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
* Report All Wastewater discharge monitoring data on this form (including No Flory and No Discharge and Permit Limit Violations) by MARCH I of each year. If
you have limit violations, you must also have turned in a Limit Violation DMA to your local Regional Office n•ithin 30 days of receiving sam le results from a lab.
CERTIFICATE OF COVERAGE NO. NCG02 0,:. al
SAMPLE COLL + CT10N EAR: oZlJ/,5
FACILITY NAME: COUNTY:
PERSON COLLECTING SAA,IkPL Q 0 PHONE NO.
CERTIFIED LABORATORY: ,ab # 4 '.CrAD1),rL I�ISTSERVE? YES ❑ NO[—] EMAIL:
Lab # G!! 1�// �I,JJ
LINHT VIOLATIONS? YES ❑ NO ❑ FEB 615I)MTRIAL SAND'? ❑ DISCHARGING TO SA WATERS'? ❑
Part A: Wastewater Monitoring Requirements CENTRAL Flies
Outfall No.
Date SampI a
Collected
Total Flow
LMIR
Total Suspended
Solids
SECTION
Turbidity3
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
MG
mg/1'"
NTU2'3
nm2
Standard'
co11mi2,4
CENTFIU�L FILES
DVVR t I
'All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
' If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters: 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Outf all. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Permit Date: 1 / 1 /2010-12/31/2014 Last Revised 0 1 -2 1 -11
Page 1 of 2

Pert A Continued: Wastewater Alonitorinp- Reouirements
Outfall No.
Date Sample
Collected[
Total Flow
Total Suspended
Solids'
Turbidity
Settleable Solids
pH
Fecal Coliforms
-
mm/ddlyr
MG
mg/1`'
NTU23
rrm2
Standard'
'4
collml2
r
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH 1 OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORd1A170N REPORTED:
A certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
l am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations."
of Permit.tee)
Permit Date: 1/l/2010-12/31/2014
( ate)
Last Revised 01-21-1 1
Page 2 of 2

ANNUAL SUMMARY DMR - WASTEWATER �
II SEND TO CENTRAL OFFICE* II
PROCESS MINEIDEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
* Report All Wosleuvater discharge monitoring data on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH 1 of each year. If
you have limit violations, you must also have turned in a Limit Violation DN4R to your local Regional Office ivithin 30 days of receiving sample results frorn a lab.
CERTIFICATE OF COVERAGE NO. NCG02-0—,f- 3 Z SAMPLE COLLEC` 1ON,YEAR:
FACILITY NAME: COUNTY: e—lon j .r.�
PERSON COLLECTING SAAIPLES• PHONE NO. (Z,fZJ r�
CERTIFIED LABORATORY: Lab#/,f--A,572 7 ADD TO LISTSERVE? YES ❑ NOD EMAIL:
Lab #
LIA11T VIOLATIONS? YES ❑ NO ❑
Part. A: Wastewater MonitorinL, Reauirements
INDUSTRIAL SAND'? ❑ DISCHARGING TO SA WATERS"? ❑
Outfali No.
Date Sample
Collected]
Total Flow
Total Suspended
Solids'
Turbidity3
Settleable Solids
pH
Fecal Coliforms
niWddlyr
MG
mg/1'"
NTU2J
mll12
Standard'
COUM '"
zz
8
7. ,z 6
z7
CENTRAL
D
R SECTION
1 All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt wafers; 50 NTU for all other streams and surface waters. Turbidity may be monitored at (he
Siorrnwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
" Only facilities discharging to SA waters are required to monitor for Fecal colifornis.
C7
■0
-W4
Permit Date: 1/1/2010-12/31/2014 Last Revised 0 1 -21 -1 1
Page I of 2

Part A Continued: Wastewater Monitoring Requirements
Outfall No.
Date Sample
Collectedt
Total Flow
Total Suspended
Solids'
Turbidity
Settleable Solids
pH
r
Fecal Conforms
-
mm/dd/yr
MG
mgll'''"
NTU2,3
mIA2
Standard'
collml2'4
a -
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Caroline 27G99-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with it system designed to
assure that qualified personnel properly gather and evaluate the information submtted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations."
ure of Permittee)
Permit bate: 1 / 1 /2010-12/31 /201 4
(Date)
Last Revised 01-21-I 1
Page 2 of 2

Environmental Chemists, Inc.
" 0 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info@environmen tale hemists.coin
Bogue Sound Septic
Date of Report: Jun 22, 2015
325 Barrington Ridge
Customer PO M
Newport NC
28570
Customer ID: 15010004
Attention:
Report #: 2015-07120
Project ID: Sand Mine
Lab ID Sample ID: Bogue Sand Mine
Collect Date/Time Matrix Sampled by
15-16578 Site: Outfall
6/8/2015 2:50 PM Water Will Coggins
Test
Method
Results Date Analyzed
Turbidity
SM 2130 B
87.6 NTU
06/09/2015
Residue Suspended (TSS)
SM 2540 D
95.3 mg/L
06/09/2015
Residue Settleable (SS)
SM 2540 F
0.1 ml/L
06/09/2015
Temperature
SM 2550 B
26.5 C
06/08/2015
pH
SM 4500 H B
7-26 units
06/08/2015
Comment:
Reviewed by:
Report #:: 2015-07120 Page 1 of 1

ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-1 392-0223 FAX 910-32A424
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729. [e-mail]
Analytical & Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
CLIENT: 1
09 q lf � D i4 q �f
PROJECT NAME: ��d , e
REPORT NO: 21 2c
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONEIFAX:
COPY TO:
email:
Sampled By: O f i SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST'= Stream, SO = Soil, SL = Sludge, Other:
Identification
Collection
4-
2
N
R o
Cg
°
o
0PRESERVATION
C
M
E9
W
ANALYSIS REQUESTED
Date
Time
Temo
tu
Ln o
x
zo
onSample
�
G
C
P
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C
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12_ CrICjICV►Q'CI %4g,`
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G
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G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
.G
C
P
G
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Transfer
Relinquished By:
Daterrime
Received By:
Date/Time
1.
2.
'i'emperature when Received: Accepted: ✓ R ected: Resample Re u sJte
.Delivered By: Received By: Date: ! Time:
Comments: TUR A OUND:

IMPORA.NT NOTICE
Camlina IDivision of Water Quality (NCDWQ) is stticdy enforcing EPA regulations for sample collection and preservation_
Client Must Provide the Following Egfor mhon
1_ SAMPLE IDENTIFICATION (C',antainerAssociatedwilh regaestedtesling)
2_ SAMPLE TYPE (Composite, Grab, Water, Soil, etc-)
3. DATE COLLECTED
4. TIME COLLECTED
5. SAMPLE COLLECTOR
6. PRESERVATION (Lcdrding Tempemtareaad p13)
Tmmpera mm Samples MUST be refrigerated or received on ice bdwcen 2 and ffC_
Samplesrcceivedwithin tywo (2)boors ofcdlection mustshows duwnwmd trend_
Thcrcforc„ please record tcmperrtnie at eallectionin space provided on collection sheet_
t'$ A two (2) howlimitto chemicallypresnvc sample by pH adjustment is athrwed, except
for metals samples reported to (he Gromdwaber Sectionwbich most be audified at the time of collection_
Cartion
These sample battles may contain small amounts of acid or other cmusive and potentially barmfd chemicals- Laboratories arc rm*rcd to add
these chemicals for cutam analyses in order
to comply widk EPA presembon requirements- Use ea-tmme care when opening and hamdling
tfic botdcs_ If any chemical should get on yam skin or dodics fresh liberally with water and seelcmedical attenti rL
DECIUAI CQV&TION INS MUCTIONS
CAUTION: DONOT ARX thimmMatewitb mid in lbatdebdarecailmWne suedes asa vialmt rmotiao'WO arnw
Detilariaat"e1; Saiplesthat Re uireArid Preservatim
I- Add 4 S granules of thi asnlfate to a bride with no acid preservative
2_ After mixing to dissolve the thiosnlfate, pmr half of the sample inlD abottle contasrring add
as.apreservative_ (Ammoaia(T>
3_ Then eampletely fii 1 both bottles with fresh sample-
6Amcord of date c�rt eed, time ooileclr sample cotledor, and um of proverree prvatives Mug be a a"ained Each sample mug deaddi yincaie elm Stare of WM& Carolina
Colle�nn site on at recwdtfan9m*finnr�- Ref HCAC 2H OS05 (a) { -
6At any fim e a labo vd4 y rives samples wlich do not m ed sam* culrchon� time, or pion req*em enK thw laboraWrymust noti[y the sample c atledw ar
cTemt and a�cure aootbrr sample if pile if ambrr sample cannot be secured, the onpoal sample maybe analyzedbot ibe remits repodked mmt be qwS ied wx(htrue nahKe
of the inftwc6no(s) and the laboratory must notify due State Labumk y about the tnfiAdion(s). The n o ific ahm most =chide a stab=end con7ective actions talus to
prevail the problem for intme samples,- RcfNCAC 2H 0s05 (a) (x) (n

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Bogue Sound Septic Date of Report: Jun 24, 2015
325 Barrington Ridge Customer PO #:
Newport NC 28570 Customer ID: 15010004
Attention: Report #: 2015-07832
Project ID: Sand Mine
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
15-18327 Site: Outfall 6/22/2015 10:45 AM Water Will Coggins
Test Method Results Date Analyzed
Fecal Coliform SM 9222D MF 270 Colonies/100mL 06/22/2015
Comment:
Reviewed by:
Report #:: 2015.07832 Page 1 of 1

Way Wilmington, NC 28405
ENVIRONMEN' •i'"'I►L CHEMIS' •S! INC OFFICE:91011392-02 3FAX[phone]
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
Analytical & Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Ci.IENT:C a
PROJECT NAME: 5(;{'G�t{ 1 vim
REPORT NO: —� n
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONEIFAX:
COPY TO:
email: -
Sampled By: SAMPLE TYPE: i = Influent, E = Effluent, W = Well, ST*= Stream, SO = Soil, SL= Sludge, Other:
Sample Identification
Collection
T
r
m
E
M
r
.a n
o. o 2
o i7
U
cC7
+° o
o (L
U
a a
c� ow
e M m m
r 5
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PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
o
Z
a
=
o
N
z
^
z
x
Y
a
Z
_o
=
w
d
� �'
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G
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Transfer
Relinquished By:
Daterrime
Received By:
Date/Time
9.
2. `
Temperature when Received:
Delivered By:
comments:
cepted: ejecte Resample Requested:
_�e Received By. .p Date: Z� STime:
TUR ARO ND:

I M PORANT NOTICE
C'aralinaDivisim of Water Quality (NCDWQ) is s[ricily ndareing EPA regulations for -sample collection andpreservatior-
Client Must Prmi& the Following Infmpation
I_ SAMPLE IDENTIFICATION (CantainerAssociatedwith requestedtesbing)
2_ SAMPLE TYPE (Cnmpnskce Grab, Water, Sail, etc_)
3_ DATE COLLECTED
4_ TEWE COLLECTED
5. SAMPLE COLLECTOR
f_ PRESERVATION (Lrladire Tempest■ re amd p13)
Tnmpera"m Samples MAST be refirigeraftd or received on. ice between 2 and 6*C_
Samples received within two (2) hours of collection must showa downward trend -
Therefore, please rcc:t" temperature at Gdlex1ion in space provided on wHedion sheet
RM A two (2) hmw limit to cbemicaddy prescfve sample by pH adjushnent is alluwcd, emnopt
fo-rmrtals samples reported to the Gtoindwatcr Section which mostbe acidified at the time ofcolleetion-
Cantiof<
TWsc sample botfies may c main small amounts of acid or other corrosive and potcatially harmfd chemical�Laborahm ies am required! nt add
these chemicals for certain analyses in order
to comply wish EPA presmwafton requirements. Use euueme care vncan opmang and hmdlmg
the botdes_ if any chemical should get on your slain or clothes flush bberally with water and seek medical a ftentioa
DECg "EINATIONINSI"CTIONS
CAIMOM IlO NOT llf thiwWmatewith MW = sumPlcs aosa vi.lent rcoction wit ndm-_
DecH rinatifr,Sa plesthat RegwireArid Preser-vatism
I- Add 4l 5 grannies of thiosalfaee to a bade with no acid preservative_
2_ After mi dn.g to &ssalve the thiasalfale, poarhalf of the sample Mi n a borule containing acid
as.apreservative_ (Ammania(TKN)
3 _ Then camplelAy fill bath baffles with fresh sample_
"ArecordefdatecolteaeAtimecolfecbed samplecollector,aodumof proper pt���vesmug bvmaintaiadE-. hsamplcmusicleadyit��OmStyeafWedhCardYm
C OIIeC�[I.OfI StiE an at �nrdtra�ona- lief��
: NCAC 2H Ot05 (a) M {t�' -
¢Ptt any iva e a Iabonrtoryratxioes sasiples �vhach do nod s ed sae�pie oolledhaq hwrti of presteivationreqptiYem entr, the laboratory jo=4 mtifyIhe sainple edlector or
client and swur e anodwr sample ifpusshie_ If anuhm sample cannot be sncwcA the oupnal sum pie maybe analyzed but the tesolts repented joust be qualified wifhtlae nature
of the infrac6un(s) and fhe dal audoiy =ad mtify the 'State L b-,,,tary abaft the infiradtion(s)_ The tau imuA include a statement initiating caacdive actions t*m to
prevefftthe probfem forfutuoe sample&- Rif NCAC 2H O20s (a) (l) (n

Environmental Chemists, Inc.
envirocheni. w 6602 Windnvll Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
y
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Bogue Sound Septic Date of Report: Jul 16, 2015
325 Barrington Ridge Customer PO M
Newport NC 28570 Customer ID: 15010004
Attention: Report #: 2015-08800
Project ID: Sand Mine
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
15-20779 Site: outfall 7/10/2015 12:30 PM Water Connie Branch
Test Method Results Date Analyzed
Residue Suspended (TSS) SM 2540 g 10.6 mg/L 07/13/2015
Comment. -
Reviewed by: _ .�D km
1
Report#:: 2015-08800 Page 1 of 1

t F 1
Analytical & Consulting Chemists
0/7
ENVIRONMENTAL CHEMISTS, INC
NCOENR; DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Witmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT: (,t2
4�
PROJECT NAME:
REPORT NO:Y � Q
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONElFAX:
COPY TO:
email: -
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST'= Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
a
"
N
a o La
3 o
U.a
6 a
"
� �
g z
PRESERVATION
ANALYSIS REQUESTED
©ate
Time
Temp
w
z
�
x
�
n
x
x
Z
o
w
o
C
P
01
,�-
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
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Transfer
Relinquished By:
Daterrime
Received By: -
Date/Time
1.
2.
temperature when Received: Accepted: -.,I-
Delivered By:_ Received By
Comments:
mple Requested;
ate: �'1S Time
TURNAROUND:

I LIMIT VIOLATION DMR - WASTEWATER I
11 - .SEND TO YOUR -LOCAL REGIONAL' OFFICE*, I�
PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000 (MINING)
*' Use this form if you have Exceeded Wastewater Limits for any parameters. Send sample results to your local DWQ Regional Off ce within 30 days of receipt from lab.
CERTIFICATE OF COVERAGE NO. NCGO %
FACILITY NAME: f
PERSON COLLECTING SAMPLES: C�
CERTIFIED LABORATORY;Lab #
Lab #
LIMIT VIOLATIONS? YES ❑ NO ❑
'art A: Wastewater iVlonitoring 1Reouirements
SAMPLE COLLECTION QUARTER: 1❑ 2 E4 3❑ 4❑
MONTHLY MONIOTORING? YES ❑ NO ® MONTH:
COUNTY: _
PHONE NO.
ADD TO LLSTSERVE? YES ❑ NOD EMAIL.:
INDUSTRIAL SAND'? ❑ DISCHARGING TO SA WATERS"? ❑
1 All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
2 If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
'The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the Stormwater
Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the SDO.
4 Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Permit Date: 1/1/2010-12/31/2014 Last Revised 01-21-1 1
Page 1 of 2

USE THIS FORM IF YOU HAVE EXCEEDED WASTEWATER LIMITS FOR ANY PARAMETERS.
SEND THIS DMR TO YOUR Dn REGIONAL OFFICE WITHIN 30 DAYS OF RECEIPT OF SAMPLE RESULTS FROM THE LAB.
DWQ REGIONAL OFFICES:
Asheville Regional Office (ARO)
Roger Edwards, Surface Water Protection
Supervisor
2090 US Highway 70
Swannanoa, NC 28778
COURIER 12-59-01
Phone: [phone]
Fax: [phone]
Fayetteville Regional Office (FRO)
Belinda Henson, Surface Water Protection
Supervisor
225 Green Street
Systel Building Suite 714
Fayetteville, NC 28301-5043
COURIER 14-56-25
Phone: [phone]
Fax: [phone]
Mooresville Regional Office (MRO)
Rob Krebs, Surface Water Protection
Supervisor
610 East Center Avenue, Suite 301
Mooresville, NC 28115
COURIER 09-08-06
Phone: [phone]
Fax: [phone]
Raleigh Regional Office (RRO)
Danny Smith, Surface Water Protection
Supervisor
3800 Barrett Drive
Raleigh, NC 27609
COURIER 52-01-00
Phone: [phone]
Fax: [phone]
Washington Regional Office (WaRO
Al Hodege, Surface Water Protection
Supervisor
943 Washington Square Mall
Washington, NC 27889
COURIER 16-04-01
Phone: [phone]
Fax: [phone] or [phone]
Wilmington Regional Office (WRO)
Rick Shiver, Surface Water Protection
Supervisor
127 Cardinal Drive Extension
Wilmington, NC 28405-2845
COUR.I.ER 04-16-33
Phone: [phone]
Fax: [phone]
Winston-Salem Regional Office (WSRO)
Steve Tedder, Surface Water Protection
Supervisor
585 Waughtown Street
Winston-Salem, NC 27107
COURIER 13-15-01
Phone: [phone]
Fax: [phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
re of Permittee)
Permit Date: 111 /2010-12/31 /2014
�7` r'
(Date)
Last Revised 01-21-1 1
Page 2 of 2

ANNUAL SUMMARY )N R - WAS`'EWAT ,R
SEND TO CENTRAL OFFICE*
PROCESS MINE/DEWATERING WASTEWATER JUN 19 zUiS
CEN7RgL 2 5
GENERAL PERMIT NO. NCG020000 DWR s�r,r,L_ .
* Report All Wastewater discharge monitoring data on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH I of each year. if f
you have limit violations, you must also have turned in a Limit Violation DNIR to your local Reeional Off -ice within 30 clays of receivin„ sample results from a lab.
CERTIFICATE OF COVERAGE NO. NCG02 Q
FACILITY NAME:
PERSON COLLECTING SAMPLES: c
CERTIFIED LABORATORY: Lab #/5-Df-3-Z ?
Lab #
LINIIT VIOLATIONS? YES ❑ NO JK
Part A: Wastewater Monitoring Requirements
SANIPLE COLLECTION YEAR: pW / 5
COUNTY:
PHONE NO. (�� —
ADD TO LISTSERVE? YES ❑ NO❑ ENTAIL:
INDUSTRIAL SAND'? ❑ DISCHARGING TO SA WATERS . ❑
Outfall No.
Date Sample
Collected
Total Flow
Total Suspended
Solids
Turbidity
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
rvIG
mgA1.2
NTCI'
mlll'
Standard'
col/m12,4
.S
QJ S
D
G.
< D.1
8.3
<
'All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
2 if an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
4 Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Permit Date: I/l/2010-12/31/2014 Last Revised 01-21-1 1
Page l of 2

Part A Continued- Wastewater Monitoring Requirements
Outfall No.
Date Sample
Collected[
Total Flow
Total Suspended
Solids[
Turbidity3
Settleable Solids
pH
Fecal Coliforms
-
`nim/dd/yr
MG
mg/1`-,
NTU2'1
ml/1'
Standard'
col/ml2'4
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Atm. DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-I617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORAIAHON REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
1 am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations."
(Signature of Permittee)
Permit Date: 1 / 1/2010-12/31 /2014
�..�Ll 1,5-
( ate)
Last Revised 01-21- l l
Page 2 of 2

ANNUAL SUMMARY DMR - WASTEWATER
SEND. TO CENTRAL OFFICE*
ECEIVED
FEB �. 6 2015
PROCESS MINEMEWATERING WASTEWATER CENTRAL FILES
GENERAL PERMIT NO. NCG020000 DWR SECT
ION
*tRepoit All Wastewater, dis tiarge.monitoring.,data on this'form (incIudirig No Flow iand:No Discharge and Perriiif'Li it Violations) by MARCH I of each year. rIf;"
ou have.lirnit violations,. you. must als6.havd turned. in a Limii.Violation DMR to our local Re 'onal Office ivith`in 30J4s of receivin sample results from a lab. ,.
CERTIFICATE OF COVERAGE NO. NC 02-0 SAMPLE COLLECTION YEAR: -40 1.5'
FACILITY NAME: - I / COUNTY: - CJ AI-6 �-OLO
PERSON COLLECTING SAMPLES: ee h PHONE NO. {23a) J93 - 64a
CERTIFIED LABORATORY: i7 e/y8 7;i Lab # {S- n!) /'7/ ADD TO LISTSERVE? YES ❑ NO❑ EMAIL:
Lab #
LIMIT VIOLATIONS? YES ❑ NO ❑ INDUSTRIAL SAND? [IDISCHARGING TO SA WATERS°. ❑
Part A. Wastewater Monitoring Renuirements
.�S"'� T^ 1
j
f �T%Vii,
,�'}y� $�•Y_
;Outfall'No ^'
rw�'.+w-.w.1,n:.�° �
:K+��.� '.` ,A :li.
�.N''',�jT.
..
i-, �) :'_.,� � i'_ .: ',a) ...��
:5: -:-^>"'Lf :xt,.'.In
Date'Sa 1'
l?
_ *r _ t't.�
f.,� CO1lQCtCtI',:•, � Z
�, G }y �
_ .h � W-::'. � ^� ir�t„ •.
i:7 i�.....�....:-.LRL
1-.
:wS�fti
t
Total=Flow 'x
+�.,r..G...%-x:+.-„_. �,' J.
h i
�y
h .,ti'.'•'*L3'S?Y.r1...
'{., .. it_ .,t f•i
Total�SuspeH&d
�F:
; �;SOb(IS
3.
� "
_KYZ'rY ;e w.�.'
2# _ 1.M.,
Tiirbidlty3.
� 1'
•..k,. ?v'�r
1
z t•_7n, i` '.br�.,Jt'uytt�v��
-Cl' - ..NT
Y i'Y _
r-SettlAW Solids
w...4•ri. .:7,...1 �ii t �
!' :J" ,:S
� �,.��
-fP.q-'! .S
-L.. -iK ��
r 'S H�
' pI3= r;
ri...,, t.u�ts:�... ..i`il?;jF
,r_fz...
1•li:`fn!iu v:.' i .�M1.-..
lid': y�; 9.'".• r
f � �� '}
.1�i "':&�..a wr�w..:.'
1•}rF�..F'I-'
fSSS, �
�, FecaliColiformsr �`'
�r•'7,`.�w.iwl, ,yrtc- t;.� r�,
Fy,? � rys Fyf � i,� �{3
mmldd/Yr-%
t � MG "J'"
.� mgll , •,
NTU
iJ mill
Standard, �
' col/ml - L •.
-5/
{
'All mines must monitor W W discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
Z If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
° Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
IMP
Permit Date: 1/112010-12/31/2014 Last Revised 0 1 -2 1 -11
Page 1 of 2

Part A Continued: Wastewater Monitoring Requirements
1k ��. '1 ..
:Outfall No
Date Sample -,r
=s i.r
Collected F
5'-TotalrFlow '
t , ; ,
V.
=Total Sus 'ended ,
pr _�,�
Solids ��
'S
: { ;Tuibidii:s
F,' ! ..,f Y
�_ _ •, '
5ettlealile'Solids-
t -.K •} �,f',.
° 1 tt
r .pH is
f s�
'w #x::. ! Lw1f:, :�%t.F r
.�k : ;c-e"•.
Fecal Cohforms-'
t
e f..r
minlda6-
MG'
'r, 3 r'�.
mg/l
NTU
_; F
Standard-`_;
col/ml
i •�
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT,
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penally of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system; or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee) (Date)
Permit Date: 1/1/2010-12/31/2014 Last Revised 0 1 -21 -11
Page 2 of 2
r'

envirochem
ANALYTICAL & CONSULTING
CHEMISTS
Envir oninenta l Chemists, Inc.
6602 Windmill Way + Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Mato, NC 27954
[phone]
NCDENR: DWQ CERTIFICATE #94. DI,S CERTIFICATE #37729
Bogue Sound Septic Date of Report: Jan 13, 2015
325 Barrington Ridge Beacham Report #: B-33972
Newport NC 28570 Report #: 2015-00090
Attention: Ricky Taylor Customer ID: 15010004
Project ID: Howard Pit
Lab ID Sample ID: 127185,127186.127187 Collect DatefTime
Matrix
Sampled by
15-00171 Site:
12/31/2014 10:00 AM
Water
Client
Test
Method
Results Date Analyzed
Turbidity
SM 2130 B
63.3
NTU
01105/2015
Residue Suspended (TSS)
SM 2540 D
36.5
mg/L
01/06/2015
Residue Settleable (SS)
SM2540F
<0.1
ml/L .
01/02/2015
pH
SM 4500 H B
5.50
units
12/31/2014
Fecal Coliform
SM 9222D MF
<1
Colonies1100ml-
12/31/2014
Comment:
Reviewed by:
Report #: 2015-00090 Page 1 of 1

�C?JL
1820 Wilmington hwy
Jacksonville, NC 28540
(910)-347-5843
NCCENR CwQ # i
CHAIN OF CUSP ICY
Client Q/ 1 G
Address-
Billing:
Page --L of
Sampled by:
Client # and abbr.;
Project:_,
PhOne #;
Fax #
Samp
Locat
Eru,D,
Date
Samp
20
Time
Samp
f9pm
Samp
Type
c,g,b
Bottle
Slze(ml)
&Type
P,G,V
Preservation
(Lab Use)
ANALYSIS REQUESTED
B
0
D
T
S
S
N
H
3
F
E
G
C
0
N
,T 1
P
T
'N
0
&
G.
�'
*T
yp
e
p
H
C
I,
a
I-3
a
***++****++x++THE SECTION eELOWi,(WHERE APPLICABLE). MPST BE COM13t EKED BY THE
1. The preservatfve must not be rinsed out of the FECAL, NH3, TN, TKN, NO3, TP, l'OC, TC, O&G or VOC bottles.
2. Sample temperature at collection time : °C. (Must be completed If temp is >6°C and transit time Is less then two hours.)
3. Composite start date: ! ! 00, and time ; AM PM,
4. If the chlorine residual Is above 0.2 PPM, all NH3 samples must property dechlorinated at collection time using the sodium thiosulfate
soiutlon provided by Beacham Lab.
S. ALL SAMPLES MUST BE RECEIVED IN ICE. IF THE TRANSIT TIME IS OVER TWO HOURS THE SAMPLE TEMPERATURE MUST 13E s6°C. IF
THE TRANSIT TIME IS LESS_ THAN TWO HOURS THE SAMPLE TEMPERATURE MUST SHOW AN APPROPRIATE DOWNWARD TREND AND #2
ABOVE MUST BE COMPLETED. IF THESE REQUIREMENTS ARE NOT MET SAMPLE REJECTION WILL OCCUR.
Relinquished late , Tjge Received Date Time Relinquished Date Time Received Oate Time
bynlryhlF)pm by 2000 am pm by 2000 am pm by 2000 am pm
SECTION BELOW IS FOR LAB USE*+++++++++++++++xx+�+++**x++�+x++++x+x+x+++++.:*+
1. Sample Temperature : °C'
2, Sample temperature not s6°C. and delivery time is s two hours, Transit time = min. ATemp = ° C.
mments :
* Preservation Codes : S= Sulfuric Acid, T= Sodium Thlosulfate, 0= Other
HOLDING TIMES : e KR§ = Fecal and Total Collform. 48 HRS = BOD, OP, NO2, MBAS. 7 DAY, = TSS, TDS. 14 DAYS = VOC
228 DAYS = NH3 r Cl-, TP, COND, 0&G, TKN, TN, TOC, NO3. 0 MON tj3 = Most,Metals.
PLEASE COLLECT ALL MONDAY BOD SAMPLES AFTER 8:00 AM, AND DELIVER ALL SAMPLES WITH HOLDING TIMES OF 48 HOURS OR LESS
BEFORE NOON ON FRIDAY. M13AS SAMPLES MUST BE DELIVERED BY NOON ON MONDAY OR TUESDAY ONLY.
Rev. 03-00

I ANNUAL SUMMARY DMR - WASTEWATER I
SEND TO CENTRAL OFFICE*
PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
Report All Wastewater discliai a monitonn data:ori this foim (including No Flow and No Discharge acid Permit Limif Violations).by MARCH7.of each year. If
you have, limit �iolaraons, you must also have turned in a Limit Violation DMR to your local Re don0'.Office.within.30,days.ofreceives satnple resuIts,froix► a lab..._ .
CERTIFICATE OF COVERAGE NO. NC 02_60 s 7
FACILITY NAME: ZZ�2U24W_A -
PERSON COLLECTING SAMPLES: ,PEA
CERTIFIED LABORATORYA_14m Lab #
Lab #
LIMIT VIOLATIONS? YES ❑ NO ❑
Part A: Wastewater Monitoring Requirements
SAMPLE COLLECTION YEAR: _. 020 /
COUNTY:
PHONE NO. (a2,sa) —
ADD TO LISTSERVE? YES ❑ NO❑ EMAIL:
INDUSTRIAL SAND'? ❑ DISCHARGING TO SA WATERS"' ❑
-au.a.�.- 'rv.
.»"':�':.- 'i 3
= Outfall No
.�} �'L �r�r�_
i L- _ a.v.r S.$'i..EM''„'v>j�,-
Date ample
t
_ _Collected
��yy��44;; -3• i
!i�'.tS. - xvY 1,
h--�
Total Flow
f-.
...� -�i"v .i'
Total'Suspended
1
Solids.
aL:,rda u;�»=.q.
f'�..'.i.l k?�...._�f ' y
Turb�dity3
.. Y'. :• �zC _ i..-,..
- �- { r �
� � �
Settleable Solids
Rj-v--`s y�wr�.{,�s
-Ike �. Y 1
pH
�. ��+. _vim+• R,
_S 1F'i - �,�r�'ii�±-�>..'�`i_..1
� -
al
FecCaUforms
mm7dd/pr
:MG
mgll,
NTU
4=` mU1
�Staodard
- -
CHI
coVml
-
.4 o
Nr
REGEWE
CENTRAL FIL
L
' All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
2 If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed; 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU` for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
4 Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
CWJ
:S
V
Permit Date: 1/1/2010-12/31/2014 Last Revised 01-21-11
Page I of 2

Part A Continued: Wastewater Monitoring Requirements
s
Outfall`No:
Date'Sample.`'
r ,.1
h Collectedc
_
Total Flout i*r
-
zj 1= ,
sTota) SuspendedI�irbidity3
Sohds 4
r e
Settleable Salsds
pH
Feca1'Gohforms
s _ .r.
_ _.2-
u�m/ddl
_ _
iVIG
_ __ u
m
NTO— -
r
nilh
_ _ _ _
--'Standard :
_ _ _
'cvllAil
MAH ORIGINAL AND ONE COPY OF THIS ANNUAL SUNIMARYANCLUDING ALL "NO FLOW' "NO DISCHARGE" & LIMIT
VIOLATIONS BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is,'to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
o- r
(Sx ature of Permittee) (Date)
Permit Date: 1/l/2010-12/31/2014 Last Revised 0 1 -21 -11
Page 2 of 2

NCDEM
,7 1
Beacham Laboratory
1820 Wilmington Highway
Jacksonville, NC 28540
910-347-5843
REPORT OF ANALYSES
ROGUE SOUND SEPTIC (BSS
NCDEH
# 37718
HO'WARD PIT
DATE: 10/09/2014
325 BARRINGTON RIDGE
NEWPORT, NC 28570-
Attn: RICKY TAYLOR
BOGUS SOUND SEPTIC, HOWARD PIT (SEPTEMBER 2014) (Page 1 of 1)
AMPLE
DELIVERY TO LAB
LAP, No. DATE TIME SAMPLER
DATE TIME
MATRIX
126432 09/24/14 1.110 ROD REEVES
00/24/14 11.40
Wil
126433 09/24/14 111.0 ROD REEVES
09/24114 1140
WV?
126434 09/24/14 1.110 ROD PEEVES
09/24/14 1140
WW
CLIENT LAB COLIF,FEC PH
TSS SETT.SOL
TUR11
STATION ID NUMBER GOL/100mL STD UNIT;
PPM ml/L/hr.
NTU
HP OF PHSSTSS 126432 N.R. 5.4
23.3 ;0.1
N.R.
HP OF FEC 126433 18 N.R.
N.R. N.R.
N.R.
HP OF TURB 126434 N.R. N.R.
N.R. N.R.
1.2.6
THE DATE ANALYZED IS STAMPED ON THE CHAIN OF
CUSTODY.
NOTE: N . R . = ANALYSIS NOT REQUIRED
LABORATORY DIRECTOR

r,"iiasn yae�qa&fCHAIN OF CUSTODY Pago of
1820 Wilmington hwy Client: Sampled by;
Jacksonville, NC 28540 Address: Client # and bbr.: %
(910)-347-5843 . _ Project : `
NCDENR DWQ # 1 Billing: _ Phone #:
Fax #
Bottle
Preservation
ANALYSIS REQUESTED
Samp
Locat
E,U,D,
MW
Date
Samp
20
Time
Samp
mom
Samp
Type
c,g,b
Slza(ml)
&Type
P,G,V
(Lab US*)
B
0
D
T
S
S
N
H
3
F
E
C
C
0
N
7
P 'N
T
0
&
G
s
!p
t�
*T
op
p
H
C
ix
-2
0
Ir
*******************+**THE SECTION BELOT(WHERE APPLICABLE) MUST BE COMPLETED BY THE
1. The preservative must not be rinsed out of. the FECAL,-NH3, TN, TKN, NO3, TP, TOO, TO, O&G or VOC battles.
2. Sample temperature at collAcUon time :_*C. (Must be completed If tamp is >G°C and transit time is less than two hours.)
3. Composite start date; I- 100, and time : AM PM.
4. If the chlorine residual Is above 0.2 RPM, all NH3 ramptos must property dochlorinated at collection time using the sodium thlosulfate
solution provided by Beacham Lab.
5. ALL SAMPLES MUST BE RECEIVED IN ICE. IF THE TRANSIT TIME IS OVER TWO HOURS THE SAMPLE TEMPERATURE MUST BE sG°C. IF
THE TRANSIT TIME IS LESS THAN TWO HOURS THE SAMPLE TEMPERATURE MUST SHOW AN APPROPRIATE DOWNWARD TREND AND #2
ABOVE MUST BE COMPLETED. IF THESE REQUIREMENTS ARE NOT MET SAMPLE REJECTION WILL OCCUR.
Rellnquished
by
Date
2012am
Time
pm
Received
by
Date
2000
Time
am pm
Relinquished
by
Date
2000
Time
am pm
Received
by
Date
2000
Time
am pm
r2�?
I f'• • `f �I
i .
�
�
***++*t*rr**r+*tt+*t*+*+*t*******ttk*t*******THE SECTION BELOW IS FOR LAB USE*rr*+*+r*r+xr***+***r*r*+**+****+++***rr**rr*++**
1. Sample Temperature : *C.
2. Sample temperature not s U*C. and delivery time is s two hours. Transit time = min, ATemp = °C.
3. Comments:
* Preservation Codes : S= Sulfuric Acid, T= Sodium Thlosuifate, O= Other
HOLDING TIMES : 6 HRS = Fecal and Total Collform. 48 HRS = SOD, OP, NO2 MBAS. i DAYS = TSS, TDS, 1. 4 DAYS = VOC
28DAYS = NH3, Cl., TP, COND, O&G, TKN, TN, TOC, NO,. 6-MQNTH$ = Most Metals.
PLEASE COLLECT ALL MONDAY ROD SAMPLES AFTER 8.00 AM, AND DELIVER ALL SAMPLES WITH HOLDING TIMES OF 48 HOURS OR LESS
BEFORE NOON ON FRIDAY. MBAS SAMPLES MUST BE DELIVERED BY NOON ON MONDAY OR TUESDAY ONLY.
Rev. 03-ft
RAR

Environmental Chemists, Inc.
'7'.chem 6602 WindmiII Way • Wilmington, NC 28405
rO
[phone] (Lab) + [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDF.NIZ: DWQ CER'ITFICATE 094. DLS CERTIFICATE OM9
Beacham Laboratories Date of Report: Sep 30, 2014
1820 Wilmington Highway Customer PO #:
Jacksonville NC 28540 Customer ID: 08100013
Attention: Rod Reeves Report #: 2014-11876
Project ID: Bogue Sound Septic
Lab ID Sample ID: 126434 Collect DatelTime Matrix Sampled by
14-29155 Site: Howard Pitt 9/24/2014 11:10 AM Water Rod Reeves
Test Method Results Date Analyzed
Turbidity SM2130 a 12.6 NTU 09125/2014
Comment:
r e'
Reviewed by:
Report #:: 2014-11876 Page 1 of 1

� • , - � �
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS,INC OFFICE: g10-392-0223FAX 910�3 2-4424
NCDENR: DWG CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info0onvironmentalchemists.com
COLLECTION AND CHAIN OF CUS7EODY AY rax Q10�34�i- q:-`Il
CLIENT: lea6 L"
PROJECT NAME:
REPORT NO:
ADDRESS: 1'g W u A 64,ay
CONTACT NAME:
PO NO:
fVC 2-K 6
REPORTTO:&ad -e-eax-.5
PHON Ax:
CAP'He: ;Tz'e.i zo -Oct1-yS1OZ
ernail: rC7GQv(�-�V�r r'
Sampled By; SAMPLE TYPE: l - Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other o ow
Sample Identification
ANALYSIS REQUESTED
Relin
f11�

I ANNUAL SUMMARY DMR - WASTEWATER I
SEND, TO CENTRAL:OFFICE*
PROCESS MINEMEWATERING WASTEWATER
GENERAL PERMIT NO. NCG620000
*=12epoii All Wasfewafer discharge monitoring data,on this form (including No Flow and No Discharge and Permit Liinit Violations) by MARCHrIof each year. If ;
ou.have.limii violations, y ou,must also,have.turned'in a^Limit Violation DMR "to our Iocal Re�onal Office.within 30,da s of receivin s* le resulis,froin a lab.
CERTIFICATE OF COVERAGE NO. NCG02Q 'S�-7 SAMPLE COLLECTION YEAR: 4-bl4
FACILITY NAME: A{OLi � � �I Tl� COUNTY: D/l%SLD(
PERSON COLLECTING SAMPLES: PHONE NO. (2"
CERTIFIED LABORATORY: Lab # ADD TO LISTSERVE? YES ❑ NO❑ EMAIL:
Lab # .
LIMIT VIOLATIONS? YES ❑ NO ❑ INDUSTRIAL SAND'? ❑ DISCHARGING TO SA WATERS'? ❑
Part A: Wastewater Monitoring Requirements
��,.e'•�_Yy;F�� y�:'
x,"iFf'v7::. yS JF
•a..i{
:OutfalI Na
z3Y»•• w 'u
1�.5 �+... a!;v+a: S_i�;A..,r(' "'-Y?� e
�NMi�i :�• ::. tl aw'TF ♦: . ri.:s
T
� t-
Date'Samy,�y
�. �1 P z
,. _ •
: Ka COIICCtCd 4
`^ef�y� ��;j r�?i
E_- t`%�n;..itrCAp.,...,
errs ,, YI
:.
#; Total�Flow;
r ..� t A
t.,+_6=h'
� •'-
4 w:� _�,�:� 1
z'N
3 Total Suspended
SOI1d5,-«k__�i;.u7
r.. :. `J..J.3.:.,:. t.:-..
_ �
wwYN.....�. .1.... Y- -..�5
n Turbid�ty3°.>.
, ;
:z1..=-. �_
t. �: i '.: � � H.,3
1 ...��='V. iV »A' w;.�:rl
�, t
Settleable Soltdsti
.a::-:_.'
1� Y .�C`�sA�ti.� t3,��. _,ip
MS.,+�•' ^'}2t�,,,•,,-w �+':1:
r + K
„� ,,pHr�r,=�
tI�rt TS
� �'s, lt.`'.,r�`�rl.7a "j` -5_:.
,iy:.ir' x _
�* rFecalfColtforms
4 yR 527::»rgk v t»:
-
w t r"k'�" _F
d ' -'^r
mm/dd/yr:
I:�S, ir+
MG
�•,r M AY. i
r mgll,
NTU �''
4 k�
nil/l x'
,}Standard
L. .�4.:�1f
'Y�r"''::fJcol/ml
�$sMLaU
- S 3
S
0 .3
.12f
o
M. .-
��2
F
�
� f
�Lj��/
l n L—
MAI
.-�►.1TRALFiLES
" nwQEEO�
' All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
2 If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
° Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Permit Date: 1/1/2010-12/31/2014 Last Revised 0 1 -2 1 -11
Page 1 of 2

Part A Continued: Wastewater Monitoring Requirements
`�OuJ lftali l No1
➢.-.
, ka. b(CaotellSecatmed tlYer`1Y tT
( �! 'l{.. f�
1 ` TYo- tFa. lSu
:Solids f
T►d
Settleable Solids
}T
t' ;1,ty
Fecaltot;liTf`erms
C
a!-
_mm/dd/Vr,
` > '
NTU
nil/l _
-'3tandard
:collml . aT_^T.
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH 1 OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system; or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee) (Date)
Permit Date: 1/l/2010-1213112014 Last Revised 0 1 -21 -11
Page 2 of 2

:enviroce'he mn]
ANALYTICAL & CONSULTING
CHEMISTS
Beacham Laboratories
1820 Wilmington Highway
Jacksonville NC 28540
Attention: Rod Reeves
Lab ID Sample ID: 125211
14-08634 Site: Smyrna Mine
Environmental Chemists, Inc.
6602 Windmill Way a Wilmington, NC 28405
[phone] (Lab) - [phone] (lax)
710 Eowsertown road a Manteo, NC 27954
[phone]
NCDENR: DWQ CERTIFICATE #94. DL$ CERTIFICATE 037729
Date of Report: Mar 31, 2014
Customer PO #:
Report #: 2014-03541
Report to: Rod Reeves
Project ID:
Collect DatelTime Matrix Sampled by
3/25/2014 2:30 PM Water Rod Reeves
Test Method Results Date Analyzed
Turbidity SM 2130 B 3.9 NTU 03/27/2014
Lab ID Sample ID: 125216 Collect Date/Time Matrix Sampled by
14-08635 Site: Howard Pitt 3/25/2014 4:30 PM Water Rod Reeves
Test Method Results Date Analyzed
Turbidity sm 2190 B .19.4 NTU 03/27/2014
Comment:
Reviewed by: 1
Report # : 2014.03541 Page 1 ar 1

i
11
nwl&&a;p ��a�r� CHAIN OF CUSTODY
1820 Wilmington hwy Client:
Jacksonville, NC 28540 tAldresS : t
(1(J) -3 4 7.5843",= x
NCDENR DWQ # I Billing
Page --L of J—
SaTpoed by
Client # and abbr.: d
Project:_
Phone # :Fax #
v
-Bottle
—-
I
NUNNfit■■■■■■■
■■■■■■M■■■■■■
—
----
- --
ANALYSIS
--
REQUESTED
—
— I
i
■��
NOON
�,GG■!
■E■
NONE
■■�
■■■■�
ON
■■■ENE■■■
■■'■■■
��■■■
■NOON■■
■■■■
��■■■■■■�
NOON
eE
■■■■■■■■■
■■r■■
�■■■■
■®■■NNt■■■
NOON■
■
-------'- ----•-----Int StI:IIUN OLLUYf (wr1EREAPPLICAWLE) MUST BE COMPLETED 13Y THE CLI EtiT. rxxxexxxxxxxxr►..xxxx,;xwxw
off•
1. The preservative must not be rinsod out of 60-FECALI NH3, TN, TKN, NOa, TP, TOO, TO, 0&G or VOC bottlos.
2. Sample tomperuturo at colloetlon Vrno : -J�7 . .0 (Must be completed If temp Is a61C and transit tlmo Is less than two hours.)
3, Composite start date : / / 00, ar d time : AM PM.
4, If the chlorine rosldual Is above Q.2 PP , fill NH3 samples must properly dechlorinated at collootlon time using the sodium thlosulfate
solution provided by Beacham Lab.
5. ALL SAMPLES MUST BE RECEIVED IN ICE, IF THE TRANSIT TIME IS -OVER TWO HOURS THE SAMPLE TEMPERATURE MUST BE s8'C. IF
THE TRANSIT TIME IS LESS THAN TWO HOURS THE SAMPLE TEMPERATURE MUST SHOW AN APPROPRIATE 'DOWNWARD TREND AND #2
ABOVE MUST $F COMPLE7F6_ IF YPtfgF R1?nIIIDr:M17)dTQ hoe Mr%T Kaer enxanf uric , nnnrlo I i
Relinquished
by
Date Time
20b am pm
Recelved
by
Date
200
Time
am pm
Rolingplshod
by
Date
20f4
Time
am pm
Revolved, Date Time
by 200 am pm
' IV
_-.--------- .......... ....It1k St(:[IUN 6ELUW IS FUR LALSV?jV........x.x.x.x.x.........r....-.......x...w.:,
I. Sample Temperature : °C.
2. Sample temperature not s6°C. and deliverytime is!; two hours, Tronslt Umo a min. ATemp = 'C.
3, Comments;
` Proservatlon Codes i S= Sulfurlo Acid, T= Sodlum Thlosulfate, 0= Other
HOLDING TIMES . 0 FIRS = Fecal and Total Conform. 0 HRS - BOD, OP, NOz, MBAS; 7 DAYS - TSS, TD5. 14 DAYS VOC
28 DAYS = NH3, Cl-, TP, COND, 0&G, TKN, TN, TOO, NO3. 0 MQNTHS = Most Metals.
5 ,
PLEASE COLLECT ALL MONDAY BOD SAMPLES AFTER 3:00 AM, AND DELIVER ALL SAMPLES WITH HOLDING TIMES OF 48 HOURS OR LESS
BEFORE NOON ON FRIDAY. MBAS SAMPLES MUST BE DELIVERED BY NOON ON MONDAY OR TUESDAY ONLY,
Rev. 03-W
RAR

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCL)ENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICF: 910-392-0223 FAX [phone]
[e-mail]
tax 9l©--3 cf7- T -%7I
CLIENT:
PROJECT NAME: J
REPORT NO:
ADDRESS: j$ VAiU ou
CONTACT NAME:
Pa NO:
J- U ��' b
REPORT TO: �.�L.�e S
PHON FAX: YfD- 3 7 Sid 3
/I
GBF*3f3-iG� -2�f y4�0�
R
entail: G�1r$21% t
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Ov 4U1
N
M) FA
Vie.allgoI
JF�
4
�
�
�

NCDEM NCDEH
# 1 It 3771.8
Beacham Laboratory
1820 Wilmington Highway
Jacksonville, NC 28540
910-347-5843
REPORT OF ANALYSES
ROGUE SOUND SEPTIC HOWARD PIT
325 BARRINGTON RIDGE
DATE: 04/04/2014
NEWPORT, NC 28570-
Attn: RICKY TAYEOR
HOWARD PIT WASTEWATER REPORT (Page 1 of 1)
SAMPLE
DELIVERY TO LAB
LAB No. DATE TIME SAMPLER
DATE TIME
MATRIX
125213 03/25/14 1630 ROD REEVES
03/25/14 1700
WW
125214 03/25/14 1630 ROD REEVES
03/25/14 1700
WW
125215 03/25/14 1630 ROD REEVES
03/25/14 1700
WW
CLIENT LAB COLIF,FEC PH
TSS SETT.SOL
TURB
STATION Ill NUMBER COG/100mL STD UNITS
PPM m1/L/hr
N`['U
HP OF PHSSTSS 125213 N.R. 5.0
9.8 0.3
N.R.
HP OF FEC 125214 1 N.R.
N.R. N.R.
N.R.
HP OF TURB 125215 N.R. N.R.
N.R. N.R.
19.4
THE DATE ANALYZED IS STAMPED ON THE CHAIN OF
CUSTODY.
NOTE: N. R. M ANALYSTS NOT REQUIRED
/fir
/'. /
LABORATORY DIRECTOR