NCG020279_MONITORING INFO_20190107

PERMIT NO.
DOC TYPE
DOC DATE
STORMWATER DIVISION CODING SHEET
NCG PERMITS
/v c-&va Dal q
❑ HISTORICAL FILE
MONITORING REPORTS
"OF ■iyr"all
rr

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
NCGNE
DOC TYPE
❑ HISTORICAL FILE
DOC DATE
❑
YYYYM M DD

L
ANNUAL SUMMARY DMR = WASTEWATER
FEND TO CENTRAL OFFICE*
PROCESS MWE/DEWATER.XNG WASTEWATER
GENE,1UL PERNIff NO. NCG020000
* Report All Wastewater discharge monitoring data on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH 1 of each year_ If
you have limit violations, you must also have turned in a Limit Violation DfvfR to our local Re Iona! Office within 30 days of nzeiving sample results from a lab
CER'TfFICATF, OF COVERAGE NO. NCG02Q Q O D Ga p, 7 rli l PLE COLLECTION YEAR: .Z 6 1 g
FACILITY NAME: 50t. hB,r" pn�c�s t S e �i c� C'y. /COUNTX: �i c h mor�r�
PERSON COLLECTING SAMPLES: Er%t NtlrfY17an PHONE NO. R( 152) a91- 3lT11
CERTIFIED LABORATORY: M JC-ro lnmcc _ Lab # ADD TO LISTSERVE? YES ® NO❑ EMAIL: &-t,'c awr
F6-�e ci e-v e. ,_N c _Lab 4
LUvIrE VIOLATIONS? YES ❑ NO O INDUSTRIAL SAND'? X DISCHARGING TO SA WATERS4? ❑
tart A: Wastewater Monitortne Keoulrements
Outfalt N6
Date Saxnp}e
r
llected.
` •
Iota] Flow
:;`
Tots] Spspended::.
:. Solids;
Turbtd�ty'
5ettleabJe Souuls
iH
F eca] Co[rforms .
=:
riiin/dd/yr
11'IG
mg/f
_. NTU
m UI
:..
$tlndard
col/mi
D
�'os
Up Re—LH,
06/ 1 9
/0. a,
.S. 9
<. 10
y, q
„-54,"n
12/ob/1g
-0
<Y.1-7
3.0
< to
3
N
� All mines must monitor WNV discharges for TSS_ Only industrial sand mine discharges are subject to TSS limits. T�
If an effluent limit is exceeded, the pertrittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurems.'nt of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 N' 7U for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Storrnwater Discharge Outfall— Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstrearn and downstream of the discharge.
Only facilities discharging to SA waters are required to monitor For Fecal coliforms.
permit Date: _ Last Revised 01-21-11
/t�GT o2 0/,S f e, 30 S, P,?—D2 0 Page 1 of 2
f. ,^IJ(—

rant A t,ontrnuea: Wastewater Monitoring KequirementS
Date Sample T661l~lorY' Total Suspended `Itii'bidity3:
Oatrall'No 1: f Settleable::Solids: ?p Tee al Cvliforms
S0l13s
-
mm/dd/yr. 7tiCG mg/1. TI [ 1} mlh :. Staiidfi it colrm]
MAIL ORIGLVAL AND ONE COPY OF THIS ANNUAL SUMMARY ELUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT
VIOLATIONS) Y MARCH I OF EACH YEAR TO:
Division of Water Quality
Alin: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate th'e information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons.directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware thqj there are significan enalties for su utting false information, including the possibility of fines and imprisonment for knowing violations.
12p1 8'
(Signature of Permittee) �j� L Tar ccc[s Li r (Date)
Permit Date: 1.12G 10 12.13 14A444 Last Revised 0 1 -2 1 -11
QG7— e? Is- 70 3Q 5,�/� o20,7- 0 Page 2 of 2

f ANNUAL SUMMARY DMR - WASTEWATER 1
11 SEND TO CENTRAL OFFICE* 11
PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
* Report All lhasrewarer discharge monitoring data on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH I of each year. If
you have limit violations, you must also have turned in a Limit Violation MIR to vour local Regional Office within 30 days of receiving sample results from a lab.
CERTIFICATE OF COVERAGE NO. NCG02:b T-
FACILITY NANIE: C
PERSON COLLECTING SAMPLES:
CERTIFIED LABORATORY: ► Lab #
Lab #
LINLIT VIOLATIONS? YES ❑ NOjz
Part A: Wastewater 114onitorinV! Reauirements
SAMPLE COLLECT IO ON YEAR: �� CE11��D
COUNTY: tZc4,�,O
PHONE NO. (it o ) 241 it JA MAR 2 6 2018
ADD TO LISTSERVE? YES ❑ NON EMAIL: GEN I RAL FILES
INDUSTRIAL, SAND'? 9 DISCHARGING TO SA WATERS'? BNR SECTION
Outfall No.
Date Sample
i
Collected
Total Flow
Total Suspended
Solids '
Turbidity3
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
MG
m9/1 ,2
NTU"
min
Standard"
col/ml'.
• 7
4 r
i. Z
P
. i _
y
3.3
r.
no -do
i
A4
Y b a
V,
d
A, .D
.�
'All mines must monitor VNV discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
5tormwater Discharge Out€all. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Permit hate: 1 / 1 /2010-12/3112014
Last Revised 0 1 -2 1 -1 1
Page l of 2

r4

1�
Part A Cotttitttred:.Wastewater b'IonitoritW Re uirements
Date Sample Total Flow Total Suspended Turbidity
Outfall No. tedl Solids` Settleable Solids pH Fecal Cnliforms
Collee
mm/dd/yr MG mg/l''Z NTLJ" ml/i" Standard eol/ml2'4
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH_1 OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
t am aw that there are A cant penalt' for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of P mitre,) (Date)
Permit Date: 1/1/2010-12/31/2014 Last Revised 0 1 -2 1 -11
Page 2 of 2

Fayetteville Division 2592 Hope Mills Road Fayetteville, NC 28306 (910) 864-19201 864-8774 fax
IRAC
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
-�" +/tq/,7
CLIENT
7N1AME&ADDRESS: j�
�Otatr4�eS, l?144 k
3 0( w S ( "'
f1c,� tJC.
PO#r
21
PRDJFCTILOCATION:
w
m
ty„
O
C1
TYPE
OF ANALYSIS
PRESERVATION (CODE)
�'}
�n
1�
CODE: A =None
B=HNO3(pH<2)+<6'C
C = H2SO4 (pH<2) + <6'C
D = NaOH + <6°C
E = ZN Acetate + <6°C
F=HCI
G. = Sodium Thio
CONTACT PERSON: A n
'�� P 14
EMAIL:
r
5
SAMPLED BY:
PHONE NUMBER:
DATE l METHOD OF SHIPMENT:
LAB ID #
SAMPLE
TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEMP'C
RES.
CHLORINE
SULFIDE
'LA s
k
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A
A
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Lab
Relinquished by:
Date
Time
Received by: (Signature)
Date
Time
Relinquished by;
Date
Time
Received by: (Signature)
Dale
Time
3
4
Relinquished by:
Date
Time
Received by: (Signature)
Dale
Time
Jr'
6
ph Field: ph Field:
Temp Field 1: Temp Field 2:
Water Level #1
Water Level #2
Initials
&AITurnaround time'. REGULAR RUSH
Comments or Special Hazards:
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH:

Fayelteville Division .2592 Hope Miils Road 4 Fayetteville, NC 28306 (91 p) 864.19201864-8774 fax
O IC OBACY
CHAIN OF CUSTODY RECORD
PAGE _ I OF 1
CIJENT NAME B ADDRESS:
�co
3 0l S
PO t+ PRn.IECTr LocanoN:
C
J
m
LL.
;O•
#
1
TYPE OF ANALYSIS
t+r�r`SrR'dATlun (CODE)0u�tCr
I
CODE: A =None
B= HNO3 (pH<2) + <6°c
C = H2SO4 (pH<2) + <6'C
D= NaOH +<B'C
E=ZN Acetate+<6'C
F=HC`l
G = Sodium Thic
CONTACTPFft50N; J i
SAMPLEn BY:
2 e �c $
PHONENr1MPtR; U 1�,a
GATSrraETHODOF SHIPMENT:
- - 1 -7
LAB lD M
SAMPLE
TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEMP'C
CHLORINE
SIrLFiDE
k
'3
A
A
A
1
o
11614
X
P�
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3
A
k
A
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1
Lab
RellnquLV,e
Date
Time
Rece by: lSlgnatural
Galt
Tbna
FaVn9mshea by:
Gaffe
Time
elvw by; Igne—k
Gate
ilmt
3
4
e
Tbne
Reserved ay, trggrmleml
Gaffe
e
5
fi
ph FIDId: ph Field: Water Level81
Temp Field 1: Temp Field 2: Water Level #2
Initials-*
Turnaround time: REGULAR RUSH
i
Comments or Special Hazards: a GG
D IG2,
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH:

�gDMICROBAC`�'
Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co Date Reported: 07/19/17
Mr. Steve Mills Project: Storm Water tramples - Semiannual Date Received: 07/13/17
4303 US Hwy I Date Sampled: 07/13/17
Hoffman NC. 28347 Sampled By: Steve/Kelly
Up Stream, grab
K7G0336-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
PH
8.5
pH Units
07/13/17 08:05
Steve/Kelly
PH
Temperature
25.8
°C
07/13/17 08:05
Steve/Kelly
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mL/L
07/13/17 11:11
JR
SM 2540 F-1997
Total Suspended Solids
4.40
mg/L
07/17/17 11:05
TAB
SM 2540 DA997
Turbidity
3.3
NTU
07/13/17 15:29
ELM
SM 2130 B-2001
Down Stream, grab
K7G0336-02
Analyte
Result
Units
Analyzed
Analyzed By
Method Qualifier
Field Data
pl-I
7.8
pH Units
07/13/17 08:50
Steve/Kelly
pH
Temperature
25.5
°C
07/13/17 08:50
Steve/Kelly
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
0.10
mL/L
07/13/17 11:11
JR
SM 2540 F-1997
Total Suspended Solids
9.60
mg/L
07/17/17 11:05
TAB
SM 2540 D-1997
Turbidity
4.1
NTU
07/13/17 15:29
ELM
SM 2130 B-2001
Discharge Point, grab
KX0336-03
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
pH
7.2
pH Units
07/13/17 09:35
Stevc/Kelly
PH
Temperature
29.1
°C
07/13/17 09:35
Steve/Kelly
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mL/L
07/13/17 11:11
JR
SM 2540 F-1997
Total Suspended Solids
6.00
ing1L
07/17/17 11:05
TAB
SM 2540 D-1997
Turbidity
6.1
NTU
07/13/17 15:29
ELM
SM 2130 B-2001
Microbac Laboratories, Inc.
Page 1 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864,8774 f I www.microbac.com

e
�A
Southern Products & Silica Co
Mr. Steve Mills
4303 US Flwy 1
1-Iof man NC, 28347
�DMICROBAC.
Fayetteville Division
Certificate of Analysis
Project: Storm Wafer Samples - Semiannual
QC Batch Run - (Vicrohar Laboratories, Mr. - Fayelleville)
Date Reported: 07/19/17
Date Received: 07/13/17
Date Sampled: 07/13/17
Sampled By: Steve/Kelly
Analytc
Result
Units
Source
RPD
Limit
Total Suspended Solids
33.0
mg/L
K7G0356
10
5
Total Suspended Solids
221
nig/L
K7GO340
6
5
Total Suspended Solids
26.9
mg/L
K7G0306
l
5
Turbidity
6.08
NTU
K7G0336
0.5
5
State Certifications:
NCDNR #11
NCoc)H u37714
Respectfully Submitted
Bonnie K. Sanders, Senior 1'roject Manager
Thank you for your business. We invite'vow-fredback on ow- level afsen-ice ro Yore !lease contact the Division Manager• Hob Dermer ai 910-864-1920 with anv
questions. line man.also coraocr J. Trevor Bnpce. President ar pmTiden( ❑!niicrohar.c•am
Microbac Laboratories, Inc.
Page 2 of 3
2592 Hope Mills Road i Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Fayetteville Division 2592_Hope Mills,Road - Fayetteville, NC. 28306 (910) 864-.1920
-CHAIN OF CUSTODY RECORD
i�su��siiuenoii
q3 ol
co
0
LL
TYPE
OF ANALYSIS
°PRESERVATIQN (CODE)
CODE: A =None
s = HNo3(pH< + .56*c
C. = - H2SO4 (0 H<2) + <P'C
Dl=NaoH4 <6,c�'
E- ZN Acetate +;t6*c
HCI
_G =§odium.Thlo
CONTACT FE
EMIAL
r I.C.4 Lo., V
SAMPLED BY:
PHONE NUMBER. U,
DATE I METHOD OF SHIPMENT.
1_3mG,7,,4
LAS ID
SAMPLE TYPE'
DATE
TIME.
CqMa
- GRAB
'PFt
FLOW Ll
ZMP'C
Tr
�ES_
CHLORINE
SULFIDE
7.
9 '35
X3
A
a
7. _Z
Lab,
Rehitquistted by:
Date,
'lime
Received 'by: fSignature},
Date
Time
2
"linquisb" by:
[Fate
rime
ReGefVe0 by: [Signature]
Date
Time
3
4
Relinquished by: bme
,32"e
Time
Received by; (Signature)
Date
Time
5
I j
ph Field:-. ph Field,
Temp Oieid 1: Temp Field 2-.
Water Level
Water Level #1
#2
lnibals-o..
Turnaround time: REGULAR RUSH
Comments or Soecial Hazards*
iq 1-7
IS'DATA.FOR REG. COMPLIANCE PURPOSE?-
NO— YES WHICH: -
I Page 3 of 3

OMICROBACS
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K7L0692
Southern Products & Silica Co Project Name: Storm Water Samples - Semiannual
Mr. Steve Mills Project I PO Number: NIA
4303 US Hwy 1 Received: 12/18/2017
Hoffman, NC 28347 Reported: 12/21/2017
Analytical Testing Parameters
Client Sample ID: Up Stream, grab
Sample Matrix: Aqueous Collected By: Steve/Gary
Lab Sample ID: K71_0692-01 Collection Date: 12/18/2017 8:00
Wet Chemistry
Result
RL
Units
Note Prepared Analyzed
Lab
Method: SM 2130 B-2011
Turbidity
2.1
0.10
NTU
1218117 1533
FAY
Method: SM 2640 D-2011
Total Suspended Solids
1."
1.20
mg/i_
12/20117 0901
FAY �..
Method: SM 2640 F-1997
r
Setteable Soilds
<0.10
0,10
mUL
12/18/17 1403 12/18/17 1503
FAY
Client Sample ID: Down Stream, grab
Sample Matrix: Aqueous Collected By: Steve/Gary
Lab Sample ID: K71_0692-02 Collection Date: 12/18/2017 9:10
Wet Chemistry
Result
RL
Units
Note Prepared Analyzed
Lab
Method: SM 2130 B-2011
Turbidity
3.8
0.10
NTU
12118/171533
FAY
Method: SM 2640 0-2011
Total Suspended Solids
4.63
1.36
mg/L
12/20/17 0901
FAY
Method: SM 2640 F-1997
Setteable Soilds
<0.10
0.10
mUL
12118/17 1403 12118/17 1503
FAY
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 283061910.864.1920 p I www.microbac.com ;.

1
C
w
1

OMICROBACOD
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K7L0692
Client Sample ID: Discharge, grab
Sample Matrix: Aqueous Collected By: Steve/Gary
Lab Sample ID: K71-0692-03 Collection Date: 12/18/2017 9:30
Wet Chemistry Result
RL
Units
Note Prepared Analyzed
Lab
Method: SM 2130 B-2011
Turbidity 20
0.10
NTU
12118/17 1533
FAY
Method: SM 2540 D-2011
Total Suspended Solids 10.5
1.67
mglL
12120/17 0901
FAY
Method: SM 2540 F-1997
Setteable Soilds <0.10
0.10
mL/L
12118/17 1403 12/18/17 1503
FAY
Laboratory
FAY: Microbac Laboratories, Inc. - Fayetteville
Definitions
Ott: Reporting Limit
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By:
Jeanne Overstreet
Project Manager
[e-mail]
12/21/2017 18:03
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 283061910.864.1920 p I www.microbac.com

L
!:
a
r

ANNUAL SUMMARY DMR ' WASTEWATE R.
SEND TO CENTRAL OFFICE`
PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
* Report Al! Wastewater discharge monitoring data on this form [including !Vo Flow and Na Discharge and Permit Crmit Viofatiorrs) by MARCH 1 of each year. If
you have firiiit violations. you must also have turned in a I imit itiolation Z3MR to Yotir local 12ekional Office within 30 days of receiving sample results from a lab.
CERTIFICATE OF COVERAGE NO. NCG0270— -00 0 SAMPLE COLLECTION YEAR: �o /7
FACILITY NAME: SOLA t.� Fi 4- Iic.A COUNTY:
PERSON COLLECTING SAMPLES: +: / PHONE NO. t q 1 0 ] S - 318 9
CERTIFIED -LABORATORY: ✓t'1 i t 4 Lab # ADD TO LISTSERVE? YES [7 NOD EMAIL: er i4� S! .r C�rar.ve.
-- - T
AlG Lab#�
LIMIT VIOLATIONS? YES ❑ NO JK INDUSTRIAL SAND'? PQ DISCHARGING TO SA WATERSa? ❑
Part A: Wastewater Monitorine Reattirernents
Ofiti'a]1 No ...
Date SailnFle
.�g1IeG[.ed �'.
Tot E low .
dotal its enrlcd :..
� ghds'•
TtthrdxLy;
5eYf1t able rSol"
pH . Fecal Colrfq`rins:;..
inm/ddlYr .
I k
m
tR]/l •tandar�i
tdl%m1
1V�A7
o
cjlar cr
r %
! O
7.
.23
u
113/17
�2_0 1
a
3.3
<.to
s
/ 7
10
7. S'
1, f_�ar �
O /13 17
(�
D
< iD
u S+recce
I/ I g/ / 7
12-0
7Z�owk tr
9-Z /7
20
63
3.g
< to,
: jC_Aa r
/ f' ` l7
/
O.
�z O
t F�
... ...... ..... ...v.. •v. .. .. yr lJ ..wb — ,--- —-I ­l/..J — Jullu .lbill. "v ."vj l tv 1. 1— -
' If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term. .
3-Me-discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: I0 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all takes and reservoirs, and all salt waters; 50 NTUfor all other streams and surface waters. 'Turbidity maybe monitored at the
Stormwater Discharge Outfall.. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
Only facilities discharging to SA waters are required to monitor for Fecal coliforms. -
Permit Date: _ Last Revised 01-21-11
ioln-T Aois fO 3c? Page I of 2

Part A Continued: Wastewater Monitoring Reouirernents
ed
T7atlample Iota714rtFo'tal$gspnd)ilrbid�ly�.
Ou�kfi}I1No . Sett}eabXt�$olras pl= FccaICQl�iorms'
,�ollectci o1�as
. a.
MAIL. ORIGINAL AND ONE COPY OF TIUS ANNUAL SUMMARY (INCLUDING ALL "NO I+LOW', "NO DISCHARGE" & LIMIT
VIOLATIONS) -BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Cmitral Files
1617 Mail Service Center
Raleigh, North. Caxoiina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best 6f my knowledge and belief, true, accurate, and complete.
I am aware that there are signiLca penalty or sit mitting false information, including the possibility of fines and imprisonment for knowing violations_"
(Si airare of i?ermittee) 7 � . /J ! e (Date)
�7AU&oz��8
Permit Date: L Last Revises! 01-2I-1 1
/ QGT o7_0IS 30 SEP oZaz O Page 2 of 2

1R.0
Microbac Laboratories, Inc. W Fayetteville
CERTIFICATE OF ANALYSIS
KiL0692
Southern Products & Silica Co Project Name: Storm Water Samples - Semiannual
Mr. Steve Mills Project 1 PO Number: NIA
4303 US Hwy 1 Received: 1211812017
Hoffman, NC 28347 Reported: 12/21/2017
Analytical Testing Parameters
Client Sample ID: Up Stream, grab
-
Sample Matrix: Aqueous Collected By; StevelGary
Lab Sample ID: K71-0692-01 Collection Date: 12/18/2017 8:00 _ �J
Wet Chemistry
Result
RL
Units
Note Prepared Analyzed
Lab
Method: SM 2130 B-2011
Turbidity
2.1
0.10
NTU
QJ18117 1633
FAY
Method: SM 2540 D-2011
Total Suspended Solids
1.44
1.20
mg1L
12/20/17 0901
FAY
Method: SM 2540 F-1997
Setteable Soilds
<0.10
0.10
mUL
12118/17 1403 12/18/17 1503
FAY
Client Sample ID: Down Stream, grab
Sample Matrix: Aqueous Collected By: Steve/Gary
Lab Sample 1D: K71-0592-02 Collection Date: 12/18/2017 9:10
Wet Chemistry
Result
RL
Units
Note Prepared Analyzed
Lab
Method: SM 2130 B-2011
Turbidity
3.8
0.10
NTU
12/18/17 1533
FAY
Method: SM 2540 D-2011
Total Suspended Solids
4.63
1.36
mg1L
12/2C117 0901
FAY
Method: SM 2540 F-1997
Setteable Soilds
<0.10
0.10
MUL
12118117 1403 12118/17 1503
FAY
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864,1920 p I www.microbac.com

r7''
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K7LOF92
Client Sample ID: Discharge, grab _ ^
Sample Matrix: Aqueous Collected By: StevelGary
Lab Sample ID: . K71-0692-03 Collection Date: 12/18/2017 9:30
Wet Chemistry Result
RL
Units
Note Prepared Analyzed
Lab
Method: SM 2130 B-2011
Turbidity 20
0,10
NTU
12/18/17 1533
FAY
Method: SM 2540 D-2011
Total Suspended Solids 10.5
1,67
mg1L
12120/17 0901
FAY
Method: SM 2540 F-1997
Setteable Soiids <0.10
0.10
mL&
12/18/17 1403 12/18/17 1503
FAY
Laboratory
FAY: Microbac Laboratories, Inc. - Fayetteville
Definitions
RL: Reporting Limit
Report Comments
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted. �@xv—&Ace-. r Gc['i�dZ' ' r-/--
The data and information on this, and other accompanying documents, represents Jeanne Overstfeet
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included. Project Manager
jeanne,[e-mail]
12/21/2017 18:03
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 2830G 1910.864.1920 p I www.microbac.com

�M1J12':R'
Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co Date Reported: 07/19/17
Mr. Steve Mills Project: Storm Water Samples _ Semiannual Date Received: 07/13/17
4303 US Hwy I Date Sampled: 07/13/17
Hoffman NC, 28347 Sampled By: Steve/Kelly
Up Stream, grab
K7G0336-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
pH
8.5
pH Units
07/13/17 08:05
Steve/Kelly
pH
Temperature
25.8
°C
07/13/17 08:05
Steve/Kelly
Field
Analyzed by, Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mL/L
07/13/17 11:11
JR
SM 2540 F-1997
Total Suspended Solids
4.40
mg/L
07/17/17 11:05
TAB
SM 2540 D-1997
Turbidity
3.3
NTU
07/13/17 15-29
ELM
SM 2130 B-2001
Down Stream, grab
K7G0336-02
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
pH
7.8
pH Units
07/13/17 08:50
Steve/Kelly
pH
Temperature
25.5
°C
07/13/17 08:50
Steve/Kelly
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
0.10
mUL
07/13/17 11:11
JR
SM 2540 F-1997
Total Suspended Solids
8,60
mg/L
07/17/17 11:05
TAB
SM 2540 D-1997
Turbidity
4.1
NTU
07/13/17 15:29
ELM
SM 2130 B-2001
Discharge Point, grab
K7G0336-03
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
pH
7.2
pH Units
07/13/17 09:35
Steve/Kelly
pH
Temperature.
29.1
°C
07/13/17 09:35
Steve/Kelly
Field
Analyzed by: Microbac Laboratories, lnc.
- Fayetteville
Settleable Solids
<0.10
mUL
07/13/17 11:11
JR
SM 2540 F-1997
Total Suspended Solids
6.00
mg/L
07/17/17 11:05
TAB
SM 2540 D-1997
Turbidity
6.1
NTU
07/13/17 15:29
ELM
SM 2130 B-2001
Microbac Laboratories, Inc. Page 1 Df 3

R0
Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co Date Reported: 07/19/17
Mr. Steve Mills Project: Storm Water Samples - Semiannual Date Received: 07/13/17
4303 US Rwy 1 Date Sampled: 07/13/17
Hoffman NC, 28347 Sampled By: Steve/Kelly
QC B2tch Run - (Microbac Laboratories, Inc. - Fayetteville)
I Analyte _
Result
Units
Source
RPD
Limit
Total Suspended Solids
33.0
mg/L
K7G0356
EO
5
Total Suspended Solids
221
mg/L
K7G0340
6
5
Total Suspended Solids
26.9
mg/L
K7G0306
1
5
Turbidity
6,08
NIT
K7G0336
0.5
5
State Certifications:
NCDNR #11
NCDQH 437714
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Thank you for your business. WL invite yourfeedback on our level ofservice to you. Please coniac9 the Division :Lfvnager, Rob termer at 910,364• I9?0 with any
questions. You may also c'onrace J. Trevor Boyce, President at pttesidentVfnicrabancam
Microbac Laboratories, Inc. Page 2 of 3

2
Fayetteville Division. 2592 Hope Mills Road -- Fayelteville, NC 28306 [phone] .
CHAIN OF CUSTODY RECORD
K7GO336*
�nu�iA��dsi�
CLIENT NAME R ADDRESS:
xe13,evn t cIh
01 i�5 ! t -
0 f t t o-1 in fv (�-
Post PROJECT I LOCATION:
v l w 011
LU
0
m
0
TYPE OF ANALYSIS
PRESERVATION (CODE)
�`
CODE: A= None
B = HNO3 (pH<2) + <6°C
C = H2SO4 (pH<2) + <6°C
C= NaOH + <6°C
E = ZN Acetate + <6*C
F = ICI
G = Sodium Thio
CONTacTpER50N: I
EMAIL: L
SAMPLEDt3Y:
SDATE!
PHONE NUMBER: it
METHOD OF SHIPMENT:
�(
Lab ID #
SAMPLE TYPE
DATE
GRAB
PH
FLOW
7EMP'C
R£S'
CHLORINE
SULFIDE
f
t
ffTIMECOMA
25.
k
3
a
���.
zIJ
Lab Initials--*
Turnaround time
Relinbuisbed by:
Date
Time
Received by: Slgnaturel
Date
Time
RelinquiSCed by-
Date
Time
Received by: {Signature♦
Date
Time
3
4
Relinquished by:
Data
Time
Received by. (Signature)
Date
Time
5
6L.
:j
ph Field. ph Fiefd:
Temp Field 1: Temp Field 2:
Water LeVel #1
Water Level #2
REGULAR RUSH
Comments or Svecial Hazards: G
i/\T �7
L1 l c L's�JLitk L� v-7' ,
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO— YES WHICH:
f _ Page 3 of 3

Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co Date Reported: 01/24/17
Mr, Bill Price Project: Storm Water Samples - Semiannual Date Received: 01/19/17
4303 US Hwy 1 Date Sampled: 01/19/17
Hoffman NC, 28347 Sampled By- Mills
Up Stream, grab
K7A0653.01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
pH
7.3
pH Units
01/19/17 07:45
Mills
pH
Temperature
14.6
°C
01/19/17 07:45
Mills
Field
Flow
20
gal/min
01/19/17 07A5
Mills
Meter
Analyzed by: Mi=bac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mUL
01/20/17 08:39
JR
SM 2540 F-1997
Total Suspended Solids
4.00
mg/L
01/20/17 10:19
JR
SM 2540 D-1997
Turbidity
3.5
NTU
01/19/17 14:00
DSK
SM 2130 B-2001
Down Stream, grab
K7A0653-02
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
PH
6.8
pH Units
01/19/17 08:20
Mills
pH
Temperature
14.4
°C
01/19/17 08:20
Mills
Field
Flow
20
gal/min
01/19/17 08:20
Mills
Meter
Analyzed by: Microbac Laboratories, Inc
- Fayetteville
Settleable Solids
<0.10
mUL
01/20/17 09:39
JR
SM 2540 F-1997
Total Suspended Solids
4.40
mg/L
01/20/17 10:19
JR
SM 2540 D-1997
Turbidity
4.1
NTU
01/19/17 14:00
DSK
SM 2130 B-2001
Discharge, grab
K7A0653-03
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
PH SA pH Units 01/19/17 09:00 Mills pH
Temperature 13.8 °C 01/19/17 09:00 Mills Field
Flow 10 galimin 01/19/17 09-.00 Mills Meter
Analyzed by: Microbac Laboratories, Inc. - FayetteJille
Settleable Solids <0.10 mUL 01/20/17 09:39 JR SM 2540 F-1997
M" b
tcro ac Laboratories, Inc.
Page 1 of 3

iM1C R 0 BC
Fayetteville Division
Certificate of Analysis
Southern Products & Silica Cc Date Reported: 01/24/17
Mr. Bill Price Project: Storm Water Samples - Semiannual Date Received: 01/19/17
4303 US Hwy. 1 Date Sampled: 01/19/17
Hoffman NC, 28347 Sampled By: Mills
Discharge, grab
K7A0653.03
I Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Total Suspended Solids 7.20 mg/L 01/20/17 10:19 JR SM 2540 D-1997
Turbidity 23 NTU 01/19/17 14:00 DSK SM 2130 B-2001
QC Batch Run - (Microbac Laboratories, Inc. - Fayetteville)
I Analyte
Result
Units
Source
RPD
Limit
Total Suspended Solids
26.0
mg/L
K7A0684
4
5
Total Suspended Solids
468
mg/L
K7A0657
2
5
Total Suspended Solids
64,0
mg/L
K7A0612
6
5
Turbidity
23.0
NTU
K7A0653
0
5
State Certifications:
NCDNR 411
NCDOi-1 #37714
Respectfully Submitted
Bonnic K. Sanders, Senior Project Manager
Thank you for your business. We invite your feedback on our level ofservice to you. Please contact the Division Manager, Rob Denner at 910-364-1920 with any
questions. You rnay also contact J. Trevor Boyce, Presidenl at pmyident(wjnicrubac.cunt
Microbac Laboratories, Inc. Page 2 of 3

Fayetteville Division 2592 Hope Mills Road - Fayetteville, NC 28306 [phone]
PMlIR0FAC
CHAIN OF CUSTODY RECORD
CUENI 1N1AMERADDRE$S: -
15 --) "i k .c ... (:�'°X 45
�i
`fy .3 ( rig 1 -
Po 111ROJECl/LOCAPON.
1P;").3',
w
m
LL
❑
�
TYPE
OF ANALYSIS
PRESERVATION (CODE)-
�
�
11
CODE: A = None
B = HNO3 (pH<2) + <B°C
C = H2SO4 (PH<2) 3 .6`C
D = NaQH + <6°C
= ZN Acetafe t <B'C
F = fAC1
G = Sodium Thio
CONTACT PER3ow j{ , I lr
EMAIL:
t C jr n-4,r i,I- (i 1)e7l • N f
SAMi'tED BY.'
r
:..CA\ �_.
pFtONE NUMBER:
l IAEFROD OF SRIPMENT_
� ' %c? �/ � _ r�,�
LAB ID 9
SAMPLE TYPE
DATE
TIME
COMP
GRAB
PH
SLOW
TEPAP"C
RLS'
CHLORINE
su(SIDE
/('J/�—/}
d
VA
Lab �Jlnitlals—o-
Reilnquislied ny,
PAO
Tlmr
Recrlve0 by, (5lUnti-cl
❑etc
Ttmc 13
j �., t
i- l g -• I
i:.�
wwr cam• 2
1 r 1
,' 6
elingwahed y;
uAtc
Titttt
Receive by: 1131gulurcj
sic
mt
3
A
RnunquisheC by:
RrCe1Ye Ly:( Sig nature)
Oate
lnrr
J
�
ph Field: ph Field:
Temp Field 1: Tamp Field 2:
Water Leval 41
Water Laval #2
"Turnaround time: REGULAR RUSH
I.Iq,I 7
Comments or Special Hazards:
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICK
Page 3 of 3

ANNUAL SUMMARY DMR = WASTEWATER
I - ' SEND TO CENTRAL OFFICE* . 11
PROCESS'MINEIDEWATER.ING WASTEWATER
GENERAL PERNUT NO. NCG020000
* Report All 1-itastewater'discharge monitoring data on this form (including No flow and No Discharge and Permit Limit Violations) by MARCH 1 of each year, If
you have limit violations, you must also have turned in a Limit Violation D?AR to -your local Regional Office within 30 days of receiving sample results from a lab.
CERTI1r ICATE O1{ COVE GE NO. NCG02 4 _0 QQ SAMPLE COLLECTION YEAR: oZ� I (�
EACILIT'4 NAME:. Sores r fv, f r+ d"O( ,s + S- /r'r,_Ca COUNTY.- Z iC_k r" t ice
PERSON COLLECTING SAMPLES: � _S'f ev? 2,1,- / -J _ PHONE NO. /p 28 / - 3 l�
CERTIRIEO LABORATORY:_o b G Lab # ADD TO LISTSERVE? YES ❑ NOVI EMAIL:
a e, iir'// NG Lab #
LIMIT VIOLATIONS? YES ❑ NO B INDUSTRIAL SAND'? ® DISCHARGING TO SA WATERS'? ❑
Part A: Wastewater Monitorint= Reauirements
`.autfatirvo:
�Pi _
Potal�lorv•
Tdtal�nSpCnded`.
7'tir'brd,f�.
�ettlefilale�y�;ds
".. �Ii.. I+lecalCol�rfprzris .
a
m��
�SlanlYd eol/ngi .:....
1 frr
O /17/ 1&
a20
.S/
0.3 /7 / 16
0
7. 6S
(,( Sfrca m
I to /05 / l b
o
6
3.7"
<• 10
S. S
owh sy-,-mw
f0 oS/ (b
o2..0
y. o
< . to
5.50
10,05/ 16
i0
7 <
< . l 0
6 : 1 y
All mines must monitor.WW discharges for "CSS. Only industrial sand mine discharges are subject to TSS limits.
'- if an effluerit limit is exceeded, the permittee is required to institute monthly monitoring for that parameter far the remaining permit term.
3 The discharge shall -not cause an instantaneous measurement of the turbidity of (he receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for ail other streams and surface waters. Turbidity may be monitored at the•
Stormwater Discharge Outfall"- Alternatively, the permit(ee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
Only facilities discharging to SA waters are required to monitor for Fecal colifor-ns"
Permit Date: Last Revised 01.21-11
/DG7oZ4/S fo 30 Page 1 of

Part A Continued: Wastewater Monitoring Reouirements
Date:�iupie �ola�`IOHo2al Sub enid�d hirbtdi .
Ouifatll`iv l 3 _ Seti�ea$1$ ohd pH: decal Cotifo'
col{cCYeti,
Standard coljrol ,
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY INCLUDING ALL "NO FLOW'.' "NO DISCHARGE" & LlMIT
VIOLATIONS) -B Y MARCH I OF EACH YEAR TO:'
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
(919) 807-C379
YO U MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were ,prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persoiks directly responsible for gathering the information, the information.submitted is, to the best df my knowledge and belief, true, accurate, and complete.
I am awa"ate here are significant penaly for submitting false information, including the possibility of fines and imprisonment for knowing violations_"
bC�ir :U /6cGi J �" (Date) pZ 7 AG(G 2191r
Permit Date: Last Revised 01-21-11
f QGT ,Z-o/.S 740 3C7 SE'P aZ O,Z O Page 2 of 2

Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co Date Reported: 10/06/16
Mr. Steve Mills Project Storm Water Samples - Semiannuai Date Received: 10/05/16
4303 US Hwy I Date Sampled: 10/05/16
Hoffman NC, 28347 Sampled By: Mills
Up Stream, grab
K6J0125-01
Analyte Result Units Analyzed Analyzed By Method Quaiifer
Field Data
PH
6.0
pH Units
10/05/16 07:10
Mills
pH
Temperature
21.4
°C
10/05/16 07:10
Mills
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mL/L
10/05/16 11:47
AC
SM 2540 F-1997
Total Suspended Solids
6.00
mg/L
10/05/16 10:40
JR
SM 2540 D-1997
Turbidity
3.7
NTU
10/05/16 15:00
ELM
SM 2130 B-2001
Down Stream, grab
K6J0t25-02
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
PH
5.5
pH Units
10/05/16 07:50
Mills
pH
Temperature
21.3
°C
10/05/16 07:50
Mills
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mUL
10/05/16 11:47
AC
SM 2540 F-1997
Total Suspended Solids
4.00
mg/L
10/05/16 10:40
JR
SM 2540 D-1997
Turbidity
4.0
NTU
10/05/16 15:00
ELM
SM 2130 B-2001
Discharge, grab
K6J0125-03
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
pH
6.1
pH Units
10/05/16 08:25
Mills
pH
Temperature
23A
°C
10/05/16 08:25
Mills
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mL/L
10/05/16 11:47
AC
SM 2540 F-1997
Total Suspended Solids
10.0
mg/L
I0/05/16 10:40
JR
SM 2540 D-1997
Turbidity
7.1
NTU
10/05/16 15:00
ELM
SM 2130 B-2001
Microbac Laboratories, Inc. Page 1 of 3

Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co
Date Reported: 10/06/16
Mr. Steve Mills
Project: Storm Water Samples - Semiannual
Date Received: 10/05/16
4303 US Hwy 1
Date Sampled: 10/05/16
Hoffman NC, 28347
Sampled By: Mills
QC Batch Ran - (Vicrubac Laboratories, lnc. - Fayetteville)
Analyte
Result
Units
Source
RPD Limit
Total Suspended Solids
52.0
mglL
K6J0097
11 5
Total Suspended Solids
46.0
mg/L
K6JO089
19 5
Turbidity
T09
NTU
K6J0125
0.3 5
Flow:
Upstream, 20mg
Downstream, 20mg
Discharge, .01 mg
State Certifications:
NGDNR #11
NCDOH i#37714
Respectfully Submitted
Jeanne Overstreet, Project Manager
Thank you for your business. We invire your feedback on our levul ofservice io you. Please contact the Division .Manager, Rob Derrner ai 910-864-1920 with cony
yaestiuru. You may also comuct J. Trevor Boyce, Presidem aipresidLnt@))ticr&buc.com
nticrubuc.com
Microbac Laboratories, Inc. Page 2 of 3

Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 1910) 864-19201, x
CHAIN OF CUSTODY RECORD
G-, j
i�j o)c i B C�
LV
ffl
CONTACT PERSON:
LrAf J
Ef"L: r
SAMPLED, Y:
_
PhONENUMBER. �j ( p
LL
0
�
DATE IMETHODOFSHPMEMT.-
LAB tD #
SAMPLE TYPE
DATE
TIME
COMP
GRAB
��.
Iz� - _i b
+ f o
y-
`�-�7
ph Field: ph Field: Water Level #1
Temp Field 1: Temp Field 2: Water Level #2
a
K6JU125*
OF
ANALYSIS
PRESERVATION (COC
CODl ; A = None
B = HNO3 (pH<2) + <6°C
C = H2SO4 (pH<2) + <6°C
D = NaOH + a69C
E = ZN Acetate + c6°C
F = HCl
G = Sodium Thio
PH
FLOW
TEM
CHLgRP'C OR 1NE
2z . Ll
b Initials--io-
Turnaround time: REGULAR RUSH
Comments or Special Hazards: q .
Gl V1 G �.
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO— YES WHICH:
Page 3 of 3
SULFIDE

0
Fayetteville Division 2592 Hope Mills Road Fayetteville, NC 28306 (910) 864-19201864-8774 fax
CHAIN OF CUSTODY RECORD
PAGE 1 OF i
CLIENT,1NAME B ADORE S:
3 D 3 us I IJ •
Pori
I%erl
PROJECT/LOCATION:
W
F-
m
u-
O
TYPE
OF ANALYSIS
PRESERVATION (CODE)
CODE: A=None
8 = HNO3 (pH<2) + <6"C
C = H2SO4 (pH< 2) + <6°C
D= NaOH + <6'C
E = ZN Acetate + <6"C
F = HCI
G =Sodium Thio
CONTACT PERSON:
i11
EMAIL:
SAMPLED YY
PAONE NUMBER: I O — 2
DATE 1 METHOD OF SHIPMENT:
r '5
LAB ID
SAMPLE
TYPE
HATE
TIME
COMP
GRAB
PH
FLOW
TEMP'C
RES
CHLORINE
SULFIDE
y-
'3
A
o
�
Lab Initials—lo
Turnaround time:
Relin shed by:
Date
Time
Rece ed by: {Signature)
Date
Time
%a
G` 2
10'&/,l
1165
Relinquished bp.
Date
Rme
Received by: (Slgnamre
Dale
Time
3
4
Rcilnqui5tre4l by:
Date
Time
Received by: (Signature)
Date
lime
rJ
ph Field: ph Field: Water Level 41
Temp Field 1: Tomp Field 2: Water Level #2
REGULAR RUSH
Comments or Special Hazards: `T .
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH:
•t.

Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-19201864-8774 fax
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
CLIENT HAMS d ADDRESS:
3 �3VA5 *J
Po a PROJECT, (-OCATiON:
r-J3 k I
Lu
O
ED
U.
O
TYPE
OF ANALYSIS
PRESERVATION (CODE)
� �
�
h
CODE: A = None
B = HNO3 (pH<2) + <6'C
C = H2SO4 (pH<2) + <6'C
D = NaOH + <6°C
E w ZN Acetate + <6'C
F = HCI
G = sodium Tnio
CONTACT PERSON:
EMAIL:
d
SAMPLED BY;
PHONE NUMBER:
DATE 1 METHOD OF SHIPMENT:
�n
LAEt ID #
SAMPLE TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEMP•C
RES
CHLORINE
SULFIDE
0
Lab Initials—* _
Turnaround time'.
Regnqul5hed by:
Date
Time
Recei by: lsigndturel
Datc
Time
3- 17-/a
jvull
lReCelved
, 1
R0inqu15heJ by:
Date
Time
by: (Slgualur
Date
Time
3
4
Relinquished by
Date
Me
Recaiwed by: (Signature)
Date
Time
5
1 6
ph Field: ph Field:
Temp Field 1: Temp Field 2:
Water Level $1
Water Level #2
REGULAR RUSH
Comments or Special Hazards:
IS DATA FOR REG, COMPLIANCE PURPOSE?
NO YES WHICK
W. C �

I Lawyer, Mike
From: Susan Cornelius <[e-mail]>
r Sent: Wednesday, August 29, 2018 11:06 AM
To: Lawyer, Mike
Subject: [External] Southern Products & Silica Co Water Quality Program
Attachments: 180829110831_OOOl.pdf
Mike,
Thanks again for taking the time to get our program in compliance.
I have attached the documents from 2016 and 2017 as requested.
Please let me know if there is anything you need from us.
Thanks,
Eric
Saran Cornelius
Southern Products & Silica Company
P.O. Box 189
4303 US Hwy 1
Hoffman, NC 28347
[e-mail]
910-281-3189, ext 2
1

STORM WATER -QUALITATIVE MONITORING
STORM SITE
DATE
SAMPLED
COLOR
ODOR
CLARITY
FLOATING
SOLIDS
SUSPENDED
SOLIDS
FOAM
OIL SHEEN
FROSION OR
DEPOSITION
AT THE
OUTFALL
OTHER
OBVIOUS
INDICATORS
OF
STORMWATER
POLLUTION
/
Z,4t4G ! S
aA,1 44"
/✓orbG
Ale, "e-
None-
A"a"e-
/vo n �
23AVfafF
Cen
N`A
Coca r
None
Allne-
/Vo
NonE.
3
Z3'4u&tr
kgk1 Glee-
r
or?C-
,��
tiDn
Nor?
Nnr,e
Total Rainfall (inches):

I ANNUAL SUMMARY DMR - WASTEWATER I
iI SEND TO CENTRAL OFFICE* it
PROCESS MINEMEWATERING WASTEWATER
GENERAL PERMIT No. NCG020000
Report All Wastewater discharge monitoring data on this form (including No Flow and No Discharge and Pernnit Limit Violations) by MARCH I of each year. If
you have limit violations, you must also have turned in a Limit Violation DMR to your local Regional Office within 30 days of receivino yarn le results from a lab.
CERTIFICATE OF COVE GE NO. NCG02�� � SAMPLE COLLFCTIO 'YEAR: a.01(0
FACILITY NAME: rn ?� �'s 5,,. �--,-. �CP.u'N'. Y: 2: ,�.
PERSON COLLECTING SAMPLES: S�cJ� M �} 115 �-CE' k;H -0NO• n 10) t-
CERTIFIED LABORATORY: MIP-C o LjGe Lab # ADD TO LISTSERVE? YES ❑ NOD EMAIL:
Lab # 2 Q 2017
LUMIT VIOLATIONS? YES ❑ NO ❑ CENTRAL g L%IgTRIAL SAND"' ❑ DISCHARGING TO SA WATERS4? ❑
Part A: Wastewater Monitorine Requirements DWR SECTION
Outfall No.
Date Sample
Collected
Total Flaw
Total Suspended
Solids'
Turbidity3
Settleable Solids
pH
a
Fecal Coliforms
-
mni/dd/yr
MG
mg/0'
NTU
InM2
Standard"
collrnl�'
,
3 ! /6
O
6
l� „o Q
b ,
,`lb
or.Jn ��t T
a S Ike
Gr
All mines must monitor R\V discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
' If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 "1'he discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters, 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Out€all. Alternatively, the pertnittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
' Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Permit Date: I/l/2010-12/31/2014 Last Revised 0 1 -2 1 -1 1
Page 1 of 2

Part A Continued: Waslewater Monitoring Re uirements
Outfall No.
Date Sample
Collected
Total Flow
Total Suspended
Solids'
Turhidity'
Settleable Solids
pH
Fecal Coiiforms
mm/dd/yr
MG
mgA1.2
NTUZ-'
m1/12
Standard
col/m12-4
c.0
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFOR,UATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware at there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee) (Date)
Permit Date: 1/112010-12/31/2014
Last Revised 0 1 -2 1 -11
Page 2 of 2

Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 [phone] 1864-8774 fax
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
0 �/l 71x-,�e
CLIENT NAME dADDRESS:
4 i) 7S N J
c
' l
PO#
V r4 �
PROJECT I LOCATION:
I
N
W
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to
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TYPE
OF ANALYSIS
PRESERVATION (CODE)
CODE: A = None
B = HNO3 (pH<2) + <6'C
C = H2SO4 (pH-2) + <6`C
D = NaOH + <6°C
E = ZN Acetate + <6'C
F = HCl
G =Sodium Thin
CONTACT PERSON: y ; II
?
EMAIL:
SAMPLED BY;
PHONE NUMBER: C) I b — '3 i
DATE I METHOD OF SHIPMENT:
LAB ID #
SAMPLE TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEMP°C
CHLORINE
SULFIDE
5)* M
3 -1716
7:3 L.
h
3
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Lab lnitials--Pp�
Relinquished by:
Date
Time
Recci by: (Signature)
Date
Time
3- 17 - /(,
Relinquished by:
Date
Time
Received by: {Signatur
Date
Time
3
4
Relinquished by:
Date
Time
Date
Time
J
lRecesvedby;iSignature)
6
ph Field: ph Field: Water level #1
Temp Field 1: Temp Field 2: Water Level #2
Turnaround time: REGULAR
Comments or Special Hazards:
RUSH
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH:

*MICROBAC"
Fayetteville Division
l
Certificate of Analysis
Southern Products K Silica Co Date Reported: 03/21/16
Mr. Steve Mills Project: Storm Walcr Samples - Semiannual Date Received: 03/17/10
4303 US fhvy t Date Sampled: 03/17/16
HofTinan NC, 28347 Sampled By: Steve/Scott
Up Stream, grab
K6C0725-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
PH
8.4
Pl1 Units
03/17/16 07:30
Stcve/S ott
P11
'temperature
19.2
°C
03/17/16 07:30
Sieve/Scott
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
nil-/L
03/19/16 07:35
AC
SM 25401�-1997
'total Suspended Solids
5.20
mg/L
03/18/16 12:49
CCR
SM 2540 D-1997 S I
"Turbidity
4.0
NTU
03/17/16 16:16
ELM
SM 2130 B-2001
I)own Stream, grab
K6C0725-02
Analyte RCsu11 Units Analyzed Analyzed By Method Qualifier
field Dala
pl-1 7.9 pl1 Units 03/17/16 08:00 Steve/Scott pH
TcmPcraturc 19.4 °C 03/17/16 08:00 Stove/~colt Ficld
Analyzed by: Microbac taboratories, Inc. - Fayetteville
Settleable Solids O.IO MIA, 03/18/16 07:35 AC SM 2540 F-1997
Total Suspended Solids 5.40 mg/1- 03/18/16 12:49 CCR SM 2540 D-ic)97
Turbidity 4.7 NTU 03/17/10 16:16 LLM SM 213013-2001
Discharge Point, grab
K000725-03
I Analyte Result Units Analyzed Analyzed Ry Method Qualifier
Field Data
pl l 7.7 PH Units 03/17/16 08:30 Stcvc/SCOLt PH
Temperature 22.6 °C 03/17/16 08:30 Steve/ScoLL Field
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Settleable Solids 0.10 mlJl. 03/19/16 07:35 AC SM 2340 F-1997
Total Suspended Solids 9.60 mg/L 03/18/16 12:49 CCR SM 2540 D-1997
Turbidity 20 NTU 03/17/16 16:16 1?1M SM 2130 13-2001
Microbac Laboratories, Inc.
Page 1 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f j www.microbac.com

( N)MIC OBAC� -
Fayetteville Division
Certificate of Analysis
SUllthe I) Products R. Silica Cu Date Reported: 03121J16
L1r, Steve Mills Prt)_ject: Storm Water tramples - Semiannual Date Received: 03117/1fi
4303 US I hvy 1 Daic Sampled: 03/17/16
1loAinan NC, 293-17 Sampled By: Steve/Scull
QC- RatCh RIND - (Uirrahac Luhorrrlaries, Inc. - Etryerleeille)
Analyle
Result
Units
Source
RI'D
Limit
'total SusPCndCd SOUCIS
275
mb/L
K6C0748
162
5
'total Suspended Solids
9.21
mglL
K6C4668
27
5
'turbidity
20.4
NTU
K6C0725
0.5
5
Total SLtspended Solids
4.60
mg/L
K6C0725
12
5
Notes and Definitions
S 1 Relulive Percent Uiticrcnce (HPD) outside accepted recovery limits
State Certifications:
NCDNR 411
NCDOli 037714
Respcxtfully Submitted
Bonnie K. Sanders, Senior Project (\tanager
Thank you for your business. V1k' turtle trun fi'rdhuck us rnu' level nJ'.ven'iee trr I'vv. 1'ku.n' [nuttier tilt• Nvimm hhmager, link !Jenne) at J 10446a-1 J 20 n'uh urn'
grreeriom 1,m num nl,tn cunim f .1. T vtoi Royce, !'rew'lent of pre'Ndenl mirrohac.cum
Microbac Laboratories, Inc.
Page 2 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

D`
as
02
M IC ROB AC'
Fayetteville Division 2592 Hope Mills Road Fayetteville, NC 28306 [phone] ,
CHAIN OF CUSTODY RECORD
1*KC1O711511*
0
CLIENT NAME 6 ADDRESS: SS
�`•�,1��'uc1�
L1 3 1771 i 5 '
AoP�C. nay '� t
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W
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0
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TYPE
OF ANALYSIS
PRESERVATION (CODE)
{
v
to
CODE: A=None
fi<2 + <
(p B- - HNO3 ) fi°C
C = H2SO4 (pH<2) + <6°C
D = NaOH + <6°C
E = ZN Acetate + <fi°C
F = HCl
G = Sodium Thio
CONTACT PERSON:
EMAIL: ,, lr
S .� cf1 �, q� r N
SAMPLED BY:
PHONE NUMBER: q I Z) - I
DATE ! METHOD OF SHIPMENT:
3 - I -) -- 4i ke (,C
LAB ID#
SAMPLE TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
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CHLORINE
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uP-51�eA,,9
3 -17-i6
7:3V
3-17 /r
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3
A
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SiEF
Lab
Relinquished by.
Date
Time
Recei by: (Signature)
Date
Time
l%UD
3 -) 7 - / (,
2
�3 1716
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ph Field: ph Field:
Temp Field 1: Temp Field 2:
Water Level #1
Water Level #2
Initials—*
Turnaround time: REGULAR RUJ
r
Comments or Special Hazards:
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH:
61 1°C
[ V. 0 0

F
Fayetteville Division 2592 Hope Mills Road -- Fayetteville, NC 28306 (910) 864-19201864-8774 fax
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
CLIENTNAME11ADDREL
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TYPE
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t
li
_
CODE: A = None
B = HNO3 (pH<2) + <6`C
C = H2SO4 (pH<2) + <6°C
D = NaOH + <6'C
E = zN Acetate + <6`C
F = HClHCI
G =Sodium Thio
CONTACT PERSON:{
✓
a J r�
1 r I
EMAIL:
S f J�_• Vj
SAMPLED BY;
PHONE NUMBER:
DATE! METHOD OF SHIPMENT:
�i�
LAB ID #
SAMPLE
TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEMP'C
L
CHLORINE
CHLORINE
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L15L
a4
91- !l,
Lab Initials
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We
Time
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Data
Time
� 2
10.5-16
1165
Relinquished b :
Date
Time
Received by: (Signature)
Date
Time
3
4
Relinquished by:
Date
Time
Received by: (Signature)
Date
Time
5
6
REGULAR RUSH
Comments or Special Hazards: -1 . S
ph Field: ph Field: Water Level #1 IS DATA FOR REG. COMPLIANCE PURPOSE?
Temp Field 1: Temp Field 2: Water Level 92 NO YES WHICH:

r�
*MICROBAC ;
Fayetteville Division
Certificate of Analysis
Southern Products & Silica Cu bate Reported: 10/06/16
Mr. Steve Mills Project Storm Water Samples - Semiannual bate Received: 10/05/16
4303 US Flwy I Date Sampled: 10/05/16
l lutlhuan NC, 28347 Sampled By: Mills
Up Stream, gra11
K6J0125-01
I Analyle
Result
Units
Analyzed
Analyzed By
Method Qualifier
Field Data
pH
6.0
PFI Units
10/05/16 07:10
Mills
pH
Temperature
21.4
°C
10/05/16 07:10
Mills
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mL/L
10/05/t6 11:47
AC
SM 2540 F-1997
Total Suspended Solids
600
mg/L
10/05/16 10:40
JR
SM 25401.E-1997
Turbidity
3.7
NTU
10/05/16 15:00
ELM
SM 2130 B-2001
Down Stream, grab
K6J0125-02
Analytc Result Units Analyzed Analyzed By Method Qualifier
Field Data
pH
5.5
Temperature
21.3
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
Total Suspended Solids
4.00
Turbidity
4.0
P11-1 Units
10/05/16 07:50
Mills
pH
°C
10/05/16 07:50
Mills
Field
mI./L
10/05/16 11:47
AC
SM 2540 F-1997
mg/L
10/05/16 10:40
JR
SM 2540 D-1997
NTU
10/05/16 15:00
ELM
SM 2130 13-2001
Discharge, grab
KfiJ0125.03
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
PVT
6,1
pH Units
10/05/16 W25
Mills
PH
Temperature
23.4
°C
10/05/16 09:25
IVIiIIs
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mL/L
10/05/16 11:47
AC
SM 2540 1=-1997
Total Suspended Solids
10.0
mg/L
10/05/16 10:40
JR
SM 2540 D-1997
Turbidity
TI
NTU
10/05/16 15:00
I;LM
SM 2130 B-2001
Microbac Laboratories, Inc.
Page 1 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Southern Products 8r. Silica Co
Mr. Steve Mills
4303 US Hwy 1
I lolTtnan NC, 28347
OMICROBAC"
Fayetteville Division
Certificate of Analysis
Pru.11ct: Sturm Haler Samples - Semiannual
QC Batch Run - (dtirrahac Laharalariev, Me. - Farelleville)
Date Rcpurtcd: 10/06/16
Date Received: 10/05/16
Date SatZiplcd: 10/05/16
Sampled By: Mills
{ Analyte
Result
Units
Soul -cc
RPD Limit
Total Suspended Solids
52.i1
mg/L
K6J0097
11 5
'total Suspended Solids
46.0
mb/1,
K6J0089
19 5
Turbidity
7.09
NTU
K6J0125
0.3 5
Flaw:
Upstream, 20mg
Downstream, 20mg
Discharge, .01 mg
State Ccnifications:
NCONR All
NCDO11 417714
Re\\\\spectiitlly Subiniillttccd
Jcannc ()verstrect. Project Managcr
Thank you for your business. Wr invile I'raer, ferdbark nr! am level a4 wavier on von. Pleaw comer! the Divdciurr blmrager, Rd, Darner w 9llbh64-192tl widr anp
qus(ina.v, lour nuav also rourart J. 1i'evor Boyre. President al previdenrcaarirrnher.rom
Microbac Laboratories, Inc. Page 2 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1 910.864.1920 p 1910.864.8774 f i www.microbac.com

.a
rY Fayetteville Division 2592 Hope Mills Road -, Fayetteville, NC 28306 (910)'864-1920 ! I
CHAIN OF CUSTODY RECORD
'K6J0125'
1,101111-111111111
cuEJIT�1NAm63 Aa ,b�
11.C.
-L B 3 `i )
Po.
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PHOJECT 1 LOCAn6H;
TYPE
OF ANALYSIS-
PRESERVATION(CODE)
'
CODE: A = None
t3 = 3 €ND3 ;pF{<Zt + <g•C
C=H250a(pH<2)+<VC
0 = N8019 + <6'C
E = ZN Aoelate r <6°C
F=iiCI
G = SDdium Thio
L
CONTACTPEMN:5 7 Gc•L >1t f Ill
7
EMAIL: l
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samP/L}EfaJpY
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PHONE NWANER: l a D L
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DATEIMETHOD OrSFUP MENT:
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TYPE
DATE
TIME
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PH
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Comments or Special Hazards: .
4�T
ph Nold: ph Raid:. water Level sty IS DATA FOR REG. COMPLIANCE PURPOSE?
Temp Field is Tam_ p Feld 2: Water Level 92 NO YES WHICH:
Page 3 of 3

Fayetteville Division 2592 Hope Mills Road - Fayetteville, NC 28306 [phone] / 864-8774 fax
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
�m I11Y l:7
CLIENT NAME SADDRESS:
?t, XA
q3,)( � 5 ) � �
l�iF�oq �'C •
Po
rik I
PROJECT I LOCATION:
J
�
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Il
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it
TYPE
OF ANALYSIS
PRESERVATION (CODE)
-�
K
'
�
In
�
l�
CODE: A =None
8 = HNO3 (pH<2) + <6°C
C = H2SO4 (pH<2) + <6*C
D = NaOH + <6°C
IF- ZN Acetate + <6°C
F = HCI
IS= Sodium Thio
CONTACT PERSON: J� `
j1 _ �tJ jl 1
EMAIL:
5 �C1e r �r'j P�•
SAMPLED BY:
5�
PHONE NUMBER:
DATE I METHOD OF SHIPMENT:
1 - 19 -/ -7 r�
LAS ID #
SAMPLE
TYPE
DATE
TIME
COMP
GRAS
PH
FLOW
TEMP •C
RES.
CHLORINE
SULFIDE
2Y1
2
6
Lab
Relinquished by:
Date
Time
Received by: (Signature)
Date
Tlme
2
Relinquished by:
Date
Time
Received by: (Signature)
Date
Time
3
4
Relinquished by:
Date
Time
Received by; (Signature)
Date
Time
51
1 6
ph Field: ph Field:
Tamp Field 1: Temp Field 2:
Water Level #1
Water Level 92
In itials--ji.
UlTurnaround time: REGULAR
ttrgd l
Comments or Special Hazards:
RUSH
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH:
�oC

(VMICROBAC 1`�f
Fayetteville Division /
Certificate of Analysis
Southern Products & Silica Co Date Reported: 01/24/17
Mr. Bill Price Project: Storm WaterSamples-Semiannual Date Received O1/ /17
4303 US I Iwy I Date Sampled: 1119117
Hoffman NC, 28347 1 Sampled 13y: Mills
Up Stream, grab
K7AO653-01
I Analytc
Result
Units
Analyzed
Analyzed By
Method Qualifier 4
Field Data
pH
7.3
p1i Units
01/19/17 07:45
Mills
pH
Temperature
14.6
°C
01/19/17 07:45
Mills
Field
Flow.
20
gal/Inin
01/19/17 07:45
Mills
Meter
Analyzed by: Microbac Laboratories, Inc, - Fayetteville
SCtticablC Solids <0.10 ml./L 01/20/17 08:39 JR SM 2540 F-1997
Total Suspended Solids 4.00 mb/L 01/20/17 10:19 JR SM 2540 D-1997
Turbidity 3.5 NTU 01/19/17 14:00 DSK SM 2130 13-2001
Down Stream, grab
K7AO653-02
Analytc Result Units Analyzed Analyzed By Method Qualifer
Field Data
pli
6.9
pl-I Units
01/19/17 W20
Mills
PH
hC1)1pCra1Urc
14.4
°C
01/19/17 08:20
Mills
Field
Flow
20
gal/Inin
01/19/17 08:20
Mills
Mctcr
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mL/L
01/20/17 08:39
JR
SM 2540 F-1997
Total Suspended Solids
4.40
mg/L
01/20/17 10:19
JR
SM 2540 D-1997
Turbidity
4.1
NTU
01/19/17 14:00
DSK
SM 2130 B-2001
Discharge, grab
K7AO653-03
Analyte
Result
Units
Analyzed
Analyzed By
Method Qualifier
Field Dala
PH
8.1
pH Units
01/19/17 09:00
Mills
PH
T(1rnperafurc
13.8
Oc
01/19/17 09:00
Mills
Field
Flow
10
gal/min
01/19/17 09:00
Mills
Meter
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Settleable Solids <0.10 mL/L 01/20/17 08:39 JR SM 2540 F-1997
Microbac Laboratories, Inc.
Page 1 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

SautIM11 Products & Silica Co
Mr. Bill Pricc
4303 US Hwy I
Hoffinan NC, 28347
(�)MICROBAC"
Fayetteville Division
Certificate of Analysis
Project: Storm 11'a(er Samples - Semiannual
Discharge, gral)
K7AO053-03
Date Reported: 01/24/17
Date deceived: 01/19/17
Date Saritpled: 01/19/17
Sampled By: Mills
I Analytc Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Total Suspended Solids 7.20 mg/L 01/20/17 10:19 JR SM 2540 D-1997
Turbidity 23 NTU 01/19/17 14:00 DSK SM 2130 B-2001
QC Batch Ron - (Werobac Laboratories, Inc. - Faye!lerille)
Analytc
Result
Uni€s
Source
RPD
Limit
Total Suspended Solids
26.0
mg/L
K7A0684
4
5
Total Suspendctl Solids
469
mg/L
K7AO657
2
5
Total Suspended Solids
64.0
mg/1-
K7A0612
6
5
Turbidity
23.0
NTU
K7A0653
0
5
Stale Certifications-
NCDNIt #11
NCD011 41377W
Respectrully Submitted
d��
kc'u-�
Bonnie K. Sanders, Senior Project Manager
Thank you for your business. IN invilr ror+r, fcerllruak orr our lcrcl q}',renice m � ou Pleave cuntart the Division Manager, Hob Dernicr u! 910-Rb4-1920 with any
quesliorm liar nu+ti' ulso rnrBuc! ,1, Tnar»r Ngrre, Presidrnl ul prrs+ilrnr u;nricruhm:crnn
Microbac Laboratories, Inc.
Page 2 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Fayetteville Division 2592 Hope Mills Road Fayetteville, NC 28306 (910) 864-19201
CHAIN OF CUSTODY RECORD
!�A�u�iH�Aa
[.€EN t MAM E a ADDRESS:
3 ( {a 5 !
PO
3 p
PROJECT 4 LOCAT€OW
TYPE
OF ANALYSIS
_ PRESERVATION(CODEl
VA
l ,
CODE., A = None
8 = HNO3 (pHt2) + <6'C
C = H2SO4 (pH<2) + 46-C
D - NaOH + <6°C
E = ZN Acetate + <6°C
F = HCI
G = Sodium Thi€]
COWACT PERSOR:
EUMLL
T i,t-lG' fb' Sr' � ��1 (� - 0
SAMPLED BY:
pHpN£ HUNGER:
tE.
Q
PATE / METMop OF SHIPMENT.
BIDE
SAMPLE TYPE
DATE
TIME
COMP
ORAa
PM
FLOW
I TEMP'C
RES"
CKLORiM£
SULFIDE
3 03
q.
Late
Raiu%qutahed try.
Dtla
T€me
Re Mwld 1,y.,,541.ww)
Drip
time
`
?At�iC�LY 2
eW+ glgahea by;
ao"M
Dme
mss
�
4
k*4imtufthed by;
a
ima
acary wta
Data
Tbne
6
ph Flald: ph Field:
Temp Hold 1s Temp Field 2:
Water Level 01
Water Level 92
�nialals-
Turnaround time: REGULAR_ RUSH
Comments or SDecial Hazards:
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH: -
�ae
Page 3 of 3

ANNUAL SUMMARY DMR -WASTEWATER
II SEND TO CENTRAL OFFICE*
PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
* Report All Wastewater discharge monitoring data on this form (including No Flow and No Discharge and Permit Lirnit Violations) by MARCH I of each year. If
you have limit violations, you must also have turned in a Limit Violation DMR to your local Regional Office within 30 days of receiving sample results from a lab.
CERTIFICATE OF COVERAGE NO. NCG02 �? � SAMPLE COL .ECTI N YEAR: i�_I T
FACILITY NAA'I1:: �J C � f c � I t- COUNTY: IZ.ekr�+x1�
PERSON COLLECTING SAMPLES: e— M;11 j:11 PHONE NO. ( 1 O - 31
CERTIFIED LABORATORY: C Lab # ADD TO LISTSERVE? YES ❑ NTO❑ EMAIL: S�x�k ��gticl • f{I j
It .C- Lab #
LIMIT VIOLATIONS? YES ❑ O>T INDUSTRIAL SAND? X DISCHARGING TO SA WATERS"? ❑
Part A: Wastew- ter Monitoring Re uiremenls
Outfall No.
Date Sample
Collected
Total Flow
Total Suspended
Solids'
Turbiditv3
Settleable Solids
pH
Fecal Coliforms
-
moVdd/yr
MG
mg/I 'Z
NTUZ'
MIA2
Standard`
covmlZ' .
ca /t• �
mot.. 1 ' t0 - l
D wt
r
`7
o - 13
fe. 3 T
'
I- —i S
. D i .r�
i
SI &
0 r 1-,)
. G!
RECEI
u.Psfa.e,��•
6 - - /s
Rage
ao
- �
a � 1 0
6 •
ou9.�f
• tr
2.0 ALf
6/, O
4/r 9
a 10
-,/
l
�+�J r
0,
�•
6
7 r
/M.
/ t.'
J i
.�rr,�
1 V
QWR SE
y 1 1
S
3,
'.
I t5
ao
y o
b _
/(,
o
' All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit terns.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stortnwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
V E D
W6
=IL ES
TIO►v
Pcrmit slate: 1/t/2010-12/31/2014 Last Revised 01-21-11
Page 1 of 2

�� ar ..
.� - � � -
ti .
r. 'J , _ls
. _ .1.

Part A Continued: Wastewater [Monitoring Requirements
Outfall No.
Date'Sample
Collected
Total Flow
Total Suspended
Solids'
Turbidity
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
DIG
mg/l1.2
NTU2"3
mI/IZ
Standard
cal/ml"'a
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT
_VIOLATIONS? BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN' THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penal ti for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee) (Date)
Permit Date: 1/1/2010-12/31/2014 Last Revised 0 1 -2 1 -11
Page 2 of 2

01
r OMICROBAG," �
Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co Date Reported: 12/16/15
Mr. Steve Mills Project: Storm Water Samples - Semiannual Date Received: 12/08/15
4303 US Hwy 1 Date Sampled: 12/08/15
Hoffman NC, 28347 Sampled By: Bill/Steve
Up Stream, grab
K5L0354-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
pH
7.5
pH Units
12/08/15 09:30 ,
Bill/Steve
pH
Temperature
19.5
°C
12/08/15 09:30
Bill/Steve
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mL/L
12/09/15 10:18
SW
SM 2540 F-1997
Total Suspended Solids
2.00
mg/L
12/10/15 13:23
SW
'SM 2540 D-1997
Turbidity
2.7
NTU
12/10/15 09:25
DSK
SM 2130 B-2001
Down Stream, grab
K5L0354-02
I_ Analyte Result Units Analyzed Analyzed By _ Method Qualifier
Field Data
PH 6.9 pH Units 12/08/15 09:50 Bill/Steve pH
Temperature 15.8 °C 12/08/15 09:50 Bill/Steve Field
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Settleable Solids <0,10 mL/L 12./09/15 10:18 SW SM 2540 F-1997
Total Suspended Solids 1.80 mg/L 12/10/15 13:23 Sw SM 2540 D-1997
Turbidity 2.8 NTU 12/10/15 09.25 DSK SM 2130 B-2001
Discharge Point, grab
K5L0354-03
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
pH
7.5
pl-1 Units
12/08/15
10:15
Bill/Steve
pH
Temperature
15.2
°C
12/08/15
10:15
Bill/Steve
Field
Analyzed by: V+Crobac Laboratories, Inc.
• Fayetteville
.Settleable Solids
<0'10
mL/L
12/09/15
10:18
SW
SM 2540 F-1997
Total Suspended Solids
5.67
mg/L
12/10/15
13:23
Sw
SM 2540 D-1997
Turbidity
16
NTU
12/10/15
09:25
DSK.
SM 2130 B-2001
Microbac Laboratories, Inc. Page 1 of 3
2592 Hope Mills Roar! I Fayetteville, NC 28306 1910,864.1920 p 1 910.864,8774 f t www.microbac.com

IIIA
�4 s �.
�n�C�o�cs�va

(!�iMICROBAC`",
Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co
Date Reported: 12/16/15
Mr. Steve Mills
Project: Storm Water Samples - Semiannual
Date Received: 12/08/15
4303 US Hwy 1
Date Sampled: 12/'08/15
Hoffman NC, 28347
Sampled By: Bill/Steve
QC Batch Run - (Mlcrobac Labaratories, Inc, - Fayetteville)
Analyte
Result
Units
Source
RPD Limit
Total Suspended Solids
8.00
mg/L
K5L0449
0
5
Total Suspended Solids
24.0
mg/L
K5L0389
0
5
Total Suspended Solids
54.0
nig/L
K5L0362
0
5
Turbidity
16.1
NTU
K5L0354
0.6
5
Stale Certifications:
NCDNR HI
NCDOH #37714
Respectfully Submitted
Jeanne Overstreet, Project Manager
Thank you for your business. We invite yourjeedback on our level ojservicc to you. Pleuse cuniact the Division Manager, Rob Dermer ar 910.864-1920 with aay
questions. You pray also contact J. Trevor Boyce, Presiders at presidenr@*[onbac.conr
Microbac Laboratories, Inc.
Page 2 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1910,864.1920 p 1910,864.8774 f I www.microbac.com

Southern Pruducls & Silica Co
Mr. Scott Bladshire
4303 US Ilwy I
Hoftinan NC, 28347
Fayetteville Division
Certificate of Analysis
Project: Storm WnterSamples
UP Stream
K5G 1053-01
Date Reported: 03/06/15
Date Received: 07/79115
Date Sampled: 07/29/15
Sampled By: Price
I Analyte
Result _
_ Units
Analyzed
w Aualyzed By
Method Qualifier
Field Data
PH
7.4
Pfl Units
07/29/15 Q7:30
Price
pH
Temperature
26.6
°C
07/29115 07:30
Price
Field
Flow
20
gal/min
07/29/15 07:30
Price
Meter
Analyzed by: Mlcrotec Laboratorig, loC. - Fayetteville
Settleable Solids <0,10 mLlL 07130/15 08:08 DSK SM 2540 F•1997
Total Suspended Solids 1.43 mglL 07/30/15 10:15 NCH SM 2540 D-1997
Turbidity 3.5 NTU 07/30/15 i L15 DSK SM 2130 B-2001
Down Stream
1<5G 1053-02
i Annivte
Result
Units
Analyzed _
Analyzed By
Method Qualifier
Field Data
PH
6.9
pH Units
07/29/15 09:00
Price
PH
-Temperature
26.9
• °C
07/29/15 09:00
Price
Field
Flow
20
gallmin
07/29/15 09:00
Price
Meter
Analyzed by: MlCmWc taboratoril W. •
Fay�ville
SelticableSolids
<0,10
l
07/30/15 08:08
DSK
SM2540E-1997
Total Suspended Solids
1.71
ills/L
07/30/15 10:15
NCH
SM 2540 D-1997 51
Turbidity
4.1
NTU
07130/15 I IA5
DSK
SM 2130 B-2001
Discharge Point
K501053.03
Analyte _
Result _
Units
Analyzed
Analyzed By
Method Qualifier
Field Data
PH
7.6
PH Units
. 07/29/15 OTAO
Price
P11
Temperature
23.8
°C
07/29/15 07:00
Price
Field
Flow
.01
gallmin
07/29/15 07:00
• Price
Meter
AnaWed by: Microbac Laboratone5, IrK. - Fayetteville
Settleable Solids <0.10 mLIL 07/30/15 08:08 DSK SN1 2540 F-1997
Mictobac Laboratories. Inc.
Page 1 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.6774 If I www,microbac.com

Southern Products & Silica Co
),It. Scott Hradshhe
4203 US flwy I
WITmdri NC, 28347
Fayetteville Division
Certificate of Analysis
Projecl: Storm Wito Samples
Discliarge Point
K5(31053-03
Date Reported: 09/06/15
Dale Received: 07/29/15
Date Swnpied: 07/29/13
Sampled By; Price
4 Analyte
Result
Units Analyzed
Analyzed By
Method
Qualifier J
Analyzed by: tlkrotiac tabomones, Inc. - FayettevOe
Tblul Suspended Solids
2.50
rng/L 07/30,'15 10:15
NCft
SNI 2540 D-1997
Turbidity
15
NTU 07/30/15 11:15
DSK
S1vl 2130 B-2001
QC Batch Run - (ar;r wb„�a�bu.n,r,r;r•r, nrr.-f'grrnndrrr)
Analyze
Resell
Units
Source
RPD
Limit
Turbidity
3,46
NTU
KSG1053
0
5
Total Suspended Solids
2.57
Ing/L
K5G 1053
40
5
tNote.c and Definitions
SI Relative percent I)JI' ence (RPD) ouisideaccepted recovery limits
w Cerfifcations:
DNR #11
DOH 017711
Respectfully Submitted
1
• Bonnie K. Senders, Senior Project Mnnager
nk you for your business. Wr unmr i nvr (redbrrck w, nur rnrl ojsavyrc ro rnu Phase c„nrt,ce die UiwioOd.,mgm Rob Drnnrr w 9i (X864-1920 o Irb a y
dons. }'rnr nrm n!m ra,+urr J. 7stronr Rntx e, Araidan rrr rvertrlenr n'minobxra„
mc:rv)ac 1,oborato+iest, Inc.
Page 2 of 3
2592 Hope Mills Road I Fayetteville, rVC 28306 1910.864.1920 p 1910,864.8774 IF I www.mlcrobac.com

Southern Products & Silica Co
Mr, Bill Price
4303 US Hwy 1
Hoffman NC, 28347
�VMICROBAC-'
Fayetteville Division
Certificate of Analysis
Project: Storm Water Samples
Discharge Point
K5A0539-03
Date Reported: 01/26/15
Date Received: 01/20/15
Date Sampled: 01/20/15
Sampled By: Bill/Scott
!_ Analyte Result Units Analyzed Analyzed By Method Qualifier f
Analyzed by: Microbac Laboratorles, Inc. - Fayetteville
Total Suspended Solids 18,0 mg/L 01/22/15 14:00 SW SM 2540 D-1997
Turbidity 46 N"1'U 01/21/15 09:20 DSK SM 2130 B-2001
QC Batch Run - (AticrobacLaborarories,Inc. -Fayetteville)
Analyte
Result
Units
Source
RPD
Limit
Total Suspended Solids
22.0
mg/L
K5A0606
0
5
Total Suspended Solids
6.80
mg/L
K5A0650
27
5
Total Suspended Solids
60.0
mg/L
K5A0602
7
5
Total Suspended Solids
5.50
mg/L
K5A0521
10
5
Total Suspended Solids
2.25
mg/L
K5A0483
0
5
Turbidity
9.56
NTU
K5A0558
0.4
5
Total Suspended Solids
2.40
mg/L
K5A0539
15
5
Notes and Definitions
Si Relative Percent Difference (RPD) outside accepted recovery limits
State Certifications:
NCDNR #11
NCDOII #37714
Rcspectfuliy Submitted
Bonnie K. Sanders, Senior Project Manager
Thank you for your business. We invite your feedback on our level ofsen ice ro yon, Please contact die Division Manager, Rob Denver of 910-664.1920 with any
gaestiona, Yon mqv also contact J, Tirvar Boyce, Presnient at president niierobac. cony
Microbac Laboratories, Inc. page 2 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

{ MICROBAC�`1
Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co Date Reported: 01/26/15
Mr. Bill Price Project: Storm Water Samples Date Received: 01/20/15
4303 US Hwy 1 Date Sampled: 01/20/15
Hoffman NC, 29347 Sampled By; Bill/Scott
Up Stream
K5A0539-01
Analyte
Result
Units
Analyzed
Analyzed By
Method Qualifier
4
yield Data
PH
7.4
p}l Units
01/20/15 09:30 .'
BRUScott
pI-I
Temperature
12.1
°C
01/20/15 09:30
Bill/Scott
Field
Flow
20
gal/min
01/20/15 09:30
Bill/Scott
Meter
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
ml/L
01/21/15 08:39
DSK
SM 2540 F-1997
Total Suspended Solids
2,80
mglL
01/22/15 10:15
SW
SM 2540 D-1997 Sl
Turbidity
2.7
NTU
01/21/15 09:20
DSK
SM 2130 B-2001
Down Stream
K5A0539-02
Result Units Analyzed
Method Qualifier
Field Data
PH
8.4
pH Units
01/20/15 10:15
Bill/Scott
pH
Temperature
15.3
°C
01/20/15 10:15
Bill/Scott
Field
Flow
20
gal/min
01/20/15 10:15
Bill/Scott
Meter
Analyzed by: Microbac Laboratories, Inc.
• Fayetteville
Settleable Solids
<0.10
mIIL
01/21/15 08:39
DSK
SM 2540 F-1997
Total Suspended Solids
1.60
mg/L
01/22/15 14:00
SW
SM 2540 D-1997
Turbidity
17
NTU
01/21/15 09:20
DSK
SM 2130 B-2001
Discharge Point
K5A0539-03
I Analyte
Result
Units
Analyzed
Analyzed By
Method Qualifier
Fleld Data
PH
8.0
pH Units
01/20/15 11:15
Bill/Scott
pH
Temperature
13.9
°C
01/20/15 11:15
Bill/Scott
Field
Flow
.01
gal/min
01/20/15 11:15
Bill/Scott
Meter
Analyzed by: Microbac Laboratories, Inc. •. Fayetteville
Settleable Solids - <0.10 mIIL 01/21/15 08:39 DSK SM 2540 F-1997
Microbac Laboratories, Inc.
Page if of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1 910,864.1920 p 1 910.864.8774 f I www.microbac.com

. 2015(WEO) 09:47 t4ICROBAC LABORATORIES (FRX)9108648774 P.002/00d
�• �DM[CROBACM
Fayetteville Divisinn
Certificate of Analysis
tinwllcrn products & Silirm Go f7atc Rcporzcd: Uf,r! Sr! 5
Mr, frill Price Prnjcat; 8rnrm Witlor',salup]es Patc.ltecc1vcd: 06/09/15
ow us I•luy 1 IJatc STImplcd; 06/09115
F1nfTrrlsm NC, 2H.W tinmpled fry: Pricc
Up Stream
K5Nn3a(,-Irl
Analvic ],cSttlt l.lnits Annlvred An:rlv7e01 kv N1C0100 011a1irllev
Field data
p)i
5.7
pH Units
06/09/15 07:30 '
Price
pH
Tclriperaturc
24.3
°C
06/09/15 07:30
Pricc
Field
Flaw
20
gil/Min
OC1/09/15 07;30
Pricc
Mctcr
Analyzed by: Mierobm Laborototics, Inc.
• Favettcv0tl
Sctticablc Solid,
•'.O,10
ml/L
06/10/15 13:35
A4Lw
SM 2540 F-1997 .
Ta1al Susprmflud Solids
.9.00
mg11.
06110/15 13:00
MIN
SM 2540 D-1997
'rurllidity
5.0
NI•U
C1WI(/15 16:20
USK
5M 2130 H-2001
Dntivn tiircam
MR346-02
AimlylC
HCF111L
1.)niLc
Anrilvzcd
Ausrly7crl iw
Mzfllod Om-klilicr
Fleld Pars
01•1
5.2
pFl LJrlitS
06M9115 N:UO
!'rice
PH
TemperaLurc
23.2
°C
06/09/15 Uh:Ou
Pricc
Field
Flow
20
gal/shin
06/09/15 08:00
Price
Mctcr
Analyzed bys Microbat L.ibontarlm Inc, - Nycrmvillr�
SctOtmble Solids
-:n,10
I11I/1..
'06/10/15 13:35
Mf W
$M 25.30 f-1997
ToLal Su,tirendad SOlidS
4,80
I1tL'IL,
06/10/15 13:00
MLW
SM 2540 D-1997
Turbidity
4.9
NTL1
06/10/15 16:20
DSK
SM 2130 B-2001
Discharge !'hint
K5F 03a 6.03
Analylc
KCSlrtt
1,41its
Arlaly7Cd
Atlply7Cd Hy
Mctllnd ()trsilitiCr
Fl�fd n
PH
6.5
PH Units
06/09/15 MR
Pricu
PH
T011113cmtnre
23.2
°c
06/09/15 OR:30
Pricc
Field
Flow
.01
gal/min
06/09/15 08,30
Price
Metcr
Analyzed by: Microbat Ubaratorlcs, Inc. - Fayetteville
Settleable Solids
-W.10
ml1L
ON10115 13:35
N1LW
SM 2540 F-1997
Microbac
Laboratories, Inc,
2592 Hope Mills Road
jFayetteville,
NC 28306
1910.864,1920 p
w
1910.864.8774 f �ww.
p �� of
-

f' 1•-2015(WE 0) 09! 47
r
MiCROBRC LRBORRTORIES
(FRX)9108648774 P.003/004
OMICROBACO
Fayetteville Division
Cer-tificate of Analysis
Southern Pruduas & Siliuu Co Du[C Reported: 06/15/15
Mr. Bill Price Prn!jed: Storm Winer Surnplerr Dale RveuiVCd. W09/15
4303 US Ilwy I Delp Sampled: 06/09/15
1luffntau NC, 26347 Sampled By: Price
Dischm-ge Point
1{5FIJ31(•lJ3
Aualyle
Result
Units
AnalYzcd Analyzcd By
Mcthod
01falifler
Analy" by: 1'llrrobor iitborutarir,;:,
Inc, - T iyrJIm'Ilho
Tu(;ii Suspended Solid?;
:3.60
mgJL
06/10/15 13A)0 ML`V
Slvi 2540 D-1997
Turbidity
16
NTU
06/10/15 1610 DSK
5M 2130 B-2001
QC Rarch Run (Afirrahur.
fahorumrir.r, fur. • rayrrfeville)
I.—lyir
Result
lj[tir9
Snurce
kill)
Unlit.
Tott{i SuspmIcil ScilJ.i
1,75
mgfr.
K5F035.1
55
S
Total Suvpendcd Solids
2.50
mg/L
K5R0324
0
5
Turbidity
15.9
NTU
K5F0346
0
5
Skdc Cur ificadf)w
NC•DNR fill
NCDOH H37714
KCspccRllIly StIllrni(CO
rcannc iwcrs[rcc[, Prlijee[ hL'u,ui;ci
Thank you Ior your bushinss. Wr nnarr r+�urjiwdhurk nn nur' lrtl+$ ufavr w,'r ill i nu. PIrtU rr i nl,rur'r rllr. Ihs Trims :1{ rnaF rr} ltuh !1cinl ', u7 Y!!1 •N(ff•!V: R M iIfI u,ry
p(e,gh„re. )is It mIrry nrin onmiaw J Pmrlr lrnvnv, Amide-rr w p r,•.nrhoogir) I x I. vII Aj..<'dnl
Microbac Laboratories, Inc.
Page 2 of 3
2592 Hope Mills Road-]1F yetteville, NC 28306 1910.864.1920 p 1910.864.8774 jwww,

STORM WATER -QUALITATIVE MONITORING
STORM SITE
DATE
SAMPLED
COLOR
ODOR
CLARITY
FLOATING
SOLIDS
SUSPENDED
SOLIDS
FOAM
OIL SHEEN
EROSION OR
DEPOSITION
AT THE
OU'1'FALI_
OTHER
OBVIOUS
INDICATORS
OF
STORMWATFR
POLLUTION
!
1- 17-Js'
,$Wok ,'dtv
AJoeo
667C BAo
mp�
A)o �tv,�lo.4--e
�o.��•
.t9 ,ti
Ae
livoc e
,uo4P
w
3
� • l7 • is
' '
' '
L,
,UV
itio K
,cjo -4
do
d -4- e
Total Rainfall (inches): _ 0

STORM WATER -QUALITATIVE MONITORING
STORM SITE
DATE
SAMPLED
COLOR
ODOR
CLARITY
FLOATING
SOLIDS
SUSPENDED
SOLIDS
FOAM
OIL SHEEN
EROSION OR
DEPOSITION
AT"ITIE
OUTFALL
OTHER
OBVIOUS.
INDICATORS
OF
STORMWATER
POLLUTION
BlAeklglae
N' o ge
/vo 0-,e
"kj o-tP
N a.c
"O1 p .c e
Pam.
!P I
t
Total Rainfall (inches):

STORM WATER -QUALITATIVE MONITORING
STORM SITE
DATE
SAMPLED
COLOR
ODOR
CLARITY
FLOATING
SOLIDS
SUSPENDED
SOLIDS
FOAM
OlL S111iEN
EROSION OR
DEPOSITION
AT TI IF
OU'CFALL
OTHER
013VIOUS
INDICATORS
OF
STORMWATER
POLLUTION
1
-1 - 1
[3td s
d9a •c
Goo
� v,c
/" O,�B
•�e� A-E
Ap P
.�
7�1
3
7- -r
,.
, •
�t
.�
Total Rainfall (inches): 0

STORM WATER -QUALITATIVE MONITORING
STORM SITE
DATE
SAMPLED
COLOR
ODOR
CLARITY
FLOATING
SL OIDS
SUSPENDED
SOLIDS
FOAM
OIL SI IP'EN
EROSION OR
DEPOSITION
AT THE
OjUTFALL
OTHER
OBVIOUS
INDICATORS
OF
STORMWATER
POLLUTION
lo-
(dos
v3on f-
G
`
IV�7n�
Q
IV i�
�
1V17��
C.1,14,
A
YkJC)
-e-
Total Rainfall (inches):

I ANNUAL SUMMARY DMR - WASTEWATER I
SEND TO CENTRAL OFFICE*
PROCESS MINEIDEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
* Report All Wastewater discharge monitoring data on this form (including iVo Flow and No Discharge and Penxit Limit Violations) by MARCH I of each year. If +
You have limit violations. you must also have turned in a Limit Violation DNIR to Your local Regional Office within 30 days of receiving sample results from a lab,wt, _ #
CERTIFICATE OF COVERAGE N N G427 4 SAMPLE C LLECI'ION YEAR: �O/ If�F-1 �v
FACILITY NAME: -fh-t" P�Q _k S %1:eA Leo.- COUN'Cl': 94 /. oi.a K4 _ �°•d
PERSON COLLECTING 5ALN7PLES: ►rr q•: e,e, PHONF, NO. 1 L -(ram 917!? i BAN 2 2015
CERTIFIED LABORATORY:&,!gAg A Lab # ADD TO LISTSERVF,? YES ❑ NOW EMAIL: .
'.tare__._ f s� �1. C• -Lab # -1 t t'eAL FILES
l.li19IT �`[OLATIONS? YES❑ NO INDUSTRIAL SAND"' DISCHARGING TO SA WATERS"'ElR SfiCTfON
Part A: Wastew ter Monitoring Rectuirements
Outfall No.
Dale Sample
t
Collected
Total Flow
Total Suspended
r
St►lyds
Turbidity
Settleable Solids
pH
-
Fecal Coliforms
-
mni/dd/yr
NIG
mg/l '
NTU
m]A
Standard"
courni ',
�- 7- 141-aiP
StaQx-%
7. 17- L!
7, o 7
•' el
-/
.L
.o
�+�. St<�t.trf
�d- Slq-
�wM
t.2.
J rQ
�•�
/.D
• /
7. 49
f �.
�o- • sY2A
datic•�.
3•Y
. io
CIC�
r
•7
All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs. and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water. directly upstream and downstream of the discharge.
Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Permit Date: 1 /1 /2010-12/31 /201 d Last Revised 01-21- I I
Page 1 of 2

r�

Pory-k Coirtinued: NVastewater Monitoring Requirements
Outfail No.
Date Sample
Collected)
Total Flow
Total Suspended,
Solids'
Turbidity`
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
MG
mg/1 '
NTUz'
ml/l`
Standard2
col/ml-''
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & L.IMIT
VIOLATIONS) BY YVIARCH 1 OF EACH YEAR TO:
Division of Water- Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU ilf UST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under gym• direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aw that there are siggificant penal ' s for submittingfalse information, including the possibility of fines and imprisonment for knowing violations."
(Signature of erns ttee) ( ate
Permit Date: l/l/2010-12/31/2014 Last Revised 01-21-1 1
Page 2 of 2

a
RESEAARCh & ANA1yTICA1
UboRAToRIES, INC.
Analytical/Process Consultations
.7.11- Carter TIT &
515? Midland Road
Sarathern Pines, NC 28387
Attn: William Mullin
V%%%"4uu 11114t►►.
ANAt
yr� ►►,► '
'two
V
'fry ,� • ,, ��,. ' �
5 �
Nate sample Collected 01/07/14.
!sutra :,ample! Received 01/08,%14
Date Sample Analyzed 01/08/14
Date of [teport 0.1/15/1.4
Analyses Performed by YJ
Lab Sample. Number
---------------
'776082
Parameter Storer- ff Results
TSS
(00530)
2.0 mg/1
Turbidity
(OQiJ76)
2.40 NTU
5ett.Matr..ex
(00545)
<0.i, ml/I
C.1.:i..Q; its Sample source DOWNSTREAM
Mviber SOUTHERN PRODUCTS
Time Collected tHrs) 1415
E? 0. Box 47.; - 106 Short Street • Kernersvidle, North Garolino 27284 • 336-996-2841 • Fax [phone]
v'Awj.randalabs,com

RESEARCh & ANA[YTiCA
LABORATORIES, INC.
Analytical/Process Consultations
J.H. Carter III & Associates
51.5P Mi-dl.aod Road
Sout:h.e.rn Pines, NC 28387
Attu: William Mullin
Date; Sample Collected
Late Sample Received
Dare Sample Analyzed
Tate of Report
?Analyses Performed by
Leah Sattt�>le Number
7'76083
Parameter Stareet 4 Results
TSS
(00530)
7.33
mg/l
"turbidity
(000'YG)
50.0
NTU
Sett -Matter
(00545)
<0.1
ml/1
C1iens Sample Source POND 2
Number SOUTHERN PRODUCTS
Time Col.1c;cteci (Hru) 1445
4111too, Ir�
'o
NC #34 z.
71%U'7/I4
01/08,14
01/08/14
01/1.5/14
YJ
P.O. Box 473 • 10b Short Street • Kernersville. Nor6fl Caralirts 27284 • 336-9136.2641 • Fax 336-996-(]326
wvnrvtir.randa lebs.com

RESEARCh & ANA[yTICA1
LAbORATORIES, INC.
Analytical/Process Consultations
J.H. Carter ITT & Assoclat=ws
51.517 Midland Road
Southern Pines, NC 28.387
Awtn: William Mullin
.Date Sample Col..lecteci
UaLe Sample Received
Date Sample Analyzed
Gate of Report
X nalyses Performed by
Lob Sample Number
--------------------
7'15084
Parameter Storer- It Results
TSS (005,10) 6,0 mg/1
Turbidity (00076) 47.76 NTU
SeCt.Matter (00545) <0.1 rail/l
--------------------
Clients Sample F,cource POND 1
Number: SOUTHERN PRODUCTS
T-,Inl Cc;i lected (Hrs) 15:10
` c��'•Yr`04P
�a
NCB
M yy
i
'+�fl14"r=DMA1�I1`11%
01/07/14
01/08/14
01/08/14
01/1.5/14
YJ
P.O. Box 473 • 10B Short 8LreeL • Kernorsv40e, North Carolina 2%2B4 • 336-996.2841 • Fax [phone]
www.randalabs.com

RESEARCh & ANA[YTlCAL
LZORATORIESI INC.
S
" .w... Analytical/Process Consultations
U.11. Carter III: & F�.`sociates
515F Midland Road
Southern fines, NC 28387
Attn: William Mullin
Date Sample C'ollected 01/0"1/14
Date Sample Received 01/08/1.4
Date Sample>. Analyzed 01/08/14
Dace. of Report 01/15/14
Analyses Performed by YJ
Lab Sample Nwnbex
--------------------
776085
Parameter Storet # Re ults
TSS
(00530)
3.33
mg/1
Turbidity
(00076)
3.77
NTU
Sett.Matter
(00545)
<0.1
ml/I
----------------------
cliento Sample Source. UPSTREAM
Number SOUTHERN PRODUCTS
Time Col lectecl (Hrs) 154 0
P.O. Box 473 • 106 Short Street • Kernersviila. North Carolina 27284 • 336-996-2841 • Fax [phone]
vAvw.randalabs.com

Southern Products & Silica Co
Mr. Bill Price
4303 US Hwy I
Hoffman NC, 28347
Fayetteville Division
Certificate of Analysis
Project•. Storm Water Samples
Date Reported: 07/17I14
Date Received: 07/15/14
Date Sampled: 07/1 V14
Sampled By: Price
Up Stream
K4G0498-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
PH
7.07
PH Units
07/15/14 09:00
Price
pH
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
mi/L
07/[ 6/14 07:15
JAO
SM 2540 F-1997
Total Suspended Solids
3,00
mb/L
07/17/14 07:40
JAO
SM 2540 D-1997
Turbidity
3.2
NTU
07/16/14 16:00
DSK
SM 2130 B-2001
Down Stream
K4G0498-02
Analyte _ Result Units Analyzed Analyzed By Method Qualifier
Fi dd Dala
PH
7.41
pH Units
07/15/14 09:45
Price
pH
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
ml/L
07/16/14 07:15
JAO
SM 2540 F-1997
Total Suspended Solids
3.25
mg/L
07/17/14 07:40
JAO
SM 2540 D-1997
Turbidity
3.5
NTU
07/16/14 16:00
DSK
SM 2130 B-2001
Discharge Point
K4G0498-03
Analyte Result Units Analyzed Analyzed By Method Qualifier
Field Data
PH
7.02
pFl Units
07/15/14 10:30
Price
pH
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
ml/L
07/16/14 07:15
JAO
SM 2540 F-1997
Total Suspended Solids
6.25
mg/L
07/17/14 07:40
JAO
SM 2540 D-1997
Turbidity
6.6
NTU
07/16/14 16:00
DSK
SM 2130 B-2001
QC Batch Run - (werobar 1,abararorle5, JJJV, - hiaycrre r!!c�
IAnalyte _ Result _ Units ^^� Source RPD Limit
Total Suspended Solids 22.7 mg/L K4G0552 18 5
Microbac Laboratories, Inc. Page 1 of
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864,8774 f I www.microbac.com

�tDMICROBAC}
Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co Date Reported: 07/17/14
Mr. Bill Price Project. Storm Water Samples Date Received: 07/1 5/14
4303 US Hwy I Date Sampled: 07/15/14
Hoffman NC, 29347 Sampled 13y: Price
QC Batch Run - (hlicrobac Laboratories, Ine. - Fayerleville)
Analyte Result Units Source RPD Limit
Total Suspended Solids 6.25 mg/L K4130498 0 5
Total Suspended Solids 197 mg/L K4G0492
Turbidity 6.63 NTU K4G0498
Slate Certi fications:
NCDNR 411
NCDOH #37714
5 5
0 5
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Thank You for your business. We irreire y oar feedback oo v u' level gfmrvice to yoa. Plca+ a comae! the Division Alanagur Rub Derurer at 910-$64.1920 with any
questions, Yon rngv also conlacl J, Tr'evOr Howe, President a1 pr'esideuf a n+icro6ac,conr
Microbae Laboratories, Inc. Page 2 of
2592 Hope Mills Road I Fayetteville, NC 28306 1 910.864,1920 p 1910.864.8774 f I www.rnicrobac.com

ICROBA `
I
Fayetteville Division
h
Certificate of Analysis
I
i
Southern Products & Silica Co
i
Date Reported: 11/62/14
Mr. Bill Price Project: Storm Water Samples
Date Received: 10/29/14
4303 US Hwy 1
Date Sampled: 10/29/14
Hoffinan NC, 28347
Sampled By: Client
Up Stream
K410884-01
Analytc
Result
Units
Analyzed
Analyzed By
Method Quaiificr
Field Data
_
pH
4.5
pH Units
10/29/14 09:45
Client
PH
Temperature
19.3
°C
10/29/14 09:45
Client
Field
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0.10
ml/L
10/30/14 08:08
JAO
SM 2540 F-1997
Total Suspended Solids
5.00
mg/L
10/30/14 08:20
JAO
SM 2540 D-1997
Turbidity
2.7
NTU
10/30/14 09:20
NCH
SM 2130 B-2001
Down Stream
W0884-02
Analytc Result Units Analyzed Analyzed By Method Qualifier
Field Data
PH 6.1 pl-I Units 10/29/14 10:00 Client pH
Temperature 19.5 °C 10/29/14 10:00 Client Field
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Settleable Solids <0.10 ml/L 10/30/14 08:08 JAO SM 2540 F-1997
Total Suspended Solids 4.25 mg/L 10/30/14 08:20 JAO SM 2540 D-1997
Turbidity 3.4 NTU 10/30/14 09:20 NCH SM 2130 B-2001
Discharge Point
K4J0884-03
Analytc
Rcsult
T Units ^�
Analyzed
Analyzed By
Method Qualifier
Field Data
PH
6.3
pH Units
10/29/14 10:45
CIient
PH
Temperature
21.8
°C
10/29/14 10:45
Client
Field
Analyzed by; Microbac Laboratories, Inc.
- Fayetteville
Settleable Solids
<0. 10
ml/L
10/30/14 08:08
JAO
SM 2540 F-1997
Total Suspended Solids
6,77
mb/L
10/30/14 08:20
JAO
SM 2540 D-1997
Turbidity
7.6
NTU
10/30/14 09:20
NCH
SN4 2130 B-2001
Microbac Laboratories, ]I3c. F Page 1 61'�
2592 Hope Mills Road l Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.micrc)bac.com

*MICROBACit.
Fayetteville Division
Certificate of Analysis
Southern Products & Silica Co
Date Reported: 11/02/14
Mr. Bill Price
Prcjcct: Storm Water Samples
Date Received: 10/29/14
4303 US Hwy I
Date Sampled: 10/29/14
Hoffman NC, 28347
Sampled By: Client
QC Batch t2un - (Alierobac Labor'arariev, Inc. -
Fayelreville)
Analyte
Result
_ Units _!
_ Source
RPD _ Limit
Total Suspended Solids
6,25
mg/L
K4J0862
13
5
Total Suspended Solids
94.0
mg/L
K4J0835
4
5
Total Suspended Solids
6.77
:ng/L
K4J0884
0
5
Turbidity
2.65
NTU
K4J0884
2
5
State Certifications:
NCDNR 411
NCDOH 437714
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Thank you for your businoss. We iuvile yuro feedbnrd wr our level gfservice 10.1m. Please corvacl the Division lbl0nager, Rob Der mer at 910-864-1920 with any
quesoulis K,it'uar also canrocl J. To evor HoYce, Pr'esidew at presiderrl rr micr'abnc.currr
Microbac Laboratories, Inc. Aage 2 of�
2592 Hope Mills Road i Fayetteville, NC 28306 1910.864.1920 p 1 910.864,8774 f I www.microbac.com

STORM WATER -QUALITATIVE MONITORING
STORM SITE
DATE
SAMPLED
COLOR
ODOR
CLARITY
FLOATING
SOLIDS
SUSPENDED
SOLIDS
FOAM
011, SHEEN
EROSION OR
DEPOSITION
AT THE
OUTFALL
OTHER
OBVIOUS
INDICATORS
OF
STORMWATER
POLLUTION'
1
/a-,2,9-lri
91" Afe
4
Goo
/an
a►c
.�o•�
�m w
�o,c10�a
e
�0�2l-�Y
/u• G,eoe
/Vf
Good
�oPte
A90Ae-
100,E e
�o.c-4
o.�e
Na K�
Blae GLe.,�
��"I
GOo�
/4J0 't
/00
a
/ o of,.e
Total Rainfall (inches):69

DR. J.H. CARTER III & ASSOCIATES, INC. DENR-FRO
Environmental Consultants
P.O. E3ox 891 • Southern Pines, N.C. 28388 DEC T.8 2010
(910) 695- 104-3 • Fax [phone] ®YYO
Letter of Transmittal
To Mike Lawycr
DWQ Faycttcville Regional Office. Datc: fob ##
Re: Southern ProdUetS Silica Mine Water Data
In PDF format.
WEAR - SEINDING YOU
Attached Reports Maps
Copy of letter Plans Data
Prints Photos
COPIES
1) ATIH
t#�S
DESCRIPTION
1
12-23-10
1 data Cl)
"fE-kE�SE ARIA "TRANSMITTED
For approval
For your use
As requcsted
For review and comment
RF"MARKS:
Approved as noted
Approved as submitted
Returned for corrections
For your in[ortrtation
t t l [ NIvIG k)
ljenclosures ore nor noted. Pleose Coon rcl us imnredialelr
I?nd<inocrcd Species Surveys . Environmcnud Assessments • Land Management • Wetlands Mapping and Pumitting

!,"-='), DR. J. H. CARTER III & ASSOCIATES, INC.
.I' ENVIRONMENTAL CONSULTANTS
Dr. J.H. Carter III
Principal,
Senior Scientist
• Biological / Environmental
515 F Midland Road
Assessments
Southern Pines, NC 28387
• Land Management
PH/FAX [phone] / 3317
• Red -cockaded Woodpecker /
Mobile [phone]
Protected Species Surveys
Email: [e-mail]
• Wetland Delineation /
Permitting / Mitigation
Phone: [phone]
Toll Free: 1-800-572-6348
Fax: [phone]
www.sandandgravel.net
Southern Products & Silica Company, Inc.
Filter Sand & Gravel • Well Gravel
Industrial Sand • Epoxy Aggregate
C. K. Smith P. 0. Box 189
General Manager 4303 US Hwy 1
Email. [e-mail] Hoffman, NC 28347

PROCESYMINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR) .
11 Please Mail Original And One Copy To Mailing Address Below
GENERAL PERMIT NO. NCG020000
Part A: Facility Information
Samples Collected In Quarte 1 l2 3 4 (all samples shall be reported within 30 days following monitoring period)
(Clnk Oae�
Certificate Of Coverage No. NCG02 dZ County of Facility 1(�in��rp��
Facility NameSbZ�h VDUG�"S� ; i GtCQrx • Name of Laboratory
Facility Contact CN .'C vk—n h, Lab Certification # (�
Facility Contact Phone No. (Club 2- L -• 3) g 1
Part B: Process lVasteivater and Mitre. Dewatering 1Vastewaler Monitoring Requirements
.00400 ..
§ 0053d'
` 00676
00545
Receiviing StreamName '� �:':
Sample Collected=
Daily Hio�t
OH
_Total Suspctided Solids '
Turbidity
Settleable Solids '
t5
?`—�:..J.. •
r . w :
:_�-� x'. 7
�'-irti r ti-,-e,+�r • r ,,, `� c a �fi
t. �w •
a
1-
- s tU's
i µ'
,sf
tnolddl r
w1GD
unit
.m 1:,-
7VTtJs �,
c'•ml/l
�-A
2-111047
3
O i
+' to
I3Ca
5
Lo.{
Da v jmA-rl: a.sm Lr .Z 3.0 1: 3 Lo . I
Measured continuously using a flow measuring device or estimated using manufacturerls pump curves and pump logs.
Part C. Certification
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Part D: Mailing Address
Attn: Central Files, DENR, N.C. Division of Water Quality, 1617 Mail Service Center, Raleigh, NC 27699-1617
(Date)
S W G-244-012005

PROCESS/MINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR)
Please Mail Original And One Copy To Mailing Address Below
GENERAL PERMIT NO. NCG020000
Part A: Facility Information
Samples Collected In Quarter: 10 zQ a040 (all samples shall be reported within 30 days following monitoring period)
II l
Certificate of Coverage No. NCG02 OZ1- County of Facility P-1 bAnOMA
Facility Name to r, t ki G(74, J:t^G • Name of Laboratory V- J--A S _
Facility Contact G V. Lab Certification # MG 4
Facility Contact Phone No. A to 99j_ -; I s71
Part B.• Process Wastewater and Mine Dew attiring Wastewater Monitoring Requirements
IfIr
f - s'Dater
'
114-
,- ,
ilec
50030�x�
y5!
00400
00530 G;, s
40�T
tir 00076`
tit 00545 , %�F
f
S m llC
P
Daily glow
H
P
�3�;
Tatei Sui tided Solids•
p!
rlildl
;. R
5ettlb c Saliii9
r
r'
.
a:%6-::,r
: * �
. RV
-1 .:ate e 4
"
x s
`
':r °xg
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old
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Dmwv+vn M • 1-13a 16 q - -. 3.3 4.-+'1, 4 ©,1
t Measumd continuously using a flow measuring device or estimated using manufacturer's pump curves and pump logs.
DOT -
Part C: Certification C'OV-1-6}W M
.t, uvi dk.n US1.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with avtoo 't"A
system designed to assure that qualiffed.personnel properly gather and evaluate the information submitted. Rased on my inquiry of the person UZ- At 1 S +pL
or persons who manage the system, or those persons directly responsible for gathering the Information, the information submitted is, to the best;, 44%',,,
of my knowledge and belief,_true, accurate, and complete. I am aware that there are significant penalties for submitting falseinformation,
including the possibility of fines and Imprisonment for knowing violations."
(Signature of Permittee) (Date)
Part D: Mailing Address
Attn: Central Files, DENR, N.C. Division of Water Quality, 1617 Mail Service Center, Raleigh, NC 27699-1617
,
ow' °�ov�Ms��•^t
yo W+�-�►tJn dt�/
SWU-244-012005

0
,`��s�r►errlijr�r�
RESEARCk & ANA[yTICAL �.� : t i L �H, r •.,�
LZORATORIES, INC. : o� o�
�' NC
Analytical/Process Consultations s
Z.
4�rrrrrrr*��
DR J.H. Carter III & Associates
515 F Midland Road
Southern PineS, NC 28387
Attn: Tracy Rush
Data S;;Mple Ccllectnf? 07/30/09
Date Sample Received 07/31/09
Date Sample Analyzed 07/31/09
Date of Report 08/06/09
Analyses Performed by :,YJ
Lab Sample !dumber
--------------------
652276
-------------------------------------------------------------------------------
-------------------------------------------------------------------------------
Parameter Storet # Results
TSS
(00530)
1,060
mg/l
Turbidity
(00076)
1,640
NTU
Sett.Matter
(0.0545)
0.213
ml/l
Clients Sample Scurcrt PC :-" 2
Number SOUTHERN PRODUCTS MI
Time Collected (Hrs) 1319
P.Q. Box 473. 106 Short Street • Kernersville. North Carolina 27264 •336-996-2841 • Fax [phone]
www.randslabs.com

RESEARCh & ANA1yTiCA1
LAb4RATORIES, INC.
Analytical/process Consultations
DR J.H. Carter III & Associates
515 F Midland Road
Southern PineS, NC 28387
Attn: Tracy Rush
Ott*tiAl
NC #34 Z �
ti
w
Date Sample Collected 07/30/09
Date Sample Received 07/31/09
Date Sample Analyzed 071131/09
Date of Report : 08/06/09
Analyses Performed by YJ
Lab Sample Number
--------------------
652277
Parameter Storet # Results
TSS (00530) 10.3 mg/1
Turbidity (00076) 254 NTU
Sett -Matter (00545) <0.1 ml/1
--------------------
Clients Sample Source POND 1'
Number SOUTHERN PRODUCTS MI
Time Collected (Hrs) 1350
P0. Box 473 • 106 Short Street • Kernersville. North Carolina 27284 • 336.996.2841 • Fax [phone]
www.ra nda la bs,com

3
RESEARCh & ANA[yTICAL
LABORATORIES, INC.
Analytical/Process Consultations
DR J.H. Carter III & Associates
515 F Midland Road
Southern Pines, NC 28387
Attn: Tracy Rush
0
'0141u1 J 1'01t+t
��% rw�Y%ttt
r �•
M w
No
r
Date Sample Collected 07/30/09
Date Sample Received 07/31/09
Date Sample Analyzed 07/31/09
Date of Report 08/06/09
Analyses Performed by YJ
Lab Sample Number
--------------------
652278
Parameter Storet # Results
TSS
(00530)
<1.0
mg/l
Turbidity
(00076)
4.64
NTU
Sett.Matter
(00545)
<0.1
ml/l
--------------------
Clients Sample Source UPSTREAM
Number SOUTHERN PRODUCTS MI
Time Collected (Hrs) 1415
P 0. Box 473. 106 Short Street • Kernersville, North Carolina 27284. 336-996-2841 • Fax [phone]
www.randelabs.com

RESEARC&, ANA[yTICAI
LABORATORIES, INC.
Analytical/Process Consultations
DP. J.H. Carter III & Associates Date Sample Collected
515 F Midland Road Date Sample Received
Southern PineS, NC 28387 Date Sample Analyzed
Attn: Tracy Rush Date of Report
Analyses Performed by
Lab Sample Number
--------------------
652279
Parameter Storet # Results
TSS
(00530)
7.33
mg/1
Turbidity
(00076)
4.76
NTU
Sett.Matter
(00545)
c0.1
ml/l
--------------------
Clients Sample Source DOWNSTREAM
Number SOUTHERN PRODUCTS MI
Time Collected (Hrs) 1445
1,`• � Aft
A ;
¢;Q 0-w
i °0 NC #34 Zi
t
••''QED ANP��.�►``�.
07/30/09
07/31/09
07/31/09
08/06/09
YJ
R0 Box 473 • 106 Short Street • Kernersville, North Carolina 27284. 336-996-2841 • Fax [phone]
www.randatabs.com
q

PROCESSIMINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR)
Please Mail Original And One Copy To Mailing Address Below
GENERAL PERMIT NO. NCG020000
Part A: Facility Information
Samples Collected In Quarter: 1 2 3 40_ (all samples shall be reported within 30 days following monitoring period)
h Oar) vv11
Certificate Of Coverage No. NCG02_ D �-q County of Facility tit Gh -onc(
Facility Name soi>v A ✓i s Vmflu t"ty,- ';;i 1 i 0— Name of Laboratory _ `4, A L1< -kf,,
Facility Contact C-G smi-tv, Lab Certification # NLr 3�
Facility Contact Phone No. (0)_ 2.531 "'- 3 i 31
Part B: Process Wastewater and Mine Dewatering Wastewater Monitoring Requirements
_
.y"^x-tiJ S6J'
*e F;V-V
1$ i�500S05-.-
''Y�'fi�
00400
00530 _ pay' �;
f..—• i�.#.."i i
M0007f r.
'drJ
:1' QlIS4S €
t '
Nu�SnpleC
Reee. 5 m Ng'
o
pa{�yF
s� pH
iTotal Stitpeaaedds`i
T1'
rCtlSol
tnbet
�
3
4
4�T _t f
+lctee
r V i csY r,
41r.
;.
tin
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D"
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%
S-q 1
5.0
A
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ray
5.2
i p
Lo.l
Po -
5 40
Dorms�vc rn-�►a.Nr.�r.�Gtc 411('jC 1 5.--- 3.?-5 �s,o4 LQ.1
Measured continuously using a flow measuring device or estimaled using manufacturer's pump curves and pump logs.
Part C. Certification
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted Is, to the best
of my, knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permlttee)
Part D: Mailing Address
Attn: Central piles, DENR, N.C. Division of Water Quality, 1617 Mail Service Center, Raleigh, NC 27699-1617
(Date)
S Wl1-244-0 l 2005

�r
♦� r
TICA• ��' `�'=•" •
RESEARCh & ANA[y,
r. LABORATORIES INC, Vt.�:'y LA'
#34Z • '
Analytical/Process Consultations tS
+� •...... • '' �j
NPv
D77. J.H. Carter i.T_d ,;, Asoa-::-atvs
515 F Midland Rd
Southern Pines, NC 2,3387
Attn: Lori Blanc
Date S�tm;.le Coll.er_teA 0,.1 /16I�9
Date Sample Received : 04/17,109
Date Sample Analyzed 04/17!09
Date of Report 04/22,109
Analysec Performed by _ YJ
Lab Sample Number
643598
643597
Parameter
Storet #
Results
Results
TSS
(00530)
145 mg/l
828 mg/1
Turbidity
(00076)
540 NTU
1,610 NTU
Sett.Mattear
(00545)
<0.1 ml/i
r0.1 ml/l
Clients Sample Source POND #1 POND #2
Number
Time Collected (Hrs) 1a08 1_233
P.O. Box 473 • 106-Short Street • Kernersville, North Carolina 27284 • 336.996-2841 • Fax [phone]
www.randelabs.com

I'
RESEARch & ANA1yTICA1
I-AbORATOR#ES, INC.
Analytical/Process Consultations
Dr. J.H. Carter ITT & Associates
515 F Midland Rd
Southern Pines, NC 28367
Attn: Lori Blanc
`mow: ��i� � C '�i►,� �+i
o
Dato Sample Collected 04/16/09
Date Sample Received 04/17/09
Date Sample Analyzed 04/17/09
Date of Report 04/22/09
Analyses Performed by YJ
Lab Sample Number
643599 643600
Parameter Storet # Results Results
TSS (00530) 3.0 mg/1
Turbidity (00076) 6.93 NTU
Sett.Matter (00545) <0.1 ml/l
Clients Sample Source
Number
Time Collected (Hrs)
3.25 mg/1
8.04 NTU
<0.1 ml/1
UPSTREAM DOWNSTREAM
. 1340
1407
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax [phone]
www.rendalabs.com

PROCESS/MINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR)
11 Please Mail Original And One Copy To Mailing Address Below
GENERAL PERMIT NO. NCG020000
Part A: Facility Information
Samples Collected'In Quarter: Q 2Q 30 4 (all samples shall be reported within 30 days following monitoring period)
Certificate Of Coverage No. NCG02 0- County of Facility
Facility Name tau. -111VI-1 Name of Laboratory
Facility Contact �G(. Srv,i±1,3 Lab Certification N NG4434• _
Facility Contact Phone No. Q I <)^ — 351 fE3
Part B.• Process Wastewater and Mine Dewatering Wastewater Monitoring Requirements
'T `Dsit
',=x4j:_
`SDtISO00480
00530..
d'l#~D0016Q0545
Rei�liFing Bti'esnt Namc •�
Samplc Go acted''
Dail Flo �tpH
Yr�";�
Total Suspended Solids'
Turbt: it- `
Settteabie'Bolldii
;1Vgt:: r
by,�
t __��
gggrr`MGDunit°':gym
t' t►�cx`�
i
I
6.0
2
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ssz
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Z
5. zr
g '
�, lr
Downsil-r-o" , - Drb4-ANin CAC- I! t2-1 zoo 1 S-Y 41.0 �•5U Lo I
I Measured continuously using a flow measuring device or estimated using rnanufacturces pump curves and pump logs.
Part C. Certification
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage'the system, or those persons directly responsible for gathering the. Information, the information submitted is, to the best
of my knowledge:and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Part D: Mailing Address
Attn: Central Files, DENR, N.C. Division of Water Quality, 1617 Mail Service Center, Raleigh, NC 27699-1617
(Date)
SWU-244-012005

00
RESEARC& ANAL TICAL Y'
LAbORATWES, INC. o=� ,'o;�,
:-
Cn
NC #34 z -.
Analytical/Process Consultations 't
i 0 Q, •
DR J.H. Carter I_TI & Associates
515 F Midland Road
Southern PineS, NC 28387
Attn: Tracy Rush
Date Sariple Collected 01/1.2/09
Date Sample Received : 01/13/09
Date Sample Analyzed 01/13/09
Date of. Report 01/20/09
Analyses Performed by YJ
Lab Sample Number
636484
636483
Parameter
Storer N
Results
Results
TSS
(00530)
123 mg/l
4,480 mg/1
Turbidity
(000,26)
382 NTU
4,460 NTU
Sett.Matter
(00545)
c0.1 ml/l
5.68 ml/1
Clients Sample Source POND 41 POND #2
Number SOUTHERN PRODUCTS SOUTHERN PRODUCTS
Time Collected (Hrs) 1340 1320
P.O. Box 473. 106 Short Street • Kernersville, North Carolina 27284 • 336.996-2B41 • Fax [phone]PS
www.randalabs.com

RESEARCh ANA[yTiCAI
LkORATWES, INC.
Analytical/Process Consultations
DR J.H. Carter TIT & Associates
515 F Midland Road
Southern PineS, NC 28387
Attn: Tracy Rush
NC #34 z:
M
/ED P,S14`���
Date Sample Collected 01/12/09
Date Sample Received 01/13/09
Date Sample Analyzed 01/13/09
Date of Report 01/20/09
Analyses Performed by YJ
Lab Sample Number
636485
636486
-------------------------------------------------------------------------------
Parameter
Storet 4
Results
Results
TSS
(00530)
2.5 mg/1
<1.0 mg/l
Turbidity
(00076)
3.62 NTU
4.50 NTU
Sett.Mattcr
(005,15)
<0.1 ml/l
<0.1 ml/I
-------------------- --------------------
Clients Sample Source UPSTREAM DOWNSTREAM
Number SOUTHERN PRODUCTS SOUTHERN PRODUCTS
Time Collected (Hrs) 1408 14'30
P.O. Box 473. 106 Short Street • Kernersville, North Carolina 272B4 • 336.996-2641 • Fax [phone]
www.randalabs.com

PROCESS/MINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR)
'Please Mail Original And One Copy To Mailing Address Below
GENERAL PERMIT NO. NCG020000
Part A: Facility Information
lak�-
Samples Collected In Quarter: 1 20.Q 40, (all samples shall be reported within 30 days following monitoring period)
,cam,
Certificate Of Coverage No. NCG02 O 7--A-ei County of Facility t G�rrb
Facility Name paas b 5i f i rA Co . Name of Laboratory iZ2c�tom �41n a A►ialu h �
Facility Contact C . St .i+41, Lab Certification N NC,#�1
Facility Contact Phone No. (offro_) S
Part B: Process Wastewater and Mine Dewatering Wastewater Monitoring Requirements
iti
x�3�'
r ✓_r i
36650-W— L
!00400
x 1
00530-_ a .,'i
VAly,�;Y.•
N-900674i
�00545YSW` i
ne �v".
;Nttt
ReeNving Stream N fa �,
rS d�plleeted
DaitysFlnwt1H
+•°.,
Total Sszsr{�tidetl 5nliiis�
ram.
7'ititilfit
�'a°'
,$olds
t .r• w +7.!tri. :F3��+..�l+C.: .3 '.;wn..lct ..�,
.4: Sri r'`' f -•�„
:G'1*'�:i'F'1 ij
ti
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BOO
Lf ;�" n M•
'�.:,-.-i 4
Ftii
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t '
WI
oN D A i-
of 14 o8
.(a
, $
4-a.1
PolioI
I ol 141 og
S.
-4 p
I
Pi7yJn�.,—Dre;*►ni ck-. to I lei' lt~ -5 L.O.I
i Measured continuously using a flow measuring dewcc or estimated using manufacturer's pump curves and pump logs.
Part C: Certification
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted Is, to the best
of my knowledge and belie!; true,. accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and Imprisonment for knowing violations."
(Signature of Permittee)
Part D: Mailing Address
Attn: Central Files, DENR, N.C. Division of Water Quality,1617 Mail Service Center, Raleigh, NC 27699-1617
(Date)
S WU-244-012005

RESEARC& ANA[yTICA[ r•••a.rr` ��'•�.
LABORATORIES, INC.:••�A':•
NC #34 z
Analytical/Process Consultations t
i •••OAR Q; t `
rrrrsi
DR J.H. Carter III 8 Associates
515 F Midland Road
Southern PineS, NC 28387
Attn: Tracy Rush
Date. .Somp(r C,i! ter.>.•H 10/14!09.
Date Sample Received : 1D/15/08
Date Sample Analyzed 10/15/08
Date of Report 10/23/08
Analyses Performed by YJ
Lab Sample Number
--------------------
Lab Sample Number
--------------------
Lab Sample Number
Lab Sample Number
629661
629662
--------------------
629663
--------------------
629664
Parameter Storet # Results
Results
Results
Results t „
TSS (00530) <5.0 mg/l
18.0 mg/l
14,960 mg/l
<5.0 mg/l
Turbidity (00076) 3.02 NTU
199 NTU
11,050 NTU
4.59 NTU
Sett -Matter (00545)
Clients Sample Source
Number
rime Collected (Hrs)
<0.1 mt/t <0.1 ml/i 13.6 m€/l <0.1 ml/t
UPSTREAM
POND #1
POND #2
DOWNSTREAM
1125
1155
1218
1056
P.D. Box 473. 106 Snort Street • Kernersville, North Carolina 27284 •336-996-2841 • Fax [phone]
www.randalabszom

REsE4RCh &, ANAlyricA[
I AbORATORIEs� INC.
Analytical / Process Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
WATER I WASTEWATER MiSC.
M � Wx
•
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•
REQUESTED ANALYSISI—
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WR
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SAMPLER NAME (PLEASE PRM
PHONECQNTACT
1 `
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11MM_■■■■■■
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IMIM-MIMMISM
■■■■■■■■
■■■■■■■■■■■■■■■
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■■■■■■■■■■■
■■■■■■■■■■■■
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■■■■■■■■■■■■
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HIM,

PROCESSIMINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT. (DMR)
I . Please Mail Original And One Copy To Mailing Address Below 11
GENERAL PERMIT NO. NCG020000
Part A: Facility Information
Samples Collected In Quarter: IQ 2 3 .4 (all samples shall be reported within 30 days following monitoring period)
Certificate Of Coverage No. NCG02 O?:a-oi County of Facility 9 ; JXh,ot-A,
Facility Name y� i i j G[� Co . Name of Laboratory 1, i P-1 UXAZ
Facility Contact [ " ser j 4jr, Lab Certification # NCa �$
Facility Contact Phone No. (G1 l0) 7 g l . 211 fKQ
Part B: Process Wastewater and Mine Dewatering Wastewater Monitoring Requirements
' , '1 `
c
`r ` Dat'
1 f �t '
r
aD0A00
00530 . .-,Pf`�
i 0W.6
..00S45VX*—,1
p� lteeeiving Stream N9Me
Satnpl :C, Ilected
liaity flow �
H
Total Seispended Solidi
7'u ty
etlt e�Splltl s
r
._ _ .4
la"i' AR33's�-.t'f".�'.�n15 ...iEl:ai "#d.a..:..
�s-v.
.3:.4i.:dauSS:Ty.{.�=�'�...4ti�.i
i -S N:7C.;i4'1:
i"ns...
:L
r �= iCF n ney ,,. y� ♦
V�.u�
mad
11
r�-
aMGDfanit
A�`r rN.Ueiirsll/i::
row ►
- =cam
I ln.o
rS : 0
4 • Z
lbu'D Z
Lk -:�o-09
: s
2.
35.1,
e-o .
WNSTV-EA "-Drwr►iCX_ LD_?F - a 15,Cl' IS 4 I3.oZ e-p.
Measured continuously using a flow measuring device or estimated using manufacturer's pump curves and pump togs.
Part C: Certification
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that,gnalified personnel. properly gather and evaluate the information submitted. Based on my Inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge.and belief, true, accurate,.and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Part D: Mailing Address
Attn: Central.Files, DENR, N.C. Division of Water Quality,1617 Mail Service Center, Raleigh, NC 27699-1617
(Date)
S WU-244-012005

RESEARCh Cat ANA1yTICA1
LABORATORIES, INC.
Analytical/Process Consultations
DR J.H. Carter, 711 S. Associates
515 F Midland Road
Southern Pines, NC 28387
Attn: Tracy Rush
Date Sample Collected 06/30/08
Date Sample ke ceived 07/01/0�
Date Sample Analyzed 07/01i08
Bate of Report 07/10/08
Analyses Performed by YJ
Lab Sample Number
620799
620800
Parameter
Storet #
Results
Results
TSS
(00530)
71.0 mg/l
328 mg/l
Turbidity
(00076)
32.9 NTU
38.6 NTU
Sett.Matter
(00545)
<0.1 mg/1
<0.1 mg/l
Clients Sample Source
Number
Time Collected (Hrs)
POND 91 POND #2
10"s2
1059
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 •336-996-2841 • Fax [phone]
www.randalabs.com

RESEARCh & ANAlyT1CA1
e&�' 0 .
LABORATORIES, INC.
Analytical/Process Consultations
DR J.H. Carter III & Associates
515 F Midland Road
Southern Pines, NC 28387
Attn: Tracy Rush
Date Sample Collected 06/30/08
Date Sample Received 07/01/0
Date Sample Analyzed 07/01/08
Date of Report 07/10/08
Analyses Performed by YJ
Lab Sampl,e.Number
620801 620798
Parameter Storet # Results Results
TSS
(00530)
Turbidity (00076)
Sett.Matter (00545)
Clients Sample Source
Number
Time Collected (Hrs)
5.6 mg/l
13.02 NTU
<0.1 mg/l
<5.0 mg/l
4.21 NTU
<0.1 mg/l
DOWNSTREAM UPSTREAM
1151
1129
P.O. Box 473 • 106 Short Street • Kernersville. North Carolina 272B4. 336-996.2841 • Fax [phone]
www.randalabs.com

PROCESS/MINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR)
Please Mail Original And One Copy To Mailing Address Below
GENERAL PERMIT NO. NCG020000
Pan A: Facility Information
Samples Collected In Quarter: -I 20 30 4 (all samples shall he reported within 30 days following monitoring period)
(coal. 0-)
Certificate Of Coverage No. NCCO2 p County or Facility 9, c NI oND
Facility Name So I,LT FEY M ?CoDU(,TS -h Sk U c-A Ca Name of Laboratory SEAe-t AN ►(,AU LA6';.
Facility Contact G,,,; µ I Tli Lab Certification # fyG # 34
Facility Contact Phone No, a to 2_5'1. 3 lr<k
Part 8: Process Wastewater and Mine Dewatering Wastewater Monitoring Requirements
�. r..
;Qatti ,
°i�4illh: 9b
r *; "a
? '` lteeeivin 6t`rea3mame'
. }' "i«*�7'.1 �fk '.'f!dYlLxtikix,e;:�wir-? .,Ls` r.
Date.
'Sa n se Cbileeted
"..lS*'F' i*.` .3'f`ai:a',2.e�'"
50050501
1r00400
00530
24100076
acr' tiD5i4St `
ID'ii�yplaow
i+1 +-„��+vrit',1°a� �.
H
Tatai Su aden 5oiida�y
:..5k`+ _3 : is7:
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a "F4�``i y+ ''F
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Measured continuously using a flow measuring device or estimated using manufacture's pump curves and pump logs.
Part C.• Certification
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that:qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the Information, the Information submitted is, to the best
of my knowledge and belief, true, accurate; and complete. I am aware that there are significant penalties for subndtting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Part D: Mailing Address
Attn: Central Files, DENR, N.C. Division of Water Quality,1617 Mail Service Center, Raleigh, NC 27699-1617
(Date)
SWU-244-012005

RESEARCh '& ANA1yTICA1
LABORATORIES, INC.
Analytical/Process Consultations
Dr. J.H. Carter III '& Associates
515 F Midland Rd
Southern Pines, NC 28387
Attn: Jennifer Freeman
I
NO 0-n
Z. .
r +
���'iI '�L�D A1�AL;•�`�
Date •Sample •Collected 04 /17; 00
Date Sample Received 04/18/08
Date Sample Analyzed 04/18/08
Date of Report 04/23/08
Analyses Performed by YJ
Lab Sample Number
614945
614946
Parameter
Storet #
Results
Results
TSS
(00530)
126 mg/l
1,660 mg/1
Turbidity
(00076)
323 NTU
1,900 NTU
Sett.Matter
(00545)
<0.1 mg/1
30.7 mg/1
Clients Sample Source POND #1 POND #2
Number SOUTHERN PRODUCTS SOUTHERN PRODUCTS
Time Collected (Hrs) 1323 1310
P.O. Sax 473 • 106 Short Street • Kernersville, North Carolina 27284 •336-996-2841 • Fax [phone]
www.randalabs.com
Filk

RESEARCh & ANALyTICA[
LABORATORIES, INC.
Analytical/Process Consultations
Dr. T.H. Carter III & Assac;a es
515 F Midland Rd
Southern Pines, NC 28387
Attn: Jennifer Freeman
i 01191110100ii+
��� ,rP• A�LYTG�fiy
t, ,,....... �l
a, W.
NC #34 : cn
r
r � �
Date fizmpl rr.;:.ec•L�--3 .
Date Sample Received 04/18/08
Date Sample Analyzed 04/18/08
Date of Report 04/23/08
Analyses Performed by YJ
Lab Sample Number
614944
614947
Parameter
Storet #
Results
Results
TSS
(00530)
5.67 mg11
<5.0 mg/l
Turbidity
(00076)
4.60 NTU
5.06 NiZT
Sett.Matter
(00545)
<0.1 mg/1
<0.1 mg/1
Clients Sample
Source
UPSTREA=ni
::�uS"_F.F•n;?
Number
SOUTHERN PRODUCTS
SOUTHERN PRODUCTS
Time Collected
(Hrs)
1341
1403
P.O. Box 473 • 106 Short Street • Kernersv€lie, North Carolina 27284 •336-996-2841 • Fax [phone]
www.randalahs.com