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NCG080365_COMPLETE FILE - HISTORICAL_20140522
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V () 3 LP y DOC TYPE HISTORICAL FILE ❑ MONITORING REPORTS DOC DATE p riD14 � 9;� YYYYMMDD STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V CAP 449 DOC TYPE ❑ HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ ao t rl a YYYYM M DD Mid Atlantic Engineering & Environmental Solutions May 13, 2014 Mr. Steve Wiggins Young's Auto Center & Salvage/U-Pull-It 4172 US 117 Alternate South Dudley, NC 28333 Subject: STORMWATER SAMPLING RESULTS YOUNG'S AUTO CENTER & SALVAGEIU-PULL-IT 4172 U.S. 117 ALTERNATE SOUTH DUDLEY, WAYNE COUNTY, NORTH CAROLINA PERMIT NCG100182 MID -ATLANTIC JOB NO. 0001131948.00 Dear Mr. Wiggins: 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 facsimile 919.250.9950 MAAONLINE.COM RECEIVED JUN 0 6 2014 CENTRAL FILES DWQIBOG Attached please find three copies of the Stormwater Discharge Monitoring Report (DMR) for the above - referenced site. Please follow the instructions below to complete this sampling event. 1. Sign and date each DMR on page 2; 2. Forward the first two copies of the report along with the attached cover letter to the Division of Water Quality (mailing address is on the first page of the DMR); and 3. Insert the third copy (labeled "FILE") into Appendix C of your Stormwater Pollution Prevention Plan. Based on the results of this sampling event, a Tier One Response should be implemented at the facility. Please complete the attached Tier One Response form, place the completed form in Appendix C and implement the designated controls. If you have any questions or need assistance, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Charles B. Hoffman, PG Project Geologist Attachments: Cover letter Stormwater Discharge Monitoring Report Laboratory Analytical Report cc: Mr. Ricky Young EXPERIENCED CUSTOMER FOCUSED INNOVATIVE Mid Atlantic Engineering & Environmental Solutions May 15, 2014 NCDENRIDWQ Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: STORMWATER SAMPLING RESULTS YOUNG'S AUTO CENTER & SALVAGEIU-PULL-IT 4172 U.S. 117 ALTERNATE SOUTH DUDLEY, WAYNE COUNTY, NORTH CAROLINA PERMIT NCG100182 MID -ATLANTIC JOB NO. 00OR1948.00 To Whom It May Concern: 409 Rogers View Court Raleigh, NC 27610 office 919.250.9918 facsimile 919.250,9950 MAAON LINE.COM Attached please find the Stormwater Discharge Monitoring Report and analytical report for the sampling conducted at the above -referenced site. A stormwater sample was collected from Outfall 006 on May 2, 2014 and analyzed for total suspended solids (TSS), pH, total recoverable lead, oil and grease and ethylene glycol. With the exception of TSS, all parameters were reported below or within their respective benchmark values. Based on these results, a Tier One Response has been implemented at the facility. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. e1w I --.- Charles B. Hoffman, PG Project Geologist Attachments: Stormwater Discharge Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE ,/ STORMWATER HISr- AGE OUTFALL (SILO) GENERAL PERMIT NO. NCG200000 Q DISCHARGE MONITORING REPORT (DMR) CERTIFICATE OF COVERAGE NO. NCG200448 FACILITY NA11[E 2 I', ti DO PERSON COLLECTING SAIIIPLES• —F fS CERTIFIED LABORATORY- Lab # 440 yvo Lab # COUNTY 16tLa V-C= PHONE NO. $c 3-) 3 �Q -q3 I I Part A: Specific Monitoring Requirements �141silairgiiial�ti%ftiinetcv'py tti sago SAMPLES COLLECTED DURING IJivrsron of,Water,Quslitiy� s CALENDAR YEAR: a 01 _ ss, 1' (This tmonitoring report is due at the Division no Afn Central 1 tles ^� �� � later than 30 days from the date the facility 1, 617+111_atl„Setce Cene,�r receives the sampling results fi-onr the laboratory.) SF it# �s'�Qj-RaletghNorthCao�tna 27699 ,1617 No ROW JAr-,tn5 Outfa❑ No: Date Sample Collected mo/ddI' Total Rainfall:' Aikhes - -00530 00340,,•. 00556 ; 00400 - 01113 _ 01119 00980 01114 01094 Total Srispended Solids iii Cheiiiical:Ozygeri, Ueiiiiiiid ' iii'Il' Oil & Grease In/I. p1I s:u: Cadmium ni"/l . Copper in" 11 Iroiri m 11.. Lead in °II Zinc iii' Il 13eiicliiiiark,. 120 - _ :: 30, : 6:0 � 9:0 01001 0:U€17 NIA 0:03 0.067 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier 1 or Tier 2 responses in the General Permit. 'Total recoverable. Only complete Part B if this facility rtses more than 55 gallons of new motor oil per nronth. Part B: Vehicle Maintenance Activitv Monitoring Requirements .Outfall No: • Date• hiiiple Ciillected :_iiuldd/'-rh 'TOtaI : N Raiiifaii - Neiv'1VIotiir Oil U"sage. :UU530. a ,., , :.00400 ., _ 00556, Total Suspended "" Solids, - pI1 Oil &. Grease � " - Beiichiriark ';, lUU 6 0 9 0' ' 30 YOU MUST SIGN 'PHIS CERTIFICATION .FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, (rue, accurate, and complete. I am aware that there are significant penalties ti)r submitting False information, including the possibility of fines and imprisonment for knowing violations." of Permi 09130111Y (Date) 04141 Form S W U-256 Page 1 of- i STORMWATER DISC__..RGE OUTFALL (SDO) GENERAL PERMIT NO. NCG200000 DISCHARGE MONITORING REPORT (DMR) CERTIFICATE OF COVERAGE NO. NCG20044$e{j{{iJ[{�:yn {ir SAMPLES COLLECTED DURING o�0 t FACILITY NAME C'91 ,6 (,a J tx DMA PERSON COLLECTING -} jecuc 11 rJ r� i � 8H31 (I; �Qutiitty + CALENDAR YEAR: This monitoring report is due at the Division no SAMPLES b o�_ -Lze f _ _ to Central Ftles' i' g CERTIFIED LABORATORY �t�,1�L �2 _ _ _ Lab # �i W i/3 -1 fi17rMatljSetwla,Gt tilerh �. later than 30 days from the date the facility y y Yea l yCO, Lab # ° It ig> Nd Ca� liii V 6g, 9 bLIT receives the sampling results from the laboratory.) COUNTY �u� PHONE NO. r<$as) �;;?.2, 3 I I r- Part A: S eelfic Monitoring Requirements Outfall No Date Sar►tple Cofi., Aaii, itno�dii/' r Total Ra6fill [fiches .00530. .. :,.00340; ..... .. ' .;. 00MC 004 .; 01113 01119 00980., .01114, 01094 . Sus Total pended Stillds' rn Clrernlcal 0#gy eii > Demand :. m i On & Grease m 1 pH . s:u Cadmiiim m : L Copper ari ll Iron - Lead --.--_- in"!L fliie iu -- - m 1.: Beiicliiiiark. 100 ;120' :^::: 30.. 6.0.=9,0 . .,. 0:001: _ :.. 7.. 0:0t) NIA 0.03,,.,; D:D67._. ' if a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier l or Tier 2 responses in the General Permit. 2 Total recoverable. Only complete Part B if thus facility uses more than SS gallons of new motor oil per rrtontlt. Part B: Vehicle Maintenance Activity Monitorin Re uirements Outfatl No: Date S,A6iple Collecte8 molddl r 'Total ~.Rainfall .= : iitclres NiWM0 f:Oil = -:-Usage. ;. el/rnoiltll ,. 00530; :;.,_: '00400:•'.... .00556.._. Total Suspended ;Solids ; iii 1 pH s u; Oil & Grease . m Beiiehinikk ` 100 6. 0 = 9 0 � 30 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person orpersons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of n imprisonment for ing violations." - -:�) q� l (Slgua ermittee) ( ate) NCG2000 MR Form SWU 256 Page l of 1 I& ENCO Laboraton"es Accurate. Tamely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, April 21, 2014 Novozymes North America (NO008) Attn: Joe Ladd 77 Perry Chapel Church Road Franklinton, NC 27525 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater Testing ENCO Workorder(s): C312928 Dear Joe Ladd, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, April 7, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. page I. or 10 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall -1 Lab ID: C312928-01 Sampled: 04/07/14 08:50 Received: 04/07/14 17:00 Parameter Hold bate/Time(s] Prep Date/Time(sl Analysis Date/Timefs) EPA 351.2 05/05/14 04/11/14 10:20 04/14/14 10:08 EPA 353.2 04/09/14 08:50 04/08/14 08:25 04/08/14 08:25 EPA 353.2 05/05/14 04/08/14 07:51 04/08/14 12:43 EPA 353.2 12/31/16 04/21/14 IM6 04/21/14 10:12 EPA 365.4 05/05/14 04/11/14 10:20 04/14/14 12:25 SM 2540D-1997 04/14/14 04/09/14 12:20 04/08/14 12720 SM 521OB-2001 04/09/14 08:50 04/09/14 07:04 04/09/14 07:04 SM 5220D-1997 05/05/14 04/1D/14 11:02 04/10/14 17:01 Client ID: Outfall - 2 Lab IO: C312928-02 Sampled: 04/07/14 09:20 Received: 04/07/14 17:00 Parameter EPA 351.2 Hold DatelTimefs) 05/05/14 Prep Date/Time(sl 04/11/14 10:20 Analysis O4/14114 Date/Time(s) 10:14 EPA 353.2 04/09/14 09:20 04/08/14 08:30 04/08/14 08730 EPA 353.2 05/05/14 04/08/14 07:51 04l08/14 12:49 EPA 353.2 12131/16 04/21/14 10:06 04/21/14 10:12 EPA 365.4 05/05/14 04/11/14 10:20 04/14/14 12:30 SM 2540D-1997 04/14/14 04/09/14 12:20 04/08/14 12:20 Sh15210B-2001 04/09/14 09:20 04/09/14 07:04 04/09/14 07:04 SM 5220D-1997 05/05/14 04/10/14 11:02 04/10/14 17701 FINAL This report relates only to the sample as received try the laboratory, and may only be reproduced in full. Page 2 of 10 Ce 010100) www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Otetfall - 1 Lab ID: C312928-01 Analvte Results Flan Hu E" Units lid Notes Biochemical Oxygen Demand 6.1 2.0 2.0 mg/L SM 521OB-2001 Chemical Oxygen Demand 45 10 10 mg/L SM 5220D-1997 Nitrate as N D.59 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.61 3 0.41 1.0 mg/L EPA 353.2 R-01 Nitrite as N 0.01B 3 0.017 0.10 mg/L EPA 353.2 Phosphorus 0,28 0.025 0.10 mg/L EPA 365.4 Total Kjeldahl Nitrogen 1.1 0.26 0,48 mg/L EPA 351.2 Total Suspended Solids 140 1.0 1.0 ri SM 2540D-1997 Client ID: Outfall - 2 Lab ID: C312928-02 Analvte Results Ela9 twi E L Units Method Notes Biochemical Oxygen Demand 12 2.0 2.0 mgJL SM 52108-2001 Chemical Oxygen Demand 55 10 10 mg/L SM 5220D-1997 Nitrate as N 0.52 0.025 0.10 mgJL EPA 353.2 Nitrate/Nitrite as N 0.52 3D 0.41 1.0 mg/L EPA 353.2 R-01 Phosphorus 0.28 0.025 0.10 mgJL EPA 365.4 Total Kjeldahl Nitrogen 1.6 0.26 0.48 mgJL EPA 351.2 Total Suspended Solids 39 1.0 1.0 mgJL SM 254OD-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full, Page 3 of 10 f Ce Nk" e 9) www.encolabs.com ANALYTICAL RESULTS Description: Outfall - 1 Lab Sample ID:C312928-01 Received: 04/07/14 17:00 Matrix: Surface Water Sampled: 04/07/14 08:50 Work Order: C312928 Project: Stormwater Testing Sampled By:]oe Ladd Chemistry Parameters Results flag Units BP = M Batch Method Analysed §11 Note;i Biochemical Oxygen Demand 6.1 mg/L 1 2.0 2.0 4DO9001 SM 521OB-2001 04/09t14 07:D4 30C [ECL-0017]^ Chemical Oxygen Demand 45 mg/L 1 10 10 4D10010 SM 5220D-1997 04/10/14 17;01 30C [ECL-01i Nitrate as N [14797-55-8]^ 0.59 mg/L 1 0.025 0.10 4D21009 EPA 353.2 04/21/14 10:12 CV Nitrate/Nitrite as N [ECL-0010]1 0.61 3 ni 1 0.41 1.0 4DO8004 EPA 353.2 04/08/14 12:43 clv R-01 Nitrite as N [14797-65-0]^ 0.018 3 ni 1 0.017 0.10 4DO8002 EPA 353.2 04/08/14 08:25 clv Phosphorus[7723-14-0]^ 0.28 ni 1 0.025 0.10 4D11005 EPA 365.4 04/14/14 12:25 C1v Total igeldahl Nitrogen [ECL-0162]^ 1.1 ri 1 0.26 0.48 4D11004 EPA 351.2 04/14/14 10:08 C1v Total Suspended S011ds[ECL-o169]^ 140 ri 1 1.0 1.0 4DO8011 SM 254OD-1997 04/08/14 12:20 MMR Description: OutPall - 2 Lab Sample ID:C312928-02 Received: 04/07/14 17:00 Matrix: Surface water Sampled: 04/07/14 09:20 Work Order: C312928 Project: Stormwater Testing Sampled By:Joe Ladd Classical Chemistry Parameters ^ - ENCO Cary certified anaryte JAC 5911 AOi ICAS Numherl Results Eba SlJL pf BU P" Batch Method Analyzed gy Notes Biochemical Oxygen Demand 12 ni 1 2.0 2.0 4DO9001 SM 521DB-2001 04/09/14 07:04 30C [ECL-0017] ^ Chemical Oxygen Demand 55 Mi 1 10 10 4D10010 SM 5220D-1997 04/10/14 17:01 30C [ECL-0035] ^ Nitrate as N [14797-55-B]^ 0.52 nni 1 0.025 0,10 4D21009 EPA 353.2 04/21/14 10:12 CV Nitrate/Nitrite as N [ECL-0010]^ 0.52 JD ni 10 0.41 1.0 4DO8004 EPA 353.2 04/011/14 12:49 Clv R-01 Nitrite as N [14797-65-0]^ 0,017 U mi 1 0.017 0.10 4DO8002 EPA 353.2 04/08/14 08:30 C1v Phosphorus[7723-14-0]^ 0,28 ri 1 0.025 0,10 4D11005 EPA 365.4 04/14/14 12:31) C1v Total Kjeldahl Nitrogen [ECL-0162]1 1.6 nni 1 0.26 0.48 4D11004 EPA 351.2 04/14/14 10:14 C1v Total Suspended Solids [ECL-0169]1 39 ni 1 1.0 1.0 4DO8011 SM 2540D-1997 04/OB/14 12:20 MMR FINAL This report relates only to the sample as recelved by the laboratory, and may only be reproduced in full. Page 4 of 10 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4DO8OO2 - NO PREP Blank (4D08002-BLKI) Prepared: 04/08/2014 08:24 Analyzed: 04/08/2014 08:24 Spike Source %REC RPD Analtrte Resul floe PQL units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (411308002-1151) Prepared: 04/OB/2014 08:15 Analyzed: 04/08/2014 08:15 Spike Source %REC RPD Analvte Result Flag P4L Units Level get %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 100 90-110 LCS (4D08002-BS2) Prepared: 04/OB/2014 08:33 Analyzed: 04/08/2014 08:33 Spike Source %REC RPD Aoalvte Result Elm PQL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 100 90-110 Matrix Spike (4D08002-MSi) Prepared: 04/08/2014 08:26 Analyzed: 04/08/2014 08:26 Source: C312928-01 Spike Source %REC RPD Aaalvte Result E&2 PAL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.1 0.10 mg/L 1.00 0.018 106 90.110 Matrix Spike Dup (4D08002-MSDi) Prepared: 04/08/2014 08:27 Analyzed: 04/08/2014 08:27 Source: C312928-01 Spike Source %REC RPD Analrte Result Elan PQL, Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.1 0.10 mg/L 1.00 0.018 106 90-110 0.2 10 Batch 4DO80O4 - NO PREP Blank (4D08004-BLK1) Prepared: 04/08/2014 07:51 Analyzed: 04/08/2014 12:40 Spike Source %REC RPD .Analvte Result flag P91 Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (4008004-BS1) Prepared: 04/08/2014 07:51 Analyzed: 04/08/2014 12:38 Spike Source %REC RPD Anahrte Result Elag QDL Units Level Result %REC Limits RPD LI131311 Notes Nitrate/Nitrite as N 1.2 0.10 mg/L 1.25 93 90-110 Matrix Spike (4D08004-MS1) Prepared: 04/08/2014 07:51 Analyzed: 04/08/2014 12:45 Source: C312928-01 Spike Source %REC RPD Analvte Result Elag P_QL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 5.4 1.0 mg/L 5,00 0.61 96 90-110 Matrix Spike Dup (4008004-MSDI) Prepared: 04/08/2014 07:51 Anaty2ed: 04/08/2014 12:47 Source: C312928-01 Spike Source %REC RPD Analyte Result Flag P- 1 Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 5.6 1.0 mg/L 5.00 0.61 100 90-110 3 10 Batch 4D08O11 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 10 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4DO8011 - NO PREP - Continued Blank (4D08011-BLKl) Prepared & Analyzed: 04/08/2014 12:20 Spike Source %REC RPD ADa[vte Result Flag M units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 1.0 U 1.0 mg/L LCS (4D08011-BSI) Prepared & Analyzed: 04/08/2014 12:20 Spike Source %REC RPD _Analvte Result Flag POL Units Level gesuR %REC Limits RPD Limit Notes Total Suspended Solids 96 1.0 mg/L 100 96 80-120 Duplicate (4D08011-DUPl) Prepared & Analyzed: 04/08/2014 12:20 Source:C312928-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 130 1.0 mg/L 140 3 10 Duplicate (4D08011-DUP2) Prepared & Analyzed: 04/08/2014 12:20 Source:C312928-02 Spike Source %REC RPD Anal Result flag POL Units Level Result %REC Limits RPD Limit ll9305 Total Suspended Solids 39 1.0 mg/L 39 0 10 Batch 4D09001 - NO PREP Blank (41309001-BLKI) Prepared & Analyzed: 04/09/2014 07:04 Spike Source %REC RPD AealYte Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Biochemical Oxygen Demand 2.0 U 2.0 mg/L LCS (4D09001-BS3) Prepared & Analyzed: 04/09/2014 07:04 Spike Source %REC RPD _Analvte Result flag PQ1 units Level Result %REC Limits RPD Limit Notes Biochemical Oxygen Demand 170 2.0 mg/L 198 87 85-115 Duplicate (4D09001-DUP3) Prepared & Analyzed: 04/09/2014 D7:04 Source:C312928-01 Spike Source %REC RPD _Analvte Result fin POL Units Level Result %REC Limits RPD Limit Notes Biochemical Oxygen Demand 5.1 2.0 m91L 6,1 18 30 Batch 4D10O10 - Same Blank (4D10010-BLK3) Prepared: 04/10/2014 11:02 Analyzed: 04/10/2014 17:01 Spike Source %REC RPD Analyte Result Flaa P-QL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (4D10010-BSI) Prepared: 04/10/2014 11:02 Analyzed: 04/10/2014 17:01 Spike Source %REC RPD Analvte Result flag POL units Level Alt %REC Limits RPD Ltmit Notes Chemical Oxygen Demand 470 10 mg/L SDO 94 90-110 FINAL This report relates only to the sample as received oy the laboratory, and may only be reproduced in full. Page 6 of 10 0 Fmm Nj'kq w www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4D10010 - Same - Continued Matrix Spike (4D30010-MS1) Prepared: D4/10/2014 11:02 Analyzed: 04/10/2014 17:01 Source: C312928-01 Spike Source %REC RPD Ana(Yse Result Elaa 1201 Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 540 10 mg/L 5o0 45 98 90-110 Matrix Spike Dup (4D10010-MSD1) Prepared: D4/10/2014 11:02 Analyzed: 04/10/2014 17:01 Source:C312928-01 Spike Source %REC RPD AnalYte Result Ela9 POL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 540 10 mg/L 500 45 99 90-110 0.4 10 Batch 4D11004 - Same Blank (4011004-BLK1) Prepared: 04/11/2014 10:20 Analyzed: 04/14/2014 10:03 Spike Source %REC RPD -Ana(YW Result E1219 POL Units Level Result %REC j,iniff4 RPD Limit Notes Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L LCS (4D11004-BSI) Prepared: 04/11/2014 10:20 Analyzed: 04/14/2014 10:06 Spike Source %REC RPD -ADHIYIS Result F132 P9L U.01L4 Level Result %REC Linlijjs RPD Limit Notes Total Kjeldahl Nitrogen 12 0.48 mg/L 12.0 101 90-110 Matrix Spike (4DI1004-MSS) Prepared: 04/11/2014 10:20 Analyzed: 04/14/2014 10: 10 Source: C312928-01 Spike Source. %REC RPD ADdlYte Result Elan QO.L Units Level Rat %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 5.6 0.48 mg/L 4.79 1.1 93 90-110 Matrix Spike Dup (4DI1004-MSD1) Prepared: 04/11/2014 10:20 Analyzed: 04/1412014 10:12 Source: C312928-01 Spike Source %REC RPD Analvte Result Ela4 POL Unite Level Result %REC Limits RPD Lialjt Notes Total Kjeldahl Nitrogen 6.3 0.48 mg/L 4.79 1.1 109 90-110 12 10 QM-11 Batch 4D11005 - Same Blank (4D11005-BLK3) Prepared: 04/11/2014 10:20 Analyzed: 04/14/2014 12:21 Spike Source %REC RPD Analvte Result Ella POL Units Level Result %REC Limits RPD Limit dotes Phosphorus 0,025 U 0.10 mg/L LCS (4D1100S-BS1) Prepared: 04/11/2014 10:20 Analyzed: 04/14/2014 12:23 Spike Source %REC RPD ADalvt Result EIa2 POL Units Level Result %REC its RPD Limit Notes Phosphorus 1.6 0.10 mg/L 1.60 97 90-120 Matrix Spike (41311005-MSS) Prepared: 04/11/2014 10:20 Analyzed: 04/14/2014 12:26 Source:C312928-01 Spike Source %REC RPD And1Yt+: Result Hag POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 0,94 0.10 mg/L 0.640 0.28 102 80-120 FINAL This report relateS only Lo the sample as received by the laboratory, and may only Oe reproduced in full. Page 7 of 10 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4DI1005 - Same - Continued Matrix Spike pup (4D31005-MSDi) Prepared: 04/11/2014 10:20 Analyzed: 04/14/2014 12:28 Source: C312928-01 Spike Source %REC RIND Anal YiC Result flag E41 units Level Result %REC Limits RPD Limit Notes Phosphorus 0.91 0.10 mg/L 0.640 0.28 99 80-120 2 25 FINAL Thls report felates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 10 (9�1 www.encolabs.com FLAGS/NOTES AND DEFINITIONS 8 The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. R-Di The Reporting Limit for this analyte has been raised to account for matrix interference. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduoeci in full. Page 4 of 10 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com s Orlando. FL32824 Dr, 4010 ,racic5onvill�Btr R 322$661]6,51rk Coun, ire 111 C.R y N 271il1ds Industrial Cr, f (407) 826.5314 Fox (407) 860 6045 (904) 296-3W7 Fax (904) 29"210 (919) 467-3090 FeK (919) 467-3515 Page of r Client Name Pre)ect Number Requested Analyses Requested Turnaround 7}., .-,rl, a Af:�ri. Mr1-r,rir'n rnarl;i+t��1 ;n vs•� Times Address Project Naine/Desc rNote: nusn requests subject to 7 acpeprarK.•e by Ihu lacilily l� F=r, � {-.lrn •# l:jltilcil f,^.a:i S.:r }r d,7ic•r iF,[Irx: City,STfbp PO 0 1 Billing Info V i-r�rk I' Tl i, €•if : /L� 5 3 '3tIf, of.13 Standard j Tel Fax Reporting Contact „"i c ' _ Expedited Sampler(s) Name. Affillatlm {Print) Bilhng•Contacl( r. /y Due I 1_ Sampler(s) gmtu Site Location I T rre Zone --' 11 „' ` _ 4 Lab Workordee.;-'x?'•^`''� U. Preservation (See Codes) {Combine as necessary) Collection Matrix Total b of { )tam y Samplo ID (Field Wenti!icaoon) (�CoP�occton Date Tmb Comp ! Grab (see codas) Containers { Sample Comments _z_': L-... x. .... x.... -. <- I - i a p ti y r 1'a Ltt i ' <-- Total iF of Container Sample rot Prepared By Datemme RelirKluished By ` Data(T-ime ?, Receh - By ,-- - , -- --- Datn/Timr � .7_1,w_ 1 '7� Corrcnents.'Speciall1eporting nequiremonts t Fleiutquished By Dam(Time Recefce4 By Date/ivne Relnquished By Datafrime Rec6i By Date/rime C.Poler 1's 8 Temps C ]CondtiUnacceptablen Receipt - -] Acceptable Match : GW GroLridwato 6O Sail DW Drinking Water SE-Sodiment SW Surtaeo Water WW-Wastewater A -Air O-Other (detau it comments) Preservation: Hoe H-HCI "NO3 S-1-1211O4 NO-NaOH O.OViae (detail in comments) We 7 All samlAes sibml[rod to ENCO Labs are In accordance with the terms and mridltlnns listed on the reverse DI this ?arm. unlam print wrurnn agreemanre exm STORIhIWATER DISI. ARGE OUTFALL (SDO) GENERAL PERMIT NO. NCG200000 DISCHARGE MONITORING REPORT (DMR) CERTIFICATE OF COVERAGE NCA. NCG2000448 FACILITY NAME(ii-,W ,., Go,2i6n PcyUi;nel -W- i'1'lpuwi'A'-h 6e-(yd'-n PERSON COLLECTING SAMPLES ' -/ CERTIFIED LABORA'TORY k5V i Ut Lab# 4q Lab it COUNTY j6vrKe. PHONE NO. (gaL�j 3,� - Part A: Specific Monitoring Requirements j1Vi'a'i1brjgiijal aua one copy't- - r,' SAMPLES COLLECTED DURING 14, "Divjstoti oiWatef Qlilrij+b� CALENDAR YEAR: k r�..-•3� �Atfri..�eiitral;Ft�es-.,,`..�`.,:ti�i� •�";F',Y. ` (This monitoring report is due at the Division no r z r , later than 30 days from the date the Facility ;161 Ivtail Service Cehtei 't�< , ' Y Y receives the sampling results from the laboratory.► Raletgh�;Noitl��Cato�ina,276�9,;; 6;17 Outfall No. Date Saiiiple Collected itiolddl' i Total Raiiifali iriclies 0053U 00340. 00556.. 00400 01113 01119 00980 01114 01094 Total Sitspended Soadi in /I Cliemical Oatygeii Deinaiid hi /l.. Oil & Grease lii I - pH s:u. Cadinium In/4 Copper nt /l __ lion nj II Lead In/1 Zinc m l Bencliniarlk , - - 100 120 30 . 6.0 - 9A O:OU1. 0:007 NIA 0.03 0.067 o©i (W JO i4 o, ,Z 5. (61 7.5 01 00 1 C3 0,05 NIA a). (h rU ), ' If a value is in excess of the benchmark, or outside the benchmark range (for pH), you. ttlUst implement the Tier I or Tier 2 responses in the General Permit. Total recoverable. Only complete Part B if this facility uses more tljart 55 gallons of new motor oil pet• month. Part B: Velticle Maintenance Activity Monitorinst Requirements Odtfall No. Date Siiinple Collected niiildd/yr 'Total Rainfall liiciies Neiv Motor Oil Usage. allniontti 00530. 00400. 0055E Total Suspended Solids rii" pH Mi. Oil & Gre.ise jIl'll 136ichiiiai•k - - - 100 6:0 = 9.0 30 RECEIVED MAR I I ZW4 CENTRAL FILEc- DWOIBOG YOU MUST SIGN 'THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared raider my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who manage the system, or those persons directly respous'sble fbr gathering Ilie information, the information submitted is, to the best of n►y knowledge and belief, true, accurate, and complete. I atn aware that there are significant penalties for submitting false irtfonnation, including the possibility of fines and imprisonment for knowing violations." (Sig[ of Permi NCG200000 R (3 06/19 (Date) Form SWU-256 Page I of l STORMWATER DISCHARGE OUTFALL (SDO) GENERAL PERMIT NO. NCG200000 DISCHARGE MONITORING REPORT (DMR) CERTIFICATE OF COVERAGE NO.-,NCG20®©©® FACILITY NAME (a' rJ 41 '---drr, KK ycl n A Y`nou'n-I-q PERSON COLLECTING SAMPLES eti u a T S J CERTIFIED LABORATORY -4-14eWlIlf- Y c Lab # CU Lab # COUNTY PHONE NO. Part A: Specific Monitorine Requirements Mail'orig)nal and one copy to: SAMPLES COLLECTED DURING Division of Water Quality CALENDAR YEAR: Attn: Central Files (This monitoring report is due at the Division no 1617 Mail Service Center later. than 30 days from the date the facility Raleigh, North Carolina 27699-1617 receives the sampling results from the laboratory.) Pow C�n� Outfall No. Date Sample Collected mold Total Rainfall inches 00530 00340 00556 00400 01113 01119 00980 01114 01094 Total Suspended Solids m9a Chemical Oxygen , Demand m Oil & Grease pH s.u. Cadmium MO Copper na Iron m Lead Zinc Benchmark - - 100 120 30 6.0 - 9.0 0.001 0.007 NIA 0.03 0.067 If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier l or Tier 2 responses in the General Permit. 2 Total recoverable. Only complete Part B if this facility uses more than 55 gallons of new motor oil per month. Part B: Vehicle Maintenance Aedvi Mo toring Re uirements Outfan No. Date Sample Collected mo/dd/yr Total Rainfall Inches New Motor Oil Usage al/month 00530 00400 00556 Total Suspended Solids RW pH s.u. Oil & Grease Benchmark - - - 100 6.0 - 9.0 30 FEB I r "ENTRA DWG? YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "l certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete: I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature o ttee) (Date) NCG200000 DMRV ✓ Form SWU-256 Page IofI