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HomeMy WebLinkAboutNCG060329_COMPLETE FILE - HISTORICAL_20190103STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT N0. DOGTYPE )4 HISTORICAL FILE ❑ MONITORING REPORTS DOC DATE ❑ aoi � a� D3 YYYYMMDD Mid Atlantic Engineering & Environmental Solutions 1125 E. Morehead Street, Suite 104 Charintte, NC 2S204-2849 Office: 980. 58S. 1271 F a c si mile: 980. 585.1272 MAAONLINE.COM December 19, 2018 W6- 0303Q 9 Mr. Brendan Conway Honda Power Equipment Manufacturing, Inc. Post Office Box 37 Swepsonville, North Carolina 27359 Subject: Storm Water Sampling Event — December 2018 j�N p 3 �415 Honda Power Equipment t=tLES Swepsonville, Alamance County, North Carolina SECTION Mid -Atlantic Project: 00OH1208.00 Dear Mr. Conway: On December 1, 2018, Mid Atlantic Associates, Inc. (Mid -Atlantic) completed a storm water sampling event at the Honda Power Equipment Manufacturing facility located in Swepsonville, North Carolina. The rain event occurred on December 1, 2018, and it began at approximately 1:30 pm and ended at approximately 11:30 pm. Stormwater samples were collected at four discharge locations (HPE-01, HPE-02, HPE- 03 and R&D-01) on the subject property. After collection, the samples were delivered to Prism Laboratories, Inc. (Prism) in Charlotte, North Carolina for analysis. Copies of the Stormwater Monitoring Records for this sampling event are provided in Attachment A. The analytical results are presented in summary form in Attachment B. A copy of the laboratory report is included in Attachment C. Sampling was conducted by Carl Hewett of Mid -Atlantic. Mid -Atlantic appreciates the opportunity to provide our environmental services on this project. Please do not hesitate to calf if you have questions or need additional information. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Carl H. Hewett Greg D. Icenhour, P.G., MBA Senior Project Manager Principal Geologist EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER MONITORING RECORD Sampling Summary Site: Honda Power Equipment 3721 NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: December 1, 2018 Storm Event Approximate Start: 1:30 pm, December 1, 2018 Approximate End: 11:30 pm, December 1, 2018 Storm Duration: approximately 10 hours Rainfall: 0.34 inches Sampling: sampled discharge point HPE-01 at 6:30 pm (1830) sampled discharge point HPE-02 at 7:15 pm (1915) sampled discharge point HPE-03 at 8:00 pm (2000) sampled discharge point R&D-01 at 8:45 pm (2045) Analytical Testing: TSS by SM 2540D oil and grease by EPA Method 1664B volatile organics by EPA Method 624.1 semi -volatile organics by EPA Method 625.1 PCBs/pesticides by EPA Method 608.3 copper, lead, zinc by EPA Method 200.7 Sampled By: Carl Hewett Mid Atlantic Associates, Inc. 1125 East Morehead Street, Suite 104 Charlotte, North Carolina 28204 Notes: + Storm duration and rainfall amount obtained from the National Weather Service daily summary for Burlington, North Carolina. Page 1 of 1 ATTACHMENT A Stormwater Monitoring Records STORMWATER MONITORING RECORD Qualitative 6bter-vatiojis Site-.' Honda P' %uer Equipment Highway 37zl- -N- igV v 119 Sweosohville,.Nbrth 'Caibllha 27359 Monitoring Date: Saiiiphe Location! pH Results: I Decembcir,l;,1618 Hp(=di Discharge Rating CommentsCharacteristic Color Aj POY45 Odor pdrity Fibatibg S61ids Sq,6efid6d Solids FOain /v 04- Oi Sheeh Oiher obwous- indicators - Characteristic rating qcale.- none, slight, minor; medium, heavy Monitoring sheet shecompleted ted by:Date':: - - � .. - - STORMWATER MONITORING RECORD Qualitative Observations is . - .. p -I.. - _. .. Site: Honda Powef EquJorn6fit 3721 NC highway 119 SwL-p§66vik, North Ca"rbliha 27359 Wnitoring bate: Decenl'bejr i, 2018 S6ffioid Location: pHResults: HPE702 Dikhargq Characteristic Rating !Com'. hnehts Color Pdoi elarity. f#K&P Floating.Solids N&K .Suspended. ofijs Foam oil Sheen N&e OtHir obvious indicatibrs pf-stormwilteLpallution Characteristic rating scale: nbh,6, slight, minor,.medium, heavy - M.6pliori,hi §heet.cbTW6t&d by.' STORMWAT.ER MONITORINGRECORD QU61hative bbser'Miohs site: H6M6 P6wer ifq6-11pm-ent 3721 NC 1-110waV 119 SwepsotMIIO, North Cardliha 27359 Wnitoiri - ng Nip: ()ecember 1, 2018 Sample .Locatibh: HPE-03 pk RL&sijlts: Discharge Characteristic Rating Comments Color Odor 44C clarity Flbifii"4 Solids SOpeqd&d- S'blids Foam Oil Shi-Lin Oth6io,bVious indicators o1stormwaterp011Ut-10h tharac'teristic rating'scdle: none, sfight,'minor, mWiUM, hedvy, Monitoring sKeOt completed tedb�.' 6die: SfORMW.ATER MONITORING RECORD Q01itat.i.ve Observations Site: Honda Po.wer Equiprfi4nt 3721 NC Hithway 119 § W,160sonvillci, North Oroiflha 27359 Monitoring onitor,ing Date; Dec *rber i, 20i8 sample L66iti 6ri: R&D-:01 pH Results: Discharge Rating Comments Color Color Oddr Clarity a hty 7r Floating Solids Suiperided Solids Foam Oil She'en dth6r.o6vious indicators chbieCtmstic rating 5COle: noire, slight qhtminor, medium, heavy Mvnitorirrg sheet completed N:.— - Dbte: 4;H10 TABLE Stormwater Analytical Results — December 2018 Honda Power Equipment Swepsonville, Alamance County, North Carolina HPE-01 HPE-02 HPE-03 R&D-01 Benchmark Values pH 6.79 6.59 7.18 6.52 6-9 total suspended solids (TSS) 4.1 120 14 160 100 EPA Method 200.8 (ug/L) copper BDL BDL BDL BDL 7 lead BDL BDL BDL BDL 30 zinc 46 BDL 50 BDL 67 EPA Method 608 (ug/L) target pesticides BDL BDL BDL BDL 1000 EPA Method 608 target PCBs BDL BDL BDL BDL 1000 EPA Method 624 (ug/L) trichloroethylene BDL BDL BDL 3.4 1000 other target volatile compounds BDL BDL BDL BDL 1000 EPA Method 625 (ug/L) target semi -volatile compounds BDL BDL BDL BDL 1000 EPA Method 1664 (mgA) oil and grease BDL it F BDL BDL 15 Notes: • Total suspended solids (TSS) and oil and grease presented in milligrams per liter (mg/L). • Other analytical results presented in micrograms per liter (ug/L). • BDL—below laboratory minimum cluantitation limits Stormwater samples collected on December 1, 2018 by Mid -Atlantic personnel. Full -Service Analytical 8 Environmental Solutions Mid -Atlantic Associates, Inc. - Charlotte Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 NC Certification No. 402 NG drinking Water Cert No. 37735 SC Certification No. 99012 Project: Honda Power Equipment Lab Submittal Date: 12/03/2018 Prism Work Order: 8120033 Case Narrative 12/17/2018 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference: Reviewed By Terri W. Cole For Angela D. Overcash Project Manager A CCV result is below range on the primary column, but passes on the secondary column. The analyte is not detected in the sample down to the MDL. No further action taken. D RPD value outside of the control limits. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.Q. Box 240543 - Charlotte, NC 28224-0543 Phone: 704152M364 - Toll Free Number: 1-8001529-0364 - Fax: 7441525-0409 Page 1 O7 29 .� Sample Receipt Summary 4 JP R IS M Fuh-Service Solu& Enviranmanfal ai Solutiotio ns 1211712018 w�Yar.ra �c Prism Work Order: 8120033 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date[Time Received HPE-01 8120033-01 Water 12/01/18 18:30 12/03/18 15:23 HPE-02 8120033-02 Water 12/01/18 19:15 12/03/18 15:23 HPE-03 8120033-03 Water 12/01/18 20:00 12/03/18 15:23 Samples were received in good condition at 3.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364-Fax: 7041525-0409 Page 2 of 29 JOz�—,"R-,L M Fui iService al Solutio sEnvironmental Sol�lians �_ Summary of Detections 12/17/2018 Prism Work Order: 8120033 Prism ID Client ID Parameter Method Result Units 8120033-01 HPE-01 Total Suspended Solids 'SM2540 D 4.1 mg1L 8120033-01 HPE-01 Zinc zoa.7 0.046 mg1L 8120033-02 HPE-02 Oil & Grease (HEM) •1664B 11 mg/L 8120033-02 HPE-02 Total Suspended Solids •SM2540 D 120 mg1L 8120033-03 HPE-03 Total Suspended Solids •SM2540 D 14 mg1L 8120033-03 HPE-03 Zinc 200.7 0.050 mg/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spring brook Road • P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529 6364 - Toll Free Number: 1.8001529-6364 - pax: 7041525-0409 Page 3 of 29 ,)��R, RaFull-Sarvice Analytical.::-�� I S M I Environmental Solutions � -%,W_ Laboratory Report . 12r17)2018 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID: HPE-01 Attn: Carl Hewett Prism Sample ID: 8120033-01 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120033 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 18:30 Time Submitted: 12/03/18 15:23 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID General Chemistry Parameters Oil 8 Grease (HEM) BRL mg1L 5.0 1.4 1 '16648 12/11118 9:46 SLS P61-0155 Total Suspended Solids 4.1 mg/L 2.5 0.40 1 'SM2540 ❑ 12/6/18 15:55 CBP PBL0074 Organochlorine Pesticides by GCIECD alpha-BHC BRL A ug/L 0,052 0.010 1 608.3 12/10/18 12:54 ZRC PSL0044 beta-BHC BRL ug1L 0.052 0.017 1 608.3 12/10/18 12:54 ZRC P81-0044 gamma-BHC BRL ug1L 0.052 0,014 1 608.3 12/10/18 12:54 ZRC P81_0044 delta-BHC BRL ugIL 0.052 0.015 1 608.3 12110/18 12:54 ZRC P81_0044 Heptachlor BRL ug/L 0.052 0.018 1 608.3 12/10/18 12:54 ZRC P81_0044 Aldrin BRL ug1L 0.052 0.016 1 608.3 12/10/18 12:54 ZRC P8L0044 Heptachlor Epoxide BRL ug1L 0.052 0.014 1 608.3 12/10/18 12:54 ZRC P81-0044 trans -Chlordane BRL ug1L 0.052 0.027 1 608.3 12/10/18 IZ54 ZRC PBL0044 Endosulfar I BRL ug1L 0.052 0.020 1 608.3 12/10/18 12:54 ZRC P81_0044 cis -Chlordane BRL ug/L 0.052 0.043 1 608.3 12/10118 12:S4 ZRC PSL0044 Dieldnn BRL ug/L 0,052 00015 1 608.3 12/10/18 12:54 ZRC P8L0044 4,4'-DDE BRL ug1L 0.052 0.011 1 608.3 12/10/18 12:54 ZRC P81-0044 Endrin BRL ug1L 0.052 0.016 1 608.3 12/10/18 12:54 ZRC P81-0044 Endosulfan II BRL ug/L 0.052 0.017 1 608.3 12110/18 12:54 ZRC P81_0044 4,4'-DDD BRL ug/L 0.052 0.021 1 608.3 12/10/18 12:54 ZRC P81_0044 Endrin Atdehyde BRL ug1L 0.052 0.030 1 608.3 12/10/18 12:54 ZRC P81_0044 Endosulfan Sulfate BRL ug/L 0.052 0.017 1 608.3 121l0118 12:54 ZRC P8L0044 4,4'-DDT BRL uglL 0.052 0.025 1 608.3 121l0118 12:54 ZRC POL0044 Endrin Ketone BRL ug1L 0.052 0.032 1 608.3 12/10118 12:54 ZRC PSL0044 Methoxychlor BRL ug/L 0.052 0.041 1 608.3 12110/18 12:54 ZRC PSL0044 Chlordane BRL ug/L 0.52 0.18 1 606,3 12/10/18 12:54 ZRC PSL0044 Toxaphene BRL ug/L 0.52 0,077 1 608.3 12/10/18 12:54 ZRC P81_0044 Aroclor 1016 BRL ug/L 0.52 0.28 1 608.3 12110/18 12:54 ZRC P81_0044 Aroclor 1221 BRL ugfL 1.0 0.11 1 608.3 12/10/18 12:54 ZRC P8L0044 Aroclor 1232 BRL ug1L 0.52 0.17 1 608.3 12/10/18 12:54 ZRC PBL0044 Aroclor 1242 BRL ug/L 0.52 0.15 1 608.3 12/10118 12:54 ZRC P8L0044 Aroclor 1248 BRL ug1L 0.52 0.15 1 608.3 12110/18 12:54 ZRC PSL0044 Aroclor 1254 BRi. ug/L 0.52 0.17 1 608.3 12110/18 12:54 ZRC P81_0044 Arocor 1260 BRL ug1L 0.52 0.33 1 608.3 12110/18 12:54 ZRC P81_0044 Surrogate Recovery Control Limits Tetrachloro-rn-xylene 72 % 40-134 Decachlarobiphenyl 69 % 13-156 Semivolatile Organic Compounds by GCIMS 1,2,4-Trichlorobenzene BRL ug1L 11 1.6 1 625.1 1217118 17:56 JMV PBL0067 1,2-Dichlorobenzene BRL ug1L 11 1.5 1 625.1 1217118 17:56 JMV PBL0067 1,2-Diphenylhydrazine (as Azobenzene) BRL ug1L 11 3.1 1 625.1 1217/18 17:56 JMV P81_0067 1,3-Dichlorobenzene BRL ug1L 11 1.4 1 625.1 128118 17:56 JMV P81_0067 1,4-Dichlorobenzene BRL ug/L 11 1.5 1 625.1 12r7118 17:56 JMV P81-0067 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364-Tall Free Number; 1-8001529-6364- Fax: 704152"409 Page 4 of 29 + Full -Service Analytical 8 ORISMI Environmental Solutions Mid -Atlantic Associates, Inc. -Charlotte Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Project: Honda Power Equipment Sample Matrix: Water Laboratory Report 12/17/2018 Client Sample ID: HPE-01 Prism Sample ID: 8120033-01 Prism Work Order: 8120033 Time Collected: 12/ 11i8 18:30 Time Submitted: 12/03/18 15:23 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datefrime ID 2,4,6-Trichlorophenol BRL uglL 11 2.0 1 625.1 12/7/18 17:56 JMV P8L0067 2,4-Dichloraphenal BRL ug1L 11 1.7 1 625.1 1 2f711 8 17:56 JMV PSL0067 2,4-Dimethylphenol BRL ugIL 11 2.3 1 625.1 1 2f711 8 17:56 JMV PBL0067 2,4-Dinitrophenol BRL ug1L 11 1.3 1 625.1 12f7118 17:56 JMV P81-0067 2,4-Dinitrotoluene BRL ug1L 11 3.2 1 625.1 1 2f711 8 17:56 JMV PSL0067 2,6-Dinitrotoluene BRL ug1L 11 3,2 1 625.1 12n118 17:56 JMV P81_0067 2-Chloronaphthalene BRL ug1L 11 2.5 1 625.1 12f7118 17:56 JMV P8L0067 2-Chlorophenol BRL uglL 11 1.2 1 625.1 1217/18 17:56 JMV PSL0067 2-Nitraphenol BRL uglL 11 1.5 1 625.1 1217118 17:56 JMV P8L0067 3,3'-Dichlarobenzidine BRL ug1L 11 3.0 1 625.1 12f7116 17:56 JMV P81-0067 4,6-Dinitro-2-methylphenol BRL ug1L 11 2.1 1 625.1 12f7118 17:56 JMV P8L0067 4-Bromophenyl phenyl ether BRL uglL 11 3.4 1 625.1 12f7118 17,56 JMV P81_0067 4-Chloro-3-methyl phenol BRL uglL 11 2.5 1 625.1 1217118 17,56 JMV PBL0067 4-Chlcrophenyl phenyl ether BRL ug1L 11 2.4 1 625.1 12/7/18 17:56 JMV P81_0067 4-Nitrophenol BRL ug1L 54 1.8 1 625.1 1217118 17:56 JMV P81_0067 Acenaphthene BRL ug1L 11 2.5 1 625.1 1 2f711 8 17:56 JMV PSLOos7 Acenaphthylene BRL uglL 11 2.5 1 625A 12f7118 17:56 JMV P8L0067 Anthracene BRL ug1L 11 3.4 1 625.1 1217118 17:56 JMV P8L0067 Benzidine BRL ug1L 110 15 1 625.1 12f7118 17:56 JMV P81_0067 Benzo(a)anthracene BRL uglL 11 3.4 1 625A 12f7118 17:56 JMV P81_0067 Benzo(a)pyrene BRL ug1L 11 3.9 1 625.1 12f7118 17:56 JMV PSL0067 Benzo(b)fluoranthene BRL ug1L 11 3.8 1 625.1 128118 17:56 JMV PSL0067 Benzo(g,hJ)perylene BRL ug1L 11 3.8 1 625.1 12r7118 17:56 JMV PSL0067 Benzo(k)fluoranthene BRL ug1L 11 4.2 1 625.1 1 Z711 8 17:56 JMV PSL0067 bis(2-Chloroethoxy)methane BRL uglL 11 1.9 1 625.1 12f7118 17:56 JMV POL0067 Bis(2-Chlomethyl)ether BRL uglL 11 1.8 1 625.1 12f7118 17:56 JMV POL0067 Bis(2-chleroisopropyl)ether BRL uglL 11 1.8 1 625.1 12r711S 17:56 JMV P8L0067 Bis(2-Ethylhexyl)phtharate BRL uglL 11 3.4 1 625.1 1217lis 17:56 JMV PBL0067 Butyl benzyl phthalate BRL uglL 11 2.8 1 625.1 1217118 17:56 JMV PBL0067 Chrysene BRL uglL 11 3.7 1 625.1 12f7118 17:56 JMV PBL0067 Dibenzo(a,h)anthracene BRL ug1L 11 3.7 1 625.1 12r7118 17:56 JMV PSL0067 Diethyl phthalate BRL uglL 11 2.5 1 625.1 1217/18 17:56 JMV P8L0067 Rimethyl phthalate BRL uglL 11 1.7 1 625.1 12/7/18 17:56 JMV P8L0o67 Di-n-butyl phthalate BRL uglL 11 3.6 1 625.1 1217118 17:56 JMV P8L0067 Di-n-octylphthalate BRL uglL 11 3.9 1 625.1 1Wit 8 17:56 JMV PBL0067 Ruaranthene BRL uglL 11 3.8 1 625.1 1 2f711 8 17:56 JMV P8L0067 Ftuorene BRL uglL 11 3.0 1 625.1 1217/18 17:56 JMV P81_0067 Hexachlorobenzene BRL uglL 11 2.7 1 625.1 12f7118 17:56 JMV P8L0067 Hexachlorobutadiene BRL uglL 11 2.2 1 625.1 12f7118 17:56 JMV P81_0067 Hexachlarocyclopentadiene BRL ug1L 11 1.8 1 625.1 12f7118 17:56 JMV P81_0067 Hexachloroethane BRL ug1L 11 1.6 1 625.1 1217118 17:56 JMV P81_0067 Indeno(1,2,3-cd)pyrene BRL uglL 11 3.3 1 625.1 12f7118 17:56 JMV P81_0067 Isophorone BRL ug1L 11 2.3 1 625.1 12f7118 17:56 JMV P81_0067 This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704I525-0409 Page 5 of 29 AL_Xl�m Laboratory Report R I S M Full -Service Analytical& Enviranmantal Solutions 12/17/2018 we Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID: HPE-01 Attn: Carl Hewett Prism Sample ID: 8120033-01 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120033 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 18:30 Time Submitted: 12/03/18 15:23 Parameter Result Units Report MDL Limit Dilution Factor Method Analysis Analyst Datefrime Batch I❑ Naphthalene BRL uglL 11 2.2 1 625.1 1217118 17:56 JMV PBL0067 Nitrobenzene BRL ug1L 11 1.5 1 625.1 12/7/18 17:56 JMV P8LOC67 N-Nitrosodimethylamine BRL uglL 11 0.90 1 625.1 1217118 17:56 JMV P81-0067 N-Nitroso-di-n-propylamine BRL uglL 11 2.2 1 625.1 1217118 17,56 JMV P81-0067 N-Nitrosodiphenylamine BRL ug1L 11 3,2 1 625.1 12f7118 17:56 JMV P81-0067 Pentachlorophenol BRL uglL 11 2.3 1 625.1 12f7118 17:56 JMV PBL0067 Phenanthrene BRL uglL 11 3.5 1 625.1 1217118 17:56 JMV PBL0067 Phenol BRL uglL 11 0.52 1 625.1 12f7118 17:56 JMV P81_0067 Pyrene BRL uglL 11 3.8 1 625.1 1 2f711 8 17:56 JMV P81_0067 Surrogate Recovery Control Limits 2,4,6-Thbromophenoi 88 % 31-144 2-Fluorobiphenyl 83 % 49-118 2-Flucrophenol 52 % 22-84 Nitrobenzene-d5 76 % 43-123 Phenol-d5 34 % 10-63 Terphenypol4 83 % 49-151 Total Metals Copper Lead Zinc Volatile Organic Compounds by GCIMS BRL BRL 0.046 mg1L mg1L mg1L 0.010 0.0050 0.030 0.0010 0.0010 0.0013 1 1 1 '200,7 '200.7 `200.7 1216/18 17:48 1216118 17:48 12/6118 17:48 JAB JAB JAB P81-0062 PBL0062 1381-0062 1,1,1-Trichloroethane BRL uglL 1.0 0.061 1 624.1 12/13/18 16:18 KDM 1381-0185 1,1,2,2-Tetrachloroethane BRL ug1L 1.0 0.036 1 624A 12113/18 16:18 KDM P81-0185 1,1,2-Trichloroethane BRL uglL 0.50 0.066 1 624.1 12113/18 16:18 KDM 1381-0185 1,1-Dichloroethane BRL uglL 1.0 0.083 1 624.1 12/13/18 16:18 KDM P81-0185 1,1-Dichloroethylene BRL ug1L 1.0 0.083 1 624.1 12113/18 16:18 KDM P81_0185 1,2-Dichlorobenzene BRL uglL 1.0 0.076 1 624,1 12/13/18 16:18 KDM P81_0185 1,2-Dichloroethane BRL ug1L 1.0 0.066 1 624.1 12113118 16:18 KDM P80185 1,2-Dichloropropane BRL ug1L 1.0 0.11 1 624.1 12113118 16:18 KDM P80185 1,3-Dichlorobenzene BRL ug1L 1.0 0.054 1 624.1 12/13/18 16:18 KDM PBLO185 1,4-Dichlorobenzene BRL uglL 1.0 0,050 1 624.1 12113/18 16:18 KDM PSLO185 2-Chlcroethyt Vinyl Ether BRL uglL 10 0.37 1 624.1 12113/18 16:18 KDM PSLO185 Acrolein BRL uglL 5,0 0.20 1 624.1 12113/18 16:18 KDM PSLO185 Acrylonitriie BRL uglL 5,0 0.20 1 624.1 12113/18 16:18 KDM P81-0185 Benzene BRL ug1L 0.50 0.048 1 624.1 12113/18 16:18 KDM P8L0185 Bromodichloromethane BRL uglL 1.0 0.062 1 624.1 12/13/18 16:18 KDM P8Lo185 Bromofonn BRL uglL 1A 0.040 1 624.1 12/13/18 16:18 KDM PSLO185 Bromomethane BRL ug1L 2.0 0.18 1 624.1 12/13118 16:18 KDM P8L0185 Carbon Tetrachloride BRL uglL 1.0 0.11 1 624.1 12/13/18 16:18 KDM P8L0185 Chlorobenzene BRL ug1L 1.0 0.062 1 624.1 12/13118 16:18 KDM PSLO185 Chloroethane BRL ug1L 1.0 0.22 1 624.1 12/13/18 16:18 KDM P81_0185 Chloroform BRL ug1L 1.0 0,076 1 624.1 12/13118 16:18 KDM 1381-0185 Chloromethane BRL ug1L 1.0 0.079 1 624.1 12/13118 16:18 KDM PBL0185 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8061529-6364 - Fax: 704/525-0409 Page 6 of 29 Laboratory Report t FullsAnalytical & LPRMEnvironrnecntalSoluticnS w 1211]1201� Mid-Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID: HPE-01 Attn: Carl Hewett Prism Sample ID: 8120033-01 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120033 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 18:30 Time Submitted: 12/03/18 15:23 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daterrime tD cis-1,3-Dichloropropylene BRL ug1L 1.0 0.079 1 624.1 12/13118 16:18 KOM P8L0185 Dibromochloromethane BRL UM 1.0 0.081 1 624.1 12/13/18 16:18 KDM P81_0185 Ethylbenzene BRL ug/L 1.0 0.061 1 624.1 12/13/18 16:18 KDM P81-0185 Methylene Chloride BRL ug/L 2,0 0.083 1 624.1 12/13/18 16:18 KDM P81-0185 Tetrachtoroethylene BRL uglL 0,75 0.098 1 624A 12/13/18 16:18 KDM P81-ol85 Toluene BRL ug/L 1.0 0.044 1 624.1 12/13/18 16:16 KDM P81-ol85 trans-1,2-Dichloroethylene BRL ug1L 2.0 0.094 1 624.1 12/13/18 16:18 KDM P8Lo185 trans-1,3-Dichlorcpropylene BRL ug1L 1.0 0.070 1 624.1 12/13118 16:18 KDM P8Lo185 Trichloroethylene BRL ug1L 1.0 0.078 1 624.1 12/13/18 16:18 KDM P81-0185 Trichlorofluoromethane BRL ug1L 1.0 0.062 1 624.1 12113/18 16:18 KDM P81_0185 Vinyl chloride BRL u91L 1.0 0.097 1 624.1 12/13/18 16:18 KDM P81_0185 surrogate Recovery Control Limits 4-Brcmoflucrobenzere 146 % 74-126 Dibromofluaromethane 97 % 75-127 Toluene-d8 98 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 7 of 29 Ps Fu11•Service Anatytical & Environmental Solutions • �yIpRATONEI ANC Laboratory Report . 1211712018 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID: HPE-02 Attn: Carl Hewett Prism Sample ID: 8120033-02 1125 E. Morehead Street, Suite 104 Prism Worm Order: 8120033 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 19:15 Time Submitted: 12/03/18 15:23 Parameter Result Units Report MDL Dilution Method Analysis Ana}yst Batch Limit Factor DaterTime ID General Chemistry Parameters Oil & Grease (HEM) 11 mg1L 5.0 1.4 1 '1664B 12/11118 9:46 SLS P8L0155 Total Suspended Solids 120 mg1L 19 0.40 1 `SM2540 D 1216118 15:55 CBP P8L0074 Organochlorine Pesticides by GCIECD alpha-BHC BRL A ug1L 0.053 0.011 1 608.3 12/10/18 13:06 ZRC P81_0044 beta-BHC BRL ug1L 0.053 0.017 1 608.3 12/10118 13:06 ZRC P81Lt7044 gamma-BHC BRL ug1L 0.053 0.014 1 608.3 12/10/18 13:06 ZRC PSL0044 delta-BHC BRL uglL 0,053 0 015 1 608.3 12110AS 13.06 ZRC PBL0044 Heptachlor BRL ug1L 0.053 0,018 1 608.3 12/10118 13:06 ZRC P81_0044 Aldrin BRL ug/L 0.053 0.016 1 608.3 12/10/18 13:06 ZRC P81_0044 Heptachlor Epoxide BRL uglL 0.053 0.014 1 608.3 12/10/18 13:06 ZRC P8L0044 trans -Chlordane BRL uglL 0.053 0.028 1 608.3 12/10/18 13:06 ZRC P8L0044 Endosulfan I BRL uglL 0.053 0.020 1 608.3 12/10/18 13:06 ZRC PSL0044 cis -Chlordane BRL uglL 0.053 0,044 1 608.3 12/10/18 13:06 ZRC PBL0044 ❑ieldrin BRL ug1L 0.053 0.015 1 608.3 12110/18 13,06 ZRC P81-0044 4,4'-DDE BRL uglL 0.053 0.012 1 608.3 12/10118 13:06 ZRC P81-0044 Endrin BRL ug1L 0.053 0.016 1 608,3 12/10/18 13706 ZRC PBL0044 Endosulfan II BRL uglL 0.053 0.017 1 608.3 12/10/18 13:06 ZRC PSL0044 4,4'-DDD BRL uglL 0.053 Q021 1 608.3 12/10/18 13:06 ZRC P81_0044 Endrin Aldehyde BRL uglL 0.053 0,031 1 608.3 12J10/18 13:06 ZRC P81_0044 Endosulfan Sulfate BRL uglL 0.053 0,017 1 608.3 12110/18 13:06 ZRC PBL0044 4,4'-DDT BRL vglL 0.053 0.026 1 608.3 12110/18 13:06 ZRC P81_0044 Endrin Ketone BRL ug1L 0.053 0.033 1 608.3 12110/18 13:06 ZRC 1381-0044 MethoxycWor BRL uglL 0.053 0.C41 1 608.3 12/10118 13:06 ZRC POLOC44 Chlordane BRL uglL 0.53 0.18 1 608.3 12/10/18 13,06 ZRC PBL0044 Toxaphene BRL uglL 0.53 0.079 1 608.3 121lO/18 13:06 ZRC PBL0044 Aroclor 1016 BRL ug1L 0.53 0.29 1 608.3 12/10/18 13:06 ZRC PSL0044 Aroclor 1221 BRL ug1L 1.1 0.12 1 608.3 12/10/18 13:06 ZRC P81-0044 Arodor 1232 BRL ug1L 0,53 0.17 1 608.3 12110/18 13:06 ZRC PSL0044 Aroclor 1242 BRL ug1L 0,53 0.15 1 608.3 12110/18 13:06 ZRC PBL0044 Aroclor 1248 BRL uglL 0,53 0,15 1 608.3 12/10/18 13:06 ZRC P81_0044 Aroclor 1254 BRL uglL 0.53 0.17 1 608.3 12/10/18 13:06 ZRC P81_0044 Aroclor 1260 BRL uglL 0.53 0.34 1 608.3 12/10/18 13:06 ZRC PBL0044 Surrogate Recovery Control Limits Tetrachloro-m-xylene 79 % 40-134 Decachlorobiphenyl 74 % 13-185 Semivolatile Organic Compounds by GCIMS 1,2,4-Trichlorobenzene BRL ug1L 10 1.5 1 625.1 12r7118 18:18 JMV P81_0067 1,2-Dichlorobenzene BRL ug1L 10 1.4 1 625.1 12r7118 19:18 JMV P8L0067 1,2-Diphenylhydrazine (as Azobenzene) BRL uglL 10 2.9 1 625.1 12r7118 18:18 JMV P81_0067 1,3-Dichlorobenzene BRL ug1L 10 1.3 1 625.1 12r7118 18:18 JMV P81_0067 1,4-Dichlorcbenzene BRL uglL 10 1.4 1 625.1 12f7118 18:18 JMV P81_0067 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 8 of 29 Laboratory Report t i,s 1 Y I ! Full Service Analytical & Environmental Solutions 1 21i712i]1 a waumwcs uic Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID: HPE-02 Attn: Carl Hewett Prism Sample ID: 8120033-02 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120033 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 19:15 Time Submitted: 12/03/18 15:23 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Datefiime Batch ID 2,4,6-Trichlorophenel BRL ug/L 10 1,9 1 625.1 12f7118 18:18 JMV P8L0o67 2,4-Dichlorophenol BRL ug/L 10 1.6 1 625.1 12r7118 18:18 JMV PBL0067 2,4-Dimethylphenol BRL ug/L 10 2.1 1 625.1 12f7118 18:18 JMV P81_0067 2,4-Dinitrophenol BRL ug/L 10 1.3 1 625.1 12f7118 18:18 JMV P81_0067 2,4-Dinitrotoluene BRL ugIL 10 3.0 1 625.1 12/7118 18:18 JMV PSL0067 2,6-Dinitrotoluene BRL ug/L 10 3.0 1 625.1 1217118 18:18 JMV P8L0067 2-Chloronaphthalene BRL ug1L 10 2.4 _ 1 625.1 1217118 18:18 JMV P8L0067 2-Chlorophenol BRL ug/L 10 1.1 1 625.1 1 2f711 8 18!18 JMV PBL0067 2-Nitrophenol BRL ug/L 10 1.4 1 625.1 12f7118 18:18 JMV PSLOO67 3,3'-Dichlorobenzidine BRL ug/L 10 2.8 1 625.1 12f7II8 18:18 JMV PSL0067 4,6-Diniiro-2-methylphenol BRL ug/L 10 1.9 1 625.1 1 2f711 8 18:18 JMV PSL0067 4-Bromophenyl phenyl ether BRL ug/L 10 3.2 1 625.1 1217118 18:18 JMV P81_0067 4-Chloro-3-methylphenol BRL ug/L 10 2.3 1 625.1 12f7118 1&18 JMV P8L0067 4-Chlorophenyl phenyl ether BRL ug1L 10 2.3 1 625.1 1217118 18:18 JMV PSL0067 4-Nitrophenol BRL ugIL 51 1.7 1 625.1 12f7118 ISIS JMV P61_0067 Acenaphthene BRL ug1L 10 2,3 1 625.1 12f7118 18:18 JMV P8L0067 Acenaphthylene BRL ugIL 10 2.4 1 625.1 1217118 18:16 JMV P8L0067 Anthracene BRL ug1L 10 3.2 1 625,1 1217118 18:18 JMV P8L0067 Benzidine BRL ug/L 100 14 1 625,1 1217118 18:18 JMV P81_0067 Benzo(a)anthrace ne BRL ug/L 10 3.2 1 625.1 1217118 18:18 JMV P81_0067 Benzo(a)pyrene BRL ug/L 10 3.7 1 625.1 1217118 18:18 JMV PBL0067 Benzo(b)fluoranthene 8RL ug/L 10 3.6 1 625.1 1217118 18:18 JMV P8L0067 Benzo(g,h,i)perylene BRL ug1L 10 3.6 1 625.1 1217118 18:1B JMV P81_0067 Benzo(k)fluoranthene BRL ug/L 10 3.9 1 625.1 12f7118 18:1B JMV PSL0067 'bis(2-Chloroethoxy)methane BRL ug/L 10 1.8 1 625.1 1217118 18:18 JMV PSL0067 Bis(2-Chloroethyl)ether BRL ug/L 10 1.6 1 625.1 1217118 18:18 JMV PSL0067 Bis(2-chloroisopropyl)ether BRL ug/L 10 1.7 1 625.1 1217118 18:18 JMV PSL0067 8 i s(2- Ethyl h a xyl) p hth a late BRL ug1L 10 3.2 1 625.1 1217118 18:18 JMV PBL0067 Butyl benzyl phthalate BRL ug/L 10 2,6 1 625.1 12/7118 18:18 JMV P81_0067 Chrysene BRL ug1L 10 3.4 1 625.1 1217118 18:18 JMV PBL0p67 Dibenzc(a,h)anthracene BRL ug/L 10 3,5 1 625.1 1217/18 18:18 JMV P81_0067 Diethyl phthalate BRL ugIL 10 2.3 1 625.1 12r7118 18:18 JMV PSL0067 Drmethyl phthalate BRL ug1L 10 1.6 1 625A 1217/18 18:18 JMV PBL0067 Di-n-butyl phthalate BRL ug1L 10 3.4 1 625.1 1217/18 18:18 JMV PSL0067 Di-n-octyl phthalate BRL ugIL 10 3.7 1 625.1 12r7118 18:18 JMV PBL0067 Fluoranthene BRL ugIL 10 3.6 1 625.1 12f7118 18:18 JMV PSL0067 Fluorene BRL ug1L 10 2.8 1 625.1 12f7118 18:18 JMV PSL0067 Hexachlorobenzene BRL ugIL 10 2.5 1 625.1 12RI18 18:18 JMV PBL0067 Hexachlorobutadiene BRL ugIL 10 2.1 1 625.1 1217118 18:18 JMV PBL0067 Hexachlorocyclopentadiene BRL ug/L 10 1.7 1 625.1 12f7118 18:18 JMV PSL0067 Hexachloroethane BRL ug1L 10 1,5 1 625.1 12f7118 18:18 JMV PSL0067 Indeno(1,2,3-cd)pyrene BRL ugIL 10 3.1 1 625.1 12RI18 18:18 JMV PBL0067 Isopharone BRL ug/L 10 2.2 1 625.1 12f7118 18:18 JMV PBL0067 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800152"364 - Fax: 7041525-0409 Page 9 of 29 11` Laboratory Report ,1 \� �1 Fun-Service Analytical & ;J PAR I S M I Environmental Solutions 12I17%2018 ��Li90N�TOlUE9 WC Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID: HPE-02 Attn: Carl Hewett Prism Sample ID: 8120033-02 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120033 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 19:15 Time Submitted: 12/03/18 15:23 Parameter Result Units Report MDL Limit Dilution Factor Method Analysis Analyst Daterrime Batch ID Naphthalene BRL ug1L 10 2.1 1 625.1 12f7118 18:18 JMV P81_0067 Nitrobenzene BRL ug1L 10 1.4 1 625.1 12f7118 18:18 JMV P81_0067 N-Nitrosodimethylamine BRL uglL 10 0.85 1 625.1 12f7118 18:18 JMV P810067 N-Nitroso-di-n-propylamine BRL uglL 10 2,1 1 625.1 1 2f711 8 18:18 JMV P81_0067 N-Nitrosodiphenylamine BRL ug1L 10 3.0 1 625.1 1217118 18:18 JMV PSL0067 Pentachlorophenol BRL ug1L 10 2.1 1 625.1 1217118 18:18 JMV PBL0067 Phenanthrene BRL ug1L 10 3.3 1 625.1 1217118 18:18 JMV PBL0067 Phenol BRL ug/L 10 0.49 1 625.1 12f7118 18:18 JMV P81_0067 Pyrene BRL ug/L 10 3.6 1 625.1 1 2f711 8 18:18 JMV P81_0067 Surrogate Recovery Control Limits 2,4,6-Tribrcmophenol 92 % 31-144 2-Fluorobiphenyl 91 % 49-118 2-Fluorophenol 54 % 22-84 Nitrobenzene-d5 85 % 43-123 Phenol-d5 38 % 10-63 Terphenykd14 92 % 49-151 Total Metals Copper Lead Zinc Volatile Organic Compounds by GCIMS BRL BRL BRL mg/L mg1L mg1L 0.010 0.0050 0.030 0.0010 0.0010 0.0013 1 1 1 '200.7 '200.7 '200.7 12/6118 18:28 1216118 18:28 1216118 18:28 JAB JAB JAB P81_0062 PBL0062 PSL0062 1,1,1-Trichloroothane BRL ug/L 1.0 0.061 1 624.1 12/13118 16:44 KOM P81_0185 1,1,2,2-Tetrachloroethane BRL ug/L 1.0 0.036 1 624.1 12/13118 16:44 KDM PBLO185 1,1,2-Trichlorcethane BRL ug/L 0.50 0.066 1 624.1 12/13/18 16:44 KDM PBLO185 1,1-Dichloroethane BRL ug1L 1.0 0.083 1 624.1 12/13/18 16:44 KDM PSLO185 1,1-Dichloroethylene BRL ug/L 1.0 0.083 1 624.1 12/13/18 16:44 KDM PBLO185 1,2-Dichlarobenzene BRL ug1L 1.0 0.076 1 624.1 12113/18 16:44 KDM P81-0185 1,2-Dichloroethane BRL ugIL 1.0 0.066 1 624.1 12/13/18 16:44 KDM P81-0185 1,2-Dlchloropropane BRL uglL 1.0 0.11 1 624.1 12/13/18 16A4 KDM P81-0185 1,3-Dichlorobenzene BRL ug11- 1.0 0.054 1 624.1 12/13/18 W44 KDM P81_0185 1,4-Dichlorobenzene BRL ug/L 1.0 0,050 1 624.1 12/13/18 16:44 KDM P81_0185 2-Chloroethyl Vinyl Ether BRL ug/L 10 0.37 1 624.1 12/13/18 16:44 KDM PBLO185 Acrolein BRL ug/L 5.0 0.20 1 624.1 12/13/18 16:44 KDM PBLO185 Acrylonitrile BRL ug1L 5.0 0.20 1 624.1 12/13/18 16:44 KDM PBLO185 Benzene BRL uglL 0.50 0.048 1 624A 12/13/18 16:44 KOM PBLO185 Bromodichloromethane BRL uglL 1.0 0.062 1 624.1 12/13/18 16:44 KDM PBL0185 Bromoform BRL ug1L 1.0 0.040 1 624.1 12/13/18 16:44 KDM P81_0185 Bromomethane BRL ug1L 2.0 0.18 1 624,1 12/13/18 16A4 KDM P81-0185 Carbon Tetrachloride BRL uglL 1.0 0.11 1 624.1 12/13/18 16:44 KDM P81-0185 Chlorobenzene BRL ug1L 1.0 0.062 1 624.1 12/13/18 16:44 KDM P81-0185 Chloroethane BRL ug1L 1.0 0.22 1 624.1 12113/18 16:44 KDM P81_0185 Chloroform BRL ug1L 1.0 0.076 1 624.1 12/13/18 16:44 KDM PBLO185 Chloromethare BRL ug1L 1.0 0.079 1 624.1 12113118 16:44 KDM P81_0185 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 10 of 29 .r . Laboratory Report �. Environmental Solulians nhp'l I S M Full -Service al solutions s 12/17/201 8 %ueawaarnra. v Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID; HPE-02 Attn: Carl Hewett Prism Sample ID: 8120033-02 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120033 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 19:15 Time Submitted: 12/03118 15:23 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daterrime ID cis- 1,3-Dichloropropylene BRL ug1L 1.0 0.079 1 624.1 12/13/18 16:44 KDM P81_0165 Dibromochloromethane BRL ug1L 1.0 0.081 1 624.1 12113/18 16:44 KDM P81_0185 Ethylbenzene BRL ug/L 1.0 0.061 1 624,1 12/13/18 16:44 KDM PSL0185 Methylene Chloride BRL ug/L 2.0 0.083 1 624,1 12/13/18 16:44 KDM P81_0185 Tetrachloroethylene BRL ug/L 0,75 0.098 1 624.1 12/13118 16:44 KDM P81_0185 Toluene BRL ug/L 1,0 0.044 1 624.1 12/13118 16:44 KDM P81_0185 trans-1,2-❑ichloroethylene BRL ug/L 2.0 0.094 1 624.1 12/13118 16:44 KDM P81_0185 trans-1,3-Dichloropropylene BRL ug/L 1.0 0.070 1 624.1 12/13118 16:44 KDM P81-0185 Trichloreethylene BRL ug/L 1.0 0.078 1 624.1 12/13/18 16:44 KDM P81-0i85 Trichlorcfluoromethane BRL ug/L 1.0 0,062 1 624.1 12113/18 16:44 KDM P8L0185 Vinyl chloride BRL ug/L 1.0 O.C97 1 624.1 12113/18 16:44 KDM P8L0185 Surrogate Recovery Contral Limits 4-Bromofluorobenzene 104 % 74-126 Dibromofluoromethane 99 % 75-127 Toluene -de 97 % 74422 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 page 11 Df 29 Na'AFR:'7 Fun-Service Analytical I S M I Environmental Solutions uep�u*owrz, we Mid -Atlantic Associates, Inc. - Charlotte Attm Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Project: Honda Power Equipment Sample Matrix: Water Laboratory Report . 1211712018 Client Sample ID: HPE-03 Prism Sample 1D: 8120033-03 Prism Work Order: 8120033 Time Collected: 12/01/18 20:00 Time Submitted: 12/03M8 15:23 Parameter Result Units Report Limit MDL Dilution Method Analysis Analyst Factor Date/Time Batch ID General Chemistry Parameters Oil & Grease (HEM) BRL mg1L 5.0 1.4 1 '1664B 12/11/18 9'46 SLS P81-0155 Total Suspended Solids 14 mg1L 4.2 0.40 1 "SM2540 D 1216118 16:55 CBP PSL0074 Organochlorine Pesticides by GCIECD alpha-BHC BRL A ug1L 0.052 0.010 1 608-3 12/10/18 13:17 ZRC PSL0044 beta-BHC BRL ug/L 0.052 0.017 1 608.3 12/10/18 13:17 ZRC PBLOO44 gamma-BHC BRL ug/L 0.052 0,014 1 608.3 12/10118 13:17 ZRC PBL0044 delta-BHC BRL ug/L 0.052 0.015 1 608.3 12/10118 13:17 ZRC 1381-0044 Heptachlor BRL ug1L 0.052 0.018 1 608.3 12/10/18 13:17 ZRC PBL0044 Alddn BRL ug/L 0.052 0.016 1 608.3 12/10/18 13:17 ZRC PSL0044 Heptachlor Epoxide BRL ug/L 0.052 0.014 1 608.3 12/10118 13:17 ZRC P81-0044 Vans -Chlordane BRL ug/L 0.052 0.027 1 608.3 12/10/18 U17 ZRC PBLOO44 Endosulfan I BRL ug1L 0.052 0.020 1 608.3 12/10118 13:17 ZRC P81_0044 cis -Chlordane BRL ug1L 0.052 0.043 1 608.3 12/10118 13:17 ZRC P81_0044 Dielddn BRL ug1L 0.052 0.015 1 608.3 12/10/18 13:17 ZRC PSL0044 4,4'-DDE BRL ug/L 0.052 0.011 1 608.3 12/10/18 13:17 ZRC PSL0044 Endrin BRL ug/L 0,052 0.016 1 608.3 12110H8 13:17 ZRC PSL0044 Endosulfan 11 BRL ug/L 0.052 0.017 1 608.3 12/10/18 13:17 ZRC PSLOD44 4,4'-DDD BRL ug/L 0.052 0.021 1 608.3 12/10/18 13:17 ZRC P8L0044 Endrin Aldehyde BRL ug1L 0.052 0.030 1 608.3 12/10118 13:17 ZRC 1381-0044 Endosulfan Sulfate BRL ug1L 0.052 0.017 1 608.3 12/10118 13A7 ZRC P81-0044 4,4'-Oi)T BRL ug1L 0.052 C.025 1 603.3 12/10118 13:17 ZRC P8L0044 Endrin Ketone BRL ug1L 0.052 0.032 1 608.3 12110H8 13:17 ZRC P81_0044 Methoxychlor BRL ug/L 0.052 0.041 1 608.3 12/10/18 13:17 ZRC P81-0044 Chlordane BRL ug/L 0.52 0.18 1 608.3 12/10118 13:17 ZRC PSL0044 Toxaphene BRL ug/L 0.52 0.077 1 608,3 12/10118 13:17 ZRC P81_0044 Aroclor 1016 BRL ug1L 0.52 0.28 1 608.3 12/10/18 13:17 ZRC P81_0044 Aroclor 1221 BRL ug1L 1.0 0.11 1 608.3 12/10118 13:17 ZRC P81_0044 Aroclor 1232 BRL ug1L 0.52 0,17 1 608.3 12/10/18 13:17 ZRC P81-0044 Aroclor 1242 BRL ug1L 0.52 OA5 1 608.3 12/10/18 13:17 ZRC PSL0044 Aroclor 1248 BRL ug/L 0.52 0.15 1 608.3 12/10118 13:17 ZRC PSL0044 Aroclor 1254 BRL ug/L 0,52 0.17 1 608.3 12/10/18 13:17 ZRC PBLOO44 Aroclor 1260 BRL ug/L 0,52 0.33 1 608.3 12/10118 13:17 ZRC P81-0044 Surrogate Recovery Control Limits Tetrachloro-m-xylene 59 % 40-134 Decachlorobiphenyl 57 % 13-186 Semivolatile Organic Compounds by GUMS 1,2,4-Trichlorobe07ene BRL ug1L 11 1.6 1 625.1 1217118 18:40 JMV PSLOO67 1,2-Dichlorobenzene BRL ug/L 11 1.5 1 625,1 1217/18 18:40 JMV PSLOO67 1,2-Diphenylhydrazine (as Azobenzene) BRL ug/L 11 3.1 1 625.1 12/7118 18:40 JMV PBL0067 1,3-Dichlorobenzene BRL uglL 11 1.4 1 625.1 1217118 18:40 JMV PSLOO67 1,4-Dichlorobenzene BRL ug1L 11 1.5 1 625.1 1217118 18:40 JMV P81_0067 This reportshould not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 12 of 29 LIPARLS M Full -Service Analytical 8 Laboratory Report Environmental Solutions 12/47/2018 aaa we Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID: HPE-03 Attn: Carl Hewett Prism Sample ID: 8120033-03 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120033 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 20:00 Time Submitted: 12/03/18 15:23 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst DatefTime Batch ID 2,4,6-Trichloraphenol BRL uglL 11 2,0 1 625.1 12f7118 18A0 JMV P81_0067 2,4-Dichlorophenol BRL ug1L 11 1.7 1 625.1 12f7118 18:40 JMV P81_0067 2,4-Dimethylphenol BRL ug1L 11 2.2 1 625.1 12f7118 18:40 JMV PSL0067 2,4-Dinitrophenol BRL uglL 11 1.3 1 625.1 12f7118 18:40 JMV P81-0067 2,4-Dinitrotoluene BRL uglL 11 3.2 1 625.1 1217118 18:40 JMV P8L0067 2,6-Dinitrotaluene BRL ug1L 11 3.2 1 625.1 1217118 18:40 JMV PBLD067 2-Chloronaphthalene BRL uglL 11 2.5 1 625.1 1217/1El 18:40 JMV PBL0067 2-Chlorophenol BRL uglL 11 1.2 1 625.1 1217118 18:40 JMV PSL0067 2-Nitraphanof BRL uglL 11 1.5 1 625.1 1217118 18:40 JMV P81_0067 3,3'-Dichlorobenzidine BRL uglL 11 3.0 1 625.1 12f7118 18:40 JMV P81_0067 4,6-Dinitro-2-methylphenol BRL uglL 11 2.0 1 625.1 12f7118 18:40 JMV PSL0067 4-Bromophenyl phenyl ether BRL uglL 11 3.4 1 625.1 12f7118 18:40 JMV P81-0067 4-Chloro-3-methylphenol BRL ug1L 11 2.4 1 625.1 12f7118 18:40 JMV P81-0067 4-Chlorophenyl phenyl ether BRL ug1L 11 2.4 1 625.1 12r7118 18:40 JMV P81_0067 4-Nitrophenol BRL uglL 54 1.8 1 625.1 12rol8 18:40 JMV PK0067 Acenaphthene BRL u91L 11 2.5 1 625.1 1217118 18:40 JMV P8L0067 Acenaphthylene BRL ug1L 11 2.5 1 625.1 1217118 18:40 JMV P81_0067 Anthracene BRL ug1L 11 3.4 1 625.1 1217/18 18:40 JMV PSL0067 Benzidine BRL ug1L 110 15 1 625.1 1217118 18:40 JMV P81-0067 Benzo(a)anthracene BRL ug1L 11 3.3 1 625.1 1217118 18:40 JMV P81-0067 Benzo(a)pyrene BRL ug1L 11 3.9 1 625.1 12f7118 18:40 JMV P81_0067 Benza(b)tluoranthene BRL uglL 11 3.8 1 625.1 12f7118 18:40 JMV PBL0067 Benza(g,hJ)perylene BRL uglL 11 3.8 1 625.1 12f7118 18:40 JMV P81_0067 Benzo(k)fluoranthene BRL ug1L 11 4,1 1 625.1 12f7118 18:40 JMV P81_0067 bis(2-Chloroethoxy)methane BRL uglL 11 1A 1 625.1 12f7118 18:40 JMV PSL0067 Bis(2-Chloroethyl)ether BRL ug1L 11 1,7 1 625.1 1217118 18:40 JMV PBL0067 Bis(2-chloroisopropyl)ether BRL ug1L 11 1.8 1 625.1 12,7118 18:40 JMV PBL0067 Bis(2-Ethylhexyl)phthalate BRL ug1L 11 3.4 1 625.1 12f7118 18:40 JMV PSL0067 Butyl benzyl phthalate BRL ug1L 11 2.8 1 625.1 1217/18 18:40 JMV PBL0067 Chrysene BRL ug1L 11 3.6 1 625.1 12f7118 18A0 JMV PBLOO67 Dibenzo(a,h)anthracene BRL ug1L 11 3.7 1 625.1 12f7118 18:40 JMV P81_0067 Diethyl phthalate BRL ug1L 11 2.5 1 625.1 12f7118 18:40 JMV PBL0087 Diethyl phthalate BRL uglL 11 1.7 1 625.1 12f7118 18:40 JMV PSL0067 Di-n-butyl phthalate BRL ug1L 11 3.6 1 625.1 12f7118 18:40 JMV P81_0067 Dkn-octyl phthalate BRL uglL 11 3.9 1 625.1 12f7118 18:40 JMV P81_0067 Fluoranthene BRL uglL 11 3.7 1 625.1 12f7118 18:40 JMV P81_0067 Fluorene BRL ug/L 11 3.0 1 625.1 12f7118 18:4D JMV P8L0o67 Hexachlorobenzene BRL ug/L 11 2.6 1 625.1 1217/18 18:40 JMV P8La067 Hexachlorebutadiene BRL uglL 11 2.2 1 625.1 12f7118 18:40 JMV P8L0067 Hexachlorocyclopentadlene BRL uglL 11 1.8 1 625A 1217118 18:40 JMV P81_0067 Hexachlorcethane BRL ug1L 11 1.6 1 625.1 12/7118 18:40 JMV P81_0067 Indeno(1,2,3-cd)pyrene BRL ug1L 11 3.3 1 625.1 1217118 18:40 JMV P81_0067 Isophorone BRL ug1L 11 2.3 1 625A 12f7118 18:40 JMV PBL0067 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1-800152M364 - Fax: 7041525-0409 Page 13 of 29 AvP "I.S IFull-Serviea AnalyticalEnvironmental Soluttons •Jn . we Laboratory Report 1211 V2018 Mid -Atlantic Associates, Inc. - Charlotte Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Project: Honda Power Equipment Sample Matrix: Water Client Sample ID: HPE-03 Prism Sample ID: 8120033-03 Prism Work Order: 8120033 Time Collected: 12/01/18 20:00 Time Submitted: 12/03/18 15:23 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Naphthalene BRL ug/L 11 2,2 1 625.1 12f7118 18:40 JMV P81_0067 Nitrobenzene BRL uglL 11 1.5 1 625.1 12f7118 18:40 JMV PSL0067 N-Nitrosodimethylamine BRL ug/L 11 0.89 1 625.1 1217118 18:40 JMV PSL0067 N-Nitroso-di-n-propylamine BRL ug/L 11 2.2 1 625.1 12f7118 18:40 JMV PBL0067 N-Nitrosodiphenylamine BRL ug/L 11 3.1 1 625.1 12f7118 18:40 JMV P81-0067 Pentachlorophenol BRL uglL 11 2.3 1 625A 12f7118 18:40 JMV P81_0067 Phenanthrene BRL ug1L 11 3.4 1 625.1 12f7118 18:40 JMV P81_0067 Phenol BRL ug1L 11 0.52 1 625.1 1217118 18:40 JMV P81_0067 Pyrene BRL ug/L 11 3.8 1 625.1 12f7118 18:40 .IMV PBL0067 Total Metals Surrogate Recovery Control Limits 2,4,6-Tribromophenol 91 % 31-144 2-Fluorobiphenyl 91 % 49-11,9 2-Fluorophenol 54 % 22-84 Nitrobenzene-d5 82 % 43-123 Phenol-d5 36 % 10-63 Terphenykdl4 92 % 49-151 Capper BRL mg1L 0.010 0.0010 1 *200.7 1216/18 18:37 JAB P81_0062 Lead BRL mg1L 0.0050 0.0010 1 `200.7 1216118 18:37 JAB P81_0062 Zinc 0.050 m91L 0.030 0.0013 1 1200.7 1216/18 18:37 JAB PBL0062 Volatile Organic Compounds by GC/MS 1,1,1-Trichloroethane BRL ug1L 1.0 0,061 1 624.1 12/13/18 17:10 KDM P81_0185 1,1,2,2-Tetrachloroethane BRL uglL 1.0 0,036 1 624.1 12/13/18 17:10 KDM P81_0185 1,1,2-Trichloroethane BRL uglL 0.50 0.068 1 624.1 12113118 17:10 KDM P81_0185 1,1-Dichloroethane BRL ug1L 1.0 0.083 1 624.1 12113/18 17:10 KDM P81_0185 1,1-Dichtoroethylene BRL ug1L 1.0 0.083 1 624.1 12113118 17:10 KDM P8L0185 1,2-Dichlorobenzene BRL uglL 1.0 0.076 1 624.1 12/13/18 17:10 KDM P8L0185 1,2-Dichloroethare BRL ug1L 1.0 0.066 1 624.1 12/13/18 17:10 KDM P81_0185 1,2-Dichloropropane BRL uglL 1.0 0.11 1 624.1 12/13/18 17:10 KDM P81-0185 1,3-Dichlorobenzene BRL uglL 1.0 0.054 1 624.1 12/13/18 17:10 KDM POL0185 1,4-Dichlorobenzene BRL ug1L 1.0 0.050 1 624.1 12M3118 17:10 KDM P81_0185 2-Chloroethyl Vinyl Ether BRL ug1L 10 0.37 1 824.1 12/13/18 17:10 KDM P81_0185 Acralein BRL ug1L 5.0 0.20 1 624.1 12/13/18 17:10 KDM P8L0185 Acrylonitrile BRL uglL 5.0 0.20 1 624.1 12113/18 17:10 KDM P8L0185 Benzene BRL uglL 0.50 0.048 1 624.1 12113/18 17:10 KDM PBLO185 Bromodichloromethane BRL uglL 1.0 0.062 1 624.1 12113/18 17:10 KDM PBLO185 Bromoform BRL ug1L 1.0 0.040 1 624.1 12/13/18 17:10 KDM PBLO185 Bromomethane BRL ug/L 2.0 0.18 1 624.1 12/13/18 17:10 KDM PSLO185 Carbon Tetrachloride BRL ug1L 1.0 0.11 1 624A 12/13118 17:10 KDM P81-0185 Chlcrobenzene BRL ug1L 1.0 0.062 1 624.1 12/13/18 17:10 KDM PSLO185 Chloroethane BRL ug1L 1.0 0.22 1 624.1 12/13/18 47:10 KDM PSLO185 Chloroform BRL ug1L 1.0 0.076 1 624.1 12/13/18 17:10 KDM P81-0185 Chloromethane BRL ug1L 1.0 0.079 1 624.1 12/13/18 17:10 KDM P8L0185 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629.6364-Toll Free Number: 1-800/529-6364- Fax: 7041525-0409 Page 14 of 29 Laboratory Report 12117/2018 LPQLSFull -Service Analytical & MEnvironmental Solutions Mid -Atlantic Associates, Inc. -Charlotte Project: Honda Power Equipment Client Sample ID: HPE-03 Attm Carl Hewett Prism Sample ID: 8120033-03 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120033 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 20:00 Time Submitted: 12/03/18 15:23 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daterrime ID cis-1,3-Dichlorapropytene BRL ug/L 1.0 0.079 1 624.1 12113/18 17:10 KDM P81-0185 Dibromochloramethane BRL ug1L 1.0 0.081 1 624.1 12/13118 17:10 KDM PSLO185 Ethylbenzene BRL ug1L 1.0 0.061 1 624.1 12/13/18 17:10 KDM P8L0185 Methylene Chloride BRL ug/L 2.0 0.083 1 624.1 12/13118 17:10 KDM P8L0185 Tetrachloroethylene BRL ug/L 0.75 0.098 1 624.1 12/13/18 17:10 KDM P81-0185 Toluene BRL ug/L 1.0 0.044 1 624.1 12M3/18 17:10 KDM P81-0185 trans-1,2-Dichloroethylene BRL ug/L 2.0 0,094 1 624A 12113/18 17:10 KDM PSL0185 trans- 1,3-Dichloropropylene BRL ug/L 1-0 0.070 1 624.1 12113/18 17:10 KDM P81_0185 Trichloroethylene BRL ug1L 1.0 0.078 1 624.1 12113/18 17:10 KDM P81-0185 Trchlorofluoromethane BRL ug1L 1.0 0.062 1 624.1 12/13/18 17:10 KDM PSLO185 Vinyl chloride BRL ug1L 1.0 0.097 1 624A 12113/18 17:10 KDM P81_0185 Surrogate Recovery Control Limits 4-Bramofluorobenzene 103 % 7e-126 Dibiomogucromethane 98 % 75-127 Toluene -de 99 % 7a-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/629.6364- Toll Free Number: 1-800/529-6364- Fax: 704/525-0409 Page 15 of 29 Futi-Sarvica Anal tical 8 /', �- Environmental Solutions '.�7'uaona�oays we Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Volatile Organic Compounds by GCAJIS - Quality Control Level II QC Report 12M7118 Prism Work Order: 8120033 Time Submitted: 12/3/2018 323:COPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81_0185 - 624 Blank (P81-0185-BLK1) Prepared & Analyzed: 12/13/18 1,1,1-Tichooroethane BPI_ 1.0 uglL 1,1,2,2-Teirachlcroethane BRL 1.0 uglL 1,1,2-Trichooroethane BRL 0.50 uglL 1,1-Dichloroethane BRL 1.0 uglL 1,1-Dichloroethylene BRL 1.0 uglL 1,2-Dichlorobenzene BRL 1.0 uglL 1,2-Dichloroethane BRL 1.0 ugfL 1,2-Dichlcropropane BRL 1.0 ug1L 1,3-Dichlorobenzene BRL 1.0 ugfL 1,4-Dichlorobenzene BRL 1.0 ugfL 2-Chloroethyl Vinyl Ether BRL 10 ugfL Acrolein BRL 5.0 uglL Acrylonitrile 3RL 5.0 uglL Benzene BRL 0.50 uglL Bromodichloromethane BRL 1.0 uglL Bromoform BRL 1.0 ugfL Bromomethane BRL 2.0 ugfL Carbon Tetrachloride BRL 1.0 ugfL Chlorobenzene BRL 1.0 ugfL Chloroethane BRL 1.0 uglL Chloroform BRL 1.0 uglL Chloramethane BRL 1.0 uglL cis- 1,3-Dichlorapropylene BRL 1.0 uglL Dibrcmochlcromethane BRL 1.0 uglL Ethylbenzene BRL 1.0 uglL Methylene Chloride BRL 2.0 uglL Tetrachlcroethylene BRL 0.75 ug1L Toluene BRt_ 1.0 ug1L trans-1,2-Dichloroethylene BRt_ 2.0 ugfL trans-1,3-Dichloropropylene BRL 1.0 uglL Trichlorcethylene BRL 1.0 uglL Tdchlorcfluoromethane BRL 1.0 ug1L Vinyl chloride BRL 1.0 uglL Heptane 0.00 uglL Surrogate:4-Bromofluorobenzene 51.6 uglL 50.00 103 74-126 Surrogate: Dibromofluoromethane 48.1 uglL 50.00 96 75-127 Surrogate: Toluene-d8 49.9 ug/L 50.00 100 74-122 This report should not he reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 16 of 29 �� �Fun-Service Analytical R I S M Enviranmentar Solutions .- ueaurawia, we Level II QC Report 12/17/18 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120033 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:OOPM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Volatile Organic Compounds by GCIMS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Lirrit Notes Batch P8LO185 - 624 LCS (P8L0185-BSI) Prepared & Analyzed: 12/13/18 1,1.1-Trichloroethane 18.7 1.0 uglL 20.00 93 52-162 1,1,2,2-Tetrachloroethane 20.9 1.0 uglL 20.00 105 46-157 1,1,2-T6rhlcroethane 21.6 0.50 uglL 20.00 108 52-150 1,1-01chloroethane 19.3 1.0 ug1L 20.00 96 59-155 1,1-Dichloroethylere 18.5 1.0 uglL 20.00 92 10-234 1,2-Dichtorobenzene 20.2 1.0 ug1L 20.00 101 18-190 1,2-Dichloroethane 20.7 1.0 uglL 20,00 103 49-155 1,2-Dichlorcpropane 21.0 1.0 uglL 20,00 105 10-210 1,3-Dichlorobenzene 20.1 1.0 ug1L 20.00 101 59-156 1,4-Dichlorobenzene 20.0 1.0 ug1L 20.00 100 18-190 2-Chloroethyl Vinyl Ether 19.8 10 ugiL 20.00 99 10-305 Acrolein 33.5 5.0 uglL 40,00 84 10-198 Acrylonitrile 41.1 5.0 ug1L 40.00 103 60-134 Benzene 20.8 0,50 ug]L 20.00 104 37-151 Bromodichloromethane 21.0 1.0 ug1L 20.00 105 35-155 Bromoform 18.7 1.0 ugIL 20.00 93 45-169 Bromomethane 16.9 2.0 ug/L 20.00 85 10-242 Carbon Tetrachloride 19.0 1.0 uglL 20.00 95 70-140 Chlorobenzene 19.9 1.0 ug1L 20.00 99 37-160 Chlaroethane 23.6 1.0 ug1L 20.00 118 14-230 Chloroform 21.6 1.0 ugtL 20.00 108 51-138 Chloromethane 17.3 1.0 ugiL 20.00 87 10-273 cis-1,3-Dichlorapropylene 19.7 1.0 ugiL 20.00 98 10-227 Dibromochloromethane 19.6 1.0 uglL 20.00 98 53-149 Ethylbenzene 20.4 1.0 ugtL 20.00 102 37-162 Methylene Chloride 20.3 2.0 ugiL 20.00 102 10-221 Tetrachloroethylene 18.7 0.75 uglL 20.00 93 64-148 Toluene 20.9 1.0 uglL 20.00 105 47-150 trans-1,2-Dichloroethylere 20.8 2.0 uglL 20.00 104 54-456 trans-1,3-Dichloropropylene 19.3 1.0 uglL 20.00 96 17-183 Trichloroethylene 20.5 1.0 ug1L 20.00 102 71-157 Trichlorofluoromethane 17.5 1.0 uglL 20.00 as 17-181 Vinyl chloride 17.5 1.0 uglL 20.00 88 10-251 Surrogate:4-Bromofluorobenzene 51.4 u91L 50.00 103 74-126 Surrogate: Dibromofluoromethane 50.3 ug/L 50.00 101 75-127 Surrogate: Toluene-d8 49.7 u97L 50.00 99 74-122 This report should not be reproduced, except in its entirety, v6thout the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800t529-0364 - Fax: 7041525-0409 Page i 7 of 29 "I` t a � R,p\{/�' Full -Service AnalylicW I S, �I , I Environmental Solullong' .weoawron:Ex Nc Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Volatile Organic Compounds by GC1MS - Quality Control Level II QC Report 12F171i8 Prism Work Order: 8120033 Time Submitted: 12/3/2018 3:23:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %RFC Limits RPD Limit Notes Batch PBL0185 - 624 LCS Dup (KL0185-eSDi) Prepared 8 Analyzed; 12/13/18 1,1,1-Trichloroelhano 18.2 1.0 uglL 20.00 91 52-162 3 20 1,1,2,2-Tetrachloroethane 21.2 1.0 uglL 20.00 106 46-157 1 20 1,1,2-Trichlcroethane 21.7 0.50 ug/L 20.00 109 52-150 0.4 20 1,1-Dichloroethane 18.8 1.0 uglL 20.00 94 59-155 3 20 1,1-Dichlaroethylene 17.8 1.0 uglL 2C.00 89 10-234 4 20 1,2-Dichlorobenzene 19.5 1.0 ug/L 20.00 97 18-190 3 20 1,2-Dichloroethane 20.5 1.0 uglL 20.00 102 49-155 0.8 20 1,2-Dichloropropane 20.5 1.0 ug1L 20.00 103 10-210 2 20 1,3-Dichlorobenzene 20.0 1,0 ug1L 20.00 100 59-156 D's 20 1,4-Dichlorobenzene 19.3 1.0 ug1L 20,00 96 18-190 3 20 2-Chlcroothyl Vnyl Ether 21.1 10 ug1L 20,00 106 10-305 6 20 Acrolein 33.0 5.0 uglL 40.00 83 10-196 1 20 Acrylonitrile 42.2 5.0 uglL 40.00 105 60-134 2 20 Benzene 20.4 0.50 uglL 20.00 102 37-151 2 20 Bromodichloromethane 20.4 1.0 ug/L 20.00 102 35-155 3 20 Bromoform 18A 1.0 ug1L 20.00 92 45-169 1 20 BTomomethane 18,9 2.0 ug1L 20.00 95 10-242 11 20 Carbon Tetrachloride 18.5 1.0 uglL 20.00 92 70-140 3 20 Chlorobenzene 19.6 1,0 uglL 20.00 98 37-160 1 20 Chloroethane 22.2 1.0 ug1L 20.00 111 14-230 a 20 Chloroform 20.9 1.0 uglL 20,00 104 51-138 3 20 Chloromethane 13.9 1.0 uglL 20.00 69 10-273 22 20 D cis-1,3-Dichloropropylene 19.2 1.0 uglL 20.00 96 10-227 2 20 Dibromochloromethane 19.8 1.0 uglL 20.00 99 53-149 0.7 20 Fthylbenzene 20.1 1.0 uglL 20.00 101 37-162 1 20 Methylene Chloride 19.4 2.0 uglL 20.00 97 10-221 5 2D Tetrachloroethylene 18.4 0.75 uglL 2C.00 92 64-148 1 20 Toluene 20.2 1.0 uglL 20.00 101 47-150 4 20 trans- 1,2-Dichloroethylene 20.3 2.0 uglL 20.00 102 54-156 3 20 trans- 1,3-Dichloropropylene 19.1 1.0 uglL 20.00 96 17-183 1 20 Trichloroethylene 20.1 1.0 ugiL 20,00 100 71-157 2 20 Thchlorofluoromethane 17.5 1.0 ugiL 20,00 87 17-181 0.2 20 Vinyl chloride 17.3 1.0 uglL 20.00 87 10-251 1 20 Surrogate:4-Bromofluorobenzene 51.7 ug/L 50.00 103 74-126 Surrogate: Dibromofluoromethane 50.2 ug/L 50.00 100 75-127 Surrogate: Toluene-d8 49.8 ng/L 50.00 100 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629.6364-Toll Free Number: 1-800/629-6364-Fax:7041525-0409 Page 18 of 29 LPRiI Full -Service Analytical& PiA6LS M I Environmental 5olutloason Level II QC Report 12/17/18 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120033 Attn: Carl Hewett Time Submitted: 12/3/2018 323:00PM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Semivalatlle Organic Compounds by GC1MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8L0067 - 3510C MS Blank (P8L0067-BLK1) Prepared: 12/06/18 Analyzed: 12/07/18 1,2,4-Trichlorobenzene BRL 10 ug1L 1,2-Dichlorobenzene BRL 10 ug1L 1,2-Diphenylhydrazine (as Azobenzene) BRL 10 ug1L 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 ug[L 2,4,6-Tdchlorophenol BRL 10 ug/L 2,4-Dichlorophenol BRL 10 ug/L 2,4-Dimethylphenol BRL 10 ug/L 2,4-Dinitrophenol BRL 10 ug/L 2,4-Dinitrotoluene BRL 10 ug/L 2,6-Dinitrotaluene BRL 10 ug1L 2-Chloronaphthalene BRL 10 ug1L 2-Chlorophenol BRL 10 ug1L 2-Nitrophenol BRL 10 ug1L 3,T-Dichlarobenzidine BRL 10 ug1L 4,6-1)initro-2-methylphenol BRL 10 ug/L 4-Bromophenyl phenyl ether BRL 10 ug/L 4-Chlaro-3-methylphenol BRL 10 ug/L 4-Chlorophenyl phenyl ether BRL 10 ug/L 4-Nitrophenol BRL 50 ug1L Acenaphthene BRL 10 ug/L Acenaphthylene BRL 10 ug1L Anthracene BRL 10 uglL Benzidine BRL 100 uglL Benzo(a)anthracene BRL 10 ug1L Benzo(a)pyrene BRL 10 ug1L Benzo(b)fluoranthene BRL 10 ug1L Benzo(g,h,i)perylene BRL 10 ug1L Benzc(k)fluoranthene BRL 10 ug1L bis(2-Chlorcetho)cy)methane BRL 10 ug1L Bis(2-Chloroethyl)ether BRL 10 ug1L Bis(2-chloraisopropyl)ether BRL 10 ug1L Bis(2-EthylhexA)phthalate BRL 10 uglL Butyl benzyl phthalate BRL 10 ug1L Chrysene BRL 10 ug1L Dibenzo(a,h)anthracene BRL 10 uglL Diethyl phthatate BRL 10 ug1L Dimethyl phthalate BRL 10 ug1L Di-n-butyl phthalate BRL 10 ug1L Di-n-octyl phthalate BRL 10 uglL Flucranthene BRL 10 ug1L Fluorene BRL 10 ug1L Hexachlorobenzene BRL 10 ug1L Hexachlorabutadiene BRL 10 ug1L Hexachlorocydopentadiene BRL 10 ug1L Hexachloroethane BRL 10 ug1L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spring brook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529.6364 - Fax: 7041525-0409 Page 19 of 29 �5 Full -Service Analytical & G,J P1R ism I Enviranmentat Solutions 37..�ow.,ow� me Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Semivolatile Organic Compounds by GClMS - Quality Control Analyte Batch PBL0067 - 3510C MS Level II QC Report 121.17118 Prism Work Order: 8120033 Time Submitted: 12/3/2018 3:23:00PM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (P81-0067-BLKi) Prepared: 12/06/18 Analyzed: 12/0711EI Indenc(1,2,3-cd)pyrene BRL 10 ug/L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitrobenzene BRL 10 ug/L N-Nitrosadimethylamine SRL 10 ug1L N-Nitroso-di-n-propylamine BRL 10 ug/L N-Nitrosodiphenylamine BRL 10 ug1L Pentachlorophenol BRL 10 ug/L Phenanthrene BRL 10 ug/L Phenol BRL 10 ug/L Pyrene BRL 10 ug1L Surrogate: 2,4,6-Tribrornophenol 93.8 ug/L toao 94 31-144 Surrogate:2-Fluorobiphenyl 47.3 ug/L 50.00 95 49-118 Surrogate:2-Fluorophenof 61.7 ug/L 100.0 62 22-84 Surrogate: Nitrobenzene-d5 43.7 ug/L 50.00 87 43-123 Surrogate: Phenol-d5 41.1 ug/L 100.0 41 10-63 Surrogate: Terphenyl-d14 46.7 ug/L 50.00 93 49-151 LCS (P8L0067-BS1) Prepared: 12/06/18 Analyzed: 12/07/18 1,2,4-Tdchlcrobenzene 34.4 10 ug/L 50.00 69 44-142 1,2-Dichlorahenzene 35.9 10 ug1L 50.00 72 32-129 1,2-D1phenylhydra7ine (as Azobenzene) 45.7 10 ug1L 50.00 91 40-135 1,3-Dichlarobenzene 34.2 10 ug/L 50.00 68 20-124 1,4-Dichlorobenzene 34.7 10 ug/L 50.00 69 20-124 2,4,6-Trichlorophenol 46.2 10 ug/L 50.00 92 37-144 2,4-Dichlorephenol 39.5 10 ug/L 50,00 79 39-135 2,4-Dimethylphenol 55.3 10 ug/L 50,00 ill 32-119 2,4-Dinitrophenol 33.3 10 ug/L 50,00 67 10-191 2,4-Dinitrotoluene 49.0 10 ug/L 50.00 98 39-139 2,6-Dinitrotoluene 51.1 10 ug/L 50.00 102 50-158 2-Chloronaphthalene 44.3 A uglL 50.00 89 60-118 2-Chlorophenol 43.0 10 ug1L 50A0 86 23-134 2-Nitrophenol 42.5 10 ug/L 50.00 85 29-182 3,3'-Dichlorobenzidine 55.2 10 ug1L 50.00 110 10-262 4,6-Diritro-2-methylphenot 36.9 10 ug/L 50,00 74 10-181 4-Bromcphenyl phenyl ether 47.0 10 ug/L 50.00 94 53-127 4-Chloro-3-methylphenol 40.0 10 ug/L 50,00 80 22-147 4-Chlorcphenyl phenyl ether 45.4 10 ug/L 50.00 91 25-158 4-Nitrcphenol 19.4 50 ug1L 50.00 39 10-132 J Acenaphthene 45.6 10 ug/L 50.00 91 47-145 Acenaphthylene 48.4 10 ug/L 50.00 97 33-145 Anthracene 51.1 10 ug/L 50.00 102 27-133 Benzidine 24.2 100 ug1L 50.00 48 15-150 J Benzo(a)anthracene 47.8 10 ug1L 50.00 96 33-143 Benzo(a)pyrene 50.8 10 ug1L 50.00 102 17-163 Benzo(b)Fluoranthene 49.2 10 ug1L 50.00 98 24-159 Benzo(g,h,i)perytene 49.1 10 ug1L 50M 98 10-219 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 20 of 29 PFult-Service Anal Ucal 8 - rnvironmen¢al Solutions 7uaoa.*own u+r. Level II QC Report 12/17/18 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Worts Order: 8120033 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:OOPM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Semivolatile Organic Compounds by GC)MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81_0067 - 3510C MS LCS (P81-0067-13SI) Prepared: 12/06/18 Analyzed: 12/07/18 Benzo(k)fluoranthene 47.8 10 ug/L 50.00 96 11-162 bis(2-Chloroethoxy)methane 45.5 10 ug/L 50.00 91 33-184 Bis(2-Chlorcethyl)ether 46.4 10 ug/L 50.00 93 12-158 Bis(2-chloroisopropyl)ether 44.8 10 ug/L 50.00 90 36-166 Bis(2-E1hylhexyl)phthalate 50.1 10 ug/L 50.00 100 10-158 Butyl benzyt phthalate 49.8 10 ug/L 50.00 100 10-152 Chrysene 47.4 10 ug/L 50.00 95 17-168 Dibenzo(a,h)anthraoene 46A 10 ug/L 50.00 92 10-227 Diethyl phthalate 47,8 10 ug/L 50.00 96 10-114 Dimethyl phthalate 47.1 10 ug1L 50.00 94 10-112 Di-n-butyl phthalate 49.8 10 ug/L 50.00 100 10-118 Di-n-octyl phthalate 57.5 10 ug/L 50.00 115 10-146 Fluoranthene 48.1 10 ug/L 50.00 96 26-137 Fluorene 48.3 10 ug/L 50.00 97 59-121 Hexachlorobenzene 45.4 10 ug/L 50.00 91 10-152 Hexachlorobutadiene 34.7 10 ug/L 50.00 69 24.116 Hexachlorocyclopeniadiene 43.2 10 ug/L 50.00 86 32-117 Hexachloroethane 33.8 10 ugfL 50.00 68 40-113 Indeno(1,2,3-cd)pyrene 61.1 10 ug/L 50.ao 122 10-171 Isophorone 47.4 10 ug1L 50.00 95 21-196 Naphthalene 38.8 10 ug1L 50.00 78 21-133 Nitrobenzene 42A 10 ug/L 50.00 84 35-180 N-Nitrosodimethylamine 31.8 10 ug/L 50.00 64 10-119 N-Nitroso-di-n-propylamine 45.0 10 ugtL 50.00 90 10-230 N-Nltrosadiphenylamine 56.8 10 ug/L 50.00 114 69-152 Pentachlorophenol 43.7 10 ug/L 50.00 87 14-176 Phenanthrene 48.2 10 ug/L 50.00 96 54-120 Phenol 19.8 10 ug/L 50.00 40 10-112 Pyrene 47.8 10 ug/L 50.00 96 52-115 Surrogate: 2,4,6-Tribromophenol 93,4 u91L 100.0 93 31-144 Surrogate:2-Fluorobiphenyl 44.9 ug/L 50.00 90 49-118 Surrogate:2-Fluorophenof 59.5 ug/L 100.0 60 22-84 Surrogate: Nitrobenzene-d5 40.8 ug/L 50.00 82 43-123 Surrogate: Phenol-d5 39.2 ug/L 100.0 39 10-63 Surrogate: Terphenyl-dM 43.6 u91L 50.00 87 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364- Toll Free Number: 1-8001529-6364- Fax: 7041525-0409 Page 21 of 29 r�> n Full-Sarvice Analytical a 1P ISM Environmental Solutions `,7 � a Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Semivolatile Organic Compounds by GClMS - Quality Control Level II QC Report 12117/18 Prism Work Order: 8120033 Time Submitted: 12/3/2018 3:23:OOPM Reporting Spike Source %REG RPD Analyte Result Limit Units Level Result %9REC Limits RPD Limit Notes Batch P81_0067 - 3510C MS LCS Dup (P81_0067-13SD1) Prepared: 12/06/18 Analyzed: 12/07/18 1,2,4-Tdchlarobenzene 32.2 10 uglL 50.00 64 44-142 7 20 1,2-Dichlorobenzene 32.1 10 ug/L 50.00 64 32-129 11 20 1,2-Diphenylhydrazine (as Azobenzene) 43.0 10 ug/L 50.00 86 40-135 6 20 1,3-Dichlorobenzene 30.7 10 ug/L 50.00 61 20-124 11 20 1,4-Dichlorobenzene 30.9 10 uglL 50.00 62 20-124 12 20 2,4,6-Tdchlorophenol 36.6 10 uglL 50.00 73 37-144 23 20 D 2,4-Dichlarophenol 34.3 10 uglL 50.00 69 39-135 14 20 2,4-Dimethylphenol 50.7 10 ug1L 50.00 101 32-119 9 20 2,4-Unitrophenal 21,7 10 ug/L 50.00 43 10-191 42 20 D 2,4-Dinitrotoluene 47.2 10 ug/L 50.00 94 39-139 4 20 2,6-Dinitrotoluene 50.3 10 ug/L 50.00 101 50-158 2 20 2-Chloronaphthalene 41.0 10 ugll- 50.00 82 60-118 8 20 2-Chlorophenal 36.4 10 uglL 50,00 73 23-134 17 20 2-Nitrophenol 36.8 10 uglL 50.00 74 29-182 14 20 3,3'-Dichlorobenzidine 53.7 10 ugll_ 50.00 107 10-262 3 20 4,6-Dinitro-2-methylphenol 26.9 10 uglL 50.00 54 10-181 31 20 D 4-Bromophenyl phenyl ether 44.8 10 ug/L 50.00 90 53-127 5 20 4-Chloro-3-methylphenol 37.8 10 ug/L 50.00 76 22-147 6 20 4-Chlorophenyi phenyl ether 43.4 10 ug/L 50.00 87 25-158 4 20 4-Nitraphenol 13.4 50 ug1L 50.00 27 10-132 37 20 D, J Acenaphthene 42.8 10 uglL 50.00 86 47-145 6 20 Acenaphthylene 45.6 10 u01L 50.00 91 33-145 6 20 Anthracene 49.7 10 ug/L 50.00 99 27-133 3 20 Benzidine 32.5 100 ug/L 50.00 65 15-150 29 20 D, J Benzo(a)anthracene 46.6 10 ug/L 50.00 93 33-143 3 20 Benzo(a)pyrene 49.6 10 uglL 50.00 99 17-163 2 20 Senzo(b)fluoranthene 48.8 10 ug1L 50.00 98 24-159 0.8 20 Benzo(g,hJ)perylene 48.9 10 ug1L 50.00 98 10-219 0.4 20 Benzo(k)fluoranthene 45.8 10 uglL 50.00 92 11-162 4 20 bis(2-Chloroethoxy)methane 43.2 10 uglL 50.00 86 33-184 5 20 Bis(2-Chloroethyl)ether 41.6 10 uglL 50.00 83 12-158 11 20 Bis(2-chloroisopropyl)ether 40.7 10 ug/L 50.00 81 36-166 9 20 Bis(2-EthylhexA)phthalate 49.9 10 ug/L 50.00 100 10-158 0.3 20 Butyl benzyl phthalate 47.9 10 uglL 50.00 96 10-152 4 20 Chrysene 45.5 10 uglL 50.00 91 17-168 4 20 Dibenzo(a,h)anthracene 44,2 10 uglL 50.00 88 10-227 4 20 Diethyl phthalate 46,4 10 uglL 5C.00 93 10-114 3 20 Dimethyl phthalate 45A 10 uglL 50,00 90 10-112 4 20 Dkn-butyl phthalate 48,0 10 ug1L 50,00 96 10-118 4 20 Di-n-octyl phthalate 56,2 10 uglL 50,00 112 10-146 2 20 Fluoranthene 46.5 10 uglL 50,00 93 26-137 3 20 Fluarene 46,6 10 uglL 50,00 93 59-121 4 20 Hexachlorobenzene 43.6 10 ug/L 50.00 87 10-152 4 20 Hexachlorobutadiene 32A 10 ug/L 50.00 65 24-116 7 20 Hexachlorocyclopentad'[ene 39,8 10 ug/L 50.00 80 32-117 8 20 Hexachloroethane 30,0 10 ug1L 50.00 60 40-113 12 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704152"409 Page 22 of 29 Level II QC Report 12/17/18 RRnn Full -Service Analytical & I S r,�► Environmental Solutions 7ueaurowca w� Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NG 28204 Semivolatile Organic Compounds by GCIMS - Quality Control Reporting Analyte Result Limit Units Prism Work Order: 8120033 Time Submitted: 12/3/2018 3:23:00PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch PSL0067 - 3510C MS LCS Dup (P8L0067-BSD1) Prepared: 12/06/18 Analyzed: 12/07/18 Indeno(1,2,1-cd)pyrene 59.5 10 ug/L 50.00 119 10-171 3 2C Isophorone 44.8 10 ug/L 50.00 90 21-196 6 2C Naphthalene 36.6 10 ug/L 50.00 73 21-133 6 2C Nitrobenzene 39.8 10 ug/L 50.00 80 35-180 6 20 N-Nitrosadimethylamine 29.0 10 ug/L 50.00 58 10-119 9 20 N-Nitroso-di-n-propylamine 40.8 10 ug/L 50.00 82 10-230 10 20 N-Nitrosodiphenylamine 55.0 10 tig1L 50.00 110 69-152 3 20 Pentachlorophenol 25.1 10 ug/L 50.00 50 14-176 54 20 D Phenanthrene 46.7 10 ug1L 50.00 93 54-120 3 20 Phenol 17.1 10 ug/L 50.00 34 10-112 14 20 Pyrene 46.3 10 ug1L 50A0 93 52-115 3 20 Surrogate:2,4,6-Tribromophenol 77.2 ug/L 100.6 77 31-144 Surrogate.,2-Ftuorobiphenyl 40.4 ug/L 50.00 81 49-118 Surrogate:2-Fluorophenol 45.8 ug/L 100.0 46 22-84 Surrogate, Nitrobenzene-d5 38.1 ug/L 50.00 76 43-123 Surrogate: Phenol{!5 33.2 ug/L 100.0 33 10-63 Surrogate: Terphenyl-d14 41.9 VgA 50,00 64 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 23 of 29 Level II QC Report 1["') h qM I Fuit-Semica Analytical & 121l 7118 Jam_, Environmental SpWllons uu Mid-Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120033 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:00PM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Organochlorine Pesticides by GClECD - Quality Control Reporting Spike Source %REC RPD Analyze Result Limit units Level Result %RLC Limits RPa Limit Notes Batch P8L0044 - 608 Blank (P81_0044-13LM) Prepared R Analyzed: 12/05/18 alpha-BHC BRL 0.050 uglL beta-BHC BRL 0.050 uglL gamma-BHC BRL 0.050 uglL delta-BHC BRL 0.050 uglL Heptachlor BRL 0.050 uglL Aldrin BRL 0.050 uglL Heptachlor Epoxide BRL 0.050 uglL trans -Chlordane BRL 0.050 ug1L Endosulfan I BRL 0.050 uglL cis-Chtordane BRL 0.050 uglL Dieldrin BRL 0,050 uglL 4,4'-DDE BRL 0,050 uglL Endrin BRL 0.050 ug1L Endosulfan 11 BRL 0.050 uglL 4,4'-DDD BRL 0.050 uglL Enddn Aldehyde BRL 0.050 uglL Endosulfan Sulfate BRL 0.050 uglL 4,4'-DDT BRL 0.050 uglL Endrin Ketone BRL 0.050 uglL Methoxychlor BRL 0.050 uglL Chlordane BRL 0.50 ug1L Toxaphene BRL 0.50 ug1L Aroclor 1016 BRL 0.50 ug/L Aroclor 1221 BRL 1.0 uglL Aroclor 1232 BRL 0.50 uglL Aroclor 1242 BRL 0.50 uglL Araclor 1248 BRL 0.50 uglL Aroclor 1254 BRL 0.50 ug1L Aroclor 1260 BRL 0.50 uglL Surrogate: Tetrachloro-m-xylene 0.842 ug/L 1.000 84 40-134 Sufogate: Decachlorobiphenyl 0.839 ug/L 1.000 84 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: l-800152M364- Fax: 7041525-0409 Page 24 of 29 P}Full-Service Analytical 8 hms v IEnvironmental Solutions Level II QC Report 12/17/18 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120033 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:00PM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Organochlorine Pesticides by GC1ECD - Quality Control Reporting Spike Sovrce %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8L0044 - 608 LCS (P811_0044-BS1) Prepared: 12/05/18 Analyzed: 12/07/18 alpha-BHC 0.663 0.050 ug/L 1.000 66 37-134 beta-BHC 0.808 0,050 ug/L 1.000 81 17-147 gamma-BHC 0.760 0.050 ug/L 1.000 76 32-127 delta-BHC 0.519 0.05a ug/L 1.000 52 19-140 Heptachlor 0.734 0.050 ug/L 1.000 73 34-111 Aldrin 0.641 0.050 ug/L 1.000 64 42-122 Heptachlor Epoxide 0.766 0.050 ug/L 1.000 77 37-142 trans -Chlordane 0.683 0.050 ug/L 1.000 68 45-119 Endosulfan 1 0.768 0.050 ug/L 1.000 77 45-153 cis -Chlordane 0.697 0.050 ug/L 1.000 70 45-119 Dieldrin 0.721 0,050 ugiL 1.000 72 36-146 4,4'-DDE 0.725 0.050 ugiL 1.000 73 30-145 Endrin 0.794 0.050 ugiL 1.000 79 30-147 Endosulfan 11 0.616 0.050 ugiL 1.000 62 10-202 4,4'-DDD 0.758 0.050 ug/L 1,000 76 31-141 Endrin Aldehyde 0.743 0.050 ug/L 1.000 74 51-132 Endosulfan Sulfate 0.676 0,050 ug/L 1.000 68 26-144 4,4'-DDT 0.769 0,060 ug/L 1.000 77 25-160 Endrin Ketone 0,786 0.050 ug/L 1.000 79 58-134 Methoxychlor 0,866 0.050 ug/L 1.000 87 54-145 Surrogate: Tetrachloro-m-xylene 0.701 ug/L 1.000 70 40-134 Surrogate: Decachlorobiphenyl 0.618 ug/L 1.000 62 13-186 LCS (P81_0044-13S2) Prepared: 12/05/18 Analyzed: 12/07/18 Chlordane 6.81 0.50 ug/L 10,00 68 50-150 Surrogate: Tetrachlaro-m-xylene 0.756 u91L 1.000 76 40-134 Surrogate: Decachlorobiphenyl 0.716 u91L 1.000 72 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 29 n P R i S M I Full -Service at Sol Analytical s Environmenfaf Solufians ��eoa�raun ac Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Organochlorine Pesticides by GCIECD - Quality Control Analyte Batch P81_0044 - 608 Level II QC Report 12/17/18 Prism Work Order: 8120033 Time Subm'itte& 12/3/2018 3:23:OOPM Reporting Spike Source Result Limit Units Level Result %REC %REC RPD Limits RPD Limit Notes LCS (P8L0044-BS3) Prepared: 12/05/18 Analyzed: 12/07/18 Toxaphene 9.16 0.50 ug1L 10.00 92 41-126 Surrogate: Tetrachloro-m-xylene 0.842 ug/L 1.000 84 40-134 Surrogate: Decachlorobiphenyl 0.754 ug/L 1.000 75 13-185 LCS (P8L0044-BS4) Prepared: 12/05/18 Analyzed: 12/07/18 Arocicr 1016 8,91 0.50 uglL 10.00 89 50-114 Aroclor 1260 8.67 0.50 uglL 10.00 87 10-127 Surrogate: Tetrachloro-m-xylene 0.724 u97L 1." 72 40-134 Surrogate: Decachlorobiphenyl 0.575 u97L 1.000 57 13-186 LCS Dup (P81-0044-8SDi) Prepared: 12/05/18 Analyzed: 12107/18 alpha-BHC 0.726 0.050 ug1 1.000 73 37-134 9 20 beta-BHC 0.820 0.050 uglL 1.000 82 17-147 1 20 gamma-BHC 0,828 0.050 uglL 1.000 83 32-127 8 20 delta-BHC 0.537 0.050 uglL 1.000 54 19-140 3 20 Heptachlor 0.836 0.050 ug1L 1.000 84 34-111 13 20 Aldrin 0.795 0.050 ugtL 1.000 79 42-122 21 20 p Heptachlor Fpoxide 0.836 0.050 ug1L 1.000 84 37-142 9 20 trans -Chlordane 0.808 0.050 uglL 1.000 81 45-119 17 20 Endosulfan 1 0.831 0.050 uglL 1.000 83 45-153 8 20 cis -Chlordane 0.811 0.050 uglL 1.000 81 45-119 15 20 Dieldrin 0.782 0.050 uglL 1.000 78 36-146 8 20 4,4'-DDE 0.852 0.050 ug1L 1,000 85 30-145 16 20 Endrin 0.858 0.050 ug1L 1,000 86 30-147 8 20 Endosulfan 11 0,824 0.050 uglL 1.000 82 10-202 29 20 D 4,4'-DDD 0.833 0.050 ug/L 1.000 83 31-141 9 20 Endrin Aldehyde 0.771 0.050 uglL 1.000 77 51-132 4 20 Endosulfan Sulfate 0.708 0.050 uglL 1.000 71 26-144 5 20 4,4'-DDT 0.842 0.050 ug1L 1.000 84 25-160 9 20 Endrin Ketone 0.619 0.050 ug1L 1.000 82 58-134 4 20 Methoxychlor 0.903 0.050 ug/L 1.000 90 54-145 4 20 Surrogate: Tetrachloro-m-xylene 0.785 ug7L 1.000 78 40-134 Surrogate: Decachlorobipheny! 0.476 ug/L 1.000 48 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-0364 - Toll Free Number: "001529-0364 - Fax: 7041525-0409 Page 26 of 29 �Pa Full-Sarviee Analytical & R M i En�ironmeniat Solutions lm Mid -Atlantic Associates, Inc. - Charlotte Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Total Metals - Quality Control Analyte Project: Honda Power Equipment Level II QC Report 12/17/18 Prism Work Order: 8120033 Time Submitted: 12/3/2018 3:23:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8L0062 - 200.7 Blank (PSL0062-BLKI ) Prepared & Analyzed: 12/06118 Copper BRL 0,010 mg1L Lead BRL 0.0050 mg/L Zinc BRL 0.030 mg/L LCS (PSL0062-BS1) Prepared & Analyzed: 12/06/18 Copper 0,496 0.010 mg1L 0,5001 99 85-115 Lead 0,499 0,0050 mglL 0.5001 100 85-115 Zinc 0.400 0.030 mg/L 0.5091 98 85-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-800152"364 - Fax: 7041525-0409 Page 27 of 29 Level II QC Report Full -Service Analytical & 12�17/18 P R M I Environmental Solullons - iwaonaromca wo Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120033 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:00111 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 General Chemistry Parameters - Quality Control Reporting Spike Source %REC li Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8111-0074 - NO PREP Blank (P81-0074-Bli Prepared & Analyzed: 12/06/18 Total Suspended Solids BRL 5.0 mg/L LCS (PBL0074-B51) Prepared & Analyzed: 12/06/18 Total Suspended Solids 480 5.0 mg1L 477.0 100 90-110 Batch P811_0155 - NO PREP Blank (Pill0155-BLK1) Prepared & Analyzed: 12/11/18 Oil & Grease (HEM) BRL 5,0 mgIL LCS (P8L0155-BS11) Prepared & Analyzed: 12/11/18 Oil & Grease (HEM) 34.8 5,0 mg/L 78-114 Sample Extraction Data Prep Method: 608 Lab Number Batch Initial Final Date)Time 8120033-01 P8L0044 960 mL 10 mL 12/05/18 8:37 8120033-02 P81_0044 940 mL 10 mL 12/05/18 11:55 8120033-03 PSL0044 960 mL 10 mL 12/05/18 11:55 Prep Method: 3510C MS Lab Number Batch Initial Final Date[Time 8120033-01 PBL0067 920 mL 1 mL 12/07/18 8:45 8120033-02 P81_0067 980 mL 1 mL 12/07/18 8:45 8120033-03 PK0067 930 mL 1 mL 12/07/18 8:45 Prep Method: 200.7 Lab Number Batch Initial Final Daterrime 8120033-01 PSL0062 50 mL 50 mL 12/06/18 8:10 8120033-02 P81_0062 50 mL 50 mL 1D06118 8:10 8120033-03 P81_0062 50 mL 50 mL 12/06/18 8:10 Prep Method: 624 Lab Number Batch Initial Final ❑atefrime 8120033-01 P8L0185 10 mL 10 mL 12/13118 10:06 8120033-02 P81_0185 10 mL 10 mi 12/13118 10:06 8120033-03 P81_0185 10 mL 10 mL 12/13118 10:06 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001629-6364 - Fax: 7041525-0409 Page 28 of 29 :ti. , Full -Service Analytical & foHAIN OF CUSTODY' RECORD Environmental Solutions PAGE ism _j_ OF QUOTE 9 TO ENSURE PROPER BILLINIG:. &MWLAaORATORIES ING Project Name: 449 Springbrook Road •Charlotte, NC 26217 - Phone 7041529-631554 Fax: 7041525.0409 Short Bold Analysis: (Yes) o UST Project: (Yes) O Client Company Name: 1 1 ti G �j 'Please ATTACH any project s c c reporting (QC LEVEL 1 Il Ill IV) provisions and/or QC Requirements Report To/Contact Name: ��C-'.l � R '/ �z 10f26! Invoice To: I b TES Reporting Address: Address: 14/j,y i01.'A QMtgcPJtF NCB tSZ0 Samples INTACT upon arrival? Received ON WET ICE? PROPER PRESERVATIVES indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES rec'd WIOUT HEADSPACE? PROPER CONTAINERS used? TEMP: Therm I Observed: YES NO NIA N sT J:'C / Com:F 'r- ° Phone:. 7r50a)—IZyF�jaz (Yes) (No):. Purchase Order No.113illing Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Address: •Rapuesled Clue Date ❑ 1 Day ❑ 2 Da s ❑ 3 Days ❑ 4 Days ❑ 5 Days /1c EDD Type: PDF_ ✓Ezee! ,'Other, "Working h Be Certification: NELAC DOD FL NC - --- ._ Days" ❑ 6-9 Days �rstendard 10 days sa pr Pno dust 1 ���f �U/P1wewT SC OTHER NIA Site Location Name: Jf�IYB{ Y '! - , Samples received after 14:00 will be processed next business day. Site Location Physical Address: '5WV5"yJ116 NG Turnaround time is based on business days. excluding weekends and holidays. Water Chlorinated: YES_ NO ✓ (SEE REVERSE FOR TERMS A CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES y N0 CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY MATRIX (SOIL, WATER OR SAMPLE CONTAINER - PRESERVA- TIMES ,yf� ANALYSIS QUES�rT�ED tJ' f)+ i, / REMARKS PRISM LAB *TYPE HOURS SLUDGE) BELOW. NO. SIZE ,per /-� �V .'`�I� • VQ% ID NO. ,SEE 1630 It - 3.'2000. ' K) 11 . ✓ ✓ ✓ ,� ,� ,� 0.3 'I f _ _ ; Sampler's Signature. - Sampled By (Print Name) Affiliation 1lpo ,4 ilnquishing, this Chain of 6.st.4 Es your authorization for Prism to proceed with the analyses as requested above. Any changes must be PRISM USE ONLY sub,61tod in.writin to.the Pr' m roject.Manager. Thera will be charges ar any changes after analyses have been initialized. Rail qu y i } am y: agnature) Date katarylHoury Additional Comments: Site Arrival Time: i !` 7 Relingmsh By: igna+u ) -Ru06WWrWt'519fr3tbTeJ 7 Site Departure Time: RRe"(Ignelurol 7-ad For P6sm La ICs T, Date Field Tech Fee:' 71 Y • Mileage: MbPWF1tWff[ent0TE: ALL SAMPLE COOLERSSHO LDBETAPEO SMUT,WITH CUSTODY SEALS F¢RTRANSPORTATION TOTH LABORATORY. up No. - SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COG UNTIL RECEIVED THE LABORATORY.I lti c� 33 ❑ Fed Ex ❑UPS O Hend-0eSlvered ❑Prism Feld Service l] Other _ PDES:: 'UST' I 'GROUNDWATER: I DRINKING WATER: I SOLID WASTE. RCRA: CERCL�4 LANDFILL. 'OTHER:' f 01, ` NC 0 SC ❑ NC''❑'SC. E] NC',13,S ZINC ❑ SC ❑ NC O'SC C] NC�❑ SC ❑ NC ❑ SC G NC ❑ SCI ❑ NC O SC f14, El — ❑.- p I "CONTAINER TYPE CODES: A=Amber C = Clear G= Gass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORIGINAL �in `SI �.S1'Y 11 LASORATORIES INC., Fult-Service Analytical & Environmental Solutions Mid -Atlantic Associates, Inc. - Charlotte Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 NC Certification No. 402 NC Drinking Water Can No. 37735 SC Cerfiricatier No. 99012 Project: Honda Power Equipment Lab Submittal Date: 12/03/2018 Prism Work Order: 8120032 Case Narrative 12/17/2018 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. .-r Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference: Reviewed By Terri W. Cole For Angela D. Overcash Project Manager A CCV result is below range on the primary column, but passes on the secondary column. The analyte is not detected in the sample down to the MDL. No further action taken. D RPD value outside of the control limits. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529 6364 - Toll Free Number: 1-8001529-0364 - Fax: 7041525-0409 Page 1 of 21 Sample Receipt Summary LPWR3, I M I EnviService Analytical s: EnvFronmenfal SolWians 12/1712018 Prism Work Order: 8120032 Client Sample ID Lab Sample ID Matrix Dateffime Sampled DaterTime Received R&D-01 8120032-01 Water 12/01/18 20:45 12/03/18 15:23 Samples were received in good condition at 3.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number; 1-8001529-6364 - Fax: 7041625-0409 Page 2 of 21 L-IjkbLSY Summary of Detections Full -Service Analytical 8I Environmental Solutions 1211712018 Prism Work Order: 8120032 Prism ID Client ID Parameter Method Result Units 8120032-01 R&D-01 Total Suspended Solids 'SM2540 D 160 mg/L 8120032-01 R&D-01 Trichloroethylene 624.1 3.4 uglL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6354-Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 3 of 21 ��,`� Laboratory Report iP a Fun -Service Analytical S M Enviranmenlal Solutions 8 12117/2018 �P-R iwaoa. we Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID: R&D-01 Attn: Carl Hewett Prism Sample ID: 8120032-01 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120032 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 20:45 Time Submitted: 12/03/18 15:23 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daterrime ID General Chemistry Parameters Oil & Grease (HEM) BRL mg1L 5.0 1.4 1 '1664B 12111/18 9:46 SLS PBLO155 Total Suspended Solids 160 mg1L 12 0.40 1 'SM2540 D 1216118 15:55 CBP P81-0074 Organochlorine Pesticides by GCIECD alpha-BHC BRL A ug/L 0.052 0.010 1 608,3 12/10/18 12:42 ZRC POLD044 beta-BHC BRL ug1L 0.052 0,017 1 608,3 12/10/18 1242 ZRC P81_0044 gamma-BHC BRL ug1L 0.052 0,014 1 608.3 12/10/18 12:42 ZRC PBLo044 delta-BHC BRL ug1L 0.052 0.015 1 608.3 12/10/18 12:42 ZRC P8Lo044 Heptachlor BRL ug1L 0,052 0.018 1 608.3 12/10/18 12:42 ZRC P8Lo044 A1ddn BRL ug1L 0.052 0.016 1 608.3 12110/18 12:42 ZRC P8L0044 Heptachlor Epoxide BRL ug1L 0,052 0.014 1 608.3 12110/18 12:42 ZRC P8L0044 trans -Chlordane BRL ug/L 0.052 0.027 1 608.3 12110/18 12:42 ZRC 1381-0044 Endosulfan I BRL ug/L 0.052 0.020 1 608.3 12/10/18 12:42 ZRC P81-0044 cis -Chlordane BRL ug1L 0.052 0.043 1 608.3 12110/18 12:42 ZRC 1`81-0044 Dielddn BRL ug/L 0.052 0.015 1 608.3 12110/18 12:42 ZRC 1`81-0044 4,4'-DDE BRL ug/L 0.052 0.011 1 608.3 12/10118 12:42 ZRC 1`81-0044 Endrin BRL ug/L 0.052 0.016 1 608.3 12/10/18 12:42 ZRC 1381-0044 Endosulfan 11 BRL ug1L 0.052 0.017 1 608.3 12/10118 12:42 ZRC P81_0044 4,4'-DDD BRL ug1L 0.052 0A21 1 608.3 12/10118 12:42 ZRC P81-0044 Endrin Aldehyde BRL ug1L 0.052 0.030 1 608.3 12/10118 12:42 ZRC P51-0044 Endosulfan Sulfate BRL ugtL 0.052 0.017 1 608.3 12/10/18 12:42 ZRC PSL0044 4,4'-CpT BRL ug/L 0.052 0.025 1 608,3 12/10/18 12:42 ZRC P8L0044 Endrin Ketone BRL ug1L 0.052 0.032 1 608.3 12/10/18 12:42 ZRC P8L0044 Methoxychlor BRL ug1L D.052 0.041 1 608.3 12/10/18 12:42 ZRC P8LD044 Chlordane BRL ug/L 0.52 0.18 1 608.3 12/10/18 12:42 ZRC P8LD044 Toxaphene BRL ug/L 0,52 0.077 1 608.3 12110/18 12:42 ZRC P8L0044 Aroclor 1016 BRL uglL 0.52 0.28 1 608.3 12110/18 12:42 ZRC P81-0044 Aroclor 1221 BRL ug/L 1.0 0.11 1 608.3 12/10/18 12:42 ZRC P81-0044 Aroclor 1232 BRL ug/L 0.52 0.17 1 608.3 12110/18 12:42 ZRC P81_0044 Aroclor 1242 BRL ug/L 0,52 0.15 1 608.3 12110/18 12:42 ZRC P8L0044 Aroclor 1248 BRL ug/L 0.52 0.15 1 608.3 12110/18 12:42 ZRC P8L0044 Aroclor 1254 BRL ug/L 0.52 0,17 1 608.3 12/10/18 12:42 ZNC PSL0044 Aroclor 1260 BRL ug/L 0.52 0.33 1 608.3 12/10118 12:42 ZRC P80044 Surrogate Recovery Control Limits Tetrachlero-m-Wene 72 % 40-134 Decachloroblphenyl 63 %, 13-186 Semivolatile Organic Compounds by GC/MS 1,2,4-Tdchlorobenzene BRL ug/L 11 1.5 1 625.1 1217/18 17:34 JMV P81_0067 1,2-Dichlorobenzene BRL ug/L 11 1.5 1 625.1 12r7118 17:34 JMV P8L0067 1,2-Diphenylhydrazine (as Azobenzene) BRL ug/L 11 3.0 1 625.1 1217118 17:34 JMV PeL0067 1,3-Dichlorobenzene BRL ug/L 11 1.4 1 625.1 1217118 17:34 JMV P81-0067 1,4-Dichlerobenzene BRL ug/L 11 1.4 1 625,1 12/7H8 17:34 JMV P8L0067 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 7041526-0409 Page 4 of 21 1 r Fut1-Service Analytical & P � ISMI environmental Solutions Mid -Atlantic Associates, Inc. - Charlotte Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Project: Honda Power Equipment Sample Matrix: Water Laboratory Report 1211772018 Client Sample ID: R&D-01 Prism Sample ID: 8120032-01 Prism Work Order: 8120032 Time Collected: 12/01/18 20,45 Time Submitted: 12/03/18 15:23 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Dateffime ID 2,4,6-Trichlorophenol BRL ug1L 11 1.9 1 625.1 1217118 17:34 JMV P81-0067 2,4-Dichlorophenol BRL ug/L 11 1.7 1 625.1 12f7118 17:34 JMV PSL0067 2,4-Dimethylphencl BRL ug/L 11 2.2 1 625.1 1217118 17:34 JMV PBL0067 2,4-Dinitrophenol BRL ug/L 11 1.3 1 625.1 1217118 17:34 JMV P81-0067 2,4-Dinitrotoluene BRL ug/L 11 3.1 1 625.1 12f7118 17:34 JMV P81-0067 2,6-Dinitrotoluene BRL ug1L 11 3.1 1 625.1 1217118 17:34 JMV P81-0067 2-Chloronaphthalene BRL uglL 11 2.5 1 625.1 1217118 17:34 JMV P81_0067 2-Chlorophenol BRL uglL 11 1.2 1 625.1 1 2f711 8 1714 JMV PBL0067 2-N'itrophenol BRL ug/L 11 1.5 1 625.1 1217/18 17-34 JMV PBL0067 3,3'-Dichlorobenzidine BRL ug1L 11 2.9 1 625-1 1217118 17:34 JMV P81_0067 4,6-Dinitro-2-methylphenol BRL uglL 11 2.0 1 625.1 12f7118 17:34 JMV PSL0067 4-Bromophenyl phenyl ether SRL uglL 11 3.3 1 625A 12f7118 17:34 JMV PSL0067 4-Chloro-3-methylphenol BRL uglL 11 2,4 1 625.1 1217118 17:34 JMV P81-0067 4-Chlorophenyl phenyl ether BRL uglL 11 2.3 1 625.1 12f7118 17:34 JMV P81-0067 4-Nitrcphenol BRL ug/L 53 1.8 1 625.1 1217/18 17:34 JMV P8L0067 Acenaphthene BRL uglt 11 2.4 1 625.1 1217118 17:34 JMV P81-0067 Acenaphthylene 8RL uglL 11 2.4 1 625.1 12C7118 17:34 JMV P81-0067 Anthracene BRL uglL 11 3.3 1 625.1 12171ia 17:34 JMV PBL0067 Benzidine BRL uglL 110 15 1 625.1 12/7/ia 17:34 JMV PSL0067 Benzo(a)anthracene BRL ugfL 11 3.3 1 625.1 12/7/18 17:34 JMV P81-0067 Benzo(a)pyrene BRL ug/L 11 3.8 1 625.1 1217118 17:34 JMV P81_0067 Benzo(b)fluoranthene BRL ugIL 11 3.7 1 625.1 12f7118 17:34 JMV PBL0067 Senzo(g,hJ)perylene BRL ug/L 11 3.7 1 625.1 12f711B 17:34 JMV P81_0067 Benzo(k)ffuoranthene BRL ug/L 11 4.0 1 625.1 1217/18 17:34 JMV P81_0067 bis(2-C hloroethoxy)methe ne BRL ug1L 11 1.9 1 625.1 1217118 17:34 JMV P8L0067 Bis(2-Chloroethyl)ether BRL ug1L 11 1.7 1 625.1 1217118 17:34 JMV P81_0067 Bis(2-chloroisopropyl)ether BRL ug1L 11 1.8 1 625.1 12f7118 17:34 JMV 1381-0067 Bis(2-Ethylhexyf)phthalate BRL ug/L 11 3.3 1 625.1 12f7118 17:34 JMV P81_0067 Butyl benzyl phthalate BRL ug/L 11 2.7 1 625.1 12f7118 17:34 JMV P81_0067 Chrysene BRL ug/L 11 3.6 1 825.1 12f7118 17:34 JMV 1381-0067 Dibenzo(a,h)anthracene BRL ug/L 11 3.6 1 625,1 12r7118 17:34 JMV PK0067 Diethyl phthalate BRL ug1L 11 2.4 1 625.1 12f7118 17:34 JMV PSL0o67 Dimethyl phthalate BRL ugIL 11 1.6 1 625.1 1217118 17:34 JMV PBL0o67 Di-n-butyl phthalate BRL ug/L 11 3.5 1 625.1 1217118 17:34 JMV P81-0067 Di-n-octyl phthalate BRL ug/1 11 3.8 1 625.1 1217/18 17:34 JMV P81-0067 Fluoranthene BRL ug/L 11 3.7 1 625.1 12f7118 17:34 JMV 1381-0067 Fluorene BRL ug/L 11 2.9 1 625.1 12f7118 17-34 JMV P81_0067 Hexachlorobenzene BRL ug/L 11 2.6 1 625.1 12f7118 17:34 JMV P8L0067 Hexachlorobutadiene BRL ug/L 11 2.1 1 625.1 1217/18 17:34 JMV PK0067 Hexachlorocyclopentadiene BRL uglL 11 1.7 1 625.1 12f7118 17:34 JMV P81-0067 Hexachloroethane BRL ugIL 11 1.6 1 625.1 12r7118 17:34 JMV P81_0067 Indeno(1,2,3-cd)pyrene BRL ug1L 11 3.2 1 625.1 121711a 17:34 JMV 1381-0067 Isophorone BRL ug/L 11 2.2 1 625.1 121711s 17:34 JMV 1381-0067 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529.6364 - Fax: 7041525-0409 Page 5 of 21 S.� pun -Service Analytical & �P R I S M I Environmental Sol"liona Laboratory Report 12117/2018 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID: R&D-01 Attn: Carl Hewett Prism Sample ID: 8120032-01 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120032 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 20:45 Time Submitted: 12103/18 15:23 Parameter Result units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Naphthalene BRL ug1L 11 2.2 1 625.1 12f7/18 17:34 JMV P81_0067 Nitrobenzene BRL ug1L 11 1,5 1 625.1 12f7118 17:34 JMV P81_0067 N-Nitrosodimethylamine BRL ug/L 11 0.87 1 625.1 12r7118 17:34 JMV P8L0067 N-Nitroso-di-n-propylamine BRL ug/L 11 2.1 1 625.1 1 2r711 8 17:34 JMV PSL0067 N-Nitroscdiphenylamine BRL ug/L 11 3.1 1 625.1 1217118 17;34 JMV PSL0067 Pentachlorophenol BRL ug/L 11 2.2 1 625.1 12/7/18 1714 JMV PSL0067 Phenanthrene BRL ug/L 11 3A 1 625.1 1217118 17:34 JMV PSL0067 Phenol SRL ug1L 11 0.51 1 625.1 12f7118 17:34 JMV PBL0067 Pyrene BRL uglL 11 3.7 1 625.1 12f7118 17,34 JMV 1`81-0067 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 96 % 31-144 2-Fluorobiphenyl 94 % 49-118 2-Ffuorophenol 56 % 22-84 Nitrobenzene-d5 85 % 43-123 Phenol-d5 39 % 10-63 Terphenykd14 91 % 49-151 Total Metals Copper BRL mg/L 0.010 0.0010 1 200.7 1216/18 17:39 JAB PSL0062 Lead BRL mg/L 0,0050 0.0010 1 '200.7 1216118 17:39 JAB P81-0062 Zinc BRL mg/L 0.030 0.0013 1 '200.7 12/6/18 17:39 JAB PBL0062 Volatile Organic Compounds by GClMS 1,1,1-Trcchloroethane BRL ug1L 1.0 0,061 1 624.1 12/13118 15;52 KOM P81_0185 1, 1, 2,2-Tetrachloroethane BRL ug/L 1.0 0.036 1 624.1 12113/18 15:52 KDM P81_0185 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 624.1 12/13118 15:52 KDM P81_0185 1,1-Dichloroethane BRL ug/L 1.0 0.083 1 624.1 12/13/18 15:52 KDM P81_0185 1,1-Dichloroethytene BRL ug/L 1.0 0.083 1 624.1 12/13/18 15:52 KDM 1381-0185 1,2-Dichlorobenzene BRL ug1L 1.0 0.076 1 624.1 12/13118 15:52 KDM PBLO185 1,2-Dichloroethane BRL ug1L 1.0 0.066 1 624.1 12/13118 15:52 KDM P81_0185 1,2-Dichloropropane BRL ug1L 1.0 00.11 1 624A 12/13/18 15:52 KDM P81_0185 1,3-Dichlorobenzene BRL uglL 1.0 0.054 1 624.1 12/13/18 15:52 KDM P8L0185 1,4-Dichlorobenzene BRL ug1L 1.0 0.050 1 624.1 12/13118 15:52 KDM P81_0185 2-Chlorcethyl Vinyl Ether BRL ugrL 10 0.37 1 624.1 12113/18 15.52 KDM PBLO105 Acrolein BRL ug1L 5.0 0.20 1 624.1 12113/18 15:52 KOM PBLo185 Acrylonitrile BRL ug/L 5.0 0.20 1 624.1 12/13/18 15:52 KDM PBLO185 Benzene BRL uglL 0.50 0.048 1 624.1 12/13/18 15:52 KDM PBLO185 Bromodichioromethane BRL ug/L 1.0 0.062 1 624.1 12113/18 15:52 KDM P8L0185 Bromoform BRL ug/L 1.0 0.040 1 624.1 12/13/18 15:52 KDM P8Lo185 Bromomethane BRL ug/L 2.0 0.18 1 624.1 12/13/18 15:52 KDM P8L0185 Carbon Tetrachloride BRL ug/L 1.0 0.11 1 624.1 12/43/18 15:52 KDM PSLO185 Chlorobenzene BRL ug/L 1.0 0.062 1 624.1 12/13/18 15:52 KOM P81_0185 Chloroethane BRL ug/L 4.0 0.22 1 624.1 12/13/18 15:52 KDM 1381-0185 Chloroform BRL ug/L 1.0 0.076 1 624.1 12/13/18 15:52 KDM PSLO185 Chloromethane BRL ug/L 1.0 0.079 1 624.1 12/13/18 15:52 KDM P81_0185 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Sprfngbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6354 - Fax: 7041525-0409 Page 6 of 21 n 4 Full -Service Analytical& Laboratory Report �P R ISM I Environmental SolulipnS 1211 T12018 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Client Sample ID: R&D-01 Attn: Carl Hewett Prism Sample ID: 8120032-01 1125 E. Morehead Street, Suite 104 Prism Work Order: 8120032 Charlotte, NC 28204 Sample Matrix: Water Time Collected: 12/01/18 20:45 Time Submitted: 12103/18 15:23 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID cis- 1,3-Dichloropropylene BRL ug/L Dibromochloromethane BRI ug/L Ethylbenzene BRL ug1L Methylene Chloride BRL ugIL Tetrachloroethylene BRL uglL Toluene BRL ug/L trans-1,2-Dichleroethylene BRL ug/L trans-1,3-Dichloropropylene BRL ug/L Triehloroethyrene 3.4 ug1L Trichlorofluoromethane BRL ug1L Vinyl chloride BRL ug/L 1.0 0.079 1 624.1 12/13/18 15.52 KDM PBLO185 1.0 0.081 1 624.1 12/13/18 15:52 KDM P81-0185 1.0 0.061 1 624.1 12113/18 15:52 KDM P81_0185 2.0 0.083 1 624.1 12113/18 15:52 KDM P81_0185 0,75 0.098 1 624A 12113/18 15:52 KDM P81_0185 1.0 0.044 1 624.1 12113/18 15:52 KDM P81_0185 2.0 0.094 1 624.1 12/13/18 15:52 KDM P81-0185 1.0 0.070 1 624A 12/13/18 15:52 KDM P8L0185 1.0 0.078 1 624.1 12113/18 15:52 KDM PBLO185 1.0 0.062 1 624.1 12/13/18 15:52 KDM P81-0185 1A 0.097 1 624.1 12/13/18 15:52 KDM P81-0185 Surrogate Recovery Control Limits 4-Bromcfluarobenzene 104 % 74-126 Dibromofluoromethane 98 % 75-127 Toluene -dB 100 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-8001629-6364 - Fax: 7041625-0409 Page 7 of 21 i, y. 4 PRISM I` Full -Service Analytical & PRISM I Environmental Solutions -7u.eon�iwus uc Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 P. Morehead Street, Suite 1104 Charlotte, NC 28204 Volatile Organic Compounds by GC1MS - Quality Control Level If QC Report 12117/18 Prism Work Order: 8120032 Time Submitted: 12/3/2018 3:23.00PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8LI1185 - 624 Blank (P81-0185-BLK1) Prepared 8 Analyzed: 12/13/18 1,1,1-Tdchloroethane BRL 1.0 ugiL 1,1,2,2-Tetrachloroethane BRL 1.0 ug1L 1,1,2-Thchloreethane BRL 0.50 ug1L 1,1-Dichloroethane BRL 1.0 ug1L 1,1-Dichloroethylene BRL 1.0 ug1L 1,2-Dichlorobenzene BRL 1,0 ugR 1,2-Dichloroethane BRL 1.0 uglL 1,2-Dichloropropane BRL 1,0 ugiL 1,3-Dichlorobenzene BRL 1.0 ugiL 1,4-Dichlorobenzene BRL 1.0 ugiL 2-Chloroethyl Vinyl Ether BRL 10 ugiL Acrolein BRL 5.0 uglL Acrylonitrile BRL 5.0 ug1L Benzene BRL 0.50 ugiL Bromodichloromethane BRL 1.0 ug1L Bromoform SRL 1.0 ug1L Bromomethane BRL 2.0 uglL Carbon Tetrachloride BRL 1.0 ugiL Chlorobenzene BRL 1.0 ugiL Chloroethane BRL 1.0 ug1L Chloroform BRL 1,0 ugiL Chloromethane BRL 1.0 ugiL cis-1,3-Dichloropropylene BRL 1.0 ugiL Dibromochloremethane BRL 1.0 ug1L Ethylbenzene BRL 1.0 uglL Methylene Chloride BRL 2.0 uglL Tetrachloroethylene BRL 0.75 uglL Toluene BRL 1.0 uglL trans-1,2-Dichloroethylene BRL 2.0 uglL trans-1,3-Dichloropropylene BRL 1.0 uglL Trichloroethylene BRL 1.0 uglL TrichloroFluoromethane BRL 1.0 ug/L Vinyl chloride BRL 1.0 ug/L Heptane 0.00 uglL Surrogate:4-Bromofluorobewene 51.6 uglL 50.00 103 74-126 Surrogate: Dibromoftuoromethane 48A ugIL 50.00 96 75-127 Surrogate: Toluene-d8 49.9 ug1L 50.00 100 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P,Q Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 8 of 2 d. Full -Service Analytical & A5�1 R I S M ! Environmental Solutivns P.Oueo uroaes e Level II QC Report 1207118 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120032 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:00PM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Volatile Organic Compounds by GC1MS - Quality Control Reporting Spike Source %REC RPD Analyze Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8L0185 - 624 LCS (P8L0185-BS1) Prepared & Analyzed: 12/13/18 1,1,1-Trichtoroethane 18.7 1.0 ug/L 20.00 93 52-162 1,1,2,2-Tetrachloreethane 20.9 1.0 ug1L 20.00 105 46-157 1,1,2-Trichloroethane 21.6 0.50 ug/L 20.00 108 52-150 1,1-Dichloroethane 19.3 1.0 ug/L 20.00 96 59-155 1,1-Dichloroethylene 18.5 1.0 ug/L 20.00 92 10-234 1,2-Dichlorobenzene 20.2 1.0 ug/L 20.00 101 18-190 1,2-Dichloroethane 20.7 1.0 ug/L 20.00 103 49-155 1,2-Dichloropropane 21.0 1.0 ug/L 20,00 105 10-210 1,3-Dichlorobenzene 20,1 1.0 ug1L 20,00 101 59-156 14-Dichlorobenzene 20.0 1.0 ug/L 20.00 100 18-190 2-Chloroethyl Vinyl Ether 19.8 10 ug/L 20.00 99 10-305 Acrolein 33.5 5.0 ug/L 40.00 84 10-196 Acrylonitrile 41 A 5.0 ug1L 40.00 103 60-134 Benzene 20.8 0.50 ug/L 20.00 104 37-151 Bromodichloromethane 21.0 1.0 uglL 20.00 105 35-155 Bromoform 18.7 1.0 ug/L 20.00 93 45-169 Bromomethane 16.9 2.0 ug/L 20.00 85 10-242 Carbon Tetrachloride 19,0 1.0 ug/L 20.00 95 70-140 Chlorobenzene 19A 1.0 ug/L 20.00 99 37-160 Chloroethane 23.6 1.0 ug/L 20,00 118 14-230 Chloroform 21.6 1.0 ug1L 20.00 108 51-138 Chloromethane 17.3 1.0 ug1L 20.00 87 10-273 cis-1,3-Dichloropropylene 19.7 1.0 ug1L 20.00 98 10-227 Dibromochloromethane 19.6 1A ug1L 20,00 98 53-149 Ethylbenzene 20.4 1.0 ug/L 20.00 102 37-162 Methylene Chloride 20.3 2.0 ug/L 20.00 102 10-221 Tetrachloroethylene 18.7 0.75 ug1L 20.00 93 64-148 Toluene 20.9 1.0 ug1L 20.00 105 47-150 trans-1,2-Dichloroethylene 20.8 2.0 ug/L 20.00 104 54-156 trans-1,3-Dichloropropylene 19.3 1.0 ug/L 20.00 96 17-183 Trichloroethylene 20,5 1.0 ug1L 20.00 102 71-157 TrichloroNuoromethane 17.5 1.0 ug1L 20.00 88 17-181 Vinyl chloride 17.5 1.0 ug/L 20,00 88 10-251 Surrogate:4-8romofluorobenzene 51.4 ug/L 50,00 103 74-126 Surrogate: Dibromoftuoromethane 50.3 ug/L 50,00 101 75-127 Surrogate: Tofuene-d8 49.7 ug/L 50.00 99 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364- Fax: 704152"409 Page 9 of 21 PFull -Service Analytical & 1?�R I S M I Environmental Solutions Level 11 QC Report 12/17/18 Mid -Atlantic Associates, Inc. -Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Volatile Organic Compounds by GC1MS - Quality Control Analyte Batch PSLO185 - 624 Prism Work Order: 8120032 Time Submitted: 12/3/2018 3:23:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS Dup (158L0185-85D1) Prepared & Analyzed: 12/13/18 1,1,1-Tdchloroethane 18.2 1.0 uglL 20.00 91 52-162 3 20 1,1,2,2-Tetrachloroethane 21,2 1.0 ug1L 20.00 106 46-157 1 20 1,1,2-Trichloroethane 21,7 0.50 ug1L 20.00 109 52-150 0.4 20 1,1-Dichloroethane 18.8 1.0 uglL 20.00 94 59-155 3 20 1,1-❑ichloroethylene 17.8 1.0 uglL 20.00 89 10-234 4 20 1,2-Dichlorobenzene 19.5 1.0 uglL 20.00 97 18-190 3 20 1,2-Dichloroethane 20.5 1.0 uglL 20.00 102 49-155 0.8 20 1,2-Dichloropropane 20.5 1.0 ugfL 20.00 103 10-210 2 20 1,3-Dichlorobenzene 20.0 1.0 uglL 20,00 100 59-156 0.8 20 1,4-Dichlorobenzene 19.3 1.0 uglL 20.00 go 18-190 3 20 2-Chlorcethyl Vinyl Ether 21.1 10 ug1L 20.00 106 10-305 6 20 Acrolein 33.0 5.0 uglL 40.00 83 10-196 1 20 Acrylonitrile 42.2 5.0 uglL 40.00 105 60-134 2 20 Benzene 20.4 0.50 uglL 20.00 102 37-151 2 20 Bromodichloromethane 20.4 1.0 uglL 20.00 102 35-155 3 20 Bromoform 18.4 1.0 uglL 20.00 92 45-169 1 20 Bromomethane 18.9 2.0 uglL 20.00 95 10-242 11 20 Carbon Tetrachloride 1 B.5 1.0 ugfL 20.00 92 70-140 3 20 Chlorobenzene 19.6 1.0 uglL 20.00 98 37-160 1 20 Chloroethane 22.2 1.0 uglL 20.00 ill 14-230 6 20 Chloroform 20.9 1.0 uglL 20.00 104 51-138 3 20 Chloramethane 13.9 1.0 tig/L 20.00 69 10-273 22 20 D cis-1,3-Dichlcropropylene 19.2 1.0 uglL 20.00 96 10-227 2 20 Dibremochloromethane 19.a 1.0 uglL 20.00 99 53-149 0.7 20 Ethylbenzene 20,1 1.0 uglL 20.00 101 37-162 1 20 Methylene Chloride 19,4 M uglL 20.00 97 10-221 5 20 Tetrachloroethylene 18,4 0.75 uglL 20.00 92 64-148 1 20 Toluene 20.2 1.0 uglL 2C.00 101 47-150 4 20 trans-1,2-Dichloroethylene 2C.3 2.0 uglL 2C.00 102 54-156 3 20 tram s-1,3-Dichlorcpropylene 19.1 1.0 ug1L 2C.00 96 17-183 1 20 Tihchoorcethylene 20A 1.0 ug1L 2C.00 100 71-157 2 20 Trichlerefluoromethane 17.5 1.0 uglL 2C.00 87 17-181 0.2 20 Vinyl chloride 17.3 1.0 uglL 20.00 87 1a-251 1 20 Surrogate:4-Bromofluorobenzene 51.7 ug/L 50.00 103 74-125 Surrogate: Dibromofluoromethane 50.2 ug/L 50.00 100 75-127 Surrogate: Toluene -dB 49.6 u97L 50.00 100 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629.6364 - Toll Free Number: 1-800t529-6364 - Fax: 704/525-0409 Page 10 of 21 S `e I S M I Envim man Analytical 8 � ' V' EnvironmentaF SoEutions '7usoaaowca u1c Level II QC Report 120 7118 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120032 Attm Carl Hewett Time Submitted: 12/3/2018 3:23:OOPM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Semivolatile Organic Compounds by GC1MS - Quality Control Reporting Spike Source %REC RP❑ Analyte Result Limit knits Level Result %REC Limits RPD Limit Notes Batch 1381-0067 - 3510C MS Blank (P81-0067-131-KI) Prepared: 12/06/18 Analyzed: 12/07/18 1,2,4-Trichlorobenzene BRL 10 uglL 1,2-Dichlorobenzene BRL 10 uglL 1,2-Diphenylhydrazine (as Azobenzene) BRL 10 uglL 1,3-Dichlorobenzene 3RL 10 uglL 1,4-Dichlorobenzene BRL 10 ug1L 2,4,6-Trichlorophenol BRL 10 uglL 2,4-❑ich1ornphennl BRL 10 uglL 2,4-Dimethylphenol BRL 10 uglL 2,4-Dinitrophenol BRL 10 uglL 2,4-Dinitrotoluene BRL 10 uglL 2,6-Dinitrotoluene BRL 10 uglL 2-Chloronaphthalene BRL 10 uglL 2-Chlorophenol BRL 10 uglL 2-Nitrophenol BRL 10 uglL 3,3'-Dichloroberizidine BRL 10 uglL 4,6-Dinitro-2-methylphenol BRL 10 trglL 4-13romaphenyl phenyl ether BRL 10 uglL 4-Chloro-3-methylphenol BRL 10 uglL 4-Chlorophenyl phenyl ether BRL 10 uglL 4-Nitrophenol BRL 50 uglL Acenaphthene BRL 10 uglL Acenaphthylene BRL 10 uglL Anthracene BRL 10 uglL Benzidine BRL 100 ug7L Benzo(a)anthracene BRL 10 uglL Benzo(a)pyrene BRL 10 ug1L Benzo(b)fluoranthene BRL 10 uglL Benzo(g,h,i)perylene BRL 10 uglL Benzo(k)fluoranthene BRL 10 uglL bis(2-Chloroethoxy)methane BRL 10 uglL Bis(2-Chloroethyl)ether BRL 10 uglL Bis(2-chloroisopropyl)ether BRL 10 uglL Bis(2-Ethylhexyl)phthalate BRL 10 uglL Butyl benzyl phthalate BRL 10 uglL Chrysene BRL 10 ug1L Dibenzo(a,h)anthracene BRL 10 uglL Diethyl phthalate BRL 10 uglL Dimethyl phthalate BRL 10 ug1L Di-n-butyl phthalate BRL 10 uglL Di-n-ocryl phthalate 3RL 10 uglL Fluoranthene 3RL 10 uglL Fluorene 3RL 10 uglL Hexachlorobenzene BRL 10 uglL hexachlorobutadiene BRL 10 uglL hexachlorocyclopentadiene BRL 10 uglL Hexachloroethane BRL 10 uglL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543 Phone: 704152M364 -Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 11 of 21 Fult-Service'Analyiical & Environmental Solutions ♦•vonian�a u,G ' Level II QC Report 12/17/18 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120032 Attn: Carl Hewett Time Submitted: 12l312018 3:23:OOPM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Sentivolatife Organic Compounds by GCIMS - Quality Control Reporting Spike Source %REG RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8L0067 - 3510C MS Blank (P81-0067-13LKi) Prepared: 12/06/18 Analyzed: 12/07/18 indeno(1,2,3-cd)pyrene BRL 10 ug/L fsaphorone BRL 10 ug1L Naphthalene BRL 10 ug1L Nitrobenzene SRL 10 uglL N-Nitrosodimethytamine BRL 10 uglL N-Nitroso-di-n-propylamine BRL 10 uglL N-Nitrosodiphenylamine BRL 10 uglL Pentachloraphenol BRL 10 uglL Phenanthrene BRL 10 uglL Phenol BRL 10 uglL Pyrene BRL 10 uglL Surrogate:2,4,6-Tribromophenol 93.8 ug1L 100.0 94 31-144 Surrogate:2-Fluorobiphenyl 47.3 u91L 50.00 95 49-118 Surrogate:2-Fluorophenol 61.7 u91L 100.0 62 22-84 Surrogate: Nitrobenzene-d5 43.7 ug/L 50.00 87 43-123 Surrogate: Phenol-d5 41.1 u91L 100.0 41 10-63 Surrogate: Terphenyl-d 14 46.7 ug/L 50.00 93 49-151 LCS (P81-0067-BS11) Prepared: 12/06/18 Analyzed: 12/07/18 1,2,4-Trichlorobenzene 34.4 10 uglL 50.00 69 44-142 1,2-Dichlorobenzene 35.9 10 uglL 50.00 72 32-129 1,2-Diphenylhydrazine (as Azobenzene) 45.7 10 uglL 50.00 91 40-135 1,3-Dichlorobenzene 34.2 10 uglL 50.00 68 20-124 1,4-Dichlorobenzene 34.7 10 uglL 50.00 69 20-124 2,4,6-Trichlorophenof 46.2 10 uglL 50,00 92 37-144 2,4-Dichlorophenol 39.5 10 ug1L 50.00 79 39-135 2,4-Dimethylphenol 55.3 10 uglL 50.00 ill 32-119 2,4-Dinitrophenol 33,3 10 uglL 50.00 67 10-191 2,4-Dinitratoluene 4M 10 ug1L 50.00 98 39-139 2,6-Dinitrotoluene 51.1 10 uglL 50.00 102 50-158 2-Chlaronaphthalene 44.3 10 uglL 50.00 89 60-118 2-Chlaropheriol 43.0 10 ug1L 50.00 86 23-134 2-Nitrophenol 42.5 10 uglL 50.00 85 29-182 3,3'-Dichlorobenzidine 55.2 10 uglL 50.00 110 10-262 4,6-Dinitro-2-methylphenol 36.9 10 uglL 50.00 74 10-181 4-Bromophenyl phenyl ether 47.0 10 uglL 50.00 94 53-127 4-Chloro-3-methylphenol 40.0 10 uglL 50.00 so 22-147 4-Chlorophenyl phenyl ether 45.4 10 ug1L 50.00 91 25-158 4-N'itrophenol 19.4 50 uglL 50.00 39 10-132 J Acenaphthene 45,6 10 uglL 50.00 91 47-145 Acenaphthylene 48.4 10 ug1L 50.00 97 33-145 Anthracene 51.1 10 ug1L 50.00 1C2 27-133 Benzidine 24.2 100 ugtL 50.00 48 15-150 J Benzo(a)anthracene 47.8 10 uglL 50.00 96 33-143 Benzo(a)pyrene 50.8 10 uglL 50.00 102 17-163 Benzo(b)fluoranthene 49.2 10 uglL 50.00 98 24-159 Benzo(g,h,i)perylene 49.1 10 uglL 50.00 98 10-219 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 12 of 21 LOR I S M 'I Fu0 servicq roruEnvironmental Solutions iwaau Level it QC Report 12'l7118 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120032 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:00PM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Semivolatile Organic Compounds by GCIMS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81_0067 - 3510C MS LCS (P8LOo67-BS1) Prepared: 12/06/18 Analyzed: 12/07/18 Benzo(k)fluoranthene 47.8 10 uglL 50.00 96 11-162 bis(2-Chloroethoxy)methane 45.5 10 ug/L 50.00 91 33-184 Bis(2-Chloroethyl)ether 46.4 10 uglL 50.00 93 12-158 Bis(2-chloroisopropyl)ether 44.8 IG ug/L 50.00 90 36-166 Bis(2-Ethylhexyl)phthalate 50.1 10 ugiL 50.00 100 10-158 Butyl benzyl phthalate 49.8 10 ug1L 50.00 100 10-152 Chrysene 47.4 10 ugiL 50.00 95 17-168 Dibenzo(a,h)anthracene 46.1 10 ugtL 50.00 92 10-227 Diethyl phthalate 47.8 10 ugtL 50.00 96 10-114 Dimethyl phthalate 47.1 10 ugtL 50.00 94 10-112 Di-n-bury! phthalate 49.8 10 uglL 50.00 100 10-118 Di-n-octyl phthalate 57.5 10 uglL 50.00 115 10-146 Fluoranthene 48.1 10 uglL 50.00 96 26-137 Fluorene 48.3 10 uglL 50.00 97 59-121 Hexachlorobenzene 45.4 10 uglL 50.00 91 10-152 Hexachlorobutadiene 34.7 10 uglL 50.00 69 24-116 Hexachlorocyclopentadiene 43.2 10 ug1L 50.00 86 32-117 Hexachloroetharie 33.8 10 uglL 50.00 68 40-113 Indeno(1,2,3-cd)pyrene 61.1 10 uglL 50.00 122 10-171 Isophorone 47.4 10 uglL 50.00 95 21-196 Naphthalene 38.8 10 ugiL 50.00 78 21.133 Nitrobenzene 42.1 10 ugiL 50.00 84 35-180 N-Nitrosodimethylamine 31.8 10 ug1L 50.00 64 10-119 N-Nitroso-di-n-propylamine 45.0 10 ugiL 50.00 90 10-230 N-Nitrosodiphenylamine 56.8 10 ugtL 50.00 114 69-152 Pentachlorophenol 43.7 10 ugtL 50.00 87 14-176 Phenanthrene 48.2 10 ugtL 50.00 96 54-120 Phenol 19.8 10 ugtL 50.00 40 10-112 Pyrene 47.8 10 ugtL 50.00 96 52-115 Surrogate: 2,4,6-Tribromophenol 93A ug1L 100.0 93 31-144 Surrogate:2-Fluorobiphenyl 44.9 ug1L - 50.00 90 49.118 Surrogate:2-Fluorophenol 59.5 ug1L 100.0 60 22-84 Surrogate: Nitrobenzene-d5 40.8 ug/1_ 50.00 82 43-123 Surrogate: Phenol-d5 39.2 ug/L 100.0 39 10-63 Surrogate: TerphenyW14 43.6 u91L 50.00 87 48.151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone; 7041529-6364- Toll Free Number: 1-800/529-6364- Fax: 704/525-0409 Page 13 of 21 PARI S MW EnviService Anaoyticels[:nvirvnmental Soiutlons Level II QC Report 12/17/18 Mid -Atlantic Associates, inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120032 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:OOPM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Semivolatile Organic Compounds by GC1MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch PSL0067 - 3510C MS LCS pup (P8L0067-8SDt) Prepared: 12/06118 Analyzed: 12/07/18 1,2,4-Trichlorobenzene 32.2 10 ug1L 50.00 64 44-142 7 20 1,2-Dichlorobenzene 32.1 10 ug1L 50.00 64 32-129 11 20 1,2-Diphenylhydrazine (as Azobenzene) 43.0 10 ug1L 50.00 86 40-135 6 20 1,3-Dichlorobenzene 30.7 10 ug/L 50.00 61 20-124 11 20 1,4-Dichlorobenzene 30.9 10 uglL 50.00 62 20-124 12 20 2,4,6-Trichlorophenol 36.6 10 uglL 50.00 73 37-144 23 20 D 2,4-Dichlorophenal 34.3 10 uglL 50.00 69 39-135 14 20 2,4-Dimethylphenol 50.7 10 uglL 50.00 101 32-119 9 20 2,4-Dinitrophenol 21.7 10 uglL 50.00 43 10-191 42 20 D 2,4-Dinitrotaluene 47.2 10 uglL 50,00 94 39-139 4 20 2,6-Dinitrotaluene 50.3 10 ug1L 50A0 101 50-158 2 20 2-Chloronaphtholene 41.0 10 uglL 50,00 82 60-118 a 20 2-Chlorophenol 36.4 10 UglL 50,00 73 23-134 17 20 2-Nitrophenol 36.8 10 uglL 50.00 74 29-182 14 20 3,3'-Dichlarobenzidine 53.7 10 ug1L 5o.0a 107 10-262 3 20 4,6-Dinitro-2-methylphenol 26.9 10 ug1L 5tl.00 54 10-181 31 20 D 4-Bromophenyl phenyl ether 44.8 10 ug/L 50.00 90 53-127 5 20 4-Chloro-3-methylphenol 37.8 10 uglL 50.00 76 22-147 6 20 4-Chlorcphenyl phenyl ether 43.4 10 uglL 50.00 87 25-158 4 20 4-Nitrophenol 13.4 50 uglL 50.00 27 10-132 37 20 D. J Acenaphthene 42.8 10 uglL 50.00 86 47-145 6 20 Acenaphthylone 45.6 10 ug1L 50.00 91 33-145 6 20 Anthracene 49.7 10 uglL 50.00 99 27-133 3 20 Benzidine 32.5 100 ug/L 50.00 65 15-150 29 20 D. J Benzo(a)anthracene 46.6 10 uglL 50.00 93 33-143 3 20 Benzo(a)pyrerte 49.6 10 Ug1L 50,00 99 17-163 2 20 Benza(b)fluoranthene 48.8 10 ug/L 50,00 98 24-159 0.8 20 Benzo(g,hJ)perylene 48.9 10 ug1L 50.00 98 10-219 0.4 20 Benzo(k)fluoranthene 45.8 10 ug1L 50.00 92 11-162 4 20 bis(2-Chloroethoxy)methane 43.2 10 ug1L 50,00 86 33-184 5 20 Bis(2-Chloroethyl)ether 41.6 10 ug1L 50.00 83 12-158 11 20 Bis(2-chloroisopropyl)ether 40.7 la ug1L 50.00 al 36-166 9 20 Bis(2-Ethylhexyl)phthalate 49.9 10 ug1L 50.00 100 10-158 0.3 20 Butyl berzyl phthalate 47.9 10 ug1L 50.00 96 10-152 4 20 Chrysene 45.5 10 ug1L 50.00 91 17-168 4 20 Dibenzo(a,h)anthracene 44.2 10 ug/L 50.00 88 10-227 4 20 Diethyl phthalate 46.4 10 uglL 50.00 93 10-114 3 20 Dimethyl phthalate 45.1 10 uglL 50.00 90 10-112 4 20 Di-n-butyl phthalate 48.0 10 uglL 50.00 96 10-118 4 20 Di-r,octyl phthalate 56.2 10 uglL 50.00 112 10-146 2 20 Fluoranthene 46.5 10 uglL 50.00 93 26-137 3 20 Fluorene 46.6 10 uglL 5C.00 93 59-121 4 20 Hexachlorobenzene 43.6 10 uglL 50.00 87 10-152 4 20 Hexachlorobutadiene 32.4 10 uglL 50.00 65 24-116 7 20 Hexachlorocyclopentadiene 39.8 10 ug1L 50.00 80 32-117 8 20 Hexachloroethane 30.0 10 uglL 50.00 60 40-113 12 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 -Toll Free plumber: 1-8001529 6364 - Fax: 7041525-0409 Page 14 of 21 P a FUD-Service Analytical R ' JP R I S M i Envimnmenlal Sotvtions AJ�,eauron Level II QC Report 12i'l7118 Mid -Atlantic Associates, Inc. -Charlotte Project: Honda Power Equipment Prism Work Order: 8120032 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:OOPM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Semivolatile Organic Compounds by GCIMS - Quality Control Reporting Spike Source %RE G RPD Analyte Result Limit Units Level Result °/aREC Limits RPD Limit Notes Batch PBL0067 - 3510C MS LCS Dup (P8L0067-BSD1) Prepared: 12/06/18 Analyzed: 12/07/18 Indeno(1,2,3-cd)pyrene 59.5 10 uglL 50.00 119 10-171 3 20 Isophorone 44.8 10 uglL 50,00 90 21-196 6 20 Naphthalene 36.6 10 uglL 50,00 73 21-133 6 20 Nitrobenzene 39.8 10 uglL 50.00 80 35-180 6 20 N-Nitrosadimethylamine 29.0 10 uglL 50.00 58 10-119 9 20 N-Nitroso-di-n-propylamine 40.8 10 ug1L 50.00 62 10-230 10 20 N-Nitrosodiphenylamine 55.0 10 ug/L 50.00 110 69-152 3 20 Pentachlorophenal 25.1 10 uglL 50.00 50 14-176 54 20 D Phenanthrene 46.7 10 ug1L 50.00 93 54-120 3 20 Phenol 17A 10 uglL 50.00 34 10-112 14 20 Pyrene 46.3 10 uglL 50.00 93 52-115 3 20 Surrogate: 2,4,6-Tribromophenal 77.2 ug/L 100.0 77 31-144 Surrogate:2-Fluorobiphenyl 40.4 ug/L 50.00 81 49-118 Surrogate:2-Fluorophenol 45.8 u97L 100.0 46 22-84 Surrogate: Nitrobenzene-d5 38.1 ug/L 50.00 76 43-123 Surrogate: Phenol-d5 33.2 u97L 100.0 33 10-63 Surrogate: Terphenyl-d14 41.9 u97L 50.00 84 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NG 28224-0543 Phone: 7041529-6364-Toll Free Number: 1-8001529.6364- Fax:7041525-0409 Page 15 of 21 AnalytiCal r �•V ! Environmental Solutions 7wowTawra we Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Organochlorine Pesticides by GCIECD - Quality Control Level II QC Report 12/17/18 Prism Work Order: 8120032 Time Submitted: 12/3/2018 3:23:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RP❑ Limit Notes Batch P8L0044 - 608 Blank (P8L0044-BLK1) Prepared & Analyzed: 12/05/18 alpha-BHC BRL 0.050 ug/L beta-BHC BRL 0.050 ug/L gamma-BHC BRL 0.050 ug/L delta-BHC BRL 0.050 ug/L Heptachlor BRL 0.050 ug/L Aldrin BRL 0.050 ug1L Heptachlor Epoxide BRL 0.050 ug/L trans -Chlordane BRL 0.050 ug/L Endosulfan I BRL 0.050 ug/L cis -Chlordane BRL 0.050 ug/L Dieldrin BRL 0.050 ug/L 4,4'-DDE BRL 0.050 ug/L Endrin BRL 0.050 uglL Endosulfan II BRL 0.050 uglL 4,4'-DDD BRL 0.050 uglL Endrin Aldehyde BRL 0.050 - ug/L Endosulfan Sulfate BRL 0.050 ug/L 4,4'-DDT BRL 0.050 ug/L Endrin Ketone BRL 0.050 ug/L Methoxychlor BRL 0.050 ug/L Chlordane BRL 0.50 ug/L Toxaphene BRL 0.50 uglL Aroclor 1016 BRL 0.50 uglL Aroclor 1221 BRL 1.0 ug/L Aroclor 1232 BRL 0.50 ug1L Aroclor 1242 BRL 0.50 ugtL Aroclor 1248 BRL 0.50 ug/L Aroclor 1254 BRL 0.50 uglL Aroclor 1260 BRL 0.50 ug/L Surrogate: Tetrachloro-m xylene 0.842 ug/L 1.000 84 40-134 Surrogate: Decachlorobiphenyl 0.839 ug/L 1.000 84 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 16 of 21 AIPP.� ....le`t S VW Full -Service Analytical & Environmental Solutions . Level II QC Report 12117118 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120032 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:00PM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Organochlorine Pesticides by GCIECD - Quality Control Reporting Spike Source %RLC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8L0044 - 608 LCS (PBL0044-BS1) Prepared: 12/05/18 Analyzed: 12/07/18 alpha-BHC 0,663 0.050 uglL 1.000 66 37-134 beta-BHC 0.808 0,050 uglL 1.000 81 17-147 gamma-BHC 0.760 0.050 _ uglL 1.000 76 32-127 delta-BHC 0.519 0.050 uglL 1.000 52 19-140 Heptachlor 0.734 0.050 uglL 1.000 73 34-111 Aldrin 0.641 0.050 ug1L 1.000 64 42-122 Heptachlor Epoxide 0.766 0.050 ugtL 1.000 77 37-142 trans -Chlordane 0.683 0.050 uglL 1.000 68 45-119 Endosulfan I 0.768 0.050 ugtL 1.000 77 45-153 cis -Chlordane 0.697 0.050 uglL 1.000 70 45-119 Dieldrin 0.721 0.050 uglL 1.000 72 36-146 4,4'-DDE 0.725 0.050 uglL 1.000 73 30-145 Endrin 0,794 0.050 u91L 1.000 79 30-147 Endosulfan II 0.616 0.050 ug1L 1.000 62 10-202 4,4'-DDD 0.758 0.050 uglL 1.000 76 31-141 Endrin Aldehyde 0.743 0.050 uglL 1.000 74 51-132 Endosulfan Sulfate 0.676 0.050 uglL 1.000 68 26-144 4,4'-DDT 0.769 0.050 uglL 1.000 77 25-160 Endrin Ketone 0.786 0.050 uglL 1.000 79 58-134 Methoxychlor 0.866 0.050 ug1L 1.000 87 54-145 Surrogate: Tetrachloro-m-xylene 0.701 ug/L 1.000 70 40-134 Surrogate: Decachlorobiphenyl 0.618 ug/L 1.000 62 13-186 LCS (P81-0044-13IS2) Prepared: 12/05/18 Analyzed: 12/07/18 Chlordane 6.81 0.50 uglL 10.00 fib 50-150 Surrogate: Tetrachloro-m-xylene 0.756 ugAL 1.000 76 40-134 Surrogate: Decachlorobiphenyl 0,715 u91L 1.000 72 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 17 Of 21 ��jy_ �r�r S• x CHAIN 0 ` Ut ODY RECORD �r-) i ,i, ISM I Full -Service ten Analytical & % Environmental Solutions PAGE_[_ OF _f QUOTE it TO ENSURE PROPER BILLING; I,1ACLO ATORIE$INC. �a" 449 Springbrook Road • Charlotte, NC 28217 Project Name: NrI r U� t ! r, rT � I . +T. Phone 7041529-6364 • Fax: 704/525.0409 Short Hold Analysis: (Ye9) (No UST Project: (Yes) NO Client Company Name:✓iJ�r4Y/uf �C. .dCj/%r Please ATTACH any project cireporting (QC LEVEL 111 II - provisions andlor OC Requirements Report TolCantact Name:L �.. Invoice To: Reporting Address; Z % T Address r3�1CTE 70� r NG Z -W YES ES NO N/A N Samples INTACT upon arrival? Received ON WET ICE? O PROPER PRESERVATIVES Indicated? N Received WITHIN HOLDING TIMES? D CUSTODY SEALS INTACT? ` VOLATILES Tecd WlOUT HEADSPACE? PROPER CONTAINERS used? TEMP: Therm lD:1:Q: f j. Observed: 3. ! °C l Ciur3•'O °C Phone:`! r r`5' -iG sl=Faz (,Yc�1es (No}: Purchase Order No.lBilling RofeienceII --- - TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Address: - _ Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DoD FL NC ✓ EDD Type: PDF"IExcel= Other-1 "Woiking days', O 6-9 Days Standard 1D'days 0 Rush pow goat Be Pra-ASite SC OTHER NIA Location Name. - Samples�reauivad afler.14:00 will be processed next Business day. ' / Site Location Physical Address. tVlN� NC. Tumaround time is based or"busiriess days: excluding uaiskendsand'holldays. Water Chlorinated: YES NO_v (SEE REVERSE FOR TERMS & coNDrnoNS REGARDING SERVICES 'Sample - — RENDERED BY PRISM LABORATORIES. INC, TO CLIENT) -Iced Upon Collection: YES 6/NO CLIENT SAMPLE DESCRIPTION I DATE COLLECTED TIME COLLECTED I MILITARY MATRIX (SOIL, WATER OR SAMPLE CONTAINER PRESERVA- TNES ANALYSIS REQUESTED ' h ' ` (� �},\ REMARKS 4 PRISM LAB 'TYPE HOURS SLUDGE) SEE BELOW NO. SIZE v. ,J �v/'Jj 0 - �{�, �+ f``. �. ID NO. # p "151 toysUJ VI r1 .- _✓. ✓ ✓' i 02 1~ 31 E IF 4 a.. T11 � n1."1r+G Sampler's Signature- Sampled By. (Print Name) - - Affiliatidn+"sio, _ ,Upon.relinquishing, this Chain of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be PRISM USE ONLY Pubmitt941n writing to,tfiqPrisAP61pct Manager: There wilt be charges for any changes after analyses hav an initialized. R qul ( , 1 R y: I ,}; nm - �dlnrylHOlus Additional Comments: Site Arrival Time: - ( na . m w- ey: (Slpnumre), Site Departure Time: elkl had .( lvod ar rttm m y;, ale Field Tech Fee: ,ra/. Mileage: hlj7manL'NOTE: ALES PL COOLERS WOULDBe.TA SH .WiTHCUSTODY $ FOR TRANSPORTATIOP TO THE LABORATORY., p ICCx SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL REC 'AT THE LABORATORY [0 N�, Fad Ex ❑ UP5 ❑ Hand�elivared ❑Prism Field Service ❑ OlhcrV `' PDES: UST: • (,GROU_NDWATER:] DRINKINGWATER: SOLIDWASTE: `RCRA: CERCLA. LANDFILL i OTHER; •� tC''❑SC t]NC ❑SC UNC OSC ❑NC ❑SC ❑NC ❑SC �❑NC❑SC ❑NC ❑SC ❑NC ❑ SC. ❑NC ❑SC �D In �n I n n " f❑ In n n *CONTAINER TYPE CODES A= Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA= Volatile Organics Analysis (Zero Head Space) ORIGINAL l RIRI S M I EEnvironmentalulEnvironmentale aAFnSolutions 7uea M.M w Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 General Chemistry Parameters - Quality Control Level II QC Report 12/17/18 Prism Work Order: 8120032 Time Submitted: 12/3/2018 3:23:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPM Limit Notes Batch P8L0074 - NO PREP Blank (P8L0074-BLKi) Prepared & Analyzed: 12/06/18 Total Suspended Solids BRL 5.0 mg1L LCS (15811-0074-BS1) Prepared & Analyzed: 12/06/18 Total Suspended Solids 480 5.0 mglL 477.0 100 90-110 Duplicate (PSL0074-DUP2) Source: 8120032-01 Prepared & Analyzed: 12/06/18 Total Suspended Solids 180 5.0 mglL 160 12 20 Batch-PBLO155 - NO PREP Blank (P811-0155-BLKi) Prepared & Analyzed: 12/11/18 Oil & Grease (HEM) BRL 5.0 mg1L LCS (P8L0155-BSI) Prepared & Analyzed: 12/11/18 Oil & Grease (HEM) 34.8 5.0 mglL 78-114 Sample Extraction Data Prep Method: 608 Lab Number Batch Initial Final Daterrime 8120032-01 P8LD044 960 mL 10 mL 12/05/18 8:37 Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 8120032-01 PSL0067 950 mL 1 mL 12107/18 8745 Prep Method: 200.7 Lab Number Batch Initial Final DatelTime B120032-01 P8L0062 50 mL 50 mL 12/06/18 8:10 Prep Method: 624 Lab Number Batch Initial Final Daterrime 8120032-01 P81_0185 10 mL 10 mL 12/13118 10:06 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041625-0409 Page 20 of 21 LklpL-am. Full-Service al Sol tlo 8 �nvironmrntalSolutions Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Attn: Carl Hewett 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Total Metals - Quality Control Level II QC Report 12/17/18 Prism Work Order: 8120032 Time Submitted: 12/3/2018 3:23:00PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81_0062 - 200.7 Blank (P8L0062-BLK1) Prepared & Analyzed: 12/06/18 Capper BRL 0.010 mg/L Lead BRL 0.0050 mg/L Zinc BRL 0.030 mg/L LCS (PBLOO62-BS1) Prepared & Analyzed: 12/06/18 Copper 0A96 0.010 mg/L 0.5001 99 85-115 Lead 0,499 0,0050 mglt. 0.5001 100 85-115 Zinc 0.490 0.030 mg/L 0.5001 98 85-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratcries, inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Numher: 1-800/529-6364 - Fax: 7041525-0409 Page 19 of 21 APRIS'Ar'�, Fu l� t Full -Service Analytical & M I Enviranmentai Solutions 7..e Toarea we Level II QC Report 2117/18 Mid -Atlantic Associates, Inc. - Charlotte Project: Honda Power Equipment Prism Work Order: 8120032 Attn: Carl Hewett Time Submitted: 12/3/2018 3:23:OOPM 1125 E. Morehead Street, Suite 104 Charlotte, NC 28204 Organochlorine Pesticides by GClECD - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8L0044 - 608 LCS (PBL0044-BS3) Prepared: 12/05118 Analyzed: 12/07/18 Toxaphene 9.16 0.50 uglL 10.00 92 41-126 Surrogate: Tetrachloro-m-xylene 0.842 ug/L 1.000 84 40-134 Surrogate: Decachlorobiphenyl 0.754 u91L 1.000 75 13-166 LCS (P8Ltl044-BS4) Prepared: 12/05/18 Analyzed: 12/07/18 Aroclor 1016 8.91 0.50 ug1L 10.00 89 50-114 Aroclor 1260 8.67 0.50 ug/L 10,00 87 10-127 Surrogate: Tetrachloro-m-xylone 0.724 u91L 1.000 72 40-134 Surrogate: Decachlorobiphenyl 0.575 ug/L 1.000 57 13-186 LCS Dup (P81-0044-13SD1) Prepared: 12/05/18 Analyzed: 12/07118 alpha-BHC 0.726 0.050 ug1L 1.000 73 37-134 9 20 beta-BHC 0.820 0.050 ug1L 1.000 82 17-147 1 20 gamma-BHC 0.828 0.050 uglL 1.000 83 32-127 8 20 delta-8HC 0.537 0.050 ug1L 1.000 54 19-140 3 20 Heptachlor 0.836 0.050 ug1L 1.000 84 34-111 13 20 Aldrin 0.795 0.050 ug1L 1.000 79 42-122 21 20 D Heptachlor Epoxide 0.836 0.050 ug1L 1.000 84 37-142 9 20 trans -Chlordane 0.808 0.050 uglL 1.000 81 45-119 17 20 Endosulfan 1 0.831 0.050 ug1L 1.000 83 45-153 8 20 cis -Chlordane 0,811 0.050 ug1L 1.000 81 45-119 15 20 Dieldrin 0.782 0,050 uglL 1.000 78 36-146 8 20 4,4'-DDE 0.852 0.050 ug1L 1.000 85 30-145 16 20 Endrin 0.858 0.050 ug1L 1.000 86 30-147 8 20 Endosulfan 11 0.824 0.050 ug1L 1,000 82 10-202 29 20 D 4,4'-DOD 0.833 0.050 ug1L 1.000 83 31-141 9 20 Endrin Aldehyde 0.771 0.050 ug1L 1Mo 77 51-432 4 20 Endosulfan Sulfate 0.708 0.050 uglL 1.000 71 26-144 5 20 4,4'-DDT 0.842 0.050 uglL 1.000 84 25-16C 9 20 Endrin Ketone 0.819 0.050 uglL 1.000 82 58-134 4 20 Methoxychlor 0.903 0.050 uglL 1.000 90 54-145 4 20 Surrogate: Tetrachloro-m-xylene 0.785 u97L 1.000 78 40-134 Surrogate: Decachlorobiphenyl 0.476 u91L 1.000 48 13-185 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phorw 7041529 6364-Toll Free Number: l-8001529-0364-Fax: 7041526-0409 Page 18 of 21 Compliance Inspection Report Permit: NCGO60329 Effective: 11/16117 Expiration: SOC: Effective: Expiration: County: Duplin Region: Wilminaton Contact Person: Nicole Reynolds Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Repiresentative(sI: Related Permits: Inspection Date: 06/27/2018 Primary Inspector: Brian P Lambe Secondary Inspector(s): 10/31118 Owner : House of Raeford Farms Inc Facility: House of Raeford - Rose Bill VM+TF 3333 US Hwy 117 S Rose Hill NC 28458 Title: Complex Manager Certification: Entry Time: 11:00AM Exit Time: 11:40AM Phone: 910-289-3191 Phone: Phone: Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Food/Tobacco/Soaps/Cosmetics/Public VVarehousing Stormwaler Discharge COC Facility Status: ❑ Compliant 0 Not Compliant Question Areas: Storm Water (See attachment summary) Pane: 1 Permit: NCGO50329 Owner - Facility: i.c2se of Rae,oro =arms Inc Inspection Date: 081271207E Inspection Type : Compliance Evaluation Reason for Visit: P,ou;irie Inspection Summary: No chance in condition of the facility. The last records central office has recorded is 2016. Please submit 2017 and 2018 records to this office. Outfalls 2 and 3 should not be part of the report since they flow to wastewater. Paae: 2 Permit: NCGO60329 Owner - Facility: Houso of Raefora Farms Inc Inspection Date: 0612712018 Inspection Type : Compliance Evaluation Reason for Visit: Routine Stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwater Pollution Prevention Plan? 0 ❑ ❑ ❑ # Does the Plan include a General Location (USGS) map? E ❑ ❑ ❑ # Does the Plan include a "Narrative Description of Practices'? 0 ❑ ❑ ❑ # Does the Plan include a detailed site map including outfall locations and drainage areas? i ❑ ❑ ❑ # Does the Plan include a list of significant spills occurring during the past 3 years? 0 ❑ ❑ ❑ # Has the facility evaluated feasible alternatives to current practices? 0 ❑ ❑ ❑ # Does the facility provide all necessary secondary containment? 0 ❑ ❑ ❑ # Does the Plan include a BMP summary? ❑ ❑ ❑ # Does the Plan include a Spill Prevention and Response Plan (SPRP)? e ❑ ❑ ❑ # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? O ❑ ❑ ❑ # Does the facility provide and document Employee Training? 0 ❑ ❑ ❑ # Does the Plan include a list of Responsible Party(s)? 0 ❑ ❑ ❑ # Is the Plan reviewed and updated annually? N ❑ ❑ ❑ # Does the Plan include a Stormwater Facility inspection Program? ■ ❑ ❑ ❑ Has the Stormwater Pollution Prevention Plan been implemented? N ❑ ❑ ❑ Comment Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring semi-annually? ❑ ❑ ❑ Comment: Submit 2017•and 2018 records to this office. Analytical Monitoring Yes No NA NE Has the facility conducted its Analytical monitoring? ❑ ❑ ❑ # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ ❑ 0 Comment: Submit 2017 and 2018 records to this office. Permit and Rutfalls Yes No NA NE # is a copy of the Permit and the Certificate of Coveraae available at the site? ® ❑ ❑ ❑ # Were all outfalls observed during the inspections N ❑ ❑ ❑ # It the facility has representative outfall status, is i1 properly documented by the Division? ❑ ❑ N ❑ # Has the facility evaluated all illicit (non stormwater) discharges? ❑ ❑ ❑ Comment: Paoe: 3 rF - Mid Atlantic Engineering & Environmental Solutions January 31, 2017 Mr. Brendan Conway Honda Power Equipment Manufacturing, Inc. Post Office Box 37 Swepsonville, North Carolina 27359 Subject: Stormwater Sampling Event — January 2017 Honda Power Equipment Swepsonville, Alamance County, North Carolina Mid -Atlantic Project: 000H1054.00 Dear Mr. Conway: 1125 E. Morehead Street Suite 104 Charlotte, NC 28204-2849 03 office 980-585-1271 MAAONLINE.COM RI V E® FEB o 3 2017 CENTRAL FILES DWR SECTION On January 17, 2017, Mid Atlantic Associates, Inc_ (Mid -Atlantic) completed a stormwater sampling event at the Honda Power Equipment Manufacturing facility located in Swepsonville, North Carolina. The rain event began at approximately 2:30 pm on January 17 and ended at approximately 8:30 pm on the same day. Stormwater samples were collected at four discharge locations (HPE-01, HPE-02, HPE-03 and R&D-01) on the subject property. After collection, the samples were delivered to the Shealy Environmental Services, Inc. (Shealy) laboratory in West Columbia, South Carolina for analysis. Copies of the Stormwater Monitoring Records for this sampling event are provided in Attachment A. The analytical results are presented in summary form in Attachment B. A copy of the laboratory report is included in Attachment C. Sampling was conducted by Carl Hewett of Mid -Atlantic. Stormwater samples were not collected at the facility during the second half of 2016 due to drought conditions in the area. This sampling event was conducted to serve as the second event for 2016. Mid -Atlantic appreciates the opportunity to provide our environmental services on this project. Please do not hesitate to call if you have questions or need additional information. Sincerely, MID -ATLANTIC ASSOCIATES, INC. r Carl H. Hewett Greg D. Icenhour, P.G., MBA Senior Project Manager Principal Geologist EXPERIENCED CUSTOMER FOCUSED r - " STORMWATER MONITORING RECORD Sampling Summary Site: Honda Power Equipment 3721 NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: January 17, 2017 Previous Measurable Rainfall Event (>0.1 inches): January 3, 2017 Storm Event Approximate Start: 2:30 pm, January 17, 2017 Approximate End: 8:30 pm, January 17, 2017 Storm Duration: approximately 6 hours Rainfall: 0.08 inches* Sampling: sampled discharge point HPE-03 at 3:45 pm (1545) sampled discharge point R&D-01 at 4:45 pm (1645) sampled discharge point HPE-02 at 5:30 pm (1730) sampled discharge point HPE-01 at 6:00 pm (1800) Analytical Testing: pH by EPA Method SM 4500-H B TSS by SM 2540D-20 oil and grease by EPA Method 1664B volatile organics by EPA Method 624 semi -volatile organics by EPA Method 625 PCBs/pesticides by EPA Method 608 copper, lead, zinc by EPA Method 200.8 Sampled By: Carl Hewett Mid Atlantic Associates, Inc. 1125 East Morehead Street, Suite 104 Charlotte, North Carolina 28204 Notes: • Storm duration and rainfall amount obtained from the National Weather Service daily summary for Burlington, North Carolina. * - rainfall amount was measured at the Burlington, NC airport. All four of the stormwater outfall locations at the property were discharging during this event. Page 1 of 1 Rectl tb JUL 2 5 2016 CENTRAL FILES DWR- SECTION 112S E. Morehead Street Suite 104 N oW Atlantic Charlotte, NC 28204-2849 Engirieering & Environmental Solutions N C G !` -36 3 a q office 980-585-1271 U MAAONLINE.COM June 6, 2016 Mr. Brendan Conway Honda Power Equipment Manufacturing, Inc. Post Office Box 37 Swepsonville, North Carolina 27359 Subject: Stormwater Sampling Event — May 2016 Honda Power Equipment Swepsonville, Alamance County, North Carolina Mid -Atlantic Project: 0001-11054.00 Dear Mr. Conway: On May 17, 2016, Mid Atlantic Associates, Inc. (Mid -Atlantic) completed a stormwater sampling event at the Honda Power Equipment Manufacturing facility located in Swepsonville, North Carolina. The rain event began at approximately 7:00 am on May 17 and ended at approximately 7:00 pm on the same day. Stormwater samples were collected at four discharge locations (HPE-01, HPE-02, HPE-03 and R&D-01) on the' subject property. After collection, the samples were delivered to the Shealy Environmental Services, Inc. (Shealy) laboratory in West Columbia, South Carolina for analysis. Copies of the Stormwater Monitoring Records for this sampling event are provided in Attachment A. The analytical results are presented in summary form in Attachment B. A copy of the laboratory report is included in Attachment C. Stormwater sampling was conducted by Carl Hewett of Mid -Atlantic. Mid -Atlantic appreciates the opportunity to provide our environmental services on this project. Please do not hesitate to call if you have questions or need additional information. Sincerely, MID -ATLANTIC ASSOCIATES, INC. �Rt Q� (�� Carl H. Hewett Senior Project Manager Greg D. Icenhour, P.G., MBA Principal Geologist EXPERIENCED CUSTOMER FOCUSED STORM_ WATER MONITORING RECORD Sampling Summary Site: Honda Power Equipment 3721 NC Highway,119 Swepsonville, North Carolina 27359 Monitoring Date: May 17, 2016 Previous Measurable Rainfall Event (>0.1 inches): May 12, 1016 Storm Event Approximate Start: 7:00 am, May 17, 2016 Approximate End: 7:00 pm, May 17, 2016 Storm Duration: approximately 12 hours Rainfall: 0.52 inches Sampling: sampled discharge point HPE-03 at 12:15 pm (1215) sampled discharge point R&D-01 at 1:15 pm (1315) sampled discharge point HPE-02 at 2:00 pm (1400) sampled discharge point HPE-01 at 2:45 pm (1445) Analytical Testing: pH by EPA Method SM 4500-H B TSS by SM 2540D-20 oil and grease by EPA Method 1664B volatile organics by EPA Method 624 semi -volatile organics by EPA Method 625 PCBs/pesticides by EPA Method 608 copper, lead, zinc by EPA Method 200.8 Sampled By: Carl Hewett Mid Atlantic Associates, Inc. 1125 East Morehead Street, Suite 104 Charlotte, North Carolina 28204 Notes: o Storm duration and rainfall amount obtained from the National Weather Service daily summary for Burlington, North Carolina. Page 1 of 1 ATTACHMENT A Stormwater Monitoring Records STORMWATER MONITORING RECORD Qualitative Observations Site: Honda Power Equipment 3721 NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: May 17, 2016 Sample Location: HPE-01 Discharge Characteristic Rating Comments Color Vp,V6 Odor N-o,VF Clarity Floating Solids ,S/oNC Suspended Solids Now Foam Flo/V"C Oil Sheen Other obvious indicators of storm water pollution Characteristic rating scale: none, slight, minor, medium, heavy Monitoring sheet completed by: 0ate: df l -7A0 ATTACHMENT B STORMWATER MONITORING RECORD Qualitative Observations Site: Honda Power Equipment 3721 NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: May 17, 2016 Sample Location: R&D-01 Discharge Characteristic Rating ' comr4�ents Color AjOM!l Odor 1,/oNE Clarity C Floating Solids i(lo,cfr Suspended Solids lvbw Foam Oil Sheen A 0412': Other obvious indicators of storm water pollution Characteristic rating scale: none, slight, minor, medium, heavy Monitoring sheet completed by:a,���Date:/�� STORMWATER MONITORING RECORD Qualitative Observations Site: Honda Power Equipment 3721 NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: May 17, 2016 Sample Location: HPE-03 Discharge Characteristic Rating Comments Color WoNE Odor NoN& Clarity Floating Solids I/P,tC Suspended Solids NoNf Foam AMA16' Oil Sheen MoN5 Other obvious indicators of storm water pollution Characteristic rating scale: none, slight, minor, medium, heavy /%��Q Monitoring sheet completed by: l.�""`- Date: � ll/le STORMWATER MONITORING RECORD Qualitative Observations Site: Honda Power Equipment 3721 NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: May 17, 2016 Sample Location: HPE-02 Discharge Characteristic Rating Comments Color Sue.,ql 4-16ttr fft"It/ f",W #VfVY, R�in1 EvenrT Odor it/aN� Clarity ' Floating Solids Molt/ Suspended Solids 41,91vF Foam N&,NC Oil Sheen �oF Other obvious indicators of storm water pollution Characteristic rating scale: none, slight, minor, medium, heavy Monitoring sheet completed by: Date: e2 L14- ATTACHMENT C Laboratory Analytical Report TABLE Stormwater Analytical Results — May 2016 Honda Power Equipment Swepsonville, Alamance County, North Carolina HPE-01 HPE-02 ` HPE-03 R&D-01 Benchmark Values pH 5.64 5.58 5.43 _ 5.49 6-9 total suspended solids (TSS) 29 38 12 56 100 EPA Method 200.8� copper 6.1 8.5 4.8 31t ,, Whit 7 lead BDL 1.2 BDL BDL 30 zinc 35 21 24 13 67 EPA Method 608 target pesticides BDL BDL BDL BDL 1000 EPA Method 608 target PCBs BDL BDL BDL BDL 1000 EPA Method 624 target volatile compounds BDL BDL BDL BDL 1000 EPA Method 625 bis(2-ethylhexyl)phthalate BDL BDL 1.6 BDL 1000 target semi -volatile compounds BDL BDL BDL BDL 1000 EPA Method 1664 oil and grease BDL BDL BDL BDL 1500 Notes: • Total suspended solids (TSS) presented in milligrams per liter (mg/L). • Other analytical results presented in micrograms per liter (ug/L). • BDL —below laboratory minimum quantitation limits Stormwater samples collected on May 17, 2016 by Mid -Atlantic personnel. �v 7208 Falls of Neuse Road, Suite 102 Raleigh, NC 27615 (919) 861-8888 FAX (919) 615-2102 ® Environmental Consulting ®& Technology of North Carolina, PLLC April 28, 2015 Mr. Brendan Conway Honda Power Equipment Manufacturing, Inc. Post Office Box 37 Swepsonville, North Carolina 27359 Re: Storm Water Sam pling Event — April 2015 Honda Power Equipment Swepsonville, Alamance County, North Carolina ECT Project No. 150246 Dear Mr. Conway: Nc� o3o3a� RECEIVED MAY 15 2015 CENTRAL FILES DWR SECTION On April 15, 2015, Environmental Consulting & Technology of North Carolina, I'LLC (ECT) completed a storm water sampling event at the Honda Power Equipment Manufacturing facility located in Swepsonville, North Carolina. The intermittent rain event began on April 14 at approximately 7:30 pm and ended at approximately 9:00 pm on April 16. Storm water samples were collected from four, discharge locations (I-IPE-01, 14PE-02, HPE-3 and R&D-01). After collection the samples were delivered to the Shealy Environmental Services. Inc. (Shealy) laboratory in West Columbia, South Carolina for analysis. A copy of the Storm Water Monitoring Records for this event are provided in Attachment A. The analytical results are presented in sutnmary form in Attachment B. A copy of the Shealy laboratory report is included in Attachment C. Storm water sampling was conducted by Carl Hewett of ECT. ECT appreciates the opportunity to offer our services on this project, and please do not hesitate to contact us if you have any questions or comments. Sincerely, ENVIRONMENTAL CONSULTING & TECHNOLOGY OF NORTH CAROLINA, PLLC Carl 1-1. Hewett Christopher Wu Staff Engineer Water Resource Project Manager An Equal Opportunity/Affirmative Action Employer www.ectinc.com STORM WATER MONITORING RECORD SAMPLING SUMMARY Site: Honda Power Equipment Manufacturing, Inc. .3721 NC Highway 119 Haw River, North Carolina 27258 Monitoring Date: April 15, 2015 Previous Measurable Rainfall Event (>0.1 inches): April 9, 2015 Storm Event Approximate Start: 7:30 pm, April 14, 2015 Approximate End: 9:00 pm, April 16, 2015 Rainfall: 0.93 inches Sampling: sampled discharge point HPE-01 at 11:00 am (1045) sampled discharge point HPE-02 at 11:45 am (1145) sampled discharge point HPE-03 at 10:00 am (1000) sampled discharge point R&D-01 at 12:45 pm (1245) Analytical Testing: pH by EPA Method SM 4500-HB TSS by SM 2540D Oil and grease by EPA Method 1664A Volatile organics by EPA Method 624 Semi -volatile organics by EPA Method 625 PCBs/Pesticides by EPA Method 608 Copper, Lead and Zinc by EPA Method 200.7 Sampled By: Carl Hewett Environmental Consulting & Technology, Inc. 6135 Park South Drive, Suite 510 Charlotte, North Carolina 28210 Notes: • Storm duration and rainfall amount obtained from Weather Underground's daily summary for Swepsonville, North Carolina. Page 1 of 1 STORM WATER MONITORING RECORD QUALITATIVE OBSERVATIONS Site: Honda Power Equipment Manufacturing, Inc. 3721 NC Highway 119 Haw River, North Carolina 27258 Monitoring Date: April 15, 2015 Sample Location: HPE-02 Outfall Description: Pipe Discharge Characteristic Rating Comments Color r Odor / Clarity f Floating .solids j Suspended Solids Foam Yes No Oil Sheen Yes Evidence of erosion or deposition Yes No Other obvious indicators of storm water pollution /von/E Rating stole from 1 to 5 (1 = not present, 5 = heavily present) Monitoring Form Completed By: Date:-�S STORM WATER MONITORING RECORD QUALITATIVE OBSERVATIONS Site: Honda Power Equipment Manufacturing, Inc. 3721 NC Highway 119 Haw River, North Carolina 27258 Monitoring Date: April 15, 2015 Sample Location: HPE-03 outfall Description: Ditch Discharge Characteristic Rating Comments Color r Odor Clarity f Fioating Solids ' Suspended Solids r Foam Yes No Oil Sheen Yes No Evidence of erosion or deposition Yes No Other obvious indicators of storm' water pollution ��iE Rating scale from T to 5 (1 = not present, 5 = heovily present) Monitoring Form Cbmpieted By: & '"`- Date: ��� f✓� STORM WATER MONITORING RECORD QUALITATIVE OBSERVATIONS Site: Honda Povrer,Equipment Manufacturing, Inc. 3721 NC Highway 119 Haw River, North Carolina 27258 Monitoring Date: Aril 15, 2015 Sample Location: R&D-01 Outfall Description: Pipe Discharge Characteristic Rating Comments Color Odor Clarity Floating Solids Suspended Solids Foam Yes No Oil -Sheen Yes oNo l' Evidence of erosion or deposition Yes Now +fits�� Other obviaus'indicators of storm water pollution /(OAIE Ratih_q scale from 1 tb 5<(1 = not present, 5 - heavily present) Monitoring Form Completed By: 6141-d4l-C46WDate: J, STORM WATER MONITORING RECORD TABLE OF ANALYTICAL RESULTS Site: Honda Power Equipment Manufacturing, Inc. 3721 NC Highway 119 Haw River, North Carolina 27258 Monitoring Date: April 15, 2015 HPE-01 HPE-02 HPE-03 R&D-01 Benchmark Values pH 6.17 5.96 6.07 5.92 6 to 9 Total Suspended Solids 17 16 11 20 100 EPA Method 200.8 Copper 0.0063 0.0076 0.0096 0.0028 0.007 Lead BDL BDL BDL BDL 0.030 Zinc 1 0.029 0.021 0,042 0.013 0.067 EPA Method 608 Target Pesticides BDL BDL BDL BDL 1 Target PCB's BDL BDL BDL BDL 1 EPA Method 624 Target volatile compounds BDL BDL BDL BDL 1 EPA Method 625 Target semi -volatile compounds BDL I BDL BDL BDL 1 EPA Method 1664 Oil and grease BDL I BDL BDL BDL 15 Notes: • Analytical results are presented in milligrams per liter (mg/L). • BDL = below laboratory minimum detection limits Storm water samples collected by Environmental Consulting & Technology personnel. SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis Environmental Consulting & Technology, Inc. 7208 Falls of Neuse Road, Suite 102 Raleigh, NC 27615 Attention: Carl Hewett Project Name: Honda Power Equipment Project Number:150246 Lot Number:QD16054 Date Completed:04127/2015 Kelly M. Nance Project Manager Q iu ACCoga This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, Inc. Page: 1 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Environmental Consulting & Technology, Inc. Lot Number: QD16054 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in Ws report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ('Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmental Services, Inc. Page: 2 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary Environmental Consulting & Technology, Inc. Lot Number: QD16054 Sample Number Sample ID Matrix Date Sampled Date Received 001 HPE-01 Aqueous 04/15/20151100 04/16/2015 002 HPE-02 Aqueous 04/15/20151145 04/16/2015 003 HPE-03 Aqueous 04115/20151000 04/16/2015 004 R&D-01 Aqueous 04115/20151245 04/16/2015 (4 samples) Shealy Environmental Services, Inc. Page: 3 of 46 108 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary Environmental Consulting & Technology, Inc. Lot Number: QD16054 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 HPE-01 Aqueous TSS SM 2540D- 17 mg/L 5 001 HPE-01 Aqueous Copper 200.8 6.3 ug1L 10 001 HPE-01 Aqueous Zinc 200.8 29 ug1L 10 002 HPE-02 Aqueous TSS SM 2540D- 16 mg1L 11 002 HPE-02 Aqueous Copper 200.8 7.6 u9/L 16 002 HPE-02 Aqueous Zinc 200.8 21 ug/L 16 003 HPE-03 Aqueous TSS SM 254013- 11 mg1L 17 003 HPE-03 Aqueous Copper 200.8 9.6 ug1L 22 003 HPE-03 Aqueous Zinc 20M8 42 ug1L 22 004 R&D-01 Aqueous TSS SM 2540D- 20 mg/L 23 004 R&D-01 Aqueous Copper 200.8 2.8 ug/L 28 004 R&D-01 Aqueous Zinc 200.8 13 ug]L 28 (12 detections) Shealy Environmental Services, Inc, Page: 4 of 46 106 Vantage Point [Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-001 Description: HPE-01 Matrix: Aqueous Date Sampled:0411512015 1100 Date Received:0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH) SM 4500-H B-2011 1 04/17/2015 1120 SKF 72764 1 (TSS) SM 254OD-2011 1 04/17/2015 1508 AMM1 72800 1 (SGT - HEM (n) 1664B 1 04120/2015 0933 TJK 72894 CAS Analytical Parameter Number Method Result Q PQL Units Run pH SM 4500-H B 6.17 su 1 TSS SM 254OD-20 17 2.0 mglL 1 SGT - HEM (non -polar material) 1664B ND 4.7 mg1L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J - Estimated result , POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 5 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-001 Description: HPE-01 Matrix: Aqueous Date Sampled:0411512015 1100 Date Received; 04116/2015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 04/24/2015 2328 PMM2 73326 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 ug/L 1 Acrylonitrile 107-13-1 624 ND 50 ug/L 1 Benzene 71-43-2 624 ND 5.0 ug/L 1 Bromodichlorometharie 75-27-4 624 ND 5.0 uglL 1 Bromoform 75-25-2 624 ND 5.0 ug1L 1 Bromomethane (Methyl bromide) 74-83-9 624 ND 5.0 ug/L 1 Carbon tetrachloride 56-23-5 624 ND 5.0 1 1 Chlorobenzene 108-90-7 624 ND 5.0 ug/L 1 Chloroethane 75-00-3 624 ND 5.0 ug/L 1 2-Chloroethylvinylether 110-75-8 624 ND 10 ug/L 1 Chloroform 67-66-3 624 ND 5.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5.0 ug/L 1 Di brom ochl oro methane 124-48-1 624 ND 5.0 ug1L 1 1,1-Dichloroethane 75-34-3 624 ND 5.0 ug/L 1 1,2-Dichloroethane 107-06-2 624 ND 5.0 uglL 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 uglL 1 trans-1,2-Dichloroethene 156-60-5 624 ND 5.0 ug1L 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 624 ND 5.0 ug1L 1 trans-1,3-Dichloropropene 10061-02-6 624 ND 5.0 ug/L 1 Ethylbenzene 100-41-4 624 ND 5.0 ug[L 1 Methylene chloride 75-09-2 624 ND 5.0 ug[L 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 uglL 1 Tetrachloroethene 127-18-4 624 ND 5.0 uglL 1 Toluene 108-88-3 624 ND 5.0 uglL 1 1,1,1-Trichloroethane 71-55-6 624 ND 5.0 ug1L 1 1,1,2-Trichloroethane 79-00-5 624 ND 5.0 ug1L 1 Trichloroethene 79-01-6 624 ND 5.0 ug/L 1 Vinyl chloride 75-01-4 624 ND 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroetha1 98 70-130 Bromofluorobenzene 101 70-130 Toluene-d8 101 70-130 POL = Practical quaniltation limit B = Detected in the method blank E = OuanStation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless Flagged with a "W' Shealy Environmental Services, Inc. Page: 6 of 46 1106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylah.com Level 1 Report v2.1 Semivolatile Organic Compounds by GCIMS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-001 Description: HPE-01 Matrix: Aqueous Date Sampled:0411512015 1100 Date Received:0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 04/21/2015 0100 ❑RBI 04/17/2015 1255 72771 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 NO 2.0 ug1L 1 Acenaphthylene 208-96-8 625 NO 2.0 ug1L 1 Anthracene 120-12-7 625 NO 2.0 uglL 1 Benzidine 92-87-5 625 NO 10 uglL 1 Benzo(a)anthracene 56-55-3 625 NO 2.0 ug1L 1 Benzo(a)pyrene 50-32-8 625 NO 2,0 ug1L 1 Benzo(b)fluoranthene 205-99-2 625 ND 2,0 uglL 1 Benzo(g,h,i)perylene 191-24-2 625 NO 2.0 ug1L 1 Benzo(k)fluoranthene 207-08-9 625 NO 2.0 uglL 1 4-Bromophenyl phenyl ether 101-55-3 625 N❑ 2.0 uglL 1 Butyl benzyl phthalate 85-68-7 625 ND 10 ug1L 1 4-Chloro-3-methyl phenol 59-50-7 625 NO 2.0 ug1L 1 bis(2-Chloroethoxy)methane 111-91-1 625 NO 2.0 ug1L 1 bis(2-Chloroethyl)ether 111-44-4 625 ND 2.0 ug1L 1 bis(2-Chloroisopropyl)ether 108-60-1 625 ND 2.0 uglL 1 2-Chloronaphthalene 91-58-7 625 NO 2.0 ug1L 1 2-Chlorophenol 95-57-8 625 NO 2.0 ug1L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 NO 2.0 ug1L 1 Chrysene 218-01-9 625 NO 2.0 ug1L 1 Dibenzo(a,h)anthracene 53-70.3 625 NO 2.0 uglL 1 1,2-Dichlorobe nzene 95-50-1 625 ND 2.0 uglL 1 1,3-Dichlorobe nzene 541-73-1 625 ND 2.0 uglL 1 1,4-Dichlorobe nzene 106-46-7 625 ND 2.0 uglL 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 uglL 1 2,4-Dichlorophenol 120-83-2 625 ND 2.0 ug/L 1 D!ethyl phthalate 84-66-2 625 ND 10 uglL 1 Dimethyl phthalate 131-11-3 625 ND 10 uglL 1 2,4-Dimethylphenol 105-67-9 625 ND 2.0 uglL 1 Di-n-butyl phthalate 84-74-2 625 NO 10 ug1L 1 4,6-Dinitro -2-methylphenol 534-52-1 625 NO 10 ug1L 1 2,4-Dirtitrophenol 51-28-5 625 NO 10 ug1L 1 2,4-Dinitrotoluene 121-14-2 625 NO 4.0 ug1L 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.0 ug1L 1 Di-n-octylphthalate 117-84-0 625 NO 10 ug1L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 NO 2.0 uglL 1 b is(2-Ethylhexyl)phth a late 117-81-7 625 ND 10 uglL 1 Fluoranthene 206-44-0 625 NO 2.0 ug1L 1 Fluorene 86-73-7 625 NO 2.0 ug1L 1 Hexachlorobenzene 118-74-1 625 NO 2.0 ug1L 1 Hexachlorobutadiene 87-68-3 625 NO 2.0 ug1L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 10 uglL 1 Hexachloroethane 67-72-1 625 NO 2.0 ug1L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 2.0 ug1L 1 Isophorone 78-59-1 625 ND 2.0 uglL 1 PQL = Practical quantization limit Fl = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PC and , MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Shealy Environmental Services, Inc. Page; 7 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www_shealylab,com Level 1 Report v2,1 Semivolatile Organic Compounds by GC/MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-001 Description: HPE-01 Matrix: Aqueous Date Sampled:0411512015 1100 Date Received : 041l 612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 04/21/2015 0100 li 04/17/2015 1255 72771 CAS Analytical Parameter Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 ug1L 1 Nitrobenzene 98-95-3 625 ND 2.0 u91L 1 2-Nitrophenol 88-75-5 625 ND 4.0 ug1L 1 4-Nitrophenol 100-02-7 625 ND 10 uglL 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 ug1L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 ug1L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 ug1L 1 Pentachlorophenol 87-86-5 625 ND 10 uglL 1 Phenanthrene 85-01-8 625 ND 2,0 uglL 1 Phenol 108-95-2 625 ND 2,0 uglL 1 Pyrene 129-00-0 625 ND 2.0 1 1 1,2,4-Trichtorobe nzene 120-82-1 625 ND 2.0 uglL 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 u911- 1 Runt Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 77 37-129 2-Fluorophenol 73 24-127 Nitrobenzene-d5 89 38-127 Phenol-d5 81 28-128 Terphenyl-d14 48 10-148 2,4,6-Tribromophenol 70 41-144 PQL = Practical quantltation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > i P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, alt soil sample analysis are reported on a dry weight basis unless flagged with a' W' Shealy Environmental Services, Inc. Page: 8 of 46 106 Vantage Polnt Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2,1 Organochlorine Pesticides and PCBs Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-001 Description: HPE-01 Matrix: Aqueous Date Sampled:0411512015 1100 Date Received:04116/2015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608 608 1 04123/20151111 PMS 04117/20151654 72807 2 608 608 1 04/21120151157 MEM 04/17120151654 72807 Parameter CAS Number Analytical Method Result Q PQL Units Run Aldrin 309-00-2 608 ND 0.040 uglL 1 Aroclor 1016 12674-11-2 608 ND 0,40 uglL 2 Aroclor 1221 11104-28-2 608 ND 0,40 uglL 2 Aroclor 1232 11141-16-5 608 ND 0.40 uglL 2 Aroclor 1242 53469-21-9 608 ND 0.40 uglL 2 Aroclor 1248 12672-29-6 608 ND 0.40 ug1L 2 Aroclor 1254 11097-69-1 608 ND 0.40 ug1L 2 Aroclor 1260 11096-82-5 608 ND 0.40 ug1L 2 gamma-BHC (Lindane) 58-89-9 608 ND 0.040 ug1L 1 alpha-BHC 319-84-6 608 ND 0.040 uglL 1 beta-BHC 319-85-7 608 NO 0.040 ug1L 1 delta-BHC 319-86-8 608 NO 0.040 ug1L 1 Chlordane 57-74-9 608 ND 0.40 uglt- 1 4,4'-DDD 72-54-8 608 NO 0.040 ug1L 1 4,4'-DDE 72-55-9 608 NO 0.040 ug1L 1 4,4'-DDT 50-29-3 608 NO 0.040 ug1L 1 Dieldrin 60-57-1 608 NO 0.040 uglL 1 Endosulfan 1 959-98-8 608 NO 0.040 ug1L 1 Endosulfan 11 33213-65-9 608 ND 0.040 ug1L 1 Endosulfan sulfate 1031-07-8 608 ND 0.040 uglL 1 Endrin 72-20-8 608 ND 0.040 uglL t Endrin aldehyde 7421-93-4 608 ND 0.040 ug1L i Heptachlor 76-44-8 608 ND 0.040 ug1L 1 Heptachlor epoxide 1024-57-3 608 ND 0.040 uglL 1 Toxaphene 8001-35-2 608 ND 0.40 uglL 1 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits Decachlorobiphenyl 48 20-131 53 20-131 Tetra chloro-m-xylene 69 26-132 88 26-132 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Noi detected at or above the PQL J = Estimated result < PQL and , MDL P = The RPD between two GG columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Shealy Environmental Services, Inc. Page: 9 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 ICP-MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-001 Description: HPE-01 Matrix: Aqueous Date Sampled:0411512015 1100 Date Received: 0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 04117120151957 CDF 04117/20151223 72769 2 200.2 200.8 1 04/20/20151948 CDF 04/17/20151223 72769 CAS Analytical Parameter Number Method Result Q PQL Units Run Copper 7440-50-8 200.8 6.3 1.0 ug1L 1 Lead 7439-92-1 200.8 ND 1.0 ug/L 2 Zinc 7440-66-6 200.8 29 10 uglL 1 POL = Practical quanlitation limit 8 = Detected in the method blank E=Ouanlitalion of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result - POL and a MDL P = The RPD between two CC columns exceeds 40% N - Recovery is out of crilena Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Shealy Environmental Services, Inc. Page: 10 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level t Report v2.1 Inorganic non-metals Glient: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-002 Description: HPE-02 Matrix: Aqueous Date Sampled:04115/2015 1145 Date Received: 0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH) SM 4500-H B-2011 1 04/17/2015 1120 SKF 72764 1 (TSS) SM 2540D-2011 1 04/17/2015 1508 AMM1 72800 1 (SGT - HEM (n) 1664B 1 04/20/2015 0933 TJK 72894 CAS Analytical Parameter Number Method Result Q PQL Units Run pH SM 4500-H B 5.96 su 1 TSS SM 254OD-20 16 3.3 mg1L 1 SGT - HEM (non -polar material) 16648 ND 4.6 mg1L 1 PQL = Practical quantilation limit 8 = Detected in the method blank E = Quantitaticn of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < PQL and > MDL P = The RPn between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" Shealy Environmental Services, Inc. Page: 11 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9411 www.shealylab.com Level 1 Repon v2.1 Volatile Organic Compounds by GC/MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-002 Description: HPE-02 Matrix: Aqueous Date Sampled:0411512015 1145 Date Received:04116/2015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 04/24/2015 2351 PMM2 73326 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 ug/L 1 Acrylonitrile 107-13-1 624 ND 50 ug/L 1 Benzene 71-43-2 624 ND 5.0 ug1L 1 Bromodichloromethane 75-27-4 624 ND 5.0 ug/L 1 Bromoform 75-25-2 624 ND 5.0 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 624 ND 5.0 ug1L 1 Carbon tetrachloride 56-23-5 624 ND 5.0 ug1L 1 Chlorobenzene 108-90-7 624 ND 5.0 ug1L 1 Chloroethane 75-00-3 624 ND 5.0 uglL 1 2-Chloroethylvinylether 110-75-8 624 ND 10 ug1L 1 Chloroform 67-66-3 624 ND 5.0 ugIL 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5.0 ug1L 1 Dibromochloromethane 124-48-1 624 ND 5.0 ug/L 1 1,1-Dichloroethane 75-34-3 624 ND 5.0 ug/L 1 1,2-Dichloroethane 107-06-2 624 ND 5.0 ug/L 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 ug/L 1 trans-1,2-Dichloroethene 156-60-5 624 ND 5.0 ug/L 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 624 ND 5.0 ug/L 1 trans-1.3-Dichloropropene 10061-02-6 624 ND 5.0 ug/L 1 Ethylbenzene 100-41-4 624 ND 5.0 ug/L 1 Methylene chloride 75-09-2 624 ND 5.0 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 ug1L 1 Tetra chloroethene 127-18-4 624 ND 5.0 ug1L 1 Toluene 108-88-3 624 ND 5.0 ug/L 1 1,1,1-Trichloroethane 71-55-6 624 ND 5.0 ug/L 1 1,1,2-Trichloroethane 79-00-5 624 ND 5.0 ug1L 1 Trichloroethene 79-01-6 624 ND 5.0 ug1L i Vinyl chloride 75-01-4 624 ND 5.0 ug1L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 97 70-130 Bromofluorobenzene 104 70-130 Toluene -dB 104 70-130 PQL = Practical quantilation limit B = Detected in the method blank E = Quantitation at compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result c PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Wnere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a Shealy Environmental Services, Inc. Page: 12 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS • Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-002 Description: HPE-02 Matrix: Aqueous Date Sampled: 0411512015 1145 Date Received: 0411612 015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 04/21/2015 0124 DRB1 04/17/2015 1255 72771 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 ug/L 1 Acenaphthylene 208-96-8 625 NO 2.0 ug/L 1 Anthracene 120-12-7 625 ND 2.0 ug1L 1 Benzidine 92-87-5 625 ND 10 ug1L 1 Benzo(a)anthracene 56-55-3 625 ND 2.0 ug/L 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug/L 1 Benzo(b)fluoranthene 205-99-2 625 ND 2.0 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 ug/L 1 Benzo(k)fluoranthene 207-08-9 625 ND 2.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 ug/L 1 Butyl benzyl phthalate 85-68-7 625 NO 10 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625 NO 2.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625 NO 2.0 u91L 1 his (2-C hloroethyl)ether 111-44-4 625 NO 2.0 ug1L 1 bis (2-C hloroisopropyl) ether 108-60-1 625 NO 2.0 ug1L 1 2-Chloronaphthalene 91-58-7 625 NO 2.0 u911- 1 2-Chlorophenol 95-57-8 625 NO 2.0 u91L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 NO 2.0 u91L 1 Chrysene 218-01-9 625 NO 2.0 ug1L 1 Dibenzo(a,h)anthracene 53-70-3 625 NO 2.0 ug1L 1 1,2-Dichlorobe nzene 95-50-1 625 ND 2.0 ug/L 1 1,3-Dichlorobe nzene 541-73-1 625 ND 2.0 ug/L 1 1,4-Dichlorobenzene 106-46-7 625 ND 2.0 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 NO 10 ug/L 1 2,4-Dichlorophenol 120-83-2 625 NO 2.0 ug/L 1 Diethylphthalate 84-66-2 625 NO 10 ug/L 1 Dimethyl phthalate 131-11-3 625 NO 10 ug/L 1 2,4-Dimelhylphenol 105-67-9 625 NO 2.0 ug/L 1 Di-n-butyl phthalate 84-74-2 625 ND 10 ug11- 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 10 ug1L 1 2,4-Dinitrophenol 51-28-5 625 ND 10 ug1L 1 2,4-Dinitrotoluene 121-14-2 625 ND 4.0 ug/L 1 2,6- Din itrotoluene 606-20-2 625 NO 4.0 ug/L 1 Di-n-octylphthalate 117-84-0 625 ND 10 ug1L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 2.0 ug1L 1 b is(2-Fthyl hexyl)phiha late t 17-81-7 625 NO 10 ug1L 1 Fluoranthene 206-44-0 625 NO 2.0 ug1L 1 Fluorene 86-73-7 625 NO 2.0 ug1L 1 Hexachlorobenzene 118-74-1 625 NO 2.0 ug1L 1 Hexachlorobutadiene 87-68-3 625 ND 2.0 uglL 1 Hexachlorocyclope nta die ne 77-47-4 625 ND 10 uglL 1 Hexachloroethane 67-72-1 625 ND 2.0 uglL 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 NO 2.0 uglL 1 Isophorone 78-59-1 625 ND 2.0 uglL 1 PQL = Practical quanhtation limit R = Detected in the method blank E = Quantitalion of compound exceeded the calibration range H - Out of holding time ND = Not detected at or above the PQL d = Estimated result < PQL and a MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported or a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 13 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS Client: Environmental Consulting R Technology, Inc. Laboratory ID: QD16054-002 Description: HPE-02 Matrix: Aqueous Date Sampled :0411512015 1145 Date Received:0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 04/21/2015 0124 DRB1 04/17/2015 1255 72771 CAS Analytical Parameter Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 ug/L 1 Nitrobenzene 98-95-3 625 ND 2.0 ug/L 1 2-Nitrophenol 88-75-5 625 ND 4.0 ug/L 1 4-Nitrophenol 100-02-7 625 ND 10 ug/L 1 WIN itrosodimethylamine 62-75-9 625 ND 2,0 ug1L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 ug1L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 ug1L 1 Pentachlorophenol 87-86-5 625 ND 10 ug1L 1 Phenanthrene 85-01-8 625 ND 2.0 ug1L 1 Phenol 108-95-2 625 ND 2.0 ug1L 1 Pyrene 129-00-0 625 ND 2.0 ug1L 1 1,2,4-Trichlorobenzene 120-82-1 625 ND 2.0 L;g1L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 ug1L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 74 37-129 2-Fluorophenol 60 24-127 Nitrobenzene-d5 74 38-127 Phenol-d5 79 28-128 Terphenyl-d14 55 10-148 2,4,6-Tribromophenol 66 41-144 POL - Practical quantization limit B = Detected in the method blank E = ouanti¢ation of compound exceeded the calibration range H - Out of holding time ND = Not detected at or above the POL J = Estimated result < POL and > MOL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reportec on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 14 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Organochlorine Pesticides and PCBs Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-002 Description: HPE-02 Matrix: Aqueous Date Sampled:0411512015 1145 Date Received70411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608 608 1 04/23/20151126 PMS 04/17120151654 72807 2 608 608 1 04121/20151211 MEM 04/17/20151654 72807 CAS Analytical Parameter Number Method Result Q PQL Units Run Aldrin 309-00-2 608 ND 0.040 ug1L 1 Aroclor 1016 12674-11-2 608 ND 0,40 ug1L 2 Aroclor 1221 11104-28-2 608 ND 0.40 ug1L 2 Aroclor 1232 11141-16-5 608 ND 0.40 ug1L 2 Aroclor 1242 53469-21-9 608 ND 0.40 ug1L 2 Aroclor 1248 12672-29-6 608 ND 0.40 ug1L 2 Aroclor 1254 11097-69-1 608 ND 0.40 uglL 2 Aroclor 1260 11096-82-5 608 ND 0.40 uglL 2 gamma-BHC (Lindane) 58-89-9 608 ND 0.040 uglL 1 alpha-BHC 319-84-6 608 ND 0.040 ug1L 1 beta-BHC 319-85-7 608 ND 0.040 uglL 1 delta-BHC 319-86-8 608 ND 0.040 uglL 1 Chlordane 57-74-9 608 ND 0.40 ug1L 1 4,4'-DDD 72-54-8 608 ND 0.040 uglL 1 4,4'-DDE 72-55-9 608 ND 0.040 ug1L 1 4,4'-DDT 50-29-3 608 ND 0.040 ug1L 1 Dieldrin 60-57-1 608 ND 0.040 ug1L 1 Endosulfan 1 959-98-8 608 ND 0.040 u91L 1 Endosulfan II 33213-65-9 608 ND 0.040 u91L 1 Endosulfan sulfate 1031-07-8 608 ND 0.040 uglL 1 Endrin 72-20-8 608 ND 0.040 uglL 1 Endrin aldehyde 7421-93-4 608 ND 0.040 ug1L 1 Heptachlor 76-44-8 608 ND 0.040 ug1L 1 Heptachlor epoxide 1024-57-3 608 ND 0.040 ug1L 1 Toxaphene 8001-35-2 608 ND 0A0 ug1L 1 Surrogate Decachlorobiphenyl Tetrachioro-m-xylene Run 1 Acceptance Run 2 Acceptance Q % Recovery Limits Q % Recovery Limits 39 20-131 40 20-131 64 26-132 79 26-132 POL = PracScal quantitalion limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MOIL P - The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Mere applicable, aTl soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 15 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab,com Level 1 Report v21 ICP-MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-002 Description: HPE-02 Matrix: Aqueous Date Sampled:0411512015 1145 Date Received:04116/2015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 04/17/2015 2002 CDF 04/17/2015 1223 72769 2 200.2 200.8 1 04/20/20151953 CDF 04117120151223 72769 CAS Analytical Parameter Number Method Result Q PQL Units Run Copper 7440-50-8 200.8 7.6 1.0 uglL 1 Lead 7439-92-1 200.8 ND 1.0 uglL 2 Zinc 7440-66-6 200.8 21 10 ug1L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitatior of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > Ml P = The RPD between two GC columns exceeds 4001 N = Recovery is out of criteria Where applicable, all sail sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc, Page: 16 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level i Reportv2.1 Inorganic non-metals Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-003 Description: HPE-03 Matrix: Aqueous Date Sampled:0411512015 1000 Date Received:04116/2015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH) SM 4500-H B-2011 1 04/17/2015 1120 SKF 72764 1 (TSS) SM 254OD-2011 1 04/17/2015 1508 AMM1 72800 1 (SGT - HEM (n) 1664B 1 04/20/2015 0933 TJK 72894 CAS Analytical Parameter Number Method Result Q PQL Units Run pH SM 4500-H B 6.07 su 1 TSS SM 25400-20 11 1.4 mglL 1 SGT- HEM (non -polar material) 1664B ND 4.3 mglL 1 PQL - Practical quantization limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at ar above the PQL J = Estimated result a PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 17 of 46 406 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (603) 791-9111 www.shealylab.com Level 1 Reportv2.1 Volatile Organic Compounds by GC/MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-003 Description: HPE-03 Matrix: Aqueous Date Sampled:04115/2015 1000 Date Received:0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 04/25/2015 0014 PMM2 73326 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 ug1L 1 Acrylonitrile 107-13-1 624 ND 50 ug1L 1 Benzene 71-43.2 624 ND 5.0 ug1L 1 Bromodichloromethane 75-27-4 624 ND 5.0 ug/L 1 Bromoform 75-25-2 624 ND 5.0 ug1L 1 Bromomethane (Methyl bromide) 74-83-9 624 ND 5.0 ug/L 1 Carbon tetrachloride 56-23-5 624 ND 5.0 ug1L 1 Chlorobenzene 108-90-7 624 ND 5.0 ug1L 1 Chleroethane 75-00-3 624 ND 5.0 ug/L 1 2-Chloroethylvinylether 110-75-8 624 ND 10 ugIL 1 Chloroform 67-66-3 624 ND 5.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5.0 ug/L 1 Dibromochloromethane 124-48-1 624 ND 5.0 ug/L 1 1,1-Dichloroethane 75-34-3 624 ND 5.0 ug/L 1 1,2-Dichloroethane 107-06-2 624 ND 5.0 ug/L 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 ug1L 1 trans-1,2-Dichloroethene 156-60-5 624 ND 5.0 ug1L 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 ug1L 1 cis-1,3-Dichloropropene 10061-01-5 624 ND 5.0 ug1L 1 trans-1,3-Dichloropropene 10061-02-6 624 ND 5.0 ug11- 1 Ethylbenzene 100-41-4 624 ND 5.0 ug/L 1 Methylene chloride 75-09-2 624 ND 5.0 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 ug/L 1 Tetrachloroethene 127-18-4 624 ND 5.0 ug/L 1 Toluene 108-88-3 624 ND 5.0 ug/L 1 1,1,1-Trichloroethane 71-55-6 624 ND 5.0 ug1L 1 1,1,2-Trichloroethane 79-00-5 624 ND 5.0 ug1L 1 Trichloroethene 79-01-6 624 ND 5.0 ug1L i Vinyl chloride 75-01-4 624 ND 5.0 ug1L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 95 70-130 BromoFluorobenzene 104 70-130 Toluene-d8 102 70-130 PQL = Practical quantltation limit e = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the POL J - Estimated result < PQL and - MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported cn a dry weight basis unless flagged with a Shealy Environmental Services, Inc. Page: 18 of 46 106 Vantage Point Drive West Columbia, SC 29172 (B03) 791-9700 Fax (803) 791-9111 www.shealylab.corrt Level 1 Report v21 Semivolatile Organic Compounds by GC/MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-003 Description: HPE-03 Matrix: Aqueous Date Sampled:0411512015 1000 Date Received: 0411612015 Run Prep Method Analytical Method 1 625 625 Dilution Analysis Date Analyst 1 04/21/2015 0147 DRB1 Prep Date 04/17/2015 1255 Batch 72771 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 ug1L 1 Acenaphthylene 208-96-8 625 ND 2.0 ug1L 1 Anthracene 120-12-7 625 ND 2.0 ug1L 1 Benzidine 92-87-5 625 ND 10 ug1L 1 Benzo(a)anthracene 56-55-3 625 ND 2.0 ug1L 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug/L 1 Benzo(b)fluoranthene 205-99-2 625 ND 2.0 ug1L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 u91L 1 Benzo(k)fluoranthene 207-08-9 625 ND 2.0 u91L 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 uglL 1 Butyl benzyl phthalate 85-68-7 625 ND 10 ug1L 1 4-Chloro-3-methyl phenol 59-50-7 625 ND 2.0 uglL 1 bis(2-CNoroethoxy)methane 111-91-1 625 ND 2.0 uglL 1 bis(2-CNoroethyl)ether 111-44-4 625 ND 2.0 uglL 1 bis(2-Chloroisopropyl)ether 108-60-1 625 ND 2.0 uglL 1 2-Chloronaphthalene 91-58-7 625 ND 2.0 uglL 1 2-ChlorOphenol 95-57-8 625 ND 2.0 uglL 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 ug1L 1 Chrysene 218-01-9 625 ND 2.0 ug1L 1 Dibenzo(a,h)anthracene 53-70-3 625 ND 2.0 uglL 1 1,2-Dichlorobenzene 95-50-1 625 ND 2.0 ug1L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 ug1L 1 1,4-Dichlorobenzene 106-46-7 625 ND 2.0 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 ug/L 1 2,4-Dichlorophenol 120-83.2 625 ND 2.0 ug/L 1 Diethylphthalate 84-66-2 625 ND 10 ug/L 1 Dimethyl phthalate 131-11-3 625 ND 10 ug/L 1 2,4-Dimethylphenol 105-67-9 625 ND 2.0 ug/L 1 Di-n-butyl phthalate 84-74-2 625 ND 10 ug/L 1 4.6-Dinitro-2-methylphenol 534-52-1 625 ND 10 ug/L 1 2,4-Dinitrophenol 51-28.5 625 ND 10 ug/L 1 2,4-Dinitrototuene 121-14-2 625 ND 4.0 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.0 ug1L 1 Di-n-octylphthalate 117-84-0 625 ND 10 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 2.0 ug/L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 ND 10 ug1L 1 Fluoranthene 206-44-0 625 ND 2.0 ug1L 1 Fluorene 86-73-7 625 ND 2.0 ug1L 1 Hexachlorobenzene 118-74-1 625 ND 2.0 ug1L 1 Hexachlorobutadiene 87-68-3 625 ND 2.0 ug1L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 10 ug1L 1 Hexachloroethane 67-72-1 625 ND 2.0 ug/L 1 lndeno(1,2.3-c,d)pyrene 193-39-5 625 ND 2.0 u91L 1 Isophorone 78-59-1 625 ND 2.0 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quaniitation of compound exceeded Me calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and ? MDL P = The RPD between two GC columns exceeds 4D% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 19 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2.1 Semivolatile Organic Compounds by GC/MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-003 Description: HPIE-03 Matrix: Aqueous Date Sampled:0411512015 1000 Date Received:0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 04/21/2015 0147 DR01 04/17/2015 1255 72771 CAS Analytical Parameter Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 ug/L 1 Nitrobenzene 98-95-3 625 ND 2.0 u9/L 1 2-Nitrophenol 88-75-5 625 ND 4.0 ug/L 1 4-Nitrophenol 100-02-7 625 ND 10 ug1L 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 ug1L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 ug1L 1 N-Nitrosodiphenylamine (Diphenylamine) 86.30-6 625 ND 2.0 ug1L 1 Pentachlorophenol 87-86-5 625 ND 10 ug1L 1 Phenanthrene 85-01-8 625 ND 2.0 ug1L 1 Phenol 108-95-2 625 ND 2.0 ug1L 1 Pyrene 129-00-0 625 ND 2.0 ug1L 1 1,2,4-Trichlorobe nzene 120-82-1 625 ND 2.0 u91L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 ug1L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 76 37-129 2-Fluorophenol 74 24-127 Nitrobenzene-d5 85 38-127 Phenol-d5 82 28-128 Terphenyl-d14 73 10-148 2,4,6-Tribromophenol 76 41-144 PQL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 20 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com tevel 1 Report v21 Organochlorine Pesticides and PCBs Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-003 Description: HPE-03 Matrix: Aqueous Date Sampled:0411512015 1000 Date Received:0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608 608 1 04/23120151140 PMS 04/17/20151654 72807 2 608 608 1 04/21120151224 MEM 04117/20151654 72807 CAS Analytical Parameter Number Method Result Q PQL Units Run Aldrin 309-00-2 608 ND 0.040 ug1L 1 Aroclor 1016 12674-11-2 608 ND 0.40 ug1L 2 Aroclor 1221 11104-28-2 608 ND 0.40 ug1L 2 Aroclor 1232 11141-16-5 608 ND 0.40 ug/L 2 Aroclor 1242 53469-21-9 608 ND 0.40 ug/L 2 Aroclor 1248 12672-29-6 608 ND 0A0 ug1L 2 Aroclor 1254 11097-69-1 608 ND 0A0 ug/L 2 Aroclor 1260 11096-82-5 608 ND 0A0 ug1L 2 gamma-BHC (Lindane) 58-89-9 608 ND 0.040 ug1L 1 alpha-BHC 319-84-6 608 ND 0.040 ug/L 1 beta-BHC 319-85-7 608 ND 0.040 ug/L 1 delta-BHC 319-86-8 608 ND 0.040 ug/L 1 Chlordane 57-74-9 608 ND 0.40 ug1L 1 4,4'-DDD 72-54-8 608 ND 0.040 ug1L 1 4,4'-DDE 72-55-9 608 ND 0.040 ug1L 1 4,4'-DDT 50-29-3 608 ND 0.040 ug1L 1 Dieldrin 60-57-1 608 ND 0.040 ug1L 1 Endosulfan 1 959-98-8 608 ND 0.040 ug1L 1 Endosulfan 11 33213-65-9 608 ND 0.040 ug1L 1 Endosulfan sulfate 1031-07-8 608 ND 0.040 ug/L 1 Endrin 72-20-8 608 ND 0.040 ug1L 1 Endrin aldehyde 7421-93-4 608 ND 0.040 ug1L 1 Heptachlor 76-44-8 608 ND 0.040 ug/L 1 Heptachlor epoxide 1024-57-3 608 ND 0.040 ug1L 1 Toxaphene 8001-35.2 608 ND 0.40 ug1L 1 Surrogate Decachlorobiphenyl Tetrach loro-m-xylene Run 1 Acceptance Run 2 Acceptance Q % Recovery Limits - Q % Recovery Limits 42 20-131 45 20-131 69 26-132 88 26-132 PQL = Practical cluanlitation limit B = Detected in the method blank E = Quantization of compound exceeded the calibration range H = Out of holding time ND r Not detected at or above the POL J = Estimated result 4 PQL and > M DL P = The RP 1) between two GC columns exceeds 40% N = Recovery is out of crilena Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a Shealy Environmental Services, Inc, Page: 21 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 ICP-MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-003 Description: HPE-03 Matrix: Aqueous Date Sampled:0411512015 1000 Date Received:0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 04/17/2015 2006 CDF 04/17/2015 1223 72769 2 200.2 200.8 1 04/20/20151958 CDF 04/17/20151223 72769 CAS Analytical Parameter Number Method Result Q PQL Units Run Copper 7440-50-8 200.8 9.6 1.0 ug1L 1 Lead 7439-92-1 200.8 NO 1.0 ug/L 2 Zinc 7440-66-6 200.8 42 10 ug1L 1 POL = Practical quantitation limit 0 - Detected in the method blank E = Quantitalion of compound exceeded the calibration range H = Out of holding time Nn = Not detected at or above the PQL J = Estimated result t PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 22 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals - Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-004 Description: R&D-01 Matrix: Aqueous Date Sampled:0411512015 1245 Date Received: 04/1612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH) SM 4500-H B-2011 1 04/1712015 1120 SKF 72764 1 (TSS) SM 254OD-2011 1 04/17/2015 1508 All 72800 1 (SGT - HEM (n) 1664B 1 04/20/2015 0933 TJK 72894 CAS Analytical Parameter Number Method Result Q PQL Units Run pH SM 4500-H B 5.92 su 1 TSS SM 25400-20 20 1.3 mg1L 1 SGT - HEM (non -polar material) 1664E ND 4.6 mg/L 1 PQL = Practical quantitalion limit S = Detected in the method blank E - Quantitation of compound exceeded the calibration range H = OLt of holding time ND = Net detected at or above the PQL J = Estimated result a PQL and? MDL P ='The RPD between two GC columns exceeds 40%. N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 23 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheatylab.com Level 1 Reportv2.1 Volatile Organic Compounds by GC/MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-004 Description: R&D-01 Matrix: Aqueous Date Sampled:04/1512015 1245 Date Received:0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 50308 624 1 04/25/2015 0037 PMM2 73326 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 uglL 1 Acrylonitrile 107-13-1 624 ND 50 u911- 1 Benzene 71-43-2 624 ND 5.0 uglL 1 Brom od ichlo ro methane 75-27-4 624 ND 5.0 ug1L 1 Bromoform 75-25-2 624 ND 5.0 u91L 1 Bromomethane (Methyl bromide) 74-83-9 624 ND 5.0 ug1L 1 Carbon tetrachloride 56-23-5 624 ND 5.0 uglL 1 Chlorobenzene 108-90-7 624 ND 5.0 uglL 1 Chloroethane 75-00-3 624 ND 5.0 uglL 1 2-Chloroethylvinylether 110-75-8 624 ND 10 uglL 1 Chloroform 67-66-3 624 ND 5.0 ug1L 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5.0 ug1L 1 Di bromochloro methane 124-48-1 624 ND 5.0 ug11- 1 1,1-Dichloroethane 75-34-3 624 ND 5.0 ug1L t 1,2-Dichloroethane 107-06-2 624 ND 5.0 uglL 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 uglL 1 trans-1,2-Dichloroethene 156-60-5 624 ND 5.0 uglL 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 uglL 1 cis-1,3-Dichloropropene 10061-01-5 624 ND 5.0 uglL 1 trans-1,3-Dichloropropene 10061-02-6 624 ND 5.0 uglL 1 Ethylbenzene 100-41-4 624 ND 5.0 uglL 1 Methylene chloride 75-09-2 624 ND 5.0 ug1L 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 ug1L 1 Tetra chloroethe ne 127-18-4 624 ND 5.0 ug1L 1 Toluene 108-88-3 624 ND 5.0 ug1L 1 1,1,1-Trichloroethane 71-55-6 624 ND 5.0 uglL 1 1,1,2-Trichloroethane 79-00-5 624 ND 5.0 uglL 1 Trichloroethene 79-01-6 624 ND 5.0 ug1L 1 Vinyl chloride 75-01-4 624 ND 5.0 ug1L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 96 70-130 Bromofluorobenzene 103 70-130 Toluene-d8 104 70-130 POL = Practical quantitation limit B = Detected in the method blank E = Quantization of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the POL J = Estimated result < PQL and - MDL P = The RPD between Iwo GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless Flagged with a "W' Shealy Environmental Services, Inc. Page: 24 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.Com Level 4 Report v2.1 Semivolatile Organic Compounds by GC/MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-004 Description: R&D-01 Matrix: Aqueous Date Sampled:04/15/2015 1245 Date Received! 0411612016 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 04/21/2015 0210 DRB1 04/17/2015 1255 72771 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32.9 625 ND 2.0 ug/L 1 Acenaphthylene 208-96-8 625 ND 2.0 ug/L 1 Anthracene 120-12-7 625 ND 2.0 ug/1- 1 Benzidine 92-87-5 625 ND 10 ug/L 1 Benzo(a)anth race ne 56-55-3 625 ND 2.0 uglL 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 uglL 1 Benzo(b)fluoranthene 205-99-2 625 ND 2.0 ug1L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 ug1L 1 Benzo(k)4uoranthene 207-08-9 625 ND 2.0 ug1L 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 ug1L 1 Butyl benzyl phthalate 85-68-7 625 ND 10 ug1L 1 4-Chloro-3-methyl phenol 59-50-7 625 ND 2.0 ug/L 1 bis(2-ChIoroethoxy)methane 111-91-1 625 ND 2.0 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625 ND 2.0 ug/L 1 bis(2-Chloroisopropyl)ether 108-60-1 625 ND 2.0 ug/L 1 2-Chloronaphthelene 91-58-7 625 ND 2.0 ug1L 1 2-Chlorophenol 95-57-8 625 ND 2.0 ug1L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 ug1L 1 Chrysene 218-01-9 625 ND 2.0 ug1L 1 Dibenzo(a,h)anthracene 53-70-3 625 ND 2.0 ug1L 1 1,2-Dichlorobenzene 95-50-1 625 ND 2.0 ug1L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 ug1L 1 1,4-Dichlorobenzene 106-46-7 625 ND 2.0 uglL 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 uglL 1 2,4-Dichlorophenol 120-83-2 625 ND 2.0 uglL 1 Diethylphthalate 84-66-2 625 ND 10 uglL 1 Dimethyl phthalate 131-11-3 625 ND 10 uglL 1 2,4-Dimethylphenol 105-67-9 625 ND 2.0 uglL 1 Di-n-butyl phthalate 84-74-2 625 ND 10 uglL 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 10 uglL 1 2,4-Dinitrophenol 51-28-5 625 ND 10 ug1L 1 2,4-Dinitrotoluene 121-14-2 625 ND 4.0 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.0 ug/L 1 Di-n-octylphthalate 117-84-0 625 ND 10 ug1L 1 1,2-Diphenyihydrazine(as azobenzene) 103-33-3 625 ND 2.0 ug1L 1 bis(2- Ethyl hexyl) phtha late 117-81-7 625 ND 10 ug1L 1 Fluoranthene 206-44-0 625 ND 2.0 ug1L 1 Fluorene 86-73-7 625 ND 2.0 ug1L 1 Hexachlorobenzene 118-74-1 625 ND 2.0 ug1L 1 Hexachlorobutadiene 87-68-3 625 ND 2.0 ug1L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 10 ug1L 1 Hexachloroethane 67-72-1 625 ND 2.0 ug1L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 2.0 ug1L 1 Isophorone 78-59-1 625 ND 2.0 uglL 1 PQL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPO between two GC columns exceeds 40% N - Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 25 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-004 Description: R&D-01 Matrix: Aqueous Date Sampled:04/1512015 1245 Date Received:04/1612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 04/21/2015 0210 DRB1 04/17/2015 1255 72771 CAS Analytical Parameter Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 ug1L 1 Nitrobenzene 98-95-3 625 ND 2.0 ug/L 1 2-Nitrophenol 88-75-5 625 ND 4.0 ug/L 1 4-Nitrophenol 100-02-7 625 ND 10 ug/L 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 ug/L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 uglL 1 N-Nilrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 u91L 1 Pentachlorophenol 87-86-5 625 ND 10 ug/L 1 Phenanthrene 85-01-8 625 ND 2.0 ug1L 1 Phenol 108-95-2 625 ND 2.0 ug1L 1 Pyrene 129-00-0 625 ND 2.0 ug1L 1 1.2.4-Trichlorobe nzene 120-82-1 625 ND 2.0 ug1L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 ug1L 1 Surrogate Run 1 Q % Recovery Acceptance Limits 2-Fluorobiphenyl 85 37-129 2-Fluorophenol 84 24-127 Nitrobenzene-d5 96 38-127 Phenol-d5 92 28-128 Terphenyl-d14 71 10-148 2,4,6-Tribromophenol 83 41-144 PQL = Practical quantitation limit B = Detected in the method blank E = Ouantltation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result , POL and > MOL P = The RP6 between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported cn a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 26 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2.1 Organochlorine Pesticides and PCBs . Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-004 Description: R&D-01 Matrix: Aqueous Date Sampled:0411512015 1245 Date Received:04116/2015 Run Prop Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608 608 1 04/23120151155 PMS 04/17/20151654 72807 2 608 608 1 04/21/20151237 MEM 04117/20151654 72807 CAS Analytical Parameter Number Method Result Q PQL Units Run Aldrin 309-00-2 608 ND 0.040 uglL 1 Aroclor 1016 12674-11-2 608 NO 0.40 ug1L 2 Aroclor 1221 11104-28-2 608 ND 0.40 uglL 2 Aroclor 1232 11141-16-5 608 ND 0.40 uglL 2 Aroclor 1242 53469-21-9 608 ND 0.40 uglL 2 Aroclor 1248 12672-29-6 608 ND 0.40 uglL 2 Aroclor 1254 11097-69-1 608 ND 0.40 ug1L 2 Aroclor 1260 11096-82-5 608 NO 0.40 uglL 2 gamma-BHC (Lindane) 58-89-9 608 NO 0.040 uglL 1 alpha-BHC 319-84-6 608 NO 0.040 uglL 1 beta-BHC 319-85-7 608 NO 0.040 uglL 1 delta-BHC 319-86-8 608 ND 0.040 ug1L 1 Chlordane 57-74-9 608 ND 0A0 uglL 1 4,4'-DDD 72-54-8 608 ND 0.040 ug/L 1 4,4'-DDE 72-55-9 608 ND 0.040 uglL 1 4,4'-DDT 50-29-3 608 ND 0.040 ug1L 1 Dieldrin 60-57-1 608 ND 0.040 uglL 1 Endosulfan 1 959-98-8 608 ND 0.040 uglL 1 Endosulfan II 33213-65-9 608 ND 0.040 uglL 1 Endosulfan sulfate 1031-07-8 608 NO 0.040 uglL 1 Endrin 72-20-8 608 NO 0.040 uglL 1 Endrin aldehyde 7421-93-4 608 NO 0.040 uglL 1 Heptachlor 76-44-8 608 NO 0.040 uglL 1 Heptachlor epoxide 1024-57-3 608 NO 0.040 uglL 1 Toxaphene 8001-35-2 608 NO 0.40 uglL 1 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits Decachlorobiphenyl 37 20-131 39 20-131 Tetrachloro-m-xylene 66 26-132 81 26-132 PQL = Practical quay ilation limit 13 = Detected in the method blank E = Quantilalion of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all sail sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 27 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab,com Level 1 Report v2.1 ICP-MS Client: Environmental Consulting & Technology, Inc. Laboratory ID: QD16054-004 Description: R&D-01 Matrix: Aqueous Date Sampled:0411512015 1245 Date Received:0411612015 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 04/17/2015 2011 CDF 04/17/2015 1223 72769 2 200.2 200.8 1 04/20/2015 2012 CDF 04/17/2015 1223 72769 CAS Analytical Parameter Number Method Result Q PQL Units Run Copper 7440-50.8 200.8 2.8 1.0 ug1L 1 Lead 7439-92-1 200.8 ND 1.0 ug1L 2 Zinc 7440-66-6 200.8 13 10 ug1L 1 POL = Pracbcal quantization limit B = Detected in the method blank E = Quantitabon of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result � PQL and > MOL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless Slagged with a "W' Shealy Environmental Services, Inc. Page: 28 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Shealy Environmental Services, Inc. Page: 29 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals - MB Sample ID: QQ72764-001 Matrix: Aqueous Batch:72764 Analytical Method: SM 4500-H B-2011 Parameter Result Q Dil PQL Units Analysis Date pH 6.78 1 0.000 su 04/17120151120 P4L = Practical quanbtation limit P = The RPD pelweer two GC columns exceeds 40% N = Recovery is out of criteria 1 i ND = Not detected at or above the PC d = Estimated result < PQL and � MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 30 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals - Duplicate Sample ID: QD16054-004DU Matrix: Aqueous Batch;72764 Analytical Method: SM 4500-H B-2011 Sample Amount Result % RPD Parameter (su) Q Dil % RPD Limit Analysis Date pH 5.92 5.95 1 0.51 20 04/17120151120 POL = Practical quantitation limit P = The RPD between two GC columrs exceeds 40% N = Recovery is out of criteria NO = Not detected at or above the POL J = Estimated result < POL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 31 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheaTylab.com Level 1 Report v2.1 Inorganic non-metals - MB Sample ID: QQ72800-001 Matrix: Aqueous Batch:72800 Analytical Method: SM 2540D-2011 Parameter Result TSS ND Q Dil PQL Units Analysis Date 1 1.0 11 04/17/2015 1508 POL = Praacal quantilalion limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria NO = Not detected at or above the PQL J = Estimalad result < PQL and > i + = RPD is but of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a W Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, tnc. Page: 32 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.ccm Level 1 Report v2.5 Inorganic non-metals - LCS Sample 11): 0072800-002 Matrix: Aqueous Batch: 72800 Analytical Method: SM 254OD-2011 Spike Amount Result % Rec Parameter (mglL) (mg/L) Q Dil % Rec Limit Analysis Date TSS 250 250 1 99 90-110 04/17/20151508 POL = PracUcal quantitation limit P - The RPD between two GC columns exceeds 40% N - Recovery is out of criteria ND = Not detected at or above the POL J - Estimated result < POL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 33 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.$healylab.com Level 1 Reportv2.1 Sample ID: QQ72894-001 Batch.72894 Analvtical Method: 1664B Parameter SGT - HENS (non -polar material) Inorganic non-metals - MB Matrix: Aqueous Result Q Dil PQL Units Analysis Date ND 1 4.0 mg/f_ 04/20/2015 0933 PQL = Practical quantitahon limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria No = Not detected at or above the PQL J = Estimated result < PQL and > MIL + m RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless Flagged with a "'W' Note: Calculations are porformed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 34 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals - LCS Sample ID: QQ72894-002 Matrix: Aqueous Batch:72894 Analytical Method: 1664B Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date SGT - HEM (non -polar material) 20 17 4 85 64-132 04/20/2015 0933 PQL - Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL d = Estimated result < PQL and > IVIDL + = RPD is out of criteria Mere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with OW Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 35 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2.1 Volatile Organic Compounds by GC/MS - MB Sample ID: QQ73326-001 Matrix: Aqueous Batch:73326 Prep Method: 5030B Analytical Method: 624 Parameter Result Q Dil PQL Units Analysis Date Acrolein ND 1 50 uglL 04/24/2015 2147 Acrylonitrile ND 1 50 uglL 04/24/2015 2147 Benzene ND 1 5.0 ug1L 0412412015 2147 Bromodichlorometharte ND 1 5.0 ug1L 0412412015 2147 Bromoform ND 1 5.0 ug1L 04/24/2015 2147 Bromomethane (Methyl bromide) ND 1 5.0 ug1L 04/24/2015 2147 Carbon tetrachloride ND 1 5.0 ug1L 04/24/20152147 Chlorobenzene ND 1 5.0 u91L 04/24/2015 2147 Chloroethane ND 1 5.0 u91L 04/24/2015 2147 2-Chloroethylvinylether ND 1 10 ug1L 04/24/2015 2147 Chloroform ND 1 5.0 ug1L 04/24/2015 2147 Chloromethane (Methyl chloride) ND 1 5.0 ug1L 04/24/2015 2147 Dibromochloromethane ND 1 5.0 uglL 04/24/2015 2147 1,2-Dichloroethane ND 1 5.0 uglL 04/24/2015 2147 1,1-Dichloroethane ND 1 5.0 uglL 04/24/2015 2147 trans-1,2-Dichloroethene ND 1 5.0 uglL 04/24120152147 1,1-Dichloroethene ND 1 5.0 uglL 04124/20152147 1,2-Dichloropropane ND 1 5.0 ug/L 04/24/2015 2147 cis-1,3-Dichloropropene ND 1 5.0 uglL 04/24/2015 2147 trans-1,3-Dichloropropene ND 1 5.0 ug1L 04/24/2015 2147 Ethylbenzene ND 1 5.0 ug1L 04/24/2015 2147 Methylene chloride ND 1 5.0 ug/t_ 04/24/2015 2147 1,1,2,2-Tetrachloroethane ND 1 5.0 ug1L 04124120152147 Tetrachloroethene ND 1 5.0 ug1L 04/24/2015 2147 Toluene ND 1 5.0 uglL 04/24/2015 2147 1,1,1-Trichloroethane ND 1 5.0 ug1L 04124/20152147 1,1,2-Trichloroethane ND 1 5.0 ug1L 04/24/2015 2147 Trichloroethene ND 1 5.0 uglL 04124/20152147 Vinyl chloride ND 1 5.0 u91L 04/24/2015 2147 Surrogate Q % Rec Acceptance Limit Bromofluorobenzerle 104 70-130 1,2-Dichloroethane-d4 98 70-130 Toluene-d8 101 70-130 PQL = Pracfical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result � PQL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 36 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v21 Volatile Organic Compounds by GC/MS - LCS Sample ID: Q073326-002 Matrix: Aqueous Batch: 73326 Prep Method: 5030B Analytical Method: 624 Spike Amount Result % Rec Parameter (ug1L) (ug/L) Q Dil % Rec Limit Analysis Date Acrolein 200 200 1 102 14-175 04/24/2015 2052 Acrylonitrile 40 40 1 100 60-130 04/24/2015 2052 Benzene 20 19 1 93 37-151 04/24/2015 2052 Bromodichloromethane 20 19 1 94 35-155 04/24/2015 2052 Bromoform 20 19 1 96 45-169 04/24/2015 2052 Bromomethane (Methyl bromide) 20 20 1 99 1-242 04/24/2015 2052 Carbon tetrachloride 20 19 1 95 71-140 04/24/2015 2052 Chlorobenzene 20 18 1 91 37-160 04/24/2015 2052 Chloroethane 20 19 1 96 14-230 04/24/2015 2052 2-Chloroethylvinylether 20 19 1 93 1-305 04/24/2015 2052 Chloroform 20 19 1 93 51-138 04/24/2015 2052 Chloromethane (Methyl chloride) 20 20 1 98 1-273 04/24/2015 2052 Dibromochloromethane 20 19 1 97 53-149 04/24/2015 2052 1,2-Dichloroethane 20 20 1 99 49-155 04/24/2015 2052 1,1-Dichloroethane 20 19 1 94 59-155 04/2412015 2052 trans-1,2-Dichloroethene 20 19 1 95 54-156 04/2412015 2052 1,1-Dichloroethene 20 19 1 95 1-234 04/24/2015 2052 1,2-Dichloropropane 20 19 1 93 1-210 04/2412015 2052 cis-1,3-Dichloropropene 20 19 1 96 1-227 04124120152052 trans-1,3-Dichloropropene 20 19 1 96 17-183 04/24/2015 2052 Ethylbenzene 20 19 1 93 37-162 04/24/2015 2052 Methylene chloride 20 20 1 98 1-221 04/2412015 2052 1,1,2,2-Tetrachloroethane 20 19 1 97 46-157 04124120152052 Tetrachloroethene 20 18 1 90 70-130 04/24/2015 2052 Toluene 20 18 1 92 47-150 04/24/2015 2052 1,1,1-Trichloroethane 20 19 1 93 52-162 04124/20152052 1,1,2-Trichloroethane 20 19 1 96 52-150 04124/20152052 Trichloroethene 20 18 1 91 71-157 04/24/2015 2052 Vinyl chloride 20 20 1 98 1-251 04/24/2015 2052 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 107 70-130 1,2-Dichloroethane-d4 93 70-130 Toluene-d8 104 70-130 PC = Practical quarittatien limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result C PQL and n MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Note: Calculations are performed before rounding to avoid round -of errors in calculated results Shealy Environmental Services, Inc. Page: 37 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (B03) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS - MB Sample ID: QQ72771-001 Matrix: Aqueous Batch:72771 Prep Method: 625 Analytical Method: 625 Prep Date: 04/17/2015 1255 Parameter Result Q Dil PQL Units Analysis Date 1,2,4-Trichlorobenzene ND 1 2.0 ug/L 04/20/2015 2241 1,2-Dichlorobenzene ND 1 2.0 ug1L 04/20/2015 2241 1,2-Diphenylhydrazine(as azebenzene) ND 1 2.0 ug1L 04/20/2015 2241 1,3-Dichlorobenzene ND 1 2.0 ug1L 04/20/2015 2241 1,4-Dichlorobenzene NO 1 2.0 ug/L 04/20/2015 2241 2,4,6-Trichlorophenol ND 1 2.0 ug1L 04/20/2015 2241 2,4-Dichlorophenol ND 1 2.0 ug/L 04/20/2015 2241 2,4-Dimethylphenol ND 1 2.0 ug/L 04/20/2015 2241 2,4-Dinitrophenol ND 1 10 uglL 04/20/2015 2241 2,4-Dinitrotoluene ND 1 4.0 ug/L 04/20/2015 2241 2,6-Dinitrotoluene ND 1 4.0 ug/L 04/20/2015 2241 2-Chloronaphthalene ND 1 2.0 ug/L 04/20/20152241 2-Chlorophenal ND 1 2.0 ug/L 04/20/2015 2241 2-Nitrophenol ND 1 4.0 ug/L 04/20/2015 2241 3,3'-Dichlorobenzidine ND 1 10 ug/L 04/20/2015 2241 4,6-Dinitro-2-methylphenol ND 1 10 ug/L 04/20/2015 2241 4-Bromophenyl phenyl ether ND 1 2.0 ug/L 04/2012015 2241 4-Chloro-3-methylphenol ND 1 2.0 ug/L 04/20120152241 4-Chlorophenyl phenyl ether ND 1 2.0 ug1L 04/20/2015 2241 4-Nitrophenol ND 1 10 ug1L 04/20/2015 2241 Acenaphthene ND 1 2.0 ug1L 04/20/2015 2241 Acenaphthylene ND 1 2.0 ug1L 04/20/2015 2241 Anthracene ND 1 2.0 ug1L 04/20/2015 2241 Benzidine ND 1 10 ug/L 04/20/2015 2241 Benzo(a)anthracene ND 1 2.0 ug/L 04/20/2015 2241 Benzo(a)pyrene ND 1 2.0 ug1L 04/20/2015 2241 Benzo(b)fluoranthene ND 1 2.0 ug1L 04/20/2015 2241 Benzo(g,h,i)perylene ND 1 2.0 ug1L 04/20/2015 2241 Benzo(k)fluoranthene ND 1 2.0 ug1L 04/20/2015 2241 bis(2-Chloroethoxy)methane ND 1 2.0 ug1L 04/20/2015 2241 bis(2-Chloroethyl)ether ND 1 2.0 ug1L 04/20/2015 2241 bts(2-Chloroisopropyl)ether ND 1 2.0 ug/L 04/20/2015 2241 bis(2-Ethylhexyl)phthalate ND 1 10 ug/L 04/20/2015 2241 Butyl benzyl phthalate ND 1 10 ug1L 04/20/2015 2241 Chrysene ND 1 2.0 ug/L 04/20/2015 2241 Di-n-butyl phthalate ND 1 10 ug/L 04/20/2015 2241 Di-n-octylphthalate ND 1 10 ug1L 04/20/2015 2241 Dibenzo(a,h)anthracene ND 1 2.0 ug1L 04/20/2015 2241 Diethylphtha late ND 1 10 ug/L 04/20/2015 2241 Dimethyl phthalate ND 1 10 u91L 04/20/2015 2241 Fluoranthene ND 1 2.0 ug/L 04/20/2015 2241 Fluorene ND 1 2.0 ug/L 04/20/2015 2241 Flexachlorobenzene ND 1 2.0 ug/L 04/20/2015 2241 Hexachlorobutadiene ND 1 2.0 u91L 04/20/2015 2241 PQL = Practical cluanttation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 38 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS - MB Sample ID: 0072771-001 Matrix: Aqueous Batch: 72771 Prep Method: 625 Analytical Method: 625 Prep Date: 04/17/2015 1255 Parameter Result Q Dil PQL Units Analysis Date Hexachlorocyclopentadiene ND 1 10 ug1L 04/20/2015 2241 Hexachloroethane ND 1 2.0 uglL 04/20120152241 Indeno(1,2,3-c,d)pyrene ND 1 2.0 uglL 04/20120152241 Isophorone ND 1 2.0 uglL 04120/20152241 N-Nitrosold i-n-propylamine ND 1 2.0 ug1L 04/20/20152241 N-Nitrosodimethylamine ND 1 2.0 ug1L 04/20/20152241 N-Nitrosodiphenylamine (Diphenylamine) ND 1 2.0 ug1L 04120/2015 2241 Naphthalene ND 1 2.0 ug/L 04/20/2015 2241 Nitrobenzene ND 1 2.0 ug1L 04/20/2015 2241 Pentachlorophenol ND 1 10 ug1L 04/20/2015 2241 Phenanthrene ND 1 2.0 ug1L 04/20/2015 2241 Phenol ND 1 2.0 ugll_ 04/20/2015 2241 Pyrene ND 1 2.0 ug1L 04/20/2015 2241 Acceptance Surrogate Q 0 7o Rec Limit 2,4,6-Tribromophenol 69 41-144 2-Fluorobiphenyl 84 37-129 2-Fluorophenol 81 24-127 Nitrobenzene-d5 92 38-127 Phenol-d5 88 28-128 Terp heny 1-d 14 90 10-148 PQL - Practical quantilalion limit P = The RPD between two GC columns exceeds 40°% N = Recovery is out of criteria NO = Not detected at or above the PQL J = Estimated result < PQL and > MOIL + = RPO is out o: diteria Where applicable, all sail sample analysis are reported on a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 39 of 46 106 Vantage Point Drive West Columbia, SC 29172 (B03) 791-9700 Fax (803) 791-9111 www.rhealylab.com Level 1 Reportv2.1 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: QQ72771-002 Matrix: Aqueous Batch: 72771 Prep Method: 625 Analytical Method: 625 Prep Date: 04/17/2015 1255 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 1,2,4-Trichlorobenzene 20 16 1 80 44-142 04/20/2015 2305 1,2-Dichlorobenzene 20 17 1 84 32-129 04/20/2015 2305 1,2-Dipheny1hydrazine(asazobenzene) 20 21 1 107 30-130 04120120152305 1,3-Dichlorobenzene 20 18 1 90 0-172 04120/20152305 1,4-Dichloroben7ene 20 17 1 84 20-124 04120/20152305 2,4,6-Trichlorophenol 20 18 1 88 37-144 04/20/2015 2305 2,4-Dichlorophenol 20 18 1 89 39-135 04/20/2015 2305 2,4-Dimethylphenol 20 18 1 92 32-119 04/20/2015 2305 2,4-Dinitrophenol 100 81 1 81 0-191 04/20/2015 2305 2,4-Dinitrotoluene 40 41 1 103 39-139 04/20/2015 2305 2,6-Dinitrotoluene 40 39 1 98 50-158 04/20/2015 2305 2-Chloronaphthalene 20 15 1 75 60-118 04/20/2015 2305 2-Chlorophenol 20 20 1 102 23-134 04/20/2015 2305 2-Nitrophenol 40 37 1 94 29-182 04/20/2015 2305 3,3'-Dichlorobenzidine 40 33 1 83 0-262 04/20/2015 2305 4,6-Dinitro-2-methylphenol 100 94 1 94 0-181 04/20/2015 2305 4-Bromophenyl phenyl ether 20 17 1 85 53-127 04/20/2015 2305 4-Chloro-3-methyl phenol 20 21 1 105 22-147 04/20/2015 2305 4-Chlorophenyl phenyl ether 20 18 1 89 25-158 04/20/2015 2305 4-Nitrophenol 100 110 1 112 0-132 04/20/2015 2305 Acenaphthene 20 20 1 100 60-132 04/20/2015 2305 Acenaphthylene 20 20 1 99 54-126 04/20/2015 2305 Anthracene 20 19 1 95 43-118 04/20/2015 2305 Benzidine 40 8.4 1 21 1-150 04/20/2015 2305 Benzo(a)anthracene 20 19 1 93 42-133 04/20/2015 2305 Benzo(a)pyrene 20 17 1 87 17-163 04/20/2015 2305 Benzo(b)fluoranthene 20 20 1 100 24-159 04/2012015 2305 Benzo(g,h,i)perylene 20 15 1 75 0-219 04/20/2015 2305 Benzo(b)fuoranthene 20 21 1 103 11-162 04/20/2015 2305 b is (2-C hloroeth oxy) methane 20 20 1 99 33-184 04/20/2015 2305 bis(2-Chloroethyl)ether 20 23 1 116 12-158 04/20/2015 2305 bis(2-Chlor6sopropyl)e1her 20 22 1 108 36-166 04/20/2015 2305 bis(2-Ethylhexyl)phthalate 20 24 1 122 8-158 04/20/2015 2305 Butyl benzyl phthalate 20 24 1 121 0-152 04/20/2015 2305 Chrysene 20 19 1 94 17-168 04/20/2015 2305 Di-n-butyl phthalate 20 22 1 110 1-118 04/20/2015 2305 Di-n-octylphthalate 20 22 1 111 4-146 04/20/2015 2305 Dibenzo(a,h)anthracene 20 18 1 88 0-227 04/20120152305 Diethylphthalate 20 21 1 105 0-114 04/20/2015 2305 Dimethyl phthalate 20 19 1 97 0-112 04/20/2015 2305 Fluoranthene 20 19 1 95 26-137 04/20/2015 2305 Fluorene 20 19 1 95 59-121 04/2012015 2305 H exachlo robe nzene 20 17 1 87 0-152 04/20/2015 2305 Hexachlorobutadiene 20 17 1 86 24-116 04/20/2015 2305 PQL = Prar6cal quantitation limit P - The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result - PQL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 40 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2,1 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: Q072771-002 Matrix: Aqueous Batch:72771 Prep Method: 625 Analytical Method: 625 Prep Date: 04/17/2015 1255 Spike Amount Result % Rec Parameter (ug1L) (ug1L) Q Dil % Rec Limit Analysis Date Hexachlorocyclopentadiene 100 26 1 26 1-150 04/20r2015 2305 Hexachloroethane 20 18 1 91 40-113 04/20/2015 2305 Indeno(1,2,3-c,d)pyrene 20 17 1 84 0-171 04/20/2015 2305 lsophorone 20 22 1 112 21-196 04/20/2015 2305 N-Nitrosodi-n-propylamine 20 23 1 115 0-230 04/20/2015 2305 N-Nitrosodimethylamine 20 25 1 123 1-150 04/201'2015 2305 N-Nitrosodiphenylamine (Diphenylamine) 20 21 1 106 1-150 04/2012015 2305 Naphthalene 20 18 1 89 21-133 04120f2015 2305 Nitrobenzene 20 20 1 101) 35-180 04/20/2015 2305 Pentachlorophenol 100 74 1 74 14-176 04/2012015 2305 Phenanthrene 20 19 1 95 54-120 04/20/2015 2305 Phenol 20 20 1 98 5-112 04/20/2015 2305 Pyrene 20 18 1 89 52-115 04/20/2015 2305 Acceptance Surrogate Q % Rec Limit 2,4,6-Tribromophenol 85 41-144 2-Fluorobiphenyl 85 37-129 2-Fluorophenol 91 24-127 Nitrobenzene-d5 96 38-127 Phenol-d5 96 28-128 Terphenyl-d14 92 10-148 PQL = Practical quanWation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result n PQL and > MDL + = RPD is out of ontena Where applicable, all soil sample analysis are reported an a dry weight basis unless flagged with a'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 41 of 46 106 Vantage Point Orive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v21 Organochlorine Pesticides and PCBs - MB Sample ID: QQ72807-001 Matrix: Aqueous Batch:72807 Prep Method: 608 Analytical Method: 608 Prep Date: 04/17/2015 1654 Parameter Result Q oil PQL Units Analysis Date 4,4'-DDD ND 1 0,040 ug/L 04/21 i2015 1738 4,4'-DDE ND 1 0.040 ug/L 04/21l20151738 4,4'-DDT ND 1 0.040 uglL 04/21/20151738 Aldrin ND 1 0.040 uglL 04/21/20151738 alpha-BHC ND 1 0.040 ug/L 04/21/20151738 Aroclor 1016 ND 1 0.40 ug1L 04/2112015 0000 Aroclor 1221 ND 1 0.40 ug/L 04/21/2015 0000 Aroclor 1232 ND 1 0,40 uglL 04/21)2015 0000 Aroclor 1242 ND 1 0.40 uglL 04l2112015 0000 Aroclor 124B ND 1 0.40 u91L 04/21/2015 0000 Aroclor 1254 ND 1 0.40 ug/L 04/21/2015 0000 Aroclor1260 ND 1 0.40 ug/L 04/21/2015 0000 beta-BHC ND 1 0.040 ug/L 04/21/2015 1738 Chlordane ND 1 0.40 uylL 04121/20151738 delta-BHC ND 1 0.040 u91L 04121120151738 Dieldrin ND 1 0.040 uglL 04/21/2015 1738 Endosulfan I ND 1 0.040 uglL 04/21/2015 173E Endosulfan II ND 1 0.040 uglL 04121/2015 1738 Endosulfan sulfate ND 1 0.040 ug/L 04/21/2015 1738 Endrin ND 1 0.040 ug/L 04/21/20151738 Endrin aldehyde ND 1 0.040 ug/L 04/21/2015 1738 gamma-BHC (Lindane) ND 1 0.040 ug1L 0412112015 1738 Heptachlor ND 1 0.040 uglL 04121/20151738 Heptachlor epoxide ND 1 0.040 ug1L 04/21/2015 1738 Toxaphene ND 1 0.40 uglL 04/21/20151738 Surrogate Q % Rec Acceptance Limit Decachlorobiphenyl 71 20-131 Tetra chloro-m-xylene 70 26-132 PQL = Praclical cluan8tation limit P = The RPn between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > MnL + = RPM is out of criteria Where applirablo, all soR sample analysis are reported on a dry weight basis unless flagged with a W Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 42 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Organochlorine Pesticides and PCBs - LCS Sample ID: QQ72807-002 Matrix: Aqueous Batch: 72807 Prep Method: 608 Analytical Method: 608 Prep Date: 04/17/2015 1654 Spike Amount Result % Rec Parameter (uglL) (uglL) Q Dil % Rec Limit Analysis Date 4,4'-DDD 0.80 0.69 1 86 31-141 04/21120151752 4,4'-DDE 0.80 0.64 1 80 30-145 04/21120151752 4,4'-DDT 0.80 0.67 1 84 25-160 04/21120151762 Aldrin 0.80 0.61 1 76 42-122 04/21120151752 alpha-BHC 0.80 0.62 1 77 37-134 04121120151752 beta-BHC 0.80 0.59 1 73 17-147 04/21/2015 1752 delta-BHC 0.80 0.64 1 80 19-140 04121/20151752 Dieldrin 0.80 0.71 1 89 36-146 04121120151752 Endosulfan 1 0.80 0.66 1 82 45-153 04/21/2015 1752 Endosulfan 11 0.80 0.76 1 95 1-202 04/21/2015 1752 Endosulfan sulfate 0.80 0.76 1 95 26-144 04/21/2015 1752 Endrin 0.80 0.64 1 80 30-147 04/21/2015 1752 Endrin aldehyde 0.80 0.59 1 74 50-130 04/21/2015 1752 gamma-BHC (Lindane) 0.80 0.61 1 77 32-127 04/21/2015 1752 Heptachlor 0.80 0.59 1 74 34-111 04/21120151752 Heptachlor epoxide 0.80 0.60 1 75 37-142 04/21/2015 1752 Surrogate Q %Rec Acceptance Limit Decachlorobiphenyl 68 20-131 Tetrachloro-m-xylene 68 26-132 PQL = Practical quanlitallon limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > MM + = RPD is out of criteria More applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 43 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.cortn Level 1 Report v2.1 Organochlorine Pesticides and PCBs - MS Sample ID: QD16054-004MS Matrix: Aqueous Batch: 72807 Prep Method: 608 Analytical Method: 608 Prep Date: 04/17/2015 1654 Sample Spike Amount Amount Result % Rec Parameter (uglL) (ug1L) (iii Q Dil % Rec Limit Analysis Date Aldrin ND 0.80 0.68 1 85 44-122 04/23/2015 1210 gamma-BHC (Lindane) ND 0.80 0.71 1 89 32-127 04/23/2015 1210 alpha-BHC ND 0,80 0.69 1 86 37-134 04/23/2015 1210 beta-BHC NO 0.80 0.67 1 84 17-147 04123/20151210 delta-BHC ND 0.80 0.73 1 91 19-140 04123120151210 4,4'-DDD ND 0,80 0.73 1 91 31-141 04/23/2015 1210 4,4'-DDF ND 0,80 0.67 1 83 30-145 04/23/2015 1210 4,4'-DDT ND 0.80 0.70 1 87 25-160 04123/20151210 Dieldrin ND 0.80 0.75 1 94 36-146 04/23/2015 1210 Endosulfan I ND 0.80 0.72 1 89 45-153 04/23/2015 1210 Endosulfan II ND 0.80 0.75 1 94 1-202 04/23/2015 1210 Endosulfan sulfate ND 0.80 0.77 1 96 26-144 04/23/2015 1210 Endrin ND 0.80 0.75 1 94 30-147 04123/20151210 Endrin aldehyde ND 0.80 0.65 1 82 50-130 04/23/2015 1210 Heptachlor ND 0.80 0.69 1 86 34-111 04/23/2015 1210 Heptachlor epoxide ND 0.80 0.69 1 86 37-142 04/23/2015 1210 Surrogate Q % Rec Acceptance Limit Decachlorobiphenyl 61 20-131 Tetra chl oro -m-xylene 74 26-132 POL = Practical quanlitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the POL J = Estimated result < POL and > i + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 44 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 ICP-MS - MB Sample ID: QQ72769-001 Batch: 72769 Analytical Method: 200.8 Matrix: Aqueous Prep Method: 200.2 Prep Date: 04/17/2015 1223 Parameter Result Q Dil PQL Units Analysis Date Copper ND 1 1.0 uglL 04117/20151928 Lead ND 1 1.0 uglL 04/20120151914 Zinc ND 1 10 uglL 04/17/20151928 PQL = Practical quantitation limit P = The RPD between two GC cviumns exceeds 4D% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result a PQL and > MOL + = RPD is out of crlteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 45 of 46 106 Vantage Polat Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 ICP-MS - LCS Sample ID: QQ72769-002 Batch: 727g9 Analytical Method: 200.8 Matrix: Aqueous Prep Method: 200.2 Prep Date: 04/17/2015 1223 Spike Amount Result % Roc Parameter (ug1L) (ug1L) Q Dil % Roe Limit Analysis Date Capper 100 110 1 111 85-115 04/17120151933 Lead 100 99 1 99 85-115 04/20/20151919 Zinc 100 110 1 114 85-115 04/17/20151933 POL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out cf criteria ND = Not detected at or above the POL J = Estimated result < POL and > MDL = RPD is out of criteria Wnere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 46 of 46 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2.1 SHEALY ENVIRONMENTAL SERVICES, INC. 108 Vanlage Point Orive - West Columbia, SC 29172 SH Chain Af �uStady AeCOrd Fglephoria No. 803.791-9700 Fax No, W3-791.9111 mvw.shealylab.com Number 47613 G4eM r PVWt JVMWt . eWSW-PAJ& rEC�xrotq, Aaxv: ro caieacr raiernlx Nn. � F.:�,X -7+1- 313i� Cl weft6ecfi� - Ouola SYb � �� A��s9 p Q�Q�VCr $ll11��j1p SempfeYs RfGrY /. �.__ �'^ PrnrP7Nar.� �' - R'raryald (AgUdi h-0rr m m samce )s nftd*: j — f PaN Af •�����ii1���fA QD16a6A Ften►arkslear�r,f.D. S•ra�ren /If� TnCaaa ��Q� � ti.J 7�t ��r�•.�_„ ✓ � N . Ll Q ( •r� -yam, IOR ari GrFi� f Propel Na f /; 4��./f �V � 1 �' v. Nb. 9g �1AfY„Y ' hN N idYa'i.�7ro by ►}�2NIvv ryFv sariwfeleirpawb rt f cnamahsactie�ryenW�nera�:,aemeh,e; Dare I ! rrie 00 5 r ✓' J ✓ t/ � 1 > -0 3 , 1f�p f .J ✓ ✓ ,� ✓H,- 'r I I 5 14 � I ✓ � ,� ✓ � ,: � ,� ,� ✓ 1 I i Ard„rd TMiie Required (Prlorle� afWrcoaf npaizdhvQ�&tad �T. Sam;.�a D;U;:ass1 Strtr sod I ' Ru fSDeelfYl d RM,-a fA CAM f 66sfi-1 AY lX- Aps,7.�Ap ff3i2rtY Jtlenti6^+h'art // ❑ Num-H=M' _ 7 Fbw zblt I I. seu' i bilt � fti cn I211id 0MV1 GEC ItaquA'+emCnM ($C�'71 f: 1 M" L L f �� c I Y. �Y (I QF� I 1 ,. y ` r -- Ls 2. Rh1'nSu MQ*v—, Dde Tim 2 R*C tl by DaR the ]. Z.7Nu,e, ey i7ars '3R+0 a Rmrii e?ar Leta Time 1. Act{7QulaAsd L]r A �h iuna� � � 4. 1�n�9.Y_8r [� L7.7f9 l� Nara: At! SampfvS 8M rei;W for Wor weeks frOtn r6C$ipt unkui oHrer arr,strgomenls ars made, rAB U,�%eOMY ReaMmd cn:rsr 1 a rya ore Rux ry Z= e O S.TR1BUTNW, MUTE d Yr1LCWRVAwn to $W ,y tn7h &,rml1 fail MNK F W&V09-d CWy E1aa�na�rtht.�r�or; F-AD-f3L7 Lffetli+wDa;ff'�Ot•a0rs. Z /� 0 `\ h SHEALY ENVIRONMENTAL SERVICES INC. S1=ly t nvir;m"=0 septets, fire. tin:urnealNuntheT: F-AW1b RetisiM NamiNc 16 , ,i P¢gc ! of ! 1 Replaces Ddm 071 SA Effective Wtc: 1!N!?ill Sample Receipt Checklist 1;SRQ Client: t1�t'.�cnc•rc .� �.� Cooler Inspected by!date:Vvv_ cv.f Lot 4: &asLgL'N� Mcans of rcccipt: 0SFSSI C-licnt ❑ UPS ❑ FedEx ❑ Airbame Exp ❑ Other Yes ❑ No 91 1_ Were custc1dy seals resent on the cooler? Yv.9 ❑ NU N&0_1 2- 117vusl(Ay scaly wuru prc 4ant. warc they intact and unbroken? Cooler ID/Original temperature upon receiptMerived (corrected) tempernttm upon receipt: i1..b rL %, } oC , _°C i oC I 1f cc Method: a npernture Blank ❑ Against Bottles IR Gun Mi A4 iR C.,un CwTtOiun Factor: °C Method of coolant: et Ice ❑ Blue ke ❑ Dl ice None Yes ❑ No ❑ NAg 3_ If temperature of any cooler excocded 6.0°C, was Project Manager notified? PM notified by SRC, phone, note (circle one), other: (For coolers received via commercial courier, Pivis are to be notified inimediatel •.) Yes ❑ No ❑ NA 4, Is The cxmmercial courier's ackin sli attanccd to this farm;' Yes No ❑ 5, Were. r4 er custody roeedurrs relin uishtedlrcQcivC ! followed? Yes ❑ No NA Sa Wen sam lcs rclin uishcd b client to commercial aciuricr? Yes No ❑ 6, Were sample IDs listed an the COC" Yes No ❑ 7. lucre sam le IDs listed on all sam 1c containers? Yes No ❑ 8. W Ds collection date & time listed on the COC? Yes -No ❑ 9. Wes collection date & time listed on tell sample conrainers? Yey Na ❑ 10. Did till container label informa[ion (ir1', date, lime a - with the CQC? YM Nu ❑ 11. Were tests to be rforuled listed on the {. M? Yels No ❑ 12. Did a]I sam les arrive in the m containers for each test? Yes No 13. Did all containers arrive in good condition (unbroken, lids oil, etc.)? Yes No U 14, Was vdN atv sHrnplc volurnG Hvailuble^ Yes No ❑ 15. were all samples received within %s the holding time or 48 hours, whichever comes first? Yes ❑ No ❑/ " 16. Were an , sam Ics containers missin ? YCb No 17. Were there an excess samples not listed on COC? Yes ❑ No 2r NA ❑ 1S. wtare hubblrr resvii1 !6"nr 6mrn in diameter in any ♦ OA vials? Ycs 10 No ❑ NA ❑ 19. Were all nietaWU&G%EIEWnutrient solo les received at a pH of <2? Yes ❑ I No ❑ NA 2r 20. Were all cyanide andlor sulfide sam Ics received at a H >12? Yes ❑ No ❑ NA Z 21. Were all alipl icable NH1TKNlcyanidr?phcnol (--0.2mSIL) samples free of residual chlorinc? Yes ❑ No ❑ _ 22_ Were collection temperatures documented on the COC. for NC samples? Yes ❑ Na ❑ NA 23. Wcrc client remurldsirequests (i.e. requested dilutions, M&INISD designations: etc,.. correctly tramcribed froin the COC into the comment section in LAMS! '; Yes ❑ No 24. Was the quote number used taken from the container label? Sample Preservation (Must be completed for any sample(s) incorrectly- preserved or with headslmce) Samples) were received incorrectly preserved and were adjusted accordin8ly i i sample recriv' with 112S043IN03,l_'CI,Na0H) mi ng SR 4 Samples were received with bubbles 36 non in diameter_ Sant le(s) were receivcd with TRC?0.2 m r!L. (If921 is No) SC Dnnkirkg Water Project Sam le(s) pH verified to be a 2 by . _ DHtc: Sam le(s) were not received at a pH of -:2and wcrc adjusttA Nc:cunlingly usirr'; S124 Saw le labels applied bv: Verified by: Datc: Comments: Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (B03) 791-9111 www.shealylab.com Lave! 1 Report v2,1 f L• N C (;o 3 o3a9 Evans, Mechwart, Hambleton & Tilton, Inc. Engineers, Surveyors, Planners, Scientists December 4, 2014 Mr. Brendan Conway Honda Power Equipment Manufacturing, Inc. Post Office Box 37 Swepsonville, North Carolina 27359 Subject: Stormwater Sampling Event — December 2014 Honda Power Equipment Swepsonville, Alamance County, North Carolina EMH&T Project No. 2014-021 1 Dear Mr. Conway: RECEIVED DEC 11 2014 CENTRAL FIEFS DWR SECTION On November 17, 2014, Evans, Mechwart, Hambleton & Tilton, Inc. (EMH&T) completed a stormwater sampling event at the Honda Power Equipment Manufacturing facility located in Swepsonville, North Carolina. A rain event began at approximately 5.00 am and ended at approximately 2.15 pm on November 17, 2014. Stormwater samples were collected from three discharge locations (HPE-01, HPE-02, R&D-01) at the property. After collection, the samples were delivered to the Shealy Environmental Services, Inc. (Shealy) laboratory in West Columbia, South Carolina for analysis. A copy of the Stormwater Monitoring Records for this sampling event are provided in Attachment A. The analytical results are presented in summary form in Attachment B. A copy of the laboratory report is included as Attachment C. Stormwater sampling was conducted by Perry Wiese of EMH&T. EMH&T appreciates the opportunity to provide our services on this project. Please do not hesitate to call if you have questions or need additional information. Respectfully submitted, EVANS, MECHWART, HAMBLETON & TILTON, INC. AkdC4(4�* Carl H. Hewett Senior Environmental Scientist A legacy of experience. A reputation to excellence. 301 McCullough Drive, Suite 109, Charlotte, NC 28262 - Phone 704.548.0333 - Fax 704.548.0334 Columbus • Allan}o , Charlotte • Cinckn all • IncranapoEs emhl.com STORMWATER MONITORING RECORD SAMPLING SUMMARY Site: Honda Power Equipment Honda Drive, NC Highway 119 Swepson-,rille, North Carolina 27359 Monitoring Date: November 17, 2014 Previous Measurable Rainfall Event (>o.1 inches): November 6, 2014 Storm E vent Approximate Start: 5:oo am, November 17, 2014 Approximate End: 2:15 pm, November 17, 2014 Storm Duration: approximately 9 1/4 hours Rainfall: 0.8 inches Sampling: sampled discharge point HPE-o1 at 1:15 pm (1315) sampled discharge point HPE-02 at 1:45 pm (1345) sampled discharge point R&D-o1 at 2:45 pm (1445) Analytical Testing: pH by EPA Method SM 450o-HB TSS by SM 254oD Oil and grease by EPA Method 1664A Volatile organics by EPA Method 624 Semi -volatile compounds by EPA Method 625 PCBs/pesticides by EPA Method 6o8 Copper, Lead, Zinc by EPA Method 200.E Sampled by: Perry Wiese EMH&T 301 McCullough Drive, Suite log Charlotte, North Carolina 28262 Notes: • Storm duration and rainfall amount obtained from Weather Underground's daily summary for Burlington, North Carolina. Page 1 of 1 A legacy of experience. A reputation for excellence. ATTACHMENT A Stormwater Monitoring Records Honda Power Equipment — Stormwater Sampling (November 201 4) emht.com I r 1 STORM WATER ATER MONITORING ORING RECORD QUALITATIVE OBSERVATIONS Site: Honda Power Equipment Honda Drive, NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: November 17, 2014 Sample Location: HPE-oi Discharge Characteristic Rating Comments Color N �� Odor�� Clarity Cf-tA Z Floating Solids Suspended Solids A)0�� Foam tj0+� {` Oil Sheen rj of c Other obvious indicators of stormwater pollution _ -- Characteristic rating scale: none, slight, minor, medium, heavy Monitoringsheet completed b : 11""z ' " �• Date: I 1 1 14 - p Y r STORM • i ATER MONITORING RECORD QUALITATIVE OBSERVATIONS Site: Honda Power Equipment Honda Drive, NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: November 17, 2014 Sample Location: HPE-02 Discharge C�haracteristic Rating Comments �r RYA v,l fi tFizr^`.: ,i 3�iii"�. �f T. �..`�'� � ..R �'��I' xyu�.«t.�i8 ":�..°'Y s `�•f r' W ��.:.� Color MAL Odor��� Clarity C4-lA R Floating Solids Al 0 .4 f- Suspended Solids��� Foamv� Oil Sheen�,�� Other obvious indicators of stormwater pollution Characteristic rating scale: none, slight, minor, medium, heavy Monitoring sheet completed by: Date: IfOf STORM WATER MONITORING RECORD QUALITATIVE OBSERVATIONS Site: Honda Power Equipment Honda Drive, NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: Sample Location: November 17, 2014 R&D-ol Discharge Characteristic Rating Comments • Color 1.f'.4AY'*Y AAIJ fA.Pr. do ODOR, OiL -roxalviry 04 Odor Ao 4 F- Clarity f-, + 7- Floating Solids gyp,,f, Suspended Solids Foam AWL Oil Sheen Other obvious indicators ofstormtvater pollution Characteristic rating scale: none, slight, minor, medium, heavy Monitoring sheet completed by: J1. Date: 11/1 -7/14' I f A lecgocy of experience. A reputation for excellence. ATTACHMENT B Analytical Results Summary Honda Power Equipment — Stormwater Sampling (November 2014) emht.com TABLE Storm Water Analytical Results — November 2014 Honda Power Equipment Swepsonville, Alamance County, North Carolina HPE-oi HPE-02 R&D-o1 PH 6.79 6.61 6.69 Total Suspended Solids 11 14 37 EPA Method 2oo.8 copper BDL 0.0055 BDL lead BDL BDL BDL zinc 0.024 BDL BDL EPA Method 6o8 target pesticides BDL BDL BDL EPA Method 6o8 target PCBs -T BDL BDL BDL EPA Method 624 target volatile compounds BDL BDL BDL EPA Method 625 target semi -volatile compounds BDL BDL BDL EPA Method 1664 oil and grease 23 5.7 BDL Notes: • Total Suspended Solids are presented in milligrams per liter (mg/L). • BDL = below laboratory minimum quantitation limits Storm water samples collected on November 17, 2014 by EMH&T personnel. A legacy of experience. A reputolicn for excellence. ATTACHMENT C Laboratory Report Honda Power Equipment — Stormwater Sampling (November 201 4) emht.com SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis EMH&T 301 McCullough Drive Suite 109 Charlotte, NC 28262 Attention: Carl Hewett Project Name: Honda Power Equipment Project Number:2014-0211 Lot Number: PK1 8047 Date Completed:12/01/2014 Date Revised:12/03/2014 Kelly M. Maberry Project Manager tiE �4 c, e •4. 4 This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, Inc Page: 1 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealyiab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative EMH&T Lot Number: PK18047 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (CAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the CAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page GC/MS Semivolatiles The LCS associated with batch 61224 had benzidine recovered below the acceptance limits. This demonstrates a low bias on analytical results. All samples were re -extracted and re -analyzed outside of the 7-day holding time and results were confirmed. Revision 1213114 Copper and zinc were added to the metals list, at the client's request. Shealy Environmental Services, Inc. Page: 2 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary EMH&T Lot Number: PK18047 Sample Number Sample ID Matrix Date Sampled Date Received 001 R&D-01 Aqueous 11/17/2014 1445 11/18/2014 002 HPE-02 Aqueous 11/17/20141345 11/18/2014 003 HPE-01 Aqueous 11117120141315 11/18/2014 (3 samples) Shealy Environmental Services, Inc. Page: 3 of 43 106 Vantage Point Drive West Cdumbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com bevel 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary EMH&T Lot Number: PK18047 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 R&D-01 Aqueous TSS SM 2540D- 37 mg/l_ 5 002 HPE-02 Aqueous TSS SM 2540D- 14 mg1L 11 002 HPE-02 Aqueous HEM (oil and grease) 1664B 5.7 mglL 11 002 HPF-02 Aqueous Copper 200.7 0.0055 mglL 16 003 HPE-01 Aqueous TSS SM 2540D- 11 mg1L 17 003 HPF-01 Aqueous HEM (oil and grease) 1664E 23 m91L 17 003 HPE-01 Aqueous Zinc 200.7 0.024 mglL 22 (7 detections) 1 Shealy Environmental Services, Inc, Page: 4 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2.1 Inorganic non-metals .Client:EMH&T Laboratory ID: PK18047-001 Description: R&D-01 Matrix: Aqueous Date Sampled:1Ili 712014 1445 Date Received: 11/1812014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH) SM 4500-H B-2011 1 11/19/2014 0902 AMM1 61207 1 (TSS) SM 254OD-2011 1 11/20/2014 1500 AAD 61357 1 (HEM (oil and) 1664B 1 11/25/2014 0945 EWR 61645 CAS Analytical Parameter Number Method Result Q PQL Units Run pH SM 4500-H B 6.69 su 1 TSS SM 254OD-20 37 5.0 mg1L 1 HEM (oil and grease) 1664E ND 4.3 mglL 1 PQL = Practical quantltation limit B = Delected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result - PQL and > MOL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless nagged with a "W" Shealy Environmental Services, Inc. Page: 5 of 43 106 Vantage Point Drive West Columbia, SC 29172 (603) 791-9700 Fax (603) 791-9111 www.shealylab.com Level 1 Report v2.1 Volatile Organic Compounds by GCIMS ,Client:EMhl&T Laboratory ID: PK18047-001 Description: R&D-01 Matrix: Aqueous Date Sampled:1111712014 1445 Date Received: 1Ill 812014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 11/25/2014 2253 PMM2 61751 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 uglL 1 Acrylonitrile 107-13-1 624 ND 50 uglL 1 Benzene 71-43-2 624 ND 5.0 uglL 1 Bromodichtoromethane 75-27-4 624 NO 5.0 uglL 1 Bromoform 75-25-2 624 ND 5.0 uglL 1 Bromomethane (Methyl bromide) 74-83-9 624 ND 5.0 uglL 1 Carbon tetrachloride 56-23-5 624 NO 5.0 uglL 1 Chlorobenzene 108-90-7 624 ND 5.0 uglL 1 Chloroethane 75-00-3 624 NO 5.0 uglL 1 2-Chloroethylvinylether 110-75-8 624 NO 10 uglL 1 Chloroform 67-66-3 624 ND 5.0 uglL 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5.0 uglL 1 Dibromochloromethane 124-48-1 624 ND 5.0 uglL 1 1,1-Dichloroethane 75-34-3 624 ND 5.0 uglL 1 1,2-Dichloroethane 107-06-2 624 ND 5.0 uglL 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 uglL 1 trans-1,2-Dichloroethene 156-60-5 624 ND 5.0 uglL 1 1,2-Dichloropropane 78-87-5 624 ND 5.1) uglL 1 Cis-1,3-Dichloropropene 10061-01-5 624 ND 5.0 uglL i trans-1,3-Dichloropropene 10061-02-6 624 NO 5.0 uglL 1 Ethylbenzene 100-41-4 624 ND 5.0 uglL 1 Methylene chloride 75-09-2 624 ND 5.0 uglL 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 uglL 1 Tetrachloroethene 127-18-4 624 NO 5.0 uglL 1 Toluene 108-88-3 624 ND 5.0 uglL 1 1,1,1-Trichloroethane 71-55-6 624 ND 5.0 uglL 1 1,1,2-Trichloroethane 79-00-5 624 NO 5.0 uglL 1 Trichloroethene 79-01-6 624 ND 5.0 uglL 1 Vinyl chloride 75-01-4 624 NO 5.0 uglL 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 103 70-130 Bromoflu ore benzene 102 70-130 Toluene-d8 106 70-130 PQL = Practical quantitation limit e = Detected in the method blank E = Quanlitalion of compound exceeded the calibration range H = Out of holding tkme ND = Not detected at or above the PQL J = Estimated result a PC and � MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of cnteria — r Where applicable, all soil sample analysis are reported on a dry weight basis unless Slagged with a `VV' Shealy Environmental Services, Inc. Page: 6 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Level 1 Report v2.1 • Semivolatile Organic Compounds by GCIMS r .Client:BMHST Laboratory ID: PK18047-001 Description: R&D-01 Matrix: Aqueous Date Sampled:ll/1712014 1445 Date Received : 1111812 014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 11/24/2014 2159 JCG 11/19/2014 1345 61224 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 ug/L 1 Acenaphthylene 208-96-8 625 ND 2.0 ug/L 1 Anthracene 120-12-7 625 NO 2.0 ug/L 1 Benzidine 92-87-5 625 NO 10 ug1L 1 Benzo(a)anthracene 56-55-3 625 NO 2.0 ug1L 1 Benzo(a)pyrene 50-32-8 625 NO 2.0 ug1L 1 Benza(b)fluoranthene 205-99-2 625 NO 2.0 ug1L 1 Benza(g,h,i)perylene 191-24-2 625 NO 2.0 u91L 1 Benzo(k)fluoranthene 207-08-9 625 NO 2.0 u911- 1 4-Bromophenyl phenyl ether 101-55-3 625 NO 2.0 ug1L 1 Butyl benzyl phthalate 85-68-7 625 NO 10 ug1L 1 4-Chloro-3-methyl phenol 59-50-7 625 NO 2.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625 NO 2.0 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625 NO 2.0 ug/L 1 bis(2-Chloroisopropyl)ether 108-60-1 625 NO 2.0 ug/L 1 2-Chloronaphthalene 91-58-7 625 ND 2.0 ug/L 1 2-Chlorophenol 95-57-8 625 NO 2.0 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 ug/L 1 Chrysene 218-01-9 625 ND 2.0 u91L 1 Dibenzo(a,h)anthracene 53-70-3 625 NO 2.0 ug1L 1 1,2-Dichlorobenzene 95-50-1 625 NO 2.0 ug1L 1 1,3-Dichlorobenzene 541-73-1 625 NO 2.0 ug1L 1 1,4-Dichl oro benzene 106-46-7 625 NO 2,0 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 NO 10 ug/L 1 2,4-Dichlorophenol 120-83-2 625 NO 2.0 ug/L 1 Diethylphthalate 84.66-2 625 ND 10 ug/L 1 Dimethyl phthalate 131-11-3 625 NO 10 ug/L 1 2,4-Dimethylphenol 105-67-9 625 NO 2.0 uglL 1 Di-n-butyl phthalate 84-74-2 625 NO 10 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 NO 10 ug/L 1 2,4-Dinitrophenol 51-28-5 625 NO 10 ug/L 1 2,4-Dinitrotoluene 121-14-2 625 NO 4.0 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.0 ug1L 1 Di-n-octylphthalate 117-84-0 625 NO 10 ug1L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 NO 2.0 ug1L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 ND 10 ug/L 1 Fluoranlhene 206-44-0 625 ND 2.0 ug/L 1 Fluorene 86-73-7 625 ND 2.0 ug/L 1 Hexachlorobenzene 118-74-1 625 NO 2,0 u911- 1 Hexachlorobutadiene 87-68-3 625 ND 2,0 ug/L 1 H exachlorocycl o pentad iene 77-47-4 625 NO 10 ug1L 1 Hexachloroethane 67-72-1 625 ND 2.0 uglL 1 Indeno(1,2,3-c,d)pyre ne 193-39-5 625 NO 2.0 uglL 1 Isophorone 78-59-1 625 NO 2.0 ug/L 1 PQL= Practical quantitation limit B = Detected in the method blank E = Quantilalion of compound exceeded the calibration range H = Oul of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MOL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, at; soil sample analysis are reported on a dry weight basis unless flagged with a W Shealy Environmental Services, Inc, Page: 7 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS .Client:EMH&T Laboratory ID: PK18047-001 Description: R&D-01 Matrix: Aqueous Date Sampled:1111712014 1445 )ate Received:1111812014 Run Prep Method Analytical Method 1 625 625 Dilution Analysis Date Analyst 1 11/24/2014 2159 JCG Prep Date 11/19/2014 1345 Batch 61224 CAS Analytical Parameter Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 ug/L 1 Nitrobenzene 98-95-3 625 ND 2.0 ug/L 1 2-Nitrophenol 88-75-5 625 ND 4.0 ug/L 1 4-Nitrophenol 100-02-7 625 ND 10 uglL 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 uglL 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 uglL 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 ug]L 1 Pentachlorophenol 87-86-5 625 ND 10 uglL 1 Phenanthrene 85-01-8 625 ND 2.0 ug/L 1 Phenol 108-95-2 625 ND 2.0 ug1L 1 Pyrene 129-00-0 625 N❑ 2.0 ug1L 1 1,2,4-Trichlorobenzene 120-82-1 625 N❑ 2.0 ug1L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 ug1L 1 Surrogate 2-Fluorobiphenyl 2-Fluorophenol Nitrobenzene-d5 Phenol-d5 Terphenyl-d14 2,4,6-Tribrorrophenol Run 1 Acceptance Q % Recovery Limits 94 37-129 76 24-127 88 38-127 82 28-128 84 10-148 103 41-144 PQL = Practical quantitation limit B = Detected in the method blank E = Quantization of compound exceeded the calibration range H = Out of holding time NO- Not detected at or above the PC J = Estimated result � PQL and > MDL P = The RPO between two GC columns exceeds 40% N = Recovery is out of Media Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Shealy Environmental Services, Inc. Page: 8 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Organochlorine Pesticides and PCBs .Client: EMHBT Laboratory ID: PK18047-001 Description: R&D-01 Matrix: Aqueous Date Sampled:1111712014 1445 Date Received: 1111812014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608 608 1 11/24120141133 MEM 11/19/20141823 61283 2 608 608 1 11/24120141121 PMS 11119/20141823 61283 CAS Analytical Parameter Number Method Result Q PQL Units Run Aldrin 309-00-2 608 ND 0.025 uglL 1 alpha-BHC 319-84-6 608 ND 0.025 uglL 1 beta-BHC 319-85-7 608 ND 0.025 u91L 1 delta-BHC 319-86-8 608 ND 0.025 ug1L 1 gamma-BHC (Lindane) 58-89-9 608 ND 0.025 ug1L 1 Chlordane 57-74-9 608 ND 0.25 ug/L 1 4,4'-DDD 72-54-8 608 ND 0,025 ug/L 1 4,4'-DDE 72-55-9 608 ND 0.025 ugll- 1 4,4'-DDT 50-29-3 608 ND 0.025 ug1L 1 Dieldrin 60-57-1 608 ND 0.025 ug1L 1 Endosulfan 1 959-98-8 608 ND 0.025 ug1L 1 Endosulfan II 33213-65-9 608 ND 0.025 ug1L 1 Endosulfan sulfate 1031-07-8 608 ND 0.025 uglL 1 Endrin 72-20-8 608 ND 0.025 ug1L 1 Endrin aldehyde 7421-93-4 608 ND 0.025 ug1L 1 Heptachlor 76-44-8 608 ND 0.025 ug1L 1 Heptachlor epoxide 1024-57-3 608 ND 0.025 ug1L 1 Toxaphene 8001-35-2 608 ND 0.25 ug1L 1 Aroclor 1016 12674-11-2 608 ND 0.25 ug1L 2 Aroclor 1221 11104-28-2 608 ND 0.25 ug1L 2 Aroclor 1232 11141-16-5 608 ND 0.25 ug1L 2 Aroclor 1242 53469-21-9 608 ND 0.25 ug1L 2 Aroclor 1248 12672-29-6 608 ND 0.25 ug1L 2 Aroclor 1254 11097-69-1 608 ND 0,25 ug1L 2 Aroclor 1260 11096-82-5 608 ND 0.25 ug1L 2 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits Decachlorobiphenyl 39 20-131 60 20-131 Tetra chloro-m-xyiene 69 26-132 101 26-132 PQL = Practical quantitation limit B = Detected in the method blank E = Quantization of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' ' Shealy Environmental Services, Inc. Page: 9 of 43 106 Vantage Point Drive West Columbia, SC 29172 (a03) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2,1 • ICP-AES .Client:EMH&T Laboratory ID: PK18047-001 Description: R&D-01 Matrix: Aqueous Date Sampled:111/17120141445 Date Received: 1111812014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.7 200.7 1 11/28/2014 1237 FTS 11119/2014 0845 61200 CAS Analytical Parameter Number Method Result Q PQL Units Run Copper 7440-50-8 200.7 ND 0.0050 ri 1 Lead 7439-92-1 200.7 ND 0.010 mglL 1 Zinc 7440-66-6 200.7 ND 0.020 mglL 1 0 PQL = Practical quantitation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result - PQL and > M DL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 10 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab,com Level 1 Report v2.1 N Inorganic non-metals .Client:EMHBT Laboratory ID: PK18047-002 Descriplion: HPE-02 Matrix: Aqueous Date Sampled:1111712014 1345 Date Received: 1111812014 Run Prep Method t Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH) SM 4500-H B-2011 1 11/1912014 0902 AMM1 61207 1 (TSS) SM 2540D-2011 1 11/20/2014 1500 AAD 61357 1 (HEM (oil and) 1664E 1 11/2512014 0945 EWR 61645 CAS Analytical Parameter Number Method Result Q PQL Units Run pH SM 4500-H B 6.61 su 1 TSS SM 254OD-20 14 2.5 mg1L 1 HEM (oil and grease) 1664E 5.7 4.5 mg1L 1 POL = Praci cal quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result � PQL and n MOL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged wah a Shealy Environmental Services, Inc. Page: 11 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 ` Volatile Organic Compounds by GC/MS f lient: EMH&T Laboratory ID: PK18047-002 Description: HPE-02 Matrix: Aqueous Date Sampled:1111712014 1345 Date Received: 1Ili 8/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 11/25/2014 2315 PMM2 61751 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 ug1L 1 Acrylonitrile 107-13-1 624 ND 50 ug1L 1 Benzene 71-43-2 624 ND 5.0 ug1L 1 Bromodichloromethane 75-27-4 624 ND 5.0 ug1L 1 Bromoform 75-25-2 624 ND 5.0 ug1L 1 Bromomethane (Methyl bromide) 74-83-9 624 ND 5.0 ug1L 1 Carbon tetrachloride 56-23-5 624 ND 5.0 ug1L 1 Chlorobenzene 108-90-7 624 ND 5.0 ug1L 1 Chloroethane 75-00-3 624 ND 5.0 ug1L 1 2-Chloroethylvinylether 110-75-8 624 ND 10 ug1L 1 Chloroform 67-66-3 624 ND 5.0 ug1L 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5,0 uglL 1 Dibromochloromethane 124-48-1 624 ND 5.0 uglL 1 1,1-Dichloroethane 75-34-3 624 ND 5,0 uglL 1 1,2-Dichloroethane 107-06-2 624 ND 5.0 ug1L 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 ug1L 1 trans-1,2-Dichloroethene 156-60-5 624 ND 5.0 ug1L 1 -1,2-Dichloropropane 78-87-5 624 ND 5.0 l lL 1 cis- 1,3-Dichloroprope ne 10061-01-5 624 ND 5.0 ug1L 1 trans -1,3-Dichloropropene 10061-02-6 624 ND 5.0 ug1L 1 Ethylbenzene 100-41-4 624 ND 5.0 uglL 1 Methytene chloride 75-09-2 624 ND 5.0 uglL 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 ug1L 1 Tetra chloroethene 127-18-4 624 ND 5.0 ug1L 1 Toluene 108-88-3 624 ND 5.0 ug1L 1 1,1, 1 -Trichloroethane 71-55-6 624 ND 5.0 uglL 1 1,1,2-Trichloroethane 79-00-5 624 ND 5.0 ug1L 1 Trichloroethane 79-01.6 624 ND 5.0 uglL 1 Vinyl chloride 75-01-4 624 ND 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 106 70-130 Bromofluorobenzene 102 70-130 Toluene-d8 106 70-130 PQL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < PQL and > MOL P = The RPD between two GO columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless Slagged with a "W' Shealy Environmental Services, Inc. Page: 12 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealyleib.com Level 1 Report v2.1 Semivolatile Organic Compounds by GCIMS ,Client:EMH&T Laboratory ID: PK18047-002 Description: HPE-02 Matrix: Aqueous Date Sampled:11117/2014 1345 Date Reoeived:1111812014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 11/24/2014 2223 JCG 11/19/2014 1345 61224 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 ug1L 1 Acenaphthylene 208-96-8 625 NO 2.0 uglL 1 Anthracene 120-12-7 625 ND 2.0 u91L 1 Benzidine 92-87-5 625 ND 10 u91L 1 Benzo(a)anthracene 56-55-3 625 ND 2.0 u91L 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug/L 1 Benzo(b)tluoranthene 205-99-2 625 ND 2.0 uglL 1 Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 uglL 1 Benzo(k)fluoranthene 207-08-9 625 ND 2.0 uglL 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 uglL 1 Butyl benzyl phthalate 85-68-7 625 ND 10 uglL 1 r 4-Chloro-3-methyl phenol 59-50-7 625 ND 2.0 uglL 1 bis(2-Chloroethoxy)methane 111-91-1 625 ND 2.0 u91L 1 bis(2-Chloroethyl)ether 111-44-4 625 ND 2.0 uglL 1 bis(2-Chloroisop ropyl)ether 108-60-1 625 ND 2.0 uglL 1 2-Chloronaphthalene 91-58-7 625 ND 2.0 uglL 1 2-Chlorophenol 95-57-8 625 ND 2.0 uglL 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 uglL 1 Chrysene 218-01-9 625 ND 2.0 ug1L 1 Dibenzo(a,h)anthracene 53-70-3 625 ND 2.0 uglL 1 1,2-Dichlorobenzene 95-50-1 625 ND 2.0 uglL 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 uglL 1 1,4-Dichlorobenzene 106-46-7 625 ND 2.0 uglL 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 uglL 1 2,4-Dichlorophenol 120-83-2 625 ND 2.0 uglL 1 Diethylphtha late 84-66-2 625 ND 10 uglL 1 Dimethyl phthalate 131-11-3 625 ND 10 ug1L 1 2,4-Dimethyiphenol 105-67-9 625 ND 2.0 ug1L 1 Di-n-butyl phthalate 84-74-2 625 ND 10 ug1L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 10 ug1L 1 2,4-Dinitrophenol 51-28-5 625 ND 10 ug1L 1 2,4-Dinitrotoluene 121-14-2 625 ND 4.0 ug1L 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.0 uglL 1 Di-n-octylphthalate 117-84-0 625 ND 10 uglL 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 2.0 uglL 1 bis(2- Ethyl hexyl)phthalate 117-81-7 625 ND 10 uglL 1 Fluoranthene 206-44-0 625 ND 2.0 ug1L 1 Fluorene 86-73-7 625 ND 2.0 u91L 1 Hexachlorobenzene 11B-74-1 625 ND 2.0 uglL 1 Hexachlorobutadiene 87-68-3 625 ND 2.0 Li 1 Hexachlorocyclopentadiene 77-47-4 625 ND 10 ug1L 1 Hexachloroethane 67-72-1 625 ND 2.0 uglL 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 2.0 uglL 1 Isophorone 78-59-1 625 ND 2.0 uglL 1 POL = Practical cluaniltation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimaled result � POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 13 of 43 106 Vantage Point Drive West Columbia, 5C 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS Client: EMH&T Laboratory ID: PK18047-002 Description: HPE-02 Matrix: Aqueous Date Sampled:1111712014 1345 Date Received:11 /1812014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 11/24/2014 2223 JCG 11/19/2014 1345 61224 CAS Analytical Parameter Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 uglL 1 Nitrobenzene 98-95-3 625 ND 2.0 u91L 1 2-Nitrophenol 88-75-5 625 ND 4.0 uglL 1 4-Nitrophenol 100-02-7 625 ND 10 uglL 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 uglL 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 uglL 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 uglL 1 Pentachlorophenol 87-86-5 625 ND 10 ug1L 1 Phenanthrene 85-01-8 625 ND 2.0 ug1L 1 Phenol 108-95-2 625 ND 2.0 ug1L 1 Pyrene 129-00-0 625 ND 2.0 ug1L 1 1,2,4-Trichlorobe nzene 120-82-1 625 ND 2.0 ug1L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 ug1L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 97 37-129 2-Fluorophenol 84 24-127 Nitrobenzene-d5 94 38-127 Phenol-d5 90 28128 Terphenyl-d 14 72 10-148 2,4,6-Tribromophenol 107 41-144 PQL = Practical quantitation limit 8 = Detected in the method blank E - Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result n POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 14 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2_I Organochtorine Pesticides and PCBs . Client: EMH$T Laboratory ID: PK18047-002 Description: HPE-02 Matrix: Aqueous Date Sampled:1111712014 1345 Date Received: 1111812014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608 608 1 11/24120141149 MEM 11/19120141823 61283 2 608 608 1 11124/20141133 PMS 11/19120141823 61283 CAS Analytical Parameter Number Method Result Q PQL Units Run Aldrin 309-00-2 608 ND 0.025 ug]L 1 alpha-BHC 319-84-6 608 ND 0.025 ug/L 1 beta-BHC 319-85-7 608 ND 0.025 ug/L 1 delta-BHC 319-86-8 608 ND 0.025 ug1L 1 gamma-BHC (Lindane) 58-89-9 608 ND 0.025 ug1L 1 Chlordane 57-74-9 608 ND 0.25 ug1L 1 4,4'-DDD 72-54-8 608 ND 0.025 ug1L 1 4,4'-DDE 72-55-9 608 ND 0.025 ug/L 1 4,4'-DDT 50-29-3 608 ND 0.025 ug1L 1 Dieldrin 60-57-1 608 ND 0.025 ug/L 1 Endosulfan 1 959-98-8 608 ND 0.025 ug1L 1 Endosulfan 11 33213-65-9 608 ND 0.025 ug/L 1 Endosulfan sulfate 1031-07-8 608 ND 0.025 ug/L 1 Fndrin 72-20-8 608 ND 0.025 ug/L 1 Endrin aldehyde 7421-93-4 608 ND 0.025 ug/L 1 Heptachlor 76-44-8 608 ND 0.025 ug/L 1 Heptachlor epoxide 1024-57-3 608 ND 0.025 ug/L 1 Toxaphene 8001-35-2 608 ND 0.25 ug/L 1 Aroclor 1016 12674-11-2 608 ND 0.25 ugIL 2 Aroclor 1221 11104-28-2 608 ND 0.25 ug/L 2 Aroclor 1232 11141-16-5 608 ND 0.25 ugIL 2 Aroclor 1242 53469-21-9 608 ND 0.25 ug/L 2 Aroclor 1248 12672-29-6 608 NO 0.25 ug/L 2 Aroclor 1254 11097-69-1 608 ND 0.25 ug/L 2 Aroclor 1260 11096-82-5 608 ND 0.25 ug/L 2 Surrogate Decachlorobiphenyl Tetrach lord-m-xyle n e Run 1 Acceptance Run 2 Acceptance Q % Recovery Limits Q % Recovery Limits 25 20-131 37 20-131 56 26-132 79 26-132 1 PQL - Practical quantitates limit B = Detected in the method blank E = Quantilation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the POL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all sail sample analysis are reported on a dry weight basis unless (lagged with a "W' Shealy Environmental Services, Inc. Page: 15 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.aom Level 1 Report v2,1 ICP-AES Client: EMH&T Laboratory ID: PK18047-002 Description: HPE-02 Matrix: Aqueous Date Sampled A111712014 1345 Date Received: 1111812014 Run Prep Method - Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.7 200.7 1 11/28/2014 1308 FTS 11/19/2014 0845 61200 CAS Analytical Parameter Number Method Result Q PQL Units Run Copper 7440-50-8 200.7 0.0055 0.0050 mg1L 1 Lead 7439-92-1 200.7 ND 0,010 ril 1 Zinc 7440-66-6 200.7 ND 0.020 mg1L 1 POL = Practical quanbtation limit B = Detected in the method blank E = Quantltation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J - Estimated result < POL and > MOL P » The RPO between two GC columns exceeds 40% N - Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 16 of 43 106 Vantage Point Drive ' West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals ,Client:EMH&T Laboratory ID: PK18047-003 Description: HPE-01 Matrix: Aqueous Date Sampled:1111712014 1315 Date Received: 1111812014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH) SM 4500-H B-2011 1 11/19/2014 0902 AMM1 61207 1 (TSS) SM 254OD-2011 1 11/20/2014 1500 AAD 61357 1 (HEM (oil and) 1664E 1 11/25/2014 0945 EWR 61645 CAS Analytical Parameter Number Method Result Q PQL Units Run pH SM 4500-H B 6.79 su 1 TSS SM 254OD-20 11 1.4 mglL 1 HEM (oil and grease) 1664B 23 4.7 mg1L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitalion of compound exceeded the calibration range H - Out of holding time ND = Not detected at or above the PQL ,1 = Estimated result < PQL and > MIX P = The RPD between two GC columns exceeds 40% N = Recovery is cut of cnteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 17 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Volatile Organic Compounds by GC/MS .Client:EMH&T Laboratory ID: PK18047-003 Description: HPE-01 Matrix: Aqueous Date Sampled:1111712014 1315 Date Received:1111812014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 11/25/2014 2339 PMM2 , 61751 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 ug/L 1 Acrylonitrile 107-13-1 624 ND 50 ug/L 1 Benzene 71-43-2 624 ND 5.0 ug/L 1 Bromodichloromethane 75-27-4 624 ND 5.0 ug]L 1 Bromoform 75-25-2 624 ND 5.0 uglL 1 Bromomelhane (Methyl bromide) 74-83-9 624 NO 5.0 ug/L 1 Carbon tetrachloride 56-23-5 624 ND 5.0 ug/L 1 Chlorobenzene 108-90-7 624 ND 5.0 ug/L 1 Chloroethane 75-00-3 624 ND 5.0 ug/L 1 2-Chloroethylvinylether 110-75-8 624 ND 10 ug/L 1 Chloroform 67-66-3 624 ND 5.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5.0 ug/L 1 Dibromochtoromethane 124-48-1 624 ND 5.0 ug1L 1 1,1-Dichloroethane 75-34-3 624 ND 5.0 ug1L 1 1,2-Dichloroethane 107-06-2 624 ND 5.0 ug/L 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 624 ND 5.0 ug1L 1 1,2-Dichloropropene 78-87-5 624 ND 5.0 uglL 1 cis- 1,3-Dichloropropene 10061-01-5 624 ND 5.0 ug1L 1 trans-1,3-Dichloropropene 10061-02-6 624 ND 5.0 u91L 1 Ethylbenzene 100-41-4 624 ND 5.0 ug/L 1 Methylene chloride 75-09-2 624 ND 5.0 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 ug/L 1 Tetra chloroethene 127-18-4 624 ND 5.0 ug/L 1 Toluene 108-88-3 624 ND 5.0 ug/L 1 1,1,1-Trichloroethane 71-55-6 624 ND 5.0 ug/L 1 1,1,2-Trichloroethane 79-00-5 624 ND 5.0 ug/L 1 Trichloroethene 79-01-6 624 ND 5.0 ug/L 1 Vinyl chloride 75-01-4 624 ND 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 101 70-130 Bromofluorobenzene 98 70-130 Toluene-d8 106 70-130 PQL = Practical quantitation limit 8 = Oetecled in the method blank E = Quanlitation of compound exceeded the calibration range H = Out of holding time NO - Not detected at or above the PQL J - Estimated result < POT and o- MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a W Shealy Environmental Services, Inc. Page: 18 Of 43 106 Vantage Point Drive West Columbia, SG 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2.1 • Semivolatile Organic Compounds by GC/MS .Client:EMHBT Laboratory ID: PK18047-003 Description: HPE-01 Matrix: Aqueous Date Sampled:1111712014 1315 Date Received: 11/18/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 11/24/2014 2246 JCG 11/19/2014 1345 61224 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 ug/L 1 Acenaphthylene 208-96-8 625 ND 2.0 ug/L 1 Anthracene 120-12-7 625 ND 2.0 ug/L 1 Benzidine 92-87-5 625 ND 10 ug/L 1 Benzo(a)anthracene 56-55.3 625 NO 2.0 ug/L 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug/L 1 Benzo(b)fluoranthene 205-99-2 625 NO 2.0 uglL 1 Benzo(g,hJ)perylene 191-24-2 625 NO 2.0 ug/L 1 Benzo(k)Ruoranthene 207-08-9 625 NO 2.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625 NO 2.0 ug/L 1 Butyl bel l phthalate 85-68-7 625 NO 10 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625 NO 2.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625 NO 2.0 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625 NO 2,0 ug/L 1 bis(2-Chloroisopropyl)ether 108-60-1 625 NO 2,0 ug/L 1 2-Chloronaphthalene 91-58-7 625 NO 2.0 ug/L 1 2-Chlorophenol 95-57-8 625 NO 2.0 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 NO 2.0 ug/L 1 Chrysene 218-01-9 625 NO 2.0 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625 NO 2.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625 NO 2.0 ug/L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 ug/L 1 1,4-Dichlorobenzene 106-46-7 625 NO 2.0 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 ug/L 1 2,4-Dichlorophenol 120-83-2 625 NO 2.0 ug/L 1 Diethylphthalate 84-66-2 625 ND 10 ug/L 1 Dimethyl phthalate 131-11-3 625 ND 10 ug1L f 2,4-Dimethylphenol 105-67-9 625 NO 2.0 ug/L 1 Di-n-butyl phthalate 84-74-2 625 NO 10 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 NO 10 ug/L 1 2,4-Dinitrophenol 51-28-5 625 NO 10 ug/L 1 2,4-DinitrotolLien e 121-14-2 625 NO 4.0 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 NO 4.0 ug/L 1 Di-n-oetylphthalate 117-84-0 625 NO 10 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 NO 2,0 ug/L 1 bis (2-Ethyl hexyl)phthal ate 117-81-7 625 NO 10 ug/L 1 Fluoranihene 206-44-0 625 NO 2.0 ug/L 1 Fluorene 86-73-7 625 NO 2.0 ug/L 1 Hexachloro benzene 118-74-1 625 NO 2.0 ug/L 1 Hexachlorobutadiene 87-68-3 625 NO 2.0 ug/L 1 Hexachlorocyclopentadiene 77-47-4 625 NO 10 ug/L 1 Hexachloroethane 67-72-1 625 NO 2.0 uglL 1 Indeno(1,2,3-c,d)pyre ne 193-39-5 625 NO 2.0 ug/L 1 Isophorone 78-59-1 625 NO 2.0 tig/L 1 PQL - Practical quantization limit B = Detected in the method blank E = Quantitation of campound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RRD between two GC columns exceeds 4D% N - Recovery is out of cnleria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 19 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2 1 Semivolatile Organic Compounds by GCIMS •Client:EMH&T Laboratory ID: PK18047-003 Description: HPE-01 Matrix: Aqueous Date SampledA 111712014 1315 Date Received: lIll 8/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 11/24/2014 2246 JCG 11/19/2014 1345 61224 CAS Analytical Parameter Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 uglL 1 Nitrobenzene 98-95-3 625 ND 2.0 uglL 1 2-Nitrophenol 88-75-5 625 ND 4.0 uglL 1 4-Nitrophenol 100-02-7 625 ND 10 uglL 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 u91L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 ug1L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 ug1L 1 Pentach loro phenol 87-86-5 625 ND 10 ug1L 1 Phenanthrene 85-01-8 625 ND 2.0 ug1L 1 Phenol 108-95-2 625 ND 2.0 ug1L 1 Pyrene 129-00-0 625 ND 2.0 ug1L 1 1,2,4-Trichlorobe nzene 120-82-1 625 ND 2.0 ug1L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 ug1L 1 Run 1 Acceptance Surrogate Q /a Recovery Limits 2-Fluorobiphenyl 99 37-129 2-Fluorophenol 86 24-127 Nitrobenzene-d5 95 38-127 Pher l-d5 92 28.128 Terphenyl-d14 86 10.148 2,4,6-Tribromophenol 105 41.144 PQL = Practical quarititation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < PQL and a MDL P = The RPD between two GC columns exceeds 40% N - Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Shealy Environmental Services, Inc, Page: 20 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.corn Level 1 Report v21 Organochlorine Pesticides and PCBs -Client: EMH&T Laboratory ID: PK18047-003 Description: HPE-01 Matrix: Aqueous Date Sampled:1 1117/2014 1315 Date Received:11118/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608 608 1 11/24120141204 MEM 11119/20141823 61283 2 608 608 1 11/24120141144 PMS 11119120141823 61283 CAS Analytical Parameter Number Method Result Q POL Units Run Aldrin 309-00-2 608 ND 0.025 uglL 1 alpha-BHC 319-84-6 608 ND 0.025 uglL 1 beta-8HC 319-85-7 608 ND 0.025 ug1L 1 delta-BHC 319-86-8 608 ND 0.025 ug1L 1 gamma-BHG (Lindane) 58-89-9 608 ND 0.025 ug1L 1 Chlordane 57-74-9 606 ND 0.25 ug1L 1 4,4'-DDD 72-54-8 608 ND 0.025 u91L 1 4,4'-DDE 72-55-9 608 ND 0.025 ug1L 1 4,4'-DDT 50-29-3 608 ND 0.025 u91L 1 Dielddn 60-57-1 608 ND 0.025 u91L 1 Fndosulfan 1 959-98-8 608 ND 0.025 ug1L 1 Fndosulfan II 33213-65-9 608 ND 0.025 ug1L 1 Fndosulfan sulfate 1031-07-8 608 ND 0.025 ug1L 1 Endrin 72-20-8 608 ND 0.025 ug1L 1 Endrin aldehyde 7421-93-4 608 ND 0.025 ug1L 1 Heptachlor 76-44-8 608 ND 0.025 uglL 1 Heptachlor epoxide 1024-57-3 608 ND 0.025 ug1L 1 Toxaphene 8001-35-2 608 ND 0.25 ug1L 1 Aroclor 1016 12674-11-2 608 ND 0.25 ug/L 2 Aroclor 1221 11104-28-2 608 ND 0,25 ug/L 2 Aroclor 1232 11141-16-5 608 ND 0,25 ug/L 2 Aroclor 1242 53469-21-9 608 ND 0.25 ug/L 2 Aroclor 1248 12672-29-6 608 ND 0.25 ug/L 2 Aroclor 1254 11097-69-1 608 ND 0.25 ug/L 2 Aroclor 1260 11096-82-5 608 ND 0.25 ug/L 2 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits Decachlorobiphenyl 34 20-131 53 20-131 Tetrachloro-m-xylene 71 26-132 101 26-132 POL = Practical quantltation limit B = Detected in the method bank E = Quantitation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the POL J = Estimated result c POL and > MOL P = The RPO between two GC columns exceeds 400A N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 21 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level) Report v2,1 ICP-AES ,Client:EMH&T Laboratory ID: PK18047-003 Descriptions HPE-01 Matrix: Aqueous Date Sampled:11l1712014 1315 Date Received: 1111812014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.7 200.7 1 11/28/2014 1316 FTS 11/19/2014 0845 61200 CAS Analytical Parameter Number Method Result Q PQL Units Run Copper 7440-50-8 200.7 ND 0.0050 r lL 1 Lead 7439-92-1 200.7 ND 0.010 n lL 1 Zinc 7440-66-6 200.7 0.024 0.020 mglL 1 PQL = Practical quanGlation limit 6 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H - Out of holding time NO = Not detected at or above the P01- J = Estimated result < POL and > hdDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 22 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level I Report v2.1 QC Summary Shealy Environmental Services, Inc. Page: 23 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Repanv2.1 Inorganic non-metals - MB Sample ID: PQ61207-001 Matrix: Aqueous Batch:61207 Analvtical Method: 5M 4500-H B-2011 Parameter Result Q Dil PQL Units Analysis Date pH 6.87 1 0.000 su 11/19/2014 0902 PQL = Practical quandlation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page: 24 of 43 Level 1 Report v2.1 N Inorganic non-metals - Duplicate Sample ID: PK18047-003DU Matrix: Aqueous Batch:61207 Analytical Method: SM 4500-H B-2011 Sample Amount Result % RPD Parameter (su) Dil % RPD Limit Analysis Date pH 6.79 6.71 1 1.2 20 11/19120140902 PQL = Practical quantita0n limit P = The RPD between two GC columns exceeds 40°! N = Recovery is out of criteria NO = Not detected at or above the PRL J = Estimated result < PQL and > MM + = RPD is out of critena Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 25 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals - MB Sample ID: P061357-001 Matrix: Aqueous Batch:61357 Analytical Method: SM 254OD-2011 Parameter Result TSS ND Q Dil PQL Units 1 1.0 mglL Analysis Date 11 /20/2014 1500 PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of crilena ND = Not detected at or above the PQL J - Estimated result < PQL and > MDL + = RPo is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless Slagged with a W Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 26 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals - Ll Sample ID: PQ61357-002 Matrix: Aqueous Batch:61357 Analytical Method: SM 254OD-2011 Spike Amount Result % Rec Parameter (mg1L) (mg1L) Q Dil % Rec Limit Analysis Date TSS 250 250 1 99 90-110 11/20120141500 f POL = Practical cluantitation limit P = The RPD between two GC columns exceeds 40% N - Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < POL and - MDL + - RPD is out of criteria Where applicable, all sail sample analysis are reported on a dry weight basis unless flagged with a' W' Note: Catculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 27 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals - MB Sample ID: P061645-001 Matrix: Aqueous Batch:61645 Analytical Method: 1664B Parameter\ Result Q Dil Pi Units Analysis Date HEM (oil and grease) ND 1 4.0 mg1L 11/25/2014 0945 PQL = Practical quantitation limit P - The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria ND = Not detected at or above the POL J - Estimated result < PQL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 28 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealytab.com Level 1 Reportv2.1 Inorganic non-metals - LCS Samplo ID: PQ61645-002 Matrix: Aqueous Batch:61645 Analvtical Method: 1664B Spike Amount Result % Rec Parameter (mg1L) (mglL) Q Dil % Rec Limit Analysis Date ITEM (oil and grease) 40 43 1 108 78-114 11/25/2014 0945 PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Dote: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 29 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab_corn Level 1 Report v2.1 Volatile Organic Compounds by GCIMS - MB Sample ID: P061751-001 Matrix: Aqueous Batch: 61751 Prep Method: 5030B Analytical Method: 624 Parameter Result Q Dil PQL Units Analysis Date Acrolein ND 1 50 uglL 11/25/20141941 Acrylonitrile ND 1 50 uglL 11/25/20141941 Benzene ND 1 5.0 uglL 11125120141941 Bromodichloromethane ND 1 5.0 uglL 11125120141941 Bromoform ND 1 5.0 ug1L 11/25/20141941 Bromomethane (Methyl bromide) ND 1 5.0 uglL 11/25/2014 1941 Carbon tetrachloride ND 1 5.0 uglL 11/25/2014 1941 Chlorobenzene ND 1 5.0 ug1L 11/25/20141941 Chloroethane ND 1 5.0 ug1L 11/25/20141941 2-Chloroethylvinylether ND 1 10 ug1L 11125120141941 Chloroform ND 1 5.0 ug1L 11/25/20141941 Chloromethane (Methyl chloride) ND 1 5.0 ug1L 11/25/2014 1941 Dibromochloromethane ND 1 5.0 uglL 11/25/20141941 12-Dichloroethane ND 1 5.0 uglL 11/25/20141941 1,1-Dichloroethane ND 1 5.0 ug1L 11/25/20141941 trans-1,2-Dichloroethene ND 1 5.0 uglL 11/25/20141941 1,1-Dichloroethene ND 1 5.0 uglL 11/25/20141941 1,2-Dichloropropane ND 1 5.0 uglL 11/25/20141941 trans-1,3-Dichloropropene ND 1 5.0 uglL 11/25/20141941 cis-1,3-Dichloropropene ND 1 5.0 uglL 11/25120141941 Ethylbenzene ND 1 5.0 uglL 11/25120141941 Methylene chloride ND 1 5.0 uglL 11/25/2014 1941 1,1,2,2-Tetrachloroethane ND 1 5.0 uglL 11/25/20141941 Tetrachloroethene N❑ 1 5.0 uglL 11125/20141941 Toluene ND 1 5.0 uglL 11125/20141941 1,12-Trichloroethane ND 1 5.0 uglL 11125/20141941 1,1,1-Trichloroethane ND 1 5.0 uglL 11125/20141941 Trichloroethene ND 1 5.0 uglL 11125120141941 Vinyl chloride ND 1 5.0 uglL 11/25/2014 1941 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 102 70-130 1,2-Dichloroethane-d4 102 70-130 Toluene-d8 105 70-130 POL = Practical quay Marion limp P = The RFD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PDL J = Estimated result a POL and , MOL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W" Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 30 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Volatile Organic Compounds by GC/MS - LCS Sample ID: PQ61751-002 Matrix: Aqueous Batch:61751 Prep Method: 5030B Analytical Method: 624 Spike Amount Result % Rec Parameter (ug1L) (ug1L) Q Dil % Rec Limit Analysis Date Acrolein 200 200 1 102 14-175 11125/20141858 Acrylonitrile 40 42 1 106 60-130 11125/20141858 Benzene 20 20 1 100 37-151 11/25/20141858 Bromodichloromethane 20 20 1 102 35-155 11/25/20141858 Bromoform 20 21 1 106 45-169 11/25/20141858 Bromomethane (Methyl bromide) 20 21 1 104 1-242 11/25/2014 1858 Carbon tetrachloride 20 22 1 111 71-140 11/25/2014 1858 Chlorobenzene 20 21 1 103 37-160 11/25/20141858 Chtoroethane 20 20 1 102 14-230 11/25120141858 2-Chloroethylvinylether 20 20 1 102 1-305 11125120141858 Chloroform 20 21 1 103 51-138 11/25120141858 Chloromethane (Methyl chloride) 20 20 1 102 1-273 11/2512014 1858 Dibromochloromethene 20 21 1 105 53-149 11/25120141858 1,2-❑ichloroethane 20 21 1 106 49-155 11125120141858 1,1-Dichloroethane 20 21 1 103 59-155 11/25120141858 trans-1,2-Dichloroethene 20 20 1 102 54-156 11/25120141858 1,1-Dichloroethene 20 20 1 99 1-234 11/25/20141858 1,2-Dichloropropane 20 21 1 104 1-210 11125/20141858 trans-1,3-Dichloropropene 20 21 1 104 17-183 11/25/20141858 cis- 1,3-Dichloropropene 20 21 1 104 1-227 11/25/20141858 Ethylbenzene 20 21 1 107 37-162 11/25/20141858 Methylene chloride 20 20 1 102 1-221 11/25/2014 1858 1,1,2,2-Tetrachloroethane 20 20 1 100 46-157 11125/20141858 Tetrachloroethene 20 21 1 106 70-130 11125120141858 Toluene 20 21 1 103 47-150 11125120141858 1,1,2-Trichloroethane 20 20 1 102 52-150 11125/20141858 1,1,1-Trichloroethane 20 21 1 105 52-162 11125/20141868 Trichloroethene 20 21 1 104 71-157 11/25120141858 Vinyl chloride 20 20 1 98 1-251 11125/2014 1858 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 107 70-130 1,2-Dichloroethane-d4 95 70-130 Toluene-d8 100 70-130 PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL . = RPD is out of criteria Where applicable, ail soil sample anall are reported on a dry weight basis unless flagged with a' W' Dote: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 31 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Sernivolatile Organic Compounds by GC/MS - MB Sample ID: P061224-001 Matrix: Aqueous Batch: 61224 Prep Method: 625 Analytical Method: 625 Prep Date: 11/19/2014 1345 Parameter Result Q ❑il PQL Units Analysis Date 1,2,4-Trichlorobenzene NO 1 2.0 ug1L 11/24/2014 2113 1, 2-Dichloro benzene NO 1 2.0 ug1L 11/24/2014 2113 1,2-Diphenylhydrazine(as azobenzene) NO 1 2.0 ug1L 11/24/2014 2113 1,3-Dichlorobenzene NO 1 2.0 ug1L 11/24/20142113 1,4-Dichlorobenzene NO 1 2.0 uglL 11/24120142113 2,4,6-Trichlorophenol NO 1 2.0 uglL 11/24/20142113 2,4-Dichlorophenol NO 1 2.0 uglL 1112412014 2113 2,4-Dimethylphenol NO 1 2.0 ug1L 11/24/2014 2113 2,4-Dinitrophenol NO 1 10 uglL 11/24/2014 21113 2,4-Dinitrotoluene NO 1 4.0 uglL 11/2412014 2113 2,6-Dinitrotoluene NO 1 4.0 uglL 11/24/2014 2113 2-Chloronaphthalene NO 1 2.0 uglL 11/24/2014 2113 2-Chlorophenol NO 1 2.0 ug/L 11/24/2014 2113 2-Nitrophenol NO 1 4.0 ug1L 1112412014 2113 3,3'-Dichlorobenzidine NO 1 10 ug1L 11/24/2014 2113 4,6-Dinitro-2-methyiphenol NO 1 10 ug1L 11/24/2014 2113 4-Bromophenyl phenyl ether NO 1 2.0 ug1L 11/24/2014 2113 4-Chloro-3-methyl phenol NO 1 2.0 ug1L 1112412014 2113 4-Chlorophenyl phenyl ether NO 1 2.0 ug1L 11/24/2014 2113 4-Nitrophenol NO 1 10 ug1L 1112412014 2113 Acenaphthene NO 1 2.0 u91L 1112412014 2113 Acenaphthylene NO 1 2.0 uglL 11/24/2014 2113 Anthracene NO 1 2.0 u91L 11/24/2014 2113 Benzidine NO 1 10 ug1L 1112412014 2113 Benzo(a)anthracene NO 1 2.0 uglL 1112412014 2113 Benzo(a)pyrene NO 1 2.0 uglL 11/24/2014 2113 Benzo(b)fluoranthene NO 1 2.0 uglL 11/24/2014 2113 Benzo(g,h,i)perylene ND 1 2.0 uglL 11/24/2014 2113 Benzo(k)fluoranthene ND 1 2.0 uglL 11/24/2014 2113 bis(2-Chloroethoxy)methane ND 1 2.0 uglL 11/24/2014 2113 bis(2-Chloroethyl)ether NO 1 2.0 uglL 11/24/2014 2113 bis(2-Chloroisopropyl)ether NO 1 2.0 ug1L 11/24/2014 2113 bis(2-Ethyihexyl)phthalate NO 1 10 ug1L 11/24/2014 2113 Butyl benzyl phthalate NO 1 10 ug1L 11/24/2014 2113 Chrysene NO 1 2.0 ug1L 11/24/2014 2113 Di-n-butyl phthalate NO 1 10 uglL 11/24/2014 2113 Di-n-octylp hth a late NO 1 10 ug1L 11/24/2014 2113 Dibenzo(a,h)anthracene NO 1 2,0 ug1L 11/24/2014 2113 Diethylphthalate NO 1 10 uglL 1112412014 2113 Dimethyl phthalate NO 1 10 ug1L 11/24/2014 2113 Fluoranthene NO 1 2.0 ug1L 11/24/2014 2113 Fluorene NO 1 2.0 uglL 1112412014 2113 Hexachlorobe nzene NO 1 2.0 uglL 1112412014 2113 Hexachlorobutadiene NO 1 2.0 uglL 11/24/20142113 PQL = Practical quan8tation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result � PQL and > Mt)L + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a W Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 32 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GCIMS - MB Sample ID: PQ61224-001 Matrix: Aqueous Batch: 61224 Prep Method: 625 Analytical Method: 625 Prep Date: 1 ill912014 1345 Parameter Result Q Dil PQL Units Analysis Date Hexachlorocyclopentadiene ND 1 10 uglL 11124120142113 Hexachloroethane ND 1 2.0 ug/L 1112412014 2113 Indeno(1,2,3-c,d)pyrene ND 1 2.0 ug1L 1112412014 2113 Isophorone ND 1 2.0 uglL 11/24/2014 2113 N-Nitrosod i-n -p ropyla mine ND 1 2.0 uglL 11/2412014 2113 N-Nitrosodimelhylamine ND 1 2.0 uglL 11/2412014 2113 N-Nitrosodiphenylamine (Diphenylamine) ND 1 2.0 uglL 11/2412014 2113 Naphthalene ND 1 2.0 uglL 11/2412014 2113 Nitrobenzene ND 1 2.0 uglL 11/2412014 2113 Pentachlo ro phenol ND 1 10 uglL 11/2412014 2113 Phenanthrene ND 1 2.0 uglL 11/24/2014 2113 Phenol ND 1 2.0 uglL 11/24/2014 2113 Pyrene ND 1 2.0 uglL 11/24/2014 2113 Acceptance Surrogate Q 0 /o Rec Limit 2,4,6-Tribromophenol 84 41-144 2-Fluorobiphenyl 94 37-129 2-Fluorophenol 78 24-127 Nitrobenzene-d5 87 38-127 Phenol-d5 86 28-128 Terphenyl-d14 93 10-148 PQL = Practical quantitalion limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and , MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 33 of 43 106 Vantage Point Drive West Columbia, SG 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Level 1 Report v2,1 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: PQ61224-002 Batch: 61224 Analytical Method: 625 Matrix: Aqueous Prep Method: 625 Prep Date: 11/19/2014 1345 Spike Amount Result % Rec Parameter (uglL) (uglL) Q Dil % Rec Limit Analysis Date 1,2,4-Trichlorobenzene 20 19 1 95 44-142 11124.12014 2136 1,2-Dichlorobenzene 20 18 1 91 32-129 11/24/2014 2136 1,2-Diphenythydrazine(as azobenzene) 20 15 1 73 30-130 11/24/2014 2136 1,3-Dichlorobenzene 20 17 1 86 0-172 11/24/2014 2136 1,4-Dichlorobenzene 20 17 1 87 20-124 11/2412014 2136 2,4,6-Trichlorophenol 20 22 1 109 37-144 11/2412014 2136 2,4-Dichlorophenal 20 20 1 102 39-135 11/2412014 2136 2,4-Dimethylphenol 20 20 1 102 32-119 11/2412014 2136 2,4-Dinitrophenol 100 160 1 164 0-191 11/2412014 2136 2,4-Dinitrotoluene 40 48 1 119 39-139 11/2412014 2136 2,6-Dinitrotoluene 40 47 1 119 50-158 11/2412014 2136 2-Chloronaphlhalene 20 17 1 86 60-118 11/2412014 2136 2-Chlorophenol 20 18 1 91 23-134 11/24.12014 2136 2-Nitrophenol 40 47 1 116 29-182 11/2412014 2136 3,3'-Dichlorobenzidine 40 ND 1 0.00 0-262 11/24/2014 2136 4,6-Dinitro-2-methylphenol 100 140 1 141 0-181 11/24/2014 2136 4-Bromophenyl phenyl ether 20 20 1 98 53-127 11/24/2014 2136 4-Chloro-3-methyl phenol 20 20 1 102 22-147 11/2412014 2136 4-Chlorophenyi phenyl ether 20 20 1 102 25-158 11/2412014 2136 4-Nitrophenol 10D 120 1 121 0-132 11/241'2014 2136 Acenaphthene 20 19 1 95 6D-132 11/2412014 2136 Acenaphthylene 20 22 1 108. 54-126 11/2412014 2136 Anthracene 20 20 1 100 43-118 11/2412014 2136 Benzidine 40 ND N 1 0.00 1-150 11/2412014 2136 Benzo(a)anthracene 20 18 1 92 42-133 11/242014 2136 Benzo(a)pyrene 20 18 1 88 17-163 11/242014 2136 Benzo(b)fluoranthene 20 21 1 106 24-159 11/24/2014 2136 Benzo(g,h,i)perylene 20 16 1 82 0-219 11/242014 2136 Benzo(k)fluofanthene 20 23 1 113 11-162 11/24/2014 2136 bis(2-Chloroethoxy)methane 20 18 1 90 33-184 11/2412014 2136 bis(2-Chloroethyl)ether 20 16 1 78 12-158 11/2412014 2136 bis(2-Chloroisopropyl)ether 20 16 1 78 36-166 11/2412014 2136 bis(2-Ethylhexyl)phthalate 20 20 1 99 8-158 11/24/2014 2136 Butyl benzyl phthalate 20 20 1 99 0-152 11/24/2014 2136 Chrysene 20 20 1 98 17-168 11/24/2014 2136 Di-n-butyl phthalate 20 20 1 102 1-118 11124/20142136 Di-n-octylphtha late 20 22 1 108 4-146 11/24/20142136 Dibenzo(a,h)anthracene 20 18 1 91 0-227 11124/2014 2136 Diethylphthalate 20 20 1 101 0-114 11/24/2014 2136 Dimethylphthalate 20 20 1 11 0-112 11/24/20142136 Fluoranthene 20 20 1 102 26-137 11/24/2014 2136 Fluorene 20 20 1 99 59-121 11/24/2014 2136 Hexachlorobenzene 20 20 1 99 0-152 11/24/2014 2136 Hexachlorobutadiene 20 20 1 100 24-116 11/24/2014 2136 PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL += RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Ervlronmental Services, Inc. Page: 34 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS - L.CS Sample ID: PQ61224-002 Matrix: Aqueous Batch:61224 Prep Method: 625 Analytical Method: 625 Prep Date: 11/19/2014 1345 Spike Amount Result % Rec Parameter (ugJL) (ug1L) Q Dil % Rec Limit Analysis Date Hexachlorocyclopentadiene 100 48 1 48 1-150 11/24/2014 2136 Hexachloroethane 20 16 1 82 40-113 11/2412014 2136 Indeno(1,2,3-c,d)pyrene 20 17 1 87 0-171 11/2412014 2136 Isophorone 20 18 1 90 21-196 11/2412014 2136 N-Nitrosodi-n-propyiamine 20 17 1 86 0-230 11/24/2014 2136 N-Nitrosodimethylamine 20 17 1 85 1-150 11/24/2014 2136 N-Nitrosodiphenylamine (Diphenylamine) 20 15 1 76 1-150 11/24/2014 2136 Naphthalene 20 19 1 94 21-133 11/24/2014 2136 Nitrobenzene 20 19 1 95 35-180 11/24/2014 2136 Pentachlorophenol 100 130 1 125 14-176 1 1/24/2014 2136 Phenanthrene 20 20 1 102 54-120 11/2412014 2136 Phenol 20 17 1 85 5-112 1112412014 2136 Pyrene 20 18 1 90 52-115 1112412014 2136 Acceptance Surrogate e Q /o Rec Limit 2,4,6-Tribromophenol 109 41-144 2-Fluorobiphenyl 96 37-129 2-Fluorophenol 84 24-127 Nitrobenzene-d5 96 38-127 Phenol-d5 88 28-128 Terphenyl-d 14 99 10-148 PQL = Practical quanUtalion limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL * = RPD is out of criteria Where applicable, all soil sample analysis are reported cn a dry weight basis unless flagged with a' W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 35 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level Report v2.1 Organochiorine Pesticides and PCBs - MB Sample ID: PQ61283-001 Matrix: Aqueous Batch:61283 Prep Method: 608 Analytical Method: 608 Prep Date: 11/19/2014 1823 Parameter Result Q Dil PQL Units Analysis Date 4,4'-DDD ND 1 0.025 uglL 11/2412014 1102 4,4'-DDE ND 1 0.025 uglL 11124120141102 4,4'-DDT ND 1 0.025 ug1L 11/24/20141102 Aldrin ND 1 0.025 ug]L 11/2412014 1102 alpha-BHC ND 1 0.025 ug/L 11/2412014 1102 Aroclor 1016 ND 1 0.25 ug/L 11/24/2014 0000 Aroclor 1221 ND 1 0.25 ug/L 1112412014 DODO Aroclor 1232 ND 1 0.25 ug/L 11/2412014 0000 Aroclor 1242 ND 1 0.25 ug/L 11/24(2014 0000 Aroclor 1248 ND 1 0.25 ug1L 11/2412014 0000 Aroclor 1254 ND 1 0.25 ug1L 11/2412014 0000 Aroclor 1260 ND 1 0.25 ug1L 1112412014 0000 beta-BHC ND 1 0.025 ug1L 11/24QO141102 Chlordane ND 1 0.25 ug1L 11/2412014 1102 delta-BHC ND 1 0.025 ug1L 11/24/2014 1102 Dieldrin ND 1 0.025 ug1L 11/24/2014 1102 Endosulfan I ND 1 0.025 ug1L 1112412014 1102 Endosulfan 11 ND 1 0.025 ug1L 11/24/2014 1102 Endosulfan sulfate ND 1 0.025 ug1L 11/24/2014 1102 Endrin ND 1 0.025 ug1L 11/2412014 1102 Endrin aldehyde N❑ 1 0.025 ug1L 11/2412014 1102 gamma-BHC (Lindane) ND 1 0.025 ug/L 11/24/2014 1102 Heptachlor ND 1 0.025 ug/L 11/24/20141102 Heptachlor epoxide ND 1 0.025 ug/L 1112412014 1102 Toxaphene ND 1 0.25 ug/L 11124120141102 Acceptance Surrogate Q % Rec Limit Decachlorobiphenyl 66 20-131 Tetrachloro-m-xylene 68 26-132 POL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND - Not detected at or above the POL J - Estimated result - POL and > MDL + RPO is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 36 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Organochlorine Pesticides and PCBs - LCS Sample ID: PQ61283-002 Matrix: Aqueous Batch: 61283 Prep Method: 608 Analytical Method: 608 Prep Date: 11/19/2014 1823 Spike Amount Result % Rec Parameter (uglL) (uglL) Q Dil % Rec Limit Analysis Date 4,4'-DDD 0.50 0.45 1 90 31-141 11/24120141118 4,4'-DDE 0.50 0.41 1 83 30-145 11/24120141118 4,4'-DDT 0.50 0.47 1 94 25-160 11124/20141118 Aldrin 0.50 0.41 1 82 42-122 11/24120141118 alpha-BHC 0.50 0.42 1 83 37-134 11/24120141118 beta-BHC 0.50 0.43 1 87 17-147 11/24120141118 delta-BHC l 0.50 . 0.45 1 89 19-140 11 /24/2014 1118 Dieldrin 0,50 0.44 1 88 36-146 11/24/20141148 Endosulfan 1 0,50 0.43 1 85 45-153 11/24/2014 1118 Endosulfan 11 0.50 0.41 1 82 1-202 11/24/2014 1118 Endosulfan sulfate 0,50 0.42 1 84 26-144 11/24/2014 1118 Endrin 0.50 0.42 1 83 30-147 11/24/2014 1118 Endrin aldehyde 0.50 0.37 1 75 50-130 11/24/2014 1118 gamma-BHC (Lindane) 0.50 0.44 1 88 32-127 11/24/2014 1118 Heptachlor 0.50 0.41 1 82 34-111 11124/20141118 Heptachlor epoxide 0.50 0.41 1 82 37-142 11/24/2014 1118 Acceptance Surrogate Q % Rec Limit Deeachlorobiphenyl 46 20-131 Tetra ch loro-m-xyle n e 75 26-132 PQL = Practical quantitation limit P - The RPD between two CC columns exceeds 401A N = Recovery is out of criteria ND = Not detected at or above the PQL J - Estimated result < PQL and - MDL + = RPD is out of criteria Where appficabie, all soil sample analysis are reported on a dry weight basis unless flagged with a W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 37 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com tevet 1 Report v2.1 ICP-AES - MB Sample ID: PQ61200-001 Matrix: Aqueous Batch:61200 Prep Method: 200.7 Analytical Method: 200.7 Prep Date: 11/1912014 845 Parameter Result Q Dil PQL Units Analysis Date Copper ND 1 0.0050 mg1L 11128120141219 Lead ND 1 0.010 mg1L 11128120141219 Zinc ND 1 0.020 mg1L 11128120141219 PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out cf cntena ND = Not detected at or above the POL J = Estimated result < PQL and > i + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 38 of 43 106 Vantage Point Orive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheaiylab.com Level 1 Reportv2l ICP-AES - LCS Sample ID: PQ61200-002 Matrix: Aqueous Batch: 61200 Prep Method: 200.7 Analvtical Method: 200.7 Prep Date: 11/19/2014 845 Spike Amount Result % Ree Parameter (mg/L) (mg1L) Q DO % Rec Limit Analysis Date Copper 2.0 1.9 1 94 85-115 11128120141224 Lead 0.40 0.40 1 99 85-115 11128120141224 Zinc 2.0 1.9 1 93 85-115 11/28120141224 PQL = Practical quantltation limit P = The RPD between two GC columns exceeds 46% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of cntera Where applicable, all soil sample analysis are reported an a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 39 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Level 1 Reportv2.1 ICP-AES - LCSD Sample ID: P061200-003 Matrix: Aqueous Batch:61200 Prep Method: 200.7 Analytical Method: 200.7 Prep Date: 11/19/2014 845 Spike Amount Result % Rec % RPD Parameter (mg1L) (mg1L) Q oil % Rec % RPD Limit Limit Analysis Date Copper 2.0 2.0 1 99 5.0 85-115 20 11128120141228 Lead 0.40 0.40 1 101 1.8 85-115 20 11128120141228 Zinc 2.0 1.9 1 97 3.7 85-115 20 11/28120141228 PC = Practical quaniiiawn limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria ND = Not detected at or above the PC J = Estimated result , PCL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged wlth a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 40 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2_1 ICP-AES - MS Sample ID: PK18047-001MS Matrix: Aqueous Batch:61200 Prep Method: 200.7 Analytical Method: 200.7 Prep Date: 11/19/2014 845 Sample Spike Amount Amount Result - % Rec Parameter (mglL) (mglL) (mg1L) Q oil % Rec Limit Analysis Date Copper ND 2.0 1.9 1 96 75-125 11128120141254 Lead ND 0,40 0.41 1 102 75-125 11128120141254 Zinc ND 2.0 1.9 1 96 75-125 11/28/20141254 PQL = Practical quanUtation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria NO = Not detected at or above the PQL - J = Estimated result a PQL and , MDL * = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W, Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 41 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 1 4 ICP-AES - MSD Sample ID: PK18047-001MD Matrix: Aqueous Batch: 61200 Prep Method: 200.7 Analytical Method: 200.7 Prep Date: 11/19/2014 845 Sample Spike Amount Amount Result % Rec % RPD Parameter (mglL) (mg1L) (mglL) 0 Dil % Rec % RPD Limit Limit Analysis Date Copper ND 2.0 1.9 1 93 3.0 75-125 20 11/28/20141259 Lead NO 0.40 0.40 1 100 2.3 75-125 20 11128/20141259 Zinc ND 2.0 1.9 1 93 2.8 ' 75-125 20 11/28/20141259 PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result - PQL and > MDL + = RPD is out of criteria Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 42 Of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report vZ1 . � r ICP-AES - MS Sample ID: PK18047-002MS Matrix. Aqueous Batch:61200 Prep Method: 200.7 Anatvtical Method: 200.7 Prep Date: 1 ill9/2014 845 Sample Spike Amount Amount Result % Rec Parameter (mg1L) (mg1L) (mg/L) Q Dil % Rec Limit Analysis Date Copper 0.0055 2.0 1.9 1 92 75-125 11/28120141312 Lead ND 0.40 0.39 1 98 75-125 11/28120141312 Zinc ND 2.0 1.8 1 92 75-125 11I28120141312 PQL = Practical quantltation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result a PQL and - MDL + = RPD is out of criteria Where applicable, all soil sample analysis are raponW on a dry weight basis unless Flagged with a'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 43 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 WWW.shealyfab,com Levet t Report v2.1 Main of, Custody Record SHEALY MVIRONMENTAL,SERVICESt INC. 106 Vantage 4?oiat Dare P We91 Calu-r4ia-SC; 29172 Tetepharie No: 801-791-970g.,Fax No. 803.791.9111 wyiw shealylab:oom' Number G1WIr Repnr! ro.coraba. � 7eraGfiarehk�, r�.�y� Ctricte No. .aedrees I Samprera Si L"- And iARxl �=r.rmarespan' sm�ea 17 vagn� or_j_ Cry a-ft = eie;r Z1 i Cede �a d � 1 A-- � , p�If6;1�gllfifll �p PKIa04r,y Pmc fi,Y. lfs& as?idr Pr4Eec71J0_: F.Q:Nn. r A{AHSr h'uu�Caxshar4'.'.+rrj+ by Amrwa0m 7jpa 5]AIA'O i'D r'SQiQ,11anAiro, T77719 �. 95, I O t t 4 3.#5 � Jr � � 7,/ ✓ V, i .�AN/r�4rP��+dThneRequ6ed�Ptlt►fatre�pry lr�anddls�►O�Pee S r. / 6A3t�rr i- I I fi-hmp-aw ❑ RdAWfiT6 wiw f(I�Sai4l "i pos'awHu ldwAnwim oft fCR'xyu'v�c�nertleA--0yj, 7 ��lp fb aid .. 'Gt�xnrmhld rlSktn GrcttaiR UPoid.� rtevrS w r. fila q! ,114V Dam T,4oe 1. RarAiVd !a 17ms 1 - P. R` • , p LI T i7� F RrCe. y Ds T ne 436 3ft&,� ,fby Oaf T94 RaZedb 341-slmy a Trare, 4, R lrryYilEh�d11 D6te Tftrie 71mgA s Are rota! wwk9 hm tEare. iMde.' �c�3G to Yas ft icv Qaflt R-io ram, _j _: a c aG7M&ffM,- ► WC S,YPLiM'Rfrllm rokbM" k"t Sa+n bfsJ; PJNK•F+eAvkrlkfuCopy.• A7cwn�r islumt`ar. F,At}f3t3 Elfrcol�a!]� : Cfl-0r.2pra N + SHEALY ENVIRONMENTAL SERVICES INC. Sbcaly E---dada SUVices, try, l7ocumal, I U]Aer_ F-AD-016 Rrnv.inn Xurr —r 16 KgALrn cwv;07:!V14 F.fYe-'Uvr Dule.. 11,107?14 Sample Receipt Cbecklist. (SRC,) Client: K .h 4 Cooler Inspected by,'date: #Y P @01 Means of receipt SESI ❑ Client ❑ UPS[IFcdEx ❑ Airhornc Exp ❑ Other Yes L1 I No UKI. lticrt custod seals present on tht cooler? Yo; D.. I No ❑ I NA V 12. If custod • seals were pruscqr,, were the intact and unbroken? f :ogler IDIOrigu temperature upon receipt'Derivcd (connected) temperature upon receipt. Method; ❑ Temperature ant: 0 Against Bottles 1R ('Tun ID= ;w4 ER Gun Correction Factor_ A °C Method of coolant: Wet Ice ❑ Blue Ice ❑ Dry Ice Q None Yes ❑ No ❑ NA 'A. If trinperulure of arty Cooler exceeded 6A°C, was Projcct Mana,gtz notified? PM notified by SRC, phone, note (circle one), other. (For rxiolm-3 received via commercial courier, P&4s are to be notified iinirlw iately- yas ❑P0 ❑ 4. Is (lie coalwercial courier's ackin ; slipaltacheli to this form? Yes No ❑5, Were er custodyr-pucdures relin uishedlreceived followed? Yes ❑ ❑ ONAO 5a Were samples relin uished b y client to commercial courier?YC5 o Eli 6. cm-4vm le InsBatedontheCOLT Ycs 7. Were sanip le 10s Iisted on all sam to utTrilainm? Yca ERINo ElS. Was collection date & time listed on the COC? Yes o ❑ 9. Was collection date & time listed nn all sample containers? Yes a ❑ 14. Did all container label inforrnarion (ID, date, time) agive with the COC? Yes t� ❑ I I - Wcrc tests lu be perfornW listed on the COC? Ycs a ❑ 12. Did all sam les arrive in Lhc propLr contalncts foi- each test? Ycs 'o ❑ 13, Did all wtltairvet-, Arrive in good condition funbroken, lids on, ctc. ? yv; ATo ❑ 14. Was adequate sample volume available? Yes tlTp ❑ 15, 'Were al! samples rccci xd within S the holding time or 48 hour;, whichever comes first^ Yea U No 16. Were any slim lc�s COT;I aineN missing? Ycs ❑ I No 17. Were there any e-xcess samples not listed on COC? Yea El No NA ❑ 18, Were bubbles pmsmit, �' a-Si7e" V"or Ciro in diameter in any VOA vials? No ❑ NA ❑ 19. Werc all meta1sr0& 1 i, H1=NVnutriant samples received at a pH of <2? Yr-c ❑ No ❑ Nil 2D. Were all cyanide and+or sulfide samples receN ed at a H ;7-12? Yrs ❑ No ❑ NA 21 _ W= all applicable NH3ITKNIcyanide/pheno1 (0 21npL) samples frue of residual chlarine'r Yes ❑ No ❑ NA 22, Were collection tempenturts documented on the COC for NC samples? Yes ❑ No ❑ NA 23. Were client remark!dre-quests (i.e. requested dilutions, MSIMSI) designations, etc...) correctlytranscribed ('roin the COC into the comment section in UMS? Yes El No 24. Was the quote number used taken from the container label? Sample Pre4ervation (Must be completed for any satnplc(s) incorrectly prescncd ur with headspaee.) Samples) :Pere rev -caved incorrectly preserved and were adjustc4 acoDrdingIZ in sainple receiving with (FT.SO4,HNO3,HC1Na0L!) using SR # Sam le(5) Wert received with buhhic.5 ;-6 mm in diameter. So-fm le(s) t+sere received with TRC = U? +'L• lf#r21 is No SC Drinking Water Project Sarnple(s) pH vcriGed to be> 2 by Date- Sam lc sj were not received at a p1l. of <2 and ware adjusted acco421vusing SR# Sample lahcls a lied b : Verified by: Late: /� Coutrnan18; Shealy Environmental Services, Inc, 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9411 www.shealylab.com Level 1 Report v2.1 ]RON]E)A Honda Power Equipment Mfg., Inc. P.O. Box 37 3721 NC Hwy 119 Swepsonville, NC 27359 Tel: (336) 578-6300 Fax! (336) 229-0768 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 To whom it may concern; Here is our stormwater sampling report for samples taken November 2014. if there are any questions concerning the results please contact me @ 336 516 5890. Thank you, Brendan J. Conway Corp EHS Group Leader Honda Power Equipment Mfg., Inc. 336 578 6307 Cell 336 516 5890 Brendan_conway@hpe.honda.com HONDA Honda Power Equipment Mfg., Inc. P.O. Box 37 3721 NC Hwy 119 5wepsonville, NC 27359 Tel: (336) 578-6300 Fax: (336) 229-0768 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 To whom it may concern; RECEIVED AUG 2 5 2014 CEpWQ BOG S N C G03o 3.-,"t Here is our storrnwater sampling report for samples taken July 2014. If there are any questions concerning the results please contact me cr 336 516 5890. Thank you, f' Brendan J. Conway Corp EHS Group Leader Honda Power Equipment Mfg., Inc. 336 578 6307 Cell 336 516 5890 Brendan—conway@hpe.honda.com Evans, Mechwort, Hombleton & Tilton, Inc. Engineers, Surveyors, Planners, Scientists August 7, 2014 Mr. Brendan Conway Honda Power Equipment Manufacturing, Inc. Post Office Box 37 Swepsonville, North Carolina 27359 Subject: Stormwater Sampling Event — Honda Power Equipment Swepsonville, Alamance County, North Carolina EMH&T Project No. 2013-7 849 Dear Mr. Conway: On July 24, 2014, Evans, Mechwart, Hambleton & Tilton, Inc. (EMH&T) completed a stormwater sampling event at the Honda Power Equipment Manufacturing facility located in Swepsonville, North Carolina. A rain event began at approximately 5:00 pm and ended at approximately 9:00 pm on July 24, 2014. Stormwater samples were collected from three discharge locations (HPE-01, HPE-02, R&D-01) at the property. After collection, the samples were delivered to the Shealy Environmental Services, Inc. (Shealy) laboratory in West Columbia, South Carolina for analysis. A copy of the Stormwater Monitoring Records for this sampling event are provided in Attachment A. The analytical results are presented in summary form in Attachment B. A copy of the laboratory report is included as Attachment C. Stormwater sampling was conducted by Carl Hewett and Perry Wiese of EMH&T. EMH&T appreciates the opportunity to provide our services on this project. Please do not hesitate to call if you have questions or need additional information. Respectfully submitted, EVANS, MECHWART, HAMBLETON & TILTON, INC. AkJ/,6,W Carl H. Hewett Senior Environmental Scientist A legacy of experience. A reputation for excellence, r 301 McCullough Drive, Suite 109,Charlotte, NC 28262 • Phone 704.548.0333 • Fax 704.548.0334 COIOrr%bUS • Ationto • CwrlvVe - Clnclmo i - IndunupcAs emht.com STORMWATER MONITORING RECORD SAMPLING SUMMARY Site: Honda Power Equipment Honda Drive, NC Highway iig Swepsonville, North Carolina 27359 Monitoring Date: July 24, 2014 Previous Measurable Rainfall Event (>o.1 inches): June 20, 2014 Storm Event Approximate Start: 5:0o pm, July 24, 2014 Approximate End: 9:00 pm, July 24, 2014 Storm Duration: approximately 4 hours Rainfall: o.6 inches (assumed value — heavy thunderstorm knocked out the rain gauge) Sampling: sampled discharge point HPE-02 at 7:15 pm (1915) sampled discharge point R&D-ol at 8:oo pm (2000) sampled discharge point HPE-ol at 8:45 pm (2045) Analytical Testing: pH by EPA Method SM 450o-HB TSS by SM 254oD Oil and grease by EPA Method 1664A Volatile organics by EPA Method 624 Semi -volatile compounds by EPA Method 625 PCBs/pesticides by EPA Method 6o8 Copper, Lead, Zinc by EPA Method 200.E Sampled by: Carl Hewett EMH&T 301 McCullough Drive, Suite log Charlotte, North Carolina 28262 Notes: • Storm duration and rainfall amount obtained from the National Weather Service daily summary for Burlington, North Carolina. Page 1 of 1 A feaacv of experience. A reputation for excellence. ATTACHMENT A Stormwater Monitoring Records Honda Power Equipment — Stormwater Sampling (July 201 A) emht.com r 1 STORM WATER MONITORING RECORD QUALITATIVE OBSERVATIONS Site: Honda Power Equipment Honda Drive, NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: July 24, 2014 Sample Location: HPE-oi Discharge Characteristic Rating Comments wr4,w.,°`.tii. Color �ed f. Odor l��d it Clarity Floating Solids �o Suspended Solids Foam Oil sheen Other obvious indicators of stormwaterpollution Characteristic rating scale: none, slight, minor, medium, heavy Monitoring sheet completed by: Date: Vz4li f STORK WATER MONITORING RECORD QUALITATIVE OBSERVATIONS Site: Honda Power Equipment Honda Drive, NC Highway 11g Swepsonville, North Carolina 27359 Monitoring Date: July 24, 2014 Sample Location: HPE-02 Discharge Characteristic Rating Comments ��l w��f :�' � I iP' T 5>. i j". . �. �' 'C :? � �. 3 S ,Y •k � ;� ;'iS.t- e�N. • "'-i- r �- ''FS" _ , Color SL1[�t}'i� 614 EJL*J� tjo Oboe - aft i t,3r a,ry ,j Odor A d'Jf, Clarity Floating Solidsd�� Suspended Solids '40 t Foam. Oil Sheen Other obvious indicators of stormwaterpollution Characteristic rating scale: none, slight, minor, medium, heavy Monitoring sheet completed by: OYY� I. 1/ -� Date: ! Lf 14 STORM WATER MONITORING RECORD QUALITATIVE OBSERVATIONS Site: Honda Power Equipment Honda Drive, NC Highway 119 Swepsonville, North Carolina 27359 Monitoring Date: July 24, 2014 Sample Location: R&D-o1 Discharge Characteristic Rating Comments v., �a ,�'r 4'- y'"ca •}cti. Se.'s �� �'+� � � ':Y s;76"6 � �a q � � a,� -s '_ �,. bra t7� ,� - -��� Color S wi ter- H"%Iy Ra1d fVLNT, A10 ODvR na T,)R a+ Drry ir1 5.4o4PLL Odor A)dPJ f- Clarity CA-1144 Floating Solids Suspended Solids Foam IJv� Oil Sheen Other obvious indicators of stormwaterpollution Characteristic rating scale: none, slight, minor, medium, heavy Monitoring sheet completed by: 1A 1.0 4v - 9A. Date: 7 L A legacy of experience. A reputation to excel ATTACHMENT B Analytical Results Summary Honda Power Equipment — Stormwater Sampling (July 2014) emht.com TABLE Storm Water Analytical Results — July 2014 HondaPower Equipment Swepsonville, Alamance County, North Carolina Hl'E-oi =HPE-02 R&D-oi pH r4 6.5 '� 6.53 6.29 Total Suspended Solids 10 i 330 150 EPA Method 200.8 jF copper 2.7 15 6.6 lead BDL 3.8 1.9 zinc 19 49 29 EPA Method 6o8 target pesticides BDL BDL BDL EPA Method 6o8 target PCBs BDL FBD BDL EPA Method 624 target volatile compounds BDL BDL BDL EPA Method 625 target semi -volatile compounds BDL BDL BDL EPA Method 1664 oil and grease BDL BDL BDL Notes: • Total Suspended Solids are presented in milligrams per liter (ing/L). • BDL = below laboratory minimum quantitation limits Storm water samples collected on July 24, 2014 by EMH&T personnel. A legacy of experience. A reputation for excener ATTACHMENT C Laboratory Report Honda Power Equipment — Stormwater Sampling (July 201 4) ernht.com r SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis EMH&T 301 McCullough Drive Suite 109 Charlotte;•NC 28262 Attention: Carl Hewett Project Name.- Name: Honda Power Equipment Project Number:2014-0211., Lot Number: PG25041 Date Completed:08/04/2014 Kelly M. Maberry Project Manager tE9 titt.ACC04, O w F K � _ This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this reportT Chain of Custody Record and Sample Receipt Checklist. t Shealy Environmental Services, Inc. Page: 1 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative EMH&T Lot Number: PG25041 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page Shealy Environmental Services, Inc. Page: 2 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary EMHBT Lot Number: PG25041 Sample Number Sample ID Matrix Date Sampled Date Received 001 HPE-02 Aqueous 07/24/2014 0715 07/25/2014 002 R&D-01 Aqueous 07/24/2014 0800 07/25/2014 003 HPE-01 Aqueous 07/24/2014 0845 07/25/2014 (3 samples) Shealy Environmental Services, Inc. Page: 3 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary EMH&T Lot Number: PG25041 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 HPE-02 Aqueous TSS SM 2540D- 330 r lL 5 001 HPE-02 Aqueous Copper 200.8 15 uglL 10 001 HPE-02 Aqueous Lead 200.8 3.8 uglL 10 001 HPE-02 Aqueous Zinc 200.8 49 uglL 10 002 R&D-01 Aqueous TSS SM 2540D- 150 mglL 11 002 R&D-01 Aqueous Copper 200.8 6.6 ug1L 16 002 R&D-01 Aqueous Lead 200.8 1.9 ug1L 16 002 R&D-01 Aqueous Zinc 200.8 29 ug1L 16 003 HPE-01 Aqueous TSS SM 2540D- 10 mg1L 17 003 HPE-01 Aqueous Copper 200.8 2.7 ug1L 22 003 HPE-01 Aqueous Zinc 200.8 19 ug1L 22 (11 detections) Shealy Envircnmental Services, Inc. Page: 4 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client:Ei Laboratory ID: PG25041.001 Description: HPE-02 Matrix: Aqueous Date Sampled:07/24I2014 0715 Date Received : 07/2512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH) SM 4500-H B-2011 1 07/28/2014 1727 AAD 52576 1 (TSS) SM 254OD-2011 1 07/29/2014 2035 HMA 52653 1 (SGT - HEM (n) 1664B 1 08/01/2014 0955 JDW 52973 CAS Analytical Parameter Number Method Result Q PQL Units Run pH SM 4500-H B 6.53 su 1 TSS SM 2540D-20 330 10 mg1L 1 SGT -HEM (non -polar material) 1664B ND 4.0 mg/L 1 PQL = Practical quantllation limit 6 = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Wtere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 5 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level i Reportv2.1 Volatile Organic Compounds by GC/MS Client:EMH&T Laboratory ID: PG25041-001 Description: HPE-02 Matrix: Aqueous Date Sampled:07124/2014 0715 Date Received: 0712512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 08/01/2014 0928 PMM2 52948 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 NO 50 ug1L 1 Acrylonitrile 107-13-1 624 NO 50 ug1L 1 Benzene 71-43-2 624 NO 5.0 ug1L 1 Bromodichloromethane 75-27-4 624 NO 5.0 ug/L 1 Bromoform 75-25-2 624 NO 5.0 ug1L 1 Bromomethane (Methyl bromide) 74-83-9 624 NO 5.0 ug/L 1 Carbon tetrachloride 56-23-5 624 NO 5.0 ug1L 1 Chlorobenzene 108-90-7 624 NO 5.0 ug1L 1 Chloroethane 75-00-3 624 NO 5.0 ug/L 1 2-Chloroethylvinylether 110-75-8 624 NO 10 u911- 1 Chloroform 67-66-3 624 NO 5.0 uglL 1 Chloromethane (Methyl chloride) 74-87-3 624 NO 5.0 ug1L 1 Dibromochloromethane 124-48-1 624 NO 5.0 ug/L 1 1,1-0ichloroethane . 75-34-3 624 NO 5.0 ug/L 1 1,2-0ichloroethane 107-06-2 624 NO 5.0 ug1L 1 1,1-Dichloroethene 75-35-4 624 NO 5.0 ug1L 1 trans-1,2-Dichloroethene 156-60-5 624 NO 5.0 ug1L 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 ug1L 1 cis-1,3-Dichloropropene 10061-01-5 624 ND 5.0 ug1L 1 trans- 1,3-Dichloropropene 10061-02-6 624 NO 5.0 ug1L 1 Fthylbenzene 100-41-4 624 NO 5.0 ug1L 1 Methylene chloride 75-09-2 624 NO 5.0 ug1L 1 1,1,2,2-Tetrachtoroethane 79-34-5 624 NO 5.0 ug/L 1 Tetrachloroethene 127-18-4 624 NO 5.0 ug/L 1 Toluene 108-88-3 624 NO 5.0 ug1L 1 1,1,1-Trichloroethane 71-55-6 624 NO 5.0 ug1L 1 1,1,2-Trichloroethane 79-00-5 624 NO 5.0 ug1L 1 Trichloroethene 79-01-6 624 ND 5.0 ug1L 1 Vinyl chloride 75-01-4 624 ND 5.0 ug1L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 109 70-130 Bromofluorobenzene 112 70-130 Toluene-d8 117 70-130 PQL = Practical quantitation limit B = Detected in the method blank E = Quanhtation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < POL and ? MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 6 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2.1 Semivolatile Organic Compounds by GC/MS Client:EMHBT Laboratory ID: PG25041-001 Description: HPE-02 Matrix: Aqueous Date Sampled:0712412014 0715 Date Received:07125/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 07/3112014 2059 DRB1 07/28/2014 1453 52551 CAS Analytical Parameter Number Method Result Q Pi Units Run Acenaphthene 83-32-9 625 ND 2.0 ug1L 1 Acenaphthylene 208-96-8 625 ND 2.0 ug1L i Anthracene 120-12-7 625 ND 2.0 ug/L 1 Benzidine 92-87-5 625 ND 10 ug/L 1 Benzo(a)anthracene 56-55-3 625 ND 2.0 ug/L 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug/L 1 Benzo(b)fluoranthene 205-99-2 625 ND 2.0 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 ug/L 1 Benzo(k)Fluoranthene 207-08-9 625 ND 2.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 ug/L 1 Butyl benzyl phthalate 85-68-7 625 ND 10 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625 ND 2.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625 ND 2.0 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625 ND 2.0 ug1L 1 bis(2-Chloroisopropyl)ether 108-60-1 625 ND 2.0 ug1L 1 2-Chloronaphthalene 91-58-7 625 ND 2.0 1 1 2-Chlorophenol 95-57-8 625 ND 2.0 ug1L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 ug1L 1 Chrysene 218-01-9 625 ND 2.0 ug1L 1 Dibenzo(a,h)anthracene 53-70-3 625 ND 2.0 ug1L 1 1,2-Dichlorobenzene 95-50-1 625 ND 2.0 ug1L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 ug1L 1 1,4-Dichlorobenzene 106-46-7 625 ND 2.0 ug1L 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 ug1L 1 2,4-Dichlorophenol 120-83-2 625 ND 2.0 ug1L 1 Diethy 1phtha late 84-66-2 625 ND 10 ug1L 1 Dimethyl phthalate 131-11-3 625 ND 10 ug1L 1 2,4-Dimethylphenol 105-67-9 625 ND 2.0 ug1L 1 Di-n-butyl phthalate 84-74-2 625 ND 10 ug1L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 10 ug1L 1 2,4-Dinitrophenol 51-28-5 625 ND 10 ug/L 1 2,4-Dinitrotoluene 121-14-2 625 ND 4.0 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.0 ug/L 1 Di-n-octylphtha late 117-84-0 625 ND 10 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 2.0 ug/L 1 bis(2-Ethyl h exyl)phtha late 117-81-7 625 ND 10 ug/L 1 Fluoranthene 206-44-0 625 ND 2.0 ug1L 1 Fluorene 86-73-7 625 ND 2.0 ug1L 1 Hexachlorobe nzene 118-74-1 625 ND 2.0 ug1L 1 Hexachlorobutadiene 87-68-3 625 ND 2.0 ug1L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 10 ug1L 1 Hexachloroethane 67-72-1 625 ND 2.0 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 2.0 ug/L 1 Isophorone 78-69-1 625 ND 2.0 ug/L 1 PC = Practical quantltation limit B - Detected in the method blank E = Quantitation or compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Fstimated resO < PQL and � MDL P - The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 7 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealy:ab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS Client:EMHBT Laboratory ID: PG25041-001 Description: HPE-02 Matrix: Aqueous Date Sampled:0712412014 0715 Date Received:0712512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 07/31/2014 2059 DRB1 07/28/2014 1453 52551 CAS Analytical Parameter Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 ug1L 1 Nitrobenzene 98-95-3 625 ND 2.0 ug1L 1 2-Nitrophenol 88-75-5 625 N❑ 4.0 uglL 1 4-Nitrophenol 100-02-7 625 ND 10 uglL 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 ug1L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 ug1L 1 N-Nitro sod iphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 ug1L 1 Penlachlorophenol 87-86-5 625 ND 10 ug1L 1 Phenanthrene 85-01-8 625 ND 2A ug1L 1 Phenol 108-95-2 625 ND 2.0 ug1L 1 Pyrene 129-00-0 625 ND 2.0 ug1L 1 1,2,4-Trichlorobenzene 120-82-1 625 ND 2.0 ug1L 1 2,4,6-Trichloropheno1 88-06-2 625 ND 2.0 uglL 1 Surrogate Run 1 Q % Recovery Acceptance Limits 2-Fluorobiphenyl 90 37-129 2-Fluorophenol 84 24-127 Nitrobenzene-d5 84 38-127 Phenol-d5 85 28-128 Terphenyl-d14 77 10-148 2,4,6-Tribromophenol 92 41-144 PQL = Practical quantitation limit B = Detected in the method blank E = euantriation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result a POT and? NIDf_ P = The RPD between two GC columns exceeds 40% N = Recovery is out of cmena More applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 8 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Level 1 Report v2.1 Organochlorine Pesticides and PCBs Client:EMH&T Laboratory ID: PG25041-001 Description: HPE-02 Matrix: Aqueous Date Sampled:07/2412014 0715 Date Received :0712512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608 608 1 07131120141527 MEM 07128120141521 52557 2 608 608 1 08/01/2014 0840 MEM 07/28/2014 1521 52557 CAS Analytical Parameter Humber Method Result Q PQL Units Run Aldrin 309-00-2 608 ND 0,025 ug/L 1 alpha-BHC 319-84-6 608 ND 0.025 ug/L 1 beta-BHC 319-85-7 608 ND 0,025 ug1L 1 delta-BHC 319-86-8 608 ND 0.025 ug1L 1 gamma-BHC (Lindane) 58-89-9 608 ND 0.025 ug1L 1 Chlordane 57-74-9 608 ND 0.25 u911- 1 4,4'-DDD 72-54-8 608 ND 0.025 ug1L 1 4,4'-DDE 72-55-9 608 ND 0.025 ug1L 1 4,4'-DDT 50-29-3 608 ND 0.025 ug1L 1 Dieldrin 60-57-1 608 ND 0.025 ug1L 1 Endosulfan 1 959-98-8 608 ND 0.025 ug/L 1 Endosulfan II 33213-65-9 608 ND 0.025 ug/L 1 Endosulfan sulfate 1031-07-8 608 ND 0,025 ug/L 1 Endrin 72-20-8 608 ND 0.025 ug/L 1 Endrin aldehyde 7421-93-4 608 ND 0.025 ug/L 1 Heptachlor 76-44-8 608 ND 0.025 ug/L 1 Heptachlor epoxide 1024-57-3 608 ND 0.025 ug/L 1 Toxaphene 8001-35-2 608 ND 0.25 ug/L 1 Aroclor 1016 12674-11-2 608 ND 0.25 ug/L 2 Aroclor 1221 11104-28-2 608 ND 0.25 ug1L 2 Aroclor 1232 11141-16-5 608 ND 0.25 ug1L 2 Aroclor 1242 53469-21-9 608 ND 0.25 uglL 2 Aroclor 1248 12672-29-6 608 ND 0.25 ug/L 2 Aroclor 1254 11097-69-1 608 ND 0.25 ug1L 2 Aroclor 1260 11096-82-5 608 ND 0.25 ug1L 2 Surrogate Decachlorobiphenyl Tetrachloro-m-xylene Run 1 Acceptance Run 2 Acceptance Q % Recovery Limits Q % Recovery Limits 29 20-131 38 20-131 62 26-132 85 26-132 PQL = Practical quantitation limit R. = Detected in the method blank E - Ouantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 9 of 43 106 Vantage Point drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheatylah.com Level 1 Report v2.1 ICP-MS Client: EMH&T Laboratory ID: PG25041-001 Description: HPE-02 Matrix: Aqueous Date Sampled:0712412014 0715 Date Received:0712512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 . 200.2 200.8 1 07/30/2014 2139 CDF 07/30/2014 1541 52762 CAS Analytical Parameter Number Method Result Q PQL Units Run Copper 7440-50-8 200.8 15 1.0 ug1L 1 Lead 7439-92-1 200.8 3.8 1.0 ug1L 1 Zinc 7440-66-6 200.8 49 10 ug1L 1 PQL = Practical quanblalion limit 6 = Detected in the method blank E = Quantltation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 10 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.rhealylab.com Level 1 Report v2.1 Inorganic non-metals Client: Eli Laboratory ID: PG25041-002 Description: R&D-01 Matrix: Aqueous Date Sampled:0712412014 0800 Date Received: 0712512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prop Date Batch 1 (pH) SM 4500-H B-2011 1 07/28/2014 1727 AAD 52576 1 (TSS) SM 254OD-2011 1 07/29/2014 2035 HMA 52653 1 (SGT - HEM (n) 1664B 1 08/01/2014 0955 JDW 52973 CAS Analytical Parameter Number Method Result Q PQL Units Run pH SM 4500-H B 6.29 su 1 TSS SM 254OD-20 150 5.6 ri 1 SGT - HEM (non -polar material) 1664B NO 4.0 1 1 PQL = Practical quantitation limit 13 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND - Not detected at or above the PQL J = Estmaled result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable. all soil sample analysis are reported on n dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 11 of 43 106 vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Client:EMHBT Laboratory ID: PG25041.002 Description: R&D-01 Matrix: Aqueous Date Sampled:07124/2014 0800 Date Received:07125/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 08/01/2014 0951 PMM2 52948 CAS Anatytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 ug1L 1 Acrylonitri)e 107-13-1 624 ND 50 uglL 1 Benzene 71-43-2 624 ND 5.0 uglL 1 Bromodichloromethane 75-27-4 624 ND 5.0 uglL 1 Bromoform 75-25-2 624 ND 5.0 uglL 1 Bromomethane (Methyl bromide) 74-83-9 624 ND 5.0 uglL 1 Carbon tetrachloride 56-23-5 624 ND 5.0 uglL 1 Chlorobenzene 108-90-7 624 ND 5.0 uglL 1 Chloroethane 75-00-3 624 ND 5.0 uglL 1 2-Chloroethylvinylether 110-75-8 624 ND 10 uglL 1 Chloroform 67-66-3 624 ND 6.0 uglL 1 Chtoromethane (Methyl chloride) 74-87-3 624 ND 5.0 uglL 1 Dibromochloromethane 124-48-1 624 ND 5.0 uglL 1 1,1-Dichloroethane 75-34-3 624 ND 5.0 uglL 1 1,2-Dichloroethane 107-06-2 624 ND 5.0 uglL 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 uglL 1 trans-1,2-Dichloroethene 156-60-5 624 ND 5.0 u91L 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 uglL 1 cis-1,3-Dichloropropene 10061-01-5 624 ND 5.0 uglL 1 trans-1,3-Dichloropropene 10061-02-6 624 ND 5.0 ug1L 1 Ethylbenzene 100-41-4 624 ND 5.0 uglL 1 Methylene chloride 75-09-2 624 ND 5.0 ug1L 1 1.1,2,2-Tetrachtoroethane 79-34-5 624 ND 5.0 uglL 1 Tetrachloroethene 127-18-4 624 ND 5.0 uglL 1 Toluene 108-68-3 624 ND 5.0 uglL 1 1,1,1-Trichloroethane 71-55-6 624 ND 5.0 ug1L 1 1,1,2-Trichloroethane 79-00-5 624 ND 5.0 ug1L 1 Trichloroethene .79-01-6 624 ND 5.0 ug1L 1 Vinyl chloride 75-01-4 624 ND 5.0 uglL 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 106 70-130 Bromofluorobenzene 111 70-130 Toluene-d8 117 70-130 PQL = Practical quantitalion limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < PQL and? MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, atl soil sample analysis are reported on a dry weight basis unless flagged with a Shealy Environmental Services, Inc. Page: 12 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS Client: EMHBT Laboratory ID: PG25041-002 Description: R&D-01 Matrix: Aqueous Date Sampled:0712412014 0800 Date Received:07125/2014 Run Prep Method Analytical Method 1 625 625 Dilution Analysis Date Analyst 1 07/31/2014 2147 DRB1 Prep Date 07128/2014 1453 Batch 52551 CAS Analytical Parameter Number Method Result Q POL Units Run Acenaphthene 83-32-9 625 ND 2.0 uglL 1 Acenaphthylene 208-96-8 625 ND 2.0 ug1L 1 Anthracene 120-12-7 625 ND 2.0 ug1L 1 Benzidine 92-87-5 625 ND 10 ug1L 1 Benzo(a)anth race ne 56-55-3 625 ND 2.0 ug1L 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug1L 1 Benzo(b)fluoranihene 205-99-2 625 ND 2.0 ug1L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 ug1L 1 Benzo(k)Huoranthene 207-08-9 625 ND 2.0 ug1L 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 uglL 1 Butyl benzyl phthalate 85-68-7 625 ND 10 uglL 1 4-Chloro-3-methyl phenol 59-50-7 625 ND 2.0 uglL 1 bis(2-Chloroethoxy)methane 111-91-1 625 ND 2.0 uglL 1 bis(2-Chloroethyl)ether 111-44-4 625 ND 2.0 uglL 1 bis(2-Chloroisopropyl)ether 108-60-1 625 ND 2.0 uglL 1 2-Chloronaphthalene 91-58-7 625 ND _ 2.0 uglL 1 2-Chlorophenol 95-57-8 625 ND 2.0 uglL 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 uglL 1 Chrysene 218-01-9 625 ND 2.0 uglL 1 Dibenzo(a,h)anthracene 53-70-3 625 NO 2.0 uglL 1 1,2-Dichlorobenzene 95-50-1 625 ND 2.0 ug1L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 ug1L 1 1,4-Dichlorobenzene 106-46-7 625 ND 2.0 uglL 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 uglL 1 2,4-Diohlorophenol 120-83-2 625 ND 2.0 uglL 1 Diethylphthalate 84-66-2 625 ND 10 uglL 1 Dimethyl phthalate 131-11-3 625 ND 10 ug1L 1 2,4-Dimethylphenol 105-67-9 625 ND 2.0 ug1L 1 Di-n-butyl phthalate 84-74-2 625 ND 10 uglL 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 10 ug1L 1 2,4-Dinitrophenol 51-28-5 625 ND 10 ug1L 1 2,4-Dinitrotoluene 121-14-2 625 ND 4.0 uglL 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.0 uglL 1 Di-n-octylphthalate 117-84-0 625 ND 10 uglL 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 2.0 uglL 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 ND 10 uglL 1 Fluoranthene 206 44-0 625 ND 2.0 ug1L 1 Fluorene 86-73-7 625 ND 2.0 ug1L 1 Hexachlorobenzene 118-74-1 625 ND 2.0 ug1L 1 Hexachlorobutadiene 87-68-3 625 ND 2.0 t1g1L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 10 ug1L 1 Hexachloroethane 67-72-1 625 ND 2.0 ug1L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 2.0 ug1L 1 Isophorone 78-59-1 625 ND 2.0 ug1L 1 PQL = Practical quamiitation limit 3 = Detected in the method blank E = Ouantitation of compound exceeded the calibration range rf = Out of holding time NO = Not detected at or above the PQL J = Estimated result t PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported an a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 13 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level i Report v2.1 Semivolatile Organic Compounds by GC/MS Client:EMH&T Laboratory ID: PG25041-002 Description: R&D-01 Matrix: Aqueous Date Sampled:0712412014 0800 Date Received:07/2512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 07/31/2014 2147 DRB1 07/28/2014 1453 52551 CAS Analytical Parameter Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 ug1L 1 Nitrobenzene 98-95-3 625 ND 2.0 ug/L 1 2-Nitrophenol 88-75-5 625 ND 4.0 ug1L 1 4-Nitrophenol 100.02-7 625 ND 10 ug1L 1 N-Nitrosodimethyla mine 62-75-9 625 ND 2.0 ug1L 1 N-Nitrasodi-n-propylamine 621-64-7 625 ND 2.0 uglL 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 uglL 1 Pentachlorophenol 87-86-5 625 ND 10 uglL 1 Phenanthrene 85-01-8 625 ND 2.0 uglL 1 Phenol 108-95-2 625 ND 2.0 uglL 1' Pyrene 129-00-0 625 ND 2.0 uglL 1 1,2,4-Trichi orobe nzene 120-82-1 625 ND 2.0 ug1L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 1 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 88 37-129 2-Fluorophenol 82 24-127 Nitrobenzene-d5 82 38-127 Phenol-d5 85 28-128 Terphenyl-d14 81 10-148 2,4,6-Tribromophenol 91 41-144 POL = Practical quantitalion limit 6 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the POL J = Estimated result s POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 14 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Level 1 Report v2.1 Organochlorine Pesticides and PCBs Client:EMH&T Laboratory ID: PG25041-002 Description: R&D-01 Matrix: Aqueous Date Sampted:0712412014 0800 Date Received:07125/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608 608 1 07/31/20141541 MEM 07/28120141521 52557 2 608 608 1 08/01/20140852 MEM 07128/20141521 52557 CAS Analytical Parameter Number Method Result Q PQL Units Run Aldrin 309-00-2 608 ND 0.025 ug/L 1 alpha-BHC 319-84-6 608 ND 0.025 ug/L 1 beta-BHC 319-85-7 608 ND 0.025 ug/L 1 delta-BHC 319-86-8 608 ND 0.025 ug/L 1 gamma-BHC (Lindane) 58-89-9 608 ND 0.025 u91L 1 Chlordane 57-74-9 608 ND 0.25 ug/L 1 4,4'-DDD 72-54-8 608 ND 0.025 ug/L 1 4,4'-DDE 72-55-9 608 ND 0.025 ug/L 1 4,4'-DDT 50-29-3 608 ND 0.025 ug/L 1 Dieldrin 60-57-1 608 ND 0.025 ug/L 1 Endosulfan 1 059-08-8 608 ND 0.025 ug/L 1 Endosulfan 11 33213-65-9 608 ND 0.025 ug/L 1 Endosulfan sulfate 1031-07-8 608 ND 0.025 ug1L 1 Endrin 72-20-8 608 ND 0.025 ug1L 1 Endrin aldehyde 7421-93-4 608 ND 0.025 ug1L 1 Heptachlor 76-44-8 608 ND 0.025 ug1L 1 Heptachlor epoxide 1024-57-3 608 ND 0.025 ug1L 1 Toxaphene 8001-35-2 608 ND 0.25 ug/L 1 Aroclor 1016 12674-11-2 608 ND 0.25 ug1L 2 Aroclor 1221 11104-28-2 608 ND 0.25 ug/L 2 Aroclor 1232 11141-16-5 608 ND 0.25 ug1L 2 Aroclor 1242 53469-21-9 608 ND 0.25 ug1L 2 Aroclor 1248 12672-29-6 608 ND 0.25 ug1L 2 Aroclor 1254 11097-69-1 608 ND 0.25 ug1L 2 Aroclor 1260 11096-82-5 608 ND 0.25 ug1L 2 Surrogate Decachlorobiphenyl Tetrachloro-m-xylene Run 1 Acceptance Run 2 Acceptance Q % Recovery Limits Q % Recovery Limits 21 20-131 26 20-131 62 26-132 96 26-132 PQL = Practical quantitation limit H = Detected in the method blank E - Ouantitalion of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < PQL and - MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 15 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report V2.1 iCP-MS Client:EMH&T Laboratory ID: PG25041.002 Description' R&D-01 Matrix: Aqueous Date Sampled:0712412014 0800 Date Received: 0712512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 07/30/2014 2143 CDF 07/30/2014 1541 52762 CAS Analytical Parameter Number Method Result Q PQL Units Run Copper 7440-50-8 200.8 6.6 1.0 u91L 1 Lead 7439-92-1 200.8 1.9 1.0 ug1L 1 Zinc 7440-66-6 200.8 29 10 ug1L 1 POL = Practical quantitalion limit B = Detected in the method blank E = Quantilation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result < POL and? MDL P = The RPD between two 60 columns exceeds 40% N = Recovery is out of cnterl Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' - Shealy Environmental Services, Inc. Page: 16 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client:EMHBT Laboratory ID: PG25041-003 Description: HPE-01 Matrix: Aqueous Date Sampled:0712412014 0845 )ate Received:07125/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (pH) SM 4500-H B-2011 1 07/28/2014 1727 AAD 52576 1 (TSS) SM 2540D-2011 1 07/29/2014 2035 HMA 52653 1 (SGT - HEM (n) 1664B 1 08/01/2014 0055 JDW 52973 CAS Analytical Parameter Number Method Result Q PQL Units Run pH SM 4500-H B 6.5 su 1 TSS SM 25400-20 10 2.0 mg1L 1 SGT - HEM (non -polar material) 1664E ND 4.0 mg1L 1 PQL = Practical quantitation limit B = Detected in the method blank E = QuantitaGon of compound exceeded the calibration range Fi = Out of holding time No = Not detected at or above the PQL J = Estimated result < Pi and > i P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Shealy Environmental Services, Inc. Page: 17 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v21 Volatile Organic Compounds by GC/MS Client:EMHBT Laboratory ID: PG25041-003 Description: HPE-01 Matrix: Aqueous Date Sampled:0712412014 0845 Date Received:0712512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 08/01/20141015 PMM2 52948 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 ug1L 1 Acrylonitrile 107-131 624 ND 50 ug1L 1 Benzene 71-43-2 624 ND 5.0 ug/L 1 Bromodichloromethane 75-27-4 624 ND 5.0 ug1L 1 Bromoform 75-25-2 624 ND 5.0 ug1L 1 Bromomethane (Methyl bromide) 74-83-9 624 ND 5.0 ug1L 1 Carbon tetrachloride 56-23-5 624 ND 5.0 ug1L 1 Chlorobenzene 108-90-7 624 ND 5.0 ug1L 1 Chloroethane 75-00-3 624 ND 5.0 ug1L 1 2-Chloroethylvinylether 110-75-8. 624 ND 10 ug1L 1 Chloroform 67-66-3 624 ND 5.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5.0 ug1L 1 Dibromochloromethane 124-48-1 624 ND 5.0 ug1L 1 1,1-Dichloroethane 75-34-3 624 ND 5.0 ug1L 1 1,2-Dichloroethane 107-06-2 624 ND 5.0 ug1L 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 ug1L 1 trans-1,2-Dichloroethene 156-60-5 624 ND 5.0 ug/L 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 ug1L 1 cis-1,3-Dichloropropene 10061-01-5 624 ND 5.0 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 624 ND 5.0 ug/L 1 Ethylbenzene 100-41-4 624 ND 5.0 ug/L 1 Methylene chloride 75-09-2 624 ND 5.0 ug1L 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 ug1L 1 Tetrachloroethene 127-18-4 624 ND 5.0 ug1L 1 Toluene 108-88-3 624 ND 5.0 ug1L 1 1,1,1-Trichloroethane 71-55-6 624 ND 5.0 ug1L 1 1,1,2-Trichloroethane 79-00-5 624 ND 50 ug1L 1 Trichloroethene 79-01-6 624 ND 5.0 ug1L 1 Vinyl chloride 75-01-4 624 ND 5.0 ug1L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 111 70-130 BromoFluorobe nzene 112 70-130 Toluene-d8 122 70-130 PQL = Practical quantitation limit 0 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the POL J = Estimated result c POL and? MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of Mena Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 18 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GCIMS Client:EMH&T Laboratory ID: PG25041-003 Description: HPE-01 Matrix: Aqueous Date Sampled:07/2412014 0845 Date Received:0712512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 07/31/2014 2211 DRB1 07/28/2014 1453 52551 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 uglL 1 Acenaphthylene 208-96-8 625 ND 2.0 uglL 1 Anthracene 120-12-7 625 ND 2.0 ug1L 1 Benzidine 92-87-5 625 ND 10 uglL 1 Benz o(a)anthracene 56-55-3 625 ND 2.0 uglL 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug1L 1 Benzo(b)Fluoranthene 205-99-2 625 ND 2.0 ug1L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 ug1L 1 Benzo(k)fluoranthene 207-08-9 625 ND 2.0 ug1L 1 4-Bromophenyi phenyl ether 101-55-3 625 ND 2.0 ug1L 1 Butyl benzyl phthalate 85-68-7 625 ND 10 ug1L 1 4-Chloro-3-methyl phenol 59-50-7 625 ND 2.0 ug1L 1 bis(2-Chloroethoxy)methane 111-91-1 625 ND 2.0 ug1L 1 bis(2-Chloroethyl)ether 111-44-4 625 ND 2.0 ug1L 1 bis(2-Chloroisopropyl)ether 108-60-1 625 ND 2.0 ug1L 1 2-Chloronaphthalene 91-58-7 625 ND 2.0 ug/L 1 2-Chlorophenol 95-57-8 625 ND 2.0 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 u91L 1 Chrysene 218-01-9 625 ND 2.0 ug/L 1 Dibenzo(a,h)anlhracene 53-70-3 625 ND 2.0 uglL 1 1,2-Dichlorobe nzene 95-50-1 625 ND 2.0 ug/L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 uglL 1 1,4-Dichlorobe nzene 106-46-7 625 ND 2.0 uglL 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 uglL 1 2,4-Dichlorophenol 120-83-2 625 ND 2.0 uglL 1 Diethylphthalate 84-66-2 625 ND 10 ug1L 1 Dimethyl phthalate 131-11-3 625 ND 10 ug/L 1 2,4-Dimethylpheno) 105-67-9 625 ND 2.0 uglL 1 Di-n-butyl phthalate 84-74-2 625 ND 10 ug1L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 10 uglL 1 2,4-Dinitrophenol 51-28-5 625 ND 10 uglL 1 2,4-Dinitrotoluene 121-14-2 625 ND 4.0 uglL 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.0 uglL 1 Di-n-octylphthalate 117-84-0 625 ND 10 uglL 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 2.0 uglL 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 ND 10 uglL 1 Fluoranthene 206-44-0 625 ND 2.0 uglL 1 Fluorene 86-73-7 625 ND 2.0 ug1L 1 Hexachlorobenzene 118-74-1 625 ND 2.0 uglL 1 Hexachlorobutadiene 87-68.3 625 ND 2.0 ug1L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 10 uglL 1 Hexachloroethane 67-72-1 625 ND 2.0 ug1L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 2.0 ug1L 1 Isophorone 78-59-1 625 ND 2.0 uglL 1 PQL = Practical quantitalion limit 8 = Detected in the method blank E = Quantization of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and ? MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W Shealy Environmental Services, Inc. Page: 19 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 WWW.shealylab-com Level 1 Reportv2.1 Semivolatile Organic Compounds by GC/MS Client: Ell Laboratory ID: PG25041-003 Description: HPE-01 Matrix: Aqueous Date Sampled:0712412014 0845 Date Received:07125/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 07/31/2014 2211 1 07/28/2014 1453 52551 CAS Analytical Parameter Number Method Result Q PQL Units Run Naphthalene 91-20-3 625 ND 2.0 uglL 1 Nitrobenzene 98-95-3 625 ND 2.0 uglL 1 2-Nitrophenol 88-75.5 625 ND 4.0 uglL 1 4-Nitrophenol 100.02-7 625 N❑ 10 uglL 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 ug1L 1 N-Nitrasodi-n-propylamine 621-64-7 625 NO 2.0 uglL 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 NO 2.0 uglL 1 Pentachlorophenol 87-86-5 625 NO 10 uglL 1 Phenanthrene 85-01-8 625 NO 2.0 uglL 1 Phenol 108-95-2 625 ND 2.0 uglL 1 Pyrene 129-00-0 625 ND 2.0 uglL 1 1,2,4-Trichlorobenzene 120-82-1 625 ND 2.0 uglL 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 uglL 1 Surrogate Run 1 Q % Recovery Acceptance Limits 2-Fluorobiphenyi 91 37-129 2-Fluorophenol 85 24-127 Nitrobenzene-d5 82 38-127 Phenoi-d5 87 28-128 Terphenyl-d 14 86 10-148 2,4,6-Tribromophenol 89 41-144 PQL = Practical quantilation limit B = Detected in the method blank E = Quantization of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > Ml P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a Shealy Environmental Services, Inc. Page: 20 of 43 106 Vantage Point Drive West Columbia, SC 291172 (803) 791-9700 Fax (803) 791-9111 www.shealylab_com Level 1 Report v2.1 Organochlorine Pesticides and PCBs Client:EMH&T Laboratory ID: PG25041-003 Description: HPE-01 Mairix: Aqueous Date Sampled:0712412014 0845 Date Received:07125/2014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 608 608 1 07131120141556 MEM 07128/20141521 52557 2 608 608 1 08101I2014 0904 MEM 07/28/2014 1521 52557 CAS Analytical Parameter Number Method Result Q PQL Units Run Aldrin 309-00-2 608 ND 0.025 ug/L 1 alpha-BHC 319-84-6 608 ND 0.025 ug/L 1 beta-BHC 319-85-7 608 ND 0.025 ug1L 1 delta-BHC 319-86-8 608 ND 0.025 ug1L 1 gamma-BHC (Lindane) 58-89-9 608 ND 0.025 u91L 1 Chlordane 57-74-9 608 ND 0.25 ug1L 1 414'-DDD 72-54-8 608 ND 0-025 ug1L t 4,4'-DDE 72-55-9 608 ND 0-025 ug1L 1 4,4'-DDT 50-29-3 608 ND 0.025 ug1L 1 Dieldrin 60-57-1 608 ND 0.025 ug1L 1 Endosulfan 1 959-98-8 608 ND 0.025 ug]L 1 Endosulfan 11 33213-65-9 608 ND 0.025 uglL 1 Endosulfan sulfate 1031-07-8 608 ND 0.025 ug1L 1 Endrin 72-20-8 608 ND 0.025 ug/L 1 Endrin aldehyde 7421-93-4 60B ND 0.025 ug/L 1 Heptachlor 76-44-8 608 ND 0.025 ug/L 1 Heptachlor epoxide 1024-57-3 608 ND 0.025 ug/L 1 Toxaphene 8001-35-2 608 ND 0.25 ug/L 1 Aroclor 1016 12674-11-2 608 ND 0.25 ug/L 2 Aroclor 1221 11104-28-2 608 ND 0.25 ug/L 2 Aroclor 1232 11141-16-5 608 ND 0.25 ug/L 2 Aroclor 1242 53469-21-9 608 ND 0.25 ug/L 2 Aroclor 1248 12672-29-6 608 ND 0.25 ug/L 2 Aroclor 1254 11097-69-1 608 ND 0.25 ug/L 2 Aroclor 1260 11096-82-5 608 ND 0.25 ug1L 2 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits ❑ecachlorobiphenyl 28 20-131 36 20-131 Tetrachloro-m-xylene 69 26-132 89 26-132 PQL = Practical cluantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range IT = Out of holding time NO = Not detected at or above the PQL J = Estimated result < PQL and? MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 21 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Level s Report v2.1 ICP-MS Client:EMHBT Laboratory ID: PG25041-003 Description: HPE-01 Matrix: Aqueous Date Sampled:0712412014 0845 Date Received: 0712512014 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 07/30/2014 2148 CDF 07/30/2014 1541 52762 CAS Analytical Parameter Number Method Result Q PQL Units Run Copper 7440-50-8 200.8 2.7 1.0 ug1L 1 Lead 7439-92-1 200.8 ND 1.0 ug/L 1 Zinc 7440-66-6 200.8 19 10 ug/L 1 PQL = Practical quantitaticn limit B = Detected in the method blank E = Quanlitation of compound exceeded the calibration range H - Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of crilena Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with SW Shealy Environmental Services, Inc. Page: 22 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v21 QC Summary Shealy Environmental Services, Inc. Page: 23 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.eom Level 1 Report v2.1 Inorganic non-metals - MB Sample ID: PQ52576-001 Matrix: Aqueous Batch:52576 Analvtical Method: SM 4500-H B-2011 Parameter Result pH 5.55 Q pil PQL Units Analysis Date 1 0.000 su 0712812014 1727 PQL = Practical quantltation limit P = The RFD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PCL J = Estimated result < PQL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -oft errors in calculated results Shealy Environmental Services, Inc. Page: 24 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals - Duplicate Sample ID: PG25041-001DU Matrix: Aqueous Batch:52576 Analvtical Method: SM 4500-H B-2011 Sample Amount Result % RPD Parameter (su) Q oil % RPD Limit Analysis Date pH 6.53 6.35 1 2.8 20 07128/20141727 PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result � PQL and > MDL + = RP() is out of criteria Where applicable, all soil samplo analysis are reported on a dry weight hasis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 25 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab,com Level 1 Report v2.1 Sample ID: PQ52653-001 Batch:52653 Analvtical Method: SM 2540D-2011 Parameter TSS Inorganic non-metals - MB Matrix: Aqueous Result Q Dil PQL Units Analysis Date ND 1 1.0 mg/L 07/29/2014 2035 PQL = Practical quarititatlon limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result a PQL and > MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W, Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 26 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheelylab.com Level 1 Report v2.1 Inorganic non-metals - LCS Sample ID: PQ52653-002 Matrix: Aqueous Batch:52653 Analvtical Method: SM 254OD-2011 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q oil % Rec Limit Analysis Date TSS 250 250 1 100 90-110 07/29/2014 2035 a PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PDL and > MOL + = RPD is out of rritena Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 27 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2.1 Inorganic non-metals - MB Sample ID: PQ52973-001 Matrix: Aqueous Batch:52973 Analytical Method: 1664B Parameter SGT - HEM (non -polar material) Result Q Dil PQL Units Analysis Date ND 1 4.0 mg1L 06/0112014 0955 PQL - Practical quantization limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND - Not detected at or above the PQL J = Estimated result a PQL and - MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 28 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reportv2.1 Inorganic non-metals - LC5 Sample ID: P052973-002 Matrix: Aqueous Batch:52973 Analytical Method: 1664B Spike Amount Result % Rec Parameter (mglL) (mglL) Q Dil % Rec Limit Analysis Date SGT - HEM (non -polar material) 20 15 1 75 64-132 08/01/2014 0955 PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and ? MDL + = RPO is out of criteria Where applicable, al4 soil sample analysis are reported on a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 29 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Volatile Organic Compounds by GC/MS - MB Sample ID: P052948-001 Matrix: Aqueous Batch: 52948 Prep Method: 5030E Analvtical Method: 624 Parameter Result Q Dii PQL Units Analysis Date Acrolein ND 1 50 uglL 08/01/2014 0020 Acrylonitrile ND 1 50 uglL 08/01/2014 0020 Benzene ND 1 5.0 uglL 08/01/2014 0020 Bromodichloromethane ND 1 5.0 uglL 08/01/2014 0020 Bromoform ND 1 5.0 ug/L 08/01/2014 0020 Bromomethane (Methyl bromide) ND 1 5.0 ug/L 08/01/2014 0020 Carbon tetrachloride ND 1 5.0 ug/L 08/01/2014 0020 Chlorobenzene ND 1 5.0 ug1L 08/01/2014 0020 Chloroethane ND 1 5.0 ug1L 08/01/2014 0020 2-Chloroethylvinylether N❑ 1 10 11 08/01/2014 0020 Chloroform ND 1 5.0 ug1L 08/01/2014 0020 Chloromethane (Methyl chloride) ND 1 5.0 ug1L 08/01/2014 0020 Dibromochloromethane ND 1 5.0 ug1L 08/01/2014 0020 1,2-Dichloroethane ND 1 5.0 ug1L 08/01/2014 0020 1,1-Dichloroethane ND 1 5.0 ug1L 08101/20140020 trans- 1,2-Dichloroethene ND 1 5.0 uglL 08101/2014 0020 1,1-Dichloroethene ND 1 5.0 uglL 08/01/2014 0020 1,2-Dichloropropene ND 1 5.0 uglL 08/01/2014 0020 trans-1,3-Dichloropropene ND 1 5.0 uglL 08/01/2014 0020 cis-1,3-Dichloropropene ND 1 5.0 uglL 08/01/2014 0020 Ethylbenzene ND 1 5.0 uglL 08/01/2014 0020 Methylene chloride ND 1 5.0 uglL 08/01/2014 0020 1,1,2,2-Tetrachloroethane ND 1 5.0 ug/L 08/01/2014 0020 Tetrachloroethene ND 1 5.0 ug/L 08/01/2014 0020 Toluene ND 1 5.0 ug/L 08/01/2014 0020 1,1,2-Trichloroethane ND 1 5.0 uglL 08/01/2014 0020 1,1,1-Trichloroethane ND 1 5.0 ug/L 08/01/2014 0020 Trichloroethane ND 1 5.0 ug/L 08/01/2014 0020 Vinyl chloride ND 1 5.0 ug/L 08/01/2014 0020 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene ill 70-130 1,2-Dichloroethane-d4 112 70-130 Toluene-d8 119 70-130 POL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < POL and > M17� + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 30 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab,com Level 1 Report v2.1 Volatile Organic Compounds by GC/MS - LCS Sample ID: PQ52948-002 Matrix: Aqueous Batch:52948 Prep Method: 5030B Analytical Method: 624 Spike Amount Result % Rec Parameter (uglL) (ug1L) Q Dil % Rec Limit Analysis Date Acrolein 200 210 1 103 14-175 07/3112014 2309 Acr&nitrile 40 39 1 98 60-130 07/31/2014 2309 Benzene 20 21 1 107 37-151 07/31/2014 2309 Bromodichloromethane 20 22 1 109 35-155 07/31/2014 2309 Bromoform 20 23 1 114 45-169 07/31/2014 2309 Bromomethane (Methyl bromide) 20 23 1 113 1-242 07/31/2014 2309 Carbon tetrachloride 20 24 1 118 71-140 07/31/2014 2309 Chlorobenzene 20 21 1 107 37-160 07/31/2014 2309 Chloroethane 20 22 1 110 14-230 07/31/2014 2309 2-Chloroethylvinylether 20 21 1 106 1-305 07/31/2014 2309 Chloroform 20 22 1 ill 51-138 07/31/2014 2309 Chloromethane (Methyl chloride) 20 21 1 105 1-273 07/31/2014 2309 Dib romochloro methane 20 22 1 109 53-149 07/31/2014 2309 1,2-Dichloroethane 20 22 1 110 49-155 07/31/2014 2309 1,1-Dichloroethane 20 22 1 109 59-155 07/31/2014 2309 trans- l,2-Dichloroethene 20 23 1 113 54-156 07/31/2014 2309 1,1-Dichloroethene 20 23 1 113 1-234 07131/2014 2309 1,2-Dichloropropane 20 21 1 106 1-210 07131/2014 2309 trans-1,3-Dichloropropene 20 19 1 96 17-183 07/31/2014 2309 cis- 1,3-Dichloroprope ne 20 22 1 109 1-227 07/31/2014 2309 Elhylbenzene 20 20 1 102 37-162 07131/2014 2309 Methylene chloride 20 23 1 113 1-221 07/31120142309 1,1,2,2-Tetrachloroethane 20 20 1 99 46-157 07131/2014 2309 Tetrachloroethene 20 22 1 ill 70-130 07131/2014 2309 Toluene 20 21 1 107 47-150 07131/2014 2309 1,1,2-Trichloroethane 20 22 1 108 52-150 07/31/2014 2309 1,1,1-Trichloroethane 20 23 1 115 52-162 07/31/2014 2309 Trichloroethene 20 23 1 113 71-157 07131/2014 2309 Vinyl chloride 20 23 1 115 1-251 07/31/2014 2309 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 113 70-130 1,2-Dichloroethane-d4 110 70-130 Toluene -dB 115 70-130 PC = Practcal quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PCL J = Estimated result � PQL and > MDL = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless tlagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 31 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fox (803) 791-9111 www.shealylab.com Level t Report v2.1 Volatile Organic Compounds by GC/MS - LCSD Sample ID: PQ52948-003 Matrix: Aqueous Batch:52948 Prep Method: 5030E Analvtical Method: 624 Spike Amount Result % Roe % RPD Parameter (ug1L) (uglL) Q Dil %P Roe % RPD Limit Limit Analysis Date Acrolein 200 200 1 102 0.99 14-175 40 07/31/2014 2333 Acrylonitrile 40 37 1 92 6.2 60-130 40 07/31/2014 2333 Benzene 20 22 1 108 0.23 37-151 34.5 07/31/2014 2333 Bromodichloromethane 20 22 1 110 0.99 35-155 32 07/31/2014 2333 Bromoform 20 23 1 116 2.2 45-169 27 07/31/2014 2333 Bromomethane (Methyl bromide) 20 22 1 110 2.9 1-242 50 07/31/2014 2333 Carbon tetrachloride 20 23 1 113 4.2 71-140 26 07/31/2014 2333 Chlorobenzene 20 22 1 108 1.5 37-160 31.5 07/31/2014 2333 Chloroethane 20 21 1 106 3.7 14-230 57 07/31/2014 2333 2-Chloroethylvinylether 20 22 1 109 3.2 1-305 40 07/31/2014 2333 Chloroform 20 22 1 109 2.0 51-138 30.5 07/31/2014 2333 Chioromethane (Methyl chloride) 20 20 1 99 5.9 1-273 50 07/3112014 2333 Dibromochloromethane 20 22 1 110 0.70 53-149 30.5 07131]2014 2333 1,2-Dichloroethane 20 21 1 106 3.5 49-155 30 07/31/2014 2333 1,1-Dichloroethane 20 21 1 106 3.3 59-155 25.5 07/31/2014 2333 trans- 1,2-Dichloroethene 20 22 1 110 3.0 54-156 28.5 07/31/2014 2333 1,1-Dichloroethene 20 22 1 Ill 2.5 1-234 45.5 07/31/2014 2333 1,2-Dichloropropane 20 22 1 108 1.4 1-210 50 07/31/2014 2333 trans- l,3-Dichloropropene 20 19 1 97 1.3 17-183 52 07/31/2014 2333 cis-1,3-Dichloropropene 20 22 1 110 1.0 1-227 50 07/31/2014 2333 Ethylbenzene 20 21 1 107 5.2 37-162 37.5 07/31/2014 2333 Methylene chloride 20 22 1 110 2.5 1-221 37 07/31/2014 2333 1,1,2,2-Tetrachloroethane 20 21 1 104 5A 46-157 37 07/31/2014 2333 Tetra chloroethene 20 23 1 115 3.0 70-130 25 07/31/2014 2333 Toluene 20 22 1 111 3.6 47-150 24 07/31/2014 2333 1,1,2-Trichloroethane 20 22 1 108 0.18 52-150 27.5 07/31/2014 2333 1.1.1-Trichloroethane 20 22 1 112 2.4 52-162 23 07/3112014 2333 Trichloroethene 20 24 1 118 4.2 71-157 33 07/31/2014 2333 Vinyl chloride 20 21 1 106 7.9 1-251 50 07/3112014 2333 Surrogate q % Roe Acceptance Limit Bromofluorobenzene 112 70-130 1,2-Dichloroethane-d4 108 70-130 Toluene-d8 116 70-130 PDL - Practical quantilation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND - Nat detected at or above the PQL J = Estimated resW t PQL and - MDL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 32 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.ccm Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS - MB Sample ID: P052551-001 Matrix: Aqueous Batch: 52551 Prep Method: 625 Analytical Method: 625 Prep Date: 07/28/2014 1453 Parameter Result Q Dil PQL Units Analysis Date 1,2,4-Trichlorobe nzene ND 1 2.0 ug1L 07131/20141858 1,2-Dichlorobenzene ND 1 2,0 u911- 07131/20141858 1,2-Diphenylhydrazine(as a7obenzene) ND 1 2.0 ug1L 07/31/2014 1858 1,3-Dichloroben7ene ND 1 2.0 ug1L 07131/20141858 1,4-Dichlorobenzene ND 1 2.0 ug1L 07131/20141858 2,4,6-Trichlorophenol ND 1 2.0 ug1L 07/31/20141858 2,4-Dichlorophenol ND 1 2.0 ug1L 07/31/20141858 2,4-Dimethylphenol ND 1 2.0 11 07/31/2014 1858 2,4-Dinitrophenol NO 1 10 ug1L 07131120141858 2,4-Dinitrotoluene ND 1 4.0 ug1L 07131/20141858 2,6-Dinitrotoluene ND 1 4.0 uglL 07131/20141858 2-Chloronaphthalene ND 1 2.0 uglL 07131120141858 2-Chlorophenol ND 1 2.0 ug1L 07131120141858 2-Nitrophenol ND 1 4.0 uglL 07131120141858 3,3'-Dichlorobenzidine ND 1 10 i lL 07131120141858 4,6-Dinitro-2-methylphenol ND 1 10 uglL 07/31120141858 4-Bromophenyt phenyl ether ND 1 2.0 uglL 07/3112014 1858 4-Chloro-3-methyl phenol ND 1 2.0 uglL 07/31/2014 1858 4-Chlorophenyi phenyl ether ND 1 2.0 uglL 07/31/2014 1858 4-Nitrophenol ND 1 10 ug1L 07131/20141858 Acenaphthene ND 1 2.0 uglL 07/31120141858 Acenaphthylene ND 1 2.0 ug1L 07131/20141858 Anthracene ND 1 2.0 uglL 07131/20141858 Benzidine ND 1 10 ug1L 07131120141858 Benzo(a)anthracene ND 1 2.0 uglL 07131/20141858 Benzo(a)pyrene ND 1 2.0 uglL 07131120141858 Benzo(b)fluoranthene ND 1 2.0 uglL 07131/20141858 13enzo(g,h,i)perylene ND 1 2.0 11 07/31120141858 Benzo(k)fluoranthene ND 1 2.0 ti 07/31/20141858 bis(2-Chloroethoxy)methane ND 1 2.0 uglL 07/31120141858 bis(2-Chloroethyl)ether ND 1 2.0 uglL 07/31120141858 bis(2-Chloroisopropyl)ether ND 1 2.0 uglL 07131120141858 bis(4-Ethyl hexyl)phthalate ND 1 10 uglL 07131120141858 Butyl benzyl phthalate ND 1 10 uglL 07/31/2014 1858 Chrysene ND 1 2.0 uglL 07/31/20141858 Di-n-butyl phthalate ND 1 10 uglL 07/3112014 1858 Di-n-octylphthatale ND 1 10 ug1L 07/31/20141858 Dibenzo(a,h)anthracene ND 1 2.0 ug1L 07/31/20141858 D iethylphtha late ND 1 10 ug1L 07131/20141858 Dimethyl phthalate ND 1 10 ug1L 07/31/2014 1858 Fluoranthene ND 1 2.0 ug1L 07/31/20141858 Fluorene ND 1 2.0 uglL 07131/20141858 Hexachlorobenzene ND 1 2.0 ug1L 07131120141858 Hexachlorobutadiene ND 1 2.0 uglL 07131/20141858 PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and - MDL * = RPD is out of critera Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 33 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylob.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS - MB Sample ID: P052551-001 Matrix: Aqueous Batch:52551 Prep Method: 625 Analytical Method: 625 Prep Date: 07/28/2014 1453 Parameter Result Q Dil PQL Units Analysis Date Hexachlorocyclopentadiene NO 1 10 ug1L 07/31/20141858 Hexachloroethane NO 1 2.0 ug1L 07/31120141858 Indeno(1,2,3-c,d)pyrene NO 1 2.0 ug1L 07/31/20141858 Isophorone NO 1 2.0 ug1L 07/31120141858 N-Nitrosodi-n-propylamine NO 1 2.0 ug1L 07/31/20141858 N-Nitrosodimethylamine NO 1 2.0 uglL 07131120141858 N-Nitrosodiphenylamine (Diphenylamine) NO 1 2.0 uglL 07/31/2014 1858 Naphthalene NO 1 2.0 uglL 07131/20141858 Nitrobenzene NO 1 2,0 ug1L 07131/20141858 Pentachlorophenol NO 1 10 ug1L 07/31/20141858 Phenanthrene NO 1 2.0 uglL 07131/20141858 Phenol NO 1 2.0 ug1L 07131/20141858 Pyrene NO 1 2.0 ug1L 07/31/20141858 Acceptance Surrogate ° Q /° Rec Limit 2,4,6-Tribromophenol 76 41-144 2-Fluorobiphenyl 91 37-129 2-Fluorophenol 84 24-127 Nitrobenzene-d5 85 38-127 Phenol-d5 86 28-128 Terphenyl-d14 90 10-148 PQL = Practical quanfitation limlt P = The RPD between two GC columns exceeds 4D % N = Recovery is cut of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > ME7L + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 34 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: PQ52551-002 Matrix: Aqueous Batch: 52551 Prep Method: 625 Analytical Method: 625 Prep Date: 07/28/2014 1453 Spike Amount Result % Rec Parameter (uglL) (ug1L) Q Dil % Rec Limit Analysis Date 1,2,4-Trichlorobenzene 20 16 1 80 44-142 07/31/2014 1923 1,2-Dichlorobenzene 20 16 1 81 32-129 07/31/2014 1923 1,2-Diphenylhydrazine(as azobenzene) 20 17 1 84 30-130 07/31/2014 1923 1,3-Dichlorobenzene 20 16 1 78 0-172 07/31/2014 1923 1,4-Dichlorobe nzene 20 16 1 79 20-124 07/31/2014 1923 2,4,6-Trichlorophenot 20 17 1 85 37-144 07131/20141923 2,4-Dichlorophenol 20 ' 18 1 88 39-135 07131/20141923 2,4-Dimethylphenol 20 18 1 92 32-119 07131120141923 2,4-Dinitrophenol 100 76 1 76 0-191 07131/20141923 2,4-Dinitrotoluene 40 36 1 90 39-139 07/31120141923 2,6-Dinitrotoluene 40 35 1 89 50-158 07131/20141923 2-Chloronaphthalene 20 14 1 70 60-118 07131/20141923 2-Chlorophenol 20 17 1 87 23-134 07131120141923 2-Nitrophenol 40 34 1 85 29-182 07131/20141923 3,3'-Dichlorobenzidine 40 24 1 61 0-262 07131120141923 4,6-Dinitro-2-methylphenol 100 65 1 65 0-181 07131120141923 4-Bromophenyl phenyl ether 20 15 1 77 53.127 07/31/2014 1923 4-Chloro-3-methyl phenol + 20 18 1 91 22-147 07/31/2014 1923 4-Chlorophenyl phenyl ether 20 16 1 78 25-158 07/31/2014 1923 4-Nitrophenol 100 92 1 92 0-132 07/31120141923 Acenaphthene 20 18 1 88 60-132 07/31120141923 Acenaphthylene 20 18 1 90 54-126 07/31/2014 1923 Anthracene 20 17 1 84 43-118 07/31120141923 Benzidine 40 4.9 1 12 1-150 07/31120141923 Benzo(a)anthracene 20 16 1 79 42-133 07/31/2014 1923 Benzo(a)pyrene 20 14 1 70 17-163 07131120141923 Benzo(b)fluoranthene 20 17 1 83 24-159 07/31/2014 1923 Benzo(g,h,i)perylene 20 13 1 65 0-219 07/31/2014 1923 Benzo(k)fluoranthene 20 17 1 85 11-162 07/31/2014 1923 bis(2-Chloroethoxy)methane 20 18 1 91 33-184 07/31120141923 bis(2-Chloroe1hyl)ether 20 18 1 88 12-158 07131/20141923 bis(2-Chloroisopropyl)ether 20 18 1 92 36-166 07131/20141923 bis(2- Ethylhexyl) phthal ate 20 16 1 82 8-158 07131120141923 Butyl benzyl phthalate 20 17 1 84 0-152 07/31/2014 1923 Chrysene 20 16 1 79 17-168 07131120141923 Di-n-butyl phthalate 20 18 1 92 1-118 07/31/2014 1923 Di-n-octylphthatate 20 17 1 83 4-146 07/31120141923 Dibenzo(a,h)anthracene 20 14 1 71 0-227 07131120141923 Diethylphthalate 20 17 1 85 0-114 07131/20141923 Dimethyl phthalate 20 17 1 87 0-112 07/3112014 1923 Fluoranthene 20 18 1 88 26-137 07/31120141923 Fluorene 20 17 1 83 59-121 07131/20141923 Hexachlorobenzene 20 15 1 77 0-152 07131120141923 Hexachlorobutadiene 20 15 1 76 24-116 07/31120141923 POL = Practical quantilalion limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the POL J = Estimated result < POL and > MOL • = RPD is out of criteria More applicable, all soil sample analysis are reported on a dry weight basis unless nagged with a Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 35 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: PQ52551-002 . Matrix: Aqueous Batch: 52551 Prep Method: 625 Analytical Method: 625 Prep Date: 07/28/2014 1453 Spike Amount Result % Rec Parameter (L lLj (L lLj Q Dil % Rec Limit Analysis Date Hexachlorocyclopentadiene 100 36 1 36 1-150 07131/20141923 Hexachloroethane 20 16 1 79 40-113 07131120141923 Indeno(1,2,3-c,d)pyre ne 20 14 1 70 0-171 07131120141923 Isophorone 20 18 1 91 21-196 07/31120141923 N-Nitrosodi-n-propylamine 20 18 1 91 0-230 07/31120141923 N-Nitrosodimethylamine 20 16 1 81 1-150 07/31/20141923 N-Nitrosod iphenylamine (Diphenylamine) 20 19 1 97 1-150 07/3112014 1923 Naphthalene 20 17 1 84 21-133 07134120141923 Nitrobenzene 20 17 1 86 35-180 07/31120141923 Pentachlorophenol 100 84 1 84 14-176 07/31/20141923 Phenanthrene 20 17 1 83 54-120 07/31/20141923 Phenol 20 18 1 90 5-112 07/31/20141923 Pyrene 20 16 1 80 52-115 07/31/20141923 Acceptance Surrogate Q % Rec Limit 2,4,6-Tribromophenol 86 41-144 2-Fluorobiphenyl 87 37-129 2-Fluorophenol 86 24-127 Nitrobenzene-d5 89 38-127 Phenol-d5 88 28-128 Terphenyl-d 14 85 10-148 PQL = Practical quantitation limit P = The RP❑ between two GC columns exceeds 40% N = Recovery is out of Mena ND = Not detected at or above the PQL J - Estimated result < POL and > MDL • = RPQ is out of criteria Where applicable, all soil sample analysis are reportec on a dry weight basis unless flagged with a' W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 36 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 wvvw.shealylab.com Level 1 Report v2.1 Semivolatile Organic Compounds by GC/MS - MS ' Sample ID: PG25041-001MS Matrix: Aqueous Batch: 52551 Prep Method: 625 Analytical Method: 625 Prep Date: 07/28/2014 1453 Sample Spike Amount Amount Result % Rec Parameter (ug1L) (uglL) (ug1L) Q ❑il % Rec Limit Analysis Date Acenaphthene NO 20 19 1 94 60-432 07/31/2014 2123 Acenaphthylene NO 20 18 1 89 54-126 07/31/2014 2123 Anthracene NO 20 14 1 72 43-118 07/31/2014 2123 Benzidine NO 40 2.5 1 6.4 1-150 07/31/2014 2123 Benzo(a)anth race ne NO 20 11 1 53 42-133 07/31/2014 2123 Benzo(a)pyrene NO 20 5.9 1 29 17-163 07/31/2014 2123 Benzo(b)fluoranthene NO 20 8.5 1 42 24-159 07/31/2014 2123 Benzo(g,h,i)perylene NO 20 6.1 1 30 0-219 07/31/2014 2123 Benzo(k)fluoranthene NO 20 8.8 1 44 11-162 07/31/2014 2123 4-Bromophenyl phenyl ether NO 20 16 1 79 53-127 07/31/2014 2123 Butyl benzyl phthalate NO 20 14 1 72 0-152 07/31/2014 2123 4-Chloro-3-methyl phenol NO 20 20 1 98 22-147 07/31/2014 2123 bis(2-Chl oroe thoxy) methane NO 20 19 1 96 33-184 07/31/2014 2123 bis(2-Chloroethyl)ether NO 20 19 1 94 12-158 07/31/2014 2123 bis(2-Chloroisopropyl)elher NO 20 19 1 95 36-166 07/31/2014 2123 2-Chloronaphthalene NO 20 15 1 73 60-118 07131/2014 2123 2-Chlorophenol NO 20 18 1 92 23-134 07/31/2014 2123 4-Chlorophenyl phenyl ether ND 20 16 1 80 25-158 07131/2014 2123 Chrysene NO 20 9.3 1 46 17-168 07/31/2014 2123 Dibenzo(a,h)anthracene NO 20 5.3 1 27 0-227 07/31/2014 2123 1,2-Dichlorobe nzene NO 20 17 1 86 32-129 07/31/2014 2123 1,3-Dichlorobenzene NO 20 17 1 83 0-172 07/31/2014 2123 1,4-Dichlorobenzene NO 20 17 1 84 20-124 07/31/2014 2123 3,3'-Dichlorobenzidine NO 40 NO 1 0,00 0-262 07131/2014 2123 2,4-Dichlorophenol NO 20 19 1 94 39-135 07131/2014 2123 Di ethylphtha late ND 20 18 1 91 0-114 07/31/2014 2123 Dimethyl phthalate NO 20 18 1 91 0-112 07/31/2014 2123 2,4-Dimethylphenol NO 20 23 1 114 32-119 07/31/2014 2123 Di-n-butyl phthalate NO 20 17 1 86 1-118 07/31/2014 2123 4,6-Dinitro-2-methylphenol NO 100 62 1 62 0-181 07/31/2014 2123 2,4-Dinitrophenol NO 100 75 1 75 0-191 07/31/2014 2123 2,4-Dinitrotoluene NO 40 37 1 94 39-139 07/31/2014 2123 2,6-Dinitrotoluene NO 40 38 1 94 50-158 07/31/2014 2123 Di-n-octylphthalate NO 20 5.3 1 27 4-146 07/31/2014 2123 1,2-Diphenylhydrazine(as azobenzene) NO 20 17 1 84 30-130 07/31/2014 2123 bis(2-Ethylhexyl)phthalate NO 20 5.5 1 27 8-158 07/31/2014 2123 Fluoranthene NO 20 16 1 82 26-137 07/31/2014 2123 Fluorene NO 20 17 1 86 59-121 07/31/2014 2123 Hexachlo robe nze ne NO 20 14 1 68 0-152 07/31/2014 2123 Hexachlorobutadiene NO 20 16 1 78 24-116 07/31/2014 2123 Hexachlorocyclopentadiene NO 100 44 1 44 1-150 07/31/2014 2123 Hexachloroethane NO 20 17 1 83 40-113 07/31/2014 2123 Indeno(1,2,3-c,d)pyrene NO 20 5.9 1 30 0-171 07/31/2014 2123 Isophorone NO 20 19 1 95 21-196 07/31/2014 2123 POL = Practical quantitation limit P = The RPD between two CC columns exceeds 40% N - Recovery is out of cnteria ND = Not detected at or above the PQL J = Estimated result - PQL and > MDL + - RPD is out of critena Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc Page: 37 of 43 106 Vantage Point Drive West Columbla, SC 29172 (803) 791.9700 Fax (803) 791-91 i l www.shealylab.com Level 1 Report v2.1 Semivolatiie Organic Compounds by GC/MS - MS Sample ID: PG25041 -001 MS Matrix: Aqueous Batch:52551 Prep Method: 625 Analytical Method: 625 Prep Date: 07/28/2014 1453 Sample Spike Amount Amount Result %Rec Parameter (ug/L) (u91L) (ii Q Dil % Rec Limit Analysis Date Naphthalene ND 20 18 1 88 21-133 07/31/2014 2123 Nitrobenzene ND 20 19 1 96 35-180 07/31/2014 2123 2-Nitrophenol ND 40 36 1 91 29-182 07l3112014 2123 4-Nitrophenol ND 100 93 1 93 0-132 07/31/2014 2123 N-Nitrosodimethylamine ND 20 18 1 91 1-150 07l31120142123 N-Nitrosodi-n-propylamine ND 20 19 1 95 0-230 07/31/2014 2123 N-Nitrosodiphenylamine(Diphenylamine) ND 20 9.6 1 48 1-150 07/31120142123 Pentachlorophenol ND 100 94 1 94 14-176 07/31/2014 2123 Phenanthfene ND 20 17 1 84 54-120 07/31/2014 2123 Phenol ND 20 19 1 95 5-112 07/3112014 2123 Pyrene ND 20 15 1 75 52-115 07131/20142123 1,2,4-Trichlorobenzene ND 20 17 1 84 44-142 07/31120142123 2,4,6-Tiichlorophenol ND 20 18 1 91 37-144 07/31/2014 2123 Acceptance Surrogate ° Q /° Rec Limit 2-Fluorobiphenyl 90 37-129 2-Fluorophenol 90 24-127 Nitrobenzene-d5 95 38-127 Phenol-d5 91 28-128 Terphenyl-d14 43 10-148 2,4,6-Tribromophenol 95 41-144 PQL = Practical quartitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > i + = RPD is out of onions Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W, Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 38 of 43 106 Vantage Point Drive West Columbia, SC 29472 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Organochlorine Pesticides and PCBs - MB Sample ID: P052557-001 Matrix: Aqueous Batch: 52557 Prep Method: 608 Analytical Method: 608 Prep Date: 07/28/2014 1521 Parameter Result Q Dil PQL Units Analysis Date 4,4'-DDD ND 1 0.025 ug1L 07/31120141457 4,4'-DDE ND 1 0.025 ug/L 07131120141457 4,4'-DDT ND 1 0.025 ug1L 07/31/2014 1457 Aldrin ND 1 0.025 ug1L 07131120141457 alpha-BHC ND 1 0.025 ug1L 07/31/2014 1457 Aroclor 1016 ND 1 0.25 ug1L 08/01/2014 0000 Aroclor 1221 ND 1 0.25 ug/L 08/01/2014 0000 Aroclor 1232 ND 1 0.25 ug1L 08/01/2014 0000 Aroclor 1242 ND 1 0.25 ug/L 08/01/2014 0000 Aroclor 1248 ND 1 0.25 ug/L 08/01/2014 0000 Aroclor 1254 ND 1 0.25 ug/L 08/01/2014 0000 Aroclor 1260 ND 1 0.25 ug/L 08/01/2014 0000 beta-BHC ND 1 0.025 ug1L 07/31/2014 1457 Chtordane ND 1 0.25 ug1L 07/31/2014 1457 delta-BHC ND 1 0.025 ug/L 07/31120141457 Dieldrin ND 1 0.025 ug1L 07/31120141457 Endosulfan I ND 1 0.025 ug1L 07/31/2014 1457 Endosulfan II ND 1 0.025 ug1L 07/31/2014 1457 Endosulfan sulfate ND 1 0,025 uglL 07/31/2014 1457 Endrin ND 1 0,025 ug1L 07/31/2014 1457 Endrin aldehyde ND 1 0.025 ug1L 07/31/2014 1457 gamma-BHC (Lindane) ND 1 M025 ug1L 07/31/2014 1457 Heptachlor ND 1 0.025 ug11- 07/31120141457 Heptachlor epoxide ND 1 0.025 ug1L 07/31/2014 1457 Toxaphene ND 1 0.25 ug1L 07131/20141457 Surrogate Q % Rec Acceptance Limit Decachlorobiphenyl 75 20-131 Tetrachloro-m-xylene 68 26-132 PQL = Practical quantitation limit P = The RPI) between two GC columns exceeds 40% N = Recovery is cut of criteria NO = Not detected at or above the PQL J = Estimated result - PQL and > MIL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "VV' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 39 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Repon v2 1 Organochlorine Pesticides and PCBs - LCS Sample ID: PQ52557-002 Matrix: Aqueous Batch: 52557 Prep Method: 608 Analytical Method: 608 Prep Date: 07/28/2014 1521 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 4,4'-DDD 0.50 0.44 1 87 31-141 07131/20141512 4,4'-DDE 0.50 0.49 1 99 30-145 07131/20141512 4,4'-DDT 0.50 0.53 1 106 25-160 07131/20141512 Aldrin 0.50 0.49 1 97 42-122 07131/20141512 alpha-BHC 0.50 0.40 1 80 37-134 07131120141512 beta-BHC 0.50 0.47 1 95 17-147 07/31/2014 1512 delta-BHC 0.50 0.45 1 90 19-140 07/31/2014 1512 Dieldrin 0.50 0.51 1 101 36-146 07/31/2014 1512 Endosulfan 1 0.50 0,49 1 98 45-153 07/31/2014 1512 Endosulfan 11 0.50 0,48 1 96 1-202 07/31/2014 1512 Endosulfan sulfate 0.50 0,47 1 94 26-144 07/31/2014 1512 Endrin 0.50 0,55 1 111 30-147 07/31/2014 1512 Endrin aldehyde 0.50 0.36 1 71 50-130 07/31/2014 1512 gamma-BHC (Lindane) 0.50 0.44 1 88 32-127 07/31/2014 1512 Heptachlor 0.50 0.48 1 97 34-111 07131/20141512 Heptachlor epoxide 0.50 0,46 1 91 37-142 07/31/2014 1512 Surrogate Q %Rec Acceptance Limit Decachlorobiphenyl 76 20-131 Tetra chloro-m-xylene 76 26-132 PQL = Practical quanWalion limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL, J = Estimated result � PQL and - MOL + = RPD is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 40 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 WWW.shealylab,com Level 1 Report v2.1 [CP-MS - MB Sample ID: PQ52762-001 Matrix: Aqueous Batch'52762 Prep Method: 200.2 Analytical Method: 200.8 Prep Date: 07/30/2014 1541 Parameter Result Q Dil PQL Units Analysis Date Copper ND 1 1.0 ug1L 07/30/2014 2124 Lead ND 1 1.0 ug1L 07/30/2014 2124 Zinc ND 1 10 ug/l_ 07/30/2014 2124 PQL = Praclioal quanLtation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J - Estimated result < P4L and > MDL * = RPD is out of criteria More applicable, all sch sample analysis are reported on a dry weight basis unless flagged with a "W Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 41 of 43 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2,1 4 4; , ICP-MS - LCS Sample ID: P052762-002 Matrix: Aqueous Batch: 52762 Prep Method: 200.2 Analytical Method: 200.8 Prep Date: 07/30/2014 1541 Spike Amount Result % Rec Parameter (ug1L) (uglL) a Dil % Rec Limit Analysis Date Copper 100 100 1 104 85-115 07/30/2014 2129 Lead 100 99 1 99 85-115 07/30/2014 2129 Zinc 100 100 1 103 85-115 07/30/2014 2129 PQL = Practical quantitation limit P = The RPD between :wo GC columns exceeds 40% N = Recovery is out of criteria ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out or criteria Where applicable, al} soil sample anatysis are reported on a dry weight basis unless flagged wAh a "W" Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. Page: 42 of 43 106 Vantage Point Drive West Columbia, SC 29172 (603) 791-9700 Fax (803) 791-9111 wwwrshealylab.com Level 1 Reportv2.1 ICP—MS — LCSD 's' Sample ID: PQ52762-003 Matrix: Aqueous Batch: 52762 Prep Method: 200.2 Analytical Method: 200.8 Prep Date: 07/30/2014 1541 Spike Amount Result % Roe % RPD Parameter (ug1L) (ug1L) Q ❑il % Rec % RPD Limit Limit • Analysis Date Copper 100 100 1 103 0.58 85-115 20 07/3012014 2134 Lead 100 100 1 101 1.4 85-115 20 07I3012D14 2134 Zinc 100 100 1 103 0.39 85-115 20 0713012D14 2134 PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria NU = Not detected at or above the PQL J = Estimated result < PQL and n MDL + = RPO is out of criteria Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc Page: 43 of 43 106 Vantage Point Drive West COurnbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 eChaim of Custody Record Shealy Environmental Servic;es,.lnc. 108 Vantage Point Drive. West Columbia, South Carolina 29172 Telephone No, (800)791-970D Fax No. (803)791-9M wWW 1AIt1Cilykab,=T1 Number 33098. CCiarti f� riapoR tq qontact >4 SpmFler (Plmt!!d Name) Q Wt9 1 �i s< i4if.F�`� Talephano No. l Fax No.1 Email ftjt M No. Pago Clly S s Zip Code 6 74 Preservefive 1.Unraz 4.e1NU3 ? ttnOm zlfoom+ZrtM1 5.xCL 1.H2904 6.ttdTft, Z. — uumb9rnlCorltahars 4 t 1i I k I 'a V4 183t2o Poe heiruclioneanh* Frq'aat Name / . 3' I I I I jL -• Praservnliaa �f1F1 fup,}�ryt I I til lI F1Pl �] ❑ ..� �„ �O Prof 1 rQ i( Pe� .ONum� 0 � 1ir6t GYP 4Y� T315 BPmplO lr} i iiREPG26041Cripli6R iConloinars'orpacl�shp wyDo eoreil19iedwl+xleTla; Cate Tlma . - 0 2- MF ' I .9,1 v/ ✓ �' �'' � ,�' �/ ,/ d - A f It -ill &0 C -v- Ve ✓ ✓ ; I I TundTtrna Raquirrtl (PrierI.aQaFpw:al rarwind iar expedtedTAI) 2,C . F4ush pipuw udf `3ampk3 Ul iwaol a Ratun to C' ml tY ' aal t W QC Reg0temurft (Sootily)P09aVa Hazard ldenditallon .dJonJierese r,)Pra nmAkle C+SNn Wmt aPubmi AlflIlflc%n 1, a r ? Doi Zp15�f1 Time 1, o4L- Receive ante 7 Time y 2 2. Holin.Tulrarod try O' rT TJ �. kec � �- ' aataJ. l Time 3. RefinqulfihAd Rain Time 3. rei Reved by f3eto Time 4. RebnntOW by Onto Time' 4. t TY ROAeive TI1�� .Nate: All >samplcs are retained for six week$ from receipt LAa unless other arran emento Oro mdo a. U5E Y J Recalodonl (ChIO) '6 oa Clio clwPaak 1pawipt 7emp, J�c Ta Blank o Y r pdj 5•E N VTI IY C_ 0 (n SHEALY ENVIRONMENTAL SERVICES, INC. ' ea S.-n;=kv- Uo">rmaar Nor. F-f1DCt ti Merw(p I$ pa:r t of I WgpbOm nave 9'_i'i7aI4 t7rrrweF) - 11MV14 Sample Receipt Checklist (SRC Client_ GO 1�_4 ` Cooler Inspected by.'daw: f1�. Lot M {, Q S 01 Means of rcmpt: SESI ❑ Client ❑ UPS ❑ TedEx ❑ AirbarIlc Fxp ❑ Olhcr Yes Na i7 I 1. 'M-re seals present on the emler? Yes No ❑ I NA 2. N cu-qWy seals were pmncnt, were thU irtm--t and unbrulizn? Cooler IDo'Orininal 4mperafure upon remprMerived (corrected) temps Lure upon receipt. Meth l: ❑ Tmupr"tu�� ak Apictst &odes lR Gktn Q]: 43 1R Caun'C.orrMtinn FmW .1-f6-1 aC -Method of c wlant: F-n-et Iw Blue I'm Dry lee Nano Yes ❑ No ❑ NA Od 3. If temperature of any cooler exceeded 6.0°C, was Project Manager notified? PM nonfood by SRC, phow, now (circle one), other (For coolers received via commercial courier, P1rfs are to be notifwd immediate Yes ❑Ko ❑ NA _ d_ rs the commercial couriers packmg s4 at=hod to this form? Yes Na _ Were roccdures (rcl" ishcad,�c¢6%Acd) failowold? Yes tr3n ❑ NA Sa WerC sx Mlcs relinquished by client to conimer,cial courice? Yes ❑ 6_ Were =-n le Ms listed on the COC? Yes VIO❑ 7_ Were sample 1Ds Listed on all sarn k conWfms? Yes ❑ 9. Was collection date & time lWcd on the COU Yes X. ❑ 9. Was c-Mcction date & time listed on all S8 to oomait ? Yes o ❑ 10_ Dial all c rouainer lnhe) inforilil (ID, date, time) agree with the COC? Yes o ❑ 11. Wem tests to be perforil Listed on the COO? Yea n ❑ 12. DW all samples arri-re in the Ta container fru c ach test? Yes Of 'o ❑ 13_ Did all cootainers airnre in goM corms Lion (unbroken, lids on, etc_ j7 Yes Ef Na ❑ 14. Was adegurte EM& wohune available? Y� ❑ No �/ 15. W= all samples rcccivcd within Yz the holding tia= or 49 hcnas, whichcVcr comes fist? Yes ❑ No 16. Were any samples co=inem mi;mn ? Yew ❑ -KO—al 1 17. Were there any excess samples not listed on COC? Yes QlNe V NA ❑ IA. Wrtu fmbblet: in dianic-mr) is as VOA vials? Yea No ❑ NA ❑ 19.'.e.'e w all ntetals.'()&WHEMinutrieur samples reeci%-ed at a pH of<2? Yex ❑ No ❑ NA M, there all gmnidc and.'or sulfide samples mucivud at t3 pH >12'' Yes ❑ No ❑ NA 21. Were all applicable NH3.gXNicsaaitWphcnol (<U.2mgeL) samples free -of residual chlorine? Ycy © No ❑ NA 22. Were collemon teqperahucs documented on the COC for NC samples? Yes ❑ No ❑ NA 23. Were client wmarkvrc ucstl; (i.c. rctlucstcd d&tkw, MSMSD destiguatioas, ell CO�tr7A9R3bcd fivm the COC into the C+lti mtofi sextFon itl LIMS2 Ytss [INo JZ 24, Was the qaotic auntber used taker: From the coatlAll ' MCI? S=ple Presrtwmtion (Must be wmpbmd for any sampWs) incorrectly prml air with hea&pam) SaMPlr(s) were received is emectly presm-ed and were adjusted acwnliaox in sample receivin u ith (]%SO4,ILN03 C N 014 USiUg SK # Sample(s) were received with hnhbles >6 ram in dll sauTLe(s t4= received with TRC ='4.2 M&I (If #21 is N101 -- SC Drinking Water Project Sample(s) pH vaifted to be > 2 by D—aw. S le(s) were not rmei%vd at a pH of {2 and were adjusted acc on irOy nosing OR$ Sample labc6 aMid try: Verified . Bate= C` M11111Cnts: Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2,1 WCDENR' North Carolina Department of Environment and Natural Resources Division of Energy, Mineral, and Land Resources Land Quality Section Pat McCrory, Governor July 31, 2014 House of Raeford Farms, Inc. Jimmy Peak, Complex Manager PO Box 40 Rose Hill, NC 28548 John E. Skvarla, II1, Secretary SUBJECT: NPDES Compliance Inspection Report Permit Number NCG060329 Rose Hill Fresh/IQF Chicken Processing Plant Duplin County Dear Mr. Peak: On July 31, 2014, staff from the Wilmington Regional Office conducted an inspection of the Rose Hill Fresh/IQF Chicken Processing Plant facility on Hwy 117, Duplin County, North Carolina. Mr. Chris Murray and Mr. Paul Shivers met with me during the inspection. Enclosed is the Compliance Inspection Report. The consistent exceedances of fecal coliform has resulted in the permit being in Tier Three. Thus you are required to sample on a monthly basis for fecal coliform. Please review your records to validate if you need to implement monthly sampling for TSS and COD as well. The actions taken by the plant to reduce the fecal coliform numbers are proving to be insufficient. A rolled product was installed, achieving some reduction, but still significantly over the benchmark levels. Please continue to pursue other avenues of reduction. The proposal of isolating the wastewater from the unloading area is good. The proposal of an infiltration basin is good, but will need permitting from the Division of Water Quality Aquifer Protection. While I understand the limitations of sampling events to deem effectiveness of each proposal, I want to reiterate the urgency of solving the problem. Please respond to this inspection report with a status update and proposed actions with a specific timeline setting goals and deadlines. If you have any questions or need further assistance, do not hesitate to contact me at 910-796-7314 or brian.lambe@ncdenr.gov Sincerely, n Lambe Environmental Specialist Enclosures: Inspection Report cc: Chris Murray, Corporate Environmental Manager NPDES General Permit Inspection Files Wilmington Regional Office 127 Cardinal Drive Extension Wilmington, NC 28405 Phone: 910-796-7215 f FAX: 910-350-2004 An Equal Opportunity/Affirmative Action Employer 50% Recycled/10% Post Consumer Paper NorthCarof ina Customer S-, ., Compliance Inspection Report Permit: NCG060329 SOC: County: Duplin Region: Wilmington Effective. 12/12/12 Expiration: 10/31/17 Owner: House of Raeford Farms Inc Effective: Expiration: Facility: Rose Hill Fresh I IQF Chicken Processing Plant 3191 US Hwy 117 N Contact Person: Nicole Reynolds Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Representative(s): Related Permits: Title: Complex Manager Certification: Rose Hill NC 28458 Phone: 910-289-3191 Phone: Inspection Date: 07/31/2014 Entry Time: 09:30AM Exit Time: 10:30AM Primary Inspector: Brian P Lambe � - phone: Secondary Inspector(s): Reason for Inspection: Routine V Inspection Type: Compliance Evaluation Permit Inspection Type: FoodlTobacm/Soaps/Cosmetics/Public Warehousing Stormwater Discharge COC Facility Status: ❑ Compliant ® Not Compliant Question Areas: ® Storm Water (See attachment summary) Page: 1 Permit: NCG060329 Owner - Faclilty: House of Raeford Farms Inc Inspection Date: 6713112014 Inspection Type : Compliance Evaluation Reason for Visit: Routine Inspection Summary: Met with Chris Murray and Paul Shivers, PE. Discussed current sampling results and reduction methods. The plant has installed a rolled product to capture fecal coliform at the three discharge points. Murray commented that the storm event overtopped the rolled product. Sampling showed 2/3 reduction in numbers, albeit still very high. Only one sampling event since spring (last meeting). Discussed plan of action with Murray and Shivers. They want more time to further investigation of best possible solution, which is acceptable considering lack of sampling events (need more data). While trying to find other possible solutions, the ultimate solution is to treat stormwater like wastewater. Discussed infiltration pond with level spreader. Shivers indicated that the ground was not ideal for infiltration, but still may be possible. Importation of sand may help with this condition. Following the infiltration pond tract will push the permittee into aquafer protection permitting. Please consult with the division of Water Quality regarding this proposal. Please send a written status update to this office summarizing actions taken and future course of action. Page: 2 Central Files: AP5 SWP 05/20/11 Permit Number NCG060329 Permit Tracking Slip Program Category Status Project Type NPDES SW In draft New Project Permit Type Food!Tobacco/Soaps/Cosmetics/Public Warehousing Stormwater Discharge COC Primary Reviewer jennifer.jones Coastal SW Rule Permitted Flow Version Permit Classification COC Permit Contact Affiliation Facility Facility Name Major/Minor Region House of Raeford Chicken Processing Plant Minor Wilmington Location Address County 3333 US Hwy 117 S Duplin Rose Hill INC 28458 Facility Contact Affiliation Clay Howard PO Box 40 Rose Hill NC 284580040 Owner Owner Name Owner Type House of Raeford Farms Inc Non -Government Owner Affiliation Robert C. Johnson PO Box 699 Rose Hill NC 284580699 Dates/Events Scheduled Orig Issue App Received Draft Initiated Issuance Public Notice Issue Effective Expiration 05/05/11 05/17/11 *0/11 q}' 12-D 12 Regulated Activities Recluested/Receiveld Events Food and kindred products manufacture RO staff report received 05/20/10 Y RO staff report requested 05/17/11 Outfall 001 Waterbody Name Stream Index Number Current Class Subbasin Beaverdam Branch 18-74-24-1-1 C;Sw 03-06-22 aceAnalytical Mwr 0weWba.cam Project: STORMWATER Pace Project No.: 9281595 Charlotte Certification 109 9800 KinceyAve. Ste 100, Huntersville, NC 28078 Louisiana/LELAP Certification #: 04034 New Jersey Certification M NCO12 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pennsylvania Certification #: 68-00784 South Carolina Certification M 99006001 Asheville Certification Ills 2225 Riverside Dr., Asheville, NC 28804 Connecticut Certification #: PH-0106 Flohda/NEtAP Certification #: E87648 Massachusetts Certification #: M-NC030 New Jersey Certification #: NC011 North Carolina Bioassay Certification #: 9 North Carolina Drinking Water Certification #: 37712 Pace Analytical Services, Inc. 2225 Riverside Or. Asheville, NC 28804 (828)254-7178 CERTIFICATIONS South Carolina Drinking Water Cart. M 99006003 Virginia Certification #: 00213 Connecticut Certification #: PH-0104 Flodda/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DHH Drinking Water # LA 100031 West Virginia Certification M 357 North Carolina Wastewater Certification #: 40 Pennsylvania Certification #: 68-03578 South Carolina Bioassay Certification #: 99030002 South Carolina Certification #: 99030001 Virginia Certification M 00072 West Virginia Certification #: 356 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc,. Pecs Analytical Services, Inc. 9800 KinceyAve. Suite 100 Hunteraville, NC 28078 (704)875-9092 Page 2 of 7 t_ permit NCGO60329 Owner - Facility: House of Raeford Farms Inc inspection Date: 07/31 /2014 Inspection Type: Compliance Evaluation Reason for Visit: Routine Stormwater Pollution Prevention Plan Does the site have a Stormwater Pollution Prevention Plan? # Does the Plan include a General Location (USGS) map? # Does the Plan include a "Narrative Description of Practices'? # Does the Plan include a detailed site map including outfall locations and drainage areas? # Does the Plan indude a list of significant spills occurring during the past 3 years? # Has the facility evaluated feasible alternatives to current practices? # Does the facility provide all necessary secondary containment? # Does the Plan include a BMP summary? # Does the Plan include a Spill Prevention and Response Plan (SPRP)? # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? # Does the facility provide and document Employee Training? # Does the Plan include a list of Responsible Pany(s)? # Is the Plan reviewed and updated annually? # Does the Plan include a Stormwater Facility Inspection Program? Has the Stormwater Pollution Prevention Plan been implemented? Comment: Due to the high samnlina data, the facility is in the Drocess of uDdatina the Bll and Sl Yes No NA NE ® ❑ ❑ ❑ ® ❑ ❑ ❑ ®❑Elm ®❑❑❑ ® ❑ ❑ ❑ ❑ ® ❑ ❑ ®❑❑❑ ®❑❑❑ ® ❑ ❑ ❑ ® ❑ ❑ ❑ ❑ ® ❑ ❑ ®❑❑❑ ® ❑ ❑ ❑ The high fecal and COD numbers are likely due to wastewater contaminating the stormwater. Methods to separate and methods of treatment are being developed. T Qualitative Monitorinq Yes No NA NE Has the facility conducted its Qualitative Monitoring semi-annually? ® ❑ ❑ ❑ Comment: Analytical Monitorinq Yes No NA NE Has the facility conducted its Analytical monitoring? ® ❑ ❑ ❑ # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ 119 ❑ Comment: Permit and Outfalls Yes No NA NE # Is a copy of the Permit and the Certificate of Coverage available at the site? ®❑ ❑ ❑ # Were all outfalls observed during the inspection? ®❑ ❑ ❑ # If the facility has representative outfall status, is it property documented by the Division? ❑ ❑ ® ❑ # Has the facility evaluated all illicit (non stormwater) discharges? ®❑ ❑ ❑ Comment: Page: 3 Jones, Jennifer From: Willis, Linda Sent: Friday, May 20, 2011 11:10 AM To: Jones, Jennifer Subject: RE: NCGO60329 - House of Raeford Farms, Inc. - Rose Hill Facility Issue as soon as possible please. Thanks. Linda From: Jones, Jennifer Sent: Tuesday, May 17, 2011 4:48 PM To: Willis, Linda Cc: Jones, Jennifer Subject: NCG060329 - House of Raeford Farms, Inc. - Rose Hill Facility Hi Linda, We've received a new NO1 from House of Raeford Farms, Inc / House of Raeford — Rose Hill Facility for their chicken processing facility in Rose Hill (Duplin County) for coverage under NCG06 (food & kindred permit). The site discharges stormwater into Beaverdam Creek and Cabin Branch (C, Sw). A copy of the NU, cashed cheque, and site plan are attached. Does the Wilmington Regional Office have any concerns about issuing this facility a COC for this general permit? If we don't receive any objections, we'll issue the COC in 30 days. Thanks, Jen Jennifer Jones Environmental Engineer NCDENR I DWQ I Stormwater Permitting Unit 1617 Mail Service Center, Raleigh, NC 27699-1617 512 N, Salisbury St, Raleigh, NC 27604 Phone: (919) 807-6379 Fax: (919) 807-6494 Email: jennifer.'ones@ncdenr.gov Website: http:/Z�ortal,ncdenr.org/webZwq/ws/su **E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties.** �jn' /s' a Pace Analytical Services, Inc. Pace Analytical Services, Inc. ace/ Ka'��KT1 2225 Riverside dr. 9800 Kinney Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 November 18, 2010 Mr, Chris Ray Town of Zebulon 450 East Horton Zebulon, NC 27597 RE: Project: STORMWATER Pace Project No.: 9281595 Dear Mr. Ray: Enclosed are the analytical results for sample(s) received by the laboratory on November 06, 2010. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, qt�n Y "-7 Erin Waters erin.waters@pacelabs.com Project Manager Enclosures F I i I REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. o sO+o Page I of 7 NC®ENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Governor Mr. Clay Howard House of Raeford Farms, Inc. P.O. Box 40 Rose Hill, NC 28458 Dear Mr. Howard: Coleen H. Sullins Director May 20, 2011 Subject: General Permit No. NCG060000 House of Raeford Farms, Inc. Rose Hill Facility 3333 US Highway 117 South COC NCG060329 Duplin County Dee Freeman Secretary In accordance with your application for a discharge permit received on May 5, 2011, we are forwarding herewith the subject certificate of coverage to discharge under the subject state — NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated October 15, 2007 (or as subsequently amended). Please take notice that this certificate of coverage is not transferable except after notice to the Division of Water Quality. The Division of Water Quality may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act or any other federal or local governmental permit that may be required. If you have any questions concerning this permit, please contact Jennifer Jones at telephone number (919) 807-6379 Sincerely, ORIGINAL B� KEN PICKLE for Coleen H. Sullins cc: Wilmington Regional Office, Linda Willis Central Files Stormwater Permitting Unit Files Wetlands and Stormwater Branch 1617 Mail Service Center, Raleigh, North Carolina 27699.1617 Location: 512 N. Salisbury St. Raleigh, North Carolina 27604 Phone: 919-807-63001 FAX: 919-807-64941 Customer Service: 1-877-623-6748 Inlemet. www.ncwaterquality.org O NorthCarolina Naturallrf STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF. WATER QUALITY GENERAL PERMIT NO. NCG060000 CERTIFICATE OF COVERAGE No. NCG060329 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, House of Raeford Farms, Inc. is hereby authorized to discharge stormwater from a facility located at House of Raeford Farms, Inc. - Rose Hill Facility 3333 U.S. Highway 117 South Rose Hill Duplin County to receiving waters designated as Beaverdam Branch and Cabin Branch, both class C, Sw water in the Cape Fear River Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, II, III, IV, V, and VI of General Permit No. NCG060000 as attached. This certificate of coverage shall become effective May 20, 2011. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day May 20, 2011. ORIGINAL B1 KEN PICKLE for Coleen H. Sullins, Director Division of Water Quality By the Authority of the Environmental Management Commission Al I: A k' QUA 7) t V House of Raeford Farms, Rose Hill Facility k' #4V N P1. e4 _N 4- B-' -�` V 4_1 J, 3k 7 4j w 41 Me) N00060329 House of Raeford Farms, Inc. Rose Hill Facility N Rose Hill,, NC Latitude: 341 51' 32" N w E Longitude: 780 01'57" W County: Duplin S Receiving Stream: Beaverdam Branch, Cabin Branch Map Scale 1: 19,200 Stream Class: both C, Sw Facility Location Sub -basin: 03-06-22 (Cape Fear River Basin) LC May 3, 2011 Ms. Jennifer Jones Environmental Engineer Stormwater Permitting Unit NCDENR- Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Re: House of Raeford Farms, Inc. — Rose Hill Facility Stormwater NOI Please find attached Notice of Intent for House of Raeford Farms, Inc., Rose Hill Facility for stormwater discharge. Included in this application package are the following: ➢ Check for $100 made payable to NCDENR; ➢ Completed application and supporting documents; ➢ Site Diagram; USGS Map showing facility location. If upon receipt and review of this application package, you should have any questions, comments or concerns, please do not hesitate to contact me at your earliest convenience. Regards, de' ()s W. Holland, P.E. P.O. Box 2928 Surf City, NC 28445 Phone: 910-803-0444 Fax; 910-803-0445 Division of Water Quality / Surface Water A 'p,A Protection Section �_ National Pollutant Discharge Elimination System NCDENR t� C R 11 DEfWiTMCNT OF EHNAOu - wx0 N'TLM.0 RE9OUfiCES NCG060000 NOTICE OF INTENT FOR AGENCY USE ONLY Date Received Year Month Day Certificate ofCovera e c 3aa Check # I Amount IUL,314 9 1 1 c o _ Permit Assigned to National Pollutant Discharge Elimination System application for coverage under General Permit NCG060000: STORMWATER DISCHARGES associated with activities classified as: SIC (Standard Industrial Classification) 20 Food and Kindred Products SIC 21 Tobacco Products SIC 283 Drugs SIC 284 Soaps, Detergents, & Cleaning Preparations; Perfumes, Cosmetics, & Other Toilet Preparations SIC 422 Public Warehousing and Storage (except 4226) W)For questions, please contact the DWQ Regional Office for your area. Seepage4. (Please print or type) 1) Mailing address of owner/operator (address to which all permit corresl2ondence will be mailed): Name House of Raeford Farms, Inc. Street Address PO Sox 40 City Rose Hill State NC ZIP Code 28458 Telephone No. 910 289-3191 Fax: (910) 289-4355 2) Location of facility producing discharge: Facility Name Facility Contact Street Address City County Telephone No. Email House of Raeford Farms, Inc. (Rose Hill Facility) - Clay Howard 3333 US HWY 117 South Rose Hill State NC ZIP Code 28458 910 289-3191 Fax: (910) 289-4355 clay,howard@houseofraeford.com 3) Physical Location Information: Please provide a narrative description of how to get to the facility (use street names, state road numbers, and distance and direction from a roadway intersection). From the intersection of US HWY 117 and West Charity Road, in Rose Hill, travel approx 2.7 miles north on US HWY 117. The plant is on the right (east). (A copy of a county map or USGS quad sheet with the facility dearly located must be submitted with this application.) 4) Latitude 34 d 51' 31" N Longitude 78 d 1' 58" W (deg, min, sec) =EWATEV14 �15) This NPDES Permit Application applies to which of the following:U❑ New or Proposed Facility Date operation is to begin® Existing inch Page 1 of 4 SWU-221-071408 Last revised 7114108 NCG060000 N.O.I. 6) Standard Industrial Classification: Provide the 4-digit Standard Industrial Classification code (SIC code) that describes the primary industrial activity at this facility. SIC code: 7) Provide a brief narrative description of the types of industrial activities and products manufactured at this facility: This plant processes live chickens to various finished food products, such as chicken tenders, drumsticks thighs, legguarters, wins etc. 8) Discharge points / Receiving waters: How many discharge points (ditches, pipes, channels, etc.) convey stormwater from the property? What is the name of the body or bodies of water (creek, stream, river, lake, etc.) that the facility stormwater discharges end up in? Beaverdam Branch Cabin Branch Receiving water classification: C:Sw, C:Sw _ Is this a 303(d) listed stream? No Has a TMDL been approved for this watershed? No If the site stormwater discharges to a separate storm sewer system, name the operator of the separate storm sewer system (e.g. City of Raleigh municipal storm sewer). NIA 9) Does this facility have any other NPDES permits? ® No ❑ Yes If yes, list the permit numbers for all current NPDES permits for this facility: NC0066320 10) Does this facility have any Non -Discharge permits (ex: recycle permit)? ❑ No ® Yes If yes, list the permit numbers for all current Non -Discharge permits for this facility: WQ0002005 11) Does this facility employ any best management practices for stormwater control? No ❑ Yes (Show any structural BMPs on the site diagram.) If yes, please briefly describe: 12) Does this facility have a Stormwater Pollution Prevention Plan? 2 No ❑ Yes If yes, when was it implemented? 13) Are vehicle maintenance activities occurring at this facility? ® No ❑ Yes 14) Hazardous Waste: a) Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility? ® No ❑ Yes b) Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste generated per month) of hazardous waste? Page 2 of 4 SWU-221-071408 Last revised 7114108 NCG060000 N.O.I. ® No ❑ Yes c) Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste generated per month) of hazardous waste? ® No ❑ Yes d) Is hazardous waste stored in the 100-year flood plain? ® No ❑ Yes If yes, include information to demonstrate protection from flooding. e) If you answered yes to questions b. or c., please provide the following information: Type(s) of waste. - How is material stored: Where is material stored: How many disposal shipments per year: Name of transport 1 disposal vendor: _ Vendor address: 15) Certification: North Carolina General Statute 143-215.6E (i) provides that: Any person who knowingly makes any false statement, representation, or certification in any application, record, report, plan, or other document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000). I hereby request coverage under the referenced General Permit. I understand that coverage under this permit will constitute the permit requirements for the discharge(s) and is enforceable in the same manner as an individual permit. I certify that I am familiar with the information contained in this application and that to the best of my knowledge and 1 elief su9ti11nfoVTrMion is true, complete, and accurate. Printe a Aof- �arson Igning: Titl 9C s (Date Signed) This Notice of Intent must be accompanied by a check or money order for $100.00, made payable to: NCDENR Page 3 of 4 SWU-221-071408 Last revised 7114l013 NCG060000 N.O.I. Final Checklist This application will be returned as incomplete unless all of the following items have been included: Check for $100 made payable to NCDENR. ® This completed application and all supporting documents. ® A site diagram showing, at a minimum, (existing or proposed): (a) outline of drainage areas, (b) stormwater management structures, (c) location of stormwater outfalls corresponding to the drainage areas, (d) runoff conveyance features, (e) areas where materials are stored, (f) impervious areas, (g) site property lines. Copy of county map or USGS quad sheet with the location of the facility clearly marked on the map. Mail the entire package to: Stormwater Permitting Unit Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Note The submission of this document does not guarantee coverage under the General Permit. For questions, please contact the D WQ Regional Office for your area. DWQ Regional Office Contact Information: Asheville Office ...... (828) 296-4500 Fayetteville Office ... (910) 433-3300 Mooresville Office ... (704) 663-1699 Raleigh Office.. ...... (919) 791-4200 Washington Office ... (252) 946-6481 Wilmington Office ... (910) 796-7215 Winston-Salem ...... (336) 771-5000 Central Office .........(919) 807-6300 Page 4 of 4 SVVU-221-071408 Last revised 7/14/08 September 9, 2010 Division of Water Quality Non -Discharge Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Permitting Signature Authority To Whom it May Concern: As an appropriate signing official for House of Raeford, Inc. — Wallace Division as designated by 15A NCAC 2T .0106(c), I hereby delegate authority to sign and certify all permit applications, reports or other permit related documents to the following staff for the following permit types (wastewater, erosion & sediment control) and/or permit numbers: Position Person Currently in Position Permit Type or Permit Number Operations Manager Clay Howard Wastewater, erosion & sediment control, srvA,u 1141150 If you have any questions, please contact me at the following: Permittee/Applicant name (please print): Title: Complete mailing add ess: �3b�C City: 1�a5E ILL State: Telephone number: � 3 / E14,LL-uG 49' /, C Zip: Z$ q S 2' Facsimile number: (_ e7 ZFT — Vv q �S O�O� WAT�RQG c t ] Q 'C BRENDAN CONWAY HONDA POWER EQUIPMENT MFG PO BOX 37 SWEPSONVILLE, NC 27359 Dear Permittee: Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.E., Director Division of Water Quality August 23, 2002 Subject: NPDES Stormwater Permit Renewal HONDA POWER EQUIPMENT MFG COC Number NCG030329 Alamance County In response to your renewal application for continued coverage under general permit NCG030000. the Division of Water Quality (DWQ) is forwarding herewith the reissued sormwater general permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983, The following information is included with your permit package: * A new Certificate of Coverage * A copy of General Stormwater Permit NCG030000 * A copy of the Analytical Monitoring Form (DMR) * A copy of a Technical Bulletin for the general permit Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility for compliance with any other applicable federal. state, or local law, rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit package please contact Bill Mills of the Central Office Stormwater and General Permits Unit at (919) 733-5083, ext. 548 Sincerely, Bradley Bennett, Supervisor Stormwater and General Permits Unit cc: Central Files Stormwater & General Permits Unit Files Winston-Salem Regional Office ATM` NCDENR N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-7015 Customer Service 1- 800-623-7748 : STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030329 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and X, regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, HONDA POWER EQUIPMENT MFG is hereby authorized to discharge stormwater from a facility located at HONDA POWER EQUIPMENT MFG NC HWY 119 HONDA DR SWEPSONVILLE ALAMANCE COUNTY to receiving waters designated as the Burlington MSSS to a UT to Haw Creek, a class C NSW stream, in the Cape Fear River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, IL III, IV, V, and VI of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective September 1, 2002. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day August 23. 2002, for Alan W. Klimek, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission \N A rf�pG Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources RICK MORRIS HONDA POWER EQUIPMENT MFG P O BOX 37 SWEPSONVILLE, NC 27359 Dear Permittee: Gregory J. Thorpe, Ph.D. Acting Director Division of Water Quality December 27, 2001 Subject: NPDES Stormwater Permit Renewal HONDA POWER EQUIPMENT MFG COC Number NCG030329 Alamance County Your facility is currently covered for Stormwater discharge under General Permit NCG030000. This permit expires on August 31. 2002. The Division staff is currently in the process of rewriting this permit and is scheduled to have the permit reissued by late summer of 2002. Once the permit is reissued, your facility would be eligible for continued coverage under the reissued permit. In order to assure your continued coverage under the general permit, you must apply to the Division of Water Quality (DWQ) for renewal of your permit coverage. To make this renewal process easier, we are informing you in advance that your permit will be expiring. Enclosed you will find a General Permit Coverage Renewal Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued coverage under the general permit. Failure to request renewal within this time period may result in a civil assessment of at least $250.00. Larger penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and could result in assessments ol'civil penalties of up to $10,000 per day. Please note that recent federal legislation has extended the "no exposure exclusion" to all operators of industrial facilities in any of the I 1 categories of "storm water discharges associated with industrial activity," (except construction activities). If you feel your facility can certify a condition of' "no exposure", i.e. the facilty industrial materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional information contact the Central Office Stormwater Staff member listed below or check the Stormwater & General Permits Unit Web Site at http://h2o.enr.state.nc.us/su/stormwater.htlnl If the subject stormwater discharge to waters of the state has been terminated. please complete the enclosed Rescission Request Form. Mailing instructions are listed on the bottom of the form. You will be notified when tine rescission process has been completed. If you have any questions regarding the permit renewal procedures please contact Corey Basinger of the Winston-Salem Regional Office at 336-771-4600 or Bill Mills of the Central Ol'iice Stormwater Unit at (919) 733-5083. ext. 548 Sincerely. 5 Bradley Bennett, Supervisor Stormwater and General Permits Unit cc: Central Files Winston-Salem Regional Office e�V NCDENR N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-7015 Customer Service 1- 800-623-7748 State of North Carolina Department of Environment, Health and Natural Resources Division of Water Quality • James B. Hunt, Jr., Governor Wayne McDevitt, Secretary D E F'**A F1 A. Preston Howard, Jr., P.E., Director September 24, 1997 DOUG GAYLORD HONDA POWER EQUIPMENT MFG P.O. BOX 37 SWEPSONVILLE, NC 27359 Subject: Reissued Stormwater General Permit for Certificate of Coverage No. NCG030329 Alamance County Dear Permittee: In response to your renewal application for continued coverage under the subject permit, the Division of Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983. The following information is included with your permit package: ■ A copy of the stormwater general permit. ■ A Stormwater Pollution Prevention Plan Certification Form. This form certifies that you have developed and implemented the Stormwater Pollution Prevention Plan (SPPP) required in your permit. This form must be completed and returned to the Division within 30 days of receipt of this letter. DO NOT send the SPPP with the signed form. ■ Five copies of Analytical Monitoring forms. ■ Five copies of Qualitative Monitoring forms. ■ A copy of a Technical Bulletin on the stormwater program with outlines program components and addresses frequently asked questions. ■ A corrected Certificate of Coverage if you indicated a name or address change on the Renewal Form returned to the Division. Your certificate of coverage is not transferable except after notice to DWQ. The Division of Water Quality may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DWQ or permits required by the Division of Land Resources, Division of Air Quality, Coastal Area Management Act or any other Federal or Local governmental permits that may be required. If you have any questions concerning this permit or other attached documents, please contact the Stormwater Group at telephone number (919) 733-5083 Sincerely, for A. Preston Howard, Jr., P. E. P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper S*ate of North Carolina Department of Environment, Health and Natural Resources Division of Environmental Management James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary A. Preston Howard, Jr., P.E., Director April 28, 1995 Koji Isujita Honda Power Equipment Mfg P.O. Box 37 Swepsonville, NC 27359 Subject: General Permit No. NCG030000 Honda Power Equipment Mfg COC NCG030329 Alamance County Dear Koji Isujita: In accordance with your application for discharge permit received on March 7, 1995, we are forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983. If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, this certificate of coverage shall be final and binding. Please take notice that this certificate of coverage is not transferable except after notice to the Division of Environmental Management. The Division of Environmental Management may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit that may be required. If you have any question concerning this permit, please contact MR. ANTONIO EVANS at telephone number 919/733-5083. Sincerely, Original Signed By Coleen H. Sullins A. Preston Howard, Jr. P.E. cc: Winston-Salem Regional Office P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-7015 FAX 919-733-2496 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper M STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES DIVISION OF ENVIRONMENTAL MANAGEMENT GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030329 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Honda Power Equipment Mfg., Inc. is hereby authorized to discharge stormwater from a facility located at Honda Power Equipment Mfg., Inc. Honda Drive Swepsonville, NC Alamance County to receiving waters designated as City of Burlington municipal storm sewer to an unnamed tributary to Haw Creek in the Cape Fear River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III and IV of General Pernvt No. NCG030000 as attached. This certificate of coverage shall become effective April 28, 1995. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day April 28, 1995. Origins! Signed By C:,leen I-l. Sullins A. Preston Howard, Jr., P.E., Director Division of Environmental Management By Authority of the Environmental Management Commission �•� .\�`-y� '''}.y� ��1 ����'r� 1=%� � r,��r% IX 111�/1?i pumping Sta p 62 uarry;t\ lr^ Sch /� �j••'• \7 •� OU <N � ``� ate. 1I�'"1 �1��1, �/_j/If sso\ -.- ��� ��•/• • • •r �_ y�.r = y} ; \ .; "� � I✓�t r • e ;':� ,�•�j i I 1I? .� �'.y _ y.,r .��• � � �i � ram• �� � � N ��81 y. r/ \ �;��:•:= . •il s _ �s 3� ;� \ , �J ! 1 'ii, to " `� r � `�\'fir., • �. . ),i; ' fj '� � p � � � { \ � • r / � � i �.' ' � � � �'!!,'iY� �pr�7-_/' �✓ i f � I 1 I �' ��''� dv'��: •.� 595',•c = � � �JN..J . �i (\ I (]�J�1� �� I l . i41 I5 `r so iJ 21 I PhMP.: 11, —J hsvei�„ r\ mm�� t1890000 FEET 648 �d, edited, and published by the Geo4ogical Survey 650 20' 651 649 t r c' FACILITY: H"n c)a Paur2r PC, COUNTY: R 6 NPDES: 03 d MAP#: DSN FLOW: l LATITUDE: LONGITUDE: N/A 03 -a 6 - o a 3Co � I �SCprr rig 0 ace' 3 a'� 1 RECEIVING STREAM: ' 11 �y' Sewed +-o a n unoc,m-e-CL ` ri bAPt C) tO Ha,� STREAM CLASS: C N S (.J DISCHARGE CLASS: STORMWATER