NCG060272_MONITORING INFO_20181018

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO. Iv C� C) � Oa
DOGTYPE O HISTORICAL FILE
MONITORING REPORTS
DOC DATE ❑ �'b) 7� I � J.
b ate'
YYYYMMDD

SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT
for North Carolina Division of Water Quality General Permit No. NCG060000
Date submitted October 16 2018
1VL (r 0 6 b 7;)-
CERTIFICATE OF COVERAGE NO. NCG060000 SAMPLE COLLECTION YEAR 2018
FACILITY NAME _Alcami Corporation 1726 N. 23`d Street FACILITY ACTIVITIES INCLUDE (check all that apply):
COUNTY New Hanover NLUENEQ ❑ use/process meats ❑ use animal fats/byproducts
PERSON COLLECTING SAMPLES Jay Baker _ nCT 1.8 201, DISCHARGING TO SALTWATERS? DYES ®NO
LABORATORY Environmental Chemists, Inc. Lab Cert. # 94
CE-N 1 i-,Al- FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4
DIP1 t SECTION
Part A: Stormwater Benchmarks and Monitoring Results
Total event rainfall z 1.32 inches or n No discharge this period3
Outfall No.
Sample Collected,
mo/dd/yr
TSS,
mg/L
pH,
Standard units
COD,
mg/L
Oil and Grease,
mg/L
Fecal Coliforml,
Colonies per 100 ml
Enterococcil,
Colonies per 100 ml
Benchmark
-
100 or 504
Within 6.0 — 9.0
120
30
1000
500
Outfall 001
08/28/18
165 mg/L
6.91
133 mg/L
6 mg/L
Outfall 002
08/28/18
7.8 mg/L
6.45
22 mg/L
<5 mg/L
Outfall 003
08/28/18
44.7 mg/L
6.87
38 mg/L
<5 mg/L
1 Only applies to facilities that use/process meats.
2 The total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here.
4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month.
Outfall No.
Sample Collected,
mo/dd/yr
Oil and Grease,
mg/L
TSS,
mg/L
pH,
Standard units
New Motor Oil usage,
Annual average gal/mo
Benchmark
-
30
100 or 504
6.0 — 9.0
-
1 Only applies to facilities that use/process meats.
2The total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here.
4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
(ifyes, complete Part 8)
SWU-249 Last Revised: October 18, 2012
Page 1 of 2

*FOR PART A AND PART B MONITORING RESULTS:
t, A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of
monitoring period in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
(Signatu7 of Permittee)
c6 1(,Is
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SWU-249 Last Revised: October 18, 2012
Page 2 of 2

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax
infoGa environmentalchemists.com
Alcami (AAIPharma) Date of Report: Sep 08, 2018
2320 Scientific Park Drive Customer PO #:
Wilmington NC 28405 Customer ID: 08100002
Attention: Elias Galloway Report #: 2018-14214
Project ID: Storm Water
Lab ID Sample ID: Alcami (AAIPharma) Collect Date/Time Matrix Sampled by
18-35926 Site: Oufall @ Front 8/28/2018 2:25 PM Water Jay Baker
Test Method Results Date Analyzed
Enterococci
Enterolert IDEXX
649 MPN1100ml
08/28/2018
Oil & Grease (O&G)
EPA 1664
6 mg/L
08/30/2018
Residue Suspended (TSS)
SM 2540 D
165 mg/L
08/29/2018
Temperature
SM 2550 B
' 31.0 C
08/28/2018
pH
SM 4500 H B
6.91 units
08/28/2018
COD
SM 5220D
133 mg/L
08131/2018
Fecal Coliform
SM 9222D MF
22000 Colon ies/100mL
08128/2018
Lab ID Sample ID: Alcami (AAIPharma)
Collect DatefTime
Matrix Sampled by
18-35928 Site: Outfall @ Middle
8/28/2018 2:35 PM
Water Jay Baker
Test
Method
Results Date Analyzed
Enterococci
EnterolertlDEXX
261 MPN/100ml
08/28/2018
Oil & Grease (O&G)
EPA 1664
<5 mg/L
08/29/2018
Residue Suspended (TSS)
SM 2540 D
7.8 mg/L
08/30/2018
Temperature
SM 2550 B
30.1 C
08/28/2018
pH
SM 4500 H 8
6.45 units
08/28/2018
COD
SM5220D
22mg/L
08/31/2018
Fecal Coliform
SM 9222D MF
4800 Colonies/100ml-
08128/2018
Report #:: 2018-14214 Paae 1 of 2

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910,392,0223 Lab • 910.392,4424 Fax
710 Bowscrtown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
in ilopenviromnentalchcmists,com
Alcami (AAlPharma)
2320 Scientific Park Drive
Wilmington NC 28405
Attention: Elias Galloway
Lab ID Sample ID: Alcami (AAIPharma)
18-35929 Site: Storm Pond
Test
Method
Date of Report:
Sep 08, 2018
Customer PO #:
Customer ID:
08100002
Report #:
2018-14214
Project ID: Storm Water
Collect DatelTime Matrix
Sampled by
8/28/2018 2:15 PM Water
Jay Baker
Enterococcl
Enterolert IDEXX
Oil & Grease (O&G)
EPA 1664
Residue Suspended (TSS)
SM 2540 D
Temperature
SM 2550 B
pH
SM 4500 H B
COD
SM 5220D
Fecal Coliform
SM 92220 MF
Comment:
Reviewed by: )
, Nf r(i n Dv)n-n
Results Date Analyzed
1550 MPN1100m1 08/28/2018
<5 mg/L
08/29/2018
44.7 mg/L
08/30/2018
29.1 C
08/28/2018
6.87 units
08/28/2018
38 mg/L
08/31/2018
19000Colonies1100mL 08/28/2018
Report #:; 201 B-14214 Noe 2 of 2

Way
dmill
min
ENVIRONMENTAL CHEMISTS, I N C OFFICEIn910-3 2-02231FAX [phone]
Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: US CERTIFICATION # 37729 Info Oenvironmentatchemists.com
COLLECTION AND CHAIN OF CUSTODY
Client: AAI Pharma (C c-Z
PROJECT NAME: Storm Water
REPORT NO:
ADDRESS:
Contact: Elias Galloway
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO:
email:
Sampled By: SAMPLE TYPE: i = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
&
H
2
(n
a)
a a
c. ` m
ci
c CS
o
v a
�,
c=
o
u E
in
m g
J
PRESERVATION
ANALYSIS REQUESTED
I
D to
Time
Temp
Urh
R
Z
=
z
=
x
a
x
o
~
w
o
/'
Outfall C. l ---"-
Z z r
l C-
C
P
X
X
TSS, Oil & Grease, COD
G
G
/
pH: L '
C
P
X
IFecal Coliform, Enterococci
G
G
C
P
G
G
/L1•d�/G
Z ~
3J c
G
G
If `- `� 5
C
P
G
G
C
P
G
G
9 "!C C /�c�
L �.1
G
-G
/
C
P
$ T-SL
i
G
G
C
P
G
G
Limits: pH (6-9 units), TSS (50 mg/L), Oil and Grease (30 mg1L), Fecal Coliform (1,000 colonies1100 ml), Enterococci (500 colonies/100 ml), COD (120 mg/L)
Transfer
Relinquished By:
Daterrime
Received By:
Date/Time
1.
2.
.�
Temperature when Received: 9 Accepted:
Delivered By:__�—,L _ _ _ _ Received

October 16, 2018
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: Stormwater Sampling, 2nd Semiannual Testing
To whom it may concern,
Enclosed is a copy of Alcami Corporation's Stormwater Discharge Monitoring Report (DMR) with lab
analysis attached as required by permit (NCG060000) and certificate of coverage, (NCG060272) for the
facility located at 1723 North 23rd Street, Wilmington, NC. Samples was collected and analyzed by an
approved Environmental Laboratory (see attached.)
Results from testing indicate exceedances at outfall 001 for TSS and COD. In accordance with General
Permit NCG060000, Alcami will enter into a Tier One procedural response as outlined on page 5 of the
permit.
Although sample results were returned to Alcami on September 8, this report was delayed due to
inclement weather from Hurricane Florence, which caused a power outage at the facility, and inability of
personnel to access data and forms for submission.
Please contact me with any questions or concerns.
Si erely,
R�
Marc Lewis
Alcami Corporation
Site Director, Wilmington Drug Product Manufacturing Operations
Office: 910.254.73211 Mobile: [phone]
ALCAMI CORPORATION 2320 Scientific Park Drive Wilmington, NC 28405 +1 800.575.4224 www.alcaminow.com

Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: Semi -Annual Stormwater Sampling
To whom it may concern,
January 5, 2018
JAIL 10 2C:3
ON SECTION
l,,''FORNIATION PROI',F II r; UNP
Enclosed is a paper copy of Alcami Corporation Semi -Annual Stormwater Discharge Monitoring Report
(DMR) with lab analysis attached as required by our permit (NCG060000) and certificate of coverage
(NCG060272). The sample was collected and analyzed by an approved Environmental Laboratory.
VaL
`
Alcami Corporation
Site Director, Wilmington Drug Product Manufacturing Operations
Office: 910.254.7321 1 Mobile: [phone]
ALCAMI CORPORATION 2320 Scientific Park Drive Wilmington, NC 28405 �l 800.575.4224 www.alcaminow.com

SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT
for North Carolina Division of Water Quality General Permit No. NCG060000
Date submitted _January 5, 2018
CERTIFICATE OF COVERAGE NO. NCG060272
FACILITY NAME _ Alcami Corporation 1726 N. 23`d Street
COUNTY New Hanover
PERSON COLLECTING SAMPLES Jay Baker
LABORATORY Enviro Chem Lab Cert. # 94
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2017
FACILITY ACTIVITIES INCLUDE (check all that apply):
❑ use/process meats ❑ use animal fats/byproducts
DISCHARGING TO SALTWATERS? [—]YES ®NO
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Total event rainfall 2 0.14 inches or n No discharae this oeriod3
Outfall No.
Sample Collected,
mo/dd/yr
TSS,
mg/L
pH,
Standard units
COD,
mg/L
Oil and Grease,
mg/L
Fecal Coliform ,`
Colonies per 100 ml
Enterococci ,
Colonies per 100 ml
Benchmark
-
100or50
Within 6.0 — 9.0
120
30
1000
500
Outfall001
12/07/2017
7.9
7.95
<20
<5
280
12
Outfall002
12/07/2017
3.3
8.66
<20
<5
6000
199
Outfall003
12/07/2017
24.7
8.57
60
<5
1270
326
1 Only applies to facilities that use/process meats.
2The total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here.
45ee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month.
Outfall No.
Sample Collected,
mo/dd/yr
Oil and Grease,
mg/L
TSS,
mg/L
pH,
Standard units
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
30
100 or 504
6.0 — 9.0
-
1 Only applies to facilities that use/process meats.
The total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here.
4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
(if yes, complete Part B)
SWU-249 Last Revised: October 18, 2012
Page 1 of 2

*FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results or at end o
monitoring period in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
! L--;- /6'
(Date)
Additional copies of this form may be downloaded at: htto.//portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
S WU-249
Last Revised: October 18, 2012
Page 2 of 2

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Wad-, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
iiilo(u)environmentalcliemists.com
Alcami (AAIPharma) Date of Report: Dec 19, 2017
2320 Scientific Park Drive Customer PO #:
Wilmington NC 28405 Customer ID: 08100002
Attention: Report #: 2017-19044
Project ID: Storm Water
Lab ID Sample ID: Alcami (AAIPharma) Collect Date/Time Matrix Sampled by
17-46201 Site: Oufall @ Front 12/7/2017 10:00 AM Water Jay Baker
Test Method Results Date Analyzed
Enterococci
Enterolert IDEXX
326 MPN/100ml
12107/2017
Oil & Grease (O&G)
EPA 1664
<5 mg/L
12/13/2017
Residue Suspended (TSS)
SM 2540 D
24.7 mg/L
12/07/2017
Temperature
SM 2550 B
10.4 C
12/06/2017
pH
SM 4500 H B
8.57 units
12/06/2017
COD
SM 5220D
60 mg/L
12/08/2017
Fecal Coliform
SM 9222D MF
1270 ColonleS/100mL
12/07/2017
Lab ID Sample ID: Alcami (AAIPharma)
Collect DatelTime
Matrix Sampled by
17-46202 Site: Outfall @ Middle
12I712017 10:15 AM
Water Jay Baker
Test Method Results Date Analyzed
Enterococci
Enterolert IDEXX
199 MPN1100ml
12/07/2017
Oil & Grease (O&G)
EPA 1664
<5 mg/L
12/13/2017
Residue Suspended (TSS)
SM 2540 D
3.3 mg/L
12/07/2017
Temperature
SM 2550 B
10.3 C
12/06/2017
pH
SM 450n H s
8.66 units
12/06/2017
COD
SM 5220D
<20 mg/L
12/08/2017
Fecal Coliform
SM 9222D MF
>60000 Colon ies/100mL
12/07/2017
e�c 1 s ion
ay'-' - /'
Reonrt 99n17.14}044 -

Environmental Chemists, Inc.
aer, igh'em
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, ✓tinted, NC 27954 • 252.473.5702 Lab/Fax
275-A Wilmington Highway; Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ill fo(inenvironnientalchemists.coill
Alcami (AAIPharma)
Date of Report: Dec 19, 2017
2320 Scientific Park Drive
Customer PO #:
Wilmington NC 28405
Customer ID: 08100002
Attention:
Report #: 2017-19044
Project ID: Storm Water
Lab ID Sample ID: Alcami (AAIPharma)
Collect Date/Time Matrix Sampled by
17-46203 Site: Outfall @ Back
12/7/2017 9:50 AM Water Jay Baker
Test Method
Results Date Analyzed
Enterococci Enterotert IDEXX
12 MPN/100m1
12/07/2017
Oil & Grease (O&G) EPA 1664
<5 mg/L
12/13/2017
Residue Suspended (TSS) 5M 2540 D
7.9 mg/L
12/07/2017
Temperature SM 2550 B
11.8 C
12106/2017
pH SM 4500 H B
7.95 units
12/06/2017
COD SM 5220D
<20 mg1L
12/08/2017
Fecal Coliform SM 9222D MF
280 Colonies/100mL
12/07/2017
Comment:
Reviewed by: °la
Rennrfk ?n17.1QnAA

6602 Windmill Way Wilmington, NC 28405
114,1110 ENVIRONMENTAL CHEMISTS, I N C OFFICE: 910-392-0223 FAX [phone]
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info Cenvironmentaichemists.com
COLLECTION AND CHAIN OF CUSTODY
Client: AAt Pharma
PROJECT NAME: Storm Water
REPORT NO: �` /qFb f `!
ADDRESS:
Contact: Pedro Colon, AAIPharma
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO: Lynette Hodgson
email:
Sampled By: SAMPLE TYPE: i = influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
1,
a
m
98 t
m
L o
m
o
m
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
_
S
o
o
g
m
ta
Outfall Crr'^t�
��
�'
X
X.
TSS, Oil & Grease, COD
G
G
pH: '
C
P
X
Fecal Coliform, Enterococci
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Limits: pH (6-9 units), TSS (50 mg/L), Oil and Grease (30 mg/L), Fecal Coliform (1,000 colonies/100 ml), Enterococci (500 colonies/100 mi), COD (120 mg/L)
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
o
Temperature when Received: 3 Accepted:
Delivered By:.. Received By:
Comments:

on, NC
dmill
min
ENVIRONMENTAL CHEMISTS, IN C OFFICEIn910-392-02231FAX [phone]
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
Analytical & Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client: AAI Pharma
PROJECT NAME: Storm Water
REPORT NO:
ADDRESS:
Contact: Pedro Colon, AAIPharma
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO: Lynette Hodgson
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
P
Collection
k
°2
E
2
s o E
°
d
2 0
i0 a
N
? 4m
v E
�w
m m
z
PRESERVATION
ANALYSIS REQUESTED
Dat
Time
Temp
W
i
�
=
o
"
s
s
i
o
~
w
o
Outfall C^^' ffl
�'D
C
P
X
X
TSS, Oil & Grease, COD
G
G�
pH: �' G
C
P
X
Fecal Coliiform, Enterococci
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Limits: pH (6-9 units), TSS (50 mglL), Oil and Grease (30 mg/L), Fecal Coliform (1,000 colonies/100 ml), Enterococci (500 colonies/100 ml), COD (120 mg/L)
Transfer
Relinquished By:
DatelTime
Received By:
Date/Time
1.
2.
P
Temperature when Received: 3
Delivered By: Received
Requested:
1 Z) Lo I -? Time: 1 1 34-
TURNAROUND:

ENVIRONMENTAL CHEMISTS, I N C oFF CE: 910-392-02 302 Windmill Way iiFAX 910-392-4on, NC 424 S
Analytical &Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
'
COLLECTION AND CHAIN OF CUSTODY
Client: AAI Pharma
PROJECT NAME: Storm Water
REPORT NO:
ADDRESS:
Contact: Pedro Colon, AAIPharma
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO: Lynette Hodgson
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
le Identification
Collection
k
0
a
C�
r
ccPRESERVATION
gL,
z
ANALYSIS REQUESTEDSam
Time
Temp
o
z
U
="
°°oa
zE
az
oDate
Outfall
ro
L
C
P
�''
X
X
'SS, Oil & Grease, COD
G
G
H: �-
C
P
X
Fecal Coliform, Enterococci
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Limits: pH (6-9 units), TSS (50 mg/L), Oil and Grease (30 mgtL), Fecal Coliform'(1,000 colonies/100 ml), Enterococci (500 colonies/100 ml), COD (120 mg/L)
Transfer
Relinquished By:
Date/Time
Received By:
DateMme
1.
2.
Temperature when Received: Accepted: elected: Resample Requested:
Delivered By: Received By:(
Date: 1 z) t- 1 -7 Time: 1 134
Comments: TURNAROUND:

t
SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT
for North Carolina Division of Water Quality General Permit No. NCG060000
Date submitted May 24, 2017
CERTIFICATE OF COVERAGE NO. NCG060000 NC6- o 60�� 7� SAMPLE COLLECTION YEAR 2017 � ��i� �
FACILITY NAME ., Alcami Corporation 1726 N. 23ra Street FACILITY ACTIVITIES INCLUDE (check all that apply): JUN 14 201I
COUNTY New Hanover ❑ use/process meats ❑ use animal fats/byp roduv1S14TRAL FILES
PERSON COLLECTING SAMPLES Cindy McDonald DISCHARGING TO SALTWATERS? []YES ®NO DWR SECTION
LABORATORY Enviro Chem Lab Cert. # 94
Part A: Stormwater Benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON THE REVERSE -->
Total event rainfall 21.51 inches or Fj No dischorge this period3
Outfall No.
Sample Collected,
mo/dd/yr
TSS,
mg/L
pH,
Standard units
COD,
mg/L
Oil and Grease,
mg/L
Fecal Coliform ,
Colonies per 100 ml
Enterococcil,
Colonies per 100 ml
Benchmark
-
100 or 504
Within 6.0 — 9.0
120
30
1000
500
Outfall 001
05/05/17
<2.9 mg/L
6.48
25 mg/L
<5 mg/L
5800
>2420
Outfall 002
No Discharge
No Discharge
No Discharge
No Discharge
No Discharge
No Discharge
No Discharge
Outfall 003
05/05/17
19.7 mg/L
7.04
<20 mg/L
<5 mg/L
1160
>2420
1 Only applies to facilities that use/process meats.
2 The total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here.
4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ®no
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month.
Outfall No.
Sample Collected,
mo/dd/yr
Oil and Grease,
mg/L
TSS,
mg/L
pH,
Standard units
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
30
100 or 504
6.0 — 9.0
-
1 Only applies to facilities that use/process meats.
z The total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here.
4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies
(if yes, complete Part B)
S WU-249 Last Revised: October 18, 2012
Page 1 of 2

*FOR PART A AND PART B MONITORING RESULTS:
+ A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEE DANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results or at end of
monitoring period in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
C I7-17
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SWU-249 Last Revised: October 18, 2012
Page 2 of 2

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6002 Windmill May, Wdnzington, NC 28405 • 910.392.0223 Lab • 910.392,4424 F-ax
710 Bowsertown Road, Mantco, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington F-ligh4vay, Jacksonville, NC 28540 • 910.317.5843 Lab/Fax
ilif'o((_DcnviI-oilmen talchemists.cozn
Alcami (AAIPharma) Date of Report: May 18, 2017
2320 Scientific Park Drive Customer PO #:
Wilmington NC 28405 Customer ID: 08100002
Attention: Pedro Colon Report #: 2017-06331
Project ID: Storm Water
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
17-14958 Site: outfall-001 5/5/2017 10:50 AM Water Cindy McDonald
Test Method Results Date Analyzed
Enterococci Enterolert IDEXX >2420 MPN/100ml 05/05/2017
Oil & Grease (0&G) EPA 1664 <5 mg/L 05/15/2017
Residue Suspended (TSS) SM 2540 D <2.9 mg/L 05/08/2017
Temperature SM 2550 B 21.5 C 05/05/2017
pH SM 4500 H B 6.48 units 05/05/2017
COD SM 5220D 25 mg/L 05/08/2017
Fecal Coliform SM 9222D MF 5800 Colonies/100mL 05/05/2017
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
17-14959 Site: outfall-003 5/5/2017 11:10 AM Water Cindy McDonald
Test Method Results Date Analyzed
Enterococci
Enterolert IDEXX
>2420 MPN/100ml
05/05/2017
Oil & Grease (O&G)
EPA 1664
<5 mg/L
05/15/2017
Residue Suspended (TSS)
SM 254o D
19.7 mg/L
05/08/2017
Temperature
SM 2550 B
23.0 C
05/05/2017
pH
SM 45oo H B
7.04 units
05/05/2017
COD
SM 5220D
<20 mg/L
05/08/2017
Fecal Coliform
SM 9222D MF
1160 Colonies/100mL
05/05/2017
Comment:
Reviewed by: ffa/mL
QI��^
_
_
Aorv�n ff'7n�7 na�o�

4M
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR. DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX 91 rx]-392-4424
[e-mail]
Client: AAl Pharma
PROJECT NAME: Storm Water
REPORT NO: F_7' (c 3j 3 !
ADDRESS:
Contact: Pedro Colon, AAIPharma
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO: Lynette Hodgson
email:
Sampled By:7= I in A SAMPLE TYPE: I = Influent, E = Effluent, W = Weli, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
d
�,
e
m
cC5
" v
c�
"
q w
m
z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
w
Z
$
_
x
_
_o
a
Outfall —
-J
C
P
X
X
�"
TSS, Oil & Grease, COD
G
G
H: -�
C
P
X
Fecal Coliform, Enterococci
G
G
C
P
G
G
C
P
G
G
C
P
G
G
X5
D CnD
G
G
�' • 4
C
P
X
Fe- c,,2- e ,+ .
G
G
C
P
G
G
C
P
G
G
Limits: pH (6-9 units), TSS (60 mg/L), Oil and Grease (30 mg/L), Fecal Coiiform (1,000 colonies/100 MI), Enterococci (500 colonies1100 ml), COD (120 mg/L)
Transfer
Relinquished By:
Datefrime
Received By:
DateMme
2.
Temperature when
Delivered By: Received
Comments:
)le Rted•
:5 Time:
TURNequ OUND:

0 1 T-7
alcami
June 9, 2017
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
To Whom it May Concern:
As part of a recent internal reorganization, Michael Dean Childers has changed roles to
the Manufacturing, Science and Technology Leader. Mr. Childers has been the authorized
representative for the compliance of General Permit NCG060000 to Discharge Stormwater
under the National Pollutant Discharge Elimination System. I, Mark Lewis, Site Director Drug
Product Manufacturing Operations of Alcami Corporation located at 1726 North 23rd Street will
act as an Authorized Representative effective immediately. According to my role I am
authorized to make management decisions, which govern the operation of the facility regulated
under the mentioned permit. Please accept this letter as an authorization for the designation of
a new Alcami Corporation Authorized Representative meeting the requirements under Permit
No. NCG060000(ill)(B)(5).
Sincerely,
0'-PC'r'
Mark Lewis
Alcami Corporation
Site Director, Wilmington Drug
Office: 910.254.7321 1 Mobile:
Product Manufacturing Operations
910,620,0467
ALCAMI CORPORATION 2320 Scientific Park Drive Wilmington, INC 28405 *1 800.575.4224 www alcaminow.com

) alcami
This is to be signed by an authorized official of your firm, as defined under General Permit
NCG060000 III B)(5)(d), after completion of this form.
I certify, under penalty of law, that this document and all attachments were prepared under
my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gather and evaluate the information submitted. Based upon my inquiry of
the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fine and/or imprisonment for knowing violations.
X
Signatur 4 Authorized Representative
Date
ALCAMI CORPORATION 2320 Scientific Park Drive Wilmington, NC 28405 t1 800.575.4224 www.alcaminow.com

SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT
for North Carolina Division of Water Quality General Permit No. NCG060000
Date submitted Jaanuary 17, 2017
7vCERTIFICATE OF COVERAGE NO. NCGO60000 �� 6 A PPLL£ECOLLECTION YEAR 2016
FACILITY NAME Alcami Corporation 1726 N. 23`d Street FACILITY ACTIVITIES INCLUDE (check all that apply):
COUNTY New Hanover _ use/process meats ❑ use animal fats/byproducts
_
PERSON COLLECTING SAMPLES Cindy McDonald K�eEimt _ RGING TO SALTWATERS? []YES ®NO
LABORATORY Envira Chem Lab Cert. # 94 JAIU 27 2017
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
CENTRAL FILES
Part A: Stormwater Benchmarks and Monitoring Results DWR SECTION Total event rainfall 2.27 in. or ❑ No discharge this period3
Outfall No.
Sample Collected,
mo/dd/yr
TSS,
mg/L
pH,
Standard units
COD,
mg/L
Oil and Grease,
mg/L
Fecal Coliform ,
Colonies per 100 ml
Enterococci ,
Colonies per 100 ml
Benchmark
-
100 or 50
Within 6.0 — 9.0
120
30
1000
500
Outfall 001
12/06/2016
13.5 mg/L
6.90
<20 mg/L
<5mg/L
N/A
N/A
Outfall 002
12/06/2016
13.9 mg/L
7.90
<20 mg/L
<S mg/L
N/A
N/A
Outfall 003
12/06/2016
12.2 mg/L
7.46
<20 mg/L
<5 mg/L
N/A
N/A
Only applies to facilities that use/process meats.
2The total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here.
`See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ®no (if yes, complete Part B)
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month.
Outfall No.
Sample Collected,
mo/dd/yr
Oil and Grease,
mg/L
TSS,
mg/L
pH,
Standard units
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
30
100 or 50
6.0 — 9.0
-
1 Only applies to facilities that use/process meats.
2 The total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here.
°See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
SWU-249 Last Revised: October 18, 2012
Page 1 of 2

=i
*FOR PART A AND PART B MONITORING RESULTS:
u A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART It SECTION B.
e 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
o TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy{ of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of
monitoring period in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gatheringthe information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
6t 2a t:i
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SWU-249
Last Revised: October 18, 2012
Page 2 of 2

7
Environmental Chemists, Inc.
' 0 1
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
C.
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 L, Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info(iem irolunenl�llchemisls.com
Alcami (AAIPharma)
Date of Report: Jan 20, 2017
2320 Scientific Park Drive
Customer PO #:
Wilmington NC 28405
Customer ID: 08100002
Attention: Pedro Colon
Report #: 2016-17403
Project ID: Storrs Water
Lab ID Sample ID:
Collect DatetTime Matrix Sampled by
16-41985 Site: outfall-001
12/6/2016 10:00 AM Water Cindy McDonald
Test
Method Results Date Analyzed
Oil & Grease (O&G)
EPA 1664 <5 mg/L 12/19/2016
Residue Suspended (TSS)
SM 2540 D 13.5 mg/L 12/06/2016
Temperature
SM 2550 B 15.1 C 12/06/2016
pH
SM 4500 H B 6.90 units 12/06/2016
COD
SM 5220D <20 mg/L 12/09/2016
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
16-41986 Site: outfall-002
12/6/2016 9:55 AM Water Cindy McDonald
Test
Method Results Date Analyzed
Oil & Grease (O&G) EPA 1664 <5 mg/L 12/07/2016
Residue Suspended (TSS) SM 2540 D 13.9 mg/L 12/06/2016
Temperature SM 2550 B 15.4 C 12/06/2016
pH SM 4500 H 8 7.80 units 12/06/2016
COD SM 5220D <20 mg/L 12/09/2016
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
16-41987 Site: outfall-003 12/6/2016 9:45 AM Water Cindy McDonald
Test Method Results Date Analyzed
Oil & Grease (O&G)
EPA 1664
<5 mg/L
12/0812016
Residue Suspended (TSS)
SM 2540 D
12.2 mg/L
12/06/2016
Temperature
SM 2550 6
15.2 C
12/06/2016
pH
SM 4500 H B
7.46 units
12/06/2016
COD
SMs220D
<20mg/L
12/0912016
Comment:
Reviewed by:
ce'�tj 12 /21r/ ��
G46l/a L-,ay
//.'2 fea,.,.,
Report #:: 2016.17403
Page 1 of 1

l Way
on, NC
min
ENVIRONMENTAL CHEMISTS, I N C OFFICE: 910€1392- 223EIFAX 910-392-4424$
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: AAI Pharma
PROJECT NAME: Storm Water
REPORT NO:
ADDRESS:
Contact: Pedro Colon, AAlPharma
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO:
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
m
E
N
C o
o
cia
c
o m
a
p W
m W
gz
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z
i
o
z
0
=
0
z
o
W
o
Out#all Q
p;
C
P
t�'
X
X
TSS, Oil & Grease, COD
G
G
pH:
C
P
I
I
L
X
Fecal Coliform, Enterococci
G
G
aC.
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Limits: pH (6-9 units), TSS (50 mg1L), Oil and Grease (30 mg1L), Fecal Coliform (1,000 colonies1100 ml), Enterococci (500 coloniss1100 ml), COD (120 mglL)
Transfer
Relinquishe B :
DatelTime
Received By:
Date/Time
z.
Temperature when Received: Acce
Delivered By:
Comments:
le Requested:
Time:
U
TURNAROUND:

. ENVIRONMENTAL CHEMISTS, INC OFFICE: 910i3 2022311FAX g9103 2-44245
%■ 4
Analytical &Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: AAI Pharma
PROJECT NAME: Storm Water
REPORT NO:
ADDRESS:
Contact: Pedro Colon, AAIPharma
PO NO:�
REPORT TO:
PHONEIFAX:
COPY TO:
email:
Sampled By:— SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
m
F
`n
H
E o
cc9
`o
siaE
F�
L
gw
m
gz
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Tem
zz
u
s
o
x
o
z
a
o
Outfali n
X
X
TSS, Oil & Grease, COD
G
G
H:
C
P
X
I
Fecal Coliform, Enterococci
G
G
t3 C
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Limits: pH (6-9 units), TSS (50 mglL), Oil and Grease (30 mg1L), Fecal Collform (1,000 coionies1100 ml), Enterococci (500 colonies1100 ml), COD (120 mg1L)
Transfer
Relinquisher! B •
Date/Time
Received By:
DatelTime
1.
`"alibc,
2.
Temperature when Received: _ _ t•� Accepted: r' Re' Resample Requested:
Delivered By: Received By:�. _ _ Date: — I L, Time:
Comments: TURNAROUND:

ENVIRONMENTAL CHEMISTS, INC
Analyticaf & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: AAI Pharma
PROJECT NAME: Storm Water
REPORT NO: -- 03
ADDRESS:
Contact: Pedro Colon, AAIPharma
PO NO:
REPORT TO:
PHONEIFAX:
COPYTO.
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
fl m
rz
�'
a
a
`o
E
U
c6
o
Y
W
c.�
o f
"
a
Ow
m
g z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
i
z
x
"=
o
x
o
z
p
o
Outfall ���
(
;u
C
P
X
X
TSS, Oil & Grease, COD
G
G
H:
C
P
I
X
Fecal Coliform, Enterococci
G
G
15 �6C
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Limits: pH (6-9 units), TSS (60 mg1L), Oil and Grease (30 mg1L), Fecal Coliform (1,000 colonies1100 ml), Enterococci (500 colonies1i00 m!), COD (120 mg1L)
Transfer
Relinquished y:
DatelTime
Received By:
DateMme
1.
t"4,
O t7'
2•
•
Temperature when Received: ''! Accepted: v Re' d: Resample Re u ted:
Delivered By: Received By. / _Date: Time:
Comments: TOR A OUND:

Yb— ; � 0 -a STQRI3WATER DISCHARGE OUTFACE (SDO)
( �/ r i4TOr1'ITOI2fNG REPORT
Permit Number NCG060000 SAMPLES COLLECTED DURING CALENDAR YEAR: '1015
9ECE1\ E 'his monitoring report shall be received by the Division no later than 30 days from
1 `I t1 the date the rncility receives the sampling results from the laboratory,)
FACILITY NAME: AAI Plzarma Services JAN d � �ui� COUNTY : New Hanover
PERSON COLLECTING SAMPLE(S) Jay Baker PHONE NO. [phone]
CERTIFIED LABORATORY(S) Euviro Chern Lab 94CENTRHL FILES
DWR SECTION SIGNATURE OF PERMITT>:E OR DESIGNEE
RIJQUIR_ 1;D ON PAGf's 2.
Part A. Specific i1'ionitoring Requirements
Outfall
No.
mate
Snntple;CoilecEcd
Total :.:.: ::pH
:Rainfall`.:V.
inu/dd/yr
rriehcs
6-9 rd uarts
Storm porrd
outfall
12/7/2015
0.65
8,27 units
NIA
N/A i
N/A
NIA
N/A I
N/A I
N/A
NIA
N/A
NIA
( N/A
NIA
NIA
N/A I
N/A I
NIA
NIA
NIA I
NIA I
N/A
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons
ifyes, complete Part 13)
ended
3.9 mg/L
<S mg/L
N/A
NIA
N/A
N/A
N/A
N/A
N/A
N/A
I
N/A
N/A
of new motor oil per month? `yes x_no
Demand
r
124 mglC,,'
<20 mo/i'....
NIA
NIA
NIA
NIA
NIA
fart IS: venicle maintenance ACtivrty morirtOM12 i<x urrenrents
Outran
No.
Date , ;
S1n;plc'`
Eollected
50050 ':
i" .. :',:,
::DOSSb.. .. " :_
:00530
00400
Total f~fo�v
(�f applicable) '
:..
TritRl
Rainfall
Or] �C Grease
{rfspl)
Noti'-polar '
OGlIPH
(lVicthad<1G64
SGT 14 M)
Total
Suspended
pH'etiv
Motor
Oil Us1ge
mo/dd/Vr
I MG
inches
m /I
unit
N/A
N/A
NIA
N/A
NIA
NIA I
NIA
NIA
N/A
NIA
NIA
NIA
N/A
N/A
N/A
NIA
NIA
NIA
NIA
N/A
I N/A
N/A
N/A
NIA
N/A
NIA
N/A
Form S WU-247, Iasi revised 2/2/1012
Page I of 2

STORM EVENT CHARACTERISTICS:
Date: Dec 7, 2015
"iota! Event Precipitation (inches): 0.65
Event Duration (hours):2.5hr(only ifapplicable —see permit.)
(if more than one storm event was sampled)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 3vlail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitied is, to the
best of my knowledge and belief, true, accurate, and complete. I am gwarc that there are significant penalties for submitting false information,
including the possibi ' f fines and imprisonment for knowing violations."
3aDrr Cx r S
(Sig ature of Permittee) (Date)
Form 5 W U-247, last revised 21212012
Page 2 of 2

hcC-r) � 61�7;� his
ri���;��ir�rlYlr7 2s20 S:;ailClilC r'cfr �!f•;�' ���I�i7'illlt';tCli, )`�C �:$:�� .r' �]f�.77�.�:}Ll� n�,��'�l�illlc7,� .17'}
December 30, 2015
Central tiles
Division of Water Quality
1617 mail Service Center
Raleigh, North Carolina 27699-1617
Subject: Bi-annual storm water sampling
To whom it may concern,
Enclosed is a paper copy of AAI Pharma Storm water outfali Discharge Monitoring Report (DMR) with
lab analysis attached as required by our permit (NCG060000). The sample was coliected and analyzed
by an approved Environmenta€ Laboratory.
If you have any questions please contact me at [phone],
Regards,
Michael D. Childers
Sr. Director Manufacturing Operations

k�e �rroc .
a --
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.342.4424 Pax
710 BOwsertoivn Road, Manteo, NC 27954 • '252'473.5702 Lab/Fax
255-A Wilmington Highway, facksonvilte, NC 28540 • 910.347.5843 tab/Fax
infoG nvironmcntafchcmists.com
AAI Pharma Date of Report: Dec 16, 2015
2320 Scieniil-rc Park Drive customer PO #:
Wilmington NC 28405 Customer ID: 08100002
Attention: Pedro Colors Report #: 2015-16290
Project ID-. Storm Water
Lab ID Sample ID: CofIect Dateffime Matrix Sampled by
15-313759 . Site; Storm Pond 1217/2015 2.45 PM Water Jay Baker
Test Method Results Date Ana
Enterococci
Emldert IDEXX
43 MPN/100ml
1210712015
Oif & Grease (D&G)
EPA 1664
<5 mg1L
1210912015
Residue Suspended (TSS)
SM2540 D
3.9 mg1L
12108/2015
Temperature
SM25500
12.6C
12/07/2015
pH
SMd500H0
8.27units
12107/2015
GOD
SM 52200
c 20 mg/L
12/1012015
Fecal Colilorm
stas222Dtar=
37 Colonies1100mL 12107/2015
Comment:
r
Reviewed by:
�
ReponX:: 201516'"M -- - — - — - Page Iofi

• _ ENVIRONMENTAL. CHEWSTS, INC
Ana[yticai 8 Consulting Chemists NCDEHR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION m 37729
COLLECTION AND CHAIN OF CUSTODY
71- C5 _/ > Y f
6502 Windmill Way Wilmington, NC 28405
OFFICE. 910.392-0223 FAX [phone]
[e-mail]
Client: AAI Pharma
PROJECT NAME: Storm Water
REPORT NO: � - /� � � o
ADDRESS:
Contact: Pedro Colon, AAIPharma
PO NO:
REPORT TO:
PHONEIFAX:
COPY T0: Lynette Hodgson
email:
Samples[ By: _._. E. ✓��� _ _ �SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludqe, Other:
Sample identification
_T�W
CollectiorT
!
q
H
e
ta' �
o
U
G
v_
a Z
U
p
PRESERVATION
ANALYSIS REQUESTED i
Date
Timemp
o
x
V
_
x
x
a
z
4
a
w
5
Qutfail
'rs
a
C
P
AS
X
X
TSS, Oil 3 Grease, COG
G
G
H: Z
C
P
X
Fecal Golilarrn, Pnterocacc'�
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
_ J
G
G
Limits: pH (6-9 units), TSS (50 mgQ, Oil and Grease (30 mg1L), Fecal Coliform (1,000 colonles110o ml), Enterecocc'l (500 cclon1astic0 ml), COD (120 mglL)
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
Temperature when Received: Accepted: Rejected: Resample Req s
Delivered By:_ _ _ �J Received By: Date: t2.4Tirne:�
Comments:_ TURNA OUND:

Permit Number NCG060000
NC& & o ;L7 9--,
FACILITY NAME: AAI Pharma Services
PERSON COLLECTING SAMPLE(S) Jay Baker
CERTIFIED LABORATORY(S) Enviro Chem Lab # 94
Part A: Specific Monitoring Requirements
STORMWATER DISCHARGE OUT.FALL (SDO)
MONITORING REPORT
01
SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 d,�s from
the date the facility receives the sampling results from the laboratory.)
RECEIVE[) COUNTY: New Hanover
MAY 18 2015 PHONE NO. [phone]
CENT SIGNATURE OF PERMITTEE OR DESIGNEE
�L FILES REQUIRED ON PAGE 2.
DwR SECTION
Outfall
No.
Date
Sample Collected
Total
Rainfall
pH
Total
Suspended
Solids
Oil & Grease
Chemical Oxygen
Demand
mo/dd/yr
inches
6-9 standard units
100 mglL
30 mg/L
120 mg/L
Storm pond
outfall
4/17/2015
0.13
8.62 units
3.2 mg/L
<5 mg/L
20 mg/L
NIA
N/A
N/A
N/A
N/A
N/A
NIA
NIA
N/A
N/A
NIA
NIA
N/A,
N/A
NIA
N/A
N/A
N/A
N/A
NIA
N/A
NIA
N/A
NIA
NIA
N/A
NIA
N/A
N/A
N/A
NIA
N/A
NIA
NIA
N/A
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
Date
50050
00556
00530
00400
Total Flow
Total
Oil & Grease
Non -polar
Total
pH
New Motor
No.
Sample
Collected
(if applicable)
Rainfall
(if appl.)
O&G/TPH
Suspended
Oil Usage
(Method 1664
Solids
SGT-HEM), if
appl.
mo/ddl r
MG
inches
m h
mg/1
unit
al/mo
NIA
NIA
N/A
N/A
N/A
N/A
N/A
N/A
NIA
NIA
N/A
NIA
N/A
N/A
N/A
N/A
NIA
N/A
NIA
NIA
NIA
NIA
N/A
N/A
N/A
N/A
N/A
Form SWU-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date: Feb 2, 2015
Total Event Precipitation (inches): 0.13
Event Duration (hours): 1 hr (only if applicable — see permit.)
(if more than one storm event was sampled)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of Iaw, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
R 1 20 i '-
(Date
•
Form SWU-247, last revised 21212012
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCG060000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME: AAI Pharma Services COUNTY: New Hanover
PERSON COLLECTING SAMPLE(S) Jay Baker PHONE NO. [phone]
CERTIFIED LABORATORY(S) Enviro Chem Lab # 94
SIGNATURE OF PERMITTEE OR DESIGNEE
• REQUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements
Outfall
No.
Date
Sample Collected
Total
Rainfall
pH
Total
Suspended
Solids
Oil & Grease
Chemical Oxygen
Demand
mo/dd/yr
inches
6-9 standard units
100 mg/L
30 mg/L
120 mg/L
Storm pond
outfall
4/17/2015
0.13
8.62 units
3.2 mg/L
<5 mg/L
20 mg/L
N/A
N/A
NIA
N/A
N/A
NIA
NIA
N/A
N/A
NIA
N/A
NIA
NIA
N/A
N/A
N/A
NIA
N/A
NIA
N/A
N/A
N/A
N/A
N/A
NIA
NIA
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
Date
50050
00556
00530
00400
Total Flow
Total
Oil & Grease
Non -polar
Total
pH
New Motor
No.
Sample
Collected
(if applicable)
Rainfall
(if Opp'-)
O&G/TPH
Suspended
Oil Usage
(Method 1664
Solids
SGT-HEM), if
appl.
mo/dd/ r
MG
inches
m /l
mg/1
unit
al/mo
NIA
NIA
NIA
NIA
N/A
NIA
N/A
NIA
N/A
NIA
NIA
N/A
N/A
NIA
NIA
N/A
N/A
N/A
NIA
NIA
N/A
N/A
N/A
NIA
N/A
N/A
N/A
Form SWU-247, last revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS:
Date: Feb 2, 2015
Total Event Precipitation (inches): 0.13
Event Duration (hours): 1 hr (only if applicable — see permit.)
(if more than one storm event was sampled)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
lY Zo _ZYM S
(Date)
N
Form SWU-247, last revised 21212012
Page 2 of 2

.qA
Environmental Chemists, Inc.
• 6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
® 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIfqCA1T, #37729
AAI Pharma Date of Report: Apr 29, 2015
2320 Scientific Park Drive Customer PO #:
Wilmington NC 28405 Customer ID: 08100002
Attention: Pedro Colon Report M 2015-04718
Project ID: Outfali
Lab ID Sample ID: Collect DatefTime Matrix Sampled by
15-10858 Site: Storm Pond 4/17/2015 10:50 AM Water Jay Baker
Test
Fnterococci
Oil & Grease (0&G)
Residue Suspended (TSS)
Temperature
pH
COD
Fecal Coliform
Comment:
Reviewed by:
Method
Results Date Analyzed
e"terolert IDS
<1 MPN1100ml
04/17/2015
EPA 1664
<5 mg1L
04/27/2015
SM 2540 D
3.2 mg/L
0412012015
sM 255013
18.6 C
04/17/2015
SM 4500 H B
8.62 units
04/17/2015
SM 5220D
< 20 mg1L
04/27/2015
SM 8222D MF
<10 Colonies1100mL 04/17/2015
Report#:: 2o15-at71e Page 1 of I

ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 MMindmlli Way Wilmington, NC 26405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: AAI Phanrna
PROJECT NAME: Storm Water
REPORT NO: ! S —
ADDRESS:
Contact: Pedro Colon, AAIPharma
PO NO:
REPORT TO:
PHONEIFAX:
COPY TO: Lynette Hodgson
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
d
E o`
m
o`
o �
ca
PRESERVATION
ANALYSIS REQUESTED
ate
Time
Temp
a
g
6
o
w
Ouffall
f C-
f�Z
X
I
I X
I
ITSS, Oil & Grease, COD
G
G
H: J• L
C
P
X
Fecal Coliform, Enterococci
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Limits: pH (6-9 units), TSS (50 mglL), Oil and Grease (30 mglL), Fecal
Coliform (1,000 coloniesl100 ml), Enterococci (600 coloniesl100 ml), COD (120 mg1L)
Transfer
Relinquished By:
Dateirime
Received By:
DateFrime
2.
.v
Temperature when Received:_ _ !S �_- Accepted: Re ect, d: ResampI Re a ted:
Delivered By: _ Received By: Date: Time:_, r
Comments: TURNAROUND:

AAIPHARMA
AAIPharma 2320 Scientific Park Drive Witminglon, NC 26405 P 910.254.7000 AAIPharma.com
Central Files
Division of Water Quality
1617 mail Service Center
Raleigh, North Carolina 27699-1617
Subject: Bi-annual stormwater sampling
To whom it may concern,
MAY 18.2015
CENTRAL FILES
DWR 'SECTION
May 14, 2015
Enclosed is a paper copy of AAI Pharma Stowmwater outfall Discharge Monitoring Report (DMR) with
lab analysis attached as required by our permit (NCG060000). The sample was collected and analyzed
by an approved Environmental Laboratory.
In case you have any questions please contact me at [phone].
Regar
/W
Pedro Colon
EHS Manager

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCG060000nc
R-4
SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
�/ (This monitoring report shall be received by the Division no later than 30 days from
FACILITY NAME: AAI Pharma Services
PERSON COLLECTING SAMPLE(S) Jay Baker
CERTIFIED LABORATORY(S) •Enviro Chem Lab # 94
Part A: Specific Monitoring Requirements
the date'the facility receives the sampling results from the laboratory.)
Z.. COUNTY: New Hanover
PHONE NO. [phone]
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Outfall
:No.
Date
Sample Collected
Total
Rainfall
pH
Total
Suspended
Solids
Oil & Grease
Chemical Oxygen
Demand
mo/dd/vr
inches
6-9 standard units
100 mg/L
30 mglL
120 mglL
Storm pond
outfall
2/2/2015
0.46
8.93 units
19 mg/L
<5 mg/L
43 mg/L
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
'
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m /l
m /I
unit
al/mo
C_7
I
Form SWU-247, last revised 21212012
Page] of 2

STORM EVENT CHARACTERISTICS:
Date: Feb 2, 2015
Total Event Precipitation (inches): 0.46
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Ail to .10
(Date)
Form S W U-247, last revised 21212012
Page 2 of 2 ,

AMPHARi V lA
AAIPharma 2320 Scientific Park Drive Wilmington, NC 28405 P 910.254.7000 AAlPharma.com
October 23, 2014
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
To Whom It May Concern,
Enclosed is a paper copy of AAIPharma Services Corp's Stormwater Discharge Outfali (SDO)
Monitoring Report for samples collected on September 17, 2014. If you have any questions, please
feel free to contact me at [phone].
Regards,
OLy nette R. Wodgden
Director, Environmental Health and Safety
AAIPharma Services Corp.

SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT
for North Carolina Division of Water Quality General Permit No. NCG060000
Date submitted _ 10-23 - 2.0 ky
CERTIFICATE OF COVERAGE NO. NCG06Q 2 3 I SAMPLE COLLECTION YEAR ktA
FACILITY NAME AA1Plnoicry-o_ Se_rvtic e_s Corp. FACILITY ACTIVITIES INCLUDE (check all that apply):
COUNTY New 1-.l,rinnve_t, ❑ use/process meats ❑ use animal fats/byproducts
PERSON COLLECTING SAMPLES 3d14 9cAokf- - DISCHARGING TO SALTWATERS? ❑YES ZNO
LABORATORY Lab Cert. # 94
Crnerfsts , Inc. PLEASE REMEMBER TO SIGN ON THE REVERSE
Part A: Stormwater Benchmarks and Monitoring Results
Total event rainfall 2 O •G;,, or ❑ No discharge this period'
Outfall No.
Sample Collected,
mo/dd/yr
TSS,
mg/L
pH,
Standard units
COD,
mg/L
Oil and Grease,
mg/L
Fecal Coliform ,
Colonies per 100 ml
Enterococci ,
Colonies per 100 ml
Benchmark
-
100 or 504
Within 6.0-9.0
120
30
1000
S00
9. '3
.19
< 5
NZA
Only applies to facilities that use/process meats.
2The total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here.
4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? 0 yes © no
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month.
Outfall No.
Sample Collected,
mo/dd/yr
Oil and Grease,
mg/L
TSS,
mg/L
pH,
Standard units
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
30
100 or 50
6.0 - 9.0
-
3 Only applies to facilities that use/process meats.
Z The total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here.
`See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
(if yes. complete Part Bj
RECEIVED
OCT 2 7 2014
CENTRAL FILES
DWR SECTION
SWU-249 Last Revised: October 18, 2012
Page 1 of 2

*FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART li SECTION B.
+ TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy_of this DMR, including all "No Discharge" reports- within 30 days of receipt of the lob results (or at end of
monitoring period in the case o "No Discharge" re arts) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
ure of Permittee)
A3oC-4ac71
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SWU-249
Last Revised: October 18, 2012
Page 2 of 2

Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CYEMISTS NCDENR: DWQ CER1'f1:ICATE #94. DLS CEI2MCATE 437729
AAI Pharma Date of Report: Oct 01, 2014
2320 Scientific Park Drive Customer PO #:
Wilmington NC 20405 Customer ID: 08100002
Attention: Sally Strickland Report #: 2014-11602
Project ID: Storm Pond
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-28519 Site: Storm Pond 9/17/2014 7:50 PM Water Jay Baker
Test Method Results Date Analyzed
Oil & Grease (O&G) EPA 16" <5 mg1L 09123/2014
Residue Suspended (TSS) SM 2540 D 9.3 mg/L 09/19/2014
Temperature SM 2550 s 27.6 C 09/17/2014
pH SM 4500 H R 9.19 units 09/17/2014
COD SM5220D 23mg/L 09/26/2014
Comment: .-
Reviewed
Report*: 2014.11602 Page 1 or 1

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION 0 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT: '4441 ` er
PROJECT NAME:
REPORT NO: lff- "662...
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO: ,r.. Sly
PHONEIFAX:
COPY TO:
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Sail, SL = Sludge, Other -
Sample Identification
Collection
10
A CL
N
r
C o
g
6 o
a
m
o�
cLi E
a
PRESERVATION
ANALYSIS REQUESTED
Du to
Time
Temp
z
1
0
=
0
x
0
i
o
P
►*
0•�
C
P
G
G
tic: T
G
G
C
P
G
G
C
P
G
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AAIPharma 2320 5clentific Park Drive Witmington, NC 28405 P 910Z54.7000 AAIPharma.com
May 29, 2014
Mr. Tom Ascenzo
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SUBJ: Biannual stormwater sampling
Dear Mr. Ascenzo:
NC• t�gNB Roalgh Regional Of CO
Enclosed is a paper copy of AA1Pharma's Stormwater Discharge Outfall (SDO) Monitoring
Report with lab analysis attached. Outfall 4001 (storm pond) was checked on 05/15/14 during a
measurable storm event. Mr. Jay Baker with EnviroChem pulled the samples and an onsite
observation was also taken. The sample had a slight grey color and was odorless without any
noticeable floating or suspended solids. None of the testing parameters were out of range. Lab
analysis results are attached for reference. , .
This report contains carefully prepared data, as factual and accurate as possible. Should you have
any questions 1 can be contacted at [phone] or [phone] cell.
i rely,
i kland
EHS Manager
AAIPharma Services
RECEIVED
JUL. 01 2014
CENTRAL FILES
DWQlBOG

EMI -ANNUAL STORMWATER DISCHARGE MON
)RING REPORT
for North Carolina Division of Water Qpalfty General Permit No.
Date submitted r Z
CERTIFICATE OF COVERAGE NO. NCG06 d -A 7 -2-
FACILITY NAME AA1 T%a "r, 5,.Tr V Ze
COUNTY __1yQ1n!{rJ�r
PERSON COLLECTING SAMPLES _ Say_ r
LABORATORY 1�,C►V 1 toc_herv1 Lab Cert. # DWgg14,"DlS 3`7129
1
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR Lo"4
juiJUN 2 5 '20 �
FACILITY ACTIVITIES INCLUDE [check all that applyj:C D2NR Raleigh Regional Office
❑ use/process meats ❑ use animal fats/byproducts
DISCHARGING TO SALTWATERS? DYES [2rNO
PLEASE REMEMBER TO SIGN ON THE REVERSE -)
Total event rainfall a or ❑ No discharge this period'
Outfall No.
Sample Collected,
mo/dd/yr
TSS,
mg/L
PH,
Standard units
COD,
mg/L
oil and Grease,
mg/L
Fecal Coliform ,
Colonies per 100 ml
Enterococci ,
Colonies per 100 ml
Benchmark
-
100 or 50
Within 6.0 - 9.0
120
30
1000
S00
c o t
f)5 /S
i S'(_ f--
91,93
-40 L
L IZ
1 Only applies to facilities that use/process meats.
ZThe total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here.
°See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ❑ no
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month.
Outfall No.
Sample Collected,
mo/dd/yr
Oil and Grease,
mg/L
TSS,
mg/L
pH,
Standard units
New Motor Oil Usage,
Annual average gal/mo
Benchmark
-
30
100 or 50
6.0 - 9.0
-
1 Only applies to facilities that use/process meats.
ZThe total precipitation must be recorded using data from an on -site rain gauge.
3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here.
°See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
(ifyes, complete Part B)
SWU-249 Last Revised: October 18, 2012
Page I of 2

*FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART 11 SECTION B.
+ 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO 5X
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DM& including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of
monitoring period in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SWU-249 Last Revised: October 18, 2012
Page 2of2

Environmental Chemists, Inc.
6602 Windmill Way • WiImington, NC 28405 ,nvirochem(910) 392-0223 (Lab) • [phone] (Fax)
® 710 bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DL5 CERTIFICATE #37729
AAi Pharma Date of Report: May 27, 2014
2320 Scientific Park Drive Customer PO #:
Wilmington NC 28405 Report#: 2014-05696
Attention: Sally Strickland Report to: Sally Strickland
Project ID: Storm fond
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-13775 Site: outfall 6/16/2014 4:25 PM Water Jay Baker
Test Method Results Date Analyzed
Oil & Grease (O&G) EPA 1664 <5 mg/L 05/2112014
Residue Suspended (TSS) SM 2540 D 12.5 mg/L 05/16/2014
Temperature SM 2550 3 26.8 C 05/15/2014
pH SM4500 H R 8.53 units 05/1512014
COD SM 52201) < 20 mg/L 05/19/2014
Comment: r
Reviewed by: dio, ` le"I
ga, 'girl
�egtiarial 0 �
N� D�
Report#:: 2014-0569B Page 1 of I

6602 Windmill Way , NC
ton
ENVIRONMENTAL CHEMISTS, INC OFFICE: 91D3 20223iFAX9910-302-44245
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: AAl Pharma
PROJECT NAME: Storm Water
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONEIFAX:
COPY TO:
email:
Sampled By: J �r n ."Pr, SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, 50'= Soil, SL = Sludge, Other:
Sample Identification
Collection
m
y
W D
o (a
m _
a
" v
m
c'
"
a
C
?
a
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
o
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d
Y
2
Z
_
o
q
o
Outfal!
rC ►�
/tL
It Y
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Received By:
Datefrime
1.
2.
Temperature when Received -_ Accepted: -�
Delivered By. �� — _ Received By:
Comments:
Resample ues d:
Re
Date: Time:
TU N OUND: