NCG060186_MONITORING INFO_20160426

STORMWATER DIVISION CODING SHEET
NCG PERMITS-.
PERMIT N0.
DOC TYPE
❑HISTORICAL FILE
� MONITORING REPORTS
DOC DATE
El C20 1 (� o y a �
YYYYMMDD

STORMWATER DISCHARGE OU'1'1+ALL (SDO)
MONITORING REI'0R'1'
GENERAL PERMIT NO. NCG060000 SAMPLES COLLECTEII DURING CALENDAR YEAR; I
C1+:UTIMCATE, OF COVERAGE NO�NCG06-0ISt (`Phis monitoring report Is dae'nt the ])!vision no later tliau 30 (lays fri,ru
�`- the date tine facility receives the aarnpling results from the laboratory.)
FACILITY NAME (nle..y�-�_�c.rn15 L.0 C -COUNTY Sufr
PERSON COI,I,ECT!NG SAMPLES �.,., o,,�`,;_ PHONE No. (33 6) -.31FG-- s 2W 1
CI�ItTII+IEU I..Al3OlC?.'1'(IItY ur n f:r„ t' 1- -Lab B. 37ij�-��11`tu --
' I al► ii
]'art A-. Specific Monitoring Requirements
APR 2 6 2016
nmm ci:rTION
PLEASE SIGN ON TILE 11EVERSE 4
OutfutU. ._
r
Date =,..
S`umple .
.. I
¢Ile(red,'
nill
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((ilnnleei'per 1lIQ nrl
lend trots! It
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,,`t..^'WifliltiCi:'4 .,�.0
`�20
;i=30, r -
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Note: If you report a sampled value in excess of [lie benchmark value, or outside the benchmark range for pil, you mast implement Tier 1 or Tier 2 responses.
See General I'em;it text.
Did this faciIily perform Vehicle Maintenance Aotivities using more than 55 gallons of new motor oil per mouili? _yes _no
(iryes, engypicte fart H)
Pad It. Vehicle Maintenance Activity Monitoring Requirements
---
'nrelfall. nute=. = 00_556 00530.::., r ;.<,:,:_': '.00400 c�;.
No: Sarnlile C trllect d; µ OLl niul Gi euse,r :']'Drat usn'etiiled Sgli(lit, ;till;!: ..Nr w, 'Iota; -- l•Usul;e;
nurldd! t om_ ; ' _wn1'"/r:, rn lL,:= Stirridgrd'iltrits .,.:..'' Ailiiititi.aV6itic al/tno
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for p11, you must implement Tier 1 or Tier 2 responses.
See General Pem►it text_
STORM EVENT CHARACTERISTICS:
Date (first event sampled)
Total Event Precipitation (inches):
Bate (list each additional event sampled this reporting period, and rainfall amount)
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central miles
1617 Mail Service Center
Raleigh, North Carolirua 27699-1617
Total Event Precipitation (Indies):
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for p11, you must implement Tier 1 or Tier 2 responses.
See General Pem►it text_
STORM EVENT CHARACTERISTICS:
Date (first event sampled)
Total Event Precipitation (inches):
Bate (list each additional event sampled this reporting period, and rainfall amount)
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central miles
1617 Mail Service Center
Raleigh, North Carolirua 27699-1617
Total Event Precipitation (Indies):

"l certify, under penalty of law, that this document and all attachments were prepared under nay direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based oil my inquiry of file person.or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete, - I Am aware that there are significant penalties for sub><nitting false information, including
the possibility of fines and imprisonment for knowing violations.,, .. I
(Signature of Pe"Ilm"ttee
B
SW U-249-1 U21 U7
Page 2 of 2

STOWWWATE'R DISCHARGE OUITAl.,I., (5I)O)
a MONITORING REIfOPT
(: ENEIZAI.. I'RIlit11T NO. NCC0600011 SA[Vi1'1,ES COLLECTED 1],C.lit.ING (:ALENDAR YEAR;
CIEUI I ICATF, 01? COVER.kCI , NO. WC06-►$% (This nlrinitrll-i ig report is dne llt the Divisiioll uo lacer than 31) Buys frilltt
the dale Hke (al:lllly r'eeClr'y the 11111I111t: rel1111iN fr-I1111 thr. 1a1101-111111'y,)
Ir.tC II,I'1'�'NAIVII, C..Ja L,=!^�_ �L Ce1la
OUN•1'Y Sur f
1'1OtSON COI.,I..VC;TI C, SAt%-4PL ?.!i _ ���Qo.,,1�, 1'I10NIt: NO.
' 1.11 h H __31111
1.,111111 .PLEASE SIGN ON 111111E REVERSE 4
Pall A: tilleciftc Mnllitnl-Ing Ilctlmirenleuts
0''0400
',�Ih:;:';; •' !,1
`f �„i%,0����h� -:-
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1\[fIIr: Irpill I-q)oI1 11 8a111pIrd vaIiir It1 excess of I I I c hrniclnnark valluc, or- olltslltr, the hCticAll11111'1i r a lgc It1r III I, volt IIII st if111)1cl11rill Ti I of TIC!' 2 rusp{)E1ani
, , (icllCrel PCI-111t1 tcxl.
1)id Ilds Facility perfilrnl Vellicic Maintennnca Antivitics using niorc Ihan 55 p1lons of flew motor oil 1101. rnonlll? _ yes _1141
ff ycs, ('nrllplctc Palt IA)
Parl It: Vl:l,lele Malllteliance Aclfvity Mmillorill IUrd
-.-011ifa11.'--f1�i11r p 'A0
• NEE: '' .!Ya„11Sic Cl,iFec��1i, ,.O'i1.lknd
NEllc: If yell report n mniplcd vahie ill exceas of 1
Ioce 6CF1CfE11 Pef-1l11[ ICxI-
4'1'()I. M I!;V11'.NT CIIAll ACI'E RISTICS:
Dale, (first event sampled)
'fetal hvcul Pleclpitatiou (Illi:hes);
ul1•en1e11t8
00530.
I'ofASuyphlirlud 51111r141 ;rilT,i��;. ' :New- �rrtnr.Ol1.T.Td:ige;
�: In !I1<.: 5tilrl'diwl 11 gial 9 Aiiprtitl:Avr„_ru1;n baVulf)
jp
Imlal lUVEdUC, of OUISWO l
u:hnlark rango for hI1, you must implonmot Tiu- 1 or Ticr 2 responscs.
Ilnft: (list each adclitiollal event snlrrfiltd tills relrnrfing lll:rinll, 1111d r11111fn11 11111(iukit)
'I ahl 1?'.Ma rkt 111-ecf111tillian (illralcNI:
Milli Orlglild and 011e emlly to:
Nvisinm of, Walter Qualily
Attll: DWQ Ccl,tial Files
1617 Mail Srrvic.c Ctider
ki.alcigh, North Carolina 27699-1617
S

0
novo nordisl<
RECEIVE®
October 26, 2015 O C T 3 0 Z 015
CENTRAL FILES
Central Files DWR SECTION
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Per the requirements of Novo Nordisk Pharmaceutical Industries' stormwater discharge General Permit
NCG060000 and Certificate of Coverage No. NCG060048, attached are the results from the qualitative
monitoring and analysis carried out on September 28, 2015.
1 may be reached at 919-550-2200 at extension 2217 if you have questions.
Sincerely
R. Paul Morris
Novo Nordisk Pharmaceutical Industries, Inc
3612 Powhatan Rd
Clayton, NC 27527

(�IaceAnalytical"
wwwpacelabs.com
October 08, 2015
Mr, Paul Morris
Novo Nordisk Pharmaceutical
3612 Powhatten Rd
Clayton, NC 27520
RE: Project: Stormwater
Pace Project No.: 92269471
Dear Mr. Morris:
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on September 28, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
'84AQnT d'. &4 ,yt-,
Brittany Gibson
[e-mail]
Project Coordinator
Enclosures
cc: Accounts Payable, Novo Nordisk Pharmaceutical
F,CCR
TNI: V:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13

Pace Analytical Services, Inc.
ace Analylca! 0 205 East Meadow Road - Suite A
Eden, NC 27288
wwwpacelabs.com [phone]
CERTIFICATIONS
Project: Stormwater
Pace Project No.: 92269471
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification*: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Bioassay Certification #: 16
worth Carolina Drinking Water Certification M 37731
Flodda/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
UrginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 13

aceAnalytrcal
www.pacejabs.com
i
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Projecl: Stormwater
Pace Project No.: 92269471
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92269471001 SW-1 EPA 1664B
JMS
1
PASI-C
SM 25400
RC
1
PASI-R
SM 5220D
WRC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fall,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 13

aceAnallytical
www.pac*labs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Project: Stormwater
Pace Project No.: 92269471
Method: EPA 1664E
Description: HEM, Oil and Grease
Client: Novo Nordisk Pharmaceutical
Date: October 08, 2015
General Information:
1 sample was analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form ($CUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 13

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Project: Stormwater
Pace Project No.: 92269471
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Novo Nordisk Pharmaceutical
Date: October 08, 2015
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: RWETI8693
D6: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
• DU (Lab ID: 1569519)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analyticat Services, Inc.. Page 5 of 13

A
aceAnalytrcal
wwwpacEgabs.com
f
Pate Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Project: Stormwater
Pace Project No.: 92269471
Method: SM 5220D
Description: 5220D COD
Client: Novo Nordisk Pharmaceutical
Date: October 08, 2015
General Information:
1 sample was analyzed for SM 5220D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc„ Page 6 of 13

acmnalytrcal
wwwpacelabs.com
i
ANALYTICAL RESULTS
Project: Stormwater
Pace Project No.: 92269471
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: SW-1
Parameters
Lab ID: 92269471001 Collected: 09/26/15 16:00
Results Units Report Limit DF
Received: 09/28/15 10:25 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L
5.0 1
10/08/15 09:50
25400 Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg1L
3.3 1
09/29/15 12:40
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg1L
25.0 1
10/01/15 16:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:14 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 13

ace Analytical
wxwpacelabs.com
QUALITY CONTROL DATA
Project: Stormwater
Pace Project No.: 92269471
QC Batch: GCSV122838 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92269471001
METHOD BLANK: 1577261
Associated Lab Samples: 92269471001
Parameter knits
Oil and Grease mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 10/08/15 09:41
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 1577262 1577263
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RP❑ RPD Qualifiers
Oil and Grease mg1L 40 35.6 36.5 89 91 78-114 2 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:14 PM without the written consent of PaceAnalytical Services, Inc..
Page 8 of 13

acmnalytical
wnwpacefabs.rnm
1
QUALITY CONTROL DATA
Project: Stormwater
Pace Project No.: 92269471
QC Batch: RWET18693 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lat) Samples: 92269471001
METHOD BLANK: 1569194 Matrix: Water
Associated Lab Samples: 92269471001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 09/29/15 12:37
Pace Anatyticat Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1569195
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 260 104 90-110
SAMPLE DUPLICATE: 1569519
92269368001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 11.6 10.2 14 D6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:14 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 13

laceAnalytical"
wwwpacelabs.mn
QUALITY CONTROL DATA
Project: Stormwater
Pace Project No.: 92269471
QC Batch: WETA124750 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92269471001
METHOD BLANK: 1570935
Associated Lab Samples: 92269471001
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 10/0111516:00
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1570936
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 731 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1570937 1570938
MS MSD
92269580001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 89.0 750 750 764 764 90 90 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1570939 1570940
MS MSD
92269653004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L ND 750 750 711 711 94 94 90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:14 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 13

ace Analytical
www.pacelabs.c=
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Project: Stormwater
Pace Project No.: 92269471
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantilation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/0812015 04:14 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 13

aceAnalytical
wwwpacelabs.com
E
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project:
Stormwater
Pace Project No.:
92269471
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92269471001
SW-1
EPA 16646
GCSV122838
92269471001
SW-1
SM 25400
RWET18693
92269471001
SWA
SM 5220D
WETA124750
Date: 10/08/2015 04:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 13

CHAIN -OF -CUSTODY / Analytical Request Document
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