NCG060101_COMPLETE FILE - HISTORICAL_20160405

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO. /V C& DLL O 1 0 1
DOC TYPE I � HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE ❑ SDI LF C'f' OG�
YYYYMMDD

Energy, Min era I
and Land Resources
ENVIRONMENTAL QUALITY
April 5, 2016
Marc Bumgarner
209 Watlington Industrial Dr.
Reidsville, NC 27320
Subject: Compliance Evaluation Inspection
Permit No. NCG 0601.01.
Dystar LP
Rockingham County
Dear Mr. Bumgamer:
PAT MCCRORY
Govemar
DONALD R. VAN DER VAART
Secretary
TRACY DAMS
On March 23, 2016 Glen White of the North Carolina Department of Environmental Quality;
Department of Minerals and Land Resources met with you and Johnny Somers at the Watlington
Road facility in Reidsville, NC to conduct a compliance inspection per the Industrial Stormwater
Permit requirements. Inspection consist of review of the Stormwater Pollution Prevention Plan,
training and monitoring records and observation of the general condition of the site and outfall.
Your assistance with the inspection was greatly appreciated.
Permit:
The Asphalt plant holds General Stormwater Permit NCG060101 to discharge stormwater from
industrial activity associated with Soaps, Detergents, Cleaning Preparations; Perfumes,
Cosmetics and Other Toilet Preparations [SIC 2841 under the National Pollutant Discharge
Elimination System (NPDES). The permit became effective December 1, 2012 and expires on
October 31, 2017. A copy of the current permit is required to be maintained with the Stormwater
Pollution Prevention Plan (SPPP) documents. The current permit was included in the file.
Recordsaeports:
This facility was required to develop and maintain a Stormwater Pollution Prevention Plan
(SPPP) in accordance with Part II, Section A of the permit. The document is well prepared. The
documents have been maintained and past documents were available for review at the time of
inspection. The last spill was reported on January 28"'. The spill and clean-up are well
documented and NCDENR was notified of the incident and clean-up. No deficiencies noted.
Facility Site Review:
This facility manufactures soaps, detergents and various chemical products for commercial
clients. Many of the products are created in the facility and shipped out with the client
company/product name. No issues noted on site review.
State of North Carolina I Environmental Quality I Energy, Mineral and Land Resources
450 Hanes Mill Road — Suite 300
Winston-Salem, NC 27105
[phone]

Self -Monitoring Program:
The facility is required to conduct qualitative and analytical monitoring twice annually. Records
show that monitoring has been conducted as required and results are within the required permit
parameters. Outfalls were observed. One had a soapy discharge but it was believed to be from
residue on the parking lot. Dystar has missed one monitoring event in the last two years and has
had one sample with elevated parameters. No other deficiencies noted. The plant was compliant
at the time of inspection.
If you have questions or need additional information, please contact Glen White at (336) 776-
9660.
Enclosures:
Inspection Report
Sincerely,
Matthew E. Gantt, P.E.
Regional Engineer
Land Quality Section
Winston-Salem Regional Office
cc: WSRO File Copy
Division of Energy, Mineral and Land Resources (WSRO)

Compliance Inspection Report
Permit: NCG060101 Effective: 12/01112 Expiration: 10/31/17 owner: Dystar LP
SQC: Effective: Expiration: Facility: DyStar LP
County: Rockingham 209 Watlinglon Industrial
Region: Winston-Salem
Reidsville NC 27320
Contact Person: Johnny Somers Title: Phone: [phone]
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 03123/2016
Primary Inspector: Glen White
Secondary Inspector(s):
Certification:
Phone:
Entry Time: 11:00AM Exit Time: 1 1:30AM
Phone: [phone]
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Food!Tobacco/Soaps/CosmetiWPublic Warehousing Stormwater Discharge COC
Facility Status: ® Compliant [] Not Compliant
Question Areas:
® Storm Water
(See attachment summary)
Page: 1

permit: NCG060101 Owner- Facility: Dystar LP
Inspection Date: 03/2312016 Inspection Type : Compliance EvaEuation Reason for Visit: Routine
Inspection Summary:
(See Compliance Inspection Report)
Page: 2

Permit: NCGO60101 Owner - Facility: Dystar LP
Inspection Date: 03/2312016 Inspection Type : Compliance Evaluation Reason for Visit: Routine
Stormwater Pollution Prevention Plan
Does the site have a Stormwater Pollution Prevention Plan?
# Does the Plan include a General Location (USGS) map?
# Does the Plan include a "Narrative Description of Practices"?
# Does the Plan include a detailed site map including outfall locations and drainage areas?
# Does the Plan include a list of significant spills occurring during the past 3 years?
# Has the facility evaluated feasible alternatives to current practices?
# Does the facility provide all necessary secondary containment?
# Does the Plan include a BMP summary?
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
# Does the facility provide and document Employee Training?
# Does the Plan include a list of Responsible Party(s)?
# Is the Plan reviewed and updated annually?
# Does the Plan include a Stormwater Facility Inspection Program?
Has the Stormwater Pollution Prevention Plan been implemented?
Comment: SPPP current and compliant.
Yes No NA NE
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9 110 ❑
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In JanuarV 2013 Anna visited the site followinq a spill that occured. Clean-up was in process.
Spill and response was well documented.
Qualitative Monitoring
Yes No NA NE
Has the facility conducted its Qualitative Monitoring semi-annually? ® ❑ ❑ ❑
Comment: Current.
Spring
2q 014
(Missed Monitoring)
Fall
2014
(Compliant)
Spring
2015
(Compliant)
Fall
2015
(Compliant)
Analytical Monitoring
Has the facility conducted its Analytical monitoring?
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
Yes No NA NE
Comment: Spring 2014 (Missed Monitoring) Since one req'd monitoring was missed and only
one sample was elevated
Fall 2014 (Compliant) Facility was found to be compliant.
Spring 2015 [Elevated/Compliant)
Fall 2015 (Complaint)
Permit and Outfalls
Yes No NA NE
# Is a copy of the Permit and the Certificate of Coverage available at the site? ® ❑ ❑ ❑
Page: 3

Permit: NCGO50101 Owner - Facility: bystar LP
Inspection Date: 03/2312016 Inspection Type : Compliance Evaluation Reason for Visit: Routine
# Were all outfalls observed during the inspection? ® ❑ ❑ ❑
# If the facility has representative autfall status, is it properly documented by the Division? ❑ ❑ ® ❑
# Has the facility evaluated all illicit (non stormwater) discharges? IM ❑ ❑ ❑
Comment: Outfalls observed. There was a soapy discharge but it is believed to be from residue on the
parking lot. One spill_was noted in January 2013. Clean up response and notification was swift
and damage was minimal.
Page: 4

v
DyStar Q'
January 30, 2013
RECEIVED
Ms. Aana Taylor -Smith N.C.aeol. of ENR
Environmental Specialist JAN 3 1 2013
North Carolina Department of Environment and Natural Resources
Division of Water Quality v,r,s�:.i� Salem
585 Waughtown Street Re Icnai office
Winston-Salem, NC 27107
Dear Ms. Taylor -Smith:
Thank you for corning to DyStar LP in Reidsville today to see the site after our phone conversation
on January 20. This letter is to document what happened as well as the proactive steps we made
to repair the incident.
At 11:45pm on January 27`h, I received a phone call at home. Our facility operates from I Ipm on
Sundays to 7pm on Fridays so the first shift for Sunday night had not been at the facility long.
Apparently sometime over the weekend while no one was at the facility, a pipe supplying water to a
safety shower in our outside storage tank farm froze and burst. Water filled the containment area
of the tank farm and went into the tanker bay containment area. This area has a valve that did not
hold and water entered into the wastewater lines to our equalization basin. This basin overfilled
and wastewater began to spill over and into the storm water spillway.
At that time, we shut an emergency -valve to prevent any more water to go into the basin and turned
off the agitators to prevent any splashing of wastewater out of the basin. "Stay -dry" was put
around the catch basins to keep any wastewater from entering the spillway as well as prevent any
soil exposure. The basin level was then lowered by treating the water in our DAF unit and sent to
the City of Reidsville. It was dark and so no evaluation could be done for the spillway and creek
until Monday the 28a'. Once it was determined that wastewater indeed entered the creek, CTW
Specialties was contracted to preform remediation and I contacted you. On the 28t°, you requested
I call the City of Reidsville to notify them and you indicated you would come to inspect today.
As you saw, the spillway, creek bed and soil around the wastewater basin were cleaned. Water
was flushed through the drains to the creek and into a vacuum truck. -The truck then discharged the
water into our wastewater basin to avoid any offsite disposal. The "stay -dry" was collected in
drums.
Again, thank you for coming today and being of assistance. If there is anything else I need to do or
if there are any questions you have, please let fuel know.
Sincerely,
Marc C. Sum er
Site Manager — Reidsville Location
DyStar LP
® ISO 8001 DyStar LP
-! Certified Worldwide 209 WoUington Industrial Drive
Reidsville. NC 27320
Phone: (336) 342-W31 Fax: [phone]
www.EYyStarlp.com

`Q�6F WAL4'R
C r
Incident Report
Report Number: 201300234
Incident Type: spill (Oil, Chemical, non -sewage) On -Site Contact:
Category: Incident
First/Mid/Last Name:
Incident Started: 01/27/2013
Company Name:
County: Rockingham
Phone:
City:
Pager/Mobile Phone:
1
Farm #:
Responsible Party:
Reported By:
Owner:
First/Mid/Last Name:
Marc Bumgamer
Permit:
Company Name:
Facility:
Address:
209 Watlington Industrial
First Name:
Middle Name:
City/State/Zip:
Reidsville NC 27320
Last Name:
Phone:
[phone]
Address
Pager/Mobile Phone:
1 [phone]
City/State/Zip:
Phone:
Material Category: Estimated Qty: UOM
DD:MM:SS Decimal
Chemical Name Reportable Qty. lbs. Reportable Qty. kgs.
Position Method:
Latitude: Position Accuracy:
Longitude: Position Datum:
Location of Incident: DyStar LP
Address: 209 Watlington Industrial Dr
City/State/Zip Reidsville NC 27320
Report Created 01/31/13 01:02 PM Page 1

i
CauselObservation: Directions:
The plant manager, Mark Bumgamer, received a call at 11:45
PM on Sunday the 27th that a potable water pipe had burst in
their tank farm and was discharging water into the tank farm s
containment area. The containment valve failed, which resulted
in the potable water being discharged into a lowered area where
there is a drain to their equalization tank for the pretreatment
system. The addition of this potable water overflowed the
300,000 gallon EQ tank, which was about 75% full prior to the
pipe bursting.
Action Taken: Comments:
DyStar staff shut off the flow, turned off agitators in EQ tank, and Aana Taylor -Smith visited site on 1/3012013. Area was clean and no
turned on OAF unit to start treatment. The catch basin was diked residue was found in or near outfall. There was no discoloration in the
to reduce flow to stream. DyStar contacted CTW Specialties of creek. Spill appears to have been cleaned up to the extent possible.
McLeansville, who diked the outfall, flushed the catch basins,
and pumped the water from the outfall. They also cleaned the
area and put down absorbent material, which has since been
raked up, All pumped water was discharged to DyStar's
pretreatment system.
Incident Questions:
Did the Material reach the Surface Water? Yes
Surface Water Name? Little Troublesome Creek
Did the Spill result in a Fish Kill? No
If the Spill was from a storage tank indicate type.
Containment? Unknown
Cleanup Complete? Yes
Water Supply Wells within 1500ft : unknown
Event Type
Event Date
Incident closed
Report Entered
2013-01-30 01:17:52
Requested Additional Information
2013-01-30 12:00:00
Report Received
2013-01-28 03:00:00
Conveyance: Unnamed tributary
Estimated Number of fish? 0
(Above Ground or Under Ground)
Groundwater Impacted : Unknown
Due Date Comment
Report Created 01/31/13 01:02 PM Page 2

a .
Referred to Regional Office - Primary Contact 2013-01-28 03:00:00
Incident Start 2013-01-27 11:00:00
Standard Agencies Notified:
Agency Name Phone First Name M.I. Last Name Contact Date
Other Agencies Notified:
Agency Name Phone First Name M.I. Last Name Contact Date
DWO Information:
Report Taken By: Report Entered By: Regional Contact:
Aana Taylor -Smith Aana Taylor -Smith Aana Taylor -Smith
Phone:
Date/Time: 2013-01-28 03:00:00 PM 2013-01-30 01:17:52 PM 2013-01-28 03:00:00 PM
Referred Via: Phone Phone
Did DWO request an additional written report? 2013-01-30 12:00:00 AM
If yes, What additional information is needed?
Report Created 01/31/13 01:02 PM Page 3

s
1
y �dy"7f
.iy

Taylor -Smith, Aana
From: Somers, Johnny [[e-mail]]
Sent: Wednesday, January 30, 2013 3:52 PM
To: Taylor -Smith, Aana
Subject: DyStar LP Clean up Photos
Attachments: EQ Basin Overflow 003.jpg; EQ Basin Overflow 004.jpg; EQ Basin Overflow 005.jpg; EQ
Basin Overflow 006.jpg; EQ Basin Overflow 007.jpg; EQ Basin Overflow 008.jpg; EQ Basin
Overflow 001.jpg; EQ Basin Overflow 002.jpg
Aana
Thanks for your visit this morning. The photos you requested are attached for your files.
Johnny Somers
Quality Manager
Aft
DyStar'•'
DyStar LP
209 Watlington Industrial Drive Reidsville, NC 27320
Phone: [phone] Fax: [phone] Mobile: [phone]
Email: [e-mail] f Skype: somers.johnny
Commlrred to susroi'nab!llty
AThImRjgreeln betare you print thls,scteen
The DyStar Group is also proud member and supporter of bluesETAD I GQTS [ REACh I SAC I SDC TE UNGC
Visit us @ www.DyStar.com i Follow us on ® Ki OUR 0
DyStar Confidentiality Notice:
This message and any attachments are confidential and intended only for use by the recipient named above.
Unauthorized disclosure, distribution or copying of this communication and the information contained in it is strictly
prohibited. If you are not the intended recipient, please notify us immediately and delete the message and any
attachments. Thank you.

Thomas, Mike
From: Basinger, Corey
Sent: Monday, October 08, 2012 1:57 PM
To: Thomas, Mike
Subject: FW: BIP MSDS
Attachments: image001.png; image002.png; image003.png,- image004,png; image005.png; image006.png;
BIP Phthalimides. pdf
Last email about Dystar
W. Corey Basinger
Regional Supervisor
Surface Water Protection Section
Winston-Salem Regional Office
Division of Water Quality
Email: corey.basineerOncdenr.eov
Phone: [phone] -
Fax [phone]
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Caw and may be disclosed to
third parties.
From: Bumgarner, Marc, DyStar/US[mailto:bumgamer,[e-mail]]
Sent: Thursday, October 04, 2012 12:03 PM
To: Basinger, Corey
Cc: Somers, Johnny
Subject: RE: BIP MSDS
Attached is the MSDS for BIP Phthalimides. As discussed, no material was spilled into any surface waters. Any material
that was spilled was contained within our wastewater pretreatment facility. Results from our water discharged to the
City of Reidsville are within the limits for BOD. As you can see in the MSDS, the BOD for this product is 349,000 mg/L
and our discharge to the City was 1100 mg/L.
Please let me know if you have any further questions.
Thanks,
Marc Bumgarner
Site Manager
Reidsville Location
Aft
DyStar
DyStar LP
209 Watiington Industrial Drive Reidsville, NC 27320
Phone: [phone] Fax: [phone] I Mobile: [phone]
Email: bUl' [e-mail] 1 Skype: bumgarner.marc
Sustaunabidity is our responsibility
Think green before you print this screen
Visit us @ www.DyStar,com I Follow us on ® 91 ® 0

DyStar Confidentiality Notice:
This message and any attachments are confidential and intended only for use by the recipient named above. Unauthorized disclosure, distribution or
copying of this communication and the information contained in it is strictly prohibited_ if you are not the intended recipient, please notify us immediately
and delete the message and any attachments. Thank you.
From: Basinger, Corey Imalto:[e-mail])
Sent: Thursday, October 04, 2012 11:16 AM
To: Bumgarner, Marc, DyStar/US
Subject: BIP MSDS
W. Corey Basinger
Regional Supervisor
Surface Water Protection Section
Winston-Salem Regional Office
Division of Water Quality
Email: [e-mail]
Phone: [phone]
fax [phone]
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to
third parties.

r
DyStiar"�' Material Safety Data Sheet
Protective Clothing
HCS
DOT
CR7 *
Class: Irritating substance.
0
Section 1. Product Identification and Uses
Synonyms
Not available.
11MIS
H 1 F 1 R 0 PE B
Commonfrrade name
BIP Phthalimides
TSCA
TSCA inventory: All components listed.
TSCA 12(b) one time export: Not
Listed.
TSCA 12(b) annual export notification:
Not Listed.
Chemical name Not applicable.
Chemical formula Not applicable.
Chemical family
Blend of n-Butyl and Isopropyl Phthalimides.
DSL
CEPA DSL: Listed.
CEPA NDSL: Not Listed.
Manufactured/Supplied
Dystar L.P.
209 Watlington Rd.
Reidsville, NC 27320
USA
[phone]
CAS#
Mixture.
Material uses
Textile industry: Dyeing assistant.
Code
FDA-0200
Validation Date
Validated on 10117/2008.
Molecular weight
Not applicable.
Revision Number
1.0
Section IA. First Aid Measures BIP Phthalimides
Eye contact Check for and remove any contact lenses. In case of contact, immediately flush eyes with plenty of water for at least
15 minutes. Get medical attention if irritation occurs. to
Skin contact In case of contact, immediately flush skin with plenty of water. Remove contaminated clothing and shoes- Wash
clothing before reuse. Thoroughly clean shoes before reuse. Get medical attention if irritation occurs.
Ilazardous inhalation It inhaled, remove to fresh air_ If not breathing, give artificial respiration. If breathing is difficult, give oxygen. Get
medical attention if symptoms appear.
Hazardous ingestion Do NOT induce vomiting unless directed to do so by medical personnel. Never give anything by mouth to an
unconscious person. Loosen tight clothing such as a collar, tie, belt or waistband. Get medical attention if symptoms
appear.
Section It. Hazardous Ingredients BIP Phthalimides
Name
CAS #
% by Weight
TLV/PEL
LCsolLDso
1) isopropyl phthalimide
304-17-6
20-30
Not available.
Not available.
2) n-butyl phthalimide
1515-72-6
60-80
Not available.
ORAL (LD50): Acute: 1100
mg/kg [Rat).
Section Ill. Physical Data BIP Phthalimides
Physical state and
Liquid. Odor Slight.
appearance
pI4 and Solution Conc.
Not applicable. Not available- Taste Not available.
Odor threshold
Not available.
Color Yellow. (Light.)
Volatility
0% (w1w).
\letting point
5°C (41 °F)
Continued on Next Page

BIP Phthatimides
FDA-0200 Page Number. 2
Boiling point
260°C (536`F)
Specific gravity
1.13 (Water = 1)
Vapor density
Not available.
Vapor pressure
Evaporation rate
Viscosity
Not available.
Not available. i
Not available.
lonicity (surface active
agent)
Not applicable.
Critical temperature
Instability temperature
Not available.
Not available.
Conditions of instability
Not available.
Dispersion properties
Not available.
Solubility
Insoluble in cold water.
VOC's (g/LXEP.1 24/24A)
0 (g/1).
HAPs or TAPS
Clean air act (CAA) 112 accidental release prevention: Not Listed.
Clean air act (CAA) 112 regulated Flammable substances: Not Listed.
Clean air act (CAA) 112 regulated toxic substances: Not Listed.
Section IV. Fire and Explosion Data BIP Phthalimides
The product is:
May be combustible at high temperature.
Auto -ignition temperature Not available.
Fire degradation products
Not available.
Flash points
CLOSED CUP: Higher than 93.3°C (200°F).
Flammable limits
Not available.
Fire extinguishing
procedures
SMALL FIRE: Use DRY chemical powder.
LARGE FIRE: Use water spray, fog or foam. Do not use water jet.
Flammability
Slightly flammable to flammable in presence of open flames and sparks.
Risks of explosion
Risks of explosion of the product in presence of mechanical impact: Not available.
Risks of explosion of the product in presence of static discharge: Not available.
Section V. Reactivity Data BIP Phthalimides
Stability
Freezell'haw Stability
The product is stable.
Freeze thaw stable, thaw and stir before using.
HwArdous decomp.
products
Oxides of carbon Not available.
Degradability
The 13OD5 is 349000 mgll [5 day(s)] SM 521 OB. The COD is 665000 mg/l EPA 410.4,
Products of degradation
Oxides of carbon Not available.
Not available.
Corrosivity
Not available.
Reactivity
Slightly reactive to reactive with oxidizing agents.
Continued on Next Page

i'
BIP Phthalimides FDA-0200 Page Number. 3
Section AToxicological Properties BIP Phthalimides
Routes of entry Eye contact. Ingestion.
TLV Refer to Section II. Hazardous Ingredients.
Toxicity to animals Acute oral toxicity (LD50): 1100 mglkg (Rat). (n-butyl phthalimide).
Chronic effects on There is no known effect from chronic exposure to this product. No carcinogenic substances as defined by [ARC,
humans NTP and/or OSHA.
Acute effects on humans Slightly hazardous in case of eye contact (irritant), of ingestion.
Aquatic Toxicity Not available.
(LC50)
Section V11. Preventive Measures BIP Phthalimides
Waste information Waste must be disposed of in accordance with federal, state and local environmental control regulations.
Waste stream Not available.
Storage Keep container tightly closed. Keep container in a cool, well -ventilated area.
Precautions Keep away from heat. Keep away from sources of ignition. Empty containers pose a fire risk, evaporate the residue
under a fume hood. Ground all equipment containing material. Do not ingest. Do not breathe
gaslfumeslvaporlspray. If ingested, seek medical advice immediately and show the container or the label.
Small spill and leak Absorb with an inert material and put the spilled material in an appropriate waste disposal.
Large spill and leak Absorb with an inert material and put the spilled material in an appropriate waste disposal. Finish cleaning by
spreading water on the contaminated surface and allow to evacuate through the sanitary system.
Protective clothing in Splash goggles. Full suit_ Boots. Gloves. Suggested protective clothing might not be sufficient; consult a specialist
case of large spill BEFORE handling this product.
Section V111. Classification BIP Phthalimides
DOT Not a DOT controlled material (United States).
Not applicable.
Not regulated. RQ Not available. Not available.
Maritime Not available.
transportation
HCS Class: Irritating substance.
Not available.
Federal and
State
Note: California Prop. 65 requires the listing of reportable chemicals that is helieved to exist in Ibis produce at any defected, or suspected, laud no matter how minute.
Regulations
CERCLA: Hazardous substances.: Not Listed.
SARA 313 toxic chemical notification and release reporting: Not Listed.
Not available.
Continued on Next Page

BIP Phthalimides FDA-0200 Page Number: 4
International Not Listed.
Lists
Section IX Protective Clothing BIP Phthalimides
Safety glasses. Gloves (impervious).
Section Xe Other Information BIP Phthalimides
References Not available.
Special Test Results Not available. Not available. Not available. Not available.
Not available. Not available. Not available. Not available.
Validated by Sandy Carter on,1011712006. Verified by Sandy Carter.
Printed 1121/2009.
CHEMTREC (24 HR) 1-500-424-9300
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RECEIVED
i ti C C"e0'. 0' Fk R
JAI Z 1 1111
'N nston-Sale—
Reaicnai C- -e
1wl"f, elk
DyStarl
DyStar Reidsville
209 Watlington tndustrial Dr.
Reidsville, NC 27320
800-443-8814
January 24, 2011
TEL[phone]
FAX [phone]
Mr. W. Corey Basinger
NC Division of Water Quality
585 Waughtown St.
Winston-Salem, NC 27107
Re: Notice of Violation — 201 1-PC-0036
Dear Mr. Basinger,
DyStar L.P. is currently taking the following measures to address the concerns brought to our
attention by the Notice of Violation dated January 12, 2011.
Tier 1 Evaluation:
DyStar LP is currently having the grass. dirt and grit removed from all stormwater inlets. We are
also having silt netting installed as needed. We are having trees removed and the silt netting
replaced around the Stormwater Outfall Discharge area to minimize any contribution to the Total
Suspended Solids.
Sampling Requirements:
DyStar LP will collect analytical samples at the next qualifying rain event and will maintain the
semi-annual analytical sampling schedule outlined in Part H Section B: Analytical Sampling
Requirements in the General Permit
Best re lardrs,
Marc C. Bumgarner
Site Manager - Reidsville Location
DyStar LP

NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
12 January 2011
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
7010 0290 0001 4856 4775
Mr. Marc Bumgarner
Site Manager
Dystar L.P.
209 Watlington Industrial Drive
Reidsville, NC 27320
Subject: Compliance Evaluation Inspection and Notice of Violation #NOV-2011-PC-0036
NPDES General Stormwater Permit NCG060000
Certificate of Coverage NCGO060101
Dystar L.P.
Dear Mr. Bumgarrtier:
Mike Thomas of the Winston-Salem Regional Office of the NC Division of Water Quality (DWQ)
conducted a compliance evaluation inspection (CEI) at the subject facility on 6 January 2011. Your
assistance and cooperation as well as that of Mr. Johnny Somers, during the inspection was greatly
appreciated. An inspection checklist is attached for your records and the inspection findings are
summarized below.
The facility is located at 209 Watlington Industrial Drive, in Reidsville, Rockingham County,
North Carolina. Stormwater related to industrial activity is discharged to Little Troublesome Creek,
which is currently classified as Class C waters in the Cape Fear River Basin.
Documentation and Monitoring Review
The Stormwater Pollution Prevention Plan (SP3) is complete and well implemented. Training
sessions are conducted annually to keep staff informed and updated. You also indicated to Mr.
Thomas that you often work with employees one-to-one to ensure that the SP3 is being followed.
Dystar L.P. has one stormwater discharge outfall (SDO) which was easily accessible for
inspection. Records and sampling results from qualifying events were made available for inspection
and appeared to be complete. As you indicated during the inspection no samples have been collected
since the permit renewal in 2007. This was due to a misunderstanding of permit conditions. Under
Certificate of Coverage #NCG060101 analytical sampling is required on a semi-annual basis. Dystar
L.P. failed to collect six analytical samples since 2007. Failure to collect samples is a violation of permit
condition as outlined in Part II Section B: Analytical Sampling Requirements in General Permit
Number 060000. To avoid further action this office requires Dystar L.P. to collect analytical samples at
the next qualifying rain event and to maintain the sampling schedule outlined above.
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St, Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone] Customer Service: 1-877-623-6748
Internet www.ncviaterquality.org
An Equal Opportunity 4 Affirmat" Action Employer
NorthCarolina
naturally

Mr, Marc Burngarner
Dystar LP.
Compliance Evaluation Inspection and Notice of Violation, NCGO60101
V1312011
Page 2 of 2
During the inspection you made it aware to Mr. Thomas that the facility exceeded the permit
benchmark for Total Suspended Solids (TSS) for the sample that was collected in 2007. Mr. Thomas
assisted you and Mr. Somers with a Tier I evaluation of the property to determine probable sources of
TSS. Mr. Thomas found accumulations of dirt and grit around several of the stormwater inlets at the
facility including the large loading and unloading area for the empty storage containers. These areas
should be cleaned to reduce the risk of TSS. Structural BMPs should also be considered for the inlet at
the storage area mentioned above.
In the event that TSS results are above benchmark levels from the next qualifying event this
office requires that sampling be elevated to the Tier Two schedule outlined in the permit. Tier Two
requires that analytical samples be collected monthly. Monthly samples will continue until three
consecutive samples below the benchmark value have been collected.
Site Review
The site was clean and well maintained at the time of inspection. Exposed industrial activity at
the facility was minimal. As indicated above, there were several stormwater inlets that need to be
cleaned. The stormwater discharge outlet was clean and well maintained.
Thank you for your attention to this matter. This Office is considering sending a recommendation for
enforcement regarding these issues. Your above -mentioned response to this correspondence will be
considered in this process. This office requires that the violations, as detailed above, be properly
resolved. These violations and any future violations are subject to a civil penalty assessment of up to
$25,000.00 per day for each violation. Should you have any questions regarding these matters, please
contact Mike Thomas at [phone],
Sincerely,
W. Corey Basinger
Interim Regional Supervisor
Surface Water Protection
Winston-Salem Region
Attachments:
1. BIMS Inspection Checklist
cc: SWP — WSRO
Central Piles .
Stormwater Permitting Unit

Compliance Inspection Report
Permit: NCG060101 Effective: 11/01/07 Expiration: 10/31/12 Owner: Dystar LP
SOC: Effective: Expiration: Facility: DyStar LP
County: Rockingham 209 Watlington Industrial
Region: Winston-Salem
Reidsville NC 27320
Contact Person: Johnny Somers Title: Phone: [phone]
Directions to Facility:
System Classifications:
Primary QRC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Certification: Phone:
Inspection Date: 01106/2011 Entry Time: 09:30 AM Exit Time: 10:30 AM
Primary Inspector: Michael S Thomas Phone:
Secondary Inspector(s):
Reason for Inspection. Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Food/Tobacco/Soaps/Cosmetics/Public Nlarehousing
Stormwater Discharge COG
Facility Status: 0 Compliant ❑ Not Compliant
Question Areas:
® Storm Water
(See attachment summary)
Page: 1

Permit: NCG060101 owner - Facility: Oystar LP
Inspection Date: 01/06/2011 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
■ Complete items 1, 2, and 3. Also complete A.
item 4 if Restricted Delivery Is desired. X
■ Print your name and address on the reverse
so that we can return the card to you. B.
Ir Attach this card to the back of the mailpiece, •--
or on the front if space permits.
gent ;
❑ Addressee
C-II ier t Bry '
D. Is deliveryladdress different from�Eem 14r ❑ Yes
1. Article Addressed to: if YES, enter delivery address below: ❑ No
Mr. Marc Bumgarner, Site Mgr.
Dystar, L.P.
2og Watlington Industrial Drive
Reidsville, NC 27320
1
3. 3rvice Type {
C9rttfied Mail ❑ Express Mall k
❑ Registered ❑ Return Receipt for Merchandise I
❑ Insured Mail ❑ C.O.D. I
4. Restricted DeliveW (Extra Fee) ❑ Yes
2• Article Humber- NOli
(rranster tryiri sen4ci l 1 t 7 010 1 0 2 9 0 it l0 0 01, 4.8 5 6 i 4 777 5 i ll 1' la7
PS Form 3811, February 20D4 Domestid Retum Receipt
t r
(DomesticCERTIFIED MAILT.RECEIPT
No insurance coverage r-r
WANT t (R
EDPostage
� Gertitisd Fee
a�SD
rq �'
r� z ostrna
0 Return Receipt Fee L 1 ` tvp �
Q (Endorsement Required) []� IA! _ a- 4 N
t-3 Restricted Delivery Fee V %
13 (Endorsement Required) QJ J
Er
ru Total PC
C3
sera ro Mr. Marc Bumgarner, Site Mgr.
Cl siree>.:a; Dystar, L.P.
Bo
r` orP° - 2og Watlington Industrial Drive I
ciiy; siei
Reidsville, NC 27320
102595-02-M-154e
Page, 2

Permit: NCG060101 Owner - Facility: Dystar LP
Inspection Date: 01/06/2011 Inspection Type: Compliance Evaluation
Reason for Visit: Routine
Stormwater Pollution Prevention Plan
Yes
No
NA
NE
Does the site have a Stormwater Pollution Prevention Plan?
®❑
n
n
# Does the Plan include a General Location (USGS) map?
®n
n
n
# Does the Plan include a "Narrative Description of Practices'?
®
n
Cl
Cl
# Does the Plan include a detailed site map including outfall locations and drainage areas?
®
n
n
n
# Does the Plan include a list of significant spills occurring during the past 3 years?
n
M
n
n
# Has the facility evaluated feasible alternatives to current practices?
®n
n
n
# Does the facility provide all necessary secondary containment?
®n
n
n
# Does the Plan include a BMP summary?
®❑
❑
o
# Does the Plan include a Spiil Prevention and Response Plan (SPRP)?
®
n
n
n
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
®
Cl
n
n
# Does the facility provide and document Employee Training?
®
n
n
n
# Does the Plan include a list of Responsible Party(s)?
o
n
n
n
# Is the Plan reviewed and updated annually?
®❑
n
n
# Does the Plan include a Stormwater Facility Inspection Program?
®
❑
❑
n
Has the Stormwater Pollution Prevention Plan been implemented?
®
n
n
n
Comment: The facility has had no significant spills in the last three years.
Qualitative Monitoring
Yes
No
NA
NE
Has the facility conducted its Qualitative Monitoring semi-annually?
®
❑
n
n
Comment:
Analytical Monitoring
Yes
No
NA
NE
Has the facility conducted its Analytical monitoring?
Cl
®
n
n
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
❑
n
®
n
Comment: The facility has not conducted Analytical sampling since the permit was
renewed in 2007. See inspection report for details.
Permit and Outfalls
Yes
No
NA
NE
# Is a copy of the Permit and the Certificate of Coverage available at the site?
®
Cl
n
n
# Were all outfalls observed during the inspection?
®
n
n
n
# If the facility has representative outfall status, is it properly documented by the Division?
n
n
®
n
# Has the facility evaluated all illicit (non stormwater) discharges?
®
n
n
n
Comment
Page- 3

f
Compliance Inspection Report
Permit: NCG060101 Effective: 11/01/07 Expiration: 10/31/12 Owner: Dystar LP
SOC: Effective: Expiration: Facility: DyStar LP
County: Rockingham 209 Watlington Industrial
Region: Winston-Salem
Reidsville NC 27320
Contact Person: Johnny Somers Title: Phone: [phone]
Directions to Facility:
System Classifications:
Primary ORC: Certification: Phone:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 01/0612011 Entry Time: 09:30 AM Exit Time: 10:30 AM
Primary Inspector: Michael S Thomas Phone:
Secondary Inspector(s):
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Food[Tobacco/Soaps/Cosmetics/Public Warehousing
Stormwater Discharge COC
Facility Status: ❑ Compliant U Not Compliant
Question Areas:
® Storm Water
(See attachment summary)
e�
Page: 1

Permit: NCGO60101 Owner -Facility: Dystar LP
Inspection Date: 01/06/2011 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
Page: 2

Permit: NCGO60101 Owner -Facility: Dystar LP
Inspection Date: 01/06/2011 Inspection Type: Compliance Evaluation
Reason for Visit: Routine
Stormwater Pollution Prevention Plan
Yes No NA
NE
Does the site have a Stormwater Pollution Prevention Plan?
n n
n
# Dees the Plan include a General Location (USGS) map?
n n
n
# Does the Plan include a "Narrative Description of Practices"?
n n
n
# Does the Plan include a detailed site map including outfall locations and drainage areas?
n ❑
n
# Does the Plan include a list of significant spills occurring during the past 3 years?
❑'
# Has the facility evaluated feasible alternatives to current practices?
n n
n
# Does the facility provide all necessary secondary containment?
n
# Does the Plan include a BMP summary?
i n n
n
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
�a_n n
n
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
_F n n
n
# Does the fa ility provide and document Employee Training?n
In
n
�t�
��Uol_\k 4 ijE0 'rw:ti.n
n n
n
# Does the Plainclude a list of Responsible Party?l
# Is the Plan reviewed and updated annually?
n n
n
# Does the Plan include a Stormwater Facility Inspection Program?
❑
n
Has the Stormwater Pollution Prevention Plan been implemented?i
n n
n
Comment:
Qualitative Monitoring
THas
Yes No NA
NE
the facility conducted its Qualitative Monitoring semi-annually?(n
n
n
Comment:
Analytical Monitoring db-,� J-0- AA_*tl-kc*1 sj�ry
ZED '. Yes No NA
NE
Has the facility conducted its Analytical monitoring?
n gi n
n
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
n n y
n
Comment:
Permit and Outfails
Yes No NA
NE
# Is a copy of the Permit and the Certificate of Coverage available at the site? 0n n n
# Were all outfalls observed during the inspection? *n n n
# If the facility has representative outfall status, is it properly documented by the Division? n n)0 n
# Has the facility evaluated all illicit (non stormwater) discharges? n n n
Comment:
Page: 3

.._ 0�0� w A rF9 pG
fir,.
o �
June 16, 2008
Mr. Marc C. Bumgamer
DyStar, LP
209 Watlington Industrial Drive
Reidsville, NC 27320
Dear Mr. Bumgarner:
Michael F. Easley, Govemor
William G- Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Coleen H. Sullins, Director
Division of Water Quality
RECEIVED
H.C. Dew- of MR !
3
JUN 18 2W8
Wknston-Sale^-
Regional Office
Subject: NPDES General Permit NCG060000
Certificate of Coverage NCGO60101
DyStar, LP
Formerly Boehme Filatex, Inc.
Rockingham County
Division personnel have reviewed and approved your request to transfer coverage under the General Permit,
received on April 10, 2008.
Please find enclosed the revised Certificate of Coverage. The terms and conditions contained in the General
Permit remain unchanged and in full effect. This revised Certificate of Coverage is issued under the requirements
of North Carolina General Statutes 143-215.1 and the Memorandum of Agreement between North Carolina and
the U.S. Environmental Protection Agency.
If you have any questions, please contact the Stormwater Permitting Unit at [phone], extension 502.
S incerely,
ORIGINAL SIGNED BY
KEN PICKLE
Coleen H. Sullins
cc: DWQ Central Files
Winston-Salem Regional Office
Stormwater Permitting Unit
iNo Carolina
Ntura!!J
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone [phone] Customer Service
Internet h2o.enr.state.mus 512 N. Salisbury St. Raleigh, NC 27604 FAX [phone]
An Equal OpportunitylAfFirmaWe Action Employer— 50% Recycled/10% Post Consumer Paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE No. NCG060101
STORM WATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
DYSTAR, LP
is hereby authorized to discharge stormwater from a facility located at
DYSTAR, LP
209 WATLINGTON INDUSTRIAL DRIVE
REIDSVILLE
ROCKINGHAM COUNTY
to receiving waters designated as a UT to Little Troublesome Creek, a class C NSW stream, in the Cape Fear River
Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I,
1I, III, IV, V, and VI of General Permit No. NCG060000 as attached.
This certificate of coverage shall become effective June 16, 2008.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day June 16, 2008. ORIGINAL SIGNED BY
KEN PICKLE
CoIeen H. Sullins, Director
Division of Water Quality
By Authority of the Environmental Management Commission

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