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NCG060098_MONITORING INFO_20190424
PERMIT NO. DOC TYPE DOC DATE STORMWATER DIVISION CODING SHEET NCG PERMITS �,v /v o"& " HISTORICAL FILE !xMONITORIN6 REPORTS YYYYMMDD PERMIT NO. DOC TYPE DOC DATE STORMWATER DIVISION CODING SHEET NCG PERMITS 0 HISTORICAL FILE VVIONITORING REPORTS 11 YYYYMMDD NC Division of Water Cluality. Regional Supervisor 450 Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 RE: Vertellus Greensboro LLC; Permit #: NCG060000 Tier 2 & 3 Notifications Dear Ms. Knight: Attached are results from March outfali monitoring. P. ��'Vertellus Smart Chemistry. Our Specialty. - April 8, 2019 Outfall #1 tested out of range for TSS and Outfall #6 tested out of range for TSS and COD. All other Outfalls and parameters were within the Benchmarks. The site is evaluating possible causes and will sample again at the next practical opportunity, Please feel free to contact me at 336-834-4903 or via email at akramer@vertellus.com if you have any questions regarding this information. T Sincerely, For, Vertellus Greensboro LLC Aaron Kramer EHS Manager, Vertellus LLC RESPONSIBLE CARE* [xiarnwarta[rn .o xisrur�tsu.m Vertellus 2110 W. Gate City Blvd. Greensboro, NC 27403 Phone: 336-292-1781 www.vertellus.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. Date submitted 4/8/2019 CERTIFICATE OF COVERAGE NO. NCG06 0098 RECEIVED FACILITY NAME �p� �� Y01A COUNTY ,'^~ - --- PERSON COLLECTING SAMPLES Aaron Kramer CENTRAL FILES Part A:StornmxvaterBenchmarks and Monitoring Results Total event rainfall 2 —0.45" or [] No discharge this period' VCjil— CY zonly applies tofacilities that use/process meats. The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at Any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3'identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? [:] yes N no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. I only applies tofacilities that use/process meats. ' The total precipitation must berecorded using data from anon-site rain gauge. , For sampling periods with nodischarge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. (Lf_ves, complete Part 8) S\YD' 4y Last Revised: October l8.20\2 'See General permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER ATANY ONE OUTFALL? YES ® NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office — Moil an original and one copy of this DMR including aN_"No Discharge" reports within 30 days ofreceipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 4/8/2019 (Date) Additional copies of this form may be downloaded at: http://Portal,ncdenr.org/web/wg/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted _1 4 2019 CERTIFICATE OF COVERAGE NO. NCG06 0098 RECEIVED FACILITY NAME Vertellus Greensboro LLC JAN 2 2 Z019 COUNTY Guilford PERSON COLLECTING SAMPLES Aaron Kramer CENTRAL FILES LABORATORY Meritech Lab Cert. # 165 DWR SECTION Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall Z 0.45' or n No discharge this period' OutfaII-No.:•: , _ - 5ample'Collected''; '-.inn/dd%yr =TSS, ';ing%L = _ ` : pH '. .Standard units' •COD; _ mg/L - Oil an_d Grease,. 1 mg/L - :Fecal CoGform',, , _Colonies per i00 ml Enterococci', : Colonies per 100 ml . ,Benchmar0j-* t '< 100 or 504 Within.6.6.g 9.0 '120 30.• 1000' . i, 500 01 12/14/18 748 6.4 27 10 n/a n/a 02 Representative --- --- --- --- n/a n/a 03 Representative - - - -- n/a n/a 04 1 Representative --- --- --- - - n/a n/a 05 12/14/18 <2.5 6.5 <15 <5 n/a n/a 06 12/14/18 38 6.6 31 <5 n/a n/a Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. ^See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No., > Sample Collected, n o/dd/yr. ' Oil and Grease, mg/L- - . TSS, mg/L. : ; pH; Standard units New_ Motor Oil,Usage, Annual average gal/mo .Benchmark" Y ` > :'° 30 :100'or 504 I 6.0 -- 9.0. only applies to facilities that use/process meats. I The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes complete Part 13) SWU-249 Last Revised: October 18, 2012 Page I of 2 a J *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO [� IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Mail an original and one col2y of this DMR includin all "No Discharge" reports within 30 days o recei t o the lab results or at end o monitoring period in the cose_ of "No Discharge" reports) to. - Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information including the possibility of fines and imprisonment for knowing violations." �j �1 3 2019 (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/`su/npdessw#tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 NC Division of Water Quality. Regional Supervisor 450 Manes Mill Road, Suite 300 Winston-Salem, NC 27105 RE: Vertellus Greensboro LLC; Permit #: NCG060000 Tier 2 & 3 Notifications Dear Ms. Knight: Attached are results from December outfall monitoring. 'Vertellus° Smart Chemistry, Our Specialty.' January 2, 2019 Outfall #1 tested out of range for TSS. All other Outfalls and parameters were within the Benchmarks. The site is evaluating possible causes and will sample again at the next practical opportunity. Outfall #1 also tested out of range for TSS on 6/20/18 with a reading of 307 mg/L and on 1/12/18 with a reading of 110 mg/L. Please feel free to contact me at 336-834-4957 orvia email at bstewart@vertellus.com if you have any questions regarding this information. Sincerely, For, Verteilus Greensboro LLC Ben Stewart Site Director, Vertellus LLC �7 RESPONSIBLE CARE nua mMu� r W rvt Tn 4niur�eii m Vertellus 2110w. Gate City Blvd. Greensboro, NC 27403 Phone: 336-292-1781 www,vertedus.com NC Division of Water Quality. Regional Supervisor 450 Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 RE: Vertellus Greensboro LLC; Permit #: NCG060000 Tier 2 & 3 Notifications Dear Ms. Knight; Attached are results from November outfall monitoring. t. V'Vertelius° Smart Chemistry. Our Specialty: December 13, 2018 Outfall #5 tested out of range for COD. The site is evaluating possible causes and will sample again at the next practical opportunity. This exceedance puts the site into Tier 2 monitoring requirements for COD at Outfall 5. The site is adhering to Tier 3 notification requirements found in Part II, Page 8 of 12 of General Stormwater Permit No. NCG060000 for COD at Outfall #5. This is the first exceedance for COD for Outfall #5 in the past 24 months. Please feel free to contact me at 336-834-4957 or via email at bstewart@vertellus,com if you have any questions regarding this information. Sincerely, l.. r For, Vertellus Greensboro LLC Ben Stewart Site Director, Vertellus LLC Ea RESPONSIBLE CARE Verteilus '- 2110 W. Gate City Blvd. Greensboro, NC 27403 Phone: 336-292-1781 www.vertellu5_Com -Zl SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted _12 14 2018 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Greensboro LLC RECEIVED COUNTY Guilford DEC192018 PERSON COLLECTING SAMPLES Aaron Kramer LABORATORY Meritech Lab Cert. # 16.5 CENTRAL _�ILE�. D11M `'_:CTio L.l Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall' 0.45" or ❑ No discharge this period' Outfall No. it .Sample"Collected, mo/dd/yr:-' T55, mg/L - pH, -, Standard units - COD, ' mg/L. Oil and Grease, mg/L Fecal Coliforml, _ Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark:% f - - 100 or 50°• Within 6.0 - 9.0 : .120 _.. 30` , 1000 S00 01 11/2/18 37 6.5 65 <5 n/a n/a 02 Representative --- -- --- n/a n/a 03 Representative --- --- --- n/a n/a 04 Representative --- --- --- n/a n/a 05 11/2/18 7 6.7 140 <5 n/a n/a 06 11/2/18 1 28 6.4 1 67 <5 1 n/a n/a 1 Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results. only for facilities averaging > 55 gal of new motor oil/month. OutfalLNo, - Sample.Collected, mo/dd/yr- "_ . Oil and Grease, rng/L TSS, .'mg/L pH, ` Standard units New Motor Oil Usage, Annual'average gal/mo Benchmark -- ; 30 100 or30° - ` . 6.0 - 9.0 - 1 Only applies to facilities that use/process meats. 2 The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. S W U-249 (if yes, complete Part B) Last Revised: October 18, 2012 Page i of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER I REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME. _Winston Salem Regional Office Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) �12 13 2018 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wg/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 NC Division of Water Quality, Regional Supervisor 450 Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 RE. Vertellus Greensboro LLC; Permit #, NCG060000 Tier 2 & 3 Notifications Dear Ms. Knight, Attached are results from June outfall monitoring. Z- ''Vertellus° Smart Chemistry. Our Specialty. - November 5, 2018 CE- 0D "V 14 DV VF,rC�ILES 1pR� Outfall #6 tested out of range for COD. The site is evaluating possible causes and will sample again at the next practical opportunity. This exceedance puts the site into Tier 2 monitoring requirements for COD at Outfall 6. The site is adhering to Tier 3 notification requirements found in Part II, Page 8 of 12 of General Stormwater Permit No. NCG060000 for COD at Outfall #6. The most recent result, along with prior results were above the permit limit of 120 mg/I are in the table below. The site will continue to investigate and attempt to determine and address the root cause of exceedances. Date Outfall #6 Result COD (me) 1/12/2018 281 7/6/2018 156 10/20/18 386 Please feel free to contact me at 336-834-4957 or via email at bstewart@vertellus_com if you have any questions regarding this information. Sincerely, For, Vertellus Greensboro LLC Ben Stewart Site Director, Vertellus LLC vertellus 2110 W. Gate City Blvd. Greensboro, NC 27403 RF,SPONSIBLE CARE Phone: 336-292-1781 t.coM.W0r 1mnrtTM-1— www.verte lus.cam SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted _10 20 2018 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Greensboro LLC COUNTY Guilford PERSON COLLECTING SAMPLES Aaron Kramer LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results NOV 14 zoI8 tqTRAL ,. ., fywr SP 11-cnc�Gi Total event rainfall z 0.84" or ❑ No discharge this period' Outfall No. Sample Collected; ; mo/dd/yr , ° `" TSS, _., " "mg/L.' pH,:' Standard tiriits•.`rng/L, ".• `COD, ' r Oil and Grease, •mg/L Fecal Coliform j. Colonies'per 100 ml Enterococci', Colonies per 100 ml Benchmark - 100 or 50' Within 6.0'-9.0' 120 30. , 1000 500 01 10/20119 26 6.3 67 <5 n/a n/a 02 Representative --- --- --- --- n/a n/a 03 Representative --- --- --- - - n/a n/a 04 Representative --- --- --- --- n/a n/a 05 10/20/18 7 6.6 48 <5 n/a n/a 06 10/20/18 17 7.1 386 <5 n/a n/a 1 Only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at and outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. ,Outfall'No. 5ample.Coilected, .; mo/dd/yr Oi1 and.Grease, . mg/L "TSS; mg/L hH,;- . ., Standard'.units New Motor Oil Usage, Annual average gal/mo Benchmark 30' n 300"ar 504 6:0 1 only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. I For sampling periods with no discharge at gny outfalls, you must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (± yes, complete Part B) SWU-249 s *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART it SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES MNOEI IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office Moil an original and one copy, of this DMRincluding all "No Discharge"' reports, within 30 days of receipt of the lob results (or at end, of monitoring period in the case o "No Discharge"' re arts to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) _11 5 2018 (Date) Additional copies of this form may be downloaded at: http://Mortal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 5 W U-249 I a.t 1?P%n.Prl- Cl't-1— IQ IAIII NC Department of ` Environmental Quality { Received E OCT 15 2018 Winston-Salem NC Division of Water Quality;. Regional Office Regional Supervisor 450 Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 RE: Vertellus Greensboro LLC; Permit #: NCG060000 Tier 2 & 3 Notifications Dear Ms. Knight: Attached are results from September outfall monitoring. Lj Vertellus-, Smart chemistry. Our specialty, - October 11, 2018 Outfall 96 tested out of range for COD. The site is evaluating possible causes and will sample again at the next practical opportunity. This exceedance puts the site into Tier 2 monitoring requirements for COD at Outfall 6. The site is adhering to Tier 3 notification requirements found in Part II, Page 8 of 12 of General Stormwater Permit No. NCG060000 for COD at Outfall 46. The most recent result, along with prior results were above the permit limit of 120 mg/I are in the table below. The site will continue to investigate and attempt to determine and address the root cause of exceedances. Date Outfall #6 Result COD (mg/1) 9/1/2017 153 1/12/2018 281 7/6/2018 156 9/14/18 142 Please feel free to contact me at 336-834-4957 or via email at bstewart@vertellus.com if you have any questions regarding this information. Sinc For, Vertellus Greensboro LLC Ben Stewart Site Director, Vertellus LLC �0 RESPONSIRU CARE vertellus 2110 W. Gate City Blvd. Greensboro, NC 27403 Phone: 336-292-1781 www.verteilus.com A SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted _9 14 2018 CERTIFICATE OF COVERAGE NO. NCGO6 0098 FACILITY NAME Vertellus Greensboro LLC COUNTY Guilford PERSON COLLECTING SAMPLES Aaron Kramer LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall 0.84" or ❑ No discharge this period' -Odtfall,No' `, -., Sample Collected mo%dd/yr y TSS,. r : mg/L_ . pH,' Standard units' COD, mg/L, " Oil'and•Grease, mg, L •Fecal Coliforml; . Colonies:per.100 ri + Enterococcil, Colonies per.100 ml Benchmark 100 or 50° . ; Wlthin.6:0:='9.0'" 120 .. 30 1000 :. ' t" ; Soo 01 9/14/18 55 6.3 44 <5 n/a n/a 02 Representative --- --- --- --- n/a n/a 03 Representative -- --- --- --- n/a n/a 04 Representative --- --- --- n/a n/a 05 9/14/18 11.4 7.5 <15 <5 n/a n/a 06 9/14/19 148 6.8 142 <5 n/a n/a ' Only applies to facilities that use/process meats. The total precipitation must be recorded using data from an on -site rain gauge. 'For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes N no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. outfall'No,, : Sample"Collected; mo/lid/yr" -'Oil and Gr""ease,;, , : mg/L `� TSS, : mg/L = ' '- '-pH,#' ss . - _Standard units : °New Mot& Oil•Usagel—. :-Annual average,ga!/mo Benchmark 30 - "- -100 of 50° " 6.0 = 9.0 -- = - 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 45ee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if ryes, complete Part B) fti SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO E] REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Mail an original and one copy of this DMR,_ including all "No Discharge" reports, within 30 days of receipt of the lob results (or at end of monitoring period in the case of "No Discharge" reports) io: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 10/11/2018 (Date) Additional copies of this form may be downloaded at: hapjlr)ortal.ncdenr.org/web/wq/ws/su/nodcssw#tab-4 SWU-249 Last Revised; October 18, 2012 Page 2 of 3 NC Division of Water Quality. Regional Supervisor 450 Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 � 'Vertellus° Smart Chemistry. Our Specialty., October 11, 2018 RE: Vertellus Greensboro LLC; Permit #: NCG060000 Tier 2 & 3 Notifications RECE IVE Dear Ms. Knight: OCT 1 CENTRF-kL Attached are results from September outfall monitoring. DWR SfrCTt" Outfall 46 tested out of range for COD. The site is evaluating possible causes and will sample again at the next practical opportunity. This exceedance puts the site into Tier 2 monitoring requirements for COD at Outfall 6. The site is adhering to Tier 3 notification requirements found in Part II, Page 8 of 12 of General Stormwater Permit No. NCGO60000 forCOD at Outfall #6. The most recent result, along with prior results were above the permit limit of 120 mg/I are in the table below. The site will continue to investigate and attempt to determine and address the root cause of exceedances. Date Outfall #6 Result COD (mg/1) 9/1/2017 153 1/12/2018 281 7/6/2018 156 9/14/18 142 Please feel free to contact me at 336-834-4957 or via email at bstewart@vertellus.co_m_ if you have any questions regarding this information. Sinc For, Vertellus Greensboro LLC Ben Stewart Site Director, Vertellus LLC Vertellus 0� 2110 W. Gate City Blvd. �� Greensboro, NC 274C3 RESPONSIBLE CARE* Phone: 336-292-1791 01M C(1 1-FM TO M W W W .v Lrtel lus.corn SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted �9 14 2018 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Greensboro LLC COUNTY Guilford PERSON COLLECTING SAMPLES Aaron Kramer LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall 2 0.84" or ❑ No discharge this period' s7utfall,No. ; Sample Calleet@'dl-' mo/dd/yr `; "' K - TSS, -�" mg/L;+ pH; t• " Staniiard'units "C617,' mgJC `,Oil and Grease,.' c. -Fecal Coliforml, .Colonies per'.100 ml' Enterococcil, Colonies per 100 mi :Berichmark +' - Y, ` `,'' 100'ar:50° wWithin.6:0 = %O0 ,_ - 120 `�`_ ` . , - :> 30: "' : 1000` _ a- - 500 01 9/14/18 55 6.3 44 <5 n/a n/a 02 Representative --- --- --- --- n/a n/a 03 Representative -- -- - - --- n/a n/a 04 Representative --- - --- n/a n/a 05 9/14/18 11.4 7.5 <15 <5 n/a n/a 06 9/14/18 148 6.8 142 <5 n/a n/a 1 Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 5S gal of new motor oil/month. ' Outfall:No. ;5ample'Collected, mnJild/.yr . Oi! and Grease; ' _ rtig/L TSS,' i mgJh :pH, : Standard. units : • New`Motor Oil Usage, "Anrival.average.galJmo ' Bencl4mark - 30. 100'or 504 ' y ' 6.0 = 9.0 1 Only applies to facilities that use/process meats. 2 The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. "See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (ifyes, complete Part B) SWU-249 last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B, • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Mail an original and one copy of this DMR including all "No Discharge" reports within 30 days o recei t of the lab results or at end o monitoring period in the case of "No Discharge" reports) to. - Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, INC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete_ I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 10/11/2018 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdesswgtab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 Im 11 �7Vertellus- NC Division of Water Quality. Regional Supervisor 4S0 Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 RE: Vertellus Greensboro LLC; Permit #: NCG060000 Tier 2 & 3 Notifications ('OD? g Dear Ms. Knight: Attached are results from June outfall monitoring. Smart Chemistry. Our Specialr/.- August 13, 2018 RECEIVE] AUG 21 2018 CENTRAL FILES DWR SECTION Outfall 4#6 tested out of range for COD. The site is evaluating possible causes and will sample again at the next practical opportunity. This exceedance puts the site into Tier 2 monitoring requirements for COD at Outfall 6. The site is adhering to Tier 3 notification requirements found in Part II, Page 8 of 12 of General Stormwater Permit No. NCG060000 for COD at Outfall 46. The most recent result, along with prior results were above the permit limit of 120 mg/l are in the table below. The site will continue to investigate and attempt to determine and address the root cause of exceedances. Date Outfall #6 Result COD (mg/1) 9/6/2017 233 9/1/2017 153 1/12/2018 281 7/6/2038 156 Please feel free to contact meat 336-834-4957 or via email at bstewart@ver-tellus.com if you have any questions regarding this information. !' 'j9 o RESPONSIBLE CARE Iff �'a ro 41151,1"Id 1W Sincerely, For, Vertellus Greensboro LLC Ben Stewart Site Director, Vertellus LLC Ver',Ous 2110 W, Gate City Blvd. Greensboro, NC 27403 Phone: 336-292-1781 www.vertehus.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted �8 13 2018 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Greensboro LLC COUNTY Guilford PERSON COLLECTING SAMPLES Aaron Kramer LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall' 0.75" or ❑ No discharge this period' Outfall No. Sample Collected, mo/dd/yr - TSS, mg/L pH,, Standard units COD, - mg/L Oil and'Grease,.. mg%L Fecal Coliforml,.- - f Colonies per 100 mf . Enterococcil, . - Colonies per 100 ml Benchmark - _ 100 or 504 Within 6.0 — 9.0 .120 • ; - 30 •1000 Soo 01 07/06/18 21A 6.4 44 <5 n/a n/a 02 Representative --- - --- n/a n/a 03 Representative -- -- --- n/a n/a 04 Representative --- --- --- --- n/a n/a 05 07/06/18 11.4 7.6 <15 <5 n/a n/a 06 07/06/18 1 97 1 8.5 156 <5 n/a n/a 1 Only applies to facilities that use/process meats. ' The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Dutfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L __ TSS, mg/L - , pH,;, Standard units , _ New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or.504 6.0 - 9.0 •', ' only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. •*°See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (ifye s• complete Part B) SWU-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART Il SECTION B. + TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES E NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office Mail an original and one -copy of this DMR including all "No Discharge" reports, within 30 day-5 of receipt of the lab results Lor of end o monitoring period in the case of "No Discharge" reports)_to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, includingthe possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 8(13L2018 (Date) Additional copies of this form may be downloaded at: http:[/oortal.ncdenr.orglweblwq/ws/su/`npde.5sw#Itab-4 .SWU-249 Last Re%rised: October 18. 2412 Page 2 of 2 1 er rl NCDepartment of Vertellus* Environmental Quality Received NC Division of Water Quality. AU6 i Ltfi Regional Supervisor Winston-Salem 450 Hanes Mill Road, Suite 300°„*,,.;, Regional Office '. Winston-Salem, NC 27105 :. RE: Vertellus Greensboro LLC; Permit #: NCG060000 Tier 2 & 3 Notifications Dear Ms. Knight: Attached are results from June outfall monitoring. Smart Chemistry. Our Specialty.' August 13, 2018 Outfall #6 tested out of range for COD. The site is evaluating possible causes and will sample again at the next practical opportunity, This exceedance puts the site into Tier 2 monitoring requirements for COD at Outfall 6. The site is adhering to Tier 3 notification requirements found in Part II, Page 8 of 12 of General Stormwater Permit No, NCG060000 for COD at Outfall 96. The most recent result, along with prior results were above the permit limit of 120 mg/I are in the table below. The site will continue to investigate and attempt to determine and address the root cause of exceedances. Date Outfall #6 Resuit COD (mg/1) 9/6/2017 233 9/1/2017 153 1/12/2018 281 7/6/2018 156 Please feel free to contact meat 336-834-4957 or via email at bstewartyerteWs.com if you have any questions regarding this information. RESPONSIBLE CARE a.�mr,.rc� r,>;i m.rv.emrr Sincerely, For, Vertellus Greensboro LLC Ben Stewart Site Director, Vertellus LLC vertellus 2110 W. Gate Cite Blvd. Greensboro, NC 274C3 Phone: 336-292-173 L www.vertellus.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted _$ 13 201$ CERTIFICATE OF COVERAGE NO. NCGO6 0098 FACILITY NAME Vertellus Greensboro LLC COUNTY Guilford PERSON COLLECTING SAMPLES Aaron Kramer LABORATORY Meritech Lab Cert. # 165 Part A, Stormwater Benchmarks and Monitoring Results Total event rainfall' 0.75" NC Department of Environmental Quality Received AUG 1 r 2018 Winston- alem RegionalO ice or ❑ No discharge this period' Outfall No. Sample Collected_, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease,.- mg/L.' Fecal Coliform.' - Colonies per 100 ml Enterococci', . : Colonies per 100 ml" Benchmark - 100 or 50' Within 6.0 — 9.0. 120 30 '. 1000 Soo 01 07/06/18 21.4 6A 44 <5 n/a n/a 02 Representative --- --- --- n/a n/a 03 Representative -- - --- --- n/a n/a 04 Representative --- --- --- --- n/a n/a 05 07/06/19 11.4 7.6 <15 <5 n/a n/a 06 07/06/18 97 8.5 156 <5 n/a n/a 'Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L .TSS, mg/L ' pH, Standard units ' -New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or'50° 6.0 — 9.0 ' Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5WU-249 (ifyes, complete Part B) Last Revised: October 18, 2012 Page I of 2 W *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES Z NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Mail an original and one col2y of this DMR including all "No Discharge" reports, within 30 da 's of receipt of the lab results Lor at end o monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including( a possibility of fines and imprisonment for knowing violations." cl-_ (Signature of Permittee) 8/13/2018 (Date) Additional copies of this form may be downloaded at: litto://portal.ncdenr.on=/web/wQ/ws/su/npdessw##tab-4 SWU-249 Last Revised: October 18, 2012 N Page 2 oI' 2 NC Division of Water Quality. Regional Supervisor 450 Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 RE: Vertellus Greensboro LLC; Permit #: NCG060000 Tier 2 & 3 Notifications Dear Ms. Knight: Attached are results from June outfall monitoring. p. Vertelluso Smart Chemistry. Our Specialty. - July 10, 2018 EC V D SUL I I Zp" C)wR s c a Outfall #1 tested out of range for TSS. The site is evaluating possible causes and wilt sampie again at the next practical opportunity. This exceedance puts the site into Tier 2 monitoring requirements for TSS at Outfall #1. The site is adhering to Tier 3 notification requirements found in Part II, Page 8 of 12 of General Stormwater Permit No. NCG060000 for COD at Outfall ##6. The most recent result, along with prior results were above the permit limit of 120 mg/I are in the table below. The site will continue to investigate and attempt to determine and address the root cause of exceedances. Date Outfall #6 Result COD (mg/1) 9/6/2017 233 9/1/2017 15.3 1/12/2018 281 6/20/18 1530 Please feel free to contact me at 336-834-4957 or via email at bstewart@vertellus.com if you have any questions regarding this information. Sincerely, For, Vertellus Greensboro LLC Ben Stewart Site Director, Vertellus LLC Vertellus @9 2110 W. Gate City Blvd. Greensboro, NC 27403 RESPONSI BLE CARE Phone: 336-292-1731 VOIMfR C.0—J. Yr rn PKl41ti•RIIST�' www.vertellus.com SEMI-ANNUAL. STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted �7 10 2018 CERTIFICATE OF COVERAGE NO. NCG06 0098 RECEIVED FACILITY NAME Vertellus Greensboro LLC COUNTY Guilford JUL 17 2018 PERSON COLLECTING SAMPLES Aaron (Kramer LABORATORY Meritech Lab Cert. # 165 CENTRAL FILES DVIJR SECTION Part A, Stormwater Benchmarks and Monitoring Results Total event rainfall z 0.75" or ❑ No discharge this period' Outfall;No. "Sample Collected; mo/dd/yr. ,- _TSS"* mg/L. -pH, .' . Standard units ' COD, t :mg/l. Oil and Grease,' .. mg%L ' Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark ' - 100 or 504 Within 6.0—..9.0 �._ .120 30 1000 .500 01 06/20/18 307 6.1 39 <5 n/a n/a 02 Representative --- — --- --- n/a n/a 03 Representative --- --- --- --- n/a n/a 04 Representative — --- n/a n/a 05 06/20/18 15.3 6.6 <15 <5 n/a n/a 06 06/20/18 1530 8.1 1 226 <5 n/a n/a 'only applies to facilities that use/process meats. 2 The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B- Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No.. : Sample Collected, mo%dd/yr: ;Oil,and Grease, mg/L TSS, mg/L :' °' .pH, Standard units New Motor Oil Usage, Annual,average gal/ma Benchmark - 30 100 or 504 ` 6.0 — 9.0 - ' Only applies to facilities that use/process meats. 2The total precipitation must he recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (i'fyes, complete Part 13) SWU-249 I-ast Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results1or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27:1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." f _7 11 2018 (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/suZnpdessw#tab-4 SWU-244 Last Revised: October 19, 2012 Page 2 of 2 NC Division of Water Quality. Regional Supervisor 450 Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 RE: Vertellus Greensboro LLC; Permit #: NCG060000 Tier 2 & 3 Notifications Dear Ms. Knight: Attached are results from June outfall monitoring. n �V'Vertellus• Smart Chemistry. Our Specialty. - July 10, 2018 NIC Department of Enviror►-rital04L1a!it'/ I,E .=r�i��ea JUG. 16 2510 Winston-Salem Regiona' Offire Outfall 41 tested out of range for TSS. The site is evaluating possible causes and will sample again at the next practical opportunity. This exceedance puts the site into Tier 2 monitoring requirements for TSS at Outfall #1. The site is adhering to Tier 3 notification requirements found in Part II, Page 8 of 12 of General Stormwater Permit No. NCG060000 for COD at Outfall #6. The most recent result, along with prior results were above the permit limit of 120 mg/I are in the table below. The site will continue to investigate and attempt to determine and address the root cause of exceedances. Date Outfall #6 Result COD (mg/1) 9/6/2017 233 9/1/2017 153 1/12/2018 281 6/20/18 1530 Please feel free to contact me at 336-834-4957 or via email at bstewart@vertellus.com if you have any questions regarding this information. Sincerely, For, Vertellus Greensboro LLC Ben Stewart Site Director, Vertellus LLC Vertellus 2110 W. Gate City Blvd. Greensboro, NC 27403 RESPONSIBLE CARE Phone: 336-292-1781 4 ? www.vertellus.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG06OOOO Date submitted _7 10 2018 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Greensboro LLC COUNTY Guilford PERSON COLLECTING SAMPLES Aaron Kramer LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall 1 0.75" or ❑ No discharge this period' Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 50' Within 6.0 — 9.0 120 30 1000 500 01 06/20/18 307 6.1 39 <5 n/a n/a 02 Representative --- --- --- --- n/a n/a 03 Representative --- I- -- -- n/a n/a 04 Representative --- --- -- --- n/a n/a 05 06/20/18 15.3 6.6 <15 <5 n/a n/a 06 06/20/18 1530 8.1 226 <5 n/a n/a 1 Only applies to facilities that use/process meats. 2 The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part B) SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Moil an ariginal and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." r_"o _7 11 2018 (Signature of Permittee) (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 NC Division of Water Quality. Regional Supervisor 450 Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 RE: Vertellus Greensboro LLC; Permit #: NCG060098 Tier 3 Notification v Vertellus.) Smart Chemistry. Our Spaclalty.• April 20, 2018 REcp Et) APR 2 6 2o18 CENTRAL. FILES DWR SECrION Dear Ms- knight: The site recently submitted outfal! monitoring results in a separate mailings for stormwater sampling conducted on Outfalls #1, #5, and #6 on 4/7/2018. All reported results are within the permit limit. The site is adhering to Tier 3 notification requirements found in Part li, Page 8 of 12 of General Stormwater Permit No, NCG060000. Please feel free to contact me at 336-834-4957 orvia email at bstewart2vertellus.eom if you have any questions regarding this information. Sincerely, For, Vertellus Greensboro LLC Ben Stewart Site Director, Vertellus LLC �0 RESPONS I BLE CARe I'MMM1 NI 10 I11MIN-NI RY Vertellus 2110 W. Gate City Blvd, Greensboro, NC 27403 Phone; 336-292-1781 wivW.vertellus.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted �4 20 2018 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Greensboro LLC COUNTY Guilford PERSON COLLECTING SAMPLES Ben Stewart LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall' 0.75" or ❑ No dischorge this period' Outfall No. Sample Collected; W..mo/dd/yr: TSS, .,mg '`' pH, Standard units COD, « mg/i Oil and Grease, mg/L.' : , , Fecal Coliforml, Colonies per 100 ml :Enterococcil, Colonies per i0o ml Benchmark - 100 or 50°= Within 6:0 — 9.0. , 120 _ . . ;-30' • 1060 500, 01 04/7/2018 3 6.8 20 <5 n/a n/a 02 Representative --- --- --- --- n/a n/a 03 Representative --- --- --- --- n/a n/a 04 Representative - - --- --- w- n/a n/a 05 04/7/2018 <2.5 7.0 13 <5 n/a n/a 05 04/7/2018 r 33 6.5 111 <5 n/a n/a ' Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. • Outfall No.,- Sample Collected, - _ mo/dd/yr Oil and Grease, • mg/L. TSS,- = mg/L pH, Standard units NeW Motor Oil Usage, Annual average gal/mo Benchmark. - ; -30 100 or 504 '6.0 — 9.0 - - 1 Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (ifye5, complete Part B) SWU-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART it SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30-days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) _4 20 2018 (Date) Additional copies of this form may be downloaded at: http:/Iportal.ncdenr.org/web/wq/wslsu/npdessw#tab-4 SWU-249 I.ast Revised: October 18, 2012 Page 2 of 2 w April 20, 2018 ?3e �1 7 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: No Flow Report — March 2018 Tier 3 Stormwater Monitoring �'Vertelius° Smart Chemistry. Our Speciaity.- RECEiIVED APR S 6 Z018 CENTRA4 FILES DWR SECTION On October 26, 2016, Vertellus Performance Materials Inc. (now Vertellus Greensboro LLC} submitted notification that the site falls under Tier III stormwater notification requirements for COD and TSS on Outfall #6. This is to report that there was no measurable flow from Outfall #6 on site during a time when sampling was possible for the month of March 2018. Please contact me at 336-834-4957 if you require additional information. Benjamin D Stewart Site Director Vertellus Greensboro LLC Vertellus Greensboro LLC 2110 W. Gate City Blvd. Greensboro, NC 27403 Phone. (336) 292-1781 Fax. (336) 854-4058 www,vertellus.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted �4 15 2018 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Greensboro COUNTY Guilford PERSON COLLECTING SAMPLES Ben Stewart LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall Z or ® No discharge this period' Outfall'No. 'Sample Collected, . = mo/dd/yr ' :, . - ;'TSS, . mg/L pH, :; Standard units COD, mg/L oil and Grease, mg/L. Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark 100 or S0" , : Within 6:0 9.0 - 120, - .30. 1000 500 01 --- --- - - - --- n/a n/a 02 --- --- --- --- --- n/a n/a 03 --- --- --- --- -- n/a n/a 04 --- --- --- --- --- n/a n/a 05 - - --- --- --- --- n/a n/a Ob - - - - --- -- - - n/a n/a ' Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No.- Sample Collected,' mo/dd/yr' 'Oil and Grease, mg/L TSS, ` mg/L.' .pH, standard units New Motor Oil Usage, Annual average gal/mo Benchmark. - 30 100 or 504 .6.0'= 9.0 - ' Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Q ve5, complete Part Bj .1 SWU-249 Last Revised: October 18, 2012 Page i of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NOEI IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Mail an original and one copy of this DMR, including) all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) �4 15 2018 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/`wglwslsu/npdessw#tab-4 16 S W U-249 Last Revised; October 18, 2012 I'age 2 of 2 oe E March 15, 2018 Page I 1 RECEIVED MAR 2 4 2018 CENTRAL DWRSECTIO' N' Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: No Flow Report — February 2018 Tier 3 Stormwater Monitoring Vertelluso Smart Chamis".Our Spacialty.- NCG-- 06 0 a Cl On October 26, 2016, Vertellus performance Materials Inc- (now Vertellus Greensboro LLC) submitted notification that the site falls under Tier III stormwater notification requirements for COD and TSS on Outfall #6. This is to report that there was no measurable flow from Outfall #6 on site during a time when sampling was possible for the month of February 2018. Please contact me at 336-834-4957 if you require additional information. Benjamin D Stewart Site Director Vertellus Greensboro LLC Vertellus Greensboro LLC 2110 W. Gate City Blvd. Greensboro, NC 27403 Phone. (336) 292-1781 Fax. (336) 854-4058 www.vertellus.com *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 3/15/2018 (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 S W U-249 Last Revised: October Is, 2012 Page 2 of 2 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT' for North Carolina Division of Water Quality General Permit No. NCGO60000 . Date submitted 11/1712017 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Greensboro LLC COUNTY Guilford PERSON COLLECTING SAMPLES Ben Stewart LABORATORY Meritech Lab Cert. ## 165 Part A: Stormwater Benchmarks and Monitoring Results To to! event rainfall' 0.84" or ❑ No discharge this period' Outfall No. i, Sample Collected, mo/dd/yr TSS,. =• mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L ' Fecal Coliforml, Colonles per 100 ml : Enterococcil, Colonies per 100 ml Benchmark 100 or 504 Within 6.0-9.0 .120 30 1000 Soo 01 9/6/2017 <2.5 7A2 <15 <5 n/a n/a 02 Representative --- - --- n/a'- n/a 03 Representative --- - - - n/a n/a 04 Representative -- - - - n/a n/a 05 Representative - - - - - n/a n/a 06 9/6/2017 32 6.94 233 <S n/a n/a 1 Only applies to facilities that use/process meats. Z The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. "See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using.more than 55 gallons of new motor oil per month? E yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. �' W Sanple Collected, , rho/dd/yr Oil and Grease, mg/L TSS, . mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark _; 30 100 or so" i 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. z The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any'outfalls, you must still submit this discharge monitoring report with a checkmark here. ''See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (lfyes, complete Part B) SWLJ-249 Last Revised: October 18, 2012 Page I o l' 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART li SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office____ Mail an original and one copy of this DMR, including all "N_ o Discharge" reports1 within 30 days of receipt of the lab results_ jor at end of monitoring period in the case of "No Discharge"' reports) to: Division of Water Quality Attn: DWQ Central Files i 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 11/17/2017 (Date) Additional copies of this form may be downloaded at: htt ): nortal.ncdenr_org//web/wq/ws/su/nodessw##tab-4 S WU-249 Last Revised: October 18, 2012 Page 2 of 2 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 I � Contact: Ben Stewart Report Date: 9/13/2017 Client: Vertellus Performance 2110 High Point Rd. Project: 1H2015 Stormwater Greensboro, NC 27403 Date Sample Rcvd: 9/8/2017 Meritech Work Order # 09081704 Sample: Outfall 41 Grab 9/6/17 Parameters Result Analysis Date Reporting Limit Method COD <15 mg/L 9/11/17 15 mg/L EPA 410.4 Total Suspended Solids <2.5 mg/L 9/11/17 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 9/12/17 5 mg/L EPA 1664E PH 7.42 S.U. 9/6/17 1.0 - 14.0 S.U. SM 4500-HB Meritech Work Order # 09081705 Parameters Sample: Outfall 46 Grab 9/6/17 Result Analysis Date Reporting Limit Method COD 233 mg/L 9/11/17 15 rng/L EPA 410.4 Total Suspended Solids 32 mg/L 9/11/17 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 9/12/17 5 rng/L EPA 1664B PH 6.94 S.U. 9/6/17 1.0 - 14.0 S.U. SM 4500-HB 1 I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336) 342-1522 Chain of Custod Record COC Client: Vertellus Address: Vertellus 2110 High Point Road Greensboro, NC 27403 Attention: Ben Stewart email: bstewart@vertellus.com NPD1 s#: Phone: 336-834-4903 Fax: Email: mkdreisffr vertOus.com Project: 1H2015 Slormwater Po #: MERITECH INC. ' Environmental Laboratories A Division oiWatcr Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Pax: 1-336-342-1522 27320 Email: wtclabobellsout_h.net Web Site: www.meritech-labs.com Turn ArOnd Time' Std (10 days) 3 25 Day t 24 -48 Hr i Sample LoeationllD # Sampling Dates & Times, Person Taking Sample (Signature): Lab Use Only START E140 Comp? Grab? # of cants. Tests Required 6n Ica? pH OK? C120K? Date Time Date Time Outfall #1 9/612017 1:10 PM Grab 1 Oil and Grease 7 ( yes Outfall #1 9/6/2017 1:10 PhI Grab 1 Total Suspended Solids yes Outfall #1 9/6/2017 1:10 PM Grab 1 COD pH = 7.42 yes ' Outfall #6 9/6/2017 1:15 PM Grab 1 Oil and Grease (, J Outfall #6 916/2017 1:15 PM Grab 1 Total Suspended Solids Outfall #6 9/6/2017 1:15 PM Grab 1 COD pH=6.94 Method of Shipment: Comments: Arm i 48RU C�.f,e M1 J UPS ❑Fed Ex ❑ Hand Delivery�-- ❑Other Will these results he used frtr regulatory pur es? Yes xx No * RUSH work must be approved prior to submitting samples. Relln I ed by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: _ Received N b b I J oat g: Time; SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 11/17/2017 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Greensboro LLC COUNTY Guilford PERSON COLLECTING SAMPLES Ben Stewart LABORATORY Meritech Lab Cert. d 165 Part A: Stormwater Benchmarks and Monitoring Results Totol event rainfall a 1.53" or ❑ No discharge this period Outfall No.' Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, . • . mg/L, Oil and Grease, . ,tng/L_ Fecal Coliform;, ' Colonies per 100 ml ...Enterococcil,* Colonies per 100 m! Benchmark' 100 or 504 •Within 6.0 — 9.0 120 30 11DO S00 ; 01 10/23/2017 105 --- 40 <5 n/a n/a 02 10/23/2017 90 -- <15 <5 n/a n/a 03 Representative --- --- --- --- n/a n/a 04 Representative - - - - - n/a n/a 05 Representative -- --- --- --- n/a n/a 06 10/23/2017 14 --- 17 <5 n/a n/a ' Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any. outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? [] yes Z no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or SW 6.0 — 9.0 - Only applies to facilities that use/process meats, xThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at i a outfalls, you must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies (ifyes, complete Part B) S"'U-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. * 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. * TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES 0 NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Mail an original and one copy of this OMR, including all "No Discharge" reports, within 30 days of receipt of the lob results !or at end of monitorina period in the case of "No_Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center IL Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signatutle' of Permittee) 11/17/2017 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wqLws/su/npdessw#ttab-4 SW U-249 Last Revised: October 18.2012 Page 2 of 2 Meritech, Inc. Environmental Laboratory - Laboratory Certification No. 165 Contact: Ben Stewart Report Date: 1 l/1/2017 Client: Vertellus Performance 2110 High Point Rd. Project:1 1-12015 Stormwater Greensboro, NC 27403 Date Sample Rcvd: 10/26/2017 Meritech Work Order # 10261701 Sample: Outfall #1 Grab 10/23/17 Parameters Result Analysis Date Reporting Limit Method COD 40 mg/L 10/30/17 15 mg/L EPA 410.4 Total Suspended Solids 105 mg/L 10/30/17 2.5 mg/L SM 254.0 D Oil & Grease (HEM) <5 nag/L 10/30/17 S nig/L EPA 1664-B Meritech Work Order # 10261702 Sample: Outfrtll #2 Grab 1D/23/17 Parameters Re ul Analysis Date Reporting Limit Method COD <15 mg/L 10/30/17 15 mg/L EPA 410.4 Total Suspended Solids 90 mg/L 10/30/17 2.5 mg/L SM 2540 D Oil & Grease {HEM) <5 mg/L 10/30/17 5 mg/L EPA 1664B Meritech Work Order # 10261703 Sample: Outfall #6 Grab 10/23/17 Parameters Result Analysis Date Reporting Litnit Method COD 17 ing/L 10/30/17 15 mg/L EPA 410.4 Total Suspended Solids 14 mg/L 10/30/17 2.5 rng/L SM 2540 l) Oil & Grease (HEM) <5 mg/L 10/30/17 5 ntg/L EPA 1664B 1 hereby certify that i have reviewed and approve these data. G. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336) 342-1522 Chain of Custody Record (COC Client: Vertellus Address: Verteilus 2110 High Point Road Greensboro, NC 27403 Attention: Ben Stewart email: bstewart@vertellus.com NPDES At:1 Phone: Fax: Email: Project: Po #: 336-834-4957 bstewa_rt ct�i vertellus.com 1H2O15 Stormwater ERI l ECH INC. -" Environmental Laboratories A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab(&bel lsauth.net Web Site: www.meritech-labs.com Turn Around Time* Std (10 d s) 3 - 5 Day © 24 - 48 Hr [� Sample LocationllD # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START FND comp? Grab? #et Cents, Tests Required on Ice—?ry pHOtc? C12 0K? Date Time Date Time Outfall #1 10/2312017 8:00 PM Grab 1 Oil and Grease, TSS, COD yes Outfall #2 1012312017 8:00 PM Grab 1 Oil and Grease, TSS, COD yes Outfall #6 10/23/2017 8:00 PM Grab 1 Oil and Grease, TSS, COD i73 yes Method of Shipment: Comments: UPS Fed Ex Haled Delivery ❑Other Will these results be used for regulatory purposes? Yes xx / No *RUSH work must be approved prior to submitting samples. Relinquished by: Date: Time: �'� / 1 _.. 1012 5 Rece b Date: Time: 0�1� R linqui h by: Date: r e: V Received by: Date: Time: Relinquished by: Date: Time: Receiv a b L� tg: I T* September 6, 2017 Page I 1 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: No Flow Report — August 2017 Tier II Stormwater Monitoring N--d6oag9 �V'Vertellus• Smart Chemistry. Our Specialty. - RECEIVED OCT 03 2017 CENTRAL FILES DWR SECTION On October 26, 2016, Vertellus Performance Materials Inc. (now Vertellus Greensboro LLC) submitted notification that the site falls under Tier II stormwater notification requirements for COD and TSS on Outfall #6. This is to report that there was no measurable flow from Outfall #6 on site during a time when sampling was possible for the month of August 2017. Please contact me at 336-834-4903 if you require additional information. L'."aatz�o e�— Michelle Kareis EHS Manager Vertellus Greensboro LLC Vertellus Greensboro LLC 2110 W. Gate City Blvd. Greensboro, NC 27403 Phone. (336) 292-1781 Fax. (336) 854-4058 w w ,vertetlus.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 9/27/2017 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Performance Materials Inc. COUNTY Guilford PERSON COLLECTING SAMPLES Michelle Kareis LABORATORY Meritech Lab Cert. # 165 . Part A: 5tormwater Benchmarks and Monitoring Results 1/20/2017 Total event rainfoll 2 .34" or ❑ No discharge this period' Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 501 Within 6.0 — 9.0 120 30 1000 500 01 9/1/2017 21 6.71 45 <5 n/a n/a 02 Representative --- - - --- - n/a n/a 03 Re resentative --- -- --- - n/a n/a 04 Representative --- --- -- n/a n/a' 05 9/ 1 /2017 9 7.05 17 5 n/a n/a 06 9/1/2017 557 7.09 153 <5 n/a n/a 1 Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. QSee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies, Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gaVmo Benchmark - 30 100 or 504 6.0 - 9.0 - 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site. rain gauge. s For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. (if ves, complete Part B) S W U-249 Last Revised: October 18, 2012 Page 1 of 2 °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: _Winston Salem Regional Office_ Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge"ports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 JL_ YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete, i am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 9/27/2017 (Date) Additional copies of this form may be downloaded at: http://portal,ncdenr.org/web/wg/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Revised Dab 912712017 Contact: Ben Stewart Report Date: 9/7/2017 Client: Vertellus Performance 2110 High Point Rd. Project: IY12015 Stormwater Greensboro, NC 27403 Date Sample Rcvd: 9/6/2017 Meritech Work Order h 09061701 Semple: OMNI #1 Grab 9/1/17 Parameters Result Analysis Date Reporting Limit Method COD 45 mg/L 9/6/17 15 ma/L EPA 410.4 Total Suspended Solids 21 ma/L 9/6/17 2.5 nig/L SM 2540 D Oil & Grease (HE,IM) <5 mg/L 9/7/17 5 mo/L EPA 1664E pH 6.71 S.U. 9/1/17 1.0 - 14.0 S.U. SM 4500-HB Meritech Work Order # 09061702 Sample: Outfall #5 Grab 9/1/17 ( Parameters Result Analysis Date Reporting Limit Method COD 17 mg/L 9/6/17 15 mg/L EPA 410.4 Total Suspended Solids 9 mg/L 9/6/17 2.5 mg/L SM 2540 D Oil & Grease (HEM) 5 mg/L 9/7/17 5 mg/L EPA 1664B PH 7.05 S.U. 9/1/17 1.0 - 14.0 S.U. SM 4500-H3 Meritech Work Order # 09061703 Sample: Outfall 46 Grab Parameters Result Analvsis Date COD 153 mg/L 9/6/17 Total Suspended Solids 557 mg/L 9/6/17 Oil & Grease (FIMM) 5 mg/L 9/7/17 PH 7.09 S.U. 9/1/17 9/1/17 Reporting Limit Method 15 mg/L EPA 410.4 2.5 mg/L SM 2540 D 5 mg/L EPA 1664B 1.0 - 14.0 S.U. SM 4500-HB I hereby certify that 1 have reviewed and approve these data. �-' 4V Laboratory Representative A 642'ramco Road, Reidsville, North Carolina 27320 tel.1`3361 342-4748 faxf3361 342-1522 Chain of Custody Record COC Client: Vertellus NPDES #: Phone: 336-834-4903 MERITECH INC. Environmental Laboratories - - Fax: --- �y r.= tG'°y A Division of Water Technology and Control, Inc. Address: Vertellus Email: _ t,rr :iiois VMl<_�lik1`J'0(n 2110 High Point Road Project: IH2015 Storniv'JateT 642 Tamco Rd Phone 1-336-342-4748 Greensboro_, NC 27403 Po #: Reidsville, NC Fax: 1-336-342-1522 l�x:� S�c°c-=cuff Turn Around Tirne" Std (10 days) 3 - 5 Day 24 - 48 Hr 27320 Email: wtclab a bellsouth.net Attention: il+'illu"lle_-Ka-reis Web Site: www.meritech-labs.com rm10:.m"T4ik �=vPrtPll r�,,, �•,-,� ��.�r�< <3 F=-� --- -1 Sample Sampling Dates & Times p g �'�' Person Taking Sample (Sic3nahrrel Lab Use only START END Comp? #nf Tests Required On pH OK? LocationllD # Date Time Dale line Grah? Cnn1s ice? C120K? � Outfall #1 91112017 8:35 AM Grab 1 Oil and Greasy Yes ll Outfall #1 91112017 8:35 AM I Grab 1 Total Suspended Solids yes Outfall #1 9/112017 8:35 AM Grab 1 COD pH = 6.71 yes Outfall #5 911/2017 8:45 AM R r, ; Grab 1 Oil and Grease 0 -� Outfall #5 9/1/2017 8:45 AM Grab 1 Total Suspended Solids Outfall 45 911/2017 8:4.r AM I •'' .4 ' ''�" - Grab 1 COD pH=7.05 Outfall #6 911/2017 8:20 AM Grab 1 Oil and Grease �' > Outfall #6 9/112017 8:20 AM Grab 1 Total Suspended Solids Outfall #6 9/1/2017 8:20 AM Grab 1 COD pH=7.09 Comments: Method of Shipment: EJ UPS Will these results be used for regulatory purposes? `RUSH work must be approved prior to submitting samples. Ex Fed Yes rx No Rehm Uiaped by: ale: �/ Time; RC ,verl t _ nar Tirne: Hand Delivery - j' ! �}X (� Reli sh d % iv Time; 1 I.; I."f Re.reived by: Dale: Tirne: Other _ Rerinq shed key; Date: Time: Reee+ved.al. 1ati LY:� p. e: Tirne: SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 2/1/2017 RECEIVED CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Performance Materials Inc. COUNTY Guilford PERSON COLLECTING SAMPLES Michelle Kareis LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results FEB 07 n i/- CENTRAL FILES DWR SECTIOnj 1/20/2017 Total event rainfall 2 .34 " orE] No discharge this period' 0 U tf U_�' all No. - .1_i�airv?_Pli'Colleited;,�� mo/dd/yrr p H —Standard unit Cow rng/L`V- Oil and Grease,' ',i n 'I ecal Colifo Colonles7per 100 mil.j.. es per 100 ml Colonies Co on Benchmarks; 100 or 504 Within 6.0 r 9&-` 120,-_tt,- .,30 1000_ ,,: 4 01 1/20/2017 64 6.43 354 <5 n/a n/a 02 Represmitatwe --- --- n/a n/a 03 Representative --- --- n1a n/a 04 Representative --- --- n/a n/a 05 1/20/2017 3 6,05 41 <5 n/a n/a 06 1/20/2017 96 8.66 79 <5 n/a n/a Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? [:] yes E no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > SS gal of new motor oil/month. Ou IN siftipli e o� -6114-d _d; rno/dd/yr_,�- - 4- ,,oil and Grease,-. 2, SS - e"pH,"A T Mg/L,- units, Hew *Woto-r-bil Usage,4 Annual iveriage ial/rno�. senchrnarWt� f,, 00 or SWt, 16.0 9.0 I Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. I For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. (if yes, complete Part B) SWU-249 Last Revised: October 18, 2012 Page I of 2 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. *FOR PART A AND PART 8 MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information; jncluding the possibility of fines and imprisonment for knowing violations." ure of Perrnittee) 2/1/2017 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 1 R, 2012 Page 2 of 2 600 rte I I u s® C C December 1, 2016 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: No Plow Report — November 2016 Tier Il Stormwater MonitoringFit. ipt� 2-- On October 26, 2016, Vertellus Performance Materials Inc. (now Vertellus Greensboro LLC) submitted notification that the site falls under Tier 1I stormwater notification requirements for COD and TSS on Outfali #6. This is to report that there was no measurable flow from Outfall #6 on site for the month of November, 2016. Please contact me at 336-834-4903 if you require additional information. `-" RECEIVFr % Michelle Kareis JAN 1.2 20 EHS Manager Vertellus Greensboro LLC DENR-LAND QUP'. STORMWATERPER.,,,, RECEIVED JAN 12 2017 DENR-LAND QUALITY STORM%tiIATER PERMITTING Vertellus Greensboro LLC 2110 W. Gate City Blvd. Greensboro, NC 27403 Phone. (336) 292-1781 Fax. (336) 854-4058 www.vertellus.com November 2, 2016 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: No Flow Report — October 2016 Tier II Stormwater Monitoring P Vertellus$§ N e &-o 46 6 -a-9' Y RECEIVED NOV 0 9 2016 CENTRAL FILES DWR SECTION On October 26, 2016, Vertellus Performance Materials Inc. (now Vertellus Greensboro LLC) submitted notification that the site falls under Tier II stormwater notification requirements for COD and TSS on Outfall 96. This is to report that, from the time the results were received until the end of the month, there was no measurable flow from Outfall 96 on site. Please contact me at 336-834-4903 if you require additional information. i af.(-��l F-a" Michelle Kareis EHS Manager Vertellus Greensboro LLC Vertellus Greensboro LLC 2110 W. Gate City Blvd. Greensboro, NC 27403 Phone. (336) 292-1781 Fax. (336) 854-4058 www.vertellus.com SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 1OL24/2016_ CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Performance Materials Inc. COUNTY Guilford PERSON COLLECTING SAMPLES Michelle Kareis LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results RECEIVED OCT 31 2016 CENTRAL FILES DWR SECTION 9/19/2016: .32" Total event rainfall' .32" or ❑ No discharge this period' Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliformx, Colonies per 100 ml Enterococcil, Colonies pei 100 nil Benchmark - 100 or 504 Within 6.0 — 9.0 120 . 30 1000 500 01 9/19/2016 6 6.87 47 17 n/a n/a 02 Representative --- --- --- --- n/a n/a 03 Representative --- --- --- n/a n/a 04 Representative --- --- --- n/a n/a 05 9/19/2016 <2.5 7.2 20 <5 n/a n/a 06 9/19/2016 932 8.5 137 <5 n/a n/a 1 Only applies to facilities that use/process meats. z The total precipitation must be recorded using data from an on -site rain gauge. s For sampling periods with no discharge at � outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at ate( outfalls, you must still submit this discharge monitoring report with a checkmark here. (if yes, complete Part Bj SWU-249 Last Revised: October 18, 2012 Page 1 of 2 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center it Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of m knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, iouding the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 10/26/2016 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw##tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 Tier 1 Stormwater Management Inspection Date: Thursday, October 20, 2016 Conducted by: Michelle Kareis Weather: Partly Cloudy, 82°F Sample Results Leading to Inspection: Outfall COD TSS O/G PH (std. Monitoring # (mg/1) (mg/i) (mg/I) units) Date period 120 100 30 6.0 - 9.0 9/19/2016 21-12O16 6 137 j 932 j <5 8.50 4/22/2016 11-12O16 6 897 1 2130 1 38 7.60 Outfall #6: Drain clear. No drainage present. No evidence of spills or other materials on ground near drain or in drum/tote storage area adjacent to Bldg. 14. Identified cause of benchmark exceedences: No specific causes were identified to contribute to identified exceedences. Area in front of drain is clean and there does not appear to be any contamination. Methods to reduce concentrations of parameters of concern: • Source Controls: None identified • Operational Controls: None identified • Physical improvements: Concrete containment wall installed around cooling towers. Action items to reduce or eliminate exceedences: None identified SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 11/19/2015 CERTIFICATE OF COVERAGE NO. NCG06 0098 i FACILITY NAME Vertellus Performance Materials Inc. COUNTY Guilford RECE-IVIED PERSON COLLECTING SAMPLES Michelle Kareis JAN 1 I LABORATORY Meritech Lab Cert. # 165 ZD16 CEf�lifiRl �� [11'/29:,1.21t LEA Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall z " i 1bor� A No discharge this period' Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococcl','4% Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 500 01 02 03 11/19/2025 3 7.0 55 <5 04 05 06 1 1 / 19/2015 4 17.14 43 <4 ' Only applies to Facilities that use/process meats. "The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50' 6.0 — 9.0 - I Only applies to facilities that use/process meats. 2 The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls; you must still submit this discharge monitoring report with a checkmark here. 45ee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. S WU-249 (if yes, complete Part B) Last Revised; October 18_ 2012 Pave 4 of 2 *FOR F4tRT A'AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART It SECTION B_ • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARKS EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days -of receipt of the lob results (or at end_of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) _ 1/5/2016 (Date) Additional copies of this form may be downloaded at: http:Z/portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 Chain of Custody Record COC Client: Vertellus Address: Vertellus 2110 High Point Road Greensboro, NC 27403 Attention: Michelle Kareis email: mkareis@vertellus.com NPDES#: Phone: 336-834-4903 Fax: Email: mkareis@yertellus.com Project: 1 H201 5 Stormwater Po #: _MERITECH INC. Environmental Laboratories A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab@bellsouth.net Web Site: www.meritech-labs.com Turn Around Time* Std (10 days) 3 - 5 Day © 24 - 48 Hr t� Sample Location/ID # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? #of Conts. Tests Required On Ice? pH OK? C120K7 Date Time Date Time ©utfall #3 1111912015 7:15 AM Grab COD yes Method of Shipment: Comments: Composite 624 vials prior to analysis. Please perform clean up procedures on organics to obtain lowest possible reporting limit. ❑ UPS ❑ Fed Ex ❑ Hand Delivery ❑Other Will these results be used for regulatory purposes? Yes JXX No *RUSH work must be approved prior to submitting samples. Relin is ad by: Date: T e: / L2. l� Receiv y Dittet Time: — U Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Received at lab by: Date: Time: SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 10/22/2015 ECC I Vim' CERTIFICATE OF COVERAGE NO. NCG06 0098 OCT 3 0 2015 FACILITY NAME Vertellus Performance Materials Inc. COUNTY Guilford CENTRAL FILES PERSON COLLECTING SAMPLES Michelle Kareis DWR SECTION LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall'. I 10/2: .93" or ❑ No discharge this period3 Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 50' Within 6.0 — 9.0 120 30 1000 500 01 10/2/2015 3 6.75 34 <5 02 10/2/2015 4 7.32 32 <5 03 10/2/2015 14 6.45 147 <5 04 10/2/2015 3 7.68 48 7 05 10/2/2015 <2.5 6.58 146 1 7 06 1 Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50' 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at anv outfalls, you must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (ice complete Part B) SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail on original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 10/23/2015 (Date) Additional copies of this form may be downloaded at: htto://portal.ncdenr.orR/web/wq/ws/su/npdessw##tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: Michelle Kareis Client: Vertellus Performance 2110 High Point Rd. Greensboro, NC 27403 Meritech Work Order # 10051506 Sample: Outfall #1 Grab Report Date: 10/13/2015 Project:1H2O15 Stormwater Date Sample Rcvd: 10/5/2015 10/2/15 Parameters Result Analysis Date Reporting Limit Method COD 34 mg/L 10/6/15 15 mg/L EPA 410.4 Total Suspended Solids 3 mg/L 10/6/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 10/12/15 5 mg/L EPA 1664A Meritech Work Order # 10051507 Sample: Outfall #2 Grab 10/2/15 Parameters Result Analysis Date Reporting Limit Method COD 32 mg/L 10/6/15 15 mg/L EPA 410.4 Total Suspended Solids 4 mg/L 10/6/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 10/12/15 5 mg/L EPA 1664A I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-474B fax(336) 342-1522 Chain of Custody Record COC Client: Vertellus Address: Vertellus 2110 High Point Road Greensboro, NC 27403 Attention: Michelle Kareis email: mkareis@vertellus.rom NPDES#: Phone: 336-834-4903 Fax: Email: mkareis@vertellus.com Project: 1H2015 Stormwater Po #: MERIT CH INC. Environmental Laboratories A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Pax: 1-336-342-1522 27320 Email: wtclab(a)bellsouth.net Web Site: www.meri•tech-labs.com Turn Around Time* Std V6 days) 3 - 5 Day o 24 - 48 Hr 0 Sample LoeationllD # Sampling Dates & Times' person Taking Sample (Signature): Lab Use Only START END Comp? Grab? # of cents. Tests Required On Ice? pH OK? C12OK? Date Time Date Time Outfall #1 1012/2012 12:05 AM Grab 1 Oil and Grease b yes ':7) tLrL €- r_ ,a Outfall #1 10/2/2012 12:05 AM Grab 1 Total Suspended Solids yes Outfall #1 10/2/2012 12:06 AM Grab 1 COD yes y J c-0 ` S• � Outfall #2 10/2/2012 12:13 AM Grab 1 Oil and Grease yes �- Outfall #2 10/2/2012 12:13 AM Grab 1 Total Suspended Solids yes Outfall #2 10/2/2012 12:13 AM Grab 1 COD yes Method of Shipment: Comments: Composite 624 vials prior to analysis. Please perform clean up procedures on organics to obtain lowest possible reporting limit. UPS ❑ Fed Ex Hand Delivery Other Will these results be used for regulatory purposes? Yes roc No *RUSH work must be approved prior to submitting samples. RelinJ%Date-_ %(� ��_ / �� J7 '�� R�Da Is Time: Re ' i ed b Dat Time: la '� t o Received by: Date: Time: Relinquished by: Date: Time: _ Receive t I b by: Dat Time: �� 1 Meritech, Inc. Environmental Laboratory r - Laboratory Certification No. 165 r Contact: Michelle Kareis Report Date: 10/14/2015 Client: Vertellus Performance 2110 High Point Rd. Project:1H2O15 Stormwater Greensboro, NC 27403 Date Sample Rcvd: 10/5/2015 Meritech Work Order # 10051508 Sample: Outfall #3 Grab 10/2/15 Parameters Result Analysis Date Reporting Limit Method COD Total Suspended Solids Oil & Grease [HEM) 147 mg/L 14 mg/L <5 mg/L 10/6/15 10/6/15 10/12/15 15 mg/L 2.5 mg/L 5 mg/L EPA 410.4 SM 2540 D EPA 1664A Meritech Work Order # 10051509 Sample: Outfall #4 Grab 10/2/15 Parameters Result Analysis Date Reporting Limit Method COD 48 mg/L 10/6/15 15 mg/L EPA 410.4 Total Suspended Solids 3 mg/L 10/6/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) 7 mg/L 10/13/15 5 mg/L EPA 1664A I hereby certify that I have reviewed and approve these data. �' 4'�' Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336) 342-1522 sl1tto�od Record COC Chain of CCu��ERI Client: Vertellus Address. Vertellus 2110 High Point Road Greensboro, NC 27403 Attention: Michelle Kareis email: mkareis@vertellus.com NPDES #: Phone: 336-834-4903 Fax. Email: mkareis a.vertellus.com Project: 1H2015 Stormwater Po #: ���I ECH INC.1� �i, N't Environmental Laboratories A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab@bellsouth.net Web Site: www.meritech-labs.com Turn Around Time Std P-days) 3 - 5 Day 24 - 48 Hr 0 Sample LocatlonllD # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? #af Conts. Tests Required On Ice? pH OK? C 2OK? Date Time Date Time Outfall #3 101212012 12:21 AM Grab 1 Oil and Grease � � yes '� • � Outfall #3 10/212012 12:21 AM Grab 1 Total Suspended Solids yes Outfall #3 10/2/2012 12:21 AM -- Grab 1 COD yes Outfall #4 10/2/2012 12:34 ANI Grab 1 Oil and Grease yes =' Outfall #4 10/2/2012 12:34 AM Grab i Total Suspended Solids yes Outfall #4 1012/2012 12:34 AM Grab 1 COD yes Method of Shipment: Comments: Composite 624 vials prior to analysis. Please perform clean up procedures on organics to obtain lowest possible reporting limit. UPS Fed Ex Hand Delivery OC?ther Will these results be used for regulatory purposes? Yes )oc No *RUSH work must be approved prior to submitting samples. Relin ui hed by: Date', Time: �/I %U�5 /� t��(� Rff a ved y: Dale Time: !i / �[ �~ / (��,3C/ Re nq Xhb y: D e: Time: Received by: Date: Time: Relinquished by: Date: Tlme: Receiveb by: DatTime: d a ae' Meritech, Inc, Environmental Laboratory Laboratory Certification No. 165 Contact: Michelle Kareis Report Date: 10/14/2015 Client: Vertellus Performance 2110 High Point Rd, Project:1H2015 Stormwater Greensboro, NC 27403 Date Sample Rcvd: 10/5/2015 Meritech Work Order # 10051510 Sample: Outfall #5 Grab 10/2/15 Parameters Result Analysis Date Reporting -Lim t Method COD 46 mg/L 10/6/15 15 mg/L EPA 410.4 Total Suspended Solids <2.5 mg/L 10/6/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) 7 mg/L 10/13/15 5 mg/L EPA'1664A ! hereby certify that 1 have reviewed and approve these data. I,. 4U 9C Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336) 342-1522 Chain of CCul1s�stod Record COC Client: Vertellus Address. Vertellus 2110 High Point Road Greensboro, NC 27403 Attention: Michelle Kareis email: mkareis@vertellus,com NPDES #: Phone: 336-834-4903 Fax: Email: mkareis0vertellus.com Project: 1H2015 Stormwater Po #: MERITECH INC. Environmental Laboratories f� A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342.1522 27320 Email: wtclab(&bellsouth.net Web Site: www.meritech-labs.com Turn Around Time* Stq (10 days) 3 - 5 Day © 24 - 48 Hr l� Sample Locationll©# Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? #of Cents. Tests Required On Ice? pH OK? C12OK? Date Time Date Time Outfall #5 10/2/2012 12:37 AM Grab 1 Oil and Grease U yes Outfall #5 1012/2012 12:37 AM Grab 1 Total Suspended Solids yes Outfall #5 1 1012/2012 12:37 AM Grab 1 COD yes Outfall #6 Gr I-- Oil and Grease yes Outfall #6 Grab— 1 Total Suspended Solids yes Outfall #6 Grab —1 COD yes Method of Shipment: Comments: Composite 624 vials prior to analysis. Please perform clean up procedures on organics to obtain lowest possible reporting limit. UPS Fed Ex �] Hand Delivery ' []Other Will these results be used for regulatory purposes? Yes JXX No *RUSH work must be approved prior to submitting samples. ter, Relinqu�iiis d by: ate: Time: Repe d J pat Time: kep qu sh by: ate: Time: cJ 1!5 (� Received by: ate: Time: Relinquished by: Date: Time: Received at by: jam— Date: 1 Time:, c/ l � ! 11 S e- I I NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. http://portal,ncdenr.org/web/wq/ws/su/npdessw#tab-4 Permit No.: N/C/_/�/_/_/_/_/_/ or Certificate of Coverage No.: Facility Name: Vertellus Performance Materials County: Guilford Phone No. 336-834-4903 Inspector: Michelle Kareis Date of Inspection: 10 2 2015 Time of Inspection: 12:00 am Total Event Precipitation (inches]: .93" Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to he performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Page 1 of 7 5WU-242, Last modified 10/25/2012 1.Outfall Description: Outfail No. 01 Structure (pipe, ditch, etc.) pine Receiving Stream: North Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Maintenance shop driveway, manufacturing building. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: clear - light tan Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none noticeable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 7 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. 02 Structure (pipe, ditch, etc.) nine Receiving Stream: North Buffalo Creek Describe the industrial activities that occur within the outfail drainage area. Stormwater discharge from driveway areas Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light tan to light beige 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none noticeable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe NONE. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. 1. Outfall Description: Page 3 of 7 SWU-242, Last modified 10/25/2012 Outfall No. 03 Structure (pipe, ditch, etc.) pipe Receiving Stream: North Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Sheet runoff, driveways, areas without secondary containment. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light tan to light brown _ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none detectable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe NONE. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 4 of 7 SWU-242, Last modified 10/75/2012 1. Outfall Description: Outfall No. 04 Structure (pipe, ditch, etc.) pipe Receiving Stream: South Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Parking Lots. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: clear to light tan_ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none noticeable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and S is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 S 7. is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe None. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 5 of 7 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. OS Structure (pipe, ditch, etc.) pipe Receiving Stream: South Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Driveways, walkways, sheet runoff from roofs. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: clear to light tan 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None detectable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe NONE. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 6 of 7 SWU-242, last modified 10/25/2012 1. Outfall Description: Outfall No. 06 Structure (pipe, ditch, etc.) pipe Receiving Stream: South Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Driveways, walkways, Roof runoff. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: no discharge observed at time of inspection 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None detectable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No B. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 7 of 7 SWU-242, Last modified 10/25/2012 � cfq- d (,00g 9 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 10 22 2015 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Performance Materials Inc. COUNTY Guilford PERSON COLLECTING SAMPLES Michelle Kareis LABORATORY Meritech Lab Cert. # 165 Part A: Stormwater Benchmarks and Monitoring Results 4/22/2016: .4" Total event rainfall ' .4" or ❑ No discharge this period' Outfall No: -_-,. Sample Collected,,, mo/dd/yr , .TS5, - mg/L.... pH, - _ '-Standard unitsi.- COD; _ ' mg/L Oil and Grease,, mg/L Fecal Coliforml, Colonies- er 1b0 ml -': Enterococci=, 'Colonies er 100 ml .- :.100 ar s04 -within 6.0 — 9.0v : _ 120 , 30 01 4/22/2016 22 615 30 <S 02 4/22/2026 77 7.4 27 17 03 4/22/2016 24 6.7 3$5 36 04 4/22/2016 11 7.8 50 46 05 4/22/2016 10 7.2 46 16 06 4/22/2016 13 7.6 873 38 ' Only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at gny outfalls. You must still submit this discharge monitoring report with a checkmark here. "See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > S5 gal of new motor oil/month. Outfall iVo:'• - 5ampl Collected; '- mo/ddJyr.rsig/L-.. #. -- OII and Grease;, „ -> .; TSS, ~ ApN; Standard units• ..-New Motor Oil usage,- _Annuil'average gal/mo Benchmark.. �.. :: t_:r _ 30 `'_ f. : •100 or 504 - 6.0 — 9.0 i ' only applies to facilities that use/process meats. ZThe total precipitation must be recorded using data from an on -site rain gauge. 3 For -sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. "See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part B) SWU-249 Last Revised: oct� 18, 2012 Page t of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES N NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO REGIONAL OFFICE CONTACT NAME. Glen White *4 COD exceedences from Outfall #3 —n side of plant along W. Lee Street Extension. This outfall comingles water from the road with plant discharge. There has been significant road repair activity upstream of this location on W. Cate City Blvd. Mr. White from NCDENR will be on site 6/2016 to review outfall location and possible changes to ensure water from roadways is not comingled with stormwater samples. Mail an original and one copy of this DMR, including a# "No Discharge" reports, within 30 d*Ks of receipt of the fob results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 5/12/2016 (Date) Additional , -es of this form may be downloaded at: http://oortal.ncdenr.org/ '1wq/ws/su/npdesswtttab-4 SWU-249 Last Reviscd: Oct 18, 2012 Page 2 of 2 I Contact: Michelle Kareis Client: Vertellus Performance 2110 High Point Rd. Greensboro, NC 27403 Meritech Work Order # 04221657 Meritech, Inc, Environmental Laboratory Laboratory Certification No. 165 Sample: Outfall #4 Grab Parameters Result Analysis Date COD 50 mg/L 4/25/16 Total Suspended Solids 11 mg/L 4/26/16 Oil & Grease (HEM) 46 mg/L 4/26/16 Meritech Work Order # 04221658 Sample: Outfall #5 Grab Parameters Re-sult Analysis Date COD 46 mg/L 4/25/16 Total Suspended Solids 10 mg/L 4/26/16 Oil & Grease (HEM) 16 mg/L 4/26/16 Report Date: 5/2/2016 Project:1H2O15 Stormwater Date Sample Rcvd: 4/22/2016 4/22/16 Reporting Limit Method 15 mg/L EPA 410.4 2.5 mg/L SM 2540 D 5 mg/L EPA 1664A 4/22/16 Reporting Limit Method 15 mg/L EPA 410.4 2.5 mg/L SM 2540 D 5 mg/L EPA 1664A Meritech Work Order # 04221659 Sample: Outfall #6 Grab 4/22/16 Parameters Result Analysis Date Reporting Limit Method COD 873 mg/L 4/25/16 15 mg/L EPA 410.4 Total Suspended Solids 2,130 mg/L 4/26/16 2.5 mg/L SM 2540 D Oil & Grease (HEM) 38 mg/L 4/26/16 5 mg/L EPA 1664A 1 hereby certify that I have reviewed and approve these data. k . Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336) 342-1522 lain of Record CO Client: Vertellus Address: Vertellus 2110 High Point Road Greensboro, NC 27403 Attention: Michelle Kareis email: mkarels@verfellus.com NPDE5 #: Phone; 336-834-4903 Fax: Email: mkareis(c7vertellus.com Project: 1H2O15 Stormwater Po #: ��Cu��stod iil INC. ` 1 ERI R ECH I -ANQ Environmental Laboratories } �_..- A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1.336-342.4748 Reidsville, NC Fax: 1.336-342-1522 27320 Email: wtclab(abellsouth.net Web Ske: www.meritech-iabs.com Turn Around Time* Sid ( 0 days) 3. 5 Day 24 - 48 Hr Sample Location/lD # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END comp? Grab? #of conts. Tests Required On 1ce7 i • pH OK? C12 OK7 Date Time Date Ttme Outfall #4 4/22/2016 10:20 AM Grab 1 Oil and Grease '737 yes � �- Outfall #4 4/22/2016 10:20 AM Grab 1 Total Suspended Solids yes Outfall #4 4/22/2016 10:20 AM Grab 1 COD yes Outfall #5 4/22/2016 9:45 AM Grab 1 Oil and Grease j �J``y yes :> Outfall #5 4/22/2016 9:45 AM Grab 1 Total Suspender! Solids yes Outfall #5 4/22/2016 9:45 AM Grab 1 COD yes L" Outfall #6 4/22/2016 10.30 AM Grata 1 Oil and Grease �� yes L._), Outfall #6 4/2212616 10:30 AM Grab 1 JTotal Suspended Solids yes Outfall #6 4/22/2016 f 10:30 AM Grab 1 COD yes Method of Shipment: Comments. - [] UPS El Fed Ex Hand Delivery [Other Will these results be used for regulatory purposes? Yes 1xx No *RUSH work must be approved prior to submitting samples. Rellnq Is d by: Date: Time: RerfelvejPbyl .', Dole: Time; .✓�•^ FCi ilT� Relinquish d by: Data: Time: ��,rta �7 ,�,�---� �'�•J'-d - 't` "a Received by: � Data: Time: Relinquished by; Rate: Time: ( Recelv4d-at-Ipt�� y: ]� l �� Date: � Tlme: Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: Michelle Kareis Report Date: 5/2/2016 Client: Vertellus Performance 2110 High Point Rd. Project:1H2O15 Stormwater Greensboro, NC 27403 Date Sample Rcvd: 4/22/2016 Meritech Work Order # 04221654 Sample: Outfall #1 Grab 4/22/16 Parameters Result Analysis Date Reporting Limit Method COD 30 mg/L 4/25/16 15 mg/L EPA410.4 Total Suspended Solids 122 mg/L 4/26/16 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 mg/L 4/26/16 5 mg/L EPA 1664A Meritech Work Order # 04221655 Sample: Outfall #2 Grab 4/22/16 Parameters Result Analysis Date Reporting Limit Method COD 27 mg/L 4/25/16 15 mg/L EPA 410.4 Total Suspended Solids 77 mg/L 4/26/16 2.5 rng/L SM 2540 D Oil & Grease (HEM) 17 mg/L 4/26/16 5 mg/L EPA 1664A Meritech Work Order # 04221656 Sample: Outfall #3 Grab 4/22/16 Parameters Result Analysis Date Reporting Limit Method COD 385 mg/L 4/25/16 15 mg/L EPA 410.4 Total Suspended Solids 724 mg/L 4/26/16 2.5 mg/L SM 2540 D Oil & Grease (HEM) 36 mg/L 4/26/16 5 mg/L EPA 1664A I hereby certify that I have reviewed and approve these data. � . &a�z Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336)'342-1522 lain of Record(COC Client: Vertelius Address: Vertellus 2110 High Point Road Greensboro, NC 27403 Attention: Michelle Kareis _ vertellus.com email: mkarei_s@vertellus.com Phone: 336.834-4903 Fax; Email, mkareis"verteitus.mm Project: 1H2015Slormwater Po #: ��Clu��sttod INC.NPDES#: 1� ERITEC H N Environmental Laboratories I A Divialon of Water Technology and Control. Inc. 642 Tamco Rd Phone 1.336-342.4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclabCEDbellsouth.net Web Site: www.meritech-labs.com Turn Around Time* Std ( 0 days) 3. 5 Day 24 - 48 Hr Sample Location/lD # Sampling Bates & Times Person Taking Sample {Signature}: Lab use only START END comp? Grab? #ot Conte. Tests Required On ice?,.,.).! — pH OK? C120K? Bate Time Date Time Outfall #1 4/22/2016 10:10 AM Grab 1 Oil and Grease �t yes ,• -, Outfall #1 4/22/2016 10:10 AM Grab 1 Total Suspended Solids yes Outfall #1 4/22/2016 10:10 AM, Grab 1 COD yes 4) Z—Viin,. Outfall #2 4/22/2016 10:05 AM Grab 1 Oil and Grease 5tj yes Outfall #2 4/2212016 10:05 AM Grab 1 Total Suspended Solids yes Outfall #2 4/22/2016 10:05 AM Grab 1 COD yes ca 605tt Outfall #3 412212016 10:15 AM Grab Grab Grab 1 Oil and Grease yes e— Outfall #3 4/22/2016 10:15 AM 1 Total Suspended Solids k yes Outfall #3 4/22/2016 10:15 AM 1 ICOD yes Method of Shipment: Comments: Composite 624 vials prior organics to obtain lowest to analysis. possible reporting Please perform clean up procedures limit. on UPS Fed Ex ❑No ❑ Hand Delivery QOther Will these results be used for regulatory purposes? Yes fTx *RUSH work must be approved prior to submitting samples. ReEln uls red by: Date: Time: 41 ,• .r �7 , `r%t,} ,/i��.-{�c.i, Re el d by: Date: Time: ;.Z• Rell� qulI ed by: ` Data: Time: l �l r% Received by: Date: Time: Relinquished bDate: Time: Received at labs y: 1n• t Date: Time: SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 6/15/ 015 CERTIFICATE OF COVERAGE NO. NCG06 0098 FACILITY NAME Vertellus Performance Materials Inc. COUNTY Guilford PERSON COLLECTING SAMPLES Michelle Kareis RECEIVED LABORATORY Meritech Lab Cert. # 165 JUN 19 2015 Part A: Stormwater Benchmarks and Monitoring Results 5121: .89" CENTRAL FILES Total event rainfall s S 2:.74" 0%044harge this period3- Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 50" Within 6.0 — 9.0 120 30 1000 Soo* 01 5/21/2015 13 5.89 39 12 02 6/2/2015 320 6.54 711 27 03 6/2/2015 296 6.45 3160 8 04 5/21/2015 42 7.69 131 <5 05 6/2/2015 6 7.08 117 <5 06 6/2/2015 11576 9.16 7110 8 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. "See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage; Annual average gal/mo Benchmark - 30 100 or 50" 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part B) SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 6 15 2015 (Date) Additional copies of this form may be downloaded at: htt : j rtal.ncdenr.org[weblwg/ws/su/npdessw#tab-4 S WU-249 Last Revised: October 18, 2012 Page 2 of 2 Tier 1 Stormwater Management Inspection Date: Monday, June 15, 2015 11:15 am Conducted by: Michelle Kareis Weather: Clear, 940 F Sample Results Leading to Inspection: Date Monitoring period Outfall # COD (mg/I) T55 (mg/1) O/G (mg/1) PH (std. units) 120 100 30 6.0 - 9.0 6/2/2015 1H2O15 2 711 320 27 6.54 3 3160 296 8 6.45 5 117 6 <5 7.08 6 7110 1576 8 9.16 5/21/2015 1H 2O15 1 39 13 12 5.89 4 131 42 <5 7.69 Outfall #1: Drain clear. No drainage present. No evidence of spills or other materials on asphalt in area of drain. Outfall #2: Drain clear. No drainage present. No evidence of spills or other materials on ground near drain, or in drain areas. Outfall #3: Drain clear. No drainage present. No evidence of spills or other materials on grass or areas upstream of drain in plant. Outfall #4: Drain clear. No drainage present. No evidence of spills or other materials on ground near drain, or in drain areas. Outfall #5: Drain clear. No drainage present. No drainage from roof. No evidence of spills or other materials in trench area or on ground outside lab door. Outfall #6: Drain clear. No drainage present. No evidence of spills or other materials on ground near drain or in drum/tote storage area adjacent to Bldg.14. Identified cause of benchmark exceedences: Outfall #4 City of Greensboro crews rebuilt and applied new asphalt to the front parking lot (affecting Outfall #4) immediately prior to the 5/21 sample date. No other specific causes were identified to contribute to identified exceedences. Methods to reduce concentrations of parameters of concern: • Source Controls: None identified • Operational Controls: None identified • Physical Improvements: None identified Action items to reduce or eliminate exceedences: None identified NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 Permit No.: N/C/_/_/_/_/_/_/_/ or Certificate of Coverage No.: Facility Name: Vertellus Performance Materials County: Guilford Phone No. 336-834-4903 Inspector: Michelle Kareis Date of Inspection: 5/21/2015 Time of Inspection: 9:48 am — Total Event Precipitation (inches): i Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Pagel of 7 SWU-242, Last modified 10/25/2012 1.Outfall Description: Outfall No. 01 Structure (pipe, ditch, etc.) pipe Receiving Stream: North Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Maintenance shop driveway, manufacturing building. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light tan - light brown Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none noticeable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. is there any foam in the stormwater discharge? Yes No S. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 7 5WU•242, Last modified 10/25/2012 1. Outfall Description: Outfall No. 02 Structure (pipe, ditch, etc.) pipe Receiving Stream: North Buffalo Creek Describe the industrial activities that occur within the outfall drainage area. Stormwater discharge from driveway areas Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light tan - light brown 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none noticeable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number'which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe NONE. Not enough rainfall to collect sample of outfall. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 3 of 7 SWU-242, Ust modified 10/25/2012 1. Outfall Description: Outfall No. 03 Structure (pipe, ditch, etc.) pipe Receiving Stream: North Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Sheet runoff, driveways, areas without secondary containment. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light tan to light brown 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none detectable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe NONE. Not enough rainfall to collect sample of outfall. Page 4 of 7 SWU-242, Last modified 10/25/2012 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. 1. Outfall Description: Outfall No. 04 Structure (pipe, ditch, etc.) pipe Receiving Stream: South Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Parking Lots. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light tan to light brown 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none noticeable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe None. Page 5 of 7 SWU-242, Last modified 10/25/2012 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. I. Outfall Description: Outfall No. 05 Structure (pipe, ditch, etc.) pipe Receiving Stream: South Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Driveways, walkways, sheet runoff from roofs. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Light tank to light brown 3. Odor: Describe any distinct odors that the discharge may have (Le_, smells strongly of oil, weak chlorine odor, etc.): None detectable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and S is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe NONE. Not enough rainfall to collect sample of outfall. Page 6 of 7 5WU•242, Last modified 10/25/2012 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. 1. Outfall Description: Outfall No. 06 Structure (pipe, ditch, etc.) pipe Receiving Stream: South Buffalo Creels Describe the industrial activities that occur within the outfall drainage area: Driveways, walkways, Roof runoff. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light tan to brown 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None detectable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe NONE. Not enough rainfall to collect sample of outfall. Page 7 of 7 5WU•242, last modified 10/25/2012 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 8 of 7 SWU-242, Last modified 10/25/2012 A� NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http://portal.ncdennorg/web/wq/ws/suJnpdessw#tab-4 Permit No.: N/C/_/�// _/T/�/`/ or Certificate of Coverage No.: Facility Name. Vertellus Performance Materials County: Guilford Phone No. 336-834-4903 Inspector: Michelle Kareis Date of Inspection: 6/2/2015 Time of Inspection: 6:15 pm Total Event Precipitation (inches): .74" Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall, The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Page 1 of 7 SWU-242, Last modified 10/25/2012 1.Outfall Description: Outfall No. 01 Structure (pipe, ditch, etc.) pipe Receiving Stream: North Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Maintenance shop driveway, manufacturing building. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light tan - light brown Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none noticeable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 7 5WU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. 02 Structure (pipe, ditch, etc.) pipe Receiving Stream: North Buffalo Creek Describe the industrial activities that occur within the outfall drainage area. Stormwater discharge from driveway areas Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: clear to light tan 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none noticeable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the Stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the Stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe NONE. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 3 of 7 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. 03 Structure (pipe, ditch, etc.) pipe Receiving Stream: North Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Sheet runoff, driveways, areas without secondary containment. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light tan to light brown 3, Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none detectable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and S is extremely muddy: 1 2. 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe NONE. Nate: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 4 of 7 5WU•242, Last modified 10/25/2012 1. Outfall Description: Outfall No. 04 Structure (pipe, ditch, etc.) pipe Receiving Stream: South Buffalo . Creek Describe the industrial activities that occur within the outfali drainage area: Parking Lots. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light tan to light brown 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none noticeable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfali? Yes la 10. Other Obvious Indicators of Stormwater Pollution: List and describe None. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 5 of 7 SWU•242, Last modified 10/25/2012 1. Outfall Description: ©utfall No. fly Structure (pipe, ditch, etc.) pipe Receiving Stream: South Buffalo Creek Describe the industrial activities that occur within the outfali drainage area: Driveways, walkways, sheet runoff from roofs. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: clear 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None detectable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2. 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 z 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes 10, Other Obvious Indicators of stormwater Pollution: List and describe NONE. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 6 of 7 SWU•242, Last modified 10/25/2012 1. Outfall Description: Outfall No. 06 Structure (pipe, ditch, etc.) pipe Receiving Stream: South Buffalo Creek Describe the industrial activities that occur within the outfall drainage area: Driveways, walkways, Roof runoff. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: dark tan to -dark brown 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None detectable 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of Floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. is there evidence of erosion or deposition at the outfall? Yes No 1.0. Other Obvious Indicators of Stormwater Pollution: List and describe NONE. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 7 of 7 5WU•242, last modified 10/25/2012 N eritec i, nc. Environmental Laboratory Laboratory Certification No.165 Contact: Michelle Kareis Report Date: 6/2/2015 Client: Vertellus Performance 2110 High Point Rd. Project:1H2O15 Stormwater Greensboro, NC 27403 Date Sample Rcvd: 5/29/2015 Meritech Work Order # 05291502 Sample: Outfall #1 Grab 5/21/15 Parameters COD Total Suspended Solids Oil & Grease (HEM) Result Analysis Date Reporting Limit Meth ualifier 39 mg/L 5/29/15 15 mg/L EPA 410.4 13 mg/L 5/29/15 2.5 mg/L SM 2540 D Q1 12 mg/L 6/1/15 5 mg/L EPA 1664A Meritech Work Order # 05291503 Sample: Outfall #4 Grab Parameters Result Analysis Date Reporting Limit 5/21/15 Methgd Qualifier COD 131 mg/L 5/29/15 15 mg/L EPA 410.4 Total Suspended Solids 42 mg/L 5/29/15 2.5 mg/L SM 2540 D. Q1 Oil & Grease (HEM) <5 mg/L 6/1/15 5 mg/L EPA 1664A Q1 Holding time exceeded prior to receipt by the lab. I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336) 342-1522 Chain of Custody Record COC Client: Vertellus Vertel lus 2110 High Point Road Greensboro, NC 27403 Attention: Michelle Kareis email: mkareis@vertellus.com NPDES #: Phone: 336-834-4903 Fax: Email: mkareis@vertellus.com Project: 1H2015 Stormwater Po #: 1. ERITECH RN. ,, Environmental Laboratories "yam j A Division of water Technology and Control, Inc.Address: �y 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclabobellsouth.net Web Site: www.meritech-labs.com Turn ArRuo Time* Sta �I daysj� -5 Da 24 - 48 Hr o Sample LocationllD # Sampling Dates & Times person Taking Sample (Signature): Lab Use Only START END comp? Grab? #of Conts. Tests Required On Ice? pH OK? C12 OK? Date Time Date Time Outfall #1 5/21/2015 9:48 AM Grab 1 Oil and Grease yes Outfall #1 5/21/2015 9:48 AM Grab 1 Total Suspended Solids yes 5 Outfall #1 5/21/2015 9:48 AM Grab 1 COD yes Outfall #1 Wk 5/21/2015 9:54 AM Grab 1 Oil and Grease yes Outfall #g 5/21/2015 9:54 AM Grab 1 Total Suspended Solids yes `-z Outfall 5/21/2015 9:54 All Grab 1 COD yes Cr _L ,k z4l�, r0 0 L, Method of Shipment: Comments: Composite 624 vials prior to analysis. Please perform clean up procedures on organics to obtain lowest possible reporting limit. ❑ UPS Fed Ex Hand Delivery Other. Will these results be used for regulatory purposes? Yes roc No RUSH wort: must be approved prior to submitting samples. Reli q -shed by: Date: Time: Q R eive Dale: Time: R [nq ! ed by Date : Ti,,,,— Received by: Date: Time: Relinquished by: De e: Time: R:co at I b by./ Date, f Time: %` ' Merxtech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Michelle Karels Client: Vertellus Performance 2110 High Point Rd. Report Date: 6/12/2015 Greensboro, NC 27403 Date Sample Rcvd: 6/3/2015 Meritech Work Order # 06031599 Sample: Stormwater 2 Grab 6/2/15 )Parameters Result Analysis Date Reporting L11rd melho COD 711 mg/L 6/4/15 15 mg/L EPA 410.4 Total Suspended Solids 320 mg/L 6/5/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) 27 ing/L 6/9/15 5 ing/L EPA 1664A I hereby certify that 1 have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336) 342-1522 Chain of Custody Record. (.COC) Client: Vertellus Address: 2110 Highpoint Rd Greensboro, NC 27403 Attention: Michael Bowen Phone: cell Email: Project: Po #: MERI 1 ECH INC. ]t nvi.ronmental Laboratories A. Division of Water Technology and Control, Inc. $ 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab@bellsouth.net Web Site: www.meritech4abs.corn Tung Around Time* Std (10 days) © 3 -5 Ray C� 24-48 Hr Sample LocationliD # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Camp? Grab? !i of conts Tests Required - On 1ce7 pH OK? c,ZOK? Time Date Time Stormwater Z //--Date L� 4,045 zz'&S- 1 TSS E Site # 1 COD (w/H2SO4) c �s IL C7 3� 1 Oil & Grease (w[HC)) y p H Method of Shipment: Comments: El UPS Fen Ex Hand Delivery Will these results be used for regulatory purposes? YesNoRUSH work must be approved prior to submitting samples. Relingesishe y: ate Time: -14219 Reee b �-. p`�;`w Tt�; ��` Date: lime; el'stlgulsh y: d�A- - f 5-- t�; Oil' lRellnquxh-ed- Receivedby: Date:Time:K/QOther ti by: Date: Time; Received at tab by: � Date; Time: \ Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Michelle Kareis Client; Vertellus Performance 2110 High Point Rd. Greensboro, NC 27403 Meritech Work Order # 060315100 Sample. Stormwater 3 Grab Parameters Resul Analysis Date COD 3,160 ing/L 6/4/15 Total Suspended Solids 296 rng/L 6/5/15 Oil & Grease (ITEM) 8 rng/L 6/9/15 Report Date: 6/12/2015 Hate Sample Rcvd; 6/3/2015 6/2/15 Re oorting Limit Method 15 mg/L EPA 410.4 2.5 mg/L SM 2540 D 5 mg/L EPA 1664A I Hereby certify that 1 have reviewed and approve these data. fY Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336) 342-1522 ..Chain. of .Custod Record..COC .. Client: Vertellus Address: 2110 Highpoint Rd Greensboro, NC 27403 Attention: Michael Bowen - - Phone: cell Email: Project: Po M MERITECH INC. - Environmental Laboratories A Division of Water Technology aad Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab@bellsouth.net Web Site: www.meritech4abs.com Turn Around Time" 5td (10 days) n 3 -5 Day EZ= 24-48 Hr Sample LocationllD # Sampling Dates & Times Person Taking Sample (Signature)_ Lab Use Only START END Comp? Grab? # of Cvrrts. Tests Required - Q On lct? PH DK? C'i20K7 Date Time Date Time Stormwater s 1 TSS Site # f2 1 COD twIH2SO4 r-p Z y= 0 1 Oil & Grease (w/HCI) C_ Method of Shipment: Comments: ❑ UPS ❑ Fed Ex ❑ Hand Delivery Pother Will these results be used for regulatory purposes? Yes No *RUSH work must be approved prior to submitting samples. Relinquished by; Date: j' IQ � Time: � � Rece by' Date:. � Relinquished / f Dat : f Time; b d f/+cam ((�2 Jz- �- Received by: Date: Time: Relinqulsh by: Date: Time: Received at lab by: Date: Time: y Meritech, InC. Environmental Laboratory Laboratory Certification No.165 Contact: Michelle Kareis Report Date: 6/12/201S Ciient: Vertellus Performance 2110 High Point Rd. Greensboro, NC 27403 Date Sample Rcvd: 6/3/2015 Meritech Work Order # a60315101 Sample: Stormwater 5 Grab 6/2/15 Parameters Result Analysis Date Reportlue Lunt Method COD 117 nig/L 6/4/15 15 mg/L EPA 410.4 Total Suspended Solids 6 mg/L 6/5/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) <5 Eng/L 6/9/15 5 mg/L EPA 1664A I hereby certify that I have reviewed and approve these data.P/;�/ Laboratory Representative 642 Tanico Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336) 342-1522 Chain of Custody. Record .(COC) _ .. Client: Vertellus Address. 2110 Highpoint Rd Greensboro, NC 27403 Attention: Michael Bowen - iVPQES ji: Phone: cell Email: Project. Po #: MERITECH INC. EnvironmeloW Laboratories �4. A Division of water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab@bellsouth.net Web Site: www.meritach4abs.com Turn Around Time* Std (10 days) © 3 - 5 Day r--= 24 -48 Hr 0 Sample LocationilD# Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only sraxr Ufa Comp? Grab? gat cons Tests Re�t uired - `t On ltn? _�' pHCKT C120K? Date Time Date Timt Stormwater �,� Z,3 = Cg-0 1 TSS Site 1 COD (wlH2SO4) i Oil & Grease (wJHCl) {.2 pti Z Method of Shipment: Comments: UPS Fed Ex Q Hand Delivery �Qther Will these results be used for regulatory purposes? Yes I I No *RUSH work must be approved prior to submitting samples. Relinquished by Datei Time: raj% Received ij Pe Time: Da Relinquished b 4 `�ty.� �� � �"dTim� 4ag zfo-1�&Relinquished Retn[ved by. Date; Time: by: Hate: Time: Received at lab by Date: Time: Mexitech, Ins. Environmental Laboratory AP ,. Laboratory Cea•tilication No.16S Contact, Michelle Karels Report Date: 6/12/2015 Client: Vertellus Performance 2110 High Point Rd. Greensboro, NC 27403 Date Sample lRcvd: 6/3/2015 Meritech Work Order # 060315102 Sample: Stormwater 6 Grab 6/2/15 Parameters $esU Analysls Date Re ortf g U1111 Method COD 7,110 mg/L 6/4/15 15 mg/L EPA 410.4 Total Suspended Solids 1,576 mg/L 6/5/15 2.5 mg/L SM 2540 D Oil & Grease (HEM) 8 mg/L 6/9/15 5 mg/L EPA 1664A I hereby certify that I have reviewed and approve these data. ,6 . X Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336) 342-4748 fax(336) 342-1522 Chain of Custody Record (COC) VertelluS Address: 2110 Highpoint Rd Greensboro, NC 27403 Attention: Michael Bowen NPDES#: S Phone: cell Email: Project: PO #: MERI ECH INC.'Client: ]Environmental Laboratories A Division of Water Technology and Control, Ino. 642 Tarneo Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab(&_belisouth.net Web Site: www.meritech4abs_com Tura Around Time" Std (10 days) 3 - 5 Day 24 -48 Hr Sample LocationIlD # Sampling Dates & Times person Tatting Sample (Signature): Lab Use Only START END comp? Grab? it of coats. Tests Required - r� On Ice? �p pH OK? C12 OK? Date Time Date Time Stormwater �jr Z fr 5 % 1 TSS !� Site f# s�7 1 COD (wIH2SO4) Ce Oil & Grease (wIHCI) �— pH (Y Method of Shipment., Comments: UPS O Fed Ex ❑Relinquished Hand Delivery Other Will these results be used for regulatory purposes? YesNo *RUSH work must be approved prior to sulsmitting samples. by: Date: Time: a Recelved / [/'�/ / Dater Time: Relinquished b /� �4 ` J`5 +me 0 eceivtd by: Date: Time: Relinquished by: Date: Time: Received at lab by: Date: rime: - 1 }�, SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 7/14/2014 CERTIFICATE OF COVERAGE NO. NCG060098_ FACILITY NAME—Vertellus Specialty Materials COUNTY Guilford PERSON COLLECTING SAMPLES _Todd Yarborough _ LABORATORY _ Lab Cert. # Part A. Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2014 e FACILITY -ACTIVITIES INCLUDE (check all that apply): RECEI VED \IVED ❑ use/process meats ❑ use animal fats/byproducts DISCHARGING TO SALTWATERS? ❑YES ®NO JUL 17 2014 CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 DWO/BOG Total event roinfall 2 or ® No discharge this period' Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark - 100 or 50 Within 6.0 — 9.0 120 30 1000 Soo 1 N/A N/A N/A N/A N/A N/A N/A 2 N/A N/A N/A N/A N/A N/A N/A 3 N/A N/A N/A N/A N/A N/A N/A 4 N/A N/A N/A N/A N/A N/A N/A 5 N/A N/A N/A N/A N/A N/A N/A 6 N/A N/A N/A N/A N/A N/A N/A 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at anyoutfalls.,You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50 6.0 — 9.0 - N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes. complete Part B) SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS. • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT DAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitorinel Period in the case, of "No Discharge" reports to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inqui ry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my Knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, incl_ ding the possibility of fines and imprisonment for knowing violations," (Signature of Permittee) -71W;&�?lq (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 Lr`7 V Vertellus- July 14, 2014 Central Files Division of Water Quality, DENR 1617 Mail Service Center Raleigh, NC 27699-1617 Attention - Central Files: Enclosed you will find one original and one copy of our Year 2 — Period 1 (2014) Stormwater Discharge Outfall (SDO) Monitoring Report. This report is for Vertellus Performance Materials Inc. permit No.NCG060098 effective date December 4, 2012. Please contact me at 336-834- 4915 with any questions. Sincerely, Todd Yarborough Engineering Manager cc: Vertellus Specialties Inc. Vertellus Specialty Materials 2110 High Point Road Greensboro, NC 27403 4Wc-on hli'twi Phone.336.292.1781 Fax.336.854.4058 www.vertellus.com ■■ Gooc ch�m��iryoi wwk STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG060000 G SAMPLES COLLECTED DURING CALENDAR YEAR: c�d9 CERTIFICATE OF CQV"ERAGE NO. NCG06 no 9 b __ _ _ (This monitoring report is due at the Division no later than 30 days from _ the date the facility receives the sa piing results from the laboratory.) FACILITY NAME -\LE 1-l—Uls?C—FIBA��Zlj\f� Zl�t 4S COUNTY t L.Fpf212 PERSON COLLECTING SAMPLES t"AE PHONE NO. (e-�36) ai CERTIFIED LABORATORY ME:(Li 'T # , --:TZ c— Lab # I -S Lab # PLEASE SIGN ON THE REVERSE -i Part A: Specific Monitoring Requirements OuffalC No. Date Sample Collected, molddb:r 00530 Q0400:. 40:I,:..::;, - .00556 31616 Total Suspended Solids, m IL pFI,. Standard units Chei�oiea� Oarygen'` Demand, ' Oil and Grease; . mglL XFeColifor , s per 0 mI Bencliimark=: . >.. - 100 Within'6:0;_ :9:0 :' r:.120. ;: 30 0 I _ 6 _ (W Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement T er 1 or Tier 2 responses. See General Permit text. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes )ao (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements ..OhtfaIl.. „ No `Date - ected, mb/dtI/ 00556. _ .«:a053.0 ....v `... ' . u 00400 . Oil and Grease, :: TotaLSitspendedsSol�ds, _ ;. , ..Skandard iinits New.Mator.0il Usage, Annual ave a aymo Benehmark - 30, :; # ;` ` , ``` :6:0'"� 9:0 - Note: u report a sampled value in excess of the benclunark value, or outsid6the bench range for pH, you must implement Tier i or Tier 2 responses. See General Permit text.=' ' Lp STORIM EVENT CHARACTERISTICS: ry� Mail Original and one copy to: a �� N Division of Water Quality Date (firsk event sampled} / ''� Wit: Attn: DWQ Central Files Total Event Precipitation (inches): �,l��L� -= 1617 Mail Service Center �7 Raleigh, North Carolina 27699-1617 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): S WU-249- I 02107 Pape 1 of2 t "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of lines and imprisonment for knowing violations." j—. (Date) SN U-249-102107 rage 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG060000 CERTIFICATE OF COVERAGE NO. NCG06 ooG� FACILITY NAME A -_R 1AL5 PERSON COLLECTING SAMPLES t "L- bow0tj CERTIFIED LABORATORY JMtr 1' %-rEC+1 . _W t= Lab # ILS Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: [9 X (This monitoring report is due at the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY lt,bt2Y) PHONE NO. M61 PLEASE SIGN ON THE REVERSE � Out fall No. Date Sample Collected, and/dd/ yr 00530 00�00`.. .. ; ,'00340 ,., .: .00556 .31616 Total Suspended Solids, mg/L. .: pH; Standard:unrts' Cfiemieal'Oxygeq = : Demand, COil:nd Grease; L mg/L�' ecal'Califor , Colo ` s per 0 ml Benchmark - 100 With iii':6.0_ : 9 0,- " . ::` 120`- r ; _ .. '30: 0 6 Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.b T See General Permit text. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? w yes _io (if yes, complete Part B) Part i3t.Lr_hicle Maintenance Activitv Monitorinty Requirements Oi;tfall0040 No.:: Sample Collecte , mtr/ad/ r. , ease, f' m /L'....Star►dard'tinits Total Sspeudedt ,: New Motor:Qil Usage, Aaittial ay.'e'ra a aVmo =Beniasii'irk Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses. See General Permit text. STORM EVENT CHARACTERISTICS-6 -.Xf ?rst e11 vent sampled) Total Event Precipitation (inches): n Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Mail Original and one copy to: Division of Water Quality Attn: DWQ Central files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 SWU-249-102107 Page I of 2 t "T certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signatu�e of Permittee 7 17 (Date) Svav-249-102107 Page 2 of 2 q $ Vertellus Specialties Inc. Incident Investigation Draft Report Plant Greensboro, NC Location Greensboro, NC Incident Date: September 15, 2008 IRIS # 10356 Investigation Period: 9/15/08 — 9/16/08 Investigation Team: Michelle Kareis, Leader EHS Manager Bryan Sepessy Operations Manager Amy Young (duality Team Leader Investigation Report Issue Date 1017108 Purpose The investigation of the effluent release was conducted to meet the requirements of the Vertellus Incident Investigation policy and to gather lessons learned to prevent recurrence. The processes involved in the incident are not regulated under the OSHA PSM or EPA RMP standard. Incident Description At approximately 1800 9/15/08, an individual near the intersection of Watts and Husband Street near the Greensboro facility noti fled the Greensboro Fire Department through Guilford Metro 911 of an odor in the storm drain across the street from his house_ Through a process of elimination, Gl~D and Greensboro Stormwater Management staff identified the material as coming from the Vertellus location. The release was identified as effluent from the plant effluent system. A contractor was called in to remove the material from the downstream storm drain and flush the storm drain system. The material was then returned to the effluent system on site. Background As a byproduct of the chemical manufacturing process, the Greensboro facility generates effluent/wastewater. Eflluent is managed on site through a series of tanks, wastewater stripper towers, pH monitoring, and finally discharged to the City of Greensboro POTW (Publicly Owned Treatment Works) TZ Osborne Wastewater Treatment Plant under a City of Greensboro Significant Industrial User Permit. The facility also has an NPDES permit for stormwater runoff. Water from process operations is collected through concrete floor drains located around the facility and pumped to the effluent tank system. Additionally, in the concrete in front of Gate #2 on the inside of the plant is a sump designed to collect any runoff and/or incidental releases and return this material to the facility's effluent system. Brief Process Description: Effluent Towers and Sump Plant effluent (reactor cleanouts, floor cleaning, splits, water washes, etc.) is discharged through floor sumps to wastewater tanks, and eventually to Tanks 351, 352, 353 and 354. T351 and T354 are holding tanks; T354 is an equalization tank for 351. In general, water flows from 351 to the stripping towers. Although it is possible to route 354 contents to the stripping towers, this is done on a very infrequent basis. From the stripping towers, water is pumped to 352 and 353. T352 and 353 are discharge tanks to City of Greensboro POTW_ Prior to discharge, the QC shift chemist verifies pH of effluent in tank to be discharged, records this in Effluent Log Book, verifies volume that has been/is to be discharged, and discharges to City POTW as appropriate. There is concrete containment around the tank farm and the stripper towers. Tank farm containment is adequate to contain at least 100% of volume of largest tank. Volume in containment immediately surrounding stripping towers is lower, though this area is gravity fed to sewer sump adjacent to laboratory building. The combined volume of the stripper tower containment and the sewer sump containment is adequate to contain at least 100% of the volume -2- of the stripper towers. The sewer sump contains a pump with a float valve that transfers material from the sump back into the wastewater effluent tanks upstream of 351, 354 and the stripper towers. There is an audible high level alarm for this sump in the QC laboratory hallway. Sequence of Events Note: All times are approximate 1730: Operator notifies PTL on duty that wastewater stripping towers were foaming over, Foam from the towers contained in the containment area for the towers and gravity fed to the sewer sump. The PTL went to the area to investigate, noted no foam or water outside the stripper containment, and turned off the pump to Tank 351. 1800: QC analyst on duty notified the PTL that the stripping towers were foaming again and that the foam was outside the containment walls. PTL investigated, identified small amount of foam immediately outside of containment wall but within property, and noted that the pump to Tank 354 was on and pumping. The pump was turned off and flow stopped to the towers. 1800: Odoi complaint called into Guilford Metro 91 1/Greensboro Fire Department (GFD) 1815: GFD arrives on site and asks the PTL on duty if anything unusual was occurring or if there had been any releases from the facility. PTL checks sump area in front of gate #2 and does not note any spill, release, or other material in the area. Reports to Fire Department that nothing unusual is occurring on site. Between 1815 and 2030: GFD personnel collect a sample of the stormwater in the storm drain in and sampled for pH using litmus paper. Reported pH 11 — 12. 2030: Greensboro Fire Department Hazardous Materials Unit and Greensboro Stormwater Management Division (GSM) arrive; on site and report to the Lead Operator on duty that release source is Vertellus. Release location was identified as the stormwater discharge pipe at the northeast corner of gate #2. 2115: Vertellus, GFD and GSM staff sample stormwater at stormwater drainage point immediately outside Gate #2 and the stormwater drainage ditch. Samples were collected in glass jars and returned the sample to the Vertellus laboratory to be run on a pH meter calibrated daily. Further downstream drainage location on Immanuel evaluated for odor to determine potential presence of effluent. None detected. GSM staff contact Guilford County Environmental Health (GCEH) for guidance on cleanup method/location. GSM/GFD/GCEH identify location for cleanup effort to be stormwater drain at Watts and Husbands. Determined best practice would be use of vacuum truck to remove material from existing drain, then flush fresh water from Vertellus through storm line to Watts/Husbands location and remove this water as well. 2330: Shamrock Environmental Services not] Pied. -3- 0100 (9/1 b/08): Cleanup of the drainage ditch begins. Material from ditch is removed via vacuum truck and approximately 1000 gallons fresh water flushed through stormwater system from Vertellus. PH sample collected approximately 10 minutes before pumping ended indicated pH of 7.51. 0230: Shamrock and Vertellus personnel departed the Watts and Husband location 0300: Shamrock unloads effluent/water from vacuum truck to Vertellus effluent system (approx. 2200 gallons) Additional Information • It appears that the float valve to actuate the pump in the sewer sump did not work properly. This would have allowed the sump to overflow and effluent to reach the city stormwater ditch. • It appears that the Sewer Sump Flooding alarm sounded in the QC laboratory, however notification was not made or not received by the PTL of the condition. Standard practice is for QC shift chemist to silence alarm and notify maintenance or PTL of alarm. • The normal maintenance shift is from 7 am — 3 pm. An additional maintenance person is on shift from 7 pm — 3 am. Maintenance staff is available for callout during off hours when there is no coverage. Causal Factors, Root Causes & Recommendations NOTE: This investigative report only investigates potential equipment failures or human errors which may have caused or contributed to the incident, allowed the incident to occur, or make incident consequences worse. The investigators have not attempted to identify or include any other potential causes such as equipment design, manufacturing and/or warning defects. Root cause information taken from ABS Root Cause Map Version 10. W Causal Factor Root Cause Recommendation Resolution Float valve for sewer sump Problem Reporting Repair float valve and Float valve repaired pump did not work properly LTA lower float. and longer arm attached 9/24/08 Sewer sump high level alarm Event based Lower alarm set point Transmitter ordered sounds without giving adequate maintenance — event on high level alarm in and will be installed time to correct problem prior to specification LTA sewer sump. when received. sump overflow QC Analyst silenced alarm, did Problem reporting Re-train all Scheduled for not verify sump level or notify LTA laboratory/rear office discussion in site PTL/Maintenance personnel on safety meetings 10/15 importance of and 16/08. investigating and reporting sewer sump hooding alarm immediately to PTL on shift and/or maintenance supervisor. -5- a ro Photo 2: Removing effluent from stormwater ditch: Watts @ Husbands -7- -8- SEMI-ANNUAL CC?MP:UXN- E RF±paRT'FOf2OCPSE;�SeI(-Moiiitaringj ' •._ I aiJ;RroCess B�l1od � Facikky . 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' sruJ'' "1ndEr pAnall y of law Thal-Ihks'documen(3 al(aliad:mints 1Fief0 pfupa[9d inEer.;my Onction.rhrsuporv%ian iri with a syelsiil disigrlod Id assure 041 5+if5`•nTl�l'FfGpyrl�'gath9r.and 9vitlu�tB'I iB llrf�rrn�7icirl su�mi!^ed l�a59d on'my.lnqu[ry otlfle gaf90ri dr p4iso1$.Yrh4..rnan3go-the. Sysl9R1„Of111C59 g6iSOSis.dSSRGif}i,};}5p0l1SiGla �asEisnkr rJhe inF iiaGoai:'ihe In ormalion:suom'�ttiEa':i.9e•the seer of-mv knawlndea and halrAf :tn a 'arruraEn and comoiala, i�am 2%6' 13'Mat (herd are sidnit;clrt( A©n311ie3 qualified f9i - tc[ iObfili(11M". j 6id�,nfRrnla[icn; kntiudinG'1Ra ao^slbiflfy of tlna-one lmpnsmnmanPfaviuluwkn vidlations. .... - ' , r, Meritecc,Jfnq.. 4'Env onmen a.�L-aboratory RX! Hio Ri 'Rd: C -ate .Sam6.le gcvd; I:c; 52-"Nl F.: P :Trip-"BiaA A 08" �',.Sampk 'MehAs 0,"affi-, '2 Niiai&irs &-suitNldhad' /L .,EP �25 '13NA dfZ 81bg 12 'NIZO-8, Q 005 n�/,L P14 ko P iijpepres lifO'Ozme� E}42.TaEnco [load, A -2,7,32U — tel.'-(j36342r47.48"f,'ix(336)3421522. ME��' INCR Eh-v;i'fO.tiffiO.ntal,L.abo.ritor'ies_ 1 7 ovZ WOMS'i6n otWater Technology and;Cd.dt..fqls: 1p(, r Oiciat: Vert7ellas nif6rm,ancc.-Ma-terads Mifitidi 1W 0227,!M% 624, _c6clit'-samplelib. Compos te:352-MR:-;35214W t:. V.WVY, samp! let O'licei'lon. ..6ksi6t .20 1C ZM PA.624'VOLATIOAGAN-S Parameter :Result. 20;0,ug/L io —0 t ugh,., , ua L Carbon Tetraofilor'ide 0 -.' L Chlorobenzene Cki.o.rodhare: • Wo .4jiL izaoo ugfL c h I et* Chloride 01orodibroinomaane WL., u ,1,'4,-1)ich1orbbcnzcne. K2j V..Wje: ,.,,2-:-1)i6h1orbbcnzcne 2 0; PF , i , i gtu 't,3,-Eii6!oro'benze-n , e I tjjibh1Q.Fo-qihyfc-nc- 2 :0,6ilL 20.0;4.L -6 1ug%L 2 6; 6 9A, .Miihjtcne 6fil6ifjo 20.0,ujiL em uW1 TO Aj -Tdchlorocthane < -<-!Xo. uitL: 0,61 4L ata. ' U T4or 2 cf "',"Reldsvi:1116', N' 1336 )L q42-4148: --,.!-2732 . P..h. *",(Sq6)442-;1 522 Fa)( Cli6t:' Project. -7-Clieni - sample:4W Shmpleico'lledion. Param etef Accnaphibenc Acenaphihylcne: ajanthracene W'enzo. , (a)'pyrene )Bini6(k)puoranthenq. Benzo(gh.f}per;lencm butY f.'i�6yl 0!6ate . Bii(2•chlorodh�.I)Ciffier' V 2-eth y .-XY.. 1)0 _Aqfajaidl -4-.Broinrio. Oh6nyl;phanl.ether ;4=Ch2graphenylpttenyl ether 'ChrysObi& ,. 1, +race=! FiibenzO4-,'h)an lChl -'A .sj qiEhIOT - 0 - enzene ble ;I A hloro'benzene, Malatc Dime i[phihalgite. 2,4�6100*luene lll���l-��`CfI ll Environnionfal "t abdtjibfidr� .. - .. - -- — i .- .. - A_MVi_sidn'df Wk& T66hnology andtonls:,Jnc; 625, , Analysis: :Composite TAr aceion: Analyst: Dilution Vaefoc: ILY _ FtAb. . 2_S,_.SEMIVOL"-_&T 'OkC A .CS :Parameter -5kd6b;fleb I F1 q`-q �h— p!Ikenq < ffg/L, Fl uprene. <5pppq.� Hexa6filorobenzene; < �250000 !UglL. f!exaAlOr. . -Mcne! . IL -4'50000 -6sUL 'Hex Woroefhani -0.0000 U&t UgIL, **t <30066: 4L ??R!M -N-.Nitfb7i6diffidth M 16Aine: - ',?"500Wuk7L - ----------- N-Nitmsodi7n=propyl . amine 45a66 P- r, 5060 4t- < '$WQ 4L. 0.4pro!p-cresol z�56600,ug/L 2, 'ia-Dich ;QSOOoo, uO" 2.' . I '4-binifrophenol _<50000. ugA,: 00 /,L-. :1-,Njfthen6l' !-e3000%, uglL *44 Iftophenoll �'56660' u �RdnlaN' .. rbpliK6p�l < 5000NUWL -Tfi c h I o r u 1) he n o I '5 50000:.-Ug/L f and.approve fhgse-:dqia.-. 0 ro M _MC 5040 Bid IOGQO,Acid -5:3-666d - -Uglh; -_k, " QQQ ;550' wl� --<S&dd 4L 4L !Ki4,000! qg(4 .<750009:,.us/C,, <50066!.Ug/L < -500-66--.5 - < 500 OJ iYL<;SQ0Q4 per: - <1 06666 UA/L_ 00006 UjIL -<306000'' 4L <00000, OS(L l'JaboraCofy Representative 642 Tamdb Road,* Reid.§,vWbl;,'K._27A2Q, 'f336) 342470'Ph' '.(3tMM2-l6&Fax. .. I - � - C harn = . , of Custody. Rec©rd .,_ Phone'.'�� T ■ 1� olc Environmental FLabvaitorYs - Dlvi3i,3pof Water Tr EteSA „ E7d:: j ccv. ect_ - ' 642 Tamco Rd Pfi�one i 335 3424T48'' _ - - _ _ _ _ urn A odn[ Tarnelax Reidsvii•-1e, NC. ,s_ 34Z 522_ 27320`=-: ii imail: wtclab(abelisoutlt:nt' Web Site:. comb i4entiOrt ► 5,td d s) ib - 3-S:Clay 24 48,Hr wvs+w:meritech-iabs r. Gt�} . ' ] Samp.l'e w Sarn..iin Dates.8� Ttm�s,mp - ie i Pers nflaicn ;Sam" pSf nature e"Iah a- - lmy _ START — r Camp? I'Grab7 # of i = Corns..; - y • �� F T,�sts equired zti. _ on tce3: pH OK7 E12aaK� Lcicati,anl.ID # . Time;. -'_Tithe; i r - - Aw 0, cif z I : 1. 11 V „ 1 7' f _ +�*'aechlaririation:.( 0, 5_ppt r} of:Ammonia, Cyarnid�. Pher of or TKN sarrtlal s rnusi b dar e;3n,,tf a fEeld prior to preservatiOrO.* ' Method:af Sh`ipnteRt: .. _ ........ Corrfinents: - Q Felt E)e,... Wtii`these;resul#s'be used for r04atary�Nrpasesl - Yes hia ''-*RUSH rv&k mast he,apprOyp prror, t07-s§46mittin ,, Samples. • y' and f]elivery, Rc rshed b -- - Llaie: �.� •.ti - E i- � %;..:�.�{:�_�_tl, �'�� �r �� _�i: :.a t ,�G tom. . _ RPIi q �s by ! r Dace; — Tune ff i fix. ��..`. �'�. , Rae h '' patfe Time- 7 Otflei• it qu T ed' Date _ c is ime;', _ h n. M fe -":h Inc: en c Environments -fabMA-'- ....Pry alioratorp C fi :(f] ien t Vdi4h-us-p p4tesam q.- a. pi. Fcv rder 0. O�fgl Taramet&.s- &Mho V 024 TIAFpTPllftk . .......... . ..... M ep r Sample;.-')vlpWs.Ctab-- , ;ie6-,wo,k:ord&* J�2 Parameters; Ae5U-1f, -Arai y �itia 4qacu. fotal '<9 %,610 MiAIW Minc, fO&II 0 653 Tzig VM - 3/5/00 EPA 615'&U 'Mei►te i t4i WoW.Order M 6127*081 MitK6d: ��4 I - 0.005 .... ....... TA, (Y4, PIPPIlqp2,1 -1496,4"" A ,!I oiv-9,04 itNqaw '042T -- qRqad,R6�69 . Jllc,-Norfhc-a Rw 03 -tel(3.�6) 342-048 64z 6) 3427!522! -T--" -N-Cff-` Enyironmenl4li Laboratories 7: - A-s. Division, of Wat6r Tethqo]bgy'grfq Controls, Inc. � 1 dfj�ff Clid6t; �j�qjja`p&f6� d, I76 %�fdf 022708103 Vs - Iii6fit Sample ID'., C_d.ih, p qs--433 '--lb 'VWV -00 :Sample Calleetion.- M/2 & 8: :10 Nrameter ;Result !,'&nzene 2� if)OA ro Z b -2 ugi ;Z 100 -497L Qro.benze.ne tWo'loeffianp. < 1,00 ul%L e t� e r� �ugfL foo 'Chlorodibromornethane !42"t-016 bromodhanc' 0 -Uw� Ajordet"hano <; 0`0.00, c oroct afe J11,4orb 1c�i` e=ne 20 Q 'uglL T17,- 20.9 Cg[L- 'f',3rDicfilbr6benzcne: c-�20.,O mgll. p✓ I tr"ans=it-,!---Ijlchlo"ro6ihyfen'ff :�c-N-0 UOT : 'r 2 I ro p r op a ri,,� vi, ne. 0.0. tiob Yliiz AMMO.' Ethj 1,;bdini zc-nio' ;� 20.0 4t. McihyIene-,chIbiid6 ugfL . - 1,,Lii-2.,'2T-Tefrachforbe-i-hanc' UeL, gf -<,20i0 uOL T. 1 hurcbyccrt41llai I have reviewedand approye'tlicsc,&ta.- 1.�a1ior3t0i}1 Representative .64 2 T4rh"cd'R6aidL,--- 'ReitsViEle,NC 27320- ,47 4 h, '(336)�342A51 Fax E M Tc INC li l i E 'n it.eib- (W"bi§, f A Divi�i6ii-6f-WziterTL-chnology-and cqnfr6is, inc Vert fl" e us. efibrm-ande,WtCHRIS-, .-Mer: fech"Wo. 022t .... Tr ject.' '623' -Ana! 4�/68 :Client sa,mpi liji g66pi (6 Extracfion:: 03103/08 Sum'lc.:(6)Lecq#; . q2/2WQS tc N tlut0nrF;ktof:',50Q0AN' z.,.- 'E'M 612 "SEMNOL fILUORGANICS. Parametee RSulf Param6ier. ,Rcstilt� fluorenc WL ,Anthmcene.. !<MQPIWL kiexachlorobenz'cne� - - _'4U , . 50000.,u He xachlor6butadl&i6: < .'.36fiij(4-)a,nth,ra' ceim <,Sdobdug/L li �kalbfddydi6&6fedl mp < A - nr Hixa6hloroethanC 4 iBinzotlutirngntheric OQOOO ugiL, %lnden6(1,2,3-cd)Oy�e Z-'.50000 ug(L. .A�W(Wuoraai hent :06666 ug!L. 6666 4L `genzo(8,6 i)pcfylciie <5009q.iiWG-7 AR i�y!napliifialcne: 000 Otte 4sutyNCf'2yl ONIfilif 450060 ug/.L, :Naphthalene z{ Wii(2-chloroeihoxy Bls(24chlorocihy6ed6*i' <50000AV amIRID *Nitrosodiincihyl " -<, r-o,*P YlWitfc- Big(N-c - tfiyIh'oxyI)phihalkc: NNitrosod "' h" qlL 4:-,!Broniop'heriy-l'pfienyl':ethet 0 0 0 0 qg/4 Fl ddiih6rene, �5 0 0 0 0 �qklL Pyrencz :;c 50OW4WE, . '6 �� '-- .4 qlqpjl(�fi� -�5666�1, ug�L - 'TF no . Qo:ug/L qfy-� ins -� 0 6670 � 4L ,'Dibcnz6(�-'fi)adhraccne, 56_66b.:Uw1:_ n=clildru=iii=crs l <2006") I )bCTjZt7rj6 < 50000 ,4L- 2=ChloroAcndl, - iZ2000o, 1 3-Di Ohl'---b--- I- '- 50QOO!ugIL 2,4-Nchibrophch6l. t720000 ugn. 1,'4Didhlordbcnzcnc. <20666 U 1. d orobqmeine' -<250000:U�-24:Htro6henol . qOOQQ 6AWL3,j,6 Diethyl pjt4ilite Alg/L - I I00066 ogle ;Dimetfiyj-phtbalate -<50.000 pgtL, 2-NjtC6pieribI. ogle bk;ib tqy"i ihalm��r 4NitrQptiencf =_ 4V 2j4- fliq*W66 ;i�;5066 U'WL , kpcntq6Wl I 1000,00! ugll, : ,6__D4niir.ot6l6cnc 1 ;.2000 lug/L Di.n- t6itte �otykph <"506 . 00. 2,*,6-Tiizjilorop'henbl me.. A ug hereby: cerii£ytliaC l.tlavc.reviewed and -approve these davi; taffi'dd.R6Adk RLWtvillip, NO-27-120 ..(336.).3.42--4748 51 .Fox t: t. Mpl V taboratot7SeO(MtMi . � _ m t .--. :Chain ;of -C-U-!§ ody" RecordjC00)�- NPDES;,#, EC ;tUvjLr.&iiAi6iitaI Sabo'raipifes,.' G' Fax: 9b lhr WvDfioi"dr.'Mit IcchnaI6 n g —77- i1. 642:Thmco. ..Rd Phone- 8 - ke'idsvJIIe;,'NC F.4x: 1':�SU-.342-1522 rh,'. roWid jrne —T u A_ 27320' M�61ab'ft 'VV6b .:Std flSdo-or .48 Rr :Site: : twww,,mentech-:IAbt'.'6d-di .SaMple, i d Times turey', 0 1'. tah.;Use n . Y "START Date Time_ ENO Time Dat!r� Grab? __r T&��fi�' qUired T� _.On n IC.0 i C12 OKI— t I v� r fib. -vo A-1 ' aamb ew_ - -*"DechlorIrnation'(<-'0",5*7 .O.pT) dfAffinoniaiCyanide PhOrioll or'-TKN!;'-z4q0Ids� Y*iustbeldond-irtth6-.-rfieid='P'tibe.td� pres'ervp3fionF"'' Meffibd bUShipment, i F _.0 S_ I P.. I Med tx. Will tfilas4 results N-.,Lfs_edI'(qT regulatory -purposes No RUS 1w.qrk,tnqS.'t-4g #j5p PrioIrIo--subr'm'iffinq' Y� R.- ,F: "10) Ftell _414-nq Ivery. j Ren ,Date. Tlmie-! S m Re jig, ZR 'pate" Tim ' e " entik , _Laboratory :Convict: .211 i 0,'r1 Pate�sam le�Rcva'-: V 29/08 -A Result- nalXsis.Daf R eff? t ih g� Li r3i i Nleihad . ., .,-, - 7rip'Mpk; S pie. P�fils Or& am 7'arAhieL I 'Methatl 0.010 mg/m, 'Grab -ResultL Jda t�.465xpKIL- 335. ZPA,, -4 -Nicrel6y°cerii - - '!�— �Lejdqtq, 6 ed d4d PPF qlk L4�2'Ti�icq Road: [ -E Tu �W 1MCM Environmi-e-hial Ldb6f4tpr .1'es Rhnolcgy and Gontroisiiqp� '.YbAdiius Vcrf&rnanaWi�teriaas Nier,iie , 0229U67' Project: `624 03/1 0/,G8 0mv 11c'm �A'm-Analyst:;� ID: C66io&ite 3S1.-AS -3-S�-'K -Analyi 'Samole t6fi&ifofi-62i27JQ$ Olution -Factor: :j '-E,PA'624 VOIATH11'ORGANICS j1d ' 7ffit� ' fie ug/L. bromom lfhane 'D-i&hl6ro e �<:20.0 , 4L, Bromciform-7 �ua lvfeihyl'B'romjde,-. "160, ug uW IQ 0. 9/L. CM6 ro-i 0 i yj vinyl ether. ther. A: 106 UjL -CHI-6rof6rm. ;�120. , 0 .4L Methy, ' I ChJOA�.jp' 7.. �;100, U95 Chlbro'di-b- 5U; ,I i?-1Dkhioroethafte-, T,41'06hlordbenze6e ,2rbi6hl6r6benzen : e. Z7 enzenc, or ethylene A 6h1bropropane `�20.0 ug/L :Cis=,439.Mlilbroprqp --�BOA` UR/L u TOri6hloroclb lene; Tpluene 20",'0 ;ug/L 20f6 Tric'hl6ff&0Wa& �T- clil&ffi o6rorn ethane: < P. 'Vin_:I ph lori de; Y I yi)L. �1',her64y certifyAhat,]. hdv&.;f.eV.i-6*0%n�d-. approvwthes6. data,;; "I TAiii66ROd *'RO)dsOfk- NC 773 26, MERIT,F', H, INC.-.-m :Er vironment.di.'L.4b.prato.ries,- A DA16n:of Water Technblo,gy add- lhd: -- .. MAterials 'Protect: (62.5 -,.Cbeni Sample- febrnoo§ite: Samp feCollection:; .62/ 2 8 Mg 02297f Atralysi�.' 03/25/08 kjaeattiow. -03/068 -Aiialysf: 'mc: W "E'ORGANICS d EVA, 62e S-C-MM iL h h. c e --,<26060 ug(i ;Flitoranthene: ;4� O000. ug/L cen ; A aphthylene < L .1borene T u .Anthracene -<200QQ, uk&, - -1 . - Nexachforobenzene ug/L. -&nz_id'i'nc i.00coo 4icxacRfdfb&tItddIe- 'a' i W. u -dopentadicne !:<100000'.;ug/i. -ainzo(4)pyrcne,, 4 _WL -o .i;xachloi eihan'e 3,; 4-;B enzoht, p roagth q* I'k.200004L 411deno 2 3 cdj yrgria :5 Mbbo: uv OCT, )f*.�f*ho <:20006, ui/L -kopkotofid, < 20000!41�1 gQ000,u9/L 'B�ufyl 6nzylphthalatv �a ne — L �:20000 , ug/L. (2 chlQroatoicy)tilut440 -5200.Q0 u_WL Nitfobt�qdlie _L Oither < iffi thylamine --<200 O'UkIL 0 yl}iiher 00 1,Nzi4itrosodin;,pr-opy'l-am-ine: "�-70906. ug/L I tO F;c--20000. uA- !!1o4 1 fro:$ o diA"eny fE�h i a 11 ether. pj��ffy��:Obdfi�I , 200'00"u WL Lfaq tl��46 <_�660W'd 4& rke ArChlorop6n 6r, 'Y1 phenyl ether IQ: 2000,0i4jIL I.; QiChforobunzenp !:2QQ0QIUgIL i--Chloropoicn4, 70 000,rUg/L- 2,4-�Dlchlotophd0i' 206RD i� 'I'i -;Kq qyeaw -.?1oodo 4L ;A .16- ;3�3' Drchiarobenzidine. 100000 ug/.L-. 2,4-Diftitrop enal '�IQQQOO :irgJL ?Dicihyf phihilaie kiZOOPP < -100000.0 9/L bimcthyi phthalate -<'..ZOOOO ug/L. 121M tropherzdl x2000 upjL-' :-,100000 #gl 7.2,4- ;--2000 C11616hiorophartol e100600 ug/L 2,6-6inj"tbItierfd m `IoQoa uit-L I I en 6 1 6,g,/L-,- y htbhtatc -s,200 (Y: u9/L . TX6-dZh(idohenol �*2000. b L tI-,2'QiohenyIhydiaiIne ,<20000'f 4WL I kreby. Laboratory I-Ta"336�,_mca.KoAd'*Ft61d` S "Vi lik ij NC27 _42-47'. 8 Ph t.(336) 34Z!IPfax; Y. Chain of Custody Record �iBf1t" Npbus C.H.- '1 N-C. E Vifonxrx'ent; Laborataii�s A-brvisec'n"n[lVatarInchsiaSogp'a dControl,rinc.Y aAdde6§s 642 Tainc.o Rd il'hnrte 1 33fi-34Z=4748 0 Reidsuille, NC Fax:: 1 336-342-'4522 - "_ Turn-Arounif Tim& z73ZtJ Email' vvtcl'a1a( biillsouth,net: 1 At�'6 tibm-. rt! 'l( •(:9n cl24iWeb Ftq Site: wvnrv.mer'iiechAaibs:corn _ Sample _ . Samplih Qates:8r, irnes. 'j r r, s rsorr ; along 5amp3e ( igriature}'` : :s';ari use flniy' --_ 'Locatloill,l4:# r -' START i - Date 1 1116e _.• ° ;� Dale" Time. ;Grab? Conti: JJR'C�U�f�d Ice?. i C120}CT I 55- -Qtle - CIA - 17 " tD6chl'oeination 0:5•pprnp of Anrt'F ohia,,C,yanicie, Ptteno! _-. orTK sainpfes;must kie done in th�:fielil pcion'to reservation ��`" Method:of'5hiprrient:; Coimmet�ts: _ 4 r .y. f µ ,I •• �I L.J Will these tesuits-be used for regulatory pUrpo'•ses . y . - 5 ` Na - y. tR a racer, o, l! U5H vsrork must he approv d p' f .s 5mattrng samples;, Fed ix` Deiivor , Fieiin Sher! by ° - ate_. x _ `� Time;. . g �� R ceived tiy:' --• _ - - - Date: �Tlrrie: r 1 f:; acid "' I Rellnqu}}s ' 'by: -'jrV.,Date ` z zvme;.` - �. i ,.%— i1 , .lit `l. ✓ N/ i ReCe d,db}: Date! Tfine �1--Y M• '„1 �. ;�� %Cl' _ ry J .❑Othet i2eilr si rids _ Q41 - T e i p _,r•,- ReGeiVedai p, yUt • ; Environmenfal, Lefboritory: Ubdfati#y i6n,46.,165 Client: "Vertd�f� P&16"ehiiinei 'gi.ir�6ps6oro,' C 27403 DiFe Sample_gc�yo. 2%19/,09 3q3e MR 2§f Aniiiis bail Regoifinj % ljmiE Wth6d A-ttachtdg; W �Wrcrerh- -Vff�6977' Merifedi, or Illp1q: `�QWS:Gris< Para Fern -&—sulb, knalysiWbAle. L60iiig-Liffift Nkhod EPA 200.,7.. k 6i�:.BNA-i Attat cig 1�4 006b Wprk"Order. W M!4GVS fsiffip iG 08; Tarametem. fjtjs`jjjt. -An&sTs b5-(q 'Agp9gin-tim'i -Wth6d -R !6A2'7'17-3'k Wl;;4 74 '(336) 3427Va' x 3'e- 'I 5k 2 z ..(336 ME , I TE INC, • • EnvIIr6hfkFhtqI LAboratb hj& r A Dlvisfbh of Water t6c'hno�fogy, lie -]it. e us' -Vqrt 11' _#e&;ftdn-eoMafteHa)s- e e -6220873 Troject." ':624 101116169 ,Cjien I Sathp ;e UW Composite35" -3 -j! G 2 Siknple- C oiled"oh- 62/2 FV.Oa -.Jsiiutldn'FaUdi.20 '624-'V--6"fA.TI.LF---'ORGk.,Ni(7'8. .EPA Parameter 20'0 -to, BrOmOfbrrn < 2 0."0 uW', L -Meihil Bromide 6tt_Wcbl,5Hd&-: IN— < .'�20.0 '�t: 1160 ua onn _Chlbrof Ai -�qgq;- Mekhy, _ZO.'O iugIL A �7!!Dibf&noethaae uo� I,I.Ochloroetban6 I '2-Dic@oroeihqd& <,20 0. . clilorob-diiie6d ,24�zene5i6lp 6� 20 t,7DicMioethylcne --�-20.0.�L !A�§J,.%2.;DJbhIO . rOefhyf,eP0-e. < 20.16,ug/L 11;2=Dichloroproparzc1 C iransi .37 _--kr9p, .26b -U. Pylene !by] 'JivIlOctf-C 4L chloride u__ - I T 2- 2-Tetrad[brot-kh*tq UWL Nuen-e 0.- f k!20;.O �.Uj/ r!Qp- fliane, S 20`0 -6ivL V. Vinyl': chloride, T:Kt rcbyccftifyih xe mvg--an 'approve,ftCTO#,-�, ;Ub6ralory- R' p?isqqUfiv k 11 .642 Tabico 7,-iROiftViII&,- NC,273-2 Ot 36).342-748'_ 342-1522'Fax INCI ME C Environmental Lei bb f6t6tibt. A oMsjon,of.-Wafer Techn6logy and Controls,.In —C bkfit.' VdifOl'" Pc-'ffbrffafide'Nfaiterials- Miriiech IDO: '622077- -Analysis: :03/25/0§ on: '090 9 om ost e: E IIracdI jj6fmt'Sddfjj1c JD- -P Sa�riple Collection;:" 02/29/08: Analyst.- -mc- Dilution f1p actor. 2000, ,m,;r625;SE M41"VOLAT ILE 'ORGAN TO., aramcter, -Result •.Parameter' Result ;<46'bbu 060 4L: T uorene! gg1j, <<20000 UEVL: '.HekachJoro'benzene r C2000O 'Bcniidinc -51000o0' ug/L Tldkzch60htga, -oik 20 00' - Ocfkz�(i);ini�roocnc <`,W66 U94-11 W4 ;,�WOOO� 6j/L '� ' ' -4j�L jj exa .0 hloro6thane 'bd6o: U�L -6�f'hfotdii-nth-cnt; il'W--,- "' - ' --" ' ' -;�-20006 uj/L ihi4eno(I . 06uzo(k)ftovaathen'6� �16066-'ujlL �1 - SOPhYQM! -�RGQCQUOl .5 WQ 5,WL, Nqpfit6ahne-- <46660 oFA !17*1- Bii(2'--61j6r6khox0mcihang, E 0666 U'jC Nifto benftne. --c-20 00 26000, -uglL < 2QoQo:'WL- K�-Njiroso&-n=propylarnine 520GOVd)#L p ' =& 'hie; ,4L 4 er :'gromop'hienyt.phen�11eth 46obo: ug(L �fitnpht� SNOW U91LI: F'Itfilbro ap Alehq -<20000 PM66 -4'Ch114- - " -<,20000.ug/L . - .1 ' 4,--Trijhior66tL-,ene. < 20000 tjg/L.; 'Chrysenc., uwf- 4h- Z;ne' K10 Ob 0 uj/1, �2 j4,zbii�ioro�6enoll 1. , 4!!D . ichlorobenzone7. -<N6k 4L -24-*1j- lig/L.- ,2" -DihWiY6hcri61 4 u -100- �L: 660 Aom. ohtFawt.' 'k2000Y UgVL-' 4, 6-1) ib ito-io-cresol'; <Wbbdo' u L 5; -m -9/ 2-Nitro hchol. [a' phthalate". Z<--2- 66* 4L N 06:p <.10.00901 ugI.L 2.;q- (�pl6d , Thenof yl phthalate <20000 U 6;yaliopheital 6611; -bi C��ifiy� P: .1,11 oh In I- # U i hereby Cekif these dat�- G— k at f h5i'& rawpm-sdn dtiqc-. T 646idsv-- 2L Nd 27320 4 '(336) :34�2414.6. Ph 022' 'Faix - -- --- ----- N PDES W, Phone: 1V,=EII;TI^ Jd U7 f Watbr Tdctniola fil d ro Af T 6TamRd -336.;342-4 4& 42 .ca .'Ph"qpq� PA#. Pel.d, jlie, NC. Fax:; I-P_q6r342'nJ522 Tu 01-�t6u-nd Time *I 2-71 .0 I wtclabpbel JtLdUtjj.'jjdt..� -on Aftenii Ac_ _I-r -S ta . - 10 d �P;% 2 N �748'H r -Ole 1 Se,MpHpq C:4ies SP.n � -- Lab U� -_&nly: LocatJbnP 1 'V_ S7_ 5,cip 1 'est &Z2 Tj7� 'Dati, .P_e .,Time — ,. Grab? Conts. OK?uIred _T. Q7 J T J0, D6chIbrihPt_VOn'( ...O.S'pprri):of Ammo6ia, -pyahidd,-Ph 6 hbl', .or; M'sampiCsfmust be.don eln' e field, ior c preOn*iq.n...- I :PP!b-od. of 5 Dups these restiltSbe' __�;ed fbf -.tO,IY p kqposes - , -_ —_ I— — RVSH warkmvv,.,4e ppprqypd- rjpr- tostibm'itting samples; _...P j,WiII I .f,.9d E� YO 4 1 , Wo� T 7�- nd DOW6N rIVIL Dal '`Elms: vv'L Ir\ ReC ved_i:y:,Time:: Iu 'i- •Time- .2z at wtaj- f: JiT! 7." A offl, M2 MORFLEX, INC. 2110 High Point Road Greensboro, NC 27403 q"W 1-336-292-1781 MATERIAL SAFETY DATA SHEET DEFT 1. CHEMICAL PRODUCT AND COMPANY IDENTIFICATION PRODUCT DEET :CAS #{.� '7 �- 134-62-3 {NAME �y .S:�Y.�. i! �A Y.�-IR. k �J.'y �..'i5�'k( ^i �F� 4.�i, II. H� • + CH»EMICAL NAME , r ' Benzamide, KCHEMlGALtFAMlLY' alkyl amide fi N=N-diethyl-3-methyl N f .„i&'rR v s,WOLECUE WEIGFiT'� 191.3 MOLECULAR FORMULA" C12H17N0 yyEF,FECT1yED�-ATE��'A:� February 2004 :`SUPERSEDESJ• December 1999 i' '..,K y YA"ii"ry.liK1'�k:. �- '^S. .a _iSl 4. f y ±�y[�!! rw �' U'_ �w'•.T' f.n'-Fa!_'_.•'S ..+r^. ,i.%/d��..�i.� ;y5• EMERGENCY NUMBER: CHEMTREC 9-800-424-9300 2. COMPOSITION 1 INFORMATION ON INGREDIENTS COMPONENTS CAS # m % by wt .. '.EXPOSURE LIMITS N,N-Diethyl-m-toluamide (DEET) 134-62-3 approx. 100 Not established 3. HAZARDOUS IDENTIFICATION ***** EMERGENCY OVERVIEW ***** An oily liquid with a mild odor. This product does not present an immediate concern for emergency personnel. POTENTIAL HEALTH EFFECTS EYES�� May cause moderate irritation. ,SKIN , Non -irritating to intact skin; keep away •Ix tl s.. " �' from mucous membranes and abraded sN�t� =: skin. INGESTION' May be harmful if ingested in sufficient quantities. INHALATION;; High gas, vapor, or mist concentrations may be harmful if inhaled. Morflex, Inc. DEET EFFECTIVE DATE: February 2004 PAGE 2OF6 CHRONIC (CARCINOGEN)" �,f Mice and rabbits exposed dermally to 0.02 mL of 10, 50 and 100% concentrations of DEFT twice a week for 160 weeks had no significant differences in the number of tumors compared to controls. JERATOGENICITY1. No significant reproductive or developmental effects were observed in = the fetuses of female and male rats or rabbits given DEET. In female rats given 125 - 750 mg/kg/day orally on gestational days 6-15, no r''• external, visceral, or skeletal malformations were observed in fetuses; however, reduced fetal weight gain was noted at 750 mg/kg. In a chronic two generation reproduction study, the F2 offspring of CD rats given 500 - 5000 ppm showed a slight increase in explQratory locomotor activity at the high dose level. ' MUTAGEN'ICITY e DEET was not mutagenic in Satmoneiia typhimurium strains TA100, TA1535, TA97 or TA98 with or without metabolic activation when tested in a preincubation assay. Exposure to Tradescantia paludose pollen mother cells in early prophase I to 1-3 spray of a commercial insect repellent containing DEET did not induce micronuclei in later 1 .,. . , _. stages of pollen maturation. 4, 4. FIRST AID MEASURES 'EYES '' Immediately flush the eyes with plenty of water for at least 15 minutes. Call a physician. SKIN s--:: Wash thoroughly after skin contact. INGESTION ' y Drink 1 or 2 glasses of water and induce vomiting by touching back of throat with finger. Do not induce vomiting or give anything by mouth to an unconscious person. Get medical attention. =IINWALATION' Remove from exposure. If not breathing, give artificial respiration and call a physician. Seek medical advice if symptoms persist 5. FIREFIGHTING MEASURES :FLAMMABLE PR©PI=RTIES `` FLASHPOINT 311°F (155°C) METHOD: COC FLAMMABLE LIMITS , LEL Not available =fJEL Not available A . AUTOIGNITION. Not available. COMBUSTION PRODUCTS,,,,' Combustion will produce carbon monoxide, carbon dioxide and oxides of nitrogen. '. EXTINGUISHING°MEDIA,,' :; `' „`:" Foam, dry chemical, carbon dioxide, water spray FIREFIGFiT,ING INSTRUCTIONS,r Wear self-contained breathing apparatus and protective clothing. : ' !Normal firefighting procedures may be used. Morflex, Inc. DEET EFFECTIVE DATE: February 2004 PAGE 3OF6 6. ACCIDENTAL RELEASE MEASURES Contain spilled liquid with sand or vermiculite and place in chemical waste container. Prevent runoff from entering drains, sewers, and streams. 7. HANDLING AND STORAGE .HANDLING Avoid contact with eyes, skin, and clothing. Use with adequate ventilation. Wash thoroughly after handling. STORAGE;• `; This product should be stored at ambient temperature in a dry, well -ventilated location. Keep container closed when not in use. 8. EXPOSURE CONTROLS 1 PERSONAL PROTECTION ENGINEERINGCUN711 ROLS ,i' Use with adequate ventilation. The use of local mechanical ventilation is recommended whenever this product is used in a confined space or heated above ambient temperature. PERSQNAUhP OTECTIVE EQUIPMENT PPPE' .;EYES 1 FACE' :•. Goggles or glasses with side shields. ,SKIN • .*` Clothing should be sufficient to minimize physical contact. Impermeable gloves recommended (i.e., neoprene). RESPIRATORY.,; The use of a NIOSH-approved organic vapor respirator is recommended =•"` whenever this product is used in a confined space or heated above ambient temperature. Air -purifying respirators must not be used in oxygen -deficient atmospheres. 9. PHYSICAL AND CHEMICAL PROPERTIES -APPEARANCE Clear, oily liquid ODOR.' F °� ,r ` Mild, characteristic , "pH Not available -PHYSICAL STATE' .," Liquid NAPOR;PRESSURE °°: 0,0017 mm Hg @ 250C . ' VAPOR DENSITY : r';; 6.7 801LING`POINT_ 291.7°C at 760 mm Hg FREEZING/MELTING ::-•" -43°C (-45°F) F :POINT (Pour point) SOLUBILITY (WATER) .; 9.04 mglmL ;SPECIFIC GRAVITwYTx;:` 0.996 @ 25125°C EVAP.,ORA7ION'RATE 1 (Butyl Acetate = 1 } ;OTHER nla Morflex, Inc. DEET EFFECTIVE DATE: February 2004 PAGE 4 OF 6 10. STABILITY AND REACTIVITY STABILITY _ ;, Stable INCOMP,4TEB1L'-'ITY' °' r Incompatible with oxidizing materials. , HAZARDOUS'DECOMPOSITION . Combustion will produce carbon monoxide, carbon dioxide and PRODUCTS oxides of nitrogen. POLYMERIZATION'.', '..i•i,' ',_ ,:`=s= Will not occur. 11. TOXICOLOGICAL INFORMATION ,'Acute toxicity Irritation Non -irritating to intact skin; keep away from mucous membranes and abraded skin. • May cause moderate irritation to eyes. Oral Oral LD50 (mouse) = 1170 mg/kg • Oral LD50 (rat) = 667 - 891 mg/kg • Oral LD50 (rat) = 1950 mg/kg + Oral LD50 (rabbit) = 1584 mg/kg * Oral LD50 (rat) = 1892 mg/kg Dermal , Dermal LD50 (mouse) = 3170 mg/kg * Dermal LD50 (rat) = 5000 mg/kg • Dermal LDSo (rabbit) = 3180 mg/kg Inhalation . Inhalation LC50 (rat) = 760 ppm 1r •, '• n .,k. r Ww '. i } _1 ,„. 5 •1 y ��..r �, �^:e S P-:..� ,,;�t•T �Wtipleydose effects'r • Mice and rabbits exposed dermally to 0.02 mL of 10, 50 and 100% concentrations of DEFT twice a week for 160 weeks had no significant differences in the number of tumors compared to controls. • DEET was not mutagenic in Salmonella typhimurium strains TA100, TA1535, TA97 or TA98 with or without metabolic activation when tested in a preincubation assay. Exposure to Tradescantia paludosa pollen'mother cells in early prophase I to 1-3 spray of a commercial insect repellent containing DEET did not induce micronuclei in later stages of pollen maturation. Morflex, Inc DEFT EFFECTIVE DATE- February 2004 PAGE 5OF6 :Repreductrve effects ? •.%, rr r,sl tel�S s pt f�rr�t k i'k Y •.a ` �5 i'h .*lv::-t it a, .ram w, '• . ° {Y,A �'��'"'i.�r. . -'!•i r ��k�` • No significant reproductive or developmental effects were observed in the fetuses of female and male rats or rabbits given DEET. In female rats given 125 - 750 mg/kg/day orally on gestational days 6-15, no external, visceral, or skeletal malformations were observed in fetuses; however, reduced fetal weight gain was noted at 750 mg/kg. In a chronic two generation reproduction study, the F2 offspring of CD rats given 500 - 5000 ppm showed a slight increase in exploratory locomotor activity at the high dose level. 12. ECOLOGICAL INFORMATION • EC50 (48h, daphnia) = 56 - 100 ppm • LC&O(96h, rainbow trout) = 71.25 ppm • LC50 (96h, Pimephales promelas - fathead minnow) = 110 mglL • LC50 (Colinus virginianus - Northern bobwhite quail) = 1375 mglkg Not predicted to exhibit significant toxicity to fish. Not expected to bioaccumulate. Modeling suggests rapid degradation in the atmosphere; biodegradation data suggests moderate rate of biodegradation. 13. DISPOSAL CONSIDERATIONS Disposal must be in accordance with Federal, State, and Local regulations. 14. TRANSPORT INFORMATION DOT SHIPPING`CLASSIFICA�TION s insect repellent other than agricultural IIA :DOT A�.ZR.yyQAS Non hazardous s.1�CLyS lJN iVUMgfrR '.F Not applicable. DOHRD4L`Ay;} Not applicable. i 4t Not listed. 15. REGULATORY INFORMATION OSHA STATUS-' Irritant (eye). SARA TITLE.III Not listed. CERCI.A , ; Not applicable. INVENTORIES 3 = TSCA Yes 4 - CANADA ; DSL EINECS 205-149-7 , JAPAN 3-1321; 3-1677 AUSTRAL'IA .` Yes KOREA- -.:.' KE-10492 Morflex, Inc. DEET EFFECTIVE DATE: February 2004 PAGE 6 OF 6 CHINA'- Yes I-PHILIOPINES, Yes SWITZERLANDI G-2482 16. OTHER INFORMATION v, " + 12 , %N 44€HEALN LA 44 6 i C I YY 12,"10 Jv1T "j P ,E iot6NAiV�+' :PROTECTION, 1 0 B -N 0 DATE GENERATED: 02-26-2004 The Information contained heroin is true and -accurate to the best of our 0ovviedge. No warranty or guarantee is expressed or implied regarding the accuracy of such data. I1 is the user's responsibi4ty to determine the suitability for his own use of the products dosenbed heroin. Nothing heroin shall constiiuta parrniSsiun, inducement, or recornmandation to practice any invention covered by any patent owned by Mordex. Inc or by others, nor as a moomrriandation to use wry product or to practice any process in violation of any tow or government F89LAAW. XXX-1111 Castor Oil Technical Data Sheet � V ertellus" Product XXX-1TA° Oil is a free flowing partially dehydrated castor oil that has Identification excellent mineral oil solubility. It is USDA accepted as a trolley lubricant for use in meat packing houses and complies with 21 CFR Part 178.3570 — Lubricants with Incidental Food contact. XXX-1T"" is an efficient plasticizer for PVC resins with excellent pigment wetting properties to formulate caulks, sealants and joint compounds. Property Value Physical Farm Clear, Moderately viscous liquid Properties Acid Value 6 Color, Gardner 5 Density, Ibs.lgal, 25'C 7.84 Fire Point, COC, 'F 615 Flash Point, COC, 'F 560 Hydroxyl Value 70 Iodine Value 120 Moisture Content, % 0.1 Pour Point, 'F -40 Refractive Index 1.480 Saponification Value 187 Specific Gravity, 25'C125'C 0.942 Viscosity, 25'C, Stokes 2.8 Volatile Matter, % 0.2 • Lubricant for use in food processing plants Applications 0 Lubricant meeting 21 CFR Part 178.3570 • Mineral oil compatible • Compatible with PVC and CPVC resins Excellent for formulating joint compounds, caulks and sealants. For toxicity or regulatory information please consult the Material Safely Data Sheet Information contained in this technical data sheaf is believed to be accurate. Vertellus Performance Materials Inc. assumes no liability and makes no warranty or representation that the information is correct or complete and EXPRESSLY DISCLAIMS ALL REPRESENTA TIONS OR WARRANTIES OF ANY KIND, EXPRESS OR IMPLIED, INCLUDING BUT NOT LIMITED TO WARRANTIES OF MERCMANTABILITYAND FITNESS FOR A PARTICULAR PURPOSE. Final determination of suitability of any material and issues of patent infringement is the sole responsibility of the user who alone knows the conditions of intended use. Our customers should ensure that any product incorporating a Vertellus ingredient is safe for its intended use pursuant to applicable law and that any necessary disclosures to consumers have been made. Vertellus Performance Materials Inc., 2110 High Point Road, Greensboro, NC 27403 USA USA To 1: 800-227-2436 USA Fax: 336-1554-4058 USA Email: VPM-TechServicos@vertellus,com Weh, www.vertellus.com Copyright0VartelluS Specialties Inc. 2006. All Rights Reserved. Page 1 of 1 Revised November, 2006 V Vertellus- XXX-1 Page: 1 16 Sections Printed:08/28/06 MATERIAL SAFETY DATA SHEET jjSECTION 1. PRODUCT IDENTIFICATION original: 10/08/89 revised: 01/28/99 Manufacturer: Vertellus Performance Materials Inc. 2110 High Point Road Greensboro, NC 27403 Information and Emergency Phone during business hours: 1-800CASCHEM For use only in the event of chemical emergencies involving a spill, leak, fire, or accident with this material: Call CHEMTREC 800 424-9300 Trade Name.......... Chemical Name.......: Synonyms .:........... CAS 4................ Chemical Family...... Product Code ........... Product Use.......... PIN## ................. WHMIS-Class.......... XXX-I Dehydrated castor oil none 64147-40-6 Drying oil polymer 71030 Food processing plant lubricant crone None SECTION 2. COMPOSITION/INFORMATION ON COMPONENTS ,COMPONENTS CAS # WEIGHT 'k Dehydrated Castor Oil 64147-40-6 - ir SECTION 3. HAZARDS IDENTIFICATION Emergency Overview: Clear, pale yellow liquid with a characteristic odor. Presents little or no immediate significant hazard if spilled or involved in a fire. Breathing: Single exposure to vapors or mist is not likely to be hazardous. Skin Contact: Extended/repeated contact may cause irritation in some individuals. Eye Contact: Contact with eyes may cause slight eye irritation. Swallowing: Not expected to be toxic by ingestion. Long Term Health Effects: Not known. continued XXX-1 Page: 2 original: 10/08/89 16 Sections Printed:08/28106 revised: 01/28/99 SECTION 3. HAZARDS IDENTIFICATION continued Conditions Aggravated By Exposure: Not known. jI SECTION 4. FIRST AID MEASURES' . - II Breathing: No specific treatment is necessary since the material is not likely to be hazardous by inhalation, If exposed to excessive levels of vapors or mists, remove to fresh air and get medical attention if.cough or other symptoms develop. Skin: Wash with soap and water. Get medical attention if irritation develops or persists. Eye. Immediately flush eyes with plenty of water forat least IS. minutes, holding eyelids apart. Get medical attention if irritation or other symptoms occur. Swallowing: Get immediate -medical attention. Never give anything by mouth to an unconscious person. I! SECTION 5.. FIRE FIGHTING MEASURES li Flash Point .. .... .. ... .. .. .. . 400 deg F 204 deg C Method ...... .... ........... pmcc Lower Explosive Limit........ N/A Upper Explosive Limit........ N/A Auto Ignition Temperature ... 840 deg. F Extinguishing Media.......... cot, dry chemical, alcohol foam, water spray Firefighting Procedure. — Evacuate area and fight fire from safe distance. Wear pressure - demand self-contained breathing apparatus (MSHA/NIOSH-approved or equivalent) and full protective gear. Special Firefighting Procedure: As with any fire, toxic gases, vapors, and fumes can be generated. Use pressure -demand self-contained breathing apparatus (MSHA/NIOSH approved or equivalent) and full protective gear. Lasing water can cause frothing with increasing fire intensity. Unusual Fire and Explosion Hazards: None known. continued ... N/A = Not Available Page: 3 XXX-1 original: lo/08/89 16 Sections Printed:08/28/06 revised: 01/28/99 SECTION 5. FIRE FIGHTING MEASURES continued Sensitivity To Explosion: None expected by mechanical impact or static discharge Conditions Of Flammability: Material may burn, but does not ignite readily. Avoid high temperatures. 11 SECTION 6. ACCIDENTAL RELEASE MEASURES 11 General: minimize entry of material into sewers and drainage systems. Refer to permit discharge limitations if applicable. Isolate spill area, preventing entry by unauthorized persons. Prevent skin/eye contact. Small Spill: Absorb -spill with inert material (e.g., dry sand, earth). Place in an approved chemical waste container. - Large Spill: Shut off leak, if safe to do so. Clean up spills immediately, observing precautions in Protective Equipment section. - Contain spilled liquid with sand or earth. Retain all contaminated water for removal and treatment. I ..SECTION 7. HANDLING AND STORAGE; Handling: Although this material does not present a,significant skin or eye concern, skin'and eye contact should be avoided as good industrial practice. Wearing of protective gloves and eye protection is recommended., wash hands and contaminated skin after handling. Storage: Store in a cool dry place away from strong oxidizers and acids. 11 SECTION 8. EXPOSURE CONTROLS/ PERSONAL PROTECTION 1 Exposure Levels: None established.' Engineering'Controls: Source of fine spray, mist or vapor should be controlled with local exhaust ventilation. continued ... N/A m Not Available XXX-1 Page: 4 16 Sections Printed:08/28/06 original.: 10/08/89 revised: 01/28/99 (SECTION 8. EXPOSURE CONTROLS/.PERSONAL PROTECTION ... continued 11 Respiratory Protection: Use a NIOSH/MSHA approved air purifying respirator as needed to control exposure. Consult with respirator manufacturer to determine respiratior selection,' use, and limitations. Use a positive pressure air supplied respirator for uncontrolled releases or when air purifying -respirator limitations may be exceeded. Follow respiratory protection program requirements (OSHA 1910.134 and ANSI z88.2) for all respirator use. Eye/Face Protection: Use safety glasses. Where contact'with the eyes is likely, use chemical. goggles. Use a face shield as needed. Skin Protection: Use impervious gloves. Use clean protective body -covering clothing as needed to minimize contact with clothing and skin. SECTION 9. PHYSICAL AND CHEMICAL PROPERTIES Appearance ....... ..... ........... .... ...... Clear, pale -yellow liquid Odor ....... .......... Characteristic Initial Boiling Point . .. ... .. .. ..... .. .. ... .. 595 deg F 313 deg C Final Boiling Point . ........ .......... ....... 595 deg F 313 deg C ,Specific Gravity (Relative to Water) .. I ...... •0.94 B 77F Vapor Density. (relative to air) ............... Heavier Vapor Pressure (mm. Hg)....................... N/A pH.......... N/A Solubility in Water .......................... insoluble Freezing/Melting Point ....................... _40.deg.F Octanol/water Partition Coefficient.......... N/A :Odor Threshold....... I ........................ 'N/A Viscosity..:..... 3 Stokes 0 77F Evaporation Rate (relative to n-Butylacetate) slower II SECTION 10. STABILITY AND REACTIVITY II Stable: Yes. Strong Oxidizer: No. Hazardous Polymerization: Not prone to hazardous polymerization: Incompatibility: Can react vigorously with oxidizing materials. continued ... N/A = Not Available XXX- 1 Page. 5 16 Sections Printed:08/28106 original: 10/08/89 revised: 01/28/99 SECTION 10. STABILITY AND REACTIVITY ... continued Conditions to Avoid: Keep from contact with oxidizing materials. Hazardous Decomposition Products: Products of incomplete combustion may include CO, CO2, and dense smoke. SECTION 11_ TOXICOLOGICAL INFORMATION Toxicology:' Not available. SECTION 12. ECOLOGICAL INFORMATION Ecotoxicological Information: Not available_ Chemical. Pate Not available. SECTION 13. DISPOSAL CONSIDERATIONS Waste Disposal: Dispose -of in accordance with all federal, state, and local regulations. Container Disposal: Dispose of in accordance with all federal, state, and local regulations. SECTION 14. TRANSPORT INFORMATION DOT Shipping Name...: Not regulated .Hazard Class.._-.... Packing Group........ UN/NA No. DOT Labels...,....... Subsidiary Label....: DOT Placards......... IMO Shipping Name...: Not regulated Hazard Class......... Packing Group........ UN No. IMO Labels........... j Subsidiary Label....: IATA Shipping Name- Not regulated Hazard Class........: Packing Group........ continued .. N/A = Not Available '' XXX -1 Page: 6 16 Sections Printed:08/28/06 original: 10/08/89 revised: 01/28/99 SECTION 14. TRANSPORT INFORMATION ... continued UN No . .............: IATA Labels ......... . Subsidiary Label....: SECTION 15. REGULATORY INFORMATION SARA 311/312 Chronic Health Hazard : no SARA 311/312 Acute Health Hazard._ : no SARA 311/312 Fire Hazard.......... no SARA 311/312 Sudden pressure...... no SARA 311/312 Reactivity Hazard_... no Section 302 Extremely Hazardous: Ingredients CAS # weight % TPQ ** None *} CERCLA Hazardous Substances: Ingredients CAS # Weight w RQ, ** None ** Section 313 Toxic Chemicals: Ingredients CAS # Weight w ** None ** NJ Environmental Hazardous Substance List: Ingredients CAS # ** None '* California Proposition 65 Ingredients: Ingredients CAS # Weight 1k , ** None ** TSCA: This substance is listed on the TSCA inventory. DSL/EINECS: This substance is listed on the Canadian Domestic Substances List & the European Inventory of Existing Commercial Chemical Substances WHMIS: This product is not classified as a controlled product under' Canadian Controlled Product Regulations. SECTION 16. OTHER INFORMATION NFPA Hazard Ratings: HMIS Hazard Rating: Health ............. : o Health............. o Fire ............... : 1 Fire ............... 1 Reactivity......... : o Reactivity......... 0 Specific Hazard..-. None continued ... N/A = Not Available XXX-1 Paae: 7 16 Sections Printed:08/28/06 original: 10/08/89 revised..01/28/99 SECTION 16_ OTHER'INFORMATION continued MSDS Revisions: 1/28/99; Added regulatory.znformati.on (sect 15) NOTE: This information is furnished without warranty, expressed or implied, except that it is accurate to the best knowledge of Vertellus Performance Materials Inc, The data on this sheet relates only to the specific material designated herein. Vertellus Performance Materials Inc. assumes no legal responsibility for use or reliance upon these data. Printed: Aug. 28, 2006: Changed manufacturer from CasChem, a Division of Rutherford Chemicals LLC to Vertellus Performance Materials Inc. Changed print date. Changed Section 16 note. N/A = Not Available