NCG030671_COMPLETE FILE - HISTORICAL_20180607

STORMWATER DIVISION CODING SI
NCG PERMITS
PERMIT NO. /V CAD 30 (1 � l
DOCTYPE I [� HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE ❑ ��Iq D (� O
YYYYM M DD

King, Melissa
From: King, Melissa
Sent: Thursday, June 07, 2018 11:43 AM
To:'[e-mail]'
Cc: Reed, Isaiah L
Subject: NCG030671 Stormwater General Permit
Attachments: 5 312016 coverage letter.pdf
Tony
Thank you for the telephone call. Please find attached a copy of Prince's coverage letter. Also, Mr. Isaiah Reed has been
copied on this. He will assist you with any questions. Thanks so much.
Melissa
ESSE QUAK VIDERI
Melissa 3. King, PE - [e-mail]
North Carolina Dept. of Environmental Quality
Asheville Regional Office
Division of Energy, Mineral and Land Resources - Land Quality
2090 U.S. 70 Highway
Swannanoa, NC'28778
Tel: [phone]
Fax: [phone]
Notice: E-mail correspondence to and from this address may be subject to the North Carolina
Public Records Law and therefore may be disclosed to third parties.

aceAnalytical.
xmwpacelab&=n
June 03, 2016
RECEIVE
JUN 13 2016
CENTRAL FILES
DwR SEC-naN
Jim Zell
Norton Door Controls
3000 Highway 74 East RECEIVED
Monroe, NC 213112
CENTRAL RAL I"'ILL S
DWR SECI]ON
RE: Project: STORMWATER
Pace Project No.: 92298406
J
r
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
IV C6- (0 -3os�/
Dear Jim Zell:
Enclosed are the analytical results for sample(s) received by the laboratory on May 19, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
Page 1 of 40

aceAralAcal
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Project: STORMWATER
Pace Project No.: 92298406
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification Ili
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification Ili
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Chinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
UrrginialVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 40

t
Pace Analytical Services, Inc.
5aceAnalyficale9800
Kincey Ave. Suite t00
Huntersville, NC 28078
w AeoWahacarn
[phone]
SAMPLE ANALYTE COUNT
Project: STORMWATER
Pace Project No.: 92298406
Analyles
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92298406001 SDO-1
EPA 200.7
CDF
1 PASI-A
EPA 625
Bpi
58 PASI-C
EPA 624
GAW
34 PASI-C
SM 2540D
SAM
1 PASI-A
92298406002 SDO-2
EPA200.7
CDF
1 PASI-A
EPA625
Bpi
58 PASI-C
EPA624
GAW
34 PASI-C
SM 2540D
SAM
1 PASI-A
92298406003 SDO-3
FPA200.7
CDF
1 PAS -A
EPA 625
Bpi
58 PASI-C
EPA 624
GAW
34 PASi-C
SM 2540D
SAM
1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 40

le
Analytical
www!peaelaLsmm
SUMMARY OF DETECTION
Pace Analytical Services, Inc.
9600 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
STORMWATER
92298406
Lab Sample ID
Client Sample 0
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92298406001
SDO-1
Collected By
J. Zell
05/17/16 10:20
Collected Date
5/17116
05/17/16 10:20
Collected Time
10:20
05/17/16 10:20
Field pH
7.4
Std. Units
0.10
05/17/16 10:20
92298406002
Soo-2
Collected By
J. Zell
05/31/16 10:55
Collected Date
5/31116
05/31/16 10:55
Collected Time
10:55
05/31/16 10:55
Field pH
7.5
Std. Units
0.10
05/31/16 10:55
92298406003
S130-3
Collected By
J. Zell
05/31/16 10:40
Collected Date
5131116
05131116 10A0
Collected Time
10:40
05131116 10:40
Field pH
7.7
Sid. Units
0.10
05/31/16 10:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 40

acMnalytical.
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PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92298406
Method: EPA 200.7
Description: 200.7 MET ICP
Client: Norton Door Controls
Date: June 03, 2016
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
3 samples were analyzed for EPA 200.7. Alf samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within OC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 40

leAnalytical
irww.pecedehtcom
PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92298406
Method: EPA 625
Description: 625 MSSV
Client: Norton Door Controls
Date: June 03, 2016
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
3 samples were analyzed for EPA 625. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 625 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below,
Method Blank:
All anatytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 40

ac0"Iytical'
wtvw.paciet"Ic"
PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92298406
Method: EPA 624
Description: 624 Volatile Organics
Client: Norton Door Controls
Date: June 03, 2016
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
3 samples were analyzed for EPA 624. All samples were received in acceptable condition with any exceptions rioted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report
Hold Time:
The Samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including INS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,_ Page 7 of 40

5ac
eAnalyiical.
M'YrW.jlgMrebS.Mrh
PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92298406
Method: SM 25400
Description: 2540D Total Suspended Solids
Client: Norton Door Controls
Date: ,tune 03, 2016
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
3 samples were anoly7ed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below_
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch- WETl45092
06: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1739707)
• Total Suspended Solids
• DUP (Lab ID: 1739708)
• Total Suspended Solids
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 40

Pace Analytical Services, Inc.
• 9800 Kincey Ave. Suite 100
;5neAnalXical Huntersville, NC 28078
PeC&q WM (704)875-9€182
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92298406
Sample: SDO.1 Lab ID: 92298406001 Collected: 05/17/16 10:20 Received: 05/19/16 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data Analytical Method
Collected By
J. Zell
1
05/17/16 10:20
Collected Date
5117/16
1
05/17/16 10,20
Collected Time
10:20
1
05/17/16 10:20
Field pH
7.4
Std. Units
0.10
1
05117116 10:20
200.7 MET ICP
Analytical Method: EPA200.7 Preparation Method: EPA200.7
Lead
ND
uglL
5.0
1
05120/16 19:00 05/24/16 05:58
7439-92-1
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND
uglL
5.0
1
05/21/16 13:40 05/25/16 06:57
83-32-9
Acenaphthylene
ND
uglL
5.0
1
05121116 13:40 05/25/16 06:57
208-96-8
Anthfacene
ND
uglL
5.0
1
05/21/16 13:40 D5/25/16 06:57
120-12-7
Benzo(a)anthrecene
ND
ug1L
5.0
1
05/21/16 13:40 05/25/16 06:57
56-55-3
Senzo(a)pyrene
ND
uglL
5.0
1
05/21/16 13:40 05/25/16 06:57
50-32-8
Benzo(b)Fluoranthene
ND
uglL
5.0
1
05121/16 13:40 05/25/16 06:57
205-99-2
Benzo(g,h,i)perylene
ND
uglL
5.0
1
0512111613:40 05125M606:57
191-24-2
Senzo(k)lluoranthene
ND
uglL
5.0
1
05121/16 13:40 05/25/15 06:57
207-08-9
4-Bromophenylphenylether
ND
uglL
5.0
1
0512111613:40 05125/1606:57
101-55-3
Butylbenzylphthalate
ND
ug1L
5.0
1
05/21/16 13:40 05/25/16 06:57
85-68-7
4-ChIoro-3-methylphenol
ND
uglL
5.0
1
05/21/16 13:40 05/25/16 06:57
59-50-7
bis(2-Chloroethoxy)methane
ND
uglL
10.0
1
05/21116 13:40 05/25/16 06:57
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
05/21116 13:40 05/25/16 06:57
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug1L
5.0
1
05121/16 13:40 05/25/16 06:57
10"0-1
2-Chloronaphthalene
ND
uglL
5.0
1
05f21/1613:40 0512511606:57
91-58-7
2-Chlorophenol
ND
uglL
5-0
1
05/21/16 13:40 05/25/16 06:57
95-57-8
4 Chlorophenylphenyl ether
ND
ug/L
5.0
1
05/21/16 13:40 05/25/16 06:57
7005-72-3
Chrysene
ND
ug/L
5.0
1
0512111613:40 05/25/16 06:57
21"1-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
05/21116 13:40 0512511606:57
53-73-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
05/21116 13:40 05/25/16 06:57
91.94-1
2,4-Dichlorophenol
ND
uglL
5.0
1
05/21/16 13:40 05/25/16 06:57
120-83-2
Diethylphthalate
ND
uglL
5.D
1
05121/16 13:40 05/25/16 06:57
84-66-2
2,4-Dimethylphenol
ND
ug1L
10.0
1
05/21/16 13A0 05/25/16 06:57
105-67-9
Dimethylphthalate
ND
uglL
5.0
1
05121/16 13:40 05/25/16 06:57
131-11-3
Di-n-butylphthalate
ND
uglL
5.0
1
05/21/16 13:40 05/25/16 06:57
84-74-2
4,6-1)initro-2-methylphenol
ND
uglL
20.0
1
05/21/16 13:40 05/25/16 05:57
534-52-1
2,4-Dinitrophenol
ND
uglL
50.0
1
05/21116 13:40 05/25/16 06:57
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
05/21116 13:40 05125/1606:57
121-14-2
2,6-Dinitrotoluene
ND
uglL
5.0
1
05/21/1613:40 05/25/16 06:57
606-20-2
Di-n-actylphthalate
ND
uglL
5.0
1
05/21/16 13:40 05/25/16 06:57
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
05121/16 13:40 05/25/16 06:57
117-81-7
Fluoranthene
ND
ug/L
5-0
1
05/21/16 13:40 05/25/16 06:57
206-44-0
Fluorene
ND
ug1L
5-0
1
05121/1613:40 05/25/16 06:57
86-73-7
Hexachloro-1,3-buladiene
ND
ug1L
5-0
1
05121/16 13:40 05/2511606:57
87-68-3
Hexachlorobenzene
ND
ug/L
5-0
1
05121/16 13:40 05/25/16 06:57
118-74-1
Hexachlorocyclopentadierte
ND
ug/L
10.0
1
05/21116 13:40 05/25/16 06:57
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
05121/16 13:40 05/25/16 06:57
67-72-1
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
Date: 06/03/2016 03:53 PM
without the written consent
of Pace Analytical Services, Inc..
Page 9 of 40

Pace Analytical Services, Inc.
aceAnalytical 9800 Kiney Ave. Suite 100
Huntersvilla, MC 28078
078
M'1dicom [phone]
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92298406
Sample: SDO-1 Lab 1D: 92298406001 Collected: 05/17/16 10:20 Received: 05/19/16 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
625 MSSV Analytical Method: LPA625 Preparation Method: EPA625
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
05/21/16 13:40 05/25116 06:57
193-39-5
Isophorone
ND
ug/L
10.0
1
05/21/16 13:40 05/25/16 06:57
78-59-1
Naphthalene
ND
ug/L
5.0
1
05/21/16 13:40 05/25116 06:57
91-20-3
Nitrobenzene
ND
ug1L
5.0
1
05/21/16 13:40 05/25/16 06:57
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
05121/16 13:40 05/26/16 M57
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
05121/16 13:40 05/25/16 06:57
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
05121/16 13:40 05/25/16 06:57
62-75-9
N-Nilroso-di-n-propylamine
ND
ug/L
5.0
1
05/21/16 13:40 05/25/16 06:57
621 64 7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
05/21/16 13:40 05/25/16 06:57
86-30-6
Pentachlorophenol
ND
ug/L
10.0
1
05/21/16 13:40 05/25/16 06:57
87-86-5
Phenanthrene
ND
ug/L
5.0
1
05/21/16 13:40 05/25116 06:57
85-01-6
Phenol
ND
ug/L
5.0
1
05121/16 1140 05/25116 06:57
Pyrene
ND
uglL
5.0
1
05/21/16 13:40 05/25116 06:57
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
0512l/16 13:40 05/25/16 06:57
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
05/21/16 13:40 05/25/16 06:57
88-06-2
Surrogates
Nitrobenzene-d5 (S)
71
%
10-120
1
05121/16 13:40 05/25/16 06:57
4165-60-0
2-Fluorobiphenyl (S)
67
%
15-120
1
05/21/16 13A0 05/25/16 06:57
321-60-8
Terphenyl-d14 (S)
96
%
11-131
1
05/21/16 13:40 05/25/16 05:57
1718-51-0
Phenol-d6 (S)
26
%
10-120
1
05121/16 13:40 05/25/16 06:57
13127-88-3
2-Fluorophenol (S)
36
%
10-120
1
05/21/16 13:40 05/25/16 06:57
367-12-4
2,4,6-Tribromophenol (5)
74
%
10-137
1
05121/16 13:40 05/25116 06.57
118-79-6
624 Volatile Organics
Analytical Method:
EPA624
Benzene
ND
ug/L
2.0
1
05/20/16 20:53
7143-2
Bromodichloromethane
ND
u911-
2.0
1
05/20/16 20:53
75-27-4
Bromoform
ND
ug/L
2.0
1
05120/1620:53
75-25-2
Bromomethane
ND
ug/L
2.0
1
05120M620:53
74-83-9
Carbon tetrachloride
ND
uglL
2.0
1
05120116 20:53
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
05120/16 20:53
108-90-7
Chloroethane
ND
uglL
2.0
1
05/20116 20:53
75-00-3
Chloroform
ND
ug/L
2.0
1
05/20/18 20:53
67-66-3
Chloromethane
ND
ug/L
2.0
1
05/20/16 20:53
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
05/20/16 20:53
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
05120/1620:53
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
0512011620:53
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
05/20/1620:53
106-46-7
1,1-Dichloroethene
ND
ug/L
2.0
1
05120/16 20:53
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1
05/20/16 20:53
107-06-2
I J-Dichloroethene
ND
ug/L
2.0
1
05120/16 20:53
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
0512011620:53
156-59-2
trans-1,2-Dichloroethene
N❑
uglL
2-0
1
05120/1620.53
156-60-5
1,2-Dichloropropane
ND
ugh.
2-0
1
05/2011620:53
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
05120/1620.53
10061-01-5
trans-1,3-Dichloropropene
ND
ug!L
2.0
1
0512011620,53
10061-02-6
Ethylbenzene
ND
uglL
2-0
1
05/20/16 20:53
100-41-4
Methylene Chloride
ND
ug/L
2.0
1
05/20116 20:53
75-09-2
REPORT OF LABORATORY ANALYSIS
This report shill not be reproduced, except in full,
Date: 06/03/2010 03:53 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 40

r
IRC, lyiica!
wwwyace(e6t.Gom
ANALYTICAL RESULTS
Project: STQRMWATER
Pace Project No.: 92298406
Pate Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SDO-1
Lab ID: 92298406001
Collected: 05/17/16 10:20
Received: 05/19/16 10:00 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
GAS No Qual
624 Volatile Organics
Analytical Method:
EPA 624
1,1,2,2-Tetrachloroethane
ND
uglL
2.0
1
05/20/16 20:53
79-34-5
Tetrachloroethene
ND
uglL
2.0
1
06/20/16 20:53
127-18-4
Toluene
ND
uglL
2.0
1
05/20/16 20:53
108-88-3
1,1,1-Trichloroethane
ND
uglL
2.0
1
05/2011620:53
71-55-6
1,1,2-Trichloroethane
NO
ug1L
2.0
1
05120116 20:53
79-00-5
Trichloroethene
Nil
uglL
2.0
1
05/20/16 20:53
79-01-6
Trichlorofluoromelhane
ND
uglL
2.0
1
05/20/16 20:53
75-69-4
Vinyl chloride
ND
uglL
2.0
1
05/20/16 20:53
75-01-4
Surrogates
4-Bromofluorobenzene (S)
112
%
70-130
1
05120116 20:53
460-00-4
Toluene-t18 (S)
99
%
70-130
1
05/20/15 20:53
2037-26-5
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
05/20/16 20:53
17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg1L 2.5 1 05/22/16 14:63
Date: 06/03/2016 03:53 PM
REPORT OF LABORATORY ANALYSIS
This report Shah not de reproduced, except in full,
without the written Consent of Pace Analytical Services, Inc..
Page 11 of 40

r
Pace Analytical Services, Inc.
aceAnalytical6 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wwwpacelahs.com [phone]
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92298406
Sample: SDO-2 Lab ID: 92298406002 Collected: 05117/16 10:55 Received: 05119/16 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
J. Zel1
1
05131/16 10:55
Collected Date
5/31116
1
05/31116 10:55
Collected Time
10:55
1
05/31/16 10:55
Field pH
7.5
Std. Units
0.10
1
05/31/16 10:55
200.7 MET ICP
Analytical Method:
EPA 200.7 Preparation Method: EPA
200.7
Lead
ND
ug1L
5.0
1
05/20/16 19:00
05/24116 06:01
7439-92-1
625 MSSV
Analytical Method:
EPA 625 Preparation Method: EPA 625
Acenaphthene
ND
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
83-32-9
Acenaphthylene
ND
ug1L
5.0
1
05/21/16 13:40
05/25/16 07:51
208-96-8
Anthracene
ND
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
120-12-7
Benzo(a)anthracene
ND
ug1L
5.0
1
05/21/16 13:40
05/25/16 07:51
56-55-3
Benzo(a)pyrene
ND
ug/i_
5.0
1
05/21/16 13:40
05/25/16 07:51
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
205-99-2
Benzo(g,h,i)perylene
IVD
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
191-24-2
Benzo(k)Ruoranthene
ND
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
207-08-9
4-Bromophenylphenylether
N❑
ug/L
5.0
1
05/2111613:40
05/25/16 07:51
101-55-3
Butylbenzylphtha late
ND
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
85-68-7
4-Chtoro-3-methyl phenol
ND
ug/L
5.0
1
0512111613:40
05125/1607:51
59-50-7
bis(2-C hloroethoxy) methane
ND
ug/L
10.0
1
0512111613:40
05/25/16 07:51
111-91-1
bis(2-Chloroethyl)ether
ND
ug/L
5.0
1
05/21/16 13:40
05125/1607:51
111-44-4
bis(2-Chloroisopropyl)ether
ND
ug/L
5.0
1
05/2111613:40
05/25/16 07:51
108-60-1
2-Chloronaphthalene
ND
ug/L
5.0
1
0512111613:40
05/25/16 07:51
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
05/2111613:40
05/2511607:51
95-57-8
4-Chlorophenylphenylether
ND
ug/L
5.0
1
0512111613:40
05/25/16 07:51
7005-72-3
Chrysene
ND
ug/L
5.0
1
05121/16 13:40
05/25/16 07:51
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
05/21/16 13A0
05/25/16 07:51
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
05/21/16 13:40
05/25/16 07:51
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
05121/16 13:40
051251116 07:51
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
05/21/16 13740
05/25/16 07:51
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
05/21/16 13:40
05/25/16 07:51
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
05121/16 13:40
05/25/16 07:51
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
05/21/16 13:40
05/25/16 07:51
534-62-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
05/21/16 13A0
05/25/16 07:51
51-28-5
2,4-Dinitrotoluene
ND
ug1L
5.0
1
05/21/16 13:40
05/25/16 07:51
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
05121/16 13:40
05/25/16 07:51
606-20-2
Di-n-octylphthalate
ND
uglL
5.0
1
05/21/16 13:40
05/25/16 07:51
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
05/21/16 13A0
05/25/16 07:51
117-81-7
Fluoranthene
ND
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
206-44-0
Fluorene
ND
ug1L
5.0
1
05/21/16 13:40
05/25/16 07:51
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
05121/16 13:40
05/25/16 07:51
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
05/21/16 13:40
05/25/16 07:51
77-47-4
Hexachloroethane
ND
ug1L
5.0
1
05/21/16 13:40
05/25/16 07:51
67-72-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 40

Pace Analytical Services, Inc.
aceAnalytical 9800 Kinsey Ave. Suite 100
Hunlersville, NG 28078
r' NWp"WAS° [phone]
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92298406
Sample: SDO.2 Lab ID: 92298406002 Collected: 05/17/16 10:55 Received: 05/191/6 10:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua;
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
I1deno(1,2,3-cd)pyrene
NO
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
193-39-5
Isophorone
NO
ug/L
10.0
1
05/21/16 13:40
05125/1607:51
78-59-1
Naphthalene
NO
ug/L
5.0
1
05/21/16 13:40
05125/1607:51
91-20-3
Nitrobenzene
NO
ui
5.0
1
05/2111613:40
05125M607:51
98-95-3
2-Nitrophenol
NO
ug/L
5.0
1
05121116 13:40
05/25/16 07:51
88-75-5
4-Nitrophenol
NO
ug/L
50.0
1
05/21/16 13:40
05/25116 07:51
100-02-7
N-Nitrosodimethylamine
ND
ug1L
5-0
1
05/21/16 13:40
05/25/16 07:51
62-75-9
N-Nitroso-di-n-propylamine
ND
ug1L
5-0
1
05121116 13:40
0512511607:51
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
0512111613:40
05/2511607:51
86-30-6
Pentachlorophenol
ND
ug/L
10,0
1
M2111613740
0612511607:51
87-86-5
Phenanthrene
NO
ug/L
5.0
1
M2111613:40
0512511607:51
85-01-8
Phenol
NO
ug/L
5.0
1
05121116 1140
05/25/16 07:51
Pyrene
NO
ug/L
5.0
1
05/21116 13:40
05/25/16 07:51
129-00-D
1,2,4-Trichlorobenzene
NO
ug/L
5.0
1
05/21/16 13:40
05/25/16 07:51
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
05/21/16 13:40
05/25/16 07:51
88-06-2
Surrogates
Nitrobenzene-d5 (S)
72
%
10-120
1
05/21/16 13:40
05/25116 07:51
4165-60-0
2-Fluorobiphenyl (S)
68
%
15-120
1
05/21/16 13:40
05/25/16 07:51
321-60-8
Terphenyl-d14 (S)
95
%
11-131
1
05121/1613:40
05/2511607:51
1718-51-0
Phenol-d6 (S)
26
%
10-120
1
05/21/16 13:40
05/25/16 07:51
13127-88-3
2-Fluorophenol (S)
35
%
10-120
1
05/21/16 13:40
05/25/16 07:51
367-12-4
2,4,6-Tribromophenol (S)
74
%
10-137
1
05/21116 13:40
05/25116 07:51
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
NO
ug1L
2.0
1
05/20/16 21:27
71-43-2
Bromodichloromethane
ND
ug1L
2.0
1
05/20/16 21:27
75-27-4
Bromot'orm
ND
ug1L
2-0
1
05/20/16 21:27
75-25-2
Bromomethane
ND
ug1L
2.0
1
05/20116 21:27
74-83-9
Carbon tetrachloride
ND
ug1L
2.0
1
05120116 21:27
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
05/20116 21:27
108-90-7
Chloroethane
ND
ug1L
2.0
1
05/20/16 21:27
75-00-3
Chloroform
NO
ug1L
2.0
1
06/20/16 21:27
67-66-3
Chloromethane
NO
ug1L
2.0
1
05/20/16 21:27
74-87-3
Dibromochloromethane
NO
ug1L
2.0
1
05/20/16 21:27
124-48-1
1,2-Dichlorobenzene
NO
ug1L
2.0
1
05/20/16 21:27
95-50-1
1,3-Dichlorobenzene
NO
ug1L
2.0
1
05/20/16 21:27
541-73-1
1,4-Dichlorobenzene
NO
ug1L
2.0
1
05/20/16 21:27
106-46-7
1,1-Dichloroethane
NO
ug1L
2.0
1
05/20/16 21:27
75-34-3
1,2-Dichloroethane
ND
ug1L
2.0
1
05/20/16 21:27
107-06-2
1,1-01chloroethene
ND
ug1L
2.0
1
05/20115 21:27
75-35-4
cis-1,2-Dichloroethene
ND
ug1L
2.0
1
05/20/16 21:27
156-59-2
trans-1,2-Dichloroethene
ND
ug1L
2.0
1
05/20/16 21:27
156-60-5
1,2-Dichloropropane
ND
ug1L
2.0
1
05/2011621.27
78-87-5
cis-1,3-Dichloropropene
ND
ug1L
2-0
1
05/2011621:27
10061-01-5
Trans-1,3-Dichloropropene
ND
ugIL
2-0
1
0512011621:27
10061-02-6
Ethylbenzene
ND
ug1L
2-0
1
0512011621:27
10041-4
Methylene Chloride
ND
ug/L
2-0
1
0512011621:27
75-09-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0610312016 0353 PM without the written consent of Pace Analytical Services, Inc.
Page 13 of 40

acaAna1jfta1 *
NMwpeGelahSarfl
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92298406
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SDO-2
Lab ID: 92298406002
Collected: 05/17116 10:55
Received: 05/19/16 10:00 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624
1,1,2,2-Tetrachloroethane
ND
ug1L
2.0
1
05/20/16 21:27
79-34-5
Tetmehloroethene
ND
uglL
2.0
1
05/20/16 21:27
127-18-4
Toluene
ND
ug/L
2.0
1
05/20116 21:27
108-88-3
1,1,1-Trichloroeihane
ND
ug1L
2.0
1
05/20116 21:27
71-55-6
1,1,2-Trichloroethane
ND
ug)L
2.0
1
05/20/16 21:27
79-00-5
Trichloroethene
ND
ug1L
2.0
1
05120116 21:27
79-01-6
Trichtorofluoromethane
ND
ug1L
2.0
1
05/20/16 21:27
75-69-4
Vinyl chloride
ND
ug1L
2.0
1
05/20/16 21:27
75-01-4
Surrogates
4-Bromofluorobenzene (S)
113
%
70-130
1
05120116 21:27
460-00-4
Toluene -dB (S)
100
%
70-130
1
05120116 21:27
2037-26-5
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
05/20116 21:27
17D60-07-0
25400 Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg1L 2.5 1 05/22/16 14:54
Date: 06/03/2016 03:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 40

Pace Analytical Services, Inc.
•
aceAnalytical 9800 Kincey Ave. Suite100
Nuntersville, NC 28078a78
Wwwproelabsoom [phone]
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92298406
Sample: SDO-3
Lab ID: 92298406003
Collected: 05/17/16 10:40
Received: 05/19116 10:00 Matrix: Water
Parameters
Results
Units
Report Limit
OF
Prepared Analyzed
CAS No, Qual
Field Data
Analytical Method:
Collected By
J. Zell
1
05/31/16 10:40
Collected Date
5/31116
1
05/31/16 10:40
Collected Time
10:40
1
05/31116 10A0
Field pH
7.7
Sid. Units
0.10
1
05/31/16 10:40
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead
ND
ug/L
5.0
1
05/20/16 19:00 05/24/16 06:04
7439-92-1
625 MSSV
Analytical Method: EPA625 Preparation Method: EPA625
Acenaphthene
ND
ug/L
5.0
1
05/21/16 13A0 05125/16 08:46
83-32-9
Acenaphihylene
ND
ug/L
5.0
1
0512111613:40 05/25/16 08:46
208-96-8
Anthracene
ND
ug/L
5.0
1
05121/16 13:40 05/25/16 08:46
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
05121/16 13A0 05/25/16 08:46
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
05/21/16 13:40 05/25/16 08:46
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
05/21/16 13:40 05/25/16 08:46
205-99-2
Benzo(g,h,i)perylene
NO
ug/L
5.0
1
05121/1613:40 05125/1608:46
191-24-2
Benzo(k)fluorenthene
NO
ug/L
5.0
1
05/21/16 13:40 05/25116 08:46
207-08-9
4-Bromophenylphenylether
NO
ug/L
5.0
1
05/2111613:40 0512511608:46
101-55-3
Butylbenzylphthalate
NO
ug1L
5.0
1
05/21/16 1140 05/25/16 08:46
85-68-7
4-Chloro-3-methytphenol
NO
ug/L
5.0
1
05/21/16 13:40 05/25/16 08:46
59-50-7
bis(2-Chloroethoxy)methane
NO
ug1L
10.0
1
05/21116 13:40 05/25/16 08:46
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
0512V16 13:40 05/25/16 08:46
111-44-4
bis(2-Chloroisopropyl) ether
NO
ug/L
5.0
1
05/21/16 13:40 05/25/16 08:46
108-60-1
2-Chloronaphthalene
ND
ug/L
5.0
1
05121/16 13:40 05/25/16 08:46
91-58-7
2-Chlorophenol
NO
ug/L
5.0
1
05121/1613:40 05/25/16 08:46
95-57-8
4-Chlorophenytphenyl ether
IND
ug/L
5.0
1
05/21/16 13:40 05/25116 08:46
7005-72-3
Chrysene
ND
ug/L
5.0
1
05/21/16 13:40 05/25116 08:46
218-01-9
Dibenz(a,h)anthracene
ND
uglL
5.0
1
05121/16 13:40 05/25/16 08:46
53-70-3
3,3'-Dichlorobenzidine
ND
uglL
25.0
1
05121/16 13:40 05125116 08:46
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
05121/16 13A0 05/25/16 08:46
120-83-2
Diethylphtha late
NO
ug/L
5.0
1
05f21116 13:40 05/25/16 08:46
84-66-2
2,4-Dimethylphenol
NO
ug/L
10.0
1
05/21/16 13:40 05/25/16 08:46
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
05/21/16 13:40 05/25/16 08:45
131-11-3
Di-n-butylphthalale
ND
ug1L
5.0
1
05/21/16 13:40 05/25/16 08:46
84-74-2
4,6- Din itro-2-methyl phenol
ND
ug/L
20.0
1
05/21/16 13:40 05/25/16 08:46
534-52-1
2,4-Dinitrophenol
ND
ug1L
50.0
1
05/21/16 13:40 05/25/16 08:46
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
05/21/16 13:40 05/25/15 08:46
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
0512l/16 13:40 05/25/16 08:46
606-20-2
Di-n-octylphthalate
ND
uglL
5.0
1
05/21/16 13:40 06/25/16 08:46
117-84-0
bis(2-Ethythexyl)phthalate
ND
ugtL
5.0
1
05121116 13:40 05/25/16 08:46
117-81-7
Fluoranthene
ND
ug/L
5-0
1
05/21/16 13:40 05125/16 08:46
2W44-0
Fluorene
ND
ug/L
5.0
1
05/21/16 13:40 05125/16 08A6
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5-0
1
W21/16 13:40 05/2506 08:46
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
05/21/16 13:40 05/25/16 08:46
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
05/21/16 13:40 05/25/16 08:46
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
05/21116 13:40 05125f16 08.46
67-72-1
REPORT
OF
LABORATORY ANALYSIS
This report shall
not be reproduced, except in
full,
Date: 06/03/2016 03:53 PM
without the written consent of Pace Analytical Services,
Inc..
Page 15 of 40

Pace
Analytical Services, Inc.
;5neAnayicale
9800 Kiney Ave. Suite
Huntersville, NC 2807878
WWW Paostat'&C3 n
(704 )875-9092
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92298406
Sample: SDO-3
Lab ID: 92298406003
Collected: 05/17/16 10A0
Received: 05119116 10:00 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No, Qual
625 MSSV
Analytical Method:
EPA 625
Preparation Method: EPA 625
Indeno(1,2,3-cd)pyre ne
NO
ug/L
5.0
1
05/21/16 13:40
0512511608:46
193.39-5
Isophorone
NO
ug/L
10.0
1
05121/1613:40
0512511608:46
78-59-1
Naphthalene
ND
uglL
5.0
1
05121/1613:40
05/25116 08:46
91-20-3
Nitrobenzene
NO
ug1L
5.0
1
05/2111613:40
05125/1608:46
98-95-3
2-Nitrophenol
NO
ug/L
5.0
1
0512111613:40
05125M608:46
88-75-5
4-Nitrophenol
NO
uglL
50.0
1
05121116 13:40
05/25/16 08:46
100-02-7
N-Nitrosodimethyla mine
NO
ug1L
5.0
1
05121/16 13A0
05125/16 08:46
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
0512111613:40
0512511608:46
621-64-7
N-Nitrosodiphenylamine
ND
ug1L
10.0
1
05/21/16 13:40
05/25/16 0&46
86.30-6
Pentachlorophenol
ND
ug/L
10.0
1
05121/16 13:40
05/25/16 08:46
87-86-5
Phenanthrene
ND
ug1L
5.0
1
05/2111613:40
0512611608:46
85-01-8
Phenol
ND
ug1L
5.0
1
0512111613:40
051251160&46
Pyrene
ND
ug/L
5.0
1
0512//16 13:40
05125M6 08:46
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
05/21/16 13A0
05/25116 08:46
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
05/21/16 13:40
05125/16 08:46
88-06-2
Surrogates
Nitrobenzene-d5 (S)
78
%
10-120
1
05/21/16 13:40
06/25116 08:46
4165-60-0
2-Fluoroblphenyl (S)
77
%
15-120
1
05/21/16 13:40
05/25116 08:46
321-60-8
Terphenyl-d14 (S)
102
%
11-131
1
05/21/16 13:40
05/25/16 08.46
1718-51-0
Phenol-d6 (S)
28
%
10-120
1
05/21/16 13:40
05/25/16 08A6
13127-28-3
2-Flttorophenol (S)
38
%
10-120
1
05/21/16 13.40
05/25/16 08:46
367-12-4
2.4,6-Tribromophenot (S)
80
%
10-137
1
05/21/15 13:40
05/25/16 08A6
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND
uglL
2.0
1
05/20/16 21:10
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
05/20116 21:10
75-27-4
Bromolorm
N❑
ug/L
2-0
1
05/20/16 21:10
75-25-2
Bromomethane
NO
ug1L
2.0
1
05/20116 21:10
74-83-9
Carbon tetrachloride
Nfl
ug/L
2.0
1
05/2011621A0
56-23-5
Chlorobenzene
NO
uglL
2.0
1
05120116 21:10
108-90-7
Chloroethane
NO
ug1L
2.0
1
05/20/16 21:10
75-00-3
Chloroform
ND
ug1L
2.0
1
05/20/16 21:10
67-66-3
Chloromethane
ND
uglL
2.0
1
05/20/16 21:10
74-87-3
Dibromochloromethane
NO
ug1L
2.0
1
05/20/16 21:10
124-48-1
1,2-Dichlorobenzene
NO
ug1L
2.0
1
05/20/16 21:10
95-50-1
1,3-Dichlorobenzene
ND
ug1L
2.0
1
05/20/16 21:10
541-73-1
1,4-Dichlorobenzene
ND
ug1L
2.0
1
05/20/16 21:10
106-46-7
1,1-01chtoroethane
NO
uglL
2.0
1
05/20/16 21:10
75-34-3
1,2-Dichforoethane
ND
ug1L
2.0
1
05/20/16 21:10
107-06-2
i,1-Dichforoethene
ND
ug1L
2.0
1
05/20/16 21:10
75-35-4
cis-1,2-Dichforoethene
ND
ug/L
2.0
1
05/20/16 21:10
156-59-2
trans-1,2-Dichforoethene
ND
ug1L
2.0
1
05/20/16 21:10
156-60-5
1,2-Dichloropfopane
ND
ug/L
2.0
1
05/20/16 21:10
78-87-5
cis-1,3-Dichloropropene
ND
ug1L
2-0
1
0512011621:10
10061-01-5
trans-1,3-Dichloropropene
ND
ug1L
2A
1
05120116 21 i 10
10061-02-6
Ethylbenzene
ND
uglL
2-0
1
05/20/16 21:10
100-41-4
Methylene Chloride
NO
ug1L
2.0
1
05/20116 21:10
75-09-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 40

laneAnalyficalo
~..pacafabic=
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 25078
[phone]
Project: STORMWATER
Pace Project No.: 92298406
Sample: SDO-3
Lab ID: 92298406003 Collected: 05117/15 10:40
Received: 05/19/16 10:00 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method:
EPA 624
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
05/20/16 21:10
79-34-5
Tetrachloroethene
ND
ug1L
2.0
1
05/20/16 21:10
127-18-4
Toluene
ND
ug/L
2.0
1
05/20/16 21:10
108-88-3
1,1,1-Trichloroethane
ND
ug/L
2.0
1
05/20/16 21:10
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
05/20/16 21:10
79-00-5
Trichloroethene
ND
ug1L
2.0
1
05120/16 21:10
79-01-6
TrichloroFluoromethane
ND
uglL
2.0
1
05/20/16 21:10
75-69-4
Vinyl chloride
ND
uglL
2.0
1
05120/16 21:10
75-01-4
Surrogates
4-Bromofluorobe nzene (S)
122
%
70-130
1
05/20/16 21:10
460-00-4
Toluene-d8 (S)
100
%
70-130
1
05/20/16 21:10
2037-26-5
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
05/20/16 21:10
17060-07-0
2540D Total Suspended Solids
Analytical Method:
SM 2540D
Total Suspended Solids
N❑
mg1L
2.5
1
05/22/16 14:54
Date: 06/0312016 03:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 40

(�55'cieAnaljdical*
wtirwpeaelahscom
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.'. 92298406
QC Batch: MPRP121786 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92298406001, 92298406002, 92298406003
METHOD BLANK: 1738823 Matrix: Water
Associated Lab Samples: 92298406001, 92298406002, 92298406003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead ug1L ND 5.0 05124I1614:20
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hvntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1738824
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Lead ug1L 500 488 98 85-115
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1738825
MS
92298303011' Spike
Parameter Units Result Conc.
Lead uglL <2.5 500
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1738827
MS
92298415002 Spike
Parameter Units Result Conc.
Lead ug]L ND 500
1738826
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
500 474 481 95 96 70-130 1
1738828
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
500 482 484 96 97 70-130 0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc..
Qual
Page 18 of 40

aceAnalytical
hMnvpsoelaGcmm
t
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.'. 92298406
QC Batch: MSV136926 Analysis Method:
QC Batch Method: EPA 624 Analysis Description:
Associated Lab Samples: 92298406001, 92298406002, 92298406003
EPA 624
624 MSV
METHOD BLANK: 1739285
Matrix: Water
Associated Lab Samples: 92296406001,
92298406002,
92298406003
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,1.1-Trichloroethane
ugJL
NO
2.0
05120J1612:14
1,1,2.2-Tetrachloroethane
ugJL
NO
2.0
05/20/16 12:14
1,1,2-Trichloroethane
ugJL
NO
2.0
05120/1612:14
1,1-Dichloroethane
ugJL
NO
2.0
0512011612:14
1,1-Dichloroethene
ugJL
ND
2.0
0512011612:14
12-Dichlorobenzene
uglL
NO
2.0
05/20/16 12:14
1,2-Dichloroethane
uglL
NO
2.0
05/20/16 12:14
1,2-Dichloropropane
ugJL
NO
2.0
05/20/16 12:14
1,3-Dichlorobenzene
uglL
ND
2.0
05/20/16 12:14
1,4-Dichlorobenzene
uglL
NO
2.0
05/2011612:14
Benzene
ugll-
NO
2 0
05/20/16 12:14
Bromodichloromethane
uglL
NO
2.0
05/20/16 12:14
Bromoform
uglL
NO
2.0
(15/20/1612:14
Bromomethane
uglL
NO
2.0
05/20/16 12:14
Carbon tetrachloride
uglL
NO
2.0
05/20/16 12:14
Chlorobenzene
ugJL
NO
2.0
05/2011612:14
Chloroethane
uglL
NO
2.0
05120/1612:14
Chloroform
uglL
NO
2.0
05/2011612:14
Chlorometharie
ug1L
NO
2.0
0512011612:14
cis-1,2-Dichloroethene
ugJL
ND
2.0
05120/1612:14
cis-1,3-Dichloropropene
ug1L
NO
2.0
0512011612:14
Dibromochloromethane
u91L
NO
2.0
0512011612:14
Ethy)benzene
ugJL
ND
2.0
0512011512:14
Methylene Chloride
ugJL
ND
2.0
05/20/16 12:14
Tetrachloroethene
uglL
NO
2.0
05/20/16 12:14
Toluene
ugJL
NO
2.0
05120/1612:14
trans-1,2-Dichloroethene
ugJL
NO
2.0
0512011612:14
trans- l,3-Dichloropropene
uglL
NO
2.0
05/20/16 12:14
Trichloroethane
uglL
NO
2.0
05/20/16 12:14
Trichlorofluoromethane
uglL
N❑
2.0
05/20/16 12:14
Vinyl chloride
uglL
NO
2.0
05/20/16 12:14
1,2-Dichloroethane-d4 (S)
%
107
70-130
05/20/16 12:14
4-Bromofluorobenzene (S)
%
119
70-130
05/20/16 12:14
Toluene-d8 (S)
%
100
70-130
05/20/16 12:14
Qualifiers
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1739286
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec. Limits Qualifiers
1,1,i-Trichloroethane ugJL 50 48.2 96 52-162
1,1,2,2-Tetrachloroethane ugJL 50 52.6 105 46-157
Resuhs presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06J0312016 03:53 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 40

ac1Analyticai
www.pecaleLsmm
1
QUALITY CONTROL DATA
Project: 5TORMWATER
Pace Project No.: 92298406
LABORATORY CONTROL SAMPLE:
Parameter
1739286
Units
Spike
Conn
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,2-Trichloroethane
ugiL
50
52.4
105
52-150
1,1-Dichloroethane
ug1L
50
44.5
89
59-155
1,1-Dichloroethene
ugiL
50
48.1
96
1-234
1,2-Dichlorobenzene
ugiL
50
50.1
100
18-190
1,2-Dichloroethane
ugiL
50
47.2
94
49-155
1,2-Dichioropropane
ugiL
50
52.3
105
1-210
1.3-Dichlorobenzene
ugiL
50
50.7
101
59-156
1,4-Dichlorobenzene
ugiL
5o
51.4
103
18-190
Benzene
ugiL
50
53.7
107
37-151
Bromodichloromethane
ugiL
50
54.8
110
35-155
Bromoform
ug1L
50
56.6
113
45-169
Bromomethane
ugiL
50
66.8
134
1-242
Carbon tetrachloride
ugiL
50
57.9
116
70-140
Chlorobenzene
ugiL
50
53.4
107
37-160
Chloroethane
ugiL
50
50.4
101
14-230
Chloroform
ugiL
50
48.0
96
51-138
Chloromethane
ug1L
50
46.8
94
1-273
cis-1,2-Dichloroethene
ug1L
50
48.4
97
68-146
cis-1,3-Dichloropropene
ug1L
50
54.3
109
1-227
Dibromochloromeihane
ugiL
50
54.8
110
53-149
Ethylbenzene
ugiL
50
51.7
103
37-162
Methylene Chloride
ugiL
50
43A
86
1-221
Tetrachloroethene
ugiL
50
58.8
118
64-148
Toluene
ugiL
50
535
107
47-150
trans-12-Dichloroethene
ug1L
5o
486
97
54-156
trans-1.3-Dichloropropene
ug1L
50
51.6
103
17-183
Trichloroethene
ug1L
50
48.9
98
71-157
Trichtorofluoromethane
ug1L
50
49.6
99
17-181
Vinyl chloride
ug1L
50
43.6
87
1-251
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
119
70-130
Toluene -dB (S)
%
102
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC; 28078
[phone]
Qualifiers
MATRIX SPIKE SAMPLE:
Parameter
1739288
Units
92298415002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1-Trichloroelhane
ug1L
ND
20
21.2
106
46-171
1,1,42-Tetrachloroelhane
ug1L
NO
20
21.7
109
73-159
1,1,2-Trichloreethane
ug1L
NO
20
23.4
117
64-152
1,1-Dichloroethane
ug1L
NO
20
20.9
104
43-172
1,1-Dichloroethene
ug1L
NO
20
22.6
113
48-189
12-Dichlorobenzene
ugiL
NO
20
22.3
112
54-154
1,2-Dichloroethane
ugiL
ND
20
19.8
98
42-171
1,2-Dichloropropane
ug1L
ND
20
22.2
111
55-157
1,3-Dichlorobenzene
ug1L
NO
20
22.4
112
57-148
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc. Page 20 of 40

le
aceAnalytifcal
wts�tvpsoetsGs.nam
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinGeyAve_ Suite 100
Muntersville, NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 92298406
MATRIX SPIKE SAMPLE:
1739288
92298415002
Spike
MS
MS
% Rec
Parameter
Units
Result
Cone.
Result
% Rec
Limits Qualifiers
1,4- Diehl orobenzene
ug/L
ND
20
21,7
108
58-149
Benzene
ug/L
NO
20
23.2
116
54-163
Bromodichloromethane
ug/L
ND
20
21.6
108
56-152
Bromoform
ug/L
ND
20
23.7
118
53-151
Bromomethane
ug1L
NO
20
27.5
138
10-200
Carbon tetrachloride
ug/L
NO
20
25.1
125
41-175
Chlorobenzene
ug/L
NO
20
23.1
116
67-152
Chloroethane
uglL
NO
20
24.8
124
23-200
Chloroform
ug/L
NO
20
21.2
106
51-166
Chloromethane
ug/L
NO
20
25.7
128
40-175
cis-1,2-Dichloroethene
ug/L
NO
20
22.3
111
45-174
cis-1,3-Dichloropropene
ug/L
NO
20
23.1
116
38-146
Dibromochloromethane
uI
NO
20
23.3
116
65-144
Ethylbenzene
ug/L
NO
20
22.5
113
57-152
Methylene Chloride
ug/L
NO
20
18.2
91
40-167
Tetrachloroethene
ug/L
ND
20
24.2
121
59-155
Toluene
ug/L
ND
20
22.5
113
47-162
trans- 1,2-D ichl oroethe ne
ug/L
ND
20
22.4
112
47-178
trans- 1,3-Dichloropropene
ug/L
ND
20
21.6
108
39-148
Trichloroethene
ug/L
NO
20
21.0
105
60-153
Trichtoroiluoromethane
ug/L
ND
20
24.1
120
42-199
Vinyl chloride
ug/L
NO
20
23-3
116
46-176
1,2-Dichloroethane-d4(S)
%
97
70-130
4-Bromoiluorobenzene (S)
%
114
70-130
Toluene-d8 (S)
%
101
70-130
SAMPLE. DUPLICATE: 1739287
Parameter
Units
92298293002
Result
Oup
Result RPD Qualifiers
1,1,1-Trichloroethane
ug/L
NO
NO
1,1,2,2-Tetrachtoroethane
ug/L
NO
ND
1,1,2-Tnchloroethane
ug/L
NO
NO
1,1-Dichloroethane
uglL
NO
ND
1,1-Dichloroethene
ug/L
NO
NO
1,2-Dichlorobenzene
ug/L
NO
NO
1,2-Dichloroethane
uglL
NO
NO
1,2-Dichloropropane
ug/L
NO
NO
1,3-Dichlorobenzene
ug/L
NO
ND
1,4-Dichlorobenzene
ug/L
NO
NID
Benzene
ug/L
NO
ND
Bromodichloromethane
ugtL
NO
NO
Bromoform
uglL
NO
NO
Bromomethane
ug/L
NO
NO
Carbon tetrachloride
ug/L
NO
NO
Chlorobenzene
ug/L
NO
NO
Results presented on this page are in the units indicated by the "Units- column except where an ahemate unit is presented to the right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 0153 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 40

�55cieAnalyfica I
wwwpeoafabsooM
QUALITY CONTROL
DATA
Project: STORMWATER
Pace Project No.: 92298406
SAMPLE DUPLICATE: 1739287
92298293002
Dup
Parameter
Units
Result
Result
Chlaroethane
ug1L
NO
NO
Chloroform
ugiL
NO
NO
Chloromethane
ug1L
NO
NO
cis- 1,2-Dichloroethene
ug1L
ND
ND
cis- 1,3-Dichloropropene
ugiL
ND
NO
Dibromochloromethane
ugiL
ND
NO
Ethylbenzene
ugiL
ND
NO
Methylene Chloride
ugR_
ND
ND
Telrachloroethene
ugiL
NO
ND
Toluene
ugiL
NO
ND
trans-1,2-Dichloroethene
ugiL
NO
ND
trans-1,3-Dichloropropene
ug1L
NO
NO
Trichloroethene
ugiL
ND
NO
Trichi orofluoromethane
ugiL
ND
NO
Vinyl chloride
ug1L
ND
ND
1,2-Dichloroethane-d4 (S)
%
105
102
4-Bromofluorobenzene (S)
%
114
110
Toluene-68 (S)
%
98
100
RPD Qualifiers
3
3
3
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the righl of five result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc..
Page 22 of 40

laneAnalytical"'
wwwpowlabs.eom
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92298406
QC Batch: OEXT142708 Analysis Method:
QC Batch Method: EPA625 Analysis Description:
Associated Lab Samples: 92298406001, 92298406002, 92298406003
EPA625
625 MSS
METHOD BLANK: 1739673
Matrix: Water
Associated Lab Samples: 92298406001, 92298406002, 92298406003
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
05/24/16 21:51
2,4,6-Trichlorophenol
ug1L
ND
10.0
05/24/16 21:51
2,4-Dichlorophenol
ug1L
ND
5.0
05/24/16 21:51
2,4-Dimethylphenol
ug/L
ND
10.0
05/24/16 21:51
2,4-Dinitrophenol
ug1L
ND
50.0
05/24/16 21:51
2,4-Dinitrotoluene
ug/L
ND
5.0
05/24/16 21:51
2,6-Dinitrotoluene
ug1L
ND
5.0
05/24/16 21:51
2-Chloronaphthalene
ug1L
ND
5.0
05/24/16 21:51
2-Chlorophenol
ug/L
ND
5.0
05/24/16 21:51
2-Nitrophenol
ug1L
ND
5.0
05/24/16 21:51
3,3'-Dichlorobenzidine
ug/L
ND
25.0
05/24/16 21:51
4,6-Dinitro-2-methylphenol
ug1L
ND
20.0
05/24/16 21:51
4-Bromophenylphenyl ether
ug1L
ND
5.0
05/24/16 21:51
4-Chloro-3-methylphenol
ug1L
ND
5.0
05/24/16 21:51
4-Chlorophenylphenyl ether
ug1L
ND
5.0
05/24/16 21:51
4-Nitrophenol
ug1L
ND
50.0
05/24/16 21:51
Acenaphthene
ug1L
ND
5.0
05/24/16 21:51
Acenaphthylene
ug/L
ND
5.0
05/24/16 21:51
Anthracene
ug/L
ND
5.0
05/24/16 21:51
Benzo(a)anthracene
ug1L
N❑
5.0
05/24/16 21:51
Benzo(a)pyrene
ug1L
ND
5.0
05/24/16 21:51
Benzo(b)fluoranihene
ug1L
ND
5.0
05/24/16 21:51
Benzo(g,h,i)perylene
ug1L
ND
5.0
05/24/16 21:51
Benzo(k)fluoranthene
ug/L
ND
5.0
05/24/16 21:51
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
05/24/16 21:51
bis(2-Chloroethyl) ether
ug/L
ND
5.0
05/24/16 21:51
bis(2-Chloroisopropyl) ether
ug/L
ND
5.0
05/24/16 21:51
bis(2- Ethyl hexyl)phihalate
ug/L
ND
5.0
05/24/16 21:51
Butylbe nzyl phtha late
ug1L
ND
5.0
05/24/16 21:51
Chrysene
ug/L
ND
5.0
05/24/16 21:51
Di-n-butylphthalate
ug/L
ND
5.0
05/24/16 21:51
Di-n-octylphlhalate
uq/L
ND
5.0
05/24/16 21:51
Dibenz(a,h)anthracene
ug1L
ND
5.0
05/24/16 21:51
Diethylphthalate
ug/L
ND
5.0
05/24/16 21:51
Dimethylphthalate
uq/L
ND
5.0
05/24/16 21:51
Fluoranthene
ug/L
ND
5.0
05/24/16 21:51
Fluorene
ug/L
ND
5.0
05/24/16 21:51
Hexachloro-1,3-butadiene
ug/L
ND
5.0
05/24/16 21:51
Hexachlorobenzene
ug/L
ND
5.0
05/24/16 21:51
Hexachlorocyclopentadiene
ug/L
ND
10.0
05/24/16 21:51
Hexachloroethane
ug/L
ND
5.0
05/24/16 21:51
Qualifiers
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 40

133ceAnalyticaI
www.peoefebscbh
QUALITY CONTROL DATA
Project: 9TORMWAT ER
Pace Project No.: 92298406
METHOD BLANK: 1739673 Matrix: Water
Associated Lab Samples: 92298406001, 92298406002, 92298406003
Blank Reporting
Parameter Units Result Limit
Analyzed
Indeno(1,2,3-c(J)pyrene
ug1L
ND
5.0
05/24/16 21:51
lsophorone
ug/L
ND
10.0
05/24/16 21:51
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
OW4116 21:51
N-Nitrosodimethylamine
ug/L
ND
5.0
05/24116 21:51
N-Nitrosodiphenylamine
ug/L
ND
10.0
05/24/16 21:51
Naphthalene
ug/L
ND
5.0
05/24/16 21:51
Nitrobenzene
ug/L
ND
5.0
05/24/16 21:51
Pentachlorophenol
uglL
ND
10.0
05/24/16 21:51
Phenanthrene
ug/L
ND
5.0
05/24/16 21:51
Phenol
uglL
ND
&0
05/24/16 21:51
Pyrene
ug/L
ND
5.0
05/24/16 21:51
2,4,6-Tribromophenot (S)
%
42
10-137
05/24/16 21:61
2-Fluorobiphenyl (S)
%
39
15-120
05124116 21:51
2-Fluorophenol (S)
%
21
10-120
05124/16 21:51
Nitrobenzene-d5 (S)
%
41
10-120
05/24/16 21:51
Phenol-d6 (S)
%
14
10-120
05/24/16 21:51
Terphenyl-d14 (S)
%
86
11-131
05/24/16 21:51
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1739674
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
31.8
64
44-142
2,4,6-Trichlorophenol
ug/L
50
42.1
84
37-144
2,4-Dichlorophenol
ug/L
50
38.0
76
1-191
2,4-Dimethylphenol
ug/L
50
40.2
80
32-119
2,4-Dinitrophenol
ug/L
250
164
66
1-181
2,4-Dinitrotoluene
ug/L
50
52.0
104
39-139
2,6-Dinitrotoluene
ug/L
50
46.4
93
50-158
2-Chloronaphthalene
ug/L
50
38.5
77
60-118
2-Chlorophenoi
ug/L
50
35.7
71
23-134
2-Nitrophenol
ug/L
50
37.4
75
29-182
3,3'-Dichlorobenzidine
u91L
100
79.0
79
1-262
4,6.Dinitro-2-methylphenol
ug/L
100
91.4
91
1-181
4-Bromophenylphenyi ether
ug/L
50
40.6
81
53-127
4-Chloro-3-methylphenol
ug/L
100
90.0
90
22-147
4-Chlorophenylphenyl ether
ug/L
50
44.6
89
25-158
4-Nitrophenot
ug/L
250
97.9
39
1-132
Acenaphthene
ug/L
50
41.4
83
47-145
Acenaphthylene
ug/L
50
41.2
82
33-145
Anthracene
ug/L
50
40.8
82
1-166
Benzo(a)anthracene
uglL
50
43.0
86
33-143
Benzo(a)pyrene
ug/L
50
40.1
80
17-163
Benzo(b)fluoranthene
ug1L
50
39.8
80
24-159
Benzo(g,h,i)perylene
ug/L
50
43A
87
1-219
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Qualifiers
Results presented on this page are In the units indicated by the "units" column except where an attemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 40

Pace Analytical Services, Inc.
lJt /`�
mai 1ical"
980Q KinceyAve_ SuitelOO
Q78
Huntersville, NC 28078
(�5ace
�
[phone]
QUALITY
CONTROL DATA
Project: STORMWATER
Pace Project No,: 92298406
LABORATORY CONTROL SAMPLE:
1739674
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Benzo(k)iluoranthene
uglL
50
40.2
80
11-162
bis(2-Chloroethoxy)methane
uglL
50
41.3
83
33-184
bis(2-Chloroethyl) ether
uglL
50
40.8
82
12-158
bis(2-Chloroisopropyl) ether
ug1L
50
60.7
121
36-166
bis(2-Ethylhexyl)phthalate
uglL
50
53.5
107
8-158
Butyibenzylphthalate
uglL
50
50.7
101
1-152
Chrysene
uglL
50
42-5
85
17-168
Di-n-butylphihalate
uglL
50
53.1
106
1-118
Di-n-octylphthalate
ug1L
50
44.5
89
4.146
Dibelnz(a.h)anthracene
ug1L
50
45.1
90
1-227
Diethylphthalale
ug1L
50
51.5
103
1-114
Dimethylphihalate
uglL
50
49.1
98
1-112
Fluoranihene
uglL
50
46.1
92
26-137
Fluorene
uglL
50
45.6
91
59-121
Hexachloro-1,3-butadiene
uglL
50
29.0
58
24-116
Hexachlorobenzene
uglL
50
39.7
79
1-152
Hexachlorocyciopentadiene
ug/L
50
30.7
61
25-150
Hexachloroethane
uglL
50
29.5
59
40-113
Indeno(1,2,3-cd)pyrene
uglL
50
45.7
91
1-171
Isophorone
ug1L
50
44.9
90
21-196
N-Nitroso-di-n-propylamine
uglL
50
45.9
92
1-230
N-Nitrosodimethylamine
ug1L
50
20.6
41
25-150
N-Nitrosodiphenylamine
uglL
50
38.5
77
25-150
Naphthalene
ug1L
50
33.3
67
21-133
Nitrobenzene
ug1L
50
405
81
35-180
Pentachlorophenot
ugfL
100
80.6
81
14-176
Phenanthrene
ug1L
50
41.6
83
54-120
Phenol
ug1L
50
19.4
39
5-112
Pyrene
ug1L
50
37.4
75
52-115
2,4,6-Tribromophenol (S)
%
85
10-137
2-Fluorobiphenyl (S)
%
80
15-120
2-Fluorophenol(S)
%
42
10-120
Nitrobenzene-d5 (S)
%
83
10-120
Phenol-d6 (S)
%
31
10-120
Terphenyl-614 (S)
%
87
11-131
MATRIX SPIKE SAMPLE:
1739675
92298406001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug1L
NO
50
30.5
61
44-142
2,4,6-Trichlorophenol
uglL
NO
50
40.6
81
37-144
2,4-Dichlorophenol
ug1L
ND
50
35.9
72
1-191
2,4-Dimethylphenot
ug1L
ND
50
37.8
76
32-119
2,4-Dinitrophenot
ug1L
NO
250
171
68
1-181
2,4-Dinitrotoluene
ug1L
ND
50
48.2
96
39-139
Results presented on this page are in the units Indicated by the "Units- column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc.. Page 25 of 40

F
Pace Analytical Services, Inc.
5aceMalXical
9800 KinceyAve. Suite 100
Huntersville, NC 28078
wwwpersfabtmm
(704 )875-9092
QUALITY CONTROL
DATA
Project: STORMWATER
Pace Project No.: 92298406
MATRIX SPIKE SAMPLE:
1739675
92298406001
Spike MS
MS
% Rec.
Parameter
Units
Result
Conc. Result
% Rec.
Limits Qualifiers
2,6-Dinitrototuene
ug/L
NO
50
44.8
90
50-158
2-Chloronaphthalene
ug/L
ND
50
35.1
70
60-118
2-Chlorophenol
ug/L
ND
50
34.3
69
23-134
2-Nitrophenol
ug/L
ND
50
37.0
74
29-182
3,3'-Dichlorobenzidine
ug/L
ND
100
73.7
74
1-262
4,6-Dinitro-2-methylphenol
ug/L
ND
100
88.8
89
1-181
4-Bromophenylphenyl ether
ug/L
ND
50
38.5
77
53-127
4-Chloro-3-methylphenol
ug/L
ND
100
85.1
85
22-147
4-Chlorophenylphenyl ether
ug/L
ND
50
41.2
82
25-158
4-Nitrophenol
ug/L
ND
250
98.0
39
1-132
Acenaphthene
ug/L
NO
50
36.8
74
47-145
Acenaphthylene
ug/L
NO
50
37.8
76
33-145
Anthracene
ug/L
NO
50
38.6
77
1-166
Benzo(a)anthrace ne
ug/L
NO
50
42.2
84
33-143
Benzo(a)pyrene
ug/L
NO
50
37.8
76
17-163
Benzo(b)fluoranthene
ug/L
ND
50
37.1
74
24-159
Benzo(g,h,i)perylene
ug/L
NO
50
39.6
79
1-219
Benzo(k)fluoranihene
ug/L
NO
50
36.6
73
11-162
bis(2-Chloroethoxy)methane
ug/L
NO
50
37.7
75
33-184
bis(2-Chloroethyi) ether
ug/L
NO
50
38.1
76
12-158
bis(2-Chloroisopropyl) ether
ug/L
NO
50
55.7
111
36-166
bis(2-17thylhexyl)phthalate
ug/L
NO
50
56.7
113
8-158
Butylbenzylphthalate
ug/L
NO
50
54.9
110
1-152
Chrysene
ug/L
NO
50
40.7
81
17-168
Di-n-butylphthalate
ug/L
NO
50
51.5
103
1-118
Di-n-octylphthalate
ug/L
NO
50
50.8
102
4-146
Dibenz(a,h)anthracene
ug/L
NO
50
42.1
84
1-227
Diethylphtha late
ug/L
NO
50
48.5
97
1-114
Dimethylphthalate
ug/L
NO
50
45.3
91
1-112
Fiuoranthene
ug/L
NO
50
42A
85
26-137
Fluorene
ug/L
NO
50
41.8
84
59-121
HexacWoro-1,3-butadiene
ug/L
NO
50
28.8
58
24-116
Hexachlorobenzene
ug/L
NO
50
37.2
74
1-152
Hexachlorocyclopentadiene
ug/L
NO
50
32.4
65
25-150
Hexachloroethane
ug/L
NO
50
28.0
56
40-113
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
43.2
86
1-171
Isophorone
ug/L
NO
50
41.6
83
21-196
N-Nitroso-di-n-propylamine
uglL
ND
50
43.5
87
1-230
N-Nitrosodimethyiamine
ug/L
ND
50
20.7
41
25-150
N-Nitrosodiphenylamine
ug/L
NO
50
36.3
73
25-150
Naphthalene
ug/L
NO
50
31.4
63
21-133
Nitrobenzene
ug/L
ND
50
37.1
74
35-180
Pentachloro phenol
ug/L
ND
100
85.8
86
14-176
Phenanthrene
uglL
ND
50
39.0
78
54-120
Phenol
ug/L
NO
50
19.8
40
5-112
Pyrene
ug/L
ND
50
38A
77
52-115
2,4,6-Tribromophenol (S)
%
84
10-137
Results presented on this
page are in the
units indicated by the "Units" column
except where an alternate unit Is
presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 03:53 PM
without the written consent of Pace
Analytical Services,
Inc,.
Page 26 of 40

aceAnalytical
www.pacelaeswm
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9600 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 92298406
MATRIX SPIKE SAMPLE:
1739675
92298406001 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
2-Fluorobiphenyl (S)
%
72
15-120
2-Fluorophenol (S)
%
39
10-120
Nitrobenzene-d5 (S)
%
78
10-120
PhenoW6 (S)
%
31
10-120
Terphenyl-d14 (S)
%
85
11-131
SAMPLE DUPLICATE: 1739676
Parameter
Units
92298406002
Result
Dup
Result
1,2,4-Trichlorobenzene
ugiL
NO
NO
2,4,6-Trichlorophenoi
ugiL
NO
ND
2,4-Dichlarophenol
ugiL
NO
ND
2,4-Dimethylphenol
ugiL
NO
NO
2,4-Dinitrophenol
ug1L
NO
NO
2,4-Dinitrotoluene
ugiL
NO
ND
2,6-Dinitrotoluene
ugiL
NO
NO
2-Chloronaphthalene
ugiL
NO
ND
2-Chlorophenol
ugiL
ND
NO
2-Nitrophenol
ugiL
NO
NO
3,3'-Dichlorobenzidine
ugiL
NO
ND
4,6-Dinitro-2-methylphenol
ugiL
ND
ND
4-Bromophenylphenyl ether
ugiL
ND
ND
4-Chloro-3-methylphenol
ugiL
NO
ND
4-Chlorophenylphenyl ether
ugiL
NO
ND
4-Nitrophenol
ug1L
NO
NO
Acenaphthene
ug1L
ND
ND
Acenaphthylene
ug1L
ND
ND
Anthracene
ugiL
NO
ND
Benzo(a)anthracene
ugiL
ND
NO
Benzo(a)pyrene
ugiL
NO
NO
Benzo(b)fluoranihene
ugiL
NO
ND
Benzo(g,h,i)perylene
ugiL
ND
ND
Benzo(k)fluorenthene
ugiL
NO
NO
bis(2-Chloroethoxy)methane
ugiL
NO
NO
bis(2-Chloroethyl) ether
ugiL
ND
NO
bis(2-Chloroisopropyl) ether
ugiL
NO
ND
bis(2-Ethylhexyl)phihalate
ugiL
ND
NO
Butylbenzylp htha late
ugiL
NO
ND
Chrysene
ugiL
NO
ND
Di-n-butylp hth a late
ugiL
NO
ND
Di-n-octylphthaiate
ugiL
NO
ND
Dibenz(a,h)anthracene
ug1L
NO
ND
Diethylphthalate
ugiL
NO
ND
Dimethylphthalate
ug/L
ND
ND
Fluoranthene
ug1L
NO
NO
RPD Qualifiers
Results presented on this page are in the units Indicated by the "Units' column except where an attemate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc..
Page 27 of 40

aceAnalytical
.
tvwtvpacehlMoom
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92298406
SAMPLE DUPLICATE: 1739676
Parameter
Units
92298406002
Result
Dup
Result
Fluorene
uglL
ND
ND
Hexachloro-1,3-butadiene
uglL
ND
ND
Hexachlorobenzene
uglL
ND
ND
Hexachlorocyclopentadiene
uglL
ND
ND
Hexachloroethane
ug/L
ND
ND
Indeno(1,2,3-cd)pyrene
ug/L
ND
ND
Isophorone
uglL
ND
ND
N-Nitroso-di-n-propylamine
uglL
ND
ND
N-Nitrosodimethylamine
ug/L
ND
ND
N-Nitrosodiphenylamine
uglL
ND
ND
Naphthalene
uglL
N❑
ND
Nitrobenzene
uglL
ND
ND
Pentachlorophenol
uglL
NO
ND
Phenanihrene
ug1L
ND
ND
Phenol
ug1L
ND
N❑
Pyrene
uglL
ND
ND
2,4,6-Tribromophenol (S)
%
74
74
2-Fluorobiphenyl (S)
%
68
69
2-Fluorophenol (S)
%
35
35
Nitroben7ene-d5 (S)
%
72
72
Phenol-d6 (S)
%
26
26
Terphenyl-d14 (S)
%
95
98
RPD Qualifiers
1
2
3
0
1
a
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NO 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in fA,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc..
Page 28 of 40

(�IacleAnalyficale
wwwpacekftccm
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92298406
QC Batch: WET145092 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92298406001, 92298406002, 92298406003
METHOD BLANK: 1739705 Matrix: Water
Associated Lab Samples: 92298406001, 92298406002, 92298406003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 05122l16 14:48
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1739706
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 230 92 90-110
SAMPLE DUPLICATE: 1739707
92298298001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg1L
84.9
65.8 25 D6
SAMPLE DUPLICATE: 1739706
92297976001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
2400
1750 31 D6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc.. Page 29 of 40

aceAnalyticaI
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QUALIFIERS
Projecl7 STORMWATER
Pace Project No.; 92298406
DEFINITIONS
Pace Analytical Services, Inc.
9800 KinceyAve_ Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot,
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values,
LCS(D) - Laboratory Control Sample (Duplicate)
MS(0) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SC - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected,
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SVV845 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C race Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full,
Date: 06/03/2016 03:53 PM without the written consent of Pace Analytical Services, Inc.. Page 30 of 40

f
aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: STORMWATER
Pace Project No.: 92298406
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92298406001
SDO-1
FLDI
92298406002
SDO-2
FLDI
92298406003
SDO-3
FLDI
92298406001
SDO-1
EPA 200.7
MPRPl21786
EPA 200.7
92298406002
SDO-2
EFA200.7
MPRP121786
EPA20U
92298406003
SDO-3
EPA200.7
MPRPl21786
EPA200.7
92298406001
SDO-1
EPA 625
OEXT142708
EPA 625
92298406002
S1)0-2
EPA 625
OEXT142708
EPA625
92298406003
SDO-3
EPA 625
OEXT142708
EPA 625
92298406001
S00-1
EPA 624
MSV136926
92298406002
SDO-2
EPA 624
MSV136926
92298406003
SDO-3
EPA 624
MSVI36926
92298406001
SDO-1
SM 2540D
WET145092
92298406002
SDO-2
SM 2540D
WET145092
92298406003
SDO-3
SM 2540D
WFT145092
Date: 06/03/2016 03:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP119539
ICP/19539
I C PI19539
MSSV112295
MSSV/12295
MSSV112295
Page 31 of 40

Document Name:
Document Revised. -April 25, 2016
CL���IIaIJCc?�
Sample Condition Upon Recei t(SCUR)
Pape 1 of 2
Document No.:
Issuing Authority:
F-CHR-CS-003-rev.19i
Pace Huntersvllie Qu a 11tZ Office
Client Name:
project ri: l`y' y
Courier: ❑Fed Ex ❑UPS ❑LISPS ❑Client
[] Commercial Pace ❑Other:
oonq /9I �w# Q9� F— In .—I 1 Ire nklI v
WO# : 922 8 Y 06
iuiigigiouumnii
Custody Seal Present? []Yes 4No Seals intact? []Yes EINo
Date/Initials Person Examining Contents /
Packing Material: ❑Bubble Wrap (ABubble Bags ❑None [:]Other:
—
Thermometer: T1505 Type-�jf Ice: ,owet []Blue ❑None ❑samples on ice, cooling process has begun
Correction Factor: 0.0'C Cooler Temp Corrected ('C): 4 Biological Tissue Frozen? ❑Yes JZNa ❑N/A
Temp should be above freezing to 6'C
USDA Regulated Soil I �1 /A, water sample)
Did samples. originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (int ationally,
❑Yes ONo Including Hawali and Puerto Rico)? [)Yes ,UNa
Comments/Discrepancy:
Chain of Custody Present?
dyes
ONO
ONJA
1.
Sam ples Arrived within Hold Time?
[''Yes
ON.
N A
2.
Short Hold Time Analysis 02 hr.)?
Yes
No
QNIA
3.
Rush Turn Around Time Re uested7
OYes
E, No
N A
4.
Sufficient Volume?
JjYIS
ONO
N A
5.
Correct Containers used?
,❑Yes
❑No
❑N/A
6.
-Pace Containers Used?
Ejyes
LINO
QYA
Containers Intact?
dyes
ONo.N
A
7.
8. Note If sediment is visible In the dissolved container
Samples Field Filtered? ❑Yes dNo N/A
Sample Labels Match COC?
16yes
❑No
❑N/A
9.
/
-Includes Date/Tlme/ID/Anal sis Matrix:
All containers needing acld/base preservation have been
10.
checked? _ ..
I'ires
❑No
QN/A
All containers needing preservation are found to be In
eaoxs
compliance with EPA recommendation?
Iosc+rlkr
(HNO), H2SO4, HCIQ; NaOH >9 Sulfide, NaOH>12 Cyanide)
❑Yes
❑No
[]N/A
n:vnpwu
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015(water)DOC,LLHg
byes
No
ONJA
NiO1�nO1`"'b'
Samples checked for dechlorination? u
es -`
N/A
11.
Heads ace In VOA Vials >5-6mm ? f rich
[(Ies
Nu
N/A
12.
Trip Blank Present?
❑Yes
No
12No
❑N/A
13.
Trip Blank Custody Seals Present?
❑Yes
❑N/A
Pace Trip Blank Lot q (if purchased).
CLIENT NOTIFICATION/RESOLUTION Field Date Required? []Yes []No
Person Contacted: Date/Time:
Comments/Sample
Discrepancy:
Project Manager SCURF Review: N""�' Data: 5 I a
Project Manager SRF Review: _ Y r LC71 Date: 5-1 1 LLL(L�
Note: Whenever there Is a discrepancy affecting North Carolina co pliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, Incorrect containers)
Page 32 of 40

_ CHAIN -OF -CUSTODY ! Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Regttlrad Client information: Required Project Information: Invoice Information: Page : t Of ,
Company. Norton Door Controls Report To: JIm Zell Attontiorc r *, a 'A l
Address: 30M K 74 East Copy To: Company Namo:
Monroe 14C2a,112
Address:
Emell: ell nortmdoorconuols.com
Purchase Order if:
Paco 4uolo:
Phorm: NONE JFax
Project Nanw Stormwator
Pace P'ojed Manager. rskofe. erowiki'pncalabs.mm,
Requested Duo Dale:
Project#:
Pace Profllo M 4304
. i
'S3Ro
uestid'Anal�..
_Flltwcd
fN
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J
MATRIX cppE
COLLECTED
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Preservatives
r
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Wade Watery W W
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SAMPLE ID 01 OL
is
START
END
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Sampio ids must be unique Ti— rs
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DATE
TIME
DATE
TIME
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REJJNOUIBHED BYIAFFI„�,1ATIpN��y
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:_ACCEP,TED
BY:f
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.SAiIIPLE CONBmONS .: i�,..�' .
Cn le oV\
to pf14-19`lG
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SAMPi:FJi
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§
PRINT Name of SAMPLER
SIGNATURE of SAMPLER:`
11ATE Slgnn
0
a
Cl)
th
a3
m
D.

2 - NCO Labora o '
.
NI
Accurate. Timely. Responsive. Innovative.
4810 Executive Park Court, Suite 111
Jacksonville FL, 32216-6069
Phone: [phone] FAX: [phone]
Friday, June 3, 2016
Pace Analytical (PA007)
Attn: Nicole Gasiorowski
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
RE: Laboratory Results for
Project Number: Stormwater, Project Name/Desc: 92298406
ENCO Workorder(s): BZ02255
Dear Nicole Gasiorowski,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, May 24, 2016.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville.
Data from outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chris Tompkins
Project Manager
Enclosure(s)
Page 34 of 40
FINAL This report relates only to the sample as received by the laboratory, and may onty be reproduced in full. Page 1 of 7

www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SDO-1
Lab ID: 8Z02255-01
Sampled: 05/19/16 10:20
Received: 05/24/16 11:00
Parameter
Hold Date/Timefsl
Prep Date/Time(s]
Analysis Date/Time(s)
EPA 1664E
06/16/16
06/01/16
10:33 06/03/16 12:14
Client ID: SDO-2
Lab ID: BZ02255-02
Sampled: 05/19/16 10:55
Received: 05/24/16 11:00
Parameter
Hold Date/Time(s)
Prep Date/Time(s)
Analysis DatelTime(s)
EPA 16643
06/16/16
06/01/16
10:33 06/03/16 12:14
Client ID: SDO-3
Lab ID: BZ02255-03
Sampled: 05/19/16 10:40
Received: 05/24/16 11:00
Parameter
Holo Da Ti
Pip Date/Time(s)
Analysis Date/Tmefsl
EPA 16648
06/16/16
06/01/16
10:33 06/03/16 12:14
Page 35 of 40
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 7

CC-== U-119199
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID; SDO-1
Lab ID: BZ02255-01
A, nalvte
Results Flag h "D PPOL
Units Math Noted
Oil & Grease (HEM)
1.66 0.622 1.30
mg/L EPA 1664E
Client ID: SDO-2
Lab 1D: BZ02255-02
Anal t
Resin f EfA9 Merl Pal,
units Method Notes
Oil & Grease (HEM)
1.25 .1 0.625 1.30
mq/L EPA 1664E
Client ID: SDO-3 Lab ID: BZ02255-03
Analvte Results Bag MIL PPOL UnItS Method Notes
Oil & Grease (HEM) 1.24 3 0,619 1.29 mg/L EPA 1664B
Page 36 of 40
FINAL This report relates only to the Sample a$ recelved by the laboratory, and may only be reproduced in full. Page 3 of 7

(9 �Go
www.encolabs.com
ANALYTICAL RESULTS
Description: SOO-1 Lab Sample ID:BZ02255-01 Received: 05/24/16 11:00
Matrix: Water Sampled:05f19/16 10:20 Work Order: B202255
Project: 92298406 Sampled By:
Classical Chemistry Parameters
^ - EACO Jacksonw11e cerrX4?d ,7n3We JAC 442]
Artalvte fCAS Number] Results Flaa units DF MDL POL Hatich Method Analyzed By Notes
Oil & Grease (HEM) [C-00071^ 1.66 1 0.259 0.622 1.30 6FO1003 EPA 1664B 06/03116 12:14 SMA
Description: SOO-2 Lab Sample ID:13Z02255-02 Received: 05/24/16 11:00
Matrix: Water Sampled:05119/16 10:55 Work Order: OZO2255
Project: 92298406 Sampled By:
Classical Chemistry Parameters
^ - FAK'olackson.ue C&Vt7ed analyte (AC 442)
lynalvte KAS NUmberl Result
Flaa
YaLl
PE MDL P L
Batch
Oil & Grease (HEM) [C-00071^ 1.25
3
rng/L
0.26 0.625 1.30
6F01003
Description: S©O-3
Lab Sample ID: BZ02255-03
Matrix: Water
Sampled: 05119116 10:40
Project: 92298406
Sampled By:
Classical Chemistry Parameters
^ - EACO Jacksanwlle r&tihed analyte lAC 4421
Analyte fCAS Number] Results
flag
Uni
PEE MdbL PQt
Batch
Oil & Grease (HEM) [C-00071 ^ 1.24
1
mg/L
0.258 0.619 1.29
6F01003
Method Anal Py Notes
EPA 1664E 06/03/16 12:14 SMA
Received: OS124116 11:00
Work Order: OZO2255
Method Anali gy Notes
EPA 1664B 06/03/16 12:14 SMA
Page 37 of 40
FINAL This report relates only to the sample as received by the lalwratory, and may only be reproduced in full. Page 4 of 7

w 6 "Go
www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 5FO1003 - EPA 1664E
Blank (6FO1003-BLKI)
Prepared: 06/01/2016 10:33 Analyzed: 06/03/2016 12:14
Spike Source %REC
RPD
Analyte
Result
Flag
POL
Units
Level Result %REC Limits RPD
LimLt
Notes
Oil & Grease (HEM)
0.613
U
1.28
mg/L
LCS (6FOI003-BSI)
Prepared: 06/01/2016 10:33 Analyzed: 06/03/2016 12:14
Spike Source %REC
RPD
Analyle
Result
Flag
POL
UnAS
Level Resu %REC Limi RPD
9mft
Notes
Oil Grease (HEM)
144
5,00
mg/L
157 92 78-114
LCS Dup (6FO1003-BSD1)
Prepared: 06/01/2016 10:33 Analyzed: 05/03/2016 12:14
Spike Source %REC
RPD
AnaMe
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Oil& Grease (HEM)
147
5.00
mg/L
150 98 78-114 1
18
Matrix Spike (61F01003-MS1)
Prepared: 06/01/2016 10:33 Analyzed: 06/03/2016 12:14
Source:BZ02241-01
Spike Source o/aREC
RPD
.Anatvte
Result
Flau
POL
Units
Level Result %REC Limi RPD
iLmil
Notes
Oil & Grease (HEM)
329
5.00
mg/L
159 183 92 78-114
Page 38 of 40
FINAL This report relates only to the Sample a5 received by the laboratory, and may only be reproduced in Full. Page 5 of 7

F. 1
Q9 �Ge)
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MIL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content,
N The analysis indicates the presence of an analyte for which there is presumptive evidence (8511/o or greater
confidence) to make a "tentative identification".
P Greater than 250% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
Page 39 of 40
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 7

1
Chain of'Custody
Wbikorder:92298406•'' WorkorderName: STORMWATER
Resulls Requested By: 513112016
' Dace Analytical
i .wwpacweas.c«n
RA art 1,InvaicC:To'"' i'� ::...
SutieoniraetTo`ds:+:-. :•
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A;
Nicole Gasiorowski
Pace Analytical Charlotte
�-� P,O. �{ l � T" o
9860 Kin* Me; Suite 100
y
Huntersville,.NC.,28078
� �d EX4{t�hv'e
Phone{704}875-9092
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,Email: nicol6.gasiorowski@pacelahs:cxim
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P.reserved.ConteinerB�Ei
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LAB USE ONLY
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Cooler Temperature -on Receipt
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Custody Seal Y or N Received on Ice r N Sant les.lntac Y r N
tD Thursday, May'19, 2016 &M;k'PM FMT,ALL-C-002rev.00 24M;v Ch2C09
A
0
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it
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Central Files: APS _ SWP
6/1/2016
Permit Number NCG030671
Permit Tracking Slip
Program Category
Status Project Type
NPDES SW
In review New Project
Permit type
Version Permit Classification
Metal Fabrication Stormwater Discharge COC
RECEIVED
COC
Primary Reviewer
JUN 0 2 Zu1t}
Permit Contact Affiliation
rick.riddle
CENTRAL FILES
Coastal SWRule
D,NIR SECTION
Permitted Flow
Facility
Facility Name
MajorlMinar
Region
Prince Manufacturing
Minor
Asheville
Location Address
County
209 Broad Pointe Dr
Henderson
Facility Contact Affiliation
Mills River NC 28759
Amanda Medlock
209 Broad Pointe Dr
Owner
Mills River
NC 28759
Owner Name
Owner Type
Prince Manufacturing
Nan -Government
Owner Affiliation
Amanda Medlock
209 Broad Pointe Dr
Dates/Events Mills River NC 28759
Scheduled
Orig Issue App Received Draft Initiated Issuance Public Notice Issue Effective Expiration
4/19/2016
Regulated Activities Requested /Received Events _
Metal products manufacture RO staff report received 5/31/16
RO staff report requested 4127116
Outfall 1
Waterbody Name Streamindex Number Current Class Subbasin
McDowell Creek 6-58 C 04-03-02

Energy, Mineral
and Land Resources
FNVIQQNMSENTAL QUALITY
Amanda Medlock
Prince Manufacturing
209 Broad Pointe Drive
Mills River, NC 28759
Dear Mrs. Medlock:
PAT MCCRORY
Go, e""K
DONALD R. VAN DER VAART
Svc/ ernr}
May 31, 2016 TRACY DAVIS
1 ti+irrnr
Subject: General Permit No. NCG030000
Prince Manufacturing
COC NCG030671
Henderson County
In accordance with your application for a discharge permit received on April 19, 2016, we are forwarding
herewith the subject certificate of coverage to discharge under the subject state — NPDES general permit.
This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated
October 15, 2007 (or as subsequently amended).
Please take notice that this certificate of coverage is not transferable except after notice to the Division of
Energy, Mineral, and Land Resources. The Division may require modification or revocation and
reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Energy, Mining, and Land Resources, or permits required by the Division of Water
Resources, Coastal Area Management Act, or any other federal or local governmental permit that may be
required.
If you have any questions concerning this permit, please contact Richard Riddle at telephone number
[phone].
Sincerely,
for Tracy E. Davis, P.E., CPM, Director
Division of Energy, Mineral and
Land Resources
cc: Asheville Regional Office
Central Files
Stormwater Permitting Files
State of North Carolina I Environmental Quality I Energy. Mineral and [and Resourm
1612 Mail Service Center 1 512 North Saiisbury Street I Raleigh. NC 27699-1612
919 707 9200 T

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030671
STORMWA'I'ER DISCHARGES
NATIONAL POLLUTANT I)ISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-21 5.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Prince Manufacturing
is hereby authorized to discharge stormwater from a facility located at
Prince Manufacturing
209 Broad Pointe Drive
Mills River
Henderson County
to receiving waters designated as McDowell Creek, a class C water in the French Broad River
Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions
set forth in Parts I, I1, III, and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective May 31, 2016.
'Phis Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day May 31, 2016.
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission

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NCG030671
N
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Map Scale 1: 24, 000
Latitude: 350 25' 8.8" N
Longitude: -820 33' 3.3" W
County: Henderson
Receiving Stream: McDowell Creek
Stream Class: C
Index Number: 6-58 (French Broad River Basin)
I
Facility Location

TWA
RCDENR
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NOTICE OF INTENT
Division of Energy, Mineral and Land Resources
Land Quality Section
National Pollutant Discharge Elimination System
NCG030000
Date Received
Year M, f)av
National Pollutant Discharge Elimination System application for coverage under General Permit
NCG030000:
STORMWATER DISCHARGES associated with activities classified as:
to
SIC (Standard Industrial Classification) 335 Rolling, Drawing, and Extruding of Nonferrous Metals
SIC 3398 Metal Heat Treating
SIC 34 Fabricated Metal Products p RECEIVED
SIC 35 Industrial and Commercial Machinery
SIC 36 Electronic and Other Electrical Equipment APR 19 2016
SIC 37 Transportation Equipment
SIC 38 Measuring, Analyzing, and Controlling Instruments DENR_LAND QUALITY
STORMWATER PERMITTING
For questions, please contact the DEMLR Regional Office for your area. See page 4.
(Please print or type)
1) Mailing address of ownerloperator
Name V9, kt1LE
Street Address _at.Q qWZ"Q -'> pQ knm 'Z>R
City M \ ILLS R\ J_V-- (L State N L
Telephone No. 9,-LB _ (2 ��1 R 8 60 - -_ - Fax: 'sue$
2) Location of facility producing discharge:
Facility Name i al e C AA 4 e. ar;r1
Facility Contact o
Street Address I Areackr6i^-te- i'
city IN It S Xiver State
County tnderscA
Telephone No. ?XZ i_ W 1 060 Fax:
Email OLIAtAldidw,012C�Icr nnaayc-'a&rrr1nj•dbr
3) Physical Location Information:
ZIP Code a87
f -7 1 , 1'7 '2 7
ZIP Code
Please provide a narrative description of how to get to the facilityuse street names, state road numbers, and
distance and direction from a roadway intersection). 0-po t G V �� � 41 +Wr, a^'�o
I�ratakC6+mot+ 'Dr _-Qntii++&A ;% lk dKi1-e c•. -K,.
(A copy of a county map or USGS g�1ua�dd sheet with the facility clearly located must .)
be submitted with this application
4) Latitude z o 3 3' J- �7 Longitude ��aS'b • YW'� (deg, min, sec)
�5,q�q3q0f
-81,_u1Q-3(
Page 1 of 4
SWU-21"71408 Last revised 7/2/14

UCG030000 N.o, l_
5) This NPDES Permit Application applies to which of the following:
❑ New or Proposed Facility Date operation is to begin
W Existing
61 Standard' industrial Classification:
Provide the 4-digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial
activity at this facility.
SIC Code:
7). Provide a brief narrative description. of the types of Industrial.acdvittes and products manufactured at
this facility: Qv ;1 C��:.n� , �� t-n4 �nG Q�l� .�1 c�w W c _\;\ � CLC�- C C) C,A su C
r-)V- Me QA P^� ��c S. ass�n-� C�l� ��T 51 PP i rKie 4A t - o�uu ..
8) Discharge points I Receiving waters:
How many discharge points (ditches, pipes, channels, etc.) convey stormwater from the property? ��L,�
What is the name of the body or bodies of water (creek, stream, river, lake, etc.) that the faoi'Iity stormwater
discharges end up in? k\N e � %lo e—
Receiving water classification: C _-- - -- - -- - Is this a-303(d}listed stream? N D Has a-TMDL been approved for this watershed? S
If the site stormwater discharges to a separate storm sewer system, name the operator of the separate storm
sewer system (e.g. City of Raleigh municipal storm sewer). /v IA
9) Does this facility have any other NPDES permits?
% No
❑ Yes
if yes, list the permit numbers for all current NPDES permits for this facility.
10) Does this facility have any Non -Discharge permits (ex: recycle permit)?
(9 No
❑ Yes
If yes, list the permit numbers for all current Nora -Discharge permits for this facility:
11) Does this facility employ any best management practices for stormwater control?
❑ No
LK Yes (Show any structural BMPs on the site diagram.)
0 Yes. please briefly describe: i~ i -oQ fYl
C\ 4 --\\C, C' C"I � CA (,Y-\ L-D 0, -V�Q rv-t -r k E, ick 2- G• L 01
12) Does this facility have a Stormwater Pollution Prevention Plan?
❑ No
®. Yes
If yes, when was it Implemented? Opt
13) Are vehicle maintenance activities occurring at this facility?
iR No ❑ Yes
14) Hazardous Waste:
a) Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facllit}f?
N No ❑ Yes
Page 2 of 4
S W U-21 "71408 Last revised 7014

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NCG030000 N.O.I.
b) Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste generated per month) of
hazardous waste?
U No ❑ Yes
c) Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste generated per Month) of
hazardous waste?
ID No ❑ Yes
d) Is hazardous waste stored in the 100-year flood plain?
R No ❑ Yes If yes, include information to demonstrate protection from flooding.
e) If you answered yes to questions b. or c., please provide the following information:
Type(s) of waste:
How is material stored:
Where is material stored:
How_ many disposal shipments per year:
Name of transport I disposal vendor:
Vendor address:
15) Certification -
North Carolina General Statute 143-215.6E (i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record, report,
plan, or other document filed or required to be maintained under this Article or a rule implementing this Article; or who
knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or
who falsifies, tampers with,.or knowingly renders inaccurate any recording or monitoring device or method required to he
operated or maintained under this Article or rules of the Commission implementing this Article shall be guilty of a Glass 2
misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000).
I hereby request coverage under the referenced General Permit. I understand that coverage under this permit
will constitute the permit requirements for the discharge(s) and is enforceable in the same manner as an
individual permit.
I certify that I am familiar with the information contained in this application and that to the best of my
knowledge and belief such information is true, complete, and accurate.
Printed Name of Person Signing:�Pc�� 4�
Title: STDya L_f"> E lZ
of Applicant)
(Date Signed)
This Notice of Intent must be accompanied. by a check or money order for $100.00, made payable tot
NCDENR
Page 3 of 4
SWU-218-071408 Last revised 712/14

NCG030000 N.O.I.
Final Checklist
This application will be returned as incomplete unless all of the following items have been included:
® Check for $100 made payable to NCDENR.
N This completed application and all supporting documents.
® A site diagram showing, at a minimum, (existing or proposed):
(a) outline of drainage areas, (b) stormwater management structures, (c) location of stormwater outfalls
corresponding to the drainage areas, (d) runoff conveyance features, (e) areas where materialsare. stored,.
(f) impervious areas, (g) site property lines.
® Copy of county map or USGS quad sheet with the location of the facility clearly marked on the map.
Mail the entire package to:
Stormwater Permitting Unit Program
Division of Energy, Mineral and land Resources
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Note
The submission of this document does not guarantee coverage under the General Permit.
For questions, please contact the DEMLR Regional Office for your area.
DEMLR Regional Office Contact Information:
Asheville Office ...... [phone]
Fayetteville Office
... [phone]
Mooresville Office
... [phone]
Raleigh Office ........
[phone]
Washington Office
-._(252) 946-6481
Wilmington Office ... [phone]
Winston-Salem ......
[phone]
Central Office .........(919)
807-6300
Page 4 of 4
5WU-21"71408 Last revised 712114

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Energy, Mineral
and Lane! Resources
£N V1P0NMEt4TAL QUALITY
Amanda Medlock
Prince Manufacturing
209 Broad Pointe Drive
Mills River, NC 28759
Dear Mrs. Medloek:
Mav 31, 2016
PAT MCCRORY
Gawrylor
DONAI-D R. VAN DER VAART
.S'ecrrars
TRACY DAVIS
Director
Subject: General Permit No. NCG030000
Prince Manufacturing
COC NCG030671
Henderson County
1n accordance with your application for a discharge perinit received on April 19, 2016, we are forwarding
herewith the subject certificate of coverage to discharge under the subject state —NPDES general permit.
This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated
October 15, 2007 (or as subsequently amended).
Please take notice that this certificate of coverage is not transferable except after notice to the Division of
Energy, Mineral, and Land Resources. The Division may require modification or revocation and
reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Energy, Mining, and Land Resources, or permits required by the Division of Water
Resources, Coastal Area Management Act, or any other federal or local governmental permit that may be
required.
If you have any questions concerning this permit, please contact Richard Riddle at telephone number
[phone],
Sincerely,
ORIGINAL SIGNED M
KEN PICKLE
for Tracy E. Davis, P,EE., CPM, Director
Division of Energy, Mineral and
Land Resources
ec: Asheville Regional Office
Central Files
Stormwater Permitting Files
State of North Carolina I Environmental Quality �Energy, Mineral and Land Resources
1612 Mail Service Center 1 512 North Salisbury Street I Raleigh, INC 27699.1612
919 707 9200 T

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030671
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Prince Manufacturing
is hereby authorized to discharge stormwater from a facility located at
Prince Manufacturing
209 Broad Pointe Drive
Mills River
Henderson County
to receiving waters designated as McDowell Creek, a class C water in the French Broad River
Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions
set forth in Parts 1, 11, III, and IV of General Permit No. NCG0')0000 as attached..
['his certificate of coverage shall become effective May 31, 2016.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day May 31, 2016.
ORIG NAL SIGNED W
KEN PICKLE
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission

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NCG030671
N
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S
Map Scale 1: 24, 000
Prince Manufacturing
Latitude: 3511 25' 8.8" N
Longitude: -821 33' 3.3" W
County: Henderson
Receiving Stream: McDowell Creek
Stream Class: C
Index Number: 6-58 (French Broad River Basin)
Facility Location

(9. 47A)
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(5. 9A)
(10, 34A)
236
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711 s
e
is
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-�.
5 Printed:Apr 07, 2016
WARNING: THIS is NOT A SURVEY. All information or data provided (whether subscribed, purchased or otherwise distributed) Is provided as is
without any warranties, including the warranties of merchantability or of fitness for a particular purpose. Henderson County and its employees
make no warranties or guarantees, either express or Imptled. Use of the Information or data subscribed, purchased or otherwise distributed,

ck
Av }
9 Broadpointe DGRM'�'AA�� PERMt
S Printed. -Apr 07, 2016
WARNING.' TEAS IS NOT A SURVEY. All I forrrration ar data presvided {WnMer subscribed, purerMsed or Marwlga dlstribu OM is prov Od as
is, without any warranties, including the warranties of merchantability or of fitness for a particular purpose. Henderson County and Its
employees make no warranties or guarantees, either express or implied. Use of the Information or data subscribed, purchased or otherwise

PA'I MCCRORY
Goremor
DONALD R. VAN DER VAART
Secrerary
Energy, Mineral
and Land Resources TRACY DAVIS
ENVIRONMENTAL QUALITY May 3 1 . 201 6
Uireeror
Amanda Medlock
Prince Manufacturing
209 Broad Pointe Drive
Mills River, NC 28759
Subject: General Permit No. NCG030000
Prince Manufacturing
COC NCG030671
Henderson County
Dear Mrs. Mcdlock:
In accordance with your application for a discharge permit received on April 19, 2016.. we are forwarding
herewith the subject certificate of coverage to discharge under the subject state — NPDES general permit.
This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the
Memorandum of'Agreement between North Carolina and the US Environmental Protection Agency dated
October 15, 2007 (or as subsequently amended).
Please take notice that this certificate of coverage is not transferable except after notice to the Division of
Energy, Mineral, and Land Resources. The Division may require modification or revocation and
reissuance of the certificate of coverage.
"['his permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Energy, Mining, and Land Resources, or permits required by the Division of Water
Resources, Coastal Area Management Act; or any other federal or local governmental permit that may be
required.
If you have any questions concerning this permit, please contact Richard Riddle at telephone number
[phone].
Sincerely,
0RiG1W SIGNED M
KEN PICKLE
for Tracy E. Davis, P.L., CPM, Director
Division of Energy, Mineral and
Land Resources
cc: Asheville Regional Office
Central Files
Stormwater Permitting Files Rece1v d
JUN
Land Quality Section
Stale of North Carolina I Environmental Quality I Energy, Mincrai and Land Resources Asheville
1617 Mail Scrvice Center 1 512 Noah Salisbury Street Raleigh, NC 27699-1612
919 707 9200 T

`i.
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030671
STORMWA'f ER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended;
Prince Manufacturing
is hereby authorized to discharge stormwater from a facility located at
Prince Manufacturing
209 Broad Pointe Drive
Mills River
Henderson County
to receiving waters designated as McDowell Creek, a class C water in the French Broad River
Basin; in accordance with the effluent limitations, monitoring requirements, and other conditions
set forth in Parts I. II, III, and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective May 31, 2016,
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day May 31, 2016,
ORIGINAL SIGNED W
KEN PICKLE
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission
' A$,

NCG030671 11 Prince Manufacturing 1
Latitude: 350 25' 8.8" N
Longitude: -820 33' 3.3" W
County: Henderson
Receiving Stream: McDowell Creek
Stream Class: C
Index Number: 6-58 (French Broad River Basin)
rz,1r ► ► r.. �
Map Scale 1:24, 000
Facility Location

-- j "'
NCD=mR
E"���Ka�R —
NOTICE aF INTENT
Division of Energy, Mineral and Land Resources
Land Quality Section
National Pollutant Discharge Elimination System
NCG03000O
Year
of
e
National Pollutant Discharge Elimination System application for coverage under General Permit
NCG030000:
STORMWATER DISCHARGES associated with activities classified as:
SIC (Standard Industrial Classtfication) 335 Rolling, Drawing, and Extruding of Nonferrous Metals
SIC 3398 Metal Heat Treating
SIC 34 Fabricated Metal Products
SIC 36 Industrial and Commercial Machinery
SIC 36 Electronic and Other Electrical Equipment APR 19 2016
SIC 37 Transportation Equipment
SIC 38 Measuring, Anatyzing, and Controtling Instruments DENR_LA;MD QUALITY
;TORMiWATER PER,�,!TTIIvG
For Questions, please contact the DEIWL.R Regional Office for your area. See page 4-
(Please print or type)
1) Mailing address of ownedoperator (address to which all permit correspondence will be mailed):
Name ?sq tr, M AiJ J F LTv z�N G C C'� maw �bC.`C�
Street Address 9,0 Ct 97'0A�> PO kc1TE CAR
city
Telephone No.
M R.\J etL State N C- ZIP Code ;t8-7Scf
SIS 1 ` 60 Fax: ?,'19 (.8 % 1, 'A.
2) Location of facility producing discharge:
Facility Name t'(e{ACt
>=ae ttty Contact
Street Address
City
County
Telephone No_
Email
3) Physical Location Information:
Please provide a narrative description of how to get to the
distance and direction from a roadway intersectim). C}
State AI L' ZIP Code
Fax: T i
l� 1
',l &V4 Al -00-
names, state road num
n PLY q iwn ow
, and
(A copy of a county map or USGS quad sheet with the facility deafly located must be submitted with this appk2tion.)
4) Wtft d ?� ° 33 " 1- N Longitude 7rod5',!rYW (del,, min, sec)
Page 1 of 4
SWU-218-071408 Last revised 7f2l14

NCGO30000 N_O.L
5) This NPDES Permit Appticatlon applies to which of the foilowing:
❑ New or Proposed i=ac::Tdy
W Existing
gj Standardlndostriaf Ciassificxffon:
Date operation is to begin
Provide the 4-digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial
activity at this facility.
SIC Code: 2- y
7). Provide a- brief narrative descriptionof the types of Industrial.activities and products tnanuiaduredat
this facility: Yu3g,\�,c\2� , 5A-c—t--R ,S ._, m.,-\ o� U_-'C_ � 0.( C C) G-A k. Iy C
2t 0.
d) Discharge points 1 Recetirttmg waters:
c L, o5u re_S
How many discharge points (ditches, pipes, Channels, etc-) convey stormwater from the property? —.1 —
What is -Ow name of the body ar bodies of water (creep, stream, river, lake, etc.) that the facilitystormwater
discharges end up in? M c .o ou f L(__ _Q �t� L 6 - S8�
Receiving water classification_ C.
Is this a 303(d) listed stream? N 0 Ha&a-TMDL bey approved for this watershed-?
If the site stormwater discharges to a separate storm sewer system, name the operator of the separate storm
sewer system (e.g. City of Raleigh municipal storm sewer). N I A
8) Does this facility have any other NPDES permits?
% No
0 Yes
if yes, list the permit numbers for all current NPDES permits for this facility.
10) Does this facility have any Non -Discharge permits (ex: recycle permit)?
1$ No
❑ Yes
If yes, fist the permit numbers for all current Non -Discharge permits far this facility:
11) Does this facility employ any best rnanagem nt practices for stormwater control?
11 No
09 Yes (Show any. structural BMPs on the site diagram.)
it yes, please briefly describe: s \ "-)V-dL CY 0F S ; oQ f}
SEt,\MrG/JC &)SONS --
12) Does this facility have a Stormwater Pollution Prevention Plan?
❑ No
tK Yes
If yes, when was it Implemented? _aouu _
13) Are vehicle maintenance activities occurring at this facility?
M No ❑ Yes
14) Hazardous Waste:
a) Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility?
0 No ❑ Yes
Page 2 of 4
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NCG030000 N.O.J.
b) Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste generated per month) of
hazardous waste?
U No ❑ Yes
c) Is this facility a Large Quantity Gererator (1000 kg, or more of hazardous waste generated per month) of
hazardous waste?
® No ❑ Yes
d) Is hazardous waste stored in the 100-year flood plain?
P No ❑ Yes If yes, include information to demonstrate protection from flooding.
e) If you answered yes to questions b. or c., please provide the following information-
Type(s) of waste:
How is material stored: _
Where is material stored:
How many disposal shipments per year:.
Name of transport / disposal vendor:
Vendor address:
15) Certification:
North Carolina General Statute 143-215.6B (i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record, report,
plan, or other document Bled or required to be maintained under this Article or a rule implementing this Article; or who
knowingly mattes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or
who falsifies,tampers with,or knowingly renders inaccurate any recording or monitoring device or method required to be
operated or maintained under this Article or rules of the Commission implementing this Article shall be guilty of a Class 2
misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000).
I hereby request coverage under the referenced General Permit. I understand that coverage under this permit
will constitute the permit requirements for the discharge(s) and is enforceable in the same manner as an
individual permit.
I certify that I am familiar with the information contained in this application and that to the best of my
knowledge and belief such information is true, complete, and accurate.
Printed Name of Person Signing:
Title: —
A---�-- ')� k'J—g Is 12 al
(Signature of Applicant) (Date Signed)
This Notice of Intent must be accompanied by a check or money order for $100.00, made payable to:
NCDENR
Page 3 of 4
S W U-218-071408
Last revised 7014

NCG030000 N.O.I.
Final Checklist
This application will'be returned as incomplete unless all -of the following items have been included:
® Check for $100 made payable to NCDENR.
N This completed application and all. supporting. documents.
® A site diagram showing, at a minimum, (existing or proposed):
(a) outline of drainage areas, (b) stormwater management structures, (c) location of stormwater outfalls
corresponding to the drainage areas, (d) runoff conveyance features, (e) areas where materials are stored,.
(f) impervious areas, (g) site property lines.
® Copy of county map or USGS quad sheet with the location of the facility clearly marked on the map.
Mail the entire package to:
Storrnwater Permitting Unit Program
Division of.Energy,.Mineral and Land Resources
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Note
The submission of this document does not guarantee coverage under the General Permit.
For questions, please contact the DEMLR Regional Office for your area.
DEMLR Regional Office Contact Information:
Asheville Office ......
[phone]
Fayetteville Office...
[phone]
Mooresville Office ...
[phone]
Raleigh Office ........
[phone]
Washington Office ...[phone]
Wilmington Office ...
[phone]
Winston-Salem ......
[phone]
Central Office .........(919)
807-6300
Page 4 of 4
SWU-21"71408 Last revised 712114

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PRINCE MANUFACTURING
209 BROADPOINTE DR
MILLS RIVER, NC 28759.4WS
66-211530 10366
j 2004550016917
DATE
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