HomeMy WebLinkAboutNCG030644_COMPLETE FILE - HISTORICAL_20181025STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
Iv L& C6o Lo 4
DOC TYPE
C' HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ a 04 I 0 a'6
YYYYM M DD
ROY COOPER NORTH CAROLINA
Governor Environmental Quality
MICHAEL S. REGAN
Secretary
WILLIAM E. (TOBY) ViNSON, JR.
Interim Director
October 25, 2018
Meritor, Inc.
Attention: Marc Houston
105 Wamsutta Mill Road
Morganton, North Carolina 28655
Subject: Compliance Evaluation Inspection
Permit: NCG030644
Burke County, North Carolina
Dear Mr. Houston:
Enclosed please find a copy of the Compliance Evaluation Inspection Report for the
inspection I conducted at the subject facility on October 9, 2018.
The report should be self-explanatory; however, should you have any questions
concerning this report, please do not hesitate to contact me at (828) 296-4500 or by email
at Isaiah.reed@ncdenr.gov.
Sincere ,
Isaiah Reed, CEPSCI, MS4 L"I/
Environmental Specialist
Land Quality Section
Enclosure: Inspection Report
North Carolina Department of Environmental Quality I Division of Energy, Mineral and Land Resources
Asheville Regional Office 1 2090 U.S. Highway 70 1 Swannanoa. North Carolina 28778
828,296.4500
Compliance Inspection Report
Permit: NCG030644 Effective; 11/16/17 Expiration: 10/31/18 Owner: Meritor Heavy Vehicle Systems LLC
SOC: Effective: Expiration: Facility: Meritor Heavy Vehicle Systems, LLC
County: Burke 105 Wamsutta Mill Rd
Region: Asheville
Morganton NC 28655
Contact Person: Jason Huskey Title: Phone: 828-764-4629
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 10/0912018
Primary Inspector: Isaiah L Reed
Secondary Inspector(s):
Certification:
Phone:
Entry Time: 02:45PM Exit Time: 04:OOPM
Phone: 828-296-4614
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Metal Fabrication Stormwater Discharge COC
Facility Status: ® Compliant ❑ Not Compliant
Question Areas:
® Storm Water
(See attachment Summary)
Page: 1
Permit: NCGO30644 Owner - Facility: Meritor Heavy Vehicle Systems LLC
Inspection Date: 1010912018 Inspection Type : Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
On October 9, 2018 this facility was inspected for compliance. I met with Mark Houston during the inspection. No issues
were observed, but the following should be considered moving forward.
1) The water discharging from outfall 2 appeared to have some possible foaming near the discharge. This shall be evaluated
by the permitee, as required by the general permit.
2) While the facility is not currently in Tier 2, investigative measure should begin immediately to evaluate the cause of the las
sample being over benchmark.
If you have any questions, please contact this office at 828-296-4614
Page: 2
Pormit• NCGO30644 Owner - Facility: Meritor Heavy Vehicle Systems LLC
Inspection Date: 10/0912018 Inspection Type : Compliance Evaluation Reason for Visit: Routine
Stormwater Pollution Prevention Plan
Yes No NA NE
Does the site have a Stormwater Pollution Prevention Plan?
IN ❑ ❑ ❑
# Does the Plan include a General Location (USGS) map?
® -❑ ❑ ❑
# Does the Plan include a "Narrative Description of Practices"?
®❑ ❑ ❑
# Does the Plan include a detailed site map including outfall locations and drainage areas?
® ❑ ❑ ❑
# Does the Plan include a list of significant spills occurring during the past 3 years?
®❑ ❑ ❑
# Has the facility evaluated feasible alternatives to current practices?
®❑ ❑ ❑
# Does the facility provide all necessary secondary containment?
®❑ ❑ ❑
# Does the Plan include a BMP summary?
® ❑ ❑ ❑
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
® ❑ ❑ ❑
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
® ❑ ❑ ❑
# Does the facility provide and document Employee Training?
®❑ ❑ ❑
# Does the Plan include a list of Responsible Party(s)?
®❑ ❑ ❑
# Is the Plan reviewed and updated annually?
®❑ ❑ ❑
# Does the Plan include a Stormwater Facility Inspection Program?
®❑ ❑ ❑
Has the Stormwater Pollution Prevention Plan been implemented?
®❑ ❑ ❑
Comment:
Qualitative Monitoring
Yes No NA NE
Has the facility conducted its Qualitative Monitoring semi-annually? ® ❑ ❑ ❑
Comment:
Analytical Monitoring Yes No NA NE
Has the facility conducted its Analytical monitoring? ®❑ ❑ ❑
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ ® ❑
Comment:
Permit and Outfalls Yes No NA NE
# Is a copy of the Permit and the Certificate of Coverage available at the site? ®❑ ❑ ❑
# Were all outfalls observed during the inspection? ®❑ ❑ ❑
# If the facility has representative outfall status, is it properly documented by the Division? 110 ® ❑
# Has the facility evaluated all illicit (non stormwater) discharges? ❑ ❑ ❑
Comment:
Page: 3
Compliance Inspection Report
Permit: NCG030644 Effective: 11/16/17 Expiration: 10/31/18 Owner: Meritor Heavy Vehicle Systems LLC
SOC: Effective: Expiration: Facility: Meritor Heavy Vehicle Systems, LLC
County: Burke 105 Wamsutta Mill Rd
Region: Asheville
Morganton NC 28655
Contact Person: Jason Huskey Title: Phone: 828-764-4629
Directions to Facility:
System Classifications:
Primary ORC: Certification: Phone:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 1010912018 Entry Time: 02:45PM Exit Time: 04:00PM
Primary Inspector: Isaiah L Reed Phone: 828-296-4614
Secondary Inspector(s):
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Metal Fabrication Stormwater Discharge COC
Facility Status: Compliant Not Compliant
Question Areas:
Storm Water
(See attachment summary)
Page: 1
Permit: NOG030644 Owner - Facility: Mentor Heavy Vehicle Systems LLC
Inspection Date: 10/0912018 Inspection Type : Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
On October 9, 2018 this facility was inspected for compliance. I met with Mark Houston during the inspection. No issues
were observed, but the following should be considered moving forward.
1) The water discharging from outfall 2 appeared to have some possible foaming near the discharge. This shall be evaluated
by the permitee, as required by the general permit.
2) While the facility is not currently in Tier 2, investigative measure should begin immediately to evaluate the cause of the las
sample being over benchmark.
If you have any questions, please contact this office at 828-296-4614
Page: 2
Permit: NCGO30644 Owner - Facility: Meritor Heavy Vehicle Systems LLC
Inspection pate: 10/09/2018 Inspection Type : Compliance Evaluation Reason for Visit: Routine
Stormwater Pollution Prevention Plan
Yes No NA NE
Does the site have a Stormwater Pollution Prevention Plan?
0 ❑ ❑ ❑
# Does the Plan include a General Location (USGS) map?
0 ❑ ❑ ❑
# Does the Plan include a "Narrative Description of Practices"?
■ ❑ ❑ ❑
# Does the Plan include a detailed site map including outfall locations and drainage areas?
■ ❑ ❑ ❑
# Does the Plan include a list of significant spills occurring during the past 3 years?
M ❑ ❑ ❑
# Has the facility evaluated feasible alternatives to current practices?
M ❑ ❑ ❑
# Does the facility provide all necessary secondary containment?
i ❑ ❑ ❑
# Does the Plan include a BMP summary?
M ❑ ❑ ❑
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
M ❑ ❑ ❑
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
0 ❑ ❑ ❑
# Does the facility provide and document Employee Training?
0 ❑ ❑ ❑
# Does the Plan include a list of Responsible Party(s)?
0 ❑ ❑ ❑
# Is the Plan reviewed and updated annually?
0 ❑ ❑ ❑
# Does the Plan include a Stormwater Facility Inspection Program?
❑ ❑ ❑
Has the Stormwater Pollution Prevention Plan been implemented?
❑ ❑ ❑
Comment:
Qualitative Monitoring Yes No NA NE
Has the facility conducted its Qualitative Monitoring semi-annually? 0 ❑ ❑ ❑
Comment:
Analytical Monitoring Yes No NA NE
Has the facility conducted its Analytical monitoring? ME][--][]
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ 0 ❑
Comment:
Permit and Outfalls
Yes No NA NE
# Is a copy of the Permit and the Certificate of Coverage available at the site? 0 ❑ ❑ ❑
# Were all outfalis observed during the inspection? 0 ❑ ❑ ❑
# If the facility has representative outfall status, is it properly documented by the Division? ❑ ❑ ■ ❑
# Has the facility evaluated all illicit (non stormwater) discharges? ❑ ❑ ❑
Comment:
Page: 3
A SjSjIfo
NCDENR
NC - URo— DEP THE G
EN�nnan-- NQunu. RcSa m—
Division of Energy, Mineral & Land Resources
Land Quality SectionlStormwater Permitting
National Pollutant Discharge Elimirlatioti System
PERMIT NAME/OWNERSHIP CHANGE FORM
FOR AGENCY USE ONLY
Date Received
Year
Month
Day
1. Please enter the permit number for which the change is requested.
NPDI S Permit (or) Certificate of Coverage
IV 0 S 0 3 10 0 0 0 N G 0 1 3 10 6 4 4
II. Permit status prior to requested change.
a. Pennit issued to (company name): Meritor Heavy Vehicle Systems, LLC
b. Person legally responsible for permit: Paul A Ingle
First M I Last
PCCE1 ir1
LJ
FtU 25
�D16
A����'�1'r771'Z
Site Mar
Title
105 Warnsutta Mill Road
Permit Holder Mailing Address
Morganton NC 28655
City State Zip
(828) 764-4789 (828) 439-8463
Phone Fax
c. Facility name (discharge): Meritor Heavy Vehicle Systems, LLC
d. Facility address: 105 Warnsutta Mill Road
Address
Morganton NC 28655
City State Zip
c. Facility contact person: j—C=lltay-Roliinson-_ _ ^(828)_764�.4644_
First / MI / Last Phone
I11. Please provide the following for the requested change (revised permit).
a. Request for change is a result of: ❑ Change in ownership of the facility
® Name change of the facility or owner
If other please explain:
b. Permit issued to (company namc):
Meritor Heavy Vehicle Systems, LLCy
c. Person legally responsible for permit:
Paul A Ingle
First MI Last
Site Manager
Title
105 Warnsutta Mill Road
Permit Holder Mailing Address
Morganton NC 28655
City State Zip
(828) 764-4789 paul.ingle Canieritoncom
I'hnne E-mail Address
d. Facility name (discharge):
Meritor 1-leavy Vehicle Systems, LLC
e. Facility address:
105 Warnsutta Mill Road
Address
Morganton NC 28655
City State Zip
f. Facility contact person:
Jason Huskey
First MI Last
(828) 764-4629 jason.liuskeyatneritor.com
Phone E-mail Address
IV. Permit contact information (if different from the person legally responsible for the pennit)
Revised Jan, 27, 2014
NPDES PERMIT NAME/OWNERSHIP CHANGE FORM
• Page 2 of 2
Permit contact: Jason Fluskey
First M 1 Last
Supervisor, Isnvironnicnt Health And Safety
Title
105 Wamsutta Mill Road
Mailing Address
Morganton NC 28655
City State Zip
(828) 764-4629 jason.huskey a meritor.cotn
Phone E-mail Address
V.
Will the permitted facility continue to conduct the same industrial activities conducted prior
to this ownership or name change?
® Yes
❑ No (please explain)
V1 Required Items: TIIIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a hill of sale) is required for an ownership change request. Articles of incorporation are
not sufficient for an ownership change.
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Certification is sufficient.
PERMIT"TEE CERTIFICATION (Permit holder prior to ownership change):
1, Paul A Ingyle, attest that this application for a name/ownership change has been reviewed and is accurate
and complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned as incomplete.
Q February- 9, 2016
Signature Date
APPLICANT CERTIFICATION
1, Paul A Ingle, attest that this application for a name/ownership change has been reviewed and is accurate
and complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting inforniation is not included, this application package will be
returned as incomplete.
February 9, 2016
Signature Date
PLEASE SEND'141E COMPLETE APPLICATION PACKAGE TO:
Division of Energy, Mineral and Land Resources
Storrnwater Pernitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Revised Jan 27, 2014
?� MERITOR
February 9, 2016
RE: Signatory Authority for NPDES Permits, Applications, and Reports
Note to File:
Meritor, Heavy Vehicle Systems, LLC.
105 Wamsutta Mill Road
Morganton, N Carolina 28655 USA
meritor.com
The Clean Water Act, under 40 CFR 122.22(b) allows for the identification of a duly authorized
representative (DAR) and the granting of signatory authority to that DAR for the purposes of
submitting NPDES permits, application documents, and reports where requested or required by NC
DENR or the US EPA. The authorization must be made in writing by the senior manager of an
operating location.
This Signatory Authorization allows for the person holding the title of:
Supervisor, Environmental Health & Safety
at the Morganton, North Carolina manufacturing facility to sign any and all NPDES permits,
applications, and reports on behalf of the Site Manager. This Signatory Authority may be
terminated at any time by either the Site Manager or the EHS Supervisor.
The original copy of this Signatory Authority shall be kept on File in the EHS Supervisor's Office and
controlled under the IS014001 Environmental Management System.
Paul A. Ingle
Site Manager
Morganton, NC Facility
RECE1 V &F---D
k 8 ,2 5 2016
�` ENR-; aND QU,4r N
r �!
February 1, 2016
Central Files
NC DENR
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Certificate of Coverage NCG030664
Southwire
12331 Commerce Station Dr.
Huntersville, NC 28078
Dear Sir/Madam:
Please be in receipt of the Qualitative and Analytical Monitoring Data for this facility.
This report covers required sampling for Year 3 Sample 6 Period 2.
Thank you,
ohn E. Moore CSP, CHIVM, MBA
Southwire Huntersville OHS Manager
JEM/jm
NCDEWR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: httl2://portal.11cdeiir,Qrg/web/wq/ws./su/npAusw#tab-4
Permit No.: NI -CI r/ 031- 2100/
Facility Name: 5VUrN V I
County: BECK V
Inspector: t4^j IIICf l
Date of Inspection: , /QL —/f ` 0/-5
Time of Inspection: 1'1004r)l
Total Event Precipitation (inches):
Was this "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See inform -}
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
j precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, Ice ify that this report is accurate and complete to the best of my knowledge:
ignature of Permittee or Designee}
Pagel of 2
SWU-242, Last modified 10/25/2012
1. OutfalDescription:
Outfall No.
Receiving Stream:��
Describe the industrial activi
%rw.rj n l CL.
occur within the outfall drai
area:
A-J D
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: 46 41)� A) _4 - h f d ( — " rn2
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.):
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 a) 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 a 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 �? 3 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes QtD
9. Is there evidence of erosion or deposition at the outfall? Yes (60,
10. Other Obvious Indicators of Stormwater Pollution: "�
List and describe nOY' -
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2of2
sWU-242, Last modified 10/25/2012
1. Outfall Description:
Outfall No. �2— Structure (pipe, ditch, etc.)
Receiving Stream: n ? rt�c hu Ccr
Describe the industrial activities that occur within the outfall draina e area:�� a
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): �n,Ca"
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 � 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 P 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 0, 3 4 5
7. Is there any foam in the stormwater discharge? Yes (N)
8. is there an oil sheen in the stormwater discharge? Yes r o
9. Is there evidence of erosion or deposition at the outfall? Yes �Ny
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
1. Outfall Description:
Outfall No.
Receiving Stream: 1:417 �
Describe the industrial activi
(pipe, ditch, etc.
I),nr tJ I
occur within the
d
2. Color: Describe the color of the dischar u ing basic colors (red, brown, blue, etc.) and tint
(light medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): _lltFl-z-P
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 -2 Q 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 ( 23_ 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 24 5
7. Is there any foam in the stormwater discharge? Yes No
B. is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious Indicators of Stormwater Pollution:
List and describe 401 -
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
6 "�y &�
SWU-242, Last modified 10/25/2012
0
wcmnalytical
www.pacelabs.cwn
January 04, 2016
John Moore
Southwire
12331 Commerce Station
Huntersville, NC 28078
RE: Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Dear John Moore:
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
Enclosed are the analytical results for sample(s) received by the laboratory on December 17, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
�� 5�_e
Taylor Ezell
taylor.ezell@pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 37
•
aceAnalytrcal
www.pacerabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336 )623-8921
CERTIFICATIONS
Project: 2015 SEMI-ANNUAL.
Pace Project No.: 92280364
Charlotte Certification IDs
9800 Kincey Ave, Ste 100, Huntersville, NC 28078
Florida/NELAP Certification M E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
Virginia/VELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NEIAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 37
aceAnalyircal
unvw.pace+abS.cam
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Lab ID Sample ID
92280364001 GRAB 1
92280364002 GRAB 2
92280364003 GRAB 3
Pace Analytical Services. Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
SAMPLE SUMMARY
Matrix
Date Collected
Date Received
Water
12/17/15 05:00
12/17/15 16:33
Water
12/17/15 05:10
12/17/15 16:33
Water
12/17/15 08:00
12/17/15 16:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 37
acmnalytical
wwwpacelahs,own
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 71288
(336)623.8921
Project:
Pace Project No.:
2015 SEMI-ANNUAL
92280364
Anaiytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92280364001
GRAB 1
EPA 1664B
JMS
1
PASI-C
EPA608
SWB
27
PASI-C
EPA 200.7
JMW
7
PASI-A
EPA625
RES
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MSH
1
PASI-A
EPA 9040
MLS
1
PASI-A
92280364002
GRAB 2
EPA 1664B
JMS
1
PASI-C
EPA608
SWB
27
PASI-C
EPA 200.7
JMW
7
PASI-A
EPA625
RES
58
PAS!-C
EPA624
GAW
34
PASI-C
SM 2540D
MSH
1
PASI-A
EPA 9040
MLS
1
PASI-A
92280364003
GRAB 3
EPA 1664B
JMS
1
PASI-C
EPA 608
SWB
27
PASI-C
EPA 200.7
JMW
7
PASI-A
EPA 625
RES
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MDW
1
PASI-A
EPA9040
MLS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 37
aceAnalytical.
w,ow.pacetoft com
ANALYTICAL RESULTS
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
Sample: GRAB 1 Lab ID: 92280364001 Collected: 12/17/15 05:00 Received: 12/17/15 16:33 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No, Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO
mg1L
5.0
1.1
1
12/23/15 07:27
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method:
EPA 3510
Aldrin
NO
ug/L
0.050
0.050
1
12/21/15 09:30
12/22/15 2157 309-00-2
alpha-BHC
NO
ug1L
0.050
0.050
1
12/21/15 09:30
12/22/15 2157 319-84-6
beta-BHC
NO
ug1L
0.050
0.050
1
12/21/15 09:30
12/22/15 23:57 319-85-7
delta-BHC
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/22/15 23:57 319-86-8
gamma-BHC (Lindane)
NO
ug/L
0.050
0,050
1
12/21/15 09:30
12/22/15 23:57 58-89-9
Chtordane (Technical)
NO
ug/L
0.50
0.50
1
12/21/15 09:30
12/22/15 23:57 57-74-9
4,4'-DDD
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/22/15 23:57 72-54-8
4,4'-DDE
NO
ug/L
0.050
0.050
1
12/21/15 09:30
12/22/15 23:57 72-55-9
4,4'-DDT
N❑
ug/L
0.050
0.050
1
12/21/15 09:30
12/22/15 23:57 50-29-3
Dieldrin
ND
ug/L
0,050
0.050
1
12/21/15 09:30
12/22/15 23:57 60-57-1
Endosulfan t
NO
ug/L
0.050
0,050
1
12/21/15 09:30
12/22/15 23:57 959-98-8
Endosulfan II
NO
ug/L
0.050
0.050
1
12/21/15 09:30
12/22/15 23:57 33213-65-9
Endosulfan sulfate
NO
ug/L
0.050
0.050
1
12/21/15 09:30
12/22/15 23:57 1031-07-8
Endrin
NO
ug/L
0,050
0.050
1
12/21/15 09:30
12/22/15 23:57 72-20-8
Endrin aldehyde
ND
ug1L
0.050
0.050
1
12/21/15 09:30
12/22/15 23:57 7421-934
Heptachlor
ND
u911.
0,050
0.050
1
12/21/15 09:30
12/22/15 23:57 76-44-8
Heptachlor epoxide
ND
ug1L
0.050
0.050
1
12/21/15 09:30
12/22/15 23:57 1024-57-3
PCB- 1016 (Aroclor 1016)
ND
ug/L
0.50
0.50
1
12/21/15 09:30
12/22/15 23:57 12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug1L
0.50
0.50
1
12/21/15 09:30
12/22/15 23:57 11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug1L
0.50
0.50
1
12/21/15 09:30
12/22/15 23:57 11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug1L
0.50
0.50
1
12/21/15 09:30
12/22/15 23:57 53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug1L
0.50
0.50
1
12/21/15 09:30
12/22/15 23:57 12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug1L
0.50
0.50
1
12/21/15 09:30
12/22/15 23:57 11097-69-1
PCB-1260 (Aroclor 1260)
NO
uglL
0.50
0.50
1
12/21/15 09:30
12/22/15 23:57 11096-82-5
Toxaphene
ND
ug/L
0.50
0.50
1
12/21/15 09:30
12/22/15 23:57 8001-35-2
Surrogates
Teirachloro-m-xylene (S)
64
%
20-110
1
12/21/15 09:30
12/22/15 23:57 877-09-8
Decachlorobiphenyl (S)
45
%
20-138
1
12/21/15 09:30
42/22/15 23:57 2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
NO
mg/L
0.0010
0.00050
1
12/18/15 21:00
12/22/15 00:47 7440-43-9
Chromium
NO
mg1L
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:47 7440-47-3
Copper
NO
mg1L
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:47 7440-50-8
Lead
NO
mg1L
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:47 7439-92-1
Nickel
NO
mg1L
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:47 7440-02-0
Silver
NO
mg/L
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:47 7440-22-4
Zinc
0.012
mg/L
0,010
0.0025
1
12/18/15 21:00
12/22/15 00:47 7440-06-6
625 MSSV
Analytical Method: EPA 625 Preparation Method:
EPA
625
Acenaphthene
ND
ug/L
5.0
0.25
1
12/18/15 10:30
12/22/15 01:40 83-32-9
Acenaphthylene
NO
ug/L
5.0
0.21
1
12/18/15 10:30
12122/15 01:40 208-96-8
Anthracene
ND
ug1L
5.0
0.14
1
12/18/15 10:30
12/22/15 01:40 120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
0.33
1
12/18/15 10:30
12/22/15 01:40 56-55-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in foil,
Date: 01104/2016 10:43 AM without the written consent of Pace Analytical Services, Inc..
Page 5 of 37
aceAnalyfical
wwwpacelabs-com
ANALYTICAL RESULTS
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 17288
(336)623.8921
Sample: GRAB 1 Lab ID: 92280364001 Collected: 12/17115 05:00 Received: 12/17/15 16:33 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Benzo(a)pyrene
ND
ug/L
5.0
0.30
1
12/18/15 10:30
12/22/15 01:40 50-32-8
Benzo(b)fluoranthene
ND
ug1L
5.0
0.28
1
12/18/15 %30
12/22/15 01:40 205-99-2
Benzo(g,h,i)perylene
ND
ug1L
5.0
0.38
1
12/18/15 10:30
12/22/15 01:40 191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
0,43
1
12/18115 10:30
12/2211501A0 207-08-9
4-Bromophenylphenyl ether
NO
ug/L
5.0
0.82
1
12/18115 10:30
12/22/15 01:40 101-55-3
Butylbenzylphthalate
NO
ug/L
5.0
0.79
1
12/18/15 10:30
12/22/15 01:40 85-68-7
4-Chloro-3-methylphenol
NO
ug1L
5.0
3.7
1
12/18/15 10:30
12/22/15 01:40 59-50-7
bis(2-Chloroethoxy)methane
NO
ug1L
10.0
0.92
1
12/18/15 10:30
12/22/15 01:40 111-91-1
bis(2-Chloroethyl) ether
NO
ug1L
5.0
1.0
1
12/18/15 10:30
12/22/15 01:40 111-44-4
bis(2-Chloroisopropyl) ether
NO
ug1L
5.0
0.95
1
12/18/15 10:30
12/22/15 01:40 108-60-1
2-Chloronaphthalene
ND
ug1L
5.0
0.98
1
12/18/15 10:30
12/22/15 01:40 91-58-7
2-Chlorophenol
ND
ug1L
5.0
1.3
1
12/18/15 10:30
12/22/15 01:40 95-57-8
4-Chlorophenylphenyl ether
ND
uglL
5.0
0.87
1
12/18/15 10:30
12/22/15 01:40 7005-72-3
Chrysene
ND
ug1L
5.0
0.21
1
12/18/15 10:30
12/22/15 01:40 218-01-9
Dibenz(a,h)anth racene
ND
ug1L
5.0
0,55
1
12/18/15 10:30
121221i5 01:40 53-70-3
3,3'-Dichlorobenzidine
ND
ug/t_
25.0
2.1
1
12/18/15 10:30
12/22/15 01:40 91.94-1
2,4-Dichlorophenol
NO
ug/L
5.0
1.7
1
12/18/15 10:30
12/22/15 01:40 120-83-2
Diethylphthalate
NO
ug/L
5.0
0.58
1
12/18/15 10:30
12122/15 01:40 84-66-2
2,4-Dimethylphenol
NO
ug/L
10.0
1.2
1
12/18/15 10:30
12122/15 01:40 105-67-9
Dimethylphthalate
NO
ug1L
5.0
0.76
1
12/18/15 10:30
12/22/15 01:40 131-11-3
Di-n-butylphthalate
NO
ug1L
5.0
0.75
1
12/18/15 10:30
12/22/15 01:40 84-74-2
4,6- Din itro-2-methylphenol
NO
ug/L
20.0
2.6
1
12/18/15 10:30
12/22/15 01:40 534-52-1
2,4-Dinitrophenol
ND
ug1L
50.0
9.0
1
12/18/15 10:30
12/22/15 01:40 51-28-5
2,4-Dinilrotoluene
NO
ug1L
5.0
0.90
1
12/18/15 10:30
12/22/15 01:40 121-14-2
2,6-Dinitrotoluene
NO
ug/L
5.0
0.98
1
12/18/15 10:30
12/22/15 01:40 606-20-2
Di-n-octylphthalate
NO
ug/L
5.0
0,66
1
12/18/15 10:30
12/22/15 01:40 117-84-0
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
0.79
1
12/18/15 10:30
12/22/15 01:40 117-81-7
Fluoranthene
NO
ug/L
5.0
0.21
1
12/18/15 10:30
12/22/15 01:40 206-44-0
Fluorene
NO
ug/L
5.0
0.21
1
12/18/15 10:30
12/22/15 01:40 86-73-7
Hexachloro-1,3-butadione
NO
ug/L
5.0
0.94
1
12/18/15 10:30
12/22/15 01:40 87.68-3
Hexachlorobenzene
NO
ug/L
5.0
0.72
1
12/18/15 10:30
12/22/15 01:40 118-74-1
Hexachlorocyclopentadiene
NO
ug/L
10.0
0.88
1
12/18/15 10:30
12/22/15 01:40 77-47-4
Hexachloroethane
NO
ug/L
5.0
1.1
1
12118/1510:30
12122/1501A0 67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug1L
5.0
0,29
1
12/18115 10:30
12/2211501:40 193-39-5
Isophorone
ND
ug/L
10.0
0,89
1
12/18115 10:30
12/22/15 01:40 78-59-1
Naphthalene
ND
ug/L
5.0
0.34
1
12/18/15 10:30
12/22/15 01:40 91-20-3
Nitrobenzene
NO
ug/L
5.0
1.1
1
12/18/15 10:30
12/22/15 01:40 98-95-3
2-Nitrophenol
NO
ug/L
5.0
0.91
1
12/18/15 10:30
12/22/15 01:40 88-75-5
4-Nitrophenol
NO
ug/L
50.0
4.1
1
12/18/15 10:30
12/22/15 01:40 100-02-7
N-Nitrosodimethylamine
NO
uglL
5.0
0,91
1
12/18/15 10:30
12/22/15 01:40 62-75-9
N-Nitroso-di-n-propylamine
NO
uglL
5.0
0.99
1
12/18/15 10:30
12/22/15 01:40 621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1.0
1
12/18/15 10.30
12/22/15 01A0 86-30-6
Pentachlorophenol
ND
ug/L
10.0
4.6
1
12/18/15 10:30
12/22115 01:40 87-86-5
Phenanthrene
ND
ug1L
5.0
0.22
1
12118/1510:30
1212211501A0 85-01-8
Phenol
ND
ug1L
5.0
1A
1
12/18115 10:30
1212211501:40 108-95-2
Pyrene
ND
ug1L
5.0
0.19
1
12/18/15 10:30
12/22/15 01:40 129-00-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01 /04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 37
aceAnalytical'
wwwpacefab.carn
ANALYTICAL RESULTS
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
Sample: GRAB 1
Parameters
Lab ID:
Results
92280364001
Units
Collected:
Report
Limit
12/17/15 05:00 Received: 12/17/15 16:33 Matrix: Water
MDL OF Prepared Analyzed GAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
1,2,4-Trichlorobenzene
NO
ug/L
5.0
0,98
1 12/18/15 10:30
12/22/15 01:40 120-82-1
2,4,6-Tdchlorophenol
NO
ug/L
10.0
1.3
1 12/18115 10:30
12/22/15 01:40 88-06-2
Surrogates
Nitrobenzene-d5 (S)
75
%
10-120
1 12/18115 10:30
12/22/15 01:40 4165-60-0
2-Fluorobiphenyl (S)
73
%
15-120
1 12/18/15 10:30
12/22/15 01:40 321-60-8
Terphenyl-d 14 (S)
85
%
11-131
1 12118/1510:30
12/2211501:40 1718-51-0
Phenol-d6 (S)
28
%
10-120
1 12/18115 10:30
12/22/15 01:40 13127-88-3
2-Fluorophenol(S)
43
%
10-120
1 12/18115 10:30
12/22/1501:40 367-12-4
2,4,6-Tribromophenol (S)
8o
%
10-137
1 12/18/15 10:30
12/22/15 01:40 118-79-6
624 Volatile Organics
Analytical
Method: EPA 624
Benzene
NO
ug/L
2.0
1.7
1
12/2811522:15 71-43-2
Bromodichloromethane
ND
ug/L
2.0
1.7
1
12/28115 2115 75-27-4
Bromoform
NO
ug/L
2.0
1.5
1
12/28115 22:15 75-25-2
Bromomethane
ND
ug/L
2.0
1.0
1
12/28/15 22:15 74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1.9
1
12/28/15 22:15 56-23-5
Chlorobenzene
ND
ug/L
2.0
1.7
1
12/28115 22:15 108-90-7
Chloroethane
ND
ug/L
2.0
1.6
1
12/28/15 22A5 75-00-3
Chloroform
ND
ug/L
2.0
1.9
1
12/28/15 22:15 67-66-3
Chloromethane
ND
ug/L
2.D
1.5
1
12/28/15 22:15 74-87-3
Dibromochloromethane
ND
ug/L
2.0
1.8
1
12/28/15 22:15 124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1.5
1
12/28/15 22:15 95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1.5
1
12/28/15 22:15 541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1.5
1
12/28/15 22:15 106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1.8
1
12/28/15 22:15 75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1.8
1
12/28/15 22:15 107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1.9
1
12/28/15 22:15 75-35-4
cis-1,2-Dichloroethene
NO
ug/L
2.0
1.8
1
12/28/15 22:15 156-59.2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1.8
1
12/28/15 22:15 156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
1.7
1
12128/15 22:15 78-87-5
cis- 1, 3-Dichloropropene
NO
ug1L
2.0
1.6
1
12/28/15 22:15 10061-01-5
trans- 1,3-Dichloropropene
NO
ug1L
2.0
1.6
1
12/28/15 22:15 10061-02-6
Ethylbenzene
NO
ug1L
2.0
1.6
1
12/28/15 22:15 100-41-4
Methylene Chloride
NO
ug1L
2.0
1.9
1
12/28/15 22:15 75-09-2
1,1,2,2-Tetrachloroelhane
ND
ug1L
2.0
1.5
1
12/28/15 22:15 79-34-5
Tetrachloroethene
ND
ug1L
2.0
1.8
1
12/28/15 22:15 127-18-4
Toluene
ND
ug1L
2.0
1.6
1
12/28/15 22:15 108-88-3
1. 1, 1 -Trichloroetha ne
ND
ug1L
2.0
1.9
1
12/28/15 22:15 71-55-6
1,1,2-Trichloroethane
NO
ug1L
2.0
1.7
1
12/28/15 22:15 79.00.5
Trichloroethene
NO
ug1L
2.0
1.8
1
12/28/15 22:15 79-01-6
Trichlorofluoromethane
NO
ug1L
2.0
1.7
1
12/28/15 22:15 75-69-4
Vinyl chloride
ND
uglL
2.0
1.5
1
12/28/15 22:15 75-01-4
Surrogates
4-Bromofluorobenzene (S)
105
%
70-130
1
12/28/15 22:15 460-00-4
Toluene -dB (S)
111
%
70-130
1
12/28/15 22:15 2037-26-5
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
12/28/15 22:15 17060-07-0
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except in full,
Dale: 01 /0412016 10:43 AM
without the written
consent of Pace Analytical Services, Inc..
Page 7 of 37
m
aceAnalyiical
www Aacefabs wm
ANALYTICAL RESULTS
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 2�2a8
(336)623-8921
Sample: GRAB 1
Parameters
LabID: 92280364001 Collected:
Report
Results Units Limit
12/17/15 05:00
MDL DF
Received:
Prepared
12117115 16:33 Matrix: Water
Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L 3.1
3.1 1
12/21/15 23:10
9040 pH
Analytical Method: EPA 9040
pH
6.7 Std. Units 0.10
0.10 1
12/21/15 11:15 H6
Sample: GRAB 2
Lab ID: 92280364002 Collected:
12/17/15 05:10
Received:
12/17/15 16:33 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed CAS No, Qual
HEM, Oil and Grease
Oil and Grease
608 GCS Pesticides and PCBs
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PC13-1254 (Aroclor 1254)
PC8-1260 (Aroclor 1260)
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
200.7 MET ICP
Cadmium
Date: 01/04/2016 10:43 AM
Analytical Method: EPA 1664E
ND mg/L 5.0 1.1 1 12/23/15 07:27
Analytical Method: EPA608 Preparation Method: EPA 3510
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:15 309-00-2
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:15 319-84.6
ND
ug/L
0,050
0.050
1
12/21/15 09:30
12/23/15 00:15 319-85-7
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:15 319-86-8
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:15 58.89-9
ND
ug/L
0.50
0.50
1
12/21/15 09:30
12/23/15 00:15 57-74-9
NO
ug/L
0.050
0,050
1
12/21/15 09:30
12/23/15 00:15 72-54-8
ND
ug1L
0.050
0.050
1
12121/15 09:30
12/23/15 00:15 72-55-9
ND
ug1L
0.050
0.050
1
12/21/15 09:30
12/23/15 0015 50-29-3
NO
ug/L
0.050
0,050
1
12/21/15 OR30
12/23/15 00:15 60-57-1
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:15 959-98-8
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:15 33213-65-9
ND
ug/L
0.050
0,050
1
12/21/15 09:30
12/23/15 00:15 1031-07-8
ND
ug/L
0.050
0,050
1
12/21/15 09:30
12/23/15 00:15 72-20-8
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:15 7421-93-4
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:15 76-44-8
ND
ug/L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:15 1024-57-3
ND
ug/L
0.50
0.50
1
12/21/15 0910
12/23/15 0015 12674-11-2
ND
ug/L
0.50
0.50
1
12/21/15 09:30
12/2311500A5 11104-28-2
ND
ug/L
0.50
0.50
1
12/21115 09:30
12/23/15 00A5 11141-16-5
ND
ug/L
0.50
0.50
1
12/21115 09:30
12/23/15 00:15 53469-21-9
ND
ug/L
0.50
0.50
1
12/21/15 09:30
12/23/15 00:15 12672-29-6
ND
ug/L
0.50
0.50
1
12/21/15 09:30
12/23/15 00:15 11097-69-1
ND
ug1L
0.50
0.50
1
12/21/15 09:30
12/23/15 00:15 11096-82-5
ND
ug/L
0.50
0.50
1
12/21/15 09:30
12/23/15 00:15 8001-35-2
53 % 20-110 1 12/21/15 09:30 12/23/15 00:15 877-09-8
31 % 20-138 1 12/21115 09:30 12/23/15 00:15 2051-24-3
Analytical Method: EPA200.7 Preparation Method: EPA200.7
ND mg1L 0.0010 0.00050 1 12/18/15 21:00 12/22/15 00:51 7440-43-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 37
m
ace Analytical
wwwpacefabs.cam
1_1110wa11111M0 1*111ItI&I
Pace Analytical Services, Inc.
205 East Meadow (toad - Suite A
Eden, NC 27288
(336)623-8921
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Sample: GRAB 2 Lab ID: 92280364002 Collected: 12117/15 05:10 Received: 12/17/15 16:33 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Isophorone
ND
u91L
10.0
0.89
1
12/18/15 10:30
12/22/15 02:08 78-59-1
Naphthalene
ND
ug1L
5.0
0.34
1
12/18/15 10:30
12/22/15 02:08 91-20-3
Nitrobenzene
ND
ug/L
5.0
1.1
1
12/18115 10:30
12/22/15 02:08 98-95-3
2-Nitrophenol
ND
ug/L
5.0
0.91
1
12/18/15 10:30
12/22/15 02:08 88-75-5
4-Nitrophenol
ND
ug1L
50.0
4.1
1
12/18/15 10:30
12/22/15 02:08 100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
0.91
1
12/18/15 10:30
12/22/15 02:08 62-75-9
N-Nitroso-di-n-propylamine
ND
ug1L
5.0
0,99
1
12/18115 10:30
12/22/15 02:08 621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1.0
1
12/18/15 10:30
12/22/15 02:08 86-30-6
Pentachlorophenol
ND
ug/L
10.0
4.6
1
12/18/15 10:30
12/22/15 02:08 87-86-5
Phenanthrene
NO
ug/L
5.0
0.22
1
12/18/15 10:30
12/22/15 02:08 85-01-8
Phenol
N❑
ug/L
5.0
1.9
1
12/18/15 10:30
12/22/15 02:08 108-95-2
Pyrene
ND
ug/L
5.0
0.19
1
12/18/15 10:30
12/22/15 02:08 129-00-0
1,2,4-Trichtorobenzene
NO
ug/L
5.0
0,98
1
12/18/15 10:30
12/22/15 02:08 120-82-1
2,4,6-Trichlorophonol
NO
ug/L
10.0
1.3
1
12/18/15 10:30
12122/15 02:08 88-06-2
Surrogates
Nitrobenzene-d5 (S)
57
%
10-120
1
12/18/15 10:30
12/22/15 02:08 4165-60-0
2-Fluorobiphenyl (S)
51
%
15-120
1
12/18/15 10:30
12/22/15 02:08 321-60-8
Terphenyl-d14 (S)
69
%
11-131
1
12/18/15 10:30
12/22/15 02:08 1718-51-0
Phenol-d6 (S)
19
%
10-120
1
12/18/15 10:30
12/22/15 02:08 13127-88-3
2-Fluorophenol (S)
31
%
10-120
t
12/18/15 10:30
12/22/15 02:08 367-12-4
2,4,6-Tribromophenol (S)
61
%
10-137
1
12/18/15 10:30
12122/15 02:08 118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
NO
ug/L
2.0
1.7
1
12/28/15 22:32 71-43-2
Bromodichloromethane
NO
ug/L
2.0
1.7
1
12/28/15 22:32 75-27-4
Bromoform
NO
uglL
2.0
1.5
1
12/28/15 22:32 75-25-2
Bromomethane
NO
ug/L
2.0
1.0
1
12/28/15 22:32 74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1.9
1
12/28/15 22:32 56-23-5
Chlorobenzene
NO
ug/L
2.0
1.7
1
12/28/15 22:32 108-90-7
Chloroethane
NO
ug/L
2.0
1.6
1
12/28/15 22:32 75-00-3
Chloroform
NO
ug/L
2.0
1.9
1
12/28/15 22:32 67-66-3
Chloromethane
NO
ug1L
2.0
1.5
1
12/28/15 22:32 74-87-3
Dibromochloromethane
ND
ug/L
2.0
1.8
1
12/28/15 22:32 124-48-1
1,2-Dichlorobenzene
NO
ug/L
2.0
1.5
1
12/28/15 22:32 95-50-1
1,3-Dichlorobenzene
ND
ug1L
2.0
1.5
1
12/28/15 22:32 541-73-1
1,4-Dichlorobenzene
ND
ug1L
2.0
1.5
1
1212811522:32 106-46-7
1,1-1)ichloroethane
NO
ug1L
2.0
1.8
1
12/2811522732 75-34-3
1,2-Dichloroethane
ND
ug1L
2.0
1.8
1
12/2811522:32 107-06-2
1,1-Dichloroethene
ND
ug1L
2.0
1.9
1
12/28/15 22:32 75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
2.0
1.8
1
12/28/15 22:32 156-59-2
trans-1,2-Dichloroethene
ND
ug1L
2.0
1.8
1
12/28/15 22:32 156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
1.7
1
12/28/15 22:32 78-87-5
cis- 1,3-Dichloropropene
ND
ug1L
2.0
1.6
1
12/28/15 22:32 10061-01-5
trans- 1. 3-D ichloropropene
ND
ug/L
2.0
1.6
1
12/28/15 22:32 10061-02-6
Ethylbenzene
ND
ug1L
2.0
1.6
1
12/28/15 22:32 100-41-4
Methylene Chloride
ND
ug1L
2.0
1.9
1
12/28/15 22:32 75-09-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2016 10:43 AM without the wntten consent of Pace Analytical Services, Inc.. Page 10 of 37
acmnalytical
wwwp"abs.=
ANALYTICAL RESULTS
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 2y2W
(336)623.8821
Sample: GRAB 2 Lab ID: 92280364002 Collected: 12/17/15 05:10 Received: 12/17/15 16:33 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Chromium
ND
mg/L
0,0050
0.0025
1
12/18/15 21:00
12/22/15 00:51 744047-3
Copper
ND
mg/L
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:51 7440-50-8
Lead
ND
mg/L
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:51 7439-92-1
Nickel
ND
mg/L
0.0050
0,0025
1
12/18/15 21:00
12/22/15 00:51 7440-02-C
Silver
ND
mg/L
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:51 7440-22-4
Zinc
ND
mg/L
0.010
0.0025
1
12/18/15 21:00
12122/15 00:51 7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation
Method: EPA 625
Acenaphthene
ND
ug1L
5.0
0,25
1
12/18/15 10:30
12/22/15 02:08 83-32-9
Acenaphthylene
ND
ug/L
5.0
0.21
1
12/18115 10:30
12/22/15 02708 208-96.8
Anthracene
ND
ug/L
5.0
0.14
1
12/18/15 10:30
12/22/15 02:08 120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
0.33
1
12/18/15 10:30
12/22/15 02:08 56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
0.30
1
12/18/15 10:30
12/22/15 02:08 50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
0.28
1
12/18/15 10:30
12/22/15 02:08 205-99-2
Benzo(g,h,i)perylene
ND
ug1L
5.0
0.38
1
12/18/15 10.30
12/22/15 02:08 191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
0.43
1
12/18/15 10:30
12/22/15 02:08 207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
0,82
1
12/18/15 10:30
12/22/15 02:08 101-55-3
Butylbenzyiphthalate
ND
ug/L
5.0
0.79
1
12/18/15 10:30
12/22/15 02:08 85-68-7
4-Chloro-3-methylphenol
ND
ug1L
5.0
3.7
1
12/18/15 10:30
12/22/15 02:08 59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
0,92
1
12/18/15 10:30
12/22/15 02:08 111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1.0
1
12/18/15 10:30
12/22115 02:08 111-44-4
bis(2-Chloroisop(opyl) ether
ND
ug/L
5.0
0.95
1
12/18/15 10:30
12/22/15 02:08 108-60-1
2-Chloronaphthalene
ND
ug/L
5.0
0.98
1
-12/18115 10:30
12/22/15 02:08 91-58-7
2-Chlorophenol
ND
ug/L
5.0
1.3
1
12/18115 10:30
12/22/15 02:08 95-57-8
4-Chlorophenylphenyl ether
ND
ug1L
5.0
0.87
1
12/18/15 10:30
12/22/15 02:08 7005-72-3
Chrysene
ND
ug/L
5.0
0.21
1
12/18/15 10:30
12/22/15 02:08 218-01-9
Dibenz(a,h)anlhracene
ND
ug1L
5.0
0.55
1
12/18/15 10:30
12/22/15 02:08 53-70-3
3,3'-Dichtorobenzidine
ND
ug/L
25.0
2.1
1
12/18/15 10:30
12/22/15 02:08 91-94-1
2,4-Dichlorophenol
ND
ug1L
5.0
1.7
1
12/18/15 10:30
12/22/15 02:08 120-83-2
D iethylphtha late
ND
ug1L
5.0
0.58
1
12/18/15 10:30
12/22/15 02:08 84-66-2
2,4-Dimethyl phenol
ND
ug1L
10.0
1.2
1
12/18/15 10:30
12/22/15 02:08 105-67-9
Dimethylphthatate
ND
ug1L
5.0
0.76
1
12/18/15 10:30
12/22/15 02:08 131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
0.75
1
12/18/15 10:30
12/22/15 02:08 84-74-2
4,6-Dinitro-2-methyiphenol
ND
ug1L
20.0
2.6
1
12/18/15 10:30
12/22/15 02:08 534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
9.0
1
12/18/15 10:30
12/22/15 02:08 51.28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
0.90
1
12118/15 10:30
12122/15 02:08 121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
0.98
1
12118/15 10:30
12/22/15 02:08 606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
0.66
1
12/18/15 10:30
12/22/15 02:08 117-84.0
bis(2-Ethyihexyl)phthalate
ND
ug1L
5.0
0.79
1
12/18/15 10:30
12/22/15 02:08 117-81-7
Fluoranthene
ND
ug1L
5.0
0.21
1
12/18/15 10:30
12/22/15 02:08 206-44-0
Fluorene
ND
ug/L
5.0
0.21
1
12/18/15 10:30
12/22/15 02:08 86-73-7
Hexachloro-1 ,3-butadiene
ND
ug/L
5.0
0.94
1
12/18/15 10:30
12/22/15 02:08 87-68-3
Hexachtorobenzene
ND
ug/L
5.0
0.72
1
12/18/15 10:30
12/22/15 02:08 118-74-1
Hexachierocyclopentadiene
ND
ug/L
10.0
0.88
1
12/18/15 10:30
12/22/15 02:08 77-47-4
Hexachloroethane
ND
ug/L
5.0
1.1
1
12/18/15 10:30
12/22/15 02:08 67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
0.29
1
12/18/15 10:30
12/22/15 02:08 193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc- Page 9 of 37
m
aceAnalytical
~Pacelbin com
ANALYTICAL RESULTS
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analyticai Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
Sample: GRAB 2 Lab ID: 92280364002 Collected: 12/17/15 05:10 Received: 12/17/15 16:33 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
624 Volatile Organics
1,1, 2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trchloroethene
Trichlorofluorometha ne
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
2540D Total Suspended Solids
Total Suspended Solids
9040 pH
pH
Analytical Method: EPA624
NO
ug1L
2.0
1.5
1
12/28/15 22:32
79-34-5
NO
u911-
2.0
1.8
1
12128/15 22:32
127-18-4
NO
ug1L
2.0
1.6
1
12/28/15 22:32
108-88-3
NO
ug1L
2.0
1.9
1
12/28/15 22:32
71-55-6
ND
ug1L
2.0
1.7
1
12/28/15 22:32
79-00-5
NO
ug1L
2.0
1.8
1
12128/15 22:32
79-01-6
NO
ug1L
2.0
1.7
1
12128/15 22:32
75-69-4
NO
ug1L
2.0
1.5
1
12/28/15 22:32
75-01-4
106
%
70-130
1
12128/15 22:32
460-00-4
108
%
70-130
1
12/28/15 22:32
2037-26-5
99
%
70-130
1
12/28/15 22:32
17060-07-0
Analytical
Method: SM 2540D
2.7
mglL
2.5
2.5
1
12/21/15 23:10
Analytical
Method: EPA 9040
6.6
Std. Units
0.10
0.10
1
12/21/15 11:15
H6
Sample: GRAB 3 Lab ID: 92280364003 Collected: 12/17/15 08:00 Received: 12/17/15 16:33 Matrix: Water
Report
Parameters Results Units Limit MOIL DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
608 GCS Pesticides and PCBs
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan i
Endosulfan it
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
ly=_ 1�iffil k,1101M- 1:9CkL•Iu
Analytical Method: EPA 1664E
NO mglL 5.0 1.1 1 12/23/15 07:27
Analytical Method: EPA 608 Preparation Method: EPA 3510
ND
uglL
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
309-00-2
NO
uglL
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
319-84-6
NO
ug1L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
319-85-7
NO
ug1L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
319-86-8
NO
uglL
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
58-89-9
NO
uglL
0.50
0.50
1
12/21/15 09:30
12/23/15 00:51
57-74-9
NO
uglL
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
72-54-8
NO
ug1L
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
72-55-9
NO
uglL
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
50-29-3
NO
uglL
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
60-57-1
NO
uglL
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
959-98-8
NO
uglL
0.050
0.050
1
12/21115 09:30
12/23/15 00:51
33213-65-9
NO
uglL
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
1031-07-8
NO
uglL
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
72-20-8
NO
uglL
0.050
0.050
1
12/21/15 09:30
12/23/15 00:51
7421-93-4
NO
uglL
0.050
0.050
1
12/21/15 09:30
12/23115 00:51
76-44-8
NO
uglL
0.050
0.050
1
12/21115 09:30
12/23/15 00:51
1024-57-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 37
Pace Analytical Services, Inc.
acmnalytrcal • 205 East MeadoEden NC 2i288
*Wwpeceisb. ,
(336)623-8921
ANALYTICAL RESULTS
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Sample: GRAB 3 Lab ID: 92280364003 Collected: 12/17/15 08:00 Received: 12/17/15 16:33 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
OF
Prepared
Analyzed
CAS No. Qual
608 GCS Pesticides and PCBs
Analytical Method: EPA608 Preparation Method: EPA
3510
PCB- 1016 (Aroclor 1016)
NO
ug1L
0.50
0.50
1
12/21/15 09:30
12/23/15 00:51
12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug1L
0.50
0,50
1
12/21/15 09:30
12/23/15 00:51
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug1L
0.50
0.50
1
12/21/15 09:30
12/23/15 00:51
11141-16-5
PCB-1242 (Aroclor 1242)
NO
ug1L
0.50
0.50
1
12/21/15 09:30
12/23/15 00:51
53469-21-9
PCB-1248 (Aroclor 1248)
NO
uglL
0.50
0,50
1
12/21/15 09:30
12/23/15 00:51
12672-29-6
PCB-1254 (Aroclor 1254)
NO
uglL
0.50
0.50
1
12/21/15 09:30
12/23/15 00:51
11097-69-1
PCB-1260 (Aroclor 1260)
NO
ug1L
0.50
0.50
1
12/21/15 09:30
12/23/15 00:51
11096-82-5
Toxaphene
NO
ug1L
0.50
0.50
1
12/21/15 09:30
12123/15 00:51
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
41
%
20-110
1
12/21/15 09:30
12/23/15 00:51
877-09-8
Decachlorobiphenyl (S)
55
%
20-138
1
12/21/15 09:30
12/23/15 00:51
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
NO
mg1L
0.0010
0.00050
1
12/18/15 21:00
12/22/15 00:54
7440-43.9
Chromium
NO
mglL
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:54
7440-47-3
Copper
NO
mg1L
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:54
7440-50-8
Lead
NO
mg1L
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:54
7439-92-1
Nickel
NO
mg/L
0.0050
0.0025
1
12/18/15 21:00
12122/15 00:54
744M2-0
Silver
NO
mglL
0.0050
0.0025
1
12/18/15 21:00
12/22/15 00:54
7440-22-4
Zinc
NO
mglL
0.010
0.0025
1
12/18/15 21:00
12/22/15 00:54
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA
625
Acenaphthene
NO
ug1L
5.0
0.25
1
12/18/15 10:30
12/22/15 02:35
83-32-9
Acenaphthylene
NO
ug1L
5.0
0.21
1
12/18/15 10:30
12/22/15 02:35
208-96-8
Anthracene
NO
uglL
5.0
0.14
1
12/18/15 10:30
12/22/15 02:35
120-12-7
Benzo(a)anthracene
NO
uglL
5.0
0.33
1
12/18/15 10:30
12/22/15 02:35
56-55-3
Benzo(a)pyrene
NO
uglL
5.0
0.30
1
12/18/15 10:30
12/22/15 02:35
50-32-8
Benzo(b)fluoranthene
NO
uglL
5.0
0.28
1
12/18/15 10:30
12/22/15 02:35
205-99-2
Benzo(g,h,i)perylene
NO
ug1L
5.0
0.38
1
12/18/15 10:30
12/22/15 02:35
191-24-2
Benzo(k)fluoranthene
NO
ug1L
5.0
0.43
1
12/18/15 10:30
12/22/15 02:35
207-08-9
4-Bromophenylphenyl ether
NO
ug1L
5.0
0.82
1
12/18/15 10:30
12/22/15 02:35
101-55-3
Butylbenzylphthalate
NO
ug1L
5.0
0.79
1
12/18/15 10:30
12/22/15 02:35
85-68-7
4-Chloro-3-methyl phenol
NO
ug1L
5.0
3.7
1
12/18/15 10:30
12/22/15 02:35
59-50-7
bis(2-Chloroethoxy)methane
NO
uglL
10.0
0.92
1
12/18/15 10:30
12/22/15 02:35
111-91-1
bis(2-Chloroethyl) ether
NO
uglL
5.0
1.0
1
12/18/15 10:30
12/22/15 02:35
111-44-4
bis(2-Chloroisopropyl) ether
NO
uglL
5.0
0.95
1
12/18/15 10:30
12/22/15 02:35
108-60-1
2-Chloronaphthatene
NO
ug1L
5.0
0.98
1
12/18/15 10:30
12/22/15 02:35
91-58-7
2-Chlorophenol
NO
ug1L
5.0
1.3
1
12/18/15 10:30
12/22/15 02:35
95-57-8
4-Chlorophenylphenyl ether
NO
ug1L
5.0
0.87
1
12/18/15 10:30
12/22/15 02:35
7005-72-3
Chrysene
NO
ug1L
5.0
0.21
1
12/18/15 10:30
12/22/15 02:35
218-01-9
Dibenz(a,h)anthracene
NO
ug1L
5.0
0.55
1
12/18/15 10:30
12/22/15 02:35
53-70-3
3,3'-Dichlorobenzidine
NO
uglL
25.0
2.1
1
12/18/15 10:30
12/22/15 02:35
91-94-1
2,4-Dichlorophenol
NO
uglL
5.0
1.7
1
12/18/15 10:30
12/22/15 02:35
120-83-2
Diethylphtha late
NO
uglL
5.0
0.58
1
12/18/15 10:30
12/22/15 02:35
84-66-2
2,4-Dimethyl phenol
NO
uglL
10.0
1.2
1
12/18/15 10:30
12/22/15 02:35
105-67-9
Dimethylphthalate
NO
uglL
5.0
0.76
1
12/18/15 10:30
12122/15 02:35
131-11-3
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full.
Date: 01104/2016 10:43 AM without the written consent of Pace Analytical Services, Inc,. Page 12 of 37
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623.8921
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Sample: GRAB 3 Lab ID: 92280364003 Collected: 12/17115 08:00 Received: 12/17/15 16:33 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
624 Volatile Organics Analytical Method: EPA 624
Dibromochloromethane
NO
ug/L
2.0
1.8
1
12/28/15 23:06 124-48-1
1,2-Dichlorobenzene
NO
ug/L
2.0
1.5
1
12/28/15 23:06 95-50-1
1,3-Dichlorobenzene
NO
ug/L
2.0
1.5
1
12/28/15 23:06 541-73-1
1,4-Dichlorobenzene
NO
ug/L
2.0
1.5
1
12/28/15 23:06 106-46-7
1,1-Dichloroethane
NO
ug1L
2.0
1.8
1
12/28/15 23:06 75-34-3
1,2-Dichloroethane
NO
ug1L
2.0
1.8
1
12/28/15 23:06 107-06-2
1,1-Dichloroethene
NO
ug1L
2.0
1.9
1
12/28/15 23:06 75-35-4
cis- 1, 2-Dichloroethene
NO
ug1L
2.0
1.8
1
12/28115 23:06 156-59-2
trans- 1,2-Dichloroethene
ND
ug1L
2.0
1.8
1
12/28/15 23:06 156-60-5
1,2-Dichloropropane
NO
ug1L
2.0
1.7
1
12/28/45 23:06 78-87-5
cis- 1, 3-Dichloropropene
NO
uglL
2.0
1.6
1
12/28/15 23:06 10061-01-5
trans- 1,3-Dichlo ropropene
NO
uglL
2.0
1.6
1
12/28/15 23:06 10061-02-6
Ethylbenzene
NO
ug1L
2.0
1.6
1
12/28/15 23:06 100-41-4
Methylene Chloride
ND
ug1L
2.0
1.9
1
12/28/15 23:06 75-09.2
1,1,2,2-Tetrachtoroethane
ND
ug1L
2.0
1.5
1
12/28115 23:06 79-34-5
Tetrachloroethene
ND
ug1L
2.0
1.8
1
12/28/15 23:06 127-18-4
Toluene
ND
ug1L
2.0
1.6
1
12/28115 23:06 108-88-3
1, 1, 1 -Trichloroethane
ND
ug1L
2.0
1.9
1
12/28/15 23:06 71-55-6
1,1,2-Trichloroethane
NO
ug1L
2.0
1.7
1
12/28/15 23:06 79-00-5
Tdchloroethene
NO
ug/L
2.0
1.8
1
12/28/15 23:06 79-01-6
Trichlorofluoromethane
NO
ug1L
2.0
1.7
1
12/28/15 23:06 75-69-4
Vinyl chloride
NO
ug/L
2.0
1.5
1
12/28/15 23:06 75-01-4
Surrogates
4-Bromofluorobenzene (S)
107
%
70-130
1
12/28/15 23:06 460-00-4
Toluene-d8 (S)
110
%
70-130
1
12128/15 23:06 2037-26-5
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
12/28/15 23:06 17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids NO mg/L 5.0 5.0 1 12/22/15 13:31
9040 pH Analytical Method: EPA 9040
pH 6.7 Std. Units 0.10 0.10 1 12/22/15 15:25
Date: 01/04/2016 10:43 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
H6
Page 14 of 37
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ANALYTICAL RESULTS
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 2h88
(336)623-8921
Sample: GRAB 3 Lab ID: 92280364003 Collected: 12/17/15 08:00 Received: 12/17/15 16:33 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-butylphthalate
ND
ug/L
5.0
0.75
1
12/18/15 10:30
12/22/15 02:35
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
2.6
1
12/18/15 10:30
12/22/15 02:35
534-52-1
2,4-Dinitrophenol
ND
uglL
50:0
9.0
1
12/18115 10:30
12/22/15 02:35
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
0.90
1
12/18115 10:30
12/22115 02:35
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
0.98
1
12/18/15 10:30
12/22/15 02:35
606-20-2
Di-n-octylphthalate
ND
ug/L
5.1)
0.66
1
12/18/15 10:30
12/22/15 02:35
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
0.79
1
12/18/15 10:30
12/22/15 02:35
117-81-7
Fluoranthene
ND
ug/L
5.0
0.21
1
12/18/15 10:30
12/22/15 02:35
206-44-0
Fluorene
ND
ug1L
5.0
0.21
1
12/18/15 10:30
12/22/15 02:35
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
0.94
1
12/18/15 10:30
12/22/15 02:35
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
0.72
1
12/18/15 10:30
12/22/15 02:35
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
0.88
1
12/18/15 10:30
12/22/15 02:35
77-47-4
Hexachloroethane
ND
ug/L
5.0
1.1
1
12/18/15 10:30
12/22/15 02:35
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
0.29
1
1211811510:30
1212211502:35
193-39-5
Isophorone
ND
ug/L
10.0
0.89
1
12/18/15 10:30
12/22/15 02:35
78-59-1
Naphthalene
ND
ug1L
5.0
0.34
1
12/18/15 10:30
12/22/15 02:35
91-20-3
Nitrobenzene
ND
ug/L
5.0
1.1
1
12/18/15 10:30
12/22/15 02:35
98-95-3
2-Nitrophenol
ND
ug1L
5.0
0.91
1
12/18/15 10:30
12122/15 02:35
88-75-5
4-Nitrophenol
ND
ug1L
50.0
4.1
1
12/18/15 10:30
12122/15 02:35
100-02-7
N-Nitrosodimethylamine
ND
ug1L
5.0
0.91
1
12/18/15 10:30
12/22/15 02:35
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
0.99
1
12/18/15 10:30
12/22/15 02:35
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1.0
1
12/18/15 10:30
12/22/15 02:35
86-30-6
Pentachlorophenol
ND
ug/L
10.0
4.6
1
12/18/15 10:30
12/22/15 02:35
87-86-5
Phenanthrene
ND
ug1L
5.0
0.22
1
12/18/15 10:30
12/22/15 02:35
85-01-8
Phenol
ND
ug/L
5.0
1.9
1
12/18115 10:30
12/22/15 02:35
108-95-2
Pyrene
ND
ug/L
5.0
0.19
1
12/18/15 10:30
12/22/15 02:35
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
0.98
1
12/18/15 10:30
12/22/15 02:35
120-82.1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1.3
1
12/18/15 10:30
12/22/15 02:35
88-06-2
Surrogates
Nitrobenzene-d5 (S)
60
%
10-120
1
12/18/15 10:30
12/22/15 02:35
4165-60-0
2-Fluorobiphenyl (S)
60
%
15-120
1
12/18/15 10:30
12/22/15 02:35
321-60-8
Terphenyl-d14 (S)
75
%
11-131
1
12/18/15 10:30
12/22/15 02:35
1718-51-0
Phenol-d6 (S)
20
%
10-120
1
12/18/15 10:30
12122/15 02:35
13127-88-3
2-Fluorophenol(S)
33
%
10-120
1
12/18/15 10:30
12/22/15 02:35
367-12-4
2,4,6-Tribromophenoi (S)
72
%
10-137
1
12/18/15 10:30
12/22/15 02:35
118-79-6
624 Volatile Organics Analytical Method: EPA 624
Benzene
ND
ug/L
2.0
1.7
1
12/28/15 23:06 71-43-2
Bromodichloromethane
ND
ug/L
2.0
1.7
1
12/28/15 23:06 75-27-4
Bromoform
ND
ug/L
2.0
1.5
1
12/28/15 23:06 75-25-2
Bromomethane
ND
ug/L
2.0
1.0
1
12/28/15 23:06 74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1.9
1
12/28/15 23:06 56-23-5
Chlorobenzene
ND
ug1L
2.0
1.7
1
12/28/15 23:06 108-90-7
Chloroethane
ND
ug1L
2.0
1.6
1
12/28/15 23:06 75-00-3
Chloroform
ND
ug/L
2.0
1.9
1
12/28/15 23:06 67-66-3
Chloromethane
N❑
ug/L
2.0
1.5
1
12/28/15 23:06 74-87-3
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full,
Date: 01 /04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 37
aceAnalytical
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QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
OC Batch: GCSV123640 Analysis Method: EPA 16648
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92280364001, 92280364002, 92280364003
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
METHOD BLANK: 1636122 Matrix: Water
Associated Lab Samples: 92280364001, 92280364002, 92280364003
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Oil and Grease mg1L ND 5.0 1.1 12/23/15 07:22
LABORATORY CONTROL SAMPLE:
1636123
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg1L
40 34.1
85
78-114
MATRIX SPIKE SAMPLE:
1636124
35221688001 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg1L
13.3 40
52.0
97
78-114
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit IS presented to the right of the resulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 37
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
205 East Meadow Road - Surte A
Eden, NC 21288
(336)623-8921
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
QC Batch: MPRP120326
Analysis Method:
EPA
200.7
QC Batch Method: EPA 200.7
Analysis Description:
200.7 MET
Associated Lab Samples: 92280364001,
92280364002, 92280364003
METHOD BLANK: 1633268
Matrix: Water
Associated Lab Samples: 92280364001,
92280364002, 92280364003
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed Qualifiers
Cadmium
mg/L
ND
0.0010
0.00050
12/22/15 00:16
Chromium
mg/L
ND
0.0050
0.0025
12/22/15 00:16
Copper
mg/L
ND
0.0050
0.0025
12/22/15 00:16
Lead
mg/1-
ND
0.0050
0.0025
12/22/15 00:16
Nickel
mg/L
ND
0.0050
0.0025
12/22/15 00:16
Silver
mg/L
ND
0.0050
0.0025
12/22/15 00:16
Zinc
mg/L
ND
0.010
0.0025
12/22/15 00:16
LABORATORY CONTROL SAMPLE: 1633269
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
mg1L
.5
0.48
96
85-115
Chromium
mg1L
.5
0.50
100
85-115
Copper
mg1L
.5
0.50
100
85-115
Lead
mg1L
.5
0,46
91
85-115
Nickel
mg1L
.5
0.48
96
85-115
Silver
mg/L
.25
0.25
99
85-115
Zinc
mg1L
.5
0,43
87
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1633270
1633271
MS
MSD
92279970001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Cadmium
mg/L
ND
.5
.5
0.52
0.47
104
95
70-130
9
20
Chromium
mg1L
ND
.5
.5
0.55
0.46
110
91
70.130
18
20
Copper
mg1L
15.9 ug/L
.5
.5
0.57
0,51
110
100
70-130
9
20
Lead
mg/L
6.6 ug/L
.5
.5
0.49
0.46
98
92
70-130
6
20
Nickel
mg/L
7.7 ug1L
.5
.5
0.52
0.47
103
93
70-130
10
20
Silver
mg1L
ND
25
.25
0.27
0,24
107
95
70-130
12
20
Zinc
mg1L
151 ug/L
.5
.5
0.62
0.61
94
91
70-130
3
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1633272
1633273
MS
MSD
92280423001 Spike
Spike MS
MSD
MS MSD % Rec Max
Parameter Units Result Cone.
Cane. Result
Result
% Rec % Rec Limits RPD RPD Qual
Cadmium mg1L ND .5
.5 0.51
0.47
102 94 70-130 8 20
Chromium mg1L 17.2 ug1L .5
.5 0.57
0.52
110 100 70-130 9 20
Results presented on this page are in the units indicated by the
"units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc..
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aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
205 East Meadow Road - Suile A
Eden, NC 27288
(336)623.8921
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1633272
1633273
MS
MSD
92280423001 Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Copper mg/L
213 ug1L
.5 .5
0.76
0.71
109
100
70-130
6
20
Lead mglL
ND
.5 .5
0.48
0.44
95
87
70-130
8
20
Nickel mglL
11.2 ug1L
.5 .5
0.52
0,48
102
94
70.130
8
20
Silver mglL
ND .25
.25
0.27
0.24
107
98
70-130
9
20
Zinc mglL
68.8 ug/L
.5 .5
0.52
0.48
91
82
70-130
9
20
Results presented on this page are in the units indicated by the "Units- column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc..
Page 17 of 37
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QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
QC Batch: MSW34964 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92280364001, 92280364002, 92280364003
METHOD BLANK: 1638072 Matrix: Water
Associated Lab Samples: 92280364001, 92280364002, 92280364003
Blank Reporting
Parameter Units Result Limit MDL
1,1,1-Trich to roethane
1,1,2,2-Telrach loroetha ne
1,1,2-Trichloroeth a ne
1,1-Dichloroethane
1,1-Dichloroelhene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
CIS- 1,3-Dichloroprope ne
Dibromochloromethane
Ethylbenzene
Methylene Chloride
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
ug/L
ug/L
ug1L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug1L
ug1L
ug/L
ug/L
ug1L
ug1L
ug/L
ug1L
ug1L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug1L
ug/L
ug/L
ug/L
NO
NO
NO
NO
ND
NO
NO
NO
NO
NO
NO
NO
ND
ND
NO
ND
ND
NO
NO
NO
NO
ND
NO
NO
NO
NO
ND
ND
NO
NO
NO
92
108
104
2.0
2.0
2.0
2.0
2A
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
70-130
70-130
70-130
1.9
1.5
1.7
1.8
1.9
1.5
1.8
1.7
1.5
1.5
1.7
1.7
1.5
1.0
1.9
1.7
1.6
1.9
1.5
1.8
1.6
1.8
1.6
1.9
1.8
1.6
1.8
1.6
1.8
1.7
1.5
Analyzed
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28115 11:47
12/28115 11:47
12/28115 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11 A7
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
12/28/15 11:47
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 21288
(336)623-8921
Qualifiers
LABORATORY CONTROL SAMPLE: 1638073
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 18.2 91 52-162
1,1,2,2-Tetrachloroethane ug/L 20 19.0 95 46-157
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to Me right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical services, Inc.. Page 18 of 37
acmnalytical
%".paoelabs.com
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
LABORATORY CONTROL SAMPLE:
1638073
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,1,2-Trichloroethane
ug/L
20
18.2
91
52-150
1,1-Dichloroethane
ug/L
20
19.3
97
59-155
1,1-Dichloroethene
ug/L
20
19.0
95
1-234
1,2-Dichlorobenzene
ug/L
20
17,8
89
18-190
1,2-Dichloroethane
ug/L
20
18.0
90
49-155
1,2-Dichloropropane
Ug/L
20
17.6
88
1-210
1,3-Dichlorobenzene
ug/L
20
18.4
92
59-156
1,4-Dichlorobenzene
ug1L
20
19.1
96
18-190
Benzene
ug/L
20
17.7
88
37-151
Bromodichioromethane
ug/L
20
19.4
97
35-155
Bromoform
ug/L
20
17.7
88
45-169
Bromomethane
ug1L
20
20.6
103
1-242
Carbon tetrachloride
ug1L
20
20.0
100
70-140
Chlorobenzene
ug/L
20
18.9
94
37-160
Chloroethane
ug/L
20
18A
92
14-230
Chloroform
ug/L
20
19.4
97
51-138
Chloromethane
ug/L
20
24.5
122
1-273
cis- 1.2-Dichloroethene
ug/L
20
20.1
101
68-146
cis- 1,3-Dichloropropene
ug/L
20
17.3
86
1-227
Dibromochloromethane
ug/L
20
19.4
97
53-149
Ethylbenzene
ug/L
20
18.1
91
37-162
Methylene Chloride
ug/L
20
26.5
133
1-221
Tetrachloroethene
ug/L
20
16.5
83
64-148
Toluene
ug/L
20
19A
95
47-150
trans-1,2-Dichloroethene
ug/L
20
20A
101
54-156
trans-1,3-Dichloropropene
ug/L
20
17.2
86
17-183
Trichloroethene
ug/L
20
18.1
91
71-157
Trichlorolluoromethane
ug1L
20
20.0
100
17-181
Vinyl chloride
ug/L
20
20.2
101
1-251
1,2-Dichloroethane-d4 (S)
%
102
70-130
4-Bromofluorobenzene (S)
%
108
70-130
Toluene -dB (S)
%
102
70-130
MATRIX SPIKE SAMPLE.
1638075
92280364003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits
1,1,1-Trichloroethane
ug/L
ND
20
22.1
111
46-171
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20.0
100
73-159
1,12-Trichloroethane
ug1L
ND
20
22.6
113
64-152
1,1-Dichloroethane
ug/L
ND
20
20.2
101
43-172
1,1-Dichloroethene
ug/L
ND
20
19.6
98
48-189
1,2-Dichlorobenzene
ug/L
ND
20
19.8
99
54-154
1,2-Dichloroethane
ug/L
ND
20
20.8
104
42-171
1,2-Dichloropropane
ug/L
ND
20
20.3
101
55-157
1,3-Dichlorobenzene
ug/L
ND
20
20.9
104
57-148
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/0412016 10:43 AM without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 19 of 37
aceAnalXical.
*WWpaceratu.com
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 2t288
(336)623.8921
MATRIX SPIKE SAMPLE:
1638075
92280364003
Spike
MS
MS
% Rec
Parameter
Units
Result
Cone.
Result
%Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
NO
20
20.9
105
58-149
Benzene
uglL
NO
20
22.0
110
54-163
Bromodichloromethane
ug/L
NO
20
22A
112
56-152
Bromoform
ug/L
NO
20
17.4
87
53-151
Bromomethane
ug/L
ND
20
12.8
64
10-200
Carbon tetrachloride
uglL
ND
20
23.3
117
41-175
Chlorobenzene
uglL
ND
20
21.9
109
67-152
Chloroethane
uglL
NO
20
20.7
104
23-200
Chloroform
ug/L
ND
20
22.1
110
51-166
Chioromethane
uglL
NO
20
22.7
113
40-175
cis-1,2-Dichloroethene
uglL
NO
20
19.9
99
45-174
cis- 1,3-Dichloropropene
ug/L
NO
20
20.3
102
38-146
Dibromochloromethane
ug/L
NO
20
20.8
104
65-144
Ethylbenzene
uglL
NO
20
20.7
104
57-152
Methylene Chloride
uglL
NO
20
25.4
124
40-167
Tetrachloroethene
uglL
NO
20
21.3
106
59-155
Toluene
ug1L
NO
20
21.6
108
47-162
trans-1,2-Dichloroethene
uglL
NO
20
19.6
98
47-178
Irans-1,3-Dichloropropene
uglL
NO
20
19.5
98
39.148
Trichloroethene
uglL
NO
20
21.9
110
60-153
Trichlorofluoromethane
ug/L
NO
20
19.9
100
42-199
Vinyl chloride
ug/L
NO
20
20.6
103
46-176
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
101
70-130
SAMPLE DUPLICATE: 1638074
Parameter
Units
92280364002
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1-Trichloroethane
ug/L
ND
NO
30
1,1,2,2-Tetrachloroethane
uglL
NO
NO
30
1,1,2-Trichloroethane
ug1L
ND
ND
30
1,1-Dichloroethane
uglL
ND
NO
30
1,1-Dichloroethene
uglL
NO
ND
30
1,2-Dichlorobenzene
uglL
NO
ND
30
1,2-Dichloroethane
uglL
NO
ND
30
1,2-Dichloropropane
uglL
NO
ND
30
1,3-Dichlorobenzene
uglL
NO
ND
30
1,4-Dichlorobenzene
uglL
NO
NO
30
Benzene
uglL
ND
ND
30
Bromodichloromethane
uglL
NO
ND
30
Bromoform
uglL
ND
NO
30
Bromomethane
uglL
ND
NO
30
Carbon tetrachloride
uglL
ND
NO
30
Chlorobenzene
ug/L
ND
NO
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, rnc.. Page 20 of 37
•
acmnalytical
wwwpacelabs.00m
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
SAMPLE DUPLICATE: 1638074
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
Parameter
Units
92280364002
Result
Dup
Result
Max
RPD RPD Qualifiers
Chloroethane
ug/L
NO
NO
30
Chloroform
ug/L
NO
NO
30
Chloromethane
ug/L
NO
NO
30
cis- 1,2-Dichloroethene
ug/L
NO
NO
30
cis- 1,3-Dichloropropene
ug/L
NO
NO
30
Dibromochloromethane
ug/L
ND
NO
30
Ethylbenzene
ug1L
NO
NO
30
Methylene Chloride
ug/L
NO
NO
30
Tetrachloroethene
ug1L
NO
NO
30
Toluene
ug/L
ND
NO
30
trans- 1,2-Dichloroethene
ug1L
NO
NO
30
trans- 1,3-Dichloropropene
ug1L
NO
NO
30
Trcchloroethene
ug1L
ND
NO
30
Trichlorofluoromethane
ug1L
ND
NO
30
Vinyl chloride
ug/L
ND
NO
30
1,2-Dichloroethane-d4 (S)
%
99
96
3
4-Bromofluorobenzene (S)
%
106
111
5
Toluene-d8 (S)
%
108
106
3
Results presented on this page are In the units indicated by the "units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc..
Page 21 of 37
aceAnalytical e
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QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
QC Batch: OEXT/39877 Analysis Method: EPA 608
QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB
Associated Lab Samples: 92280364001, 92280364002, 92280364003
METHOD BLANK: 1634138 Matrix: Water
Associated Lab Samples: 92280364001, 92280364002, 92280364003
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
4,4'-DDD
ug/L
ND
0.050
0.050
12/23/15 04:25
4,4'-DDE
ug1L
ND
0.050
0,050
12/23/15 04:25
4,4'-DDT
ug1L
ND
0.050
0,050
12/23/15 04:25
Aldrin
ug1L
NO
0.050
0.050
12/23/15 04:25
alpha-BHC
ug/L
ND
0.050
0.050
12/23/15 04:25
beta-8HC
ug1L
ND
0.050
0,050
12/23115 04:25
Chlordane (Technical)
ug/L
ND
0.50
0.50
12/23/15 04:25
delta-BHC
ug/L
ND
0.050
0.050
12/23115 04:25
Dieldrin
ug1L
NO
0.050
0.050
12/23/15 04:25
Endosulfan I
ug1L
NO
0.050
0.050
12/23/15 04:25
Endosulfan II
ug/L
NO
0.050
0.050
12/23/15 04:25
Endosulfan sulfate
ug/L
NO
0.050
0.050
12/23/15 04.25
Endrin
ug/L
NO
0.050
0.050
12/23/15 04:25
Endrin aldehyde
ug1L
NO
0.050
0.050
12/23/15 04:25
gamma-BHC (Lindane)
ug1L
NO
0.050
0.050
12/23/15 04:25
Heptachlor
ug1L
ND
0.050
0.050
12/23/15 04:25
Heptachlor epoxide
ug1L
ND
0.050
0,050
12/23/15 04:25
PCB-1016 (Aroclor 1016)
ug1L
NO
0.50
0.50
12/23/15 04:25
PCB-1221 (Aroclor 1221)
ug1L
ND
0.50
0.50
12/23/15 04:25
PCB-1232 (Aroclor 1232)
ug1L
NO
0.50
0.50
12/23/15 04:25
PCB-1242 (Aroclor 1242)
ug1L
ND
0.50
0.50
12/23/15 04:25
PCB-1248 (Aroclor 1248)
ug/L
ND
0.50
0.50
12/23/15 04:25
PCB-1254 (Aroclor 1254)
ug/L
ND
0.50
0.50
12/23/15 04:25
PCB-1260 (Aroclor 1260)
ug1L
NO
0.50
0.50
12/23/15 04:25
Toxaphene
ug/L
NO
0.50
0.50
12/23/15 04:25
Decachlorobiphenyl (S)
%
79
20-138
12/23115 04:25
Teirachloro-m-xylene (S)
%
62
20-110
12/23/15 04:25
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 2f288
(336)623.8921
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1634139
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
.25
0.26
106
31-141
4,4'-DDE
ug1L
.25
0.22
87
30-145
4,4'-DDT
ug1L
.25
0.18
72
25-160
Aldrin
ug/L
.25
0,18
72
42-122
alpha-BHC
ug1L
.25
0.21
86
37-134
beta-8HC
ug1L
.25
0.21
85
17-147
delta-BHC
ug1L
.25
0.23
91
19-140
Dieldrin
ug1L
.25
0.22
91
36-146
Endosulfan I
ug1L
.25
0.21
86
45-153
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 01 /0412016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 22 of 37
aceAnalytical
wwwpacelabacorri
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
LABORATORY CONTROL SAMPLE:
Parameter
1634139
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Endosulfan II
ug/L
.25
0.23
95
1-202
Endosulfan sulfate
ug1L
.25
0.23
91
26-144
Endrin
ug1L
.25
0.24
96
30-147
Endrin aldehyde
ug1L
.25
0,19
76
50-150
gamma-BHC (Lindane)
ug/L
.25
0.21
86
32-127
Heptachlor
ug/L
.25
0A 8
75
34-111
Heptachlor epoxide
ug1L
.25
0.21
83
41-126
Decachlorobiphenyl (S)
%
74
20-138
Tetrachloro-m-xylene (S)
%
77
20-110
MATRIX SPIKE SAMPLE:
Parameter
1634140
Units
92280364002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
ND
.25
0.23
91
31-141
4,4'-DDE
ug/L
ND
.25
0A8
74
30-145
4,4'-DDT
ug/L
ND
.25
0.17
68
25-160
Aldrin
ug1L
ND
.25
0.16
63
42-122
alpha-SHC
ug1L
ND
.25
0.19
76
37-134
beta-BHC
ug/L
ND
.25
0.20
81
17-147
delta-BHC
ug/L
ND
.25
0.21
84
19.140
Dieldrin
ug/L
ND
.25
0,20
82
36-146
Endosulfan I
ug/L
ND
.25
0.19
79
45-153
Endosulfan II
ug/L
ND
.25
0,22
90
1-202
Endosulfan sulfate
ug/L
ND
.25
0.23
94
26-144
Endrin
ug/L
ND
.25
0.22
88
30-147
Endrin aldehyde
ug/L
ND
.25
0.20
80
50-150
gamma-BHC (Lindane)
uglL
ND
.25
0.19
78
32-127
Heptachlor
ug/L
ND
.25
0.16
64
34-111
Heptachlor epoxide
ug/L
ND
.25
0.18
74
41-126
Decachlorobiphenyl (S)
%
37
20-138
Tetrachloro-m-xylene (S)
%
69
20-110
Results presented on this page are In the units Indicated by the -hits" column except where art alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shad not be reproduced, except in full,
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 23 of 37
aceAnalytical
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QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
QC Batch: QEXT139843 Analysis Method: EPA 625
QC Batch Method: EPA625 Analysis Description: 625 MSS
Associated Lab Samples: 92280364001, 92280364002, 92280364003
METHOD BLANK: 1632654 Matrix:
Associated Lab Samples: 92280364001, 92280364002, 92280364003
Blank
Parameter Units Result
Water
Reporting
Limit
MOL
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
0.98
12/2111514:22
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.3
12/2111514:22
2,4-Dichlorophenol
ug/L
ND
5.0
1.7
12/2111514:22
2,4-Dimethylphennl
ug/L
ND
10.0
1.2
12/2111514:22
2,4-Dinitrophenol
ug/L
ND
50.0
9.0
12/21/15 14:22
2,4-Dinitrotoluene
ug/L
ND
5.0
0.90
12121/1514:22
2,6-Dinitrotoluene
ug/L
ND
5.0
0.98
12121/1514:22
2-Chloronaphihalene
ug/L
ND
5.0
0.98
12121/1514:22
2-Chlorophenol
ug/L
ND
5.0
1.3
12121/1514:22
2-Nitrophenol
ug/L
ND
5.0
0.91
12121/1514:22
3,3'-Dichlorobenzidine
ug/L
ND
25.0
2.1
12/2111514:22
4,6-Dinitro-2-meth ylphenol
ug/L
ND
20.0
2.6
12/2111514.22
4-Bromophenylphenyl ether
ug1L
ND
5.0
0.82
12/21/15 14:22
4-Chloro-3-methylphenol
ug1L
ND
5.0
3.7
12/2111514:22
4-Chlorophenylphenyl ether
ug1L
ND
5.0
0.87
12/21/15 14:22
4-Nitrophenol
ug/L
ND
50.0
4.1
1212111514:22
Acenaphthene
ug1L
ND
5.0
0,25
12/2111514:22
Acenaphthylene
ug1L
ND
5.0
0.21
12/2111514:22
Anthracene
ug1L
ND
5.0
0.14
12/2111514:22
Benzo(a)anthracene
ug1L
ND
5.0
0.33
1212111514:22
Benzo(a)pyrene
ug1L
ND
5.0
0.30
12/21/15 14:22
Benzo(b)fluoranthene
ug/L
ND
5.0
0.28
12/2111514:22
Benzo(g,h,i)perylene
ug1L
ND
5.0
0.38
12/2111514:22
Benzo(k)fluoranthene
ug1L
ND
5.0
0.43
12/21/15 14:22
bis(2-Chloroethoxy)methane
ug1L
ND
10.0
0.92
12/2111514:22
bis(2-Chloroethyl) ether
ug/L
ND
5.0
1.0
12/21/15 14:22
bis(2-Chloroisopropyl) ether
ug/L
ND
5.0
0.95
12/21/15 14:22
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
0.79
12/21/15 14:22
Butylbenzylphthalate
ug1L
ND
5.0
0.79
12/21/15 14:22
Chrysene
ug/L
ND
5.0
0.21
12121/1514:22
Di-n-butylphthalate
ug1L
ND
5.0
0,75
12/21/15 14:22
Di-n-octylphthalate
ug/L
ND
5.0
0.66
12121/1514:22
Dibenz(a,h)anlhracene
ug/L
ND
5.0
0.55
1212111514:22
Diethylphtha late
ug/L
ND
5.0
0,58
12/21/15 14:22
Dimethylphthalate
ug/L
ND
5.0
0.76
12/2111514:22
Fluoranthene
ug/L
ND
5.0
0.21
12121/1514:22
Fluorene
ug/L
ND
5.0
0,21
12/21/15 14:22
Hexachloro-1,3-butadiene
ug/L
ND
5.0
0.94
12/2111514:22
Hexachlorobenzene
ug1L
ND
5.0
0.72
12/21/15 14:22
Hexachlorocyclopentadiene
ug1L
ND
10.0
0,88
12/2111514:22
Hexachloroethane
ug1L
ND
5.0
1.1
1212111514:22
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 23288
(336)623-8921
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full,
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 24 of 37
aceAnalytical
*Ww.P&X0b$ com
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
METHOD BLANK: 1632654
Matrix: Water
Associated Lab Samples: 92280364001,
92280364002, 92280364003
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Indeno(1,2,3-cd)pyrene
ug1L
NO
5.0
0.29
12121/1514:22
Isophorone
ug/L
NO
10.0
0.89
12/2111514:22
N-Nitroso-di-n-propylamine
ug1L
NO
5.0
0,99
12/2111514:22
N-Nitrosodimethylamine
ug1L
NO
5.0
0.91
12/2111514:22
N-Nitrosodiphenylamine
ug1L
NO
10.0
1.0
12/2111514:22
Naphthalene
ug1L
NO
5.0
0.34
12/2111514:22
Nitrobenzene
uglL
NO
5.0
1.1
12/2111514:22
Pentachlorophenol
uglL
NO
10.0
4.6
12/2111514722
Phenanthrene
uglL
NO
5.0
0.22
12/2111514:22
Phenol
uglL
NO
5.0
1.9
12/2111514:22
Pyrene
ug1L
NO
5.0
0.19
12121/1514:22
2,4,6-Tribromophenol (S)
%
82
10-137
12/21/15 14:22
2-Fluorobiphenyl (S)
%
64
15-120
12/21/15 14:22
2-Fluorophenol (S)
%
38
10-120
12/21/15 14:22
Nitrobenzene-d5 (S)
%
73
10-120
12/21/15 14:22
Phenol-d6 (S)
%
25
10-120
12/21/15 14:22
Terphenyl-d14 (S)
%
83
11-131
12/21/15 14:22
LABORATORY CONTROL SAMPLE:
Parameter
1632655
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
uglL
50
34.5
69
44-142
2,4,6-Trichlorophenol
ug1L
50
44.0
88
37-144
2,4-Dichlorophenol
ug1L
50
39.7
79
1-191
2,4-Dimethylphenol
ug1L
50
41.0
82
32-119
2,4-Dinitrophenol
ug1L
250
253
101
1-181
2,4-Dinitrotoluene
uglL
50
44.8
90
39-139
2,6-Dinitrotoluene
uglL
50
42.6
85
50-158
2-Chloronaphthalene
uglL
50
39.2
78
60-118
2-Chlorophenol
ug1L
50
36.0
72
23-134
2-Nitrophenol
uglL
50
40.4
81
29-182
3,3'-Dichlorobenzidine
uglL
100
83.8
84
1-262
4,6-Dinitro-2-methylphenol
ug1L
100
98.7
99
1-181
4-Bromophenylphenyl ether
ug1L
50
40.5
81
53-127
4-Chloro-3-methylphenol
uglL
100
80.3
80
22-147
4-Chlorophenylphenyi ether
ug1L
50
40.2
80
25-158
4-Nitrophenol
ug1L
250
105
42
1-132
Acenaphthene
ug1L
50
41.3
83
47-145
Acenaphlhylene
uglL
50
41.3
83
33-145
Anthracene
ug1L
50
47.0
94
1-166
Benzo(a)anthracene
uglL
50
46.0
92
33-143
Benzo(a)pyrene
uglL
50
43.3
87
17-163
Benzo(b)Fluoranthene
uglL
50
42.7
85
24-159
Benzo(g,h,i)perylene
uglL
50
40.4
81
1-219
Pace Analytical Services, Inc.
205 East Meadow Road • Suite A
Eden, NC 27288
(33f3]f323-8921
Qualifiers
Qualifiers
Results presented on this page are in the unite indicated by the 'Units- column except where an alternate unit is presented to the right of the result -
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 25 of 37
s
acmnalytical
www.p"abs.c=
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336}623-8921
LABORATORY CONTROL SAMPLE:
1632655
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
%Rec
Limits
Qualifiers
Benzo(k)Auoranlhene
ug/L
50
52.0
104
11.162
bis(2-Chloroethoxy)methane
ug/L
50
37.9
76
33-194
bis(2-Chloroethyl) ether
ug/L
50
37.5
75
12-158
bis(2-Chloroisopropyl) ether
ug1L
50
25.5
51
36-166
bis(2-Elhylhexyl)phthalate
ug1L
50
46.5
93
8-158
Butylbenzylphthalate
ug/L
50
45.3
91
1-152
Chrysene
ug1L
5o
47.5
95
17-168
Di-n-bulylphthalate
ug/L
50
46.1
92
1-118
Di-n-octylphthalate
uglL
50
43.7
87
4-146
Dibenz(a,h)anthracene
ug/L
50
43.0
86
1-227
Diethylphthalate
ug1L
50
43.9
88
1-114
Dimethylphthalate
ug1L
50
43.2
86
1-112
Fluoranthene
ug1L
50
46.9
94
26-137
Fluorene
ug1L
50
45.0
90
59-121
Hexachloro-1,3-butadiene
ug/L
50
31.4
63
24-116
Hexachlorobenzene
ug1L
50
46.1
92
1-152
Hexachlorocyclopentadiene
ug1L
50
41.7
83
25-150
Hexachloroethane
ug/L
50
29.3
59
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
44.2
88
1-171
Isophorone
ug/L
50
38.7
77
21-196
N-Nitroso-di-n-propylamine
ug/L
50
38.9
78
1-230
N-Nitrosodimethylamine
ug/L
50
26.1
52
25-150
N-Nitrosodiphenyla mine
ug/L
50
40.3
81
25-150
Naphthalene
ug/L
50
35.8
72
21-133
Nitrobenzene
ug/L
50
38.6
77
35-180
Pentachlorophenol
ug/L
100
102
102
14-176
Phenanthrene
ug/L
50
43.3
87
54-120
Phenol
ug/L
50
17.3
35
5-112
Pyrene
ug/L
50
46.1
92
52-115
2,4,6-Tribromophenol (S)
%
91
10-137
2-Fluorobiphenyl (S)
%
77
15-120
2-Fluorophenol (S)
%
44
10-120
Nitrobenzene-d5 (S)
%
79
10-120
Phenol-d6 (S)
%
30
10-120
Terphenyl-d14 (S)
%
87
11-131
MATRIX SPIKE SAMPLE:
1632656
92280303010
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
ND
50
22.0
44
44-142
2,4,6-Trichlorophenol
ug/L
ND
50
30.6
61
37-144
2,4-Dichlorophenol
ug/L
ND
50
23.9
48
1-191
2,4-Dimethylphenol
u91L
ND
50
24.1
48
32-119
2,4-Dinitrophenol
ug/L
ND
250
174
70
1-181
2,4-Dinitrotoiuene
ug/L
ND
50
36.5
77
39-139
Results presented on this page are In the units indicated by the "Units- column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 26 of 37
m
acmnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
MATRIX SPIKE SAMPLE: 1632656
92280303010 Spike MS
Parameter Units Result Conc. Result
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
MS % Rec
% Rec Limits Qualifiers
2,6-Dinitrotoluene
ug1L
ND
50
33.7
67
50-158
2-Chloronaphthalene
ug1L
ND
50
23.5
47
60-118 M1
2-Chlorophenol
ug1L
ND
50
20.2
40
23-134
2-Nitrophenol
ug1L
ND
50
22.5
45
29-182
3,3'-Dichlorobenzidine
ug1L
ND
100
59.2
59
1-262
4,6-Dinitro-2-methylphenol
ug1L
ND
100
76.3
76
1-181
4-Bromophenylphenyl ether
ug1L
ND
50
33.0
66
53-127
4-Chloro-3-methylphenol
ug1L
ND
100
63.5
64
22-147
4-Chlorophenylphenyl ether
ug1L
ND
50
30.5
61
25-158
4-Nitrophenol
ug/L
ND
250
86.9
35
1-132
Acenaphthene
ug/L
ND
50
27.9
56
47-145
Acenaphthylene
ug/L
ND
50
28.9
58
33-145
Anthracene
ug/L
ND
50
38.8
78
1-166
Benzo(a)anthracene
ug/L
ND
50
38.6
77
33-143
Benzo(a)pyrene
ug/L
ND
50
36.0
72
17-163
Senzo(b)fluoranthene
ug/L
ND
50
36.0
72
24-159
Benzo(g,h,i)perylene
ug/L
NO
50
34.0
68
1-219
Senzo(k)fluoranthene
ug/L
ND
50
42.5
85
11-162
bis(2-Chloroethoxy)methane
ug/L
ND
50
21.2
42
33-184
bis(2-Chloroethyl)ether
ug/L
ND
50
21A
43
12-158
bis(2-Chtoroisopropyl) ether
ug/L
ND
50
14.8
30
36-166 M1
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
38.7
77
B-158
Butylbenzylphtha late
ug/L
ND
50
38.6
77
1-152
Chrysene
ug/L
ND
50
40.2
80
17-168
Di-n-butylphthalate
ug/L
ND
50
39.7
79
1-118
Di-n-octylphthalate
ug1L
ND
50
39.8
80
4-146
Dibenz(a,h)anth racene
ug/L
ND
50
35.2
70
1-227
Diethylphthalate
ug1L
ND
50
37.6
75
1-114
Dimethylphthalate
ug1L
ND
50
35.1
70
1-112
Fluoranthene
ug1L
ND
50
40.6
81
26-137
Fluorene
ug1L
ND
50
34.1
68
59-121
Hexachloro-1,3-butadiene
ug1L
ND
50
21.1
42
24-116
Hexachlorobenzene
ug1L
ND
50
38.6
77
1-152
Hexachlorocyclopentadiene
ug1L
ND
50
15.0
30
25-150
Hexachloroethane
ug1L
ND
50
19.5
39
40-113 M1
Indeno(1,2,3-cd)pyrene
ug1L
ND
50
35.0
70
1-171
Isophorone
ug1L
ND
50
21.8
44
21-196
N-Nitroso-di-n-propylamine
ug1L
ND
50
22.0
44
1-230
N-Nitrosodimethylamine
ug/L
ND
50
15.5
31
25-150
N-Nitrosodiphenylamine
ug1L
ND
50
33.9
68
25-150
Naphthalene
ug1L
ND
50
22.6
45
21-133
Nitrobenzene
ug1L
ND
50
22.7
45
35-180
Pentachlorophenol
ug/L
ND
100
65.7
66
14-176
Phenanthrene
ug/L
ND
50
36.7
73
54-120
Phenol
ug/L
ND
50
10A
21
5-112
Pyrene
ug/L
ND
50
36.2
72
52-115
2,4,6-Tribromophenol (S)
%
72
10-137
Results presented on this page are in the units indicated by the "Unite" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 27 of 37
aceAnalytical o
wowpacelabs mn
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623.8921
MATRIX SPIKE SAMPLE:
1632656
92280303010 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
2-Fluorobiphenyl (S)
%
44
15-120
2-Fluorophenol (S)
%
25
10-120
Nitrobenzene-d5 (S)
%
46
10-120
Phenol-d6 (S)
%
17
10-120
Terphenyl-d14 (S)
%
55
11-131
SAMPLE DUPLICATE: 1632657
Parameter
Units
92280303011
Result
Dup
Result RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzone
ug/L
NO
NO
30
2,4,6-Trichtorophenol
ug/L
NO
NO
30
2,4-Dichlorophenol
ug/L
NO
NO
30
2,4-Dimethylphenol
ug/L
NO
NO
30
2,4-Dinitrophenol
ug/L
NO
NO
30
2,4-Dinitrotoluene
ug/L
ND
NO
30
2,6-Dinitrotoluene
ug/L
NO
ND
30
2-Chloronaphthalene
ug/L
ND
ND
30
2-Chlorophenot
ug1L
NO
ND
30
2-Nitrophenol
ug/L
NO
ND
30
3,3'-Dichlorobenzidine
ug1L
NO
ND
30
4,6-Dinitro-2-methylphenol
ug/L
NO
ND
30
4-Bromophenylphenyl ether
ug/L
NO
NO
30
4-Chloro-3-methylphenol
ug/L
NO
NO
30
4-Chlorophenylphenyi ether
ug/L
NO
NO
30
4-Nilrophenol
uglL
NO
NO
30
Acenaphthene
uglL
ND
NO
30
Acenaphthyiene
ug1L
ND
NO
30
Anthracene
uglL
NO
NO
30
Benzo(a)anthracene
uglL
NO
NO
30
Benzo(a)pyrene
uglL
NO
ND
30
Benzo(b)fluoranthene
ug/L
NO
ND
30
Benzo(g,h,i)perylene
ug/L
NO
ND
30
Benzo(b)fluoranthene
ug/L
NO
ND
30
bis(2-Chloroethoxy)methane
ug1L
NO
NO
30
bis(2-Chloroethyl) ether
ug1L
ND
NO
30
bis(2-Chloroisopropyr) ether
ug1L
ND
NO
30
bis(2-Ethylhexyl)phthalate
ug1L
ND
NO
30
Butylbenzylphthalate
ug1L
1.3J
NO
30
Chrysene
ug1L
ND
NO
30
Di-n-butylphthalate
uglL
ND
NO
30
Di-n-octylphthalate
ug1L
ND
NO
30
Dibenz(a,h)anthracene
uglL
NO
NO
30
Diethylphthalate
ug/L
NO
NO
30
Dimethylphtha late
ug/L
NO
NO
30
Fluoranthene
ug/L
NO
NO
30
Results presented on this page are In the units Indicated by the "Units" colurno except where an alternate unit Is presented to the right at the result -
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc..
Page 28 of 37
aceAnalytical
www.pacelabs.cam
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
SAMPLE DUPLICATE: 1632657
Parameter
Units
92280303011
Result
Dup
Result
Fluorene
ug1L
N❑
ND
Hexachloro-1,3-butadiene
uglL
ND
NO
Hexachlorobenzene
uglL
NO
NO
Hexachlorocyclopentadiene
uglL
NO
NO
Hexachloroethane
ug1L
NO
ND
Indeno(1,2,3-cd)pyrene
ug1L
ND
NO
Isophorone
ug1L
ND
ND
N-Nitroso-di-n-propylamine
ug1L
NO
ND
N-Nitrosodimethylamine
ug1L
ND
ND
N-Nitrosodiphenylamine
ug1L
ND
ND
Naphthalene
ug1L
ND
NO
Nitrobenzene
ug1L
ND
NO
Pentachlorophenol
uglL
NO
NO
Phenanthrene
ug/L
NO
NO
Phenol
ug/L
NO
ND
Pyrene
ug/L
NO
ND
2,4,6-Tribromophenol (S)
%
71
84
2-Fluorobiphenyl (S)
%
63
69
2-Fluorophenol (S)
%
33
39
Nitrobenzene-d5 (S)
%
62
69
Phenol-d6 (S)
%
22
27
Terphenyl-d14 (S)
%
70
71
RPD
16
9
17
11
19
1
Max
RPD
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the resutL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical Services, Inc..
Page 29 of 37
acmnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
QC Batch: WET142117
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended
Solids
Associated Lab Samples: 92280364001,
92280364002
METHOD BLANK: 1635025
Matrix:
Water
Associated Lab Samples: 92280364001,
92280364002
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifefs
Total Suspended Solids
mg1L
ND
2.5
2.5 12121/15 23:04
LABORATORY CONTROL SAMPLE: 1635026
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Total Suspended Solids
mg1L
250
272
109
90-110
SAMPLE DUPLICATE: 1635027
92280512005
Dup
Max
Parameter
Units
Result
Result
RPD
RPD Qualifiers
Total Suspended Solids
mg1L
ND
ND
5
SAMPLE DUPLICATE: 1635028
92280235002
Dup
Max
Parameter
Units
Result
Result
RPD
RPD Qualifiers
Total Suspended Solids
mg1L
29.3
25.3
15 5 D6
Results presented on this page are in the units indicated by the -Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01104/2016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 30 of 37
Pace Analytical Services, Inc.
aceAnalytical ® 205 East Meadow Road - Suite A
Eden, NC 27288
wwwpacel ftcorrr
(336)623-8921
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
QC Batch: WET142128 Analysis Method: SM 2540D
QC Batch Method: SM 25400 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92280364003
METHOD BLANK: 1635431 Matrix: Water
Associated Lab Samples: 92280364003
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 2.5 12/22/15 13:29
LABORATORY CONTROL SAMPLE: 1635432
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 246 98 90-110
SAMPLE DUPLICATE: 1635433
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 1635434
Parameter
Total Suspended Solids
92280364003 Dup
Units Result Result
mg1L ND ND
92280387001 Dup
Units Result Result
mg/L 7.8 8.0
Max
RPD RPD Qualifiers
5
Max
RPD RPD Qualifiers
3 5
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2016 10:43 AM without the written consent of Pace Analytical services, Inc.. Page 31 of 37
aceAnalytical
www.pacelabs.own
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)523-8921
QC Batch: WET142094 Analysis Method: EPA9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92280364001. 92280364002
SAMPLE DUPLICATE: 1634108
92280338001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH Std. Units 8.6 8.6 0 9 H6
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/0412016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 32 of 37
m
acmnalytical
www.pacelabs.=n
QUALITY CONTROL DATA
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
QC Batch: WET142121 Analysis Method: EPA9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92280364003
SAMPLE DUPLICATE: 1635112
Parameter
pH
92280576004 Dup
Units Result Result
Std. Units 6.6 6.7
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 272M
(336)623-8921
Max
RPD RPD Qualifiers
2 9 D6,H6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of pre result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/04/2016 10A3 AM without the written consent of Pace Analytical Services, Inc.. Page 33 of 37
acmnalytical.
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QUALIFIERS
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOIL -Adjusted Method Detection Limit.
PQL - Practical Quanlitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(0) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyle is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01104/2016 10:43 AM without the written consent of Pace Analytical Services, Inc.. Page 34 of 37
aceAnalytical
wwwpacelabxc=
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 2015 SEMI-ANNUAL
Pace Project No.: 92280364
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8921
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92280364001
GRAB 1
EPA 1664E
GCSV123640
92280364002
GRAB 2
EPA 1664B
GCSV123640
92280364003
GRAB 3
EPA 1664B
GCSV123640
92280364001
GRAB 1
EPA 3510
OEXT139877
EPA 608
GCSV123624
92280364002
GRAB 2
EPA 3510
OEXT139877
EPA 608
GCSV123624
92280364003
GRAB 3
EPA 3510
OEXT139877
EPA 608
GCSV123624
92280364001
GRAB 1
EPA 200.7
MPRP120326
EPA 200.7
ICP118344
92280364002
GRAB 2
EPA 200.7
MPRP120326
EPA 2003
ICP118344
92280364003
GRAB 3
EPA 200.7
MPRP120326
EPA 200.7
ICP118344
92280364001
GRAB
EPA 625
OEXTI39843
EPA625
MSSVl11684
92280364002
GRAB 2
EPA 625
OEXT/39843
EPA 625
MSSV111684
92280364003
GRAB 3
EPA 625
OEXT139843
EPA 625
MSSV111684
92280364001
GRAB 1
EPA 624
MSVI34964
92280364002
GRAB 2
EPA624
MSVI34964
92280364003
GRAB 3
EPA624
MSVI34964
92280364001
GRAB 1
SM 2540D
WETI42117
92280364002
GRAB 2
SM 2540D
WET142117
92280364003
GRAB 3
SM 2540D
WET142128
92280364001
GRAB 1
EPA 9040
WET142094
92280364002
GRAB 2
EPA 9040
WET142094
92280364003
GRAB 3
EPA 9040
WET142121
Date: 01l0412016 10:43 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 35 of 37
Document Name: Document Revised: 2fOCT2015
0017 aceAnalyticalO Sample Condition Upon Receipt(SCUR) Page of 2
Document No.: Issuing Authority:
F-CHR-CS-003-rev,17 Pace Huntersville Quality Office.
iN Client Name: Project #: ( LJO# ' 92280364
Courier: LIFed Ex Dun El USPS ieCi nt
❑Commercial ❑Pace ❑Other:
922603 111 � 111 111111�1
Custody Seal on Cooler/Box Present? ❑Yes No Seats Intact? Elves [)No I:
Packing Material: ub61e Wrap ❑ ubB b!e Bags ❑None []Other;
Thermometer T1505 None +I s oa ice coolie process has begun
Used: Type of Ice: et ❑efue ❑ [�$a p e g p g
Cooler Temp Corrected ('C): /f Biological Tissue Frozen? ❑Yes -,-..❑No :. ❑NJl�
Temp should be above freezing to 6°C Correction Factor: 0.01C Date and Initials of Person Examining.Cdntents:
USDA Regulated Soil (❑ N/A, water sample)
Did samples orloate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate frorfi'a'foreign source (internationally,
❑Yes []No including Hawaii and Puerto R16j?' .. ❑Yes ❑Na
If Yes to either question, fill out a Regulated Soil Checklist and include with .SCUR/COC paperwork. -
COMMENTS:
Chain of Custody Present?
0 es
ONo,
❑N/A
1.
Chain of Custody Filled Out?
es
No --❑N/A
2.
Chain of Custody Relinquished?
es
JoNo
❑N/A
3.
Sampler Name and/or Signature on COC?
13No
N/A
4.
Samples Arrived within Hold Time?
.'
[IN..
❑N/A
5.
Short Hold Time Analysis (<72 hr)?
❑Yes
Biuo
2 N/A
6.
Rush Turn Around Time Requested?
❑Yes
o
❑N/A
7.
Sufficient Volume?
Dfeos
❑No
❑N/A
8.
Correct Containers Used?
ee No
[]N/A
9.
-Pace Containers Used?
Dyes
` No
N/A
Containers Intact?
es
[]No
[:]N/A
0,
Filtered Volume Received for Dissolved Tests?
Dyes
❑No "
N/A
11.
Note If sediment is visible in the dissolved container
Sample Labels Match COC?
El Yes
No
❑N/A
12.
+ r , sn rL(J'
-Includes Date/Tlme/ID/Analysis Matrix:
J/ Mu fl M C.
All containers needing acid/base preservation have been
checked?
Elves
❑No
[]N/A13.
All containers needing preservation are found to be in
compliance with EPA recommendation?
ZY'011o
(HNO3, H2SO4, HCt<2; NaOH >9 Sulfide, NaOH>12 Cyanide)
❑N/A
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC,LLHg
Yes
❑No
❑N/A
Samples checked for dechlorization
nyes
❑No
❑N/A
14.
Headspace in VOA Vials (>5.6mm)?
❑Yes
[]No
❑N/A
15.
Trip Blank Present?
❑Yes
❑No
❑ /
16.
Trip Blank Custody Seals Present?
[]Yes
[]No
(]N/A
Pace Trip Blank Lot P (if purchased):
CLIENT NOV FICATION/RESOLUTION
Person Contacted:
Comments/Resolution;
Date/Time: .
Field Data,Required? ❑Yes ❑No
Project Manager SCURF Review: ,j bate: _ R/ _
Note: Whenever there is a discrepancy affecting North Carolina ca?npliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of
hold, incorrect preservative, out of temp, incorrect containers).
Page 36 of 37
CHAIN -OF -CUSTODY 1 Analytical Request Document
•-- The Chain -of -Custody is a LEGAL DOCILIMENT, All relevant fields must be completed accurately.
Section A Section B Section C
Requlred Client Information: Required Project Information: Invoice Infom7ation: Page 1 Of 1
Company SouVnrire - f0ffnerty A86 Report To. John m. Atlenitom
Address: 12331 Commerce Sialion Copy T7; Company Name: Sod .{.`
Hunlersville. NC 28078
Address: / 2 :3 31 ('�-�y y,�, _ .mot
R ulato A x
Email: hn,s.mopre southwire.com
Purchaseonlarv; r1��.• t{_- "C�[�,,.,
PawQuole;
Ali - &I= S
Phone: 704.371)-9626 Fax
Prclect Norse: 2016 Semi- Annual
Pace Project Manager; to lor.e=elt abs.com,
- - State I Location '
Requested Due Dale: �^, f
Project 0:
Pace Profile
V C
•
R
ted
Ana
is
Filtered
N
-'
a
2
wTRu CODE
Q
COLLECTED
z
Preservatives
}
a.�nP wws pw
wArr. ov:
8
m
�
weaw wv' ww
SAMPLE ID o �
=
D
START
END
m
One Character par box. w.w WP
..
a
m
=
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Sample
Same Idt muun must be ique Taw. �s
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a
m
m
p
of
T
y
rd
'Ift
to
C
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DATE
TIME
DATE
TIME
7,1
QT
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12
- ,- .-{ .'`� _AUOITTDNAL GDMMFJYT9: • ��a: Y�.r..'••
." RELJNCllISHFD F3Y l AFFlLU1TtON •k`-:'
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w- h :.r-^rF 'AGCEPTF� EIY f AFFIL1ATtON�*
DATE.
Y: _TtYE
"PLE CONDITIONS • .
SAMPLER NAME AND SIGNATURE ,- r`
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_
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PRINT Name of SAMPLER:�i1�lti
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SIGNATURE of SAMPLER•
/7 !
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a
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client:
Meritor
105 Wamsutta Mill Road
Morganton, NC 28655
Attention:
Ray Robinson
Date Received:
28-Sep-15
Report Date:
09-Oct-15
Sample Date:
25-Sep-15
BRL #:
BRI-2015-0761
Lab Sample ID:
LSID-2015-03087
Client Sample ID:
Outfall I
Parameter
TSS
�a
blueridgelabsienoir@gma il.com
Result MQL Unit Method
* 5.2 mall 2540D 1997
Analysis Analysis
Time Date Analyst
15:36 9/30/2015 l{CJ
Reported By:-
S. . Johnson, D.R. Wessinger
x Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No, 275
Page l of 9
Blue Ridge Labs
PO Box 2940
Le►zoir, NC 28645
828-728-0149 blueridgelabslenoir@gmail.com
Client :
Meritor
105 Wamslltta Mill Road
Morganton, NC 28655
Attention:
Ray Robinson
Date Received:
28-Sep-15
Report Date:
09-Oct-15
Sample Date:
25-Sep-I5
SRL P:
BR1-2015-0761
Lab Sample ID:
LSID-2015-03088
Client Sample ID:
Outfall 1
Analysis
Analysis
Parameter
Result
MQL
Unit
Method
Time
Date
Analyst
Cu
0.006
0.001
mg/l
200.7 1994
14:27
10/8/2015
KCJ
Pb
*
0.01
m&1l
200.7 1994
14:27
10/8/2015
KCJ
Zn
0.045
0.001
mg/1
200.7 1994
14:27
10/8/2015
KCJ
Z
Reported By:
S. J wson, D.R. Wessinger
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 2 of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client :
Meritor
105 WamSutta Mill Road
Morganton, NC 28655
Attention:
Ray Robinson
Date Received:
28-Sep-15
Report Date:
09-Oct-15
Sample Date:
25-Sep-15
BRI, #:
BRL-2015-0761
Lab Sample 1D.
LSID-2015-03089
Client Sample ID:
Outfall I
Parameter
Result MQL
Oil & Grease
* 5
blueridgelabsienoir@gmail.com
Unit Method
mg/l 1664-A 0&G
Analysis Analysis
Time Date Analyst
9/29/2015 WtrQtly
Reported By: >1
S. hnson, D.R. Wessinger
Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 3 of 9
Blue Ridge Labs
PO Box 2940
Leiroir, NC 28645
828-728-0149
Client ; Meritor
105 Wamsutta Mill Road
Morganton, NC 28655
Attention: Ray Robinson
blueridgela bslenoir@gma il.com
Date Received: 28-Sep-I5
Report Date: 09-Oct-15
Sample Date: 25-Sep-15
13RL #. BRL-2015-0761
Lab Sample ID: LSID-2015-03090
Client Sample ID: Outfall 2
Parameter Result MQL Unit Method
TSS 5.1 ing/I 2540D 1997
Analysis
Analysis
Time
Date
15:37
9/30/2015
Reported By: >E61 _ -
S. J. tinson, D.R. Wessinger
Concentrations are below Minimum Quantification Limit except where rioted.
NC Laboratory Certificate No, 275
Page 4 of 9
Analyst
KCJ
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client : Meritor
105 Wamsutta Mill Road
Morganton, NC 28655
Attention: Ray Robinson
Date Received: 28-Sep-15
Report Date:
09-Oct-15
Sample hate:
25-Sep-15
BR #:
13RL 2015-0761
Lab Sample 1D:
LSID-2015-03091
Client Sample ID:
OMNI 2
Parameter
CU
Pb
Z.11
Result
0.003
0.026
blueridgelabsienoir@gmaii.com
Analysis Analysis
MQL
Unit
Method
Time
Date
0.001
mg/l
200.7 1994
14:29
10/8/2015
0.01
mg/l
200.7 1994
14:29
1002015
0.001
mg/I
200.7 1994
14:29
10/8/2015
Reported By:
S. I Irnson, D.R. Wessinger
" Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 5 of 9
Analyst
KCJ
KCJ
KCJ
Blue Ridge.Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client:
Mentor
105 Wamsutta Mill Road
Morganton, NC 28655
Attention:
Ray Robinson
Date Deceived:
28-Selo- 15
Report Date:
09-Oct-15
Sample Date:
25-Sep- 15
BR1, 9:
BRL-2015-0761
Lab Sample ID:
LS1D-2015-03092
Client Sample ID:
Outfall 2
Parameter
Oil & Grease
blueridgelabslenoir@gmail.com
Result MQL Unit Method
5 mg/l 1664-A O&G
Analysis Analysis
Time Date Analyst
9/29/2015 WtrQtly
Reported By:
S.I >y�tj�(son, D.R. Wessinger —
Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 6 of 9
Blue Ridge Labs
PO Box 2940
Leizoir, NC 28645
828-728-0149
Client : Meritor
105 Wamsutta Mill Road
Morganton, NC 28655
Attention: Ray Robinson
Date Received: 28-Sep- 15
Report Date: 09-Oct-15
Sample Date: 25-Sep-15
BRL #: BRL-2015-0761
Lab Sample ID: LSID-2015-03093
Client Sample ID: Outfall 3
blueridgelabslenoir@gmail.com
Parameter Result MQL Unit Method
TSS 5.1 mg/I 2540D 1997
Analysis Analysis
Time Date Analyst
15:38 9/30/2015 KCJ
Reported y:
S. J. "son, D.R. Wessinger
Concentrations are below Minimum Quantification limit except where noted.
NC Laboratory Certificate No. 275
Page 7 of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client: Meritor
105 Wamsutta Mill Road
Morganton, NC 28655
Attention: Ray Robinson
bl€teridgelabslenoir@gmaii.com
Date Received:
28-Sep-15
Report Date:
09-Oct-15
Sample Date:
25-Sep-15
BRI, #:
BRL-2015-0761
Lab Sample ID:
[,S1D-2015-03094
Client Semple ID:
Otal'all 3
Analysis
Analysis
Parameter
Result
MQL
Unit
Method
Time
Datc
Analyst
Cn
0.006
0.001
mg/1
200.7 1994
14:32
10/8/2015
KC.I
Pb
x
0.01
mg/l
200.7 1994
14:32
10/8/2015
KCJ
Zn
0.061
0.001
mg/I
200.7 1994
14:32
10/8/2015
KCJ
Reported By:*.'f'Foi:.°'b'""""
S. J inson, D.R. Wessinger
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 8 of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client: Mentor
105 Wamstitta Mill Road
Morganton, NC 28655
Attention: Ray Robinson
blueridgelabslenoir@gmail.com
Date Received:
28-Sep-15
Report Date:
09-Oct-15
Sample Date:
25-Sep-15
BRI, #:
BRL-2015-0761
Lab Sample ID:
LSID-2015-03095
Client Sample ID:
Ontfall 3
Parameter
Result MQL Unit Method
Oil & Grease
5 mg/l 1664-A O&G
Analysis Analysis
"Time Date Analyst
9/29/2015 WtrQtly
Reported By: ? +'`a=a:.r"<`•:k
S. J. jo &6n, D.R. Wessinger
Concentrations are below Minimum Quantification Limitlexcept where noted.
NC Laboratory Certificate No. 275
Page 9 of 9
OCT/08/2015/TH0 02:15 FM F A ylL Ids, P. 001/1001
WATER QUALITY LAS & OPP-RATIONS, INC.
P.O. BOX 1167
BANNER ELK, NO 26604
(828) 898-6277
CLIENT: BLUE RIDGE LASS
ADDRESS: P.O, BOX 2940
CITY: LENOIR
STATE: NC ZIP 28645
ID#-.
REPORTED DATE:
a-Oct-i 5
AA -50
.......... ...............
...
ANALyt(t
.....
I iii
n$.0
. .....
......... ..
.......... :-:.,
........
.... .1A......
M
.T
OIL & GREASE
2841
45
5.00
MG/L
29-Sep-15
pf
OIL & GREASE
2892!
<5
5-00
J MGIL
29-Sep-1 51
PI I
OIL & GREASE
3070
<5
5.00
MG/L
29-5ep-15
Pi
OIL & GREASE
3078
<5
5,00
MGIL
29-Sep-I 5
PI
OIL & GREASE
30891
5.00
MG/L
129-Sep-15
P1
OIL & GREASE
3092
_<5
<5
5.00
MG/1-
29-Sap-1 5
Pi
OIL & GREASE
3095
<5
1 5.00
MG/L.
29-Sep-15
Pi
REPORTED BY: NC CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR
PCC1 o& Z
N13DS Reporting / Grol_mdwater
Report To:
f-kaztTufL r"e..
4 1-c- Lz
Blue Ridge Labs, Inc.
P.O. Box 2940
Lenoir, NC 28645
Telephone (828) 728-0149 Fax (828) 728-0131
Chain of Custody
Sanitary Landfili Hazardous Waste
UST/Trust Fund Reporting
Bill To:
dKt�ztip62 ti ,.� >~
_foS t.]A"ASy'lami Aim aU
f4o tZ GA-,TD t-le- dross
Field
IndustriaL or QC Non State Reporting ___
Project Name: San yje,�-_
PO Number:
Ice Present: Y N
Preservatives Lab Check
Time &
Field
Resid
Temp
Field
Sulfide
Chlor
Field
Sample ID
Sample
Date
Time
Sulfide
Present
Field
Dechlorination
pH
Resid
Temp
Sampler
Analysis Requested
Type
HR:MM
Cheek
Removed
Check
Chlor
°C
Initiais
°C
Y N
Y N
Y N
Y N
P or A
G
r ss
e�OT fF hL4-2
-�
ab Cv Z/V
f—o u-
t
iz. y
;3��,
o s
Pb cu Z
j2li
Relinquished By: Date:
,t2lk`t -ia k
Tirne: R*'B5.
D te: Time:
/✓ -
G,V pH
6 .-Vi'
(p XiAl
Upun submission ot'samples, client agrees that invoices are due at the time work is completed. Open accounts are due 20 days following invoice date. A finance charge of 1.5% per month will be imposed on all padue accounts.
When relinquishing samples to Blue Ridl c Labs (811L), buyer authorizes IBRL to perform only the analysis indicated above and also agrees to pay collection and attorney teef the account becomes delinquent. Blue Ridge Labs
reservcs the riglll to deny documentation for any %vork where payment has nos been made. in effect rendering that data unsupported for regulatory purposes. BRL cannot guarantee that any regulatory authority will accept any work,
submi[te 1. therefore it is the clicnt's responsibility to request on [his form appropriate tests. NC DCNR Certified Lab #275
±Jf'VGE, Z o 2
NPDS Reporting ✓ Grt'ounclwater
Report To:
B. lue Ridge Labs., Inc.
P.O. Box 2940
Lenoir, NC 28645
Telephone (828) 728-0 i 49 Fax (828) 728-0131
Chaim of Custody
Sanitary Land -fill hazardous Waste Industrial or QC Non State Reporting
UST/Trust Fund Reporting
Bill To:
aJ�EYL rn�L . J A-; L
� �lZ GAa.a7zYv ,vim— 5
Field
Project Name:
PO Number:
Ice Present: Y N
Preservatives Lab Check
Sample iD
Sample
Type
Date
Tinie
Time &
Temp
HR:NN1
°C
Field
Sulfide
Cht:ck
Y N
Ficld
Sulfide
Present/
Removed
Y N
Resid
Chlor
Field
Check
Y N
Field
Dechlorination
Y N
pH
Resid
Chlor
P o r A
Temp
°C
Sampler
Initials
Analysis Requested
i
7
F
Reliliquished By: Date: Time: Rece' y: Date: "Time:
lipull submis;ion of samples. client ugrces dial invoices arc due at the time work is completed. Open accuunls arc due 20 days following invoice date. A finance charge of 1.5% per month Avill be imposed on all p,educ .accounts.
When relinquishin s;mgples to Blue Ridge Labs [i3RL). huger authorizes BRI, Lo perform only the analysis indicated above and also agrees to pay collection and attorney feef the account becomes delinquent. Mue 12id�ac Labs
rescrves the right to denp ducumenrat ion for any %rorli wlim payment has not hcen made. in effect rendering that data unsupported for re_Qulatary purposes. RRL cannot guarantee that any regulatory authority will accept any work:
suhmiticd. thMk)rc it is the clicnt'.� responsibility to request on this form approprialc tests. NC D£NR Ccrtiried Lab Q75
North Caro, a Department of Environme,..dl Quality
Pat McCrory
Governor
Donald R. van der Vaart
Secretary
Received
October 6, 2015
OCT 14 2015.
Mr. Paul Ingle
Meritor Heavy Vehicle Systems, LLC Land Quality Sectlon
105 Wamsutta Mill Road Asheville
Morganton, NC 28655
Subject: NPDES General Permit NCG030644
Meritor Heavy Vehicle Systems, LLC
Formerly Sypris Technologies, Inc.
Certificate of Coverage NCG030644
Burke County
Dear Mr. Ingle:
Division personnel received your request to revise your stormwater permit Certificate of Coverage to
accurately reflect your new company and/or facility name.
Please find enclosed the revised Certificate of Coverage. The terms and conditions contained in the
General Permit remain unchanged and in full effect. This revised Certificate of Coverage is issued
under the requirements of North Carolina General Statutes 143-215.1 and the Memorandum of
Agreement between North Carolina and the U.S. Environmental Protection Agency.
If you have any questions or need further information, please contact the Stormwater Permitting
Program at (919) 707-9220.
Sincerely,
ORIGINAL SIGNED 131
KEN PICKLE
for Tracy E. Davis, P.E., CPM, Director
Division of Energy, Mineral and Land Resources
cc: Asheville Regional Office
Stormwater Permitting Program Files
Central Files
Division of Energy, Mineral, and Land Resources
Energy Section • Geological Survey Section • Land Quality Section
1612 Mail Service Center, Raleigh, North Carolina 27699-1612.919-707-92001 FAX: 919-715-8801
512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http:tiportal.ncdenr,org/web/Ir/
An Equal Opportunity 1 Affirmative Action Employer — 50% Recycled 110% Post Consumer Paper
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030644
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Meritor Heavy Vehicle Systems, LLC
is hereby authorized to discharge stormwater from a facility located at:
Mentor Heavy Vehicle Systems, LLC
105 Wamsutta Mill Road
Morganton
Burke County
to receiving waters designated as Catawba River, a class WS-IV water in the Catawba River
Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions
set forth in Parts I, II, III, and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective October 6, 2015.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day October 6, 2015.
ORIG1NAl. SIGNED FT',
KEN PICKLE
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission
,` North Carolina Department of Environmental Quality
Pat McCrory
Governor
October 6, 2015
Mr. Paul Ingle
Meritor Heavy Vehicle Systems, LLC
105 Wamsutta Mill Road
Morganton, NC 28655
Donald R. van der Vaart
Secretary
Subject: NPDES General Permit NCG030644
Meritor Heavy Vehicle Systems, LLC
Formerly Sypris Technologies, Inc.
Certificate of Coverage NCG030644
Burke County
Dear Mr. Ingle:
Division personnel received your request to revise your stormwater permit Certificate of Coverage to
accurately reflect your new company and/or facility name.
Please find enclosed the revised Certificate of Coverage. The terms and conditions contained in the
General Permit remain unchanged and in full effect. This revised Certificate of Coverage is issued
under the requirements of North Carolina General Statutes 143-215.1 and the Memorandum of
Agreement between North Carolina and the U.S. Environmental Protection Agency.
If you have any questions or need further information, please contact the Stormwater Permitting
Program at (919) 707-9220.
Sincerely,
ORIGINAL SIGNED 131
KEN PICKLE
for Tracy E. Davis, P.E., CPM, Director
Division of Energy, Mineral and Land Resources
cc: Asheville Regional Office
Stormwater Permitting Program Files
Central Files
Division of Energy, Mineral, and Land Resources
Energy Section • Geological Survey Section - Land Quality Section
1612 Mail Service Center, Raleigh, North Carolina 27699-1612.919-707-9200 I FAX: 919-715-8801
512 North Salisbury Street, Raleigh, North Carolina 27604 - Internet: http:/Iportal.ncdenr.org/web/Irt
An Equal Opportunity I Affirmative Action Employer — 50% Recycled 110% Post Consumer Paper
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030644
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Meritor Heavy Vehicle Systems, LLC
is hereby authorized to discharge stormwater from a facility located at:
Mentor Heavy Vehicle Systems, LLC
105 Wamsutta Mill Road
Morganton
Burke County
to receiving waters designated as Catawba River, a class WS-IV water in the Catawba River
Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions
set forth in Parts 1, II, II1, and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective October 6, 2015.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day October 6, 2015.
ORIGINAL SIGNED B`
KEN PICKLE
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission
LTMA
i
NCDENR
Nrn Cu+ _ Derxn W _ o
E.,�.E, — NR — R�C—
Division of Energy, Mineral & Land Resources
Land Quality SectionlStormwater Permitting
National Pollutant Discharge Elimination System
PERMIT NAMEIOWNERSHIP CHANGE FORM
FOR AGENCY USE ONLY
Date Received
Year
Month
flay
Ca .
I. Please enter the permit number for which the change is requested.
NPDES Permit
(or) Certificate of Coverage
N C7 0 3 1
0 10
0 1 0
C.1
0
1 3 1 0 6 4 4
11, Permit status prior to requested change.
a. Permit issued to (company name):
Sypris Technologies, Inc.
b. Person legally responsible for permit:
John A Rhyne
First MI Last
Ehs Director
Title
101 I3ullitt Lane, Suite 450
Permit Holder Mailing Address
Louisville KY 40222
City State "Lip
(828) 433-4600 (828) 439-8463
Phone Fax
c. Facility name (discharge):
Sypris 'l'echnologies, Inc.
d. Facility address:
105 Wamsutta Mill Road
Address
Mor anton NC 28655
City State Zip
e. Facility contact person:
ttVt ( ) oZa� j
First 1 MI 1 Last Phone
11I. Please provide the following for the requested
change (revised permit).
a. Request for change is a result of:
X Change in ownership of the facility
❑ Name change of the facility or owner
If other please explain: Purchase of operations and lease of real estate
b. Permit issued to (company name):
Mentor Heavy Vehicle Systems, LLC
c. Person legally responsible for permit:
V L Ingle
First MI Last
RECEIVED
st-� �h.���-�
--
Title
SEP Z 3 2015
105 Wamsutta Mill Road
Permit Holder Mailing Address
DENR-LAND QUALITY
Morganton NC 28655
STQRMWATER PERMITTING
City State Zip
(BZ® ) W.4 -10 99 t�v�.�✓GtE Q AM-1ht .Co..,.
Phone E-mail Address
d. Facility name (discharge):
Meritor Heavy Vehicle Systems, LLC
e. Facility address:
105 Wamsutta Mill Road
Address
Morganton NC 28655
City State Zip
f. Facility contact person:
,4 Robinson
First MI Last
(816 )71,4 -4&gLf 0,5 ►-ie MCA fy'2.ca"
Phone E-mail Address
IV. Permit contact information (if different from the person legally responsible for the permit)
Revised Jan. 27, 2014
NPDES PERMIT NAME/OWNERSHIP CHANGE FORM
Page 2 of 2
Permit contact:
Robinson
First MI Last
FACIt-1 r"a&ia.tc'm
Title
105 Wamsutta Mill Road
Mailing Address
Morganton NC 28655
City state Zip
(e,,249 ) Ay yGyti
Phone I -mail Address
V. Will the permitted facility continue to conduct the same industrial activities conducted prior
to this ownership or name change?
® Yes
❑ No (please explain)
VI Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is required for an ownership change request. Articles of incorporation are
not sufficient for an ownership change.
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Certification is sufficient.
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
1, John A. Rho, attest that this application for a name/ownership change has been reviewed and is
accurate d complete to the best of my knowledge. I understand that if all required parts of this
appli ati are not completed and that if all required supporting information is not included, this application
pack, e 11 bet returned �� incomplete.
Signaturb
i
CERTIFICATION
ate
I, '"-'' ', attest that this application for a name/ownership change has been reviewed and is accurate and
comple to the best of my knowledge. I understand that if all required parts of this application are not
complet d and that if all required supporting information is not included, this application package will be
returned as incomplete.
Signature
9-/G-/s
Date
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Revised Jan. 27, 2014
01"
BILL OF SALE AND ASSIGNMENT AND ASSUMPTION AGREEMENT
BILL OF SALE AND ASSIGNMENT AND ASSUMPTION AGREEMENT, made and
entered into as of July 9, 2015 (this "Bill of Sale"), by and between Meritor Heavy Vehicle
Systems, LLC, a Delaware limited liability company ("Buyer"), and Sypris Solutions, Inc., a
Delaware corporation ("Sypris '), Sypris Technologies, Inc., a Delaware corporation ("Sypris
Technologies"), and Sypris Technologies Kenton, Inc., a Delaware corporation ("Sypris
Kenton") (each of Sypris, Sypris Technologies and Sypris Kenton are sometimes herein referred
to individually as a "Seller" and collectively as "Sellers").
RECITALS
A. Sypris and Buyer have entered into an Asset Purchase Agreement dated as of July 9,
2015 (the "Asset Purchase Agreement") pursuant to which Sypris agreed to sell, and to cause the
other Sellers to sell, the Assets, and Buyer agreed to assume the Assumed Liabilities.
Capitalized terms used herein but not defined herein shall have the meanings given to such terms
in the Asset Purchase Agreement.
B. Sellers desire to sell, assign, transfer, convey and deliver the Assets to Buyer, and Buyer
desires to purchase and acquire the Assets.
C. Buyer desires to assume and Sellers desire to transfer to Buyer the Assumed Liabilities.
NOW, THEREFORE, in consideration of the premises and for other good and valuable
consideration, the receipt and sufficiency of which are hereby acknowledged by each of the
parties hereto, Sellers and Buyer hereby agree as follows:
I. Sellers hereby sell, assign, transfer, convey and deliver to Buyer, free and clear of
all Liens other than Permitted Liens, and Buyer hereby purchases, acquires and accepts from
Sellers, all of the right, title and interest of Sellers in and to the Assets.
2. Buyer hereby assumes and undertakes to pay, perform and discharge, the
Assumed Liabilities.
3. The provisions of Section 2.2 of the Asset Purchase Agreement are incorporated
herein by reference; provided, however, that upon receipt of a consent to the assignment of any
Contracts or Permits of a Seller included in the Assets after the date hereof, this Bill of Sale shall
automatically sell, assign, transfer, convey and deliver such Contract or Permit to Buyer without
the requirement of any further instrument executed by or action taken by any Seller.
4. Nothing in this Bill of Sale, express or implied, is intended or shall be intended to
confer upon or give to any person, Firm, entity or corporation other than Sellers, Buyer and their
respective successors and permitted assigns, any remedy or claim under or by reason of this Bill
of Sale or any term, covenant or condition hereof, and all of the terms, covenants and conditions,
promises and agreements in this Bill of Sale contained shall be for the sole and exclusive benefit
of the parties hereto and their successors and permitted assigns.
5. To the extent any provisions of this Bill of Sale are inconsistent with the Asset
Purchase Agreement, the provisions of the Asset Purchase Agreement shall control.
b. This Bill of Sale shall be construed and interpreted according to the laws of the
State of Michigan, excluding any choice of law rules that may direct the application of the Laws
of another jurisdiction.
7. This Bill of Sale shall be binding upon and inure to the benefit of Sellers and
Buyer and their respective successors and permitted assigns.
8. This Bill of Sale may be executed in separate counterparts, each such counterpart
being deemed to be an original instrument, and all such counterparts will together constitute the
same instrument.
[Signature page follows]
-2-
IN WITNESS WHEREOF, the parties hereto have caused this Bill of Sale to be executed
by their respective duly authorized officers as of the date first above written.
MERITOR HEAVY VEHICLE SYSTEMS,
LLC
By: P
Name:
Title: Av77foUn S/G��C
SYPRIS SOLUTIONS, INC.
By:_
Name:
Title:
SYPRIS TECHNOLOGIES, INC.
By:_
Name:
Title:
SYPRIS TECHNOLOGIES KENTON, INC.
By:_
Name:
Title:
[Signature Page to Bill of Sale and Assignment and Assumption Agreement]
IN WITNESS WHEREOF, the parties hereto have caused this Bill of Sale to be executed
by their respective duly authorized officers as of the date first above written.
MERITOR HEAVY VEHICLE SYSTEMS,
LLC
By:_
Name:
Title:
SYPRIS SOLUTIONS, INC.
By;_ _7�
Name:
Title:
SYPRIS TECHNOLOGIES, INC.
r J,
Name:
Title:
SYPRIS TECHNOLOGIES KENTON, INC.
By: �/L
Name:
Title:
[Signature Page to Bill of Sale and Assigninew and Assumption Agreement]
CONFIDENTIAL
EXECUTION COPY
ASSET PURCHASE AGREEMENT
by and between
MERITOR HEAVY VEHICLE SYSTEMS, LLC
and
SYPRIS SOLUTIONS, INC.
Dated as ofJuly 9, 2015
CPAM, 7653631/4
TABLE OF CONTENTS
Page
ARTICLE I DEFINITIONS ............................................
ARTICLE II SALE AND PURCHASE OF ASSETS .....
Section 2.1.
Sale and Purchase of Assets.........................................................
I
Section 2.2.
Non -Assignable Contracts and Permits........................................3
ARTICLE III ASSUMPTION OF LIABILITIES..........................................................4
Section 3.1.
Assumed Liabilities......................................................................4
Section 3.2.
Retained Liabilities......................................................................5
ARTICLE IV PURCHASE PRICE................................................................................5
Section 4.1.
Purchase Price .............................. ...................5
ARTICLEV CLOSING................................................................................................9
Section5.1.
Closing.........................................................................................9
Section 5.2.
Closing Deliveries of Seller.........................................................9
Section 5.3.
Closing Deliveries of Buyer.........................................................9
Section 5.4.
Transfer Taxes............................................................................10
ARTICLE VI REPRESENTATIONS AND WARRANTIES OF SELLER................10
Section 6.1.
Organization...............................................................................10
Section 6.2.
Authority....................................................................................10
Section6.3.
No Breach...................................................................................I
1
Section6.4.
Taxes..........................................................................................I
I
Section 6.5.
Proprietary Rights......................................................................12
Section 6.6.
Assets and Properties.................................................................13
Section 6.7.
Litigation....................................................................................16
Section 6.8.
Environmental Matters...............................................................16
Section 6.9.
Governmental Approvals...........................................................17
Section 6.10.
Compliance With Applicable Law.............................................17
Section 6.11.
Employees Matters.....................................................................18
Section 6.12.
Sufficiency of Assets..................................................................20
Section 6.13.
Absence of Material Adverse Effect and Certain Changes or
Events.........................................................................................20
Section 6.14.
Contracts.....................................................................................20
Section 6.15.
Financial Information.................................................................21
Section 6.16.
No Brokers.................................................................................22
ARTICLE VIl REPRESENTATIONS AND WARRANTIES OF BUYER.................22
Section 7.1. Organization ......................................... ......22
................................
Section 7.2. Authority....................................................................................22
CPAM: 7853833.14
(f) the purchase orders with USM set forth on Schedule 2.1(f) (the "USM
Purchase Orders");
(g) all assignable (after both parties have complied with their obligations
under Section 2.2 to facilitate such assignment) rights under licenses or other agreements
that are necessary for the continued operation of the Business (excluding only those
software licenses listed in item 16 of Schedule A to the Transition Agreement (other than
the software licenses listed in item 15 of Schedule A to the Transition Agreement which
are contemplated to be transferred to Buyer)), including those referenced in Section
2.1(c) and those set forth on Schedule 2.1(g) (the "Business Contracts"); provided,
however, that the parties acknowledge such rights shall not be deemed "necessary" to the
extent that practical alternative sources of supply are reasonably available on a timely
basis under the circumstances (it being understood that nothing herein will limit Buyer's
rights under the Transition Agreement);
(h) all rights under Permits (to the extent transferable) that relate to the
Business, including those set forth in Schedule 2.1(h);
(1) except to the extent based upon, arising out of, relating to or caused by
any Excluded Asset or Excluded Liability (or otherwise subject to indemnification by
Seller or Seller Subsidiaries or their Affiliates) and then solely to the extent that Seller is
not fulfilling any of its indemnification obligations with respect thereto, those causes of
action, claims, rights under express or implied warranties, guarantees, indemnities and
similar rights in favor of Seller and/or any Seller Subsidiary, rights of recovery, rights of
set-off, rights of subrogation and all other rights and demands of any nature available to
Seller and/or any Seller Subsidiary to the extent related to the Assets or the Business;
0) the benefits of coverage provided by insurance policies of Seller and
the Seller Subsidiaries (with respect to the Business or the Assets) in respect of matters
occurring on or prior to the Closing Date to the extent set forth in Section 8.7; and
(k) all books and records that are reasonably required to operate the
Business and other books and records as may be mutually agreed by the parties acting
reasonably and in good faith.
The assets, properties and rights of Seller and the Seller Subsidiaries to be
sold, assigned, conveyed, transferred and delivered to Buyer pursuant to this Agreement
are herein collectively referred to as the "Assets".
Section 2.2. Non -Assignable Contracts and Permits. Anything contained
herein to the contrary notwithstanding, this Agreement will not constitute an assignment,
an attempted assignment or an agreement to assign any Contract (or rights thereunder) or
3
CPAM! 7853833.14
Permit (or rights thereunder) if an assignment or attempted assignment of the same
without the Consent of any other party or parties thereto would constitute a breach
thereof or in any way impair the rights of Seller, any Seller Subsidiary or Buyer
thereunder. If any such Consent is not obtained or if an attempted assignment would be
ineffective or would impair Seller's, any Seller Subsidiary's or Buyer's rights under any
such Contract or Permit so that Buyer would not receive all such rights, then Seller will,
and will cause each Seller Subsidiary to, and Buyer will use its commercially reasonable
efforts to cause the full benefits of any such Contract (or rights thereunder) or Permit (or
rights thereunder) to be provided to Buyer in the most cost-effective and practical manner
available under the circumstances. In addition, Seller will, and will cause each Seller
Subsidiary to, take such other actions (at Seller's reasonable expense) as may reasonably
be requested by Buyer in order to place Buyer, insofar as reasonably possible, in the same
position as if such Contract (or rights thereunder) or Permit (or rights thereunder) had
been transferred as contemplated hereby and so that all the benefits relating thereto shall
inure to Buyer. Notwithstanding the foregoing, if any such Consent is not obtained prior
to the Closing, Seller will continue to use and will cause each Seller Subsidiary to
continue to use, and Buyer will use, its commercially reasonable efforts (at Seller's
reasonable expense) to obtain all such Consents (and, if and when such Consents are
obtained, the transfer of the applicable Contract (or rights thereunder) or Permit (or rights
thereunder) will be effected in accordance with the terms of this Agreement). The parties
agree that if such Consents relate to Contracts that are necessary for the continued
operation of the machinery and equipment at the Morganton Facility or Permits that are
necessary for the continued operation of the plant, machinery and equipment at the
Morganton Facility, Seller shall be responsible for all expenses incurred in obtaining such
Consent pursuant to this Section 2.2. The parties further agree that if such Consents
relate to other Contracts or Permits not covered by the immediately preceding sentence,
Seller will be responsible for all expenses incurred in obtaining such Consents pursuant
to this Section 2.2 up to an aggregate amount of $20,000 and, if Buyer determines to
incur such expenses, Seller and Buyer will share equally such expenses in excess of
$20,000.
ARTICLE III
ASSUMPTION OF LIABILITIES
Section 3.1. Assumed Liabilities. Subject to the terms and conditions set
forth herein, and in reliance upon the representations and warranties contained herein, at
the Closing, in consideration for the sale, assignment, conveyance, transfer and delivery
of the Assets to Buyer, Buyer will assume and undertake to pay, perform and discharge,
in accordance with the terms thereof, only the following Liabilities of Seller and the
Seller Subsidiaries (the "Assumed Liabilities"):
4
CPAM: 7853833,14
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149 blueridgelabslenoir@gmail.com
.I
Client
Syprls
105 W, ISutta N1ill Road
i �anlon. NC 28655
Attention:
Larry Stephens
Date Received:
I5-Apr-15
Report Date:
08-i1\9ay-15
Sample Date:
15-Apr-15
B111.#:
JWL-201 -0210
Lab Sample ll):
LS117-2015-00966
(:Bent Sample ID:
{..)ut]'all 1
03
�y
Analysis Analysis
I'araIII der. Result 1mQI, Unit (Method Time Date Analyst
I'SS * 5.6 raio
l] SA919 2540D 17:26 4/16/2015 KCJ
RECEIVED
MAY 18 2015
DENR-LAND QUALITY
STORMWATER PERMITTING
Reported By:
S. ,). , ohnson. D.K. Wessinger
Concentrations are helow Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page Iof9
Blue Ridge .Labs
PO Box 2940
Lenoir; .' C 28645
828-728-0149
blueridgelabslenoir@gmail.com
Client:
Svlins
105 Wamsritta Mill Road
Morganton. NC 280
Attention:
1_ 11'ry Stephens
Date Received:
15-Apr-15
Report Date:
OS-May-15
Sample Date:
15-Apr-15
I3111. #:
13Rl--2015-0210
Lab Sample Ill:
I,SID-2015-00967
Client SaIIII)Ie Ill:
Outfall I
Analysis
Analysis
Parameter
Result
MQL
Unit
Method
Time
Date
Analyst
Cu
0.00;
0.001
moll
EPA 200.7
17:29
4/22/2015
KCJ
Pb
T
0.01
mod
EPA 200.7
17:29
4/22/2015
KO
Zn
*
0.001
mg/1
EPA 200.7
17:29
4/22/201
1<CJ
RECEIVED
MAY 18 2015
DENR-LAND QUALITY
STQRWATER PERMITTING
Reported By:
S. ,I. t nson, D.R. Wessinger
Concentrations are below Minimum Quantification Limit excclit where noted.
NC Laboratory Certificate No. 275
Pa��e 2 of 9
Blue Ridge Labs
PO Bo.r 2940
Lenoir, PVC 28645
828-728-0149
Client: Sypris
105 Wanistitta Mill Road
Morganton. NC 28655
Attention harry Stephens
Date Recehvd: 1 i-Apr- 15
Report Date:
HAW-I5
Sampe Dale:
15-ApP I5
HRL W
HRL-20110210
Lab Sautple Ilk
L AIN2015-00968
Climl kntplf IU:
(WISH I
Parameter
Result MQI.
W An Creasr 5
bWeddgela bsK noW@gma Hxom
Unit Method
ingd 1664-A O&G
Analysis Analysis
Time Date Analysl
51 5M 5 llr Ntly
Reported By:
S. . , ohnsun, U.R. wessinger
Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 3 of" 9
Blue Midge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
blueridgelabslenoir@gmail.com
Client :
SypriS
105 WMIISutta Mill Road
Morganton. NC 2 W 5
Attention:
Lan-y Stephens
Date Received:
15-Apr-15
Report Date:
08-May-15
Sample mite:
15-Apt'-15
BR[. #:
HKI.-2015-0210
Ulb Sample 11):
LSID-201 S-00969
Client Sattiple ID:
01)11':311
Analvsis Analysis
Parameter
Result iwQL Unit Method Time Date Analyst
TSS
5.6 nag/l SM 19 25401) 17:38 4/16/2015 1:.C.1
RVI)OI-ted By:
5.11. z, D.R. Wessinger
Concentrations arc below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Pa«e 4 of 9
Flue Ridge Labs
110 Box 2940
Lenoir, NC 28645
828-728-0149
Client :
Sypris
105 WMISutta 1 III Read
Morgani,on. NC 28655
Attention:
Larry Stcphens
Bate Received:
15-Apr- l 5
Report Date:
08-IMay-15
Sample Date:
15-Apr-15
IMI. #:
13RL-2015-0210
Lab Sample 11):
I.SID-2015-00970
Client Sample 11):
Outiial] 2
Parameter Result
Cii 0.003
I' b
L.n
blueridgela bslenoir@gmail.com
Analysis
Analysis
NIQL
Unit
Method
Time
Date
Analyst
0.001
IPA 200.7
17:33
4I22/201 ti
KCJ
0.01
mod
IPA 200.7
17:33
4/22/2015
KCJ
0.001
m�,l]
EPA 200.7
17:33
4/22/2015
KCJ
Reported li}:
S. J. J4eson, D.R. Wessinger
* Concentrations are below Minimum Quantification Limit except where noted.
NC Lahoratorl• Certilicaie No. 275
Pagc 5 of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client:
Sypris
105 Wamsutta Mill Road
Moi-anton, NC 28655
Attention:
Larry Stephens
Date RCCCiyed:
15-Afar-15
Report Date:
08-M;ty - 15
Sample Dale:
15-Apr-1
13111, 0:
l3RL-2015-0210
Lab Sample 11):
LSID-2015-00971
Client Sample 11):
Outfall ?
ParilInefer
oil Grc'asC
Result NIQI,
5
blueridgelabslenoir@gmail.com
Unit method
rngll 1664-A OS-,G
Analysis Analysis
Time Date Analyst
5I5h015 WtrQIIN,
Reported BN :
Wessinger
Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
l"w e 0 of 9
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client .
Sypris
105 1Amsutta 14HI Road
Mjanwn, NC 28655
Atlemli m:
IMny Stephens
(late Received:
15-Apr-15
Deport Dale:
08-May-I5
Sarnple Dale:
15-Apr-15
HR1. 0:
liltl.- M 5-02 10
Lab Sample ID:
I.SID- 015-00972
Client Sample 110.
(IIINll 3
t'ammuer
Result ImQ1,
fSS
5j
blueridgelabslenoir@gmail.com
Unit Method
rngh SM 19 25 40D
Analysis Anaysis
Time Date Analyst
17:27 K61 M KCJ
Reported By:
S. J. J nson, D.R. Wessinger
Concentrations are below Minimum Quantification Limit except where noted.
NC laboratory Certificate No. 275
Page 7 of t)
Blue Ridge Labs
PO Box 2940
1_c nob-, NC 28645
828-728-0149
Client :
Sypris
105 Wanlsutta Mill ]toad
Morganton. IS: 28655
Attention:
I'arry Stephens
Date Received:
15-Apr-15
Report Date:
i1$-Nl ,15
Sanlple Date:
15-Apr-15
tilts. #:
]IRL-20 15-02 10
1,31) S:11111)le 11):
LSID-2015-00973
Client Sample 1D:
Outfall
Parametcr Result
Cu 0.006
Pb
Zn 0.020
bl ueridgela bQenW r@gma il.com
An;lhwN Anaksis
NIQL
Unit
Method
Tinle
Date
0.001
mgli
EPA 200.7
1735
=212013
0.01
nng/l
EPA 200.7
17:35
4122i2015
0.001
m;/l
EPA 200.7
17:35
4/22/2015
Reported 13y: �/
S. A Jo n, D.R. Wessinger
Concentrations are below MAW= Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Ilge 8 of 9
Analyst
KCJ
KCJ
KCJ
Client
.AttentioIl:
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Sypris
105 WMIISLIU2 Mill Road
Mor-anton_ NC 25655
Larry Stephens
Date Received:
15-Apr- I i
Report (late:
08-1\1,Iy-15
S:IIIaI)le Da(e:
1-5-Apr- 15
;RI k.
13RL-2015-0210
Lab Sample 11):
LSID-2015-0097-3
Client Sample ID:
Outfali
Paran!etc r
Result NIQL
DiI CK: GT% LISC 5
blueridgelabsienoir@gmail.com
Unit Method
mg/I 1664-A O& G
Awalysis Analysis
Time Date Analyst
5/5/2015 WlrQtl�
Reported 13y:
D.R. Wessinger
Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 9 of 9
WATER QUALITY LAB & OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NC 28604
(828) 898-6277
CLIENT: BLUE RIDGE LABS
ADDRESS: PO. BOX 2940
CITY: LENOIR
STATE: NC ZIP 28645 REPORTED DATE: 6-May-15
IM
.... . .
............... ......................
............
............
.
LYSIS::::
!OIL & GREASE
963
8.2
5.00
MG/L
5-May-15
Pi
OIL & GREASE
9651
5.7
5.00
MG/L
5-May-1 5
PI
OIL & GREASE
968
<5
5.00
MG/L
5-May-15
pi
OIL & GREASE
971
<5
5.00
MGIL
5-May-15
PI
OIL & GREASE
9741
<5
5.00
MG/L
5-May-15_L
P1
REPORTED BY: NC CERTIFIED LAB # 544
PALL ISENHOUR, SUPERVISOR
P.O. 130:: 2940
1. enuk, NC 23645
oWnhons (82f) 728-0149 Pan (828) 7200131
`, ;E jl, t it ii"i. ,;✓ "Jl �.l�rva F�I'.,.j
.i
I p'L trYTcL rl? r d .
N c ZAS
!nCILL51= ai or `I
PrOjecL Mime: C, �''
PC NUfflLer:
Ice prcSci?t: `_' 1\1
.3
I I fTimc
Femp
Fi" ; . !-11 76"
chlos-
Field
I
;.Imf}Ic fl: I
')tt
1�1f)6c
Fi:lc
�echlorinationp
1-1
Resid
�n
An5arP1ej alvsiss?rgtC;-cri
S:Iv! iv;
Chlor
°�
mitt:l:
l � �
14
Peck
CLL Z�
AN
C d
[,c..r-
r
Jai' 69
;.int;, w. dim; asmen lieu 111WIc__: arc ;It.e a? the time '. ri, iti completed. ()ncn accaunx. ats due 20 daes following invnice date. A Iinanec charLC nt I.5%hCT 11101101 gill i,,' ,lilp, ;._ r'. ,„! :t;l
�'hr;, rcl,Ituln:.hln^ •.Imhhr. ;;, lifo-: 12.id_,: I.-hs (11W.!. I,mcr authorizes IiRl-. to L,cr!'r�rm Inl': the :Inalysis indicated above and also agrees to pav collection and attorney fss Tc ace; w" h• wmrti ,;cii I: rent-
t;rrvc. the 11�!I!! P; uCn_, 1J„cnllr_nlali,,n !nl :al) nork Mae N"XIII has nc" hrcn rmuit- in cifect rcndcfing flim data unsuppnrfed for rcgulaiory purpascs. BRL Cultnm gttaranmc Mm m, rcgt+l:I!an Atrl,7, mk ,.'rill any
d:ntrt:, 1. 01t, 1w': 11 i, the cliCr}! ; rcSp'nr;ihilih'tn rctluc�l nn thi; I'nrrl api,runruttr. rots. i'!(' !JIiNR Certified Lab 4275
Groulld%va cr
• clurrt o:
Blue U^dge Labs., 4�Ca
P.C. Box 2940
lsenoir, NC 29645
! clephone (828) 728-0149 Fax (828) 728-013I
Chain of Custody
t_.itar�� L ndli i Hazardous NVaste industrial Or Q;
r J ST ; Trust Fund Reporting
'3iIi TO:
— — — Project Name: W
ice Present: Y N
Field Preserwitives Lab Check
N(l], Mate 1Ci7UrtinY_' --
5 tlttpStltm-flc1
laic.'
TMI:
Tine &
Temp
FIRNM
°C
Field
SifiIfdC
Check
Y \i
rield
S41111de
Present/
Removed
Y N
Resld
Chlor
Field
.heck
Y IN
Field
Dechlorination
Y N
pH
Resid
Chlor
PorA
Temp
°C
Sampler
lnitials
Analysis RequeSt.d
i
I
1
I
l
i
I
E
j
l
1
liiI-11!1<h. i. v:
Date: i-i f .ie:
g ar,�
R`-'Celvcd BV_
Date: I ll1;C:
I'lxm suhnil,sism ol',:nnplc,. client acrces that invoiccn me dLic at the time tiwrk is completed. Open accounts are dLtc 20 days rollowini invoice date. A finance charge of I -SN- pet momh will 'nr [mLnwwd on ail pr eEur •,Iccouniti.
11'hcn Iclinqul,hin'• ,:unpte; ul IliLn Ri&-, i-abs i RI:!..}. htl\'Cr authurizes RR3_. w perronit �lnly the analysis indicated above and also agrees to pay collection and attornq fce�NIle lcecrLnit htulmc, deliMjLR: t. Hltir kili_'c
r,,CrYCti the r:'all1 to UCi1P dUCi l illef it 2tioil t"lf all) lSnrk where pity fllent Ila% no hccn made, ill crtect miderimi that data Llnstippmed ibr reg Ll l atO17�1 pUrpOSCS. BRL cannot 2llaYiUl tee Ill:n a-m% CC2LlI ill MV :iLI IhOrI I% M I I :1ccC p? il!1%' v,.oI t:
sribnlillcd. ilocr.'Inle if is the clicwS s rccponsihiiih Io rcgncst nrl this loan approprtatc tc;ls. NC I)I_NR Certified Lah ?i27i
ncG-o3o� 4�-
aoi
NPDS Reporting K Groundwater
Report To:
syprts
Blue Ridge Labs, Inc.
P.O. Box 2940
Lenoir, NC 28645
Telephone (828) 728-0149 Fax (828) 728-013 l
Chain of Custody
Sanitary Landfill Hazardous Waste
UST/Trust Fund Reporting
Bill To:
Field
Industrial or QC Non State Reporting —
Project "Name: CJf; �VVL vim' f
PO \!ttmbCf:
Ice Present: Y N
Preservatives Lake Check
Sample ID
Sample
Ivpe
Date
Time
Time &
Temp
HR:MM
°C
Field
Sulf-ide
Check
Y NY
Field
Sulfide
Present /
Removed
N
Resid
Chlor
Field
Check
Y N
Field
Dechlorination
�' It
pH
Resid
Chlor
P or A
Temp
°C
Sampler
GInitials
Analysis Requested
Outfall I
TSS
Outfall ;
I
L
f��t/�
/
0
v
L 2
r t
Pb f C% 3�
Outl'l.11 I
��,!
a7Do
L 2
+!
O&G L y EPA 1 L( y
I
Relinquished By: Date:: Time:
Ll
Rec , e [)at .: Time:
Upon -Submission Clitn[ agrcxs that invoices are clue at the time work is completed_ Open accounts arc due 20 clays 1ollow11IR invoice date- A f finance charnc nl I.5 "o per month will he imPoscd an all p.ectuc accounts.
When relinquishing saniplr; to 131uc Ricigc Lah> (BRI.)_ huyer authorizes BRL to perform only die analysis iridicated above and also agrees to pad' collection and attorrIn' JeC3 the �tca>unt brcone; ddmquem. More Ridge Labs
reserves the ri2h, to dcnV documentation fix any work where pac.nent has not been made. in effect rendering that data unsupported for reguiamy ourpnsei BRL cannot szmm uec that airs' rceulatory authority gill accept am work
sohmined_ tlterefiire it is the client's responsibiliw to request on this form appropriate tests. NC DENR CcrW—,'.d Lab 4275
hCC-O 3D(oq �
N PDS Reporting _Groundwater
Report To:
Sypris
Blue Ridge Labs, Inc.
P.O. Box 2940
Lenoir, NC 28645
Telephone (828) 728-0149 Fax (828) 728-0131
Chain of Custody
Sanitary Landfill Hazardous Waste Industrial or QC Non State Reporting
UST/Trust Fund Reporting
Bit To: , j ,p 5�,` 0�--Jf p ��
I i t7 Clc, . AL � U� �f [ E C� Project Name:
l PO Number:
Ice Present: Y N
Field Preservatives Lab Check
Sample 1D
Sample
Type
Date
Time
Time &
Temp
HR:MM
°C
Field
Sulfide
Check
Y N
Field
Sulfide
Present /
Removed
Y N
Resid
Chlor
Field
Check
Y N
Field
Dechlorination
Y N
pl-1
Resid
Chlor
P or A
Temp
7
Sampler
CInitials
Analysis Requested
OLltfall 2
J
O
gym
TSS
Outfall 2
��r�.
V�
�
D�
G 2
tt
Pb J
Outfall 2'{l(d
/
n
b1
2
t l
O&G KQ Ar t 6
Relinquished By:. Date:
. l �
Time: Ree d Date: TiMe:
Upon submission nl'samples. ciieni agrees that invuices are due at the time work is completed. Open accounts arc; due 20 days following invoice date. ,\ ttnariec char_c Of 1.5% per nionth will be imposed on all ptrdue accounts.
When relinquishing sanlpics to Blue Ridge Labs (HRL), buyTr authorizes 13RL to perform only the analysis Indicated above and also agrees to pay collectiom and aitoraey led'ihe account becomes dchoqucni. 131uc Kid4c Labs
reserves the right to dcnv dOCmllentitlon 6or anv work where payment ha; not been made, in el'tect rendering that data unsupported for regulauxy purposes. BKI. cannot uarsntec that an)' relulalory authority %cili accept am work
subnuttcd. theretiuc it is tiie clicrtt,s respolls N1ily to request on this form appropriate tests. NC DFNR Certified Lab 9275
G-0 �'u(�y�
NPDS Reporting X Groundwater
Report -ro:
sypris
Blue Ridge Labs, Inc.
P.O. Box 2940
Lenoir, NC 28645
Telephone (828) 728-0149 Fax (828) 728-013 l
Chain of Custody
Sanitary Landfill Hazardous Waste _
UST/Trost fund Reporting
Bill To:
Field
Industrial or QC Non State Reportinc
Pro_ject Name: �{� ��� `^� �C ✓
PO Number:
Ice Present: Y N
Preservatives Lab ClZeck
Sample ID
Sample
Type
Date
Time
Time &
Tetnp
1-lR MM
°C
Field
Sulfide
Check
Y N
Field
Sulfide
Present /
Removed
Y N
Resid
Chlor
Field
Check
Y N
Field
Dechlorinaticn
Y Nt
pH
Resid
Chlor
PorA
Temp
°C
66 a
Sampler
leitials
Analysis Requested
Outfall '
//
V��
�l
441
c.
z`
TSS
Outfall 3
(
p�Zo
Li
.�
Pbi Co-
Outtall 3
&eAp
�ltE
p
1Zo
L Z
'
O&G l✓ (;iJ
7
Relinquished By: Date: Tillie:
L -_ \C-\- %lit ) I I ly1 1) 9 S P
Rece' DAZXX
Tillie:
5
Upon submission ofsamples, client agree; that invoices are due at the iinte work is completed. Open accounts are due 20 days following invoice date, A finance charge of 1.5%per nwnth Will be imposed on all pa-tuc accounts,
l\'hen relinquishine samples to Blue Ridge Lab% (BRL), buyer authorize, BRi, to perform only the analysis indicated above and also agrees io pay collcciion and attorney f"flhe account beconics delinquent. Blue Ridge Labs
rescrvcs the right to dun' dOCUMV111iltlml For any Nvork "'here payment has not been made, in cffcct rendering that data unsupported for rcgulaurn• }lurposes. 13R1. cannot ;uarantcc that any regulatory authority will accept aun_ work
suhittitted. therefore it is the client's responsibility to request on [his form appropriate tests. NC DFNR Certilled Lab #27 V
- A��
NC®ENR
North Carolina Department of Environment and Natural Resources
Division of Energy, Mineral, and Land Resources
Land Quality Section
Tracy E. Davis, PE, CPM
Director
December 6, 2013
Mr. Lee Kearson
Sypris Technologies, inc.
105 Wamsutta Mill Rd.
Morganton, NC 28655
Pat McCrory, Governor
John E. Skvarla, III, Secretary
Subject: General Permit No. NCG030000
Sypris T ecL-nologies
COC NCG030644
Burke County
Dear Mr. Kearson:
In accordance with your application for a discharge permit received on November 14, 2013,
we are forwarding herewith the subject certificate of coverage to discharge under the subject state -
NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General
Statute 143-215.1 and fhe Memorandum of Agreement between North Carolina arid the US
Environmental Protection Agency dated October 15, 2007 (or as subsequently amended).
Please take notice that this certificate of coverage is not transferable except after notice to
the Division of Energy Mineral & Land Resources (DEMLR). !f the facility changes Ownership or is
closed, DEMLR may require modification, revocation, or reissuance of the certificate of coverage.
Per the requirements of the Catawba Riparian Buffer Rule, all stormwater drainage to
stream buffers, from portions of this site that have been constructed after June 30, 2001, must be
discharged through a correctly designed level spreader or another device that meets diffuse flow
requirements per 15A NCAC 2B .0243. Diffuse flow requirements are described in Chapter 8 of the
North Carolina Stormwater BMP Manual, available at:
hap: / f portal.ncde nr.org/web/wq Jws/su/bmp-manual.
This permit does not affect the owners legal obligation to obtain other permits which may be
required by DEMLR, or permits required any other federal, state, or local governmental authorities.
If you have any questions concerning this permit, piease contact Larry Wade PE at telephone
number (919) 807-6375
Sincerel ,
for Tracy E. Davis, P.E,
cc: Asheville Regional Office
Central Files
Stormwater Permitting Unit Files
DEC " 9 2013
Land Quality Section
Asheville
1612 Wail Service Center, Raleigh, North Carolina 27699-1612 • Telephone 919-707-9220 / FAX: 919-733-2876
512 North Salisbury Street, R1.leigh, North Carolina 27604 • Internet: http:I/portal.ncdenr.org/web/Ir/land-guality
An Equal Opportunity 1 Affrmative Action Employer — 50% Recycled 110% Post Consumer Paper
1
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030644
STORMWATER DISCHARGES
NATIONAL. POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Sypris Technologies
is hereby authorized to discharge stormwater from a facility located at
Sypris Technologies
105 Wamsutta Mill Rd.
Morganton
Burke County
to receiving waters designated as Catawba River, a -class WS-IV water in the Catawba River
Basin, in accordance with the effluent limitations, monitoring requirements, and other
conditions set forth in Parts I,1I,111, IV, V, and VI of General Permit No. NCG030000 as
attached.
This certificate of coverage shall become effective December 6, 2013.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day December 6, 2013.
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission
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STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030644
STORN41%1VATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the federal Water Pollution Control Act, as amended,
Sypris Technologies
is hereby authorized to discharge stormwater from a facility located at
Sypris Technologies
105 Wamsutta Mill Rd.
Morganton
Burke County
to receiving waters designated as Catawba River, a class WS-IV water in the Catawba River
Basin, in accordance with the effluent limitations, monitoring requirements, and other
conditions set forth in Parts I,11,1I1, IV, V, and VI of General Permit No. NCG030000 as
attached.
This certificate of coverage shall become effective December 6, 2013.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day December 6, 2013.
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission
Division of Water Quality / Surface Water
{
r�ti�r
Protection Section
NCDENR
N�tllOn�i Pollutant Discharge EliminationSy5t0E17
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rot R'„WI 11 AN.N MA. Mgb.4-X6
NCG030000
NOTICE OF INTENT
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National Pollutant Discharge Elimination System application for coverage under General Permit
NCG030000 :
STORMWATER DISCHARGES associated with activities classified as:
SIC (Standard Industrial Classification) 335 Rolling, Drawing, and Extruding of Nonferrous Metals
SIC 3398 Metal Neat Treating (�
SIC 34 Fabricated Metal Products
SIC 35 Industrial and Commercial Machinery ._
SIC 36 Electronic and Other Electrical Equipment NOV 1 ?! 2013
SIC 37 Transportation Equipment
SIC 38 Measuring, Analyzing, and Controlling Instruments DENR- WA•iERQUALITY
WETLANDS AND STORMWATER BPUI KC
^ C For questions, please contact the DWQ Regional Office for your area. See page 4.
(Please print or type)
1) Mailing address of owner/operator (address to which all permit correspondence will be mailed :
Name
Street Address
City
Telephone No.
11�'TZ -4 State N(- ZIP Code aeK5-S
0 c, — Fax:
2) Location of facility producing discharge:
Facility Name `j l ��=S %Ec�fi✓oLr;(t Lz�
Facility Contact C-p ' SC) /V _
Street Address C� S� [n/.4�t�t 3-✓77-4 /Ylrt L Pert
City _r {j2G,IN %ark!_, Slate fVe- ZIP Code---
Countyc�/�--
Telephone No. Z`k V63 Fax: Sz.F _y3 f- F y�2
Email L i4rr,15.. F1' S(1 •S, r_ca,�
3) Physical Location Information:
Please provide a narrative description of hoW to get 10 the facility (use street names, state road numbers, and
distance and direction from a roadway intersection). _Z:_yv G Ida= fftiertt =tend
D[ —t c-r - '� L r ..1_N (-Cr ' i../ r "� c-O •`� - 4-s S F741Y,XONi
L,4, , ^�t� c>ti Z:•, L, 1 - "T- /)/7,r Ilwk - W4mcyH, c,,v I I- - �'bhyi L l !- L.r.25
(A copy of a county map or USGS quad sheet with the lacility clearly located must he submitted with this application.)
4) Latitude 35 y5 "7 Longitude 3(deg, min, sec)
Page 1 of 4
SW11.218-071408 Last revised 7114108
NCG030000 N.O.I.
5) This NPDES Permit Application applies to which of the following:
❑New or Proposed Facility Dale operation is to begin
Existing
6) Standard Industrial Classificailon:
Provide the 4-digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial
activity at this facility.
SIC Code: 3 :�- /
7) Provide a brief narrative description of the types of industrial activities and products manufactured at
thisfaciiiiy: C—,rMinll LOP k1", -vV J-ru(_ dV-:';c_
8) Discharge points I Receiving waters:
How many discharge points (ditches, pipes, channels, etc.) convey stormwater from the properly?
What is the name of the body or bodius f Water (creek, stream, river, lake, etc.) that the facility stormwater
discharges end up in? - ±- :kAI)
Receiving water classification:
Is this a 303(d) listed stream? E S Has a TMDL been approved for this watershed?
If the site stormwater discharges to a separate storm sewer system, name the operator of the separate storm
sewer system (e.g. City of Raleigh municipal storm sewer). . Aj A
9) Does this facility have any other NPDES permits?
4 N o
❑ Yes
If yes, list the permit numbers for all current NPDES permits for this facility:
10) Does this facility have any Non -Discharge permits (ex: recycle permit)?
*NO
Cl Yes
It yes, list the permit numbers for all current Non -Discharge permits for this facility:
11) Does this facility employ any best management practices for stormwater control?
❑ No
❑ Yes (Show any structural BMPs on the site diagram.)
If yes, please briefly describe:
12) noes this facility have a Stormwater Pollution Prevention Plan?
❑ No
eyes
If yes, when was it implemented? g' 2(, rrZd 1
13) Are vehicle maintenance activities occurring at this facility?
xNo ❑ Yes
14) Hazardous Waste:
a) Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility?
❑ No fJ Yes
Page 2 of 4
SWU-218-071408 Last revised 7114l08
NCG030000 N.O.I.
b) Is this facility a Small Quantity Generator (less than 1000 kg, of hazardous waste generated per month) of
hazardous waste?
n No I(Yes
c) Is this facilty a Large Quantity Generator (1000 kg. or more of hazardous waste generated per month) of
hazardous waste?
f (No O Yes
d) Is hazardous waste stored in the 100-year flood plain?
f(No ❑ Yes If yes, include information to demonstrate protection from flooding.
e) If you answered yes to questions b or c , please provide the following information:
Type(s) of waste: +ram k r-J 121uo,,- s1 c— � �, M p s — - —
How is material stored: 5 6'40ry P (/Iah- "%' 1 w L."- n )'d _
Where is material stored:. UNv, c,.,,ti
How many disposal shipments per year: 1
Name of transport i disposal vendor: 141/t-F &�-/11 ri.;_-eo/VAet1IV
Vendor address: 1.2, 1 /Fc man; ✓+-V/ li�C 0 NL
15) Certification:
North Carolina General Statute 143-215.68 (i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record, report,
plan, or other document filed or required to be maintained under this Article or a rule irmplemeniing this Arlicle; or who
knowingly makes a faise statement of a material fact in a rulemaking proceeding or contested case under this Article; or
who falsilies, tampers wish, or knowingly renders inaccurate any recording or monitoring device or method required to be
operated or maintained under [his Article or rules of the Commission implementing this Article shall be gullty of a Class 2
misdemeanor which may include a fine not to exceed ten lhousand dollars ($10,000).
hereby request coverage under the referenced General Permit. I understand that coverage under this permit
will constitute the permit requirements for the discharge(s) and is enforceable in the same manner as an
individual permit.
I certify that I am familiar with the information contained in this application and that to the best of my
knowledge and belief such information is true, complete, and accurate.
Printed Name of Person Signing;
Title: E�FIS CoU.e�xN 2
(Signature bi Applicant)
fi j !f ,2ul3
(Date Signed)
This Notice of Intent must be accompanied by a check or money order for $100.00, made payable to:
NCDENR
Page 3 of 4
SWU-218-071408 Last rovisud 7/14/08
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`•1:' SYPRIS SOLUTIONS
meq,, I 'IU5 WAMSUTTA MILl=. LOAD
MORGANTON, NORTH CAROLINA
PREPARED DATE- C-iECK�J'�--- I�ArI JOB NUMBER fIGUCtt_
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SYPRIS SOLUTIONS
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1
01114
xAJFIC
1VUrtrl UdrUllrld OCUeLdry Ul - LWt
ragc l ul
Account Login Register
North Carnlins
Elaine F. Marshall DEPARTMENT OF THE
Secretary SECRETARY OF STATE
PO Box 29822 Raleigh, NC 27626-0622 (919)807-2000
Date: 12/4/2013
Click here to:
View Document Filings I File an Annual Report 1
al Print a pre -populated Annual Report Form I Amend A Previous Annual Report
Corporation Names
Name Name Type
NC SYPRIS TECHNOLOGIES, LEGAL
INC.
Business Corporation Information
SOSID:
0705634
Status:
Current -Active
Effective Date:
1/7/2004
Citizenship:
FOREIGN
State of Inc.:
DE
Duration:
PERPETUAL
Annual Report Status:
CURRENT
Registered Agent
Agent Name: CT CORPORATION SYSTEM
Office Address: 150 FAYETTEVILLE ST., BOX 1011
RALEIGH NC 27601
Mailing Address: 150 FAYETfEVILLE ST., BOX 1011
RALEIGH NC 27601
Principal Office
Office Address: 101 BULLITT LANE, SUITE 450
LOUISVILLE KY 40222
Mailing Address: 101 BULLITT LANE, SUITE 450
LOUISVILLE KY 40222
Officers
Title: ASSISTANT SECRETARY
Name: ANTHONY C ALLEN
Business Address: 101 BULLITT LANE, SUITE 450
LOUISVILLE KY 40222
Title: CHAIRMAN OF THE BOARD
Name: JEFFREY T. GILL
Business Address: 101 BULLITT LANE, SUITE 450
LOUISVILLE KY 40222
Title: GENERAL COUNSEL
Name: JOHN R. MCGEENEY
http://www.secretary.state.nc.us/corporations/Corp.aspx?Pitemld=6177654 12/4/2013
lvortn t.aronna oecretary or orate
rage z 01 L
Business Address: 101 BULLITT LANE, SUITE 450
LOUISVILLE KY 40222
Title: PRESIDENT
Name: PAUL LAROCHELLE
Business Address: 101 BULLITT LANE, SUITE 205
LOUISVILLE KY 40222
Title:
SECRETARY
Name:
NORMAN E ZELESKY
Business Address:
101 BULLITT LANE, SUITE 205
LOUISVILLE KY 40211
Title:
V;CE PRESIDENT
Name:
IZICHARD L. DAVIS
Business Address:
101 BULLITT LANE, SUITE 450
LOUISVILLE KY 40222
Title: VICE PRESIDENT
Name: BRIAN LUTES
Business Address: 101 BULLITT LANE, SUITE 450
LOUISVILLE KY 40222
Title: VICE PRESIDENT
Name: JON Q. SHELLHAAS
Business Address: 101 BULLITT LANE, SUITE 205
LOUISVILLE KY 40222
Title: VICE PRESIDENT
Name: STEPHEN W. STRAUB
Business Address: 101 BULLITT LANE, SUITE 205
LOUISVILLE KY 40222
Title: VICE PRESIDENT
Name: MARK N. CAIN
Business Address: 101 BULLITT LANE, SUITE 205
LOUISVILLE KY 40222
This website is provided to the public as a part of the Secretary of State Knowledge Base (SOSKB) system. Version:
2038
http://www.secretary.state.nc.us/corporations/Corp.aspx?Pitemld=6177654 12/4/2013
Wade, Larry
From:
Kearson, Lee [Lee.Kearson@sypris.com]
Sent:
Wednesday, December 04, 2013 3:43 PM
To:
Wade, Larry
Subject:
SypFis Technologies - - Authority to Sign
Attachments:
Auth to Sign-pdf
Larry,
I have attached the Authority to Sign document that is or. file. The authorization is ri.,en by the local plant
fliall'ager.
Sy ris does have a Corporate EHS Manager in Louisville, activities
Ky. But I am responsible for the day to day EHS activ .pn
at the Morganton site.
If the attached document does not meet the requirements I will have Corporate EHS submit the application.
Lee Keareon 1 EHS Coordinator
W5 Walll6ulta N1111 M01-gallton, NU 286Si
"'Q28,) 7(-1 A
, C^. G zi 3 9 81 `3 7 Fa,,
lee. kearson@svt)ris.com !
105 Wawsutld 101; road Moroantor.. 14C 28655
Authority to Sl t the State and federal Reports
1, (Michael Shows, Plant Manager), delegate the authority to sign
environmental documents to (Lee ICearson, Environmental, Health and Safety
Coordinator) in accordance with corporate procedures.
I certify under penalty of law that this document and all attaclunents were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. Based upon my inquiry of the person or persons who manage the
system, or those person directly responsible fogy gathering the information, the infomiation submitted is, to
the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fine and imprisonment for knowing
violations.
Michael Shows
Plant Manager
fZ Z �n/l
Date
REF: 40 CPR 122.22, A&B
EMS-007 Rev, Date 10/31/11
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TUDEX NUMB llm(323)
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Jonathan Stepp--Jonathan.Stepp@nedenr.gov
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Energy, Mineral, and Land Resources - Land Quality Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Tel: 828-296-4500
Fax: 828-299-7043
Notice: E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and
therefore may be disclosed to third parties.
From: Wade, Larry
Sent: Friday, November 15, 2013 10:21 AM
To: Stepp, Jonathan
Subject: NCG030644 Sypris Technologies
Hello Jonathan,
Please review the attached NO1 for the subject facility and let me know if you have any concerns with issuing a permit.
If a response is not received within 30 days from the date of this email, I will proceed with issuing the permit contingent
upon my review.
If you have any question or need additional information please let me know.
Larry W. Wade PE Telephone: (919) 807-6375
Fax: (919) 807-6494
Stormwater Permitting Program
North Carolina Department of Environment & Natural Resources
Division of Energy Mineral and Land Resources
161-2 Mail Service Physical Address - 512 N. Salisbury St. Room
9425
Raleigh, NC 27699-1612
Raleigh, NC 27604
************************This is a government E-mail address****************************
*********E-rails sent and received from this address can be disclosed to third parties************
2
Division of Water Quality / Surface Water
Protection Section
NCDENRNational Pollutant Discharge Elimination System
'jc— CA.C. iL t)EPWRT.. OF
Fx, m mrm Ann Rmtnv tie Rcrs
NCG030000
NOTICE OF INTENT
FOR AGENCY USE ONLY
Date Received
Ycar
Month
Da
14
11
14
Certificate of Coverage
Check #
Amoun:
34,1a7 1 4100
P rmii ASsi ned to
National Poiluiant Discharge Elimination System application for coverage under General Permit
NCG030000:
STORMWATER DISCHARGES associated with activities classified as:
SIC (Standard Industrial Classification) 335 Rolling, Drawing, and Extruding of Nonterrous Metals
SIC 3398 Metal Heat Treating
SIC 34 Fabricated Metal Products I? �� R 0W
SIC 35 Industrial and Commercial Machinery
SIC 36 Electronic and Other Electrical Equipment NOV 1 c! 2013
SIC 37 Transportation Equipment
SIC 38 Measuring, Analyzing, and Controlling Instruments DENR-Wkf ,RQUALITY
WETLANDS AND ST(Rt,41YATER BRAiV&
1
For questions, please contact the DWO Regional Office for your area. See page 4.
(Please print or type)
1) Mailing address of owner/operator (address to which all permit correspondence will be mailed):
Narrle -�, Y)On--i:� re f-/Iyoto G-�`r~ S
Street Address l o S`yn,o AASo-Fib OdF- Zt 12611A
City LIAQ91ti, l TD-4 State nr(- ZIP Code vMST-
Telephone No. y2t 176 q 1600 Fax: Fz T Y-? i-- s,Y;? Y--
2) Location of facility producing discharge:
Facility Name �Y�2=S Tcc.1¢NDLOC-zzr5
Facility Contact
Street Address
City
County
Telephone No.
Email
lU S- 11,/1¢1M s,1TT-4 /YrscL /lard _
lklo i26efr4- r✓ State IV r; ZIP Code AX-5',r-
15
v Rke-
3) Physical Location Information:
�/- `!l03G Fax: SzT
F
Please provide a narrative description of how to get to the facility (use street names, state road numbers, and
distance and direction from a roadway intersection). _E- go C�<iF lap - j1-#trcfTor�A .ed, /� Fa<
C4 L-'WCA: '1- —
l__"it AAk o N 2 j^� 1, f - f,5 T- &V r lftZk - W4m s,� onr X,'5 z I- - S i>'�, r j I !- 1- 4--r2 S
(A copy of a county map or USGS quad sheet with the facility clearly located must be submitted with this application,)
a to � I r �.�r �� �>✓ I�prj js f'
4) Latitude 35 q' Longitude VOW 3`� (deg, min, sec)
Page 1 of 4
SWU-218-071408 Last revised 7114/08
NCG030000 N.O.I.
5) This NPDES Permit Application applies to which of the following:
❑ ew or Proposed Facility Date operation is to begin
Existing
6) Standard Industrial Classification:
Provide the 4-digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial
activity at this facility.
SIC Code: 3 3- j
7) Provide a brief narrative description of the types of industrial activities and products manufactured at
this facility:�,�`n��W� eJ(N{�_�Lt/kja�N N- --° — i� e`"v.�
8) Discharge points 1 Receiving waters:
How many discharge points (ditches, pipes, channels, etc.) convey stormwater from the property?
What is the name of the body or bodies ater (creek, stream, river, lake, etc.) that the facility stormwater
discharges end up in? IQ dam}
Receiving water classification: K/ 5 TV ; Cf
Is this a 303(d) listed stream? `rE S Has a TMDL been approved for this watershed? NC
If the site stormwater discharges to a separate storm sewer system, name the operator of the separate storm
sewer system (e.g. City of Raleigh municipal storm sewer). MA
9) Does this facility have any other NPDES permits?
-qrNo
❑ Yes
If yes, list the permit numbers for all current NPDES permits for this facility:
10) Does this facility have any Non -Discharge permits (ex: recycle permit)?
*No
❑ Yes
If yes, list the permit numbers for all current Non -Discharge permits for this facility:
11) Does this facility employ any best management practices for stormwater control?
❑ No
❑ Yes (Show any structural BMPs on the site diagram.)
If yes, please briefly describe:
12) Does this facility have a Stormwater Pollution Prevention Plan?
❑ No
Yes
If yes, when was it implemented?
13) Are vehicle maintenance activities occurring at this facility?
KNo ❑ Yes
14) Hazardous Waste:
a) Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility?
❑ No x Yes
Page 2 of 4
SWU-218-071408 Last revised 7l14108
NCG030000 N.U.I.
b) Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste generated per month) of
hazardous waste?
❑ No l4Yes
c) Is this facility a Large Quantity Generator (1000 kg
hazardous waste?
['No ❑ Yes
or more of hazardous waste generated per month) of
d) is hazardous waste stored in the 100-year flood plain?
G6o ❑ Yes It yes, include information to demonstrate protection from flooding.
e) If you answered yes to questions b. or c., please provide the following information:
Type(s) of waste: Jvkt"J Vac,,Sce--�
How is material stareL
Where is material stored:v,
How many disposal shipments per year: 1
Name of transport 1 disposal vendor: Z — wtfi-i C /V V-;leol lJ 1161V
Vendor address: ,21 DA-L'-corms• A -VC, _ LDS ev(— `Zga
15) Certification:
North Carolina General Statute 143-215.6B (i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record, report,
plan, or other document filed or required to be maintained under this Article or a rule implementing this Article: or who
knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or
who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be
operated or maintained under this Article or rules of the Commission implementing this Article shall he guilty of a Class 2
misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000).
I hereby request coverage under the referenced General Permit. I understand that coverage under this permit
will constitute the permit requirements for the discharge(s) and is enforceable in the same manner as an
individual permit.
I certify that I am familiar with the information contained in this application and that to the best of my
knowledge and belief such information is true, complete, and accurate,
Printed Name of Person Signing: Lac�'`�
Title: E[kS GaGze42TNA-'re2
lure UApplicant)
t f f it /,7-0/3
(Date Signed)
This Notice of Intent must be accompanied by a check or money order for $100.00, made payable to:
NCDENR
Page 3 of 4
SWU-218-071408 Last revised 7114108
r s
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it
If I q.
90;
'k N11V -j�
Site Location
W
X,
7" 0
'6. 4
5
r
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—1054�
1- 7
k
X
N., I
Source: 2009 National Geographic Society, i-cubed; htip://goto.arcgisonline.cornlmaps?USA—Topo_Maps
ZVI-
VA
N4
Site Location N
0 1,000 2,000 4,000 6,000 8,000
u2izmmmzms= Feet
TOPOGRAPHICISITE LOCATION MAP
SYPRIS SOLUTIONS
106 WAMSUTTA MILL ROAD
amec-- MORGANTON, NORTH CAROLINA
PREPARED DATE CHECKED DATE JOB NUMBER I FIGURE
BY wil-I 1 1011-1 IBY m V'-J I 10) -Z�v 1 6252-11-1943
a Storm Sewer Inlet/Piping
OIL STORAGE LOCATIONSIOUTSIDE DRAINAGE
SYPRIS SOLUTIONS
105 WAMSUTTA MILL ROAD
MORGANTON, NORTH CAROLINA
rn�rnr 6252-11-1943 ��.,�.� 3
av 5 w1 iu � sal ev 1M 17.1 1 �w