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NCG030613_MONITORING INFO_20190305
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. I /v C) 3 O co 13 DOC TYPE ❑HISTORICAL FILE [K MONITORING REPORTS DOC DATE ❑ aD I Of 03 D5 YYYYM M DD %%ATERS EDGE ENVIRONMENTAL, LLC 1434 GHESTER ROAD • RALEIGH, NC 27608 • PHONE 919.219.5820 February 25, 2019 Mr. Joe Edwards, EHS Officer Matcor Metal Fabrication 835 Salem Road Welcome, North Carolina 27374 RECRVED MAR 0 5 Z019 CEN i FILES 0WR SECTION IVCGn3a6/3 Reierence: Stormwater Discharge Outfall Qualitative Monitoring Report, Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication- Year 2- Period I- January-June-2019 Welcome. North Carolina Waters Edge Job No R l 1-47 Dear Mr. Edwards: Waters Edge Environmental, LLC (Waters Edge) is pleased to provide two copies of the Year 2- Period I- January -June 2019 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome, North Carolina (see Figures I and 2). The past permit has expired in October 2017; however, it is our understanding that Matcor does not have to petition to renew since they are under a General Permit NCGO300000 (Part III -Section B- Subpart #1) and want merely to continue under the existing permit. We have completed the Discharge Outfall Qualitative Monitoring Report. Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A)_ Laboratory analytical results are documented in Appendix B. Based on these results, we have exceedances for the following: + Outfall001 1. Exceedance for copper which was detected at 0.0158 ntg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0.474 mg/L versus a benchmark at 0.067 mgfL. • Outfall 002 I. Exceedance for copper which was detected at 0.0228 mg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0,752 mg/L versus a benchmark at 0.067 mg/L. Based on the permit conditions, we will conduct a Tier 1 inspection of the facility. Any action items which will be reviewed and potential deficiencies addressed. The Tier 1 response will be recorded in the Stormwater Pollution Prevention Plan. Again, as detailed in earlier reports, due to the lowered benchmark thresholds resulting in benchmark exceedances. we previously sampled an upgradient surface water stream on the site (upgradient Lake Drive) as well as two samples collected from the roof drains. Both roof drain Stormwater Discharge Monitoring Report and Tier 1 Response Year 2- Period 1-January-June 2019 Matcor Metal Fabrication 61'elcome, 1VC Page 2 of 2 February 25, 2019 samples exceeded the zinc benchmark level at 0.067 mg/L (Roof- l at 1.9 mg/L, and Roof-2 at 0.23 mg/L). The background upgradient surface water samples were below the zinc benchmarks. Based on these results, we would conclude the following: Metals are present in the upgradient surface water sample at the facility. Even though they are below the zinc benchmarks. this metal is still present and can potentially be a constituting factor to the outfall values detected. Copper and zinc contained in the building materials or downspouts are also contributing to the zinc in the stormwater which would have nothing to do with the industrial activity at the site. While use understand that multiple exceedances from the same Outfall require a Tier II response, we believe that the other contributing factors to the exceedances are mitigating factors; therefore, we will continue with our normal sampling frequency. While we will continue to attempt to improve the stormwater quality at the facility, we believe that these type of metals exceedances are largely due to non -industrial sources and can be found in a wide variety of non -industrial settings (e.g. residential or any structures with metal components). If there are any questions, please contact us at Arahn(?watersed_ eenv_com. Sincerely, WATERS EDGE ENVIRONMENTAL, LLC -; �4 :zl-! Phillip L. Rahn President cc: NCDEQ Stormwater (two copies) 19-017/PLR di tt ! , OC • f ' J �- � �-- I� + `- �/ 1j � r • '� � ` � "rV`r�/J5/ : � �.'' • 11� am IF y�. � 1 ti l.`r•} � f ��IY. SITE vj �; , , _ :�, .•hailer! , , �' , , �_� - l`••�� --�..�� _ �-;., '{s ,�-.'f� ����, _r. •Par � ,t . � � �, ; � ��. 40 i . - --�- ' � ,. �; _ �I� . � ; ' r' � �'- c = •�I � - �� =. f- ; � , ,, ram. ,; ► . ,, . . - J ram-- � � t .. ,r� _ .c n I !'1 t r .� AS '� fi��i i - i 1L _ . • L1.�r-'f r- •1�= MA,ATr- R S EDGE ENVIRONMENTAL, LLC Job NO. R1147 Topo Quad Welcome Date 1.19.2012 Title Project Location Map File Name Figure Scale Project Mateor tiPl'1' R1147.xIs 1 unknown WclwTnc, North Carolina ®C sin r rf: �, i tch Basin FF Catch 5' Job No. lmagelPhoto Dam Title Site &Surrounding Properties Map �7RS EDGE ENMRONMENTAL, LLC R1147 Davidson Co. GIS 10.27.2011 File Name Figure Scale Pro)ecr Matcor SPPP RI I47.xls 2 unknown Weleome, North Carolina Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No, NCG030000 Date submitted 2.25.19 CERTIFICATE OF COVERAGE No. NCG030613 FACILITY NAME Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace, Lab Cert. n _37706_ Comments on sample collection or analysis: None Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _,2019` SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly' _ (mouth) DISCHARGING TO CLASS ®ORW ❑HQW ❑Trout ❑PNA ❑Zero -flaw - ❑Water supply [:]SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfalt No. Date Sample Collected' (mo/dd/ r) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar OR,G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks =__> - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 Z/12/19 0.16 21.4 6.5 0.0158 NO 0,474 NA NA 002 2/1Z/19 0.16 22.9 6.7 0.0196 NO 0.752 NA NA Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. `See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as fount in 40 CFR 469A2; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page t of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall indude a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan.' Name (Print name) Ell S Title (Print title) ignature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, tliev must be tepprted in the format, "<XX ms/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfdli No. Date Sample Collected' {mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended SvftdS pH Benchmarks 1s mg/L 106 mg/L or 50 mg/L' 6.0 — 9.0 Sul Footnotes from Part A also apply to this Part B See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012.10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION 9, • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mallon original and d one copy of this_DMR_ including -all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the passibility of fines and imprisonment for knowing violations." 23 nature of Permittee) (Date) Permit Date: 11/1/2012-10/31/200 SWU-245, last revised 10/25/2012 Page 3 of 3 a Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onftlling outthisfornr, please i,isil: http://h2o.enr.state.nc.US/su/Forms_ DOCllments.htm4iniscCorms Permit No.: I N I C I G' 0 1 3 1 0 0 1 0` 01 or Certificate of Coverage No.: I N E C G 0 3 10 16 1 1 3 Facility Name: Matcor Metal Fabrication County: Davidson Inspector: Thomas Haynes Date of Inspection: 2.12.19 Time of Inspection: 10:45 AM Total Event Precipitation (inches): 0.16 Phone No. 336.731.5742 Was this a Representative Storm Event? (See information below) ® Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be pe?formed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: _& ;Z/ (Signature of Permittee or Designee) I Outfall Description: Outfall No. 001/002 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Unnamed Tributary of Swearincl Creek Describe the industrial activities that occur within the outialI drainage area: Metal Fabrication 2 Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Liqht brown Page 1 of 2 SWU-242-1 12608 3 Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak: chlorine odor, etc.): No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: (J 2 3 4 5 S Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with Floating solids: lO 2 3 4 5 G Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: I Q 3 4 5 7 Is there any foam in the stormwater discharge? Yes No 8 Is there an oil sheen in the stormwater discharge? Yes No 9 is there evidence of erosion or deposition at the oulfall? Yes No 10 Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-1 12608 aceAnaiytical' www.paadab&=" February 19, 2019 Mr. Phil Rahn Waters Edge Environmental 1434 Chester Road Raleigh, NC 27606 RE: Project: Matcor R11-47 Pace Project No.: 92417670 Dear Mr. Rahn: Pace Analytical Services, LLC 205 East Meadow Road -Suite A Eden, NC 2728a (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2019, The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Clayton McCrickard clayton.mccrickard@pacelabs.com (336)623-8921 Project Manager Endosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pact: Analytical Services, LLC. Page f of 11 aceArralyt►cal www.pacelatucam Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-6921 CERTIFICATIONS Project: MatcorR11-47 Pace Project Na.: 92417670 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Cerlification #: M-NC030 VrginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 Eden Certification lDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37739 North Carolina Wastewater Certification #: W3 VirginiaNEtAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 11 aceAnalytical. wwwpaostabswm Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 SAMPLE SUMMARY Project: Matcor R11-47 Pace Project No.: 92417670 Lab ID Sample ID Matrix Date Collected Date Received 92417670001 Outfall001 Water 02/12/1913:30 02/1311916;02 92417670002 Outfall002 Water 02/1211914:00 02/13/1916;02 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written Consent of Pace Analytical Services, LLC. Page 3 of 11 aceftlytical' wow omelabsoam SAMPLE ANALYTE COUNT Project: Matcor R11AT Pace Project No.: 92417670 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 2728a (336)623-8921 Lab ID Sample ID Method Analysts Analytts Reported Laboratory 92417670001 Outfall 001 SM 264OD-2011 SOB 1 PASI-E EPA9040C NMH 1 PASI-E EPA 200.7 Rev 4.4 1994 IDS 3 PASI-A 92417670002 Outfall 002 SM 254OD-2011 SOB 1 PASI-E EPA 9040C NMH 1 PASI-E EPA 200.7 Rev 4.4 1994 IDS 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 11 aceAnaiximl # www.pawsbs cam ANALYTICAL RESULTS Project: MatcorR11-47 Pace Project No.: 92417670 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Sample: Outfall 001 Lab ID: 92417670001 Collected: 02112119 13:30 Received: 02/13/19 16:02 Matrix: Water Report Parameters Results units Limit MDL DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 21.4 mg1L 2.6 2.6 1 02114119 13:47 9040 pH Analytical Method_ EPA 9040C pH at 25 Degrees C 6.5 Std. Units 0.10 0,10 1 02/15119 10:41 H3 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Capper 15.8 ug/L 5.0 2.5 1 02/15/19 02:49 02/18/19 00:41 7440-50-8 Lead ND ug1L 5.0 2.5 1 02/15/19 02:49 02/18/19 00:41 7439-92-1 Zinc 474 uglL 10.0 2.5 1 02/15/19 02:49 02/18/19 00:41 744Q-66-6 Sample: Outfall 002 t_ab ID: 92417670002 Collected: 02112/19 14:00 Received: 02113/19 16:02 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 22.8 mg1L 3.5 3.5 1 02/14/19 13:48 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.7 Std. Units 0.10 0.10 1 02115119 10.44 H3 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 19.6 ug1L 5.0 2.5 1 02/15/19 02:49 02/16/19 00:44 7440.50-8 Lead ND ug1L 5.0 2.5 1 02/15/19 02:49 02/18/19 00:44 7439-92-1 Zinc 752 ug1L 10.0 2.5 1 02/15/19 02:49 02/18/19 00:44 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/19/2019 10:22 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 11 aceAnafytical wwwpacefaGscnm QUALITY CONTROL DATA Project: Matcor R11-47 Pace Project No.: 92417670 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 2728E (336)623-8921 QC Batch: 458184 Analysis Method: SM 2540D-2011 QC Batch Method: SM 25400-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92417670001, 92417670002 METHOD BLANK: 2498144 Matrix: Water Associated Lab Samples: 92417670001, 92417670002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 2.5 02/14/19 13:33 LABORATORY CONTROL SAMPLE: 2498145 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 232 93 90-110 SAMPLE DUPLICATE: 2498146 92417521001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mglL ND NO 5 SAMPLE DUPLICATE: 2498147 92417521002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L NO ND 5 Results presented an this page are In the units Indicated by the "Units- column except where an alternate unit Is presented to the fight of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/19/2019 10:22 AM without the written censent of Pace Analytical Services, LLC. Page 6 of 11 • aeemalximie www.pacsbbs.com QUALITY CONTROL DATA Project: Matcor R11-47 Pace Project No.: 92417670 QC Batch: 456387 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH EDEN Associated Lab Samples: 92417670001, 92417670002 Pace Analytical. Services, Lt-C 205 East Meadow Road - Suite A Eden, NC 27288 (338)6238921 SAMPLE DUPLICATE: 2499000 92417670001 Dup Max Parameter Units Result Result RPD RPD Qualifiers pH at 25 Degrees C Sid. Units 6.5 6.6 1 9 H3 Results presented on this page are to the units indicated by the -Units- column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02119/2019 10:22 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 11 acMnalytical" www.pacobsx" QUALITY CONTROL DATA Project: Matcor R11.41 Paoe Project No.: 92417670 QC Batch: 458308 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA200.7 Rev4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92417670001, 92417670002 .A Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NO 27288 (336)623-8921 METHOD BLANK: 2498777 Matrix: Water Associated Lab Samples: 92417670001, 92417670002 Blank Reporting Parameter units Result Limit MDL Analyzed Qualifiers Copper Ug1L ND 5.0 2.5 02/18/19 00:09 Lead ug/L ND 5.0 2.5 02/18/19 00:09 Zinc ug/L ND 10.0 2.5 02/18/19 00:09 BC LABORATORY CONTROL SAMPLE: 2498778 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper ug/L 500 524 105 85-115 Lead ug/L 500 509 102 85-115 Zinc ug/L 500 526 105 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2498779 249B780 MS MSD 92417505001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual Copper ug/L 69.4 500 500 587 597 104 106 70-130 2 20 Lead ug/L 16.9 500 500 496 501 96 97 70-130 1 20 Zinc ug/L 1060 500 500 1520 1540 93 96 70-130 1 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2498781 2498782 MS MSD 92417720MI Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qua[ Copper ug/L 70.5 500 500 600 597 108 105 70-130 1 20 Lead ug/L 29.1 500 500 470 465 88 87 70-130 1 20 Zinc ug/L 193 500 500 695 685 101 98 70-130 2 20 Results presented on this page are in the units inclicatep 4y the "Units" column except where an alternate unit is presented to the right or the re5utt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/1912019 10:22 AM without tyre written consent of Pace Analytical Services, LLC. Page 8 of 11 Paco Analytical Services, LLC 205 East Meadow Road - Suite A ace,naiyrical Eden. NC 27280 WvVW.p7CErab c0M (336)623-8921 QUALIFIERS Project: Matcor R11-47 Pace Project No-: 92417670 DEFINITIONS DF - Dilution Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit- RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydra2ine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) OUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acryton"ttrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS BC The same analyte was detected in an associated blank at a concentration above 112 the reporting limit but below the laboratory reporting limit. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/19/2019 10:22 AM without the written consent of Paco Analytical Services, LLC. Page 9 of 11 acmnalytical ~.Pacelahs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Matcor R11-47 Pace Project No.: 92417670 Pace Analytical Services, LLC 205 East Meadow Road - Sulte A Eden, NC 27288 (336)623-8921 Lab ID Sample ID QC Batch Method QC Batch Analytical Analytical Method Batch 92417670001 Outfall 001 SM 2540D-2011 458184 92417670002 Outfall 002 SM 2540D-2011 458184 92417670001 Outfall 001 EPA 9040C 458387 92417670002 Outfall 002 EPA 9040C 458387 92417670001 Outfall 001 EPA 200.7 Rev 4.4 1994 458308 EPA 2007 Rev 4A 1994 458330 92417670002 Outfall 002 EPA200.7 Rev 4.4 1994 458308 EPA200.7 Rev 4.4 1994 458330 Date: 02119/2019 10:22 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC- Page 10 of 11 rrtYw-WFG== CHAIN -OF -CUSTODY Analycinl Request Rocumenc WU?:w YRLL �° „�� @Y*� �•� U�Ibuilt�� •.uurl,u 7.0 ra prrwrkkr...4RN.Ysu'.w.F�R+•_-_� ¢41'� If 1# vJYI�,M .Y•H,e [,wWr�,Y�•.d YY TWY Yaww.ya, Y.w.:¢�ldwwi •^ \ vnPrl .,, wsa Y=..w./Y. n�iM�xwrwri' wwr.`�rer/ - • rs.. �irl., �xJw e wMfelwa Yal.� �N 1l v¢�r. 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Nen,ryl¢A YYw� rr'..OIMr{OTI mW�w SF+e�Y4 M.nrt•� ���' 4� W'nPunwu�=1 w� rYn. �0�'[rY an. rww a �tl r � r n+law.r..,y..�yp.,ta-a+a.l�..rMrww� Y,xakz.k.a n..- d, vro., xour,.mu„l.nrr.�n. w kt� t�snw.r.marnw.at: rn n•W }�»�' 4dYr lr'vm (.+.IMm.,f�,�aC [Mn:Cc+w..tl Src:.Cl YAK ..r:kl.:.w.lUxW canr,n-1 2360312 40NMxWmkY4•eMMI•sRl<ynl. v m¢w,rne'rwx.L: / IYOYi aY/ (y.r drr VInP•�,N r.kl+�x Mtr '7/34 .f�r.li�Yk'.1� � MIk WYfSY GLL CSYw[nY �NnG e.K vq'll'I�••1 YY �h'.Yn+�YYrx',19Frw+1 Px.ftcw. hnaYY 4� 2t3•R 1MirYlkpYw¢r , H0. H 111 qlv nM,Y.Y.k,dlwYCaraY�k: lS.e,r.Y e,w. .+, rkY.Ywstr•�rr UW++•Y: 1�.,-.w. �.�w�.n..w •+Y.� •ti � Y.c K _L WATERS EDGE ENVIRONMENTAL LL,C 1� 34 CHESTER ROAD e RALEIGH, NC 27608 - PHONE 919.219.5820 August 14. 2018 Mr. Joe Edwards, EFIS Officer 03 a(/ 3 Matcor Metal Fabrication 835 Salem Road Welcome, North Carolina 27374 Reference: Stormwater Discharge Outfall Qualitative Monitoring Report, Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication- Year I- Period 2- July-December-2018 Welcome, North Carolina RECEAVE® Waters Edge Job No R 1 1-47 Dear Mr. Edwards: CEINITRAL FILES DWR SECTION Waters Edge Environmental. LLC (Waters Edge) is pleased to provide two copies of the Year 1- Period 2- July-Decembcr 2018 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome, North Carolina (see Figures 1 and 2). The past permit has expired in October 2017, however, it is our understanding that Matcor does not have to petition to renew since they are under a General Permit NCG0300000 (Part II[ -Section B- Subpart 4 1) and want merely to continue under the existing permit. We have completed the Discharge Outfall Qualitative Monitoring Report. Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A). Laboratory analytical results are documented in Appendix B. Based on these results, we have exceedances for the following: • Outfall001 . Exceedance for copper which was detected at 0.0286 mg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0.442 mg/L versus a benchmark at 0.067 mg/L. • Outfall002 1. Exceedance for copper which was detected at 0.0076 mg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0,250 mg/L versus a benchmark at 0.067 mg/L. Based on the permit conditions, we will conduct a Tier I inspection of the facility. Any action items which will be reviewed and potential deficiencies addressed. The Tier I response will be recorded in the Stormwater Pollution Prevention Plan. Again, as detailed in earlier reports, due to the lowered benchmark thresholds resulting in benchmark exceedances, we previously sampled an upgradient surface water stream on the site (upgradient Lake Drive) as well as two samples collected from the roof drains. Both roof drain Stormwater Discharge Monitoring Report and Tier 1 Response Year 1- Period 2-July-December 2018 Alatcor Metal Fabrication Welcome, NC Page 2 of 2 August 14, 2018 samples exceeded the zinc benchmark level at 0.067 mg/L (Roof I at 1.9 mg/L. and Roof-2 at 0.23 mglL). The background upgradient surface water samples were below the zinc benchmarks. Based on these results, we would conclude the following: • Metals arc present in the upgradient surface water sample at the facility. Even though they are below the zinc benchmarks, this metal is still present and can potentially be a constitutim, factor to the outfall values detected. • Copper and zinc contained in the building materials or downspouts are also contributing to the zinc in the stormwater which would have nothing to do with the industrial activity at the site. While we will continue to attempt to improve the stormwater quality at the facility, we believe that these type of metals exceedances are largely due to non -industrial sources and can be found in a wide variety of non -industrial settings (e.g. residential or any structures with metal components). If there are any questions, please contact us at prahnOwwatersedgeenv.com. Sincerely. WATERS EDGE ENVIRONMENTAL. LLC Phillip L. Rahn President cc: NCDEQ Stormwater (two copies) 18-064/PLR/aht ti '•• '„ .�.� t�( f \,off ir r ■� -.#. _,_-_ -- �._�—�•, L �\ '/ i•� f1 / ���� Sat �• �. r�'% �3 � �+� `I" � \�� tea- � •� '//'�_ 1 ' l f'- `■ 1� ���� ���'''�"' __��- �^ `� a��'1 •. cam- ✓f-"�' y rp,�• 1- '��- {� �� �� r ■ � ~ �_� ` � � ` -? • pis L • r ' • L`` "� il _� �`�y� � _I tit � __ •�. �.t�` � •\` 1 r ego • ■ .ems ��. �� 1� 1+ �. • 'bra l_1 y-r ; , j\+ �I I i ` `r �. ] ,V 1.4 ^-1 // /ff 'j+-�� \,.� �F v i� ^ r' •�•-_. .J0 • 1 rL r ✓ �`' N all \ • `/ `■ �JJDl2 IC �! .- - - l �✓ { � •: S •r ,f% - y- / - 1 y • 1 , 1 ` 1 �� 1c fi1�•Jf� ! �f''(�:�' _ WATERS EDGE ENVIRONMENTAL, LLC Job No. R11-47 Topa Qeud Welwme fate 1.19.2012 Title Project Location Map File Name Figure Scale Project Mateot SPPP R11-07.xls 1 unknown Welcome, North Carolina 01 Job No. Image/Photo Bate ride kTERS EDGE ENVIRONMENTAL, LLC R1147 Davidson Co. GIS 10.27.201 i Site &Surrounding Properties Map File Name Figure Scafe Project Matcor SPPP RI147.xis 2 unknown I Welcome, North Carolina Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 8.14.1$ CERTIFICATE OF COVERAGE NO. NCG030613 FACILITY NAME _Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace Lab Cert. 9 _37706_ Comments on sample collection or analysis: None Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _ 2018_ SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ®ORW ❑HCLW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA []Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches} Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics" Benchmarks 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L i mg/L 001 8/1/18 0.78 49.4 6.8 0.0286 ND 0.442 NA NA 002 8/1/18 0.78 ND 6.9 0.0076 ND 0.250 NA NA ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies_ s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the 770 monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (T O), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in,the Stormwater Pollution Prevention Plan." Name (Print name) IF/V:.5 Title (Print title) gnature) (Date) Note: Results must be reported in numerical format, Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Mote: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses- See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?2 Outfall No. Date Sample Collected"'amount, (mo/dd/yr) 24-hour rainfall inches Non -polar O&G/TPH by, EPA 1664 (5GT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/Lk 6.0 — 9.0 5U Footnotes from Part A also apply to this Part 8 ' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER I REQUIREMENTS_ SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION 8. ■ TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DM& including all "No Discharge" reports, within 30 days of receipt of the lab results o_ r_at end of monitoring period in the case of "No Discharge" reports) to: Division of water Quality Attn: DWCI Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete_ I am aware that there are significant penalties for submitting false information, including the passibility of fines and imprisonment for knowing violations." (Si&dature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: hlt :/lh2o.enr.state.nc,us/su/Forms Documents.htm#miscforms Permit No.: I N I C I G1 0 13 10 10 10 1 0� or Certificate of Coverage No.: I N I C I G 10 13 10 16 l 1 13 Facility Name: Matcor Metal Fabrication County: Davidson Phone No. 336.731.5742 Inspector: Thomas Haynes Date of Inspection: 81.18 Time of Inspection: 10:20 Total Event Precipitation (inches): 0.78 Was this a Representative Storm Event? (See information below) ® Yes ❑ No Please check your permit to verify if Qualitative Monitoring must he performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature. I certify that this report isaccurateand complete to the best of my knowledge: (Signature of Permittee or Designee) 1 Outfall Description: Outfall No. 001 /002 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Unnamed Tributary of Swearing Creek Describe the industrial activities that occur within the outfall drainage area: Metal Fabrication 2 Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Liaht brown Page l of 2 SWU-242-1 12608 3 Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 2 0 4 5 5 Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: tD 2 3 4 5 6 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: l 2 3a 4 5 7 is there any foam in the stonnwater discharge? Yes No 8 Is there an oil sheen in the stormwater discharge? Yes No 9 Is there evidence of erosion or deposition at the outfall? Yes No 10 Other Obvious Indicators of Storrawater Pollution: List and describe Norte Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosionldeposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S WU-242-1 12608 5ac ( e Analytical wwwpacetabseom August 13, 2018 Mr. Phil Rahn Waters Edge Environmental 1434 Chester Road Raleigh, NC 27606 RE: Project: Matcor R11-47 Pace Project No.: 92394134 Dear Mr. Rahn: Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Enclosed are the analytical results for samples) received by the laboratory on August 02, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Clayton McCrickard clayton.mccrickard@pacelabs.com (336)623-8921 Project Manager Endosures ,o geORA�~ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 acmnalytrcal' www.pacelaUcom Project: Matcor R11-47 Pace Project No.: 92394134 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 North Carolina Wastewater Certiflcation #: 633 VrginiaNEL-AP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden. NC 27288 (336)623-8921 Page 2 of 13 aceAnalyffcal. wwwpacelabs.cvm Project: MatcorR11-47 Pace Project No.: 92394134 Lab ID Sample ID 92394134001 Outfa ll 001 92394134002 Outliall002 SAMPLE SUMMARY Matrix Date Collected Date Received Water 08/01/18 13:00 08/02/18 09:20 Water 08101/1813:30 08/02/1809:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical services, LLC. Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 3 of 13 aceAnalyfical. wwrpacerafteam SAMPLE ANALYTE COUNT Project: Matcor R11-47 Pace Project No.: 92394134 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92394134001 Outfall 001 SM 254OD-2011 NMH 1 PASI-E EPA9040C NMH 1 PASI-E EPA200.7 Rev4A 1994 SH1 3 PASI-A 92394134002 Outfall 002 SM 2540D-2011 NMH 1 PASI-E EPA 9040C NMH 1 PASI-E EPA 2007 Rev 4.4 1994 SH 1 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 r � aceAnaIXical wrw.pe09aUMn ANALYTICAL RESULTS Project: Matcor R11-47 Pace Project No.: 92394134 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Sample: Outfall 001 Lab ID: 92394134001 Collected: 08/01/18 13:00 Received: 08102I16 09:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No, Qual, 2640D Total Suspended Solids Analytical Method: SM 2WD-2011 Total Suspended Solids 49.4 mg1L 5.0 5.0 1 08/06/18 10-04 06 9040 pH Analytical Method: EPA 9040C PH at 25 Degrees C 6.8 Std. Units 0,10 0.10 1 08/03118 11:24 H3,H6 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 28.6 ug1L 5.0 2.5 1 0810411606-10 0810911816:26 7440-50-8 Lead ND ug1L 5.0 2.5 1 08104118 06-10 08/09/18 16:26 7439-92-1 Zinc 442 ug1L 10.0 2.5 1 08104118 06:10 08109/18 16:26 7440-66-6 Sample: Outfall 002 Lab ID: 92394134002 Collected: 08/01/18 13:30 Received: 08/02/18 09:20 Matrix: Water Report Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual 25401) Total Suspended Solids Analytical Method: SM 2WD-2011 Total Suspended Solids ND mg1L 5.0 5.0 1 08/06/18 10:05 9040 pH Analytical Method: EPA9040C PH at 25 Degrees C 6.9 Sid. Units 0.10 0,10 1 08103/18 11:35 H3,H6 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA200.7 Rev 4A 1994 Copper 7.6 ug/L 5.0 2.5 1 08F04118 06:10 08/09118 16:29 7440-50-8 Lead ND ug1L 5.0 2.5 1 08/04/18 06:10 08109/18 16:29 7439-92-1 Zinc 250 u91L 10.0 2.5 1 08M4118 06:10 08/09118 16:29 7440-66-6 Date: 0811312018 06:52 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 5 of 13 acMnalytiical s wwwpacalabacam QUALITY CONTROL DATA Project. Matcor R11-47 Pace Project No.: 92394134 QC Batch: 423246 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92394134001, 92394134002 METHOD BLANK: 2341681 Matrix: Water Associated Lab Samples: 92394134001, 92394134002 Blank Reporting Parameter Units Result Limit MDL Analyzed Total Suspended Solids mg/L NO 2.5 2.5 08/06/18 10:03 LABORATORY CONTROL SAMPLE: 2341682 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2341683 Parameter Units Total Suspended Solids mg1L Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)62M921 Qualifiers Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 250 264 106 90-110 92394134001 Dup Max Result Result RPD RPD Qualifiers 49.4 96.0 64 5 D6 SAMPLE DUPLICATE: 2341684 92394134002 Dup Parameter Units Result Result Total Suspended Solids mg/L ND NO Max RPD RPD Qualifiers 5 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/13/2018 06:52 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 acmnalytrcal. www.pacefabscarn QUALITY CONTROL DATA Project: MatcorR11-47 Pace Project No.: 92394134 QC Batch: 422920 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH EDEN Associated Lab Samples: 92394134001, 92394134002 Paco Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NG 27288 (336)623-6921 SAMPLE DUPLICATE: 2340300 92393858003 Dup Max Parameter Units Result Result RPD RPD Qualifiers pH at 25 Degrees C Sid. Units 7.7 7.8 0 9 H3,H6 Results presented on this page are In the units indicated by the "units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/13/2018 06:52 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 lacmnalXimle rww.paoelabt: =m QUALITY CONTROL DATA Project: Matcor Rll-47 Pace Project No.: 92394134 QC Batch: 423092 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92394134001, 92394134002 METHOD BLANK: 2341237 Associated Lab Samples: 92394134001, 92394134002 Parameter Units Copper LVL Lead uglL Zinc ug1L Matrix: Water Blank Reporting Result Limit ND 5.0 ND 5.0 ND 10.0 MDL Analyzed 2.5 08/09118 1611 2.5 08/09/1816:11 2.5 08/09/18 16:11 Pace Analytical Services, LLC 205 Cast Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Qualifiers LABORATORY CONTROL SAMPLE: 2341238 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug1L 500 496 99 85-115 Lead ug1L 500 465 93 85-115 Zinc ug1L 500 459 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2341239 2341240 MS MSD 92394429001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc, Result Result %Rec %Rec Limits RPD RPD Qual Copper uglL ND 500 500 517 496 103 99 70-130 4 20 Lead uglL ND 500 500 488 467 98 93 70-130 4 20 Zinc ug/l_ ND 500 500 491 467 97 93 70-130 5 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2341241 2341242 MS MSD 92394408001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc, Conc. Result Result % Rec % Rec limits RPD RPD Qual Copper ug1L 8.0 500 500 471 474 93 93 70-130 1 20 Lead ug1L ND 500 500 461 464 92 93 70-130 1 20 Zinc uglL 11A 500 500 499 500 98 98 70-130 0 20 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right Of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/13/2018 06:52 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 aceAnalj&al. wwwpBr�fe6seam QUALIFIERS Project: Matcor R11-47 Pace Project No.: 92394134 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit, Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitfosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/13/2018 06:52 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 Pace Analytical Services, LLC 205 East Meadow Road - Suite A acaAnalytrea! Eden, NC 27288 www.Petelabs.corn (336)623-8924 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Matcor R11-47 Pace Project No.: 92394134 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92394134001 Outfall 001 SM 264OD-2011 423246 92394134002 Outfall 002 SM 254OD-2011 423246 92394134001 Outfall 001 EPA 9040C 422920 92394134D02 Outfall 002 EPA 9040C 422920 92394134001 Outfall 001 EPA 200.7 Rev 4.4 1994 423092 EPA 200,7 Rev 4.4 1994 423109 92394134002 Outfall 002 EPA 200.7 Rev 4.4 1994 423092 EPA 200.7 Rev 4A 1994 4231 D9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/13/2018 06:52 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised. February 7' 20" Sample Condition Upon Recelpt(SCUR) j Page 1 of 2 �C--Andlyfical' powment No.: issuing Authority: i F-CAR-CS-033-Rev,06 1 Pace Carolinas Quality Offlce Laboratory receiving samples: Asheville ❑ Ede nit Greenwood ❑ Huntersville❑ Raleigh[] Mlechanicsville❑ XNEWAIM Client Name: FWO#: 92394134 Project N-Courier: ❑Fed6 ❑UP ❑USPS lent11I111I1I1 III � III ❑ Commercial ❑Pare ❑Other: 134 Custody Seal Present? ❑Yes Seals intact? ❑Yes ❑No Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap ❑Bubble Bags one ❑ Other Biological issue Fras ? Thermometer. j}n= ❑Yes ❑No /A ❑fR Gun 114L `- 1 Type of ice: et ❑81ue Q:^Icae Cooler Temp ('C): 2'H Correction Factor. Add/Subtract (°C) - i . ,Z � Temp shouldheabove freezing tofi'[ Cooier Temp Corrected ('C): [samples out of temp criteria. Samples on Ice, cmling process has beget USDA Regulated SoiE N/A, water sample) Did samples crl in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did sarnplesoriginate from a foreign source (fnternat) Ily; l-1Ye o indudh¢Havail and Puerto Rico)? nYes No Comm ents/Discre ancy: Chain of Custody Present? �EINu N/A 1. Samples Arrived within Hold Time? TnYC5 ao ❑N/A 2. f 4 Short Hold Time Analysis (02 hr.)? Na [QN/A 3. Rush Turn Around Time Requested? f ]Yes No ❑N(A b. Sufficient Volume? Yes ❑No ❑N/A S. Correct Containers Used? Yes []to CJN/A 6. -Pace cog tainersUsed? ❑No [IN/A Containers Intact? es ❑No [3N/A 1 7. Dissolved analysis: Samples Feld Filtered? ❑yes No ❑N/A S. Sample Labels Match COC? a ❑No ❑N/A 9. W-r -includesDatafnine/ID/Analysis Matrix: Headspace in VOA Vials (>5-6mm)? ❑Yes ❑No LhNJA 10. Trip Blank Present? ❑Yes (]no N/A 11. Trip Blank Custody Seals Present? ©Yes []No N/A COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATIONjRESOLLMON Person contacted. Project Manager SCURF Review: Project Manager SRF Review: K1J Field Data Required? ❑Yet ❑No Lot IO of split containers: i}ate�me: Date. Date: � Page 11 of 13 CHAIN -OF -CUSTODY 1 Analytical Request Document -PaceAnalytieal' The Chain-ol-Custody is a LEGAL DOCUMENT. All relovant fields must be completed accurately. o [V of / tm Section A Section B Section C.Pago. To Required Client Iniamtalion: RagWrod Project Inlormation: Invoice Inlormalion, Company: /_ _ Report To: /f _ Attention: L•� f' •1 • �7 A e� l i 18 0 J O L.- 3.. ! V L 2178020 Address: •' �f •% %J. C _ Copy To: r r Company Name: REGULATORY AGENCY drew NPOES C- GROUND WATER F PRINKING WATER y i UST r RCRA OTHER Email To: • ^ / Purchase Order No.: �� "'7 Pnco Quota ` _ / Rm� ea: Phone: Fax: Proioct Name: �/� Prgnct ir5artager: Vie LOcatlon STATE: Requested Duo DatafTAT: Project Number: 7 P Pam" `���, s Regtiested Analysis Filtered (YIN) Section D Matrix Codes a z Required Chanl hslorma:ion MATR,x r Cooe o COLLECTED Praseiva[ivas r Drinking Water DW V z11 Water wT waste water ww ty m� cO"'P0S"E compaSnE O chi t=OdVCt P S START ENOR,RAB Z So;vsolid SL Q .r► } SAMPLE ID oil OL .. F ce N Wipe WP (A-Z. 0-91 r1 Air AR Lu "' W G a z 'a m ' Sample IDS MUST BE UNIQUE Tissue TS O Other OT X to L4O i. H. CL,i IL OLL ii O O 0 O 4: ar C y litN ~ PATE TIME GATE TIME tOY T r Z z t O y Pace Project No./ Lab I.D. 1 i ` l j b i .•(] i 3 4 5 6 7 9 10 1i t2 ADDITIONAL COMMENTS RELINQUISHED BY 1 AFFILIATION DATE TIME ACCEPTED BY i AFFILIATION DATE TIME SAMPLE CONDITIONS R1,2h 0?� SAMPLER NAME AND SIGNATURE v ORIGINAL v w z c PRINT Name of SAMPLER: f, 'n rr z c y w SIGNATURE of SAMPLER: DATE Signod MMiDDrfY): i fO 'Important Note: By signing iris form you are =ePlmrg Paco s NET 30 day payment terns end agreeing to fate charges at I.5%Per monitrig-any invoices Paid % F-ALL-Q-020rev.07, 15-May-2G07 Document Name: Condltlon Upon Rec, Document No.: 'Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Collform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle Document Revised: February 7, 2018 Page 1 of 2 Issuing Authority Pace Carolinas Quality Office Project #- WO# : 92394134 PM: CHM Due Date: 08/16/18 CLIENT: 95-Waters Ed 2 Z 41 c a N Q E rr c a m z TyA L O e N a = Lod N m a6 m 2 Z1 Z N e YJ A a E 1[1 N a Gococcm M ¢ V N O u H .4 a, a S 4 A i% E Ln a a N V i H n E y©� fV m n. A C3 d d u N a E t^ �j a a. m '� ^ m Vrn N a E �, N v a � A L E a 3 k c d d ¢ d = rr f9 a G u d b L r S l7 a u N Q A C ¢ E N 9 �rf t7 a N V O .a E `m = p,, a V 0 = J E vat ry tit rn U a U E E d m Q d in q d z a >O E p d S a c7 a _ fTl a 4 F- at C7 Q E Y a C7 O a a A. et r7 n v� `q a 9 ' Y d Q w A > Y L7 i r A J E v, F= trf °u t V m in J E a N F ry 0-m 01 N z yV 14 o J c a N d a A. E 1 E 8 rl o 6 1 o — C E p 9 9 l7 7 c C! 4 E o Q 7 s a 1 1hN[W\N1N1NNNH1HHNN111! 2 I 1 l 3 N I 4 5 fi 7 8 9 10 13 12 -- — --—.------ -pH Adjustment Log. for Preserved. Samples Sample ID Type of Preservative pH upon receipt Data preservation adjusted Time presernt7on adjusted Amount of Preservative added tot 4 Note: Whenever there is a discrepancy affecting; forth Carollna compliance samples, a copy of this farm will be sent to the North Urauna ULMNK Ceftlrkattan Offce 1ue. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 13 of 13 + + .> WATERS EDGE ENVIRONMENTAL, LLC �01 WATERS EDGE DRIVE, SUITE 201 • RALEIGH. NC 27606 . PHONE 919.859.9987 . FAX 919.859.9930 October 23, 2017 RECE/1"', Mr. Jde Edwards, EHS Officer OCT 27 20p Matcor Metal Fabrication SrCENR-L4ND QU'AL835 Salem Roadrrr Welcome, North Carolina 27374 nll��,gTRP �cil7'i'Ir� Reference: Stormwater Discharge Outfall Qualitative Monitoring Report and Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication- Year 5- Period 2- July -December 2017 Welcome, North Carolina Waters Edge Job No R11-47 Dear Mr. Edwards: Waters Edge Environmental, LLC (Waters Edge) is pleased to provide two copies of the Year 5- Period 2- July -December 2017 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome. North Carolina (see Figures 1 and 2). We have completed the Discharge Outfall Qualitative Monitoring Report. Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A). Laboratory analytical results are documented in Appendix B. Based on these results, we have exceedances for the following: Outfall 001 1. Exceedance for zinc which was detected at 0.734 mull, versus a benchmark at 0.067 mg/L. Outfa11002 1. Exceedance for zinc which was detected at 0.943 mg/L versus a benchmark at 0.067 mg/L. Based on the permit conditions, we will conduct a Tier 1 inspection of the facility. Any action items which will be reviewed and potential deficiencies addressed. The Tier 1 response will be recorded in the Stormwater Pollution Prevention Plan. Again, as detailed in earlier reports, due to the lowered benchmark thresholds resulting in benchmark exceedances, we previously sampled an upgradient surface water stream on the site (upgradient Lake Drive) as well as two samples collected from the roof drains. Both roof drain samples exceeded the zinc benchmark level at 0.067 mg/L (Roof-1 at 1.9 mg/L, and Roof-2 at 0.23 mg/L). The background upgradient surface water samples were below the zinc benchmarks. Based on these results, we would conclude the following: Metals are present in the upgradient surface water sample at the facility. Even though they are below the zinc benchmarks, this metal is still present and can potentially be a constituting factor to the outfall values detected. Stormwater Discharge Monitoring Report and Tier 1 Response Year 5- Period 2- July -December 2017 Matcor Metal Fabrication Welcome, NC Page 2 of 2 October 23, 2017 • Zinc contained in the building materials or downspouts are also contributing to the zinc in the stormwater which would have nothing to do with the industrial activity at the site. While we will continue to attempt to improve the Stormwater quality at the facility, we believe that these type of metals exceedances are largely due to non -industrial sources and can be found in a wide variety of non -industrial settings (e.g. residential or any structures with metal components). Waters Edge appreciates this opportunity to work with Matcor Metal Fabrication. If you have any questions or require any additional information, please contact me at 919.8599987 or at prahn@watersedgeenv.com. watersedgeenv.com. Sincerely, WATERS EDGE ENVIRONMENTAL, LLC �42V Phillip L. Rahn President CC: NCDEQ Stormwater (two copies) 17-069/PLR/aht �`,, �` .�� ; `� � �'��- :.. «.. k'( 1�1 � • •i --ter_: l,'�-����'�..�'-'�j�, ... �1 !'�� �� %/ �~-rr.-. ��� `�.,��-�I �• �f e nip 1 , �' i•, ,.,,�,��J..--^\� kl ��,1(�;1) ■ r..�. 1• 11 L �iF �.. 4r \ice ` ;, f .a��i� ,()\�p�~ • �� t '�I./ ti l VN ♦" �% V/ * �� (' \ Iwr ,: }, ���L"( L-�fJ t • '�y, �r 4 \ �jj= ,.�/ �■�• `t� 4 r 510 i v ✓ I !'`w� ,�.'" � � I� � y` t � �_.J r a _! * 1 C".'f�'1 ..1 "� 1�'1 }� ��.�. �F 4"..r�� _ ..� � L� �� f� �� j i �t ■Y � • � 4 S(y��'� j _f, � " •,1 E i L ,..1 ,J t r /%'"`\ �' rr ,. \;r ^ { 1/ / �y ■ ■ ` ■ �t •7 V • Y i .` • ��-•i`•R w. /. ^^. y r•_ +liR ' F� k—r �'r / . 'ti. 73 .�� / � w 3..•-.. a..r • s a • -�' i 5 f �� �.'� % E r, r'f i I • l s rr r`- ~� J y . __ ff fa f i !f✓"r' r M r�i� • `,i. 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Can, '� � �.7+�' n -' r +,i' +16' e r '1 � - '� .3 +•s�,ygA{T�J �.,,�' ' .nr'j �`h: 3 .y�a.a Nq • r�" ALI NX r a � atch+Basin ,MY . It t �.. t t•��y _'r^ A i � 1 f � �h� ��� >Y of t� t' T. ors R •:� {;. - r - r - �. -1. Catci Jab AV ImagelPhoto Dare Title T � RIl117 Davidson Co, GIS 1p,27,2011 Site &Surrounding Properties Map WATERS EDGE ENVIRONME:NTAL., LLC File !Lame Figure scale Project Mateor SPIT RI 147,xls 2 unknown Wcicomc. North Carolina Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 10.23.17 CERTIFICATE OF COVERAGE NO. NCG030613 SAMPLE COLLECTION YEAR _2016` FACILITY NAME _Matcor Metal Fabrication SAMPLE PERIOD ❑ Jan -June ®July -Dec COUNTY Davidson c r-. or []Monthly' (monthl PERSON COLLECTING SAMPLES T. Haynes RECEi,1! V EDIsCHARGING TO CLASS [gORW ❑HQW ❑Trout ❑1PNA LABORATORY Pace_ Lab Cert. # 37706_ Comments on sample ❑Zero -flow []Water Supply []SA collection oranalysis; None OCT 31 2017 ❑Other CENTRAL. FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 DWR SECTION Part A: Stormwater Benchmarks and Monitoring Results ❑ No discharge this period?2 outfall No. pate Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&GJTotal 'total Petroleum Hydrocarbons Toxic Organlcss Benchmarks 100 mg/L or SO mg/L 6.0 -- 9.0 0.007 mg/L 0,03 mg/L 0.067 me/L 15 mg/L 1 mg/L 001 916/17 0.25 ND 6.3 ND ND 0.734 NA NA 002 9/6J17 0.25 12.5 6.5 ND ND 0.943 NA NA x Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines forthe facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for I TO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) L L! Title (Print title) (5' ture) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format,_"<--XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No.Date Sample Collected, {mo/ddlyr) 24-hour rainfall amount, inches' Non -polar O&G/TPH by EPA 1664 jSGT-HEM) Total Suspended Solids pN Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/112012-10/31/2017 5WLI-245, last revised 10/25/2012 Page 2 of 3 Nate: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART_B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART 11 SECTION 8. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an orfaina l and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring perlod in the case of "No -Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YCWU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of taw, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permittee) Permit Date: 11/1/2012-10/31/2017 10-a0 � (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 �a I � F Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidan6e on filling out this form, please visit: httn://h2o.enr.state.nc.us/sulForms_Documents.htm#miscforms Permit No.: 1 N I C I G 10 13 10 10 10 10 I or Certificate of Coverage No.: j N I C I G 10 j 3 10 16 1 1 13 Facility Name: Matcor Metal Fabrication County: Davidson Phone No. 336.731.5742 Inspector; Thomas Haynes Date of Inspection: 9.6.17 Time of Inspection: 10:00 Total Event Precipitation (inches): 0.25 Was this a Representative Storm Event? (See information below) ® Yes ❑ No Please check your permit to verb if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report isaccurateand complete to the best of my knowledge: Z (Signature of Pertnittee or Designee) I Outfall Description: Outfall No. 001/002 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Unnamed Tributary of Swearing Creek _ Describe the industrial activities that occur within the outfall drainage area: Metal Fabrication 2 Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Liaht brown Pagel of 2 SWU-242-112608 3 Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: OI 2 3 4 5 5 Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and -5 is the surface covered with floating solids: 1 O 3 4 5 6 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: I 0 3 4 5 7 Is there any foam in the stormwater discharge? Yes No 8 Is there an oil sheen in the stormwater discharge? Yes No 9 Is there evidence of erosion or deposition at the outfall? Yes No 10 Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 aceAnalj cal' www,paaafabs.com September 18, 2017 Mr, Phil Rahn Waters Edge Environmental 1434 Chester Road Raleigh, NC 27606 RE: Project: Matcor Rll-47 Pace Project No.: 92354210 Pace Analytical Services, LLG 205 East Meadow Road - Suite A Eden, NC 27288 (336)62M92 t Dear Mr. Rahn: Enclosed are the analytical results for sample(s) received by the laboratory on September 06, 2017. The results relate only to the samples included in this report. Results reported h erein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, �er� � /�" Clayton McCrickard Clayton. mccrickard @ pacelabs.com (336)623-8921 Project Manager Enclosures rb REPORT OF LABORATORY ANALYSIS Tt�l This report shall not be reproduced, except In full, + without the written consent of Pace Analytical Services, LLC. gg��Sp4� Page 1 of 13 /5a'ceAnalyticai" w�rw.pacelaCa.mrri f I Project: Matcor R11-47 Pace Project No.: 92354210 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8$21 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification*: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification Ills 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 1lrginiaNELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 VrginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This reporl shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnalytical wwwpacefaucm I SAMPLE SUMMARY Project: Matcor R11-47 Pace Project No.: 92354210 Lab ID Sample ID Matrix Date Collected Date Received 92354210001 92354210002 Outfali 001 Outfall002 Water Water 09/06/17 12:00 09/0611712:30 09/06/17 16:00 0910611716:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L.L.C. Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 3 of 13 aceAnalj6caf' www,pacBfaGs.CAR1 SAMPLE ANALYTE COUNT Project: Ma1Cor R11-47 Pace Project No.: 92354210 Pace Analytltal Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-6921 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92354210001 Outfall 001 SM 2540D CTB 1 PASI-E EPA 9040 RAY 1 PASI-E EPA 200.7 SER 3 PASI-A 92354210002 Outfail 002 SM 2540D CT8 1 PASI-E EPA904D RAY 1 PASI-E EPA 200.7 SER 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 Pace Analytical Services, LLC e aceAnaly�ical 2D5 East Meadow Road -Suite A Eden, NC 27288 www.pacelabs.com (336)623-8921 I ANALYTICAL RESULTS Project: Matcor R11-47 Pace Project No.: 92354210 Sample: Outfall 001 Lab tD: 92354210001 Collected: 09/06/17 12:00 Received: 09/06117 16:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids ND mg/L 2.5 2.5 1 09/08/17 12:09 9040 pH Analytical Method: EPA 9040 pH 6.3 Sid. Units 0.10 0.10 1 09/07/17 16:38 H1,H6 200.7 MET iCP Analytical Method: EPA 200.7 Preparation Method: EPA 200,7 Copper ND ug/L 5.0 2,5 1 09/16/17 17:35 09116117 08:00 7440-50.8 Lead NO ug/L 5.0 2,5 1 09116117 17,35 09/18/17 08:00 7439-92-1 Zinc 734 ug/L 10.0 2,5 1 09/16/17 17:35 09118/17 08:00 7440-66.6 Sample: Outfall 002 Parameters Lab 1D- 92364210002 Collected: Report Results Units Limit 09/06117 12:30 MDL OF Received: 09/06/17 16:00 Matrix: Water Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 12.3 mg1L 2.5 2.5 1 09/08/17 12:10 9040 pH Analytical Method: EPA 9040 pH 6.5 Std. Units 0.10 0,10 1 09/07/17 16:38 1-11,1-16 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper NO ug/L 5.0 2.5 1 09/16/17 17:35 09/18/17 08:04 7440-50-8 Lead NO ug/L 5.0 2.5 1 09116/17 17:35 09118/17 08:04 7439-92.1 Zinc 943 ug/L 10.0 2.5 1 09/16/17 17:35 09/18/17 08:04 744"6.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2017 04:12 PM without the written consent of Pace Analytical Services, LLC. page 5 of 13 aeenalytical� www.pacelabs.com Project: Matcor R11-47 Pace Project No.: 92354210 QC Batch: 376870 QC Batch Method: SM 2540D Associated Lab Samples: 92354210001. 92354210002 METHOD BLANK: 2087808 Associated Lab Samples: 92354210001, 92354210002 Parameter Units Total Suspended Solids mg1L Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit MDL Analyzed Qualifiers ND 2,5 2.5 0910811712:08 LABORATORY CONTROL SAMPLE: 2087809 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 240 96 90-110 Results presented on this page am In the units Indicated by Jhe -Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2017 04:12 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 15a'ceAnalytical` www pacala6s txxn f QUALITY CONTROL DATA Project: Matcor R11-47 Pace Project No,: 92354210 QG Batch: 376775 Analysis Method: EPA9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN Associated Lob Samples: 92354210001, 92354210002 SAMPLE DUPLICATE: 2087482 Parameter pH 92354210001 Dup Units Result Result Std. Units 6.3 6.3 Pace Analytical Sarvlcas, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Max RPD RPD Qualifiers 0 9 H1,H6 Results preseited on this page are in the units indicated by he "Units" colurm exceptwhere an altemate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2017 04:12 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 L � 1�;a'ce Analytical www.pacefabs cam t r I Project: Matcor R11-47 Pace Project No.: 92354210 QC Batch: 377829 QC Batch Method: EPA 200.7 Associated Lab Samples: 92354210001. 92354210002 METHOD BLANK: 2093442 Associated Lab Samples: 92354210001, 92354210002 Parameter Units Copper ug/L Lead uglL Zinc ug/L QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit ND 5.0 ND 5.0 ND 10.0 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 MDL Analyzed Qualifiers 2.5 09/18/17 06.39 2.5 09/18/17 06.39 2.5 09/18/17 06:39 LABORATORY CONTROL SAMPLE: 2093443 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 498 100 85-115 Lead ug/L 500 495 99 85-115 Zinc ug/L 500 502 100 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2093444 2093445 MS MSD 92354077001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Copper uglL 8.9 500 500 512 475 101 93 70-130 7 20 Lead ug/L ND 500 500 498 471 99 94 70-130 6 20 Zinc ug/L 39.5 500 500 542 513 100 95 70.130 5 20 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2093446 MS 92354170001 Spike Parameter Units Result Conc, Copper ug/L 15.9 500 Lead ug/L ND 500 Zinc ug/L 0.10 mglL 500 2093447 MSD Spike MS MSD MS MSD % Rec Max Conc. Result Result % Rec % Rec Limits RPD RPD Qual 500 490 497 95 96 70-130 2 20 500 456 459 91 92 70-130 1 20 500 596 601 98 99 70-130 1 20 Results presented on this page are In the units Indicated tly the "Units" colurn except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2017 04:12 PM without the written consent of Pace analytical Services, LLC. Page 8 of 13 • aceAnalytical www.pepefatu.aDm i QUALIFIERS Project: Matcor R11-47 Pace Project No.: 92354210 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MID -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenytamine using Method 8270. The result reported for each analyte is a combined concentration, Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2017 04:12 PM without the written consent of Pace Analytical Services, L-C. Page 9 of 13 aceAnalytical wwwpacalabs m" I QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Malcor R11-47 Pace Project No., 92354210 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92354210001 Outfall 001 SM 2640D 376870 92364210002 Outfall 002 SM 25400 376870 92354210001 Outfall 001 EPA 9040 376775 92354210002 Outfall 002 EPA 9040 376775 92354210001 Outfall 001 EPA 200.7 377829 EPA 200.7 92354210002 Outfall 002 EPA 2007 377829 EPA 200.7 Date: 09118/2017 04:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 378089 378089 Page 110 of 13 Document Name: Document Revised: August 4, 2017 _ �WeAriafyticaJ'H Sample Condltion U on Retel t SCUR Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ EdenR] Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ !J Client w0 92�3542,1® L�l7xi_" �- Project q ent j I I jj Courier: OFed t OURS ' ❑USPS 0Cii ❑ Commercial []Pace ❑Other: jjjj I I a 1 11 I' .92354210 Custody Seal Present? ❑Yes ❑No Seats Intact? ❑Yes ❑No m DateJlnitta[s Person Examining Contents:27 `Lr -1 7 Packing Material: ❑Bubble Wrap []Bubble Bags []None 0 Other Biological Tissue Frozen? Thermometer: ❑Yes ❑Nu ❑N/A IR Gun ID: Ype o e; • �NeF QBlue ❑None T Correction Factor: Cooler Temp Corrected ('Cl: L' V Temp should be above freezing to WC ❑Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Sall (❑ N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? aid samples originate from a foreign source (internationally, Flyer FINn Indudina Hawaii and Puerto Rico)? I7lYes nNo C6mmenLS/QISCre: artttr: Chain of Custody Present? Yes No N/A 1. Samples Arrived within Hold Time? Yts No N/A 2. Short Hold Time Analysis (V2 hr.? ZlYes ❑No N/A 3. Rush Turn Around Time Ae nested? Yes No N/A 4. Sufficient Volume? Z Yes ©No ❑N/A S. Correct Containers Used? -Pace Containers Used? ,ffYes Yes [:)NO QN. QN/A N/A 6. Containers Intact? ovel LING EINfit, 7. Dissolved anal sir: Samples Field Filtered? YeS No N A 8. Sample Labels Match COL? -rnctudesDate/Time/ID/Analysis Matrix: ©Yes ❑No QN(A 9. Headspace in VOA Vials (sS•bmm)? 0YfS ❑Ho 14/A la. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ❑Na No ;?N/A /A 11- CLIENT NOTIFICATION/RESOLUTION Person'Contacted; Comments/5ample DiscrepanCy: Lot ID of split containers: Date rime: Field data Required? UYes L_JNo Project Manager SCURF Review: ��L Date: 4.1 7 Project Manager SRF Review: Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be seat to the North Carolina DENNR Certification Office (Le - out of hold, incorrect preservative, out of temp, incorrect containers) Page 11 of 13 2ceAnaVical' wrr,panlcbs.caln Section A Required Client Inlumation: Section B Required Project InformaWrl: CHAIN -OF -CUSTODY / Analytical Request Document The C"n�ot-Cuslody Is a LEGAL DOCUMENT. All relevant fields nwst be completed acc"tely. r 0 N Page: / of f mpg Section C to Invoice Informalien: CanpanY:, Repw TD: r / ,ji !/ Attenlian: 2 1. 36026 Address: // I Copy TO: .�, Company Name:'.... ;....... REGULATORY.AGENGY Address: ["- NPDES F— GROUNDWATER IT DRINKING WATER r UST i RCRA FX OTHER Emaa To: Purch;= Order No.: _ ` ' Pnw Quam Relurenr : Phone: Fax: P-Mct Name: ,H /�i'1PAWLager Paco Pmact Site Location �' Requested Duo DaterTAT: Project Number. Paw Prvr°a a STATE: Requested Analysis Filtered (YIN) Section D Matrix Codes Aoqulrod Clionl Information MarR€z r cool s C COLLECTED Preservatives y .....-•.c: �_..:..:.-::.. Drinking Water pw � o water WT Waste water NFW � QG� a rm ST4RT E Cr�GMa U � z Product P Soillserd SL SAMPLE ID oil oL C7 0 y WP (A•2. I19 ! ;) . Airpe AR W Sample IDa MUST BE UNIQUE Tissue TS O tt ha- ". N' �: U. d _ 0 ti to i O A_'t}1 11 11 b W. H -C -M Z U .�'Q' C' Lab I.D. • TIME DATE TIME N a Z T 2 Z p .w CC pace Project Nod .r•...' +DATE 2 c,-z�i a - i 6 8 S. to 41 12 ADDITI6N4L'C0I4IA ENTS RELINQUISHED BY f AFFILIATION F DATE - TIME ACCEPTED BY I AFFILIATION 1 DATE'. TIME SAMPLE CONDITIONS 012 to ! t 1 SAMPLER NAME AND'SIGTIATURE - v oG ORIGINAL PRINT Name of SAMPLER: �r�=�.** � l[, µ «C'� SIGNATURE of SAMPLER: "%� / f DATE Signed c^r / _ " U �, E d+ ,,�.G._ �..`—.�.�—' (MMt0DIYY): /i�I rn 'Impon:mt 34oie: Ey aigrrinQ th*J form yw a:o accepline Pam S MET 30 day payment fwrrs and agreaarg to gala c"rges of 9'.5%per month For any inroiws not wAhin 30 days. ! ` F-ALL-0-020rev.07. 15•May-2007 w 0 w 3 m D v K m t N 's n L 3 4 o � b N e. v K ? n � n � .n b r O 7 ft N ^ z r m � a m W M a9 � n � c c b V a �p � VI D 3 c b o- a v f1 m CL M e e n 0 Itemtl BP4U-125 mL PtastiC UnpreserVPd jN/Aj (Cl-) BP3U-250 mL Plastic Unpreserved (N/A) BP2U"DO mL Plastic Unpresefved (N/A) BP1U-1 liter Plastic Uapreserved (N/A) BP4S-125 mL Plash[ H2504 (pH < 2) In-) 5O mL plastic HNO3 )pH c 2) mL Plastic ZN Acetate & NaOH (>9) MZOPU-1,25 S ml Plastic NaOH (pH a 12) JO-) Wide -mouthed Glass jar Unpresened AG1U-1 Ioter Amber Unprese nred (N/A) ICI-) ZZAGiH-1 liter Amber HCI (pH < 2) AGIIU-250mLAmber Vnpres euJN[A)(Cl•) AG15-1 liter Amber HZSO4 (pH < 2) AG3S-250 mL Amber k2S44 (pH < 2) AG3A(DG3A)-250 mL Amber NH4Ct (N/A)(a) DG9H-40 mt VOA HC4 (N/A) VG9T.40 mL VDA Na2S203 (N/A) VOU-40 mL VDA Unp IN/A) OG9P.40 mL VOA H3PO4 (N/A) VOAK 16 via is par kit)-5035 kit (N/A) rr� V/GK (3 vials per kit)-VPH/Ga5 kit (N/A) i SPST-125 mL SLerile Plastic (N/A - lab) SP2i-M mi. Sterile Plastic (N/A - lab) F BP3A-2S0 mL Plastic (NH2)2504 (9,3.9.7) ! Cubitainer ! MU-10mUdintillationvials (N/A) 1. GN r 10 N 0 0 C O � S O m, 3 0 Cu3 tT 'O a � in 0 n :S- m n W a -s x a 't3 S tv a C- O k T Y tu CL 0 0. m n s O 3 m w 0 3 *- 1VATERS EDGE: ENVIRONMENTAL, LLC 4901 WATERS EDGE DRIVE, SUITE 201 • RALEIGH, NC 27606 • PHONE 919.859.9987 • FAX 919.859.9930 April 21, 2017 Mr. Joe Edwards, EHS Officer Matcor Metal Fabrication 835 Salem Road Welcome, North Carolina 27374 PCP_IVIr"S'❑ APR 2 6 2017 CENTRAL FILES DWR SECTION Reference: Stormwater Discharge Outfall Qualitative Monitoring Report and Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication- Year 5- Period I - January -June 2017 Welcome, North Carolina Waters Edge Job No R 1 l -47 n1 C U 0 3 O to /_3 Dear Mr. Edwards: Waters Edge Environmental, LLC (Waters Edge) is pleased to provide two copies of the Year 5- Period 1- January -June 2017 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome, North Carolina (see Figures 1 and 2). We have completed the Discharge Outfall Qualitative Monitoring Report. Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A). Laboratory analytical results are documented in Appendix B. Based on these results, we have exceedances for the following: • Outfal1001 1. Exceedance for copper which was detected at 0.0 12 1 mg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0.659 mg/L versus a benchmark at 0.067 mg/L. • Outfall002 1. Exceedance for zinc which was detected at 0.819 mg/L versus a benchmark at 0.067 mg/L. Based on the permit conditions, we will conduct a Tier 1 inspection of the facility. Any action items which will be reviewed and potential deficiencies addressed. The Tier 1 response will be recorded in the Stormwater Pollution Prevention Plan. Again, as detailed in earlier reports, due to the lowered benchmark thresholds resulting in benchmark exceedances; we previously sampled an upgradient surface water stream on the site (upgradient Lake Drive) as well as two samples collected from the roof drains. While there were no exceedances for copper, both roof drain samples exceeded the zinc benchmark level at 0.067 mg/L (Roof- I at 1.9 mg/L, and Roof-2 at 0.23 mg/L). The background upgradient surface water samples were below both the copper and zinc benchmarks. Based on these results, we would conclude the following: Stormwater Discharge Monitoring Report and Tier 1 Response Year 5- Period 1- January -June 2017 Matcor Metal Fabrication Welcome, NC Page 2 of 2 April21, 2017 • Metals are present in the upgradient surface water sample at the facility. Even though they are below the copper and zinc benchmarks, these metals are still present and can potentially be a constituting factor to the outfall values detected. • Zinc contained in the building materials or downspouts are also contributing to the zinc in the stormwater which would have nothing to do with the industrial activity at the site. While we will continue to attempt to improve the stormwater quality at the facility, we believe that these type of metals exceedances are largely due to non -industrial sources and can be found in a wide variety of non -industrial settings (e.g. residential or any structures with metal components). Waters Edge appreciates this opportunity to work with Matcor Metal Fabrication. If you have any questions or require any additional information, please contact me at 919.859.9987 or at prahn@ watersedgeenv.com. Sincerely, WATERS EDGE ENVIRONMENTAL, LLC Phillip L. Rahn President CC; NCDEQ Stormwater (two copies) 17-027PLR/aht dv j ?p Ix. IL w e tpo,. a 11 %1A u 4L ..13 -- . �A . 'I— I u Z % , A SITE '4 rh 40 N FY d 411 a' 'd J; 1% 1 JP r I Alt Job VO. Topo Quad Date 77de 1'roject Location Map 'ATE R S EDGE ENVIRONMENTAL, LLC R1 1-47 welcome 1.19.2012 File Name Figure Scale Project Matcor SPIT RI 1-47.xls I mknown Welcomo. North Carolina ? Ax, "i .6 m _AL5.3 L; I La- .0 -A . . Cat Y t71n ? 77 n .4 cc atch- Basin Cc, wv k, X- w WI JIL T I.: Yli 0 V how %",ff A 15N t n7 t 7. Tv� Ik 14. T.,,, V F -.V 4 A Y Job No, linage/Photo Dare Title Site & Surrounding Properties Map ENVIRONMENTAL, LLC R 11-47 Davidson Co. GIS 10.27.2011 rile Name Figure Scale Project Matcor SPPII RI 1147..x1s 2 unknown Welcome, North Carolina Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 4.21.17 CERTIFICATE OF COVERAGE NO. NCG030613 FACILITY NAME _Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace` Lab Cert. # `37706_ Comments on sample collection or analysis: None Part A. Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2016 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly' '"month) DISCHARGING TO CLASS ®ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow []Water Supply []SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period?' Outfall No. Date Sample Collected'" (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organicss Benchmarks __> - 100 mg/L or 50 mg/0 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/I. 1 mg/L 001 3/28/17 0.22 5.7 6.3 0.0121 ND 0.655 NA NA 002 3/28/17 0.22 5.3 6.8 0.0057 ND 0.819 NA NA ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. ` For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here, 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ' See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor . manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the 5tormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those Facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (70), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the 5tormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the 5tormwater Pollution Prevention Plan." Name (Print name) - eF11 a ((1: t0 U r_ Title (Print title) 7 ,f ,iatiure) (Date) Note: Results must be reported in numerical format, Do'not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc, in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No dischorge this period. z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non=polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids PH Benchmarks 15 mg/L 100 mg/L or SO mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/201. Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text, FOR PART A AND PART B MONITORING RESULTS: c A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT DART II SECTION B. 0 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALI. TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. 0 T11 R 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports,, within 30 da s of receipt of the lab results Lor at end of monitoring eriod in the case of "No Discharge" reports to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false informationjncluding the possibility of fines and imprisonment for knowing violations." (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://h2o.enr.state.nc.us/su/Forms_ Doe uments.htm#miscforms Permit No.: I N I C I GI 0 1 3 1 0 10 10 0 or Certificate of Coverage No.: I N 1 C I G 10 3 10 16 1 1 13 j Facility Name: Matcor Metal Fabrication County: Davidson Inspector: Thomas Date of Inspection: Time of Inspection: maynes 11.29.16 13:10 Total Event Precipitation (inches): 0.16 Phone No. 336.731.5742 Was this a Representative Storm Event? (See information below) ® Yes ❑ No Please check your permit to verift if Qualitative Monitoring must be performed during a representative storm event (requirements vm}). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, 1 certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) l Outfall Description: Outfall No. 001/002 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Unnamed Tributary of Swearing Creek Describe the industrial activities that occur within the outfall drainage area: Metal Fabrication 2 Color: Describe the color of the discharge using basic colors (red, brown. blue, etc.) and tint (light, medium, dark) as descriptors: Lioht brown Page I of 2 S W U-242-1 12608 3 Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: O 2 3 4 5 5 Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with gloating solids: 3 4 5 6 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 3 4 5 7 Is there any foam in the stormwater discharge? Yes No 8 Is there an oil sheen in the stormwater discharge? Yes No 9 Is there evidence of erosion or deposition at the outfall? Yes No 10 Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-1 12608 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 12.8.16 CERTIFICATE OF COVERAGE NO. NCG030613 FACILITY NAME _Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace^ Lab Cert. #—37706_ Comments on sample collection or analysis: None Part A: 5tormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2016 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' I onth) DISCHARGING TO CLASS ®ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply []SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfail No. Date Sample Collected' (mo/dd/yr) ' 24-haur rainfall amount, a Inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics$ Benchmarks - 100 mg/L or 50 mg/0 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 11/29.16 0.16 70.3 7.2 1 0.0472 0.0078 D.622 NA NA 002 11/29/16 0.16 27.8 6.9 0.0104 ND 0.545 NA NA ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. S Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture- use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1of3 Facilities that incorporate a solvent management plan into the 5tormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTQ monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (70), 1 certify that to the best of my knowledge and belief, no clumping of concentrated toxic organics into the stormwater or'areas which are exposed to rainfall or 5tormwater runoff has occurred since filing the last discharge monitoring report. i further certify that this facility is implementing the all the provisions of the solvent management plan included in the 5tormwater Pollution Prevention Plan." Name (Print name) / Title (Print title) (,5ignature) (Date) Note_ Results must be resorted in numerical format. Do not report Below Detection Limit, BDL, <PQL, felon -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<X,X mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this perlod?2 Dutfall No.' Sample Collected' Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total'5uspended'Solids pH Benchmarks===> _ - 15 mg/L 100 rn %/Uor 50 mg/L* 6.0-9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note.- if you report a sample value in excess of the benchmark, you must implement -Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: a A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART R SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO D IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699.1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ✓"'"- ature of Perrnittee) Permit Date: 11/1/2012-10/31/2017 /-�?— 1 2 r l(., (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 aceAnalytical �mwpacelabs.com December 08, 2016 Mr. Phil Rahn Waters Edge Environmental 4901 Water's Edge Drive Suite 201 Raleigh, NC 27606 RE: Project: Matcor R11-47 Pace Project No.: 92321164 Dear Mr. Rahn: Pace Analytical Services, LLC 2p5 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on November 29, 2016, The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Clayton McCrickard cayton, mccrickard@pacelabs.com Project Manager Enclosures TNI. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page i of 13 Pace Analytical Services, LLC ® 205 East Meadow Road - Suite A aeeAnalytical Eden, NC 27288 www.pacelabs-oom Jr (336)623-8921 1 CERTIFICAT#ONS Project: Matcor R11-47 Pace Project No.: 92321164 Asheville Certification IDs 2225 Riverside Drive, Asheville, NO 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A. Eden, NO 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification * 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 UirginiaNFLAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnalytical>9 VMw.pacelabs.own 1 PaceAna"cal Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 SAMPLE SUMMARY Project: Matcor R11.47 Pace Project No.: 92321164 Lab 10 Sample 10 Matrix Date Collected Date Received 92321164001 Outfall001 Water 1112911611:00 1112911616:35 92321164002 Outfall002 Water 1112911611:30 11/2911616:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written Consent of Pace Analytical Services, LLC. Page 3 of 13 MAnalyticaf 3' wwwpacelabs.o= SAMPLE ANALYTE COUNT Project: Matcor R11-47 Pace Project No.: 92321164 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-a921 Lab ID Sample Ill Method Analysts Analytels Reported Laboratory 92321164001 Outfall 001 SM 2540D DWJ 1 PASI-E EPA 9040 DWJ 1 PASI-E EPA200.7 SH1 3 PASI-A 92321164002 Outfall 002 SM 2540D DWJ 1 PASI-E EPA 9040 DWJ 1 PASI-E EPA200.7 SH1 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 or 13 Pace Analytical Services, LLC ® 205 East Meadow Road - Suite A eAnalytical Eden. NC 27288 ac www.Pscelabs.com (336)623-8921 ANALYTICAL RESULTS Project: Matcor R11-47 Pace Project No.: 92321164 Sample: Outfall 001 Parameters Lab ID: 92321164001 Collected: Report Results Units Limit 11/29/16 11:00 MDL ❑F Received: 11/29/16 16:35 Matrix: Water Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 70.3 mg/L 7,1 7.1 1 11/30116 10:07 9040 pH Analytical Method: EPA 9040 pH 7.2 Sid. Units 0.10 0.10 1 11/30/16 09;45 H6 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Melhod: EPA 2001 Copper 47.2 ug1L 5.0 2.5 1 12102/16 22:40 12/06116 03:17 7440-50-8 Lead 7.8 uglL 5.0 2.5 1 12102/16 22:40 12/06/16 18:36 7439-92-1 Zinc 622 ug1L 10.0 2.5 1 12102/16 22:40 121M16 18:36 7440-66-6 Sample: Outfall 002 Parameters Lab ID: 92321164002 Collected: Report Results Units Limit 11/29/16 11:30 MDL DF Received: 11/29116 16:35 Matrix: Water Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 27.8 mglL 5.0 5.0 1 11/30/16 10:07 9040 pH Analytical Method: EPA 9040 pH 6.9 Sid. Units 0.10 0.10 1 11/30/16 09:45 H6 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 10.4 uglL 5.0 2.5 1 12102/16 22:40 12/06116 03:20 7440-50-8 Lead ND ug1L 5.0 2.5 1 12/02116 22A0 12/06/16 18:39 7439-92-1 Zinc 545 ug1L 10.0 2.5 1 12/02/16 22:40 12/06/16 1839 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2016 12:53 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 �;a'ceAnalytical' WW..pacsfatr3.cam 1 QUALITY CONTROL DATA Project: Matcor R11-47 Pace Project No.: 92321164 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden. NC 27288 (336)623-8921 QC Batch: 338724 Analysis Method, SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92321164001, 92321164002 METHOD BLANK: 1878077 Matrix: Water Associated Lab Samples: 9232t164001, 92321164002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 2.5 11/30/16 09:58 LABORATORY CONTROL SAMPLE: 1878078 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 248 99 90-110 SAMPLE DUPLICATE: 1878079 92321066001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mglL 52.0 87.0 50 5 D6 SAMPLE DUPLICATE: 1878080 92321144002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg1L 77.3 58.3 28 5 _D6 Results presented an this page are in the units indicated by the "Volts" column except where an alternate unit Is presented to the right or the result REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 12/08/2016 12:53 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalytica! www.pacelab3.com QUALITY CONTROL DATA Project: Matcor R11-47 Pace Project No.: 92321164 QC Batch: 338721 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN Associated Lab Samples: 92321164001, 92321164002 SAMPLE DUPLICATE: 1878047 92321007001 Dup Parameter Units Result Result RPD pH Std. Units 6.2 6.2 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Max RPD Qualifiers 9 H1,H6 N Results presented on this page are in the units Indicated by the " Units' column except where an allemate unit Is presented to the right of the resuk. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2016 12:63 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 a acmnalytical j wwwpacelads.com 1 QUALITY CONTROL DATA Project: Matcor R11-47 Pace Project No.: 92321164 QC Batch: 339077 Analysis Method: EPA 200.7 QC Batch Method: EPA200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92321164001, 92321164002 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 METHOD BLANK: 1880248 Matrix: Water Associated Lab Samples: 92321164001, 92321164002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Copper ug/L ND 5.0 2.5 12l06l16 01:45 Lead ug1L ND 5.0 2.5 12106/1617:12 Zinc ug/L ND 10.0 2.5 12106/1617:12 LABORATORY CONTROL SAMPLE: 1880249 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper ug1L 500 490 98 85-115 Lead ug1L 500 507 101 85-115 Zinc ug1L 500 513 103 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1880250 1880251 MS MSD 92321569008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual Copper uglL ND 500 500 491 494 98 99 70-130 0 20 Lead uglL ND 500 500 507 505 101 101 70-130 0 20 Zinc uglL 14.2 500 500 492 494 96 96 70-130 0 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1880252 1880253 MS MSD 92321092003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Cone, Result Result % Rec % Rec Limits RPD RPD Qual Copper ugJL 63.8 500 500 562 551 100 97 70-130 2 20 Lead ugJL ND 500 500 468 464 93 92 70-130 1 20 Zinc uglL 46.4 500 500 565 558 104 102 70-130 1 20 Results presented on this page are in the units Indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2016 12:53 PM without the written consent of Pace Analytical Services, LLC. Page8o(13 55'ce Analytical I rre+xpecelapa.c+Om I QUALIFIERS Project: MalcorR11-47 Pace Project No.: 92321164 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, LLC 205 bast Meadow Road - Suite A Eden, NC 27288 (336)623-8921 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration, Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate via] preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Aerylonitrile by EPA Method 8260, N-Nitrosodiphenyiamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of awediled analytes. TN - The NE1AC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. ❑ate: 12I0612016 12:53 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 wnw.pace&b3.abrn QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Matcor Rit-47 Pace Project No.: 92321164 Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden. NC 27288 (336)623-8921 Lab ID Sample ID GC Batch Method QC Batch Analytical Method 92321164001 Outfall 001 SM 2540D 338724 92321164002 Outfall 002 SM 2540D 338724 92321164001 Outfall 001 EPA 9040 338721 92321164002 Outfall 002 EPA 9040 338721 92321164001 Outfall 001 EPA 200.7 339077 EPA 200.7 92321164002 Outfall 002 EPA 200.7 339077 EPA 200.7 Date, 12/08/2016 12:53 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 339243 339243 Page 10 of 13 Doctrinent Name: - : Document Revised: Sept. 21, 2016 . o aCBAnal<jdwl Sample condition a oa lieceipt(SCUR). Pace 1 of 2 ootirmentNo:r hiu16gA6thority: ' F•CAR-M03346:01.- Pace Quality Office laboratory receiving samples: : - Ashei ille [Q Edeno greenwood ❑ Huntersville El Raleigh❑ Mechaniesviili E] M. CIl nt Name: �/ rp Projt WO# • 92321164 Courier: ❑Fed Ex ❑UPS USPS ❑Cilent ❑ Commercial ❑Pace ❑other: I t I1 !I I 92321164 CustodySea€-Present? ❑Yes.... []No ..Seals intact? ..- .❑Yes ' ❑No -. - •• L_• • • ': DateJfnit a' fs Person EKamining Contents r , PatkfngMateriat: ❑Subbte Wrap" ❑Bubble Bags ']None . . Qother. Ui aIJ iherntomater: ; fR Gun ID: Type of i e; • -• ❑wet ❑Blue : ❑Nane ❑Samples on lce; cooling process has begun Correction Factor: Cooler Temp Corrected('CG - L Blulogical Tissue frozen? []Yes .: []No ❑NIA Temp shuld be.above freezing t o 6'G USDA Regulated Soil NIA, water sample} Did samples originate In a quarantine zone wvhhln the United $tates: Cll, NY, orSC (check maps}? .old samples originate from a foreign source {fntemalfanalty, ny,?i nw. IntImUne naivali and Qve� A nlrnl? t'0. ' nNa - Comments/Dlscfepancy: Chain of Custody Present? y s ❑No- .❑N/A' 1..' Sam lesArrivedwithinHoldTime? Yes ONo ❑N/A 2. - 5hod Hv1d Tlmo Analysis {a7Z hr.)? Yes Vr6 ❑N A' 3, Rush Turn Around Time Requested? QYes f2ho. ❑0/A 4. SufficfentVolume? es ❑No ❑NIA 5. ' Correc# Contain ers Used? -Pace tontalners Used? Q es yes . pr o .' ❑No : [3N/A, 01& 6.' Containers intact? es ❑No , ❑NIA 7, .Samples Field Filtered? - ❑Yes .'❑No -` f IA. 8. Note lfsedirilentIsvisible Inthe dissolved conialner Sample Labels match COC? -Includes Datefrime/11DIAnafy9s Matrix: yes .prto : bN/a 9.= _ Heads ace in VOA Vials (>5-6mm)? Yes ❑No . !A. 10: Trip BlankPresent? 'Trip Blank Custody seals Present? ❑Yes jYe3 .:❑I�o ❑No JA ®N/A 11.. Project Manager SCURF Revle}v: \�`� 11 Date: 11 l Project Manager SRF Review: 1 Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy ofth€s form hill to sent to the North Carolina DERNR Certification Offptog.11 of 13 Out of hold, incorrect preservative, out of temp, incorrect containers} zzOP413-125 mL Plastic Unpreserved (N/A) (CF-) SP3tS-750 mL Plastic Unpremerved (N/A) EP2U-500 mL Plastic Unpreseived (N/A) _BPIU-1 l'iW Plastic Unpresurved (NIA) BP4s-zSO mL Plastic H2SO4 (pH < 2) (CI-) OPM-2S0 mL pl**C, NNOi.(pH < 2) BP3C-2SOmLplastic NaOH (pH >.Iz)'(CI-) WGFU-WidL-.m=hnd GlaStjar L�nproserved Ar.1U-1 1faer Arnber UnpreServed (NIA) (CI-) zz z z AGIN-1 fiteiAMber KCI (pH < Z AG3U-2SOMLAmber Unprase!*rved(.IJ/A),(CI-) AGi,S-I liter Amber H2SO4 (pH A M 6 -2SO ml. , Amber H2SO4 (pN < 2) 462A(Dr.3A)-2SO rnLAmber NH4CI (.H/A)(CIk) oG9H-40mL voA Ho (11/A) VGOIT-40 mL VOA Na2S203 (N/A) VG . 9U-40MLVOAUnp(NIA) C'" D(i9P-40.LVOA HSP04-(N/A) VOAK(&v-Lats.per kit)-503$kit .(i4/A) VIGK (S via>< $;IPST.j>S-M.LStei',le Plastic (N?A —tab) SM-250 mL Sterile PListio - (?�/A — tab) ttt SP3A250 mL Pta..-:z (NK2P504 (9Z-9.7} -20 ML scinti �VSGU thation vWs; (WA) / �PaceAnalytical unw_eaerlaez_eem CHAIN -OF -CUSTODY 1 Analytical Request Document The Chainof-Cus" is a LEGAL DOCUMENT. All relevant fieFCs must be completed accvratety. Paga: 1 of / Section A Section 8 Section C Required Client Information: Required Project Information: Invoice Information: To: Attention: lVl 3 Company; Report f' r : S � ,Y .�! A /,4: �J L, Addresa. Copy To- C=paM:,ame. REGULATORY AGENCY Address! i NPDES I— GROUND WATER I DRINKING WATER i UST RCRA Q7i-!ER Emas Tv: / %J. Purchase Order No,: �I Pa:.c Owte f� Phone: Fax: Project Nama: Pax Prolsa Site Location 14A% [L� Nart3ger: STATE: Requested Duo DaWTAT: Project Number Face Prot* Requested Analysis Filtered (Y)N) Section D Matrix Codes _ y z RegalrodCkeM lnArm•Mion vxTRlx r CODE COLLECTED Preservatives 5. ±Drinking Water DW H O Wntor WT waste Water WW 3t tl U Cel+!POSiTE coN�aoSltB w WJ PToduet P - m START ENprGRpe Sosysofrd SL � � SAMPLE I® wipo wP w " U " (A-Z. ll-5 l : Alr AIR to W 0. z a h � � o Sample tDs MUST BE UNIQUE Tissue TS p � w r Z CDy i' U [)tiler Or V x !- w O O C c -N 71 J '0 .' ~ ORTE�� TIME PATE TSME V) r MPace Project No.! Lab I.D. A 5 r 7 8 9 11 I I 12 ADDITIONAL COMMENTS RELINOUFSHED BY / AFFILIATION DATE TIME ACCEPTED BY ! AFFILIATION DATE TIME SAMPLE CON ITIONS V SAMPLER NAME AND SIGNATURE 6l U r (D PRINT Name of SAMPLER: ry„rls �+.�L 'n ? i✓ ° ti z a v-' ...+•7 DATE Signed SIGNATURE of SAMPLER: /� = m E 0 IMrQDDrYrj: '&*onant Nc:o: By sign.ng tlYr. form you are acceaung Paces NET 30 day payment lerms]M agrecing to late snarycs Or 1.5%per a:a TN Tar wy invO.c.� 30 days. � / F-ALL-0-020rev.07. 15-May-2007 From: ncblg@bellsouth.net Sent: Wednesday, April 19, 2017 11:04 AM To: prahn@watersedgeenv.com Subject: Individual Renewal Thank you for your renewal. Your transaction has been processed. Please keep this email for your records. Online Transaction Number: 01346D Amount Paid: $85 Name: Rahn, Phillip License No: 0386 if you have any questions or concerns, please contact our office at: Tel: 919-850-9669 --- --- ------------- Thank you, NC Board for Licensing of Geologists 3733 Benson Drive Raleigh,.NC-27609 P.O. Box 41225 Raleigh, NC 27629 From: ncblg@hellsouth.net Sent: Wednesday, April 19, 2017 11:02 AM To: prahn@watersedgeenv.com Subject: Corporate Renewal Thank you for your renewal. Your transaction has been processed. Please keep this email for your records. Online Transaction Number: 56073D Amount Paid: $25 Name:, License No: C-311 If you have any questions or concerns, please contact our office at: Tel: 919.850-9669 Thank you, NC Board for Licensing of Geologists 3733 Benson Drive -------------- Raleigh,-NC.276�9 P.O. Box 41225 Raleigh, NC 27629 Semi-annual Stormwater Discharge Monitoring Report (DPY for North Carolina Division of Water Quality General Permit No. NCG03000w Date submitted 12.8.16 0 CERTIFICATE OF COVERAGE NO NCG�613- FACILITY NAME _Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace, Lab Cert. # 37706_ Comments on sample collection or analysis: None Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2016 SAMPLE PERIOD C] Jan -June ® July -Dec p �+ 1 or ❑ Monthly' _ (month) RECE IME&LING TO CLASS [DORW ❑HQW QTrout ❑PNA DEC 18 Lllio ❑Zero -flow ❑watersupply ❑SA ❑Other CENTRAL FILES ,,PLEASE REMEMBER TO SIGN ON PAGES-2 AND/,OR 3 DWR SECTION ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pli, Standard units Copper I Lead Zinc Non -Polar O&G/ Total Petroleum . Hydrocarbons Total Taxis Organ& Benchmarks : = > - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.00-1 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 11/29.16 0.16 70.3 7.2 0.0472 0.0078 0.622 NA NA 002 11/29/16 016 27.8 6.9 0.0104 ND 0.545 NA NA x Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. `See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-1o/31/2017 f, SWU.245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic arganic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the T O monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (70), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report I further certify that this facility is implementing the all the provisions of the solvent management plan included in the 5tormwrater Pollution Prevention Plan." Name (Print name) / Title (Print title) -;2--its (�ignature) (Date). Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, NO, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L",where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period: Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar 08G/TPH by EPA 1664 (56T•HEM) Total Suspended Solids pH 8enchmorb 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU footnotes from Part A also apply to this Part B ` See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: il/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 2, Tier Z or Tier 3 responses. See General Permit text. FOR PART _A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS_ SEE PERMIT PART II SECTION 8, • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reeorts,within 30 days of receipt of the lob results jot at end of monitoring period In the case o "No Discharge' reportsl to: Division of Water Quality Attn. DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST•SIGN TH15 CbMFICATION•FOR ANY. INFORMATION REPORTED:. "I certify, under penalty of law, that this document and ali attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. t am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permitteej Permit Date: 11/1/2012-10/31/2017 (bate): SWU-245, last revised 10/25/2012 Page 3 of 3 RECEIVED Stormwater Discharge Outfall (SDO) DEC 16 Nib Qualitative Monitoring Report EN SECTION Forguidance on filling out this form, please visit: httL)://h2o.onr,stnte.nc; us/su/t orrns_Documcnts.hjM#lUjjscfonns Permit No.: I N 1 C 1 G 01310 10{ 0 It 0 i or Certificate of Coverage No.: I N i C I G10 13 10 1 6- 1 1_ 1 3 Facility Name: Matcor Metal Fabrication County: Davidson Inspector: Thomas Haynes Date of Inspection: 11.29.16 Time of Inspection: 13:10 Total Event Precipitation (inches): 0.16 Phone No, 336.731.5742 Was this a Representative Storm Event? (See information below) ® Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has. 1 occurred. A sinpJe storm event may contain unto 10 consecutive hours of no precipitation. I By this signature, I certify that this report is accurate and complete to the best of my knowledge: -��.� z Z (Signature of Permince or Designee) 1 Outfall Description: Outfall No. 001 /002 Structure (pipe, ditch, etc.) Pi Receiving Stream: Unnamed Tributary of Swearing Creek Describe the industrial activities that occur within the outfall drainage area: Metal Fabrication 2 Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: _Light brown Page I of 2 SWU-242-112608 3 Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc). - No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: (D 2 3 4 5 5 Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 3 4 5 6 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 O 3 4 5 7 Is there any foam in the stormwater discharge? Yes No 8 Is there an oil sheen in the stormwater discharge? Yes No 9 Is there evidence of erosion or deposition at the outfall? Yes No 10 Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 FaceAnalyfical ww�rpxekxCsoam December 08, 2016 RECEIVED DEC 16 2016 Mr. Phil Rahn Waters Edge Environmental 4901 Water's Edge Drive Suite 201 Raleigh, NC 27606 CENTRAL FILES DWR SECTION RE: Project: Matcor Rll-47 Pace Project No.: 92321164 Dear Mr. Rahn: Pace Anaytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on November 29, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel Free to contact me. Sincerely, Clayton McCrickard clayton.mccdckard@pacelabs.com Project Manager Enclosures , 01 T� C'4eQRA��` REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 1 of 13 1-- .Pj/ceAnalytical www.pae sLcan r Project: Matcor R1147 Pace Project No.: 92321164 Pace Analytical Services. LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 Eden Certification Ids 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 UrginiaNELAP Certification #: 460222 North Carolina Wastewater Certification 0: 633 VrginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 2 of 13 `FaceAnaV cal WWW4kX Wb&Cam ) Pace Analytical Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 SAMPLE SUMMARY Project: Matcor R11-47 Pace Project No.: 92321164 Lab ID Sample ID Matrix Date Collected Date Received 92321164001 92321164002 Outfall001 Outfall002 Water Water 1112911611:00 11/2911611:30 11/2911616:35 1112911616:35 REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 -._,,Pace Analytical' wmrpanei�scarn I SAMPLE ANALYTE COUNT Project: Matcor R11-47 Pace Project No.: 92321164 Pace ArtA tkal Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92321164001 Outfall 001 SM 2540D DWJ 1 PASI-E EPA9040 DWJ 1 PASI-E EPA200.7 SH1 3 PASI-A 92321164002 Clutfall 002 SM 2540D DWJ 1 PASI-E EPA9040 DWJ 1 PASI-E EPA200,7 SH1 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Servkxs, LLC. Page 4 of 13 1FiceAnalytdcal www.ptxa+ uC= I ANALYTICAL RESULTS Project: Matcor R11-47 Pace Project No.: 92321164 Pace AnaNikal Servkas. LLC 205 East Meadow Road - Suite Eden, NC 27288 (336)523.8921 Sample: Outfall 001 Parameters Lab ID: 92321164001 Collected: Report Results Units Limit 11129/16 11:00 MDL OF Received: 11/29/16 16:35 Matrix: Water Prepared Analyzed CAS No. Qual 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 70.3 mg1L 7.1 7.1 1 11/30/16 10:07 9040 pH Analytical Method: EPA9040 PH 7.2 Std. Units 0.10 0.10 1 11/30/16 09:45 H6 200.7 METICP Analytical Method: EPA200.7 Preparation Method: EPA200.7 Copper 47.2 ug1L 5.0 2.5 1 12/02/16 22:40 12/06/16 03:17 7440-50-8 Lead 7.8 ug1L 5.0 2.5 1 12/02/16 22:40 12/06/16 18:36 7439-92-1 Zinc 622 ug1L 10.0 2.5 1 12/02/16 22:40 12/06/16 18:36 7440-6" Sample: Outfall 002 Lab tD: 92321164002 Collected: 11/29/16 11:30 Received: 11/29/16 16:35 Matrix: Water Report Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 27.8 mg/L 5.0 5.0 1 11/30/16 10:07 9040 pH Analytical Method: EPA 9040 PH 6.9 Std. Units 0.10 0.10 1 11/30116 09:45 H6 200.7 MET ICP Analytical Method: EPA 2007 Preparation Method: EPA 200.7 Copper 10.4 ug1L 5.0 2.5 1 12/02116 22:40 12106/16 03:20 7440-50-8 Lead NO ug1L 5.0 2.5 1 12/02116 22:40 12/06/16 18:39 7439-92-1 Zinc 545 ug1L 10.0 2.5 1 12/02116 22:40 12/06/16 18:39 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 12/08/2016 12:53 PM without the written consent of Pace Analytical Services, LLC, Page 5 of 13 �FaceAnalical www.paoolabsoom Pace A-Vical Services. LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-W21 QUALITY CONTROL DATA Project: Matcor R1147 Pace Project No,: 92321164 QC Batch: 338724 Analysis Method: SM 25400 OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92321164001.92321164002 METHOD BLANK: 1878077 Matrix: Water Associated Lab Samples: 92321164001,92321164002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 2.5 11W116 09:58 LABORATORY CONTROL SAMPLE: 1878076 Spike LCS LCS % Roe Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 248 99 90-110 SAMPLE DUPLICATE: 1878079 9232106e001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mglL 52.0 87.0 50 5 D6 SAMPLE DUPLICATE: 1878080 92321144002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg1L 77.3 58.3 28 5 D6 It"uRs presented on tide page am to the units Mdicsted by the "Units" column except when an aRemate unit is presented to the right dine tesulL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 12108/2016 12:53 PM without the written consent of pace Analytical Services, LLC. Page 6 of 13 �Fice Analytica! I QUALITY CONTROL DATA Pace AmNtkal Services, LLC 205 East Meadow Road - Suite A Eden. NC 27268 (336)6234Wl Project: Matcor R11-47 Pace Project No.: 92321164 OC Batch: 338721 Analysis Method: EPA9040 QC Batch Methad: EPA9040 Analysis Description: 9040 pH EDEN Associated Lab Samples: 923211 W01, 92321164002 SAMPLE DUPLICATE: 187BD47 92321007001 Dup Max Parameter Units Result Result RPD RPD Qualifiers PH Std. Units 6-2 6.2 0 9 H1,1-16 Results presented on this page are In the units Indicated by the "Units" Column CKcept where an alternate unit Is prrssrded to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall net he reproduced, except in fut[. Date: 12108l2016 12:53 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 �FaceAnalytical wwwp ,xbb&=n 1 QUALITY CONTROL DATA Project: Matcor R11-47 Paco Project No.: 92321164 QC Batch: 339077 Analysis Method: EPA200.7 QC Batch Method: EPA200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92321164001, 92321164002 Pace Analyticat Services, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-a921 METHOD BLANK: 1880248 Matrix: Water Associated Lab Samples: 92321164001. 92321164002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Copper ug1L NO 5.0 2.5 12106t16 01:45 Load ug1L NO 5.0 2.5 1210611617:12 Zinc ug1L ND 10.0 2.5 12/0611617:12 LABORATORY CONTROL SAMPLE: 1680249 Spike LCS LCS % Rec Parameter Units Conc_ Result % Rec Limits Qualifiers Copper ug1L 500 490 98 85-115 Lead ug/L 500 507 101 85-115 Zinc ug/L 500 513 103 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1880250 MS 92321569008 Spike Parameter Units Result Conc. Copper ug1L ND 500 Lead ug1L ND 500 Zinc ug1L 14.2 500 1880251 MSD Spike MS MSD MS MSD % Rec Max Cono. Result Result % Rec % Rec limits RPD RPD Qual 500 491 494 98 99 70-130 0 20 500 507 505 101 101 70-130 0 20 500 492 494 96 96 70-130 0 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1880252 1880253 MS MSD 92321092003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Copper ugiL 63,8 500 500 562 551 100 97 70-130 2 20 Lead ug1L NO 500 500 468 464 93 92 70-130 1 20 Zinc ug1L 46.4 500 500 565 558 104 102 70-130 1 20 Results presented on this page am In the units lndk zed by the "Units" column except whew an altemate unit Is presented to the right of the resulL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2016 12:53 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 I? ` aceAnalytical wara�{�acBlabsmm QUALIFIERS Project: Matoor R11-47 Pace Project No.: 92321164 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data duo to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Anatytteat Servkgs, LLC 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-b921 S - Surrogate 1,2-Diphenyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each anatyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP- Sample Duplicate RPD- Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 ChloroethytOnyl ether. A separate vial preserved to a pH of 4.5 is recommended in SWB46 Chapter 4 for the analysis of Acrolein and Acryionitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenytamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNl accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services - Asheville PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS 06 The precision between the sample and sample duplicate exceeded laboratory control limits. Hi Analysis conducted outside the EPA method holding time. H6 Anatysls Initiated outside of the 15 minute EPA required holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 121=2016 12:53 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 .r:•x...... 'f �, _ t Pace Amytkal Services, LLC Ar�aiyrfCai 0 205 East +Aeadow Road• fe e 2 a47.�P'ac Eden NC 272aa *WW Patst:ctCM I (336)62 M821 QUALITY CONTROL DATA CROSS REFERENCE TABLE Projoct: Matcor R11-47 Paco Pro}ect NO.: 92321164 Analytical L.at? lD Sample 10 QC Batch Method QC Batch Analytical Method Batch 92321164001 Outfall 001 SM 2540D 338724 92321164002 Outfall 002 SM 2540D 338724 92321164001 Outfall 001 EPA 9040 338721 92321164002 Outfall002 EPA9040 338721 92321164001 Outfall 001 EPA200.7 339077 EPA 200,7 339243 923211U002 Outfall002 EPA 200.7 339077 EPA 200,7 339243 Date: 12/08/201612:53 PM REPORT OF LABORATORY ANALYSIS This report: shall not ce reproduced, except in fo. without the written consent of Pace Analytical Services, LLC Page 10 of 13 o ceRnal�trcal Document Name: .• Sample Cohelitlon U tr.N mi (509) . • Document Revised: SepL 21, 2016 _ page 10 2 _ Oasament•fsa:• : f3suingAufhorty: �• F CAR SS 033 Reu.Oi .• Pace Quality 0111ce labnratm receiving samples, = `' Ashe' We El EdenVf Greenwood ❑ muntersville [] Ralt:ighQ MechankWileo . Cll ntlume: , WO : 92321164 - U v� i•L , - Pro c Gautier QFed Ex (]UPS LISPS Client ❑ Commercial QPace [)Outer: ! j j j ii 1 11i 92321164 CustodySeal.Present? []Yes.-,. []No ._Sealsintact? ._..QYes: =.. ONO' ,- OateJtrrltials Person Exarnlntng Contents Cl� Packing Mateital:• 080ble Wrap []BubbleBags _ 3igorie ]Other: Thermometer' • fRGsuEID: QQ� 7ppeoll ; '• OWct :Qaiue: ❑Nave =QSampfesonlce;caDlingproa�ss has begun Correctlon Factor, bm1er7emACarrectcd('CJ,. 81010gicaiTissue,Frozen?_ QYes .: [ i+fo []N/A Temp should bgabove free:ing to 6 C ; USDA Regulated Soil (❑ ft/A,water sample) Old samples originate In a quarantine zone vrithtn the UDtted States: Ck NY or,SC (check neaps)? [tut sairgr[es wlginats fear» a foreign sourto (tnterrratiorraity, es' Mo Induding Hawaii and Puerto Rlcol? QYes ' []NO • -Coinmeats/DtscrBparc : j Chain ofcuit Present? Y Sam TesArrivedwItUn HofdTime? es No ©N A• 2 " ShartHoldTfineAna[ysis <72hr.?r1yei No NA' 3.' Hirsh Turn Around Time Requested? 12ho. ON A 4..' SuHidentVolume? es []No ' QN/A 5.- forrectCantainers6d? -Paco Containers Used? J es .QNo Yes ." No : QNJA- • Q A Containers Intact? es ❑No . ©N/A I. Sam es Fleld Fllteredl QYes . QNv . ' /A . 8 we if sediment Is visible Tn the d(ssolved contaVo ' Sa*e Lanais Ma%h C0C? • 4nrhttfoc[tafn/lfmofrrllerulvck aA�htx Yes . Qhb : 1V t]N/A Heads atelnVOAvlais a5.6mm? es No E3011A. I 10: Trip Blank Present? []Yes ❑tio ly/A: 11,. Tt BlankCtestadySealsPresent? Yei - :QNa I..f.J(N/A CLIENT NOTIFICATION/RESOLUT1017 Field Qato Requtred?- []Yes []No. Person Contacted: Date/Time: . • . Cornments/Sampie ,. - - . Discrepancy: Project Manager SCURFAevievr. �1" 1 / 1 Date; t Project Managet 5RF Revlety: r j Note: Whenever there Is adfwrePhCyet€ectingNorthGrcUnaCompRaacesample-kac6pyofthfsformEvHibesmttotheNorthCarolinaDEHNRCertiftation0%4,4.11 a113 i OtEtafttn4d,fncorrecttuesennttve,oartoftemp taosrrecteantaWersj •. Dacutt�ent Name;: Docgment Rerised: Sept. 21, 2016 - � Satir1719 Cortdltioh l! arr I;et'eipt SCtiR} - - P3 e 2 Off . , ' lc� fj�f�Ca1. Docu ontNo::;'= i3suiiighutiiority: Pace civaty office 9�321164 Check mark top half of box if pH and/or dethlotinatian Prajt; w�* Isvt?rifiedand within the acceptance rangafor'.. Due Date- 12/13/16 preservation samples. Ph: CHtt **Bottom half of box Is to list number of bottles , CLIENT: 95—waters Ed x a z.T2;! ?. z z ti Y N � y Z 0. E E E J E E r E E E' is . M t7 Q Q 7 STD 5 YT 1A 93 • - ei a- 4Mv m : - 1 2 4 5 G 7 6 9 N- �1. 12 pii A.djusttna�Y Cog for Preserved -- - - Samples ' Sample rip eofprmervatin pH uponncelpi Date presetaaiipnicJu ed Time.pmervatlan adjusted AmountofPteservative added Letd D . -Face Arralytica!' x-I�he CHAIN -OF -CUSTODY / Analytical Request Document The C:Main•of-Custody Is a LEGAL DOCUMENT. All relevant f4ld3 must W Completed tocvtelely. Page: S ctlon A Section B Section C Rcquir" C/Lent Mfortnati`Lon: Raqulrod ProoV. Infotmatlan: Invoice Irearma:ion: Compamr./' • RepodTp /. �i', % Attentim % 0 j v 3 72,2) f.',7 .ar /s.•4e! �✓ Addrttss:" - Copy To: CompanyN$ms: REGULATORY AGENCY i AtlCreas: 'i NPDES -', GROUNDWATER i DRINKING WATER UST ..^ RCRA OTHER Ema:l To: �� . / :�, j PuMNM Orw No.: /l- ! r PR a Phorn: Fare Project Noma: � a -Cc P nearegcr: Site Location STATE: . . Rege.essad Due DaRNTAT: Projec! Ntmrber. /°r�- �,-..-� Pacevrouoa. Requested Analysis Filtered (YIN) Scetlon D Matrlx Codes e = RagetrodCtbrt tn:omoaan u�4MA r me o COLLECTED Preservatives } orminp Vvater DW p Z Water vVT Waste Werii VVWr y @ cpWo$:rc VAXT ppllaoa.:a ENN6F/D V z Product P S Soivsoiid SL SAMPLE ID OL W'De WP (A-Z. 04 r ; 3 Air AA a n +y V Sample IN MUST BE UNIQUE Tissuo TS p Z a # Otncr OT X tu �= N Z Z +� DATE TIME DATE TIME" = 216 R Pace Project No.l' Lab I.D. �! !� !7 r r�t. !r • 7 j a r A . S 8 7 6 a to ]t 121 ADDITIONAL COMMENTS REONQUISHEO BY I AFFILIATION OATE TIME ACCEPTED BY l AFFILIATION DATE TIME SAMPLE CON iTIONS /Z' Vt Y� l� r -D SAMPLER NAME AND SIGNATURE f � PRINT Kanto of SAMPLER:y., Y f8g w DATE Signed swoNATURE of SAMPLER: (MDD : 1W 'Irnmrant 3:0•.o: Cy sigring %.. farm you are J%evwv P=IJ NE r 3C aay payr�a-•4le-1 aae agrarirg to Law anrgoa di 1.5%Par march rer any inra.a..z>o d3ya. / / F-ALL-0-020rev.07, 15-May-2047 WA'I'I €2S 1 DG1 tsNVIRONMENTAL, LLC 901 WATERs EDGE DRIVE, Sur<E 201 . RANCH, INC 27606 • PHoNE 919.859.9987. FAx 919.859.9930 December 8, 2016 RECEIVED Mr. Joe Edwards, EHS Officer DEC 6 U16 Matcor Metal Fabrication CENT 835 Salem Road RAL FILE Welcome, North Carolina 27374 DWR SECTS Reference: Stormwater Discharge Outfall Qualitative Monitoring Report and Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication- Year 4- Period 2- July -December 2016 Welcome, North Carolina Waters Edge Job No R11-47 Dear Mr. Edwards: Waters Edge Environmental, LLC (Waters Edge) is pleased to provide two copies of the Year 4- Period 2 (July -December 2015) 2015 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome, North Carolina (see Figures 1 and 2). We have completed the Discharge Outfali Qualitative Monitoring Report. Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A). Laboratory analytical results are documented in Appendix B. Based on these results, we have exceedances for the following: Outfall 001 1. Exceedance for copper which was detected at 0.0472 mg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0.622 mg/L versus a benchmark at 0.067 mg/L. Outfall 002 1. Exceedance for copper which was detected at 0.0104 mg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0.545 mg/L versus a benchmark at 0.067 mg/L. Based on the permit conditions, we will conduct a Tier 1 inspection of the facility. Any action items which will be reviewed and potential deficiencies addressed. The Tier 1. response will be recorded in the Stormwater Pollution Prevention Plan. Again, as detailed in earlier reports, due to the lowered benchmark thresholds resulting in benchmark exceedances, we previously sampled an upgradient surface water stream on the site (upgradient Lake Drive) as well as two samples collected from the roof drains. While there were no exceedances for copper, both roof drain samples exceeded the zinc benchmark level at 0.067 mg/L (Roof-1 at 1.9 mg/L, and Roof-2 at 0.23 mg/L). The background upgradient surface water Stormwater Discharge Monitoring Report and Tier 1 Response Year 4- Period 2- July -December 2016 MatcorMetal Fabrication Welcome, NC Page 2 of 2 December 8, 2016 samples were below both the copper and zinc benchmarks. Based on these results, we would conclude the following: • Metals are present in the upgradient surface water sample at the facility. Even though they are below the copper and zinc benchmarks; these metals are still present and can potentially be a constituting factor to the outfall values detected. • Zinc contained in the building materials or downspouts are also contributing to the zinc in the stormwater which would have nothing to do with the industrial activity at the site. While we will continue to attempt to improve the stormwater quality at the facility, we believe that these type of metals exceedances are largely due to non -industrial sources and can be found in a wide variety of non -industrial settings (e.g. residential or any structures with metal components). Nonetheless, we do understand that this exceedance will result in a Tier 2 response requiring monthly sampling for both Outfalls. Waters Edge appreciates this opportunity to work with Matcor Metal Fabrication. If you have any questions or require any additional information, please contact me at 919.859.9987 or at prahn@watersedgeenv.com. Sincerely, WATERS EDGE ENVIRONMENTAL, LLC -;4.;�� Phillip L. Rahn President CC: NCDENR Stormwater (two copies) 16-089PLR/aht 0, 161.1 dr r � i ! 1; IJ ',sky, y , • ' l l��sin H r� _ A. r ` y. 411 Job No. Image/Photo Date Title Site &Surrounding Properties Map /IrhWKrERS EDGE ENVIRONMENT /V , 1.1 R1147 Davidson Co, GIS 10.27.2411 � File Name Figure Scale project Matcor SPPP RI 147.x1a 2 unknown Welcome, North Carolina NG0306(3 ak�WATERS EDGE ENV1R0NMENTAL. LLC 901 WATERS EDGE DRIVE, SUITE 201 . RALEIGH, NC 27606 • PHONE 919.859.9987 • FAx 919.859.9930 December 23, 2015 Mr. Joe Edwards, EHS Officer Matcor Metal Fabrication 835 Salem Road Welcome, North Carolina 27374 Reference: Stormwater Discharge Outfall Qualitative Monitoring Report and Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication- Year 3- Period 2- July -December 2015 r;DEC72 M Welcome, North Carolina Waters Edge Job No Rl 1-478 2015 Dear Mr. Edwards: Waters Edge Environmental, LLC (Waters Edge) is pleased to provide two copies of the Year`s Period 2 (July -December 2015) 2015 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome, North Carolina (see Figures 1 and 2). We have completed the Discharge Outfall Qualitative Monitoring Report. Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A). Laboratory analytical results are documented in Appendix B. Based on these results, we have exceedances for the following: Outfal1001 l . Exceedance for copper which was detected at 0.0084 mg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0.171 mg/L versus a benchmark. at 0.067 mg/L. Outfall 002 I. Exceedance for zinc which was detected at 0.507 mg/L versus a benchmark at 0.067 mg/L. Based on the permit conditions, we will conduct a Tier 1 inspection of the facility. Any action items which will be reviewed and potential deficiencies addressed. The Tier I response will be recorded in the Stormwater Pollution Prevention Plan. Again, as detailed in earlier reports, due to the lowered benchmark thresholds resulting in benchmark exceedances, we previously sampled an upgradient surface water stream on the site (upgradient Lake Drive) as well as two samples collected from the roof drains. While there were no exceedances for copper, both roof drain samples exceeded the zinc benchmark level at 0.067 mg/L (Roof-1 at 1.9 mg/L, and Roof-2 at 0.23 mg/L). The background upgradient surface water samples were below both the copper and zinc benchmarks. Based on these results, we would conclude the following: Stormu,ater Discharge Monitoring Report and Tier 1 Response Year 3- Period 2- July -December 2015 Marcor Metal Fabrication Welcome, NC Page 2 of 2 December 23, 2015 • Metals are present in the upgradient surface water sample at the facility. Even though they are below the copper and zinc benchmarks, these metals are still present and can potentially be a constituting factor to the outfall values detected. • Zinc contained in the building materials or downspouts are also contributing to the zinc in the stormwater which would have nothing to do with the industrial activity at the site. While we will continue to attempt to improve the stormwater quality at the facility, we believe that these type of metals exceedances are largely due to non -industrial sources and can be found in a wide variety of non -industrial settings (e.g. residential or any structures with metal components). Nonetheless, we do understand that this exceedance will result in a Tier 2 response requiring monthly sampling for both Outfalls. Waters Edge appreciates this opportunity to work with Matcor Metal Fabrication. If you have any questions or require any additional information, please contact me at 919.859.9987 or at prahn a@watersedgeenv.com. Sincerely, WATERS EDGE ENVIRONMENTAL, LLC Phillip L. Rahn President CC: NCDENR Storm,,vater (two copies) 15-099PLR/aht L/ ' • •� i. � ` � r� ((,��'�.�. t 1 * �1 � ley A. 14 J \ rr 1 (C /� ^ - 1� _ • ",.' r'■ + t "' - -1` EL a■ 1 IV job No. Topo Quad Dote Tale WATERS EDGE ENVIRONMENTAL, L.LC RII-47 weleomo 1.19.2012 Project I ocatirn Map OeNanu Figure Scale Project Matcor SPPP Rtl�l7aL 1 unknown Welcome, North Carolina _ IL Al Cate \ -ry � `� 4a c atch Bann , 1 fs ,1 •.11� h � f Job No. 1—ge/Pholo Dare Tale WATERS EDGE ENVIRONMENTAL, LLC RI 147 Davidwo Co. GIS 10.27.201 i Site 6Y Surrounding Properties Map File Name Figure Scale Project Mat=SPpp RI 147.xb 2 unknown Welcome, North Carolina 3(�tj _3j Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit; littl2://h2o.enr,state.ne.us/su/Fornis Documents. htm#miscforms Permit No.: I N I C I G I 0 13 10 I 0 1 0� 0 or Certificate of Coverage No.: I N � C I G 10_ 3 10 1 6 1' 3 I Facility Name: Matcor Metal Fabrication County: Davidson Inspector: Thomas Haynes_ Date of Inspection: 11.19.15 Time of Inspection: 13:30 Total Event Precipitation (inches): 1.1 Phone No. 336.731.5742 Was this a Representative Storm Event? (See information below) ® Yes ❑ No Please check your permit to verb if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A sinele storm event may contain up to 10 consecutive hours of no trecipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) I Outfall Description: Outfall No. 001/002 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Unnamed Tributary of Swearing Creek Describe the industrial activities that occur within the outfall drainage area: Metal Fabrication 2 Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Lioht brown Pagel of 2 S WU-242-1 12608 3 Odor: Describe any distinct odors that the discharge may have (i.e., smeIls strongly of oil, weak chlorine odor, etc.): No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: I O 3 4 5 5 Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 O 3 4 5 6 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: Q 2 3 4 5 7 Is there any foam in the stormwater discharge? Yes No 8 is there an oil sheen in the stormwater discharge? Yes No 9 Is there evidence of erosion or deposition at the outran? Yes Vo 10 Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S WU-242-112608 aceAnalytical. Wwwpaacelabs. = December 04, 2015 Mr. Phil Rahn Waters Edge Environmental 4901 Water's Edge Drive Suite 201 Raleigh, NC 27606 RE: Project: MATCOR R11-47 Pace Project No.: 92277061 Dear Mr. Rahn: Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on November 20, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sam pie analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Brittany Gibson brittany.gibson@pacelabs.c om Project Coordinator Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc._ Page 1 of 12 1�;a'ceAnalj4ical' wKwpacelabs. cam Project: MATCOR R11-47 Pace Project No.: 92277061 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Ashevifie Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Vtrginia[VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 aceAnalXical' wwxcpecefebs.com r SAMPLE SUMMARY Project: MATCOR R11-47 Pace Project Na__ 92277061 Lab ID Sample ID Matrix Date Collected Date Received 92277061001 92277061002 OUTFALL 001 OUTFALL 002 Water Water 11/19/15 11:30 11/19/15 12:00 11/20/15 06:30 11/20/15 W30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 3 of 12 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 55'ceAnalytical' Eden, NC 27268 www.PMlabs 4om (336)623-8921 I SAMPLE ANALYTE COUNT Project: MATCOR Rif-47 Pace Project No.: 92277061 Lab ID Sample ID Method Analysts Analytts Reported Laboratory 92277061001 OUTFALL 001 SM 2540D DWJ 1 PASI-E EPA 9040 DWJ t PASI-E EPA 200.7 CDF 3 PASI-A 92277061002 OUTFALL 002 SM 2540D DWJ 1 PASI-E EPA 9040 DWJ 1 PASI-E EPA 200.7 CDF 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pate Analytical Services, Inc.. Page 4 of 12 1�;WeAnalytical wavw.parrla6s.cam I ANALYTICAL RESULTS Project: MATCOR R11-47 Pace Project No.: 92277061 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Sample: OUTFALL 001 Lab lD: 92277061001 Collected: 11/19115 11:30 Received: 11/20/15 08:30 Matrix; Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids 14.4 mg1L 2.5 2.5 1 11/23/15 14:35 9040 pH Analytical Method: EPA 9040 pH 6.1 Sid. Units 0.10 0.10 1 11/20/15 11:20 H6 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 8A ug/L 5.0 2,5 1 11125/15 19:00 12/03/15 02:44 7440-50-8 Lead ND ug/L 5.0 2,5 1 1112511519:00 12/03/15 02:44 7439-92-1 Zinc - 171 ug/L 10.0 2,5 1 11 /25115 19:00 12103/15 02:44 7440-66-6 Sample: OUTFALL 002 Lab ID: 92277061002 Collected: 11/19/15 12:00 Received: 11/20/15 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 19.3 mg/L 2.5 2.5 1 11/23115 14:36 9040 pH Analytical Method: EPA 9040 pH 6.3 Std. Units 0.10 0.10 1 11/20/15 11:20 H6 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND ug/L 5.0 2.5 1 11/25115 19:00 12/03/16 02:47 7440-50-8 Lead ND ug/L 5.0 2.5 1 11/25115 19:00 12/03/15 02:47 7439-92-1 Zinc 507 ug/L 10.0 2-5 1 11/25115 19:00 12103/15 02:47 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/04/2015 12:37 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 1 aceAnalytical (/ wuw,Asccle4t rnm t QUALITY CONTROL DATA Project: MATCOR Rll-47 Pace Project No.: 92277061 QC Batch: EDEN120856 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description; 2540D Total Suspended Solids Associated Lab Samples: 92277061001, 92277061002 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 METHOD BLANK: 1613266 Matrix: Water Associated Lab Samples: 92277061001, 92277061002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 2.5 11/23/15 1414 LABORATORY CONTROL SAMPLE: 1513267 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 228 91 90-110 Results presented on this page are In the units Indicated by fit "units' column except where an alternate unit Is presented to the right ut the resuil. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/04/2015 12:37 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceAnalyrlcal. wwa!pacelabs.com QUALITY CONTROL DATA Project: MATCOR Rll-47 Pace Project No.: 92277061 Pace Analytical Services. Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)1623-8921 QC Batch: EDEN120841 Anatysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN Associated Lab Samples: 92277061001, 92277061002 SAMPLE DUPLICATE: 1611855 92277061001 Dup Max Parameter Units Result Result RPD RPD Qualifiers PH Std. Units 6.1 6.1 0 9 H6 Results presented on this page are In the units indicated by he "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report sha4 not be reproduced, except in full, Date: 12/04/2015 12W PM without the written consent of Pace Analytical Services, inc.. Page 7 of 12 aceAnaly iical` 1 www.pacalabs.com f Project: MATCOR R71-47 Pace Project No.: 92277061 QC Batch: MPRP/20119 QC Batch Method: EPA 200.7 Associated Lab Samples: 92277061001, 92277061002 METHOD BLANK: 1615691 Associated Lab Samples: 92277061001, 92277061002 Parameter Units Copper uglL Lead ug1L Zinc ug1L QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit ND 5.0 ND 5.0 ND 10,0 MDL Analyzed 2.5 12/03/15 02:07 2.5 12103I15 02:07 2.5 12103/15 02:07 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (338)623-8921 Qualifiers LABORATORY CONTROL SAMPLE: 1615692 Spike LCS LCS % Rec Parameter Units Conc- Result % Rec Limits Qualifiers Copper ug1L 500 506 101 85-115 Lead ug1L 500 486 97 85-115 Zinc uglL 500 479 96 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1615693 1615694 MS MSD 92277053005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual Copper ug1L 0.025 500 500 590 544 113 104 70-130 8 20 mg1L Lead ug1L ND 500 500 526 476 105 95 70-130 10 20 Zinc ug/L 0,16 mglL 500 500 674 629 102 93 70-130 7 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1615695 1615696 MS MSD 92277097001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual Copper uglL 7.7 500 500 572 521 113 103 70-130 9 20 Lead uglL NO 500 500 524 468 105 94 70-130 11 20 Zinc uglL 30.1 500 500 558 503 106 95 70-130 10 20 Results presented an this page are In the units Indicated by Cie" Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/04/2015 12:37 PM without the written consent of Pairs Analytical Services, Inc.. Page 8 of 12 1�;5'ceAnalytical` wnwpeCNeSs.tom Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eaen, NC 27288 (336)623-8921 QUALIFIERS Project: MATCOR Rt1-47 Pace Project No.: 92277061 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. POL - Practical Quantization Limit. RL - Reporting Limit. S - Surrogate 1,2-DiphenylhydraZlne decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenytamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyze is a combined corEcentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute, LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS hf8 Analysis initiated outside of the 15 minute EPA recommended holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reprOduCed, except in full, Date: 12/04/2015 12:37 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 /5a'ceAnalyfical" WWW.Pa0dab7.C1.1R1 i' QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: MATCOR R11-47 Pace Project No.: 92277061 Pace Analytical Services. Inc. 205 East Meadow Read - Suite A Eden, NC 27288 (336)623-6921 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92277061001 OUTFALL 001 SM 2540D EDEN120856 92277061002 OUTFALL 002 SM 2540D EDENI20856 92277061001 OUTFALL 001 EPA 9040 EDEN120841 92277061002 OUTFALL002 EPA9040 EDENI20841 92277061001 OUTFALL 001 EPA 200.7 MPRP120119 EPA 200.7 92277061002 OUTFALL 002 EPA 200.7 MPRPl20119 EPA 200.7 Date: 12/04/2015 12:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in tufl, w4hout the written consent of Pace Analytical Services, Inc.. Analytical Batch ICPl18148 ICPI18148 Page 10 of 12 / 7acie Analytical' + wWW.PacelaDa.wm CHAIN -OF -CUSTODY r Analytical Request Document N The Chain-of-Cuslody Is a LEGAL DOCUMENT. All relevant Holds must bo completed accurately. d7 Section A Section g Section C cO Yap*: of {> Required Client Information: Required Project infomtatiom Invoice Information: Come Report To: Attention: r w 1 `�,]J 41889 Address' /ec` ��• CwY Tc: �� Company Name- - - - - REGULATORY AGENCY.' Addra¢s: IT NPDES GROUND WATER j- DRINKING WATER r UST F RCRA OTHER Ema l To: Purchase Order No.: Pace Quote Reference: Phone: Fax: Project Name: Pam Mgeu Site Loeahon Manapar. � f Requested Due DaNlTA7: Project Number: pace Pmna :RequastedAnalysts Fittered.{YlNJ ' Section D Matrix Codes z Required Client lnfpnnation MATRIX 1 CODE S 0 COLLECTED - Preservatives'- ❑rinking Water DW U zz Water WT Waste Water WW Product P SoiVSolitl $L A m qa a COMPosrrE sTarcT CouppslTE Ermcnna � -•� r _ Z SAMPLE ID OV Aper a v w ; (A-i3O.91.-) Air AR w a z -.( o Sampie IDs MUST BE UNIQUE Trsque TS O a V - Other OT U 1—- z as a a ULL z m _C v r g� O 41 C DATE TIME CATE TIME Z = x z z 2 Q 'y Pace Project NoJ Lab I.D. 00 �I 1 5 F? �3= AD 12 Y ADD1TiONAi COMMENTS '.r MT-- r-.z-RELiN41iISiiE6i3Yl AFFtLIATION� # F DATE 'i a TIME.----- �ACCEPTEDBY-I AFFILIA71Ot1j -DA7Ep t..-4TEME SAMPLE CONDITIONS ,A.,S^,.'R.: r_ .-:z a:._ �•c ,.� a}.•- 4 r -. _:-. - :-r*.0 .r!. �.1 ru - � ,e.. SAMPI.EiiNAMEANDSIGNATURE Y • tr s fn-sr �#� � ;y- s-�} `d ORIGINAL �• Name PRINT of SAMPLER: E 4 DATE Signed ti, m SIGNATURE of SAMPLER' (MMIDerm: !, i / S 'Important Note: By slgning this rrnm you are accepting Pams NET 30 day Peyr M terma 00 agreeing ro late charges of 1.5% Par month for any nwkea not pa j7+r3p deyF. F-ALL-0-020rev.07, 15-May-2007 Document Name: Sample Condition Upon f}acitlnent Revised: May 15, 2015 c?L@AI%iiGr7l-s Receipt ISCURI Page 1 of 2* Document No.: Issuing Authorities: F•EDN-CS-003-rev.1 i Pace Eden Quality 6ifice 'Page 2 of 2 is for Internal Use Only Client Name. - Courier (circle): Fed Ex UPS LISPS Eno t Commercial Pace Other r Custody Seal on Cooter/Box Present: ❑yes Seals intact: . ❑yes ❑ no Packing Material: .❑3ubble' Wrap ❑Bubble Bags 12'oNoneeT�❑ Other Thermometer Used: IR'Gun EDOOT _Tdoe of lCel UVet]. Blue None Samotes en ice- conllno orocess has bean Temp Correction Factor: Add 15ubtract C Date "and InitlaLp of person examining contents resew lion J: 'i Corrected Coo16 mp.. C Biological ilssue is Frozen:•Yes No NIA Ci1eCk Temp should be above freezing to 6T Comments: Chain of Custody Present: Yea. ONo .. ❑WA 'i.: . Chain of Custody Fined Out: ONo .. DWA 2.. . . Chain of Custody Relinquished: DYea , ON, ❑WA 3. . Sampler Name & Signature on COC: .6yea ON". ❑€VIA 4,: . . Sam les Arrived within Hold Time: 2(Yea ON. QWA 5. .: Short Hold Time Analysis e72hr : QYas- o ❑WA 6. Rush Turn Around Time Requested: ❑Yes two., l7NlA 7. ... - 5uffiClentVolume: eye,.. ON, ❑WA 8......, Correct Containers Used, , Idyes ONO' . Q WA 9. -Pace Containers Used: - es ,.ONo - ❑WA Containers-lritact• PfW ❑No ❑WA 10. Fittered volume received for Dissolved tests ' OYes" ❑No Sample Laheis match COG: t;rYes ONO .�❑✓WA 12. 4ndudes dale rnellD/Analysis itAafrnc `t AN containers needtnp preservation have been decked- C]Yas ONo , qf�A 13. _ All containers needing preservation are found to be in Dyes ONO QN compliance with EPA recommendation. exce lions: VOA, cofiform, TDC, 0&G, W! DRO (water} ❑Yes ❑ No Samples checked for dechlorination: ❑Yea ❑Na.1NlA 14. _, Heads ace in VOA Vials >6mm : Dyes ONO A 15. . Trip Blank Present: ❑Ys ❑Na • 6. Trip Blank Custody Seals Present dyes 13NO . AIA Pace Trip Blank Lot # if purchased): Client Notification/ Resolution: Feld Data Requiiad7 Y ! N Person Contacted: DateMma: Comments/ Resolution: SCURF / SRF . - Date: Review: D -R3 iS ` Note: Whenever there is a discrepancy affecting North Carolina oompllai ce samples, a copy of this form will be sent to the North Carolina DEHNR �s1���� i l 11{ llllll Certifieatlon Office (i.e out of hold, Incorrect preservative, out of temp, incorrectoontainers) 12 of 12 MW,ATER ENVIRONMENTAL, LLC 4901 WATERS EDGE DRIVE, SUITE 201 • RALEIGH, NC 27606 • PHONE 919.859.9987 • FAx 919.859.9930 December 23, 2015 Mr. Joe Edwards, EHS Officer Matcor Metal Fabrication 835 Salem Road Welcome, North Carolina 27374 Reference: Stormwater Discharge Outfall Qualitative Monitoring Report and Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication- Year 3- Period 2- July -December 2015 Welcome, North Carolina Waters Edge Job No R11-47 Dear Mr. Edwards: Waters Edge Environmental, LLC (Waters Edge) is pleased to provide two copies of the Year 3- Period 2 (July -December 2015) 2015 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome, North Carolina (see Figures I and 2). We have completed the Discharge Outfall Qualitative Monitoring Report. Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A). Laboratory analytical results are documented in Appendix B. Based on these results, we have exceedances for the following: 0 Outfall00i 1. Exceedance for copper which was detected at 0.0084 mg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0.171 mg/L versus a benchmark at 0.067 mg/L. Outfal1 002 1. Exceedance for zinc which was detected at 0.507 mg/L versus a benchmark at 0.067 mg/L. Based on the permit conditions, we will conduct a Tier 1 inspection of the facility. Any action items which will be reviewed and potential deficiencies addressed. The Tier 1 response will be recorded in the Stormwater Pollution Prevention Plan. Again, as detailed in earlier reports, due to the lowered benchmark thresholds resulting in benchmark exceedances, we previously sampled an upgradient surface water stream on the site (upgradient Lake Drive) as well as two samples collected from the roof drains. While there were no exceedances for copper, both roof drain samples exceeded the zinc benchmark level at 0.067 mg/L (Roof-1 at 1.9 mg/L, and Roof-2 at 0.23 mg/L). The background upgradient surface water samples were below both the copper and zinc benchmarks. Based on these results, we would conclude the following: Stormwater Discharge Monitoring Report and Tier I Response Year 3- Period 2- July -December 2015 Matcor Metal Fabrication Welcome, NC Page 2 of 2 December 23, 2015 • Metals are present in the upgradient surface water sample at the facility. Even though they are below the copper and zinc benchmarks, these metals are still present and can potentially be a constituting factor to the outfall values detected. • Zinc contained in the building materials or downspouts are also contributing to the zinc in the stormwater which would have nothing to do with the industrial activity at the site. While we will continue to attempt to improve the stormwater quality at the facility, we believe that these type of metals exceedances are largely due to non -industrial sources and can be found in a wide variety of non -industrial settings (e.g. residential or any structures with metal components). Nonetheless, we do understand that this exceedance will result in a Tier 2 response requiring monthly sampling for both Outfalls. Waters Edge appreciates this opportunity to work with Matcor Metal Fabrication. If you have any questions or require any additional information, please contact me at 919.859.9987 or at prahn@watersedgeenv.com. Sincerely, WATERS EDGE- ENVIRONMENTAL, LLC Phillip L. Rahn President CC: NCDENR Stormwater (two copies) 15-099PLR/aht W. < I 7 U� vm� -7 dR ar ol k 44Z % A % Dw NAN p ra i ter., U 4 r ri d 14 Au,✓- N 1re. '5 M, fte a q+ A No. Topo Quad Date Title Pr�jecl Location Map MWATERS ENV[RONMENTAL. LLC R1 1-47 VICICOMe 1.19,2012 File Natne Figure scale Project matcor SPPP RI 147,xis 1 unknown Welcome, North CaroUnn CO in ~a • / f� • r� ■ s �. a� � � �� � ,'�, p I'r% J/• ` i I; : u _.-.J' [ ■ liFw•y • i III �. \ I" SITE s f f ra1Io41 .--"� l�� , , • r -� f /ffI-r^f� �e� � ,� a�-'� .3��" .�_ yam_-� � WAFERS EDGE ENVIRONMENTAL, LLC job No. x11.47 Topo Quad Welcome Date 1.193012 7Yde Projed Locatien Map File Name R1147.x6 Figure 1 Scale unknown Project Matcor SPPP welcome, North Carolina y. 4 ; Cat ,SRC , r • � r job NO. lmuge/Photo Days rids Site & WATESumwndin Properties M RS EDGE ENVIRONMENTAL, Lt.( AII47 D,vWd Co. GIS 10.27.2011 B �`rt doAfms Figure Soak Prowl Matcor SPPP 8[147.& 2 naka Welcome. North CB Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http:/lh2o.enr.state.ne.us/su/Fornis_Documents,htm#miscfbrms Permit No.: IN! C: G 10 13 10 10 1 0 0 or Certi ficate of Coverage No.: ! N I C 1 G! 0 13 10 1 6 113 f Facility Name: Matcor Metal Fabrication County: Davidson Phone No. 336.731.5742 Inspector: Thomas Haynes Date of inspection: 11 A 9.15 Time of Inspection: 13:30 Total Event Precipitation (inches): 1.1 Was this a Representative Storm Event? (See information below) ® Yes ❑ No Please check your permit to verb if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that 1 is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) l Outfall Description: Outfall No. 001/002 Structure. (pipe, ditch, etc.) Pipe Receiving Stream: Unnamed Tributary of Swearing Creek Describe the industrial activities that occur within the outfall drainage area: Metal Fabrication 2 Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Light brown Pagel of 2 S WU-242-1 12609 3 Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where i is clear and 5 is very cloudy: l O 3 4 5 5 Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where l is no solids and 5 is the surface covered with floating solids: 1 O 3 4 5 6 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: O 2 3 4 5 7 Is there any foam in the stormwater discharge? 8 Is there an oil sheen in the stormwater discharge? 9 Is there evidence of erosion or deposition at the outfall? to Other Obvious Indicators of Storm water Pollution: List and describe None Yes No Yes No Yes No Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-1 12608 Semi-annual Stormwater discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted _7.6.15 CERTIFICATE OF COVERAGE NO. NCG030613 FACILITY NAME Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pacer Lab Cert. # �37706_ Comments on sample collection or analysis: None Part A: Stormvuater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR �2015� SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' month DISCHARGING TO CLASS NORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA []Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?Z 011 No. utfa _._....;_. .. tl Date:Sample Collected (mo/dd/yr)_ 24 hour;rainfall amount, _.. s _.: Inches., Total Suspended:Solids pW, Standard units Copper �= ''L'ead Zinc- Non -Polar 0&G/ Total Petroleum.: Hydrocarbons-. . 'TatalToxic. -S Organics:.; 8enchmixrks ===� _ `" `'' 100 mg/L or 50'mg/L° 6.0 -- 9 0 _'0.007 mg/L 0 Q3`mg/L 0.067 mg/l 15 mg/l 1 mg/L. 001 11/19/15 1.1 14.4 6.1 0.0084 ND 0.171 NA NA 002 11/19/15 1.1 19.3 6.3 ND ND 0.507 NA NA 1 Monthly sampling (instead of serni-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit, For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TrO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. 1 further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." ,.)� ! CLi J be s Name (Print name) /, ' r' Title (Print title) - (sjgKature) J (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg%L", where XX is the numerical value of the detection limit, reporting limit, etc, in mgJL. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?' T .Outfa!! No Date Sample .ti Collected) (mo%dd/yr) 24-hour rainfall — amount;'. ;= Inches- Non polar Q&GJTPH,by EPA!1664(SGT-HEM) TotaFSuspended Solids.. pH' , .. 8enchmprks 15 mgJL w 100°mg/L or 50 mg/L* 6.0 - 9.0 5U Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmarlr, you must implement Tier 1, Tier 2, or Tier responses. See Genera! Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. * 2 EXCEEDANCES IN A ROWTOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART it SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the tab results Lor at end gf monitoring eriod in the case of "No Discharge" reports): Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPOBTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the hest of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permit Date:11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 aOAnalytkal e www.pacel©Ls.com 1 { December 04, 2015 Mr. Phil Rahn Waters Edge Environmental 4901 Waters Edge Drive Suite 201 Raleigh, NC 27606 RE: Project: MATCOR R 1 f -47 Pace Project No.: 92277061 Dear Mr. Rahn: Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on November 20, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sam ple analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, 9. Brittany Gibson brittany.gibson@pacelabs.com Project Coordinator Endosures REPORT OF LABORATORY ANALYSIS This report shall not tle reproduced, except in hull, without the written consent of Pace Analytical Services. Inc.. Page 1 of 12 aceAnalytical wxw.pacelabs cam f Project: MATCOR R11-47 Pace Project No.: 92277061 Pace Analytical Services, InC. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Asheville Certification IDs 2225 Riverside Drive, Asheville, INC. 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification t 99030001 West Virginia Certification #: 356 VirginialVELAP Certification #: 460222 North Carolina Wastewater Certiflcation #: 633 Virainia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced. except in full, without the written Consent of Pace Analytical Services, Inc.. Page 2 of 12 /55'ceAnalyfical- WW.P8CeJ8b.&C= Project: MATCOR R11-47 Pace Project No_: 92277061 Lab ID Sample ID 92277061001 OUTFALL 001 92277061002 OUTFALL 002 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 {336)623-8921 SAMPLE SUMMARY Matrix Date Collected Date Received Water 11119/1511:30 11/20/1508:30 Water 11/19/16 12:00 11/20/15 08:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical services, Inc.. Page 3 of 12 aceAnalytical• www.po*abs.com j SAMPLE ANALYTE COUNT Project: MATCOR R11-47 Pace Project No.: 92277061 Pace Analytical Services, Inc- 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92277061001 Ol1TFALL 001 SM 2540D DWJ 1 PASI-E EPA 9040 DWJ 1 PASI-E EPA 200.7 CDF 3 PASI-A 92277061002 OUTFALL 002 SM 2540D DWJ 1 PASI-E EPA 9040 DWJ 1 PASI-E EPA 2003 CDF 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 aceAnalytical s wxwpacelabs.cam I ANALYTICAL RESULTS Project: MATCOR R11-47 Pace Project No.: 92277061 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden. NC 27288 (336)623-8921 Sample: OUTFALL 001 Lab ID: 92277061001 Collected: 11/19/15 11:30 Received: 11/20/15 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids 14.4 mg1L 2.5 2.5 1 11/23/15 14:35 9040 pH Analytical Method: EPA 9040 pH 6.1 Std. Units 0A0 0,10 1 11/2011511:20 H6 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 8.4 ug1L 5.0 2.5 1 11125115 19:00 12103/15 02:44 7440-50-6 Lead ND ug1L 5.0 2.5 1 11/25/15 19:00 12/03/15 02:44 7439-92-1 Zinc 171 ug1L 10.0 2.5 1 11/25/15 19:00 12/03/15 02:44 7440-66-6 Sample: OUTFALL 002 Lah ID: 92277061002 Collected: 11119/15 12:00 Received: 11/20115 0&30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No- ©ual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 19.3 mg1L 2.5 2.5 1 11 /23/15 14:36 9040 pH Analytical Method: EPA 9040 pH 6.3 Std. Units 0.10 0,10 1 11/20/15 11:20 H6 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND uglL 5.0 2.5 1 11/25/15 19:00 12/03/15 02:47 7440-50-8 Lead ND ug1L 5.0 2.5 1 11125115 19:00 12103/15 02:47 7439-92-1 Zinc 507 uglL 10.0 2.5 1 11/25/15 19:00 12/03/15 02:47 7440-66-6 Date: 12/0412015 12:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. Inc.. Page 5of12 aceAnalytical www.Paoefabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Prajett MATCOR R11 47 Pace Project No.: 92277061 QC Batch: EDEN120856 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92277061001, 92277061002 METHOD BLANK: 1613266 Associated Lab Samples: 92277061001, 92277061002 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 1613267 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit MDL Analyzed Qualifiers ND 2.6 2.5 11123/1514:34 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 228 91 90-110 Result presented on this page are lathe units Indicated by the `Units' column except where an atternate unit is presented to the rigM of tha resuX REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/0412015 12:37 PM without the wriften Consent of Pace Analytical Services, Inc.. Page 6 of 12 1�!aceAnalytical o ftvrrw.pacNabsrom I QUALITY CONTROL DATA Project: MATCOR R11-47 Pace Project No.: 92277061 QC Batch: EDEN120841 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN Associated Lab Samples: 92277061001. 92277061002 SAMPLE DUPLICATE: 1611855 Parameter pH 92277061001 Dup Units Result Result Std. Units 6,1 6.1 Pace Analytical Services, Inc, 205 East Meadow Road • Suite A Eden, NC 27288 (336)6234W I Max RPD RPD Qualifiers 0 9 H6 Resu is presened on this page ate in the units Indicated by tte "units" colulm exceptwhere analternate ann Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 12/0412015 12:37 PM mthout the written consent of Pace Analytical Services, Inc.. Page 7 of 12 s aceAnalytical w4w.pacelabs.com i t Project: MATCOR R11-47 Pace Project No.: 92277061 QC Batch: MPRP120119 QC Batch Method: EPA 200.7 Associated Lab Samples: 92277061001, 92277061002 METHOD BLANK. 1615691 Associated Lab Samples: 92277061001, 92277061002 Parameter Units Copper ug/L Lead ug/L Zinc ug/L QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit ND 5.0 ND 5.0 ND 10.0 MDL Analyzed 2.5 12103/15 02:07 2.5 12/03/15 02:07 2.5 12/03/15 02:07 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (335)623-8921 Qualifiers LABORATORY CONTROL SAMPLE: 1615692 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 506 101 85-115 Lead ug/L 500 486 97 85-115 Zinc ug1L 500 479 96 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1615693 MS 92277053005 Spike Parameter Units Result Conc. Copper ug1L 0.025 500 mg1L Lead ug/L ND 500 Zinc ug/L 0.16 mg1L 500 1615694 MSD Spike MS MSD MS MSD % Rec Max Conc. Result Result a% Rec % Rec Limits RPD RPD Qual 500 590 544 113 104 70-130 8 20 500 526 476 105 95 70-130 10 20 500 674 629 102 93 70-130 7 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1615695 1615696 MS MSD 92277097001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Copper ug/L 7.7 500 500 572 521 113 103 70-130 9 20 Lead ug/L ND 500 500 524 468 105 94 70-130 11 20 Zinc ug/L 30.1 500 500 558 503 106 95 70-130 10 20 Results preserved on this page arc In the units Indtcated by he "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/04/2015 12:37 PM without the written consent of Pace Analytical Sefvices, Inc.. Page 8 of 12 /5a'C6Ana1j4Jica1' f»mwpeoefebs.com I Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)523-a929 QUALIFIERS Project: MATCOR R11-47 Pace Project No.: 92277061 DEFINITIONS OF - Dilution factor, it reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. POL - Practical Ouantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NEL C; Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA recommended holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/04/2015 12:37 PM without the written consent of Pace Analytical Services, Inc_. Page 9 of 12 aceAnalytical„ wawP&cqieLs.coro QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: MATCOR R11-47 Pace Project No.: 92277061 Pace Analytit:at Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27268 (336)623-8921 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92277061001 OUTFALL 001 SM 2540D EDENl20856 92277061002 OUTFALL 002 SM 2640D EDENl20856 92277061001 OUTFALL 001 EPA 9040 EDENI20841 92277061002 OUTFALL 002 EPA 9040 EDENf20841 92277061001 OUTFALL 001 EPA 200.7 MPRP120119 EPA 200.7 92277061002 OUTFALL 002 EPA 200.7 MPRPt20119 EPA 200.7 Date: 12104/2015 12:37 PM REPORT OF LABORATORY ANALYSIS Tttiis report shall not be reproduced, except in full, without the wrtften vonsent of Pace Analytical Services, Inc.. AnalyticalBatch ICP118148 ICP118148 Page 10 of 12 YneV.paCElaei,eam CHAIN -OF -CUSTODY / Analytical Request Document v Tho Chain-ot-Cusuody is a LEGAL DOCUMENT. All relavant fields must be completed accurately- U1 Section A Section 8 Section C - Papa: of d Required Criani lillomtatlon: Required Arojoet Imam W.. Invoice Inlorrnalion' (:ampsI Report Ta: AEention: Address: Copy To: Company Noma: REGULATOR_Y AGENCY `GROUND - Address: r NPDES r WATER r DRINKING WATER j" UST r RCRA OTHER (=rr a:l 'o_ 1 Purchase Order No.: 1'—� PB�Q�� nJ Retaren:,e: Phone: Fax: Project Nartl6: Pecs Project Site Lncatlori Manages. � �/' Raquasied Due DatofTAT: ?roja,! Numter, - �'ece Pmtile a: / (y ' STATE. Requbsfed Analysis FlItered (Y/N)t _ R Section 1) Matrix Codas — a S'3 R.q,Ir.dciledl mfdrmaricn I+�4__T317S� COpg ` COLLECTED - PresQrvafives' ,�._ _; Drinking Water DW L) zQ tvatar V ty Waste water ww PrOducI C a A co tPosrtE COMPOSITE 0 _ _?.. SoluSalid SL $ ca 0 SAMPLE ID Woe wP - � 0 � "N: — Air AR C z `o V Sample IDS MUST BE UNIQUE Tissue TS O a w F- Olhar OT X d j O c v (\nJn\1flJ ILL Q 0 =�z�°� Z� a — N M d DAIE. TIME DATE TIME to R _ S T Z Z y �' Paco Project No.l Lab UY st: /wit-.� EJVr/ 1jj I 12- I ", ._ hj 6s .10 f.. COMMENTSF f - REL01CU15HE6 8Y l AFFILIATION-._ �' TIME r," ^ay.'.;�3-. -ACCEPTED BYI AFFILIATION 01TIME SAMPLE CONDITIONS .�A�„IADDRIONAL ix '/r,»'sue _ ,DRTE� l 1 SAMPLER 01d J ��� ORIGINAL PRINT Namo of 5AMPLERY n 2 v U 4 PATE 5i0nad � u U F.SIGNATURE E o1 SAMPLER: ^l of m 'imporlanl Now By signing this farm you are accaplmg Paco t NET 30 say aay. l t tang, and ngreairq >n 1.r charges of 1.5% per mcrntn for eny nvoices rot ? ," ""all / / F-ALL-Q-020rov-07, 15-MW2007 7 Document Name: Sample Condition Upon Document Revised: May 15, 2015 CE, a1 C81 Receipt SCUR Page 1*of 2*- Document No.: Issuing Authorities: F-EDN-CS-003-rev.11 Pace Eden Quality Office *Page 2 of 2 Is for internal Use Only' Client Name: Courier (circle): Fed Ex UPS LISPS fno t Commercial Pace Other Custody Seal on Cooler/Box Present: ❑yes Seals Intact:. ❑ yes ❑ no Packing Material: .bubble Wrap ❑Bubble Bags ;2rNonee Other' Thermometer Used: IR Gun E0007' -Tdoa of ice'/ Weti Blue None n Samples on ice_ coolina morass has hanun Temp Correction Factor: Add ISubtract C Date and Initial of person examining � contents resew tlon `. i J- ' i'S Corrected'Coolei•Temp. = C $laioglcal Tissue is Frozen:• Yes No NIA check. Temp should be above heezing to 6'0.. Comments: Chain of Custody Present: rec. ❑No - QNIA 1. Chain of Custody Filled Out: s QNo . i3NUA 2.. Chain of C4stodyAdinquished. OYU , ©No DNA 3— Sampler Name & Signature on COC: 1Yes ON.. ❑N1iA 4• -. Sam les Arrived within Hold Time: • Yes ❑No„ ❑N1A 5. Short hold Time Anal is <72hr :. C]Yes o ❑N1 6. Rush Turn Around Time Requested: Dye* 911o. 01`UA,i 7. -.. Sufficient Volume: RKS.. ONO.. ❑NIA t3. ... __ . Correct Containers Used: Y` ©No..OVA 9. -Pace Containers Used:. �-. ❑No.; bwA Containers Intact:. ;Was, ©No. ©wA ,10. Filtered volume received for Dissolved tests ©Yee l7No rrA 11. " Sample Labels match COC: ❑NO,.❑✓Nun 12. -includes date Mrne11D1Anal sis Matrix: ` All contalners needing proservatlon have been decked. ❑Yes Iallo . !A 13. An containers needing preservation are found to be In DYe$ ONO 00 - compliance with EPA recommendation. exce liana: VOA. oollfarm. TOO. 0&0, W]-DRO (wa ) ❑Yes []No Samples checked for dechlorinat(on: - E[Yes ❑No .: Yr1wA 14 ,. Heads ace in VOA Vials >6mm : Oyes ONo A 16. - Trip Blank Present: aces ❑lvo . !A B, Trip Blank Custody Seals Present Oyes ❑No...❑ A . •.. Pace Trip Stank Lot # if urchased): ClientNotifleationl Resolution: Field Data Required? Y 1 N Person Contacted: DateMme: Comments/ Resolution: Ala#SCURF I SRF Date hF Y y Review Note: Whenever there is a discrepancy affecting North Carolina compliance i i i samples, a copy of this form will be sent to the North Carolina DEHNFt �i� ■y!� M#I : Wl I �i Certification Office (Le out of hold, Incorrect preservative, out of tahip, 22 706'1 Incarrect,conlainers) 42a9i12 of 12 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 7.6.15 CERTIFICATE OF COVERAGE No. N00030613 FACILITY NAME Matcor Metal Fabrication COUNTY --Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace_ Lab Cert. t# _37706_ Comments on sample collection or analysis. None Part A, Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2015_ SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ®ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA []Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 —) ❑ No discharge this period?' Outfall No. _ _.. .: Date Sample; i - Collected - (moJddJYr). _ 24 hour rainfall amount, .inches' — Total Suspended Solids pH, Standard units x, Copper . Lead - Zinc . Non -Polar O&G/- Total Petroleum Hydrocarbons Tata! Toxic' = s organics 8enchmixrks:===> ............,.....r... _ _....-.__._ 100 mg/L or:50��rng/(. 6.0 -- 6.0 �0.007 mgJL 0 03 mg/L 0.067 mg/l : _' 15 mg/L 1.mg/L 001 11/19/15 1.1 14.4 6.1 0.0034 ND 0.171 NA NA 002 12/19/15 1.1 19.3 6.3 ND ND 0.507 NA NA ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended. sites may be eligible for a waiver of the rain gauge requirement, See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture - electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit hate: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the 5tormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring maQ'be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping or concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the 5tormwater Pollution Prevention Plan." Name (Print Warne) Title (Print title) (sja6ture) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND,.or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z Outfail NonT " = :.. Date 5ample toliectedl (mo/dd/Yr) 24-hour ralnfali amount': a Inches..-- rt Non polar O&G/fRH:by W4 166G SGT-HEM) TotalSuspended Solids pH' benchmarks == >:._ is mg/L. _; 100, mg/L or 50 mg/L* 6.0 -- 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B, • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART 11 SECTION 6. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on final and one copy of this DMR inGludin alf "Na Dischar e" re arts within 30 days a revel t of the lab results(or at end of, monitorina period in the case o "No Dischar e" Etports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFO IMATION REPORTED: "i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the hest of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing Violations." of Permit Date:11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 7.6.15 CERTIFICATE OF COVERAGE NO. NCG030613 FACILITY NAME _Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace_ Lab Cert. # _37706_ Comments on sample collection or analysis: None Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2015 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly" (month) DISCHARGING TO CLASS ®ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other PLEASE4EMtMBER-TD SIGN ON PAGES 2AIVDJOFi 3 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks =__> _ - 100 mg/L or 50 mg/0 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 6/9&19/15 0.59/0.13 ND 6.00 0.0122 ND 0.709 NA NA 002 6/9&19/15 0.59/0.13 10.5 6.3 ND ND 0.307 NA NA " Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TT'O monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. 1 further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) signature) (Date} Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, N<XX me/l.", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you most implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No_ Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH b EPA 1664 (5GT-HEM)y Total Suspended Solids pH Benchmarks ==-> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:12/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sermple value in excess of the benchmark, you must implement Tier 1, Trer ,, or Tier 3 responses See General Permit text. FOR PART A AND PARTS MONITORING RESUUT : o A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAV£ YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports within 30 days of recent of_the lab results (or at end of monitoring period in the case of "No Discharge" reports to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOii'ANY I FORMATION REPORTED'. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permitteej Permit Date: 11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 /55'ceAna1Xim1* iww.psceiabscnm October 24, 2014 Mr. Phil Rahn Waters Edge Environmental 4901 Water's Edge Drive Suite 201 Raleigh, NC 27606 RE: Project: MATCOR R11-47 Pace Project No.: 92221551 Dear Mr. Rahn; Pace Analytical Services, Inc. 20$ East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on October 15, 2014, The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me_ Sincerely, Terri Page terri.page@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 15 0 aceAnalytrcal www.pacslab$.mm CERTIFICATIONS Project: MATCOR R11-47 Pace Project No.: 92221551 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 15 aeeAnalylieal j ww'.paoelahamm 1 SAMPLE SUMMARY Project: MATCOR R11-47 Paoe Project No.: 92221551 Lab ID Sample ID Matrix Date Collected Date Received 92221551001 92221551002 OUTFALL 001 OUTFALL 002 Water Water 10/15/14 10:00 10/15/14 10:15 10/15/14 15:55 10/15/14 15:55 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc._ Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)6238921 Page 3 of 15 aceAnalWical, INYW.PSCOW&WM SAMPLE ANALYTE COUNT Project: MATCOR R11-47 Pace Project No.: 92221551 i I Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC f1 288 (336)623-8921 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92221551001 OUTFALL 001 SM 2540D CHM 1 PASI-E EPA 1664B CLW 1 PASI-C EPA200.7 JMW 28 PASI-A 92221551002 OUTFALL 002 SM 2540D CHM i PASI-E EPA 1664E CLW 1 PASI-C EPA 200.7 JMW 28 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 15 5axAnal1�'ytical � irwi PscWabacam ANALYTICAL RESULTS Project: MATCOR R11-47 Pace Project No.: 92221551 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Sample: OUTFALL 001 Lab ID: 92221551001 Collected: 10115/14 10:00 Received: 10/15/14 15:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 9.6 mg1L 2.6 2.6 1 10/17/14 08:55 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1.1 1 10/21/14 08:50 200.7 MET tCP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Aluminum 235 ug1L 100 50.0 1 10/17/14 15.15 10/22/14 23:13 7429-90-5 Antimony 5.8 ug1L 5.0 3-9 1 10/17/14 15:15 10122/14 23:13 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 10/17/14 15:15 10122/14 23:13 7440-38-2 Barium 21.1 ug1L 5.0 2.5 1 10/17/14 15:15 10122/14 23:13 7440-39-3 Beryllium ND ug/L 1.0 0.050 1 10/17/14 15A5 10122/14 23:13 7440-41-7 Boron ND ug/L 50.0 25.0 1 10/17/14 15:15 10/22/14 23:13 7440-42-8 Cadmium ND ug1L 1.0 0.50 1 10/17/14 15:15 10/22/14 23:13 7440-43-9 Calcium 3970 ug/L 100 50.0 1 10/17/14 15:15 10122/14 23:13 7440-70-2 Chromium ND ug/L 5.0 2.5 1 10/17/14 15:15 10122/14 23:13 7440-47-3 Cobalt ND ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:13 7440-48-4 Copper 15.2 ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:13 7440-50-8 Iron 302 ug/L 50.0 25.0 1 10/17/14 15:15 10122/14 23:13 7439-89-6 Lead ND ug/L &0 2.5 1 10/17/14 15:15 10122/14 23:13 7439-92-1 Magnesium 406 ug/L 100 50.0 1 10/17/14 15:15 10122M4 23:13 7439-95-4 Manganese 6.7 ug1L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:13 7439-96-5 Molybdenum ND ug1L 5.0 2.5 1 10/17/14 1515 10/22114 23:13 7439-98-7 Nickel ND ug/L 5.0 2-5 1 10117114 15:15 10122114 23:13 7440-02-0 Potassium NO ug/L 5000 2500 1 10/17/14 15:16 10/22/14 23:13 7440-09-7 Selenium ND ug/L 10.0 5.0 1 10117/1415,15 10122/14 23:13 7782-49-2 Silicon 1300 ug/L 100 50.0 1 10/17/14 15:16 10/22/14 23:13 7440-21-3 Silver ND ug/L 5.0 2.5 1 10/17114 15:15 10122i14 23:13 7440-22-4 Sodium ND ug1L 5000 2500 1 10/17/14 15:15 10/22/14 2313 7440-23-5 Strontium 26.5 ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:13 7440-24-6 Thallium ND ug/L 10.0 5.0 1 10/17/14 15:15 10/22/14 23:13 7440-28-0 Tin ND ug/L 5.0 2.5 1 10/17/14 1515 10/22/14 23:13 7440-31-5 Titanium 5.8 ug/L 5,0 2.5 1 10/1.7/14 15:15 10/22/14 23:13 7440-32-6 Vanadium ND ug/L 5.0 2.5 1 10/17/14 15:15 10122/14 2313 7440-62-2 Zinc 840 ug/L 10.0 2.5 1 10/17/14 15:15 10/22/14 23:13 7440-66-6 Sample: OUTFALL 002 Lab ID: 92221551002 Collected: 10/15/14 10:15 Received: 10115/14 15:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 9.6 mglL 2.5 2.5 1 10117/14 08-56 HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1.1 1 10/21/14 08:50 Date: 10/24/2014 09:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 15 Pace Analytical Services, Inc. aceAnalyirca! a 205 East Meadow Road - Suite A Eden, NC 27288 wwwPWBbd OM (336)623-8921 ANALYTICAL RESULTS Project: MATCOR Rll-47 Pace Project No.: 92221551 Sample: OUTFALL 002 Lab ID: 92221551002 Collected: 10/15/14 10:15 Received: 10/15/14 15:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA200.7 Preparation Method: EPA200.7 Aluminum 943 ug/L 100 50.0 1 10/17/14 15:15 10/22/14 23:16 7429-90-5 Antimony ND ug/L 5.0 3.9 1 10/17/14 15:15 10/22/14 23:16 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 10/17/1415A5 10/22/14 23:16 7440-38-2 Barium 69.0 ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7440-39-3 Beryllium ND ug/L 1.0 0.050 1 1011711415:15 10/22/14 23:16 7440-41-7 Boron 64.1 uglL 50.0 25.0 1 10/17/14 15:15 10/22/14 23:16 7440-42-8 Cadmium ND ug/L 1.0 0.50 1 10/17/14 15715 10/22/14 23:16 7440-43-9 Calcium 13700 ug/L 100 50.0 1 10/17/14 15:15 10/22/14 23:16 7440-70-2 Chromium ND ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7440-47-3 Cobalt ND ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7440-48-4 Copper 6.2 ug/L 5.0 2.5 1 1CI17114 15:15 10/22/14 23:16 7440-50-8 Iron 983 ug/L 50.0 25.0 1 10/17/14 15:15 10/22/14 23:16 7439-89-6 Lead ND ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7439-92-1 Magnesium 1160 ug/L 100 50.0 1 10/17/14 15:15 10/22/14 23:16 7439-95-4 Manganese 19.3 ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7439-96-5 Molybdenum ND ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7439-98-7 Nickel ND ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7440-02-0 Potassium ND ug/L 5000 2500 1 10/17/14 15:15 10/22/14 23:16 7440-09-7 Selenium ND ug/L 10.0 5.0 1 10/17/14 15:15 10/22/14 23:16 7782-49-2 Silicon 3030 ug/L 100 50.0 1 10/17/14 15:15 10/22/14 2316 7440-21-3 Silver ND uglL 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7440-22.4 Sodium 5400 ug/L 5000 2500 1 10/17/14 15:15 10/22/14 23:16 7440-23-5 Strontium 63.4 ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23A6 7440-24-6 Thallium ND ug1L 10.0 5.0 1 10/17/14 15:15 10/22/14 23:16 7440-28-0 Tin ND ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7440-31-5 Titanium 24.6 ug1L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7440-32-6 Vanadium ND ug/L 5.0 2.5 1 10/17/14 15:15 10122N4 23:16 7440-62-2 Zinc 720 uglL 10.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7440-66-6 IDOMEiUlPZ.lPKtiC[fill cYX1►i REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 15 �:2acleAnalyticale wtnvpacslabs.carrt QUALITY CONTROL. DATA Project: MATCOR R11-47 Pace Project No.: 92221551 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QC Batch: EDENl16110 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92221551001, 92221551002 METHOD BLANK: 1309366 Matrix: Water Associated Lab Samples: 92221551001, 92221551002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 10117/14 08:52 LABORATORY CONTROL SAMPLE: 1309367 Spike LCS LCS a% Rec Parameter Units Conc. Result %Ree Limits Qualifiers Total Suspended Solids mg/L 250 240 96 90-110 SAMPLE DUPLICATE: 1309368 92221535001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 55.7 56.1 1 10 SAMPLE DUPLICATE: 1309369 92221714001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mgfL 102 90.8 12 10 D6 Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 09:32 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 15 aceAnalytrcal. www.psceleba.00m QUALITY CONTROL DATA Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC �7288 (336)623-8921 Project: MATCOR R11-47 Pace Project No.: 92221551 QC Batch: GCSV119242 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92221551001, 92221551002 METHOD BLANK: 1311267 Matrix: Water Associated Lab Samples: 92221551 001. 92221551002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mglL ND 5.0 10/21/14 08:50 LABORATORY CONTROL SAMPLE: 1311268 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mglL 40 37.8 94 78-114 MATRIX SPIKE SAMPLE: 1311269 92222103001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL <5.0 40 36.6 92 78-114 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 09:32 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 15 /55'ceAnilyfical" n1vw.P�sctam Project: MATCOR R11-47 Pace Project No,: 92221551 QC Batch: MPRP117151 QC Batch Method: EPA 200.7 Associated Lab Samples: 92221551001, 92221551002 METHOD BLANK: 1309860 Associated Lab Samples: 92221551001, 92221551002 Parameter Units Antimony ug1L Arsenic ug1L Beryllium ug1L Cadmium 1-1911- Calcium ug1L Chromium ug/L Copper ug/L Lead ug/L Magnesium uglL Nickel ug/L Selenium uglL Silver uglL Thallium ug/L Zinc uglL QUALITY CONTROL DATA Analysis Method: Analysis Description: Matrix: Water EPA 200.7 200.7 MET Blank Result Reporting Limit Analyzed N{? 5.0 10122114 22:48 NO 10.0 10122114 22:48 NO 1.0 10/22/14 22:48 ND 1.0 10122114 22:48 NO 100 10122/14 22:48 NO 5.0 10122/14 22:48 NO 5.0 10/22/14 22:48 NO 5.0 10/22/14 22:48 NO 100 10/22/14 22:48 NO 5.0 10/22/14 22:48 NO 10.0 10/22/14 22:48 NO 5.0 10/22/14 22:48 NO 10.0 10/22/14 22:48 NO 10.0 10/22/14 22:48 Qualifiers Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 LABORATORY CONTROL SAMPLE: Parameter 1309861 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug1L 500 464 93 85-115 Arsenic uglL 500 440 88 85-115 Beryllium uglL 500 430 86 85-115 Cadmium ug1L 500 431 86 85-115 Calcium uglL 5000 4520 90 85-115 Chromium uglL 500 428 86 85-115 Copper uglL 500 441 88 85-115 Lead uglL 500 441 88 85-115 Magnesium uglL 5000 4680 94 85-115 Nickel uglL 500 435 87 85-115 Selenium ug1L 500 445 89 85-115 Silver ug1L 250 233 93 85-115 Thallium ug/L 500 436 87 85-115 Zinc ug1L 500 471 94 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1309862 1309863 MS MSD 92221547001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD RPD Qua[ Antimony ug1L ND 500 500 472 460 94 92 70-130 3 20 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 09:32 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 15 aceAnalytfcal www.pecWabs.WM QUALITY CONTROL DATA Project: MATCOR R11-47 Pace Project No.: 92221551 Pace Analytical Services, Inc. 205 East Meadow Road - Syite A Eden, NC 27288 (336)623-8921 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1309862 MS 92221547001 Spike Parameter Units Result Conc. MSD Spike Conc, 1309863 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits Max RPD RPD Qual Arsenic uglL ND 500 500 446 435 88 86 70-130 2 20 Beryllium ug/L ND 500 500 434 426 87 85 70-130 2 20 Cadmium uglL ND 500 500 438 424 88 85 70-130 3 20 Calcium ug/L 3.1 mglL 5000 5000 7590 7350 90 86 70-130 3 20 Chromium uglL ND 500 500 438 423 87 84 70-130 3 20 Copper ug/L 0.0067 500 500 458 442 90 87 70-130 4 20 mglL Lead ug1L ND 500 500 446 430 89 86 70-130 4 20 Magnesium uglL 0.60 mglL 5000 5000 5410 5210 96 92 70-130 4 20 Nickel uglL ND 500 500 442 428 88 85 70-130 3 20 Selenium uglL ND 500 500 458 438 91 87 70-130 4 20 Silver uglL ND 250 250 238 230 95 92 70-130 3 20 Thallium uglL ND 500 500 442 431 88 86 70-130 3 20 Zinc uglL 0.059 500 500 490 473 86 83 70-130 4 20 mglL MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1309864 MS 92221690005 Spike Parameter Units Result Conc. MSD Spike Conc. 1309865 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits Max RPD RPD Qual Antimony uglL ND 500 500 473 486 94 97 70-130 3 20 Arsenic uglL ND 500 500 442 457 88 91 70-130 3 20 Beryllium uglL ND 500 500 440 461 88 92 70-130 5 20 Cadmium uglL ND 500 500 438 451 88 90 70-130 3 20 Calcium uglL 1370 5000 5000 5960 6190 92 96 70-130 4 20 Chromium uglL ND 500 500 441 461 88 92 70-130 4 20 Copper uglL ND 500 500 453 472 90 93 70-130 4 20 Lead uglL ND 500 500 444 455 89 91 70-130 2 20 Magnesium uglL 270 5000 5000 5050 5230 96 99 70-130 3 20 Nickel uglL ND 500 500 442 461 88 92 70-130 4 20 Selenium uglL ND 500 500 451 459 90 92 70-130 2 20 Silver ug/L ND 250 250 237 240 95 96 70-130 1 20 Thallium uglL ND 500 500 440 449 87 89 70-130 2 20 Zinc uglL 97.4 500 500 524 544 85 89 70-130 4 20 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 09:32 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 15 acmnalytical J www.pacowmcom F QUALIFIERS Project: MATCOR R11-47 Pace Project No.: 92221551 191o171:lrti ORK Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 09:32 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 15 aceAnalytical. wvw.psaafabscom QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: MATCOR R11-47 Pace Project No.: 92221551 Pace Analytical Services, Inc, 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92221551001 OUTFALL 001 SM 2540D EDEN116110 92221551002 OUTFALL 002 SM 2540D EDEN116110 92221551001 OUTFALL 001 EPA 1664B GCSVI19242 92221551002 OUTFALL 002 EPA 1664B GCSVI19242 92221551001 OUTFALL 001 EPA 200.7 MPRP117151 EPA 200.7 92221551002 OUTFALL 002 EPA 200.7 MPRP117151 EPA 200.7 Date: 10/24/2014 09:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batc h ICP115462 ICP115462 Page 12 of 15 '10,21, eAnalXicat* www.oacalahs.eorn CHAIN -OF -CUSTODY /Analytical. Request Document The Chairt-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately - Section A Section 0 Section C Page: or Required Client information: Required Project Information: Involve Information: Company: Report To: Attention: AY 1 810515 Address: P Copy To: - Company Name: REGULATORY AGENCY a :.: Address: T- NPDES r GROUNDWATER DRINKINGWATER T— UST RCRA OTHER EffkaJ TO: Purchase Order No. Pace Ouote Raforence Phone; Fax: �7Z-'o Pace Project Ll Manager. Requested Due DaterTAT: Project Number: Pam PM00 4 ,Requested Analysis Filileriid'(Y/ Section D Matrix Codes RoquiredGlient Inlonnation MATRIX I CODE 2 COLLECTED Presorvativas Drinking Wow Dw R 8 Z Water wr waste weVM COMPWITE COWDSITE F- Producttu P STAU ENDJORAH Soivsolid SL SAMPLE ID Oil OL Wipe wP (A-Z, 0-9 1,-1 Air AIR uj L) o. Lu z -2 CD Sample 0s MUST BE UNIQUE Tissue TS o 8 w M Other OT X Lu 0 0 ca ca al C, fn `; < IV DATE TIME DATE TIME 0 Oz T z v z i 0 I co Pace Project No.! Lab I.D. tT14- ldidw� aco 1,311 -17- A I I 2 4 7 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY' AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS <n SAMPLER NAME AND SIGNATURE ti C.) ORIGINAL PRINT Name of SAMPLER: Z 3� f � � DATE Signed SIGNATURE of SAMPLER:rc (MMIDOIYYi: Ito) z;-/ 4 important tkAa: By Wing this Iorm you are Dwepbng Pace's NET 30 day payment terms and agreeing to late charges of 1.5% Winonthf.-rany imolres not P;��Illn 30 days / / F-ALL-Q-020rov,07, 15-May-2007 �aceAnalyfical' r � rrrfr.pacel>!rs-earn . , . CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All televani fldlds must be completed accurately. Section A Section 6 Section C Page: Required Gient Infminatlon: Required Proiact Inforrnatlon: €frvoice Informatbn:- Companly: Report To: ' Attention: - 1 Address: h j� �Or Copy To: '"y Name' - REGULATORY AGENCY /f J - - y Address: ]— NPDES F-. GROUND WATER J" - DRINKING WATERY UST RCRA OTHER Ema;l To: / Purchase Order No.: r Pace Quote i fi Jiti Reference: Fax: Project Name: Pam Project Site Locatlori _ - '- a Le: Manager: STA TE- s r ,. uested Due Dete/TAT: • Project Number; J Pace Profile N: RequestedAnaiysisFiltered:(Y!N} - Section D Matrix Codes 2' ' Requlrad Client lnroim2tfon MATRIX r CODE 9 IML COLLECTED Preservatives tom' s', 0dnldng Water DW U Water WT Waste Water WW Product P ij m COyMPPOSITE -J -- t-TART ,' i� z _ -, •-- ��- ` - So'lusolid SL - . p-- SAMPLE ID O1� wP �? Q W `�� (A-Z, 0.9 7 ,.) Air Ate Sample IDs MUST BE UNIQUE Tissue 7$ d O w ._ - „ d C V v ul z Z ffn11 Other OT X ul w- 6 . w „ O 8 ,.T � :c tL a U. O x v7 w . is '—n \\ - w m 7 2 Z Z .� ~ - DATE T1ME t]ATE T1ME 2 e5 tY Pace Project Nod Lab I.D. _2 , 3 r . 4 'g s 7 ti - 9 t0 tt 42 AODMONAL COMMENTS - RELINQUISHED BY f AFFIL€ATION DATE TIME ACCEPTED BY t AFFILIATION - DATE TIME SAMPLE CONDITIONS ' SAMPLER NAME AND SIGNATURE -6 U PRINT Name of SAMPLER: .r^� SIGNATURE of SAMPLER: 0.GATE 5Egned `—� v (MMlDOlYY): %Q w 'Important We: By signing this lurm you are accepting Pace's NET 30 day paymort terms end agrea'ag to We charges of 1.59E per Monthlor any invoices not 30 days, F-ALL-Q-U21)rev,07, 35-May-Z007 ... OW Aactrmer�t �m�:Sainpie.�on_ dt�tcn.Upah. Recei _ S !i _ pocumenf ttet�rsed: t�4arch 4;3, 2t)73 . . ,: ; page 1 of 2 E?eeiJM- "t F- I3 E-CS-Q03 1 i?9 EssutngAtlftiorlties: Pace Eden QuoliE t?ffice Client Name-neirw� -Aso Where Received: ❑ HuntemVilte ❑ Ashevltie Eden ❑ leigh courlerpmej, r*dac . ups lisps C et>f Cbmmerctat dace other-'' _ custody Sea! on:Cootedsm( Presertt: ❑O$ � na Seats lgt6t: - ❑ yes ❑ . no PaoldotHAi4al:: 03abbte•Wmp ❑BabbiiBaos dNona ❑ other- Thermameter,U,sed� ER Cun MOO-, iy�� o� Ice: et Biuc: E�one . � ,Saii�je� or io>a, �O�ilr�§ Vas trds bean 'pomp;Corrr,•l:a�ofor��ici�/Subir�ot�;,�;�,,�6 ��ti' r `,,� •� ...•--':.�.,�: - :.. " iologi 7itss a !s Ff+ c Yes W6 r� A �te'agd inrt�ars ;�srsoh exalnin'trig� Carteied C4oIe:3`emp.; ' - C - : contai�ts •FB1viCtSh0��68haYEirP.ezftMfOd'ii'• - - -...-'E[4t11lnalif�_ .. <.r.. �•_ ..... Qi1a[il af. iuStO Pr6S : . " es-13No = 3Wq Vf" C#tain of Gtrsta ' : IIIA 2; eiiah of. usta F�eiin iafishedr UNd'.:0W S�il1 t game & roan COG: _ e ONO arrived e�fthi� `E tin6:; e3 - - ;Qr�fl4 i ' ; ' t Short Fioid, M0: Aftel ysis USit Tn fCtiiiti �[ITIb.REgUPSted, • QYt:,Q_Na: - : a Sa OientVohir»B, •`�- ear No WAy Cor ed GatitOhm Used: . -_ . E es:,»t� - Owk 0... ' a[oa;Cor�tnexs {Is9ck as iW • •f tWA coi, rlers lrEtsot:. Citso QWk Ia.' FAked'volu 's io'cetved for .D S'otred wis ms ONO • 64 .#. -, � .r . � s `. r ,` • � -fncludesdatelfimeAUlAr!aiysis-. Wft:. canfamersneedir presenmonhave beenchecked es ONO CNA 1$, Al car! alners nead<rpresetYaiibtr areionndtc 60 6t Yes t3A[o 111J/ll campiiasicaidfhY�PAre�rnmetsdatien, • mplla VOA ovrfimlT000A[VITRO &W C7YPs ONO - , ittatK'fi"e ✓T ' •� : �'.'"1 ; !. :'� t; Sala ies.bhectted for dechfoi'mditorij'. "G3ve Cit Ea' & t; " .. Head �ace�t-V(�FC.VIat's ,ysrriir�' •;. •..�es�:i,' 1�..• .. .;. -' . . 37ip.Blenk Aresenh :. : t3Yes ©No -. WA [ip Blank N*dySdaTs Preseiii" Pacer t3f�nk Last if `rattase' Client Notification) Resotutian: Field Data Rogdred? Person Co4a*& .. Ant Oommentsl Resolutfan: SCURF Jevtew: live;- `t Pfac$ dahel here n-.. SRF Review: + pays�. ��_. OR Now, Whar!ever the" is a disorepaney affei lq No*Oarolina camPi? I�4e...' , saerpies, 3 oopyof this form besoato lha N*M 0arolin.a•Pf1 iN.9 Oettifroagon Ofte { Lo out of hold, frwrfoo preservative, but oftft t-landwritb prDjeot Iii kb'6f age 15 of 15 :noorrsctoontainera) (if no label available) ace Analytical" July 01, 2015 Mr. Phil Rahn Waters Edge Environmental 4901 Water's Edge Drive Suite 201 Raleigh, NC 27606 RE: Project: MATCOR Rll-47 Pace Project No.: 92255434 Dear Mr. Rahn: Pace Analytical Services, Inc. 205 East Meadow Road - cite A Eden, NC 27288 (336)623-8921 Enclosed are the analytical results for sample(s) received by the laboratory on June 22, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Terri Page terri.page@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 aceAnalyti►cal. r www.paoelabs.com i Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 CERTIFICATIONS Project: MATCOR R11-47 Pace Project No.: 92255434 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification M 357 North Carolina Wastewater Certification #: 12 V rginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 T aceAnalytical www,pacalabscam SAMPLE SUMMARY Project: MATCOR R11-47 Pace Project No.: 92255434 Lab ID Sample ID Matrix Date Collected Date Received 92255434001 92255434002 OUTFALL 001 OUTFALL 002 Water Water 06/19/15 18:30 06/19/15 19:00 06/22115 13:55 06/22/15 13:55 REPORT OF LABORATORY ANALYSIS This report shalf not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 3 of 11 y aoAnalytical f www.pacefabscavn i SAMPLE ANALYTE COUNT Project: MATCOR R11-47 Pace Project No.: 92255434 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92256434001 OUTFALL 001 EPA 1664B JMS 1 PASI-C 92256434002 OUTFALL 002 EPA 1664B JMS 1 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the writter consent of Pace Analytical Services, Inc.. Page 4 of 11 leAnalytical. wWW.patelabtWM ANALYTICAL RESULTS e Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC Z7288 (336)623-8921 Project: MATCOR R11-47 Pace Project No.: 92255434 Sample: OUTFALL 001 Lab ID: 92255434001 Collected: 06/19/15 18:30 Received: 06/22/15 13:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1.1 1 07/01/15 08:56 Sample: OUTFALL 002 Lab ID: 92255434002 Collected: 06/19/15 19:00 Received: 06/22/15 13:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No, Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1.1 1 07/01/15 08:57 Date: 07/01/2015 04:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 a ce Analytical wwtr patafabs.sorrt QUALITY CONTROL DATA Project: MATCOR R11-47 Pace Project No.: 92255434 QC Batch: GCSV121822 Analysis Method: EPA 1664E QC Batch Method: EPA 16648 Analysis Description: 1664 HEM, Oil and Grease Associated tab Samples: 92255434004, 92255434002 METHOD BLANK: 1499006 Matrix: Water Associated Lab Samples: 92255434001, 92255434002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg1L ND 5.0 07/01/15 08:48 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 LABORATORY CONTROL SAMPLE: 1499007 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 35.5 89 78-114 MATRIX SPIKE SAMPLE: 1499008 92255903001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 37.6 94 78-114 Results presented on this page are in the units Indicated by the " Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07101/2015 04:33 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 ace Analytical WWW.Pacelaftwn QUALIFIERS Project: MATCOR Rll-47 Pace Project No.: 92255434 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit, PQL- Practical Quantitation Limit. RL - Reporting Limit, Pace Analytical Services, Inc. 205 East Meadow Road - Svite A Eden, NC 27288 (336)623-8921 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. 'rNI - The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/01/2015 04:33 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnalytical' www.p cam QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: MATCOR R11-47 Pace Project No.: 92255434 Pace Anatytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-B921 Analytical Lab ID Sample Id OC Batch Method QC Batch Analytical Method Batch 92255434001 OUTFALL 001 EPA 16648 GCSV121822 92255434002 OUTFALL 002 EPA 16648 GCSV/21822 Date: 07/01/2015 04:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 CHAIN -OF -CUSTODY / Analytical Request Document aceAnalytica!' m. �-C—". a LEG u o0CvUEKi.'a .w.an MG.rw 6� caroMre �:�ry . OWN SAMPLE ID Ts - . ® + , _: � ... �r���r��i��i���■i■■■■ran e■■■■■■■■■■vim iii■iiiiiii�i ■■■■n■■■■■■■ ■■■■■■■■■■■■■ ■■■■■■■■■■■■■ ■■■■■■■■■■■■■IN ® �iiii ■i■i■iiiiiiiii� e �■�■■■■■■■ mono ■■■■I ® m �■■�■■■■■r�■ir■■r■■■■■■■■■ i■■■■■■■r■■■■■�■■n■■■■ ® �■�■■�■n■n■■r■■■■■■■■ IMM MIN M 94 A� omen •ww'w+Iw dwMN{lw b�.ywN hn\eef io �r T�.+rR.�.. wbA�6b4M n+owd56%ovaai�la wi.Msnba Aan. / FJa-C-0020—.W. 1SM V-2XP CHAIN' I'Analyt.. Ow . . . . . . . ..... is a NMI swoons tsommalummummma musummummmuss ummummummmmus wommmusummums ERNMEN INNON INNEN IN if NENEVEMMEMN sommoommummus Mimmommummom IN! Eg 1• Document Name: Sampto Con_ dltion Upon. Real !(SCUR - Document Reylsed: May 1 , 211f6 Page t ot2 - Oocument No F-EDN-05-003-rev.1 i Issofng Au%odi ": Pace ECn Qual4 Oftt e ' `Page 2 of 2 is for Intemal Uta Only ` - a Courter(drdek FrdE>t UPS Um -CGam :i0dlanaiCla! Pace Cthar CustodySeaf on Coakditx PMwt E)m no Seat$ hox ...Q_ Y —L no Patk[nq Nateifal: EPL93 t* Wrep j]Btd1flag, E] None © 09, I — - — - : - - - The ' r'Used: IR Gun ED007 Tune e[1rw "wPa.'. sa i' Nnne f 1 s ay. M man. h . nb,m Temp Conw on Factor Add 1 Subtiaot CI.... onto and I4ld00 of wraan x+ ma , :n� f -. conk ulv ue'. ' , .•, .0 Conwtsd Cooler Tamp. _- 9lologleal Tlsalre i• Frrixeni,Y: Fa WA eheok Teapthesebealawtreempme'C . , Comments:` Chain of CustAPrasant UNo .OWA Cliebt of Capod RadnGu<shsts: - w chb EhAk 3. ' Sate Ater Neme6 S' m on CpC: • m ON;. Olwk 9:, ' Sam be AnNed YAft Hold The: w ONo . OwA 5...... • . ,' Short14 ld 11mi "Irt, <72h : Q7'a-.26, OVA a.. ' RuahTumAroundTlmrRe aast3ed: ', l7Ya 1" 7.,-.-. Suit'denl Votume: : �- ra; ONO .OwA &.. ,. ConaGCe!h}alnere Ueed: i a' ONO Otiu 4.... .. ... .. , '.-Pa00 COGWflM llaed: - -, 'ei' ON.: OWA .. . Caste:ran Intact 't5rb ONat fD. Fbmd vok" received tofLxissaEYad tests i]Yr ONe� it Sample Labeis match COC:-' Yes ONO D' Mk'12. - - anchrdeadatelBme4DlAna is Adatdr AS ° ° n *,9 RONMUM 11M been &aeW _ OYa ON. 13, Aecontwn"I neaft preeervaWn era found to de In lw/A Dy« ON. z", .. ConVA rpe With EPA Wommen439on. rmgttlanr VOA, of fe, TM Ow."C' , .. oy� Q,M Sam W checked fnrdachlorination: OYa ONO.. - .. 14. ... .. + ' Heeds ace In VOA Via!$ >5ra.1 : Di. ONO k5. TAP elenk P wt MW OM 1lt. Trip Blank Custody Seals Present OY« ONO. ._ F'PWTdp Blank Lot R Otpurchmdi + C1iem Nov"catlonl Resolution: i1W Rafe ne AW? Y I N , person Cmtected: DateRlme: CommanWResoMon' SCURF 18 QaOe:W.;w q j,-n`m+ vr� RevleW; - Now WMra'm there b a 0"cft l 0M) CPf� {j'x■"•�' 1 etmpMs, a k� of cif lam nrP 6e ea:i b Cre h,'orfa ;yoElre 0t7^h'-R �I 1���1� •- t � � � i - f• Ce Mosam0"(Le ow of hold, a+mn d Procanaew, oul often,;,, in<mect wma4�w) ks>i 56 34_^ir, J'�t= t.. '�'7"�-.a�"Jt.•.� '. Page 11 of 11 WATERS EDGE ENVIRONMENTAL, LLC 493'01 WATERS EDGE DRIVE, SUITE 201 • RALEIGH, NC 27606 • PHONE 919.859.9987 • FAX 919.859.9930 July 8, 2015 Mr. Joe Edwards, EHS Officer Matcor Metal Fabrication 835 Salem Road Welcome, North Carolina 27374 Reference: Stormwater Discharge Outfall Qualitative Monitoring Report and Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication- Year 3- Period 1- January -June 2015 Welcome, North Carolina Waters Edge Job No R 1 1-47 Dear Mr. Edwards: Waters Edge Environmental, LLC (Waters Edge) is pleased to provide two copies of the Year32- Period I (January -June 2015) 2014 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome, North Carolina (see Figures 1 and 2). We have completed the Discharge Outfall Qualitative Monitoring Report. Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A). Laboratory analytical results are documented in Appendix B. Due to a sampling error, we did have to do the TPH samples on a second event on June 19, 2015 but it was still within the sampling period. Based on these results, we have exceedances for the following: • Outfall001 1. Exceedance for copper which was detected at 0.0122 mg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0.709 mg/L versus a benchmark at 0.067 mg/L. • Outfall 002 1. Exceedance for zinc which was detected at 0.307 mg/L versus a benchmark at 0.067 mg/L. Based on the permit conditions. we will conduct a Tier 1 inspection of the facility. Any action items which will be reviewed and potential deficiencies addressed. The Tier I response will be recorded in the Stormwater Pollution Prevention Plan. Again, as detailed in earlier reports, due to the lowered benchmark thresholds resulting in benchmark exceedances, we previously sampled an upgradient surface water stream on the site (upgradicnt lake drive) as well as two samples collected from the roof drains. While there were no exceedances for copper, both roof drain samples exceeded the zinc benchmark level at 0.067 mg/L (Roof-1 at 1.9 mg/L.. and Roof-2 at 0.23 mg/L). The background upgradient surface water ' i r . Stormwater Discharge Monitoring Report and Tier I Response ` Year 3- Period I — January -June 2015 Matcor Metal Fabrication Welcome, NC Page 2 of 2 July 8, 2015 samples were below both the copper and zinc benchmarks. Based on these results, we would conclude the following: • Metals are present in the upgradient surface water sample at the facility. Even though they are below the copper and zinc benchmarks, these metals are still present and can potentially be a constituting factor to the outfall values detected. • Zinc contained in the building materials or downspouts are also contributing to the zinc in the stormwater which would have nothing to do with the industrial activity at the site. While we will continue to attempt to improve the Stormwater quality at the facility, we believe that these type of metals exceedances are largely due to non -industrial sources and can be found in a wide variety of non -industrial settings (e.g. residential or any structures with metal components). Nonetheless, we do understand that this exceedance will result in a Tier 2 response requiring monthly sampling for both Outfalls. Waters Edge appreciates this opportunity to work with Matcor Metal Fabrication. If you have any questions or require any additional information, please contact me at 919.859.9987 or at prahn@watersedgeenv.com. Sincerely, WATERS EDGE ENVIRONMENTAL, LLC _;�. 2� /1' Phillip L. Rahn President CC: NCDENR Stormwater (two copies) l 5-062/PLR/aht My.. • �. -` _ `�\ e �� '4'�- �+ Wti} "• � o a x feel 49 dr � f• 4��/ 5 ❑ 3 Z` X_�Z \ 1 o Cat asin 4ti . qamq- h Basin Aft r 40 IPA ~Catch B _ 1 Job No. Image/Photo Dare Title Site & Surrounding Properties Map WATERS ED6E ENVIRONMENTAL, LLC R11-47 Davidson Co. GIS 10.27.2011 File Name Figure Scale Project Matcor SPPP R1147.x1s 2 unknown Welcome, North Carolina APPENDIX A RECEIVED JUL 15 2015 Stormwater Discharge Outfall (SDO) CENTRAL FILES Qualitative Monitoring Report DWR SECTION For guidance onfrlling out thisform, please visit: htto://h2o.enr.state.nc.us/su/Forms_ Documents.htm#miscforms Permit No.: I N I C I G[ 0 13 I 0[ 0 10 1 4 1 or Certificate of Coverage No.: I N I C I G 10 13 10 16 I 1 13 Facility Name: Matcor Metal Fabrication County: Davidson Inspector: Thomas Haynes Date of Inspection: 6.9.15 Time of Inspection: 15:30 Total Event Precipitation (inches): 0.59 Phone No. 336,731.5742 Was this a Representative Storm Event? (See information below) ® Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, 1 certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1 Outfall Description: Outfall No. 001/002 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Unnamed Tributary of Swearing Creek Describe the industrial activities that occur within the outfall drainage area: Metal Fabrication 2 Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Liaht brown Page] of 2 S W U-242-112608 3 Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): - No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: iO 2 3 4 5 5 Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2O 3 4 5 6 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 O2 3 4 5 7 Is there any foam in the stormwater discharge? Yes No 8 Is there an oil sheen in the stormwater discharge? Yes No 9 Is there evidence of erosion or deposition at the outfall? Yes No 10 Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S WU-242-1 12608 SI I' M�4 TS EDGEENVIRONMENTAL. LLC �Jo1 WATERS EDGE DRIVE, SUkTE 201 • RALEIGH, NC 27$06 • PHONE 919,859,9987 • FAX 919.859.9930 November 11. 2014 Mr. Joe Edwards, EHS Officer Matcor Metal Fabrication 835 Salem Road Welcome, North Carolina 27374 RECEIVED CENTRAL FILES DWR SECTION Reference: Stormwater Discharge Outfall Qualitative Monitoring Report and Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication- Year 2- Period 2- July -December 2014 Welcome, North Carolina Waters Edge Job No RI 1-47 Dear Mr. Edwards: Waters Edge Environmental, LLC (Waters Edge) is pleased to provide two copies of the Year 2- Period 2 (July -December 2014) 2014 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome, North Carolina (see Figures 1 and 2). We have completed the Discharge Outfall Qualitative Monitoring Report, Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A). Laboratory analytical results are documented in Appendix B. Based on these results, we have exceedances for the following: • Outfall001 1. Exceedance for copper which was detected at 0.0152 mg/L versus a benchmark at 0.007 mg/L. 2. Exceedance for zinc which was detected at 0.840 mg/L versus a benchmark at 0.067 mg/L. Outfall002 1. Exceedance for zinc which was detected at 0.720 mg/L versus a benchmark at 0.067 mg/L. Based on the permit conditions, we will conduct a Tier 1 inspection of the facility. Any action items which will be reviewed and potential deficiencies addressed. The Tier 1 response will be recorded in the Stormwater Pollution Prevention Plan. Again, as detailed in earlier reports, due to the lowered benchmark thresholds resulting in benchmark exceedances, we previously sampled an upgradient surface water stream on the site (upgradient lake drive) as well as two samples collected from the roof drains. While there were no exceedances for copper, both roof drain samples exceeded the zinc benchmark level at 0.067 mg/L (Root 1 at 1.9 mg/L, and Roof-2 at 0.23 mg/L). The background upgradient surface water samples were below both the copper and zinc benchmarks. Based on these results. we would conclude the following: Stornnvater Discharge Monitoring Report and Tier 1 Response Year 2- Period 2 — July -Dec 2014 Mateor Metal Fabrications Welcome, NC Page 2 of 2 November IL 2014 • Metals are present in the upgradient surface water sample at the facility. Even though they are below the copper and zinc benchmarks, these metals are still present and can potentially be a constituting factor to the outfall values detected. • Zinc contained in the building materials or downspouts are also contributing to the zinc in the stormwater which would have nothing to do with the industrial activity at the site. While we will continue to attempt to improve the stormwater quality at the facility, we believe that these type of metals exceedances are largely due to non -industrial sources and can be found in a wide variety of non -industrial settings (e.g. residential or any structures with metal components). Nonetheless, we do understand that this exceedance will result in a Tier 7 response requiring monthly sampling for both Outfalls. Waters Edge appreciates this opportunity to work with Matcor Metal Fabrication. if you have any questions or require any additional information, please contact me at 919.859.9987 or at prahn@watersedgeenv.com. Sincerely, WATERS EDGE ENVIRONMENTAL, LLC Phillip L. Rahn President CC: NCDENR Stormwater (two copies) 14-090/PLR/aht �` ' ! h�: �_ i `` l '� „�� • �� ! CIF ' • in i tt ( •'�. � ,r•] n _ f a V L � Ir � y�� •--� � tee, } `. r + f / � - i 1 • SITE, �, '. -f rat Ierf t 1Til f Job No. Tam Quart Date yule Project Location Map �TERSEDGE ENVIRONMENTAL, LLC R11-47 Welcome 1.19.2012 File home Figure Scale Project Matcor SPPP R11r47.xls I unknown Welcome, North Carolina ®Ca asin ■ �jrlk t-'"f y tch Basin t } , , Catch Bas Job No. Image Phato Date Title Site &Surrounding Properties Map l J WAI RS LDCiE E NI VIR0N..V1EN l AL, LLC RI1-47 WvKisan Co. GIS 10.27.2011 File Name Figure scale Project Mntcor SPPP kI I47.xls 2 unknown Welcome. North Carolina Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 11.7.14 CERTIFICATE OF COVERAGE NO. NCG030613 FACILITY NAME _Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace Lab Cert. # _37706_ Comments on sample collection or analysis: None Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2014� SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ®ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other PI:EASE REMEMM0 t0 SIGN ON PAGES Z Ai bl6fi 3 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/w) 24-hour rainfall amount, lnches3 Total Suspended Solids PH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks =__> - - 100 mg/L or 50 mg/0 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 10/15/14 0.76 9.6 6.31 0-0152 ND 0.940 ND NA 002 10/15/14 0.76 9.6 6.47 0.0062 ND 0.720 ND NA ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tunes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since fling the last discharge monitoring report. 1 further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name C/(Prin name) Title(Printtitle) dnature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, Way -must be reported in the format. "<XX mg L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or rer 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, a Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks _> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier z, or Titer 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS- SEE PERMIT PART iI SECTION 8. • 2 EXC£EDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3, HAS YOUR FACILITY HAD 4OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this AMR, including all ' No Discharge" reports, within 30 days of receipt of the lab results for at, end of monitoring period in the case o "No Dischar e" re orts to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YQU-MUST 519IN THIS CERIVIC6110N FOR 6N,jr iNFORMATIONREPO ; "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations_" of Permittee) Permit Date:11/1/2012-10/31/2017 l/ iv —f tf p5te) SWU-245, last revised 10/25/2012 Page 3 of 3 0 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on frlting out ihis form, please visit: http://h2o.enr.state.ne.us/su/Fonns Docuinents.1-itni;4m iscforms Permit No.: L N! C; GI 0 3 1 0 1 0► 01 0 1 or Certificate of Coverage No.: I N 1 C I G j 01310; 6 1 11 3 Facility Name: Matcor Metal Fabrication County- Davidson Inspector: Thomas Haynes Date of Inspection: 10.15.14 Time of Inspection. 10:30 Total Event Precipitation (inches): 0.76 Phone No. 336.731.5742 Was this a Representative Storm Event? (See information below) ® Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is--.........-.r -event that p a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) I Outfall Description: Outfall No. 001/002 Structure (pipe, ditch, etc.) Pi Receiving Stream: Unnamed Tributary of Swearing Creek Describe the industrial activities that occur within the outfall drainage area: Metal Fabrication 2 Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Lioht brown Pagel of 2 S WU-242-112608 3 Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.). No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 O 3 4 5 5 Floating Solids: Choose the number which best describes the amount of floating solids in the stonnwater discharge, where I is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy I () 3 4 5 7 Is there any foam in the stormwater discharge? Yes No 8 is there an oil sheen in the stormwater discharge? Yes No 9 Is there evidence of erosion or deposition at the outfail? Yes No 10 Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S WU-242- I t 2608 Pace Analytical Sorvlces, Inc. acer��+n /� I % �+ J 205 East Meadow Road - Suite A G ,r' lafj�/fr<I��1:•, j A - Eden,:NC 2728e yviviuptce,'ahs;aorrr, t - r Oddil ','24,' 2014: Mr.-Phii.. lin.;. 1 a. ' Waters l=dge Ehvieonmental ,4901.;Water.VEdge3Drioe Suite.201 Raleigh 'NCr27606ti • RE:,. Project:.MATGOR�R ! =47 E _ A ;Pace.Project92221551 ` f Dear W.,Rahn' T Encloseli are th-e.-analytical results for sample(§);;received by the laboratory on October 15, 2b.14. The resultsi,relate only to the samples included. in this report. Results reported - herein conform to the . most currant TNl.standards and the laboratory's Quality Assurance Manual, where applicable, unless .,otherwise noted �injhe body of the report. Analyses were•performed at the Pace Analytical Services location indicated on the sample .analyte page for analysis unlessotherwise footnoted. If you have•any questions concerning this report, please feel free to contact me. Sincerely, Terri'Page• - . . - - terri.page@pacelabs.com Project Manager Enclosures 1 NI REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Page 1.0f 15 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A aceAnal .6cal 4 r t aen:`ive 2728e_ wwkmmdabs-mm i336}623 BS21 CERTIFICATIONS W Project: MATCOR R11-47 Pace Project*.: 92221551 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginlaNELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FioridaiNELAP Certification #. E87648 South Carolina Certification #: 99030001 Massachusetts Certification #, M-NC030 West Vlrginla Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 Eden Certification IDs 205 East Meadow Road Suite A, Eden, INC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 633 VirainiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 15 Pace Analytical Servlces, Inc. e 205 East Meadow Road - Suite A aceAnalyicalo Eden, NC 27268' ' ivwst'. celabs.aom (336)62M921 SAMPLE SUMMARY Project: - 4 '. , _MfATCOR R1147 Pace Project W: .92221551 Lab ID Sample ID Matrix Date Collected Date Received 92221551001 Ot3TFALL 001 Water 10/15/14 10:00 10/15/14 15:55 92221561002 OUTFALL 002 Water 10/15/14 10:15 10/15/14 15:65 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 15 ,. Pace Analytical Servlcea, Inc. aceAnalX cal 206 East Meadow Road - Suite A _. _. _:. Eden;NC 27288 wwwpacedabs mm ._"'b(336)623=8921 ' SAMPLE'ANALY.TE COUNT Project: MATCOR R11-47 Pace Project No.:,92221551 Anatytes Lab ID Sample ID Method Analysts Reported . Laboratory _ 92221551001 OUTFALL 001 SM 25400 CHM 1 PASI-E EPA 16648 CIN 1 PASI-C EPA200.7 JMW' 28 PASI-A 92221551002 OUTFALL 002 SM 2540D CHM 1 PASI-E EPA 1664B CLW 1 PASI-C EPA200.7 JMW 28 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, without the written consent of Pace Analytical Services, Inc.. Page 4 of 15 Pace Analytical Services, Inc. 205 east Meadovr Road - Sulte A 11a'ceAnalXicalo F-den, NC 27288 ANALYTICAL`RESULTS . Project: +",MATCOR R11-47. - Pace Project No.: 92221651 Sample: OUTFALL 001 Lab tD: 92221551001 Collected: 10/16/14 10:00 Received: 10/15/14 15:55 Matrix: Water Report Parameters Results Units Limit MOIL OF Prepared Analyzed CAS No. Qua] 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 9.6 mg1L 2.6 2.6 1 10/17/14 08:55 HEM, Oil and Grease Analytical Method: EPA 1664B Offand Grease ND mg/L 5-0 1.1 1 10121114 0&50 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA200.7 Aluminum 235 ug/L 100 50.0 1 . 10/17/14 15:15 10/22/14 23:13 7429.90-5 Antimony 5.8 ug1L 5.0 3.9 1 10/17114 15:15 10/22/14 23:13 T440.36-0 Arsenic NO ug11- 10.0 5.0 1 10/17/14 15:15 10/22/14 23:13 7440-30 Barium 21.1 ug/L 5.0 2.5 1 10/17/14 15:15 10122114 23:13 7440.39-3 Beryllium NO ug/L 1.0 0.050 1 10117/14 15:15 10122/1423:13 7440.41-7 Boron ND ug/L 50.0 25.0 1 10/17/14 15:15 10122/14 23.13 7440.42-6 Cadmium ND ug/L 1.0 0.50 1 10117/14 15:15 10/22/14 23:13 7440-43-9 Calcium 3970 ug/L 100 50.0 1 10/17/14 15:15 10/22/14 23:13 7440-70-2 Chromium ND ugiL 5.0 2.5 1 1011711415:15 10/22/14 23:13 7440-47-3 Cobalt ND ug1L 5.0 2.5 1 10/17/14 115:15 10/22/14 23:13 7440-444 Copper 15.2 ug[L 5.0 2.5. 1 10/17/14 15:15 10/22/14'23:13- 7440.50-8- Iron 302 ug1L 50.0 25.0 1 10/17/14 15:15 10/22/14 23:13 7439-89-6 Lead ND ug/L 5.0' 2.5 1 10/17/14 15:15 10/22/14 23:13 7439.92-1 Magnesium 406 ug l- 100 $0.0 1 10/17/14 15:15 10/22114 23:13 7439-95-4 Manganese 6.7 ug/L 5.0 2.5 1 10/17/14 1515 10122/14 23:13 7439-96-5 Molybdenum NO ug/L 5.0 2.5 1 10117114 15:15 10122/14 23:13 7439-98-7 Nickel NO ugiL 5.0 2.5 1 10/17/14 15:15 10/22/14 23:13 7440-02.0 Potassium NO ug/L 5000 2500 1 10/17/14 15:15 10/22/14 23:13 7440-09-7 Selenium NO ug/L 10.0 5.0 1 10/17114,15:15 10/22/14 23:13 7782-49-2 Silicon 1300 ug/L 100 • 50.0 1 10/17114 15:15 10/22/14 23A3 7440-21.3 Silver NO ug/L 5.0 2.5 1 10/17/14 15:15 10122/.14 23:13 7440.22-4 Sodium NO ug/L 5000 2500 1 10/17/14 15:15 10/22/14 2313 7440.23-5 Strontium 26.5 ug/L 5.0 2.5 1 10/17/14 15:15 10/22114 23:13 7440-24-6 Thallium ND ug/L 10-0 5.0 1 10117/14 15:15 10i22114 23:13 7440-28-0 Tin ND ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:13 7440-31-5 Titanium 5.8 ug/L 5.0 2:5 1 10/17/14 15:15 10/22/14 23:13 7440-32-6 Vanadium ND ug/L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:13 7440-62-2 Zinc .840 ug/L 10.0 2.5 1 10/17/14 15:15 10/22/14 23:13 7440-66-6 Sample: OUTFALL 002 Lab ID: $2221551002 Collected: 10/15/14 10:15 Received: 10/15/14 15:55 Matrix: Water Parameters 2540D Total Suspended Solids Total Suspended Solids HEM, Oil and Grease Oil and Grease Report Results Units Limit Analytical Method: SM 2540D 9.6 mg/L 2.5 Analytical Method: EPA 1664B MOL OF Prepared Analyzed CAS No. Qua] 2.5 1 10/17/14 08:50 ND mg/L 5.0 1.1 REPORT OF LABORATORY ANALYSIS 10121/14 08.50 This report shall not be reproduced, except in full, Date: 10124/2014 09:32 AM without the written consent of Pace Analytical Services, Inc., Page 5 of 15 Pace Analytical Services, Inc. ® 205 East Meadow Road - Suite A 11eAnalytiical Eden. NC 27288 www.pso0abs.com - (336)623-89211 ANALYTICAL RESULTS Project: MATCOR R11-47 Pace Project No.:, 92221551 Sample: OUTFALL 002 Lab ID: 92221551002 Collected: 10/15/14 10:15 Received: 10/15/14 15:55. ,Matrix: Water - Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS ND. Qual 200.7 MET ICP Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum Nickel Potassium Selenium Silicon Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc Date: 10/24/2014 09:32 AM Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 943 ug1L 100 50.0 1 10117114 15:15 1012211423:16. 7429-90+5 - ND ug1L 5.0 3.9 1 10/17/14 15:15 10/22/14 23:16 .7440-36-0 ND ug1L 10.0 5.0 1 10/17/14 15:15 10/22/14 23:16 7440-38-2 69.0 ug1L 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7440-39-3 ND ug1L 1.0 ' 0.050 1 10/17/14 1 5: 15.10/22114 23-.16. ,7440-41-7 64.1 ug1L 50:0 25.0 1 10/17/14 15:15 10/22/14 23:16 7440-42-8 ND 41- 1.0 0.50 1 10/17/14 15:15 _ 10/22/14 23:16 :7440-43-9 ' 13700 uglL 100 50.0 1 10/17/14 15:15 10/22/14 23:16';,.7440-70-2 NDuglL 5.0 2.5 1 10/17/14 15:15 10/22/14 2316 7440-47-3 ND -uglL 5.0 2.5 1 10/47/14 15:15 10/22/14 2316 7440-48-4 6.2 uglL 5.0 •` 2.5 1 10/17/14 15:15 10122114.23:16 7440-50-8 983 uglL 50.0 25.0 1 1011711415:15 10122114'23:16 7439-89-6 ND ug1L 5.0 2.5 1 10/17/14 15A5 10/22/14 23:16 7439-92-1 1160 ugll- 100 50.0 1 10/17/14 15:15 10/22/14 23:16 7439-95r4 19.3 ug1L 5.0 2.5 1 10117/1415:15 10122/14,23:16 7439-96-5 ND uglL 5.0 2.5 1 10/17/14 15:15 10/22/14 23:16 7439-98-7 ND ug1L 5.0 2.5 -"' 1 10/17/14 15:15 10/2211423:16 7440-02-0 ND uglL 5000 `..` 2500 1 10/17/14 15:15 10/22/14 23:16 7440-06-T ND ug1L 10.0 5.0 1 10/17/14 15:15 10/22/14 23:16 7782-49-2 3030 ug1L 100 50A 1 10117/14 15:15 10122/14 23:16 7440-21.3 ND uglL 5.0 2.5 1 10/17/14 15:15 1012211423:16 7440-22.4 - 5400 ug1L 5000 2500 1 1011711415:15 1012211423:16 7.440-23-5 63.4 ug1L 5.0 2.5 1 i 0li 7l14.15:15 i 0122114 23:16 7440; 24-6 ND uglL 10.0 5.0 1 10/17/14 15:15 10/22/.14 23:16 7440-28-0 -ND uglL 5.0 2.5 1 10/1711415:15 10/2211423:16 7440-31-5 24.6 ug1L 5.0 2.5 1 1011711415:15 10122/14,23;16 7440-32-6 .: ND ug1L 5.0 2.5 1 10/17/14 16:15 10122/14 23:16 7440-62-2 720 ug1L 10.0 2.5 1 10/17/14 15:15 10122114.23:16 7446-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,' except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 15 accAnapical o I tvwwpat�lahs.cvrrr QUALITY CONTROL DATA Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: MATCOR R11-47 Pace Project No.: 92221551 QC Batch: EDEN116110 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92221551001, 92221551002 METHOD BLANK: 1309366 Matrix: Water Associated Lab Samples: 92221551001, 92221551002 Blank Reporting: Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 10/17/14 08:52 LABORATORY CONTROL SAMPLE: 1309367 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 260 240 96 90-110 SAMPLE DUPLICATE: 1309368 . 92221535001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 55.7 56.1 1 10 SAMPLE DUPLICATE: 1309369 92221714001 Dup Max Parameter Units Result ' Result RPD RPD Qualifiers Total Suspended Solids mg/L 102 90.8 12 10 D6 neeutta presented on this page are In the units Indicated by the "Units" column except where an alternate unit is preserded to the right of the nesuit REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 09:32 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 15 11ce Analytical wm4.AacelaCs.mm QUALITY CONTROL DATA. Project: MATCOR R11-47 Pace Project No.: 92221551 QC Batch: GCSV119242 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Latr Samples: 92221551001, 92221551002 METHOD BLANK: 1311267 Matrix: Water Associated Lab Samples: 92221551001, 92221551002 r Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 1 OY21114 08:50 Pace Analytical Services, Inc. 205 fast Meadow Road - Suite A Eden, NC 27288 (336)623-8921 LABORATORY CONTROL SAMPLE: 1311268 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 37.8 94 78-114 MATRIX SPIKE SAMPLE: 1311269 92222103001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L <5.0 40 36.6 92 78-114 Results presented an this page are In the units indicated by the "Units" column except where an alternate unit in presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full. Date: 10/24/2014 09:32 AM without the written consent of Pace Anaiyllcal Services, Inc.. Page 8 of 15 Pace Analytical &ertrices, Inc. 205 East Meadow Road - Suite A 11!;aneAnaVica1* Eden, NC 27288 - (336)623-8921 i 'QUALITY-GONTROL DATA' ' Project: MATCOR R41-47 Pace Project No,:. 9222155 E QC Batch: MPRP117151 Analysis Method: EPA 200.7 QC Batch Method: EPA200.7 Analysis Description: 200-7 MET Associated Lab Samples: 92221551001, 92221551002 ; METHOD BLANK: 1309860 Matrix: Water Associated Lab Samples:- 9.2221551001, 92221551002 Blank Reporting Parameter Units - Result Limit Analyzed Qualifiers Antimony ugfL NO 5.0 10/22/14 22:48 Arsenic. ug/L NO 10,0 10/22/14 22:46 Beryllium ug/L NO : 1.0 10122J14 22:48 Cadmium ug/L NO 1.0 10/22/14 22:48 Calcium ug/L NO too 1022114 22A8 Chromium ug/L ND 5.0 10122/14 22:48 Copper ugfL NO.', . 5.0 1022/1422A8 Lead ug/L NO 5,0 1022114 22A8 Magnesium ug/L ND 100 1022114 22:46 Nickel uglL NO 5.0 10/22/14 22A8 Selenium ug/L NO 10.0 10/22114 22--48 Silver ug/L NO 5.0 1022114 22:48 Thallium ug/L NO 10.0 10/22/14 22:48 Zinc° ug/L NO 10.0' 10/22/14 22:48 LABORATORY CONTROL SAMPLE: 1309861 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug1L 500 464 93 85-115 Arsenic ug/L 500 440 88 65-115 Beryllium ug/L 500 430 86 85-115 Cadmium ug/L '500 431 86 85-115 ` Calcium ugfL - 5006 4520 90 85-115 Chromium ug/L 500 426 86 85-115 Copper 6g/L 500 441 88 85-115 Lead ug/L 500 441 88 85-115 Magnesium ug(L 5000 4680 94 '85-115 , Nickel, ug/L 500 435 67 85-115 Selenium ug/L 500 445 89 85.115 Silver . ug1L 250 233 93 85-115 Thallium ug1L 500 436 87 85-115 Zinc ug/L 500 471 94 85.115 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1309862 1309863 MS MSD _ - 92221547001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Conti. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND ' • 500 500 472 460 94 92 . 70-130 •3 20 Results presented on this page are In the units Indicated by the"Untta" column except where an aftemate unit Is, presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/2412014 0912 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 15 ., Paca Analytical Services, Inc. 205 East Meadow Road - Suite'A aceAnalytica( Eden, NC 27298 wwwpapslahs.com (336)523-8921 i QUALITY CONTROL DATA Project: MATCOR R11-47 Pace Project No.: 92221551 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1309862 1309863 MS MSD 92221547001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Arsenic uglL NO 500 500 446 435 88 86. 70-130 2' 20 Beryllium uglL ND 500 500 434 426 87 85' 70-130 2 20'. Cadmium uglL NO 500 500 438 424 88 85 70-130 3 20 Calcium ug/L 3.1 mglL 5000 5000 7590 7350 90 86 70-130 3 20 Chromium uglL NO 500 500 438 423 87 84 70-130 3 20 Copper uglL 0,0067 500 500 458. 442 90 87 "° 70-130 —4 20 mg1L Lead ug/L NO 500 500 446- 430 89 86 70-130 -4 20 . Magnesium uglL 0.60 mg[L 5000 5000 5410 5210 96 92 70-130 • 4 .20 Nickel uglL NO 500 500 442 428 88 85 70-130 3 ' 20 Selenium ug1L NO 500 .500 458 438 91 87 70-130 4 20 Silver ugk NO 250 250 238 230 95 92 70-130 3 20 Thallium uglL NO 500 500 442 431 86 86 70-130 ..3 20 Zinc ug/L 0.059 500 500 490 473 86 83 70-1130 4 20 mglL MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1309864 1309865 MS MSD 92221690005 Spike Spike MS MSD MS - MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L NO 500 500 473 486 94 97 70-130 .3 20 Arsenic uglL NO 500 500 442 457 88 91 70-130 3 20 Beryllium uglL NO 500 500 440 461 88 92 70-130. 5 20 Cadmium uglL NO '500 500 438 451 88 90 707130 3 20 Calcium ug/L 1370 5000 5000 5960 6190 92 96 70-130 4 20 Chromium ug/L ND 500 500 441 461 88 92, 70-130 4 20 Copper ug1L NO 500 500 453 472 90 93 70-130 4 20 Lead ug/L NO 500 500 444 455 89 91 70-130 2 20 Magnesium uglL 270 5000 5000 5050 5230 95 99 " 70-130 3 20 Nickel uglL NO Soo 500 442 461 88 92 70-130 4 20 Selenium ug/L ND 500 600 451 459 90 92 70-130. 2 20 Silver uglL ND 250 250 237 240 95 96 70-130 1 20 Thallium uglL ND 500 500 440 449 87 89 70-130 2 20 Zinc uglL 97.4 500 500 524 544. 85 89 70-130 - 4 , 20 Results presented an this page are In the units Indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 09:32 AM without the written consent of Pace Analytical Services, Inc - Page 10 of 15 L a r aI"Analytical �� wwwpacelabs.cam f QUALIFIERS Project: MATCOR R11-47 Pace Project No.: 92221551 DEFINITIONS Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 2T288 (336)623-8921 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. ' PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration, Acid preservation may not be appropriate for 2-Chloroethylvinyl ether. Styrene, and Vinyl chloride. Pace Analytical is TNI accredited_ Contact your Pace PM for the current list of accredited anatytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PAST-C Pace Analyticai Services - Charlotte PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS 06 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full. Date: 10/24/2014 09:32 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 15 /IceAnaWical' Km .pacelabs.com 1 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project:. MATCOR R11-47 Pace Project No.: 92221551 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92221551001 OUTFALL 001 SM 2540D EDEN116110 92221551002 OUTFALL 002 SM 2540D EDEN116110 92221551001 OUTFALL 001 EPA 16646 GCSV119242 92221551002 OUTFALL 002 EPA 1664B GCSV/19242 92221551001 OUTFALL 001 EPA 200.7 MPRP117151 EPA 200.7 92221551002 OUTFALL 002 EPA 200.7 MPRP/17151 EPA 200.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 09:32 AM without the written consent of Pace Analytical Services, Inc.. ICPI I5462 ICPIi 5462 Page 12 of 15 1�2ceAnal J` trwr.paselah.core CHAIN -OF -CUSTODY I Analytical. Request Document The Chain -of -Custody is a LEGAL DOCUMENT. AD felevent fields must be completed eccumt iy. Section A Section B Section C �• of Required Criont Information: Required Project Inf6tration: IrnoNa Irdonnatlon: Corrlpany: Report To: - Attention: 1810515 w Address: `mac C- Copy To: _ , Coapany Nerno: !-AG_ ENCY _REGULAfdi ; 7 N3 DES ' r' GROUNDWATER j- OR NKING WATER � UST J"" RCRA -OTHER Era11To: erPtrchmOrderNo: r f� f'xaQwOs � Reference: Phone: Fax Project Name: Pew Prolod- IRrolod Mar�ar- C� R nested Due DatefTAT: wsrarE NumberPaw PmFle p: --N ;^ Requested Ariai"ir , : a 3ectbn D Matrix Codes . z Re"redCllent lnkm4fion MATRIX l COFJE COLLECTED P/85E15rdt11R3S Drinking Wa%K DW n 0 Water WT V -: Waste Water ww Product P m RT r3fART ENafsw S.RfSo0.d SL p r C SAMPLEID Wipe — " � W _ WP (A-Z, 0-9 f ,-1 Ak AR W ' C a Z'f�, Sample IDs MUST BE UNIQUE Tissue TS V Other OT X r 0 M O -,:a R i� F a2� ILL, O a p vi r a� 'a: . 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Yea'C1No MNtA' complt@t►cewE��iAr�acor�mertdatlgr�, - . .lita�5ufi�eti�'' MOM 22 E5 M, 0A •DRO htje gyp 0% ; f �� � : A .�'f; • ..:'f ' $ 198.�clG9d r. deahfQftnatlQaS':' • •' ''I3Y ' CINe' � • Y�' ., "' � .. � . ' • Heedse�rii�i:Vfals` asil4i ti = ;. :.':; 'wA .t 17tp.8r�nk Pr enf:• PYas,ElNa . NSA 10 17Yos" t jS Blanc Giltody SSTs t?it cxo (v,4 r�plm.Tro t3rik t.l c9ptHo#itoetlon! Rpulattan: Meld Data Repm? :y::'t •; N , Pemon Oontected, , • #gat r e. 4':. ConunenW ftoldon. VURf'�8i�9Vlf: r. .iQlalw• s !�• :'a :iw - _ Flai 61 1 p SRO+ tROVI9W: • Oates.: a t� t • , k Nod Whenever there Is a dtsprepAMY oM"..., esttrplee, a wpy of thisform WILE be sent 6t€te, Not Qw4rra t3R E Eandwrtte ro age 15 of i 5 Oeriklodon Offlos { f e out of hofd, Uwrreat ervative, oaEot trip; Ef no- [OW available Inoorraot containers) LE WATER$ EDGE ENVIRONMENTAL, LLC + 7 4 1 WATERS EDGE DRIVE, Sum 201 • RALEIGH, NG 27606 . PHONE 919.859.9987 . FAX 919.859 9930 July 2, 2014 RECEIVED Mr. Joe Edwards, EHS Officer JUL 10 ZQIq Matcor Metal Fabrication CENTRAL FILes 835 Salem Road DWO/BOG Welcome, North Carolina 27374 Reference: Stormwater Discharge Outfall Qualitative Monitoring Report and Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication- Year 2- Period 1- Jan -June 2014 Welcome. North Carolina Waters Edge Job No Rl 1-47 Dear Mr. Edwards: Waters Edge Environmental, LLC (Waters Edge) is pleased to provide two copies of the Year 2- Period 1 (Jan- June 2014) 2014 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome, North Carolina (see Figures 1 and 2). We have completed the Discharge Outfall Qualitative Monitoring Report. Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A). Laboratory analytical results are documented in Appendix B. Based on these results, we have exceedances for the following: • Outfall001 i . Exceedance for total suspended solids (TSS) which was detected at 167 mg/L versus a benchmark at 100 mg/L. 2. Exceedance for copper which was detected at 0.0104 mg/L versus a benchmark at 0.007 mg/L. 3. Exceedance for zinc which was detected at 0.212 mg/L versus a benchmark at 0.067 mg/L. • Outfall002 1. Exceedance for total suspended solids (TSS) which was detected at 181 mg/L versus a benchmark at 100 mg/L. 2. Exceedance for copper which was detected at 0.0115 mg/L versus a benchmark at 0.007 mg/L. 3. Exceedance for zinc which was detected at 0.233 mg/L versus a benchmark at 0.067 mg/L. Based on the permit conditions, we will conduct a Tier 1 inspection of the facility. Any action items which will be reviewed and potential deficiencies addressed. The Tier 1 response will be recorded in the Stormwater Pollution Prevention Plan. Due to the lowered benchmark thresholds resulting in benchmark exceedances, we previously sampled an upgradient surface water stream on the site (upgradient lake drive) as well as two Stormu,ater Discharge Monitoring Report and Tier 1 Response Year 1- Period — July -Dec 2013 Matcor Metal Fabrication Welcome, _'VC Page 2 of 2 ATovember 8, 2013 samples collected from the roof drains. While there were no exceedances for copper, both roof drain samples exceeded the zinc benchmark level at 0.067 mg/L (Roof-1 at 1.9 mg/L, and Roof-2 at 0.23 mg/L). The background upgradient surface water samples were below both the copper and zinc benchmarks. Based on these results, we would conclude the following: * Metals are present in the upgradient surface water sample at the facility. Even though they are below the copper and zinc benchmarks, these metals are still present and can potentially be a constituting factor to the outfall values detected. • Zinc contained in the building; materials or downspouts are also contributing to the zinc in the stormwater which would have nothing to do with the industrial activity at the site. While we will continue to attempt to improve the stormwater quality at the facility, we believe that these type of metals exceedances are largely due to non -industrial sources and can be found in a wide variety of non -industrial settings (e.g. residential or any structures with metal components). Nonetheless; we do understand that this exceedance will result in a Tier 2 response requiring monthly sampling for both Outfalls. Waters Edge appreciates this opportunity to work with Matcor Metal Fabrication. If you have any questions or require any additional information, please contact me at 919.859.9987 or at prahn@watersedgeenv.com. watersedgeenv.com. Sincerely, WATERS EDGE ENVIRONMENTAL, LLC Phillip L. Rahn President CC: NCDENR Stormwater (two copies) 14-061 /PLRJaht eu1103eJ 41JON'atua012M umouyun I slx'Lir101 dddsMew isafosd mass al►*j awaNal& dew uoi;ewl pafoad ZIOZ 6Il awoalaM LIrI Is 31 1 `'1 lN9Wi 0X[ANH 3DG9 S1191 M al1�L arnU -10L 'ON Qof .i✓��."! ram` ; i � r ��•- f r V0. /j w '■ R jj -- � -- _ ■ � �� � ,� ,gyp � r • 1 - i, t ■ ■ t� ^ `• r« IP sir �. • i.i t .• • ' ' r °, �� dINCb • - — OS elm It 00C Catch Jab No. IniagelPhoto Date Tale MkAkTERS EDGE ENVIRONMENTAL, LLC R1 147 Davidson Co. GIS 10.27-2011 Site & Surrounding Properties Map File Name Figure Scale Project Matcor SPPP RI 147.xls 2 unknown Welcome, North Carolina Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 7.2.14 CERTIFICATE OF COVERAGE NO. NCG030613 FACILITY NAME _Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace Lab Cert. # _37706— Comments on sample collection or analysis: None Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2014_ SAMPLE PERIOD ® Jan -June July -Dec or 0 Monthly' (month) DISCHARGING TO CLASS NORW [:]HQW Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 E No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks ===> - - 100 mg/L or 50 mg/O 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 6/25/14 0.24 167 6.4 0.0104 ND 0.212 ND NA 002 6/25/14 0.24 181 6.51 0.0115 ND 0.233 ND NA ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) ,Ir,` �f S ar _u Ftc� Title (Print title) 3gnature) (Date) Note. Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B s see General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: 1f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera! Permit text FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. O 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. o TIER3- HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL. OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one cony of this DMR includingall "No Discharge" reports _ within 30 days of receipt of the lob results (ar at end of monitoring period in the curse of "No Discharge" reruorts) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Ybu MUST SIGN THIS,CERTIFICATION•FOR NY INFORMATION REFORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: httn://h2o.enr.state.ne.us/sulForms_Documents.htm#migforms. Permit No.: IN I C I GI 0 13 10 10 10 10 1 or Certificate of Coverage No.: I N I C I G 10 13 10 16 11 13 Facility Name: Matcor Metal Fabrication County: Davidson Phone No. 336,731.5742 Inspector: Thomas Haynes Date of Inspection: 6.25.14 Time of Inspection: 10:30 Total Event Precipitation (inches): 0.24 Was this a Representative Storm Event? (See information below) ® Yes [] No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). j A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that � I is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) A 2KZ I Outfall Description: Outfall No. 001/002 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Unnamed Tributaryof Swearing Creek Describe the industrial activities that occur within the outfali drainage area: Metal Fabrication 2 Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Light brown Page I of 2 S W U-242-1 12608 3 Odor: Describe any distinct odors that the discharge may have (i.e.. smells strongly of oil, weak chlorine odor, etc.): No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 2 3 4 5 5 Floating Solids: Choose the number which best describes the amount of floating solids in the stonnwater discharge, where I is no solids and 5 is the surface covered with floating solids: `..`J 2 3 4 5 6 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is eytremely muddy: 1 3 4 5 7 Is there any foam in the stormwater discharge? Yes No 8 Is there an oil sheen in the stormwater discharge? Yes No 9 Is there evidence of erosion or deposition at the outfalI? Yes Na 10 Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S WU-242-1 12608 aceAn#1j&af ® w w.pacalaftoxn July 01, 2014 Mr. Phil,Rahn Waters Edge Environmental 4901` Water"s Edge Drive Suite 201 - Raleigh, NC 27606 RE:' .Project: MATCOR Rll-47 Pace Project No.: 92206995 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Dei aii" lr. Rahn: Enclosed are the analyticalresults for sample(s) received by the laboratory on -June 26, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page:for analysis.unless otherwise footnoted. If.you have'any questions concerning this report, please feel free to contact me. Sincerely, \Au - Terri Page terri.page@pacelabs.com Project Manager Enclosures Q&C gg�R_Atp�j , REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc., Page 1 of 13 ace A. nalytical m w.paaelaf* wm i 1 ' CERTIFICATIONS Project: MATCOR R11-47 Pace.Project No.: 92206995 Charlotte Certification IDs 9800 KinceyAve. Ste 100, Huntersville, NC 25078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field.Services Certification #: 5342 West Virginia Certification C 357 North Carolina Wastewater Certification M 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 Pace Analytkal Services, Inc, 205 East M096 w Road - Suite A Eden, NC 27288 (336)623-8921 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida7NEt.AP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222 Eden Certification lDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 13 _ 1_ aceA�aiytical f wnw.pecQ1m.wm SAMPLE SUMMARY Project: MATCOR R1147 Pace Project No.: 92206995 Lab ID Sample ID Matrix Date Collected Date Received 92206995001 92206995002 OUTFALL 001 OUTFALL 002 Water Water 06/25/14 19:00 06/25/14 19:15 06/26/14 15:40 06/26/14 15:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-892 t Page 3 of 13 _r aceAnalytica!a wmpacefabs.cam I SAMPLE ANALYTE COUNT Project: MATCOR Rll-47 Pace Project No.: 92206995 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-a921 Lab ID Sample Ili Method Ana"ts Analytes Reported Laboratory 92206995001 OUTFALL 001 SM 2540D CHM 1 PASI-E EPA 1664E CLW 1 PASI-C EPA 200.7 JMW 3 PASI-A 92206995002 OUTFALL 002 SM 2540D CHM 1 PASI-E EPA 1664E CLW 1 PASI-C EPA200.7 JMW 3 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 13 acmnalytreal wwwpsmWxs.cam i - I ANALYTICAL RESULTS Project: MATCOR R11-47 Pace Project No,: 92206995 Pate Analytical Services, Ina. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Sample: OUTFALL 001 Lab ID: 92206995001 Collected: 06125/14 19:00 Received: 06/26114 15:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua] 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 167 mg1L 83 8.3 1 06/30/14 10:25 R1 HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mglL 5.0 1.1 1 07/01/14 07A1 200.7 MET ICP Analytical Method: EPA 2001 Preparation Method: EPA 200.7 Copper 10-4 ug/L 5.0 0.30 1 06►28/14 15:35 06/30/14 15.11 7440-50-8 Lead ND mg/L 0,0060 0.0040 1 06►28114 15:35 06/30114 15:11 7439-92-1 Zinc 212 ug/L 10.0 0.40 1 06/28114 15:35 06/30114 1511 7440-66-6 Sample; QUTFALL 002 Lab ID: 92206995002 Collected: 06125/14 19:15 Received: 06/26/14 15:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 181 mg/L 8.1 8.1 1 06/30/14 10:25 HEM; OII and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1.1 1 07/01/14 07:42 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 11.5 ug/L 5.0 0.30 1 06/28/14 15:35 06/30/14 15:24 7440-50-8 Lead ND mgfL 0.0050 0.0040 1 06128/14 15.35 06/30114 16:24 7439-92-1 zinc 233 ug/L 10.0 0.40 1 OW8114 15:35 06130/1415:24 7440-66-6 Date: 07/01/2014 04:16 PM REPORT OF -LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 13 aceAnalytical g r www,jrece?sDs.cam I QUALITY CONTROL DATA Project: MATCOR R11-47 Pace Project No.: 92206995 QC Batch; EDEN114991 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92206995001, 92206995002 METHOD BLANK: 1232214 Associated Lab Samples: 92206995001, 92206995002 Parameter Units Total Suspended Solids mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 06/3011410:22 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 272B8 (336)623-8921 LABORATORY CONTROL SAMPLE: 1232215 Spike LCS LCS % Rec, Parameter Units Cone, Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 254 102 60-120 SAMPLE DUPLICATE: 1232217 92206986001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total suspended Solids mg1L 212 333 44 10 R1 SAMPLE DUPLICATE: 1232774 92206995001 Dup Max Parameter Units Result Result RPD RPD Qualifiers ToW Suspended Solids mg1L 167 204 20 10 R1 Results presented on this page are In the units Indicated by the "Unite" column except where en ettemate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/01/2014 04:16 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 13 /JceAnalytical' www.psaaJabs.com I QUALITY CONTROL DATA Project: MATCOR R11-47 Pace Project No.: 92206995 Pate Anttlyt "i Sarvkes, Inc. 205 East Meadow Roast - Suite A Eden, NC 27288 (336)623-8921 QC Batch: GCSV118083 Analysis Method: . EPA 16648 QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92206995001, 92206995002 METHOD BLANK: 1232689 Matrix: Water Associated Lab Samples: 92206995001, 92206995002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 07/01/14 07:34 LABORATORY CONTROL SAMPLE: 1232690 Spike LCS LCS % Rec Parameter Units Cone. _Result % Rec Limits Qualifiers Oil and Grease mg/L 40 38.6 96 78-114 MATRIX SPIKE SAMPLE: 1232691 922069620b1 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL ND 40 36.7 90 78-114 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is preserrted to the right or the reaull REPORT OFIABORATORY ANALYSIS This report Shall not be reproduced, except in full. Date: 07/01 /2014 04:16 PM without the written consent of Pace Analytical Services, Inc., Page 7 of 13 1_�aceAnalytieal a 1 w� wwwpece/atxsoam 1 QUALITY CONTROL DATA Project: MATCOR R11-47 Pace Project No_: 92206995 OC Batch: MPRP116337 Analysis Method: EPA 200.7 QC Batch Method: EPA200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92206995001, 92206996002 METHOD BLANK: 1231956 Associatedtab Samples: 92206995001, 92206995002 Parameter Units Copper ug1L Lead mg1L Zinc ug/L Matrix: Water Blank Reporting Resutt Limit Analyzed Qualifiers ND 5.0 06/30/14 14:22 ND 0,0050 06130/141412 ND 10.0 06130/1414:22 Pace Analytical Service., Inc. 205 East Meadow Road - Suite A Eden, NC 272ea (330)G23-8921 LABORATORY CONTROL SAMPLE: 1231957 Spike LCS LCS % Rec Parameter Units Corte.- Result %Rec Limits Ouatifiers Copper ugtL 500 613 103 85-115 Lead mg/L .5 0.49 97 85-115 zinc ug1L 500 462 92 85-115 MATRIX SPIKE &'MATRIX SPIKE DUPLICATE: 1231958 1231959 MS MSD 92207182013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD RPD Quai Copper. ug1L ND 500 500 511 510 102 101 70-130 0 20 Lead mg1L ND .5 .5 0.47 0.47 94 94 70-130 0 20 Zinc ug1L 119 500 . 500 572 572 91 91 70-130 0 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1231950 1231961 MS MSD 92206995002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Resutt Cane. Cone. Result Result % Rec % Rec Limits RPD RPD Qual Copper ug1L 11.5 500 500 519 519 102 101 70-130 0 20 Lead mg1 ND .5 .5 - 0.48 0.47 94 94 70-130 0 20 Zinc ug1L 233 600 500 684 683 90 90 70-130 0 20 Results presented on this page are in the units indicated by the'UrdW column except when an attertuts unit Is presented to the rSpffl of the resulL REPORT OF LABORATORY ANALYSIS ' This report shall not be reproduced, except in full, Date: 07/01/2014 04:16 PM without the written consent of Pace Analytical Services, Inc.. ar. Page 8 of 13 _ aceAnalytical www.p&c&1ab&wm j QUALIFIERS Project: MATCOR R11-47 Pace Project No.: 92206995 DEFINITIONS Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 DF'- Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. c S - Surrogate 1,2-Diphenylhydrazine (8270listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG -. Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. LOD - Limit of Detection. LOQ - Limit of Quantitation. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-At. Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/01/2014 04:16 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 13 _ 2ceAnalyfical" I www.psceleb3ma Project: MATCOR R1147 PaCe Project No.: 92206995 � . x Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALITY CONTROL DATA CROSS REFERENCE TABLE Anatytical Lab Ili Sample ID QC Batch Method QC Batch Analytical Method Batch 92206995001 OUTFALL 001 SM 2540D EDEN114991 92206995002 OUTFALL 002 SM 2540D EDENl14991 92266995001 OUTFALL 001 EPA 1664B GCSVf18083 92206995002 OUTFALL 002 EPA 1664B GCSVI18083 92206995001 OUTFALL 001 EPA200.7 MPRP116337 EPA200.7 ICPl14763 92206995002. OUTFALL 002 EPA200.7 MPRP116337 EPA200.7 ICP114763 Date: 07/0112014 04:16 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 13 �.! i ts*r,pacslaps-CIID 'dam CHAIN -OF -CUSTODY 1 Analytical Request Document The Chalnot-Custody is a LEGAL DOCUMENT. An relavant fields must be completed accurately. r Paw: of r SecSbn A Section B Section C Required Cgent Info,,, " Company Requlrvd Projad �nfar-,ado,: Report To III Ilfomw r,: lion: 1725671 Address. Copy To: t Company Name:- - REGULATORYAGENCYw�, j'rsi'1 UT, 5.�:_4.;da �?Y3 Address' r NPDES GROUNDWATER r' DRINKING WATER .- _ r UST r RCRA f� DTIiER Email jv X A.J Purchase Order No,: _ PaOe QLCe nererence: Fax: Project Name: r Pam Manager' --: 5tteLjlOi1 *;4 t -nut, 1 dnjx of '� ?i 1.` t_ r - 5 ��.�itF JR7".-tad Due 6DteITAT: Project Number. Pace Prutae a: _ .[ "fi - tr 12equested,AnalWi FUtered {'Ylk yd lIx Irtl x - } Section D IAatrlz Codes FbgW edClentlnforridlon MATRIiC! CODE s COLLECTED Preservatives a•.! ',"+`,?A.� 5'.Iti� i,�` ,-:l _ ``' Drinking Water DW ti Wastewater WW Product P y2 ¢ rz Couvos 11. srritr coruPOStTE ENo+Crtne U ;>- t�� `�1 - _ Z / C (�✓) Soinobd SL L) SAMPLE ID (A-Z OX OL Wipe WP Nr AR C ui 01 i4 t� SampAr IDa MUST BE UN10UE TLssue T$ O Ot er OT X Ll q 7, J a Ll J aLL U N © ¢ O O �p O — DATE TIME DATE TIME y � 2 x S z z 2 O ' Pace Project NoJ Lab LD. {/ [( Thy �2_ htl^. J 1i' »fie '4'•: 5 . s r ADOlf10NALCOMY�NTS s REUN[1Ut5HEnaYfAFFIWTglF a �- OATE ~ 1151E ACCFP�FD•BYlAFFG11►710M DA7E� TAIE.': SAMPLE CONDITIONS r 07 &AMpLERNAHIE'ANDSICsNAjI1RE - t ` x C .. -.. .. ` ORIGINAL. PRINTNameofSANPLER:r-. SAMPLER. a 8 ��� SIGNATURE of SAMPLER:(1,1My)pgtyyj;ned DATE ~ TL E 'a I •tmponnnt Note- by sIgNng fits Tam you are accapling Pace's NET 30 day prn—t temp ana agm&V to late tharpas Df 1.5%Per month DClrq k..ic. not p®Id wltl dayw % t F-ALL-0-020rev.07, 15-May-2007 26e na;�ica I*. 'CHAIN-OF=CUSTODY I Analytical Request Document T7 a Chaln-d-Custody is.a LEGAL DOCUMENT. All YiHovant tielde must be completed accumtefy :. Saetlon A Sacdon 9 Sec@on C ' Raqulnd C erd 1 rfn madon[. _R�qukad Pmj0CtW _+M*0 '. Irnrobrs lrYarrnatlon . ' CompenY Report Tlx AttentWnc 7 //� �y adaresg: Go" TM � � Company �.. AJY -- _L� ,:•?Y':"t. rs..9i.. .o-..� 3:4";r3zF Address: NPDES C GROUND WRIER (" DRINKING WATER r" LIST i" RCRA `% OTHER EmeliTo Purchase Order No.: Pew Quot. rtet�a,ce: Phone:,. •. FeX - Project Name: _ .Paco PtpJdd' Manager Site Locat[on ;f S7A /1 r r a # k �, Requeai4d Due DatelTAT:" Pplect Num"r Paae Pmde O ., y� a; ..r, n.• . ,R _Requested Analysts Ftitered'(YINj�`�"*`,,. '�y F, I �; ,; „ I5, r r�k 3sa t Section D . • . Matrix Codes RegvindCtienr rnlormelbn' .' MATRIX !'CODE"' o COLLECTEt? ' ' 'Preservalnres '. y q Donking Water - DW z s= Water W7 - Wastewater' WW Product P ' SoWSokd SL $ s; O correoerrE ' • START - •cnra - . 9."GRA8 _ _ U `� F 1' a w• - Z .. - SAMPLE ID oa : OL (A-�Z.O-91.).- '_AAiirr. AR - -d a Z_ Fm• '. 1 .... _ SarnPle Me MUST 8E UNIQUE Tissue TS O a _ W LL,P O - DATE TIME nAiE ; . Pace Project Mal Lab ID. }- 5,.J. R yA IftON�L"LQiOYIElifi k:� RE[jk6atliSlif DBYJ7it?t?IILITION i 4DATE- 7pHE , =•AGCr 1�..BYIAFF/LIATION- x DATE'P_L� $Alkik C a 44, NAME AND t.. w i ..,.: ..1 .. '+w :.I L'v t �f1V :�Iy'�•`� - Y 9. :�W��f V � .� PRINT Name o1 SAMPLER:,:.. CD • , - QQj•• SAMPLER: � DATE Signed .SIGNATURE of //77 .(MMlDOIYY):. it .. 'aiportant Note: By e%Fkp this torso you are aaeptinQ PaceY NET 30 day paynlant tMRli and ayreainp totate thargee of 1:5% Per month,%r any linrotcea not paldQays.., . [ F•Ai.L•Q-020feV.07. 15-h1aJF2tK1T' F. - Document Names Sample Condltlori.Upon Document Revl§ed: Mar+ 13, 2013 rAnal ices!' -Recel t SCUIT Page 1 oft Issuing Auftioil%s. . "^ F-EDN-CS-003-mv,09 . Pace Eden Qualu o floe Client Name. Where Received: ❑ Nuntersvllle ❑Asheville 5den elg� Courier (circie): Fed Fx TIPS USPS + n Commerclai Pace Other Pacidng Material: bubble Wrap ❑Bubble BagsA Nona [] Other Themtometer Used: IN Gun ED007 Type of Ice:. a Blue Norte samples ah'Ice, cooltng [mom hss begwt Tema Coniatlon Factor. Add I Subtract .0 Corrected CbOfetTemp.; C Biblogtcal Tissue Is Frroien:'Yee 'w WA Temp shatdd be.abow freezing to s' C .. •Commonts: Pants: of n i✓hain of sto .Present:. a, ©No OWA 1. Chaln of Filled Out: os. QNo OWA 2. Chaln cf Cu Retin fished; .. • ea 17Na OWA 3. . Sam let name & SI nature on COO: P7w ONo- OWA q., - . t344;e Wi feed wfthln Hold Finer_ es ONO •©WA 5; Shock Fiold.T me Aria sis (<724:. i]vse , ©No .. A g, Flush'Tirhkqund "rn6Requested: ClYee ❑ko. V4 7, 8Ufff0IWv01UntA::. • Yes. 11W QWA $,:.. , Cow Containers Used: Yes ❑No DIVA -hooContainers Used: fdYas ❑No . ©WA 9; Containerslntact:: ae ONo.. ❑WA 10. I'ilterad valufrie received for [)issolved tests No A 11. &le Lebels.matah coc:_ as. ❑No ❑NIA 4noludesdatelme=Analysis Matri • �� 12. All oorm nm needing pMervalion Imve been eheoked. O [3No . CJWA All containers needing prosarvation are found to be In 11 0No OWA mm*nc�with EPA reoommendii,,W.f"- VOA, oogoan, i'OC, O&G. WI-DRO (water'] ❑Yee ❑No . 1& tnttial when od feted Samples ahaftd for deohlorination: is faro!:.❑wA 14; Heads ceInVOAWls(>13rn ,};" ❑Yoa .lallo A 1fa. Tdp alark pmsent ❑Yes ONO 17A Tftp Blank Custody Seals Fresent 17Yes 0No E]/ A Two Trip l3larilc I:ot # (if urohasectj: 16. . Client NatiticaSon! Ftesoh{':or: Field DataRequfred? Y f' N Comments/ Resolution: SCURF Review: �; j Datei Place label here . . SRF Review: Date: OR Note: Whenever:there is a discropWr:,y affecting north n aO lianoe `¢aieow,a cojVot this ton; �,vill I;a sent to the i�arth Gar Tina D h1R Cerdfloadan Offices ( Le ou: I L:•.i, incorrect pre8erv0A Out of temp, Handwrite project number irmrrec! containers) (If no label available),.. Page 3 of 13 Semi-annual Stormwater Discharge Monitoring Revort for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 11.8.13 CERTIFICATE OF COVERAGE No. NCG030613 FACILITY NAME _Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace_ Lab Cert. # _37706_ Comments on sample collection or analysis: None Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR �2013� SAMPLE PERIOD ❑ Jan -June ® Ju[y-Dec or ❑ Monthly' !_ (monthl DISCHARGING TO CLASS ®ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA []Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --> ❑ No discharge this period?2 44 f`,•"itii:?w . � 4tN ... „n='-" ,.�'w°� .ysr „�.;, � :'�' �), w J;• �:".n..t:.<1 i �-i _ �v,1-' Date Sam ie,- 24'hour rainfall ... Yotal:5upended - Total -Toxic ��Collected Solids= ,, ,Coppr.;.. � � �,,tled F. Zinc. �Toia1 Petraleurt3 . :s- .s. .. Y un •,��.::'� - .,._ drotarbors ...... l.r :..'. ... r;; .,:.r h., ,'J "�-..: .:..t ..-.�.:� r•Yr •.:.. .l�:li•ff< - � -�:.� -:�:�� `f�• :s't - �.r_•a.- 'f _',-� Benchmarks > •' : r'lrµ iD0 mg/L or 5i} mg/L � 5 0 '9 d f 0.007 mg/Lfi4S"t x0:03 mgf L �.c�owst�l-r 0 067 rng{L �5 mg/L 1 rng/L ,..,.-�s.<.:rn.wisk.,. '`^:' :.. ..._.:• ..-'�,�.r_,r'L .. -" .: ..I .. .:.•...... �.esrw-��sz.: r ...-- .. ^a i.., � -- .-niL _ 001 10/7/13 0.86 23.9 6.3 0.021 ND 0.42 ND NA 002 10/7/13 0.86 23.0 6.3 0.006 ND 0.38 ND NA Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites maybe eligible for a waiver of the rain gauge requirement. See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines forthe facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 -r�•4•oert^:-.�-•-.., a.,.,�;;..y.�..r.__.r w � �^-----^••r—.. ......... ..... .... ..... .. .,. .... _.. .._._._.._._..._--..-..-._, .. ._ - -_. -..... .... � nrlr ...... . « ... _.. ........ ... .._,........ .. :.. „.. .... .... M...,: «..... .. Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for 170 monitoring may he waived, The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions ofthe solvent management plan included in the Stormwater Pollution Prevention Plan." Name ((Print name) Ld t{_� COOr �of TiiCe (Print title) nature) (Date) Opl Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, the must be reported in the format, ,•`<XX mslV where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note., if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. D No discharge this periodr'2 3 Date sample 24'hotir rainfall S r Outfall No ` eallected' '_ "+ Non=polar O&G/TPH by_ _ a; tr amount s Total Suspended Solids �, % EPA 1664 a 11 .Inches [SGT;HE r{ 8ertthmaiks > �r�, °° ws a: :15 mg/L`' =:'1Q0 mg/L or SO mglt*`i { 6 0 9 0 SO Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012_-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 IE Note. if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: o A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. Y 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on ina! and one cop o this DM(?, includin all "Na Dlschar e" re arts within 30 da s o rece! t p the lab results or at end o manitorin eriad in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YQU MIDST SIGN THIS CERTIFICATION FOR Ably INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. i am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ature of Permittee} Permit Date: 11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stolrmwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 6.28.13 CERTIFICATE OF COVERAGE NO. NCG030613 FACILITY NAME _Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes LABORATORY Pace— Lab Cert. # _37706_ Comments on sample collection or analysis: None Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2013 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly' month DISCHARGING TO CLASS ®ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow []Water Supply []SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks =__> _ - 100 mg/L or 50 mg/0 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 06/17/13 0.13 ND 7.13 0.0096 ND 0.271 ND NA 002 06/17/13 0.13 73 7.07 0.0011 ND 0.314 ND NA 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you -must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. ' Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31), Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX m L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, IncheS3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 ,' Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: a A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. 0 2 EXCEEDANCES 1N A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. + TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Marl an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date:11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3of3 �✓�% �TERSEDG ENVIRONMENTAL, LLC 01 WATERS EDGE DRIVE, SUITE 201 • RALEIGH, NC 27606 • PHONE 919.859.9987 • FAX 919.859.9930 KR21onpa January 18, 2012 Mr. Joe Edwards. ENS Officer Matcor Metal Fabrication 835 Salem Road Welcome, North Carolina 27374 Reference: Stormwater Discharge Outfall Qualitative Monitoring Report and Stormwater Discharge Outfall Monitoring Reports Matcor Metal Fabrication ' Welcome, North Carolina Waters Edge Job No R11-47 _ Dear Mr. Edwards: Waters Edge Environmental, LLC (Waters Edge) is pleased to provide two copies of the Fall 2011 forms for the semi-annual site inspections at the Matcor Metal Fabrication facility located in Welcome, North Carolina. We have completed the Discharge Outfall Qualitative Monitoring Report. Waters Edge also performed the stormwater sampling and have filled out the Stormwater Discharge Outfall Monitoring Report (both report included in Appendix A). Laboratory analytical results are documented in Appendix B. Based on the TSS exceedances above the benchmark value in your permit, you are required to submit a stormwater management inspection within two weeks to identify potential causes of the exceedances and then implement corrections within two months which is all recorded on your Stormwater PPP. Waters Edge appreciates this opportunity to work with Matcor Metal Fabrication. If you have any questions or require any additional information, please contact me at 919.859.9987 or at prahn@watersedgeenv.com. Sincerely, WATERS EDGE ENVIRONMENTAL, LLC RECEIVED `.' JAN 2 7 2012 Phillip L. Rahn ,f CEi ITRAL FILES President A�;� DWQ/BQQ l "- 1 2-002/PLR/aht �:�'� j i4�d�1 .- fi F-r STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG0300000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2011 CERTIFICATE OF COVERAGE NO. NCG030613 (This monitoring report is due at the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Matcor Metal Fabrication COUNTY Davidson PERSON COLLECTING SAMPLES T. Haynes PHONE NO 336.731.5742 CERTIFIED LABORATORY Face Lab #>' 37706. Lab # PLEASE SIGN ON THE REVERSE4 Part A: Vehicle Maintenance Areas Monitoring Requirements Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor.oil per month? yes ✓ no (if yes, report your analytical results in the table immediately below) 4utfa1l Date '' Q0530, 00400,00SS6 Total Siis entletitSolid[ .k "7' i \,; * H r '!�. , i�!"Y. r. % ��(; :(i�l and`Grease'?, - fTo#a� Tox:c'Qr am �' - No' xSsmple'�Cotlecteci :Al` 3 .f� J n'-:.'•.'',• �:,: ---':Mg-/L, ����t �...:5tandardtunits :� •�nl ::,�:=��,�,�:_ , >�„xt;C�.4..4~m n "S sue' r' ti k., Y ,,� 1'00,�:3D�_ ::>s'�:i`. .`' 4.: %�:•L!':4:: ;C2.�. ?: �.. ;Benchmark fi h 001 12.27.11 179 6.6 N❑ N/A Note: if you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier I or Tier 2 responses. See General Perutit text. Dart R- C)il/watPr CenarAtnm And'Srenndary C'nntninment Areas nt Petrntenm Bulk Statinns and Terminals �,� Outfali. � Y�°Date ,� �` �:. � , 'DOSSS' ; � � .� <,� � k 5,;° ,�•.,,",Q0534 fi n � �•^� , 00400 ;�`;,.�� Nevw.�Vl6tnr 0i1'Usa e ;�� NA STORM EVENT CHARACTERISTICS: Date 12.27.11 (first event sampled) Total Event Precipitation (inches): 0,60 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Mail Original and one copy to: Division of Water Quality Attn: DWQ Central Fifes 1617 Mail Service Center Raleigh, North Carolina 27699-1617 S WU-250-102107 Page I of 2 "I certify, under penalty of law, that this document and all attachments were prepared under my direction► or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee) (Date) SWU-250-I 02107 Page 2 of 2 �3 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report IFor guidance on filling, out this form, please visit: htip:/lh2o_enr.state.nc.as/su/Forms Documents. htm#miscforms Permit No.: I N; CI G' 01 3 01 0101 01 or Certificate of Coverage No.: I N C 1 G 0 ', 3 0 6 1 1 3 Facility Name: Matcor Metal Fabrication County: Davidson Phone No. 336.731.5742 Inspector: Thomas Haynes Date of Inspection: 12,27.11 Time of Inspection: 09:30 Total Event Precipitation (inches): 0.60, Was this a Representative Storm Event?(See infonnation below) ® Yes ❑No IPlease check your permit to verb if Qualitative Monitoring must be performed during a representalive storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. j By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) ' 1 Outfall Description: Outfall No. 001 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Unnamed Tributary of Swearing Creek Describe the industrial activities that occur within the outfall drainage area: Metal Fabrication 1 2 Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, (lark) as descriptors: ' Light brown ePage 1 of 2 SWU-242-1 12608 3 Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): No odor noted 4 Clarity: Choose the number which best describes the clarity of the discharge, where l is clear and 5 is very cloudy: 1 0 3 4 5 5 Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where l is no solids and 5 is the surface covered with floating solids: O 2 3 4 5 6 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 0 3 4 5 7 Is there any foam in the stormwater discharge? Yes No g is there an oil sheen in the stormwater discharge? Yes 9 is there evidence of erosion or deposition at the outfall? Yes 10 Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S WU-242-112608 . aceAnalyti+caf .•:�vwwpeeefe6s.00m January'05, 2012 Mr. Phil Rahn Waters Edge Environmental 4901 Water's Edge rive Suite 201 Raleigh, NC 27606 Pace Analytical 5ervices, Inc. 21)5 East Meadow Road - Suite A Eden, NO 27288 (338)823-8921 RE: Project: Matcor=Matsu R11-47 Pace Project No.: 92109205 Pace Analytical Servkaa, Inc. 2225 Riverside Dr. Asheville, NO 28804 (828)254a176 PaceAnalytical Services; Inc. 9800 KinceyAye., suite 100 Huntersville, NO 28078 (704)875-9092 Dear Mr. Rahn: Enclosed are the analytical results for sample(s) received by the laboratory on December-27; 2011:. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the'bbdy of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample,analyte,, ;,,, page for analysis unless otherwise footnoted. Report re -issued on January 5, 2012 with corrected metals compound list. If you have any questioris concerning this report, please feel free to contact me. Sincerely, 1 4 Charles Hardin for Bonnie McKee bonnie.mcicee@paceiabs.com Project Manager Enclosures pccR�p� REPORT OF LABORATORY ANALYSIS Page 1 of 11 This report shall not be reproduced, except in full, s without the written consent of Pace Analytical Services, Inc- ..-. aceAnafytical WW..Pacafabs.= Project: Matcor-Matsu R11-47 Pace Project No.: 92109205 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, H u ntersvi Ile, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Virginia Drinking Water Certification #: 00213 Asheville Certificatfon IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Eden Certification IDS M East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 633 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (82B)254-7176 CERTIFICATIONS Connecticut Certification #: PH-0104 FloridalNELAP Certification #: E87627 Kentucky LIST Certification #: 84 Louisiana DHH Drinking Water # LA i00031 West Vrgfnia Certification #: 357 VirginiaNELAP Certification #: 460144 South Carolina Certification #: 99030001 Virginia Certification #: 00072 West Virginia Certification #: 356 VrginaNELAP Certification #: 460147 Virginia Drinking Water Certification #: 00424 VrginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, lac. ' 9800 KineeyAve. Suite 100 Huntersville, INC 28078 (704)875-9092 1 1 Q Page 2 of 11 aC6A'nafY cal ' sri4WPS6al9J'3.MT 1 Project: Matcor-Matsu R11-47 Pace Project No.: 92109205 Lab 10. Samplo ID 92109206001 O utfa l l 001 i 1 1 - 1 r Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Fden, 127288 (336)623-8921 Pace Analytical Servlces, Inc, 2225 Rivarslde Dr. Asheville, 1 28804 (828)254-7176 SAMPLE SUMMARY Pace Analytical Services, Inc. 9800 Kincey Are, Suite 100 Hunternville, NC 28078 (704)875-9092 Matrix Date Collected Date Received water 1212711112:00 12127/1116:03 ' • 'I li ' r •! i . 3 '. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of i.1 aceAnalytical wwwpacefahscam Project: Matcor-Matsu R11 -47 Pace Project No.: 92109205 Lab ID Sample ID 92109205001 O utfall 001 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Sden, NC 27288 (336)623.6921 Pace Analytical Services, I 2225 Riverside Asheville, NC 28 . (828)254-7 SAMPLE ANALYTE COUNT Method SM 2540D EPA 9040 EPA1664A EPA 200.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. nc. Pace Analytical Services, Inc. ' Dr. 9800 KinceyAve. Suite 100 804 Huntersville, NC 28078 176 (704)875-9092 ' Analytes i Analysts Reported Laboratory CLM i PASi-E CLM 1 PAS!-E AM 1 1 PASi-C JDA 1 PASI-A e 1 1 1 Page 4 of 11 1 A Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalyl�ical 205 East Meadow Road -Suite A 2225 Riverside Or 9800 Kincey Ave. Suite 100 �vwpacelab�c�n Eden, NC 27288 Asheville, NC 28804 Huntersvilte, NC 28078 ' (336)623-8921 (828)254-7176 (704 )875-9092 ANALYTICAL RESULTS Project: Matcor-Matsu R11-47 Pace Project No.: 92109205 ' Sample: Outfall 001 Lab ID: 92109205001 Collected: 12/27/11 12:00 Received: 12/27/11 16:03 Matrix: Water Report Parameters Results Units .;Limit MDL DF Prepared Analyzed ; CAS No.,'- Qual 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 179 mgfL 30.9 30.9 1 1228111 09:15 9040 pH Analytical Method: EPA 9040 ` PH 6.6 Sid. Units 0.10 0,10 1 12128111.13:00 H6 HEM, Oil and Grease Analytical Method: EPA 1664A Oil and Grease NO mg1L 6.0 1.1 1 01105112 08:39 200.7 MET ICP Lead Analytical Method: EPA200.7 Preparation Method: EPA 200.7 7.0 ug1L 5.0 4.0 1 12/30111 10:00 1213011.1 18:47 7439-92;i_. Date: 01/05/2012 03:50 PM REPORT OF LABORATORY ANALYSIS Page 5 of 11 ' This report shall not be reproduced, except in full, wittlout the written consent of Pace Analytical Services, Inc.. CBAnalyt►Cal� winepacelabs.cnm Project: Matcor-Matsu R11-47 Pace Project No-: 92109205 QC Batch: EDEN18291 QC Batch Method: SM 2540D Associated Lab Samples: 92109205001 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids METHOD BLANK: 704728 Matrix: Water Associated Lab Samples: 92109205001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/28/11 08:57 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 , 1 s LABORATORY CONTROL SAMPLE: 704729 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers , Total Suspended Solids mg/L 250 254 102 80-120 SAMPLE DUPLICATE: 704730 ' 92109203001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids rrig/L 151 184 20 10 SAMPLE DUPLICATE: 704731 3 92109205001 Dup Max- e Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mgfL 179 179 0 10 Date: 01/0512012 03:50 PM REPORT OF LABORATORY ANALYSIS Page 6 of 11 This report shall not be reproduced, except in Tull, r without the written consent of Pace Analytical Services. Inc.. aceAnalytrcal ' wlvw.patelahs.com Project: Matcor-Matsu R11-47 Pace Project No.: 92109205 Pace Analytical Sarvleea, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QC Batch: EDENIB292 QC Batch Method: EPA 9040 Associated Lab Samples: 92109205001 SAMPLE DUPLiCAM 704882 Parameter Units pH Std. Units e 1 Date: 01/05/2012 03:50 PM Paco Analytical5ervicea, Inc. 2225 Riverside Dr, Asheville, NC 26804 (828)254-7 9 76 QUALITY CONTROL DATA Analysis Method: EPA 9040 Analysis Description: 9040 pH EDEN Pace Analytical SaMces, Inc. 9800 KinoeyAve. Suite l00 Hunteraville, NC 28076 (704)875-9092 92109205001 Dup Max Result Result RPD RPD Qualifiers ' 6.6 7.0 6 20 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc., Page 7 of 11 aceAnalytical Kw,vp�aelabscam Project: Matcor-Matsu R11-47 Pace Project No.: 92109205 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Or. Eden. NC 27288 Asheville, NC 28804 (336)623.8921 (828)254-7176 QC Batch: GCSV/11156 QC Batch Method: EPA 1564A Associated Lab Samples: 92109205001 METHOD BLANK: 706709 Associated Lab Samples: 92109205001 Parameter Units Oil and Grease mg/L LABORATORY CONTROL SAMPLE: 706710 Parameter Units Oil and Grease mg/L MATRIX SPIKE SAMPLE: 706711 Parameter Units Oil and Grease mg/L Date, 01/05/2012 03:50 PM QUALITY CONTROL DATA Analysis Method: EPA 1664A Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 5.0 01/05/12 08:37 ' Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 ' 1 Spike LCS LCS °% Rec Conc. Result °% Rec Limits Qualifiers 40 36.0 90 78-114 , ' °% 9210945400.1 Spike MS MS Rec Result Conc. Result °% Rec Limits Qualifiers NO 44.9 39.2 87 78-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ' ® Pace Analytical Services, Inc. Pace Anatytical Services, Inc. aceAnalytrcal 205 East Meadow Road - Suite A 2225 Riverside Dr. waN pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: Matcor-Matsu Rll-47 Pace Project No.: 92109205 ■ QC Batch: MPRP19671 QC Batch Method: EPA 200.7 Associated Lab Samples: 92109205001 METHOD BLANK: 705601 Associated Lab Samples: 121092050111 Parameter Units Lead uglL LABORATORY CONTROL SAMPLE: 705602 ' Parameter Units Lead ug1L ' MATRIX SPIKE SAMPLE: 705603 Parameter Units Lead ug1L MATRIX SPIKE SAMPLE: 705605 eParameter Units Lead uglL SAMPLE DUPLICATE: 705604 Parameter Units Lead uglL Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/30/11 16:56 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 1 o0 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 500 492 98 85-115 92109234001 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers NO 500 406 81 70-130 92109246008 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers ND 500 462 92 . 70-130 92109238001 Dup Result Result RPD ND ND SAMPLE DUPLICATE: 705606 , - 92109246009 Dup Parameter Units Result Result RPD Lead uglL ND ND 1 , ' Date: 01/05/2012 03:50 PM REPORT OF LABORATORY ANALYSIS This report shot) not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Max RPD Qualifiers 20 Max RPD Qualifiers 20 al Page 9 of 11 a0Arralytical ~'Pacelebacom Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALIFIERS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ' Pace Analytical Services, Inc. 9800 Kinoey Ave. suite 100 Huntersville, NC 28078 (704)875-9092 ' Project: Matcor-Matsu R11-47 Pace Project No.: 92109205 DEFINITIONS ' DF - Dilution Factor, if reported, represents,the factor applied.to the reported data due to changes in sample preparation; dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted, method detection limit and below the adjusted reporting limit. „ MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. ' SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. ' Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden e ANALYTE QUALIFIERS H6 Analysis initiated more than 15 minutes after sample collection. ' Date: 01/05/2012 03:50 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, tnc.. Page 10 of 11 aceAnalytical NM'v �peCe19b5.4orn Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 1 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Matcor-Matsu R11-47 Pace Project No.: 92109205 Lab ID Sample ID 92109205001 Outfall 001 92109205001 Outfall 001 92109205001 92109205001 Outfal l 001 Outfal 1001 1 e ' Date: 01/05/2012 03:50 PM Pace Analytical Services, Inc. 9800 KinceyAve, Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical QC Batch Method QC Batch Analytical Method Batch SM 25400 EDENl8291 EPA 9040 EDEN18292 EPA 1664A GCSVII1156 EPA 200.7 MPRPl9671 EPA 200.7 &/P 932 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc., Page 11 of 11