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NCG030548_COMPLETE FILE - HISTORICAL_20180119
STORMWATER DIVI5IDN CODING SHEET NCG PERMITS PERMIT NO. V DOC TYPE l HISTORICAL FILE ❑ MONITORING REPORTS DOC DATE ❑ a b I ! YYYYM M DD ® WE1L-McLAIN 523 New Street • Eden, NC 27288 Tel: (336) 627-6037 • Fax: (336) 627-6075 January 10, 2018 Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Dear Sir or Madam: RFr`;=ll/FD JAN 19�0;8 Wfi0RM,4T ON PRXESSING UNIT In accordance with NPDES (NCG030000) Stormwater Permit we are submitting our TTO statement for the 2"d half of 2017. After communication with Glen White at the Winston-Salem Regional office, it was determined that with the elimination of an outdoor storage area we would me the requirements for the No Exposure Certification from the North Carolina Division of Energy, Mineral, and Land Resources Stormwater Permit. We have made the necessary adjustments and submitted that application to the Stormawater Permitting Program office. If you have any questions or comments regarding the enclosed reports, please contact me at {336} 627-6015 N us- 03015_q� Sincerely, eFiddens�d� � Compliance Manager Eden, NC Facility TTO Certification Statement Period July 2017 — December 2017 Based on my inquiry of the person or persons directly responsible for managing compliance with the permit limitation for Total Toxic Organics (TTO), I certify to the best of my knowledge and belief, no leak, no spill, or no dumping of concentrated toxic organics into the stormwater or onto areas which are exposed to rainfall or stormwater runoff has occurred since filing of the last monitoring report. I further certify that this facility is implementing all of the provisions of the Solvent Management Plan included in the Stormwater Pollution Prevention Plan. Date/0- -�Zz--W Tc Energy, Mineral & Land Resources ENVIRONMENTAL QUALITY Melinda Smith, EHS Specialist 523 New Street Eden, NC 27288 Subject: Technical Assistance Permit No. NCG 030548 Weil -McLain Rockingham County Dear Ms. Smith: August 15, 2016 PAT McCR,.O.RY .. Gowrnor DONALD R. VAN DER VAART Secretory TRACY DAVIS B[rector On August 5, 2016 Glen White and Sue White of the North Carolina Department of Environmental Quality; Department of Energy, Minerals, and Land Resources, met with you at the facility located at 523 S New Street in Eden. You had requested assistance with determination of Representative Outfalls (RO). The facility has thirteen (13) locations identified as outfalls on the SPPP. Each has an identifier label near it. Outfall 6 is currently RO for Outfalls 1 thru 5. You and the inspectors walked most of the site perimeter and observed outfalls. Many of them are located offsite. It was determined that offsite locations will need to be relocated to within the property boundary for safety of personnel and to eliminate liability issues. No offsite monitoring should be required. Outfalls can be determined by pouring non -toxic dye into grates and inlets upstream of the discharge points and seeing where the color discharges from the pipes. Site review also revealed that the only exposure this facility possesses is located in the storage area or boneyard located at the rear of the facility. if stored materials located in this area can be either, removed from the site or stored inside, possible exposures can be eliminated. The facility would qualify for "No Exposure Exclusion." This would eliminate the required SPPP and monitoring. Outfall determination would not be required. Please contact Glen White at 336-776-9660 if you need additional information or assistance. Sincerely, Matthew E. Gantt, P.E. Regional Engineer Land Quality Section Winston-Salem Regional Office State of North Carolina I Environmental Quality I Energy, Mineral and Land Resources Winston-Salem Regional 0ftlte 1450 Hanes NU Road, suite 30o I Winston-Salem, NC Z7103 336 776 9800 Enclosures: Inspection Report cc: file Copy Division of Energy, Mineral and Land Resources (WSRO) State of North CariAna I Environmental Quality I Energy, Mineral and Land Resources Winston-Salem Regional Office 1 450 Hanes Mi41 Road, Suite 300. 1 'Kinston-5aleh NC 27103 336 776 9800 Compliance Inspection Report Permit: NCG030548 Effective: 11/01/12 Expiration: 10/31/17 Ownei : Weil -McLain SOC: Effective: Expiratiom Facility: Weil -McLain County: Rockingham 523 S New St Region: Winston-Salem Eden NC 27288 Contact Person: Gary R Connor Title: Phone: 219-873-0392 Directions to Facility: System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): e On -Site Representative(s}: Related Permits: Inspection Date: 08/05/2016 EntryTime: 10:00AM Exit Time: 11:30AM Primary Inspector: Glen White Phone: 336-776-9800 Secondary Inspector(s): Reason for Inspection: Routine Inspection Type: Technical Assistance Permit Inspection Type: Metal Fabrication Stormwater Discharge COC Facility Status: ® Compliant Not Compliant Question Areas: Storm Water (See attachment summary) r Page: 1 Permit: NCG030548 owner- Facility; Weil -McLain Inspection Date: 08/0512016 Inspection Type: Technicai Assistance Reason for Visit: Routine Inspection Summary: (See Compliance Summary) Compliant. Page: 2 Permit: NCG030548 Owner - Facility: Weil -McLain Inspection Date: 0810512016 Inspection Type : Technical Assistance Reason for Visit: Routine Analytical Monitoring Has the facility conducted its Analytical monitoring? # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? Comment: Monitoring is beinq conducted as required. Permit and Outfalls # Is a copy of the Permit and the Certificate of Coverage available at the site? # Were all outfalls observed during the inspection? # If the facility has representative outfall status, is it properly documented by the Division? # Has the facility evaluated all illicit (non stormwater) discharges? Yes No NA NE ❑o■❑ Yes No NA NE !❑❑❑ ®❑❑❑ ® 110 ❑ ® ❑ ❑ ❑ Comment: Facilitv currentiv has RO Status (for 1 thru 51 at Outfall 6. Additional Outfalls will need to be dve tested at rates to determine new samlin_q locations. All monitoring current!y conducted offsite will need to stop. Outfalls are the location where stormwater leaves the property. This site appears that it will qualify for No -Exposure Exclusion to stormwater permitting if the bonevard at the rear of the property can be covered, removed from the site or moved to indoor locations. Exclusion would eliminate the annual fee and costly analytical monitoring. Owner is evaluating options. Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring semi-annually? ® ❑ ❑ ❑ Comment: No.deficieny noted. stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwater Pollution Prevention Plan? E ❑ ❑ ❑ # Does the Plan include a General Location (USGS) map? ® ❑ ❑ ❑ # Does the Plan include a "Narrative Description of Practices'? ® ❑ ❑ ❑ # Does the Plan include a deta0ad site map including outfall locations and drainage areas? ® ❑ ❑ ❑ # Does the Plan include a list of significant spills occurring during the past 3 years? ® ❑ ❑ ❑ # Has the facility evaluated feasible alternatives to current practices? ® ❑ ❑ ❑ # Does the facility provide all necessary secondary containment? ® ❑ ❑ ❑ # Does the Plan include a BMP summary? ® ❑ ❑ ❑ # Does the Plan include a Spill Prevention and Response Plan (SPRP)? ® ❑ ❑ ❑ # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? ® ❑ ❑ ❑ # Does the facility provide and document Employee Training? ■ ❑ ❑ ❑ # Does the Plan include a list of Responsible Party(s)? ® ❑ ❑ ❑ Page: 3 s7 Permit: NCG030548 Owner - Facility: Weil -McLain Inspection Date: 08/0512016 Inspection Type : Technical Assistance Reason for Visit: Routine Stormwater Pollution Prevention Plan Yes No NA NE # !s the Plan reviewed and updated annually? ® ❑ ❑ ❑ # Does the Plan include a Stormwater Facility Inspection Program? ® ❑ ❑ ❑ Has the Stormwater Pollution Prevention Plan been implemented? ® ❑ ❑ ❑ Comment: SPPP was reviewed and appears to be complete. Responsible party's has been updated and employee training has been conducted annually as required. No deficiency noted. Page: 4 A41Mm MCDEMR North Carolina Department of Environment and Natura Division of Water Quality Pat McCrory Thomas A. Reeder Governor Acting Director 11 June 2013 Melinda Roberts, Environmental Health and Safety Specialist Weil -McLain 523 South New Street Eden, North Carolina 27288 Subject: NPDES Stormwater Permit No. NCG030548 Representative Outfall Status Request Weil -McLain Rockingham County Dear Ms. Roberts: Resources John E. Skvarla, III Secretary The Winston-Salem Regional Office staff has reviewed your request received 10 June 2013 for determination that Outfall 6 be granted representative outfall status for Outfalls 1, Z 3, 4, & S. Based on Aana Taylor -Smith's site inspection on 20 May 2013, we are approving this request. In accordance with 40 CFR §122.21(g)(7), you are authorized to sample Outfall 6 as the representative outfall. This approval is effective with the next sampling event. However, this approval is contingent on the following requirements: (1) All outfalls, regardless of representative status, must have a cleared path and the right of way to the outfall must be properly maintained. (2) The permit still requires that Qualitative Monitoring be performed at all Stormwater Discharge Outfails, regardless of representative status. In addition, please remember that any actions you initiate in response to benchmark exceedences as directed in the tiered response provisions of your permit must address oil drainage areas represented by Outfall 6, where appropriate. The site drains to an unnamed tributary to the Dan River, this section of which is currently classified as Class C waters, in the Roanoke River Basin. Please append this letter to your Stormwater Pollution Prevention Plan or permit to document that representative outfall status has been approved. If changes in drainage areas, structures, processes, storage practices, or other activities occur that significantly alter the basis of this approval, representative outfall status may no longer be valid. You should either resume sampling at all storm water discharge outfalls, or reapply to this office for representative outfall.status.based on updated information,il � SUN : 6� L013 North Carolina Division of Water Ouaiiiy, WinstonSafem Regions! Office UVAIM - tayrau� " Location: 585 Waughtown St. Mnslon-Salem, North Carolina 27107 1�1[4`a�d' One �t, Phone: 336-771-50001 FAX: 336-771-46301 Customer Service: 1-877-623-6748 NofthCaxolina Internet: www.nrwaterquatity.org .V17h.lt'7111./ An Equal Opportunity 1 Affirmative Action Employer Weil McLain 06/11/2013 Page 2 of 2 If you have any questions or concerns concerning this letter and the attached report, please contact Ms. Taylor -Smith at (336) 771-4950 or at aana.tavlor-smith@ncdenuov. Sincerely, W. Corey Basinger Surface Water Regional Supervisor Winston-Salem Regional Office Division of Water Quality cc: SWP — WSRO "Storrriwater Permitting Unit SWP — Central Files, NPDES Permit NCG030548 Taylor -Smith, Aana From: Miller, Jim H. <jhmillerl@weil-mclain.com> Sent: Tuesday, June 11, 2013 11:50 AM To: Taylor -Smith, Aana Cc: Roberts, Melinda Subject: Re: ROS Request Approval Thanks for your help with this! Regards, Jim Sent from my iPhone On Jun 11, 2013, at 10:38 AM, "Taylor -Smith, Aana" <Aana.Ta for -Smith ncdenr. ov> wrote: Hello, We received the hardcopy of your Representative Outfall Status (ROS) request in the mail yesterday and I was able to go ahead and get the request approved today! The approval letter was sent this morning, so you should have it soon. If you have not yet done your first monitoring event for 2013, you will only have to perform Analytical Monitoring (sampling) at Outfalls 6-13. For the purpose of Analytical Monitoring, Outfall 6 will be representative of Outfalls 1-6. However, please keep in mind that you do have to perform Qualitative Monitoring for ALL of the outfalls (1-13), regardless of ROS. Hopefully, that will still save you some time and money when conducting your monitoring! Thank you very much for your attention to this matter, and please do not hesitate to contact me at any time with any questions you may have! Aana Taylor -Smith Surface Water Protection Section Winston-Salem Regional Office Division of Water Quality Phone: (336) 771-4950 Fax (336) 771-4630 E-mail correspondence to and from this lyddress may be subject to the North Carolina Public Records Low and may be disclosed to third parties. FF 40� Q �N sk NC®ENR NCw [..ap( DeP mcw OF EN+nrt .t--D Nai Resowcee Division of Water Quality 1 Surface Water Protection National Pollutant Discharge Elimination System REPRESENTATIVE OUTFALL STATUS (ROS) REQUEST FORM FOR AGENCY USE ONLY Date Received Year Month Da RECEIVED N.C. Dept. of ENR JUN 10 2013 If a facility is required to sample multiple discharge locations with very similar storm water'dlsclia"rge's, the permittee may petition the Director for Representative Outfall Status (ROS). DWQ may grant Representative Outfall Status if stormwater discharges from a single outfall are representative of discharges from multiple outfalls. Approved ROS will reduce the number of outfalls where analytical sampling requirements apply. If Representative Outfall Status is granted, ALL outfalls are still subject to the qualitative monitoring requirements of the facility's permit —unless otherwise allowed by the permit (such as NCG020000) and DWQ approval. The approval letter from DWQ must be kept on site with the facility's Stormwa ter Pollution Prevention Plant. The facility must notify DWQ in writing if any changes affect representative status. For questions, please contact the DWQ Regional Office for your area (see page 3). (Please print or type) 1) Enter the permit number to which this ROS request applies: Individual Permit (or) Certificate of Coverage 'N' sC 'S IVYC ' G-- 0 3 0 5 4 8 2) Facility Information: Owner/Facility Name Weil -McLain Facility Contact Street Address City County Telephone No. Melinda Roberts 523 S. New Street Eden State NC ZIP Code 27288 Rockingham E-mail Address mroberts@weii-mclain.com (336) 627-6037 Fax: (336)627-6067 3) List the representative outfalls) information (attach additional sheets if necessary): Outfall(s) 1,2,3, 4, and 5 is representative of Outfall(s) 6 Outfalls' drainage areas have the same or similar activities? L/Yes ❑ No Outfalls' drainage areas contain the sabre or similar materials? /Yes ❑ No Outfalls have similar monitoring results? Yes ❑ No ❑ No data* ` Outfall(s) _ is representative of Outfall(s) Outfalls' drainage'areas have the same or similar activities? e1 Yes ❑ No Outfalls' drainage areas contain the same or similar materials? a Yes c, No Outfalls have similar monitoring results? ❑ Yes ❑ No ❑ No data* Outfall(s) is representative of Outfall(s) Outfalls' drainage areas have the same or similar activities? rJi Yes ❑ No Outfalls' drainage areas contain the same or similar materials? ❑ Yes ❑ No Outfalls have similar monitoring results? ❑ Yes ❑ No u No data" *Non-compliance with analytical monitoring prior to this request may prevent ROS approval. Specific circumstances will be considered by the Regional Office responsible for review. Page 1 of 4 SV1U_RQS-2009 Last revised 12/30/2009 Representative Outfall Status Request 4) Detailed explanation about why the outfalls above should be granted Representative Status: (Or, attach a letter or narrative to discuss this information.) For example, describe how activities and/or materials are similar. Representative status for the outfalls mentioned above was discussed with Ms. Aana Taylor -Smith — Environmental Specialist for the Division of Water Quality during our Stormwater inspection on 5/20/13. All 6 outfalls are in the same general area, which is adjacent to our traffic circle. Monitoring results are also similar for the outfalls. I will be attaching the recommendation included in our Stormwater report. 5) Certification: North Carolina General Statute 143-215.6 B(i) provides that: Any person who knowingly makes any false statement, representation, or certification in any application, record, report, plan, or other document filed or required to be raintained under this Article or a rule implementing this Article, or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the [Environmental Management] Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000). I hereby request Representative Outfall Status for my NPDES Permit. I understand that ALL outfalls are still subject to the qualitative monitoring requirements of the permit, unless otherwise allowed by the permit and regional office approval. I must notify DWQ in writing if any changes to the facility or its operations take place after ROS is granted that may affect this status. If ROS no longer applies, I understand I must resume monitoring of all outfalls as specified in my NPDES permit. I certify that I am familiar with the information contained in this application and that to the best of my Knowledge and belief such information is true, complete, and accurate. Printed Name of Person Signing: WInCU ?abegJo Title: F W)gwc(abst 5/30/!3 (Sig Lure of Applicant) (Date Signed) Please note: This application for Representative Outfall Status is subject to approval by the NCDENR Regional Office. The Regional Office may inspect your facility for compliance with the conditions of the permit prior to that approval. Final Checklist for ROS Request This application should include the following items: 6 This completed form. Letter or narrative elaborating on the reasons why specified outfalls should be granted representative status, unless ali information can be included in Question 4. Page 2 of 4 SWU-ROS-2009 Last revised-1 213012009 Representative Outfall Status Request r-l"' Two (2) copies of a site map of the facility with the location of all outfalls clearly marked, including the drainage areas, industrial activities, and raw materials/finished products within each drainage area. d Summary of results from monitoring conducted at the outfalls listed in Question 3. d Any other supporting documentation. Mail the entire package to: NC DENR Division of Water Quality Surface Water Protection Section at the appropriate Regional Office (See map and addresses below) Notes The submission of this document does not guarantee Representative Outfall Status (ROS) will be granted as requested. Analytical monitoring as per your current permit must be continued, at all outfalls, until written approval of this request is granted by DWQ. Non-compliance with analytical monitoring prior to this request may prevent ROS approval. Specific circumstances will be considered by the Regional Office responsible for review. For questions, please contact the DWQ Regional Office for your area. Asheville Regional Office 2090 U.S. Highway 70 Swannanoa, NC 28778 Phone (828) 296-4500 FAX (828) 299-7043 Fayetteville Regional Office Systel Building, 225 Green St., Suite 714 Fayetteville, NC 28301-5094 Phone (910) 433-3300 FAX 910/ 486-0707 Mooresville Regional Office 610 East Center Ave. Mooresville, NC 28115 FAX (704) 663-6040 Raleigh Regional Office 1628 Mail Service Center Raleigh, NC 27699-1628 Phone (919) 791-4200 FAX (919) 571-4718 Washington Regional Office 943 Washington Square Mail Washington, NC 27889 Phone (252) 946-6481 FAX (252) 975-3716 Page 3 of 4 W)U-ROS-2009 Last revised 12130I2009 r Representative Outfall Status Request Wilmington Regional Office 127 Cardinal Drive Extension Wilmington, NC 28405 Phone (910) 796-7215 FAX (910) 350-2004 Winston-Salem Regional Office 585 Waughtown Street Winston-Salem, NC 27107 Phone (336) 771-5000 Water Quality Main FAX (336) 771-4630 Central Office 1617 Mail Service Center Raleigh, NC 27699-1617 Phone (919) 807-6300 FAX (919) 807-6494 SSNU-ROS-2009 Page 4 of 4 Last revised 1213012009 4� NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Pat McCrory Charles Wakild, P. E. Jahn E. Skvarla, !II Govemor Director Secretary 20 May 2013 Melinda Roberts, Environmental Health and Safety Specialist Weil McLain 523 South New Street Eden, SEC 27288 Subject: Compliance Evaluation Inspection NPDES General Stormwater Permit NCG030000 Certificate of Coverage NCG030548 Weil McLain Rockingham County Dear Ms- Roberts- Aana Taylor -Smith of the Winston-Salem Regional Office of the NC Division of Water Quality (DWQ) conducted a compliance evaluation inspection at the subject facility on 20 May 2013. Your assistance and cooperation during — the inspection were greatly appreciated. An inspection checklist is attached for your records and the inspection findings are summarized below. This facility is located at 523 South New Street in Eden, Rockingham County, -North Carolina. Stormwater related to industrial activity is discharged frorn the site to an unnamed tributary to the Dan River, this section of which is currently classified as Class C waters, in the Roanoke River Basin. Documentation & Monitoring•. Review The Stormwater Pollution Prevention Plan (SPPP) is complete, well -established, and current. It is updated on a yearly I✓asis and all required records were available for inspection. Documentation for employee training was available and signed by all in attendance. The facility has had no significant spills in the past three years. Facility inspections are also completed and recorded as required. The facility has thirteen Stormwater Discharge Outfalls (SDOs) at which monitoring is performed on a semi- annual basis. Qualitative monitoring has been conducted and documented as required. Analytical monitoring has also been conducted and documented as required. Pace Analytical is used as a contract lab and pH is monitored by Weil McLain staff using approved methods. Records of calibration of the pH meter were available for inspection. Site Review The facility was found to be very dean and well -maintained. All necessary secondary containment is implemented as required. Each of the thirteen outfalls was examined during the inspection. The SDOs were Na'vi Ceraina Dhisiun of Water Qua;i,r,',°firs on -Salem Regior„I Office ! ocatien_ Ss wdj-�Ncr n St. A instazSz'e; r,,'gc.;h Car fna 27107 One Form:,36771-5CMtFAX: 336-77i-<630%CustomerSeftke:"77.623-0748 No['thCa O/i/ilia Inwrm rrvnl,nchaterqua6,7.or� Naturally An Eei:l Oppowaiy i Af urrPM Action Emp!o;er Weil McLain 05/20/2013 Page 2 of 2 clearly marked and very well -maintained. The receiving waters at each outfall looked clear with no visible foam or floating solids. It was noted during the inspection that outfalls #1-6 were very similar and may qualify for Representative Outfall Status (ROS). You must formally apply for ROS by submitting the ROS application form, which can be found and downloaded From the following website, along with the required accompanying materials: http:Z/gortal.ncdenr.ore/weblwq/ws/s /npdessw (Click an the "Miscellaneous Farms" tab at the top of the table) During the inspection, it was noted that exposure of industrial activities and/or materials to precipitation is minimal, with the exception of one uncovered materials storage area. You mentioned that Weil McLain may install a storm -resistant shelter for that storage area. When a storage area has been installers, Weil McLain may consider applying for a No Exposure Certification for the facility, which would preclude the need for the stormwater permit, SPPP, and any qualitative and/or analytical monitoring, for as long as the No Exposure condition is maintained at the site. For more information on this program, please review the "NC No Exposure Application Form," which can be found and downloaded from the following website: httf)://Portal.ncdenr.org/weblwu/ws/su/npdessw (Click on the "No Exposure" tab at the top of the table) We appreciate your efforts to comply with the stormwater general permit. No additional response to this letter is required. Please do not hesitate to contact Aana Taylor -Smith or me at (336) 771-5000 if you have any questions regarding the inspection or this letter. Sincerely, W. Corey Basinger Surface Water Regional Supervisor Winston-Salem Regional Office Division of Water Quality Attachments: 1. BIMS Inspection Checklist CC: Central Files w/attachments WBSPC Unit w/attachments WSRO/SWP w/attachments Permit: 14CG030548 Owner - Facility: Well -McLain Inspection Date: 0512=013 inspection Type: Compliance Evaluation Reason for Visit: Routine Comment: Facility may wish to consider Representative Outfall Status for Outfalls #1-6. If storm -resistant shelter is provided for materials storage area, facility may be eligible for No Exposure Certification. Outfalls were very well -maintained and clearly marked. Page: 4 ac6h7aillical " i f Pace Analytical Services, Ine- 205 East Meadow Road - SIAL A Eden,'W 27288 1336j523-8921 Qctober 30, 2012 [Mr, Darrell Freeman %,%Ieil McLain 523 S_ New St. Eden, NC 27288 RE. Project- Storm Water 1W15112 Pace Project No.: 92135182 Dear Mr. Freeman-. Peoe Arralyftat Setvlces, Inc. 2225 Rtyamide Dr. AfbaWle. NC 2a804 (828)254-7176 pace Art -"cal S*ralce&, Inc. ?900 Kincey Ave. Suite ioo Hu^!eMIfllL, !IC 28078 (704)W5-9992 Enclosed are the analytical results for sarriple(s) received by the laboratory on October 15, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the race Analytical Services location ind:ca:ed on the sample analyte page for analysis unless otherwise footnoted. laneAna"cal" Profecf: Storm: "Wer 10f15112 Face Project No.: 92135182 Pace Anarytiral Services, Inc. 23S East Meado Raed - SvO A Eden, NC 272M Charlotte Certification fOs 9800 KfteyAvo- Ste 100, NurA&sr=i_e. NC 28076 North Cafolfra Dnnkina V.10ter Certification x: 377,16 North Carolina FWd Serv7ce5 Certlfftation 4' 5-42 North Carollna WaStewaterCer,iiicaJon A: 12 SoWh Carolina Cerlitiration it;: 99006r01 (335)6234321 Pace Ana"cnr Services, Inc. 2225 Ra-ss3de C-r. Ashmvale, NC 28804 CERTIFICATIONS (828)250-7176 FloidalNELAP Cerllficatlon M: E87627 Kentucky UST Certi%alfon A: 84 West Vglria Crrtircaticn #: 357 ViryfriaNELAP Certification #: 460221 Pace Ana"cal Services, Inc. 88DOK'incay Avt. S:+°a 100 Y.urftru .'a, NC 28078 Asheville Cerificatron I7s 2225 Riverside Dr., Ashevire. NQ 28304 North Carolina Wastewater Cefi icatian #: 40 FloridalNEU4P Certification #: E87648 South Carolina Certification —, 99030001 ffA.sachuse(1s CerliHcatron *: M.NC030 West VlTyinia Curfilication t: 3," North Carolina Drinking .Maier Certification t: 37712 VirriniaNELAP Certification Y:460222 Eden Certification IDs 205 East A leadow I'load Suite A. Eden, NC 2728E North Carolina Wastewater CertiticaSion :633 North Carolina Certification #: 37738 Vrgi: ia/VE! AP Cerifica'don #: 450025 (774)375-90S2 I i• r l I r;EG€ii.?r�.Lt�DgC.f1TGRY..1�i�VlLY3iS.. ;, rage2_e'7u- _ ti . - ':,"•..^eil ;fnC-nsant��r.�Airart::+l'S"•.=::a,'r. - =c• - -- '1 '.1 I. s Paco AnatytiCalSe'Vlc-a, Inc. Pace AnvlydczlSwvic",Inc. Pace AnalyticalSomIces,(no, / C16Anat U.a. o f 205 Easi Meadow Pond - Sure A 2225 Rt *mWe Dr. S8W Komey Ave. Svra 100 eTye. Edcn, NC 27268 A.sheyfl.e, r4C 28804 HvnteyWle• NC 2807 5 (336)823-a921 {828)254-7176 (70A}675-90a2 SAMPLE ANALYTE COUNT Project: Storm %later1Of! 5112 Pace Project Vo.: 92135182 Analytes Lab ID Sample iR Method Analysts Reported Laboratory 92135192001 $00 #2 pH 7.0 $.M 2540D CUM 1 PASi-E EPA 16Cr'.A CLV'1 1 PASS-C EPA 606 RES 27 PASI-C EPA 200.7 JDA 1 PASI-A EPA675 RPM 65 PAS[-C EPA624 AW 73 PASI-C EPA 420.4 EVVS 1 PASi-A SM 4540-cm•E JDA 1 PAS( -A 92135182.002 900 1!3 pH 6.3 SN12540D C(.It4 1 PASI-E EPA 1664A GvJv 1 PASI-c EPA808 RES 27 PASI-C EPA 200.7 JDA 1 PASI-A I EPA025 PPFrt 65 PAS1-c EPA624 AW 73 PASf-C EPA420A E1111S 1 PASI-A I SM 4500-CN-E JOA 1 PASI-A ` 92135182003 5DO #5 oti 6.7 SM 25400 CUM 1 PASI-E i EPA 1664A CLV4 1 PASI-C EPA008 RES 27 PASI-C EPA200.7 1CA 1 PASI-A EPA625 PFUi 65 PASf-C i EFA624 AVl 73 PASi-C I EPA420.4 EWS 1 PASI-A 'SiA F _ JDA + 1 PASI-A _45+J0-CN - 92135:82004 5D0 Lfi pN 6:4 SM'25400 CLM . _ .-. _ - ::ram_•:^.-.-:'• ,....,r.-• 1 PASi E i EPA It 64A ` 1 ; - .. - . CLIN.. � �r 1 PAS? C t EPA608 itE5 47 PASS-G 1 EPA200.1 JDA 1 PASI-A EFA625 PPM 65 PASf-C EPA624 AW 73 PASS-C i ... .. .. . , - EPA'420 A HNIS.................. 1 ...i?ASI _A: ._..... _ .,... '213<i$2�85 SD^ r7 Pi i_0 _ S.M, 754C0 Cw;.1 i :.PAS[-E. •ti CPA 1364p':;;; ` �s:.. - C .;7 1' >P L = 7. DA PA EPA f2"i RPu r5 FfSf-C: - , Ft�0:4% ems=- a0 •�?Or7Y•€iitikLY5�5 . Po�' e� 7a.- f . +.`::.• A. s��_r.:^.. zcer,re r^ .9- _ ••r" - Pace Analytk4i SaMees, hic. Pae•Analyticat Sonic". Inc. Paco Arnalylleal Servtaes. Inc aeeAnalytical 20.5 t*34 Meadow Road - 9uLe A =5 Rtft s e Dr. 9800 KhMAve- Suds j - Eden. NC V268 AshevMv. NC 26BD4 Huntewfle, NC 28078 i (3M)623-6921 {825j2544176 (704)375-SM2 ' SAMPLE ANALYTEC COUNT Project: Stonrl Water 10f15112 Pace Pra;eci No.: 92135182 Analyfes Lab ID Sample I❑ Method Analysts Reported Laboratory EPA524 AW 73 PASI-C EPA4204 EWS 1 PASI-A SM 4500-CN-E JDA i PASI-A 9213.":102005 SOO f.8 pl# 9.0 Sid 2540E) CUM 1 PASI-E I FPA 1664A CLV-J 1 PASI-C EPA608 RES 27 PASI•C EPA200.7 JDA 1 PASI-A EPA625 PPM 65 PASI-C EPA624 A'f 73 PASI•C EPA 420.4 EWS f PASI-A. I SM 4500-CN-c JDA 1 FASI-A i ! 9213sl82007 SDO =9 pH 5.8 SM 2540D CLI11 1 PAST 1 ' f EPA 1664A CLvi i PASI-C I EPA608 RES 27 FASI-C EPA 200-7 JDA I PASI-R ' CPA625 IRMA 65 PASI•C EPAS24 AV; 73 PASI-C EPA 428.4 EV`1S 1 PASt-A SM 4500-CN-E JDA 1 PASk-A ?• I, 12135182003 SOO +11 pH M SPA 25400 CL%4 PAS1-F EPA 1554A CL\Tf 4.PASI•C EPAC-08 RES 27 PASI•C EPA 200.7 JDA t .' - ' PASI-A EPN625 = FPA/e' "'65 : PEA 624 ..:..'• Aw 73 PASt•C j f - �•. ;: 'EPA 420 4 ' EWS 1 PAS1•A SM 4500-CN-E JDA PAS; -A 92135182009 Sc7t3 n12 pH 6.9 SM 2540E CLm 1 PAS1-E ; EPA 1664A CLVV 1 PASI-C EFAE08 P•ES 27 PASIC :. Azoa.7 JDA. 1. .f?asl-A r '$rAA27.4- k. STA'45nO CN Jr t P'S[-A }, `;4R�F- - °21 SL10"'-'i: pirt�r.}?. .. - �SOO,c 'C A .. :i\,ie•F is a, c 7:-O...J-t.�OFATO�Y r1�FiE:Y51S..::��.. f - *lY- `S_N - -r C f .`Il i iG A^s� cr Servr 9 isl i •�'' -1 _ .•1_ _ ••ass. -�% Pace Anatocai Services, Im Pace AnxlyLlcal Smlcpm, Inc. Pace AWOW Services, One. HoeAnaViWIR 205 East Meadow Road - Sufte A 2225 Riverside Or. WW Kkney Ave. Suite 100 Eden, NC 272H N211804 murrcrsvft' arc 2a778 (336)623-0921 (820254-7176 (704)975 S02 SAMPLE ANIALYTE COUNT pro;ect Stan-n Water I Oil 511Z PaCe Project No.. 92135182 Anaiytes LablD Sam Pic 10 Method Anatysts Reported Laboratory EPA 508 RES 27 PAST-C EPA 200.7 JDA I PASI•A EPA 625 Ppm 65 PASTPC EPA 624 AW 73 FASI-C EPA 420,A EWS I PASI-A m SM 4500-CN-E JDA 1 PASI-A P_ 'T REPOR --OF LASORAT6.R ..... ..... 7 k:e m % 7� k 7 i a ri�, h11 f #com !(,al Pact Anatytical Servlcts,;nc. 205 East Meadow Road - Sulta A Pace Anfrc. afydcal Servlcm. t 2225 RNerOde Or. Pace Anafi?11=1 SarACea, Inc. 98001Cstcey Ave. Siitr 1 DO ,�„Y Jos" _den, NC 27288 ?shavft. PVC 28804 Huntarsvlllo. NC UM (awez: -.Mi 028)254.7176 (704)67$-8047 ANALYTICAL RESULTS Project: Storm Water 10f15r12 Pace Project No.: M351-82 Sample: SDO 42 pH 7.0 Lab ID: 921351$2001 CoFected: 101151i2 08:30 Received: IWIE/12 12:05 nlalrix' Water Parameters Rksults Units Report Limit RF Prepared Analyrred CAS No. Qua! 2540❑ Total Suspended Solids Ana lyticai Niethod: S612540D Total Suspended SoWs ND fagIL 2.5 1 101i6/12 0$ 3 HEM, Oil and Grease Araiyllcat Method: EPA 1064A Oil and Grease ND rrg/L 5.0 1 10/24/12 11:19 6D8 GCS F'estleldes andAC6s AnatytiCal Meihod: EPAB08 Preparation Method: EPA3535 Alc rdn ND mglL alpha-BHC ND mg/L beta-GHC NO mg/L delta-SHC NO rn0/L gamma-91-IC (Lirldane) ND ng1L Chtvtdane (Technical} ND r1g.L 4,41.DDO .40 mn,,IL 4,41•DBE NO rrtg/L 4.4'-DDT NO mgfL Deldrin ND mg,'L Endosultan t ND (r1g,IL Endosulisrl II ND mgfL Endesullan sulrate NO mcfL End6n rW) rr,gfL Fndrin aldehyde NO mg/L Heptachlor ND mgfL Heptachlor epoxide NO mjfL PCB-1016 (Aroclor 101-3) ND m81L FCB-1221 (Arcclur 122 i) ND mgfL PCB-1232 (Amcior'222) `.D eng11_ FC(� 1242 (AroclOr ', 242} N D. mgfL ",'FC8-1248',(>{roctor 12QE] ND'mg PC8-1254 (Ariiclor 1254)_ `mralt _: PG9.:12fiQ.(krodtr.1250); ':: :. ND rri�x • 70Xapl ND mgli 1a11�chloro-m-xyiene (5) 47 % D».rhlprphipheilyE ($) 55 % 0.000050 1 10116//2 17:09 10119/12 22:12 309-00-2 D.000050 1 10116/12 17:00 1Oil 9112 27:12 319-84.6 0.000050 1 1011V12 17:00 1.011V12 22:12 319-85-7 0.000050 1 10116112,, 17:00 10;19112 2112 319-86-8 0.000050 1 1011&1217:00 10/1917212:i2 58-89.9 0.00050 1 10116/12 17:00 10119112 22:12 57-74-9 0-0ON50 1 10/16/12 17:00 10119/12 22:12 72-54.8 0.000050 1 10/16112 17:00 1,0119112 22:12 72-55-9 0.000050 1 10/16/12 17:00 10119/12 22,12 50-29-3 0,000050 1 1C116f1217:00 10119/1222:12 60-57-€ i 0.000050 1 1011Ul217:00 1011911222:12 059-98-6 0.W0050 1 1011$11217:00 ,WlO1222:12 33213-65-9 0.000050 1 10116f12 17:00 101IS112 27•:12 1031-07.8 0.^00050 1 10/16112 17:00 10/19112 22:12 72-20.8 0.00.3050 1 10116/12 17:00 10/19/12 22:12 7421-93-4 1 0-0000ho 1 101i6/12 17:00 10/19/12 22:12 75-d4-8 t 0.000050 1 10116112 17:00 10/19112 22:12 1024.57-3 0.00050 1 10115/12 17:00 1011?112 72:12 12574.11-2 D.00650 1 10116112 17:00 16/19/12 22:12 11104-28-2 " 0.00050 1 1,0/1611217:00 IOIIW121.2:12 11141-155 ! 0.00050 '3 101.18112 17:00-10119/12 22:12 53469-21-9 000050, -' f 101.1&121700 1 C1.1 X 12 22-1 212672.29.6 � O i7o450 f,: 10Hu112,17 00 :10119117 22i12 11097r 9 1.. O.00WO 1 14/7G/12.17:Q0.S_4019?I12.Y2:12.1.1R96$2�.:,._".;r``•.:�''� •• o.eaDSa i �. 10116I12 17:00 i017811222a2 '600i=35 2• ;.' . • i 20-1i0 1 10/16/12 17:00 10/19112 22:12 877-0@-8 2D-138 1 10116/12 17:00 1,011912 22712 2051,24-3 200.7 MET ICF1 Analylicat Mlethad: EPA 200.7 Preparation Mmficd: EPA 200.7 Lead ND ntg/L 0.0050 1 ,0A81i211:35 10119142 15:05 7439-92-1 625 i51SSV AnotytlG013Se ud: EPA,625 Fn paralion 1+�et*red: EPAE25 ' �cEn h'w �: " , - .. "1idt. , ... _ : J.n:':0: _ !, s!•'y,{ 1� �i,. tir�t,f4Z'0L:. '43 _ 37-_li:• .'.. ''.�' •'E- Ac:h20httt•rhr,R :KOrrclL 0,0010:' 1;.' i.0.5112.1600, V312Q11202:137,243-36.8 r- -F,cetC;t+.eie.,, S' - Ox,051 V- ' 1011W i5:40`.:i012lT/17-02:97 :.1_6-2': tilt 10e _ 1� n .i = n- KD . »IL d30 • '1-• _;rJIF ii2 tom"!..` _!tl?lt2.C1.2...r _3 J•- - "Amhre, _ 'rti7.^CfL Q.SQSOt 1` 70I;811215:04 L/201izC2'"7'.i120-12.7 :. cenzid! _ oiJ�n1.fL` 0.0�0'. 7%_ r.1Q�3?JiZ 1n00 4!420i12.0ZtG7.9Z-a"7-5' -fita+xja,,€:.ape _ c•ttnL OQO50 3•: 0ltsri2s�r4 1a2CIiZ,47-:07::'S�55•S": -- :n2(1`.SM3'Sf;1'ir•C- 5^PM c S:CY�Z--of> ' 6'nfORI0RYANALY - 'r. per' ,aq �'tte re_'•'a•:•.[ :'4�'.•II _ �-q:.�n .,. nW.l.'.n r:SA 1- �S it^.: ••�1] e�y!'^�: • i - - - - - _ - .;; : _ :-.tit: ___ - Pace An&4,Ocal Serrfc". rnc. Pace Analytical ServrceS, Inc. Paces Arts"eal Servlev8, Inc. (�Ci'Pr�Q1 Ld1 105 East 1readow Road - Suite A 2225:z versidv Or. GBOC Kncey Ave, 51rte 100 x,M f Eden. NC 17288 Asheville, NC 2630A Hu-�:ds•Rb, ,NC 28076 i (336)623-642 t (828)25a-7 t 7B t76e)675-W92 ANALYTICAL REStlf_7S Project: Storm haler 1OM5112 Pace Pro;eu No.: 92135182 Sarnpte: SDO 02 pit 7,0 Lab ID; 92135182001 Co!i`Ged: 10175112 08:zO Received: 10115112 12:05 Matrix: 1Natar Parameters Results Unlls ?epoll Limit OF f-'repared Analyzed CAS No. Qual 625 r'dSSV Analytical tAoViod: EPA 625 Preparation Method: EPA 625 Denzo(a)pyrene NOrrigIL 0.0050 1 1011811216:00 1012011 Z 02:07 50-32-8 i3enza(tr} iuoranthene NO mQfL 0,0050 1 10118112 16:00 10/2O/12 02:07 205-90-2 5ere4o(g,h,i)pery1ene NO rngrl 0.0050 1 10/18112 16:00 10120/1202:07 191-24-2 Benzo(K)'uoranthene NO nlg/L 0.0050 1 10/15112 15:DO 10120112 02:0'/ 207-08-9 4-8rornophenylphenyi elhcr ND mg/L 0.0050 1 10118/12 16:00 1020112 02:07 103-55 3 Hulytbenzy!phihalate NU mg/L 0.0050 1 10118M2 16:00 tOf20/12 02:07 85-68.7 4-Chloro•3•methylphenol NO mg/L 0.0050 1 WORM 16:CC 1012011202:07 59.50.7 bi6(2-Ch1or0elhoxy)methane ND mg/L 0.010 1 1011811Z 16:00 1tl12011202:07 111-91-1 1 bis(2-CAkruethyl) ether 140 mS/L 0.0050 1 10118/72 16:00 1012C/12 02.07 111-44-4 bis(2-Chlorolsopropyl)ether NO mgfL 0.0050 4 IVIU1216:00 10120/1202:07 108-60-1 a 2-CAlcronaph"talene NO rr.g/L 0.050 1 ION8/12 10:00 10120112 02:07 91.56-7 2-Chtorophenoi ND ❑lg1L 0.0050 1 10118/1216:00 10120202:07 95-57.8 , ! 4-Ghtorophenysphenylother NU mg1L 0.0050 1 10M8/4216:00 1C420A202:07 7005-72-3 Chrysene NO trig/L 0,0050 1 10JI811216:00 10120112 02:07 215-01-9 r 0ibenz(a,h)awbracene NO nrg1L 0,0050 1 10118/12 16:00 10/20/12 02;07 53-70-3 F 1 1,2-Oichlurobenzene NO rng1L 0.0050 1 10118/1216-00 IM911202-G7 95-50-1 i 1,3-Dichlorobesi4ene NO mgfL 0.0050 1 tO118/42 1G:00 10/2011202:07 541-73-1 t. 1,4-01ichlornbernzene ND mg& 0.0050 1 10/18/12 15:00 1 C120112 02:07 105-46-7 3,3'•Dich1arabenzidine NO mgR- C.025 1 ' t0fleflZ 16:0C I=011202:07 91 94-1 2,4-Dichlcrophenot ND mg/L 0.0050 1 10118/12 MOO 1012011202!07 120-63-2 DiethytphthaLate NO mg/L 0.0050 1 10118/1216:.0 10120A202:07 B4-65.2 2 4-0ir:lethylphenol NO rag/L 0.010 1 1011802 16:00 10170112 02:07 105-67-9 ; Oirnethylphthatate ND n1g/L 0.0050 1 1C/18/1216:00 10120/1202:07 131-11-3 ; Di-n-bu:ylphLhalate \U mg/L O.ty350 1 t0/18/1216:00 1W2011202:07 84-74.2 4,6.Oinitrc-2-methytphenol v0 mgfL 0.020 4 1011811216,00 1M1Y1202:07 534-52-1 i 2,4.Oini(tophenot NO mg/L 0.050 1 10118112 16:00 10f20112 02:07 51-28.5 � 2-4.01ni;rotoluene NO. mg1L O.005O 10/18/12 15.00 10/20112 02:07 121-14-2 2,6-Dinilrutcluene NO mg11_ .. 0,0050 1 10/18112 16:C0 1 C120/12 02:07 506-20-2 j 'Ol-n-acly,IpFrthaldte .,- NO-:ngeti'•. '0.h05U 1 1i}118Ii2;1E:03 1017.p1i2C2C7 11784-0 F i :.1.2-Oiphanylhydrazine,. •. ,. _ N rrlg/L-• -.0_ 66 . i ft?118l12?1540:10/20Jt20207 122-6&7; bis,2,EIh} htx/1)ptllhp.late NO, mgll 0.01) 1 • 10116/12 15 �0 1017Clsz 02 07 317 817 { t Flu'v'ra lttsere " NO rm/L 0,0050 1' "'1011812d6:M0 10120/12.02:07t'r206-44-0,7`'. '- Flcoreite = NU rng1L 0,0050 1 1C118/12 i6:C0' 10f241T2 02:07:.'8Cr'3.7 > ' Hexactilorc-1.3-bufadlena ND mg/L 00050 1 10118/121500 IM011202-07 67-68.3 Hexachlorobencene NO mg/L 0.0050 J. 10118112 16:00 10/20112 02:07 118-74-1 , 1'•exachlorccyclopentadiene NO ma1L 0.010 10/16/12 16:00 10120/12 02:07 77-47.4 Hexachbroethane Hu Mgf,- 0.0050 I 10M8112 16:00 10120/12 02.07 67-72.1 j. Indono(1,2,3-cd)pyrene ND r7g1L O.C950 1 10118/4216:00 1012011202.07 193-39-5 r :.. Isaphpiont;;;.. .... , :. - NO.mg/L. -C:010 .. 1-IGJA8112 16:00 .10120/12.02:07. 78-59-1. _ i, • _.?�nL lL-l' eta .. Citi.ltt i5:;;,,- 10:2tai202:yr v :'2-Ntroa en71 . CIS mo 0. 350 j.1-..;::"1C' 3r12:;5:;Q. 10120112A2:07< ;_75:5-`..;..:;` 4: M,e 0"1 10fj 215:001012/12 7CT 80TO'r•�2 7 i- 1-:1iC,9sOC SJryl2Tir6 Ns7 ntt" 0;!^SC 1;' T01T°.r17.,15:04 .012C/1202.n7 62.75_0. <. -� �Ittcso-�i-it;pre yls7:ir,= -NO mg/1-tOri'412i5:G2. ;!213M20207-g24-5zr ;. N•N?tieacd'F1ss ry ;rt :0 NC PTiL O:Otp t 1011?V12 T6:@Q' SOIcC1T 7.Q2`47 'E5-3S =:; - �crtnCilC:ct!^aCt` :;f� i=iurL' - OA%.t :,SO!1u1i7 f5:0C'.iCi20it2O%:^7. $7-56-5 1 �� CRT o� _asJ+lrOnf/rYlllS* P+•ciA; 7-:(.Fn - _ �.,..o:, _;.� .c_ai 'o: ce At•il .:% e.ri:-!f 'rc.. _ - �f. ;fi Jr e Paw An2"cal Services, Inc- za'AnNytS 2p5 E71st Meadow Rwc - Su Re A „M *tMM Eeen, h'C 272H ;335,'ST..-9321 Ptoieot: Storm Water foil5!12 Paw Projcct No.: 92135182 pace Analyrical5arvkaa, irrc. 2225 2iversfdo 0% AfhWle, NC 22504 (828)254-7176 ANALYTICAL RESULTS Pace Anity4cal Serrtce% Irrc. 9800 K rM Ave. Swe 100 Huoterevft. NC 28078 1704)67%-30'd2 Sample: SDO T2 pH 7.0 Parameters Lab 10: 92735182001 Results Units Co'lee.ed: 1P'15112 08W Report Limit OF Received: 10/15/12 12:05 viatft %vater f Prepared Analyzed CAS No. Qua] 625 MSSV Analylical Methed: EPA625 Preparation Method: EPA325 Phertanthrerig NO rmt l- 0.3050 1 IW18112 16.00 10120/12 02:07 85.01.8 Phenol NO rr:gtL O. M 1 10/18112 16:00 10120112 02:07 108-95.2 ?Irene 1,10 mg1L 0,0050 1 10l18112 16:00 1020112 02:07 129 00.0 1.2.4-TrichIc:robenzene NO mglt. O.0050 1 10118I12 1&W 100-0J1202:07 120-82-1 2,4,6-Tsi_h1arophanc1 NO mg1L 0-010 i .W1811216,00 1012011 Z 02,07 38-o6-2 Surrogates Niirobenzone-0 (S) 47 % 10-120 MUM 1"0 10/20112 02 01 4165-60-0 2-Fluornbiohenyl(S) 42 °! 15-120 1 10118fi216:00 10120II202:07 321-60-e Terphcnyl•d14(S) i1 % 11-131 1 IWIB11216:CQ I=011202:07 1718-51-0 = honor-d6 (S) 17 % 10.120 1 10O W12 16:00 10/20/12 02:07 13 €27-68-3 2-9uorcphencl (S) 23 56 40-120 1 10,18112 16:00 1O UM 02:07 367-12-4 2,4,5-Tribromophrno1(S) 68 % 10-437 1 10116112 16:00 1WWI 202:37 118-79.6 624 Yolatiie Orgahies AralviiCat Method: E:PA024 Acelone ND rngiL 0 426 1 10/22112 16:56 67-64-1 Acrolein ND mglL O.f 0 1 10r72112 16:56 107-02.0 i Acrylonitrile NO mg1L 0.11i i IM2112 16:56 i07-13.1 l 6enzCne ,d© mgk 0{YJ50 1 10/22/12 15:55 71.43.2 Bromobenzene NO r^.efL 0,W50 1 10122J12 15:55 1G8-6$•i Bromechlorcr,w�t:•rane ND my1L U050 1 1G,'22112 16:56 74-97-5 f Srumodlchloromalhane ND rnglL 0.6050 1 10r22112 '1&56 75-27-4 Bromororm NO mg1L 0-0050 1 10/22/12 16:55 75-25.2 Rromcmethane NO rr1g1L 0.010 1 10122J€216',58 74.83-9 2-Butanorm (MEK) NO mgJL 0,010 1 10122112 16:5G 79-93.3 n-Butylbenzene NU mc1L 0-0050 1 10122i12 16:56 104-51.5 i sec-Butylbenzene NO rngiL 0.0050 1 50122J12 16:56 135-gB-8 tart-Uufylbenzene NO mgiL 0,0050 1 10122i1216:56 •98-06 8 s Catbon disul(de NO crigil. 0.010 1 10/22/12 16:56. ;75-15.0 . r Carbon tetrachloride ND mglL 7,0050 1 :1tN22tt2•iEi:bB 5fit23 5.::: ,:.-' '-i 1 ; .. Cliiorahenzere NC1,rrgrL -Opso 1 ifl12?i�2116:55" ,NE) Mg/L -010 ! - • 1D72Yl 2aFi:58 .75 00-9 i `- -2�Ch3pfvCRtylvl::yl eher' • ' . •. „ ' : `l�Ci;a't1ClL"-= :: •+ �'0 G10 ' '' �. i • i 0122i12 15:5G � Z i Q-75.8 Chiorotor�n NDirtigJL - 0.0050 ` 1 1002711216:56 67•456.3 c3 i6ranie'ihane NO rilg/L 0.0050 1 10/22/12 16:56 74.87.3 Z:chlulotoluene NO ma1L 0.000 1 1012211216:55 95.49-8 E 4-Chlorotoloerre N0 mg/L 0.00v0 i 1C/22112 16:56 106-43 4 1)ibrorrochloron:e t:ane ND mg1L 0.0050 1 10122J1216:56 124.4g-1 ;•2-Uibromoerhane (GCB) ND mar- ^.0450 1 10122112 16;56 :CS-934 Ribrpmorry lhann ry0 mo1L 0.0050 1 10122I12.16:56::74.95-3 , ' .Q.2-.S)C4e`s'Tt'S."1.` -. - '-4:'1: _:A- -'-i1.•.�L•Fij ;;Ef{,1'.1:..lyrr'•9$.y.i�-- - --- -.i. D!c'ro+c^ec,_ers SD:m2iL Q.r0307r6'yz1-73- .-LM1I::iu:c5eiize_ 'r•NCrciL" O,OC).--,.1.i:: 16I27ri2;5:5�'iC5-4S:7 --- .' .i,'iCichiOro�t�'zne t ^ ^.10/2i117 i3: i5 75 ./•3, .. -- 1.a-Oi.51s1obt4z^?- - r\� ,me, _9'�450 ; a^l2zhz 1 ,SB'j.C7-^S•c. :.< .. �i`! rc�ihereY '1rtir3 L iL u Q050 1 ^li2,t2 :c; w':.-75.g5:4 - 1.2 Dirti;. n here D L i^12i1i'21!C- 5' _ F_ ;n_'•0: 5 r4.5 i. RCFORt:0,,LAs0RfITO';Y/xfVAGYstS-.:: . =;` Pase,5c,'O:::" -- t r - Ss _ . ih7ll,n=�•"^ 1e�:7� y l r. - 1 , . • in � : +rr: ;an (wC�4e� C r ?Arta.'} _tCRr 3Cf�'"=RS, m - - � ( e Pace Aaalyticei Services, Ine. Pete Ans!yticsl Servkra, Inc, PaceAnalyt!cal Services, tne. / 205 East Meadow Road • S.Ae A 2225 Rhwdde 0r, 8800 Kncey Ave. SUP`.a 1 M rom Eden- NC 27-,U Acnevft, NC ZMU r,untersvl&. hrC 28078 (336I62a_ew-1 18281254.7176 (704)875-9092 ANALYTfCAL RESULTS Project- Storm Vhter10f-,5f12 Pace Project No.: 921,35182 Sample: SOO #2 pli 7.0 Lah fM 92135182001 Co;lected: 10115112 Oti:3G Received: 10/15112 12:05 Ma:rfx::Naler Paramelers Results Units Report Limit DF Prepared Aaialyzed CAS No. Qual 6Z4 Volatile Organics AnalytiraE Me:.l,od: EPA924 1,2,Dfchloropropane NO mgfL 0.0050 1 10122ri2 16:56 78-37-5 i. - ir-Moroprapane NO mg1L 0.0050 i 10122112 16:56 142-28.9 2.2-DIChloropropane ND mc1L 0.0050 1 10/22/12 16:56 594-20.7 1,1-Oiutiroropropene NO n41L 0-OM I IC122112 16:56 563-58.6 cfs-1,3-DicNaropropene NO rrg1L OXOSC 1 1WIM2 16:56 10051-01-5 trans-1,3•Did-iloropropene NO mg1L 0.0050 1 10.r2211216:56 :0061-02-6 ; Fthylbenzene NU mglL 0-OG50 1 f0122112 16:56 100.41.4 Hoxachlom-i•3-buladiene ND rtg1L 0.0050 1 10122i1216:56 87.68-3 2-Haxonone NO mgf! 0-010 1 10122/12 16:55 591-78.6 lodamethane NO mg1L 0.010 1 10/22/12 18:58 74-884 s 15opropyttlenzene (Cunene) ND mg1L 0.0050 1 1OUW.2 16,56 98.02-6 p4sopropyltuluene NO mg(L 0.0050 1 '0122112 16:56 99.87-6 Methyfene Uaorlde ND mglL 0.0050 1 10122f12 16:56 7"13-2 4-;lathy:-2-psntanone ('rf19K) NO mg1L 0.010 1 10122112 16:56 108-10-1 Methyl-lerl-butyl e,her NO noR 0.0050 1 10122112 16:56 1634-04.4 Naphthalene ND mglL 0.0050 1 1C122112 16:56 9I.20-3 n-PiOpylaerzer.D ND mg1L 0.0050 1 10422112 16:56 103-65-1 S yrene N0 rng11, O.GG60 1 10122112 16:56 100-42-5 1,1.1,2-Tetrachlcroethane NO mCII, 0.0050 1 10127A2 t6:56 630-20.6 ; 1,1,2,7-Tetrach:oroethane NO mg1L 0.0050 1 1C'122112 16:56 79-34-5 Tetrachfcrowhene No mull, 0-005G 1 1L'122112 16'.56 127-18.4 Taluene NO m91L 0.0050 1 16/22/12 16:56 106-88.3 1,2,3-T-wMorobenzene NO rig& 0.0050 1 1WM12 16:50 e7.61-6 1.2 A-1i:chlarobenzene No mgdL 0.0050 1 10122r12 16:55 120-82.1 1,1,1-Tr,.Waroethane Ni) ,Pg/L 0.0050 1 i0122112 16:56 71.55.6 1,1•2-T.richlo(Gethane NO mgfL D,0050 1 10122112 16:56 79.00-5 Tficr�la:cethcno. ND mcfL 0.OD50 1 P0/2?J.12a6,5G.,79-01-6 Tr=chfere I_ororrtethane ya mglt. = 0-oto - - :1 „iC122i12 48:56:.75=69.4 . - _ iciiidropiopane. .. :ND''mglL::: - - - �0:0050 : - ' i : - -- ..- ... _ ,.1012.2M216:55,: S&IE4, 1,1,2-Mchlorotrillaor6ethane,. ,•.l,2A_'rimethylbenzene.,...- hD m911 O:OC�Sp: `•'--1.: 10122112 1656 7&?J 1 ;. ,.:.1,.'.. ..- NDnAIL. 0.0050 1 10122112,,1G356 S5a63-6 Crii¢thy!{ienztfire •`ND rig/L' 0.0050 t 10122/1215:55 10867-8 -UPnylace,a;e ND rngfL 0.010 1 10/22/12 16:56 1D8-05.4 mny- chWride ND mcll O.00SO 1 t0722112 16:55 75.01-4 t1iP{i Xy'ene NO mg1L 0,0050 1 10122112 15:56 M601-23-1 a-Xylere NO mg/L 0.0050 10122112 16-58 95-4'i-6 Surrogates ' Llibrpmafiucronlethane (S) 110 % 70-130 1 10122112 16:56 1563-53-7 i 3f3 rtoRunrabenzene (S) too % 70-130 ' 1 10127112 16:55 -460-OC-4 : •70-130 -1 101Z2112-16:50 2037.26.5- 1',._-Die st• HF?,'r �:�;a) {'i .F-. ;.7�1 :"1 i.. SOf22?•.a15:55 i7C6C-9i-0••' 4.c_ r7er:o� s.:o:x -A dly'ica. -phemSE - ._ - 1t-1 .•�.}[rti "�i;7? i.. _ iC'271':21-J:.'ri: .i SF,{.tj:.j' .. .Oats: 2C1:52?lk. _ RERQ TG :LAoOR.A.OPYAtlALYSiS. %• stafS•lot bee,z�.:.0 .:�� r thv rr1:,6 co, :`_Pt'ef vets An?'Ki;af 7erV'C^s. `+:, • - - . - - ' Pace Anali-tIcel Ser,,Iees, Inc. Pace AneryticaF Serekn. trm. Pace Analytcal Svrvices, true, s ac PArralyticaf 205 East Mesta, Road - Su'te A 2225 Riverside Dr. 9800 Khcey Ave. Sure 100 r eny ayacvrn Elen, NC 2728E AshwvWe, HC 29804 HviWs)Te. NC 23073 (338)623-8921 (828)254-7176 (704)$MW92 i ANALYTICAL RESULTS Project.Storm Water 1(1115112 Pace Proffer. No.: 92135182 Sample: SOO #2 pH 7.0 Lab I6: 92135182001 Collected: iQH5112 08:30 Received: 1011511212:05 °dal^x: Water Parameters Results Units RE! pert Limn DP Prepared Analyzed CAS No_ qua[ 45COCNE Cyanide, Total Cyanide Analytical Method: StA 4500-CN-E NID rng1L 0.0050 1 10/25/12 15:26 57-12-5 Sampto: SDO #-3 pH 6.3 Lab IO: 92135182002 Coffered: 101161;208:30 Rscolved; 1011511212:05 1vlal6v Water Parameters Results Units Report Limit OF Prepared Analyzed CAS .No. Quaff 254013 Total Suspended Solids Total Suspended Solids HEA1, Oil and Grease Qil and Grease 608 GCS Pesticides and PC9s Anasy cat Method: SDI 2540D 33.0 rAg/L 3-9 1 10/10/17 08:34 Analytical Method, EPA 1664A NO mg1L 5.0 1 1012411211:16 Analytical Method: EPA 608 Preparation Me',1wd: EPA 3535 AWAn Nil;nwL 0.000060 3 1011611217:00 1011911222-30 3D9.0E12 alpha-314C Lip m9ft. 0.000050 1 i011511217:00 ;011911222:30 319-84-6 beta-BHC Np mg/L. 0.000D50 1 10/16/12 17:DD 10/19112 22:30 319.65-7 delta-81-10 NO mglL 0.00005D 1 10/16/12 17:00 ,0119t12 22-30 319.86-8 gamma-SHC (Lindane) NO mg/L 0,000050 1 10/16112 17:00 10l19112 22:30 56-89.9 i Chlordare (Technical) ND mg1L 0,00050 1 10116J1217r00 101i9112 22:30 57-74.9 4.4'-DpO NO mq/L 0,000050 1 10J1011217:00 10/19M222:30 72-54-8 ; 4,4'-DOE NO mglL D.CDO050 t 1D11611217:00 10N911222:30 72-55-9 4,4'-DOT NQ rnglL 0,000050 1 10i1cI1217:00 1011911222:30 50-29-3 Oietdrin ND rng1L 0.00005C 1 10/16/12 iT.00 10119112 22:30 6D-57.1 Endosulfan l NO mglL 0.00D050 1 IW16112 17:00 10l19112 22:30 959.98-3 f Endayullm II NO rng1L 0.000050 1 101/6/12 17:00 10/19112 27.30 33213-65-3 Endosul:arl sulfate NO mg1L 0.000050 1 101161,12 17:00 IQM1 412 22:30 1031-07-8 i Ertdcin ::,, NO,ingiL• 0000050 1 101161.12-17:00-101i91,2 22:30.72_7b-8 endrinaldehyde Np;m01L ' 6A07E)50 '1 S0f16117 17 OG #0119112 2Z3U ,;742t 43 r ; HeptacFrlor, ; ?: : - Np iiili. 0.000050 '10961.12 17 00. 1011 Q112 22:30 -.76-?4-8 _ HCptaGhior ept}xi p, NO mgil, 0.000050 1 10ff G112 17:00 10115/12 22:3Q :1024-67-3 PCQ-1Qt6{Aiodar,}016) Nq mg/L 0.00050 1 10I1511217:00 1011911222:30 12674-11-2 1?CE3=1221 (.hrgcoc122.) NO mcr1L O.a005O 1 10flQ11217',00 1011911222:3Q 11104-28-2 PCB 1232 (Arttctor 1232) NO mglL 0.00050 1 iU!}E/12 1T.0D 10119112 22.30 11141.16 5 PCB-1242 (Arador 1242) NO mg1L 0.00050 1 10/16112 17:00 10/19/12 22:30 53869-21-9 PCB-1243 (Arodur 1248) NID mg1L 0.00050 1 10/16112 I TOD 10119/12 22:30 12G72.29-6 PCB-1254 (Arodw 1254) NO rm1L O.00050 1 10/16112 17:00 10/19112 22:30 11097-69-1 FCB_1260 (Arodor 1260) ND mWL 0,00050 1 10115112 17:00 10119/12 22:30 1t096-8?.-5 NO MOIL., .... O,COO5D......1.. --.#4f15112-17:00. ;0I1911222:30. 800j 35-2 3lrrq l:ro-^•x': ^,•a (31 ?e 2Q 1.10 1. 101tc112'_17:40 3nfiEit2 22:C0 Err- a_ r5'ii - . ;.2n_73g' 1 1!7191i2 ;7:{1D 10?iW1222:s0, 2031.2e-3 t 2G".r" rtET 1 �? A a!VtIGz, \re:".:'j: F?r", ( .7 'Qre9aral!on Mi=t'lz E?A ",r'4.7; . - Lel.. C_a:e:1,lc_" ;2r•4.r�s _`r",=£t?FT!J Q+� T6,?Y` 1:Y5€^ PavelO.er70,:; (, •r'll. _ - pia :E_r �• ,Ct t2:{••r0�'::RC. °::rC^: - - -'ir�rr.: •� rr.;: c^:^�.es;i ct rr�e.r..a; -scrl'g-;Y�s. �:��.: :; �. i} ace Mews Frojeoi: Storm Water I0115112 Pace PmfedNo.: 92135182 Paco Anaryttcar Services, Inc. 205 Last Mraeo. Road - Soils A Eden. NC 27289 (336)60-e971 Pace Anatytkal Services, Inc. 2225 Rh*mrly Of. AshvQlo. NC 28MA ANALYTICAL RESULTS (828)254.7176 Pace Anatyttcat Services, lno. 980e KinwyAve. 5Jite lgO Flun'ersvllo, MC 28075 (7041e75-9092 Sample: S+30 Y,3 pH b.3 rwab !D: 92135182002 Coileoted: 10116112 08:30 Received; 1MI5112 ! 2:05 Nafrix: VOW, Parameters Resu::s Units Report Limit OF Prepared Anaiyred CAS No. Qual 625 MSSV Anai;liul Method: EPA 625 Prepara',Irr Method: EPA 525 Acenaphthene NO mg/L 0.0050 1 10/13112 15;00 10/20112 02:35 BS�42-9 Acenapi:thylenc ND mgiL 0.0050 1 10/18/12 76:00 10120112 02:35 208-9&-8 Acetophenone NO mgiL 0.0050 1 1011W12 16:00 1012(N#20233 98-86-2 Aniline NO 019fl- 0.010 1 10115112 16:00 10120112 02:35 62-53-3 Anthracene NO mgiL 0.0050 1 10/18112 16:00 10120112 02:35 120-12-7 E3enzidfnc NO [ng/L 0.050 1 10/18/12 15:00/0120112 (M35 92-87-5 eenzo(a),lafh(scene NQ mg/L 0 0050 1 /0/18112 16:00 10120112 02:35 58-55-3 8enao{a)pyrene ND mg,`L 0-0050 1 10//8112 76:OD HY20112 02:35 50.32-8 8enzo(F)lh:oranlhene %D mg1L 0,0050 1 10/18112 15:00 10120/12 07.:35 205.99.2 i 8enzo(a,11,i)pery!ene ND rnoL 0,0050 1 10/1811215:00 10120/1202:35 191-24-2 Benzo(k)flucrenthene ND rng/L 0.0050 1 10118/1218:00 1012011202:35 207-08-0 4-Brcmapherlylphenyl ether ND mg1L 0.0050 1 10/18/12 10:00 1020112 02:35 101-55.3 uutylbeozylphOle late NO mgiL 00050 10/18112M20 10MI1202:35 ?35.68-7 4-Ch:or0-3-methyfphenol NO mg1L 0,0050 1 10/18112 15:00 10120/12 02:35 59-50-7 bis(2-Chiaroeihoxllmethanc ND mgiL 0.010 1 1oil wl21b:00 10/2011202:35 111-91.1 bis(2•Chlvroathyl) ether ND mgiL 0,0050 1 10118/12 16:00 100YI2 0235 114-44-e l bis(2-Chloroisoprvpyo ether NO malL 0.0050 1 101/8/12 16:00 1012CJ12 02:35 108.5C-1 2-Chlorvnaphiholene ,ND mgfL 0.0050 1 10f18112 18:00 1020112 02:35 9 i R8 T 2-Chlcrophenol NO mg/L 0.0050 1 1011811216:00 1DMI1202--35 95-57-8 a-C.h'Mphenylphenyt ether ND rng)L a-0050 1 10118112 15:00 1012CI12 02:3$ 7005-72.3 Chrysene NQ rnglL OA050 1 10/18/12 MOD 101 OM 02:35 218.01-9 Dibenz(a.h)arlhramne NO mgiL 0.0050 1 10/18112 16:00 10/20/12 02:35 53.70-3 1,2-Dichloraoerzene ND rng1L C.0059 1 10118112 i6;00 1012V12 o2:35 95-50-1 i 1,3-Dioh;orobenzena Nn algIL 0.0050 1 10f1811216:00 10120A202:35 541-73 1 F 1 1,4-Dichlarobenzene NO mgiL 0.0050 1 10110112',B:00 1012011202:35 105--:6-T i 3,3'-Dlchlorabenzidirut ND mgfL 0,025 1 10i1811216:00 1M011202:35 91-94-1 ; 2,4-Dichrorophenal ND mgiL O.D050 t 011811213:00 10120112 02:35 120-fs3-2 Die'"Iphthafaz ND mgiL 0.0050 1 10118/12 ,6:00 10/20112 02:3$ 84-56-2 2;4-DfinethXipherlcl NQ mg/L 0.010 1 1011&1215:00 1Or40"202:--- 5 105-67-9 Dimethylph,thalote \0 mg,1L 0.6050 f 10I.M12 10:00 1 C72,0112 02:35 131-11-3 c1 n-butylph t!alata_ NO mgiL 0.0050 .1 -10118112 16:00 10(20112 02:35 84-74-2 e 5 f7initra-2{rr0thylpttenvl .- NDrrr I :.Q_02Q.... j...=..101 Gl.12:'6;00:>1�120112 92'35-:.535-52,t-._ .-. 2,a-f3i [UopFeFiol;_ ::;':' NDMgh_ 0.0511 A.::''..7olif3liz_;5Ot}.:'.1Dr20J`:z.o2:35 51'28'5 2'4-01niVatoluerie„ No mgfL 00050: '-'1 '-10118/1238A0 JW20/12.02:3S.+t2:l;14-2-:-_:.:: 2eR-t�in)Srolviuene _ N4 m_dl. 0.0051) t t01i3J12 i5:00 "1iA0112 02.35s606-20-2 al n (yfph6rdl to NO 1tg _ 0.0050 1 10/10/12 15:09 1=0112 02:35 117-84-0 I:2-DiphenyThydrazine NO rrgfL 0.0050 1 1011811216:00 10CM202:35 122-66-7 bis{2-Eihylfle�ryl)p!1t::aia:e NO mglL 0.050 1 101 8/12 16:00 10170il2 02:35 117.51-7 Ruwanlhone ND rnniL 0.0050 1 10118/12 MOE! Iot2011202:35 205-440 Fiuorene Ng mgiL 0.0050 1 10/t811216:00 10120112 02:35 "-73-7 -!sera lii^io_; s!+11zr_;en.+ AD_c/L 4.0^50_...: t iCr12.1121$:OO i^r2n112L!2_?a7fa3 : ' 1-c> h ti�•1 �r . , Il _ CNI2 ::i ) '.:-e:C•; ::ecA:l1�,-ere • fi:• ;.^.�':.. tliitr'. • .. 1•'3.':::1)2 5 `^ :'t01LC112 02.'�g...vr.,�;,5- ,. . 1 _' .:4zrC. . a1'4:r_ ' O.00S i... i iC111 [:12,?S:nE) a0r12 ^2:35 Se-i a-1. Indenn,, .2,: cd)pyren_ � :] n+� 0.00:1J . c iC;32l.:2 8: c0 20 'S t9333-: 1 L� is f14:.: i:.?ssi!: 0.010 1 •- ^ 10li li^',n;rR r. _ - 1 0.7:_ ..78 -.c _ f R-Pht -spe `7 xr�. 0,�05G 70i1�i121a.00.102^!:^,,'02:?5'51=�C_3 'F• on:ot' l.'11 of70 - r.'. - ' _ `•ier=,ar;s': eU n_;N i^^':'cC^': �xCs'1 i.'c7." - -=seals Af7alocal i Pace Ahx4tcal Strvkes, Inc. 205 Cast Meadow Reed - ". A Ed". r•rC 272U (3S6)8234921 Pace AnafytJcal Sm vkez, Inc. Pact AnaryJ"I SWY[C", Inc. 2225 kN-stde Dr U00 K'rncey Ave. Svl.e 100 AshMie. NC 2ae04 Hunlersvlve, NC 2607A (6Y6)254-717s (7C4)375-5�-2 ANALYTICAL RESULTS Project: Storm Water 10/15/12 Pace Project No.: 92135182 Sampla: 5DO43pH13.3 Labf0; 92135132002 Collected: IW511203:30 Rcceived: 10J1511212:05 Matrix:Walor Parameters Resofts L1nis RoportLirmit dF Preoared Analyzed CAS No. ©ual 625 MSSV Analytical-'Aethcd: CPA 525 Preparaficn Method: EPA 525 Niirobon;wne ND mgJL 0.0050 1 10116112 16:00 10120112 02:35 98-95-3 2-Mtrophenol Nfl mg1L 0.0050 1 10AW12 16:00 10120/12 02:35 88-75 5 4-Nitropherlo# NO mall- 0,050 1 10/18112 16:00 10120/12 02:35 100-02-7 t!-Nivosodir: ethylamine ND mg1L 0.0050 1 10/18ft2 15:00 10/20112 02:35 62-75-9 N-Nilroso-&II-PTopylaminu NO nrg/L 0.0050 I 10i1811216:00 10J20/1202:35 621-6A-7 WMrI sodiphenytzmirm NO mg1L (y.O1Q 1 10,8112 18:00 1012C11202;35 86-30-6 Pantachlorop enol NO rgJL 0.025 1 10118117 16:00 1012011202:35 67-86-5 Pharanthrere NO mgJL 0.0050 1 i01i811216:00 IC12VI20235 65-01-8 Phenol NO moll- 0.0030 1 10118112 16:00 10121J112 02:35 108-95-2 Pyrene ND mgJL 0.6050 1 1011811716:00 10/2011202:35 129-00-0 1.2,4-Trichiorahanzena NO mg1l 0.0059 1 401180216:00 102011202:35 120-$2-1 2,4,6-Trichlomphenol NOmQfL 0010 1 1W,311216:00 10J21JO202:35 88-0113-7 swrogates 1 43 % 10-120 1 10118/12 16:00 i0120112 02:35 4165-60.0 2•Fluarobiphe yi (S) 37 V. 15-120 1 i0J12112 18:00 10120/12 02:35 321-60-8 Terphenyl-d14(S) 70 % It-131 1 1011811216-00 1012011202;35 1718-51-0 Phenol-d6 (a) 15 % 10-120 I 10I1&12 16:00 10J20112 02:35 13127-83-3 2-Fluorcphenel(6) 21 % 10-120 1 10;1811216:90 1012C(1202:35 367-12-4 2.4-$-1ribromcphenul(S) 55 1/6 10-137 1 1011,9112 16:00 IW0112 02:35 118-79-6 624 Volatile Organics Anatykal :Method: EPA 624 Acetona NC mclL 0.025 1 10122112 17:14 67-64-1 Acmiein ND mg,'L 0.10 1 1=214217:14 107-02-8 Auylontirile NO mg1L 0-10 1 10122/12 17:1L 107.13-1 Benzene \rD r:1glL 0.0050 1 1012211217;14 71-43-2 8remcbenzene NO mg/L 0.0050 1 .(V27112 17:14 ;08-86-1 t3 omechlaronre07ane MCI mgA. 0.0050 1 1012..2112 17:14 74-97-5 8rolmodKhJorcnwVi;-ne ND rng1L 0.0050 1 10122112 17;14 75-27-4 Srowfurm, NO irq/L 0.0051) 1 i0f27J12 17:14. 75-25r2 Bromometflane NO mgJL 0.010 1 10122112.17:tA ;,74-83;9..,. 2 13u goons (rtBiC) .., ND mg1L .0.010 1 101271f2 i7;14 79-93-3 -- '.?n 8t.lylbienzene ::.... .•.. r: •,''•- -' - P.'C mnlL: -.- 0.005�7 '. 1.':1 ; •-- -: -: -:-:i017.2/1217c1a - 1{N 57-81- .•.:.:.. .. __ - lsect3uylbenxrnei0r2211217:t4.S3598-8 tert B�+yl( enzenc - ;. :: ND. maIL, 0 0050 1 ' :', '. ` W22112 17:14 9e-06-6 _ Carba i,Clsulfide','' 1 I�t].mO1L'" 10122i12 17:14 75-15.0 Carbon le6Jchieride 46 mgJL C.0050 I 10/22112 17:14 56-23-5 CNorobenzerre ND m91L 0.0050 1 10/22112 17;1» 103-90-7 cNorocthane IND mg/L 0-010 I IGIZ J12 17:14 75.003 Z-ChroruethyMriyi wher Nt? r:rylL C D 10 1 10122112 17:14 110.75-8 ChIcrc:orm = NUJ marL 0,0050 1 i0122/12 17:14 67-66-3 -rL•-C.�.. •y't �i .. - we R;�.':J'�3' - 1L-i/ -rr;: : � -_ f'.L i:31 : - n.'y.2r' " l•' !:'1 i - `•:J - - - - - - - CT:'^. .e^•• - - _ �'� it7ci� '),C...O i.,J2i.'�7•�1 r'i. i^7 - - - '.L''ijrCSCC^ i<^ 0.9050 IC42W,2 ;4i 124.4y-. ' ;C1.7•r`ih+om!+elh6ne IEDDI. - - \[1 rne:L •3.`°.759 - 1 •r/Iu12 751•.23-•t _ - - m.-.e Ic - Ala;c1L --. 0.0r'SO <'iit 9r:f4..7A_9 •' i•C vi;o u1:e.t; S • .. �C a:erF' ry nn_r iCl?711.2 1.7:4' _e,;61 ft�--C T C, RpATdRY.AA-ALY..la uS- 0-'- :iA9( r- -�'' - - - - •. ;Lri•ZV•t _ e vriCei / pate Analytical Servlcee, Inc. 2D$ test Mtsdcw Road - S j*e A Pace Anriyt{sal Services, ln0. 2225 Riversrde Dr. Pace Arrlyicel Somkv*, Inc_ 9800 K��cey Ave. S0e 100 I�WcekiafyVcal'a cdrn, VC MBS Fsrevare, NC 28804 HuMerswiRe, NC 28078 i r (3'4)523-492 t t8213j254417s t704)P.3S-90--2 ANALYTICAL RESULTS Project: Storm Mier0115112 Pace Rrojeclhto.: 92135182 Sampfc: *00 X3 PH 6.3 Lab ID; 92135182002 Cotfodod: 1,115112 08:30 Rocefved: 10115112 12:05 Matrix: Water Parameters Results units Report Limit ❑F Prepared Analyzed CAS l.o. Qua, $74 Volatile Organics An2tyaca! iv'L`thad: EPA 624 1,3-Dichlarobenzen, NO mSn- 0.0050 1 10/22112 17:14 541-73-1 1,4-Dlchlormboirene NO ma.+L 0•C050 1 i01Z2112 17;14 106-A8-7 1.1-Cicitiornotharro ND 1119fl- 0.0050 1 10/22/12 17:14 15-34-3 1,2-01chicroelhane NO mall 0.0050 1 1012211217:14 107-06-2 I,1-Dichlorcelhene NO mg1L 0.0050 1 10122112 17:14 75-35-4 cis-S,2-D;chforaellrene NO mg/L 0,0050 1 10122112 17:14 156-59.2 Vans-1,2-DicNoroethene ND mg/L 0.005n ; 10/22112 17:14 15"0-5 i,2-Dictiloropropane ND mg7L 0.0050 1 10/22/1217;14 18-87.5 1,3-Dic-Noropropane NO nxt/L 0.0050 1 10/22/12 I7.1e. 142-28.9 2,2-Cichtefopronrine NO mS1L 0.0050 I t0122112 17:14 594-20-7 1,1-Dich ropropene ND nog/L 0.0050 1 1012211217,14 563-58-6 c3g :,3 DldrlorpprCpene ND mg1L 0.005Y 1 IW2211.2 17:14 10051-01.5 trans-1,3-Dictvoropropene ND malL l?,0050 1 1012-1/12 17:14 100G1-02.8 Elhylbenzere NO mg,'L OMAI t 10/22112 17:14 100-41.4 Vezachloro-1,3-buladiene NU nrglL 0.0050 1 1012211217;14 87.68.3 2-ilexanone ND mg1L 0.010 1 10122112 17:14 591-78-0 ! lo4om,.ethone NO ma1L 0.010 1 IGWJ12 17:i4 74.58-4 t;opropylbeniene (Cumene) MID mg1L 0.0050 1 .MD12 :7:14 9M2-8 p-Is0pr0nyreolrren0 NO Ing& 0.0050 1 1007112 17:14 95-87-6 fAethyiene04aride ND mc/L 0.0050 1 lof2211217:1.4 75-09-2 4-1aethyl-2-ponlanone (1,119K) NO mg1L 9.010 1 1,3122112 17:1A 108-10-1 lie,hyl-ten-butyl ether NO mgll 0,0050 1 W12211217:14 1G34-04-4 Naphth,lone ND mgk 0.0050 1 10122112 17:14 91-20-3 i n-Prooylbenzene NU mg1. 0.0050 1 ':C122112 17:14 103 65 1 Styrene NO mg(L 9.0050 1 10122/12 17:14 ;00_:2.5 1,t,1,2-TeUachfcroethane ND mr11- @.D050 1 10/22/12 17:14 530-2046 t,i.2,2-Terachloroe:hane NO rng/L 0.0050 1 1012211217:14 79.34-5 TelfaG'10 oolllsnQ 1D m91L 0,0050 1 10122112 17:14 A27-18-4 Toluene i'ti;• ND rt:glL 1Q127JlQ 17agii08 88=3 r,;G122/12.1;i9.:871 1,2,3•Trichiorobenzene VD:ng[L 0.003d-_ i • Ei ' 1,2,4.Trichfarabenzenu .'NO rNk 0.0050 1 1.0122112 i7:14 120.82-1 ^ i;1;1"=T6011kooeihane _- - -jNU inulL 0.0050 1 10112112 i7:14. 7i-55-0 1;1';2'-Triihicr4eUiate': _ `.' '. ND,frr11:. 0.0)50 1 10/22/12 17:14 79-005 Trici[aroethene,, _: IVU rtg/1_ 0.0050 1 1072211217:14 79-01-6 Tiieh[croliuoromethane NO mc1L 0.010 1 10122112 17:14 75-69•d 1,2,3'Trdticr.propane ND-EJL 0,0050 1 101i211217:1d 551'# 1J.2Trichforotnlluoroeihane ND mglL 0.0050 T IMV1217:14 75-13-1 1,2,4:16metflylbenrene NO mg1L 0.0050 1 1012211217:14 95.62•5 i?,S-Triine,hyl9enzene NO mg/L 0,0050 1 1Cr2211217:14: •.08.67-0 Urryfacelata .NDmg1L 0.ojo 1 10122112,.17:14'.1C805-4. - .. 'rA'.i.;.f;:lei=: _ ••i,, tt�".iw . .-_ - ..x 4s.JC - - - - ';,'22: 7:1��':•ic'S- - '' `•'"• .... • . �F'� c:i. - .. ... �, rugri_ _ > s _t, _ :7,r ._ - _ 1012Z'1? 17:1:c :ClS:ore^�C:cmEihn =($) :65:1J6 70-13^. 1e122ii2.17:14 18C3-R3.7;••-• . ' 1?e °.6 - - 70-ia0-":;S• -- _ : 1Cl7•<l12�77:;4 "80-C'0.� _ .. •t. 7t:S+errs e($)n - - i• - - 2'-•7^_ - - _ .r0-._^0_ :i• _ •10.17.rlt257;1!''2`7:17Zri-•a, r! _ - oa1e:1013121 .2, an' ?� tr.�F.i Rt30�AT0�`l'APiF��1 cIS i.•. 1- _ fuyQ13.�`rC, :{ -_ ,'." _ : wP`•c�; n carsen a^sF^a S^n eF r_ 3 V: _ j. 'T •, aC ARa!}/l1L'al Pace AnalytlCat Servlccs, Inc_ P11C! Analytical Services, Ire- Pare Analytical Servlcelr, tnc. 205 East Meadow Road - S.P.eA 2225 R-*nAt Dr. 8800 KmCevAve. Suite 100 Eden. NC 27283 Achevdb. NC 2980A Huntalmlle, NC 28073 {3S5)523S52s (S211)25e..7176 I7CA)875-9092 ANALYTICAL RESULTS Project: Stone Water 141115112 P21:e Froject No.: 92135182 Sample: 5130,43 pH 5.3 - Lab ID: 92135IS2002 CoNm-fed: 10115/12 0c:30 Received: i0115112 12:05 bl-aOx: Wafer Parameters Resu11s UniL; Report limit OF Prepared Ar&yred CAS No_ Qual 624 Volatile Organics As a] f'ca1 tole:hod: EPA 624 Surrogafes 1,2•Dich(ormhen"A(S) 113 % 70A30 1 1012211217:14 17000.07-0' 420-4 Phenoliog, Total Analytical Method: EPA 420.4 Phenol 0.0058 mg1L 0.0050 1 TO/26112 15:38 109-95.2 450OCNECyanide, Total Anatyticalltelhod:S.%,14500-CN-E CyoniOe NO mg/L 0.0050 1 10r'6112 ',5:27 57-12-5 s Sampla: SDQ #5 pH 6.7 La5 [D: S2136182003 Collected: 10115/12 06:30 Received: 10/15/12 12.05 Ma;rix: Water Parameters Resvlls units Report Limit OF Prepared Analyzed CAS Na. Qual 2540D Total Suspended Solids Analytical'Method: SiM 2540D i Total Suspended Solids 10.9 mg/L 2.7 1 10/16112 08:34 HEM. Oil and Grease Analytical h10(hQd: 5FA 1654A i Oil and Grease NO mg/L 5.0 1 10/201211:17 608 GCS Pas ticides and PCBs Analytical Melhod: C-PA603 Preparation N•eihod: EPA3535 ; Aldr;n NO rrN& 0,000050 1 10/16112 17:00 10119112 23:22 3W-00-2 ; alpha-BHC ND mg1L (IM0050 1 I Orl 6112 17:00 10119//2 23.22 319-44.6 i beta-BHC; NO 1ng1L 0.01)W50 1 10/16/12 17:00 10/19112 23:22 31945-7 delta-BHC NO mg1L 0.000050 1 10116112 17:00 10119/42 23:22 319-85-8 gamnt2-6HC (Lindane) ND mg/L 0.090050 1 IOII W12 17:00 10/19112 23:22 $a-69-4 j Chlordane (Technical) '1 FO.,mgIL O.QU050 1 101161.12 MOO 1W19f12 23.22 57-74-9 2W-DDD NO,mgfl_ t1.COG1]51J, f ..'..i01161i2,17:00 i 10/19112 2.3:22 72-54-8 i 4,4%DDE ` ND rrlg L,: OOOQO50 ':'-1 . 10116/121700 ;i01191122322 ''4 •'" '-` O;OUODSO 'T 10116l12H7:00:;10119112.23:22,;50=29=3-:'' Dielarin" ND'mc/L 0.01=50 1 1p1T8112 "i-00; 10119112 23:P2':60.57-'I =. Endtisuilar� I ..; ND moll- 0 000050 1 10/16/12 17 1)D-�Cl.191i2,23:22 ;959-98-8' Endosvlfar, Il NO mg1L 0.900050 1 10116/1217-00 10119112 23:22 53213-65-9 i Eridosulfan sulfate yD mg1L 0.000059 1 10/18112 17:00 ',0119(12 23,22 1031.07-5 Erii Tin ' ND rg/L 0,000050 1 1011EJ7217:00 101t9112 23:22 72-20-8 s Emi rnn aldehyde ti'D mull_ 0,000050 , 10/16112 T7t00 10/19/12 23:22 7421-93-4 Hepmcycr No (ng/L 0.000050 1 IOIISI1217:00 10AS1122122 76.44-8 Hep,ac.:lorepoxide NO mall 0,400050 1 10(16/1217:00 T0/15(122122 1024-57 2 " PCB-1616IbVoO Jor.1016) ND.mg!L 000050 - t _ 10/16112 17:00 • 10/191t2 23:22 12874.11-2 F.C?-12??'l/�roCl:r1221+ NC:riglL .0:00050':..1 10i-12-1TO0 �19l1911223:22 11104-F2r2 ' y 'PC8 2:(F odcl124,.1 i<?'nia 0.�0:aIJ t'l01 n'f34 1 r'1 g 1 2':E_' •53d"'3-2i 5 n. `FC8=1248 fA:oalr• 12121' ld tr7�!L OIr"350 I. :1Q1:6112 1'.. •Q 1 ++.•.. 07 :1Z54;,Aro:lor 1254) ' \ry m 1 =`O.r!!vJ;9; - ':t " 't01,15112.17:GQ t01i£ii223: % i;C�;:6^ 1 a RC8-i20G.(Ar7:1^: 1 r5G) iii) € t:IL: Li.60050'::_ 1:: O1eri1L 1r 00 t�11?!12 23 i7 li^•33-?2.5 �. �: anp: �Z 17(jji• O.F13090: :1•;-'10J1Slt2:}7:+30•_7©119t:223:22•,500.-35-2 i REFOR i O^ ;-A,2C7R�tTQRY1ai4ALYSIS .. .:•::- -. .. ,.: , _: -_ - ter - - Blrrwa'S - - - - e AM1 :'fY.'G!i� : .;` ,r �t /7;aceAnapieal' i Projeci: Storm Water 10115fi2 Pace Project No.: 92t 35f 82 Pact Anoty' lCzl Sarvlcef. lw- 2C5 »tf1 f.!caC'7v Rzae • Suke A Eiden. NC 27288 (33s)673-as21 Pecs Anatrlie l Services, Inc. =5 Rivt r1* Dr. Ashe-,Ma, HC 28904 ANALYTICAL. RESULTS t82e1254-1178 Pate AnalyUul Servleea, Inc. SZOO Kixey Ave. Sutt_'00 *•'Ln!e.,vv0e, NC 2607$ (7 c74)a7S9;'a2 Sample: SDO 45 pM 6,7 Lail ID: 92135182003 GalleCed: 1011511208:30 Received: 1WI5112 12:05 0.latdr_ Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No- Oual 608 GCS Pesticides and PCBs Surrogates Tetrachloro-rr-xylene (5) Uccaehlorotiphenyl (S) 200.7 MET 1CP Lead 62S1dssv Ara!yticar Method: EPA60.3 P,eparabon?tethod: EPA3535 55 % 20.110 1 10/16/12 17:00 10119/12 23:22 877.09.8 77 % 20.138 1 1006112 17:00 10119112 23:22 2051.24.3 AnaWlical Method: EPA 20(?.7 Preparetlon Method: EPA 200-7 NO m421L 0.0050 1/0118112 17:35 101/9112 15:22. 7439-92-1 AnaiyJcz1 `.4cthoti: EPA625 Prepara0on Method: EPA625 Acenaphthene Nf) rngiL 0.0050 1 10/18112 t6:CO 101241t2 03:59 83-32-9 Acenaph;hyrene NO M911. 0-0050 1 M18/12 76:00 10/20/12 03:59 208-96-8 Ace!vphenone NO mg1L 0.0050 1 10118/12 16.00 10/20/1203:59 9846-2 Aniline NO mg1L 0,010 1 1C11$1121OVO 10/201120159 52-53-3 Anlhracene NO mgfr_ 0.0050 1 1Oil (VI 2 15:00 10120112 03:59 120-12.7 Benzidice NU n:g1L 0.050 1 10/18/12 16:00 1012.0112 0159 92-67-5 Uenzc(o)ar1hracene NOrrg& 0.0050 1 1011811216:00 1012011203:59 56-55-3 Benzo(a)pyrene NO mglL O.U059 1/01181/2 15:00 1Or0/12 03:59 50-32-8 Benzo(b)iluoramhene tip mgA_ t3.0050 1 W118112 MOO IU/2011203:59 205.994 Genzo(y,h,i)perysene NO mg1L 0,0050 1 10A8112 16:00 1 C120172 03:59 191-24.2 Bertxo(k} lu4:anthene NO rrglL 0.OU50 1 10/18112 16:00/01201/2 03:59 207.08-9 4-6romophenylpheny! ether ND myiL 0.0050 t/0118/12 16:00 10120112 03:59 101.55-3 i Butyl azyrph;halate NO snglL 0.0050 1 10/18112 16:00 1=0112 03:69 85-68-7 e-Chlore3-mcthylphenol NO mg1L 0.0050 1 10/18/12 15:00 10/20112 03:59 59-56-7 tris(2-Clioroelhrx})meihane Nr) rng1L 0.010 1 Iu11811216:00 10)20:1203:59 111.91-1 bis(2-Ghloroethyl) ether NO mgfL 0.0050 1 1C11802 16:00 10,120112 03:59 111-,4-4 6s(2-Ch1oiu;soprgpyQ ether NO mg/L 0.0050 1 10/16112 15:C0 M40112 03:59 108.60.1 2-Chloronapnthatene MD mg/L 0.0050 1 101t8112lS:CO 10=0203:59 91-58-7 ' i 2-4311loropher l NO rnglL 0,0050 1 1011SM213:00 10/20/1203:59 95-57-8 ! 4-CWoronhenylphenyl elt:er NO rn IL 0.0050 1 101€8112 f6:00 1012011203.59 7005-72-3 .` r Ghrysene. NIO mg1L O.0Q50 1 10/18,112 15:00 IMM12 0159 218.0;-9 1JiCe1(a,h)anthracene. iJFl.rrg/L; • :. 0.0050 ? 10l181121B:Up 1nr20112 n3:59 53-70-3 [ 2 CEch oratenzene :. :; 1:D n15lL : 0-Q450 •. t .' 10/18112 1S 00 '19120112 01: 12 95-50-1 1301bh1oivbeniers`:' 1Jt3 ^1;1L 0.0050� ...1' 101i8112 i8CO,:10rp112-0359 54173-f .:.; 1:4 [3icRloioherizene`• ' PJ❑ r gr O.U050 1 'tU(18/12r13f0o' ! 3;3zt)iihlurcbenzldjne NO mg/L O.D2$ f IOlft1i1215:0U�;:tU120112,03:58• 9f-84=1 •,:," .. 2;4:Djch!orophenol NO mg1L 0,0050 1 10118112 €e:00 101<0112'63:59 'j7U t3.2 Cieihy9p'1thElate NO mg/L 0.0050 1 IOf18112 16:00 1Of20117 03:57 $466-2 ' 2,4•l7ime1hylp iersol U0 rr911- 0.01(1 1 10l16112 1f3:00 10/2OM 2 03.59 105 57-9 CiEnet4vlphthatafe NO mg/L U-0050 t 10/181t216:00 101201t209:59 t31-€1-3 ❑i-n-5a;ylph t+ata;2 ND m91L 0,0050 1 10/f8112 16.00 f0120/12 03:% 84-71-2 4.6-Dinit;o-2-rnethvlphenol NO mg{L -O.I?20 1 1pr18r12 13:00 .10120112 03:59 524.62-1 ;'- :2�:Riq{„bt•�nc - x�_-I^.r.. ,��[D•....;...i- �'�',r€2�„`��"'Ci�;1fi2.C3:5^r,ri1:-2°=5 - ?c�n't1�^-^ti 'a.7•DR.r. yrN n,.Y;i 0.0a`C.' 1. .,lei%58112`-5rry;i0Yc1I20a:5?:.rN:2r.7. - ;V�•l-'X.,I7i^hE'2i2;: •yi �;^IC .. 'J.C`^50- i.iu11c11215:".`.):..1?!%1112Q3`59 li7�v=:0_- ; 7:2-u;gh ,ysh4r;s;.:ng, D mn!L 0_0050: 1 'WIM12 :(is:9 ;012G112 03:59.'.122-CH-J. '- • 'bis{2-y(h}•�nex�rir`I�ai:!a .. ••�r'.ir�a.� 'a.aLSi`, '1 riilj,P112:c:e010r:gr1z05:89 •1T--1-7 - -• .. � _'Qa:e: iC4'3M7n12�rrJRT.OF i_AcOFATCPY kv 1 Fs�e.1:Ci - !•+ -- -.. __ _ --•^,'yiare�c.^.`sSzil•irEht:ep;`vd::c�_.r-:e,.tara•P:•'•''.. ... _ f - - _ - • _ - . Y.'^.`.7•: ;,M; tttK:A•r ^-�r:fe�l _ __ :1 i? A.:t;V--41 <1rry:CB's. Q/�� a '�C6 wy. `� Paco ArWocal Services, inr- 205 Fes: IJeatim Road- Suite A Poet An2rytkat Sorvltee, Inc. 2225 Rtversida Dr. Pate Analytical Sorvrcts, Inc. 9800 K"incey Ave. Suile 100 Eden, NC 272W A5!terpc, NC MC4 'i>rI"v ft. NC 28078 ,� (336;523-8521 f704)875.9a42 ANA1_YMAL RESULTS Project: Storm Water 10/15112 Pace Project No.: 22135182 Sampie: 5'JO iF5 PH 6.7 Lab ID: 92136182003 Copected: IVII5112 08;30 Received: 1G11E;12 12:05 Mmtdx: Water parameters 625 WISSV Results Units Reporl L:.'nit DF Prepared Analyzed CAS No. Qua] Arlaly cal %Iv-,.od: EPA 525 Preparation N,rlhed: EPA625 Fluoranhene NO rmg/L 0.0050 10118/t2 16:09 1LV20112 03:59 206-14-0 Fluorene NO mg1L 0.0051) 1 10/18/12 16:00 10120112 03:5g 86-73-7 flexachl4wm-1.3•butadiene NO mg1L 0.0050 1 101181t716:00 1012011203.59 87.68-3 HexachlorobenZene NO mg& 0.0050 1 10 UW2 t&:C-0 101201120159 119.74-1 Hexachlorocyclopentadiene NID rng/L 0.010 1 10l181i2 10:00 10IM12 03:59 77-47-4 ? Hexacllloroethane NO mck 0.0050 1 10118112 10.00 1WO112 03:59 G7-72-1 Irxfcno(1,2.3-erf)pyrcne ND mglL 0-050 1 10118112 16:00 IW..0112 03:59 193-39.5 I5ophofone NC mg/L 0.010 1 101/8/12 16:00 10.2011Z 03:59 78-59-1 Naphthalene ND rng/L 0.0050 1 10/1811216;00 1020112 03:59 91-20-3 Nitrobertzene ND moll- 0.0050 1 1011802 16:00 10/20l,2 03:59 98.95.3 2-Nitrophenol NO mg1L 0.005C 1 t01181t2 18:C0 fo/20112 03-69 88.75.5 4-Nl{rophenol ND mg/_ 0.050 1 10/18/12 18:00 10I20112 03:59 100-02-7 i N-t.itrosedimethylan•.Lne ND mglL 0.Q050 i 10MBA215:90 1CfzQ11203:59 62.75-9 N-Nitrosa-di-n-propylamine NO mg1L 0.0050 1 101181f218:00 101201120359 621-64-7 N-NitrosodtptenyiarniaM NU mglL 0-010 1 1CIi81i216:00 10/20lf203:59 88.30-8 Fen'.300rcphencl NO mg/L 0,025 1 10l1all 21$:o0 10/20/12 03:59 87-86-5 Phenanttlrene NO mglL 0.9050 1 1011BA216:00 10f10/1203:59 85.01-8 : Phenol NO angiL 0.0050 1 10/18112 15:00 10120/12 03150 108-95.2 ?yrene h:D mgrL O.Q050 I 10 RAZ 16:00 10f:0112 03:159 129-00-0 1,2,4=frichtorubenzene ND mg/L 0.0050 1 1Oil W1216:00 1MWI203:59 120-82-1 1 2a-6-Tri:1dorophenol ND m91L 0.010 1 1011811216:00 MUM 03:59 EB-06-2 } 5 wragates i : Nitrobrnzene-d5 (5) 59 96 10-120 1 101/8112 10:00 10120/12 03:59 4165-60.0 } 2-Fluorablphenyl (3) 51 oA 15-120 1 10118112 16:00 10120;12 03:59 321-60-8 Turphenyl<114 (6) 83 % 11.131 1 1Of! 8/1216-00 1020112 03:59 1716-51-0 PhenOt-d6 (S) 21 °A 10A20 1 10118112 15:00 10.20112 03:59 t3127-88-3 { 2-Fluorophenol (S? 28 % 10-110 1 10/18112 16:00 10/20/12 03:59 367-12-4 2,4.5-Titromophenol (S) 83 '% 10-137 1 10l16lI2 16:00 10120112 03:59 M-79.6 624 Voratile Organics Analytical Mailrod: EPA624 Acetone : , No 7ML 0.025 1 1 0122I12.; 7:33 6744-t.. :As(O;CirS.:' ND rTglL' 0.10 f 10ft2112tir7:33 `ep7d2-8 t . A' lonitrile •".:.::.`;:'. •.-...°.ra,:-�.,r1:-.l`.-.,,ht,D'rr; i try, �fl.1D:..'1• •.: ' .°:�"t0±72f1217.33�-1 ,r :. e8enzene;. B ron'.abenXene ---' _Nb r1g!(. • =-- :D.OV50,:• -'t '''-t012211 297:33--ti08-E6-1 8ramoch!aramethane NO nrglL 0-0950 1 ID122112 17:33 74-97.5 Lromodictdcromelhane ND rrg1L 0.0050 1 -0)22/12 17:33 75-27-4 Hromoforrl NO mgiL 0.005a i 10122/t217:53 75-25.2 - elUrr7f)rtethane ND rnglL 0.010 1 10-22112 17:33 74•t 3.9 - 213iet2n_�nr{P Eiq NO mg1L 0,010 : WW1217.-33.=78-93-3 2,1' 2 c,ti' i0^•�Er:c -N-1 r r;A* ,.4:5C ', . i0%�2;i2 i7 t>..3c C •3.- n.01C 17:33%75.1:•0 . - - O3rboa4al"zG`il :irt3. ir0 crgl_ _ C-^_Q54.. f. i0tZ2i1Gi7:33 S+j-23.5 i :Cnorcen;.dr? �`PeD..,p/L - tLrsE]" r•: 10r221i2-9r:33-f08-_?.i: , - - - 010 : : t^r7..rii,,ti7:S3'75 rs 3i C2.e''61: .2')12-r•4: 26M .L1.f;fi'CRYAYA a$ •C3 LY•�' PaaC,=o 70' iS�_ _ Cl-, 9t_eLiw _ t•.f1: _•; ;hg-a*.^.ten ��senl7. Pa�AS^. P6''N:aI $lne:cel,: - - .: - ._ - -k Z!20eAnalAcaf" +�rwraL�.r�r i pra;ect: Storm Water 10115112 Pace Projed No.: 92135132 Pace Analytical SeMce3, fn- Pace Andy" Servkes, Inc. PaceAnWyftal Servkes, Inc. 2CS SaV Alealew Road - Sune A 2226 Riverside Dr, 880014nmy Ave. Suite 100 Eden. Mr, 272W Ash"a, NC 26304 i wftrW09, NC 28078 � (336)82M221 ANALYTICAL RESULTS ;92iZ2.54.7176 (704)a75-9o?2 Samples S0015 pH 0.7 Lab D: 922135182003 Collected: 1011511208:30 Received: 10115/12 12:05 rlatrx: `1;a1er f aramelei5 Pe5u,l5 Units Report Urvit Dr Prapared Anaryzed CAS No. Gu3F 624 Volatile Organics Anatytzc-al Method: EPA S24 2-Ch!orcett ylvinyrl,dther ND mr.1L 0.010 1 10/22712 17:33 110.75-8 Chloroform NO mgfL 0.0050 1 '0122112 17:33 6T-66-3 Ch€aromethane ND mg1L 0.0050 1 10122J12 17:33 74-87-3 2•Chrorolcluene NO mgfL 0.0050 i 10,122,'12 iTa'- 95-4" 4.Chlarololuene NO mg1L 0."50 1 10122/12 17:33 106.43-4 0€brumoch1oromethane NO mgll. 0,0450 1 10122M2 1713 124.48-1 1,2-0ihro. sae:hare (EDBI ND m911. 0,0050 i 10/22/12 17:33 106-93-4 D€brumcfreftr�-- N0 m9it- 0.0050 1 10122/12 17:33 74-95.3 1,2-Dichlorabenzene NO mg1L 0.0750 1 1022112 17:33 95-50-1 11-Dlchlorobenzene NO mg& 0.0050 1 10/22/12 17:33 541.73-1 1,4-Dlchlorobenzene ND mgrL 01000 1 10/22112 17:33 106-46-7 1,1-Dich1crae:har1e NO mq& 0.0050 1 10/22/12 17:33 75-34.3 - 1,2-Dir-Norcelhane NO mg11_ 0.0050 1 MUM 17:33 107-06-2 1,1.DicNorcethene No mg1L 0.0050 1 90122J72 17:33 75-35-4 c€s-1,2-Dic-`<loroethene NO :ng1L 0.0050 1 10/22/12 17,33 156-59-2 trans-1,2-Qiphtoraeihene NC nigfL 0,0050 1 10MV12 17:33 156.60-5 1,2-Dichloropropanc NO mg1L 0,0050 1 10/22/12 17:33 78-97.5 1.3-0ichlaropropanr. ND mg1L U.0050 1 1W-20217:33 142-28-9 2,2-Dichroropmpane ND mglL 0.0050 1 10122/12 17:33 594-20-7 1.1-Djoloropropere ND mg1L 0.0050 1 10rZ211217:33 563.58-6 cis-1,3•Dichlaropropene NO mgfL C_0050 1 10IM2 17:33 10061-01-5 trans-l.3-0ir~'ricrc¢ cp8r e - 1D mgrL 0.0050 1 10127J12 17:33 10061-02.6 Ethylbenzene NO mgfL 0.0050 1br'2211217:33 10-41-d Hexachloro-1,3-5utediene NC mg1L 0.0050 1 10122./12 17:33 87-68-3 2-Hexamme ND 111g1L 0.010 1 10122112 17:33 591-7a-6 `adomeih me ND mgfL 0.010 1 /0122112 17:33 74-88-'. Iscpropyitenzefae (Cunene) ND mgfL U.0050 1 10127Ji2 17:33 98-32-8 p•lsoprapyltoluene NO mgfL 0.0050 1 101.W2,17:33 •9M7-6 r.'ethyieneCh€oride ND mgfL 0.0050,.: I. 1CI221T2:17:33 " 4-Methyl Z-clentanone (MISK) ND mgJL 0.010: '- `t ' a0/22112 17 33 i11t3 10 1 nlethyFied buyPelher Nq mgiL' 0.0050 1 10112l12 ,17 33 1634.04-4 ,.-- •', tJap!¢itielene, A . , 10122J12 1T 33 91-20-3 -. n,PFopytb�nzesle;,: .•'• ;-:.. -a=:- ..-.::'•:>ND._my1L:.: 0.0050 1 10/22/1217:33 103.65-1 Siyreile : !- : • .:.:. .. : ..::... .. .... .ND nJ21L 0.0050 1 10/22112 17:33 100-42-5 :1'J'1 •Te;raM70rualhano . ND mgfL 0.0050 1 1012211217:33 030-205 7�1.2.2-Telrcrlaroe tlana NOmg7L 0.0050 1 10122/12 17:33 7$-34.5 Tetrachlomethene NO mgfL 0.0050 1 1012211217:33 12T-18- vurene NO mg/L 0.0050 1 10122/12 17:33 108 88-3 1;2,3-Trichtorobenzene NO mg(L 0,0050. 1 1'✓/2211217:33'V-61-6 1,2,4-T,'kNnrobenrern No mgrL 0.0050 1 -WZZ712,17:33.. 120-82-1 - -- f.9.='^d.`�..eetP.are RD r••.rr_ : G,GG_i;.... .t :.90n?!72'1T:�'':7s_�5�5-• -_ - - ',7.-?r}C`r��dG: „r.� - q��rr�: _. = :t!.t ... �:.• _ '�1l... r... '_-il(1-w., __ :ratl:xtc"1117Lf1 = 17 r° �'1,•a . 1�127192 i733 1f_ag v . . ?,2.3-i�c: roprc;Er N7 r*1 (_ 0.005: 3 ,1DIM121.7:33 ES 1&:i 9,1,2 r ati:oai:r luorcelhac:^ • D. na:1; - 0.4050'; .1 =. :14i<2112 97:33 i5-13-; - j.2: ;:in><tRy!tenzsre NG.r{i.n- °0.0050 }{!2213z-I';:_- 953.r,. iwa:e: 0J?^.."101zCt:•2"-r,9. FEFORT OF LASOP.ATO YJ„.NAiYSiS`, _ rz%e i .a€.73 q.. ZE rt �-'_ a}vaC. . -, t I • ... _. _ ' . ':'7L':; ` : wr�C^.c_^s cnt of ?tc�'An a:ri=C[ SSf:�i:CE; trst - - - .._ _ - _ i Lti fif l�{ LCi! Pace Arufyt#col Ssrvlcw, irrc- 205 East We-,dow Road - SlIite A PacaPrutyKleal Servtcas, lne. Ms Rrve1+Cc -Dr. Pace Artatytic2i SerWeeg-lnC. 984o Kinsey,ave. 50e fOD I/f ! rden. nG 27288 (4-W)523-&9.21 Astieviae, YC 288J4 M283254-7 t TO Hunleravtlk, NC 26078 t704j875-SM2 ANALYTICAL RESULTS Project: Starm Water 10116/12 pace Project No.: 9713$152 Sample: SOO m5 p14 s.7 : -z'a l�: 92135182003 Collected: 10,15112 D5:30 Received: 10115112 12:05 Matrix: 14ratar Parameters Re5LiL5 Units F.eportUrnd DF prepared Analyzed CAS No. Qval 624 Volatile Organics Ana:yffCai Mr-•111od: F:PAG24 I.3,5-TrimethylSew.w ND mgfL 0.0050 1 10127117 T7:33 103-67.8 Vnyl acetota ND mgli_ 0.01D E 10122M2 17:33 108-05-4 Vinyl Chloride 14D rnq/L 0.0050 1 10/22/12 17:33 7$-01-4 m8p-Xyfone ND rngrL 0.0050 : 10/2211217:33 179601-23-1 -Xylene ND mgit 0.005D 1 10122/12 17.33 95-47-5 Surrogales tJi6romolluoromeltrane (S) 101 °L 70-130 1 10/22112 17:33 lEOS-53-7 4-Ocznnufuorotlenzene (S) 95 % 70-130 1 f012211217:33 460-00-4 Tainene•da (S) 90 % 70-130 1 10122M2 17:33 2037-25-5 1,2-Uichlorosthsnrt-d4 (5) 111 % 70.130 1 10122112 17:33 17060-07-0 420.4 Phenolics, Tomf Analytical leetisod: EPA 42.0.4 Phenol ND mg1L 0.0050 1 1012611.215:41 108-25.2 46DLCNE Cyanide, Total Analytical Method: SIM 4500-CY-E Cyanide NO mg1L O.C•050 7 10/26/12 15-28 57-12-5 Sample: SOO46 pH 6.4 Lab ID: 9213SI82004 CoVected: 10/15112 09:00 Received; 10115M2 12:05 Matrix- Ybler Parameters Rasvlls Units Report Limit DF Prepared Analyzed CAS No. Ouai 25400 Total Suspended Sofids Analytical Method: SN1 2540D, Total Suspended Solids 23.2 mg1L 3.2 1 101171i209:06 HEM, 011 and Groase Analyicat Mclhod: EPA 1664A G:1 and Grease . VO, mg1L _ 5.0 1 10/24/12 11-17 608 GCS Pesticides and PCHS Analytical ,Method: 'EPA 50.8: Pfeparalion'Mathod,• EPA 3535 - •:, . _ A!cr n; •;': NE7.'mg}L : " . O Otli36 r0 1 " 1013 6112 17 00 10119112 23:40 s 309 00.2 .', • • ' alpha B1iC ;,..:.:: ..:... . . ::::;'{ •` : tJD.`mgll O OJ0750` ' t 10116li2 17 00 g0l19112 23 a4 319-tt4n6,:; .. beia af?C hll] �g/L 0.7G305t) 1 a1 6Jj? r Q0:_io11'Ji2'23.40_13i9-95-I . deI 6HC NO mgiL 0.000050 1 10!j8l1217,00 101113112 23:aft '319.154.8 g3niir a?HIJC (Undaiie) NO ;ngJL 0.0000,90 1 10(16/12 17:00 10/19112 2140 58-29-9 Chlordane Crechnicat) ND mgfL 0.00050 t 10/16/12 17:00 10119112 23:40 57.14-9 4,4'-DOD ND mg1L 0.000050 1 10Ji8/1217.00 10119J1223-40 72-54-8 4,C-DOE No mgA 0.000050 1 10116112 17:00 141/9112 2140 72-55-9 4,4'-DDT VD ma1L 0.00ea50 T I0fI01.12 17;00 10(19112 23:e0 50.29-3 Ole4drin NO.rrg1L 0.000050 1 1C11.61.1217:00.1C119/[223:40 5.7-51-1 Ens^s.Itan 1 :1Jp n glt ...:U.ni1+}750 "_ '^71E17Z t•7:0r} .10119/12 23:40, :859-2p-lt E!'ai?mt.'ai'-s:: _dr t;U :iu1C:' ^0S•U0150" 1011;/1 .iif 7'.:N:fi?it2 23<50 :1n"si-Je_#S. ' ' Erdr;n- ' .. - "tdi3 -`Gr;L .. -:�O.C+O^0�0. 1"-SQlis'1•i2aF:6't1 19/15;i$9.a.0 7-Zri-e . . rfrrr, al:4�vcs Nr?GrSC750 - .:i '' 30;15112.37:00. 10ftW12.2 .Q•.74?.1-23 t - h[ep+,as"•17r - - ei! p,JC0050 • f ' :i ' . iMt5ri2_,17.70`• i011^ili s3:d4.`:75�<= ?p12c lOrnnOvidR i7 nLrl. DL�GL��:rO' il'e.i@1i2 ti:on 11}11@11'7_236r�• tL"_451-3; f Ca'.s:•tC/3^-.15]_C<<a?:`• ,R-EPCRi CF=LA QRAT0}?YANALYSIS, Ls2e13bf70 ~_gyp'. _ � - .`..,y .e,•._:.:- ��,,,.;::, i:.;�" Pace AnaWicalServices. Inn. PaCeAnatytkalSerr!tes,InCPace Ant!yticalSarvlcus,Inc. f ceAna& j N Za5 East Meg -tow Roil • SvxA 2225 Rheffee Or. KlnccyAvn. Su-:,e 190 / �" •J `- cden• NO 2728E Ashevii'a, NC 28804 NoMermft, NM 28078 (336)623-8921 (828)254-7176 (704)e75-?092 ANALYTICAL RESULTS Protect: Storm Water 10115M Pare Projeet No.: 92135182 i I� { 4 ! i Samprs: SDO "•r6 p116.4 Labill). 92135182004 CG1ec ed: 101i5112 09:C0 Received: 10/15112 12:05 Matrx; Water Parameters Results Units Report Limit OF F Opared Analyzed CAS No_ G1ual 608 GCS Pegticldes and PCBs AnaV.6=1 A1e:'1oc: EPA608 Freparatien A19thod: EPA3535 PCB-1016 (Araelor 1016) ND woo, 0.00050 1 10/16112 17:00 40119/12 2$:40 12674-11-2 PCB-122: (Arollor 1221) MD mg/L 0.00050 1 10/16/12 17:00 10I19/12 23:40 1110E-28-2 PC13-1232(AroJor1232) NDrnglr 0.0001) 1. 1011611217:00 10118/1223:40 11141-16.5 PCB- 1242 (Arocim 1242) MD mg1L 0,00050 1 10MG1121770D 1011u/1221:40 53409-21-9 PCB-1248(Arodor124E) NDmg/L 0,00050 1 1W611217A0 I LV19112 23:40 12672-29.6 FCE-1254 (Aroclor 1254) MID mg1L 0.00050 1 10116112 i7.t70 10119/12 23:40 11097-69.1 PC13-1260 (/ mclor 1260) 140 mg/L 0.00050 1 1011G/12 17:00 10119il2 23:40 11096-82-5 { Toxaphere WD mn/L 0.00050 /0116112 17;00 10/1n112 23:40 6001-55-2 5vrroy�tes 7g rachlora•m xylenc (S} 63 % 20-110 . 10/161/2 17.00 10/19/12 23AD 877-09-8 Decachlorob;phonyl(S) 58 % 20.138 1 1011611217:00 1011911223:40 7..051.24-3 200.7 MET ICP Anatykal f*tilcd: EPA 200.7 Preparation Me' hod-- EPA 2017 Lead 1+10 mg/L 0,0050 1 1C/18112 17:35/0119112 15:29 7439-92-1 625NSSV Analy,iCa[1+Ie:1co4:1;FA625 Preparaticn Method,. EPA 625 i Arenaphthene IVD rr -/L 0,0050 1 10/18/12 16:00 10/22112 22:32 63-32.9 ACeraphthyrena NO n3g1L 0.0050 1 10118112 16:00 10/22/12. 22:22 208.90-8 Acetophesone NID mglL 0.0050 1 101181t2 16-00 10/22/12 22W 98-86-2 Aril4l a 1q4 rrlg/L 0.010 1 10/18/12 16:00 IW2112 22:32 62.53-3 i Anthracene ND mg/L 0.0050 1 101181/2 16:00 10/22/12 2.2:32 120.12-7 Benzidine QED m91L C.050 1 1011811216:04 1WWI 222:32 92-87-5 Banm(a)anihraoenr: ND mg1L 0.0050 t t0116112 1.6:00 10122/t2 22:32 55-55-3 's Benzo(a)pyreno ND mg/L 0.0050 1 101181121&00 1C/2211222:32 50.32.8 &nzo(b):iucranthena 140 mg1L 0.0050 1 10/18/12 16;00 l(22112 22:32 205-99-2 E3enzc(y,hjl,perylenc N13 mg/L 0.0050 1 10/18112 16.00 10122i12 22:$2 191.24-2 aenze(k)Sluoranthene NDmg/L 0.0050 1 10/t811216:00 1, 0/22112 22:32 207-08-9 4-Btam:pherylphenyl ether NO mg/L 0.0050 1 70118M2 76:00 10J22/12 22:32 101-65-3 Buglbanzylph:harass ;MR,rna/L ; 0.0650- •.,1 10/7811216:90 101221'1222:52 55-68-7 4-Ctloro-3 0ethylphenol :'NiJ'iir3R- ",0,005,0.. • 1 ;-.1RI181..12.16A0 • 10172112,22< 32 59-50-7 t Ci:tore thsxy)m<e6halle ND.mg1� '.O.C1I1 • . 1 101181,1.2 16 00 '.10122142 22,32..111 91-1 } b=s(2'Gt!Fcrpethyl) ether : `ND mg1L' = O.0050-'' 7 10118/12 t6 00 a[1/22112 22 37 11t.44 Ch'loroiso�riopyl)e:her Nb'rig/! 0.0050 10/t'8l12'16:CO3=1022/1222:32FtD360=i,"" 2Ghlaionaphttialeno' No mull. 0.M50 1 101.181i21$tfpr'tW22/t2.22:32,,6 r,,i7,, 2-Chlaraphenor '' ND mg/L 0.0050 1 l(VM2 16:00 10122l122a:32; 85 57-8 : 4-Chiaropherl,)phenyt emer ND me/L 0,0050 1 10/18112 lC00 10122/12 2282 7005.72.3 Chrysene ND mg/L 0.00!0 1 ,0(18tl2 :8:00 102-Jl222:32 218.01-9 Dlbenz(a,h)antr,racene W)mg& 0.0050 1 !GAW1216.00 10=1222:32 53.70-3 ), t.2 E icfiic(obzrzenc (0 mg/L :0.0050 1 10/18/12 16:00 1g122112221.32 95.50-1 1,3 ]ichlarcu rcer g ND.mg1 L 0A650 1 401/8/12 1S:01) . I R2112 22:32 ; 54,773-11 n r0?s: !,-5,r 4r-:i` •-rs ^^ 0 .i:: 1(1?.£r1c S va 10lrz/s222:2� �5 -4G•7: - .;. 7. .2,•=-t'ictlwoa :-i: i6/t3';2 6:^ 'tOnz/i222 12 z 'J• Y2 7ietn ;p`t`ah.:4 \D c.'L O.C^50. 10/➢f'l12 :5.C^. 0/22:12222 -66-2 2,4;D2met7y:pEsn^l r\rLi' clL C.�iO 1, ',Cll.-V12116:00,7(3122/1221.:?7 165.67-9- Oir^A:t:ripO.r305rJ E 10!'rJ12 11 :00 in12.2.112 22:22 131• .i1-3 = • REFORT'OF-E_ABORATORYANALY•SfS• 2gg19ol:q;?: TL o�"" mat i1 "Ste'2SS}^sf �rricrs'rnc.:' - - -- t{ I e �ZeAnalyfical Paw Anayncal Servlees, irm. Pacm Analybul SoMc", Inc. 245 East =Meadow Road _ Sul s A Z225 RNMr Je Dr. Pacl Analyticat SarYi.- ,T=_ 5a00 x4xty Ave. Sure 190 Eden. NC 27206 AshM!te. NC 2$004 Hume sv0s. NC =78 (338)623-d821 (9281254-7178 (704}875-"2 ANALYTICAL RESULTS Praecl: 5tarm'+Yater .0115112 Pate Froject No.: 92135182 Sample: SOO #6 pH GA Lab ID: 92135182004 CnReCted: 10115112 09.0G I4ecOved: 10115112 12:05 tfatrt: Water P2r2meters Rcsulls Units Report Limil OF Precared Anelyzed CAS No. Qual $25 MSSv Analytical Method: EPA 625 Pleparatiun A4elhed: GPA U5 Di-n-ttt;tylphlhalate NO mgIL 0.0050 1 10/1811216:01) 1D12211222:32 84.74.2 4,6-5]initro-2• rrelhylphenot No mg& 0.020 1 10118112 15:0D 1GR2112 27. 32 534-52-1 7,4-DiniLrophenal ND mg/1. 0.050 1 101tall 2 16:00 1022112 22:32 51-28.5 2,4-Dinilrc;aluene ND mg1L 0.0050 1 1011&1216:00 10/2211222-32 121.1--2 2,6-Oinitrotoiuers NC mg1L 0.0050 i 10118/12 16:00 10/22112 22:32 606-20-2 Dt-n-octylphlhaiale NO mglL 0,0050 1 10/18112 16: DO 1O122Ii222:32 117-84-0 1.2-Dlphenylhydrozir;e ND mglL O.G050 1 10118/12 16:00 10/22112 22:32 122-60-7 bls(2-Ethylhexytjphthalatw NU rng1L 0.0050 1 1011SA216:00 IC12211222:32 117-81-7 Ruoranthene NO mgrL 0.0050 1 10118/12 16:00 10r27Jt2 22:32 206-44-0 Fluorene ND mglL 0.0050 s 'Of-,&(12 t6-00 10122112 22:32 86.73-7 Hexachlorn-1.3-bu.adiene NO mglL 0.0050 1 10118112 1&.00 1WV12 22:32 87.68-3 Hexachl0rc4enzene NO mg1L 0.0050 r 1011EIi2 IU3Ofj :Or2?J12 22:32 118-74-4 Hexachlotocydc--pentadene NO mg1L 0.010 1 t01t611216:00 1G!22f1222:32 77-47.4 :•lexac.'ilorealhare NO mglL 0.0050 1 10/18/12 16-00 10122112 22:32 67-72-1 ; Indelle(1,2,3-cd)pyrene NO mgrL 0.0050 1 10/1&i216:00 10122A222:32 193-39.5 Isspharorsc NO mg1L 0A10 1 101'811216,00 10122A222732 76-59.1 Naphthalene NO mglL 0.0050 1 i0!181,216:00 10r22J1222-32 91-20.3 Nitrobetstene NO mg1L 0.0050 1 1011&;1216.00 1Or2211222:32 08-0-3 2-Nltrapl enal ND mg1L 0.0050 1 10116112 16:00 10/22112 22:32 88.75.5 i 4-Nitroghenol NO mg1L 0.050 1 1C!1811216:00 10122(1222:32 100-52.7 N-144'tosodinlplhylamire NO mgiL 0.0050 1 10/18112 16:00 10122/12 22-32 62-75.9 N-Nitrow-di-n-propyWnine NO mgiL 0.0050 1 10/1611216:00 10122JI222:32 621-64-7 E' i N-Nilrosodiphenyl=_mine NO mg1L 0.010 1 1C1i8117. 16:CO 1012211222:32 85-30-6 Pentachio-op'teml NO mglL 0.026 1 101'811216:00 1012211222:32 37.80-5 p Phenarlth(ene NO mg1L 0,0050 1 1oil 811216:00 1 Crs2112 22:32 85-01.8 Phenol NO mylL 0.0050 1 i0118112 16:00 10122112 22:32 108-95.2 r E rlyrene NO my)L 0.0050 1 10/18112 16:00 10122/12 22:32 129-00-0 1,2,4-TrjChlor0jaPr1z6nL NO mgiL 0,0050 1 1011&1216:00 1022J1222:n 120-62-1 1. 2,4.6-Trki tcrcphenol NO mg _ 0.010 1 i0118112 16:00 10122112 22:32 88-06-2 I Nitra's6nzene-d3 (S) 58 % 10-120 1 10!18l12 16:00 10/22112 2,2:3x -.4165.6U-0.',' 21ludrob horyltS} : 52,%.,• 15,12D i i01ie1121600 4i22lt2'222 327 80- ;'.::1.,:_.;;•;:', • - ' . ' ,: erpheoy! d14-(5};:' 79: P6 • ., 11.13, . :1' - _:1Of1&.12 -1. 16 00-1.0122J12 22 32. 17i8 5T=(S , '• v ?'jenvl d6 (5} :• �.t 7 a). . ; 10•120..- - 101181i2,15 00 '-lU/22/72 22 32 •:1312T.-86-3 i 2 Ftiio(opherol{5} 25.°!. :1042Q•-::.1 SW:B/12,16. -AlDI 2li222:32 387-12-4 f 2 4.S-Tribrcrnochencl(S) 94 % 10-137 1 1011&12 15.00 10/22/12 22:32 118-79-5 624 Yolatile Qrganica Ana. tical Method: EPA 624 . Acel4Pe ND mr,/L 0.025 1 iO.W112 17:51 61-64.1. I acrvlpin- , NO mg& 0.10 10122f12 17:51 :107-02-8 i . r •" Av;lt.:••r :._- _ -- a\t7".ztglL ''' 'R. ;0'_ i0172/i2'17:51::- _ •n•r (1C-_ 4''r '•T,' ' t%2_J1'< 17:51.`i7a?{r1.: "❑ er icu'ri�.;r,,_ ,-_ _ VOL21:L 17:91.' - Bc nsd°o��erea:p iD `14/# 0.4050 t.; tCl7_zn7. 17:9i ;.rS z7 4- L;rnme_airy' t4 in�.K Q.t054=- -1= 1WXZ2 2 7i:51 '7fi-25 2A. ea;: ~'hb �1c)L �� O.rJiO ? c; 10 2r 2 'De'_'4' Lv1'2912.rcSZP?.i r.EF91;T.OFIA3QRATQr'tY-AiY6,i:YSiS:-:' �agc24vlr;G: p= :`W:7114 Hr`"C•1 LC b! `t(._A ay^Cat SQ:vi��S, if`C„.. _ _� a aCCAnaWCal II�NiOST Pvoiecl: Sio11n Water 10115112 Pace Projotl No,! 92135182 Pace AnslyV"l Semicts, lric. 205 Earl, Mewlo Roid - SAC E6m. MC 27295 (336)52345211 Pace Anslytical Services. 1rkr- 2225 Rivamica dr. silevxa. Ke 2$> nt ANALYTICAL RESULTS 1828j254-717g Pete Anaiydcal Servicaa, Inc. 98L: Khcey.A a $upe 100 HUntemv!'3e, NC 28073 (T04)87S9= Sample: Sao #G pH 6.4 Lab ID: 92'1351132004 CalfeCed: 10115/12 09:00 Received:/0115/12 12:05 Wkrix; Water Parameters Res[sRs units Reoort Limit DF Prepared An2lyzed CAS No. Ouat 524 volatile organics Analytical lAcIh0u: F-PA 624 2-80anone (MEK) NO mg1L 0.010 1 10122/12 17:61 78-93-3 n-P,utyibenzene 114 mgll. 0.0050 1 1012211217:51 404.51-8 set-8ulylben7ene ND rngtL 0.0050 t 10/22172 17:51 135.96-8 tert-Butyibenzene ND mglL 0.0050 4. 1=2112 17:51 98-05 6 Carbon disulfide 140 mg1L. 0,010 1 1C122112 17:51 75-15-0 Carbon teVachler+Ce ND mglL 0,0050 i 10122112 17:51 513-23-5 Chlombenzerle ND mg& 0.0050 1 10/22/12 17:51 1t a-90.7 Chlorue:hane ND mglL W)lu 1 10221521T51 75-00-3 2-Chloreeihylvinyl ether N0 mg1, 0.010 IW22/12 17:51 110-75-8 Chloroform NO mgiL 0.0050 1 10122/12 17:51 67-56.3 Chlommedlare ND mglL 0.0050 1 /0122112 17:5, 74-87-3 ! 2-Chlorotcluene N0 mglL 0.0050 1 10122/12 17.,51 95-49-8 4-Chlorotoluene NO mgiL 0.0050 1 M22112 17:51 106-43-4 Dibromoartoromethane fiD rng1L 0.0050 1 16122/12 17:51 124-48-1 1,2-Dihromoeihane(EDG) NO mg1L 0.0050 1 102211217:51 106-914 'r Dibromomethane IlD eng1L 0.0050 1 10122/12 17:51 74-95-3 1,2-Mchlcrcbenzene ND mg1L 0.0050 1 1G122112 17:51 55-50-1 1,3-Diehlorcbenzer.a R0 mg1L 0,0050 1 f0/22112 17:51 541.73-1 1,4-Di0larobenzene N0 nrg1L 0,0050 1 10122/12 17:51 106.46-7 1•i-C]ichloroeLrdne ND mg& 0.0050 1 1GfW1217:51 75-34-3 1,2-Dichloreethane MD mg1L 0.0050 1 1017.2i12 17:51 107.06-2 1,1-Dirhloroethene N0 mglL 0.0050 1 10122/12 17:51 75-35-4 cis-1.2-Di.hloroeiheno No rrgrL 0.0050 1 11N22.r1217:51 156.$g-2 trans-1,2-DioNcreeihene NO rngA, 0-0050 1 10)22/12 i7:51 156.60-5 1,2.0i:hto-opropsae xO m9it- 0.0050 1 10122r'12 17:51 78.87-5 i 1.3-Dichloropropane ND mgfL 0.0050 1 W12711217:51 142-28-9 2,2•Richlorapropare NO rng L 0.0050 1 10122112 17:51 594-20.7 1,1-DiGtfOro>mrrne N U mg?!. 0.0050 10127Jj217:51'.$63 S&6: cis-1.3-01chloropropene NO mg.'L '0,0050 s 10r22112 t7:51 1008i_fl 5 Brans-1,3-dichloroeroper.e P:D mg1L O.EID�aO `-..1 : • •. - 701?2i1.2-i7.51 10081-_02,6 '.Ethylbenzene.; .. wD rnglL -m'a.005Q :'`.i- ;'.1C71221121fi61 ,`1001 4 - 1 Hexanore , ,NR mgtC: 0.0t0 "1 til1221t2 17:51 591.70 6 aodorr elharie.`: IL 0.010 1 10122112 17:5 i 74.88.4 Iso1}ropyibenzene (Cwnenej`''" - i3'mg1L Q.0050 1 10r22112 17:51 98-82-8 e -r-.Ar _,... p:lsopropylsoluerte ND mg(L 0.0050 1 10/22/12 17:51 99-87-6 Methylene Ct' ,ide NO nlgA- 0.0050 1 10122/12 17:51 75109-2 _ 44/ethyl-2-pentanone (MISK) N1) mg1L 0.010 1 10/22/12 17:51 '108-tU-1 Vlethvf-;ce htyl ether NO mglL o.4650 1 10122M 17:61 1634A4-4 Naphttlaiar:e NI) Mgil- 0,005.0 1 10122112 17:51 :91 20.'3 . ---a.CRSO- 1.1 r _0s+ tiD:^i^. _ �•0D3:'}'_ �012^. J 1� vI ie TeL•echlcr0 "t err," 'ti 4 r _1L :Q:n_C?t? - :7 t^/221.2 17:51 ::127;1$-� • ''• Tn•, a\!O01wt, n.0050:. '1'. jot22112:1T51''n8%83' - i.t;-Trc1!arccr^zs+ir- tip rec+l_ O.;iCSd ''i•' i12211217iS; •°,7-515°'__ cx,s-101'17SQ;2e3:5i!'lti E. f2T'OF_L1EO7-ZATORYAINl1LYSr3:, '.Pace2l.r_fn ��• : _ _ ' 7pi� -as '19C t'e.Mprmute4. 9 ^pl In N ., .. -Face A-St!!Tt!STnrr�s,L_ - y. j Pacest knatyllcal Se, 4cea, Inc. Pece Analytical Sxvicos.Im PaLeAnalytIcal Swkes, tnc. /! aC6AnalVt(� 2C5 EaMeadew Road - SGBe A 2225 Rrvemkle or. D600 KisceyA; v- SYRCCe 1 Eden. SIC 27288 AcheWti, NC 288C6 Hunlers Me. XC 2807D a/ (398)6238921 (826125s-7176 (704)675.9092 ANALYTICAL RESULTS PrcjecL' $form I ter 1C/15112 Pace Project No-: 921351,82 Sample: SDO 96 pH 6.4 Lab lD: 92135182004 Collected; 10/15112 09;00 Received; 10115I12 12:05 142tnx: VvItP-r Parzm iers Results Units Report Limit DF Pr9parerl Analyzed CAS No. Qua# SZ4 Watile Organics Analytical Method: EPA624 1,2,4.Trichlniobenzene NO n:giL 0-0050 1 10122M 17:51 12"2.1 1.1.1-lrichloroeLhane NO mglL 0.0050 1 1027.11217:51 71-55-5 1,1.2-Tiichloroelhane NO tng/L 0.0050 1 1022112 17:51 79.00-5 Tlichlorcethene NO mg/L 0.0050 1 IM2112 17:51 75.01-6 Tvich#aroiluoromeihar',e ND mg1L 0.010 1 W/27J1217:51 75.694 1,2,3-Trichloropropane NED mg/L 0-0050 1 1122112 17:51 96-13-4 1.1.2-Trichtorobilluaroetharte NO rng/L 0-CO50 1 10)'22?17. 17:51 76-13-1 1,2,4-Trimethy%enzene AND rng1L O.0050 1 1012211217:51 95-63-6 1,3.5-Trimethylbenzene, ND mall. 0-0050 1 1017.2M 17:51 108-67.8 Vinyl ac la:c ND mall. 0.010 1 10/22/1217:51 1DS-05.4 Vinyl chlorine ND mg& 0.0050 1022112 17:51 75.01.4 msp-Xytcne NO mglL 0.0050 1 10/22M2 17:51 i79601-23•i a-Xylene SD rngil• 0.0050 ; 1022112 17:51 95.47-6 Surroga[ps gibsomolUorome:har_ (S} 101 %, 70-130 1 10122112 77:51 180-53-7 4-Brurnoiluorobanzer.e (S) 103 % 70-i30 1 1=2712 17:51 460-00-4 Tuluerre-d$ (5) 96 %a 70-130 1 10/22112 17:51 2D37-26.5 1.2-Dichleroethane-d4 (5) 113 % 70-120 1 io/22112 17:51 17050-07-0 4W-4 Phenolics, Total Analytical Method: EPA420.4 Phenol NO mail_ 0,0050 1 IO/M1215:42 108-95-2 450OCNE Cy -ankle, Total Analy'ical athcd; SfA 4500-CN-C- Cyanide NO rngiL 0.0050 1 WM12 15:29 57.12-5 Samp;e: $DO 07 pH 7.0 Cab 10, 92135182006 C011WA-d:, -10/15112 09:00 . Received: 10/15/12 12:C5 Mlabix: Water _ Rarameters Resells Urnts 1Reaort Limn :: DF ;.''Anatyzeu ; :--'CAS \o.'. Qual ' 25 0D Total -Suspended Solids Analytical Method: $M 2540D To,a1.5u5pended'.Solids '. "5,5 mg1L Z.5 t 1D/16112 08:35 aiE ;.0 and,6ea;o Anai/lital Method: EPA 1664A 04 and Greasu ND moll- 5,0 1 W/24112 11.11 608.GGS Pesticides and PCBs Analytical -'Method: EPA60a Preparation Method: EPA3535 Aldrin ND.mglL "-0.000050'' i=10/47112:16:20 1Oil Oil 223:57-309-OU2 ©Ipha:BF?CI IM rrlg?L - :O.000050 1 :10117112 16:20- •10119112 23:57 319-84-6 • �• ?}4 m 7 h.000[15r 1 . 7117112 8 0 ,.011 ¢I - 2 .•il..,l..t, - •�;)-tio.rE' � J.O....rJti:" �_itlfi-:1i2_ :5:26i��_ ..�F-a ., iLi: Ur.=_ _ k. ..:� .-1?..�aJ,.'7 • '.iUliSl1� .o.2}',1_!+.lia�2...7�• n3•t..•:1. 1L.:nc.'!. ili7l2_tit?:2A 1Cr9£11Z23:L•ir �7,r'•:-y i r_CD? •C ncll- 9.000050 tOtir112 i6:20, i01i2:^.223.37;'l2.54.3 N� l toil.: O.00nO$G :;:_1. ^', 1J'i71121`fa:ZG 1Gf i4fi2.23:57° '.CDT i^l1,Ij7;5i2O i0IiE?:223:57;'ry.2_:t- -_ -L'zte'nr".22012-C4:5zniv_- :, �'EF.G1 i. #JanCRAT Y i� Piice22o1TC= i= This' Y-�aii^ :e rC"r�ryr�w �.ce^Lh •,j7- - - - - - /S - r:,i:Q<i;.'1C:•=T^+l,.i':f?1t Gri?L411^.'y;ic?'1 s:rY�_SF,:M_'. �.. - •. - - ,- �EAllc�tr�l�c7ja r - rNm'.p�tl;S.tAn April 16, 2012 Mr. Darrell Freeman Neil McLain 523 S. New St. Eden, NC 27288 Pace Analytical Services, Inc, 205 East ASeadaw Road - Suite A Eden. NC 27288 (336;623-8921 RE: Project: Storm Water 03/31/12 Pace Project No.: 92115467 Pace Analytical Services, Inc. 2225 Riverside Dr. AsheoUe, NC 2880t (828)2 54-7 t 76 Pace Analytical Services, Inc. 9so01CrnceyAve. 5ui:e t00 Ht,me,wVe. NC 28078 (70a)875�9092 Dear Mr, Freeman. - Enclosed are the analytical results for sample(s) received by the laboratary on April 02, 2012. The results relate only to the samples included in this report. Resuits reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the saraple annlyte page for anaiysis unless othertrrise footnoted. if you have any questions concerning ;his report, please feel free tc contact me. Sincerely, \ _J ftxgL_ Terri Page terri.page@pacelabs-corn Project Manager Endcsuras REPORT OF LABORATORYA14ALYSIS 'Etas reper; sn;i; r•,or as r€ xlw+ced, except in'crll, r,:lhatn the xri:len cnnsenl of Pace A.nalylical Services, !nc.. ?age 1 a. 85 % ceAnalytical mnr Wcfll:s.pn Project: Storm Water03f31A2 Pace Project No.: 92115467 Pace Analytical Services, Inc. 205 East Meadow Road . Suie A Eden, NC 27263 (336)623-8921 Pact Analytical Services, Inc. 2225 P.ivers[de Cr. Asheville, NC 25804 (1126)254-7175 CERTIFICATIONS Charlotte Certification 10s 9800 Kince i Ave. Ste 100. Huntemitle. NC 28078 Conr1ECticul Certification :t; PH•0104 North Carolina Drinking Water Certification 1f: 37706 Fio.idalNELAP Certirica(ioit »: E87627 Norh Carolina Field Services Cerli icalion 9: 5242 Kentucky UST" Ceriificalinr, 4: 84 North Carolina Wastewater Cer ifrcation 9: 12 Louisiana DHH Drinking Water a LA 100031 South Carolina Cerlifica:ion ;V: 99006001 West Virginia Certification Z: 357 South Carolina Drinking Water Cerl. fir: 99005003 VlrgiNaA/ELr\P Certification 4i 460144 Virginia Dfinkiog Water Certification #: 00213 Asheville Certiftvilion IDS 2275 Riverside Dr., Asheville. MC 258D4 ' South Carolina CeitifrcaGon -- 99030001 FloridalNELAP Certification A: E87643 Virginia Cer icalicn 4: 0007Z Massachusetts Certification f: 1,1-NC030 West Virginia Cortificn,ion 9: 358 North Carolina Drinking Water Certification : 37712 Virgina/VELAP Certification 9: 46D147 North Carolina WWSietiYaler Certification #: 40 Eden Certification 10s 205 East Meadow Road Suite A. Eder, NC 27288 `Arginia Drinking Water Certifcatioo ;#: 00424 North Carolina Drinking Waver Certihcilion 0: 37738 WginiaN LAPCeKiflcalion M:460025 North Carolina Wastat:a.er CCrtilicalior, 9: 533 Paco Analytical Services, Inc. 9800 rincey Ave. Suite 100 Hunlersnlle. NC 2"76 (77 G[)875-2W2 REPORT OF LABORATORY ANALYSIS Page 2 of 68 i his rtpan shag n.Cl he reproduced, except :n rull. rrahoul The wmt¢n consent of Pace Analytical Sery ices. Inc_ Pace Analyttcel5ervlces,Inc. Pace AnelytkaiServices, Inc. Pace Analy3icalServlces,lne. 205 East Meadow road - SrAe A 2226 Rivetside Dr. 980o IGncey Ave. Suite 100 1!2CeAr?a1j4ica1' Eden, NC 27298 AsAevdfe, NC 28804 Huraersv.IM, NC 23078 i (336)623.8921 (82B)254-7176 (704)fi75.5092 Project' Storm Writer 03131/12 Pace Project No.: 92115467 Lat! 10 Sample 10 92115467001 5002 9211 5457002 S00 5 92115467003 SD0 6 92115467004 SDO 7 92115467005 S00 0 SAMPLE ANALYTE COUNT Method SM 7540D EPA 9040 EPA 1654A EPA 608 EPA 200.7 EPA 625 EPA 624 EPA 420.4 SPA 4500-CN-E SM 25400 EPA 9C40 EPA 1654A EPA 608 EPA 200.7 EPA 625 EPA 624 EPA 420.4 SM 4500-CN-E SM 2540D EPA 9040 EPA1664A EPA 608 EPA 200.7 EPA 625 EPA 524 EPA A20.4 SM 4500-CN-E SM 2540D EPA 9040 EPA 1664A PA 506 EPA 200,7 EPA 625 EPA 624 EPA 420.4 SM 4500-CN SM 2�4007 REPORT OF LABORATORY ANALYSIS This repor, mall rut be reproduced, except in full. , KLhoul tl:e written consent aI Pace Se:vim:s. Inc.. Analytes Analysts Reported Laboratory KPP t PASI-E CLt i 1 PASI-E CLW 1 PAM-C RES 27 PASI-C SHB i PASI-r1 PPM 68 PASi-C KJM 73 PASI-C SDH 1 PASI-A JDA i PASI-A KPP 1 PAS6E CLM 1 PASII_ CLW 1 PASI-C RES 27 PASI-C SHB 1 PASI-A PPN! 65 PAS(-C KJM 73 PASI-C SDH 1 PASI A JDA 1 PASI-A KPP 1 PASI-E CLM t PASI-r: CLW 1. PASI-',' RES 27 PASI-C SMB 1 PASI-A PPIti4 68 PAS!-C KJh1 73 PASI-C SCH 1 PASI-A JDA 1 PASI-A KPP 1 PASI-E CLM I PASI-E CLW 1 PASI-C RES 27 PASS-C SH8 1 PASI-A PPM 68 PAS)-C KiM 73 PASI-C SIM t PASI-A JDA t PASI-A KPP e PASI-F Pays 3 a, 56 ari e /'11Ialyfica Project: SIDrm Waler03131112 Pace Project No.: 92115467 Lab ID SM11PIB ID 92115467DOG S00 9 92115467007 SGO t t 92115467008 SD012 92115467009 SOO13 Pace Anatytkai Services, Inc. Pace AnOidral Services, Inc. 205 East Mea3ow Road - Suite A 2225 Riverside pr, Eden, NC 27288 Ashe011e, NG 28804 (338)6238421 (828)254-7176 SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)675.5092 Method Anatysts Analytes Reported Laboratory EPA 9040 URI I PAST-E EPA 1664A CON 1 PASt•C EPA608 RES 27 PAS1,G EPA 200.1 SHS I PASI-A EPA 625 PPm 68 PASI-C EPA62-1 KJM 73 PASI-C EPA 420.4 SOH 1 PASI-A SM 4500-CN-E JDA 1 PASI-A SM 2540D KPP 1 PASI-E EPA 9040 CLM 1 PASi-E EPA ID64A CLW 1 PASI-C EPA608 RES 27 PASI-C EPA 200.7 SHB 1 PA51-A EPA 625 PP -)A 68 PASI-C EPAb24 KJM 73 PASI-C EPA 420.4 SDH 1 PASi-A SNI4500-CN-E JDA 1 PASI-A SPA 25400 KPP 1. PASI-E EPA 91740 CUM 1 PASf-c EPA1664A CLiN 1 PASI-G EPA 608 RES 27 PASI-C EPA 200.7 SHG 1 PASI-A EPA625 PPM 68 PASI-C EPA 624 KJh4 r"3 PASI-C EPA 420.4 SCfi 1 PASI-A SM 4500-cm-E JDA 1 PASI-A SM 2540D KPP 1 PAS(-E EPA 9040 CL14i i PASI-E EPA Ib64A CLW 1 PASI-C EPA508 RES 27 PASI-C EPA 2001 SHE ; PASI-A EPA 625 PPNI Eli PASI-C i_PA624 KJM 73 PASI-C EPA 420,-t SDH I PASI-A SM 4500-CN-E JDA I PA51-A SPA 25400 KPP 1 PASI-E EPA 9040 CODA 1 PASI-E REPORT OF LABORATORY ANALYSIS Page 4 of 65 This repot shall not be reprodtxed, ezccpt in tuP. Wa4LWt tire written consent cf Pace Anal- t'.cW Srrv-'Ces. ine- 1 acamalocal ' - mnvpccata4irom Project: Storm Water 03/31/12 Pace Project No.: 92115467 tab ID Sample ID Pace Analytical Servteas, Inc. 205 Cast Meadow Road • Suite A Eden, NC 27286 (336)r-23-5921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheviila, NC 28MA (M)254-7178 SAMPLE ANALYTE COUNT Method EPA iE64A EPA 608 EPA 200.7 EPA 625 EPA 628 SM 4500-CN-E REPORT OF LABORA'fORYANALYSIS Ths report shall not be Yep+oduceC, e-cept In full, without the wfiLlen r-onsenl of PaCe Aaa7yii d Se";ccs-aC.. Pace Analytical Services, Inc. 96001(inocyAve. State-loo Hurdersville, NC 28076 (704)675-9m2 Analytes Analysts Reported Laboratory CLIN 1 PAS1-C RES 27 PASi-C SN© 1 PAS' -A PPM 6u° PASI-C KJU 73 PASI-C 5DF1 1 PASI-A JDA 1 PASI-A Purge 5 ,t 66 e ?Wnaoical Pace Analytical So vtcss, Inc. Pace Analytical Services, Inc. Pace Analytic$$ Services, Inc. /4 2l}S Eats$14eadow Road - Sute A 2225 Riverside Jr, 98W Kincey Ave. Svho Soo umrpax�ht as Eden. NC 27265 Ashevilte- NC 2B804 rtuntersville. NC 2e078 (336)6218921 (92s)25-4-7176 {704}675-902 ANALYMAL RESULTS Project: Storm Water 03131112 Pace Project No.: 92115467 Sample: $DO 2 Lab ID: 92115467001 Collected: 03131112 10:30 Received: 04/02112 09:10 M;)trfx: Water Parameters ReSUISS Units Report limit DF Prepared Aratyzed CAS No. Quaff 2540D Totat Suspended Solids AnatyGcal-'Velhod: Stet 2540D Total Suspcnded Sutids 10.6 mg1L 2.5 1 04/03112 13TO 9040 pH Analytical Method: EPA 0040 PH 6.4 SM. Units 0.10 1 0s103112 08:57 H6 HFI14, Oil and Grease Analytical 4lethoC: EPA 16G4A Oil and Grease ND mg1L 5.0 1 04104/12 08.09 608 GCS Pesticides and PCBs Arialyticat „4elhod: EPA 608 Preparation Method: EPA 3535 Mdrirl NO n1g1L 0.000050 1 04103/12 18:Q0 0,1105112 04:45 309-00-2 alpha-SH(; NO mgr'L 0.000050 1 04/03/12 1&00 34MP2 04:45 319-84-6 beta-SHC NO n1gfL 0.000050 1 04M112 18:00 04105i42 04:45 319-P.5-7 delta-SHC NO mg1L 0.000050 1 04103112 18:00 04105112 04:45 310.866-8 gamma-6HC (Lindane) ND mglL 0A00050 1 04103/12 18:00 04/05112 04:45 58-89-9 Chlordnne (Technical) ND mg1L 0,00050 1 04/03112 18:00 04105l12 Q4:45 57-74-9 4,4'-ODD NO rngfL 0.000050 1 04103/12 1181•30 041'05112 04:45 72-54-8 4,4'-DOE NO mg/L 0.000050 i 04103112 18:UO D4105112 04:45 72-55-9 4 4'-CUT' NU nng1L 0.000050 1 04/D3112 16;00 04/05112 O'4:45 50.29-3 Dieldrin ND rageL L•.000050 1 04.'"12 18:00 04/05/112 D4:45 60-57-1 End95ulfan f NO mg,'L 0.000D50 1 04103J17 18:00 04/05112 04:45 959-1�8-8 Endosulfan li NO mg1L 0.000050 1 04JOYi2i 18:00 0005112 04:45 33213-65.9 c`ndusulfan sulfate NO mglL 0.000050 1 04103/17 M00 04/05112 C4; 45 1031-07-8 Endrin N0 rngfL 0.000050 1 04103f12 18:00 04105112 04:45 72-20-8 Endrin aldehyde "D rag1L 0.000050 1 04t03112 18:00 04105112 (14:45 742I-93-4 Heptachlor NO mgll O.OU0050 1 04103/12 18:00 C4105112 04:45 76-41-3 Heplachlor epoxide 111) mg?L 0.000050 1 041'03112 t8:00 04105/12 04:45 102.1-57.3 PC3-1016 (Aroclor 1015) NO n1911- 0,00050 1 04/03/12 MOO C4105f12 04:45 12674-1t-2 PCB-1221 (Aroclor 1221) -ND mg1L 0.00050 1 04/03112 18:00 04105112 04:45 11104-2S•2 PCB-1732 (Aroclor 1232) ND m4jA 0.D0050 f 04M31i2 18:00 D410-3112 04:45 1114t-16-5 PCB. I2e2 (Aroclor 1242) NO rngfL 0.00050 1 04T3/12 18:00 04/05112 04:45 53469-21-9 PC9-1248 (Aroclor 1248) NO mg1L 0.00050 1 04103112 18:00 04/05/12 0-4:45 12872-29.6 PCB-1254 (Aroclor 1254) NO n,g/L 0.00050 i 04/01/12 18:00 0/Vf)51T2 04:45 11097-69.1 PCS-1260 (Aroclor 1260) AID mg1L 0,00050 1 04/03112 18:00 04/05112 C4145 1 t096-82-5 Toxaphene ND rngfL 0.00050 1 04103112113:00 0410511204:45 6001-35-2 Surrorgales Telrachloro-m-xylane (5) 124 % 20-110 1 04iO3/12 18:00 04/06/12 04:45 877-09-8 55 Decachlorobiphenyl (8) 125 % 20.138 1 U•1103f12 113:00 04/06112 04:45 2(151-24-3 20Q.7 MET ICP Analylical l;.eth! J: EPA 200.7 P,eoaratioa Melbod: EPA Z00.7 Lead ND mg1L O.0050 1 04105/12 11:30 041063112 0126 7439-92-1 625 Y1SSV Analytical Method: EPA 525 Praparalicn Method: EPA 625 Acenaphtherle 140 mgiL 0,0050 1 04/132112 16:00 Od101112 03:05 83-32-9 Acerlapillhylene NO mg1L 0.0050 1 (14193112 16:00 041071/2 03:05 208-effi-8 Ace(ophenone ND moll 0.0050 1 04103112. 1500 04107/12 03:05 98.85-2 Arxilitle NO mgtL 0.01E 1 0410311216:00 04M7:1203:05 62.53-3 Date: 041161201201:35PM. REPORT OF LABORATORY ANALYSIS Pag)eaof66 Tkis repon shalt nol kse reproduced. accept In lull, virhec: the •.vr t^.n cn^seni of Pace Any; $loci Services, list.,, s ace Analytical ! wmrpacelaascom Project- Storm Water 03131112 Pace Project No.: 92115467 Paco Analytical Services, Inc. 205 Ea- Meadax Road - SuiFe A Eden. NO 27288 (336)623-e921 Pace Analytical Services, Inc. 2225 Riverside pt. Ashevine. NC 28804 ANALYTICAL RESULTS (8?9)254-7176 Pace Analytical Servlce5, Inc. 9800 kincey AV0, SVlte i00 Hwifersv'le, NC 28078 (704)875-9092 Sample; SOO 2 Lab 10: 92115467001 Collected: 03131112 10:30 Received: 04/02/12 09:10 Matrix: Water Parameters Results Units Depart Limit OF Prepared Anatyzed CAS No. Quat 625 N1SSV Analytical Meshed: EPAC25 Prepasa(fon Method; EPA625 Anlhracene NO mg!L 0?J050 1 04103112 16.00 0di07/i 2 03:05 120-12-7 Benzidine ND mg1L 0.050 1 L14103112 15:00 04137112 03:05 92-87.5 Bewa(a)anlhracene ND mgiL 0.0050 1 N103112 16:00 04loYll2 03:05 55-55-3 Eenzo(a)pyrene ND rny1L 0.0050 1 041031i2 16:00 04/07/12 03TS 50-32-0 8snzcrb)RucranIhene ND irg/L GA050 1 04/03112 .6:00 04/07/12 03:05 205-99-2 lienro(g,h,i)perylene ND rng1L 0.0050 1 04103112 16:00 04/07/12 03:05 191.24-2 6anzo(K)Iluoranthene NO m9h. 0.0050 1 G4703112 16:00 04/07112 0105 207.06-9 4-Bromaphcnylphenyi ether ND mg1L 0.0059 1. 041031/2 15;00 04/07/12 03:05 101-55-3 ButylbenzylphIialow NO mg/L 0 0050 1 0,'103112 19:00 04/07112 03:05 85-68.7 carbazole NO mg/L 0.0050 1 04103.r121500 04197/1203-05 86-7d-8 4-Chiero-3•methylphenol NO mg/L 0.0050 1 04103112 IGTO 0007112 03:05 59-50-7 bis(2-Chloroethoxy)melhane NO mg1L 0.010 1 04103/12 16'00 04/07112(13:05 111-91-1 bis(2-Chloroethyl) ether NO mg/L 0-0050 1 04103112 16:00 04/07/12 03:05 111.44.4 bis(2-Chloroiscpropyl) ether ND mglL 0 0050 1 04/03/12 16:00 04/07/12 03:05 108.60.1 2-Chloronaphilialene ND mglL 0.0050 1 04103/12 15:00 C4107112 03:05 91-50.7 2-Chlorophenol ND mg& 0.0050 1 04103/12 16:00 C4107112 03:05 85-57-6 4-Chlcropf1enyiph0nyl elher N13 mg1L 0.0050 1 C4103112 16:00 04/07/12 03-05 7005.72-3 Chrysene ND mg/L 0.0050 1 04/03112 16.00 04107A2 03:95 218.01-9 n-Decane NO mg/L 0.010 1 04103/12 16.00 04/07/12 03:05 124-18-5 Dibenz(a F1+anthra;.erua ND mall- 0.1)050 1 0-403112 16:00 0410702 03:05 53-70.3 1,2-01chiorobenzene NO no-rg/L 0,0050 1 04103112 16:00 04/07/12 03.05 95-50.1 1,3-Dichlofobenzene NO mg/L 0.0050 1 0410311216:00 04107112.0105 541.73-1 i,4-1-34chloroberuene ND mg1L 0.0050 1 04/03M216:00 0410711203:05 106-46-7 3,3'-Dichlorobenzidina NO mg/L 0.025 1 C41031i216:00 OQ0711203:05 91-94-1 2,4-Dichloraphertol ND mg1L 0.OG50 1 04103112 16:00 04107112 03:05 120.83-2 Diehl)€phthalate NO mg/L 0.0G50 I 04103112 16:00 04/07112 03:05 84-66-2 2,4-Dimethylphenol NO mg/L 0.0i0 1 & 03112 i6:00 94/0711203:05 105.67-9 Dime!hylphthataie NO mg1L 0.0050 1 G4103l12 16:00 G4/07/12 03:05 131-11-3 Di-n-biaylphlhalate NO mg1L 0.6050 1 04103112 16;00 04/07i12 03:05 84-74-2 4,6-Oini!ro-2-methytphe Hof NO mg1L 0.020 1 04103M216:00 04/071i203:05 53-i-52-i 2,4-Dinivophenot ND mglL 0.050 1 04/0311216:00 0410711203:05 51-28,5 2,4-Dinitrotoluene ND my1L 0.0050 1 04/03/12 16:00 0410711203:05 1211-i4-2 2.5-Dinitrn,oruene ND mglL 0.0050 1 G4103112 16:00 04107/12 03:05 60.20-2 Di-n-octyiphthalate NO rrig!L 0.0050 1 04103112 16:00 04107112 03:05 117-84-0 1.2-Dipheny!hydr8zine ND mg11- 0.0000 1 04103112 16:00 0410711203:05 ,22.66-7 his(7_ cthyltex}E)phthaiate 0.0065 :rgll- 0.0050 t 04;0311216:00 0410711203:05 ii7-81-7 Rvcranthene ND krgll- 0.0050 1 0a103112 16:00 0411)7/12 03:05 20f,14.0 FluorerB NO mg/L 0.0050 1 0410311216:00 04107A203:05 96-73-7 Hexachloro-l.3-buladielie NO mglL 0.005(: 1 04103112 16:00 04107!12 03:OS 67-03-3 Hexachlorobenzene 1ND rnglt- 0.0050 1 04103112 16:00 04107,12 03;D5 118.74-1 ttexachlorocyclopentadiene NO mg/L 0.010 1 04103/17 15:00 04/07112 03:05 77-47-4 Hexacirloroelhane ND i%il- 0.0050 1 04103/12 16:00 04107/12 03:05 67-72.1 lnrlenc(1,2,3-cd)pyrene NO r601- OM50 1 04103/12 16:00 0410711203'.05 193.39-5 isoo4orone NO M91L 0,010 1 04!03112 16:00 04107112 0105 78-59-1 Naphthalene ND rng/L 0.0050 1 94/03/12 16:00 04107/12 03:05 91-20.3 Nitrcb,cnzene NID rng1L 0.0050 1 D41C31i2 16:00 041071 i2 03:05 98-95.3 2,Nitrvrihenal NT1 mg1L 0.0050 1 04103/12 16!00 04107r12 03:05 68-75-5 Dale: O4 IM912 01:355 PM REPORT OF LABORATORY ANALYSIS i nis ream shall mt be repredisceo. except in full, Aithout 1ha wdren convent or Pace Anarydcal Surrces, im. Page 7 of 66 ,f , oAna"cal- - mex rAea'�nsoom Project; Storm WaterCW31112 Pace Protect No.; 92115,67 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27280 (336)623-9921 Pace Analytical Services, Inc. 2225 $rLverside Dr_ Ashevilla, NC 25604 (e28)254-7176 ANALYTICAL RESULTS Pact Analytical Services, Inc. MW Kincey Ave- Slrte 100 liunterwe, NC 28078 (704)975-9092 Sample: SOO 2 Faramelers Lab ID: 92115467001 Results Units Collected: 03131112 10:30 Report Urnil OF Received: 04102/12 09:10 Matrix: Water Prepared Analyzed CAS No, Oual 625 MSSV Analytical Method: EPA 625 Preparation 1vlalhurf: EPA 025 A-M',rophenol NO mg/i- 0.050 1 04iO3f12 18:00 04/07i12 03:05 100-02-7 r1•Nitroscdimelhyiamine NO mg/L 0.0050 f 04103/12 16700 04107112 03:05 62-75.9 N-Nifroso-di-n-plopylamine NO rn80- 0,0050 1 04,,03/12 16:00 04M7112 03:05 621-64-7 N-i,,lilrosodiphenyiaminz AND mgh- 0.010 1 04J03/12 16:00 04/C7112. 03:05 W-30.6 n-0cta0ecene ND mg1L 0,010 1 04:03n2 16:00 04f07i1203:05 593,45-3 Penlachlorophenol NO mg1L 0,025 1 o vi)3112 16:00 04107;12 03:05 87-86-5 Phetianthiene NU mg/L O.0C5G 1 04fO3112 16:00 04/07112 03:05 85-01.8 Phenol NO mg,'L 0.W50 1 04/03/12 16:00 04;07112 0105 108.95-2 P,rene ND mgrL 0.0050 1 O4r03112 16:C0 04107112 03:05 129.00-0 1,2,4=fYichlcrobenxene NO mg1L 0,0050 1 04:03112 16:00 0410711203:05 120.82-1 2,4.6-Trichlorophencl NO r:rg1L 0.010 1 04103/12 16:00 0-1107112 03:05 80-06-2 Srr1r'ogaivs Nitrobenzene-d5 (S) 4D % 10-120 04110311,2 16:00 04/07/12 D3:05 4165.60.0 2-Fluorobiphonyl iS) 35 % 15-120 1 04703112 16:00 04107112 03:05 321-60-8 Terphonyi-d14 t5) S6 % 11-131 1 fl4103/12 16:00 04W11203:05 1718-51-0 Phenol-66 (S) 1S % 10-120 1 04/03112 16:00 04107/12 03:C5 13127-0B-3 2-Fluomohenol (S) 27 % 10.120 ; 04/03/12 16:00 D.W7172 D3:05 367-12-4 2,4,6-Tribromcphenol (5) 62 %. 10-137 1 D4103112 16:00 04/07112133:05 118-7" 624 Volatile Organics Analytical Me' hod: EPA624 Acetone NO eig1L 0,075 1 04112112 06:39 67-64.1 Auolein .140 mg1L 0.10 1 04/12112 05:39 1 C7.02-8 Acrylonitnita NO rng1L 0.10 1 04112112 06:39 107-13-1 Benzene NO mg/L 0.0050 1 04112112 06:39 71-413-2 Brurrrohanzeae NO mglL 0.0050 1 04/12/12 06:09 108-86-1 Bromochlaromelllarie NO mgfL 0,0050 1 0411211206:39 74.97-5 Bromocid,loromeihane N0 rng1L 0.0050 1 04112/12 06'.39 75-27-4 Btomoforrrl NO mg/L 0.0050 1 04f12112 06:39 75-25-2 $rarn0rner#lane NO mg1L 0.010 1 04112/12 05:39 74-a3.9 2-Butanono (MEK) ND mg/L 0.0050 1 04f12112 0619 78-93-3 n-Butylbe:lrene ND +ng1L 0.0050 1 04/12/12 06:39 104-51-8 zeC-Butylbenzene NO rqiL 0.0050 1 04112112 05:39 135-96-8 lert-Butylhanzeoe ND rnt11L 0.0050 1 04/12/12 06:39 (18-06.6 Carbon disuffida NO mg1L 0.010 1 04/12/12 06:39 75-15.0 Carbon tetrachloride IN mgrL 0,0050 1 04112/12 06:39 56-23-5 Chlwobenzene NO rng/L 0.0050 1 04!12112 00:39 103-90-7 C41or0e0tane NO m{}lI- 0.010 1 04/12112 06:39 75.00-3 2-Chloroelliylvinyl ezher NO -g1L 0.010 1 G4112112 06:39 110-75-0 Chloroform NO mglL 0.00.50 1 041121/12 06:39 67-c6-3 Chioromethana ND nxj1L 0,0050 1 04712112 06:39 74-57.3 2-Chloiwoluene ND rnglL 0.0050 1 0411211208:39 95-49-8 4-Chlorotoluene NO mg.+L 0.0050 s C4/12112 06:3G 106.43-4 D+broml:ch}oromeGhane ND mg14 0.0050 1 041?2112 C6:39 124,49-1 1,2-DiUromoethane (EDBI NO moll. 0,0050 1 04/12/12 06:39 105.93-4 Dibromomethene ND mgIL 0,0050 1 G4112/12 05:39 74-45.3 1,2-DichlorobenLery ND mg1L 0,0950 04112112 06:39 95-50-1 1,3-Dichlofobenzene NOrrtjlL 0.0050 1 04AW206:39 541.73-1 Date:04i,612012 01-35 PM REPORT OF LABORATORY ANALYSIS Page e or 66 Th''s report &hall not be reproduced, excr..H iA kAl, :a;holt: ire wrJ',en consent of Pace Aayylkal gerkes, ;rc I awnaWical i Project Storm Water03/31112 Pace Project No.: 92115467 Pace Analytical ServIres. Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riversida Dr. Eden, NC 27288 Asheville, NC 28804 (336)673-8921 (928)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc, 9B00 KirtwyAve. Suite 100 Huntemvillo, NC 28078 (704)875-S092 Sample: 5DO 2 P:srameters Lab ID: 92115467001 Resul(s Units Collected: 03131112 10:30 Report Limit OF Received: 04/02112 09:10 (Matrix: Water Prepared Analyzed CAS N0- Qual 624 Volatile Organics An3lytical Method: EPAS24 1,4-0ichlerobenzen( ND I-rg1L 0.0050 1 0411211206:39 105-46.7 1.I-Nchloraethene ND mg?L 0.0n50 1 04112/12 06:39 75-34.3 1,2Dichlaroell,ane NOrngP- 0.0050 1 0411211206:39 tO7-06-2 1,1-Dichloraa0rane NO mg1L 0-0050 1 0411211206739 75-35.4 cis-1,2-Dichtorcelllerie MO rmS/L 0.0050 1 0411211206:39 156-59-2 trans-l.2-Oichloroelhene NO ntgfL 0.0050 1 ()411211 z 06:39 156-00.5 1,2-Dlchloropropane ND mg1L 0.0050 0411211206:39 78-87-5 1.3-01chloropropare NO mgiL 0.0050 1 04112M2 06:39 1z2-28.9 2,2-Dich[arc propa7e ND inglt 0,0050 1 04112/12 06:39 594-20-7 1,1-Dichforopropene WO rng!L 0,0050 1 04112/12 06:39 563-58.6 Cis-I,3-Dicllioroprcpere NO rng!L 0,0050 1 U411211206:39 10061.01-5 4ans-11,3-0ichlaroprapene NU rslglL 0,0050 1 04/12/17.06:39 10001-02-6 Lthyibenzene NO mgrL 0,0050 1 04112/12 06:39 too-41.4 Hexachloro-1,3-buladiene NO mg1L 0-0050 1 04)12/12 06:39 87-68-3 2-Hexanunc NO mgli. 0.010 1 04112/12 06:39 5-31-78-6 lodomethane ,vey mgiL 0.010 1 04/12112 06:39 74-88.4 tsopmpy?benzene (Curnene) MD in,1L 0.0050 1 W1211206:39 ga-82-8 p-Isopropynnluene INC mgA. 0.0050 1 04112/12 06:39 99-67.6 Mettlylone Chtoiide IN ng1L 0.0050 1 04/12/12 U13:39 75-09.2 4-tMethyl-2-perlanone (MIOK) ND mg1L 0,010 1 0d112112 06:39 10$-10-1 1MoMyb(eri-bulyl ether NO mg,L 0.0050 1 0012/12 06-39 1634-04-4 rtMaphrhalene ND mgiL 0.0050 1 04/12112 06:39 91-20.3 n-Prapyibenzenc ND mgrL 0.0050 1 0411211206:39 103-65.1 Styrene NO mgrL 0.0050 1 04/12112 06:39 100-02.5 1,1,1,2-Telrachioreethane NO mg& 0.00511 1 0411211206:39 639-20.6 1,1,2,2-Tetrachtoroethane NO mgiL 0,0050 1 04/12112 06:39 79-34.5 7etracNoroethen e NO mgiL GD050 1 04112/12 06:39 127-18-4 toluene ND r: g1L 0.0050 1 04/12/12 06,39 108-88-3 1.2.3-Trichlarobervene NO oig;L 0.0050 1 04112/1206:39 i37-61.6 1.2,4-Trichforabenzene N© mg(L 0.0050 1 04112112 00'39 120-82.1 1,1,t:;richloreelhane NO mgiL 0.0050 1 0411211206:39 71-55-6 1,1,24ficl+loroethane id0 rnglL 0-0050 1 04/12/12 06.39 79-00-5 Trichloreethene NO rr.glL 0,0050 1 04112112 06:39 7M1-6 Trichlorofluoramethane NO mgiL 0,010 1 04112112 00:39 75-69.4 1,2,3-Tdch1orepropane NO mgiL 0,0050 1 04112M206:30 96-18-4 1,1.2-Trtrh:orotriflucroelhaaa NO mgiL 0.0050 1 04112112 06:39 76-13-1 1.2,4-"I'fininOy!benzene NO mgiL 0.0050 1 04f1Zr12 06 39 95-63.6 1.3,5-Trimethy:benzene NO mg1L U.0050 1 04112lt2 06.39 103 67.8 %Anyl acetate ND mgiL 0,01D 1 04/12/12 O�,-3g 106,05-d Vinylchtotide NC mgrL 0.0060 1 04/12112 05:39 ?5-01.4 m&p-Xylene NO mglL 0.0050 i 04/12112 06:39 179601-23.1 a-X}Iene Nt] mg1(_ 0.0050 1 041121/2 0G:39 95-47.6 SurrognieS ie4br0moilucramethane ;8) 123 % 70-130 1 04112112 06:39 i 868.53-7 4-Sromo!luorob 5nzeno (S) 98 °J 70.130 1 04112112 08:39 C-U-00-4 Toluene-d8 (S) 93 % 70.130 1 04/12112 05:39 2037.26-5 1,2-Dichlorpelhan.e-r4 tS) 124 % 70.130 1 0/112/12 06-39 ,7060.07.0 Date: 04115/2012 01:35 PM, REPORT OF LABORATORY ANALYSIS Page 9 of 68 i 195 ref>O- shaR rr_r be re;,rCWVCed. sxcept ih W. without :he written consent Cf Paco Ar Ayli .art Seivites, Irc.. I r�s Pace Analytical Services, Inc. Face Analyticai Services, Inc. Pace Analytical Services, Inc. a �+ eAnalytical 205 Easl Meadow Road, Suite A 2225 Riverside Dr. 9800 KinCtyAve, Ssite 100 xvnrpe�s. a cnrl Eden, NC 27288 Asheville, NC 28804 Huniersvillo, NC 20076 (336�623-8921 (828)254-7175 (7GAj975-57°2 ANALYTICAL RESULTS Project; Storm tinter 031.31/12 Pace Project No.: 92115467 Sample: Soo 2 Lab [D: 92115467001 Collected: 03/31112 10:30 Received: 041021120"0 Malrk Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 420.4 Phenolics, Total PhenOi 460GCNE Cyanide, Total Cyanide Sample: Sioa 5 Parameters 254OD Total Suspended Solids Total Suspended Solid's 9040 pH pH PMEN1, Oil and Grease Oil and Grease 608 GCS Pesticides and PCBs Aldrin alpha-SHC t:eia-SHC delta-131 iC gartlnia-UHC (Lindane) CHOrdime (TechnicaQ 4,4'-DDD 4,1'-DDE 4,4--DQ7 VI?tdfln Endosulfan I '1-,d OSIl113t1 It Endosulfan sultMe Endrin Endfil aldehyde H.eptachi0r Fteptaclilor epoxide PCB-1015 (Aredor 1016J PCB-1221 (Arocior 1221) PCB-12-2 (Aroclor 1232) PCB-124Z (Atoclor 1242) PCB-M 24B (Aroclor 1748; PCB-1254 (Aroclor 1254) PC8.1200 (Ainclor I280) Toxaphene Analytical Meihcd: EPA 420.4 NO nig1L 0.010 1 04/11112 15:07 108-95-2 Analytical Melhod: SM 4500-CH-E ND mg!1- 0-0050 1 04113112 15:38 57-12.5 Lab 10: 92115467002 Collected: 00131/12 10:30 Received: 04/02/12 09:10 Matrix: Water Results units Report Limit DF Prepared Analyzed CAS No. AisalyliCal Method: SM 25400 $2.9 ing:L 9.1 1 C4i=12 13:01 AI13iyftal hlethcO: EPA 0040 12.5 cold. Units 0.10 1 441113/1208:67 Analytical Nlethcd: EPA 1664A NO mg:L 5-0 1 04104112 08 09 Atialytical Melhod: EPA 60a Preparaticn klethnd: EPA 5535 NO mg1L 0.000050 1 04103112 18'.00 O 05112 05:38 309-00.2 NO mg1L 0.000050 1 04103/12 18:0 04:'05112 05:38 319-6446 NU mgl- O.000D50 1 C410112 16;00 04(05112 05:38 3ig-85.7 ND mglL 0,000051) i 04103112. 18:00 04165112 05:38 319-86-8 ,ND mg;L 01000050 1 0410302 18:00 0,40511205:38 58-80-9 CAD n1g1L 0.00050 1 04102M218:00 041051t205:38 57-74.9 NO mg!L 7.000050 1 04103/12 18:00 04;05112 05:38 72-54-0 NO mgtL 0.000050 1 04103/12 18:00 Oa105112 05:38 72-55.9 NA mg1L 0.000050 1 041a3l12 18:00 04,,05/12 05:38 50.29-3 ND mg/L 4.000050 1 04103112 18:00 04105i 12 05:38 60-57-1 NO rnglL 0.000050 1 04103112 18:00 04/05112 05:38 959-98.6 t.D millL 0,000050 1 04103112 18.00 04105112(15:38 33213-65-9 NO mgtL 0,000050 1 041031121&00 04;051120528 1031-07-8 NO n1r,1t. (1000050 1 04f03112 18:00 04105/12 05;38 72-20.6 ND mglL 0.000050 1 04103112 18:00 0410511205:38 742.1-93-4 NO rnglL O.n60050 1 04103/12 18:00 04105112 05:38 76-44.5 NO mg1L 0.000050 1 G41`03112 18:00 04/05112 05:30 1024.57-3 NO mgr4 a ucosG 1 ]4r03n2 16:00 04105112 05:33 12674-11-2 610 nigh- 0.00050 1 041031,.2 18:00 0410511205:38 11104.28-2 O mgrl- 0.00050 1 0Ai03112 18:00 041051-2 65:38 11141 • i 6-5 "D mgl1. 0.00050 1 04/D3112 18:00 C4105112 05:38 53-trig-21-9 NO nrr'L 0.0010 0 1 04/0311218:00 04r0511205:38 12672.29-6 NO mgrL 0.00050 1 04/02/12 18:00 GCOV12 05:38 11097.69-1 O mgrL 0.00050 1 r,41t1311 Z 16:00 04/05112 05:38 11096.82-5 NO z1g1L 0.D0050 1 041031M218:00 l?410511205:38 9001..35-2 Qual H6 DOW 0 4r 1612012 01:35:^hl REPORT OF LABORATORY ANALYSES Page 10 of 6f3 Thos report Shag rtn: be reyradjced. cheep: in PAL - wilhoui the wraien consent of Pace An31y''jcw Semces. Inc.. /�aceAnalyficala uvAr,pxei,��sxca r Faro Anatocal Services, Inc. Pace Analytical Services, Inc. 205 East rdeadaw Rued - Su:e A 2225 Riverside Cr, Eden, NC 27288 Ashev,7e, NC 28804 (338�2�521 (829)2:E-7576 ANALYTICAL RESULTS Pate Analytical Services, Inc, 98D6 Ki,^cey Ave. S ae I OC Huntersville, NC 28078 (74458759692 Project: Storm Water 03/31112 Pare Protect ho.: 92115467 Sarnplo: SOO 5 Lab 10: 92115467002 Collected: 03131I12 10:30 Received: 04102/12 09:10 Matrix: % toter parameters Results Units Report Limit DIP Preparea Analyzed CAS No. Quat 608 GCS pesticides and PC3s Analy!ical1Ve1hcd: EPA606 Preparation lutelhod: EPA 3535 S urro rga ter letrachloro-m=xylene (S) 91 % 20-110 1 ri-i,03112 13:00 34105112 05:38 677-09-9 Decichlorobipheiiyl (S) 160 %, 20-135 1 04103/1? 18:00 D005112 05:38 2051-24-3 S5 200.7 MET ICP Analytical 1Ae:liod: EPA 200.7 Preparalion hieihod: EPA 200.7 Lead ND mg1L 0,0050 1 0»105/12 11:30 04106/12 03:30 7439-92-1 625 MSSV Anarytical Method: EPA 625 I'reparatien Method: EPA 625 Acenapbri'lene NO mg1L 0.0050 1 04103fl2 16:00 04107112 03:32 83.32-9 Acenaphlhylene ND rgfL C.0050 1 0410311216:00 0410711203:32 208-96-8 Acetophenone NO mg1L 0.0050 1 04/03112 16:00 0-VQ7/12 03:32 98-86-2 Aniline NO mg/L 0.1110 1 04/0311216:00 04107ii20132 62.53-3 Anthracer,,e NO mg/L 0.0050 1 04MBJ1216:00 04107P203:22 120-12-1 Benzidirte NO mg/L 0.050 1 04103112 ,6:00 04/07112 03:32 92.87-5 Benzo(a)anlhirpcene NO mg/L 0.0050 1 04/03112 ,5:00 0410711203:32 56-55-3 Banzo;a)pyrene ND mg1L 0.0050 1 C4f03112 15:00 04JO7112 03:32 50-32-8 Bezzo(b)fluoranthene ND mull- 0.0050 1 0410T12 16:00 04/07112 03:32 205-99-2 Benzo(g,h,i)pefylere NO mg/L 0.0050 1 04103112 16:00 04/07112 03:32 191-24-2 Senzo(R)7uotanthens NO mgrL 0.0050 1 04/03/12 16:00 04/07112 03:32 201-08-9 4-13romaphenylohenylether Nr mg1L 0.D050 1 04M311216:00 04/07112 03:32 101-55-3 Buiyibenzyirhthalate NO ing/L 0,0060 1 04/03/12 16:00 04/07112 03:32. 85.68-7 Carbazole NO mgtL 0,00--b i 04103/12 16:00 04107117. 03:32 86-74-8 4-Chic fo-3-111e:hylphenol NO mg/L 0,0050 1 04103/12 16:00 04107112 03:32 59.50.7 bis(2-Ch1oro0lroxy)methane ND rng!L 0.010 1 04103112 16:00 04107il2 03:32 111-91-1 bis1,2-C[rloroelhyf) ether NO mg1L U.DDSO 1 0410312 16:00 04i0711? 03:32 111-44-4 bis(2-Chh3F0isopr(3pyl) ether NO mg1L D.00SC 1 04/03/12 16:OG 04107/1'L 03:32 108-60-1 2-Chloronaphthalene NO nrgfL 0,0050 1 04/03/12 16:00 04/07112 03:32 91.58-7 2-Chlorophenol ND infl. 0.0050 1 04103112 16:00 C4107112 03;32 95-57-8 4-Chlorophenylphenyl ether NO inglL 0.0060 1 04M3/12 16:00 04107/12 03:32 7005-72-3 Chryaene NO mg1L O,CO50 11 04103f 12 16:00 0410711203:12 218-Di-9 n-Oecane NO 11141/1. UA10 1 04i03112 16:00 04107/12 01: 2 124.18-5 piberta(a,ttj2n ilracene ND m2fL 0.0050 1 04103/12 16:00 04107/12 03:37 53.70-3 1,2-0ichicrobenzene ND mg1L 0.0050 1 04/03112 18:00 04107it2 0 3; 32 95•SG 1 1,3-Dichlnaobenzene NI) ntglL 0.0050 1 0.1103112 16:00 0410711203:32 541-73-1 1,4-Oi&,1crobenzene ND mg1L 0.0050 1 04/031'r 2 15:00 C-410711203:32 106-46-7 IX-Dichlorobenzidine ND mg1L 0.025 C4i03112 159 00 04/07/12 03:32 91-94-1 2,4-Oichloroohcncl ND mg& 0.0G50 1 04103fl2 16:00 04107/12 03:32 120-83-2 plethylp;Ithllal- 141) rrglL 0.0050 1 04103112 10:00 04107/12 03:32 84,66-'L 2,4-Oirnethylphenol ND rnVL 0.010 1 04103/12 16MO 0410,112 03:32 105-67-11 Dimethylehthala:a NO mg/L 0.0050 1 04103112 t9:00 04107/1203:32 131-11-3 0i-n-b4:ylPhlllz131e ND i1g/L 0.0050 1 Oc:93112 -IUD 04/07112 03:32 84.74-2 ,6-Dinitrc-2-methylphenoi NO mOtL 0.020 1 04 u31 i2 16.00 04107112 03:32 534-52-1 2.4-Dinitrophenc? NO mgiL 0.050 1 04103112 16',00 04/07/12 03:32 51.28.5 2,4-Dinilreloluere NO mg/L 0.0050 i 04103I121S:00 04/07I1203:32 121-14-2 2,5-Dinitrololuene ND moll- 0.0050 1 04i03112 16:00 04/07/12 03:32 606-20-2 Di-n-octylphlhalate ND mg/L 0.0050 1 04103J12 16,00 0410ill 203:32 117.84-0 Date: 04I16/2012 01:35 PM REPORT OF LABORATORY ANALfS13 Page 11 of fib THs report she l not be reproduced, a,_cept in fuli, • iw%oui the wvePA rwi"n d Pace Are21yt cal Scr.4css. tic.. I 7 iV Pace AnaiydcaI Services, Inc. Pace Analytical Services, fnc. Pace Analytical Services, Inc. aceAnaiXical 205 Easi Meadrnv Road - Surie A 2225 Riverside Or. 9$00 Kincev Ave- Suitt 100 Eder. NC 272U Ashe�Ce, NC 283C4 Hur;erswtle, NC 28078 r,338!62"921 t826)2S4-7178 (7C4)875.9092 ANALYTICAL RESULTS Projed: Storm'/s'ater03-4 1112 Pace Project No.: 92115467 Sample: SOO 5 Lab ID, 92116467002 Collected: 03/31/12 10:30 Received; 04M2112 0910 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. oval 625 MS5V 1,2-Dipheny1hydrarine his (2 - E1hy lh a xy i) p ht ha l a t e FlMar:hone Fluprene I lexaeh:oro-1 ,3-bola die ne Hexacti!o ra benzene Hexachlpl oryClopenladiene Hexachloroothane Inder.-o(1,2,3-cd)ayrene lsaphware Maphiluslene Nilrahenzene 2-Nitropnenol 4-,Nilroplienol N-Ni(rosodimethyfamine h-idlirO50-di-rl-pro;)yla rniile !-Mitresodiphenylamine n-Octadecane Pentachloropherlol Plienanthrene Phenol Pyrene 1,2,4-TriChlQrober Irene Z, ?,6-Tr(Chlorophe7at Surrogales N:vobenrone-d5 (5) 2-Flumobipheryl (S) Teiphenyl=d14 (S) Phenol-96 (S) 2-1`luorophenol (S) 2,4.6-Tribromopbenol (S) 62.1 VolNtile 07n2nic5 Acetone Acrolein AcryMmil(ile Benzene Bromobenzene 6rcmuchtorom a Ilia ne Bromodichlora+ne Ilia ne afoit.a.eli l 6romonlettlane 2-13uianone f'MEK) n-Butyibenzene sa:: l3v(ylbenzeae ter,-BLilyibenzerte Carbon disc frde Daic: 04/76/2012 01; 35 PM Analyticei Method, EPA 625 Preparation n4ettled: EPA 625 VD mgrL 0-0050 1 04/031121G:M OA10711203:32 122.66-7 NID mg/L 00050 1 C4103l12 I STO 04107/12 03:32 117.81-7 ND mgrL 0,0050 1 U410311216:00 04107112113-32 206-44-0 14D mgrL 0-00$0 1 0410s712 i6:00 04107112 0132 36-73-7 !p nig1L 0.0050 1 04103/12 1G:00 0410711203:32 87.68-3 ND mgrL 0.0050 04/03112 16:00 (14107112 03 32 118-74-1 Nl0 mgrL 0.010 i )4t03/!2 15:G0 04/07112 0132 77-47-4 ND rrgiL 0.0050 1 04103112 16:00 04107112 03:32 67.72-1 ND urd1L 0.0050 i 04103112 16',00 04107/12 0132 193-39-5 `.D mgfL 0-010 1 04103,112 M00 04)071120132 78.59-1 NO n1g1L 0.0050 1 04103112 16:00 04M7112 03:32 91-20-3 ND mgrL 0.0050 1 04103M 16:00 0007112 03:22 98-95-3 ND rraa!L (.0050 1 04,103112 16:00 04/07112 C3:32 88-75-5 NO mg1L 0.050 i 04103112 16:00 04107r12 03:32 100.02-7 FAD mgrL 0.0050 1 041031f2 46:00 04/07/12 03:332 62-75-9 NO rrg1L 0,0050 1 04103/12 16:00 04107/12 03:32 521.64-7 ND rwl/L 0.010 1 Or103112 16:00 04107712 03:32 86-30 6 ,V0 n)g7L 0.010 1 C4103!12 16:00 C4J07112 03:32 593.45-3 NU mgrL 0.025 1 041031t2 16:01) 0410 12 03:32 87.86-5 rye mglL 0.0050 1 0410Yl2 16:00 04107112 03:32 66.01-3 ND mg1L 0.0050 1 D4t03112 16:Q0 04/07112 03:32 108-95-2 NO rrig1L G-0050 i 04;03/12 16:Co 04/07112 03:32 129.00-0 NO mglL 0.0050 1 04103r12 16:00 04107112 0312 12.0.82-1 NU rrg1L 0.010 1 04103112 1&00 04107/12 03:32 8"G-2 •12 % 10-120 1 04103,112 16:00 04M7112 O:32 4165-60-0 38 % 15-120 1 04103112 16:00 04107112 03-32 321.60-8 53 % 1 i-131 1 041L13112 16:00 04107112 03:32 1718-51-0 18 % 10-120 1 04,03112 16:00 04107112 03.32 13127-86.3 30 % 10-120 1 04/03/12 16700 04107112 03'32 367-12-4 69 % 13-117 1 04/03/12 16:00 0410M2 0132 118-79-5 Anatyticat Method: EPA 624 NO rnglL Or= 1 04112/12 07:05 67-64-1 NO mgrL 0.10 1 0411211207:05 107-02.5 NO 1rIg1L 0.10 1 041121l2 07:05 107-13-1 ND nt91L 0.0050 1 04112!t207:05 71-43-2 ND m91L O.OU50 1 04/1211207:05 108-86-1 ND mWL 0,0050 1 04/12/12 07:05 74-97-5 lap r!rg1L 0-9050 04/12112 07:08 75-27-4 MD mgfL 0,0050 1 04/12/12 07:05 75.25-7 ND mU,L O-Ot0 1 0411211207:05 74-83-9 ND mgrL 0.0050 1 04112./12 07:05 76.03-3 ND mgrL 0.0050 1 04112/1207:05 104-51-8 NO rr:yll- 0.0050 1 04/12/12 07.05 135.0S-8 ND mgrL 0.0050 1 04112!f 2 07.06 9l)-06-6 ND ft-PA 0.010 04112112 07.05 75.15-0 REPORT OF LABORATORY ANALYSIS T Aia rapad shall not he ieprodur i¢. "cep, in full. witt.aut the writtan ccrseot of ?ace Analytical Ser lees. Inc.. Page 12 of 65 =- ceAnalytical x�rr.patefa9s.f�rrt Project: Storm Water03131i12 Pace Project No.: 92115467 Pace Analytical Seryices, Inc. 205 Enst Meadow Road - Suite A Eucn, NC 272U (33S)523-R921 Paco Analydcal Services, Inc. 2225 Riverside Dr. Athevlle, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Sefvices, Inc. 9800v(inoeyAve. Su;te 1-00 Hunlersville. NC 28078 (704)875.9092 Sample: SOO 5 PararreterS Lab ID: 92115467002 Resuils Units Collected: 03/31/12 10= Received: Report Limit t7F Prepared 04102/12 09:10 Matrix: Water Analyzed CAS No. Qual 624 Volatile Orgarlics Analytical Methad: EPA624 Carbon lelszchlor•ide NO mg1l. 0.0050 1 04112/12 07:05 56.23.5 Chiowbevzenn NO mg1L 0.0050 1 04112/12 07:05 108.90-7 Chloroetherle NO mg1L 0.010 1 04112112 0 7:05 75-00-3 2-Chlorne ftivinyt ether NO +r:g1L 0.010 1 04112i 12 07:05 110.75-8 C111oroforrn NO mg1L 0.0050 1 04112/12 07:05 37.66.3 Chforcme(hane; ND mgiL 0.0050 1 (34J12112 07:05 74-87-3 2-CHoroioluene ND mg1L 10050 1 04112/12 07:05 95-49-6 4-Chlorataluene NO mg1L 0.171050 1 0411212 07:05 106-43-4 Oibrornochlarnrnelhane NO mg1L 01)050 S O4112112 07:05 124.413.1 1,2-01bromaethaneiE05) NO mg1L 0-0050 1 ()4/1211207:05 106-93-4 C7ibr0f1.1cmefhzre ND nig;l- 0.0050 1 041i2112 07:05 74.95-3 1,200(orobenzene ND nlg1L 0.0050 i C4112112 07:05 95.50-1 0-01chlorohonzene NO mg1L 0.0050 1 04/12/12 07:05 541-73-1 1,4-Dichlorobenzeno ND mgiL 0.13050 1 04/12112 07:05 )06.46.7 1,1-01chlorcelhane NO mg!t. 0.0050 1 041121t207:05 75-34-3 1,2-01chtoroethane NO mg1L 0.0050 1 04112112 07:05 107.06-2 1.1-Dichloroethena NO mgiL 0.0050 1 04112/1207:05 75-35-4 as-1.2-Ofchloroethene NO mg1L 0.0050 1 0z112112 07:05 156.59-2 trans-1,2.Oichlorvethene ND mgii, 0.0050 1 041121i 2 07:05 156-60-5 1,2-D,chlaropropane ND mg1L 0.0050 1 0411211207:05 78.87-5 1.3•01cnlorcpropane NO Mg1L 0.0050 1 0411211207:05 142-28-9 2.2 Dinforopropane ND frig/L 0.0050 1 041l2112 07:05 594.20-7 1,1-Dictlloeoprepcne NO mg1L 0.0010 1 0411211207:05 563.58-6 cis 1,3-17iCITlo='npropene ND mg1L 0.0050 1 04112h2 07:05 10061-01-5 trans-1 .3-Dictrlaroprouene ND mg1L 0.0050 1 04/12112 07:05 10001-02-6 Pthylbenzeno NO rng1L 0.00$0 1 04112/12 07:05 100-41.4 W.exachtoro-1,3-buladiene 11D m31L 0.0050 1 04112112 07:05 87.68-3 2-1-lexanone NO mg1L 0.010 1 04112/12 07:0$ 591.78-6 rcaomelnane ND mg1L 0.010 1 04112/12 07:05 74-88-4 lsopmpylbenxena (Crmene) NO mr,1L 0.0050 1 041/2112 07:05 s8.82-8 p-Isopropyltuluene NO.m51L 0.050 1 04112112 07:05 99-87-6 Methylene Chloride ND mg1L (.0050 1 0 .112112. 07:05 75.09-2 4-fylethyl-2-penlanone jN118k) NO mg1L 0.010 1 Q4112/12 07:05 108-10-1 Methyl-terl-butyl ether NO mgiL 0-0050 1 04/12112 07:05 1634-04-4 Naphthalene Np 171g11, 0,0050 1 041/2112 07:05 91.20-3 n-Propylbsnzene NI-1 mg1L 0.0050 1 04!1211207:06 103.65-1 _ Styrene NO mg& 0.0050 1 04112112 07:05 10U-42-5 1,1.1.2'l;rarhlcrcetha�e ND mglL 0.0050 1 0411211207:05 630.20-6 1,1,2,2-Tetrachlc!oe1lv-fre NO mg1L 0-0050 1 04112112 07:05 79-34-5 feirachioroethene ND rng1L 0.0060 1 04112/12 07:05 127-13-4 Toluene NO mg1L 0.0050 1 04A2/12 07:05 108 n8-3 1,2,3•-5ichlor9benzene N'D mg1L 0.0050 1 04112h--07:05 87.61-a 1.2.4•Tdchtorcbenz3ra NO mglt 0.0050 1 0•:112112 07:05 120-82.1 1.1,1-1-richioroe thane 1*40 mr,1L 0.0050 1 04112112 07.05 71-55-6 1.1,2-TrichloroeIhaoe NO Mg/L 0.0050 1 0.1112112 0 7:0 5 79.07-5 T0671orot0ent; ND rng1L 0.0050 1 04/12112 07:05 19.01-6 T6rh1000Ruoron.ethtlno ND mgll- t1-010 1 041s211207:05 15.69-4 UnW WIlf$12012 01:35 PM REPORT OF LABORA-I-ORY ANALYSIS Paga 13 of 00 This rxpoe, Shan." oe reproduces. exrr-pi in full, ' wt%Gui the wnllen ccinsem of Pace Analytical Sefvines. !nr. , pate Analytical Services, lnc- Paco Analytical Services, Inc. Pace Analytical Services, Inc. ace Analytical 205 Eau Meadow Road - Suita A MS Rivemida Or, 98001Gncey Ave. Su t" 1CC / Eden, NC 272W Ashevilfe, NC 28804 Huntcr ville, NC 2EC78 w,�r..�p:a5strrn+ (336)523.8921 (8n)2-54.7176 (704)875-9092 ANALYTICAL RESULTS Prnject Storm UwaterOW1/12 Pace Project No.: 9211W7 Sample: S00 S Parameters Lab ICI: 921IW7002 P.esults Units Collected: 03131112 10:30 Report limit OF Received: Prepared 04102/12 09:10 Matrix: wai0r Aralyzed CAS N'o. Quat 62.4 Votatile Organics Analytical Method: ERAG24 1,2,3-Trichtoroprop2ne NO rng)l- 0.0050 1 04l17J42 07:05 96-18-4 1,1,2-TrichlAraldll::araethane ND nig1L 0.0050 1 0d/121.207.05 76-13-1 1,2,4-Tnmethylherzane ND nx31L 0,0050 1 0411211207:05 95-63.6 1,3,5-Tr6r18lhy95enzene ND mgll- 0,0050 1 04/12/12 07:05 108.67-8 Vinyl acetate ND mg1L 0.010 1 04112112 07.05 108-05-4 'Fnyt chloride ND nW_ 0,0050 1 04112/12 07:05 75.01.4 ai&p-Xylene INN mg1L 0.0050 1 04/12/12 07:05 17S601-23-1 0-Xylene WD mutt. 0.0050 1 Q4112112 07:05 05-47-6 Surrogates Dibremo uo(ameaaane(y) 122 % 70-130 1 0411211207:05 186e-53-7 4-Brort10tluoroher•.zene (S) 101 % 70-130 1 04/12/12 07:05 460.00- 4 Toluene -a (S) 97 fo 70-130 1 04/12/12 07:05 2037-26-5 1,2-DlChlorpe:h Ilse d4 (S) 12a 5u 70-130 1 04112112 OT.05 17080.37-0 420.4 Pherolles, total A^:dylleaI Method-. EPA 420.4 Phenol NE) mg1L 0.013 1 04/11112 15:06 108.95-2 450OCNE Cyanide, fatal Analytical Method: SPA 4500-011-E Cyanide N❑ rtgf'L 0.0050 1 0d1131t2 15:40 57-12-5 S;Imple: SDO 6 Lab iC: 92115467003 Collected: 03131/12. 10:30 Received: 0402112 09:10 Maliix: Wier Parameters Results Units Report Urlil DF Prepared Analyzed CAS No. Cuai 2540D Toter Suspended Solids Analytical Wilted: SM 2.5.100 Toiai Suspended Sofrds 12.3 mg/L 2.5 1 (14103112 13:05 9046 pit Analytical h:elhad: EPA 9040 pi i 9A Sid- Units 0-10 1 04/03112 08:57 H6 HEM, 011 and Grease Analytical i•.leihod: EPA 16;4A Oil and Gte:lse ND mgli_ 5.0 1 04104/17. 06:10 608 GCS PczAicldes and PCBs Analytcal Methad: EPA608 Preparation Ffsthcd: EPA 3635 Aldd,% 1'40 ntg1L 0.000050 1 04/03/12 1800 04105/12 05:55 309.00-2 alpha•B iC NO mu1L 0.000050 1 04/03/12 18:00 0410502 Oh:55 319-84-6 hela-GHC N 0 mg/L 0.000050 1 134/031-, 2 13:00 04105/12 05:55 319.65-7 del'a-BHC ;.In mg1L 0.000050 0410302 16:00 04i"GW12 05:55 314.8C-8 gamma-8HC (Lindane) ND ntglL 0.000050 1 pa103n2 18:00 0410511205:55 58-69-9 Chlordane (Technical) ?:0 mq& 0.00050 1 04/03112 18:00 04105112 05:55 57-74-9 4,4`-DDD ND mg1L 0.000050 ; U4r03/t21u:00 04105/1205:55 72-54-3 4,4'-Q0E ND mijrL 0-000050 1 C4103112 18:00 Ci4r`05112 05:55 72-55-9 NO m9k 0-000050 1 04M3112 15:00 04105117 05:55 50-29-3 Dieldrirl ND murL 0,0000511 1 0410 !1218:00 0410511205:55 60-57-1 Eltdasuffan l ND mg1L 0.00,9050 1 04103+12 18:00 0410:112 05.65 059.98-8 Dole: 0.' 1' 612012 01:35 PNI REPORT OF LABORATORY ANALYSIS Page 14 of C5 This ropart shall nol be reproduger:. except in fort. ve:ho�r the,ntitlen consc:d of Pace-.ralyUcn6 $arVi4Y5, Inc,- ' Pace Analytical Services, Inc, pace Analytical Services, Inc. Pace Analytical Services, Inc. A aceAnap cat 205 East µaadaw Road - Suite A 2225 Rtmrside Dr. 9800 Kiamy Ave. Suite 100 _ rf eCaxlaSs.ava Eden. NC 27288 Asheville, NC 25604 HurY.etsviila, NC 2807E {336)623-E42S (928)254-7178 (704)675-9092 ANALYTICAL RESULTS Project: Storm ftterOW31/12 Pace Project No.: 92115467 Samplo: SDO6 Lab ID: 9211SA67003 Collected: 0313111210:30 Received; 04I0211209:10 Malrix:Water Pefamaiers Results Units Repert Limit DF Prepared Analyzed CAS No. Qrsal 608 GCS PesEic ides and PCBs. Analytical Method: EPA 608 Preparadoll Method: EPA 3535 Endosutfan 11 NO mg/L 0.000050 ) 0410302 16:00 04106/12 05:55 33213-65.9 Eneasulfart sulfate NO mg/L 0.000050 1 04M3i12 I&CG C4105112 05:55 1031-07-8 Endrin ND mg/L 0.000050 1 04/03/12 E8:OO 04f05/12 05:55 72-20-6 Endrin aldehyde NO mg/L 0.000050 04/03/12 18:00 34105/12 05:55 7421-93-4 Heptachlor Ni) mg1L 0.00005G 1 0<103112 1$:00 04105112 05:55 76-44.8 Heptachlor epoxi(le Ni) mglL 0.0001350 ! G4103112 18:00 04105A2 05:55 1G2-i-57-3 PCB-1016 (Arcclor 1015) NO rngiL 0.00050 1 04103M2 18:00 04105112 05:55 12674.11.2 PCB-1221 (Aroclor 1221) ND rr,g11- 0.00050 1 04/03112 18:00 04105/12 05:55 11104-28-2 PCH-1232 (Aroclor 1232) NO rrtyfl 0.00A50 1 0003112 18:00 041M12 05:55 11141-16-5 PCB-1242 (Arvclor 1242) NO mg1L 0.00050 1 04103il 2 1 &00 04/05112 05:55 51469.2 i •9 PCO-1248 (Aroclor 1243) ND mg/l. 0.00050 1 04103/12 18:00 04/05112 05:55 12072-29.6 PCB-1254 (Aroclor 1254) NO m,;L 0.00050 11 04/03/12 i&GO 0410511205:55 11097.69.1 PCB-1260 (Aroclor 1260) ND mm& 0.00050 1 041G3(l P 18:00 04:0602 05:55 11090-82-5 Toxaphule- ND mg/L 0.00050 1 04/03112ISTO 04/0611205:65 6001.35-2 Surrogates Tetrachloro-m-xyterie (S) 86 % 20-110 t 04103/12 18:00 04105M7 05,55 877-09-8 Decadiiorobiphenyl (5) 129 % 20.138 1 04103r12 180) 04105112 05:55 2051-24-3 200.7 IAET ICP Analytical Meit:od'. EPA 200.7 Preparation Method: EPA 200.7 Lead ND rngiL 0.0G50 1 04105/12 11:30 041G6112 03:33 7439.92-1 625 n4SSV Analytical Method: EPA 525 Preparation Netltad'. EPA 625 Acenaphihene ND mglL 00150 1 041`03112 16:00 041071i2 04:00 83-32-9 Acewuphlnyler,e NO mg/L 0 0050 1 04103/12 16;00 0410?112 04:00 208-96-a Ace(ophenoste NO mgrL 0-0050 1 OVUM! 16:00 04107112 04:00 98-85.2 Aniline NO mg/L 0.010 1 04103112 16:00 04/07112 04:00 62-5: -3 Anlhracen® ND mg1L 0.0050 04/03112 M00 0410711204:00 120-12-7 Henzidttle NO rrg/L 0.050 1 04/03112 16:00 04107112 04:00 92-87.6 Benze(a)anthrGcrne NO rng.rl- 0,0050 1 0410311 � 16:00 04r'07112 04:()0 56-55.3 Benzo(a)pyrene NO mgrL 0.0050 1 041O3f12 16:00 04i0.11120400 50-32.8 Benzo(b)11:1ur2nthene NO nrg/L 0.0050 1 04103112 16:00 04107/12 04:00 205.99-2 Benzu(g,h.i)peryierle NO rr,c11L 9.0050 1 0.1103112 16:00 04107/12 04:00 191-24-2 Benzo(x)iluoraritllene ND mg1L 0,0050 1 0-110311216:00 0410 7112 04:00 207-03-9 4-8romoplienylphenyl ether NO rngiL 0.0050 1 C4f03/12 15'00 0410702 04,00 101-55-3 Gutytbenzylp!d ialate NO mg/L 0.0050 1 04/03/12 15:00 0007112 04:00 85-68.7 Carbazole NO m01i. 0DOW 1 (14103112 16:00 04/07112 04:00 86-74-8 4-Chloro-3-methylphenol .1D n1g1L 0,0050 1 04103)12 1G00 04/07112 04:00 59-50.7 bis(2-ChIoroer1soxy)rne01ane ND mg/L 0.010 1 04(0311216:00 04f07/1204:00 i11-31-? 5:s(2-;hlcrue1,hyl)ether tZmgiL 0.0050 i 0410311216:00 04107)1204:00 t11-4-1-n bis(2-Vi!croisopropyl) ether NO mg1L 0.0050 1 04103/12 16:00 04/07112 04:00 108-60-1 2-Chioronaphihalene ND rng?L 0.0050 1 041D3112 16:00 04107112 04:G!3 91-58-7 2-Ch!prOphenc1 `G mgf(. 0,0050 1 04103r12 !6:00 0411371i204:00 95-57-6 4-ChEoropheily!pher,}i ether ND a:y1L 0.13-050 1 U4103A2 16:00 C•1101112 04'.00 7005.72-A Chrysene NO mgil- 0.0050 1 04103117 16:00 04107117 04:00 218-Oi n-Decane NO mg/L 0.010 04103/12 MOO 04YO7112 04;00 124-18-5 Ciberz(o,h)anthiacerte NO mr 0.OG50 i C4103112 16:00 04i07112 104:00 83.70-3 Dais-, 04/16/2912 0 1;3 5 PNI REPOR F QF LABORATORY ANALYSIS pace Is 0t5e This rcpcd shM rol be reproduced, except io Full, yrlhnuf the sgr(ten CbnGer,1 0, Pace Analy;iw7! SenwmS, Inc . /� aceAna"cal KN11raxB1�S,C�n Project: Storm %,rFater 0MV12 Pace Anatyticar Services, fnc. 2t1S Fast Meador Road - Suite A Eden, NC 27288 (335)623-6921 Fece Ar,atytical Services, Inc- 2225 Riverside Or AsheviLe. NC 26a04 .ANALYTICAL RESULTS (e26)254-717F Pace A n atytical Services. Inc. 96GO Kincey Ave. State 100 Hunle:svil!e, NC 26075 Pace Project No 92li5467 Sarnp!e: SDO 6 Lab ID: 92115467003 Collected: OU31112 10:30 Received: 04/02112 09:10 Malrix: Water (704)875-9092 Parameters Results Units Report Limit DF Prepared analyzed CAS No. Quit 625 NISSV Analytical Method. EPA 625 preparation Method: EPA 625 1,2•DicMoroben7ere NO mg/L D.0050 t 0.1103112 16:00 04107112 04:00 95.50.1 0-DichtoroberzeFte AID mg1L 0,0050 1 04102/1210,00 04/07N204:00 541-73.1 1,4-Cichlorobenzeoe ND mg.F1. 0.0050 1 0410311216:u0 04107112 04:00 106-46-7 3,3'•C!chforoCenzidtne NO mg1L 0.025 1 04/03/12 16:00 04/07112 04:00 01-94-1 24-Dich!oropheno! ND mq!L 0.0060 1 04103112 10:00 04107t12 44:00 120-83.2 Oielhylphlha{ate ND mgli- O.D050 1 04l031121fi:00 04107112 04:00 84.6C-2 7.4-Dimelhytphenol ND Mg/L 0.0€0 1 04103/12 15:00 04107/12 04!00 105-67-9 Diole4hylphasa€ate ND nlgil. 0.0050 1 04JO3112 16:00 04tt77ti204:00 131-11-3 ui-n•butylphihalate NO mgrL 0.0050 1 041031Q iG-.00 04107/1704:00 84-74-2 4,6 rinitro 2 met rylphenol NO mall. 0.020 1 04103/12 ,6:00 04107/12 04:00 534-52•1 2 4-Dioitrnpheno{ NG mg/L 0.050 1 04103112 i6:00 04107112 04:00 11-28-5 2.4-pin1tro*1UCcnc ND nm/L 0,0050 1 04103112 10:00 04107/12 04:00 121-14-2 2,6-0;ritrotoluene 41) mgiL 0.0050 1 041031i2 16:00 0410711204:00 GOB-20-2 Di-n-mlyiphihalate ND mg11- 0.0050 1 041C3112 t6:00 04i0711204:00 117-84-0 1,2-01pheny1hyc;ar.irm NO rng;L 0,0050 1 041031t216:00 0410111204:00 122-66-7 bis(2-E1hyr~,exyl),at:Ihalato ND nsr/i. 0-0050 1 04/01112 16:00 04107112 04:00 117-81-7 Fiuoranthene ND MOIL 0.0050 1 04/03/12 16:00 04/07/12 04:00 20C,44-0 r-luornnu ND mg1! 0,0050 1 04/03/12 IOU) 041071i204:00 86-73-7 Hexachloro-1.34butadiene ND Ing1L D,0050 1 0410311216:00 Or i07112 04: 00 87-58-3 1iexachl0rabenzCne ND myiL 0.0e50 i 04I03112 16:00 04m7112 04:00 118-74-1 Huxachlerocyclopenladio:)u NO mc,IL D.010 1 04/03112 1B.00 04/0711204:00 77-47-4 tlexaehlerrelha:te ND mg1L 0,0050 1 04/03/12 16:00 04/07112 04:00 67-72.1 :adeno(1,2,3•cd3 pyren2 NO rng1L 0.0050 1 04143/12 16:00 04107t12 04:DO 193-39-5 `.Sophrrone NO mcA 0.010 1 (WOW11 16:00 04107/12 04:00 78-59-1 Nophllialene ND mc3!4_ 0.0050 t 041GOI12 €6:00 C4107,1204'00 91-ZO.3 litrobeozene NO mg1L 0.0050 1 04103/12 15:00 04107112 04:00 88-95-3 2-Nitraphenol NO mg1L 0.0050 1 134103112 16:00 04107/1204:00 88-75.5 4-1`Jitrnphenol °20 mg1L 0.050 1 04/03112 16:00 04107/12 04-00 100-02-7 iJ-Nit(osodhnelhylaw!ile riD n101L 0,0050 1 04103i12 16:00 0-10711204:00 62-75.9 N-Nltreso-di-n-propylamine NO rrr.'L 0.0050 0,103112 16:00 ;4)0711204,00 621,64-7 N-' iitresodiphenylamine NO mg1L 0.010 1 04/03/12 16:00 04/07it 2 04.00 65-30.6 n-Ocladecane ND mg/L 0.010 1 04103/12 16:00 04107!€2 04:00 593-45-3 Pentachlorophenel WD mg/4 0.025 t 04103/12 16:00 04.07112 04:00 37-E6.5 Phenanthrene ND rngli- 0.0050 1 04103/12 16100 04107112 04:00 85-01-8 Phenol ND mo1L 0 OG50 04103t12 WOO 04107/12 04:00 108-95-2 Fyrene NO mg/L 0.0050 1 04/03/12 16:00 04107i12 04:00 112s-00-0 1.2,440chtorrbenzeile oil rngJL 0.0050 1 C4/03112 1&00 04107112 04:00 120-82-1 2.4,G-Tr1Ch1Croptlettr1 1JD my/L 0.010 1 041D3112 16:00 04107!12 04.00 88-06.2 Sorrrga(es Nitt0be:tzene-d5 55 % 10-:20 1 04MVi 2 16:00 04107112 04700 4165-60-0 2-Fluorobipheny{ (S) 52 '% 15-120 1 04/03/12 16:00 04/07117, 04:00 321-E0-13 T:_fphenyr,dl4fS) 70 35 11-1331 1 0410112 16:00 0A107112 04,00 171g-51-0 Phenol•r16 r,S) 20 °k 10,120 1 04103/12 16:00 04/07112 C4:00 13127.88.3 2-Fluoropt-.crlut (S; 3o % 10-120 I 04MV12 16:00 04/07112 04:00 367-12-4 2.4,6-Tri6romcphcrol (S) 70 °J 10-137 1 04103/1: 16:00 04107M2 04:00 116-79-6 Date: 04116,201204:35PM REPORT OF LABORATORY ANALYSIS Page 160:56 T 1ps wrwt shusl not be repiaduced. exccpt in full, :vi:.hou;!he wri-. en censenl of Pacei.nafytical Services. Inc.- Pace AnalyGcaf Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ytical 205 Eas: Meadow ra2d - State A 2225 Riverside Or. 98U0 Kincey Ave. Suite 10o wmrparo7k�Wn Edrn, NC 272a8 AshevrCe, NC 28804 HamerwAfe, NC 28078 i 1336)623-6921 (828)25a•7176 (704)875.9092 ANALYTICAL RESULTS Project: Stour Wafer M1112 Pace Project No.: 92115467 Sample; $DO 6 Lab 10: 92115467003 Collected: 03/31/12 10:30 Received! 04102/12 09:10 Malrfx: Water Peramefers Results knits Report Limit DF Prepared Analyzed CAS No. Quoll 624 Volatile Organics Ana ly ticaI'Ail hod: CPA 624 Acetone ND inglL 0-025 1 04/12112 07.30 67-64-1 Acrclein ND mgiL 0.10 1 04112/12 97:30 107.02-8 Acrylarulrilo NO mg11- 0.10 1 04112/12 07:30 307.13-1 9enzene 1`113 mg1L 0.0050 1 04112112. 07:30 71-43-2 Sromoberizeno ND mg/L D.0050 1 04/12/12 07;30 108.86-1 Bromochleromethane ND mg/L 0.0G50 IL C4/1211207:30 74-97-5 9romodictlaramethan8 1:D mgiL 0,0050 1 04112M2 07:30 75.27-4 Bromoform ND mg/L 0.0050 1 04112112 0:30 75.25-2 Slomamettlane ND mg1L 0.010 1 04/12112 07:30 74-83-9 2-801none (FAEK) NO mp7L 0.0050 1 0411Z11207:30 78-03-3 n•6ulylhanzene ND mg/L 0,0050 1 0411?112 07!30 104.51-8 sec-6atylbenzene NO mg/L 0.0050 1 04112/12 07:30 135-9.3-8 lent-Bu!ylborzene ND rngit 17.U050 1 04/12112 07:30 98.06.6 Carban disulfide NO mg/L O.D10 t 04112112 07:20 75.15-0 Carbontelrachlorde NO mgiL 0.0050 1 04fl2/1207.30 5C-23-5 Chlorobenzene ND mg/L 0.0050 1 04112/12 07:30 108-90-7 Chlomethare Mn rng!L 0.010 1 0411211207:30 75-00-3 2-Chiaraelhyivinyl ether vD mt IL 0.010 1 04/12/12 07:30 i 10.75-0 Chloroform ND nlgrl- 0.0050 1 040 2112 07:30 67-6E-3 Chiorontelhane ND mgfL 0.0050 1 04!12112 07:30 74-87-3 7.-Chlomtoluene VLF mg/L 0.0050 i C41iM207:30 95-49-8 4-Chiowtuttrene ND mgiL 0.0050 1 04112A2 07:30 106.43-4 Oibrornoclllororne€hnne N0 mg/L 0.0050 1 04/12112 07:30 124-48-1 1,2-Dibromaethane (EC8) NO n1gli- 0.11050 1 D4112112 07:30 ,013-93.4 Dibromomethane IND mg/L 0.0050 1. 04MM2 07:30 74-95.3 1,2-DiOhlombenzene NO rng/L 0.005D 1 0411211207:30 95.501-1 1,3-Dichlorobemene NO mg/L 0.0050 1 04/1211207:30 541.73-1 1,44--ichl0robenzene ND mr31L 0,0051i 04112112 07:30 106.46-7 t,i-Dichlaraelhane NO mgiL 0.0050 1 0411211207:30 75-34-3 1,2-Dichforocthane NO mgfL 0,W50 1 04/12/12 07:30 107-06-2 1,1-Dich(crcethene ND mgfL 0.00.W 1. 04(12/12 07:30 75.35-4 cis -1.7-Dichtoroelhene NO mgiL 0.0050 1 04M/12 07:30 155-59-2 Trans l,2-Dicylloroethe, r NO mg/l, 0.0050 1 04112112 07:30 15e-50-5 1,2-Gi0forcproparte N0 mgli. 0.0050 1 0411211207:30 78.87-5 1,3-Oictiloropropare ND tslylL 0.0050 1 04112/12 07:30 142-25-9 2,2-111chloropropane ND mg/L 0.0050 1 0'112/12 07:30 594.20-7 1.1-l7ichloroprullene ND mg(!- 0.0050 1 04/12/12 07;30 563-50-6 cis-1,3-Dicttiarolampe,7e ND mg:L 0.0050 1 04/12112 07:30 10061-111-5 trans '.1•Uict!oroprapcne 'vC nls,ii- 0.0050 1 04112112 0710 10061-Lr2.6 Ethy ben2ane NO r%q/t 0.0051) 1 04112//2 07:30 100•41-4 hlexachiora-1.3•buiocliene ND mcll 0.0050 1 04112112 07:30 87-68-1 2-Hexdnone NO mgiL 0.010 1 04112112 07:30 591.78-n lodume(hanu ND m&L G.010 1 04/17/12 07:30 74-88-4 !saplopylbencene (Curriene) NO mgiL 0,0050 1 04/12112, 07;30 98-82-8 p-Nopropylrotuene NO mgiL 0.0050 1 04112//2 07:30 99-87-6 MOhyien-2 ChIcride ND mGIL O.OG50 1 04il2112 07:30 75-09-2 4-Mcthyl-2-pontanone (WOK) NO MOIL 0.010 1 04112112 07:30 108-10-1 Gate: 041161202 01:35 rM REPORT OF LABORATORY ANALYSIS Page 17 of 66 This tepa,l shall rol be reproduceet, except im full, wnhoc:! the wimert consent ri Pace Ana:ytical Services, :nr- Pace Analytical Services, Inc. Pace Anotydcal Services, Inc. Pace AnalyucaI Services, Inc. I r- a7ce Anal J/ticala• 2GS East N-eedow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Srile 100 am` s Eden. NC 77Ze8 Ashevige, NC 288G4 Hun:ersvilli e, NC 23078 (336)623-8921 (E128)254.7176 (704)875-DC92 ANALYTICAL RESULTS Project: Storm Water 0131112 Pace Project No-: 92115407 Sample. SIDO 6 1-ah lD] 92115467003 Collected: 03/31112 10:30 Received: 04/02/12 09:10 Matrix: Water Parameters RUSLAS Units Report Limit OF Prepared Analyzed CAS r.0. Qual 624 Volatile Organics Anafy0ral Methcd: EPA 624 Methyl-lerl-butyl ether NO ing/L 0.0050 i 04117J12 07:30 1534-04-4 Naph0mlene ND rrlorl_ 0,0050 1 041f2f1207:30 91.20-3 n-Propylbenzene NO mglL 0.0050 I Da112/12 07:30 103.55-1 Styrene `:D mglL D,0050 1 04/12112 07:30 100-42-5 1,1.1,2.Tetfachloroethane 140rus1L 0.0050 1 OC12112U7:30 610-20-6 1,1,2,24elrachloraelllane NO mglL 01)050 1 04112/12 07:30 79-34-5 Te1raG#'.lorr7etl�nne .VD MOIL 0.0050 1 04112/12 07:30 127.18-4 foluer;e ND ngrl- 0,0050 1 04112/12 07:30 108-88-3 1,2,3-11chlcsobenzene NO rogIL 0.0050 1 04112112. 07:30 87.61-6 1,2,4-Trichleroberzene ND wg/L 0.0-350 1 04/12112 07:30 120-82-1 1,1,1-Tfichloweltiane ND ms,'L O.OD50 1 0411 Z/1 2 07 : 30 71-56-6 1,1,2-Trichloroethane NO nlglL 0.0050 1 04112Y 2 07:30 79.00-5 Tfichiorcethene ND Ing1L 0,0050 1 04112/12 07:30 79.01.E Trirhtcrolluorone:hune ND mglL 0.010 1 0411211207=30 75.69-4 1,2,3-Trich!aroorapane ND mgfL 0.0050 1 040211207:30 96-18-4 1,1,2-Trichloralri3uoroethar-e NO my/L (1.0050 1 0411211207:30 76-13-1 1,2,4-Trimethylbenzene ND nlgrt 0.0050 1 041121120710 95.63-6 t,3,5-Tfinclhy4benzene NO mg1L 0 0050 1 04/12112 D7:30 108.07-h Vinyl aoetate NO moil- 0.010 1 0»112112 07:3C 108-05-4 'Vinyl chloride ND rug/L 0.0050 1 04)12112 07:30 75.01-4 m3p-Xylene ND mg1L 0.0050 1 OQ12112 07:30 17960i-23-1 o-Xylene ND rng1L 0.0050 1 0402112 07:30 95.47-6 Surrogates Dibmina lurrornwhane (S) 123 % 70.130 1 0411ZIIZ 07:30 1868-53-7 4-11oinofturuhenzene t5) 107 % 70-130 1 04112/12 07:30 460.00-4 Toluene-d8 (5) 100 % 70-1.10 7 04f1202 07;30 2037-26-5 1,2-Uichloroethane-d4 (S) 123 % 70-130 11 04112112 07:30 17060-07.0 420.4 Phenolics, Total Analytical Method: EPA420.4 Phenol Na m911- 0.010 1 04111112 15:09 106.95-2 4500CNE Cyanide, Total Analytical hieshod: S`d 4500-CN-E Cyanide NO mgll- O.D050 1 G4113112 15:42 57.12-5 Samlrle: SOOT Lab ID: 921154671D04 Collected_ 03/31112 11:00 Received: 04/02112 09:10 Maui,(: tVater Parameters Results- units Report limit OF Prepaied Analyzed CAS Hu. Qual 25400 Total Suspended Solids Total Suspended SOWS 13049 pN PIi Analytical 10.3thod: &M 25zUD NO my1L 2,8 1 04103M2 13:05 Anaiytica? Memcd: EPA 9040 6.1 Sid. units 0-10 I 04103117. 08:57 lib Date: N11612012 a1:35 PM REPORT OF LABORATORY ANALYSIS Page 18 of 613 Ti,iS repay; shSls nut be reprodviced, except in %01, wiincRA the written eorsert of dace Afw-r r,4 se. -vices, Int. is ` �-,;::•/' rr In ��:"- i'��ti.•-__�`ti•1 •�S •�, •€.�? ��" fr i Yr,^� .tea _ f .*�il�_.f` _ �.��,ti„; �- ::�r•-• .,:�.},�r�-`? �� �`rvil -- •. "� ' Fri•C, Air r! �r ^�. i• ,.• Mi F.'y1".+.5'. t ' ?`SSS='[:%``i r fiaJY _ i' �1}'`ti , 4 _ °s• �� l Prr3'6:3 �_..3. :A-�€ i �€ r� '^ - � . rr:• 1 •.•' •r .i r yam. �i�• KF•'__' ; �• i .., / : _;•.ic�s� " f,. • S R �'' —sue'.. 'Natelp � 4 ./' 'j�- _ -_.• f fl `� +�'�-"sSr�:' n',:,ff.�''�" :�i` ,3 •-- ,l v ti" • ter. • •" • � t % 7170 S- - d'"S•`f W£� �i d ,r��� �� •,�':?. �.��y -. �t�• '1t .i' % a s � / ^v .r � f s• : e:;•17y 1 q � 3 t, • t, 1` �]j y=rif••2{�0µr Errilntt\It 1 n I�• 't}.f:!"`�- '` � rs � � � ,�: /v •,ice nT '^, , i. ? vt� "� 3, :R.f r'r � �� a - S+'� �`,�\'% _� :� 1� tea' p///v1 Weil-Me�ain`��rs` - 75 r`• I 'g' j $Cf• n `� f._-f * Z p�Va ; 4 ! L3 J y �' a. �� a�� %�i' '1 • 3 Mnad7W €� w r%p � 1 l li! i i ,h ��� i � 5 !� 0 5 ..._� ��i' 'o � ` F SS �•:- s t �j } 1 Fl`h ` /1Gi CDYr�eh r {{�a UnramBd fr5utaries ems- J[ n i t t�irIPz/f t ,' ii �C ' :%rr •lf,� �� 4�.. �S Aii�i to ` + X� ° �8� y-. V �I.`+�•1`i\� � f� �,�ca ,�r . -°��� `,I A+"'xe �If1 1� '/`w �r -:•t� L�'' II � �i •+iy� f.-•� n � -,� • Q,,f r'1 0���11�-L"\ `��� I� ,n`' r�•j4il�n��.�1. ,i�s ��rr/ ��.f-� �����5 � l ti}'/., nE skrui Wf Pond* � (.j` r+�(!g f)(".' y 4 '�C' �� j� .%� - --�! ir•.= r_.., ,. �� �fff ��- i ! ,- �,��' _ : j +•�.ee';rnrts `moo•? •3d Tops],aas Ca{ , gm IM DeLar:ne YwTnoutN ME G4M Scum Uala USG3 . • . ' a SCALE IN =EET DRAWN BY: FERRYW Weil -McLain Eden, north Carolina APPROVED By; TGG PROJECT NO. 00\71 W12.01 P Figure 7 FILE NO. 71MS01-AV.'G Location and Drainage Map DATf:: 2/23/2005 FIGURE 3 OUTFALL DRAINAGE AREA MAP StkYPP?-.-OH D W unri'low s Taylor -Smith, Aana From: Roberts, Melinda [mroberts@weil-mclain.com] Sent: Thursday, May 30, 2013 3:36 PM To: Taylor -Smith, Aana Subject: RE: SDOs Not a problem thanks Aana! rM_]WE1L,MdA1N Melinda Roberts Environmental Health and Safety Weil -McLain 523 S. New Street Eden, NC 27288 TEL +1-336-627-6037 MOB +1-336-392-7134 FAX +1-336-627-6067 m robe rts(cDweil-mcla in. com www.marleymep.com 1 www.weii-mclain.com Please consider the environment before printing this email The information contained in this electronic mail transmission is intended by Marley Engineered Products LLC and/or Weil -McLain, a division of The Marley-Wylain Company for the use of the named individuals or entity to which it is directed and may contain information that is confidential or privileged. if you have received this electronic mail transmission in error, please delete it from your system without copying or forwarding it, and notify the sender of the error by reply email so that the sender's address record can be corrected. From: Taylor -Smith, Aana [mailto:Aana.Taylor-Smith@ncdenr.gov] Sent: Thursday, May 30, 2013 3:15 PM To: Roberts, Melinda Subject: RE: SDOs Sorry it took me so long to respond — I have been out in the field. You can send it to my attention if you want or to W. Corey Basinger, my supervisor. Thanks! Aana Taylor -Smith Surface Water Protection Section Winston-Salem Regional Office Division of Water Quality Phone: (336) 771-4950 Fax (336) 771-4630 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. From: Roberts, Melinda [mailto:mroberts@weil-mclain.comI Sent: Thursday, May 30, 2013 11:33 AM To: Taylor -Smith, Aana Subject: RE: SDOs Aana, Please see the attached ROS request form. ! will go ahead and mail this to the Winston Salem office today!. Thank you again for all your help! FR-M]WEILuMt LAIN Melinda Roberts Environmental Health and Safety Weil -McLain 523 S. New Street Eden, NC 27288 TEL +1-336-627-6037 MOB +1-336-392-7134 FAX +1-336-627-6067 mroberts@weil-mclain.com www.marleymep.com / www.weii-mclain.com Please consider the environment before printing this email The information contained in this electronic mail transmission is intended by Marley Engineered Products LLC and/or Weil -McLain, a division of The Marley-Wylain Company for the use of the named individuals or entity to which it is directed and may contain information that is confidential or privileged. If you have received this electronic mail transmission in error, please delete it from your system without copying or forwarding it, and notify the sender of the error by reply email so that the sender's address record can be corrected. From: Taylor -Smith, Aana [mailto:Aana.Taylor-SmithCa)ncdenr.govl Sent: Thursday, May 30, 2013 8:00 AM To: Roberts, Melinda Subject: RE: SDOs Hi Melinda, Yes, I am really glad we have a short week —especially since I am going to Charleston this weekend! Hope your holiday was great as well! Q This looks great! If you want to date this copy, re -scan it, and email it to me, I'll get started on the paperwork on our end We will also need the original in the mail, but I can get started on it today if you'll just email me the dated page. Thank you so much! Aana Taylor -Smith Surface Water Protection Section Winston-Salem Regional Office Division of Water Quality Phone: (336) 771-4950 Fax (336) 771-4630 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. From: Roberts, Melinda [mailto:mroberts(&weil-mclain.com] Sent: Wednesday, May 29, 2013 3:39 PM To: Taylor -Smith, Aana Subject: RE: SDOs Aana, I hope you had a wonderful memorial day weekend! Best part about a long weekend is a short work week O. When you get a chance would you mind looking over our representative outfalls status request form. All comments, criticism and suggestions are appreciated. Regards, FR]WEILORLAIN Melinda Roberts Environmental Health and Safety Weil -McLain 523 S. New Street Eden, NC 27288 TEL +1-336-627-6037 MOB +1-336-392-7134 FAX +1-336-627-6067 mroberts(dweil-mclain.com www.marleymep.com'/ www.weii-mclain.com Please consider the environment before printing this email The information contained in this electronic mail transmission is intended by Marley Engineered Products LLC and/or Weil -McLain, a division of The Marley-Wylain Company for the use of the named individuals or entity to which it is directed and may contain information that is confidential or privileged. if you have received this electronic mail transmission in error, please delete it from your system without copying or forwarding it, and notify the sender of the error by reply email so that the sender's address record can be corrected. . From: Taylor -Smith, Aana [mailto:Aana.Taylor-Smith(a)ncdenr.gov] Sent: Wednesday, May 29, 2013 8:14 AM To: Roberts, Melinda Subject: RE: SDOs The only TTO certification statement I have from Weil -McLain is from 2008. I'm not sure we received the analytical results from 2012 either, but those may have been received by Central Office and not forwarded to Winston-Salem. That happens sometimes... Aana Taylor -Smith Surface Water Protection Section Winston-Salem Regional Office Division of Water Quality Phone: (336) 771-4950 Fax (336) 771-4630 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. From: Roberts, Melinda [mailto:mroberts weil-mclain.com] Sent: Wednesday, May 29, 2013 7:57 AM To: Taylor -Smith, Aana Subject: RE: SDOs Thank you very much! Also, have we not submitted that statement yet in regards to out TTO Plan? FR—M]WEILeMi LAIN Melinda Roberts Environmental Wealth and Safety Weil -McLain 523 S. New Street Eden, NC 27288 TEL +1-336-627-6037 MOB +1-336-392-7134 FAX +1-336-627-6067 mrobertsCa@weil-mclain.com www.marleymep.com I www.weii-mclain.com Please consider the environment before printing this email The information contained in this electronic mail transmission is intended by Marley Engineered Products LLC and/or Weil -McLain, a division of The Marley-Wylain Company for the use of the named individuals or entity to which it is directed and may contain information that is confidential or privileged. If you have received this electronic mail transmission in error, please delete it from your system without copying or forwarding it, and notify the sender of the error by reply email so that the sender's address record can be corrected. From: Taylor -Smith, Aana [mailto:Aana.Taylor- Smith (Ja)ncdenr.qav] Sent: Wednesday, May 29, 2013 7:55 AM To: Roberts, Melinda Subject: RE: SDOs Sure thing! I am about to go out in the field for the morning, but I would be happy to review it this afternoon when I return. Thanks, Aana Taylor -Smith Surface Water Protection Section Winston-Salem Regional Office Division of Water Quality Phone: (336) 771-4950 Fax (336) 771-4630 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. From: Roberts, Melinda[maiIto: mroberts(@weil-mclain.com) Sent: Wednesday, May 29, 2013 7:53 AM To: Taylor -Smith, Aana Subject: RE: SDOs Aana, Can I send over my representative outfall status request form for you to review prior to submitting? Any input, comments, suggestions would be appreciated? FA]VERnMewN Melinda Roberts Environmental Health and Safety Weil -McLain 523 S. New Street Eden, NC 27288 TEL +1-336-627-6037 MOB +1-336-392-7134 FAX +1-336-627-6067 mrobertsO,weil-mclain.com www.marleymep.com 1 www.weii-mclain.com Please consider the environment before printing this email The information contained in this electronic mail transmission is intended by Marley Engineered Products LLC and/or Weil -McLain, a division of The Marley-Wylain Company for the use of the named individuals or entity to which it is directed and may contain information that is confidential or privileged if you have received this electronic mail transmission in error, please delete it from your system without copying or forwarding it, and notify the sender of the error by reply email so that the sender's address record can be corrected. From: Taylor -Smith, Aana [mailto:Aana.Ta for -Smith ncdenr. ov] Sent: Friday, May 24, 2013 10:52 AM To: Roberts, Melinda Subject: RE: SDOs Hi Melinda, I was just reading through your permit and I realized that there is a clause under Part II, Section A, #10 about toxic organics that you might find helpful. I thought I remembered seeing a Total Toxic Organics (TTO) or Solvent Management Plan in your Stormwater Pollution Prevention Plan (SPPP)? if that Management Plan contains the following items, and you submit a certification statement, then DWQ can waive your sampling requirement for organics at all outfalls: (a) an annually updated and quantified inventory of the total toxic organic compounds present on site during the previous three years; (b) a narrative description of the in -plant locations and uses of the toxic organic compounds, the method of disposal including quantities disposed on- and off -site; (c) the management procedures and engineering measures for assuring that toxic organics do not spill or leak into stormwater. If that's something you'd be interested in, send me a scan of the Management Plan and the following signed statement, and you can stop sampling for organics: "Based upon my inquiry of the person or persons directly responsible fir managing compliance with the permit monitoring requirement for total toxic organics (TTO), 1 certify that to the best of my knowledge and belief, no leak, spill, or dumping of concentrated toxic organics into the stornnwater or onto areas which are exposed to rainfall or stornnwater runoff has occurred since filing the last discharge monitoring report. 1 further certify that this facility is implementing all the provisions of the Solvent Management Plan included in the Stormwater Pollution Prevention Plan. " You'll still have to sample for pH, TSS, oil & grease, copper, lead, zinc, and record the rainfall, but taking out organics ought to save you ail some time and money. The only requirement is that you have to review that Management Plan and send in the above signed statement semi-annually along with your sampling results on the Discharge Monitoring Report (DMR). Hope that helps! Aana Taylor -Smith Surface Water Protection Section Winston-Salem Regional Office Division of Water Quality Phone: (336) 771.-4950 Fax (336) 771-4630 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Low and may be disclosed to third parties. From: Roberts, Melinda(mailto:mroberts*weil-mclain.com} Sent: Monday, May 20, 2013 2:04 PM To: Taylor -Smith, Aana Cc: Miller, Jim H. Subject: RE: SDOs Thank you Aana! It was also a pleasure meeting you today and I greatly appreciate all the information you've provided! rM_]WEIMMIN Melinda Roberts Environmental Health and Safety Weil -McLain 523 S. New Street Eden, NC 27288 TEL +1-336-627-6037 MOB +1-336-392-7134 FAX +1-336-627-6067 mroberts0weil-mclain.com 1 www.marleymep.com I wvvw.weii-melain.com Please consider the environment before printing this email The information contained in this electronic mail transmission is intended by Marley Engineered Products LLC and/or Weil -McLain, a division of The Marley-Wylain Company for the use of the named individuals or entity to which it is directed and may contain information that is confidential or privileged, if you have received this electronic mail transmission in error, please delete it from your system without copying or forwarding it, and notify the sender of the error by reply email so that the sender's address record can be corrected. From: Taylor -Smith, Aana [maiIto.,Aana.Taylor-Smith@ncdenr.gov] Sent: Monday, May 20, 2013 1:23 PM To: Roberts, Melinda Subject: SDOS Melinda, It was great to meet you today! Here's some information on the stormwater discharge outfalls that we talked about earlier: As far as Representative Outfall Status (ROS) goes, I have attached a form that you can fill out and submit for outfalls 1-6 1 think I told you earlier that this had to go to Raleigh, but I was thinking of the No Exposure form —you can send the ROS form to the Winston-Salem office. I have attached the No Exposure Certification (NEC) application form, which lists all of the requirements for getting NEC at your facility. The cover for materials just has to be protected by a "storm resistant shelter to prevent exposure to rain, snow, snowmelt, and/or runoff," which leaves you with a lot of choices. I would not, however, recommend a tarp because that doesn't seem quite storm -resistant or permanent. As for the other outfalls that are not on your property, you will unfortunately have to keep sampling them unless you receive NEC status. The outfalls convey stormwater from your property, where it may be exposed to industrial activity, to surface waters of the State, even though said surface waters may not be on your property. Sorry about that! Let me know if there's anything else I can help you with! Have a great week! Aana Taylor -Smith Surface Water Protection Section Winston-Salem Regional Office Division of Water Quality Phone: (336) 771-4950 Fax (336) 771-4630 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. Taylor -Smith, Aana From: Roberts, Melinda (mroberts@weil-mclain.com) Sent: Monday, May 20, 2013 2:04 PM To: Taylor -Smith, Aana Cc: Miller, Jim H. Subject: RE: SDOs Thank you Aana! It was also a pleasure meeting you today and I greatly appreciate all the information you've provided! MONEILaMcLAIN Melinda Roberts Environmental Health and Safety Weil -McLain 523 S. New Street Eden, NC 27288 TEL +1-336-627-6037 MOB +1-336-392-7134 FAX +1-336-627-6067 mrobertsCcDweii-mclain.com www.marleymep.com 1 www.weii-mclain.com Please consider the environment before printing this email The information contained in this electronic mail transmission is intended by Marley Engineered Products LLC and/or Weil -McLain, a division of The Marley-Wylain Company for the use of the named individuals or entity to which it is directed and may contain information that is confidential or privileged. if you have received this electronic mail transmission in error, please delete it from your system without copying or forwarding it, and notify the sender of the error by reply email so that the sender's address record can be corrected. From: Taylor -Smith, Aana [mailto:Aana.Taylor-Smith@ncdenr.gov] Sent: Monday, May 20, 2013 1:23 PM To: Roberts, Melinda Subject: SDOs Melinda, It was great to meet you today! Here's some information on the stormwater discharge outfalls that we talked about earlier: As far as Representative Outfall Status (ROS) goes, 1 have attached a form that you can fill out and submit for outfalls 1- 6. 1 think I told you earlier that this had to go to Raleigh, but I was thinking of the No Exposure form — you can send the ROS form to the Winston-Salem office. I have attached the No Exposure Certification (NEC) application form, which lists all of the requirements for getting NEC at your facility. The cover for materials just has to be protected by a "storm resistant shelter to prevent exposure to rain, snow, snowmelt, and/or runoff," which leaves you with a lot of choices. I would not, however, recommend a tarp because that doesn't seem quite storm -resistant or permanent. As for the other outfalls that are not on your property, you will unfortunately have to keep sampling them unless you receive NEC status. The outfalls convey stormwater from your property, where it may be exposed to industrial activity, to surface waters of the State, even though said surface waters may not be on your property. Sorry about that! Let me know if there's anything else I can help you with! Have a great week! Aana Taylor -Smith Surface Water Protection Section Winston-Salem Regional Office Division of Water Quality Phone: (336) 771-4950 Fax (336) 771-4630 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. IL Pat McCrory Governor MEW North Carolina Department of Environment and Natural Resources Division of Water Quality Charles Wakild, P. E. Director 20 May 2013 Melinda Roberts, Environmental Health and Safety Specialist Weil McLain 523 South New Street Eden, NC 27288 Subject: Compliance Evaluation Inspection ` NPDES General Stormwater Permit NCG030000 Certificate of Coverage NCG030548 Weil McLain Rockingham County Dear Ms. Roberts: John E. Skvarla, III Secretary Aana Taylor -Smith of the Winston-Salem Regional Office of the NC Division of Water Quality (DWQ) conducted a compliance evaluation inspection at the subject facility on 20 May 2013. Your assistance and cooperation during the inspection were greatly appreciated. An inspection checklist is attached for your records and the inspection findings are summarized below. This facility is located at S23 South New Street in Eden, Rockingham County, North Carolina. Stormwater related to industrial activity is discharged from the site to an unnamed tributary to the Dan River, this section of which is currently classified as Class C waters, in the Roanoke River Basin. Documentation & Monitorin Review The Stormwater Pollution Prevention Plan (SPPP) is complete, well -established, and current. It is updated on a yearly basis and all required records were available for inspection. Documentation for employee training was available and signed by all in attendance. The facility has had no significant spills in the past three years. Facility inspections are also completed and recorded as required. The facility has thirteen Stormwater Discharge Outfails (SDOs) at which monitoring is performed on a semi- annual basis. Qualitative monitoring has been conducted and documented as required. Analytical monitoring has also been conducted and documented as required. Pace Analytical is used as a contract lab and pH is monitored by Weil McLain staff using approved methods. Records of calibration of the pH meter were available for inspection. Site Review The facility was found to be very clean and well -maintained. All necessary secondary containment is implemented as required. Each of the thirteen outfalls was examined during the inspection. The SDOs were North Carolina Division of Water Quality, Winston-Uem Regional Office Location: 685 Waughtown St. Winston-Salem, North Carolina 27107 One Phone: 336-771-5000 i FAX: 336-771-46301 Customer Service: 1-877-623-6748 NofthCarolina Internet: www.ncwaterquaiity.arg Naturally JNNa ura ly An Equal opportunity 1 Affirmative Action Employer �/ `f i 6` Weil McLain 05/20/2013 Page 2 of 2 clearly marked and very well -maintained. The receiving waters at each outfall looked clear with no visible foam or floating solids. it was noted during the inspection that outfalls ##1-6 were very similar and may qualify for Representative Qutfall Status (ROS). You must formally apply for ROS by submitting the ROS application form, which can be found and downloaded from the following website, along.with the required accompanying materials: http://portal.ncdenr.org/web/wg/ws/su/npdessw (Click on the "Miscellaneous Forms" tab at the top of the table) During the inspection, it was noted that exposure of industrial activities and/or materials to precipitation is minimal, with the exception of one uncovered materials storage area_ You mentioned that Weil McLain may install a storm -resistant shelter forthat.storage area. When a storage area has been installed, Weil McLain may consider applying for a No Exposure Certification for the facility, which would preclude the need for the stormwater permit, SPPP, and any qualitative and/or analytical monitoring, for as long as the No Exposure condition is maintained at the site. For more information on this program, please review the "NC No Exposure Application Form," which can be found and downloaded from the following website.- .http://Portal.ncdenr.org/vieblwqLws/su/npdess (Click on the "No Exposure" tab at the top of the table) We appreciate your efforts to comply with the stormwater general permit. No additional response to this letter is required. Please do not hesitate to contact Aana Taylor -Smith or me at (336) 771-5000 if you have any questions regarding the inspection or this letter. Sincerely, W. Corey Basinger Surface Water Regional Supervisor Winston-Salem Regional Office Division of Water Quality Attachments: 1. BIMS Inspection Checklist CC: Central Files w/attachments WBSPC Unitw/attachments °WSRCi/ WP w/attachmentsl ti Compliance Inspection Report Permit: NCG030548 Effective: 11/01/12 Expiration: 10/31/17 . Owner: Weil-MoLain SOC: Effective: Expiration: Facility: Weil -McLain County: Rockingham 523 S New St Region: Winston-Salem Eden NC 27288 Contact Person: Gary R Connor Title: Phone: 219-873-0392 Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Representative(s): 24 hour contact name Related Permits: Melinda Roberts Inspection Date: 05/20/2013 EntryTime: 10:00 AM Primary Inspector: Aana Taylor -Smith Secondary Inspector(s): Certification: Phone: Exit Time: 11:00 AM Phone: 336-627-6037 Phone: 336-771-5000 Reason for Inspection: ' Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Metal Fabrication Stormwater Discharge COC Facility Status: ® Compliant ❑ Not Compliant Question Areas: 0 Storm Water (See attachment summary) Page: 1 j Permit: NCG030548 Owner - Facility: Weil -McLain Inspection Date: 05/20/2013 Inspection Type: Compliance Evaluation Reason for Visit: Routine Inspection Summary: Please refer to attached inspection letter. Page: 2 Permit: NCG030548 Owner - Facility: Weil -McLain Inspection Date: 05120/2013 Inspection Type: Compliance Evaluation Reason far Visit: Routine Stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwater Pollution Prevention Plan? ®❑ n ❑ # Does the Plan include a General Location (USGS) map? ❑ ❑ ❑ # Does the Plan include a "Narrative Description of Practices"? ® ❑ ❑ ❑ # hoes the Plan include a detailed site map including outfall locations and drainage areas? ®❑ ❑ ❑ # Does the Plan include a list of significant spills occurring during the past 3 years? ®❑ ❑ !3 # Has the facility evaluated feasible alternatives to current practices? B ❑ ❑ ❑ # Does the facility provide all necessary secondary containment? ® `r l ❑ ❑ # Does the Plan include a BMP summary? ®❑ ❑ Cl # Does the Plan include a Spill Prevention and Response Plan (SPRP)? up ❑ ❑ # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? ®❑ ❑ # Does the facility provide and document Employee Training? ® I•l ❑ ❑ # Does the Plan include a list of Responsible Party(s)? ®❑ ❑ ❑ # Is the Plan reviewed and updated annually? ®❑ Cl ❑ # Does the Plan include a Stormwater Facility Inspection Program? ®❑ ❑ ❑ Has the Stormwater Pollution Prevention Plan been implemented? M 0 ❑ ❑ Comment: SPPP is very thorough and well -maintained. Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring semi-annually? ®❑ ❑ ❑ Comment: Analytical Monitoring Yes No NA NE Has the facility conducted its Analytical monitoring? ®❑ ❑ 0 # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ ® ❑ Comment: Analytical monitoring performed by Pace Analytical. pH measured by Weil McLain staff via approved method; calibration records available. Permit and Outfails Yes No NA NE # Is a copy of the Permit and the Certificate of Coverage available at the site? ®❑ ❑ ❑ # Were all outfalls observed during the inspection? a ❑ ❑ Cl # if the facility has representative outfall status, is it properly documented by the Division? ❑ Q 0 ❑ # Has the facility evaluated all illicit (non Stormwater) discharges? ®❑ ❑ 0 Page: 3 Permit: NCG030548 Owner - Facility: Weil -McLain Inspection pate: 0512o12o13 Inspection Type: compliance EvalLion Reason For Visit: Routine Comment: Facility may wish to consider Representative Outfali Status for Outfalls #1-6. If storm -resistant shelter is provided for materials storage area, facility may be eligible for No Exposure Certification. Outfalls were very well -maintained and clearly marked. Page: 4 ' CRS S ,pej�_ M�,i Ada R ovj,exfiS � ' If t — V u coo V) q n - 1 nd Permit: NGG030548 Owner - Facility: Weil -McLain N G 7 -- LZ v4w s-h-, yvt�e, � Inspection Date: 09/04/2008 Inspection Type: Compliance Evaluation 6ta Reason for Visit: Routine Q��A Stormwater Pollution Prevention Plan Yes No - NA NE Does the site have a Stormwater Pollution Prevention Plan? ✓ ® 0011 # Does the Plan include a General Location (USGS) map? ✓ ®❑ Cl n # Does the Plan include a "Narrative Description of Practices'? ✓ ® n n n '# Does the Plan include a detailed site map including outfall locations and drainage areas? ✓ ® n n n # Does the Plan include a list of significant spills occurring during the past 3 years?I/ ® n n n # Has the facility evaluated feasible alternatives to current practices? ❑ ❑ n # Does the facility provide all necessary secondary containment? �% ® n n n # Does the Plan include a 8MP summary? t/ ® n n n # Does the Plan include a Spill Prevention and Response Plan (SPRP)? ✓ ®❑ 0 n # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? ✓ ®n n n # Does the facility provide and document Employee Training?, ✓ ®n n n # Does the Plan include a list of Responsible Party(s)? ® n n n # Is the Plan reviewed and updated annually? ✓ M n n n # Does the Plan include a Stormwater Facility Inspection Program? ✓ ® n n n Has the Stormwater Pollution Prevention Plan been implemented? {/ n ❑ n Comment: Qualitative Monitoring Yes No NA NE Has the Facility conducted its Qualitative Monitoring semi-annually? ✓ ® n n n Comment: Not all outfalls have been monitored. Analytical Monitoring Yes No NA NE Has the facility conducted its Analytical monitoring? ✓ pa t4- 11G► U ®❑ n n # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? Nr� , n ❑ ® Cl Comment: Not all outfalls have been monitored. Permittee currently claims ROS but has no documentation from the Division granting ROS and there is no documentation on file with the Division: Permit and Outfalis Yes No NA NE # Is a copy of the Permit and the Certificate of Coverage available at the site? ® n n n # Were all outfalls observed during the inspection? fl ® ❑ n # If the facility has representative outfall status, is it properly documented by the Division? t-A /A n n M n # Has the facility evaluated all illicit (non stormwater) discharges? ✓ ® n n n Page: 3 W� ` u m 1.t01 i� c��r�� p rQ C.�C �''e a+ -Wow tM � . Toju_ p l-F -I-J- t*y1p d "*- ' y � am a, 1(4 C�a �d s cs� 6bLU 6yAA1 an old . Permit: NCGO30548 Owner - Facility: Weil -McLain Inspection Date: 09/04/2008 Inspection Type: Compliance Evaluation Reason for Visit: Routine Comment: Permittee currently claims ROS but has no documentation from the Division granting ROS and there is no documentation on file with the Division. Page: 4 Compliance Inspection Report Permit: NGG030548 Effective: 11/01/07 Expiration: 10/31/12 Owner: Weil -McLain SOC: Effective: Expiration: Facility: Weil -McLain County: Rockingham 52.3 S New St Region: Winston-Salem Eden NC 27288 Contact Person: Gary R Connor Title- Phone: 219-873-0392 Directions to Facility: System Classifications: - Primary ORC: Secondary ORC(s): On -Site Representative(s): On -site representative Related Permits: Dolores Green Certification: Phone: Phone: 336-627-6016 Inspection Date: 09104/2008 Entry Time: 12:30 PM Exit Time: 02:30 PM Primary Inspector: Ron Boone Phone: 704-663-1699 Secondary Inspector(s):���I d� Ext.2202 Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection type: Metal Fabrication Stormwater Discharge COC Facility Status: 0 Compliant ® Not Compliant Question Areas: ® Storm Water (See attachment summary) Page: 1 Permit: NCG030548 Owner - Facility: Weil -McLain Inspection pate: 09/04/2008 Inspection Type: Compliance Evaluation Reason for Visit: Routine Inspection Summary: Please refer to attached inspection summary fetter. Page: 2 NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Governor Gary Connor Weil -McLain 500 Blaine St Michigan City, IN 46360 Dear Permittee: Charles Wakild, P. E. Director December 4, 2012 Dee Freeman Secretary Subject: NPDES Stormwater Permit Coverage Renewal Weil -McLain COC Number NCG030548 Rockingham County In response to your renewal application for continued coverage under stormwater General Permit NC6030000 the Division of Water Quality (DWQ) is forwarding herewith the reissued General Permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October 1S, 2007 (or as subsequently amended). The following information is included with your permit package: • A new Certificate of Coverage (COC) • A copy of General Permit NCG030000 • A copy of the Technical Bulletin for the General Permit • Two copies of the Discharge Monitoring Report (DMR) Form • Two copies of the Qualitative Monitoring Report Form The General Permit authorizes discharges of stormwater, and it specifies your obligations for discharge controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself with all the changes in the reissued permit. Your facility has six (6) months from the time of receipt of the permit to update your current SPPP to reflect all new permit requirements. The first sample period of your permit begins January 1, 2013. Your facility must sample a "measureable storm event" beginning during the periods beginning January 1 and July 1 of every year (or, if applicable, report "No Flow," as outlined in Part III, Section E). Also, please note that Tier 3 Actions in Part II of your permit are triggered by benchmark exceedances on four occasions beginning on the effective date of this permit and do not count prior exceedances. The more significant changes in the General Permit since your last COC was issued are noted either in the Draft Permit Fact Sheet that accompanied the public notice (http://Portal.ncdenr.org/weblwci/ws/su/current- notices), or in the Response to Comments / Summary of Changes and Technical Bulletin documents that are posted on the 5tormwater Permitting Unit's website with the new General Permit. Please visit htti)://Portal.ncdenr.org/web/wq/ws/su/npdessw (click on `General Permits' tab) to review that information for your specific General Permit carefully. 1617 Mail Service Center, Raleigh, North Carolina 27699.1617 Location: 512 N. Salisbury St. Raleigh, North Carolina 27604 Phone: 91M07-V1 o 1 FAX: 919-807-6492 Internet: www.ncwa`e�r ality.org An Equ810pportunily Affr.mtivt Action Employer One N orthCarol ina VatLll'6 llw Gary Connor December 4, 2012 Page 2 of 2 Some of the changes include: Part II: • Section A: The Stormwater Pollution Prevention Plan (SPPP) section, if applicable, has been updated to the most current language of our permits. Additional conditions for specific industry sectors have been added to the SPPP requirements in some cases. • Sections B, C: Failure to perform analytical stormwater monitoring may result in the Division requiring that the permittee begin a monthly sampling scheme. • Sections B, C: A lower TSS benchmark of 50 mg/1 for HOW, ORW, PNA and Tr Waters applies to these more sensitive waters. • Sections B, C: The monitoring parameter Oil & Grease (O&G) has been replaced by the parameter Total Petroleum Hydrocarbons (TPH) for vehicle maintenance areas, and in some cases, other analytical monitoring requirements. • Sections B, C, D: Inability to sample due to adverse weather must be recorded in the SPPP, or in separate on -site records if your General Permit does not require an SPPP. Adverse weather is defined in the "Definitions" section of the permit. • Sections B, C: The term "Representative Storm Event" has been replaced by "Measurable Storm Event." A measurable storm event is defined in the permit. • Section D: If the permittee fails to respond effectively to problems identified by qualitative monitoring, DWQ may require the permittee to perform corrective action. Please review Parts III and IV to understand the Standard Conditions of your new NPDES General Permit, including Compliance and Liability, Reporting, Monitoring and Records requirements; Operation and Maintenance obligations; and Definitions. Please note that all samples analyzed in accordance with the terms of this permit must be submitted to the Division on Discharge Monitoring Report (DMR) forms available on the Stormwater Permitting Unit's website above. DMR forms must be delivered to the Division no later than 30 days from the date the facility receives the sampling results from the laboratory. Also note that existing permittees do not need to submit a renewal request prior to expiration unless directed by the Division. Your coverage under the General Permit is transferable only through the specific action of DWQ. This permit does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit package, please contact the Division's Stormwater Permitting Unit at (919) 907-6300. Sincerely, for Charles Wakild, P.E. cc: DWQ Central Files Stormwater Permitting Unit Files Winston-Salem Regional Office STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030540 STORMWATER NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Weil -McLain is hereby authorized to discharge stormwater from a facility located at: Weil -McLain 523 S New St Eden Rockingham County to receiving waters designated as DAN RIVER (North Carolina portion), a class C waterbody in the Roanoke River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, 11, III, and IV of General Permit No. NCGb30000 as attached. .This certificate of coverage shall become effective December 4, 2012. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this 4« day of December, 2012. for Charles Wakild, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission �m WEILAdAIN Weil -McLain Company • 523 New Street • Eden, NC 27288 Tel: (919) 627-6011 -Fax: (919) 627-6067 September 6, 2011 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Stormwater Analytical Monitoring Dear Sir or Madam: 1RECE-:1 VEd SEP 2 0 ,20rf QUA;.tTy SEC7iON ln;ormction Arocessing Unit In accordance with NPDES (NCG030000) Stormwater Permit Condition Part II Section B Tables 1 and 2 of Year 4 Period l is being submitted. Monitoring was conducted for all 13 stormwater discharge outfalls (SDO) as identified in the SWPPP, and "NO FLOW" is being reported. Per the attached letter dated July 11, 2011, attached is Analytical Data from a Stormwater event for all 13 stormwater discharge outfalls (SDO) as identified in the SWPPP. Our onsite pH readings, which were recorded when samples were taken, show SDO's with flow at 5.7 and 6.71. The total rainfall recorded with an onsite gage recorded 0.25" for the period. No Flow was detected in the other I 1 SDO's. The pH meter was confirmed to be in calibration prior to testing using buffer solutions certified at 4, 7, and 10 pH. If you have any questions or comments regarding the enclosed reports, please contact Michael Thomason, Manufacturing Engineering Manager, at (336) 627-6024. Sneer y, V Bob Somers General Manager, Weil -McLain Eden Operations, Eden Cc: Division of Water Quality Enclosure WEILuMcLAIN Weil -McLain Company • 523 New Street • Eden, NC 27288 Tel: (919) 627-6011 - Fax: (919) 627-6067 July 11, 2011 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Stormwater Analytical Monitoring Dear Sir or Madam: In accordance with NPDES (NCG030000) Stormwater Permit Condition Part 11 Section B Tables land 2 of Year 4 Period i is being submitted. Monitoring was conducted for all 13 stormwater discharge outfalis (SDO) as identified in the SWPPP, and "NO FLOW" is being reported. Also attached for your review is the Total Toxic Organic (TTO) certification statement. In an effort to collect two samples per year Weil -McLain will look to pull both these samples during the remainder of the 2011 calendar year. If you have any questions or comments regarding the enclosed reports, please contact Michael Thomason, Manufacturing Engineering Manager, at (336) 627-6024. Sincerely, Larry Miller General Manager. Weil -McLain Eden Operations, Eden Cc: Division of Water Quality Enclosure Weil McLain Storm water Report Report Date 8/24/2011 Permit No. NCG 030000 SDO Onsite pH Lead Oil & Grease TSS TTO Benchmark 6.0-9.0 .033 mg1I 0 m9 100 mgll 1 mg/I 1 No Flow 2 No Flow 3 No Flow 4 No Flow 5 6.71 ND ND 16.3 NA 6 No Flow 7 5.7 ND ND 32.2 NA 8 No Flow 9 No Flow 10 No Flow 11 No Flow 12 No Flow 13 No Flow Note: We have a solvent management plan and do not monitor or TTO. Onsite pH meter checked for calibration with buffers 4, 7, 10 Buffer Meter reading 4 pH 4 7 pH 7 10 pH 10 Meter check by: Michael Moretz Date 7/19/2011 Rain Fall for 7/19/2011 .25" per onsite rain guage Tier One Inspection Inspection of the facility was conducted on 712112011, no other issues were noted. Inspection performed by: Darrell Freeman, Maintenance Supervisor _.PaceAnah�ical' CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be cangoted accuretety. Page-, C of Section A Section B Section C Rsgnhsd C3wd 1Mwmatlom R*cNd rod Proj5d I !on7 atipn: InvnJon lrrfrnmatfon Rspon To AItaml°n: 1306518 . - c L 2 ; ,. Atldre� S� r� e 8 CopyT°: Company Name: REG_ ULATORY`AGENCY.'. r� fV ` Address: r PDE5 F GROUND WATER F DRINKING WATER UST r RCRA ("' OTHER Email To: Purchase Order No.: P+ Orrots RMIa^arra., Phone: Fax: Protect N 2011 Pea pm site Lucfizlon •; ; M, .ref � j : K':'; STATE: N r Requested Out DatdfAT: Protect Number: Pea vronr a: .Requested Analysis Flltored (YIN) •'; - _• Section D Matrix Cortex R.cwr.acfi_+ tsrtsuz r cool p COLLECTED Preservatives S thinking Water DW o Water WT Product star taw tiowposrTE W-1 cokvv3ut ENDicRAa Lij � �+ SAMPLE ID Sdriolbd Oil °L ~ « k m yl LJ �• wP (A-Z. 0.91:) Air AR W w V l Sample *s MUST BE UNIQUE Th.. TS on,ar or 0 a 2 o Npr D _ n �V �! y , O O = O �u C O � z U m m DATE TIME ITJITE TIME a 2 2 z z 2 y Pace Project No.1 Lab I.D. 5 DO OH Ito F uZkax� `': '," z D Z .a PJo - 3 •� 3 u 1- lam; x 1�p a o S' 6.7 ! 7 l IFIOo x 0, A e v� 6 Nu /= (jl k� x e D 0 D 14 A), l` e..r &I x N1 (-= G x x o rr k r k . ADD=NAL COMMEiw7'S . ,.'tq ,' RELINQU SHED BY! A LiATI03J ...:�` , DATE [ .i -TIME, • `S' - ''.'ACC PTED BY f AFFLLIATtOW .; DATE ; :TIME SAMPLE CONDITIONS 7--?0-11 Y3 v �� F) iO SAIMPLE_R NAME AND SIGNATURE:' •': ' ORIGINAL PRINT Name of SAMPLER: t,L t�. b�' �, E 3 SIGNATURE of SAMPLER: DATE Signed Q MMlO 'vrroor rrt tlote� lay elgdrip Tb tmn you are eczeplry Paws NF7 30 day payrr*M tsnm and a¢eeN to late aMrg a c 1.5% per mostn for arty Invo" not patd hitfrin X days'.) F-ALI-4-020vY.07, 15-May-2007 (�2eAnalyfical Wwwpareiahs mm August 03, 2011 Mr. Darrell Freeman Weil McLain 523 S. New St. Eden, NC 27288 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 RE: Project: Stormwater 2011 Pace Project No.: 9298716 Pace Anstocal Services, Inc, 2225 Riverside Dr, Asheville, NC 28804 (828)25d-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. guile 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Freeman: Inclosed are the analytical results for sample(s) received by the laboratory on July 20, 2011. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, \' t Terri Page terri.page@pacelabs.com Project Manager Enclosures is TNI REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 31 ceAnaiytrcal e wrw4<3w4-ftcwn Project: Stormwater 2011 Pace Project No.: 9298716 Pace Analytical Services, Inc. 206 East Meadow Road - Suite A Eden, NC 2728B (336)623-8921 Ormond Beach Certification IDs 8 East Tower Circle, Ormond Beach, FL 32174 Alabama Certification #: 41320 Arizona Certification #: AZ0735 Colorado Certification: FL NEI-AC Reciprocity Connecticut Certification #: PH 0216 Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Kansas Certification #: E-10363 Kentucky Certification C 90050 Louisiana Certification #: LA090012 Louisiana Environmental Certificate #_ 05007 Maine Certification #: FL1264 Massachusetts Certification #: M-FL1264 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Virginia Drinking Water Certification M 00213 Asheville Certification IDs 2225 Riverside Dr.. Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Bioassay Certification #: 9 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadaw Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 633 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (826)254.7176 CERTIFICATIONS Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Montana Certification #: Cert 0074 Nevada Certification: FL NELAC Reciprocity New Hampshire Certification #: 2958 New Jersey Certification #: FL765 New York Certification #: 11608 North Carolina Environmental Certificate #: 667 North Carolina Certification #: 12710 Pennsylvania Certification #: 68-547 Puerto Rico Certification #: FLO1264 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity Virginia Certification #: 00432 Wyoming Certification_ FL NELAC Reciprocity Connecticut Certification #: PH-0104 Florida/NELAP Certification #: E87627 Kentucky LIST Certification M 84 Louisiana DHH Drinking Water # LA 1 ON31 West Virginia Certification #: 357 Virginia/VELAP Certification C 460144 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia Certification #: OOD72 West Virginia Certification #: 356 Virgina/VELAP Certification #; 460147 Virginia Drinking Water Certification #: 00424 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shaft not be reproduced. except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite ioo Hunlersville. NC 28078 (704)875-9092 Page 2 of 31 �G A alyl fial • wwwpacalesmm Project: Stormwater 2011 Pace Project No-_ 9298716 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, inc- 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Analytical Services. lnc. 9800 KinceyAve. Suite too Huntersville. NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Anatytes Reported Laboratory 9298716001 SDO #8 SM 2540D WKS i PA$I-E EPA 1664A CLW 1 PASI-C EPA608 BAG 27 PASI-O EPA 200.7 SHB 1 PASI-A EPA 625 PPM 65 PASI-C EPA 624 TLS 73 PASI-C EPA420.4 LEP 1 PASI-A SM 4500-CN-E JDA 1 PASI-A 9298716002 SDO #7 SM 2540D WKS 1 PASI-E EPA 1664A CLW 1 PASI-C EPA 608 BAG 27 PASI-0 EPA 200.7 SHB 1 PASI-A EPA 625 PPM 65 PASI-C EPA 624 TLS 73 PASI-C EPA420.4 LEP 1 PASI-A SM 4500-CN-E JDA 1 PASI-A REPORT OF LABORATORY ANALYSES Page 3 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. eAnaocal wwWpawlafte m Project: Stormwater 2011 Pace Project No_: 9298716 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analocai Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Anatytical Services, Inc. 9800KinceyAve- Suite too Huntersville, NC 28078 (704)875-9092 Sample: SDO #5 Lab ID: 9298716001 Collected: 07119111'18:00 Received: 07/20/11 15:30 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 16.3 mg1L 3.7 1 07/25/11 08:58 HEM, Oii and Grease Analytical Method: EPA 1664A Oil and Grease NO mg/L 5.0 1 07/25111 08:34 608SF GCS Pesticides and PCBs Analytical Method: EPA 608 Aldrin NO uglL 0,011 1 07/25/11 08:45 07/29/11 23:23 309-00-2 alpha-BHC NO ug/L 0.011 1 07/25/11 08:45 07/29/11 23:23 319-84-6 beta-BHC ND ug/L 0.011 1 07/25/11 08:45 07/29/11 23:23 319-85-7 delta-BHC NO ug/L 0,011 1 07/25/11 08:45 07/29/11 23:23 319-86-8 gamma-BHC (Lindane) NO ug/L 0.011 1 07/25111 08:45 07/29/11 23:23 58-89-9 Chlordane (Technical) ND ug/L 0.56 1 07125/11 08:45 07/29/11 23:23 57-74-9 4,4'-DDD ND ug1L 0.011 1 07125111 08:45 07/29/11 2313 72-54-8 4,4'-DDE NO ug/L 0.011 1 07/25/11 (18:45 07/29/11 23:23 72.55-9 4,4'-DDT NO ug/L 0.011 1 07/25/11 08:46 07/29/11 23:23 50-29-3 Dieldrin NO ug/L 0.011 1 07/25/11 08:45 07/29/11 23:23 60-57-1 Endosulfan I NO ug/L 0.011 1 07/25/11 08:45 07/29/11 23:23 959-98-8 Endosulfan 11 NO ug/L 0,011 1 07/25111 08:45 07/29/11 23:23 33213-65-9 Endosulfan sulfate NO ug/L 0.011 1 07/25111 08:45 07/29/11 23:23 1031-07-8 Endrin NO ug/L 0.011 1 07/25111 08:45 07129/11 23:23 72-20-8 Endrin aldehyde ND ug/L 0,0056 1 07125/11 08:45 07/29/11 23:23 7421-934 Heptachlor NO ug/L 0.011 1 0725111 08:45 07/29111 23:23 76-44.8 Heptachlor epoxide NO ug/L 0.011 1 07126/11 08:45 07/29/11 23:23 1024.57-3 PCB-1016 (Aroclor 1016) NO ug/L 0.56 1 07/25111 08:45 07/29/11 23:23 12674-11.2 PCB-1221 (Aroclor 1221) NO ug/L 0.56 1 07/25/11 08:45 07t29111 23:23 11104-28-2 PCB-1232 (Aroclor 1232) NO ug/L 0.56 1 07/25111 08:45 07/29/11 23:23 11141-16-5 PCB-1242 (Aroclor 1242) NO ug/L 0.56 1 07/25111 08:45 07/29/11 23:23 53469-21.9 PC8-1248 (Aroclor 1248) NO ug1L 0.56 1 07/25/11 08:45 07/29/11 23:23 12672-29.6 PCB-1254 (Aroclor 1254) NO ug1L 0.56 1 07/25111 08:45 07/29/11 23:23 11097.69.1 PCB-1260 (Aroclor 1260) ND ug/L 0.56 1 0725/11 08:45 07/29111 23:23 11096-82.5 Toxaphene NO ug/L 0.56 1 0725111 08:45 07/29/11 23:23 8001.35-2 Tetrachloro-m-xylene (S) 103 % 53-110 1 07125/11 08:45 07/29/11 23:23 877-09-8 Decachlorobiphenyl (S) 78 % 61.121 1 07/25/11 08:45 07/29/11 23:23 2051-24-3 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Lead ND mg1L 0.0050 1 07/25/11 15:00 07/27/11 01:01 7439-92-1 626 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Acenaphthene NO mg1L 0.0050 1 07122/11 16:00 07/25/1122:31 83-32-9 Acenaphthytene NO mglL 0.0050 1 0722111 16:00 07/25111 22:31 208-96-8 Acetophenone NO mg/L 0.0050 1 0722/11 16:00 07/25/11 22:31 98-86-2 Aniline NO mg/L 0,010 1 07/22/11 16:00 07/25/11 22:31 62-53-3 Anthracene NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 120-12-7 Benzidine NO mg/L 0,050 1 07/22/11 16:00 07/25/11 22:31 92-87-5 Benzo(a)anthracene NO rng1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 56-55-3 Benzo(a)pyrene NO mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 50-32-8 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 4 of 31 This report shalt not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. e laciekla"cal Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Surte A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 WWW Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 i336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Stormwater 2011 Pace Project No.: 9298716 Sample: SOO #6 Lab ID: 9298716001 Collected: 07/19/11 18:00 Received: 07/20/11 15:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Benzo(b)fluoranthene ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 205-99-2 Benzo(g,h,i)perytene ND mg1L 0.0050 1 07/22/11 16:00 07/26/11 22:31 191-24-2 Benzo(k)fluoranthene ND mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 207-08-9 4-Bromophenylphenyl ether ND mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 101-55-3 Butylbenzylphthalate ND mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 85-68-7 4-Chloro-3-methylphenot ND mg/L 0.0050 1 07122111 16:00 07125/11 22:31 59-50-7 bis(2-Chloroethoxy)methane NO mg1L 0.010 1 07rMl1 16:00 07125/11 22:31 111-91-1 bis(2-Chloroethyl) ether NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 111-44-4 bis(2-Chloroisopropyi) ether NO mglL 0.0050 1 07/22111 16:00 07/25111 22:31 108-60-1 2-Chloronaphihalene ND mg1L 0,0050 1 07/22/11 16:00 07/25/11 22:31 91-58-7 2-Chlarophenol ND mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 95-57-8 4-Chlarophenylphenyl ether ND mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 7005-72-3 Chrysene ND mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 218-01-9 Dibenz(a,h)anthracene NO mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 53-70-3 1,2-Dichlorobenzene ND mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 95-50-1 1,3-Dichlorobenzene ND mg1L 0.0050 1 07/22/11 16:00 07125111 22:31 541-73-1 1,4-Dichlorobenzene NO mg/L 0,0050 1 07/22111 16:00 07/2$/11 22:31 106-46-7 3,3'-Dichlorobenzidine NO mg/L 0.025 1 07/22/11 16:00 07/25/11 22:31 91-94-1 2,4-Dichlorophenol ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 120-83-2 Diethylphthalate NO mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 84-66-2 2,4-Dimethylphenol ND mg/L 0.010 1 07/22/11 16:00 07/25/11 22:31 105-67-9 Dimethylphihalate ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 131-11-3 Di-n-butylphthalate ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 84-74-2 4,5-Dinitro-2-methylphenol ND mg/L 0.020 1 07/22111 16:00 07125/11 22:31 534-52-1 2,4-Dinitrophenot NO mg/L 0.050 1 07/22/11 1&00 07/25/11 22.31 51-28-5 2,4-Dinitrotoluene ND mg/L 0.0050 1 07122111 16:00 07/25/11 22:31 121-14-2 2,6-Dinitrotoluene ND rnglL 0.0050 1 07/22111 16:00 O1125111 2Z31 606-20-2 Di-n-octylphthatate ND mg/L 0.0050 1 07/22111 16:00 07/25/11 22:31 117-84-0 1,2-Diphenylhydrazine ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 122-66-7 bis(2-Ethythexyl)phthalate ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 117-81-7 Fluaranthene NO mg/L 0.0050 1 07/22111 16:00 07/25/11 22:31 206-44-0 Ftuorene NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 86-73-7 Hexachloro-1,3-butadiene ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 87-68-3 Hexachlorobenzene ND mg/L 0.0050 1 07/22/11 16:00 07125/11 22:31 118-74-1 Hexachlorocydopentadiene ND mg/L 0.010 1 07/22/11 16:00 07/25/11 22:31 77-47-4 Hexachloroethene ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 22:31 67-72-1 lndeno(1,2,3-cd)pyrene ND mg1L 0,0050 1 07/22/11 16:00 07/25/11 22:31 193-39-5 lsophorone ND mg/L 0.010 1 07/22/11 16:00 07/25/11 22:31 78-59-1 Naphthalene NO mg/L 0.0050 1 07/22/11 16:00 07/25111 22:31 91-20-3 Nitrobenzene NO mg/L 0.0050 1 07/22/11 16:00 07/25111 22:31 98-95-3 2-Nitrophenol NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 88-75-5 4-Nitrophenol ND mg1L 0.050 1 07122/11 16:00 07/25111 22.31 100-02-7 N-Nitrosodimethylamine ND mg/L 0.0050 1 07122/11 16:00 07/25111 22:31 62-75-9 N-Nitroso-di-n-propylamine ND mg/L 0.0050 1 07/22111 16:00 07/25/11 22:31 621-64-7 N-Nitrosodiphenylamine NO mg/L 0.010 1 07/22/11 16:00 07/25/11 22:31 86-30-6 Pentachlorophenot ND mg/L 0.025 1 07/22/11 16:00 07/25/11 22:31 87-W5 Phenanthrene ND mg/L 0.0050 1 07122/11 16:00 07/25/11 22:31 85-01-8 Date: 08/0312011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 5 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. laneAnalyfical' www4 acerabsmm Project: Stormwater 2011 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254.7176 ANALYTICAL RESULTS PaceAnelytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 Pace Project No.: 9298716 Sample: SOO 05 Lab ID: 9298716001 Collected: 07/19/11 18:00 Received: 07/20111 15:30 Matrix: Water (704)875-9092 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 626 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Phenol NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 108.95-2 Pyrene NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 22:31 129-00-0 1,2,4-Trcchlorobenzene NO mg1L 0.0050 1 07/22/11 16:00 07125/11 22:31 120-82-1 2,4,6-Trichlorophenol NO mg/L 0.010 1 07/22/11 16:00 07/25/11 22:31 88-06-2 Nitrobenzene-d5(S) so % 10-120 1 07122/11 16:00 0725111 22:31 416560-0 2-i=luorobiphenyl (S) 68 % 15-120 1 07122/11 16:00 07/25/11 22:31 321-60-8 Terphenyl-d14 (S) 74 % 11-131 1 07/22/11 16:00 07/25111 22:31 1718-51-0 Phenol-d6 (S) 35 % 10-120 1 0722111 16:00 07/25/11 22:31 13127-88-3 2-Fluoroptlenol (S) 38 % 10-120 1 0722111 16:00 07125/11 22:31 367-12-4 2,4,6-Tribromophenol (S) 131 % 10-137 1 0722111 16:00 0725111 2131 118-79-6 624 Volatile Organ les Analytical Method: EPA 624 Acetone 0.073 mgiL 0.025 1 07/28/11 08:02 67-64-1 Acrolein NO mgiL 0.10 1 07/28/11 08:02 107-02-8 Acrylonitrile NO mg1L 0.10 1 07/28/11 08:02 107-13-1 Benzene NO mg/L 0.0050 1 0728111 08:02 71-13-2 Bromobenzene NO mg1L 0.0050 1 07/28/11 08:02 108-86-1 Bromochloromethene NO mg1L 0.0050 1 0728111 08:02 74-97-5 Bromodichto rom ethane NO mg1L 0.0050 1 0728111 08:02 75-27-4 Bromoform NO mg/L 0.0050 1 07/28/11 08:02 75-25-2 Bromomethane NO mg1L 0.010 1 07/28/11 08:02 74-83-9 2-Butanone (MEK) NO mgJL 0,0050 1 07/28/11 08:02 76.93-3 n-Butylbenzene NO mgJL 0.0050 1 0728/11 08:02 104-51-8 sec-Butylbenzene NO mgJL 0,0050 1 0728/11 08:02 135-98-8 lert-Butylbenzene NO mg/L 0,0050 1 0728111 09:02 98 06-6 Carbon disulfide NO mg/L 0.010 1 0728111 08:02 75-15-0 Carbon tetrachloride NO mg1L 0,0050 1 07/28/11 08:02 56-23-5 Chforobenzene ND mgiL 0.0050 1 07/28111 08:02 108-90-7 Chloroethane NO mg/L .0.010 1 07/28/11 08:02 75-00-3 2-Chloroethylvinyl ether NO mg/L 0.010 1 07/28/11 08:02 110-75.8 Chloroform NO mg/L 0.0050 1 07/28/11 08:02 67-66-3 Chloromethane NO mg/L 0.0050 1 0728/11 08:02 74-87-3 2-Chlorotoluene NO mg1L 0.0050 1 0728/11 08:02 95-49-8 4-Chlorotoluene NO mg1L 0.0050 1 07/28/11 08:02 106-43-4 Dibromochloromethane ND mg1L 0.0050 1 07/28/11 08:02 124-48-1 1,2-Dibromoethane (EDB) ND mg1L 0.0050 1 07/28/11 06:02 106-93-4 Dibromomethane NO mg1L 0.0050 1 0728111 08:02 74-95-3 1,2-Dichlorobenzene NO mg1L 0.0050 1 0728111 08:02 95-50-1 1,3-Dichlorobenzene NO mg1L 0.0050 1 0728111 08:02 541-73.1 1,4-Dichlorobenzene NO mg/L 0.0050 1 0728111 06:02 106-46-7 1,1-Dichloroethane NO mg1L 0.0050 1 0728/11 08:02 75-34-3 1,2-Dichloroethane NO mg1L 0-0050 1 0728/11 08:02 107-06-2 1.11-Dichtoroethene NO mgiL 0.0050 - 1 0728111 08:02 75-35-4 cis-1,2-Dichloroethene NO mgiL 0.0050 1 0728111 08:02 156-59-2 trans-1,2-Dichloroethene NO mgJL 0.0050 1 07/28/11 08:02 156-60-5 1,2-Dichlaropropane NO mgJL 0,0050 1 0728111 08:02 78-87-5 1,3-Dichloropropane NO mg1L 0,0050 1 07/28/11 08.02 142-28-9 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS This rep" shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 31 aceAnalytlr'caf e www.paoe(ans com Project: Stormwater 2011 Pace Project No.: 9298716 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Anatytkei Services, Inc. 9800 Kincey Ave. Suite 100 Huntersv0e, NC 28078 (704)875-9092 Sample: SOO #5 Parameters Lab ID: 9298716001 Results Units Collected: 07/19111 18:00 Report Limit DF Received: 07/20/11 15:30 Matrix: Water Prepared Analyzed CAS No. 4ual 624 Volatile Organics Analytical Method: EPA 624 2,2-Dichloropropane ND mg/L 0,0050 1 07/28/11 08:02 594-20-7 1,1-Dichloropropene ND mg1L 0.0050 1 07/28/11 08:02 563-58-6 cis-1,3-Dichloropropene ND mg& 0,0050 1 07128/11 08:02 10D61-01.5 trans-1,3-Dichloropropene NO mg/L 0.0050 1 07/2&11 08:02 10061-02-6 Ethylbenzene NO mg/L 0.0050 1 07/28/11 08:02 100-41-4 Hexachloro-1,3-butadiene NO mglL 0.0050 1 07/28/11 08:02 87-68-3 2-Hexanone NO mg/L 0,010 1 07/28/11 08:02 591-78-6 lodomethane NO mg/L 0.010 1 07/28/11 08:02 74-88.4 Isopropyl benzene (Cumene) NO mg/L 0,0050 1 07/28/11 08:02 98-82-8 p-isopropyltoluene ND mg/L 0,0050 1 D7128111 08:02 99-87.6 Methylene Chloride ND mg/L 0.0050 1 07/28/11 08:02 75-09-2 4-Methyl-2-pentanone (MIBK) NO mg/L 0.010 1 07/28/11 08:02 108-10-1 Methyl-tert-butyl ettw ND mg/L 0.0050 1 07/28/11 08:02 1634-04-4 Naphthalene NO mg/L 0.0050 1 07/28/11 08:02 91.20-3 n-Propylbenzene NO mg/L 0.0050 1 07/28/11 08:02 103-65-1 Styrene NO mg/L 0.0050 1 07/28/11 08:02 100-42-5 11,1,2-Tetrachloroothane NO mg/L 0.0050 1 07/28/11 08:02 630-20-6 1,1,42-Tetrachloroethane NO mg/L 0.0050 1 07/28/11 08:02 79-34-5 Tetrachloroethene NO mg/L 0.0050 1 07/28/11 08:02 127-18-4 Toluene NO mg/L 0.0050 1 07/28/11 08:02 108-88-3 1,2,3-Trichiorobenzene NO mg/L 0,0050 1 07/28/11 08:02 87-61-6 1,2,4-Trichilorobenzene ND mg/L 0.0050 1 07/28111 08-02 120-82-1 1,1,1-Trichloroethane NO mg/L 0.0050 1 07/28/11 08:02 71-55-6 1,1,2-Trichloroethane NO mg/L 0,0050 1 07/28/11 08:02 79-00-5 Trichloroethene NO mg/L 0.0050 1 07/28/11 08:02 79-01-6 Trichlorofluoromethane NO mg/L 0,010 1 07/28/11 08:02 75-69-4 1.2,3-Trichloropropane NO mg/L 0,0050 1 07/28/11 08:02 96-1" 1,1.2-Trichlorotrifluoroethane NO mg/L 0,0050 1 07/28/11 08:02 76-13-1 1,2,4-Trimethylbenzene ND mg/L 0.0050 1 07/28/11 08:02 95-63-6 1,3,5-Trimelhylbenzene ND mgtL 0.0050 1 07/28111 08:02 108-67-6 Vinyl acetate ND mg1L 0.010 1 07/2&11 08:02 108-054 Vinyl chloride NO mg/L 0.0050 1 07/28/11 08:02 75-01-4 m&p-Xylene NO mg/L 0.0050 1 07/28/11 08:02 179601.23-1 o-Xylene NO mg/L 0.0050 1 07/28/11 0&02 95-47-6 Dibromofluoromethane (S) 88 % 70-130 1 07/28/11 08:02 1868-53-7 4-Bromofluorobenzene (S) 97 % 70-130 1 07/28/11 08:02 460-DO-4 Toluene -dB (S) 95 % 70-130 1 07/28/11 08:02 2037-26-5 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 07/28/11 08:02 17060-07-0 420.4 Phenolics, Total Analytical Method: EPA 420-4 Phenol 0.026 mglL 0,010 1 07/29/11 12:01 108-95-2 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide 0.014 mg/L 0.0050 1 07/31/11 12:43 57-12-5 Date: 081031201104:12 PM REPORT OF LABORATORY ANALYSIS Page 7 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalytical' wrrwpacelaDsoan Project: Stormwater 2011 Pace Project No.: 9298716 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NG 27288 (336)623-892 f Pace Analytical Services, Inc. 2225 Riverside Dr, Asheville, NC 28804 (828)254.7 V6 ANALYTICAL RESULTS Pace Analytical Services. Inc. 9800 Kincey Ave. Suite 100 Huntersvole, NC 28078 (704)875-9092 Sample: SDO #7 Lab ID: 9298716002 Collected; 07/19/11 18:00 Received: 07/20/11 15:30 Matrix: Water Parameters Results units Report Llmit OF Prepared Analyzed CAS No. Qual 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 32.2 mg1L 6.2 1 07/25111 08:59 HEAR, Oil and Grease Analytical Method: EPA 1664A Oil and Grease ND mg1L 5.0 1 07125/11 08:34 608SF GCS Pesticides and PCBs Analytical Method: EPA 608 Aldrin NO ug/L 0,010 1 07/25/11 08:45 07/29111 23:42 309-00-2 alpha-BHC NO ug/L 0.090 1 07/25/11 08:45 07/29/11 23:42 319-84-6 beta-BHC NO ug/L 0.010 1 07/25/11 D8:45 07/29111 23:42 319-85-7 delta-BHC ND ug/L 0,010 1 07/25/11 08:45 07/29/11 23:42 319-86-8 gamma-BHC (Lindane) Nil ug/L 0,010 1 07/2511 f 08:45 07129/11 23:42 58-89-9 Chlordane (Technical) ND ug/L 0.52 1 07/25111 08:45 07129111 23:42 57-74-9 4,4`-DOD NO ug/L 0.010 1 07/25/11 08:45 07/29/11 23:42 72-54.8 4,4'-DOE NO ug/L 0.010 1 07/25/11 08:45 07/29111 23:42 72-55.9 4,4'-DDT ND ug/L 0.010 1 07125/11 08:45 07/29/11 23:42 50-29-3 Dieldrin ND ug/L 0,010 1 07/25/11 08:45 07/29/11 23:42 60-57.1 Endosulfan I NO ug/L 0.010 1 07/25/11 08:45 07129/11 23:42 959-98.8 Endosulfan 11 NO ug/L 0.010 1 07/25/11 08:45 07/29/11 23:42 33213-65-9 Endosulfan sulfate NO ug/L 0.010 1 07/25/11 08:45 07/29/11 23:42 1031-07.8 Endrin NO ug/L 0.010 1 07/25/11 08:46 07/29/11 23:42 72-20.8 Endrtn aldehyde NO ug/L 0.0062 1 07/25/11 08:45 07/29/11 23A2 7421-934 Heptachlor NO ug/L 0.010 1 07125111 08:45 07/29111 23:42 7"4-8 Heptachlor epoxide ND ug/L 0,010 1 07/25/11 08:45 07/29111 23:42 1024-57.3 PCB-1016 (Aroclor 1016) ND ug/L 0.52 1 07/25/11 08:45 07/29/11 23:42 12674-11-2 PCB-1221 (Aroclor 1221) NO ug/L 0.52 1 07/25/11 08:45 07/29/11 23:42 11104-28-2 PCB-1232 (Aroclor 1232) NO ug1L 0.52 1 07/25/11 08:45 07/29/11 23:42 11141-16-5 PCB-1242 (Aroclor 1242) NO uglL 0,52 1 07125/11 08:45 07/29/11 23:42 53469.21-9 PCB-1248 (Aroclor 1248) NO ug/L 0.52 1 07/25/11 08:45 07/29/11 23:42 12672-29-6 PCB-1254 (Arociar 1254) NO ug/L • 0,52 1 07125/11 08:45 07129111 23:42 11097.69-1 PCB-1260 (Aroclor 1260) NO ug/L 0.52 1 07125/11 08A5 07/29111 23:42 11096-82-5 Toxaphene NO ug/L 0.52 1 07125fll 08.45 07129f11 23:42 8001-35-2 Tetrachloro-m-xylene (S) 82 % 53-110 1 07/25/11 08:45 07/29/11 23:42 877-09-8 Decachlorobiphenyl (S) 77 % 61.121 1 07/25/11 08:45 07/29/11 23:42 2051.24-3 200.7 MET ICP Analytical Method: EPA 2007 Preparation Method: EPA 200.7 Lead NO mg/L 0.0050 1 07/25/11 16:00 07127/11 01:04 7439-92-1 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Acenaphthene NO mg/L 0.0050 1 07/22/11 16:00 07/25/11 23:54 83-32.9 Acenaphthylene NO mg/L 0,0050 1 07122/11 16:00 07/25/11 2154 208-96-8 Acetophenone NO mg/L 0.0050 1 07/22/11 16:00 07/25/11 23:54 98-86.2 Aniline NO mg1L 0.010 1 07/22/11 16:00 07/25/11 2154 62-53-3 Anthracene NO mg/L 0.0050 1 07/22/11 16:00 07/25/11 23:54' 120-12-7 Benzidine NO mg1L 0.050 1 07/22/111 16:00 07/25/11 23:54 92-87-5 Benzo(a)anthracene ND mg/L 0,0050 1 07/22/11 16:00 07/25/11 23:54 56-55-3 Benzo(a)pyrene NO mg/L 0.0050 1 07/22/11 16:0D 07/25/11 23:54 50-32.8 Date: 06103120110412 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytioal Services, Inc.. Page 8 of 31 aceAnalytical www.paaa;*soom Project: Stormwater 2011 Pace Project No.: 9298716 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)423.8921 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28075 (704)575-9092 Sample: SDO 07 Lab ID: 9298716002 Collected: 07/19/11 18:00 Received: 07/20/11 15:30 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 625 MSSV Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)ttuoranthene 4-Bromophenyiphenyl ether B u tyl b enz ylp hth a late 4-Chtoro-3-methylphenol bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloro€sopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 3,3'-Dichlorobe nzidine 2,4-Dichlorophenol Diethylphtha late 2,4-Dimethylphenol Dimethylphthalate Di- n-butylphthalate 4,6-Dinilro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate 1,2-Diphenylhydrazine bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1, 3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-ed)pyrene Isophorone Naphthalene Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitrosodimethylamine N-Nitroso-di-n-propylam€ne N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Date: 08/03/2011 04:12 PM Analytical Method: EPA 625 Preparation Method: EPA 625 NO mg1L 0,0050 1 07/22/11 16:00 07/25/11 2154 205-99-2 NO mglL 0,0050 1 07/22/11 16:00 07/25/11 23:54 191-24-2 NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 23:54 207-08-9 NO mg/L 0,0050 1 07/22/11 16:00 07/25/11 23:54 101-55-3 NO mg/L 0.0050 1 07/22/11 16:00 07/26/11 23:54 85.68-7 NO mglL 0,0050 1 07/22/11 16:00 07125111 23:54 59-50-7 NO mg/L 0.010 1 07122111 16:00 07/25/11 23:54 111-91-1 NO mg1L 0.0050 1 07/22111 16:00 07/25/11 23:54 111-44-4 NO mg1L 0.0050 1 07E22111 16:00 07125/11 23:54 108-60-1 NO mg/L 0.0050 1 07/22/11 16:00 07/25/11 23:54 9t-58-7 NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 23:54 95-57-8 NO mg/L O.D050 1 07/22/11 16:00 07/25/11 23:54 7005-72-3 NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 23:54 218-01-9 NO mg1L 0.0050 1 07/2211i 16:00 07/25/11 23:54 53-70-3 NO mg/L 0,0050 1 07/22/11 16:00 07/25/11 23:54 95-50-1 ND mglL 0,0050 1 07/22/11 16:00 07/25/11 23:54 541-73-1 ND mg/L 0,0050 1 07/22/11 16:00 07/26/11 23:54 10646-7 ND mg1L 0,025 1 07/22/11 16:00 07/25/11 23:54 91-94-1 ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 23:54 120-83-2 ND mg1L 0.0050 1 07/22/11 16:00 07/25/11 23:54 84-66-2 ND mg1L 0.010 1 07/22/11 16:00 07/25/11 23:54 105-67-9 ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 23:54 131-11-3 NO mg1L 0.0050 1 07122/11 16:00 07/25/11 23:54 84-74.2 NO mg/L O,020 1 07122/11 16:00 07/25/11 23:54 534-52-1 NO mg1L 0.050 1 07122111 16:00 07/25/11 23:54 51-28.5 ND mg1L 0.0050 1 07/22/11 16:00 07/25/11 23:54 121-14-2 ND mg/L 0.0050 1 07/22111 16:00 07/25/11 23:54 606.20-2 ND mg/L 0.0050 1 07/22/11 16:00 07125/11 23:54 117-84-0 ND mg/L 0.0050 1 07122/11 16:00 07i25/11 23:54 122-66-7 NO mg/L 0.0050 1 07/22/11 16:00 07125/11 23:54 117-81-7 NO mg/L 0.0050 1 07/22/11 16:00 07125/11 23:54 206-44-0 NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 23:54 86-73-7 NO mg1L 0.0050 1 07/22/11 16:00 07125/11 23:54 87-68-3 NO mg/L 0,0050 1 07/22/11 16:00 07/25/11 23:54 118-74-1 NO mg1L 0.010 1 07/22/11 16:00 07/25/11 23:54 77-47-4 NO mg1L 0.0050 1 07/22/11 16:00 07/25/11 2334 67-72-1 NO mg/L 0.0050 1 07/22/11 16:00 07/25/11 23:54 193-39-5 NO mg/L 0.010 1 07/22/11 16:00 07/25/11 23:54 78-59-1 NO mg/L 0.0050 1 07/22/11 16:00 07/25/11 2334 91-2D-3 ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 23:54 98-95-3 ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 23:54 88.75-5 ND mg/L 0-050 1 07/22/11 16:00 07126/11 23:54 100-02-7 NO mg/L 0.0050 1 07/22111 16:00 07/25/11 23:54 62-75-9 ND mg/L 0.0050 1 07A22111 16:00 07/25/11 23:54 621-64-7 ND mg1L 0-010 1 07{22111 16:00 07/25/11 23:64 W30-6 ND mg1L 0.025 1 07/22111 16:00 07/25/11 2154 87-86-5 ND mg/L 0.0050 1 07/22/11 16:00 07/25/11 23:54 85-01-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 31 aceanalytical' www.pao9faA wm Pace Anatydcel Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-B921 Pate Analytical Services, Irrc, 2225 Riverside Dr. Asheville, NC 28804 (828)254-7116 ANALYTICAL RESULTS Pace Arse"cal Services, Inc. 9800 Kincey Ave. Suite 100 Hvntersville, NC 28078 (71)4)875-9092 Project: Stormwater 2011 Pace Project No.: 9298716 Sample: SDO 97 Lab ID: 9298716002 Collected: 07/19/11 18:00 Received: 07/20/11 15:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 626 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Phenol NO mg1L 0.0050 1 071M11 16:00 07/25/11 23:54 108-95-2 Pyrene NO mg/L 0.0050 1 07/22/11 16:D0 07125/11 23:54 129-00-0 1,2,4-Trichlorobenzene ND mg/L 0.0050 1 07IM11 16:00 07IM11 23:54 120-82-1 2,4,6-Trichlorophenol NO rrtg/L 0.010 1 07/22/11 16:00 07125/11 23:54 88-06-2 Nitrobenzene-d5 (S) 59 °% 10-120 1 07/22/11 16:00 07125/11 23:54 4165-60-0 2-Fluorobiphenyl (S) 72 °% 15-120 1 07/22/11 16:00 07125/11 23:54 321-60-8 Terphenyl-d14 (S) 73 °% 11-131 1 07/22/11 16:00 07/25/11 23:54 1718-51-0 Phenol-d6 (S) 33 °% 10-120 1 07/22/11 16:00 07/25/11 23:54 13127.88-3 2-Fluorophenol (S) 37 °% 10-120 1 07/22/11 16:00 07/25/11 2154 367-12-4 2,4,6-Tribromophenol (S) - 127 •% 10-137 1 07/22/11 16:00 07/25/11 23:54 118-79-6 $24 Volatile Organics Analytical Method: EPA 624 Acetone 0.078 mg/L 0.025 1 07/28/11 08:20 67-64-1 Acrolein ND mg1L 0,10 1 07/28/11 08:20 107-02-8 Acrylonitrile NO mg/L 0.10 1 07/28/11 08:20 107-13-1 Benzene NO mg1L 0,0050 1 07/28/11 08:20 71-43-2 Bromobenzene NO mg/L 0,0050 1 07/28/11 08:20 108-86-1 Bromochloromethane ND mg1L 0.0050 1 07MIll 08:20 74-97-5 Bromodichloromethane NO mg1L 0.0050 1 07/28/11 08:20 75-27-4 Bromoform ND mg/L 0.0050 1 07/28/11 08:20 75-25-2 Bromomethane NO mg/L 0.010 1 07/28/11 08:20 74-83.9 2-Butanone (MEK) NO rnA 0.0050 1 07/28/11 08:20 78-93.3 n-Butylbenzene NO mg1L 0,0050 1 07/28/11 08:20 104-51-8 sec-Butylbenzene NO mg1L 0.0050 1 07/28/11 08:20 135-98.8 tert-Butylbenzene NO mg1L 0.0050 1 07/28/11 08:20 98-06-6 Carbon disulfide ND mg1L 0,010 1 07/28111 08:20 75-15-0 Carbon tetrachloride NO mg1L 0.0050 1 07/28/11 08:20 56-23-5 Chtorobenzene ND mg1L 0.0050 1 07/28/11 08:20 1OB-90-7 ChlDroethane ND mg/L 0,010 1 07/28/11 08:20 75-00.3 2-ChioroethyMnyl ether ND mg1L 0,010 1 07/28/11 08:20 110-75-8 Chloroform ND mg/L 0,0050 1 07/28/11 08:20 67-66-3 Chloromethane NO mg1L 0.0050 1 07/28111 08:20 74-87-3 2-CMorotoluene ND mg/L 0.0050 1 07/28111 08:20 95-49-8 4-Chlorotoluene NO mg1L 0,0050 1 07/28/11 08:20 106-43.4 Dibromochloromethane NO mg/L 0.0050 1 07/28/11 08:20 124-48.1 1,2-Dibromoethane (EDS) NO mg1L 0,00$0 1 07/28/11 08:20 106-93.4 Dibromomethane NO mg/L 010050 1 07/28/11 08:20 74-95-3 1,2-Dichlorobenzene NO mg1L 0,0050 1 07/28/11 08:20 95-50-1 1,3-Dichlorobenzene NO mg/L. 0,0050 1 07128111 98:20 541-73-1 IA-Dichlorobenzene NO mg/L 0.0050 1 07/28111 08:20 106-46-7 1,1-Dichloroethane NO mg1L 0.0050 1 07/28/11 08:20 75-34-3 1.2-Dichloroethane ND mg1L 0.0050 1 07/28/11 08:20 107-06-2 11-Dichloroethene ND mg1L 0.0050 1 .07/28111 08:20 75-35-4 cis-1,2-Dichloroethene ND mg/L 0.0050 1 07/28/11 08:20 156.59-2 trans-1.2-Dichloroethene NO mg1L 0,0050 1 07/28/11 08:20 156-60-5 1,2-Dichloropropane NO mg/L 0.0050 1 07/28/11 08:20 78-87-5 1,3-Dichloropropane NO mg1L 0.0050 1 07/28/11 08:20 142.28.9 Date: 0810312011 04:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 31 a Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. /j j acemalxicat 205 East Meadow Road - Suite A 2225 Riverside Dr_ 9800 Kincey Ave. Suite 100 WWW &oom Eden, NC 27288 Asheville, NC 2a804 Huntersville, NC 28078 (336)623-8921 (828)254.7175 (704)875-9092 ANALYTICAL RESULTS Project: Starmwater 2011 Paoe Project No.: 9298716 Sample: SDO 97 Lab ID: 9298716002 Collected: 07119/11 18:00 Received: 07/20/11 15:30 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 624 Volatile Organics Analytical Method: EPA 624 2,2-Dichloropropane NO mg1L 0.0050 1 07/26/11 08:20 594-20-7 1,1-Dichloropropene NO mg/L 0.0050 1 07128/11 08:20 563-58.6 cis-1,3-Dichloropropene ND mg/L 0.0050 1 07/28/11 08:20 10061-01-5 Iran-1,3-Dichloropropene ND mg/L 0.0050 1 07/28/11 08:20 10061-02.6 Ethylbenzene ND mg/L 0.0050 1 07/28/11 08:20 100-41-4 Hexachloro-1,3-butadiene NO mg1L 0.0050 1 07/28/11 06:20 87-68-3 2-Wexanone ND mg1L 0.010 1 07/28/11 08:20 591-78-6 lodomethane NO mg1L 0,010 1 07/28/11 08:20 74-88-4 Isopropylbenzene (Cumene) NO mg1L 0.0050 1 07/28/11 08:20 98-82-8 p-Isopropyltoluene NA mg/L 0,0050 1 07/28/11 08:20 99-87-6 Methylene Chloride NO mg/L 0,0050 1 07/28/11 08:20 75-09-2 4-Methyl-2-pentanone (MIRK) ND mg/L 0,010 1 07/28/11 08:20 108-10-1 Methyl -tent -butyl ether ND mg/L 0.0050 1 07128/11 08:20 1634.04-4 Naphthalene ND mg1L 0,0050 1 07/28/11 08:20 91-20-3 n-Propylbenzene NO mg1L OA050 1 07/28/11 08:20 103-65-1 Styrene NO mg/L 0,0050 1 07/28/11 08:20 100-42-5 1, 1, 1,2-Tetrachloroethane ND mg1L 0,0050 1 07/28/11 08:20 630-20-6 1,1,2,2-Tetrachloroethane NO mg1L 0.0050 1 07128/11 08:20 79-34-5 Tetrachloroethene NO mg1L 0.005D 1 07128/11 08:20 127-18-4 Toluene NO mg/L OW50 1 07/28/11 08:20 108.W3 1,2.3-Trichlorobenzene ND mg/L 0.0050 1 07/28/11 08:20 87.61.6 1,2,4-Trichlorobenzene ND mg/L 0.0050 1 07/28111 08:20 120-82.1 1,1,1-Trichloroethane NO mg1L 0.0050 1 07/28/11 08:20 71-55-6 1,1,2-Trichloroethane NO mglL 0.0050 1 07/28/11 08:20 79-00-5 Tichloroethene ND mg/L 0.0050 1 07/28/11 08:20 79-01-6 Trichlorofluoromethane NO mg/L 0.010 1 07/28/11 08:20 75-69-4 1,2.3-Trichloropropane NO mg/L 0,0050 1 07/28/11 08:20 96-18-4 1,1,2-Trichlorotdfluoroethane ND mg1L 0.0050 1 07/28/11 08:20 76-13-1 1,2.4-Trimethylbenzene NO mg/L 0,0050 1 07/28/11 08:20 95-63-6 1,3.5-Trimethylbenzene NO mg/L 0.0050 1 07128/11 08:20 108-67-8 Vinyl acetate NO mg/L 0.010 1 07/28111 08:20 108.05.4 Vinyl chloride NO mg/L 0,0050 1 07/28/11 08:20 75-01.4 m8p-Xylene NO mg1L 0,0060 1 07/28/11 08:20 179601-23-1 o-Xylene NO mg/L 0.0050 1 07/28/11 08:20 95-47-6 Dibromofluoromethane (S) 91 % 70-13D 1 07/28/11 08:20 1868.53-7 4-Bromofluorobenzene (S) 99 % 7D-130 1 07/28/11 08:20 460-00-4 Toluene-d8 (S) 97 % 70-130 1 07/28/11 08:20 2037.26-5 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 07/28/11 08:20 17DBO.07.0 420.4 Phenolics, Total Analytical Method: EPA 420.4 Phenol 0.023 mg1L 0.010 1 07/29/11 12:01 108.95-2 460OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide NO mg1L 0.0050 1 07/31/11 12:44 57-12-5 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 11 of 31 This report shalt not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. leAnalytical� www.Aace1136sOom Pace Analytical Services, Inc. 205 East Meadow Road - Suae A Eden. NC 27288 (336)623-8921 Project_ Stormwater 2011 Pace Project No.: 9298716 QC Batch: EDEW7460 QC Batch Method: SM 2540D Associated Lab Samples; 9298716001, 9298716002 METHOD BLANK: 637834 Associated Lab Samples: 9298716001, 9298716002 Parameter units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 637835 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 637836 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 637837 Parameter Units Total Suspended Solids mg1L Pace Analyflcat SeMces, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 07/2511106:57 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 250 100 80-120 9298642003 Dup Result Result RPD Qualifiers 3570 3570 0 9298772001 Dup Result Result RPD Qualifiers 1190 935 24 R1 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 12 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, tnc.. aceAnafyiical' www.pacalaw.wM Project: Stormwater 2011 Pace Project No.: 9298716 Pace Analyocat Services, Inc_ 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Anstytleal Services, Inc, 9800 Kinsey Ave_ Suite t no Huntersville, NC 28078 (704)875-9092 QC Batch: GCSV/10179 Analysis Method: EPA 1664A QC Batch Method: EPA 1664A Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 9298716001, 9298716002 METHOD BLANK: 637178 Matrix: Water Associated Lab Samples: 9298716001, 9298716002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 07/25/11 08:29 LABORATORY CONTROL SAMPLE: 637179 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease rrtrlL 40 32.3 81 78-114 MATRIX SPIKE SAMPLE: 637180 9298776002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L <5.0 40 36.3 90 78-114 Date: 0810W011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 13 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. (� aceAnalytical' werpacabhccom Project: Stormwater 2011 Paoe Project No.: 9298716 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Im- 2225 Riverside Dr. Ashevine, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: GCSW5237 QC Batch Method: EPA 608 Associated Lab Samples: 9298716001, 9298716002 Analysis Method: Analysis Description EPA608 608 GCS Pest PCB METHOD BLANK: 227176 Matrix: Water Associated Lab Samples: 9298716001, 9298716002 Blank Reporting Parameter Units Result Limit Analyzed 4,4'-DDD ugfL ND 0.010 07/29/11 21:47 4,4'-DDE ug/L ND 0.010 07/2911121:47 4,4'-DDT ug/L ND 0.010 07/2911121:47 Aldrin ug/L ND 0.010 07/2911121:47 alpha-BHC ug1L ND 0.010 07/29/11 21:47 beta-BHC ug1L ND 0.010 07/2911121:47 Chlordane (Technical? ug/L ND 0.50 07/29/11 21:47 delta-BHC ugfL ND 0.010 07/2911121:47 Dleldrin ug1L ND 0,010 07/29ft121:47 Endosulfan I ugfL ND 0.010 07/29/11 21:47 Endosulfan II ugfL ND 0.010 07/29/11 21:47 Endosulfan sulfate ug/L ND 0.010 07/29/11 21:47 Endrin uglL ND 0.010 07/2911121:47 Endrin aldehyde ug/L ND 0,0050 07/29/11 21:47 gamma-BHC (Lindane) ug/L ND 0.010 07/29/11 21:47 Heptachlof ug/L ND 0.010 07/2911121:47 Heptachlor epoxide ugli- ND 0.010 07/29111 21:47 PCB-1016 (Aroclor 1016) ug/L ND 0.50 07129111 21:47 PCB-1221 (Aroclor 1221) ug/L ND 0.50 07/29/11 21:47 PCB-1232 (Aroclor 1232) ug/L ND 0.50 07/29/11 21:47 PCB-1242 (Aroclor 1242) ug/L ND 0.50 07/29/11 21:47 PCB-1248 (Aroclor 1248) ug/L ND 0.50 07/29/11 21:47 PCB-1254 (Aroclor 1254) ug1L ND 0.50 07/29/11 21:47 PCB-1260 (Aroclor 1260) ug1L ND 0.50 07/29/11 21:47 Toxaphene ugfL ND 0.50 07129/1121:47 Decachlorabiphenyl (S) % 109 61-121 07129/11 21:47 Tetrachloro-m-xylene (S) % 93 53-110 07/29/11 21:47 LABORATORY CONTROL SAMPLE: 227177 Parameter 4,4'-DDD 4,4'-DDE 4A'-DDT Aldrin alpha-BHC beta-BHC delta-BHC Dieldrin Endosulfan I Endosulfan II Date: 08/03/2011 04:12 PM Spike LCS Units Conc. Result ug/L .5 0.54 ug/L .5 0.53 ugfL .5 0.64 ug/L .5 0.49 ugfL .5 0.46 ugfL .5 0,52 ug/L .5 0.58 u911- .5 0.57 ug/L .5 0,54 ug/L .5 0.58 Quaiifers LCS °% Rec °% Rec Limits 107 31-141 105 30-145 128 25-160 99 42-122 96 37-134 103 17-147 117 19-140 115 36-146 109 45-153 116 10-202 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc,. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hurttersvitre, NC 28078 (704)875-9092 Qualifiers Page 14 of 31 aceAnalytical' wwwpatelabsmm Project: Stormwater 2011 Pace Project No.: 9298716 Pace Analytical Services, Inc. 295 East Meadow Road - Suite A Eden, NC 27268 (336)623-8821 LABORATORY CONTROL SAMPLE: 227177 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 2BB04 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc, 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9D92 Parameter Units Spike Conc, LCS Result LCS % Rec % Rec Limits Qualifiers Endosulfan sulfate ug/L .5 0.57 113 26-144 Endrin ug/L .5 0.54 109 30-147 Endrin aldehyde ug[L .5 0.55 109 70-130 gamma-BHC (Lindane) ugfL .5 0.50 100 32.127 Heptachlor ug/L .5 0.54 108 34-111 Heptachlor epoxide UgIL 5 0.56 111 37-142 Decachtorobiphenyl (S) % 124 61-121 S1 Tetrachloro-m-xylene (S) % 104 53-110 LABORATORY CONTROL SAMPLE: 227184 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L 2.5 2.5 100 50-114 PCB-1260 (Aroclor 1260) ug/L 2.5 2.8 112 10-127 Decachlorobiphenyl (S) % 107 61-121 Tetrachloro-m-xylene (S) % 95 53-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 227760 20904028 Parameter Units Result MS Spike Conc, MSD Spike Conc. 227761 MS Result MSD Result MS %Rec MSD %Rec % Rec Limits RPD Oual 4,4'-DDD ug/L ND '55 53 0.49 DA7 89 90 31-141 4 4,4'-DDE ug/L ND 55 .53 0-47 OA6 85 87 30-145 3 4,4'-DDT ug/L NO '55 .53 0.66 0.65 120 123 25-160 2 Aldrin ugIL ND 55 '53 0.44 0-44 79 83 42-122 .7 alpha-BHC ugIL 0.18 '55 _53 0.74 0.74 101 107 37-134 .5 beta-BHC ug1L 0.43 .55 .53 0.94 0.93 92 95 17-147 1 delta-BHC ug/L 0.41 .55 .53 1.2 1.1 135 138 19-140 2 Dieldrin ug/L ND .55 .53 0.51 0.50 92 94 36-146 2 Endosulfan I ugIL ND .55 .53 0.49 0.48 88 91 45-153 2 Endosulfan tl ugIL ND .55 .53 0.51 0.50 92 94 10-202 2 Endosulfan sulfate ug/L ND .55 .53 0.56 0,54 100 102 26-144 3 Endrin ug/L ND 55 .53 0.51 0.50 92 95 30-147 2 Endrin aldehyde ug/L ND '55 53 0.47 0.45 84 85 70-130 4 gamma-BHC (Lindane) ug/L NO '55 .53 0.47 0,47 85 89 32-127 .8 Heptachlor ug/L ND .55 .53 0.58 0,56 105 107 34-111 3 Heptachlor epoxide ug/L ND .55 .53 0.54 0,54 97 102 37-142 .2 Decachlorobiphenyl (S) % 89 90 61.121 Tetrachtwo-m-xylene (S) % 83 87 53-110 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 15 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc„ ace Analj cale www.pawlRh1*= Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)623.8921 (828)254.7176 Project_ Stormwater 2011 Pace Project No.: 9298716 QC Batch: MPRPf8791 QC Batch Method: EPA 200.7 Associated Lab Samples: 9298716001, 9298716002 METHOD BLANK: 638043 Associated Lab Samples: 9298716001, 9298716002 Parameter Units Lead mgfL LABORATORY CONTROL SAMPLE: 638044 Parameter Units Lead mgfL MATRIX SPIKE SAMPLE: 638045 Parameter Units Lead mgfL MATRIX SPIKE SAMPLE: 638047 Parameter Units Lead mglL SAMPLE DUPLICATE: 638046 QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 2001 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.0050 07/2711100:30 Pace Analytical Services, Inc. 9800 KinceyAve_ Sum too Huntersvilte. NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers .5 0.47 94 85-115 9298863001 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers ND .5 0.40 81 70-130 9298876001 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers ND .5 0.43 87 70-130 9298593007 Dup Parameter Units Result Result RPD Qualifiers Lead mg1L ND ND SAMPLE DUPLICATE: 638048 Parameter Lead 9298876003 Dup Units Result Result mg1L ND ND RPD Qualifiers Date: 08/0312011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 16 of 31 This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. e Pace Analyticar Services, Inc. Pate AnaWall Services, Inc. ' L'i�/'U 1 ly t�Rl 205 East Meadow Road - Suite A 2225 Riverside Or, ate, `'JM PaW&C" Eden, NC 27288 Ashevitte, NC 28804 (336)623-8921 (828)254.7176 QUALITY CONTROL DATA Project: Stomtwater 2011 Pace Project No.: 9298716 QC Batch: 0EXT114303 Analysis Method: EPA 625 QC Batch Method: EPA 625 Analysis Description: 625 MSS Associated Lab Samples: 9298716001, 9298716002 METHOD BLANK: 637617 Associated Lab Samples: Parameter Matrix: Water 9298716001, 9298716002 Stank Reporting Units Result Limit Analyzed 1,2,4-Trichlorobenzene mg1L NO 0.0050 07125/1121:09 1.2-Dichlorobenzene mg1L ND 0.0050 0712511121:09 1,2-Diphenylhydrazine mg/L NO 0,0050 0712511121:09 1,3-Dichlorobenzene mg1L NO 0.0050 07125/1121:09 1,4-Dichlorobenzene mg1L NO 0,0050 07125/1121:09 2,4,6-Trichlorophenol mg1L NO 0,010 07125/1121:09 2,4-Dichlorophenol mg/L NO 0.0050 0712511121:09 2.4-Dimethylphenot mg1L NO 0.010 0712511121:09 2,4-Dini1rophenol mg/L ND 0.050 07125/1121:09 2,4-Dinitrotoluene mg/L ND 0.0050 07125/1121:09 2,6-Dinitrotoluene mg1L ND 0.0050 0712511121:09 2-Chloronaphthalene mg/L ND 0,0050 0712511121:09 2-Chlorophenol mg1L NO 0.0050 0712511121:09 2-Nitrophenol mg1L NO - 0.0050 07/25/11 21:09 3,3'-Dichlorobenzidine mg1L ND 0.025 07125/1121:09 4,6-Dinitro-2-methylphenol mg/L ND 0.020 0712511121:09 4-Brdnophenylphenyl ether mg/L NO 0.0050 07/25111 21:09 4-Chloro-3-methytphenol mg/L NO 0.0050 07125/1121:09 4-Chlarophenylphenyl ether mg1L NO 0,0050 07/25111 21:09 4-Nitrophenol mg/L NO 0.050 07125/1121:09 Acenaphthene mg/L ND 0.0050 07125/1121:09 Acenaphthylene mg1L ND 0,0050 0712511121:09 Acetophenone mg/L NO 0.0050 0712511121:09 Aniline mg1L ND 0,010 07125/1121:09 Anthracene mg1L NO 0.0050 0712511121:09 Benzidine mg/L ND 0,050 07125M121:09 Benzo(a)anthraeene mg/L NO 0.0050 07/2511121:09 Benzo(a)pyrene mg1L NO 0.0050 07/25/1121:09 Senzo(b)tluoranthene mg/L ND 0.0050 0712511121:09 Benzo(g,h,i)perylene mg/L ND 0.0050 0712511121:09 Berizo(k)ftuoranthene mglL ND 0.0050 07125/1121:09 bis(2-Chloroethoxy)methane mg1L ND 0.010 07125/1121:09 bis(2-Chloroethyl) ether mg1L NO 0.0050 07/25/11 21:09 bis(2-Chloroisopropyl) ether mg1L NO 0,0050 07125//11 21:09 bis(2-Ethy1hexyQphthalate mg1L ND 0.0050 07/2511121:09 Butytbenzylphthaiaw mg/L NO 0.0050 07/25/1121:09 Chrysene mg1L NO 0.0050 07/25/1121:09 Di-n-butylphthalate mg1L NO 0.0050 07125/1121:09 Di-n-octylphthalate mg1L NO 0,0050 0712511121:09 Dibenz(a,h)anthracene mg1L ND 0.0050 0712511121:09 Diethylphtha late mg11- NO 0,0050 0712511121:09 Dimethylphthalate mg/L ND 0.0050 0712511121:09 Fluoranthene mg1L ND 0.0050 07125/1121:09 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Pete Analytical Services, Inc. WWKin eyAve, Suite too Huntersville, NC 28078 (704)875-9092 Page 17 of 31 (�5a'neA*6cal' www.pateabtaxn Project: Slormwater 2011 Pace Project No.: 9298716 Pace Analytical Services, Inc. 205 East Meadow Read - Suite A Eden, NC 27288 (336)623-8921 Pace Anatocal Services, IrK. 2225 Riverside Dr. Asheville, NC 28804 (928)254.7176 QUALITY CONTROL DATA METHOD BLANK: 637617 Associated Lab Samples: Parameter 9298716001, 9298716002 Units Matrix: Water Blank Reporting Result Limit Analyzed Fluorene mg1L NO D.0050 07125/1121:09 Hexachloro-1,3-butadiene mg1L NO D.0050 07/25/1121:09 Hexachiombenzene mg/L ND 0.0050 0712511121:09 Hexachlorocyclopentadiene mg1L ND 0.010 07/25/1121:09 Hexachloroethane mg/L NO 0.0050 07125/1121:09 Indeno(1,2,3-cd)pyrene mg/L ND 0.0050 07/25/1121:09 Isophorone mg/L ND 0.010 07/2511121:09 N-Nitroso-di-n-propylamine mg/L ND 0.0050 0712511121:09 N-Nitrosodimethylamine mg/L ND 0.0050 0712511121:09 N-Nitrosodiphenylamine mg/L ND 0.010 07125/1121:09 Naphthalene mg1L ND 0.0050 0712511121:09 Nitrobenzene mg1L NO 0-0050 0712511121:09 Pentachlorophenol mg1L ND 0.025 071.25J1121:09 Phenanthrene mg/L NO 0.0050 07125/1121:09 Phenol mg/L ND 0,0050 07125/1121:09 Pyrene mg/L ND 0.0050 07125/1121:09 2,4,6-Tribromophenol (S) % 105 10-137 07/25/11 21:09 2-Fluorobiphenyl (S) % 59 15-120 07/25/11 21:09 2-Fluarophenol (S) % 40 10-120 07/25/11 21:09 Nitrobenzene-d5 (S) % 54 10-120 07/25/11 21:09 Phenol-d6 (S) % 29 10-120 07/25111 21:09 Terphenyl-04 (S) % 70 11-131 07125111 21:09 Qualifiers LABORATORY CONTROL SAMPLE: r Parameter 637618 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4-Trichlorobenzene mg/L .05 0.032 65 44-142 1,2-Dichtorobenzene mg/L -05 0.028 57 32-129 1,2-Diphenyihydrazine mg1L -05 0.030 59 25-150 1,3-Dichlorobenzene mg/L .05 0.027 53 1-172 1,4-Dichlorobenzene mg1L .05 0.028 55 20-124 2,4,6-Tdchlorophenol mg/L .05 0.042 83 37-144 2,4-Dichlorophenol mg/L .05 0.040 81 1.191 2,4-Dimethylphenol mg/L .05 0,016 32 32-119 2,4-Dinitrophenol mg/L .25 0.23 93 1-181 2,4-Dinitrotoluene mg/L .05 0.043 87 39-139 2,6-Dinitrololuene mg/L .05 0.041 81 50-158 2-Chloronaphthalene mg/L -05 0.034 69 W118 2-Chlorophenot mg/L .05 0.037 75 23-134 2-Nitrophenol mg1L .05 0.035 70 29-182 3,3'-Dichlorobenzidine mg1L A 0.075 75 1-262 4,6-Dinitro-2-methyiphenol mg/L :1 0.095 95 1-181 4-Bromophenylphenyl ether mg/L .05 0.044 88 53-127 4-Chloro-3-methylphenol mg1L .1 0.079 79 22-147 4-Chlorophenylphenyl ether mg/L .05 0.046 93 25-158 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc" 13800KinceyAve, Suitefa0 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 18 of 31 IC eftOiLil e WWWpaaalabs.ccm Project: Stonnwater 2011 Pace Project No.: 9298716 Pace Anatydca) Services, Inc. 205 East Meadow Road - Suite A Eden, NC 272a8 (336)623-8921 LABORATORY CONTROL SAMPLE: 637618 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 26804 (828)254.7176 QUALITY CONTROL DATA Paco Analytical Servlcas Inc- 9800 Kincey Ave- suite 100 Huntersvllle, NC 28078 (704)875-9092 Parameter Spike Units Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 4-Nitrophenol mg1L .25 0.12 47 1-132 Acenaphthene mglL .05 0.037 74 47-145 Acenaphthylene mglL .05 0.034 68 33-145 Acetophenone mg1L -1 0,037 37 25-150 Aniline mg1L .05 0.029 58 25-150 Anthracene mg1L .05 0.038 76 1-166 Benzidine mg1L .1 .005W 6 25-150 L2 Benzo(a)anthracene mg1L .05 0.036 72 33-143 Benzo(a)pyrene mg1L .05 0.036 71 17-163 Benzo(b)fluoranthene mg1L .05 0.037 75 24-159 Benzo(g,h,i)perylene mglL .05 0,039 77 1-219 Benzo(k)fluoranthene mg1L .05 0.037 75 11-162 bis(2-Chloreethoxy)methane mg/L .05 0.036 73 33-184 bis(2-Chloroethyl) ether rng1L .05 0.035 70 12-158 bis(2-Chloroisopropyl) ether mg1L .05 0.025 49 36-166 bts(2-Ethylhe)cyl)phthalate mg1L .05 0.027 54 8-158 Butyibenzyiphthatate mg1L .05 0.026 52 1-152 Chrysene mg1L .05 0,037 75 17-168 Di-n-butylphthalate mg1L .05 0,034 68 1-118 Di-n-ectylphthalate mg1L .05 0,024 49 4-146 Dibenz(a,h)anthracene mg1L .fly 0.040 79 1-227 Diethylpttthatate mg1L .05 0.040 79 1-114 Oimelhylphthalate mg1L .05 0.040 81 1-112 Fluoranthene mg1L .05 0.042 85 26-137 Fluerene mg/L .05 0.041 82 59-121 Hexachloro-1,3-butadiene mg1L .05 0.030 59 24-116 Hexachlorobenzene mg1L .05 0,048 95 1-152 Hexachlorocyclopentadiene mg1L .05 0.032 64 25-150 Hexachloroethane mglL .05 0,023 47 40-113 Indeno(1,2,3-cd)pyrene mg1L .05 0.038 75 1-171 Isophorone mg1L .05 0.037 73 21-196 N-Nitroso-di-n-propylamine mg/L .05 0.036 73 1-230 N-Nitrosodimethylamine mg1L .05 0.024 49 25-150 N-Nitrosodiphenylamine mg1L .05 0.036 72 25-150 Naphthalene mg1L .05 0,032 64 21-133 Nitrobenzene mglL .05 0.034 68 35-180 Penlachlorophenol mg1L .1 0,073 73 14-176 Phenanthrene mg1L .05 0.038 75 54-120 Phenol mglL .05 0,023 45 5-112 Pyrene mg/L .05 0.033 65 52-115 2,4,6-Tribromophenol (S) % 118 10-137 2-Fluorobiphenyt (S) % 73 15-120 2-Fluorophenol (S) % 50 10-120 Nitrobenzene-d5 (S) % 68 10-120 Phenol-d6 (S) % 38 10-120 Terphenyl-d14 (S) % 76 11-131 Date: 08103l2011 04.12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 19 of 31 13 c6Analyfical wnryac81MftLmm Project: Storrawater 2011 Pace Project No.: 9298716 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Seryless, Inc. 2225 Riverside or. Asheville, NC 28804 (828)254-7175 QUALITY CONTROL DATA Pace Analytical Services. Inc. SSW Klncey Ave. Suite 100 Huntersvine, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 637627 9298716001 Parameter Units Result MS Spike Cone. MSD Spike Conc. 637628 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Quat 1,2,4-Trichlorobenzene mg/L ND .1 .1 0.067 0.066 67 66 44-142 0 1,2-Dichlorobenzene mg/L ND .1 .1 0.052 0.054 52 54 32-129 4 1,2-Diphenylhydrazine mg/L NO _1 .1 0.052 0.055 52 55 25-150 5 1,3-Dichlorobenzene mg/L NO .1 .1 0.050 0.050 50 50 1-172 1 1,4-Dichlorobenzene mglL ND .1 .1 0.051 0.052 51 52 20-124 2 2,4,6-Trichlorophenol mg1L ND .1 .1 0.086 0.085 86 85 37-144 1 2,4-Dichlorophenol mg1L ND .1 .1 0.082 0.086 82 86 1-191 5 2,4-Dimethylphenol mg1L ND .1 .1 0.069 0.071 69 71 32-119 3 2,4-Dinitrophenol mg)L ND .5 .5 0.44 0.44 88 88 1-181 1 2,4-Dinitrotoluene mg)L - ND .1 A 0.082 0.084 82 84 39-139 3 2,6-Dinitrotoluene mg1L ND .1 .1 0.078 0.079 78 79 50-158 1 2-Chloronaphthalene mglL NO _1 A 0.071 0,068 71 68 60-118 5 2-Chlorophenol rnWL NO _1 A 0.066 0.071 66 71 23-134 7 2-Nitrophenoi mg1L NO .1 A 0.069 0.070 69 70 29-182 2 3,3'-Dichlorobenzidine mg)L ND .2 .2 ND NO 0 1 1-262 MO,M1,R1 4,6-Dinitro-2-methylphenol mg1L ND .2 .2 0.17 0.18 84 89 1-181 6 4-Bromophenylphenyl ether mg1L ND .1 .1 0.084 0.082 84 82 53-127 2 4-Chloro-3-methylphenol mg1L ND .2 .2 0.16 0.17 79 87 22-147 9 4-Chlorophenylphenyl ether mglt NO .1 .1 0.090 0.091 90 91 25-158 1 4-Nitrophenol mg1L ND .5 .5 0.29 0.31 58 62 1-132 7 Acenaphthene mg1L NO .1 .1 0.074 0.072 74 72 47-145 3 Acenaphthylene m9it- NO _1 A 0.067 0.057 67 67 33-145 0 Acetophenone mg/L NO .2 .2 0.067 0.073 33 36 25-150 8 Aniline mg/L ND A .1 NO 0.037 0 37 25-150 M0,M1,R1 Anthracene mg1L ND .1 .1 0.071 0,071 71 71 1-166 1 Benzidine mglL ND .2 .2 ND ND 0 0 25-150 M0 Senzo(a)anthracene mg1L ND .1 .1 0.067 0,068 67 68 33-143 2 Benzo(a)pyrene mg1L NO .1 .1 0.064 0.065 64 65 17-163 2 Benzo(b)fluoranthene mg1L NO .1 .1 0.070 0.067 70 67 24-159 3 Benzo(g,h,i)peryiene mg/L NO .1 .1 0.071 0.071 71 71 1-219 0 Benzo(k)fluoranthene RV& ND A .1 0.070 0.067 70 67 11-162 4 bis(2-Chloroelhoxy)methane mg1L ND A A 0.069 0.071 69 71 33-1 &4 2 bis(2-Chloroethyl) ether mg1L ND .1 A 0.064 0.065 64 65 12-158 3 bis(2-Chloroisopropyl) ether mg1L ND .1 .1 0.040 0.042 40 42 36-166 5 bis(2-Ethyihexyl)phthalate mg1L ND .1 .1 0.052 0.052 52 52 8-158 1 Butylbenzylphthalate mg1L NO .1 .1 0.052 0.052 52 52 1-152 1 Chrysene mg1L NO .1 .1 0.070 0.070 70 70 17-168 1 Di-n-butylphthalate mg1L ND .1 .1 0.065 0.063 65 63 1-118 3 Di-n-oUylphthalate mglt- NO _1 _1 0.050 0.049 50 49 4-146 2 Oibenz(a.h)anthracene mg1L NO .1 .1 0.073 0.074 73 74 1-227 2 Diethylphthalate mg1L ND .1 .1 0,075 0.077 75 77 1-114 2 Dlmethylphthalate mg1L ND ,1 ,1 0,076 0.077 76 77 1-112 1 Fluoranthene mg1L ND ,1 .1 0.079 0.078 79 78 26-137 1 Fluorene mg1L NO .1 .1 OA79 0.080 79 ' � 80 59-121 1 Hexachloro-1,3-butadiene mg1L NO .1 .1 0.065 0.063 65 63 24-116 2 Hexachlorobenzene mg1L ND .1 .1 0.086 0.085 86 85 1-152 1 Hexachlorocyclopeniadiene mg1L ND .1 .1 0.072 0.066 72 66 25-150 8 Date: 08103l2011 04.12 PM REPORT OF LABORATORY ANALYSIS Page 20 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ceanalyncal wwwpauWtrscarn Project: Stolmwater 2011 Pace Project No.: 9298716 Pace Anaiytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 QUALITY CONTROL DATA Pace Analytleal Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 637627 637528 MS MSD 9298716001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result %Rec %Rec Limits RPD Qual Hexachlorcethane mg1L NO A .1 0.045 0.046 45 46 40-113 1 Indeno(1,2,3-cd)pyrene mglL NO A A 0.070 0.072 70 72 1-171 2 Isophorone mg1L ND .1 A 0.069 0-071 69 71 21-196 3 N-Nitroso-di-n-propylamine mg1L NO -1 .1 0.065 0.072 65 72 1-230 10 N-Nitrosadimethylamine mglL ND .1 A 0.046 0.047 46, 47 25-150 1 N-Nitrosodiphenylamine mg/L NO .1 ,1 0.070 0.070 70 70 25-150 0 Naphthalene mg1L ND .1 .1 0,064 0.064 64 64 21-133 0 Nitrobenzene mg1L NO .1 .1 0.062 0.061 62 61 35-180 2 Pentachlorophenol mg1L NO .2 .2 0.16 0.17 80 86 14-176 6 Phenanlhrene mg1L NO 1 .1 0.071 0.069 71 69 54-120 2 Phenol mg1L NO A .1 0.050 0.057 50 57 5-112 14 Pyrene mg1L NO .1 .1 0,064 0.062 64 62 52-115 2 2,4,6-Trtbromophenot (S) % 118 121 10-137 2-Fluorobiphenyl (S) % 74 70 15-120 2-Fluorophenol (S) % 49 50 10-120 Nitrobenzene-d5 (S) % 60 61 10-120 Phenol-d6 (S) % 50 54 10-120 Terphenyl-d14 (S) % 75 74 11-131 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 21 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. a0klalytieal e www.pacela6AGLm Project: Stotmwater 2011 Pace Project No.: 9298716 QC Batch: MSV/16116 PaceAnatytical Services, Inc. PaceAnsiyttcat Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QC Batch Method: EPA 624 Associated Lab Samples: 9298716001, 9298716002 QUALITY CONTROL DATA Analysis Method: EPA 624 Analysis Description: 624 MSV METHOD BLANK: 638543 Matrix: Water Associated Lab Samples: 9298716001, 9298716002 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1,2-Tetrachloroethane mg/L NO 0.0050 07128/1105:33 1,1,1-Tdchloroethane mg/L NO 0.0050 0712811105:33 1,1,2,2-Tetrachloroethane mg/L ND 0,0050 07128/1105:33 1,1,2-Tdchloroethane mg1L ND 0.0050 07128/1105:33 1,1,2-Trichlorotrifluoroethane mg1L NO 0,0050 0712811105:33 1,1-Dichloroethane mg/L NO 0,0050 0712811105:33 IIJ-Dichloroethene mg/L NO 0,0050 07/2811105:33 1,1-Dichloropropene mg1L NO 0.0050 07A2811105:33 1,2,3-Trichtorobenzene mg1L ND 0.0050 07/2811105:33 1,2,3-Trichloropropane mg1L ND 0.0050 07/28/11 05:33 1,2,4-Trichlorobenzene mg1L ND 0,0050 0712811105:33 1,2,4-Trimethylbenzene mg1L NO 0,0050 07128/1105:33 1,2-Dibromoethane (EDB) mg/L NO 0,0050 07/28/11 05:33 1,2-Dichlorobenzene mg1L ND 0.0050 07/28/11 05:33 1,2-Dichloroethane mg1L ND 0,0050 07/28/11 05:33 1,2-Oirhioropropane mg1L ND 0.0050 0712811105:33 1,3,5-Trimethylbenzene mg/L ND 0,0050 0712811105:33 1,3•Dichlorobenzene mgiL ND 0.0050 07128/1105:33 1,3-Dichloropropane mglL ND 0.0050 07/2811105:33 1,4-Dichlorobenzene mg1L ND 0.0D50 07/28/11 05:33 2,2-Dichloropropane mg/L ND 0,0050 07/28/1105:33 2-Butanone (MEK) mg1L ND 0.0050 07/28/11 05:33 2-Chloroethylvinyl ether mg1L NO 0.010 07/28/11 05:33 2-Chlorotoluene mg1L NO 0,0050 07/28/11 05:33 2-Hexanone rng1L ND 0.010 0712811105:33 4-Chiorotoiuene mg1L ND 0.0050 0712811105:33 4-Methyl-2-pentanone (MIRK) mg/L ND 0.010 07128111 05:33 Acetone mg1L ND 0.025 07128/1105:33 Acrolein mg1L ND 0.10 07/28/11 05:33 Acrylonitrile mg1L ND 0.10 07/2811105:33 Benzene mg1L ND 0.0050 07128/1105:33 Bromobenzene mg/L NO 0.0050 07/28/11 05:33 Bromochloromethane mg1L NO 0.0050 0712811105:33 Sromodirhloromethane rrg/L ND 0.005D 07128/1105:33 Bromolorm mgAL NO 0.0050 07128/1105:33 Bromomethane mgAL ND 0.010 07128/1105:33 Carbon disulfide mg/L ND 0.010 07/28/11 05:33 Carbon tetrachloride mg/L ND 0.0050 07/28/11 05:33 Chlorobenzene mg/L ND 0.0050 07/28/11 05:33 Chloroethane mg/L ND 0.010 07/28/11 05:33 Chloroform mg/L ND 0,0050 0712811105:33 Chloromethane mg/L ND 0.0050 07128/1105:33 cis-1,2-Dichloroethene mg/L ND 0.0050 07128/1105:33 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Pau Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 (704)875-9092 Page 22 of 31 w wwpwdabsowe Project: Stonnwater 2011 Pace Project No.: 9298716 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Servltss, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA METHOD BLANK: 638543 Associated Lab Samples: Parameter 9298716001, 9298716002 Units Matrix: Water Blank Reporting Result Limit Analyzed cis-1,3-Dichloropropene mg/L ND 0.0050 07128/1105:33 Dibromochloromethane mg/L ND 0.0050 0712811105:33 Dibromomethane mg/L NO 0,0050 0712811105:33 Ethyibenzene mg/L ND 0,0050 07128/1105:33 Hexachloro-1,3-butadiene mg/L ND 0,0050 07/2811105:33 lodomethane mg/L ND 0.010 07/2811105:33 Isopropylbenzene (Cumene) mg/L ND 0.0050 07/28/11 05:33 m&p-Xylene mg/L ND 0.0050 07/28/1105:33 Methyl-tert-butyl ether mg/L NO 0.0050 07/28/11 05:33 Methylene Chloride mg/L ND 0.0050 07/28/11 05:33 n-Butylbenzene mg1L NO 0.0050 07/2811105:33 n-Propylbenzerte mg/L NO 0.0050 07/28/1105:33 Naphthalene M91L NO 0.0050 0712811105:33 o-Xylene mg/L ND 0.0050 07128/i105:33 p-Isopropyltotuene mg/L ND 0.0050 07/2811105:33 sec-Butylbenzene mg/L ND 0.0050 07/2811105:33 Styrene mg/L NO 0,0050 0712811105:33 tert-Butylbenzene mg/L ND 0,0050 07128/1105:33 Tetrachloroethene mg/L ND 0.0050 07/2811105:33 Toluene mgiL NO 0,0050 07/28/1105:33 trans-11,2-Dichloroethene mgiL ND 0.0050 07128/1105:33 trans-1,3 Dirhloropropene mg/L NO 0.0050 07128111 05i33 Trichtaroethene m91L ND 0.0050 0712811105:33 Tdchlorofluoromethane mg/L ND 0.010 07/2811105:33 Vinyl acetate mg/L ND 0.010 07/28/11 05:33 Vinyl chloride mg/L ND 0.0050 07/28/11 05:33 1,2-Dichloroethane-d4 (S) % 97 70-130 07/28/11 05:33 4-Bromofluorobenzene (S) % 100 70-130 07/28/11 05:33 Dibromofluoromethane (S) % 93 70-130 07/28/11 05:33 Toluene-8 (S) % 97 70-130 07128111 05:33 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 638544 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1.1,2-Tetrachloroethane mg/L .02 0.018 91 70.130 1,1,1-Trichloroethans mg/L 02 0,017 86 52-162 1,1,2,2-Tetrachloroelhane mg/L .02 0.017 84 46-157 1,1,2-Trichioroethane mgiL .02 0,017 87 52-150 1,1,2-Trichlorotrifluoroethane mg/L .02 0.016 80 70-130 1.1-Dichloroethane mg/L .02 0.017 86 59-155 1,t-Dichloroethene mg/L .02 0.016 82 1-234 1,1-Dichloropropene mg/L .02 0.016 78 70-130 1,2,3-Trichlorobenzene mg/L .02 0.015 73 70-130 1,2,3-Trichloropropane mg/L .02 0.017 87 70-130 1,2,4-Trichlorobenzene mg/L .02 0.016 77 70-130 Pace Analytical services, Inc- 9M KinCey Ave, Suite100 Huntersville, NC 28078 (704)875-9092 Qualifiers Rate: 08103/2011 04.12 PM REPORT OF LABORATORY ANALYSIS Page 23 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ceAnalytical e WWWP&M1M&WM Project: Stormwater 2011 Pace Project No.: 9298716 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc- 2225 Riverside Of. Asheville. NC 28804 (828)254.7176 QUALITY CONTROL DATA Pace Analytical Sarvtces, Inc_ 9800 Kincey Ave. Suite 1OD Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: Parameter 6385" Units Spike Cone. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2,4-Tdmethylbenzene mg1L .02 0.017 86 70-130 1,2-Dibromoethane (EDB) mglL .02 0.017 85 70-130 1,2-Dichlorobenzene mglL .02 0.017 87 18-190 1,2-Dichloroethane mglL .02 0.018 88 49-155 1,2-Dichloropropane mg1L .02 0.017 84 1.210 1,3,5-Trimethylbenzene mg1L .02 0,017 87 70-130 1,3-Dichlorobenzene mg1L .02 0.017 85 59-156 1,3-Dichloropropane mg1L .02 0.017 83 70-130 1,4-Dichlorobenzene mg1L 02 0.017 87 18-190 2,2-Dichloropropane mg1L .02 0.013 67 70-130 L0 2-Butanone (MEK) mg1L .04 0.033 82 50-127 2-Chloroethylvinyl ether mg1L .04 0.025 62 1-305 2-Chlorotoluene mg/L .02 0.017 86 70-130 2-Hexanone mg1L .D4 0.030 74 70-130 4-Chlorotoluene mg1L .02 0.018 88 70-130 4-Methyl-2-pentanone (MIRK) mg1L 04 0.032 80 70-130 Acetone mg1L .04 0,037 93 70-130 Acrolein mg1L .1 .083J 83 15-152 Acrylonitrile mg1L .1 .0851 85 75-132 Benzene mglL 02 D.016 77 37-151 Bromobenzene mg/L .02 D.017 85 7D-130 Bromochioromethane mglL .02 0,017 87 70-130 Bromodichloromethane mglL .02 0.018 69 35-155 Bromoform mg1L .02 0.018 90 45-169 Bromomethane mg1L 02 0.021 106 1-242 Carbon disulfide mg1L .02 0.034 172 70-130 L3 Carbon tetrachloride mg1L 02 0.017 85 70-140 Chlorobenzene mg1L .02 0,018 88 37-160 Chloroethane mglL .02 0.020 98 14-230 Chloroform mglL .02 0.018 90 51.138 Chioromethane M91L .02 0.018 91 1-273 cis-1,2-Dichloroethene mg1L .02 0.017 84 68-146 cis-1,3-Dichloropropene mg1L .02 0.016 79 1-227 Dibromochloromethane mg/L .02 0.018 89 53-149 Dibromomethane mg1L .02 0.018 91 70-130 Ethylbenzene mglL 02 0.017 85 37-162 Hexachloro-1,3-butadiene mg1L .02 0.014 71 70-130 lodomethane mglL .04 0,036 91 70-130 Isopropylbenzene (Cumene) mg/L .02 0.017 83 70-130 m&p-Xytene mg1L -04 0,034 86 70-130 Methyl -tent -butyl ether mg1L .02 0.022 109 70-130 Methylene Chloride mg1L .02 0.017 85 1-221 n-Butylbenzene mg1L .02 0.015 76 70-130 n-Propylbenzene mg1L .02 0.017 86 70-130 Naphthalene mglL .02 0.017 84 70-130 o-Xylene mg1L .02 0.018 88 70-130 p-Isopropyltoluene mg1L .02 0.017 83 70-130 sec-Butylbenzene mg1L .02 0.017 84 70-130 Date: 0810312011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 24 at 31 This report shall not be reproduced, except in full, without the written Consent of Pace Analytical Services, Inc.. cMnalytical e WWW4%ac0L1b&o0m Pace Analytical SorAces, Inc. 206 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: Stormwater 2011 Pace Project No-_ 9298716 LABORATORY CONTROL SAMPLE: 638544 Pace Analocai Services, Inc. 2225 Riverside Or. Ashevitle, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 980D Kincey Ave. Suite tfb Huntersvllle. NC 28078 (704)875-9092 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Styrene mg/L .02 0.018 89 70-130 ten-Butylbenzene mg1L .02 0.017 86 70-130 Tetrachloroethene mg1L .02 0,017 84 64-148 Toluene mgiL .02 0.017 83 47-150 trans-1 ,2-Dichbraethene mg/L 02 0.022 108 54-156 trans- 1,3-Dichloropropene mg/L .02 0.016 79 17.183 Trichloroethene mg/L .02 0.017 86 71-157 Trichlorofluoromethane mg/L .02 0.018 90 17-181 Vinyl acetate mg1L .04 0.038 95 70-130 Vinyl chloride mg1L .02 0,020 99 1-251 1,2-Dichloroethane-d4 (S) % 95 70-130 4-Bromofluorobenzene (S) % 100 70-130 Oibromofluorornothane (S) % 99 70-130 Toluene-d8 (S) D/S 100 70-130 MATRIX SPIKE SAMPLE: Parameter 638546 Units 9298590002 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane mg/L ND .02 0.020 102 70-130 1.1.1-Trichloroethene mg1L ND .02 0.017 87 46-171 1,1,2.2-Tetrachloroethane mg/L ND .02 0-021 107 73-159 1,1,2-Trichioroethane mg1L ND .02 0-020 99 64-152 11,2-Trichlorotrifluoroethane mg/L ND .02 0.016 79 59-168 1,1-Dichloroethane mg1L ND .02 0.017 85 43-172 1,1-Dichloroethene mg1L ND .02 0.017 85 48-189 1,1-Dichloropropene mg1L ND .02 0.015 76 70-130 1,2,3-Trichlorobenzene mg1L ND .02 0.014 71 70-130 1,2,3-Trichloropropane mg1L ND •02 0.022 112 70-130 12,4-Trichlorobenzene mg/L ND .02 0-015 75 70-130 1,2,4-Trimethytbenzene mg1L ND .02 0-018 89 70-130 1,2-Dibromeethane (EDB) mg/L ND .02 0.021 103 70.130 1,2-Dichlorobenzene mg/L ND .02 0.019 90 54-154 1,2-0ichloroethane mg/L ND .02 0.019 96 42-171 1,2-Dichloropropane mg/L ND .02 0.018 88 55-157 1,3,5-Trimethylbenzene mg1L ND .02 0.018 91 70-130 1,3-Dichlorobenzene mg1L ND .02 0.019 93 57-148 1,3-Dichloropropane mg/L ND '02 0.020 101 70-130 1,4-Dichlorobenzene mg/L ND .02 0.019 95 58-149 2,2-Dichloropropane mg1L ND .02 0.0090 45 70-130 W 2-Butanone (MEK) mg1L ND .04 0.035 89 70-130 2-Chloroethylvinyl ether mg/L ND .04 ND 0 70-130 P5 2-Chlorotoluene mg1L ND 02 0.019 93 70-130 2-Hexanone mg1L ND .04 0.040 99 70-130 4-Chlorotoluene mg1L ND .02 0.019 97 70-130 4-Methyl-2-pentanone (MIBK) mg1L ND .04 0.039 97 70-130 Acetone mg1L ND .04 0.060 109 70-130 Acrolein mg1L ND .1 .0531 53 7D-130 MO Date: 08103/2011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 25 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc Pace Analytical Services, Inc. Pecs Analytical Services, Inc. Pace Analytical Services, Inc. t Ma�`� f al 'J ` 205 East Meadow Road - Suite A 2225 Riverside Or, 9800 Kincey Ave. Suite 1o0 � ¢com Eden, NC 27288 Asheville, NC 28804 Kuntetsville, NC 28078 (336)623-8921 (828)254.7176 (704)875-9092 QUALITY CONTROL DATA Project: Stormwater 2011 Pace Project No.: 9298716 MATRIX SPIKE SAMPLE: 638546 9298590002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Acrylonildle mglL ND .1 .094J 94 70-130 Benzene mg1L ND .02 0.017 83 54-163 Bromobenzene mgfL ND .02 0.019 97 70-130 Bromochloromethane mgfL ND .02 0.017 86 70-130 Bromodichloromethane mgfL ND .02 0.020 99 56-162 Bromoform mgfL ND .02 0.022 109 53-151 Bromomethane mgfL ND .02 0.021 106 10-200 Carbon disutfide mgfL ND .02 0.035 175 70-130 MO Carbon tetrachloride mgfL ND .02 0.019 96 41-175 Chloroberizene mg1L ND .02 0.020 99 67-152 Chloroethane mgfL ND .02 0.020 100 23-200 Chloroform mgfL ND 02 0,019 94 51-166 Chloromethane mg1L ND .02 3.019 95 40-175 cis-1,2-DichIGroethene mg1L ND .02 0.017 84 45-174 tas-1,3-Dichloropropene mgfL ND .02 0.014 72 38-146 Dibromochloromethane mgfL ND .02 0.021 103 65-144 Dibromomethane mgfL ND .02 0.021 104 70-130 Ethylbenzene mgfL ND .02 0.018 91 57-152 Hexachloro-1,3-butadiene mgfL ND .02 0.010 51 70-130 MO lodomethane mgfL ND ,04 0.036 89 70-130 Isopropyl benzene (Cumene) mgfL ND .02 0.018 89 70-130 m8p-Xylene mgfL ND .04 0.037 93 70-130 Methyl-terl-butyl ether mgfL ND .02 0.023 115 70-130 Methylene Chloride mgfL ND .02 0.019 90 40-167 n-Butylbenzene mgfL ND 02 0.015 74 70-130 n-Propytbenzene mgfL ND .02 0.018 90 70-130 Naphthalene mg1L ND .02 0.018 92 70-130 o-Xylene mgfL ND .02 0.019 94 70-130 p4sopropyltoluene mgfL ND .02 0.016 82 70-130 sec -Butyl benzene mgfL N❑ 02 0.016 82 70-130 Styrene mgfL ND .02 0.018 90 70-130 tert-Butylbenzene mgfL ND .02 0.018 88 70.130 Tetrachloreethene mgfL ND .02 0.018 91 59.155 Toluene mg1L ND .02 0.017 84 47-162 trans-1,2-Dichloroethene mgfL ND .02 0.022 110 47-178 trans-1,3-Dichloropropene mgfL ND .02 0.016 80 39-146 Trichloroethene mg1L ND .02 0.019 93 60-153 Trichlorofluoromethane mg/L ND 02 0.019 97 42-199 Vinyl acetate mgfL ND 04 0.025 63 70-130 MO Vinyl chloride mgfL ND .02 0.020 100 46-176 1,2-Dichloroelhane-4(S) % 97 70-130 4-Bromofluorobenzene (S) % 101 70-130 Oibromofluoromethane (S) % 89 70-130 Toluene-d8 (S) % 95 70-130 Date: 08/0312011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 26 of 31 This report shall not be reproduced, except in full, without the whiten consent of Pace Analytical Services, Inc.. leanalytica!' www.pacelebxcWn Project: Stormwaler 201f Pace Project No.: 9298716 SAMPLE DUPLICATE: 639703 Parameter 1,1,1,2-Tetrachloroetha ne 1,1,1-Trichloroethane 1,12,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1, 2-Trichlorotrilluoroethane 1,1-Dichloroethane 1,1-Dichloroethene 1, 1 -Dichloropropene 1,2,3-Trich lorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2.4-Tiimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroelhane 1,2-Dichloropropane 1,3, 5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane II A-Dichlorobenzene 22-Dichloropropane 2-Butanone (MEK) 2-Chloroethytvinyl ether 2-Chloratoluene 2-Hexanone 4•Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane ds-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochlorometha ne Dibromomethane Ethylbenzene Hexachloro-1,3-butadiene Date: 08/03/L011 04:12 PM Pace AnaWal Services, Inc. Pace Anaiyilcal Services, Inc. 205 East Meadow Road - Suits A 2225 Riverside Dr, Eden, NC 27288 Asheville, NG 26804 (336)623-8921 (828)254.7176 QUALITY CONTROL DATA 9298716002 Units Result mglL ND mg/L ND mg1L ND mg/L ND mg/L ND mg/L NO mg1L NO mg1L NO mg/L NO mg/L NO mg/L . ND mg/L ND mg/L ND mg1L NO mg1L NO mg1L NO mg/L NO mg1L NO mg1L NO mg/L NO mg/L ND mg1L NO mg/t_ ND mg1L NO mg1L NO mg/L NO mg1L NO mg1L 0.078 mg1L NO mg/L NO mg1L NO mg[L ND mgiL NO mg/L NO mg/L NO mg1L NO mg1L NO mg/L NO mg1L NO mg1L NO mg/L NO mg/L NO, mg/L NO mg/L NO mg/L NO mg/L NO mg/L NO mg/L NO Dup Result NO N❑ ND ND ND NO ND NO NO NO NO NO NO ND NO ND ND ND NO NO NO NO ND NO NO NO ND 0.053 NO NO NO NO NO ND ND NO NO NO NO ND ND NO NO NO ND ND NO NO RPD Qualifiers REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc- 37 C9,R1 PaceAnalytical Services, Inc. 98W Kincey Ave. Suite 100 HuntersviIle, NC 28078 (704)875-9092 Page 27 of 31 ceAnalWica!` eww.pacetahsaom Project: Stormwater 2011 Pace Project No_: 9298716 Pace Anatytical Services, Inc_ 205 East Meadow Road - $uite A Eden, NC 272BB (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Or. Asheville, NC 28804 (828)2544176 QUALITY CONTROL DATA SAMPLE DUPLICATE: 639703 Parameter Units 9298716002 Result Dup Result RPD Qualifiers lodomethane mg/L ND NO Isopropylbenzene (Cumene) mg1L ND NO m&p-Xylene mg1L ND NO Methyl -tent -butyl ether mglL ND ND Methylene Chloride mg/L ND ND n•Butylbenzene mg/L NO ND n•Propylbenzene mg/L ND NO Naphthalene mg/L ND ND o-Xylene mg/L ND NO p-Isopropyttoluene mg/L NO NO sec-Butylbenzene mg/L NO NO Styrene mg/L NO NO terl-Butylbenzene mg/L ND NO Tetrachloroethene mg1L ND NO Toluene mg/L ND ND trans-11,2-Dichloroethene mg/L NO NO trans-1,3-Dichloropropene mg/L NO ND Trichloroethene mg/L ND NO Trichlorofluoromethane mg/L NO NO Vinyl acetate mg/L N❑ NO Vinyl chloride mg1L NO ND t ,2-Dichtoroethane-d4 (S) % 99 103 5 4-Bromofluorebenzene (S) % 99 96 3 Dibromofluoromethane (S) % 91 96 5 Toluene-d8 (S) % 97 96 0 Pace AnsWal Services, Inc. 9B00 Kincey Ave- Suite 100 HuntersvIlle, NC 28078 (704)875-9G92 Dale: 08/0312011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 28 of 31 This report shall not be reproduced, except in run, wimout the written consent of Pace Analytical Services, Inc., 18c, Pace Analyttcat Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Analytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9600 KinceyAve. Suite 10o wwwpawfaftam Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Stormwater 2011 Pace Project No.: 9298716 OC Batch: WETA110201 Analysis Method: EPA 420.4 OC Batch Method: EPA 420.4 Analysis Description: 420.4 Phenolics Associated Lab Samples: 9298716001, 9298716002 METHOD BLANK: 639633 Matrix: Water Associated Lab Samples: 9298716001, 9298716002 Blank Reporting Parameter Units Resutt Limit Analyzed Qualifiers Phenol mg1L ND 0.010 07/2911111:54 LABORATORY CONTROL SAMPLE: 639634 Spike LCS LCS % Rac Parameter Units Conc. Result % Rec Limits Qualifiers Phenol mglL .25 0.25 101 90-110 MATRIX SPIKE SAMPLE: 639635 9298714001 Spike MS MS % Rec Parameter Units Result Canc. Result % Rec Limits Qualifiers Phenol mg/L 0.052 .25 0.26 82 90-110 M1 MATRIX SPIKE SAMPLE: 639640 9298714002 Spike Ms MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Phenol mg1L 0.15 .25 0.37 91 90-110 SAMPLE DUPLICATE: 639641 9298714003 Dup Parameter Units Result Result RPD Oualifiers Phenol mg1L 0.050 0.055 9 SAMPLE DUPLICATE: 639642 9298561002 Dup Parameter Units Result Result RPD Qualifiers Phenol mglL 0.012 0.013 12 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 29 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ceAnalytical wwwpacela8s.com Project: Stormwater 2011 Pace Project No.: 9298716 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Rivenide Dr - Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254.7176 QUALITY CONTROL DATA QC Batch: WETA/l0216 Analysis Method: SM 4500-CN-E . QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide. Total Associated Lab Samples: 9298716001. 9298716002 METHOD BLANK: 640425 Associated Lab Samples: 9298716001, 9298716002 Parameter Units Cyanide mg/L LABORATORY CONTROL SAMPLE: 640426 Parameter Units Cyanide mg1L Matrix: Waater Blank Reporting Result Limit Analyzed Qualifiers ND 0.0050 07/31/11 12:31 Pace Analocat Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers .1 0.11 112 80-120 MATRIX SPIKE SAMPLE: Parameter 640427 Units 9298721005 Result Spike MS MS % Rec Conc. Result % Rec' Limits Qualifiers Cyanide mg/L ND .1 0.11 111 75-125 SAMPLE DUPLICATE: 640428 9298721005 Dup Parameter Units Result Result RPD Qualifiers Cyanide mg/L ND ND Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 30 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalytical' www.pxvlabs ccwrr Project: Stormwater 2011 Pace Project No.: 9298716 DEFINITIONS Pace Analytical Services, Inc. 205 East Meadow Road - Suge A Eden. NC 27286 (336)623-8921 QUALIFIERS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 98DD Kincey Ave. Suite 100 Huntersville, NC 28078 OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. NO Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Dipheny[hydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate "A recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Sllics Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyle is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden PASI.O Pace Analytical Services - Ormond Beach ANALYTE QUALIFIERS C9 Common Laboratory Contaminant. L0 Analyte recovery in the laboratory control sample (LCS) was outside QC limits_ 1 9 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias. M0 Matrix spike recovery andlor matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. PS The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be achieved in sample matrix spikes. R1 RPD value was outside control limits. $1 Surrogate recovery outside laboratory control limits (oontirmed by re -analysis). (704)875-9092 Date: 08/03/2011 04:12 PM REPORT OF LABORATORY ANALYSIS Page 31 of 31 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. NNA WEILmMcLAIN VOMR SAFETY BROCHURE "SAFETY IS EVERYONE'S JOBI'* 523 S. New Street Eden, NC 27288 www.weil-mclain.com tT Michael F, Easley, Governor William G. Ross Jr., secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.E. Director Division of Water Quality March 24, 2006 Mr. Gary R. Conner, Manager Facility & Environmental Engineer Weil -McLain 523 S. New Street Eden, North Carolina 27288 Subject: General Permit No, NCG030000 Weil -McLain COC No. NCG030548 Rockingham County Dear Mr.Conner: In accordance with your application for a discharge permit received on March 6, 2005, we are forwarding herewith the subject certificate of coverage (COC) to discharge under the subject state — NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated May 9, 1994 (or as subsequently amended). If any parts, measurement frequencies, or sampling requirements contained in this permit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, this certificate of coverage shall be final and binding. Please take notice that this certificate of coverage is not transferable except after notice to the Division of Water Quality. The Division of Water Quality may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act or any other federal or local governmental permit that may be required. If you havc any questions concerning this permit please contact Bill Diuguid at telephone number (919) 733-5083 ext. 382. S1ncerely, vrclL�t:1l�1. ' BRADLE 1 BY;`lNT7 L. ,,,Njan,W. Klimek, P.E. cc: Winston-SalemRegional Office Central Files Stormwater Permitting Unit Files N_�o�ftttCarolina Attachments _ Vaturally North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone (919) 733-5083 Customer Service Internet: www.newaleraualsy—orfr Location: 512 N. Salisbury St. Raleigh, NC 27604 Fax (919) 733-9612 1-877-623-6748 An Equal Opportunity/AffirmatNe Action Employer —50% Recycleri110% Post Consumer Paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030548 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Weil -McLain is hereby authorized to discharge stormwater from a facility located at Weil -McLain 523 S. New Street Eden Rockingham County to receiving waters designated asUT to Dan River, a class C. river, in the Roanoke River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, 11, II1, IV, V and V1 of General Permit No. NCG030000 as attached. This Certificate of Coverage shall become effective March 24, 2006. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day March 24, 2006, 1' ORIGINAL SIGNET) gY °. BRADLEY Bt NNr=T1- : J Alan W. Klimek, P.E. Director Division of Water Quality By Authority of the Environmental Management Commission nlV'�t• ice-- Tr /r/ ttl 7 Mon � ! 1 F /'� .a-� I' \ ,lam•. 3 { ,�.. - � \ r '' j. � j'. Markers Name: NCGO30548 — Weil -McLain Short Name: 030548 Coordinates: 0361 30' &19" N, 0790 42' 35.89" W Comment: Weil -McLain, UT to Dan River, Roanoke River Basin, Rockingham County, Re: NCG03548 Weil -McLain NOI Subject: Re: NCG03548 Weil -McLain NOI From: Corey Basinger <Corey. Basinger@ncm ail. net> Date: Tue, 21 Mar 2006 11:52:26 -0500 To: Bill Diuguid <bil l.diuguid@ncmai 1. net> Proceed with issuance. Thanks! Corey Corey Basinger Corey.Basinger@NCmail.net NC DENR Division of Water Quality 585 Waughtown street Winston-Salem, NC 27107 (336) 771-5000 Fax (336) 771-4630 On 3/16/2006 9:37 AM, Bill Diuguid wrote: Corey Basinger: Please either review the attached application yourself or pass this information on to the appropriate person for approval. In addition to the table below, I've also attached a scanned copy of the NOI for review. COC # ;� cility Location- City INCGO30548 Weil -McLain 523 S. New Street Eden If you need any more info, give me a call. If you could respond by 4/16/2006, I'd appreciate it, so I can issue their COC. Thanks. Bill Diuguid William H. Diuguid, A1CP Community Planner, Wetlands and Stormwater Branch Division of Water Quality Department of Environment and Natural Resources 1617 mail Service Center Raleigh North Carolina 27699-1617 Phone: 919-733-5083, ex 382 - Fax: 919-733-9612 1 of 2 3/24/2006 8:47 P.M NCG03548 Weil-Nict_ain NOI Subject: NCG03548 Weil -McLain NOI From: Bill Diuguid <bill. diuguid@ncmai I. net> Date: Thu, 16 Mar 2006 09:37:57 -0500 To: Corey Basinger <Corey.Basinger@ncmail.net> BCC: bdiuguid@nc.rr_com Corey Basinger. Please either review the attached application yourself or pass this information on to the appropriate person for approval. In addition to the table below, I've also attached a scanned copy of the NOI for review. COC # NCGO30548 Facility Location Weil -McLain ! 523 S. New Street City Eden If If you need any more info, give me a call. if you could respond by 4/16/2006, I'd appreciate it, so I can issue their COC. Thanks. Bill Diuguid William H. Diuguid, AICP Community Planner, Wetlands and Stormwater Branch Division of water Quality Department of Environment and Natural Resources 1617 Mail Service Center Raleigh North Carolina 27699-1617 Phone: 919-733-5083, ex 382 Fax: 919-733-9612 NCG030548 Weil -McLain Mar 16 06.pdf Content --Type: application/pdf, Content -Encoding. base64 1 of 1 3/16/2006 1154 PM N idK R yyt" V M owl "'Q: 1: - TI AN 1 T,. 61,, A tilt ko ............ Xx iV INN 1) C; A g A lei' M - n 11�-ill � EDEIN --S --------- 3v Eno RC gf, 71 1 "A I 7-q imp - — V "021 5 30 WE A C lxn- 104T IM A— J5 a, 11 lQ x vv-� Markers Name: NCG030548 -- Weil -McLain Short Name: 030548 Coordinates: 0360 30' 8.19" N, 0790 42' 35.89" W Comment: Weil -McLain, UT to Dan River, Roanoke River Basin, Class C, Rockingham County, Quad A20SW, Southeast Eden f.r&. END wEiL•m<<niN �Mrl Mr�iKg4v dwkw far&Yra N =; 4 �. WA Air i. MTM _ rF MW 00 -- r -�4 1 Ott i 6io4rlr� MIMnF a .nmq,�� so 81MOMOMPAw Your safety is our # 1 priority. Please review our visitor and contractor safety policy prior to entering our manufacturing facility. Please follow these safety rules 0 All visitors and contractors must sign in to the VISITOR LOG prior to entering the facility. 0 Visitors must be escorted by their host while in the facility. 0 SAFETY GLASSES with side shields are required throughout the plant. 0 Open toe, fabric, canvas, and high heel shoes are prohibited on production floor. 0 Please stay in the designated pedestrian walkways and do not enter restricted or unauthorized areas without approval 0 Please follow instructions on all posted signs and warning placards 0 BE ALERT. Watch for moving vehicles and overhead hazards. Stop at all intersections, and keep a safe distance from all powered industrial vehicles. 0 NO PHOTOGRAPHY, unless authorized. 0 NO SMOKING in the plant. Smoking is only permitted outside in designated smoking areas. .Emergency Procedure In the event of an emergency, an alarm or verbal order to evacuate the building will sound over the announcement system. When this is heard, all employees and visitors must evacuate the building using the nearest exit. Once you have evacuated, report your name to the Evacuation Area Coordinator or tour guide immediately. Follow all instructions given during the evacuation. Release and Hold Harmless and demands whatsoever, including but not limited to Agreement those arising out of Visitor's presence and participation at the Weil -McLain Facility, including those arising from the WHEREAS, Weil -McLain, a division of The negligence or tortuous misconduct of Weil -McLain. Marley-Wylain Company ("Weil -McLain") has agreed to provide the undersigned visitor with access to Weil-McLain's facilities in Eden, North Carolina ("Facility") for the purpose of participating in a Facility tour and related activities; and has asked to participate in a tour of Weil-McLain's facility and related activities. NOW THEREFORE, in consideration of the above Visitor agrees to comply with all safety rules, directions, and practices of Weil -McLain. Visitor agrees, for self and for the employer which he/she represents, to treat as confidential all the Company information to which visitor may be exposed, not to use Company Information for any purpose except for work with the Company, and not to disclose Company Information to any third party, without the Company's prior written permission. Nothing contained herein shall restrict disclosure of any technical information which is now generally available to the public through no act of mine or my employer; provided, however, the Company shall not be identified in any such matter as using, having an interest in, or being associated with such information. Visitor hereby releases Weil -McLain and its shareholders, subsidiaries, successors and assigns, and all of their respective directors, officers, employees, and agents (collectively "Representatives") from all manner of claims, actions, causes of action, suits, contracts, covenants, agreements, promises, trespasses, damages, Visitor shall indemnify, defend and hold harmless Weil -McLain and its Representatives from and against any and all losses, liabilities, claims, demands, penalties, fines, settlements, damages and any related expenses (including without limitation, legal, accounting, consulting, and investigation expenses and litigation costs) of any nature whatsoever caused by, arising out of, or relating to the Visitor's presence and participation in activities at this Weil -McLain facility. This agreement may not be terminated or changed unless in a written agreement signed by Weil -McLain and the Visitor. Visitor's Name (Print) Company Visitor's Signature Date IN PRESENCE OF Weil -McLain Representative's Signature This Waiver is valid for one year from the date of signature.