NCG030543_MONITORING INFO_20190111

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO. ,v C�,& 1)305y3
DOC TYPE ❑HISTORICAL FILE
Ei MONITORING REPORTS
DOC DATE L7 jOI 7 D I / /
YYYYMMDD

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted I LII119
CERTIFICATE OF COVERAGE NO. NCG03 O S y 3 SAMPLE COLLECTION YEAR Z
FACILITYNAME 14VJ1500 fV1410e fiDy✓ipyvlemfs-9eimVlPIP w) SAMPLE PERIOD ❑Jan -June Ef1uly-Dec
COUNTY $0V1�Vr4Of, or ❑Monthly' _ _ (month)
PERSON COLLECTING SAMPLES, I/VlliU�i/�'Uil�i��R DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY PIAC-e LU19S LabCert.# 92yIMWI RECEIVED ❑Zero -flow ❑water Supply []SA
CuiTentS on iaiple collection or analysis;
JANIS2019 I—Inther
u
Part A: Stormwater Benchmarks and Monitoring Results
ceNT;lwL r-ICEPLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 i
S
DWR SECTEpiJ
❑ No discharge this period?2
Outfall No.
Date Sample
collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics'
Benchmarks
-
-
100 mg/L or 50 mg/L"
6.0 - 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
46529
C0530
00400
01119
01051
01094
-00S52
78141
1
IZ/2o iS
I. )S inch
ti •Z "5/t
l0•1
,DQ 71
0•0n
0,a79S
O.OD
DIDD
i
1 Monthly sampling (instead of semi-annual) must begin with the second consdcutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
"See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definij ion as found in 40 CFR 433.11; for semiconductor
use
ce the definition as fe—H in An f Ff; R AQ 12; for electronic crystal manufacture use the deflihitinn nc fniinrl in An r rP Ar.Q 11- nnr4 fnr r thnAe ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring' ---
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. 1 further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
��, 1 Ts_cl r
Title (Print titleLj
Jn�
Signa ure K-� Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?2
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches'
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
15 mg/L
100 mg/L or 50 mg/O
Parameter Code
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS: SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
4: 1 6�" A , — a�
Signature of Permittee Dafe
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 3 of 3

4%
*0
allUniia'iyiiUUI
www.pacafabs.com
1
ANALYTICAL RESULTS
Pace Analytical Services. LLC
2225 Niver5ide Or.
Asnev0e, NC: ?6804
[phone]
Project: Stormwater 401 12/20
Pace Project No.: 92411753
Sample: SW401
Lab ID: 92411753tD01 Collected: 12/20/18 10:00
Received: 12/20/18 13:58 Matrix: Water
Parameters
Results
Units
Report Limit DF
Prepared
Analyzed
CAS No. Oual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND
mg1L
5.0 1
12/23/18 15:22
608 PCB Pest AVE
Analytical Method: EPA608,3 Preparation Method: EPA608.3
Aldrin
ND
ug/L
0,050 1
12/21/1815:56
12127/1809:30
309-00-2
alpha-BHC
ND
ugiL
0.050 1
12.!21/18 15:56
12/27/18 09:30
319-84-6
beta-BHC
ND
ugiL
0.050 1
12/21/18 15:56
12127118 09:30
319-85-7
delta-RHC
ND
ug/L
0.050 1
12/21/18 15:56
12!27/18 09:30
319.86-6
gamma-BHC (Lindane)
ND
ugiL
0.050 1
12/21/16 15:56
12/27/18 09:30
58-89-9
Chlordane (Technical)
ND
ugiL
0.50 1
12/21/18 15:56
12127/18 09:30
57-74-9
alpha -Chlordane
ND
ugiL
0.050 1
12.!21/1815:56
12/27/18 09:30
5103-71-9
gamma -Chlordane
ND
ug/L
0.050 1
12/2W815:56
12127/1809:30
5103-74-2
4,4'-DDD
ND
ugiL
0,050 1
12121/18 15:56
12!27/18 09:30
72-54-8
4,4'-DDE
ND
ug/L
0.050 1
12,12l/18 15:56
12/27;118 09:30
72-55-9
4.4'-DDT
ND
ug/L
0.050 1
12i21/18 15:56
12/27l18 09:30
50-29-3
Dieldrin
ND
ug/L
0.050 1
12/21/18 15:56
12/27/18 09:30
60-57-1
Endosulfan 1
ND
ugiL
0.050 1
12/21/18 15:56
12/27/18 09:30
959-98-8
Endosuifan ii
ND
ugiL
0.050 1
12;21/18 15:56
12,27118 DOOR
33213-05-9
Endosulfan sulfate
ND
ug/L
0.050 1
12/21/18 15:56
12127/18 09:30
1031-07-8
Endrin
ND
ugiL
0.050 1
12/21/18 15:56
12127/18 09:30
72-20-8
Endrin aldehyde
ND
ugiL
0,050 1
12,121/1815:56
12/27/1809:30
7421-93-4
Heptachlor
ND
ug/L
0.050 1
12/21118 15:56
12r27/18 09:30
76-44-8
Heptachlor epoxide
ND
ug/L
0-050 1
12/21/18 15:56
12/27A8 09:30
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ugiL
0,50 1
12/21/18 15:56
1212T18 09:30
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0,50 1
12/21/18 15:56
12,127/18 09:30
11104-28-2
PC6-1232 (Aroclor 1232)
ND
ugiL
0.50 1
12/21/18 15:56
12127'18 09:30
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ugiL
0.50 1
12/21/18 15:56
12/27/18 39:30
53469.21-9
PCB-1248 (Aroclor 1248)
ND
ugiL
0.50 1
12/21/18 15:56
12/27/18 D9:30
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ugiL
0.50 1
12/21/18 15:56
12/27/18 09:30
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0,50 1
12121/18 15:56
12/27/18 09:30
11096-82-5
Toxaphene
ND
ugiL
0,50 1
12/2111815:56
12127/1809:30
8001-35-2
Surrogates
Teirachloro-m-xylene (S)
104
46
60-140 1
12121118 15:56
121.,2711$ 09:30
877 09 8
Decachlofobiphenyl (S)
49
%
60-140 1
12,121/18 15:56
12127111809:30
2051-24-3 lg,S0
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Arsenic
ND
ug/L
10.0 1
12/2l/18 03:45
12123118 21:09
7440-38-2
Cadmium
ND
ugiL
1.0 1
12,•'21118 03A5
12123il8 21:09
7440-43-9
Chromium
ND
ugiL
5.0 1
12/21/18 0145
12i23118 21:09
7440-47-3
Copper
5.7
ugiL
5.0 1
12/21/18 03:45
12,123118 21:09
7440-50-8
Lead
ND
ugiL
5.0 1
12121/1803:45
12/23/1821:09
7439-92-1
Nickel
ND
ugiL
5.0 1
12/21/18 03:45
12/23118 21:09
7440-02-0
Silver
ND
ugiL
5.0 1
12121/18 03:45
12/23118 21:09
7440-22-4
Zinc
79.5
ug/L
10.0 1
.2121118 03:45
12123M 8 21 �09
744Q-B8-6
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Mercury
ND
ugiL
0.20 1
12/20/18 23:11
12/21/18 17:28
7439-97-6
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced; except in
full,
Date: 01 /03!2019 11 :54 AM
without the written consent of Pace Analytical Services. LLC.
Page 4 of 32

uvQ � u y�ivuf
i www.pacelahs.com
i
l
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr. i
AStieville, NG 28804
[phone]
Project: Stormwater 401 12I20
Pace Project No.: 92411753
Sample: SW401 Lab ID: 92411753001 Coliected: 12/20118 10:00 Received: 1212011 B 13:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Acenaphthene
NO
ug/L
5.0
1
1212111812:23
12127/1816:17 83-32-9
Acenaphthylene
NO
ug/L
5.0
1
12/21/1812:23
12127/1818:17
208-96-8
Anthracene
ND
ug/L
5.0
1
12/21/1812:23
12/27/1818:17
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
12/21/1812:23
12/27/1818A7
56-55-3
Benzo(a)pyrene
NO
ug/L
5.0
1
12/21/1812:23
12/27/1818:17
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
12/21/18 42:23
12/27/18 18:17
205-99-2
Benzo(g,hJ)perylene
ND
ug/L
5.0
1
12121/1812:23
12/27/18 1 8: 17
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
1212V1812:23
12127/1818:17
207-08-9
4-Bromophenylphenyl ether
NO
ug/L
5.0
1
12/21/18 12:23
12/27/18 18:17
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
12/21/18 12:23
12/27/18 1 B:17
85-68-7
4-Chloro-3-methylphenol
NO
ug/L
5.0
1
12/21/1812:23
12/27,11818:17
59-50-7
bis(2-Chioroethoxy)methane
NU
ug/L
9.9
1
12121/1812:23
1212711818:17
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
12/21/18 12:23
12/2711818:17
111-44-4
2-Chloronaphthalene
NO
ug/L
5.0
1
12/21/181223
12/27/1818:17
91.58-7
2-Chiarophenol
ND
ug/L
5.0
1
12/21/1812:23
12/27/1818A7
95-57-8
4-Chlorophenylphenylether
NO
uglL
5-0
1
12121/1812:23
12/27/1818A7
7005-72-3
chrysenne
ND
ug/L
5.0
1
12/21l18 12:23
12/27118 8:17
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
1212111812:23
12/27/1818:17
53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
24.8
1
12/2111812:23
1212711818:17
91-94-1
2,4-Dichlorophenol
NO
ug/L
5.0
1
12121/1812:23
12/27/1818:17
120-83-2
Diethytphlhalate
ND
ug/L
5.0
1
1212111812:23
12/27/1818:17
84-66-2
2,4-Dimethylphenol
NO
ug/L
9.9
1
12121/1812:23
12/2711818:17
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
12/21/1812:23
12/27/1818:17
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
12121/1812:23
12/27/1818:17
84-74-2
4,6-Dinitro-2-methylphenol
NO
ug/L
19.8
1
1212111812:23
12/27/1818:17
534-52-1
2.4-Dinitrophenol
ND
ug/L
49.5
1
12/21/181223
1212711818:17
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
12/21/1812:23
12127/1818:17
121-14-2
2,6-Dinitrotoluene
NO
ug/L
5.0
1
12/21/1812:23
12/27,11818:17
606-20-2
Di-n-octylphthalate
NO
ug/L
5.0
1
12121/1812:23
12/27/1818:17
117-84-0
bis (2- Ethylh exyl) p htha late
ND
ug/L
5.0
1
12/21/1812:23
12127/1818:17
117-81-7
Fluoranthene
NO
ug/L
5.0
1
12/21/1812:23
12127/1818:17
206-44-0
Fluorene
ND
ug/L
5.0
1
12/21/1812:23
12127A818:17
86-73-7
Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
12/21/1812:23
1212711818:17
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
12/21/1812:23
12/27/1818:17
116.74-1
Hexachlorocyclopentadiene
NO
ug/L
9.9
1
12/21/1812:23
12/27/1618:17
77-47-4
Hexachlaroelhane
NO
ug/L
5.0
1
12/21/1812:23
12127/1818:17
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
12121/1812:23
12/27/1618:17
193-39-5
Isophorone
ND
ug/L
9.9
1
12/21/1812:23
12/27/1618:17
78-59-1
Naphthalene
NO
ug/L
5.0
1
12121/1812:23
12127/1818:17
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
12/21/1812:23
12127/1818:17
98-95-3
2-Nitraphenol
NO
ug/L
5.0
1
12/21/1812:23
12/2711818:17
88-75-5
4-Nitraphenol
ND
ug/L
49.5
1
12121/1812:23
1212711818:17
100-02-7
N-Nitrosodimethylamine
ND
on.1
5-0
1
19121 812:2.3
1719711818:17
62-75-9
N-Nitroso-di-n-propyiamine
ND
ug/L
5.0
1
12/21/1812:23
12/27/1618:17
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
9.9
1
12121/1812:23
1212711818:17
86-30-6
2,2'-Oxybis(1-chloropropane)
NO
ug/L
5.0
1
12121/1812:23
12/27/1818:17
108-60-1
Pentachlorophenol
NO
ugI
9.9
1
12121/1812:23
12/27/1618:17
87-86-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01103/2019 11:54 AM without the written consent of Pace Analytical Services, Lt.C. Page 5 of 32

']/+❑ Awilt rt17•?l
yam/! CI V U /-i! !Uly it UfAl
www.pscelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Hiverside Dr.
%15flevilie, m- 26UVN
[phone]
Project: Stormwater 401 12/20
Pace Project No.'. 92411753
Sample: SW401 Lab 1D: 92411753001 Collected: 12!20!18 10:00 Received: 12/20/18 13:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
625 MISSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Phenanthrene
NO
uq/L
5.0
1
12/21/18 12:23
12/27/1816:17
85-01-8
Phenol
NO
ug/L
5.0
1
12121/1812:23
12/27/1816:17
108-95-2
Pyrene
ND
ug/L
5.0
1
12121/1812:23
1 2127J 18 18:17
129-00-0
1,2,4-Trichlorobenzene
ND
ugiL
5.0
1
12/2111812:23
12127/1818:17
120-82-1
2,4.6-Trichlorophenol
NO
ugiL
9.9
1
12121/1812:23
12127/1818:17
88-06-2
Surrogates
Nitrobenzene-d5 (S)
38
%
10-120
1
12121/18 12:23
12/27118 18:17
4165-60-0
2-Fluorobiphenyl (S)
39
°b
15-120
1
12/21/18 12:23
12/27/18 16:17
321-60-8
Terphenyl-dl4 (S)
38
%
11-131
1
12/21/18 12:23
12127i18 18:17
1718-51-0
Phenol-d6 (S)
15
5;
10-120
1
12/21/18 12:23
12127/18 16:17
13127-88-3
2-Fluorophenol (S)
19
%
10-120
1
1212118 12:23
12I27118 18:17
367-12-4
2,4,6-Tribromophenol (S)
55
%
10-137
1
12/21/18 12:23
12127/18 18:17
118-79-6
624 Volatile Organics
Analytical Method: EPA 624.1
Benzene
NO
ugiL
2.0
1
12,123/1 B 02:27
71-43-2
Bromodichloromethane
NO
ug!L
2.0
1
12/23/18 02:27
75-27-4
Bromoform
ND
ugiL
2.0
1
12/23/18 02:27
75-25-2
Bromomethane
NO
ugiL
2.0
1
12,r23/18 02:27
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
12/23/18 02:27
56-23-5
Chlorobenzene
NO
ugiL
2.0
1
12/23/18 02:27
108-90-7
Chloroethane
ND
ugiL
2.0
1
12123/18 02:27
75-00-3
C:hlornform
ND
uo1L
2.0
1
12123118 02:27
67-66-3
Chloromethane
NO
ugiL
2.0
1
12/23/18 02:27
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1
12/23/18 02:27
124-48-1
1,2-Dichlorobenzene
ND
ugiL
2.0
1
12,123/1802:27
95-50-1
1,3-Dichlorobenzene
NO
ug/L
2.0
1
12123/18 02:27
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
12/23! 18 02:27
106-46-7
1,1-Dichtaroethane
NO
ugiL
2.0
1
12/23l1802:27
75-34-3
1,2-Dichloroethane
ND
ugiL
2.0
1
l212311802:27
107-06-2
1,1-Dichloroethene
NO
ugiL
2.0
1
12/23/18 02:27
75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
2.0
1
12/23/18 02:27
156-59-2
trans-1,2-Dichloreethene
NO
ugiL
2-0
1
12;23.11802:27
156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
1
12/23/18 0 2:2 7
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
12r23/1B02:27
10061-01-5
trans-1,3-Dichlorepropene
NO
ugil-
2.0
1
1212311802:27
10061-02-6
Ethylbenzene
ND
ugiL
2.0
1
12/23/18 02:27
100-41-4
Methylene Chloride
NO
ugiL
2.0
1
12123/18 02:27
75-09-2
1,1,2,2-Tetrachloroethane
NO
ugiL
2.0
1
12123/18 02:27
79-34-5
Tetrachloroethene
ND
ugiL
2.0
1
12123!18 02:27
127-18-4
Toluene
NO
ugiL
2.0
1
12123/18 02:27
108-86-3
1,1,1-Trichloroethane
NO
uglL
2.0
1
12123/18 02:27
71-55-6
1,1 .2-Trichloroethane
ND
ugiL
2.0
1
12/23/18 02:27
79-00-5
Trich!oroethene
NO
r,n11-
2.0
1
12/23/18 02:27
79-01-6
Trichlorofluoromethane
NO
ugiL
2.0
1
12/23/18 02:27
75-69-4
Vinyl chloride
NO
ugiL
2.0
1
12123/18 02:27
75-01-4
Surrogates
4-Bromoffuorobenzene (S)
103
%
70-130
1
12123/18 02:27
460-00-4
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in
full,
Date: 01/0312019 11:54 AM
without the written consent
of Pace Analytical Services, LLC.
Page 6 of 32

2"3rP.4nqh1tirq1'
Pace Analytical Services. LLC
X�
2225 Riverside Dr.
ifs,/. Mww..''w')..—
Asheville, NG28804
wwwpocelbbs.com
F(
r
[phone]
ANALYTICAL RESULTS
Project: Stormwater 401
12120
Pace Project ND.: 92411753
Sample: SW401
Lab ID: 92411753001 Collected: 12/20!18 10:00
Received: 12/20118 13:58 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624.1
Surrogates
Toluene -dB (S)
104 % 70-130 1
12/23/18 02:27 2037-26-5
1,2-Dichloroethane-d4 (S)
105 % 70-130 1
12/23/1802:27 17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
22.2 mg/L 6.2 1
12/21/18 16:41
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+i3-2011
pH at 25 Degrr'es C
6-2 Std. Units 1.0 1
12i26118 16:40 H3
420.4 Phenolics, Total
Analytical Method: EPA 420.4 Rev 1,0 1993 Preparation
Method: EPA 420.4 Rev 1.0 1993
Phenol
ND mg/L 0.010 1
12/2811811:24 12f28/1814:51 108-95-2
450OCNE Cyanide, Total
Analytical Method: SM 4500-CN-E-2011 Preparation Method:
SM 4500-CN-E-2011
Cyanide
ND mg -IL 0.0080 1
12/24/1812:27 12/27/1818:11 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 j0312019 11 :54 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 32

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Resources G neral Permit No. NCG030000
Date submitted bta hal A 1
CERTIFICATE OF COVERAGE NO: NCG03
SAMPLE COLLECTION YEAR20 It
FACILITY NAME Oe 0MA-hl Vt SAMPLE PERIOD ®.Jan -June ❑ July -Dec
COUNTY _90 h WV0 bZ or ❑ Monthly' (month)
PERSON COLLECTING SAMPLES 61Xa DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
r `ECE1, V �� Zero -flow [:]WaterSupply ❑SA
LABORATORY $ Lab Cert. ii `�i ❑
JUL n [ `n1A Iulnther
Comments on sample collection or analysis: u U -
Part A: Stormwater Benchmarks and Monitoring Results
CC-NTRAL F11_115 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
pWR SECTIOV
❑ No discharge this period:
Outfall No.
Date 5ample
Collected'-
Imo/dd/yrJ
24=hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics s
9enchmarks =4=>
.
.lu
100 mg/L or 50 mg/L
6.0 - 9.0
0.007 mg/L
0.03 mg/L
. 0:067 mg/L
15 mg/L
1 mg/L
I
os
O.uo
0. 0 2$
0. oo
0.00
' Monthly sampling (instead of 3enii-ariuival) nmst begin with the second consecutive benchmark exceedance for the same parameter a, the ,am-. outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
' See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
iJanie (Print riarr5e)
QC(Cfly ,,(r a
Title (Print ti le
- W n
j(�)
( nature) Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, thev must be reported in the format,_"<XX mg&', where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: ff you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n No discharge this period?2
Outfall Na.
Date Sample
Collected 1
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM(
Total Suspended Solids
pH
Benchmarks =__>
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
(
I
I
I
I
I I
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR R PART AAND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCE5 IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end
in the case of "No Discharge" reports) to:
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware tht t rjare s;g�ni�pen. s for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permitte (Date)
Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Pace Analytical Services, LLC
.inn A.a. 1. .i;—nl
2225 Riverside Dr.
/_J--IrQ1,V 111ILItyLIbQ1Asheville, NC 28804
wwwpaceiabs.com [phone]
ANALYTICAL RESULTS
Project: SW 502 5/16
Pace Project No.: 92385007
Sample: SW 502
Lab ID: 92385007001 Collected:
05116/18 14:39
Received: 05116118 16:00 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Oual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L
5.0 1
05/24/18 05:11
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
18.4 mg/L
3.3 1
05/22/18 23:41
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.8 Std. Units
1.0 1
05/17/18 17:30 H1,H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2018 03:25 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 31

aceAnalXical
wmpacaleb$corn
Ir
ANALYTICAL RESULTS
Project SW 502 5/16
Pace Project No.: 92385007
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 25504
(828}254-7176
Syrnp!e- SW 502 1 --n In- 92385007002 Collected n5118118 14:39 Received: 05116118 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Cual
608 PCB Pest RV E Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Aldrin
ND
ug1L
0.050
1
05/20/18 18:42 05/21/18 22:37
309-00-2
alpha-BHC
ND
ug/L
0.050
1
05120/1818:42 05/21/18 22:37
319-134-6
beta-BHC
ND
ug/L
0.050
1
05/20/18 18:42 05/21/18 22:37
319-85-7
delta-BHC
ND
ug/L
0.050
1
05/20/18 18:42 05/21/18 22:37
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
1
05/20/18 18:42 05/21/18 22:37
58-89-9
Chlordane (Technical)
ND
ug/L
0.50
1
05/20/18 18:42 05/21/18 22:37
57-74-9
alpha -Chlordane
ND
ug/L
0.050
1
05/20/1818742 05/21/1522:37
5103-71-9
gamma -Chlordane
ND
ug/L
0.050
1
05/20/1818A2 05121/1622:37
5103-74-2
4,4'-DDD
ND
ug/L
0.050
1
05/20/18 18:42 05/21/18 22:37
72-54-8
4,4'-DDE
ND
ug/L
0.050
1
05/20/18 18:42 05/21/18 22:37
72-55-9
4,4'-DDT
ND
ug/L
0.050
1
05/20/18 18:42 05/21/18 22:37
50-29-3
Dieldrin
ND
ug/L
0.050
1
05/20/18 18:42 05/21/18 22:37
60-57-1
Endosulfan 1
ND
ug1L
0.050
1
05/20/18 18:42 05/21/18 22:37
959-98-8
Endosulfan II
ND
ug/L
0.050
1
05/20/18 18A2 05/21/18 22:37
33213-65-9
Endosulfan sulfate
ND
ug/L
0,050
1
05/20/18 18:42 05/21/18 22:37
1031-07-8
Endrin
ND
ug/L
0.050
1
05/20/18 18:42 05/21/18 22:37
72-20-8
Endrin aldehyde
ND
ug/L
0.050
1
05/20/18 16:42 05/21/18 22:37
7421-93-4
Heptachlor
ND
ug1L
0.050
1
05/20/18 18:42 05/21/18 22:37
76-44-6
Heptachlor epoxide
ND
ug1L
0.050
1
05/20/18 18:42 05/21/18 22:37
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
1
05/20/18 18:42 05/21/18 22:37
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
1
05/20/18 18:42 05/21/18 22:37
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
1
05/20/18 18A2 05/21/1822:37
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
1
05/20/18 18:42 05/21/18 22:37
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug1L
0,50
1
05/20/18 18:42 05/21/18 22:37
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug1L
0.50
1
05/20/18 16:42 05/21/18 22:37
11097-69-1
PCB-1260 (Aroclor 1260)
ND
uglL
0.50
1
05/20/16 18:42 05/21/18 22:37
11096-82-5
Taxerohene
ND
uglL
0.50
1
05/20/18 1 BA2 05/21/18 22:37
8001-35-2
surrogates
Tetrachtoro-m-xylene (S)
49
%
60-140
1
05/20/18 18:42 05/21/18 22:37
877-09-8 5o
Decachlorobiphenyl (S)
29
%
60-140
1
05/20/18 18:42 05/21A8 22:37
2051-24-3 so
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Antimony
ND
ug/L
5.0
1
05/29/1816:05 05/3011814:56
7440-36-0
Arsenic
ND
ug/L
10.0
1
05/2911816:05 05/3011814:56
7440-38-2
Beryllium
ND
ug/L
1,0
1
05/29/1816:05 05/30/1814:56
7440-41-7
Cadmium
ND
ug1L
1.0
1
05/29/1816:05 05130/1814:56
7440-43-9
Chromium
ND
ug1L
5.0
1
05/29/1816:05 05/30/1814:56
7440-47-3
Copper
6.3
ug/L
5.0
1
05/29/1816:05 05130/1814:56
7440-50-8
Lead
ND
ug/L
5.0
1
05/2911816:05 0513011814:56
7439-92-1
Nickel
ND
ug/L
5.0
1
05129/1816:05 05/3011814:56
7440-02-0
Selenium
ND
ug/L
10.0
1
05/29/1816:05 05/30/1814:56
7782-49-2
Silver
ND
ug/L
5.0
1
05129/1816:05 05/30/1814:56
7440-22-4
Thallium.
ND
11^yr`
Inn
t
05/29/1816:05 0511011814;56
7440-PA-0
Zinc
28.0
ug/L
10.0
1
05129/1816:05 05130/1814:56
7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2018 03:25 PM without the written consent of Pace Analytical Services, LLG. Page 5 of 31

2--
Pace Analytical Services, LLC
A --1 .i..,.,f o
2225 Riverside Dr.
clua t1! laryLlual
Asheville, NC 28804
www.pacwabs-tom
[phone]
ANALYTICAL RESULTS
Project: SW 502 5/16
Pace Project No.: 92385007
Sample: SW 502 Lab ID: 923MO7002 Collected: 05116/18 14:39 Received: 05/16/18 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
245.1 Mercury
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Mercury
ND
uglL
0.20
1
05/22118 17: 10 05123/1811:25
7439-97-6
625 MSSV
Analytical Method: EPA 625 Preparation
Method: EPA 625
Acenaphthene
ND
ug/L
48.1
10
05120/1 B 18:34 05/29/18 12:36
83-32-9
Acenaphthylene
ND
ug/L
48.1
10
05/20/1818:34 0512911812:36
208-96-8
Anthracene
ND
ug/L
48.1
10
05120/1618:34 05/2911812:36
120-12-7
Benzo(a)anthracene
ND
ug/L
48A
10
05/20/1818:34 05129/1812:36
56-55-3
Benzo(a)pyrene
ND
ug/L
48.1
10
05/20/1818:34 05/29/18 12:36
50-32-8
Benzo(b)fluoranthene
ND
ug/L
48.1
10
05120/1818:34 05/29/18 12:36
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
46.1
10
05/2011818:34 05129/1812:36
191-24-2
Benzo(k)fluoranthene
ND
ug/L
48.1
10
05/2011818:34 05/29/18 12:36
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
46.1
10
05/20/18 18:34 05/29/18 12:36
101-55-3
Butylbenzylphthalate
ND
ug/L
48.1
10
0512011818:34 0512911812:36
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
48.1
10
0512011818:34 05129/1812:36
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
96.2
10
05/20/1818:34 05129/1812:36
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
48.1
10
05/20/18 18:34 05/29/18 12:36
111-44-4
2-Chloronaphthalene
ND
ug/L
48.1
10
05/20/1818:34 a51291i812:36
91-58-7
2-Chlorophenol
ND
ug/L
48.1
10
0512011818:34 05129/1812736
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
48.1
10
05/20/18 18:34 05/29/18 12:36
7005-72-3
Chrysene
ND
ug/L
46.1
10
05/201181834 05/29/18 12:36
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
48.1
10
05120/1818:34 05/29/18 12:36
53-70-3
3,3'-Dichloiobenzidine
ND
ug/L
240
10
05/20/11318:34 05/29/1812:36
91-94.1
2,4-Dichlorophenol
ND
ug/L
48.1
10
05/2011818:34 05/29/18 12:36
120-83-2
Diethylphthalate
ND
ug/L
48.1
10
0512011818:34 05/2911812:36
84-66-2
2,4-Dimethylphonol
ND
ug/L
96.2
10
05/20/1818:34 0512911812:36
105-67-9
Dimethylphthalate
ND
ug/L
48.1
10
05/2011818:34 05/29/18 12:36
131-11-3
Di-n-butylphthalate
ND
ug/L
48.1
10
05/20/1818:34 0512911812:36
84.74.2
4,6-Dinitro-2-methyl phenol
ND
ug/L
192
10
0512011B 18:34 05/29/18 12:36
534-52-1
2,4-Dinitrophenol
ND
ug/L
481
10
0512011B 18:34 05/29/18 12:36
51-28-5
2,4-Dinitrotoluene
ND
ug/L
48.1
10
0512011618:34 05129/1812:36
121-14-2
2,6-Dinitrotoluene
ND
ug/L
48.1
10
05/20/1618:34 05129/1812:36
606-20-2
Di-n-octylphthalate
ND
ug/L
48.1
10
0512011818:34 05/29/18 12:36
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
48.1
10
05120/1818:34 05129/1812:36
117-81-7
Fluoranthene
ND
ug/L
48.1
10
05/2011818:34 05/29M812:36
206-44-0
Fluorene
ND
ug/L
48.1
10
05/20/1818:34 05/29/18 12:36
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
48.1
10
05/20/1818:34 05129/1812:36
87-68-3
Hexachlorobenzene
ND
ug/L
48.1
10
05/20/1818:34 05129/1812:36
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
96.2
10
05/20/1818:34 05/29/18 12:36
77-47-4
Hexachloroethane
ND
ug/L
48.1
10
05/20/1818:34 05129/1812:36
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
48.1
10
05/20/1818:34 05/29/18 12:36
193-39-5
Isophorone
ND
ug/L
96.2
10
05/20/1818:34 05/29/18 12:36
78-59.1
Naphthalene
ND
ug/L
48.1
10
0512011818:34 05/29/18 12:36
91-20-3
Nitrobenzene
ND
ug/L
48.1
10
051201188 18:34 05129/18 12:36
93-95-3
2-Nitrophenol
ND
ug/L
48.1
10
05120/1818:34 05/2911812i36
88-75-5
4-Nitrophenol
ND
ug/L
481
10
05120/1818:34 05/2911812:36
100-02-7
N-Nitrosodimethylamine
ND
ug/L
48.1
10
05/20/1816:34 05/29/1812:36
62-75.9
N-Nitroso-di-n-propylamine
ND
ug/L
48.1
10
05/20/1818:34 05129/1812:36
621-64.7
REPORT OF LABORATORY ANALYSIS
This report shall not
be reproduced, except in full,
Date: 05/31/2018 03:25 PM
without the written consent of Pace Analytical Services, L-C.
Page 6 of 31

"1102
/�TQi.G MI fal y tllrp!
www.pac&%Ebs.com
F
t
ANALT T iC.AL RESULT S
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: SW 502 5/16
Pace Project No.: 92365007
Sample: SW 502 Lap ID- QViRRM07002 Cnilorted: OS116I18 14:39 Received: 05/16/18 16:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA625 Preparation Method: EPA625
N-Nitrosodiphenylamine
NO
ug/L
962
10
05/20/18 18:34
05/29/18 12:36
86-30-6
2,2'-Oxybis(1-chloropropane)
NO
ug/L
48.1
10
05/20/1818:34
05/2911812:36
108-60-1
Pentachlorophenol
NO
ug[L
96.2
10
05120/1818:34
0512911812:36
87-86-5
Phenanthrene
NO
ug[L
48.1
10
05/20/1818:34
0512911812:36
85-01-8
Phenol
NO
ug/L
48.1
10
05/20/1818:34
05/2911812:36
108-95-2
Pyrene
NO
ug/L
48.1
10
05/20/18 18:34
05/29/18 12:36
129-00-0
1,2,4-Trichlorobenzene
NO
ug[L
48.1
10
05/20/18 18:34
05/2911812:36
120-82-1
2,4,6-Trichlorophenol
NO
ug/L
96.2
10
05120/1818:34
0512911812:36
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
10-120
10
05120/1818:34
05129/i8 12:36
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
15-120
10
05120/1818:34
05/29/18 12:36
321-60-8
S4
Terphenyl-d14 (S)
0
%
11-131
10
05/20/18 18:34
05/29/18 12:36
1718-51-0
S4
Phenol-d6 (S)
0
%
10-120
10
05/20/18 18:34
05/29/18 12:36
13127-88-3
S4
2-Fluorophenol (S)
0
%
10-120
10
05/20/18 18:34
05/29/18 12:36
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
10-137
10
05/20/18 18:34
05/29/18 12:36
118-79-6
S4
624 Volatile Organics
Analytical Method: EPA624
Benzene
NO
ug/L
2.0
1
05/19/18 02:11
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1
05/19/18 02:11
75-27-4
Bromoform
NO
uglL
2.0
1
05/19/16 02:11
75-25-2
Bromomethane
NO
ug/L
2.0
1
05/19/18 02:11
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
05/19/18 02:11
56-23-5
Chlorobenzene
NO
ug/L
2.0
1
05/19/18 02:11
108-90-7
Chloroethane
NO
ug/L
2.0
1
05/19/18 02:11
75-00-3
Chloroform
NO
ug/L
2.0
1
05/19/18 02:11
67-66-3
Chloromethane
NO
ug/L
2.0
1
05/19/18 02:11
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1
05/19/18 02:11
124-48-1
1 ,2-Dichlorobenzene
NO
ug/L
2.0
1
05/19/18 02:11
95-50-1
1,3-Dichlorobenzene
NO
ug/L
2.0
1
05/19/18 02:11
541-73-1
1,4-Dichlorobenzene
NO
ug1L
2.0
t
05119/1802:11
106-46-7
1,1-Dichloroethane
NO
ug/L
2.0
1
05/19/18 02:11
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
05/19/18 02:11
107-06-2
1,1-Dichloroethene
NO
ug1L
2.0
1
05/19/18 02:11
75.35-4
cis-1,2-Dichloroethene
NO
ug/L
2.0
1
05/19/18 02:11
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1
05/19/18 02:11
156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
1
05119/1802:11
78-87-5
cis- 1,3- Dichloropropene
NO
ug/L
2.0
1
05119/1802:11
10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
2.0
1
05/19/18 02:11
10061-02-6
Ethylbenzene
NO
ug/L
2.0
1
05/19/18 02:11
100-41-4
Methylene Chloride
ND
ug/L
2.0
1
05/19/18 02:11
75-09-2
1,1,2,2-Tetrachloroethane
NO
ug/L
2.0
1
05/19/18 02:11
79-34-5
Tetrachloroethene
NO
ug/L
2.0
1
05/19/18 02:11
127-18-4
otuene
NO
U. n
2.0
1
05rt art 8 02:11
1 n8-aa-3
1,1,1-Trichloroethane
NO
ug/L
2.0
1
05/19/18 02:11
71-55-6
1.1,2-Trichloroethane
NO
ug/L
2.0
1
05/1911802:11
79.00-5
Trichloroethene
NO
ug/L
2.0
1
05/19/18 02:11
79-01-6
Trichlorofluoromethane
NO
ug/L
2.0
1
05/19/18 02:11
75.69-4
REPORT
OF LABORATORY ANALYSIS
This report shall not
be reproduced, except in
full,
Date: 05/31/2018 03:25 PM
without the written consent of Pace Analytical Services, LLC.
Page 7 of 31

/ !X — - A 1-4:. 1 a
,.rdL M11dly11(;dr
www.pacelabs.com
1
ANALYTICAL RESULTS
Project: SW 502 5116
Pace Project No.: 92385007
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: SW 502
Parameters
Lab ID: 92385007002 Collected: 05/16/18 14:39
Results Units Report Limit DF
Received: 05/16/16 16:00 Matrix: Water
Prepared Analyzed GAS No- Qual
624 Volatile Organics
Analytical Method: EPA 624
Vinyl chloride
ND ug/L
2.0
1
05/19/18 02:11
75-01-4
Surrogates
4-Bromoftuorobenzene (S)
103 %
70-130
1
05/19/18 02:11
460-00-4
Toluene-d8 (S)
113 %
70-130
1
05/19/18 02:11
2037-26-5
1,2-Dichloroethane-d4 (S)
91 %
70-130
1
05/19/18 02:11
17060-07-0
420.4 Phenolics, Total
Analytical Method: EPA 420.4
Phenol
ND mg/L
0.010
1
05/3014817:45
108-95-2
450OCNE Cyanide, Total
Analytical Method: SM 4500-CN-E
Cyanide
ND mQ/L
0.0060
1
05/2511812:01
57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/31/2016 03:25 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 31

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted I I I
CERTIFICATE OF COVERAGE NO, NCG03a
FACILITY NAIVE vv_t•iSu.r_i —
?itYCOUNTY COYbe. i.mn±}
PERSON COLLECTING SAMPLES m,n IJiStnP.�i 1
LABORATORY ihPAJ &i(,fnnrh-n+nV Lab Cert. t; 324
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR XI_�-
SAMPLE PERIOD 7Jan-June M July -Dec
or ❑ Monthly'_ (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
RECEIVED ❑Zero -flow ❑Water Supply ❑SA
©Other, �,�(155 C
NOV 2 9 20PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
CENTRAL FILES
DWR SECTION
❑ No discharge this period?'
Qutfall No:
Date Sample
Collected i
(rno%ddij-L
24-hour rairifall
amount;"
3 :.
Inches ', ..
Total Suspended Salyds,
- .
:..
- pH;
5tandaid'units
Coppet
;
Lead
Zmr9k
Non POlarO&G/:
Total Petroleum '
Hydrocarbons `
Total Toxic
-+Organics s
•.
Bericfimarks===> '
-
100'mg/Uot_50 mg%L`r
b.0'-'9 0
o:007`ing/E"'
0.03 mg/L ..0:067
mg/L
15 mg/C• '
S:mg/L
1oo
10 23 1-7
a.5
Iq
.5
0,00333
0•0009to3
o-Og
1.11 s
I
o
b. 5
0.00IS 3
o.00o 1,�
0.18o
q.�
N Pt
I S
a3
a,5
q8
v 5
0.00S
o-aoa
0.190
3.5 S
'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance.for,the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total Precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially'sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469,31).
�X 5*3ec-f 51k, gMnt-ed regulaiO" ME kV �10M exee<doners aF zinc and Coffer, S-64;e3 in 0, leff�r receiJed
from NCDE%i .sollj & ++led %PDES S�-Omwzc +rtrj�i Rec{tJe.S� �r Rerdvta�" P0;9-
Union "kne- CamPonen�s, Inc- da}� `Jar y, 7-1t 2014
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
S: f e LAr.
Title (Print title)
E //—/7-(7
(Signatur (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L', where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark/ you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mniddivr)
24-hour rainfall
amount,
inches'
Non -polar O&G/7PH by
EPA 1664 (SGT-HEM)
Total Suspended Solids -
pH -
Benchmarks =__>
15 mg/L
100 mg/L or 50 mg/L`
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

, Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
FOR PART AAND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. 5EE PERMIT PART 11 SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑NO❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal and one coov of this DMR, includina all "No Discharae" reports. within 30 days of receipt of the lab results for at end of monitorina period
in the case of "No Discharae" reports) to:
..f Water Quality
�ivi�ivi, �,i vvo�ci 4�a„�y
Attw DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
1/^f 7-f 7
(Signature of Permrttee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted tl h � f 11
CERTIFICATE OF COVERAGE NO. NCG03 © Ip g 5
FACILITY NAME I S
COUNTY
PERSON COLLECTING SAMPLES. rnniin Nisb _A-)
LABORATORY Melly tirmrnen fa J Lab Cert. # 7k74 -
Comments on sample collection or analysis:
7J er- / R. fov e6—A/e (-.(
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 11�01-7
SAMPLE PERIOD ❑ Jan -June ® July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
11..th__ /Jlna /�
�vu�c� ��u� t. ,
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --)
n No discharge this period?'
Date Sample
24 hour rainfall
pH, ",
Total Toxic
Outfall No <
,
Collected .
amount,
Total Suspended Solids
Standard units
Copper
lead
Zinc
Total PetrolOum ,
Organics s
(mo/dd/yr)
Inches 3
Hydrocarbons '
Benchmarks -=>.
100 mg/L or 50 mg1l!
6.0-9.0 „-
. 0.007 mg/L
L.O.03mg/L":
0:067 mg/L
y 15 mgJL
1"rmg/L.
3.
b.5
o.Oo15
o.o�q
I S 5
S
l
5
9 a
ro 5
o-oo�i3
cno
0.15
a O s
0
2
,.i
io•
p.009lc
6
0.0a
L Mo
I NA
y
a
a-s
b•s
o.00l�S
<D.' s
o.oao
< 1•�NEI
cxl 11 QS_5
o a
�• 6
ill, 3
1 b. s
o. Co 12 S
o- 000a-T
I 0.0-lq
I < I - io
N R
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfaii.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
"See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subiect to the requir6ment'to sample (for metal finishing use the definition as found in 40 CPR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CPR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CPR 469,31).
Permit Date:11/1/2012-10/31/201-7 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
S.TC L�se%r
Title (Print title)
�ignature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, theVmust be reported in the format, "<XX mg/L". where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
Ej No dischorge this period?z
Outfall No.
Date Sample
r ,
[ollected
(ma/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar 0&G/TPHby
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks
15 mg/L
100 mg/L or 50 mg/L'r
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
R Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A. AND PART R MONITORING RFSI71_TS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitorina period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
�l
2.7-1?
(Signature of Permittee) (Date)
Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water QuajIIty General Permit No. NCG030000
vate submiiicd injQ, l l -1
CERTIFICATE OF COVERAGE NO. NCG03 O 4 3
FACILI„1 NA.pME I l:,i-6n
o;,
COUNTY UA Dlntbf_ CmAi4i '11
PERSON COLLECTING SAMPLES $ .v`ue�W�in
LABORATORY�C !f P_V7Vl(ONA7re5M (Lab Cert. # 3Z9
Comments on sample collection or analysis:
Part A; Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR ZO (_-
SAMPLE PERIOD ® Jan -June [7]July-Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
RECEIVED ❑Zero -flow ❑Water Supply ❑SA
f1 ®Other C' ASS L
JUN 12 2017
- -. rI A I ­1 CC
1,ocl% 1`mmk_ r11..1_.,
MR -SECTION
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --)
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches;
Total Suspended Solids
pH,
Standard units
Copper*
Lead
Zinc*
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organicss
Benchmorks ===>
-
100 mg/L or 50 mg/O
6.0 - 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
O.JQ C)of
05 1,1 1 tj
0.110
.054
5.0 L
N
i. 1i1 tl nnn
UM tOAL b
�t1�I
, 1
v
A n _ ft
-�.., Pn
�. C
n And. Y-11
v.v a
Ln —,C-
- - ,
, b
y.v1T -
c I e.
.T P.M I I
I mn
0
og of iT
6.10
$3 M L.
(o. �j
D.OM oke, L
0.0026 wt
0. 31D L
1.4 MAIL
IIJA
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
"See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electelectronic r talc manufacture cathode ray tubed For purposes of this permit the definit inn of Tntal Tnvir rlraa nirc is That riofin itinn r ntaineri in the FPo
ronic r••5...,.,, or mangy
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
- 5tAit 4 54'1, gr 4CA fe�u�,4ry 0-(itp G---tr_"Jo tuA J -i,1L, d-1 CoFrtr, 5-k+cd iA slek+u- reCcive.cc
f,C-oho StAlow+ }i�U "wor'S 5iW,40WT r `Crwti� : �tc�ut5} 4-, Renr6ttb,y fieUetn
(�niS�n �noJilc I;o,�po�w{5 , �,,,c, ,1 dat��l 5anuary 2l, Zol4
Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff hac nrriirrpd since filine the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
A-- 4w-e ( C9c-rigs
Name (Print name)
5,7'c Lescicr
Title (Print title)
/%
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L". where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
(Vote: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?2
Outfall No.
Date Sample
Collected,
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar 0&G/TPHby
EPA 1664 (SGT-HEM)
?ota! _
pu
"
Benchmarks =__>
15 mg/L
100 mg/L or S0 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text; Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Nate: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
_Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to. -
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
8 17
(Signatur i tee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater_D_ischarge Monitoring_R_e_port
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted J�'a� d��6
CERTIFICATE OF COVERAGE NO. NCG03 0 { 3
FACILITY NAME 0-616­% - AS1 ew ll[,
COUNTY (_0u,4,1 ff,,
PERSON COLLECTING SAMPLES 'P) o.a ` IS�CXh
LABORATORY vi Lab Cert. # 37-1
Comments on'sample collection or analysis:
`1
Part A: Storrs Dater Benchmarks and Monitoring Results
1
SAMPLE COLLECTION YEAR Z.o I (,
SAMPLE PERIOD ❑ Jan -June ;C July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply []SA
P's r—.-- ..
iXC:ut Vt® L&Otner ixi5
JAN 0 J 2017 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3
CENTRAL FILES
DWR SECTION
n No discharge This Period?'
OutFall No.
Date Sample
Collected'
(mo/dd/yr)
24"hcrairifall
amount,
Inches;
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc*
Non-POlar,O&G/ou
Total Petroleum
Hydrocarbons
Total Toxic
Organicss
Benchmarks
i00 mg/L or 50 m/a
6.0-9-0
0.007 giL
0.03 „g/L
OA57 mg/L
mg/L
g/L
�u}�qll Oal
1t 29 Ito
I.o
lP �L
0.00{(I
0o
/L
nlA
<7rA}�r,�( 002
i1 2q IL.
t.0
2.Co m !/L
(v.'S
D.0032
0.00015
1.4 M (-
Ai -
Ou ll 005
Il 2.9 It,
1.0
('05 m Il
Co 5
0,o m L.
10.0023 L
10.190 L
Z 5 /L
NA
Monthly sampling.(instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites maybe eligible for a waiver of the rain gauge requirement.
`See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 410 CFR 469.31)). 1 ( u
�
- evL-w(' l fi r- rfanfid A- at i'0ry rt,kieL -vom CX LCL c�ovi CZL5 °T dirt(- Gv1a C. PPGf, 5- 4,d in o, Ie--�+Cw� cc-u-i vGd
I` t L �p r
r�tAF QO %,-Mu,e Cr R,-il' gel (A CS+ `�qr
U,viiSon �n�in� ��^Qonttn�5 , _`^`.� ci•tcc) ✓A�1N4Y11,J 21 f ZDi$
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), i certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the stormwater Pollution Prevention Plan."
Name (Print name)
Fi,rEfl FRuUTij V6_11 4#,
Title (Print title)
z& 4 -ate_ 8-a°1 b
ignature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc, in mg/L.
Note:- ff you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
No discharge this period?Z
Outfa€I No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non-polar.O&G/TPH by
EPA 1664'(SGT-HEM)
Total Suspended Solids
pH
Benchmarks
15 mg/L
100 mg/L or 50 mg/L*
6.0 — %0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART AAND PART MONITORING RESULTS:
• A BENCHMARK EXCEFDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART] I SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑NO❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
001
(Signature of Permittee) (Date)
Permit Date: 11/1/2D12-10/31/2017 SWU-245, last revised 10/25/201R
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000^
jt W Date submitted '7-P7 aQ 4;
CERTIFICATE OF COVERAGE NO1�.� NCG03 0 6 3 SAMPLE COLLECTION YEAR Z
FACILITY NAME Awl�n ' f•,SIn2Vi±ia =SAMPLE PERIOD ❑iC Jan -June ❑ July -Dec
COUNTY F_, n wylaQ. or ❑ monthly' month .�
PERSON COLLECTING SAMPLES o wnnY DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
_01,- s
LABORATORY L•�12a1 E✓�vlr�n Lab Cert. Ji 3Zq � r� /� �liv ❑Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: 'RCV `° n" `� "� `'
TRAL FILES Z�164n!rIPJrEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
Part A: 5tormwater Benchmarks and Monitoring Results
pWR SECTION
.❑ No dischorae this oeriod?Z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics5
Benchmarks ===>
-
-
100 mg/L or 50 mg/L4
6.0 - 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
0,49 N 001
in'2 I
1.0
i2 w, L_
(a.S
o.014 L
0.4on L
0.3 M /L
3.2- ,++ 4._
NAA It 00-L
Jo FCoO
�
i 005
ti9 Z}- 11.E
1 . o
o. ool L
0. )-
< 2. ti M _
N
'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2, For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31). A
- Sv lojec� si i L granccQ r.g .(a�r� tc �ie �,n eKce�eia✓IceS ni �I„c anr� GoFpe�r, S�CtcrX cz i�1"*X
(~(Si�uQ �m >JLpE,Q Svb,lc � "�?PF_S S{vrN,w ar fGfwii�: t�e�uts} r�¢,taAri (F.-VAS
V�i �rl��ne C_0A&fa,ne� 1
Permit Date: 11/1/2012-10/31/2017 G1ate far uoYy 2� Zp(�} S11JU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
�3
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature)
(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX ms/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
VVtC. " you report,
Y sample VY1YC I-nI eALCJs Of •lhe L_ _L.11 ...wa •T:.1 :-. I -_ 1:J ..-------
lVV
VCIILIII Il YI A, YVY II IYJL 111l'dIG I IICI.L ! ICI 1, IICI L, VI Il CI J IGJJ-13CJ. .)CC VCUC/UI Tef I ME LCAL,
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?2
outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Non -polar 0&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
15 mg/L
10D mg/L or 50 mg/L*
6.0 — 9.0 Su
Footnotes from Part A also apply to this Part B ,
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit nntp, i 1 PI/7m-'In/�kj Onj7 OAlIIJdS Inct r—i—i 1nhGhrll7
Permit __�-• --- -� --- -� --- --- Page 2 of 3 _..

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART_A ANG-PART B MONITORING RESULTS:
A btNUIMAK& EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART ii SECTION B.
2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
an, aware that /,erre s t Pena ies for submitting false information, including the possibility of a) imprisonment for knowing violations."
� a/f140
(Signature of Permittee) {Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report —99
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
ICRIiFIAIE OF IOVERAGEVO. I1�V1%3n7
A�_SAMPLE ZOl
FACILITY NAME un15o,1- A4&y& q� /r ,�gE PERIOD ❑ Jan -June July -Dec
COUNTY Buv LacMhr (A-n�l RECE�V�tLi or [:]Monthly' (month)
53 �•s� �j DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
PERSON COLLECTING SAMPLES' T]Oanl(iwl/L I`iU V 1 � LUEJ �
LABORATORY biW e m'Ion Lab Cert. # 32°[ ❑Zero -flow ❑Water Supply ❑SA S
Comments on sample collection or analysis: CENTRAL FILES ®Other Class C.
DWR SECTION
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3
Part A. Stormwater Benchmarks and Monitoring Results
❑ No discharge this period:f"
Outfall No.
Date Sample`
r _
Collected
24-hourralnfall
amount
3
Total Suspended Solids
pH,
Standard units
co, per,71
'Lead
Zncye�•
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Tota[Toxic
S
Organics
Benchmarks =__>
100 mg/L',orSO mg/L°
6.0 - 9.0
0.007:mg/L-
'-'0:03 mg/L , :
0.067,!mg/L,
;,' ' 15 mg/L
1 mg/L
l�u bl opl
bq z9 IS
1.3
w
0,3 L
1 0.0034
C.0}g L
< Z.q /L
JA
n
U,P 1l MCI
/ /,
U-1 L'1 lu
I 2
I' �
1.
k..J m
(p.'j
/.
V. vuiT L.
I.
V.VUUX3
r_
b�'�'C'> L
L• I Mq (L
I NK
Qu} 6l 005
09 17,q I�
I.3
�g m a
�
0.05 L
0.003 -1 L
D.J3 MA L
{ 2.9 mt IL
tlA
'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites maybe eligible for a waiver of the rain gauge requirement.
° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
( '- Su��cc..E- Sikc11 g�arrtt��ii'lrt (cA��tu.lO.'Y�ry Ifek;c I�j-amn GlCc.t�dOAncora oi'k p��n'c.L old!)(ppp, -, s4n" (,4 -, a (e,"t`'cr tC-C,fiivP�
-I'W rn 1AC,0C � $U 4�(,L? 4,4 40DES St�N14J0.s<r SCfmi�; Req.u.s� ¢fr \�4.�^�Tbry/ 1SG1,iep 1MiSd1 Ine IAMpo"C' '
L, v v
Permit Oate: 11/112012-10131/2017 :�amkvy ZI 2,01¢ SW U-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Storm water Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TFO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible form an agi rig compliance with the permit monitoring requirement for total toxic organics
(TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature)
(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L". where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging> 55 gal of new oil per month-
n No dischoroe this Deriod?z
Date Sample 24-hourrainfall r
Outfall No J,Collected'• ' amount, Non -polar O&G/TPH
e Total Suspended Solids pH _. 4,
(mo/ddjyr) I inches trFk 1664'(1U 11-F CIVI)f_"
Benchmarks , > ;: 100'mg/L or 50 mg/L` 6 0'—.9:OaDt i
Footnotes from Part A also apply to this Part B
" See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier Z, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART AND PART B MONITORING RESULTS:
A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
e 2 EXCEED AN CESSN A TR W '0R THI E FRARAMaEER AT THE SAME 0L„ LL , RI G G ERn TI E R 2 REQU1RE ..E . S. SEE PERMIT PART 11 SECTION 5.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER ATANY ONE OUTFALL? YES []NOD
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES 0 NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to: T
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
am a e that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
�/ --2
-�s-
(' n u Of PArr iTAee) (Date)
Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03 D S g _
FACILITY NAME (iy)*,!�D/, - AS)GYiIIL
CVVNTy
PERSON COLLECTING SAMPLES A," ;A A;i6x
LABORATORY Lab Cert. #
Comments an ssample collection or . nalysiS:
Part A: Stormwater Benchmarks and Monitoring Results
—r-7
SAMPLE COLLECTION YEAR 20 f S
SAMPLE PERIOD D<Jan-June ❑ July -Dec
or ❑ Mnnthlvl /mnnthl
� `�i�ISvHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNNAA
❑Zero -flow ❑Water Supply ❑SA
JUL 3 0 2015 Bother Class G
CENTRAL TILES DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
dNo discharge this period?Z
Outfall No
°Date Sample
1
Collected ,
rrio/dd/yr) ;
24=h6ur rainfall `
i amount .
3'
Inches
;-Total Suspended Solids
pH,
Standard units'
Copper
Lead
Zinc
'Non -Polar O &G/
:Total Petroleum 1
-Hydrocarbons,
TotalToxic
' -. 5,:
Organics
Benchmarks > .,;
-s.,
- _
100 mg/Lor 50 mg/0
6.0-9.0
0.007,mg/L ,
,:i0.03 mg/L
0:067 mg/L
15mg/L.
1'mg/L
001
0 FL.0o
001.
t to noo
003
rAD F o
004
rlo Foe)
006
00 Ala
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
rnay•be'waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filingthe last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
__mil rr 1C 7 ISO i1J 4W .y
Name (Print C �(Z
name)
/7 S
Title (Prin title)
'7-z3—rs—
n r (Qa
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BOL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format,_"<XX mg/L" where XX is the numerical value of the detection
Iinnift, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text.
Part B: vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?Z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar 0&G/TPHby
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART AAND PARTS MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQCentral Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons direly responsible for gathering the information, the -InfOriYiation Submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aw�re thare are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
/ ,, ( na r of Permittee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03 0 15 4 3 SAMPLE COLLECTION YEAR Zo15
FACILITY NAME UyL- ` SAMPLE PERIOD EJan-June ElJuly-Dec
COUNTY 9S4000mIa& (Dv,-k)4 or Monthly' _ (month)
PERSON COLLECTING SAMPLES �ow—, —, pjC�ocU DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout ❑PNA
LABORATORY ' Lab Cert. # ❑Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: ®Other _ OaSS C_
Part A: Stormwater Benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
No discharge this period?
Oiicraii No.
Date
Date Sample
(mo/dd/yr)
24 hour rainfall
amount,
Inches3
Total Suspended Solids
pD
Standard units
Copper
Lead
Zinc
Non -Polar 11&Gj
Total Petroleum
hydrocarbons
Total Toxic
Organicss
Benchmarks =__>
_
100 mg/L or 50 mg/O
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
00(0
d0
1 Mont_hly sampling (Instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subiect to the requirement to sample (for metal finishing use the definition as found ,n 40 CFR 433.11' for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page Iof3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this_DMR including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
am a thatthere are significant penalties for submitting false information, includingthe possibility offines and imprisonment for knowing violations."
nat Perrt1ctie (Date)
Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
J //a cr/ryt.r
Name (Print name)
-e i4_r 2,
Title (Pri ttitl
-��-zs-
ign re) te)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX me/L where xx is the numerical ,value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n No discharge this period
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inche2
Non-polarO&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. N00030000
Date submitted ff) l 7�l
CERTIFICATE OF COVERAGE NO. N0003 0 S 4 _ SAMPLE COLLECTION YEAR 2ol+
FACILITY NAME yll5cn- �A6i6wiSAMPLE PERIOD ❑ Jan -June ❑X July -Dec
COUNTY Sunwoln►x¢ co"'41y or ❑ Monthly' (month)
PERSON COLLECTING SAMPLES 2&niaxin AiSS ;'In DISCHARGING TO.CLASS ❑ORW ❑HQW (:]Trout❑PNA
LABORATORY 1'oL Am•l }i l Lab Cert. q 40 &N& -4u1- ❑Zero -flow [7]water Supply ❑SA
-� rvl _,_-
Comments on sample collection or analysis: RECEIVED
CEIiVED Lpwulel
fl OCT 3 0 201144LJ PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
Part A: Stormwater Benchmarks and Monitoring Results CENTRAL FILES
DWR SECTION ❑ No discharge this period:
Outfall No.
Date Sample
Collected
(mo/dd/yr)
24-hour rainfall I
Total Suspended Solids
amount,
Inches"
pH,
Standard units
Coppe?l
Lead
�
Zinc
ivon-Poiar ~31
Total Petroleum
Hydrocarbons
Organics Total Toxic
5
/
Benchmarks =__>
100 mg/L or 50 mg/0
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
xmg/L
DO(
10 03 If
0.4
14.E L
6.5
o.00aSM
<O.00S
0.0
.4 S.n tr
�Ih
QD2
l0 03 144
0 4
< 7. 5
10•5
0.o0u, 2!.47L
<17.005
0.o211e
< 50 w L
nlh
O 3
10 03 14
0.
S. 8 _r t
b.5
p. 0051 "[Ll
0. OOZ& v
0. o9}4r
5.0 M v L
aA
004
10 03 1
o.¢
+ ,„ L
1a.5
D.0051 m L
1-0-OK1n
b-M n L
<5.o L
NA
005
l0 03 I
O.-t
100 wl JL_
Io
0.011.1 m (L
0. W5 ju
O.18? my[L
< 5.0 m.11L
^IA
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
ClJelt Guidelines IUI t1e 1[[1]UuLt to t1e requirement LU sample (IUIICLal finishing use t1e1nit Ul as IIIU I4U CFR 4JJ.11IUI Se11UUfUUllUrflIdl11l 1l1111 UIU!
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufactureusethe definition found in 40 CFR 469.31).
- (51 ut�o�ecT Srri,�ltp gfa+Q (( uIkIK�`r�f/q, Ce`kilet-' -Prowl �f of L o o� rzin(_ `ov 1 CoF�, �tl 'to oL WiGf ►�CC_IJd
1ioNl GN� � Ai7;L( tra ItlVlY� ✓1�w1GR�fC ?PXMI12 d0rF�,,JL;T &jf� �iIl al Gy ,Y_ COMPWI 51 ll( r!
J / �1
rian� Tav�l�ru T, ?.l n1�4
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature)
(Date)
Note: Results must be reported in numerical format. Do not resort Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the, format, "<XX ms/L'. where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: 1/ vnu renort a camnle value In PvcPC of the benchmark you mutt imnl--t Ti- 7 Tier 7 nr Tier :1 romance CPP ronernl D-H fnvf
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3
Page ��

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART AND PARTS MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES U NO U
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal and one coov of this DMR, includina all "No Discharae" reports, within 30 dovs of receipt of the lab results (or at end of monitorina period
in the case of "No Discharoe" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
/a_7.r-�Y
of Permittee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/2512012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Dare suti.. med
CERTIFICATE OF COVERAGE NO. N0003 0 5 -or 3
FACILITY NAME lLnison - i�slnev Mac
COUNTY 6w4(A."4 Coo-{�
PERSON COLLECTING SAMPLES �u1�aK i. t E ;sbt44, _
LABORATORY ?acew, AA iCOA Lab Cert. ii 40 wA -1l'12
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2o14
SAMPLE PERIOD ❑ Jan -June ® July -Dec
or []Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow [:]Watersupply [:]SA
Other Class Cr
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -)
❑ No dischorge this period?z
Outfall No.
Date Sample
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
�'
Copper
Lead
�y
pt
Zinc
Non-PolarO&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks =__>
-
100 mg/L or 50 mg/L°
6.0 - 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
l0 03 1
D•4
11.3 L
(,•5
o.00u, r
401.005'm C
0.4
< 5.0.n L
N4
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
"See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469..31). r (�
- S`uI6`c�s,:. sikc. 9rani� v kla�or'� ceA;tP � m� Bx`C1cec�_avtes ol- eivi(_ orcope-1 S�oiuf (1 i,� oL �e- V- lecf-lveA t �w+h
IVt-V R 5 Xb3,� A '1 Pm5 l rr1 U�+�rOr leiw,'�' �¢5� }af ui�cCinf[I �¢� 2t qi_W i& g;,it, &04WR I _D".
.49IM i QCX>7LIO� 2I J Z011T
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(70), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature)
(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results arebelow 'he applicable limits, they be reported in format. —vIIF-I1.411• Vhere vIv Is the numerical value of tI�IC detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n No discharge this period?2
Outfall No.
Date Sample
1
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS;
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES U NO U
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, includina all "No Discharge" reports. within 30 days of receipt of the lob results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am awar that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations,"
AO Z3—iy
of Permittee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03_Q_ a 4 3 SAMPLE COLLECTION YEAR 20 *
FACILITY NAME 11%Apn A,,wvika SAMPLE PERIOD ® Jan -June ❑ July -Dec
COUNTY :RtA Lj)y 6_ (&&Wj or ❑ Monthly' (month)
PERSON COLLECTING SAMPLES 8Gn' II`Si7c,I{, DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout❑PNA
�avw�n. I
LABORATORY QOkU ikne b(A Lab Cert. # 410 and 12��- �� ® [:]Zero -flow ❑Watersupply ❑SA
Comments on sample collection or analysis: Butner Uas'3 k.
JUL 1 S 2014
CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
Part A: Stormwater Benchmarks and Monitoring Results DWOtBOG
❑ No discharge this period:
Outfall No.
Date Sample
,
Collected
{mo/dd/vrl
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Copper
Lead
�
Zinc
Non -Polar 0&G/
Total Petroleum
Hydrocarbons
OrganicsTotal Toxic
s
Benchmarks =__>
_
100 mg/L or 50 mg/L4
6.0 — 9.0
0,007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
DO(0
oco 0 14
D-Z6
38.5 rn 1_
(0,5
0.00b1 M
'0.00 L
0.254YM
< 5-0 It,
K
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition
++found in 40 CFR 469.31).
- �JubjCU 5+ 9CaY+�ed fequ�Ua��lvrY �e�ia UcCee�awc¢o dirt(, ow� Go>;pur I StuTW' iny�a (t{(c1.r (pG�i�cci
tom �c��K �b-o 4C N�S 4D(rrtQ4tf �( Win : kL%&s fVre�wv� ?Wi� U050n Gvl irte '1.0ap 5, �c..
do1e4 SaAuary 21 ZD14 J
Permit Date: 11/1/2012-10/31/2017 I SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
No discharge this period?z
Outfall No.
Date Sample
Collected,
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar 0&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =_=>
15 mg/L
100 mg/L or 50 mg/L*
6.0 —9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Dane 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES HAVE YOU CONTACTED THE DWQ REGIONAL OFFICF? YES ❑I NA ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal and one copv of this DMR, includina all "No Discharge" reports. within 30 dovs of receiat of the tab results for at end of monitorina period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly Rather and evaluate the information submitted. Based on my inauiry of the person or persons who manaee the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware�t t ere are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
I e Permittee) (Date)
Permit Date:11/1/2012-10/31/2017 SWU-24S, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03_ A 3 SAMPLE COLLECTION YEAR Z o 1't
FACILITY NAME rliSO - &KCV14 SAMPLE PERIOD ® Jan -June ❑ July -Dec
COUNTY (71Ah(0 YVl10J? CGyn i1/ or I ] ne..nthl. 1
r ou i, ii,)
PERSON COLLECTING SAMPLES DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY ca. n.i Lab Cert. # 40 oAd 412. ❑Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: ®Other G 1455 G
Part A: Stormwater Benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?'
Date Sample
24-hour rainfall
pH,
Non -Polar O&G/
Total Toxic
Outfall No.
Collected'
amount,
Total Suspended Solids
Standard units
Copper�'
Lead
Zinc�
Total Petroleum
Organicss
(mo/dd/yr)
Inches3
Hydrocarbons
Benchmarks =__>
100 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
0o 1
0[0 10 14
0-25
b9.0 on&
(,.5
0, 0139 !!Jkl
0.00Yt L
O.1Mp L
I < 5.0 1- t�
14 A
2 1 _ Ir
/_ C"
A An, ___ h
yr
e n nnc__ 1,
v.vv1
n Y1na __ 1,
V.+
{ c.. __- /
•v • 1V
1 A
NI1
003
O(o 0 (.
0.25
(0.0
(0.5
0.00
<0.005
0.04
< 5.0
NA
0 04
Oro 10 14
0.25
'l . 0 4/
I, •
o. o /L.
<0.005
0.
< 5.0 it
WA
OD
o la [
o•25
130 h, L
(a h`
0.0125 (,
< O.Ib5 L.
0.215 L
< 5.0 L
NA
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for a same pa meter at the ame outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic Crystals, or rrlanufacture cathode ray tubes. For purposes of this permit the definition OT'I Otal'1 Oxlc Organics Is that definition contained In the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Si}e �f (gnu,�&{nry vclif� lP"*% eK(_e1ia+ cza 6► ZiAC, 04 CDFre'r, S�o �ca in o �c (r fteiJ,�
��� �c� r1� SubJJc c t lt� tc t�PD�S S�wmubiku Pc& : Kggttxt4jkvr K83 4,}o RG1ie ur,,&n &1irlt ctm pW 4S ,-,T . 3r
G10ti}u� �'aat�y 2l[ 201�¢
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2D12
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature)
(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
No discharge this period?'
Outfall No.
Date Sample
Collected,
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A RFNf HMA.R.K. F.X.CFFD.A.NCF TRIf;GFR$ TIFR 1 RFnUIRFMFNTS, SFF PFRMLT PART LI. SECTION R_
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME'
Mail an on inaf and one copy of this DmR including ali ",No Discharge- reports, within 30 days of receipt of the lab results or at end of monitoring eriod
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
am aware��h t t ere are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
I e Permittee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03-L
FACILITY NAME UMiSoA A6k&villa
COUNTY &VJw MlaP_ i y All
PERSON COLLECTING SAMPLES RLa�wuA /JiSI]I
LABORATORY && h-k.1viic.1 'Lab Cert. # 40 awd -#12-
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR Zpt9'
SAMPLE PERIOD M Jan -June ❑ July -Dec
r-I we-. -1 '---�--'-
RECE�y ��°° ur L_I rvronuuy rhrUnuri
� �❑ORW ❑HQW ❑Trout ❑PNA DISCHARGING TO CLASS
JUL 1$ 2014 ❑Zero -flow [:]WaterSupply ❑SA
®Other ClaS5 G
CENTRAL FILES
DWQ/BOG PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?'
Outfall No.
Date Sample
Collected)
(mo/dd/yr)
24-hour rainfall
amount,
Inches;
Total Suspended Solids
pH
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organicss
Benchmarks =__>
_
100 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
001
14
0. Z6
f09.0 Auli,
1,.5
p. o l39 fi.
0.OM L
0.144, wAIL
< 5.0 - L
4 A
001-
3.1 M 1.
• 5
0. 002
<0.005
0.01i3
< 6.0 It.
03
Ofo 11 o (
D• 25
(0.0
6.5
0.00 51 it.
<0.005 vft IL
0•044
< 5.0
t4A
O04
OG o 1+
0.15
¢ 0 /
0,D L
<0-OK
0.
< S.o L
t-JA
OD
ow to I
o•25
130 L
�•ti
0.D145 L
<0.00r L
0.243 L
<5•o t
NA
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same pArneter at the%me outfall.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
"See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Af- Ste, U, 1, fa►n(eG� (F�u��roi Y rca�e� �oY►. efcc.�ounuo �'
_�IfoM_ Nc. ew, sulp bl�,A C',4mSS�wmu�oti7X YUMi# f� es� ko�
da�ed �a��y 2ll 201�
Permit Date:11/1/2012-10/31/2017
Vvi c 04 co f fc+r, 4. W i n a (c.}+ir vlP_eiVc.
Kegv�iCL{0�/ 1(tlic i ni5a► LA ;wG Wcork
SWU-245, last revised 10/25/2012
Page 1 of 3

r
_'i.r ,. ,. !1. - � .. � !�•`3. .. I � fir„ r.j�: r'� t-tom ... 1 ". .. e� v •
Z

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
• _t
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management ent pl-... included h the SLor.. Owat..r n..I1. �F:.... n..........:.... nI. u
n�ivcn� inai agc uo,t plan uiu uucu ui uic aw�niwa�o rvuu uu,i ri cvoiuui, rian.
Name (Print name)
Title (Print title)
(Signature)
(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format When results are below the ❑nnlir-able limits the- must he reported in the format -evv m /I —hore YY is the ni imeri—I value of+he
limit, reporting limit, etc. in mg/L.
hfntpr tf unu rpnnrt n cmmnlP unlup in pyrpcc of the hpnrhmnrir. vnu mutt imnlpmpnt Tipp 1 _ Tior 2. nr Tipp 9 rpcnnncpc Coo Rpnorni Aprmit fort
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?Z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches;
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks = ->
_
15 mg/L
100 mg/L or 50 mg/t*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Nate:. If. you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART 8 MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including oil "No Discharge" reports, within 30 days of receipt of the tab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aw re that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
u Per ttee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Dawn 3 of 3

AA
FAa
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance onfilling out thisform, please visit,
Permit No.: N/C/_/_/_/_/_/_/_/ or Certificate of Coverage No.: N/C/G/_0_/ j/ ems/
Facility Name: ((oison- AskGviIU
County: SIA11 LOM b4 �K.�F Phone No.
Inspector: 'geNFamir, tJ,',cUq
Date of Inspection: _ (z /io bl
Time of Inspection: l t 2 D
Total Event Precipitation (inches): p. 2 in e6l
(828) 244 - 4S¢o
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
® Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" -or "meosureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary, Most permits require qualitative monitoring to be
Pei -formed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
f
i A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
i 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
1 obtains approval from the local DWQ Regional Office.
By this,6 nature, I cf�ytify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
Pagel of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No. 001 Structure (pipe, ditch, etc.) PlFc. _
Receiving Stream:, Mcd 4';L{'X 6 5u&fi' Crccic _
Describe the industrial activities that occur' within the outfall drainage area: j
SIL 3 7'7ZA 41,cr444 E✓�dr`-1L GLSQ ✓tR7 �14 �a/?i l%1G1h Ct GYLf �f �C
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Glcar - tl (otor
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): No Ddo,
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids:
D 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and S is extremely muddy,
1� 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

NCDENR
Stormwater Discharge Outfall (SDO)-
Qualitative Monitoring Report
For guidance on filling out this form, please visit: http://portal.ncdenl-.org/web/wq/ws/su/nodessw#tab-4
Permit No.. N/C/_/_/_/`/_/�// or Certificate of Coverage No.:
Facility Name: idols.,- Asktvilke-
County: tSuocowilu �Phone No. (szS) ?74- 4Sfo
Inspector, '6..7a.i^
Date of Inspection: l�
Time of Inspection:
)2-
Total Event Precipitation (inches): 0. 2- inches
Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
❑ Yes E] No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "rneasureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
son -le pef itiiis uu iioi have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
' and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
13y this signature, i certify that this report is accurate and complete to the best of my knowledge:
Permittee or Designee)
Page t of 2
5wU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No. 00'1- Structure (pipe, ditch, etc.)
Receiving Stream: (.AV,-nam,?A :fri6,4-q 1a �e.,r, (.Hea(s
Describe the industrial activities that occur within the outfall drainage area:
SlL 374� �i�Gra E7,qIAr4jyYlav,tti c',c to ,.
2. Color: Describe the color of the discharge using basic colors (1 ed; hr nwn; blue, etc.) and tint
(light, medium, dark} as descriptors: i D Flown_
3. Odor: Describe anv distinct odors that the discharge mail have r; P ells strongly o fo;,
o- .l l'...., smell.- ng�y vu,
weak chlorine odor, etc.): o,,)
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4
7. Is there any foam in the stormwater discharge? Yes No
A. Is there an o:l ylRenn in th t.... d- ..1...rg i
�:e o yr mvva�u u�a�iigl �C. I CS !Vo
9. Is there evidence of erosion or deposition at the outfall? Yes No
10, Other Obvious Indicators of Stormwater Pollution:
List and describe o V�oc�J r'� a S (( cot.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
inlay be Indicative of Pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/M12

�Ilh
A&I
ji j
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Dui �,�[ 003
For guidaoce on filling out this farm, please visit. httg://portal.ncdenr,org/w�, rg/w�,U./wq./ws/"su/npdesswhtab-4
Permit No.: N/C/_/�/_/_/ _/�/_/ or Certificate of Coverage No.:
Facility Name: U4;3" - A t.-
County: _�uNLyvsn ��y._ Phone No. i8a$) 2-14- 45¢u
Inspector:
Date of Inspection: l2
Time of Inspection:
12,
0
Total Event Precipitation (inches): 0- -2 it c( t.S
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
® Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary; depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some pernnits u'O irui nave this requirement.rlease refer to these definitions, it applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By thiX,b`XVature„ Certify that this report is accurate and complete to the best of my knowledge:
ermittee or Designee)
Page 1 of 2
SWU-242, Lastmodited 10/25/2012

1. Outfall Description:
Outfall No. 003 Structure (pipe, ditch, etc.) l&e-
Receiving Stream: Utz L (XaA< _
Describe the industrial activities that occur within the outfall drainage area:
41,traf4 Encs!nc
2. Color: Describe the color of the discharge using hasic colors frari, hrown, blue, etc,, and tint
(light, medium, dark) as descriptors: Vicar-o
3. Odor: Descrihe an distinct odors that the dischargbe „aJt, have ,smale1.3Os- strongly Of oil,
weak chlorine odor, etc.): tL Odor
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
9 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy.
U 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes
a... 1.] cilc! c c!!! V�.1 .]11CCi1 11! ills Stul litwatei u1sLlsaFge % if es INV
9. Is there evidence of erosion or deposition at the outfall? Yes N
10, Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

"AT.;
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
ou�c.�( Odd- _.
Forguidance on ftlling out this form, please visit: htt�:f f portal,ncdenr.org/web/wq/ws/su npdessw#tab-4
Permit No.: N/C/_/`/_/ _/_/ `/_/ or Certificate of Coverage No.:
Facility Name: A
County: Co..HII Phone No. (_92s) 244- 4Sfo
Inspector: 'Ben�vnan ry�5�t
Date of Inspection: 12
Time of Inspection:
11
Total Event Precipitation (inches): d' 2- i,40
Was this a "Representative Storm Event" or "Measureahle Storm Event" as defined by the permit?
(See information below.)
© Yes ❑ No
Please verify whether Qualitative Monitoring must he performed during a "representative storm
event" or "measureahle storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureahle storm event." However,
some permits do not have this requirement. Please
refer
to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
(),I inrheg has occu..r a h S
emu. � sn;g�C s�o� r�� event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DW(
al Office.
By this 00h tore, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
Page 1 of 2
SWU-242, Last modified 10/29/2012

1. Outfall Description:
Outfall No. QJ Structure (pipe, ditch, etc.) '&C
Receiving Stream: _ cf tek
Describe the industrial activities that occur within the outfall drainage area:
S1L 37a A4/Cr4L E✓IdI�nG c;nd EovyAr- 1ckr41 M&Ah kA.& --
2. Color: Describe the color of the discharge using basic colors (red; brnwn, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe anv distinct odors that the discharge may have RP [mane strongly f oil,
weak chlorine odor, etc.):. 0,
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 3 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
i 2 J UV
a
7. Is there any foam in the stormwater discharge? Yes
R; is there a.1 oil s::een 4- tiie StDr ilV✓at%r discharge? YeS iI�VU!
9. Is there evidence of erosion or deposition at the outfall? Yes C3
10. Other Obvious indicators of Storrnwater Pollution:
List and describe �� i eon o S rmWa , u '�,,� Vlo+ cv;
o 6e-Le" I ( r5 r
`
,n�PPW,o J [i..so., of slid. aAA o- dD_rxrl�r� o rlcwr�l-v.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
rimy be Indicative of poiiutant exposure, These conditions warrant further investigation.
Page 2 of 2
5wU-242, Last modified 10/25/2012

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
maybe waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible forma naging compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics Into the stormwater or areas which are exposed to rainfall or
stormwate r runoff has nrrurred Since tiling the last discharge monitoring report. 1 further ceirtlfytthcit this facility is inipie meming the ail the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Titl rinttitle
�-- 9 �3
atu (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
fumiat. When results are below the applicable iimits, they, must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note; Ifyou report a Sample Value in c_w-CeSS f .08 benchmark, you must implement Tier i, Tier z, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results_: only for facilities averaging > 55 gal of new oil per month.
No discharge this period:
Outfall No.
Date Sample
collected'
(mo/dd/yr)
24-hour rainfall
amount,
inches;
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =_=>
_
15 mg/L
100 mg/L or 50 mg/L;
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* see General Permit text, Takla S identif,/Ing the especially sensitive receiving water classifications where Tile more protective benchmark a lies. ,,,,6 ...,r�..o��r e A Pp
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART Il SECTION B.
• TIER-4- HAS YOI IR FAC! UTY HAD n OR MCRE BENCHMARK EXC..EEDENCES FOR THE PARAM, �r.rvi` M"" RAiviETER AT ANYONE Ull I LACE+ YES ❑ NO LJ
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME'.
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end ofmonitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attw DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
„gyre that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware-t—hat there are signifjt penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations-"
(Signa Permittee (-Dattee)—) -�
Permit Date: 11/1%2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for Forth Carolina Division of Water Quality General Permit No. NCG030000
Date submitted I - og 2-13
CERTIFICATE OF COVERAGE No. NCG03 v 5 4 3 SAMPLE COLLECTION YEAR Zv 12-
FACILITY NAME SAMPLE PERIOD ❑Jan -June ©July -Dec
COUNTY 1�twil ppnl�2 �o why � or ❑ Monthly' (month)
PERSON COLLECTING SAMPLES i3e�n nwv NiSDt DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA
LABORATORY k, Lab Cert. # 4o once -tt 1'Z []Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: ❑X Other GIA55 C-
Part A: Stormwater Benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
l vI No discharge this period-? 002
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organicss
Benchmarks =__>
100 mg/L or 5o mg/L°
6.0 -- 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
OQ(0
(z to I2
0.2
a•oos L
40.005 L
0.op2 <
< 5.0 �L
�f}
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3 The total precipitation rust be recorded using data from an on -site raingauge. Unattended sites may be eligible for a waiver ofthe rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode rav tubes, For per
mit ses o nlirpof this pit the definition of Total Toxic Organics that definition d `, he - - - - 1 contained t'Pllletl , 1 tI1C CPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit tent.
FOR PART AND PART B MONITORING RESULTS'
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART q SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALLTRIGGERTIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FAClLITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME: - -
Mail an original and one coPy Of this DMR including all "No Discharge' re orts within 30 da s of receipt of the lab results or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
or
g u of Permittee) (Date)
Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/2S/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted � -0� - Toil
CERTIFICATE OF COVERAGE NO. N0003 0 5 -4 3
FACILITY NAME uvli5on - 'Asi h
COUNTY 'r)1 WlcAw10.t. (.ouhiv I
PERSON COLLECTING SAMPLES Sehawii� tJ15be�1
LABORATORY Ypc - kylal�ab ert. # 40 &n4 16 fZ
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR x 0 12-
SAMPLE PERIOD ❑ Jan -June X❑ July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply [:]SA
©Other Class C.
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
[? No discharge this period:2 DLL Q
002
Non-Polar O&G/
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark ezceedance for Ne same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3 I IIC total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
e1 ectron is _!ysta is or man ufa ctu, re oath vde ray ubcs, Foi pur poses of this permit the deliniti on of Tuta1 Toxic 0r ga rl ics 15 LF]dL de fl n itian co nta lned m the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22, and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
jn
rint title)re (Date)
Note: Results must be reported in numerical format. Do not t report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format,"<XX me/L where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. .
U No discharge this period?z
Outfall No.
Date Sample
Collected
(mo/dd/yr)
24-hour rainfall
Inches'
;von -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Senchmorks ===>
_
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
`See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-1D/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

NCDENR
Stormwater Discharge Outfail (SDO)
Qualitative Monitoring Report
Forguidanceonfrllingoutthisform,pleasevisit; http�{/flosta].ncdenr.o�/wehjwtws/suJnndessw#tab-4
Permit No.: N/C/ /_/4 /_/^/ /_/ or Certificate of Coverage No.:
Facility Name: U,1i3 - AslicviIU_
County: l a.ncom 4 Co nr2i- Phone No. (82 $) 21-4 - 4 Soo
Inspector: be-11ckm n lJis
Date of Inspection (2 toy
Time of Inspection: _ 113
11
Total Event Precipitation (inches): 0• -- iArl�eI
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
W Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some perrriits do not have thhis requirernerlL. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has.occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted slit uutfail. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this sigr)ture, I cer� that this report is accurate and complete to the best of my knowledge:
(Sig .41VIf Permittee or Designee)
Page I of 2
SWU-242. Ldh-L mudified 10/25/2012

1.. Outfall Description:
outfall No. 00; Structure (pi e, ditch, etc.) ?i
Receiving Streami,: _ o-dlameA -1-ri ;-a �ocAc l.Cccl�
Describe the industrialactivitiesthat occur within the outfall drainage area: !� 1
4i Ai,cr44 cmd Enallie- Pajj �ANL•+rnGf{�Srr�sc.61
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: CSC r
3. Odor: Describe anv distinct odors that the discharge may have
o- J •. r�;,.e...,osturvng,y of Jit
,
weak chlorine odor, etc.): �o Odor
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 3 4 5
5. Flnating Cniidc: Choose the number which bedescribescn 3]St � the c aiiioii[it of oaLing SOl]d5 In
the stormwater discharge, where 1. is no solids and 5 is the surface covered with floating solids:
LJ - 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
i.
F
Vol
1 A]1
1 Ic.f J
Is there any foam in the stormwater discharge?
4 5
Yes .
Is there an oil sheen in the stormwater discharge? ' Yes o
Is there evidence of erosion or deposition at the outfall? Yes 0
io, 0 t h e r 0b-1,-. mus Inuicator s o'If Stor mitwater 1'ol'lution:
List and describe _
Dote: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
.,WI,11-242, L aslmouijfieu' 100/255/2012

{
NCDENR
Stormwater Discharge 4utfall (SDO)
Qualitative Monitoring Report
04�y ob (, -
For gitidance on filling out this form, please visit: httl2://i3ortal.ncdeor.org/web/wq /wsJ�u%npdessw#tab-4
Permit No.: �I/C/_//`/_/_/_/_/ or Certificate of Coverage No.: N/C/G/.o/
Facility Name: Upliso - A (G
County: CoK Phone No. ( 926 ) Z44 - 45-¢o
Inspector: --be"'Ic
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches): 0. 2- f-tips
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to he
performed during a "representative storm event" or during a "rrieasureable storm event." However,
somme permits do not have this requh-ti7itnt. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 01 inches of rainfall
and that is -preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.� inches has accursed. A single siorrn event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this sign# ire, I certify that this report is accurate and complete to the best of my knowledge:
(SignaWejif/ern ee or Designee)
Page 1 of 2
SWU-242, Last modified 10/25/2012

1. dutfallDescription:
Outfall No. _QQ(o . Structure (pipe, ditch, etc.) h"o&�
Receiving Stream: _ l�Jee ev, (LI4: _
Describe the industrial activities that occur within the outtfall drainage area:
S 3 rG 4,crR EoLe,GLt G✓t f G �QrT !/i�ANLL G
67
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: 04-,- - t�o CeLd
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly nfnil,
weak chlorine odor, etc.): rJo Odor
4, Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 Q 3 4 5
5. Floating Solids: Choose the number which best describes the amount of Floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 3 4 5
5. Suspended Solids: Choose the numberwhich best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
109
1 r 3
Is there any foant in the stormwater discharge?
e.
Yes
IS there an nil sheen in the Sterrnwater diSc arge? Yus iU
Is there evidence of erosion or deposition at the outfall? Yes f�o
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
-,,y be i n-1icatiVe of pollutant exposui e. 1 iiese conditions warrant further investigation.
Page 2 of 2
Swll-242, Last modified 10/25/2012

me® .10
MWMAE"
BUNNELL-LAMMONS ENGINEERING, INC,
GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS
January 8, 2014
NCDENR
Asheville Regional Office
Division of Energy, Mineral, and Land Resources - Land Quality Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Attention: Ms. Laura Herbert
Land Quality Supervisor
JAIL 1 4 2014
Rand Quality Secticm
Asheville
Subject: Request for Regulatory Relief from Tier 2 and 3 Response for Copper & 'Line
Unison Engine Components
Sweeten Creek Industrial Park; Asheville, North Carolina 28803
Certificate of Coverage NCG030543
ivruiJS atormrvaier ixenerai Permit ivC%03"u"u00
Dear Ms. Herbert:
On behalf of Unison Engine Components (Unison), Bunnell-Lainmons Engineering, Inc. (BLE) has
prepared this letter as requested by Mr. Jonathan Stepp of your office. The purpose of this letter to review
and summarize prior assessment findings, to document the November 2013 stonnwater sampling results
from the subject facility, to document materials stored at the facility, and to request regulatory relief from
the Tier Two and Tier Three response requirements for copper and zinc.
As you are aware, BLE prepared a report titled Report of Special Storms ater Sampling Ewnt — April 19,
2013 dated May 23, 2013, The report was submitted to Mr. Tim Fox of the NCDENR Division of Water
Quality (DWQ). The report documented the exceedence of copper and zinc benchmark values in the
facility stonrlwater and identified naturally occurring metals in parking lot sediments as the probable
source. A manufacturing -related source of copper and/or zinc was not identified. Regulatory relief from
the required tiered response for copper and zinc was requested for the subject facility. On November 5,
2013, BLE received an email from Mr. Stepp which indicated that NCDENR was evaluating the copper
and zinc issue that that Unison should continue to sample and report results following the required tiered
response actions.
On November 26, 2013, BLE performed the second semi-annual stormwater sampling event at the subject
site as required by the facility permit. The results indicated that concentrations of zinc exceeded the
benchmark value at 3 of the 6 sampling locations (Figures 1 & 2 -- Outfalls 004, 005, & 006). As
required by the permit,- BLE-and -Unison-conducted- a- Tier, One,inspection-on-Decei-nber-30,-2013. The
Tier One inspect`hon`fo�and-laboratory-data-are included -in Appendix A: The Ti�-One-inspec_ ti n
conanned i'n`at no manufacturing -related sources of zinc were identified and that the most probable source
of the zinc was from naturally occurring sediments. ~�
The exceedence of zinc benclunark value in November 2013 represents the second exceedence for Outfalls
Md fin; ,Q. nr)A ,;,,A F.Ar.6...a�w.n-tf�llc T.I..P
.. t.....-- ... 1— 11..... .,n �Psp.nsP!,r--..
.
6004
PONDERS COURT PHONE [phone]
GREENVILLE, SOUTH CAROLINA 29615 FAX (864) 288A430

KILLS
Unison Engine Components January 8, 2014
BLE Project No. J14-1009-73 Request for Regulatory Relief from Tier 2 and 3 Response for Copper & Zinc
Tier Two response requires monthly analytical and qualitative monitoring for all parameters at each
offending outfatl.
As -previously stated, the concentrations of copper and zinc detected at the facility�do not_appear_to-be
(related,to a� ufacturing-sourcei We understand that NCDENR requested a manufacturing material
inventory for the subjecvfacihty: A -copy of Table 2 Material Inventory (updated 10/16/2012) is included
in Appendix B for reference. The table is sourced from the facility SPPP dated May 30, 2013.
The laboratory data collected to date suggest that the most -likely primary source of detected copper and
zinc appear -to -be •naturally occurring men sedits inn s6ils-and'on-pavetnents•at-the•facilityI It is our opinion
that the Tier -Two requirements for monthly monitoring,places-an-undue -financial-hurden•on permit holders
and that any additional monitoring data will not solve the issue of naturally occurring metals in sediments.
We request that the NCDENR suspend the requirement for Tier 2 and 3 response actions for copper and
zinc benchmark exceedances at the subject site (Certificate of Coverage NCG030543).
We look forward to working with NCDENR on this issue. If you have any questions or connnents please
contact us at [phone]. We respectfully request an expedited response.
Sincerely,
BUNNELL-LAr iMONs ENGINEERING, INC.
v 1/t/
Andrew W. Alex �P,,
Senior Hvdro�!eolodst
Registered, North Carolina # 1475
cc: C2Jeff Bowman — Unison
P. N sbeth, P.G.
Staff Geologist
Registered, North Carolina #2134
Attachments: Figure 1 — Site Location Map
Figure 2 — Stonnwater Sewer Plan
Appendix A —Tier One Inspection and Laboratory Data
Appendix B — Table 2 — Material Inventory
c:tawa�active projectsluuison smiths nci\phasc73 stormwater 2O!411e1ter to dwq concerning teir 2 atier nov 2013 sarnpling
eventltinal unison stcmnwater nov 2013 event request 1009-73.doc
,tSy111111ff!!!!!
'�1l11111t1tWt

J
f
� •1C
�II 7
rI
i
y
• I e Ltd •�- � - I `�� = • �• �`•. �.
q r.;
c• • • „e jr._ J
• ' .� . • . Cam` - . � I '� f r
a ' • '> � , � as `. . �1 „ /-; 1� o �j
�� , •• r •_ ,' �� fit, u � � �
�� • +- ' � �• fir. ,.. IF
Iv
� \ , • • o� .= _ �'+, . `-tee
�� �1� �•• OUTFALL 001: 35'32.914'N 82'31.143'W
OUTFALL 002: 3534.933'N 82'31.094'W
OUTFALL 003: 3532.825'N 82'30.964,W
OUTFALL 004: 35'32.743 N 82'30.992 W
r, '-� �• i OUTFALL 005: 35'32.885'N 82'31.177'W
OUTFALL 006: 3532.826'N 82'30.968'W
�* II 1' 1 RECEIVING WATER: SWEETEN CREEK
NOT IMPAIRED [303(d)]
NO TMDL ESTABLISHED
2000 1000 0 2000 4000 REFERENCE:
USGS TOPOGRAPHIC MAP, 7.5 MINUTE SERIES,
APPROXIMATE SCALE IN FEET ASHEVILLE , N.C. QUADRANGLE, PHOTOREVISED 1991,
DRAWN: ACE DATE' 05-31-13
SITE LOCATION MAR IBLEWL FIGURE
CHECKED: CAD: UNISON ENGINE COMPONENTS
AWA UNISON65-SLM L{AIyONI llffissmaNA, W. SWE£NTEN CREEK INDUSTRIAL PARK ROAD
APPR6004 PONDERS OWRT
ASHEMLLE, NORTH CAROLINA
PHONE
;(64SOUh1 CARoA 6sJ13-1009-65 -1265 FAX: (8642-"30

0
0

INsrECI ]ON FORM
Date_
December 30, 2013
Time,
0900-1000
Inspector:
Ben MOO,, PG
Weather Conditions:
Clearl40"F-42*F
Purpose:
Housekeeping
Waste Storage
AST
Storm Water Stmdures
Comabrmcnt Sui ctme
Foe PNe entwr, Ephipoent
Spill Res...se Earm n nt
,Tier One Ins, ectim. eficr the N., ml— 26. 21113 Na m1ding R. rnr
hem
Observation audlar Problems Noted
Corrective Action Needed
pro used Com Ietion Date
Surveu' of Outfalls 004, 005 and 006 including the
FILE represrntative observed the drainage areas for each oulfall. Inlet for Outfall 005 was
drainage areas of each outfall arc..
observed to have a rubber mat covering the artire inlet.
Rubber mat removed
Complete on 12.30-13
FILE r presentative observed the drainage areas Ibr mrarnial sources of Zinc.
Thr ddeded concentrations ofZine are naturally occurring and are derived
derived
ncesen
Manufacluring-related d sources ofZ.ine on the Unison properp could not be idendRed_
from sediments in the parking lots. No corrective action is
Outf lls 004, 005, and 006 (Exceedettee of Zinc)
Each drainage area includes significant areas ofpaved parking. Parking areas have been
The -N needs to revise the permit benchmark values fin Zinc and
Complete on 12-30-13
shown to contain de minions amounts ofsedirnems which are the sources of Zinc (and
Capper as discussed in the April 2013 rcp.n cited below.
Copper as
Copper 1.
Note. Report of Special Stnrmwntet Sampling Event — April 19, 2013 was submitied to NCDENR on May 28, 2013. This suppk"ental report
contains discussion of total vs. dissolved metals (copper and zinc) at sevaal sampling
locations including compliance and
additional non-compliance locations,
UNISON REPRESENTATIVES SIGNATURE
Date.
! ......
12/30/2013
OLLi RI:E'RLSF.NTATIVIfS SIGNAT UR]S
'
Doe,
Table 11 urtlia—'r- 0eae Sc—� F.—D,0013. vlr
ID

1�;a'ceAnalyfical'
www.pacelans.com
December 18, 2013
Mr. Andy Alexander
Bunnell-Lammons Engineering
6004 Ponders Court
Greenville, SC 29615
ce Analytical Services, Inc.
., East Meadow Road - Suite A
Eden, NC 27288
(336 )623-8921
RE: Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Dear Mr. Alexander:
Pace Analytic, :es, Inc.
22�, erside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 27, 2013.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
J w--- (D 0_-q
Tabitha M Dacal for
Tom Williams
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 17

ce Analytical Services, Inc. Pace Analytica as, Inc.
2ce,Malytical' East Meadow Road - Suite A 222c, erside Dr.
Eden, NC 27288 Asheville, NC 28804
wwwpecabb com [phone] [phone]
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
FloddalNELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia[VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiafVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 17

aceAnalytical
www.pacelabs.com
ce Analytical Services, Inc.
o East Meadow Road - Suite A
Eden, NC 2728B
[phone]
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Pace Analytica :es, Inc.
222- erside Dr.
Asheville, NC 28804
[phone]
SAMPLE SUMMARY
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92181242001
OUTFALL 001
Water
11/26/13 10:35
11/27/13 09:52
92181242002
OUTFALL 002
Water
11/26/13 10:30
11/27/13 09:52
92181242003
OUTFALL 003
Water
11/26/13 10:15
11/27/13 09:52
6.1242004
OUTFALL 004
Water
11,126/13 10:00
11!27113 09:52
92181242005
OUTFALL 005
Water
11/26/13 10:40
11/27/13 09,52
92181242006
OUTFALL 006
Water
11/26/13 10:20
11/27/13 09:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 17

leAnalytical "
www.pacelabseam
:e Analytical Services, Inc.
East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytica;as, Inc.
222, arside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HuntersvNe, NC 28078
[phone]
Project:
Pace Project No.:
Unison -Asheville Stormwater
92181242
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92181242001
OUTFALL 001
EPA1664B
CLW
1
PASI-C
EPA6010
SH1
3
PASI-A
SM 2540D
MDW
1
PASI-A
92181242002
OUTFALL 002
EPA 1664E
CLW
1
PASI-C
EPA6010
SH1
3
PASI-A
SM 2540D
MDW
1
PASI-A
92181242003
OUTFALL 003
EPA 1664B
CLW
1
PASI-C
EPA6010
SH1
3
PASI-A
SM 2540D
MDW
1
PASI-A
92181242004
OUTFALL 004
EPA 1664B
CLW
1
PASI-C
EPA6010
SH1
3
PASi-A
SM 2540D
MDW
1
PASI-A
92181242005
OUTFALL 005
EPA 1664E
CLW
1
PASI-C
EPA6010
SH1
3
PASI-A
SM 2540D
MDW
1
PASI-A
92181242006
OUTFALL 006
EPA 1664B
CLW
1
PASI-C
EPA6010
SH1
3
PASI-A
SM 2540D
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 17

aceAnalyiical
www.p9w abs.com
se Analytical Services, Inc.
East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytica' Les, Inc.
222:, erside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704 )875-9092
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Sample: OUTFALL 001
Lab ID: 92181242001 Collected:
11/26/13 10:35
Received: 11/27/13 09:52 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mglL 5.0
5.0 1
12/05/13 11:02
6010 MET ICP
Analytical Method: EPA6010 Preparation
Method: EPA3010
Copper
2.8J uglL 5.0
2.0 1
12/03/13 10:45
12/04/13 04:15
7440-50-8
Lead
5.0
4.0 1
12/03/13 10:45
12/04/13 04:15
7439-92-1
Zinc
41.1 uglL 10.0
5.0 1
12/03/13 10:45
12/04/13 04:15
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
18.3 mg/L 4.2
4.2 1
12/03/13 07:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/1812013 11:56 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 17

�55'ceAnalyfical_
mvw.paceiaas.Cam
ceAnalytical Services, Inc.
--,East Meadow Road -Suite A
Eden, NC 27288
[phone]
Project: Unison -Asheville Storrrtwater
Pace Project No.: 92181242
Pace Analytica :es, Inc.
222;, erside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: OUTFALL 002
Parameters
Lab ID: 92181242002 Collected:
Report
Results Units Limit
11/26/13 10:30
MDL DF
Received: 11/27/13 09:52 Matrix: Water
Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mg/L 5.0
5.0 1
12/05/13.11:02
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA
3010
Copper
ND ug1L 5.0
2.0 1
12/03/13 10:45
12/04/13 04:18
7440-50-8
Lead
ND ug1L 5.0
4.0 1
12/03/13 10:45
12/04/13 04:18
7439-92-1
Zinc
28.5 ug/L 10.0
5.0 1
12/03/13 10:45
12/04/13 04:18
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
3.1 mg1L 2.5
2.5 1
12/03/13 07:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/18/2013 11:56 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 17

/�;alceAnalytical-
e Analytical Services, Inc.
East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Pace Analytical es, Inc.
222b drside {fir,
Asheville, NC 28804
{B28)254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)81b-yUy2
Sample: OUTFALL 003
Lab ID: 92181242003 Collected:
11/26/13 10:15
Received: 11/27/13 09:52 Matrix: Water
Rtyu i i
Parameters
Results Units Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
NO rl 5.0
5.0
1
12/05/13 11:03
6010 MET ICP
Analytical Method: EPA 6010 Preparation
Method: EPA 3010
Copper
3.3J uglL 5.0
2.0
1
12/03/13 10:45
12/04/13 04:22
7440-50-8
Lead
ND uglL 5.0
4.0
1
12103/13 10:45
12/04/13 04:22
7439-92-1
Zinc
33.7 uglL 10.0
5.0
1
12/03/13 10:45
12/04/13 04:22
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
7.4 mglL 2.5
2.5
1
12/03/13 07:18
Date: 12/18/2013 11:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7of17

"Analytical
www.pacebbsm"
:e Analytical Services, Inc.
East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Pace Analytica! es, Inc.
2225. _erside Dr,
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OUTFALL 004
Parameters
Lab ID: 92181242004 Collected:
Report
Results Units Limit
11/26/13 10:00
MDL DF
Received: 11/27113 09:52 Matrix: Water
Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mg/L. 5.0
5.0 1
12/05/13 11:03
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA
3010
Copper
2.9.1 ug/L 5.0
2.0 1
12/03/13 10:45
12/04/13 0425
7440-50-8
Lead
ND-uglL 5.0
4.0 1
12/03/13 10:45
12104/13 04:25
7439-92-1
Zinc
67.8 u v 10.0
5.0 1
12/03/13 10:45
12/04/13 04:25
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L 3.1
3.1 1
12/03/13 07:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/18/2013 11:56 AM without the written consent of Pace Analytical Services, Inc- Page 8 of 17

lacieAnalyfical'D
www.pacelabs cam
ce Analytical Services, Inc.
. o East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Pace Analytica '.es, Inc,
222b ....erside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9900 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OUTFALL 005
Parameters
Lab ID: 92181242005 Collected:
Report
Results Units Limit
11/26/13 10:40
MDL DF
Received: 11/27/13 09:52 Matrix: Water
Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mg1L 5.0
5.0
1
12/05/13 11:03
6010 MET ICP
Analytical Method: EPA6010 Preparation
Method: EPA3010
Copper
5.5 uglL 5.0
2.0
1
12/03/13 10:45
12/04/13 04:28
7440-50-8
Lead
ND uglL 5.0
4.0
1
12/03/13 10:45
12/04/13 04:28
7439-92-1
Zinc
107 gIL L V,V 10.0
5.0
1
12/03/13 10:45
12/04/13 04:28
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
34.4 mg1L 5.0
5.0
1
12J03/13 07:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/18/2013 11:56 AM without the written consent of Pace Analytical Services, Inc.. Page 9017

0
!;aceAnaMical
Knvw.paCe1abstaro
e Analytical Services, Inc.
East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical :s, Inc.
2225. rside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Sample: OUTFALL 006 Lab ID: 92181242006 Collected: 11/26/13 10:20 Received: 11/27/13 09:52 Matrix: Water
Parameters
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
6010 MET ICP
Copper
Lead
Zinc
2540D Total Suspended Solids
Total Suspended Solids
Date: 12/1812013 11:56 AM
Report
Results Units Limit
MDL
DF
Prepared
Analyzed
CAS No.
Analytical Method: EPA 1664E
ND mg/L 5.0
5.0
1
12/05/13 11:04
Analytical Method: EPA6010 Preparation Method: EPA3010
7.0 ug/L 5.0
2.0
1
12/03/13 10:45
12/04/13 04:31
7440-50-8
5.0
4.0
1
12l03113 10:45
12/04/13 04:31
7439 92-1
�u�l
�1�14110.0
5.0
1
12/03/13 10:45
12/04/13 04:31
7440 6fi 6
Analytical Method: SM 2540D
31.2 mg/L 10.0
10.0
1
12/03/13 07:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 10 of 17

1106 Analytical
wnw,prirr'aL,tur:,:,
zAnalytical Services, Inc -
East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Pace Analytical is, Inc.
2225 , . .;rside Dr.
Asheville, NC 28304
[phone]
QUALITY CONTROL DATA
QC Batch: GCSV116155 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92181242001, 92181242002, 92181242003, 92181242004, 92181242005, 92181242006
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(N4)d t5-9092
METHOD BLANK: 1098947 Matrix: Water
Associated Lab Samples: 92181242001, 92181242002, 92181242003, 92181242004, 92181242005, 92181242006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L NO 5.0 12/05/13 10:51
LABORATORY CONTROL SAMPLE: 1098948
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg1L 20 17.2 86 64-132
MATRIX SPIKE SAMPLE: 1098949
92181709002 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L ND 20 19.2 82 64-132
Date: 12/18/2013 11:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I nc..
Page 11 of 17

aceAnalytical
wwwpacefabscorn
ceAnalytical Services, Inc.
d East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Pace Analytica :es, Inc.
222z, --.erside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP114767 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET
Associated Lab Samples: 92181242001, 92181242002, 92181242003, 92181242004, 92181242005. 92181242006
METHOD BLANK: 1097117
Matrix: Water
Associated Lab Samples:
92181242001, 92181242002, 92181242003, 92181242004, 92181242005,
92181242006
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Copper
ug/L
ND 5.0
12/04/13 02:52
Lead
ug/L
ND 5.0
12/04/13 02:52
Zinc
ug/L
ND 10.0
12/04/13 02:52
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1097118
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Copper
ug/L
500
469 94 80-120
Lead
ug/L
500
474 95 80-120
Zinc
ug/L
500
480 96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1097119
1097120
MS
MSD
92181194001
Spike
Spike
MS
MSD
MS
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
Copper ug/L
44.7
500
500
528
528
97
Lead ug/L
ND
500
500
425
427
85
Zinc ug/L
12.0
500
500
489
488
95
Date: 12118/2013 11.56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
MSD % Rec Max
% Rec Limits RPD RPD Qual
97 75-125 0 20
85 75-125 0 20
95 75-125 0 20
Page 12 of 17

aoAnalytical
www.pacelebsoam
ce Analytical Services, Inc.
--i East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Pace Analytica :es, Inc.
222- drside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WET128392 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92181242001, 92181242002, 92181242003, 92181242004, 92181242005, 92181242006
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntesville, NC 28078
[phone]
METHOD BLANK: 1097024 Matrix: Water
Associated Lab Samples: 92181242001, 92181242002, 92181242003, 92181242004, 92181242005, 92181242006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 12/03/13 07:13
LABORATORY CONTROL SAMPLE: 1097025
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 252 101 80-120
SAMPLE DUPLICATE: 1097026
Parameter
Total Suspended Solids
92181197001 Dup
Units Result Result
mg/L ND ND
Max
RPD RPD Qualifiers
10
SAMPLE DUPLICATE: 1097027
92181242005 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg1L 34.4 35.4 3 10
Date: 12/18/2013 11:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 17

e Analytical Services, Inc.
Pace Analytical es, Inc.
Pace Analytical Services, Inc.
®
aceMalytical
_ cast Meadow Road - Suite A
2225. . erside Dr.
9800 Kincey Ave. Suite 100
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
www.paselabs corn
[phone]
[phone]
[phone]
QUALIFIERS
Project: Unison -Asheville
Stormwater
Pace Project No.: 92181242
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting•limtt7
MDL - Adjusted Method Detection Limit.
PRL-Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylviny( ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C . Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full,
Date: 12/1812013 11:56 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 17

1�2ceAnalytical'
www.paceianacorn
e Analytical Services, Inc.
East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical es, Inc.
2225. .. crside Dr.
Asheville, NC 28604
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Unison -Asheville Stormwater
Pace Project No.: 92181242
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92181242001
OUTFALL 001
EPA 1664E
GCSW16155
92181242002
OUTFALL 002
EPA 1664E
GCSVI16155
92181242003
OUTFALL 003
EPA 1664E
GCSV116155
92181242004
OUTFALL 004
EPA 1664E
GCSV116155
92181242005
OUTFALL 005
EPA 1664E
GCSV116155
92181242006
OUTFALL 006
EPA 1664E
GCSV116155
92181242001
OUTFALL 001
EPA 3010
MPRP114767
EPA 6010
92181242002
OUTFALL 002
EPA 3010
MPRP114767
EPA 6010
92181242003
OUTFALL 003
EPA 3010
MPRP114767
EPA 6010
92181242004
OUTFALL 004
EPA 3010
MPRP114767
EPA 6010
92181242005
OUTFALL 005
EPA 3010
MPRP114767
EPA 6010
92181242006
OUTFALL 006
EPA 3010
MPRP/14767
EPA 6010
92181242001
OUTFALL 001
SM
2540D
WETI28392
92181242002
OUTFALL 002
SM
2540D
WETI28392
92181242003
OUTFALL 003
SM
2540D
WETI28392
92181242004
OUTFALL 004
SM
2540D
WETI28392
92181242005
OUTFALL 005
SM
2540D
WET128392
92181242006
OUTFALL 006
SM
2540D
WETI28392
Date: 12/18/2013 11:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICPI13420
ICP113420
ICP113420
I C PI13420
I C PI13420
ICP113420
Page 15 of 17

current Name Sample Condttron Upon, ment !Revised: Juhe4, 2013 '
aceAnaMicalk
'Recerpf (SOUR)
Page 1 of 2 .
WWN'.Arcofobe.yoin
t•1.. �..�--a '� _
,-,-v VLUInCIIr IVU, -- -'�
_ - 1.-:.:i .:.. n. A.,lL—�:4:.....'.
- - -.IJJ 41111� f1U L11V11 LIGJ. ";
f
F-ASV=CS-003-rev.11. .:
Pace'Asheville Quaht dffice
Client Name..�1�e�^o.,7`:.:
Where Received: Huntersville Ashev,iil =:0 ;Eden ' :.` ` ;i.
Raleigh
Courier (Circle): Fed Ex UPS LISPS I" t Commercial Pace
other
no Seals intact: yes,
Custody Seal on Cooler/Box Present:�Bbbel,
0 no
Packing Material: Bubble Wra ags (] Nono,�I��1+ Other
Gun
Circle Thermometer Used -130265963 Tvde of tce. WRt1 ulllo Nnno
'....... .,.." L� :,....
fRGn#2- 003,44039
C YCamnlnc'nn Ir-a rnn-li:nn pm:-c-ess h2s.bengun -
Temp Correction Factor: Add / Subtract:
Corrected Coolor Tomp.: ' C.
Biological Tissue Is'Frozen: Yes' No Q
date andini ' 1 ,pf'p rso exar�Ining "
Temp should be above freezing to 6'C
Comments•':.'
Chain of Custod y Preseni:
es too
❑NIA
1. '
Chain of Custody Filled Out:
es No
❑NJA
2.
Chain of Custody Relinquished:
es o
DNiA
3,
Sampler Name & Signatw'e on COC:
es No ❑NIA-
a.
Samples Arrived within Hold Time:
ISK116 ❑No
'❑nlrA
5.
Short Hold Time Analysis (<72hr):'
❑Yes
❑NIA
6. c
Rush Turn Around Time Requested:
es. No
❑N!A
7.
Sufficient Volume:.
as Ptqo
QNIA
8.
Correct Containers Used: s o ❑NIA
9,
-Pace Containers Used:
ss'' o
ON1A
��c:ntainers intact.'"
�.
_ LJNc
" f-rnllti
Filtered volume received for Dissolved tests
QYes 00
11.
Sample Labels match COO:
9 ' Qo'
QNIA
12.
-Includes date/time/lD/Analysis Matrix:
,
All contalners'needing preservation have been checked.
.,
- Yes,.❑No
-ONiA
13. ...._. -. .. .,
All containers needing preservation are found to be in
&_.s 0No
❑NIA
_
compliance with EPA recommendation.
N
exceptiorsl VOA, coldcrm, TOC, D8,Ci, WI-DRO (water) ".
Ely-s o
-
Samples checked for dechlorination:
es QNo
DwA
14.
Headspace in VOA Vials { >6mm):
❑Yea []No
2<A
Trip Siank Presont;
❑Yes•-QN6'
Q&A1W
Trip Blans Custody Seals Present'
❑Yes ' QNo
14wl<..-.
Pace Tri,::71ank Lot fl (if purchased):
Client Notification! Resolution: Field Data Requlred7, Y 1 N
Person Contacted: DatelTime:
Comments/ Resolution:
SCURF Review: Date: `t ••'Place.labef here " --
SRF Review: Date: lo ZZ t OR
Note: Wherievor there is a discrepancy. affecting No h Carolina
compllarlvu Salilple5, a copy of tFlis foraui will be stint to UIU Nuliil Handwrite project number
Carolina DEHNR Certification Office ( Le out of hold, Incorrect (if 6o label available)
preservative, out of temp, incorrect containers)
Page 16 of 17

CHAIN -OF -CUSTODY 1 Analytical Request Document
1!'ace Analytical • The CI,31 af-Custody is a LEGAL DOCUMENT. All relevant fields must ba completed acwr Iy.
www.aaceaus.wm
a.
S ectfon A Section 8 Section C
l of
Requtrcd Client lnf.—tien: Regoirud P�olem lnfq anon: Inval�o lnranna0— '
Qpmpany:. Report Ye: Anemia,:
f
174 8271
�— -
Addm55: T Copy
5 <<
To:
Company Na c: �-� .
REGULATORY
AGENCY' -
+r �4r1d5
L.
Add— !r NPDES
�•yl
r GROUNDWATER (- DRINKING WATER
.r RCRA (- OTHER
Ema11 Ta: Purcbege
,� @ LOW. LDlv,.
ONer No.:
+ara pave
r UST
P nq' F Project
Name:°Ce
P'gea Site Location
mm
srATE:
C
Requeaed Due Date,7AT: Proles
Number.
N P�l�e e: ��
Ja`3
J
.�-
- :
"I. Qquested
Analysis
Filtered
(YN)...-..
SactionD MaalKCodeg
-
R.gm.eau.mmm,,,,xle„ rwTRixt
s
COLLECTED
Preservatives
.5-
DdrxiaBWelereODW
$
.. TE
so—,
waste Water w
Product P
Sruer
y�
:.;, •,.,
Z
SaiaSolld St.
;
s
~�
6
SAMPLE IU w� a WP
�?
a
w
z
�
�' _ '�
�g
o �j1 j�
(A-Z.0-9/;) Airp AN
Sample IDs MUST DE UNIQUE Tasoe TS
p
O
V
w
I�H'
a
l
Other OT
n ON
U
O N
m t:Q'
0
.�
DATE
TIME
DATE
TIME
7 =
S =
Z 2
O
'
a Pace Project KaJ Lab I.D. .
lnni
13
fay
3
"
<
_xX,1X
''-.,
"2
l 'L
CT
[l•Zta•13
oJ03
SC
X X
X
4 k
It w�
ui
[
IL-�, ..�
jnr�
_
V
X r
A KI
xi
I I(]
5
O
loio
xx
xx
I K XX
•�.
w
ItlZn
J
x x
y
7',
S
9
70
14
72
ADDITiONALCOMMENTS
.,RELINQUISH DYIAFN NATION-
''.DATE.
TIME
ACCEPTEDBYf AFFILIATION
ATE'
' TIME'
SAMPLE CONDITIONS
SAMPLER NAME AND SIGNATURE
ORIGINAL.
E
'�
o$L
°L
PR1NTName at SAMPLER: o-1++tA
DATE Signed
R: -
SIGNATURE of SAMPLE�/��w. �! y %
H
-Imams-.. Nme: ey syrvog ws roes yuu am eo:ept, Par<'a NET W day poy le.ms eM —1W of P-ALL-0 020rev.07, 15-May-2007

Page 1 of 17
Table 2
Completed by: Jennifer Rendon
Title: EHS Coordinator
Material Inventory
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quamty Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
(eq., covered, bermed,
...crave L'n,its
if yes, decribe
reason
Alloy Steel - HR & CR. Alloy Leaded Steel
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Aluminum Alloys, Aluminum Alloys Containing Lead
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Brass
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Bronze
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Carbon Steel - HR & CR, Leaded Carbon
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Copper- CR & HR, Copper Leadtex Sheet
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Stainless Steel
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
various
to Rain
NA
Titanium
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
COBALT -BASED ALLOYS
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA

Page 2 of 17
Completed by: Jennifer Rendon
Table 2
Title: EHS Coordinator
Material Inventory
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
(eg., covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
NICKEL -CHROMIUM ALLOYS
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Garnet Abrasive Grains and Powders
Shot Peen/ Garnett
Special Processes
250 Ibs
None
Stored Inside
Easy Task
Floor Finsh
Maintenance
5 Gallons
None
Stored Inside
PYROMET CTX-909
Forgingsl Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
ILOBROACH 11
401 Oil Storage
Special Processes
Room
55 gallons
None
Stored Inside
Techniclean 2000
401 Oil Storage
Cleaner
Room
110 Gallons
None
Stored Inside
Factory Formula HP
Cleaner
iMaintenanre
5 Gallons
lNone
iStored Inside
MOBIL DTE 24
401 Oil Storage
Machine Oil
Room
330 Gallons
None
Stored Inside
MOBIL VELOCITE OIL NO, 3
401 oil Storage
Machine Oil
Room
110 Gallons
None
Stored Inside
MOBIL VELOCITE OIL NO. 6
401 Oil Storage
Machine Oil
Room
4 Gallons
None
Stored Inside
Texaco Meropa
401 Oil Storage
Machine Oil
Room
55 Gallons
None
Stored Inside
Brown use Aluminum Oxide
Shot Peen/ Garnett
Special Processes
25 bags
None
Stored Inside
Aluminum Alloys Containing Chromium
Forgingsf Raw
South Loading
Inert- Exposed
FNA
Materials
Dock
Various
to Rain

Page 3 of 17
Completed by: Jennifer Rendon
Table 2
Title: EHS Coordinator
Material Inventory
Date: 10116/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
(eg., covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
WD-40 Aerosol
Production/ Tool
Lubricantion
Crib
124 cans
None
Stored Inside
ZYGLO PENETRANT ZL-37
FPI Line (Old &
FPI
New)
700 Gallons
None
Stored Inside
ZYGLO EMULSIFIER ZR-10B
FPI Line (Old &
New), 401 Oil
FPI
Storage Building
365 Gallons
None
Stored Inside
ZYGLO EMULSIFIER ZE-413
FPI
Old FPI Line
55 Gallons
None
Stored Inside
ZYGLO DRY POWDER DEVELOPER ZP-4B
FPI (Old & New
FPI
Line) & MRB
80 Ibs
None
Stored Inside
Aluminum Alloy (Alloy series 1000, 2000, 3000, 5000, 6000 and
7000)
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Carbon and Alloy Steels
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Stainless Steels
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
ALLOY STEELS AND DIE STEELS
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
CARBON STEEL
Forgings( Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA

Page 4 of 17
Comoleted bv: Jennifer Rendon
i abie 2
Title: EHS Coordinator
Material Inventory
Date: 10116/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
(eq., covered, bermed,
Average units
If yes, decribe
drum sealed)
reason
PACD15, PACR77, PACR80, PACR80F, PAC713F, PAC713,'
PAC713-1,PAC713LC, PAC713HV, PAC718A, PAC7186,
PAC718F, PAC718F1, PAC718BA, PAC718BB, PAC718VF,
PAC718VF1, PAC 718F3, PAC718W, PAC738, PAC
738F,PAC738HV, PAC8118, PAC939, PAC520F, PACBRB,
PACDF4B, PACDF3, PACDF3-325,PAC8411, PAC8303MOD,
Forgings/ Raw
South Loading
Inert- Exposed
PAC8303
Materials
Dock
Various
to Rain
NA
PAC701, PAC70113, PAC701NS, PAC701SF, PAC701SP, PAC705,
PAC705-1, PAC705-2, PAC705-3, PAC705-200, PAC705HPSF,
Forgings! Raw
South Loading
Inert- Exposed
PAC GKI I U, PAC 8616
Materials
Dock
Various
to Rain
NA
PAC900, PAC900C, PAC90002, PAC900F, PAC906, PAC906PA,
PAC906PAF, PAC906PAF1, PAC 906W, PAC909, PAC909R,
Forgings! Raw
South Loading
Inert- Exposed
PAC90913, PAC 909W, PAC5906 PAFHV, PAC6906
Materials
Dock
Various
to Rain
NA
TT-P-1757 Comp G Type 1 Primer
Stored Inside/ will no
longer be use on site
once product expoires in
Special Processes
Special Processes
1 Gallon
None
2013
Commercial Odorized Propane
Tank Outside 401
PIT Fuel
Building
1000 gallons
None
Tank Sealed
Metco 101, 101NS, 101BNS, 101SF, 101FP, Metcolite 14, C, F, F36,
VF, AMDKY 187, 6200, 6202, 6203. 6204, 6208, PEMI 10-231,
Sulzer Metco 6203, XPT-D 705, 644, PT 1100, AMDRY XPT W631,
GRIT BLAST MATERIAL 0.4-0.8MM, GRIT BLASTING MATERIAL G
Grit Blastl 401 Oil
24, PT-1100, XPT DH 1079
Part Cleaner
Storage Room
4lbs
None
Stored Inside
Nickel -Chromium -Aluminum/ Bentonite Powder
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA

Page 5 of 17
Completed by: Jennifer Rendon
Table 2
Title: EHS Coordinator
Material Inventory
Date: 10116/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
leg., covered, bermed,
„
if yes, ciecribe
reason
Klean-Strip Acetone
Tool Crib/
Parts Cleaner
Production
5 Gallons
None
Stored Inside
MS-3110 YELLOW PRIMER
Stored Inside/ will no
longer be use on site
once product expoires in
Production Paint
ISpecial Processes
11 Gallons
lNone
12013
CT9612
401 Oil Storage
Cutting Oil
Room
60 Gallons
None
I Stored Inside
MOBILMET 404
401 Oil Storage
Waiter Grinder OR
Room
5 Gaiions
None
Stored inside
Lacquer thinner
Tool Crib
Parts Cleaner
Production Floor
2 Gallons
None
Stored Inside
Denatured Alcohol
Gage Cleaner
OC (401 & 601)
5 Gallons
None
Stored Inside
CLC CHEM FINISH EDM 3033
401 Oil Storage
Process Oil
Room
110 Gallons
None
Stored Inside
Brulin 1990 GD
FPI Wash Tank/ TI
Clean Room/ 401
Immersion Part
Chemical Storage
Cleaner
Room
1100 Gallons
None
Stored Inside
Hyspin AWS 68
401 Oil Storage
Machine Oil
Room
320 Gallons
None
Stored Inside
Magna BD 68
401 & 601 Oil
Machine Oil
Storage Room
660 Gallons
None
Stored Inside
MOBIL DTE 26
401 Oil Storage
Machine Oil
Roam
320 Gallons
None
Stored Inside
MOBILGEAR 629
401 Oil Storage
Machine Oil
Room
4 Gallons
None
Stored Inside

Page 6 of 17
Completed bv: Jennifer Rendon
Tabie 2
-
Title: EHS Coordinator
Material Inventory I
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
(eg., covered, bermed,
Average Units
If yes, decribe
dru"' sealed)
reason
Paint Thinner
QC (401 & 601)/
Part Cleaner
Maintenance
1 Gallons
None
Stored Inside
MOBILGEAR 627
401 Oil Storage
Equipment Lube
Room
4 Gallons
None
Stored Inside
MOBILGEAR 630
401 Oil Storage
Equipment Lube
Room
5 Gallons
None I
Stored Inside
MOBILGREASE XHP 222
Maintenance Dept.
& 601 Oil Storage
120
Equipment Lube
Room
Gallons
None
Stored Inside
Mobilux EP 023
601 Oil Storage
Machine Oil
Room
5 Gallons
None
Stored Inside
ZYGLO PENETRANTZL-27A
FPI (Old Line), 401
FPI Line
Oil Storage Building
110 Gallons
None
Stored Inside
TRIM VHP E210
401 Oil Storage
Machine Oil
Room
55 gallons
None
Stored Inside
SintoGrind TTS-US
401 Oil Storage
Machine Oil
Room
110 Gallons
None
Stored Inside
Simple Green All -Purpose Cleaner, Simple Green Scrubbing Pad,
Simple Green Concentrated Cleaner/Degreaser/Deodorizer
Wash Tank/ 401 Oil
Farts Gleaner
Storage Room
110 Gallons
None
Stored inside
Alusol AU 38
401 Oil Storage
Coolant
Room
330 gallons
None
Stored Inside
Magna CF 220
401 & 601 Oil
Machine Oil
Storage Room .
375 Gallons
None
Stored Inside
SHELLZONE ALL -SEASON Antifreeze/Coolant
DMG Coolant/ PIT
Maintenance
5 Gallons
None
Stored Inside
TECH CLEAN 7011
401 Oil Storage
Cleaner
Room
165 Gallons
None
Stored Inside

Page 7 of 17
Completed bv: Jennifer Rendon
Tabie 2
-
Title: EHS Coordinator
Material Inventory
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
leg., covered, bermed,
Average i.lnits I
If yes, decribe
uul uill seaieul
reason
TAP MAGIC Formula 2 ECO-OIL Cutting Fluid
Process Oil
Tool Crib
3 Gallons
None
Stored Inside
R-11
HVAC
AC Room
60lbs
None
Stored Inside
PB-75 Prussian Blue Paste .76 oz, Tube
Blue Marking
Tool Room
2 tubes
None
Stored inside
Fluid Resistant Epoxy Primer
Stored Inside/ will no
longer be use on site
once product expoires in
Asembly
Special Processes
11 Gallon
INone
12013
MB-40-5, MB-40-55 or MB-40-330 HONING OIL
401 oil Storage
Snocial Prnco —
Rnnm
zn r,�unn�
NnnP
J
St—Prl 1-er�P
HONING OIL 9260
401 Oil Storage
Special Processes
Room
30 Gallons
None
Stored Inside
Havoline Automatic Transmission Fluid Type F
PIT/ Company
Vehicles
Maintenance
3 pints
None
Stored Inside
CASTROL MAGNA 220
401 Oil Storage
Machine Oil
Room
660 gallons
None
Stored Inside
Syntilo 9918
401 & 601 Oil
Special Processes
Storage Room
1 110 Gallons
None
Stored Inside
WATER CARE 7500
Cooling Tower
AC Room
5 gallons
lNone
18tored Inside
QUAKERCOOL 2778 AE
401 Oil Storage
55 -1-1T
CT9605
401 Oil Storage
Cutting Oil
Room
60 Gallons
None
Stored Inside
DEFOAMER31
601 Oil Storage
Deformer
Room
55 Gallons
None
Stored Inside
STRIPADD2
401 Oil Storage
Cleaner
Room
110 Gallons
None
Stored Inside

Page 8 of 17
Completed by: Jennifer Rendon
Table 2
Title: EHS Coordinator
Material Inventory
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
leg., covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
PROTECH 1999LCMS
601 Oil Storage
Machine Oil
Roam
15 Gallons
None
Stored Inside
Project 70+ Custom 630 (17CR-4NI) Stainl
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Carpenter Stainless Type 316/316L
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Stainless 1 Type 410 Turbine Quality
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Carpenter Stainless Type 316 Forging Qua
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Type 304E Forging Quality
Forgings/ Raw
nno#criele
South Loading
r)—L
Vnrfn�
Inert- Exposed
4n Re;n
AI4
Carpenter Stainless Type 347
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Clean Image
401 Compressor
Glass Cleaner/
Room/ 601
General Purpose
Chemcial Room
100 Gallons
None
Stored Inside
TECH COOL 3325LF
401 8 601 Oil
Coolant
Storage Room
1595 Gallons
None
Stored Inside

Page 9 of 17
Completed by: Jennifer Rendon
Table 2
Title: EHS Coordinator
Material Inventory
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
(eg., covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
FR Epoxy Priner Curing Solution
Stored Inside/Will no
longer be use on site
once product expoires in
Special Processes
Special Processes
1 Gallons
None
2013
Hyspin AWS 32
401 Oil Storage
Machine Oil
Room
660 Gallons
None
Stored Inside
Isopropyl Alcohol
OC Central/ Work
Parts Cleaner
Stations/ Tool Crib
5 Gallons
None
Stored Inside
Hysol MB 50
401 & 601 Oil
Machine Oil
Storage Building
695 Gallons
None
Stored Inside
SPRAYON Blue Layout Fluid
OC South/
FPI Line
Production
12 cans
None
Stored Inside
Stainless Steel & Maraging Steel
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
nlioy Steel ingot
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
STAINLESS STEEL, NICKEL, COBALT AND TITANIUM BASED
ALLOYS
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Low Alloy and Tool Steel
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
KRYLON Lacquer Thinner
Part Cleaner
IT001 Crib
12 Gallons
iNone
1 Stored Inside
SHELL TETRA OIL 10SP
li
iMaehiiic ^vii
401 Oil Storage
iRoom
i55 Gaiiuri5
iiJ ^unc
iStu^red i�Sidc

Page 10 of 17
Completed by: Jennifer Rendon
Ta'vie 2
Title: EHS Coordinator
Material Inventory
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
(eg-, covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
MOBIL VELOCITE OIL NO. 10
401 Oil Storage
Machine Oil lRoom
15 gallons lNone,
I Stored Inside
Alpha SP 150
401 Oil Storage
Machine Oil
Room
55 Gallons
None
Stored Inside
Isopropyl Alcohol
n_r Centra!!!Ncrk
Parts Cleaner
Stations/ Tool Crib
5 Gallons
None
Stored Inside
Isopropyl Alcohol
QC Central/ Work
Parts Cleaner
Stations/ Tool Crib
5 gallons
None
Stored Inside
Castrol AP Gear 80W-90
401 Oil Storage
Machine Oil
Room
15 Gallons
None
Stored Inside
SS4044P 01 P-Bottle (0.900 Ibs-0.409 kg) Silicone primer solution
601 Special
Spinner Cones
Processes
20 ozs
NONE
Stored Inside
ChemTreat C2189T
Water Treatment
Chiller Room
50lbs
None
Stored Inside
ChemTreat CL1453
A/C Water Tower
Treatment
Chiller Room
5 Gallons
None
Stored Inside
Aluminum billet
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Tribaloy T-400
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Tribalov T-80G
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
INA
Professional LYSOL Brand III Disinfectant Spray (all sizes, all
scents)
Disinfectant Spray
Restrooms
12 cans
None
Stored Inside

Page 11 of 17
Completed by: Jennifer Rendon
Table 2
Title: EHS Coordinator
Material inventory
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm water.
(eg., covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
ATI Allvac Alloys: AM 355
Forgingsl Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
ATI Allvac Alloys: ATI 9-4-30, VascoMax C-250, VascoMax C-300,
VascoMax C-350, ATI 23, ATI AL-6XN, ATI 13-8Mo, ATI 13-8
SuperTough, ATI 15-5, ATI 17-4 PH, ATI XM-19, ATI 304 L. ATI 316
L, REX 734, ATI H-46, ATI 455, ATI Jethete M152, ATI A-286, ATI
Forgingsl Raw
South Loading
Inert- Exposed
S240, AM 355, ATI 9310. ATI 1014. ATI Greek Ascoloy
Materials
Dock
Various
to Rain
NA
INCONEL, INCOLOY, INCOCLAD, MONEL, UDIMET, UDIMAR,
NILO, NILOMAG, NIMONIC, NIMOLOY, NI-SPAN-C, BRIGHTRAY,
KOTHERM & NIOTHERM alloys; FERRY alloy, Nitinol, Nickel,
DEPOLARIZED & DURVANIC nickel, Electroformed nickel foil,
Cupro 107; Miscellaneous designations, Mixed nickel alloy revert
Forgingsl Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
STEEL ALLOYS - 1045, 17-4, 2169, 310, 35CD4, 4330, 4340M,
9310, ACI 17A PH, AISI-4340, Alloy 90, Custom 4SS, HP-9-4-20,
Jethete, N155, Nickel Maraging, PH-13-8MO, PH-15-5
Forgingsl Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Titanium Alloys T100 ALLOYS - HAYNES Ti-6AI-4V alloy
Forgingsl Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
High performance, heat resistant alloys - L-605 (Haynes 25)
Forgingsl Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Titanium Alloys: Ti 17. Ti 6-2-4-2. Ti 6-4
Forgingsl Raw
(South Loading
lVarious
ExposedMaterials
�:o
INAnert-
Dock
Rain

Page 12 of 17
Completed by: Jennifer Rendon
Table 2
Title: EHS Coordinator
Material Inventory
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water,
(eg., covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
LAPELLOY C ALLOY
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Metal alloys of Aluminum, Stainless steel, Steel and Nickel:
Aluminum alloys 6D61
Forgings/ Raw
outh Loading
k
Inert- Exposed
INA
Mararialc
nrk
\/arinuc
to Rain
Metal alloys of Aluminum, Stainless steel, Steel and Nickel:
Stainless Steels 17-4 PH
Forgings/ Raw
South Loading
Inert- Exposed
�NA
Materials
Dock
Various
to Rain
Metal alloys otAiuminum, stainiess steel, Steel and Nickel:
Stainless Steels 321
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Metal alloys of Aluminum, Stainless steel, Steel and Nickel:
Stainless Steels 410
Forgingsl Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
Metal alloys of Aluminum, Stainless steel, Steel and Nickel -
Stainless Steels 15-5 PH
Forgings/ Raw
South Loading
Inert- Exposed
Materials
Dock
Various
to Rain
NA
KRYLON LINE-UP Striping Paint (Solvent Based), Highway Yellow
Maintenace in
proper storage
Spray Paint
cabinet
2 Cans
None
Stored Inside
HARDHT LSPR 6PK STRIPE YELLOW STRIPING
Maintenace in
proper storage
Spray Paint
cabinet
2 Cans
None
Stored Inside
II carbide tools sold under the AMAMCO Tool name
Tool crib)
Tooling
Production
Various
None
Stored Inside
II Sandvik Coromant cemented tungsten carbide and cermet
Tool crib/
nrados
Tnnlina
Production
Varinus
NOYIe
Stored Inside

Page 13 of 17
Completed by: Jennifer Rendon
Table 2
Title: EHS Coordinator
Material Inventory
Date: 'i0116/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
(eg•r covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
All Greenleaf Cemented Carbide Grades
Tool crib/
Tooling
Production
lVarious
None
Stored Inside
Cemented Carbides
Tool crib/
Tooling
Production
Various
None
Stored Inside
Tungsten Carbide product with Cobalt binder - K-0963-001
Tool crib/
Tooling
Production
Various
None
Stored Inside
Group C: K420
Tool crib/
Tooling
Production
Various
None
Stored Inside
Group A: K313, KC5010, KC730, KC7310, KC732
Tool crib/
Tooling
Production
Various
None
Stored Inside
Group A: 2210
Tool crib/
Tooling
Production
Various
None
Stored Inside
KT175, KT175Y02
Tool crib/
Tooling
Production
Various
None
Stored Inside
Group A - BP154, BP200, KYON 1540, KYON 2000
Tool crib/
Tooling
Production
Various
None
Stored Inside
All tun—t——rhiria —deS avrant (solid titanium carbine nrnriocl
I
Tnnl rrihl
Tooling
Production
Various
None
Stored Inside
Carbide Grades and Brazed Tools and Sludges
Tool crib/
Tooling
Production
Various
None
Stored Inside
ALL BAY STATE BARBIDE CEMENTED CARBIDE GRADES,
Tool crib/
BRAZED, AND COATED TOOLS
Tooling
Production
Various
None
Stored Inside
High Speed Steel Cutting Tools
Tool crib/
Tooling
Production
Various
None
Stored Inside
II Rotary Tool Carbide Grades, Brazed Tools and slugs -
Tool crib/
CEMENTED CARBIDE: Cobalt binder
Tooling
Production
Various
None
Stored Inside
Group B - BP210, KYON 2100
Tool crib/
Tooling
,Production
,
,Nna
,St— H I—iria\arinus ._._..___

Page 14 of 17
Table 21
Completed by: Jennifer Rendon
aurc
Title: EHS Coordinator
Material Inventory
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
(eg., covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
Group C - BP300, KYON 3000
Tool crib/
Tooling
Production
Various
None
Stored Inside
Carbide proauct basea on tungsten carbine wan cobait binaer
Tooi crot
Tooling
Production
Various
None
Stored Inside
II Rotary Tool Carbide Grades, Brazed Tools and slugs -
Tool crib!
CEMENTED CARBIDE: Nickel binder
Tooling
Production
Various
None
Stored Inside
All Rotary Tool Carbide Grades, Brazed Tools and slugs -
Tool crib/
CEMENTED CARBIDE: coated
Tooling
Production
Various
None
Stored Inside
Rotary Tool Carbide Grades, Brazed Tools and slugs -
Tool crib/
rII
CEMENTED CARBIDE: brazed Droducts
Toolin_q
Production
Various
None
Stored Inside
All Rotary Tool Carbide Grades, Brazed Tools and slugs -
Tool crib/
CEMENTED CARBIDE: tube rod
Tooling
Production
Various
None
Stored Inside
All Hannibal Carbide Tool, Inc. reamers, drills, counterbores, end
mills, cutters, & single po
Tool crib/
Cemented Carbide, Sintered Carbide, Hardmetal
Tool crib/
Tooling
Production
Various
None
Stored Inside
Cemented Tungsten Carbide with Cobalt/Nickel Binder, Tungsten
Tool crib/
Carbide Grade Powder
Tooling
Production
Various
None
Stored Inside
Cemented Tungsten Carbide Cutting Tools with Cobalt / Nickel
Tool crib/
binder, All Grades
Tooling
Production
Various
None
Stored Inside
Group D: KC9125
ITool crib/
Tooling
Production
Various
None
Stored Inside
Group H: KC8050
Tool crib/
Tooling
Production
Various
None
Stored Inside
Group D: K715, KC5025, KC522M, KC525M, KC5510, KC610M,
Tool crib/
KC635M, KC720, KC7215, KC725M, KC735M
Tooling
Production
Various
None
Stored Inside
II Mitsubishi Carbide Grade and Coated Carbide Grade
Tool crib/
Tooling
Production
Various
None
Stored Inside

Page 15 of 17
T_able „
Completed by: Jennifer Rendon
u
Title: EHS Coordinator 1
Material Inventory
Date: 1011612012 I
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm water.
(eg., covered, bermed,
Average Units
If yes, decribe
reason
drum sealed)
PTOUCH +SSPR 6PK GLOSS MEADOW GREEN 12
Stored in Flammable
Spray Paint
Maintenance
11 Can
None
Cabinet
PRO 1-GL 2PK STRIPE TRAFFIC YELLOW
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
PRO 1-GL 2PK STRIPE TRAFFIC WHITE
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
SPECLT SSPR 6PK FLUOR ORANGE
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
SPECLT SSPR 6PK FLUOR RED -ORANGE
Stored in Flammable
Snrav Paint
Maintenanca
1 C:an
Nnna
C:ahinat
STRUST +SSPR 6PK GLOSS SUNRISE RED
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
GLOSS WHITE 0002281
Stored in Flammable
Jplay Pal{1l
Ivl all ltellan�;e
I Cafl
I�Vlle
l•ablllet
Americas Finest Aerosol Topcoats
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
Gorilla Glue
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
PRO LSPR 6PK SAFETY YELLOW
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
PTOUCH +SSPR 6PK GLOSS CANDY PINK
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
PTOUCH +SSPR 6PK GLOSS REAL ORANGE
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
PTOUCH +SSPR 6PK GLOSS PURPLE 12 OZ
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
PTOUCH +SSPR 6PK GLOSS SPA BLUE
Stored in Flammable
11
Spray Paint
Maintenance
11 Can
None
Cabinet

Page 16 of 17
Completed by: Jennifer Rendon
Ta'vie 2
Title: EHS Coordinator
Material Inventory
Date: 10/16/2012
Instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
(eg., covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
PTOUCH +SSPR 6PK GLOSS SUN YELLOW 12 OZ
Stored in Flammable
Spray Paint
IMaintenance
11 Can
lNone
lCabinet
PRO 1-GL 2PK GLOSS WHITE
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
INeldwood Non -Flammable Contact Adhesive
Adhesive
Maintenance
4 tubes
None
Stored Inside
KRYLOiJ indourivutdoor Paint, True Blue
Siureuu in Fianirrrabie
Spray Paint
Maintenance
1 Can
None
Cabinet
KRYLON Indoor/Outdoor Paint, Peekaboo Blue
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
Premium Plus Interior Satin Enamel Ultra Pure White No. 7050
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
Premium Plus Interior/Exterior Hi -Gloss Enamel Deep Base No.
Stored in Flammable
8300
Spray Paint
Maintenance
1 Can
None
Cabinet
Premium Plus Interior Interior/Exterior Hi -Gloss Enamel - Pastel
Stored in Flammable
Base No. 8500
Spray Paint
Maintenance
1 Can
None
Cabinet
Premium Plus Interior/Exterior Hi -Gloss Enamel Red No. 8610
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
1-Part Epoxy Concrete & Garage Floor Paint Deep Base No. 930
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
PREMIUM PLUS Exterior Semi -Gloss Enamel Deep Base No. 5340
Stored in Flammable
Spray Paint
Maintenance
1 Can
None
Cabinet
SS4004P 01 P-Bottle (0.900 LBS-0.409 KG) Silicone primer solution
601 Special
Spinner Cones
Processes
20 ozs
None
Stored Inside
Varincut C 83,9
1
1401 Oil Storaae
.,
Special Processes
p
Room
55 Gallons
None
Stored Inside
�ROA_DRU_NNER ICE MELTING COMPOUND
Ice Melt
Maintenance
200 Ibs
when ice melts
Safe for stormwater

Page 17 of 17
Completed by: Jennifer Rendon
Table 2
Title: EHS Coordinator
Material Inventory
Date: 10/16/2012
instructions: List all materials used, stored or produced onsite. Assess and evaluate these materials for their potential to contribute
pollutants to storm water runoff.
Quanity Used,
Produced, or
Likelihood of
Describe Material
Chemical Product
Purpose
Location
Stored
contact with
Management Practice
Storm Water.
leg., covered, bermed,
Average Units
If yes, decribe
drum sealed)
reason
MOBIL DTE 21
601 Oil Storage
Machine Oil
Room
15 Gallons
None
Stored Inside
Super D Dry Powder Extinguishant
Metal Fire
401 Deburr & 601
Extinguisher
Campbell Grinder
2 Extinguishers
None
Stored Inside
Battery Acid Spill Kit - SPILFYER YELLOW UNIVERSAL (HAZMAT)
Forklift Charging
SORBENT PRODUCTS
Acid Spill Kits
Stations
2 Kits
None
Stored Inside
Battery Acid Spill Kit - KOLORSAFE LIQUID ACID NEUTRALIZER
Forklift Charging
Acid Spill Kits
Stations
2 Kits
None
Stored Inside
Battery Acid Spill Kit - AQUALOCKIT - SUPER POLYMER
Forklift Charging
Acid Spill Kits
Stations
2 Kits
None
Stored Inside
South Loading
Wooden Boxes/ Pallets
Shipping & Storage
Dock
Various
Non -Reactive
NA
Chips (Metal Cuttings)
Recyclable Waste
Chip Tailers
Ivarious
jUnlikely
I Covered Trailer
Recyclables
Transfer to
Cardboard
Recyclable Waste
Container
Various
Hopper
Covered Container
Recyclables
Transfer to
Plastic
Recyclable Waste
Container
Various
Hopper
Covered Container
Recyclables
Transfer to
Wood
Recyclable Waste
Container
Various
Hopper
Covered Container
Waste Product- Spill
Transfer to
Sawdust (sorbant)
Cleanup
Drum Storage Area
Various
Truck
Sealed Drum
Waste Product- Spill
Transfer to
Pad and Socks (sorbant)
Cleanup
Drum Storage Area
Various
Truck
ISpill
Sealed Drum
Waste Product- Spill
n,..i, r..,, _nt Mix
„y v
cio�
�..
anon—, nsT
�,,.,.,., a
��
or i ea%
I�......,
Covered) Contained ST

ANALYTICAL REPORT ;-r; Tsc
L-a e S-C 1 E.N-G E.5 November 30, 2016 ylux-
i
TBL Laboratory i
I
{ Sample Delivery Group: L873538 '
' Samples Received: 11/18/2016 b5
Project Number: TBL-27427 -
Description: Town of Red Springs i
RECEIVED
T
Report o. Pam Hester JAN 0 3 2017 I
P.O. Box 589 s
Lumberton, NC 2$359 CENTRAL FILESDWR SECTION
i
I
Entire Report Reviewed By
J
Darren Reeder
Technical Service Representative
unh,to Me lle ° t' ed —ESHEPOr, Shallbe
reproduced, except In full, without written approval of the laboratory. Where applicable, saroplipg coriducted by ESc is
g�; �' performed per guidance proMed in laboratory slandard operating procedures: 060302. 060303. and 060304. I., .

TABLE OF CONTENTS
ONE LAB. NATIOWDE.
'Cp: Cover Page
27c: Table of Contents
3Ss: Sample Summary
4Cn: Case Narrative
5Sr, Sample Results
EFFLUENT L873538-01
r'Qc: Quality Control Summary
Gravimetric Analysis by Method 2540 C-2011
Wet Chemistry by Method 130.1
Wet Chemistry by Method 1664E
Wet Chemistry by Method 300.0
Wet Chemistry by Method 350.1
Wet Chemistry by Method 351.2
Wet Chemistry by Method 365.4
Wet Chemistry by Method 420.4
Wet Chemistry by Method 450OCN E--2011
Mercury by Method 245.1
Metals (ICP) by Method 200.7
Metals (ICPMS) by Method 200.8
Volatile Organic Compounds (GC/MS) by Mr,thod 624
Pesticides (GC) by Method EPA 608
Polychlorinated Biphenyls (GC) by Method EPA-608
Semi Volatile Organic Compounds (GC/MS) by Method 625
7GI: Glossary of Terms
a„ _ o
r-u: i-�CCieuitaii0iia cac %.uiaifOnS
9Sc: Chain of Custody
I
2
3
4
5
5
9
9
10
11
12
14
15
16
17
18
19
20
22
23
26
28
29
33
J4
35
ACCOUNT - PROJECT �15DG. DATElTIrdIE PAGE,
,TBL Laboialory' TBL-27427 L873538 1113Dlt6 08 t4 2 of 37

0
EFFLUENT - L873538-01 WW
SAMPLE SUMMARY
Collected by
Brian Stephens
ONE LAB. NATIONWIDE.
Collected date/time Received date/time
11117P6 09:30 11/18/16 09:00 r C
p
Method
Batch
Dilution Preparation
Analysis
Analyst
dateltime
dateltime
Gravimetric Analysis by Method 2540 C-2011 Mw �
WG928463
1 11/21/1614:17
11121/1614;50
MMF
Mercury by Method 245.1
WG927925
1 11/19/16 05:46
11/21/16 15:14
NJR
Metals fIfP) by Method 200.7
WG927935
1 1171811613:23
11118/16 22:46
ST
Metals (ICPMS} by Method 200.8
WG928193
1 11/19/16 07:00
11121/16 01:13
LAT
Pesticides (GC) by Method EPA 608
WG929028
1 1V2311616:34
11/2511610:06
VKS
Polychlorinated Biphenyls (GC) by Method EPA-608
WG930296
1 11/23/16 16:34
11/29/1610:50
JNS
Semi Volatile Organic Compounds (GUMS) by Method 625,
WG928430
1 11/22/16 01A2
11/22/16 20:02
JF
Volat#le Organic Compounds (GUMS) by Method 624
WG928854
1 11124AG 06:01
11/24/16 06:01
LRL
Wet Chemistry by Method 130.1
WG928658
1 11122/1612:51
1112211612:51
JER
We; Chemistry by Method 16648
WG928805
1 11/22/16 08:21
1V2211611:44
SHG
Wet Chemistry by Method 300.0
WG927944
1 11/18/1616:56
11/18/1616:56
SAM
Wet Chemistry by Method 350.1
WG928551
1 11121/1613:13
11/21/1613:13
DR
Wet Chemistry by Method 351.2
WG928067
1 1111811617:53
11/21/1610:54
JER
Wet Chemistry by Method 365.4
WG928120
1 11/18/16 17:54
11/21/1610:24
JER
Wet Chemistry by Method 420.4
WG928071
1 11/22/16 09:33
11/22/1615:05
ASK
'Wei Chemistry by Method 450OCN E-2011
WG9296i9
i W25116 10:22
1V2811612:18
JER
ACCOUNT ,,PROJECT SDG DA7ElfIME PAGE
` 2L873538TBL ,. 375TBLaboratory; . i "

CASE NARRATIVE
ONE LAB. NATIONWIDE. V
All sample aliquots were received at the correct temperature, in the proper containers, with the
i !7
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
ITC
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample resu€ts. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by -the
55
r
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
Fr
rGl
Darren Reeder
VAi
Technical Service Representative
5c
i s ACCOUNT _ PROJECT -- '5DG .'DATE/TIME, .L. PAGE: -
TI3 Laborato TBL 27427 L873538 1
ry 1130/15 0814i 4 of 37,.+

EFFLUENT SAMPLE RESUL'TS'- 01 ".' ONE LAi3,'NATIC3NWIDE.'
Coileczed'dateli!me: 411l17ti6-09:30 L873538.
Gravimetric Analysis by Method 2540 C-2011�
Result Qualifier RDL Dilution Analysis Batch LP
Analyte mgA mgA date / time
Dissolved Solids 140 10.0 1 111211201614,50 WG928463 YC
Wet Chemistry by Method 130.1 I3S5 i
Result
Analyte mgll
Hardness, Total Img1L as CaCO3) 40.3 —
Wet Chemistry by Method 1664B
Result
Analyte mgA
Oil & Grease [Hexane Extrj - ND
Wet Chemistry by Method 300.0
Result
Analyte mgll
Nitrate as (Ni 8.39
Nitrite as(N) ND
Wet Chemistry by Method 350.1
Result
Analyte mg/1
Ammonia Nitrogen ��— ND
Wet Chemistry by Method 351.2
Result
Ana lyte mgA
Kjeldahl Nitrogen, TO ND
Wet Chemistry by Method 365.4
Qualifier RDL
Dilution
Analysis
Batch
I--
mg/l
mgll
date !time
dale-
1
201612:51
WG928656
Fln
QuaEiBer RDL
Dilution
Analysis
Batch
mgA
date ltime
FC]
5.26�-
1 .••-111221207611:44
WG928805
GI
Qualifier RDL
Dilution
Analysis
Batch
mgll
date 1 time
AI
0,100 1 11/18/201616:56 WG927944 5
0.100 .1 111181201516:56 WG927944 - Sc
Qualifier RDL Dilution Analysis Batch
mgA date! time
0.250 - 1-- 11121/201613:13—�WG928551
Qualifier RDL Dilution Analysis Batch
mgA date 1 time
0.250 1 111211201610:54��� WG928067
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte mgA
mgA
date! time
Phosphorus,Total 0.449
0.100
1
111211201610:24
WG928120
Wet Chemistry by Method 420.4
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte mgA
mgA
date / time
Total Phenol by4AAP ND�
0.0400
--1
11/221201615:05 ---_--
4VG928071
Wet Chemistry by Method 450OCN E-2011
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyze mgll
mgA
date / time
Cyanide ND
0.00500
1
11128/201612:18
WG929519
Mercury by Method 245.1
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte mgll
mgll
date 1 time
Mercury ND
0.000200
1
11/21/201615:14
WG927925
onn ICl'T SDG_ fin TE mu.�. - nnr_C. -
�rr �.
TBL-27427 L873538 11/30116 08:14 .5 of 37

E F FL U-E•N.T
:•'
- Collected.dateltlme:
1.1/17/16 09`.3.0
Metals (ICP) by Method 200.7
Result
Analyte
mgA
Antimony
ND
Arsenic
ND
Ber" um
un
Cadmium
�ND
Chromium
ND
Copper ... •
ND
Lead
ND
Nickel
ND
Selenium
ND
Silver_.
,. ND .
Zinc
ND'
Metals (ICPMS) by Method 200.8
5,4 M P L• E R;E S U L'T S .- :0.1' : ONE LAB+NATIOiVWIDE.
L873538
4ualifier RDL
mgll
0.0100
v 0.0100
0.00200
0.00200
0.0100
0.0100
0.00500
0.0100 .
0.0100
0.00500
0.0500
Dilution
Analysis
Batch
date 1 time
1
11/18/2016 22:46
WG927935
:." '1 .,
1
11/18/2016 22:46
11.118,1201.6 22:46
" WG927935
IhIC927925
1. "•
1V1812016 22:46
WG927935
1
1111812016 22:46
WG927935
.1
11/1812016 22:46
WG927935
1
11/18/2016 22:46
WG927935
1
'11/18/201622:46
WG927935
1
11/18/2016 22:46
WG927935
1 `;
1111812Q16 22:4e'-'
.: WG927935"
i
1V1812016 22:46
WG927935
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mgll date 1 time
Thallium --- ND�-_ 0.00100� 1 11/21/2016 01:13 WG928193
Volatile Organic Compounds (GC/MS) by Method 624
1
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte
mgll
mgll
date 1 time
Acrolein
ND
J4 0.0500
1
11/24/2016 06:01
WG928854
Acrylonitrile,
ND
40100-
i.i
111241201606:07
WG928854 '.
Benzene
ND
0.00100
1
11/24/2016 06:01
WG928854
Brornodlchloromethane
0.00137' 0.60100
1
11124/2016DUl ..
WG928854
Bromotorrrl
ND
0.00100
1
IV24/2016 06:01
WG928854
Bromometharie.:
ND
D.005oo
,1 .1112412011606:07
.',
WG928854
Carbon tetrachloride
ND
0,00100
1
11/241201606:01
WG928854
Chforobe izene ` • .
ND
-0.00100
7 ,
11124/2016 06:01':
WG926854
Chlorodibromomethane
ND
0.00100
1
11/24/2016 06:01
WG928854
Chloroethane, % '+
ND
1}`s.
11124/2016OU'l
WG926854
•
��
{.'OA0500
; ,
2-Chloroethyl vinyl ether
ND
0.0500
1
1V2412016 06:01
WG928854
ChI0Y6i0rm- • r _
-•, ? ND
- - _ 0.00500,_
1 -- .,1V24/2016
06.01
WG9281 4 •
1 ._ . �,.., t _ , . , ' _ _ _,,,.', •,4
Chloromethane
ND
0.00250
1
11/241201606:01
WG928854
1,1 Dlc WQI[hane
ND
6.00100
1 ' .
11124I2016 06:01
1.2-Dichloroethane
ND
0.00100
1
111241201606:01
WG928854
1,1 Dlchloa oethene '-
ND
0.00100
1 <
11/2412016 06:Oi
•°;WG928859
y
:
; ;
} ,'
y F`
trans-1,2-Dichloroethene
ND
0.00100
1
lV2412016 06:01
WG928854
1.2-Diciil6ropropane ' .
ND
0,00100
i
1V241201606'.03
'`-.WG928854
cis-1,3-Dichloroproperle
ND
0.00100
1
1V2412016 06:01
WG928854
�11
111241201606:Dinns13Dchlorapropene 3
;WG928854ND..
;,
Ethylbenzene
ND
0.00100
1
11/24/2016 06:01
WG928854
Meth ylene,CWcride
ND
O.00500
1 '
112412016 06:01
WG928854
"
1,1,2,2-Tetrachloroelhane
ND
0.00100
1
11/241201606:01
WG928854
Tetrachloroethene
:ND
0.0010Q
1 ; '
1112412016,06:01
WG928854
- r
Toluene
ND
0.00500
1
11/24/2016 06:01
WG926854
1.11 Tnchloroethane ,
ND
., *, '
-0:00100
; ;= 1
1112412D1601
6:0
WG9 :::28854
1.1,2-Trichloroethane
ND
0.00100
1
11/24/2016 06:01
WG926854
Trichloroetliene'
ND '.
: 0-OD100
1'
111741701611F01
W(97RR54
�a .-
>.
Vinyl cWoride
ND
0.00100
1
11/24/2016 06:01
WG928854
109"
" �` 900115
11/�4/101B060T'.
'WG928854.
;;?,(SJToluerred8
(S) DibromoRuoromelhone
103
79.0-121
1129/1016 06:01
WG928854
(S) 4 r ramofluorobertzene
: 7D6 ;
801 126 'r
; '
1U2912016 06:01 `
,WG928854
- - -. -
a
Arrol INN - ,. ❑pn i`CT
iSvv DAT`rrl��G
•! , s--r - r... mot.
I F76C L'aboralory TBL=27427 L873538 11/30/16 08:14' a 6 of 37

1
E F F LU ENT: : ' S,A M P L E , R,E -O L T S -' 01 ONE LAD: NA710rvwlbE. '
ColleEted,datettim6: "4111'/16749:34 L873538_
Pesticides (GC) by Method EPA 608
Analyte
Result Qualifier
mgA
ROL Dilution
mgA
Analysis
date ! time
Batch
C?
Aldrin
NO
0.0000500 1
1V251201610:06
WG929028
7
^Tc
Alpha BHG
`', ND
0.0000500 r 1 _
11125/201610:Dfi
_ '.WG929028
y
Be:aBHC
Delta BHC`
ND
�ND
00000500 '
0.0000500 1:_'
11125i201610'D5
'
1V251261610:&4:-
WG929028r-
WG929028
3
SS
Gamma BHC
ND
0.0000500 1
11/251201 6 10:06
WG929028
Chlordane
NO
0.000500 1
111251201610:06
46929028 '
rq
4,4-ODO
NO
0.0000500 1
IV25/201610:06
WG929028
4,4-1)DE .
ND
O.00D0500 1 1
11125/2016,16:06
WG929028
4,4-DDT
ND
0.0000500 1
11125/201610:06
WG929028
Dieldrin
ND E
0.0000500 1,•:,
a11125/2016IoN •-,
-,. WG929028_ <
Endosulfan I
ND
0.0000500 1
11/251201610:06
WG929028
F
QC
Endosulfan II
NO
0 4000500 1
111251201610:06
WG929028
Endosulfan sulfate
ND
0.0000500 1
111251201610:06
WG929028
Endrin.
. `'ND
0.0000500 . : 1 '
11/251201610:06
WG929028
Gl
z.'
. .
-
Endrin aldehyde
ND
0.0000500 1
11/25/201610:06
WG929028
Endrin ketone'" -..
N.D
0 0000500' 1 ,'
1V251201610:Ofi
WG929028
_rAI
Hepiachiar
ND
0000500 1
11125120ifi 10 06
WG929026
Heptact}ior,`epoxide .'s
' N0. s ':
O.O066560: 1`
r'.i1125120161006
wG929028 '.
- �M
y
Hexachlorobenzene
NO
0.0000500 1
11/251201610:06
WG929028
SC
Methoxychlor
ND -1r
0,0000500 1.,'
1112512016 10:06
` WG929028 -
'
Toxaphene
NO
0,000500 1
11/251201610:06
WG929028
(SJPecnchlaro6lphenyl'
`• _ ` 7t5
1.
10.'0-156
s IP2512016 10:06
t wG929028
^
(5) Tetrachloro-m-Wene
520
13.9-137
IV2512016 1006
WG929028
Polychlorinated Biphenyls (GC) by Method EPA-608
Result Qualifier
ROL Dilution
Analysis
Batch
Analyte
-_-----_--ND
mgll
--��-�•�•� ��--•-4Y0.000500
mgA
-1-�111291201610:50
date 1 time
���•--WG930296 Y_.-----�.------�-_----^-•--w--
PC81016
PC91221
ND - .
O.00D500 1 -
11/29/201610:50
WG930296
PC91232
NO
0.000500 1
11/291201510:50
WG930296
PCB 1242 -
NO
0.f)DD500 "' - : 1 ': +'.'
�'11129I2016 i0 50
WG930295
PCB 1248
NO
0.000500 1
1V29/201510:50
WG930296
PCB•1254`
1"' ND,
;, 0.000500_':` 1 -
11129I20161050_',. WG930296'
a
PCB &0
ND
0.0001500 1
111291201610:50
WG930296
:"(veco hlaro6iphenyl 75.8
100156 •` r
11129120161050
WG930296
(S) retrochloro-m-),ylene
672
13.9-137
W912016 10.'50
WG930296
Semi Volatile Organic Compounds (GC/MS) by Method 625
Result Oualifier
ROL
Dilutio^ Analysts
Batch
Analyte
mg/l
mg/l
date 1 time
AeenapMhene -
ND
0.00100
1 11/22/2015 20:02
WG928430
Acenaphthylene
ND'
0.00100
1 171221201fi20:02
'WG928430 k.
-
Anthracene
NO
0.00100
1 11122/2016 20:02
WG928430
Benzidine,
NO ' ,,
0.0106"
1 11122/201620:02
:'WG92$430
Benzo(a)anthracene
ND
0.00100
1 1V22/2016 20:02
WG928430
Be'nzo(b)flucranthene-
ND '.+
0.00100
1 .11122/201620:02
WG92843D
Benzo(k)fluoranthene
ND
0.00100
1 11/22/2016 20:02
WG928430
Ran7nfg h i;raNlana
`. •Nrl .
.n nn5nn :..
-. 1 - 11n J17r116 7Q•fl7
' WC-
.._ ... - -
,
,
__410
.
Benzo(alpyrene
ND
0.00100
1 11122/201620:02
WG928430
Bi (7chldretho'ky)methane
ND
: rr0.0100 �r
1 :11l22120162D:02'
WG928430
Bis(2-chIoroethyl)e[her
NO
D.o100
1 yW221201620:02
WG928430
Bis(2-chloroisopiapyllether
ND :
. • 0 0100
1 :'` ;1V2212016 20-02.
WG92843D 3 =
_
_
4-Bromophenyl-phenylether
ND
0.0100
1 11/22/2016 20:02
WG928430
2-Chloronaphthaiene _ = a '
ND•`. •
6.00140
i _t:i W2_2l2016 20:02:-
WG928430
4-Chlorophenyl-phenylether
ND
0.0100
m
1 1112212016 20:D2
WG928430
h�
ACCOUNT PROJECT SDG DATEhW . PAGE':,I =
TBL La ` fay o536L87f 37boratoryT8L 27427 /6t

ONE LAB. NATIONWIDE:
EFFLUENT SAMPLE RESULTS - 01
Ccllected'Cateltime: 11/17/16 09:30 L873538'.
Semi Volatile Organic Compounds (GUMS) by Method 625
Result Qualifier
RDL
Dilution Analysis
Batch
Analyte
mgn
mgA
dateltime
Chryseneyr
ND' •
0.00100`
1
.11/221201520:02
WG928430
Dibenz(a,h)anthracene
ND
0.00100
1
IV22/2016 20:02
WG928430
3;3Dlchlor6kieniidine;
-ND
0.0100.
=1.
'. ;11/2212016'20:02:
•: WG928430
2,4-Dinitrotoluene
ND
0,0100
1
11/22/2016 20:02
WG928430
2,6-Di iitrotoluene ""
ND
0.01D0.,
' 1
Y 1i122/2015 20:02 '
" WG928430
Ruoranthene
ND
0.00100
1
11/22/2016 20:02
WG928430
Fluorene-ND.-
.0.001p0
1.
111221201620A2'
" WG92843D
;
Hexachlorobenzene
ND
0.00100
1
11122/2016 20:02
WG928430
Hexa6loro4,31butadiene
ND
0.0100
1
,1112212016 20:02' .'
W628430
'
Hexachlorocyclopentadiene
ND
0.0100
1
11/22/2016 20:02
WG928430
Hexachloroethare
ND
: 0.0100
1.
.'-111221207620:02
WG92843D
Indeno(1,2,3-cd)pyrene
ND
0,00100
1
11/22/2016 20:02
WG928430
Isophorone
ND
0.0100
' 1
1112212616 20:02
WG928430
Naphthalene
ND
0.00100
1
11/22/2016 20:02
WG926430
Nitrobenzene, ".
ND
• 0.0106
1
11122126% 20:02
WG928430
n-Nitrosodimethylamine
ND
0.0100
1
11/22/2016 20:02
WG926430
n ivi,w»viNiienyiai7iir0,"s '
ivv,^
D 0100
-' i
1ii22r'2viti 2v:C2
n-Nitrosodi-n-prGpylamine
ND
0.0100
1
11/22/2016 20:02
WG928430
Phenanihrene
;'ND
a DD100..'
1`
., '11122/201620:02
iWG928430
Benzylbuiyl phthalate
ND
0,00300
1
tV2212016 20:02
WG929430
Bis(2=eihylhexy1Jpfi-thaIat-e '
.-, ND :
0.0030.6
1;
11/22/2015 20:02
WG928430
Di-n-butyl phthalate
ND
0.00300
1
11/22/2015 20:02
WG928430
Diethyi phthalate ..
ND
0-00300,
. 1
:' 11122120i5 20A2
WG928430
Dimethyl phthalate
ND
0.00300
1
11/22/2016 20:02
WG928430
Ds n 6clyl phthalate .'
ND _
0.00300
1
= ' 11/22/2016 20:02'
WG928430
= 1
Pyrene
ND
0.00100
1
11/22/2016 20:D2
WG928430
1,2,4 Trichlorotieniene'
ND
0.D100
'1 -
1ll22120t6 20:02
WG92843D
" c„ ? `
4-Chloro-3-methylphenol
ND
0.0100
1
11/22/2016 20:02
WG928430
2-016rophen6l :' ' _
ND
0.0100
1
IV2212016 20:02'
~WG92843D' '
2,4-Dichlorophenol
ND
0.0100
1
11/22/2016 20:02
WG928430
2,4-DimP[hy4phenpl' -
'ND :
U.U1UU
1
i'u22120ib 20'02
WG9228430
4,6-Dinitlo-2-methylphenol
ND
0.0100
1
11/22/2016 20:02
WG928430
2,4-DinitrophenGl `, :1
� ND
: 0.0100.
1
7112212016:20:02
WG928430
2-Nitrophenol
ND
0.0100
1
1V22/2016 20:02
WG928430
4-Nitrophenol
ND."
D 4-
0.0100
1 {
20:02
-
.,11/22/2016
;:WG928430
Pentachlorophenol
ND
0.0100
1
1V2212016 20:02
WG928430
Phenol;ND
0.0100
1
i1122/20i620:02
VJG928430
[
2,4.5-Trichlorophenol
ND
0.0100
1
11/22/2016 20:02
WG928430
1,2-Diphenylhydraiine`
ND
O.OtODy
111221201620:02
; rWG928430 `;•,
1 >,., ;," i.
(S) 2-Fluoropheno!
68.7
10.0-77.9
11/22/201610:02
WG928430
(SjPherrG!-d5 t
55.2
5.00`701
11/22/201620:02
(S)Nitrobenzene-d5
77.6
21.8-123
111221201620:02
WG928430
(Sf2-Fluorobiphen
86.6 s
29 5'131
` `' '
W22/201610:OZ
„ WG92843D -;
" 't
(S) 2.4,6-Tribronrophenol
95.2
11.2-130
*2212016 20:02
WG928430
(5)p-Terpheny.- 4 -94.7• ; - 293137, ib/ 21201620:02 ;,. W6928430 f
ACCOUNT PROJECT SDG DATE/TIME:tc_. PAGE:,
„ TBL Laboratory TBL 27427 L873538 t1%30rt6 08a4 . 8 of 37_

•Y'C(DNTROL``SUMrMARY ONE LAeNAT�O,'ID,E
WG928463' 6UALE7
Gravimet ric..Analysis by Methbd 2540.C-2011 . - L873538.01
Method Blank (MB)
(Ma) R3180255-1 1V2tJ1614:50
M8 Result
Analyze M91
Diss0ed Solids U
MR Ouabrier MR MDI MR RDL
rnwl m9n
2.82 too
L873317-03 Crfglnal Sample (OS) • Duplicate (DUP)
(OS) L873317-03 11121l16 14:50 - (DUP) R31802SS-4 1V21/16 14:50
Original Result DUP Result Dilution DUP RPD DUP Oualirieo DUP RPD Limits
Analyte mgA mgA % %
Dissolved Solids 3350� 3350 _ 1 0.000 — 5 —
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
{LCS) R3180255-2 IV2V1614:50 • (LCSD) P13180255-3 1112VIG 14:50
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Oualiriel LCSD OualiOer RPD RPD UnnJts
Analyte mgA mgrl mgA % % % % %
Dissolved 5ofids BBoo 8520 _ 8540 F� 96-8 µ 97-0 �85.0.115 — 0.234 -- 5 �
%ACCOUNT: PROJECT - • SOG - OAYElrIME e - PAGE
' TEL Laboratory TRL-27427 L873538 + 1V3071608:14 � r _96137

WG9.28658.', QUALITY CONTROL -SUMMARY oNeiAB.NATIONWIDE..-`
W er'ChemistrY' by:Method.130-1' - - - - ,. - - 1.873538'-01
Method Blank (MB) ❑
(M6) R3179962-1 IV221161235
MB Result MB OuaVer MB MDL MB RDL
Analyzemo mg!! mgA ,___. .____ .—,__��.___.._..._._...,_,_. .._,---.__.. .... __........_._.--_..•....•..�..--.,_„,,..,,,., _Y.___--,.._�__.__ ,� C
Hardness __...�.�..,�. 264 J .""-".._.._ i
L872538-02 Original Sample (OS) • DupliCate (DUP)
(OS) L872538-02 IW:M6 1239 • (DUP) R3179962-4 11/22I161140
Original Result DUPResult Dilution DUP RPD DUPQualifier DUP RPD Limits
Anatyte mgA my
Hardness — 166 165 1 1,0C 2C�
Laboratory Control Sample (LCS) • Laboratory Contra! Sample Duplicate (LCSD)
(LCS) R3179962-2 W2 ,16 1235 • (LCSD) R3179962-3 11122/16 12:37
Spike Amoum LCS Result LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits LCS Ouallflet LCSD Qualifies RPD RPD Limits
Anayze mgA mgA nv
%
%
% % %
Hardness 150 146 146
97.0 —
97,0
85.0-115 0000 20�
-ACCOUNT I-' PROJECT SDG DATElrIME - •fPAGE._
1 TBL Laboratory ' - . •' TBL-27427 ' L873538 - IV30AG o8 14 - 10 a137. - -

ING92,8805 "QUALItt CONTROL SUMMARY 4 oNeL'ne lvAri
W ef'Chemis try. `by Mefhotl 7664B- - • • L873538,01. - - • - , _ _ _, -�, -„ , ,, - - ,� "-ir_. ,� „ _ __
Method Blank (MB)
(M9) R3179876-1 11/22/1611:38 (•��
ME Result ME DUalirier ME MDL ME RDL
AnaMe mpg mgA m¢I—
011 G Grease (Hexane Exi l U 1,16 W 5.00
s
55
Laboratory Control Sample {LCS} • Laboratory Control Sample Dtipllcate (LCSD)
(LCS(R3179876-2 W2/161112•ILCSD)R3179876-3 1V22/16it.36 �Cn
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits—
Analyte mgA mgA mgA % % % % % 5f
Oil & Grease (Hexane Exa)40,0 -- 367 37.5 --� 91.8 � 93 8 78.11-114 ...._..�._�_-� 2.16 � -� . 20—
..wuv.
�GI
AI
BSc
— , - .._ _ r _._�__._._—_ ____ --T --.. .•k` � ._._ ti ! r � PAGE ..
ACCOUNT PRDJECT - - SDG DATEfT1ME I of 37
-
•Tahoratory TBL 27427 - - t873536
BL L

_�Wet•Chemist�Y-tiy,Meth od 900.0 '
Method Blank (MB)
(MB) R3179298-1 1YIW16 GBA8
MB Result MBaUOifier
Analyze mgA ...__�.
Nitrate U
Nitrite _ '+,.. '- tJ, • V .
QUYALITY'.CONTROL SUMMARY
-;L 873538 ., .. ..
MB MDL MR RDL
m9A M/I
0.0227 __--0.100�_.�—'______.-__._
L.M7 59-41 Original Sample (OS) • Duplicate (DUP)
-t ONE LAB NATIONWILIE . I ;
�..
ti.)7
R 1Tc
Ss
aCn
(OS) LB73559-01 ,1116fi6 13:51 - (DUP) R3179298.5 11/18116 14:06
Original Result DUPResult Dilution DUPRPD
OUP Oualifier DUP RPD Unifts
~�
rsr
Analyte mgA mgA %
%
karate 6.42 6.17 _ 5-- 4
20
Nitrite "•ND• D.00p 5 0 _
20
�GI
L873558-05 Original Semple (OS) ` Duplicate (DUP)
(OS) LB73558-05 1111EV1616:25 • (DUP) R3179298-6 11/18A616741
Al
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD Limits
mgA A e NDA %
Anatyl --^_
%
&0
ND t 0
20
-- --- — 5t
kikile ;,-ND -•_t.. 0000.. 1.- .. 0'
.,2p•,
i
Laboratory Control Sample (LCS) • Laboratory COntrOl Sample Duplicate jLCSD)
(LCS) R3179298-2 IV18116 09.03 • (LCSD) R3179298-3 11N8116 09.,9
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS OualiOer LCSD OueliOer RPO RPD Limits
Analyze nVA mgR mgA % % % % %
N;trale --------8.00 � 0.19 -- W 9-27 ;�w._............._103_.,.............. w110........------.,..........._... O ..._.�.— 20 _.........-.....__._ .,...._.�-,�_......�
kitrile "-`� '•,�0.00 7,93 7.94 : ;99� - �99:- ' 90110 • - 0 . 20
L873559-04 Original Sample (O5) • Matrix Spike (NIS)
(OS) LB73559-04 11/18/16 132Q - (MS) R3,79298-4 1013116 1336
SpNeAmouni OligmalResult MSResult MS Rec. Dilution Rec. Limits MS Qualifier
Analyze mgll mgA MW % %
wtraie 6.00» t34 6.24� gg --- t
Nitrite�5.01 "•106 -. -"1 ,,96-120s :i-
r
ACCOUNT --PROJECT SDG - DATElrIME PAGE: �'.
,TBL Lahorauxy - - TDL-27477 5 L1173538 1V30115 68:14 �120137

WG92;7944 QUALITY -CONTROL SUMMARY:,
flNELAB: NA71Dd4VIDE•x."
Wet. Chemistry"6y Me1had300.0 .- .. L873538-01
L873559-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Dilplicatc, (MSD)
(OS) L873569-03 11/18116 19:15 - (MS) R3179298-7 11/18/16 1930 - (MSD) R3179298-8 11118116 19:46
}J
Spike Amount Origlnaf Result M5 Result MSD Result MS Rec. MSD Rec. Dilution Rec. Lim61s M5 oualifer
MSD Oualifler RFD RPD Limits
Anatyte mgA MV mgA mgA % % %
% %
Nltoate 5,00 NO 518 5-05 104 101 1 W120
NiHite 5.00 N0. 5.25 -5.23 " ]05 �105 - - -1 90-120 �
-Ss
Y 3 20
0 24). -
�
Fn
.,SL
rGI
'AI
r—�
Sc
ACCCl1NT 2 PROJECT.. r - `. rSDG • 51 CATEITIMIJ= a t - PAGE
r_ A •r- k
r L : ' TBL'Lehoratory :�_ ' ,, a ';! TDL-2Z427 y� , L073538 1V3011fi OH:14 F - - - 13 of 37

WG9285'5,1'' -` ' 'QUALITY CONTROL,SUMMARY.
``'` G 0NEUA6 NATIOP;WDF'.
We[ Criemistiy pyMethod 350.1:• - _ - - : L873539:01
Method Blank (NIS)
IMBI R3179626-1 11121116 12:51
MB Result MB Qualifier MB MDL MB RDL '
Analyze mgA mgA mgA
....
Ammonia Nitrogen U 0.03E 0.250
3S5
L873511-03 Original Sample (05) • Duplicate (DUP)
(051I 873511.03 1112VI612:58 - Q IP) R3179626-4 1417r116!S:0 1
Cn
Original Result DUP Result DiluBon DUP RPD DUP Qualifier DUP RPD Limits
Analyze mgn mgll % %
4Sr
Ammonia Nitrogen ND O.D00 1 0 20
R
L873552-02 Original Sample (OS) • Duplicate (DUP)
(05) L873552-02 11121/16 13:17 • (DUP) R3179626.6 11/21/16 13:19
GI
011glnalliesull DUPRasult Dilullon OUPRPD DUPOuaUer DUPRPDUmits
Analyze mgA mgA % %
❑
Ammanla Nitrogen u 0.D00 1 0 20
F_ I
Labcilatciv Control Sample (LCS) • Labor6tory Conliol Sample Duplicate (LCSD)
(LCS) R3179626-2 11l2U16 12:52 - (LCSD) A3179626-3 IV2 V16 12:54
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyle my mgII mgll % % % %
%
AmmunlaNitrogen 7.50 699 _._... 7.04 93 T T 94 90-110_.. ._:.._..._.��.�.......�«.....�. 1
20
1.873523-01 Original Sample (OS) - Matrix Spike (MS)
(OS) L873523-01 1V2VI613-02 - (MS) R3179626-5 R72V1613:03
Spike Amount Original Result k4S Resull MS Rec, Dilution Rec. Limits MS Qualifier
Analyze mgll mgll m911 % %
Ammonia Nitrogen ID.0 _ ND 9.54 93 1 90-110-��--_..-
�• w___.___-��---
1-873556-01 Original Sample (OS) - Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(IDS) L873SSG-01 110111613:30 - (MS) R3179626-7 1112VI6 13:32 • (MSD) R3179626-8 1V2VI6 1133
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec, Dilution Rec. Limits MS Quallfier
MSD Qualifier RPD RPD Limits
Analyze mgA mgA mgA mgA % % %
_
% %
Ammonia Nitrogen 10.0 NO 9.52 9,54 95 95 1 911-110 ^�
�- 0 M� 20
.. -ACCOUNT y• PROJECT �SDG..- r _3 DATUTIME
TBL tab acalory' • > -' ` _ • TBL-27427 i r L873538 ° ' ,1VjOA6 0814 �,14 f 37

WG9280 .'',-;
QUALITY CONTROL'SUMM:ARY.
:`oJE LA NA71EJNwIDE::' .
Wet.Chernlstry by Method 351.2
1-873539-111.
_ - ram, „_3 .••- . " - , .
Method Blank(MB)
h"}�
(M8) R3179573-i 112U76 1035
MI3 Result Ma Qualif+er ME MOL M8 RDL
Analyte mgA mgA mgA
� ITC]
KJeloahl Nitrogen, TKN U 0.0350 0.250
_
35s
L873247-01 Original Sample (OS) . Duplicate (DUP)
/
(OS) L873247-01 11J2 Vl6 i0:41 • {DUP) R3179S73-4 11/21116 10.42
.... -
^'
Cr1
OvglndResult DUP Result Dilution OUPRPD
DUPDuaidier DUPRPDLimits
Anayte mgn mgA %
%_
Sr
Kjeldahl Nitrogen, TKN 1.62 �i-69 1 4.00
20
l_a5oralory Control Sarrlpie (LCS) • Laboratory Control Sample
Duplicate {LCSD)
'
(LCS) R3179573-2 1V21r16 10:36 - (LCSD) R3179573-3 112V1G 1D:37
GI
Spike Amount LCS Result LCSD Result LC5 Rec.
Anayte mgA mgA mgA %
-
KSD Rec. Rec. Limits LCS Oualitier LC5D Oualifier RED
% % %
~ � - '�--
RPD Limits '
% _
KJeldahl Niuogen TKN..,._ 17.4"—*—---16,8 16.4 970
�-_
� 94-0 9D.0.116 2.00
20
BSc
L87353a-Oi Original Saii)ple (05) • hAatrix Spike (IVi51
JOS) L873536-01 1I21,176 10:54 - (MS) R3179573-5 1V21l16 10:55
Spike Amount Original Result MS Result MS Rec.
Dilution Rec Umits MS Duatlnel
Anayte mgA mgA ingn %
%
--- 99.0
KWId hi NArogen, TKN 5,00 N0�_- 4.96m
1 � 9 0.a110
ACCOUNT: Pii OJECT ',' _ - SDG: _ DATEfrimE y ,PAGE:
r ,TBL Laboratory - • TDI.-27427- LII73538 - SV30lS608:14 ,IS"o137

'C,ON'
W,G92$120 QUALITY= '� � ' .' � .�RO.L' SUMMARY
;
orle`LAe.NdTloN4vlQE..,�
Wet'ehemistry byFMelhod'365.4 - - - _ L873538-01
_
1
Method Blank (MB)
(MS) R3179566-2 IV2V16 10:09
t
ME Result MR Oualifer M0 µOL MR RDL
Anayle mgA m9A mgA
------------
Phosphorus,Total U 0.0350 0.100
-----
------------
e
L873511-03 Original Sample (OS) • Duplicate (DUP)
(05) t873511-03 1V21/7610:I5 - (DUP) R3179566-5 1V2V16 10.17
C n
Original Result DUP Result Dilution DUP RPD DUPOualMer OUPRPDtimd
Anatyte mgA mgA % %
__---__---__-.—
Phosphotus,iotal 0.196 0.174 1 12.0 20 ,
L873699-01 Original Sample (OS) • Duplicate (DUP)
7C'I
(05) L873699-01 11121/1612:09 - (DUP) R3179566.8 1V21/161210
0rigmal Result DUP Result Dilution DUPRPD DUPOuallfier DUPRPDtimlts
Anayle mgA mgA % %
' Al
Ptsosphorus.Total _----4.79 _ 4.591 4.00 20
75c
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3179566-3 11121116 10,10 - (LCSO) R3179566-4 11121/le 10:12
SplkeAmount LCSResult LCSD Result LCS Rec. LCSD Rec. Rec. Urrats LCSQualifler LCSOQualifier RPD
RPD Limits
Analyie m91T mgA mgA % % %
%
Phos horus,Tdtal 100 0,935 0.941 94.0 94A 4670 L.00
20
'
L873558-06 Original Sample (OS) • Matrix Spike i iS) - Malfix Spike Duplicate (MSD)
(OS) L873558-06 IV21116 1033 • (MS) R3179566-6 1112i/1610.35 • (MSD) R3179566-7 1V20610:38
Sfte Amount ohglnai Result M5 Result MSD Result MS Rec. M50 Ret. Dilution Rec. Limits M5 Qualifier
MSD Oualiter RPD
RPD tlmlts
Analyle mgA mgA mgA m9A % % %
%
%
Phosphoius,Tolal 2.50 �— 0.729 2.82 2.66 84.0 77.0 1 90.0.110 ~ J6
JG 6,00 —�
20
. ACCOUN1:
- PROJECT: ,
- SDG:
- DATHTL 4E:
fill-Laboretary
TDL-27427
Lt373539
1 Vd0116 C8&14
16 o137

Vi/G928071`. QUALM-Y'r.CONTROCsb-mM'ARY "AT ONE } WIDC.
r
-. Wet Ctie�misLy-h y;Methou 420.4
Method Blank (MB)
(MR) R3180006-1 1V22716 14:51
MBResult MBOuallOer M8MDL MBROL
Anayte mg1 mgn mgll
Total Phenol by 4AAP W U 0.00830 -- 0.0400 -
L872746-02 Original Sample (OS) • DLIpllC8te (DUP)
(05j La72748.02 i,,22,;o 14,54 - (D'Ur1 R3180006-4 11i22ii5 14.55
Orlgnal Result DUP Result Dilution DUP RFD DUP DuafCer DUP RPD Limits
Anayte mgA mgA % 96------___.._---
Total Phenol py 4AAP -- ND ._-_-_- 0.0411 1 22.0 ----- Pi 20
L873538-01 Original Sample (OS) • Duplicate (DUP)
(OS) L873538-01 1V2211615:05 • (DUP) R3180006-6 W22116 15:06
Odginal Result DUP Restil1 Dilution DUP RPD DUP Ouallfier DUP RPD Limits
Anayte mgA mgA % %
Total Phenol by 4AAP NO NO 1 0.000 ~� 20 ..
Laboratory Comrul Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3180006-2 IV22nG 14:52 • (LCSD) R3180006-3 1V22116 14:53
Spike Amount LCS Result LCSO Result I CS Rec, LCSD Rec. Rec. Umtts LCS OuallOer LCSD OuallOer RPD RFD Limits
Analyte mg11 mgll mgn % % % % %
Total Pheolny 44AP 0500
'..,.,- 0525 .__—__ __....... sDS,...»..-,....,......V,,,_, „v...«.._..».»,............_...............�..- LV ,......_
0535
L873363-02 Original Sarnple (OS) , Matrix Spike (1:•1S)
(05) L873363-02 IV22116 14:58 - (M$ R3180006-5 11/22/16 iS:01
Spike Amount 0iiginal Resuk MS Result MS Rec. Dllatlon ReC. Limits MS Ouali4er
Anayte mgll mg11 mg11 % %
lotal Phevi by 4AAP 1.00 NO 0.994 86.0 1 90.0-110 J6
_873554-02 Original Sample (OS) • Matrix Spire (MS) • Matrix Spike Duplicate (MSD)
(OS) LSY3554-02 11122M 1507 • (MS) R3180006.7 11/22/16 15:09 • (MSDI P3180006-8 IV224615:10
SpikeAmoum Original Result MS ReSull MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Ouelikf MSO OualiBer RPD RPD Limits
Anayte mgA mgA mgA mgA A6 % % % %
Total Phenol by 4AAP 1.00 ND 0.881 0.898 «.w 88.0 90.0 1 90.0-1110 J6 2.00 �2D
77,-- r --
ACCOUNY ;. 'y ._ .PROJECT r ' SDGDATE7TIME .4� T PAGE
TBL Latwra:ary ,7 N - L873538- J . IY3fll1608a4 = P - 17 f37;
TBL.2742

k QUALIT-Y, GQ,NTRO� SUMMARY' ' '
WG929619
or1eL D NaTloNvlot. t
._.
-
1
Wet Chemistry by Metho W4, 00CN E-2015 - ''. L873538 01-
Method Stank (MB)
(M8) R3180847-2 1V2V6 17:12
MB Result MB Oualife_r MB MDL MB RDL
AMlyte mg/1 mgll mgfi
---`------
�TC
--------�.—J-...-
Cyanide U 0.001110 0,00500
35s
L874100-02 Original Sample (OS) • Duplicate (DUP)
:OS) i R74100-02 .1l2 on6 12'35 - (CL'. �� R�1w^847 i t-,'&16 12..aa
Odg;nalResult DUPResult Dilution DUPRPO DUPOualKier DUPRPD Limits_---_�--
Analyze mgA mgA % %
-_._--........_....._.—.U43
$r
--�—
..__ 0.345 ..,__. _._. 5 ..._._.1.00--_—.--- 20
Cyaaldc�
-_--—_—---_-
»�
Laboratory Control Sample (LCS) • Laboratory Control San'lple Duplicate (LCSD)
GI
(LCS) R3180847-3 1V28116 12:13 - LCSD) R3160847-4 11128AG 12:14
Spike Amount LCS Result LC50 Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD
Anar/te mgA mgll mgA % % % %
RPD Limits -
%
...
Cyanide 0.100 0.109 0.106 � 109 106 �— 0(115 3-DO
20
oSC
L874354-02 Original Sample (OS) . Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L874354-02 11/28716 1230 • (M5) R3180847-5 lV28716 1231 • (M5D) R3180847-6 1V28A612:32
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec. llmtts MS Qualirer MSD Qualifier RPD RPD Limits
Analyze mgA mgA mgll mgn % % % % %
Cyanide 0.700 ND 9.V9 01,85 ----.�..._.. 3.00 .._._ _20 ---- �---_^_----
rr :ACCOUNT �. - i PROJECT. _ 15RG-- DA7FJTIME
TBI: LaGorai ry _ - ' TDL-27AZ7 ,L073538 1173073608_t4 _ 180137 {

WG9,2,7925, :' =QUALkTy cbNT'ROL_SUMMARY
{L )NEAB.NATIONWIDE. �
Mcrctlry by Method.245 ILt17353 B=01
Method Blank (MB)
C€7
(MB) R3179680-1 1V2t1161438
MB Result MB Oua0.fler MB MDL MB RDL
_
•TC
Ana.yle mgA m9A m9n _—.—....--___._,
---T—...
_„__.__�. —_
.... .._�—_..--._.�.—..__
Mercury— U 0.000049 0.000200
__._.
3
JS
Laboratory Control Sample (LCS) • Laboratory Control Sample Dupllcate (LCSD)
dCn
(LCS) R3179680.2 1V2V1614A0 • (LCSD) R3179680-6 WV16 15t40
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS OuaB4er LCSD Ouafiner RPD
Anatyte mgA mgA mgA %
RPD Limits
Mercury 0.00300 0.00270 0.00286 90 95 95-115 6
20
Li;i�iw-vi viif�iilai $aiTt l;lle (G5) - IVIIdtrix Spike (IVIS) • ivittiiix Spike DtlplicaLe (MSD)
{OS) t87329401 11/2V1614:45 - (M5) R3179680-4 1iRVl6 14A7 - (MSD) R3179680-5 11/21AG 14,49
�I
Spike Amount Original Result M5 Result MSD Result M5 Rec. MSD Rec. Dilution Rec. Limits MS Oualirier
MSD oualifier RPD
RPD Limits
Analyte mg11 mg/1 mgA mgll % % %
Mercury 0.003DD RD 0.00235 D.00232 78 77 1 70-130
1
20
ACCOUNT:>' - - ': PROJECT: - �",SDG: DATEfTIME -. PAGE ,
' TI3L Leho story _ . - TCL-27427 L873538 . 1V3or6 c;6:14 - - t9 of 37

.WG9,279352
- QUALIT:Y`CONTRd' SUMMARY''-
oN laB.'v��iorvwinc
r° '
Metels•(1Cp1.byMethod 200.7. '
1 L873538.03
Method Blank (MB)
_
(MB) R3179281-1 11118116 22:02
MR A -It MR n...liFnr MR MRI
MA ADI
r-1
Analyse mgA MqA
._._ ._. �0,0077
mgn
TC
Antimony__�.._. u
0.0700--------.-•-----------'�---.._.._._�-------------.._..
------�--____�--..--
Arsemc _ U-:0.0064
061oo
3SS
Beryllium U 0,0007
0.002DO
Ladmlum U O.ODD7
Chromium U 0.0018
00100
Cn
Copper " - • U 0.007
0.0100
Lead U 0.002
0100500
4$r
Nickel U 0.0058
" 0.0100
Selenium U 00076
0,0100
Silver •- U ,. - 0.0027 -
', 0.00500
"ItC �.001-1
GI r
Laboratory Control Sample (LCS) • Laboratory Control
Sample Duplicate (LCSD)
(LCS) R3179281.2 11118A5 22:04 - (LCSD) R3179281-3 11118/16 22:07
f�l
Spike Amount LCS Result LCSD Result
Anaryrte mgA mga mg"!
LCS Rec. LCSD Rec.
% %
Rec. Limkts LCS Qualifier LCSD Qualifier RPO
% %
AP0 Limits
%
a
SC
❑
Antimony 100 L02 1.02
102 102
65.115
0
20
Arsenic "..-., t00 1.01 . 1,02
101 - 102
85-115
1
_10
BeryNium 1,00 1,01 1,02
101 102
85-115
0
70
Catlmivm ' ,' -TOO - '• 1,03 1.03
-103 • 103
85-115
1
20
Chromium 1,00 1,04 1,05
104 105
85.115
1
20
Capper ' '. -,'.: too 0.997 �1,00
,
100 100
85-115 '- ;"'.�,
• 0
.20
- -
Lead 1.00 1,02 1,02
132 102
85-115
0
20
-
1.00 : . - 102 ., r- 102.
- .102 - 102 -
85-115' :
0
Selenium 1.DO 1.02 1.04
102 104
85-115
1
20
Slldnr ,::^,..,,, 0200 �� r �,0.185,
;92, .' '. -' �93
..85-115-'..,:
-
1
.. 20', - -
- {- - • 1 -
Zinc 1 DO 100 1-01
100 101
85.115
1
20
L873528-01 Original Sample- (OS) - Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(05) L873528.01 1Y18l16 22:09 • (MS) R3179281.5 1ll18f16 2215 • (M5D) R3179281.6 M 116 22:17
Spike Amount Original Result MS Result
MSD Result MS Rec,
MSO ARC. Dilution Ret. limits
MS Ouelliler
MSD Qualifier RPO
RPD Limits
Analyse mall m01i man
mgA %
% 16_
%
%
Antimony .......^...__.__....._ 1.00 _..__.__.._.No 1.00---
1.01_........,e1GO._.,..�...._�.,.101.W_.......
1 ..,�... 70-130
1-.,_...............
20 ._....�_._.-.�_.�....,-_._.
Arsenic` .. •.. :. • . TOO , --"- : ' NO -- ' 1.02 -
.
I.C4 - - - '102 .
" 104. -_° 1 , 70-136
r
.:'s -, 1
;^ 2pR; . .
- ...� '
13LPAIlum 1.00 NO Too
1.01 100
... -
101 1 � 70.130
� 1
70
Catlmmm Pfi;.1D0 ND- 1.02
103
_703
r
...'102:. ..
,"�;
' -20
Chromium 1.00 0.0105 1.03
1.04 102
t03 1 70.130
1
- ACCOUNT:-
,PROJECT:
' •SOG::-)
OATElTIME
TBL Laboratory -
T0L-27a77•
- - L873530
1V3071G 08.14
.. 20 or 37-

WG92,7935
0UfALITY_:;C.0NTR0L SUMMARY.
or iAJ3.rwaT#oNwIDE`
;,
-
Metali (ICP] by Method 200-7 -
- 1.873536�01
L873528-01 Original Sample (OS)
• Matrix Spike
(MS) • Matrix Spike Duplicate (MSD)
(OS) L873528-01 1171F06
22709 • (MS) R3179281.5 11/18/16 2215 •
(MSD) R3179281-6 1U18116 22:17
Spike Amount
Original Result MS Result
MSD Result MS Rec. MSD Rec. Dilution
Rec. Limits
MS Oualil MSD OuauSer
RPD
RPD Limits
Analyte
m9A
mgA mgA
mgll % %
%
%
%
I I C I
Copper -
1.00 '- • -ND: `0-987
0.997� 99` - 100 1'
70-130
-:77.
Lead
1., 0
ND 1.01
_
1.03 101 103 1
70-130
1
20
5s
Nickel -
1.00
-ND 1.02,-
1.03 , 102', 163 �' - 1
•70-130 "-
'
-,F'1
'4 20
Selenium
1,00
ND 1.03
104 103 104 1
70-130
1
20
a
Silver .
..
0.200
- ND - 0.184
0.186 .92 93 i
74130
1
_
�. 20 is - 1
- -A- -
C fl
Zinc
100
ND 101
102 100 102 1
70.130
1
20
'FSr
L873588-01 Origillal Sample (QS) • Matrix Spike (MS) • MaWx Spike Duplicate (MSD)
(OS) L873586-01 11118/16
22:20 • (MS) R3179281-7
11AM6 22:22 •
)MSD} P3179281-8 11118l16 22:25
Splle Amount
ORglnal Result M5 Result
MSD Result MS Rec. MSD Rec- Dilution
Rec. Limits
MS Ouaiifier
MSD 0ualifier
RPD
RPD Limits
Analyte
....... --I
m9A
mgA mgA
—I
mgA % %
-.._.� --
%
%
%
�-
Gl
_._.�_.
—ND
1,44 130 444--•--- I
70-130-J5_-...,.._�.....
10---._
20
Arseni£
1.00
NO 1.34
lA8 134 148 1
70-130
J5
JS
10
20
AI
Berylilum
100
ND 129
143 179 143 1
70-130
J5
10
20
Cadet
100 _
ND_- ' 1.32
1.47 y__S32 147 _7
70-130• "
JS ;-
- J5,
10
¢ 20 Q.
e
Chromium
100
ND 1.30
1.44 130 414 1
7D130
J5
10
20
SC
COPPer - ..
1.00' -
,D p142i •_ 1,29,
-
1,43 • ', 127 _ 142 -. 1'�'
. -1
70-130'
.-. J5'-,
-11 --, i
-' 20
lead
100
NO 1,32
1,46 132 146
70-130
J5
J5
10
24
NickeV -
1.60 ,- ''
ND ''.•. ` 1,35
.1,50 134- `.�149 ", •; f
70-130_
J5
..
10�- .,
,:}•H2O� .. - �.
Selenium
1.00
NO 1,35
1.50 L35 150 1
70430
J5
J5
11
20
Silver: •-
0.200 - �'_
ND ,, , -' 0.239
6,264 - 120 2 1'
70-130:
10�%-, = ':, 20-
Zinc
1.00
0.536 1.93
2.13 l39 159 1
70.130
J5
J5
10
20
..__-------------------.— _,_-- -__
ACCOUNT: .. PROJECT. " i 5OG e S DATE/TIME PAGE: -
TBLLabdalory. TDL'-27,Ai27 S'-�`L073538. SV301S6081437--

WG928193 QUAL(TY' CONTROL SUMMARY
"`'
;` ONE ia©.IVATIO WDL. .
'Meia is (ICPMS1 by. Method 200.8 _ L87353B 01
Method Blank (MB)
(MS) R3179474-1 11/71/16 00:41
M3 Resuh M8 Oualifier MB MDL M8 RDL
..
�TC
Analyle mg11 mgA mgA
Thallium U 0,00028 0100100
RS
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
,
Cn
(LCS) R3179474-2 112V16 00:44 • (LCSD) R3179474-3 1V2U16 00:48
Spike Amount LCS Resull LCSO Result LCS Rec, LCSD Rec. Rec- Umits LCS Ouatiner LCSD Qualifier RPD
RPD Llrnts
Analyle mgA mgA mgA % % % %
`- _-0 --�
%
Thallium-��- 0.0500 0.0482�`--0.0481 46....._.�... 96-- 85-115�
20
L873544-01 griginal Sample (0S) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
T
(OS) L873544.01 11121116 00:51 • (MS) R3179474-5 1112V16 00:59 • (MSD) R3179474-6 11121/16 OT02
GI
Spike Amount Original Resull MS Result MSD Result MS Rec. MSD Rec, 011utlon Rec. Limits MS OuaiiOer
MSD Oualifler RPO
RPD Limits
Analyte mgA mgA mgA mgA % % % -
%
Thallium — 0,0500 ND 0.0506,_�_..- 0.0500 101
1
Sc
1
.. ACCOUNT ' - PROTECT - SDG. DATE/TIME:' PAGE:.,
- TBL Laboratory - TBL-27427 L873538 IV30/16 0814 22 of 37•

WG92885a ; '
DU`AI`ITY''CON`TROL`SUMMARY
- ONE NATI MIADF.
,°'.-'
k
Voletlfe'Orgarik Compounds (GUMS) by,,Mathod,624
, , - , ;: L673538 61 rr `,
` .'�+IT
Mcthod Dank (MB)
(MB) R3180611-3 1V24/16 02:55
MB Resuh
Analyte mg0
MB Oualifer MB MDL
M911 _
MS RDL
mgn_--------.----_..___....
AuWOn V
0-00887
00500
Acrylarn rPBr-:�<;. ,''tU-�
.- • :0.60187
0.0100
Benzene u
0.600331
0.00100
Bramod chloiamelh6ne ' Ll
Brumoform U
, - 0.000380
C.000469
0.00100 a . ' - -
C.00100 r
• -- ` ,
r_
aCrl
Bromomethane ':U
0.006866
0.00500 - - -
Carbon tetrachloride V
0.000379
C.001D0
'Sr
Chlorobenzene:'. tl
0000348
0.00100
Chlorod bromomethane u
0.000327
0.060453
0.00100
0.00566_
2-Chloroelhyl vinyl ether U
0.00301
0.0500
Chloaofoim-: , 'fall
..-0.000324, .; ,0.00500_ -- - ...,1. -. -, -
- ..,. .. ,. ,..
•GI
Chloramethane u
0.000276
0.D0250
... _
qeilr
"-• 0,060254
--000700 -
rrn=}
`
u
0,0003GI
- •_ _r
0.00100
-
Ell1,2-Dichloroethane
1,hDlcnloroeihene ,;U
0000398 .
- 0.00100
trans 1 2 Dlchloroethene U
0000396
D.00100 • •
c5C
1.2.661orbpropane. = U -
Y _ ' 0.006306
"000106 -
-
cis-1,3-Dichlorop7opene U
0,000418
0.0000
J -
trans 13 Dkhlompropene,, - r u
•'i �'r'.- O.D0D419
- .0.000384
0 00100 t;', - • - -?'
r _
Ethm ylitemne U
0.00100
Methylene Chloride -- �' -U ; ' '
-' - 0.00700
0,00500
1 7 7 7_7ol;arhlnrr,nthana I I
- - rvvtt30
D OD10C- - •-
. " 1
Tetrachl(r ' Iterie - - •,11 -
6.000372
-: D
•
..
0010D
Toluene u
0.000780
0.00500
t,t,t-Lkll�roethane : • u
_, D.DC0319
0.00100
- _� . `,; . ,' '• . `:' .
1.1,2-Tikhtoroethane D
0-000383
0.00100
Tr We oethene.•_ '; -. .U, • .
v„s
- 0600398
-0.00100 -
- '-
90.0-115
(SJDibromolluoromeMone 104
79.0-121
fsJ 4 BramoRuo a7enrene' `.rD4
80_1-170
i Y I ACCOIJNT ti --� PROJECT - `45DG - DATF1iiME
78L Laboratory - TBL 27427 ' Y ; , L873536 1V30A6 08:14 t �- _t 23 r 37

WG9'28854 QUALiT,Y'CbNT'ROE'SUMM4RY
-V olarlle'Orga nlc Compo6nds IGCIM5) by Method 624- ' L67353 E-01'
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
- ONE LAB NAnoNwfo[' :
(LCS) R3180611-1 11124116 01:54 • (LCSD) R3180611-2 1V24716 0214
Spike Amount LCS Result
LCSOResull
LCS Rec.
LCSD
Rec. Rec. Limits LCS Oualifier
LCSD OualiTer RPD
RPD Limits
Analyte
mgA
mryl
---
mgA
%
�75.1
%
%
»......,..
%
%
Acroleln
0.125
0.0939
0,102
815
$5.0-17$ J•7
J4
8.11
28.1
Acroorvtrllel "
-0.125
_ 0126 -..
0.121'
101..
_kl
- -
•71.0.135 „• •,l.
-
,4'07
': 20.�'
Benzene
0,025C
0.0233
0.0239
93.1
95.8
73,0.122
2.79
20
BromotlicMoromelhane,
0,0250 -
-0.0221
-.0.0237
• ,90.8.
- 94.9.
.75.5-121 ., .. _
4,35.
Bromoform
0,0250
0.0245
0.0265
98.1
106
71.5-131
7.79
20
Brcmomethane .
' 00250
.0-0253 '
0.0221
161
�88.5
22.4.187
13.3
Carbon tetrachloride
0.0250
0,0227
0.0238
90,7
95.1
70.9.129
4.74
20
Chioroeenxene .;.
_ 0,0250
0-0243
0.025E
_ 97.3
, 102
79.7.122
4.9E
Chlorodihromoirethane
0,0250
4.0241
0.0259
96.2
ID4
78,2-124
7.29
20
Chloroethane'' _
0A250
"00211,,
0.0221
-. S4,5
'88.6
'4i.2153
-
4,67
20
2-Chloroethvl vtm4 ether
0.125
0.113
6.114
an-5
Q0
234-162
e7g
Chloroform-.. •:� °'
^_-0.0250
09132
6.0239
923 ;
95.E
73.2-125
-
- 3.14
20 ,-
,- _ •< -
Chlaromethane
O.D250
0.0222
0.0225
US
89.9
55.8-134
1,21
20
1.1-Dichlmr t4 a _.
0.0250
0.0235,-
0.0242
94.5
"96.6
71.7.127 ..
-
223 -
20
1,2-Drchloroe0ane
0.0250
0.0223
0.0230
89.2
92,2
65.3-126
3.26
20
1,1-Dichloroelheoe -
0.0250'.,
0,0215 ,,
00222
...86.2
88-8
59.9-137'- - _
'-
2.98
r •20
trans-1,2-Dichlorcethene
0-0250
0.0240
0.0243
96.0
97.3
72.E-125
135
20
1,2-Dichloroprop" "
^ ' 0. 250' '
0 0230 '
' 0.. 0 ,.
- 92.2 . ,
a 95.8.
-' 77 4-125
3,84
- ; � 20
„-
cis-1,3-001oropropene
0.0250
0.0236
0.0248
94.3
99.4
77.7-124
5,18
20
trans 13 O,"fopmpene.
00250
0,0231 c
96.0
73.5.127 7'-'
:-'i; '
399
-, 20
...
f
,
�0.0247
.0.0244.
:97.3 ,
{ `'
:
E1hylDenzene
C.0250
OA257
98.9
103
80.9-121
378
20
Methylene Chiaride
'f,0.0250
-00216,,0.4720
'+
86.2
-879
- '1.69.5420
1.894,'•.,,.;-
2D `,-
a
1,1,2.2-Tetrachlorcethaoe
0.0250
0.0237
0.0250
94.7
100
79.3-123
5.55
20
Tel rachloroethene-..: . ,
; 0.0250,,
- 0-0245�' -
,. 0.0259
' 97,9
,<104„
.-73.5_130 ', �
-
5.78 '
�246
'20 "�-
Toluene
0.0250
0.0236
0.0242
94.3
96.7
77.9.116
20
LI,i-Trichloroelhene'
; 0.0250 _
- 0.0238 , -_
• o.O246
95.2
986
71.1-129 . -
` --� -
- 3.50
11,246chloroelhane
0.02$0
0.0236
0.0249
94-6
99,6
81.E 120
5,20
20
TrtcnloroeNene ..:.
_. 0.0250 ;-
0-0243,1E
:,„0.0248°
97.1 .'
'•-99.2
'-
.'79.5.121� - _ ,,,.-
-
.'-
N2,12
- -20 -_.' _-<, _ �_ _ •<• •--t sz `, _.-. •�,_
-_
Vinyl chlodrip
p.0750
0.0227
gn237
907
ga c
615134
4.52
0
- -
.-_.-105t-
15) Drbromofluoromelhone
705
104
19.0421
.(5� 4 BIOmoRuoroben7Pne
`
106
, -106
_ 60.1-120
9 ACCOONT PROJECT I �; SDG- - Y DATFJTIME PAGE
i 7BL'Latomtory L073536 - '.-IV3pl1608,14 ? 24 of 37 "
,

W.G'92 88 54 Q U AU TY .0 Q N T R OL -SUMMARY .,ONE LAU. NATIONWIDE,
Volndle. Organic'Compounds -(GCWS)"by Method_624. - L873538-01'„ -
L873673-01 Original Sample (OS) - Matrix Spike (MS) • Matlix Spike Duplicate (MSD)
(OS) L873673-01 1V24n6 05:20 - (MS( R31BO611-4 IV241IG 03:57 - (MSD) FZ31BD611-5 1V24/16 0419
Snike Amgunl Original Result MS Result MSD Resull M5 Re[. M50 Rec. Dilution Rec. Limits MS Dualirrer MSD Oaahfler RPD RPD Limits
Analyte mgA mgA n19A mgR % % % % %
Acrolein __...
0.125
NO
30.8
30.3 _
i230
1210
20
10.0-200 E J5
Ad oralrtle ' I
- 0125
ND,'
_ ', 2.80 -
2.81 -
112
,-'113 ;--
- 20-°�
: 49.4933.;'., '
Benzene
0.0250
0.0851
0.61I
0.664
105
116
20
58.6-133
BrDnVdi61or6melhanel
,0.0250 '
NO
.> 0.523 - .
' O.572
i05
114
- 20-'`
' 69,2-127
Bromoform
0.0250
NO
0-554
0.621
111
124
20
663-140
Bromomethare
0,0250 '
ND.
0.496
0.536
99.1
.:107
'f 20
16 6.183 4 . -
Carbontelrachloride
0.0250
NO
0.534
0.588
107
118
20
60.6-139
Chlorabenzere ,:
:_ 0.0250
ND
'0.562
.0,635
- 112 :
'' 127
24-
i71.&132
Cnlorodibromomelhane
0.0250
ND
0.574
0,629
115
126
20
Cnlorcethanei,: •.
0.0250 -
ND
'' 0.517
0.5E4
,:103 _-
_ 'T73
..20,
33,3-155-
2-Chloroethyl vinyl ether
0.125
ND
1.213
1.35
513
54.5
20
5.00-149 _
Chcaroform .'
" 0-0250 _;
-NO
0532 _ - -'
0.575
106.
715
20.
..:56.1-133:
Chlaromelhane
0.0250
_
ND
0499
0.553
99.8
Ill
20
40.7-139
11-Dtchlo�oeiharie -
' 0.0256
ND
, • 0.540
: 0.578 -
108 "' .
.116
• 20
-,` 64.0.134
1,2-Dichloroethane
6.0250
ND
0.502
0.536
100
107
20
50.7-I32
i1-Dichloioethere .
0,0250 .
ND
, 0,497
0.547
99-5 -
1C9
2D
,-48.8-144
Vans-1,20chloroethere
0,0250
ND
0.548
0,594
110
119
20
610-132
1,2.0ichlolopropane
�, 0.4250
ND
_0.521 "
0.573
-104'..
115
•20
69.7.130
65-1,3.Oichlompmpena
0.0250
ND
0.559
0.615
112
123
20
71.1-129
transl3OtchloroproPene^-•.O.D250i.
•--
ND' �'sr,r-,0.529' "
.i0.583
,;;50fi';'•
_ 117•`-'
20
663136�,r
"62.7136
Ethylbenzene
0.0250y
0.251
0.817
0.912
113
132
20
Methylerie Chloride -
-; 0050,
"-
f04
'20"".. 615-125
va..vNO
0.533
4•588
507
110
70
EA 9.165,
7etrachloroetnerie
',=0.0250 -
' NO
`'0.5fl7,-
'0-653
117
�131-
,-20.
-57-441
Toluene
O.D250
ND
0,539
0.592
108
118
20
67.8.124
1.1.1-Trich10' ethane--
.-0.0250
-N4 `-
- :':055.19
0.617„
'11.2
' 113
•;20'
58.7.134. -
11,2-Trkhloroethane�
0.0250
ND
0.535
D.600
107
-
12G
20
74-1-130
TNchlwoelheoe
0DAD
'NO
0.545' -, ..
, D.508 -
,. ;,.109" _
�-.122 .. ,
..• 20 r
- ,48.9.1* .- -
vMID
.02
iia
20
443-143
-(SJ rohrene-di"+
r`
- -
'rD5
106
. -
- 90
Y
(SJDibromoAuwomefhone
174
r0.2
79J0-I21
(5/4"BromofluoroDenierie'" - - ;._r05" ''r05 _ `80.r-120i
EJ5 1.57
277
0:356 - `
''. 25.3'
8.34..
20
20
11.4
20
960
20
.:12.2
.
9,07^
20•
6,03
40
-7.71
20
10.3
20
- -6.74
20
6.70
20
'- '-9.51
20 _•s
8.11
20
. -
.
9.77
20.
96
111
20
992
20
'107
20
9.51
20
• :9.96.:.:
r
20,
11.4
20
R_ 93
20
ACCOUNT: PROJECT: - ,SDG1-DATE7TIME - "i '!PAGE:
I`-TOL Laboratory •TBL-27427 ... i573538 , 1V3OA6 DB 14 - " 25 of 37

WG929028., .
,QUALITY CONTROL'? SUMMARY
Dr4E,i4D.NATIONWIDE
110
Pesticld•es (GC) by 7Mclhod EPA 608
-
- L873538.01
Method Blank (Ate)
_
(MB) R3180928-3 1V25A6 09:28
MR Result MB Dualifer
MR MDL
M8 RDL
•TC
Anaiyre mgA
mg/1
mgA--._-^-�
__._•-
Aldan U
0.00DO0813
0.0000500
Alpha BHC -U -.. -
6.00D0166
'00000500
Beta BHC U
0,0000184
0,0000500
Delta DHC U -
0.0000197
;, ;' '',
O.00D050D 1
fi
e
Gamma BHC U
0.0000176
0,0000500
Cn
0.0000170
0.0000500
L�
4,4-ODE U
0.0000154
0.00005DO
_
5Sr
4.4-00T
0.0000177
0.0000500_: `
D,Pldnu U
0.00000751
0.0000500
Endosulfanl U _
0.o.00m 9
0.00005pp
Endesulfan II U
0-0000176
1)D000500 •
- - -
Endosulfansullate,;- - ,:U - J i00000196
0.0000500'�, ,, �. _,
- •r,.
,..
�GI
Endnn u
0.0000189
_ - - ___
0.0000500 -
... _
Endnn aldehyde-__ . U -
00000142 `
0.000050D •
yAl
Endnn kelone U
0.0000170
0.00005D0
Heptachlor - ', U _.
0.0000103
0.0000500,-
Hentachlor ennxide I I
n nOM175
0 nnnnk'm
I`
HexacnlO100enxene . -•U ' -
0,0000I34
0.0000500
Melhoxychlor U
0,0000193
0.0000500
Chlordane: �. '„ U, ,
0-6000973
- OL000500 ._, ,,... -
.
Toxaphene U
0.000168
-
0.000500
jSJ l?ecd�hlaobrpheny!-_:�827 � '
1L1.4156 s _ , r
.. . _
f.51 Tahnrhlnrn-m xWana 501
fi 9-fl7
Lahoralory Contr'al Sample (LCS) - La tloiatoly Control Sample Duplicate (LCSD)
(LCS( R3180928-2 1V25116 09:15 • (LCSD) R3160928-1 11/25/16 OS02
Spike Amount LCS Resull LCSD Result
AnNy4e mgA mgn mgA
LCS Rec.
%
LCSD Rec.
%
Rec. Limps
%
LCS Ouallfier LCSD Qualifier RPD
%
RPD Umits
%
Aldrin
0.00100
0.000724
0.000677
72A
67.7
10.0.120
6.70
33.9
Alpha BfiC-
-. ,0.00100 v't
0.000753
•0,000798
-75.3,
79.6
;.535125,•;.
`,. -582--
;..22.3
Bela BHC
0.00100
O.OD0864
0000B77
86A
87,7
551-530
1,49
20.6
Delta BHC ,
, -; D.00loo
0.000906 -
0,00091,
.90.6 _ '
91.1 i
42.2-135•
': 0.570
23.3
- `• ' ' '''t
Gamma BHC
0.00100
9.000797
0,000830
79.7
83.0
54.7.125
4.13
21.1
414-ODD" -,
'r-0.00100 �.,
'0.00100
'.-.0.D00924..
0.000918
• 92.4
' 91.8,�•,
416-1441-.
-- 0.720 '•.
24,3-
4c-ODE
OA00816
9.000875
87.6
07.5
45.0.124
0,170
25.7
4,4-01DT
• 40.0010D
' 0 000913 -
0000511
91.3 _
_ 91.1 ' •
' 49.8 130,
25.4 •
- .'; i. - , • _
Dieldrin
0.00100
0.000905
0.000900
90.5
90.0
55.0-127
01630
22.9
Endosulfanl -}..:
;_ ..'O.Of1100'
70-000897
O.D00889
88.7
' BRA 4
.� 54.7-127�'
, 0.170,
24.3
.
.ACCOUNT:-.
-
PROJECT:-
,SDG:
pATE?IME:
_ PAGE: -
' '
TEC Lehoratary ,
-
TOL-27427
L873538
1113011G 08 %
.26 0f 37
0

WG,9.29028:: .QUALITY .CONTROL`SUMMARY r LONELAH NATIONWIDE; '
Pe tildes (GC1.6y'Meihotl EPA 608• L873536-01-'
Laboratory Control Sample (LCS) • Labormciy ControE SarnpEe DLlplicate (LCSD) n
(LCS) R3180928.2 11125/16 09.15 • {LCSD) R3180928-1 11125116 09:02
Spike Amount LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits LCS Oualiter
LCSD DualiTler RPD
AnaWe
mg4
mgA
...
mgA
%
%
%
%
-
Endosulfan li
0,00100
0,000908
0.000096
90.6
BIG
�53.1-135
1,31
Endpsulfan sulfaie-, •-
1 , 0.00190 :
0,060917 :
' ,' 0.000906
.'91.7
'90.6 •
- 515-132 - ;'' -
1.16 -
Endrin
0100100
0-000916
0.000914.
91,6
91.4
50.1-131
0.290
Endnnaldehyde_."•+�, �
0-00100-
�' 0.000669-'�"�.OA
OD852--�
86-9�
�-85.2 �
39.5.137 _ rr.
� .-200f,t
Endnn ke110ne
0.00100
0.000906
0.000892
90.6
89.2
53.5.139
1.57
Heptachlor,-.,;_ _
0.00100
D.000765
', '0.000746
76'5 -
,-.74.6
.20.7-i27
-_ 2.54.'. -
Heptarhloreporlde
0.00100
0.000859
0.000889
86.9
88.9
-_
56.4.124
2.23
Hexachbrobeniene
., DA01D0 .
-0-000629 _•
..0.000600
' 62.9
'60.0 -
26.7-114 _
- 4.67 _
Me[ho ycntol
0.00f00
0.000924
0.000906
92.4
90.G
48.2-144
1.90
' (5)De[oChlorPtupherry!
, , '
- - -
--
-&7
_ 83.9
10.4156• - -
- .
NTerrorhlmo-m-aylene
-
584
582
1391137
RPD Limits
23.5 }
26.3 ... E .
29.1
35s
28.4 -
128.a
n
Cn
-`30.5
L�
23.1
27.6
`• �.
27.9
AI
u
-- ___ _ __ __�____..-------_-._-- -_ - -- - _
1
ACCOUNT:_ - PROJECT, SDG:' DATHTIMS PAGE.
TBL Laboletory - .7BL-].7427 iL873538 7 of 1V3011608,14 - 737.�i

'W.G9302r96 _
C?lJAC11TY=�CON,Ti O6'C U.MMARY
y ` ` SCA6LAI3 NATI.oNWIaC.
Palychlo rineletl-Biph enyls (GC)'by Melhotl`EPA-608
1.873538-01.' •..-
1;
Method Blank (tv1B)
{MB) R3161209-1 11/29/16 10:13
M3 Result MO QualAer
MB MDL
MB ROL
Analyte mgA
mgll
mgA
PCB 1260 U
0.000120
0.000500
PCB 1016 „ U _
0.000100
0.000500'
PC61221 U
0,0000730
0,000500
PC81232-• - - _ -U .... - -
0,0000420 -
0.00D500_- - -
-
q
PCB 1247 U
0,0000470
0.000500-
-
Cn
PCB 1248 - -U - "
0.0000860
- 0.000500 -
PCB 1254 U
0,0000470
D.000500
Y
5
.� 0--hloroblpherryf 81.2
- 10.0-156 - _ ., _ ' .
. • -
.sir
Q Telrnchlor&-m-xylerte 68.9
139-137
Laboratory Control Sample (LCS) . Laboratory Control
Sample Duplicate (LCSD)
GI
(LCS) R3181209-2 11/29/1610:25 • (LCSD) R3181209-3 1V2911610.37
Spike Amount LCS Result
LCSD Result
LCS Rec, LCSD Rec. Rec. LFmlts LCS QualESier LCSD Qual{0er RPD
RPD Limits�
Analyte mgA mgll
Mgt!
% % % %
%
---
PCB1260 0.00250 00267
PCB 1016 '-' '. - •,. 0.00250, - 0.00234
060265
- 0.00225 �
— —
104 106 477.149 1-66
93-5. 90,0;. '' 24.7-128 - - - 3.87-
28.8
-34.9 i,.,; .!-, ';.v*` ' , . _
SC
A)N40cRkfobiphenyl
80.0 78.9 !o0-I'S6
_ ,t •, _
,(S)Tef�arhloro-m-nyleoe-
68.6
ACCOUNT: PROJECT:T SDG-1•• h DATFJT{Mc"
iBL Lnbra[ory, , TBL-27427 - L873538', - 7V30,160814 - '� � _ 28 of 37 •1

QU_ ALIT=l ' CONTR0L'.SUMMARY:'. `
CANE LAB- NATIQNWIQF.
" `
tWG928430
,, ;
Semi -Volatile Organic Compounds jGCJMS) by Method 625 - LB73536'07
.... -
-
Method Blank (MB)
(MB) R3180199-3 11722/1612:39
U
MS Result
MB OuRKer
MBMDL MS ROL
+TC
Analyze mgll
M9n mg0
� �-
Acenaphthene U
0.000316 0.00100
ACenaphthylene-. _• U-,.
0.000309 `0.00100.
Anthracene U
D.000291 0.00100
Benzidine- - , 'U
0.00432 UZI)
a
Benzo(alanlhrarana ll
noon n475 n,nnlnn
u
Sen70(b)tILINranthene U - .
0.0060896 .0.00100
Benzo(k)Buoranthene U
0.000355 0.00100
�1Sr
Wzo(g,h,iperylene U
OM0161 0.00100
- -
Benzo(a)pyiene U
0,000340 C.00100
Bis{2-ch16rethW;jmethane U.
_ _
0.000329 0.0100
BIs{2-chloraethy"ther U
0-00162 0.0100
Bis{2-chloroisopropgl)ether;. •._ U -
- 0.000445 ' 0.0160-
4-Bromophenyl-phenylether L
0.000335 0.0100
2-Chloronaphthalene - U
.r
'.O.6OD330 0.00100 '
i
4-Chtoro he„ r-
p rryl-phe ether ll
0.000303 0A100
Chrysene _ - ,U.
000D332 0, 00100
-
-�
rnn r hla rb a n
3,3 Olchbrtibenridlne U •
n nnnno n nn 00
0.002Q2 , 0 0100 -
.,
., ..,
r �-
SC
2,4-Dinitrololuene U
0.00165 0.010D
2,6-Dinitthtoluene _ .. U
0.000279 0.0100
Fluoranlhene U
0-000310 0.00100
Fluarene r, '' U
,..
OA00323 •; 0.00700
Hex 9C hlorDbenzene U
0.000341 000100
HeMachlpro-1,3-butad�ene-U
-0.000329 0,0100 a
He.achloroCyclopenladiene U
0.00233 0,0100
Heaachbroeihane,' `' -_ U ,.' •.
6000365 D.D10D =
lndeno(1,2,3-cdjpyrene U
0,000279 O.DO10D
Isophorone _ ,' _ U .'
0,000272 .0.0100_.,3' -
Naphthalene U
0-000372 0.00100
Nitrobenzene 'U
0-000367 OAi00 --
n-Nitrosodimethylamine U
000126 0.0100
n-Nawsodiphenylamine, U
0.0003(A - 0.0100
n-Nihosodi-n"propylamine U
0.000403 0,0100
Phenaothrene,- - -';U'--
0.000366-. o,OD100 r -
- __ •-� ,_•,, _,. ,, - -
6iA2�zhylli ir; phthalate;U.
is _ y .
0.000709, 0,00300.
Di-n-butyl phthalate U
0000266 000300
Dieshyl phthalate • '` U -
- 0,D00262 ' ;0.00300
....
Dimethyl phihalala U
-
0.000283 O.OD300
Di-n-octylphthalate" - <U -
_ -. -
0-OOoM ' 0_.00306-
r
_ - ;ACCOUNT -
'
PROJECTSOG -
Y DATERIME f ,v PAGE
" '. TBt Laboratory
-
.,7DL.27427^: s', L87353R _
'"` 1i130116116a4-290137 -

W.G9.28430
"
QUIaLI i'YP CONTROL''SUMM''ARY
"
oN Lae riailolvwloE.
Sem1,Vo lelllo Organic
CDmPeunds.={G
CIM 51 by-Me1hod,625 ., -, •„ ,•-L87753e`01' - -
.- -'•i� �+ �. ,
_ - .1, ,-
Method Blank (MB)
(MB) R3180199-3 iV22l1612:39
p
MB Result
MB Ouahfier
MB MDL
MB RDL
�TC
Anatyte
�-
m91
_
m9A
mgn
�0.00100
rvU
Pyrene
0.000330
- --
1,2A-Trichlpro5emene
U'-
,0-000355
00100"
Ss
1.2-Diphemyplydrazine
11
0.000318
0.0100
4CMoro3 meihylPhenol -
U'.'
'a '„
�.. 0.000263.
O.C10_0 - - • .. -
.
-, .,.., ... _ _
a
2-Chiorophetoi
U
0,000283
MOD
Cn
2-N lrophei; l,.
U
'OAO0320
0.0100 .
_
4-Nitrophenol
U
_
0.00201
0.0100
Pentacmorophenol.
t!,
.,
0.000313
001D0
Phenol
2,4.&Trlchlorophenoi
U
-U -
-
000334
0000297
0.C100
, 0.0100
` -
2 4-Dkhlorophenbf
U
0-000284
0.0100
2,4-DimelhylphenDI - ..:
U ' .,
_
0 DOD624-
- 0.0100
4,6-Dinitro-2-methylphenol
U
0.00262
0.0100
2.dDlnitroPhenol -'
(SJ Nitrobenzene-d5
U'
79.0 '
rt ..
0.00325-
�OAIOO
21.812J
(SJ3FluoroWpAeny!
90H_-,
29.5137 ': ,- -
,
_
(S)p-Terpheny4 d74
95.3
29.3137
}
5c
jsJ Phenol d5 � ''55.4
F
- -
3.r70.17. r .t. -., , - - , -
- - ..
-
(Sf2-F7uarOphenO!
Laboratoi„ Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3180199-1 IV2211611:53 • (LC5Dj R3180199-2 1V22A6 12:16
Anatyte
Spike Amount
m971
LCS Result
mgn
LCSU Result
mgA
LCS Rec.
%
LCSD Rec.
%
Rec. Limiis
%
LCS Oualifier LCSD Ouallfier RPD
%
RPD Limits
%
Acenaphthene
00500
0.0453
0.0448
90.7
. B9.5
38.7.109
1.29
2115
Acenaphlhylene - ..
10,0500 -
',004fi9_"
- -00463
:. 93.8
•-92-6 ;'�' '--
3fi0-106 ••-
- •. 1.35
'.27
Anthiacene
OV500
U457
0.0450
91.5
89.9
43.6-113
1.75
18.0
BenzUne' Z:_
;
: 0.0500
.0.0214 ��-'
--0,Oi95-
' �42.9
-389- -
100165 -
9.63'
'40 :-
_
Benzo(a(anthracene
0-0500
0,0436
0.0424
87,2
B4.9
51.2-112
2,76
20
Beh2o(6}Ruoranthene `-
-0.0500 .
0.0449--
,- 0.0449
89.9 -
89.8 -
47.6-171 -
- - • 0.0800,
20
Benzo(k)8uoranthene
0.0500
C.D442
0.0435
88,4
87.1
49.4-114
1,46
20
Benzo(g,h,4perylene
0.0500
0.0452-
0.0456
90.3
91.2 .45.2-It7
0.910
- 20-
Benzo(a)pylene
0.0500
0-U444
C.0443
8819
88.5
45.6�106
0.290
20
Bis(2-chloreth6vhniethane ,
0.0500
OA441
- 6.0434
88,1 . -•
86.9'
37.2-111 g.; ••
- -.. - 1.42
-, 24.1'-
8is12thloroelho)eLher
0.0500
0.0391
00394
78.2
78A
22.6408
0.800
27.9
Bisj22hioroi19PTI,ytlether•- • ' 0 0500 _"
0 04231-:,
; : D.0415'
..847 -_ .
`-, 83 i - •
32.9-100'
, - - -" . "1.84 -
, 251 - - • - _ �, - '
4-Bromopkayi-phenylether
0.05110
0.0434
0.0425
86.7
,
851
40.7-116
1.96
21
ACCOUNT: - ::-PROJECT it DA;97TIME - 4� .PAGE
THL laboratory' TBL-27427 _•L873538 - _ 1V307160814 0 - - - .30 of 37

WG928430 '
QUALI`f 'tONTEWL SUMMARY
=.
ONE LAe NA71pN,NIQE-
r
-Semi: Volatile Organic Compound
(GC 7M91
by;Methotl 625 _
'
•t R7353a"0i •' "• - '-
,. _
,
_
Laboratory Control Sample
(LCS) • Laboratory Contro{
Sample Duplicate
(LCSD)
(LCS) R3180199-1 11/22/16 11:53 • (LCSD) R3180199-2 11122P612:16
' p
Spike Amooni tC5 Result LCSD Result LCS Rec. LC5D Rec.
Rec. Limits LCS Duahfer LCSD Duali6er RPD
RPD Limits
Analyle MgA
mgA
RIP-
%
%
%
%
%
2-ChloroaaphtAslene` , 0,0500 •
0,0419
.�_ ; '•,1,- 0.0416.
83.7 '
-"--83 2
733-6- 45'
"-0 620 '.
-.y - 23
4-Chloraphertyl-phenylether 0,0500
00443
0.0437
88.6
1173
-
39.0-113
1.50
209
7
Chrysene'_ •- 0.0500-,
_ 00462
-' .-' 0.0445-`,
'92.5
891
54.E-120.+ '-L`
3.75
20
s - •a t£
Dibenz(a,h)anthracene 0.0500
0.0452
0.0449
90.4
89.9
42,8119
0.596
20
4
._
3,3-Oichbrobenxdine Q.0500
0.0435
r .. _
0.042E
B6.9
85.2 •
-'- -
27.2-142
�31.2.105
"203..
---
2Z3;t.
r. 1
",
Cfl
2,4.Olmtrotoluene 0.0500
0.0482
0.0482
96.5
96.5
-
0.000
22
L-J
T,6Dmltrotoluene _ 0-0500•-"
-0.0433_
0.0428
8153
85.6 ,., ",
,•306-406 --" -�
124'"%`
'23.1 --'� -
f
Fluoranthene 0.0500
0.0453
0.0452
90.7
90.4
45.9-1115
0.240
20
Fluorene '. '„ 0.0500
.-0.0456
- 0.0449
91.2
SU -
41,0-112 _ - �
143
20.2
Heeachlolobenzene 0.0500
0.0422
0.0415
84.3
83.0
38.5-116
1.,53
20,1
1-!exachloro-0:1 utad+ene 0.0500 '.
-0.0390
0.0381
76.1
761 ' -
- 16.ta04 -
2.50 .
- 312-
Hexachlorocyclopenlaolene 0.0500
0.0515
0.0494
103
98.8
10 0-121
4 05
27,9
GI
Hexachlbrcelhane ` 0.0500
'0.0358
0.0359
11.7
.71.8 -
•- ,16.5.898 -
0,120
307
Indeno(1,2,3-cd)pyrene 0.0500
0.0456
0.0457
91.3
91.3
45.D-116
0,0700
20
IsoAhororie -0,0500
' 0.0467.
.0.0465
93.4
92.9
35.4-112•,
-0.470
lrapmtlalene 0,0500
0.0401
0.0299
80.1
797
32.2-101
0.540
23.9
.0.0500s
-_
00422
.,
047R'
R44
R36',
n_.r_70
77Nlrobe
_ II
F--
v
n-NiBosadimethylamse 0.0500'
00251
0p229
50.2
._..
45,7
_
10,0.1
9.35
-
37.5
n-Nltrosodiphenylamine' 00500_,.
-i00460"',
^D.0459
1921
91.7; 5�„
44.4i13 -
0390 r...'
ti 20;. .. .,,,.
„ .-, •a, 71,.,, . • ,
n-Nitrosodi-mprcpylamine 00500
0.0436
0.0425
87.2
85.0
33,2.106
2.60
23.7
,
Phenanlhrene" .' 0.050Dt_'
0.0438-'
''0.0432
�87.6
864 ,. ,.;5 45A173y '- . _
1.37
' y20
6enzylbutyl phthalate 0.0500
0.0479
0.0459
95.8
9119
31.8-123
4,24
20.7
8is12"ethyt6eayRphthalate'�'-'t00500-"-,
l_. '00471 .,
-.;,. 0.0531.:"`
-94.3
.:107.•�,'
36913A:-; •'r•`•'
=,130'
," 236:"•_
Di-n-outyl phthalate 0.0500
0.0413
0.04615
94.5
93.1
41.8.120
1.51
20.2
Diethyl phthalate0.0500• ,
'0.0460
0.0465 ,
`•; 92,0
930 -•+;;_`
_ 36.5-129 -_�� _ -
1.11 _
'• z0. ; _ '
�20�8
r •-; "' ,
D+methyl phthalate 0-05u0
0.C461
C.0462
92.2
923
35.3428
0.180
Di-0cty4'phinala1[e6' 0.0500-
0.0415-
=,84.3630.1.61,t,
•_ 211'-
!9.0422
s
Pyrene 0.0500
0.0455
0.0440
91.0
87.9
46-3-117
3.45
20
1.2CTrectllorobenzene' L_OA5pQ>
003771.'-`;0.0380
r,-y.75.4
.759 -229.96.1' }-',''
1,2-Diphery1hydrazine 0.0500
0.0463
0.0452
92.5
90.3
37.6-111
2.38
21,1
4-Chldro=3-methylPhenol , .. 0.0500
t^-0.0453
.. ,
- - ;00446'
--_ 90-5
_, .. ;
-.- .892
- . .. .:,
357-10D;= •e
"1.47 ' •-
_ -'>.' ''-�'_
_
2-CWD[Dphend 0.0500
0,0390
0.0387
76D
77.4
26.2.91.5
1.88
26.5
2,4.Dlchlor6phenal" 0.C500. -
0.0438
_0-0432 -
87.6 .
86.4 -'._
314.103
1.41 - ;
- 24.9,,"_-
24"DimeMylphenol 0.0500
0,043fi
00429
87.2
85,8
31.9.107
1.60
25.7
4 fi-D ildw -7-mo: h6 M-M - a r;nn
f -
.n nSaN
n n;ai
17n
Ila
5n a-14A
0.200
V
-
- 1
2.4-Dinilrophmil 0.C500
0.0569
0.0579
114
1tfi
24.2.128
1.80
20.5
2-Nitrophenol - :'„0.0500.
0.0459
`"-�0.0459
91.7
9LB,
2.5..
0,0500
• 26.9
4"Nitrophend 00500
0.0295
0.0290
59.0
57.9
10.0.52.7 J4 J4
1.67
40"
Penlachloropnend - 00500 '
- 0.0408
- -•'' 0.0409 '
'!z 81 fi
, 818 -_� --
t 1D 9 97.4 - - ,. -
0.300
"35.1.'
Phenol 0,0500
0.D264
C.0264
52.8
52.9
_
10.0-57.9
0.13C
35
' `ACCOUNT. -
-
-
- PROJECT.
-SUG: .
_ DATMiPAE `
- t PAGE
'
- - TBlrLaboratory
,
.TEW.27427
r -, LR7353E -
_
?11l3011fi 0814 L
- - 310137

WG921943'0"
QUALITY CONTROL SUMMARY
QNEl.AE.NATIoNWIDE. "
Seml Volatile Oiganic-Compounds (GCIMS). by.Method.625
•L873538-01
Laboratory Control Sample (LCS) • Laboratory Convot Sample Duplicate (LCS )
(LCS) R3180199-1 IV22/161t53 • (LCSD) R3180199-2 11/22/16 12:16
Spike Amount LCS Result LCSD Result
LCS
Re[. LCSD Rec, Re[, Limits LC5 Oualiner LCSD Ouabilei RPD RPO Limits
Analyte mgA mgA mgA
%
% % % %
2,4 6 TrichlaropflenoI '. 0 0500 0.0461 0.0470 • -
96 i."
94.1 29 8.107 " — - ,. 2.17 ' - 24.1
. •
(S)Nilrobenzened5
84.7
...
783 218173
_ .,
1
(S) 2-PluoroblpneM . .. - - --
.9L4
.:87.4 - _ - 2M-131 - -
...
(SJ p-Terphenyl-dN
102
89.7 293 137
e
(S)Phena4d5 - -
579
52.7 - 50&70.1
(S) 2-Fl"ophenol
72.1
659 10.0-77.9
-(S)2,4,6-Tribromriphenol: -
Fp9
•91.6 AZ-i30
Sr
�GI
'AI
1
�Sr
u
ACCOUNT: - -PROJECT: BOG: . DATEITIML: PAGE:
- .TOL Laboratory _ . TK-27427 L87353B lV30,15 08,14 -32 of 37'

GLOSSARY OF TERMS
ONE LAD. NATIONWIDE.
Abbreviations and Definitions
SDG
Sample Delivery Group.
Ep
MDL .
RDL
Method Detection Limit: "
Reported De'teCtiGn Limit.
Tc
ND
Not;detected at the Reporting Limit (or MDL where applicable): ' -. -.. ,-
U
Not detected at the Reporting Limit (or MDL where applicable).
3SS
RPD.
"Relative Percent Difference.-
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD),
4
from a quality control sample. The Original Sample may not be included within the reported SDG.
Cn
(S)....`
Surrogate (Surrogate Standard) : Analytes added to every.blank; sai'mple,'Laboratorytontrol
Sample/Duplicate and,Matrix Spike/Duplicate; used to evaluate analytical efficiencylk byasuring
recovery: Surrogates are not ekpected to be detected in all environmental media.. °
Sr
Rec.
Recovery.
c
QC
Qualifier
Description
E
The analyte concentration exceeds the upper limit of the calibration range of the instrument
established by the initial calibration (ICAL).
The ldentifcation of the analyte is aeceptabte; the reported value is an estunafe. a
CAI
A
The associated batch QC was outside the established quality control range for accuracy.
J5
ThesaFmple rnatrlx Interfered wrth the abllity,to make;any accurate de'terminatloh spike value Is
^high
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is
low,
p1
OD value not -applicable for-sample;concentrations less tha6.5,times iherepoing Ilmlt' , t"
1
ACCOUNT: PROJECT S.DG DATEMME."� PAGE
T8L Laboratory TeL-27A27 L873538 11/30/16 Off l4 i 33 of 37° ;

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
ESC Lab Sciences Is the only environmental laboratory accieditedkenified to support your work nationwide kom one location. One phone call, one point of contact, one laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry. The most significant benefit to our "one location" design is the design of our laboratory campus. The model Is conducive to accelerated producimly,
decreasing turn -around time, and preventing cross contamination, thus protecting sample Integrity. Our focus an premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
' Not all certifications held by the laboratory are applicable to the results reported In the atlached report.
State Accreditations
1
Tc
Alabama
40660
Nevada _
T_N-03µ2002-34
Alaska
UST-080
New Hampshire
2975
S5
Arizona
AZ0612
New Jersex—NELAP
Ti
Arkansas
88-0469
New Mexico
TN00003
nia Califor
01157CA
New York
11742 ____
rC ]n
Colorado
TNO0003
North Carolina
Env375
Conneticut
PH-0197
North Carolina
DW21704
Fri
Florida
E87487
North Carolina'
41
Georgia
Georgia'
NELAP
923
North Dakota
01
R-140
CLO069
Oc
Idaho
TN00003
Oklahoma
9915
Illinois
Indiana _
200008
C-TN-01
Oregon
Pennsylvania
TN200002
68-02979
G�
Iowa
364
Rhode Island
221
Kansas
Kentucky'
E-10277
90010
South Carolina
South Dakota
84004
n/a
+
Kentucky, _
16
Tennessee "
2006
Louisiana
Maine
A13079.2
TNO002
_Texas _
Texas
—
T 1_04704245-07-7X
LAB0152
9
Sc
Maryland
324
Utah
6157585858
Massachusetts
M-TN003
Vermont
VT2006
Miehigan
9958
Virginia
109
Minnesota
047-999-395
Washington
C1915
Mississippi
TN00003
West Virginia _
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
Wyoming
A2LA
Nebraska
-OS-15-05
__NE _ ...-_-.._ ..._ _.
- --_ -----
Third Party & Federal Accreditations
A2LA —'ISO 17025 1461.01
Ali. 100789
A2LA —ISO 110255 1461.02
DOD 1461,01
Canada 1461.61
USDA S-67674
EPA—Crypto TN00003
Drinking Water '- Underground Storage Tanks
' Aquatic Toxicity ` ChemlcalrMicrobiological
s Mold ^" Accreditation not applicable
Our Locations
ESC Lab Sciences has slxty-lour Client support centers that provide sample pickup andlor the delivery of sampling supplies. If you would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at out central laboratory.
ap`.`---'---�
MT n�
O 4 PA
NV
IV
T UT avv .
KS
CA CO ~ - ® O VA
4 ter � • Kr��� ®.c
fi� 1
O rms - AirT SC�
�0Ms TCsA
a r
� trr
ACCOUNT: , PROJECT SDG: ' pATEfTiME:. PAGE:
T8L Laboratory, ' Tr3C-27427 L873538 11/30/16 0814 3A of 37

Ew"lnlotmatlOn
0,�
"
F�L,—,l
TBL Laboratory s", i:
Pam Hester
P.O. -EIGN 589
IE SCJ
P.O: 80x Sao lLumberton, NC 283S9
Lumberton, NC 28359
M
40
1—0
Repon w
Pam Hes,te,
E
no
,
I-IW.Wl ME
IR
D—
Lb P
R
JF
z
Fhxi -�91(1-73"M
983:1
X
Car., 3w by f0rd): UWFadll%VlUV
C3
2
Taii
A-
R.h? JLb MUST D.Y.flfiedj D4� I 1�NJ-rd
:.c 1
AM
Ir
3
—.2m E�ifl X_Y.,
go.
-ly
T
b9745
FAX? Y.i
�f IE
AM,
5—pllD
C.M/Gub
"A't,
D,Pih
Daw
r�
10.
f
ww
A
I-TRI
'X i
x
x
x
x
Mal
RMIN,
I-M,41
, UN
0M I
I
14
WN
M
Al I
N
RAI
Ain
qRT
G
IWA
a"[
Ift
j
L
Mao
_xwg
MEN
'T.
Tj­'' j by.
I M-1
I 6 r
mw,
WS WE a 12
"W�

TBL Laborato rY
BRIIng (ntoimation; - +
�.
;.Anahsisl
Cantzlaei
JPtrel�eF"J"
..
Qsaxtxtustody P+R=` or_
Pam Hester
P.O. Box 589
P.O.' Box sag
Lumhcrton, NC 28359
a
s
''
,
Lurnbcitan,NC28359Fill,+
t ;cla
ii atSa:
Pam Hitter
CmaB To: tara.knecht•tblfholmzLLmm;
parnAwer-Wonal meR.mm
.gC:"
f
-
5
v_-
����
,
o
tpEFi69•SaSy ri
rs: sli•tu.us9_ {]' • "
Project
Cl;ylSta[e -.
�.-
Ctdfeued;
yv
Gr-,
,t'
fit`
Da<scriptlnu - _. fg.
-
[ 3g
rl rz+. x + e.+
ishosfe. 10.738 6I4O
CEfent Project
Lnb Project 0
fa>,: 910-671.8837
� : -�. � U
Colle(ltd 4Y jprial): -"
I {{
Coi4cted by jtiynat ej; -
Si"rl�attilTY I6 A a
Rtish7 ILah MUST8c Notliiedj
P D. R .;
t ^" ,
'Da Re s edcd`-:.
li
`�
�g
{
lrfs'
w.
;rc
-
ACLtrtflL TBlLt9 - _
teaT53833
sine Day ___.T—molt
F •
E
"
5
ea, P569745 sirj�
�
��'
�mmed.atclY
....,,, NW p ` ...„.........'.-167f4
brip
�i3O."'2
554 29(r�• RPz•[kb Rfieti
PwtkedCnkf N Y.
— —
TTTreeDls..y.�—�5%
FAYT t�0 YCS
of
7�QOA�aa
31
-s^
�
trthlR��al,Via:.FedE?fGiounf
wan/tava:�aai
r+mas!luuaa:i
Samp!e ID
•
Ccmp/O3 b:
Maw"
Dcpth
Data
T1t�re
"
4.
23
YMnriw
Mill
55•Soii GW•GroundwatvL- Aastawatcr DW-.Drlti}jritiwater dT Other
amarits: t
DW
6 ngUiftd by (51t atvc �, - J
., �� �'&
Data Ttme
F — �. y
- yx Rerclved
`,Q.b
ej
h"•,Y �.�
Samp7c atfud Ka _ l_7PS
j'edEz NCCIri�.tr Q�=.�-..�;
Cu , - -Na , ?1�" -
.•
f �id .'� - t
ti •
arnwishedbY sty e$
" iinw',.-
Dati: /t
_-
... Recrvrd
W 45Ign tare
ReaoeZvrd'
�,�C,�/�'�i
`.. «crl�
r
'+-f
h.C4C:.
•
i
}„>'"-'& ..'shx:;"!i:
I' ptsu .o.�Fl�r_•
Rellnqulshed b'I r#StEjaatUj?' t
Rn
� }lg'R u C r
t_ fists
1a > :f iitt�E �"
_buhae'k +&
U- %. . ,�.

ct,�R�: g1 LRF SDGv
��,�
Cooler Rixelved/01)(Red Vn- i 1) �jj 116 �S�L'mperiiure Upon Roccijt:
UUU
°C
ltmeiwd By: Joseph Itolierts
Si�naIare:
Rkeipt Check List
Yes
No iJ/A
Were custody -seals oh outside of cooler and intact?
Were Custody`papers'p'raperiy,filled'oul? `.,< r;;�',;n"k :: ,. w.F _r >>' r. , u ` , ,
,,., ,✓'wp
:u�x4
r� M
Dld afl bottles arrive In gow,wndilion? —
VJere corrL(,t bottles'u"sed foritlie'anaiyses requested?, "r4 � t , �y}y��jfNf
Fib
-iY
' Y��'
Vas sufficient amount vfsample sent in each bottle?
Wore al ajiplica6le sampt contaEiters correcxly p served nd �`i V
hGckedif4r,rgsrz
��„ �5s
rvaton?r(A�.Ylnrat.�n,atceptedrange
If applicable, n s;an' observable-VOA,headspace present?
�t�on;ConformanCeeneraf_ccE=,{Cf�yee�attaehedNCFOR NO MEMO,

Billing Information:
Analysis I
Container Preservative
Chain of Custody Page of
TBL Laboratory
Pam Hester Ji
T
� lIl
A
P.O. Box 589
P.O. Box 599
!Lumberton, NC 28359
-J'
���
Lumberton, NC 28359
W_
---
L-AB SC1-E-N-C-E-S
1201111ol—RI
EW❑ Mount Ju! et, TN 37122
Report to:
Email To: [e-mail];
Pam Hester
pahi.hester-tb[@hotmail.com
z
Phone
'ho
Fax: st ... . ....
-------
Descripti( v;—
City/State
Collected:
Client Project 0
Phone: [phone]
Lab Project
"_X.
#
Fax! 910-671-8837
Collected by (print): Site/Facility ID q
P.O. 9
U'
OE
8
Q11
A.
JIG
0
M
3:
:;
1 Eq
0
FMGg 5697
Collected by (signature)'
Rush? (Lab MUST Be Notified)
Date.Results Needed
Same Day ........................... 200%
Next Day ............................. 100%
E,
c).
IF,
0
tE
_�"' Y
1.5A -256 wrrenfK eaer
a.
Email? No X Yes
E
Immediately
Packed on Ice N Y
_T_ Day .................... ... 50%
Three Day ........................... 25%
FAX? —No —Yes
No.
61
0,
Ln
f-4
PL
-
- 0'
X:
_Ln'
CA
J
2:
iz
LA."
I
6.,
_i dtX
Matrix
Date
Time
Cntrs
R—JC.M­ir.rt
8amplepllahonlyl
Sample ID
Comp/Grab
Depth
11'�
177,
WW
4
CdX
X
rvX
X
"4X
X
V�
I X
I
I X
AP
ON
12
1,14
115
WN
I J.
PER
ar
X,
Matrix! SS -Soil GW - Groundwater VVW - WasteWater DW - Drinking Water OT- Other
Remarks: pH Temp
A
H
Flow Other
t' ild Me,;
ui
Refinq shed by: (Signature)
Date:
Received by: (Signature)
Samplei returned via: 11 UPS
1:1 Fed ❑ Courier 13
C6ndlit& prgb� USeonq
"
341
k6tirou fished .h­K,—t4rMA`
b(S­4m
;�e m M
I
O
;
Relinquished by':(Si
Date:
Time:
Reserved for,lab by (Signature) .
Date 4�
3 t Time
l3H�Chiecke
4,
it

Billing Information: 1,
Analysis/Container/Preservative
'Chain
of Custody Page=of
TBL Laboratory
Box 589
Pam Hester P.O. Box 589P.O.
Lumberton,
�'-'
NC 28359 �
-
_
,.' b�,*ESC
L-n.B s c•t-E N.°.�.5
Lumberton, NC 28359
u.
,���
r
'
1
``is
f--�c
.y
4 $ _ ip�r
-
12065 Lebanon Rd
moanu.1ie:,Tu97 22 �©
Phone [phone] •
Prlone Bo0.767-5859 '
Re part to: Email TO: tara.knecht-tbl@hotmaiLcom
Pam Hester pa m.h ester-tbl@hotmaiLcom
Project
city/state
,,g
F :615 7585859 -
t
Description: 't
Client Project g. _
Collected:
Lab Project N i•
�J;
r
i `
# r.. s
Phone: [phone]
Fax: [phone]ft'
..
P ti�
rl+
• ak«. Lii�ti:
Te# R3a,
Collected by (print): Site/Facility ID a.
P:O. N
_$rt
,�-,
1",
s^may=-;-, •? ,+ ;
Collected b(signature): p
YRush. (Lab MUST Be NotifiedE
)
Res
��T-
...........
ctnum nTBLLA6
n, 97x45
Same Da z00%pTemPla�teT53833
. Next Day. ... 100%
—
Immediately Two Day .............................. 50%
- �yy $
• _
}
-
1 f
_
P.relogm
T�SR 296 fiDarr 'en Reeder "-
ouItXNeeded
Email?
� _ _
No
Packed on Ice N Y '' _Three Qay.... .. ._ 25%
FAX. No _Yes
7—
•
b,.
Shppe$ia%.F.edEXaGrotind�
•
aem. comam nanr
/
sam i a done
P e I = Y)
Sample ID
Comp/Grab
Matrix
Depth
Date
Time
WW
I_
nC1 .�_1/1
V
Fw,
RX.,' �
�
F
wa
1
V � e�
a
R
f
'
s_
_ �:. �
It
E N21
}(�[�
LEI
man
'W,
_` '..'I
. ,i° k
'f.p�.{�^"
Matrix: SS - Soil GW- Groundwater WW- WasteWater DW- Drinking Water OT - other
Remarks: pH Temp
- Flow Other Hold N T�
Relinquished by:'(Sig 1,,,re r.:�
ClawTime•.
Receiveddb
kSrgn.�si)
Samples returned via: ❑ UPS
Condition
1i
r;.I ���
❑ FedEx ❑Courier ❑
elinquished by: jSignat reJ 't�
Date
Time: Received
by (Signatu�e)�"°`
Temp: C riBottles Redeivetl
r;?.,
1,1.•-
.. -
.� }-..° �._�....�.�__.GOCSeaUlntact
cv.Y�,a'r..9N•.._N A
_
Relinquished by'(Signature -
Date:
Time: Recerved
fPorlablby 1Signatu re),�'�._k '"� =
Date:' a ,Time ,-
pH Checked ?:dl.y
NCF 9--