NCG030529_MONITORING INFO_20170616

PERMIT NO.
DOC TYPE
DOC DATE
STORMWATER DIVISION CODING SHEET
NCG PERMITS
HISTORICAL FILE
MONITORING REPORTS
. ] Q L) ] I 0 Q ) (,,
YYYYMMDD

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _June 16, 2017
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Pace Analytical Lab Cert. #40
Comments on sample collection or analysis:
?art A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2017
SAMPLE PERIOD ® Jan -June ❑ July -Dec
or []Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HCIW [-]Trout ❑PNA
[]Zero -flow ❑Water Supply ❑SA
®Other: Class C, Swannanoa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?2
Outfall No.
Date Sample
Collected"
(mo/dd/yr)
24-hour rainfall
amount,
Inches;
Total Suspended Solids
PH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks
-
-
100 mg/L or 50 mg/L
6.0 - 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
05/01/2017
0.87
4.8 mg/L
7.1
0.013 mg/L
0.005 mg/L
0.031mg/L
<5.0 mg/L
BRL
2
OS/01/2017
0.87
19.S mg/L
7.2
0.011 mg/L
0.005 mg/L
0.018mg/L
<5.0 mg/L
BRL
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31). Received
J U N 2 0 2017
Land Quality Section
Permit Date: 11/1/2012-10/31/2017 Asheville SWU-245, last revised 10/25/2012
Page 1 of 4

r

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(170), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan." Received
Jason Stone
Name (Print name) 2017
General Manaeer
Title (Print title) .and Quality Section
ASheVille
c 6/16/2017
Olignakr_� (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME: _ Laura Herbert, P.E.
Mail an original and one copy of this DMR including all "No Dischar e" reports, within 30 days of receipt of the lab results or at end of monitoring eriod
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
ature of Permittee)
6/16/2017
(Date)
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 4

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _December 18, 2016
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls_ Received
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Pace Analytical Lab Cert. #40 JAN - 9 2011
Comments on sample collection or analysis:
Land Quality section
evine
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2016
SAMPLE PERIOD ❑ Jan -June ® July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow []WaterSupply []SA
®Other: Class C, Swannanoa River
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ,
❑ No discharge this period?Z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics5
Benchmarks ===>
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
12/18/2016
0.24
mg/L
7.2
>0.005 mg/L
>0.005 mg/L
>0.005mg/L
<.01 mg/L
BRL
2
12/18/2016
0.24
mg/L
7.2
>0.005 mg/L
>0.005 mg/L
>0.005mg/L
<.01 mg/L
BRL
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/2S/2012
Page 1 of 4

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Jason Stone
Name (Print name)
General Manager
Title (Print tiJ — " tl
1/3/2017
(Si nature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > SS gal of new oil per month.
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General permit text
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME: —Laura Herbert, P.E.
Mail an original and one copy of this DM& including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge' reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
re of
1/3/2017
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 4

aceAnalytical
*W..pepeh"e m
December 30, 2016
Gerald Runkles
Pentair Vales & Controls
953 Old US Hwy 70
Black Mountain, NC 28711
RE: Project: Stormwater 12-2016
Pace Project No.: 92323876
Dear Gerald Runkles:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 19, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT. OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 33

Pace AnatyticaI Services, LLC
aceAnalyticale
9800 Kincey Ave. Suite 100
Fiuntersville, KC 2$078
www pacsfebsmm
[phone]
CERTIFICATIONS
Project: Stormwater 12-2016
Pace Project No.: 92323876
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water CertificaUon #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
VirginialVELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
Virginia[VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 33

aceAnalytical'
wrvw.prtehds.WD
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project: Stormwater 12-2016
Pace Project No.: 92323876
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92323876001 Outfall #1 EPA 1664B
JMS
1
PASI-C
EPA608
SWB
27
PASI-C
EPA200.7
SH1
3
PASI-A
EPA625
RES
58
PASI-C
EPA624
GAW
34
PASI-C
SM 2540D
MJS1
1
PASI-A
EPA 420.4
DMIV
1
PASi-A
SM 4500-CN-E
DMN
1
PASI-A
92323876002 Outfall #2 EPA 1664B
JMS
1
PASI-C
EPA608
SW8
27
PASI-C
EPA200.7
SH1
3
PASI-A
EPA625
RES
58
PASI-C
EPA624
GAW
34
PASI-C
SM 2540D
MJS1
1
PASI-A
EPA420.4
DMN
1
PASI-A
SM 4500-CN-E
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 33

aceAnalytical
wwwP&DO &cum
SUMMARY OF DETECTION
Project: Stormwater 12-2016
Pace Project No.: 92323876
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92323876001
Outfall #1
Collected By
Gereld
12/18/16 14:00
Runkles
Collected Date
12/18/16
12/18116 14:00
Collected Time
14:00
12/18/15 14:00
Field pH
7.2
Std. Units
0.10
12/18/16 14:00
SM 2540D
Total Suspended Solids
20.6
mg1L
3.1
12/20/16 18A9
92323876002
Outfall #2
Collected By
Gereld
12/18/16 14:00
Runkles
Collected Date
12118116
12/18/16 14:00
Collected Time
14:00
12/18/16 14:00
Field pH
7.2
Std. Units
0.10
12/18/16 14:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written Consent of Pace Analytical Services, LLC.
Page 4 of 33

ace ft yrical
Mww.psceia6s am
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater 12-2016
Pace Project No.: 92323876
Sample: Outtall #1 Lab ID: 92323876001 Collected: 12/18/16 14:00 Received: 12/19116 10:46 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual
Field Data Analytical Method
Collected By
Gereld
1
12/18/16 14:00
Runkles
Collected Date
12118/16
1
12/16/16 14:00
Collected Time
14:01)
1
12/18/16 14:00
Field pH
7.2
Sid. Units
0.10
1
12/18/16 14:00
HEM, Oil and Grease
Analytical Method: EPA 16648
Oil and Grease
ND
mg/L
5.0
1
12/30/16 06:52
608 GCS Pesticides and PCBs
Analytical Method: EPA608 Preparation Method: EPA3510
Aldrin
ND
ug/L
0.050
1
12120/1616:16
12128/1617:28
309-00-2
alpha-BHC
ND
ug/L
0.050
1
1212011616.16
1212811617:28
319-84-6
beta-BHC
ND
ug1L
0.050
1
12120/1616:16
1212811617:28
319-85-7
delta-BHC
ND
uglL
0.050
1
12120/1616:16
12/2811617;28
319-86-8
gamma-BHC (Lindane)
ND
uglL
0.050
1
12/20/16 16:16
12/28/10 17:28
58-89-9
Chlordane (Technical)
ND
ug/L
0.50
1
12/20/16 16:16
12/28/16 17:28
57-74-9
4,4'-DDD
ND
ug1L
0.050
1
12/20/16 16:16
1212811617;28
72-54-8
4,4'-DDE
ND
ug1L
0.050
1
12/2011616:16
1212811617:28
72-55-9
4,4'-DDT
ND
ug/1-
0.050
1
12120/1616:16
12/2811517:28
50-29-3
Dieldrin
ND
ug1L
0.050
1
12120/1616:16
12/28/16 17:28
60-57-1
Endosulfan I
NO
ug1L
0,050
1
12/20/16 16:16
12/28/16 17:28
959-98-B
Endosulfan 0
ND
uglL
0.050
1
12/20/16 16:16
12/28/16 17:28
33213-65-9
Endosulfan sulfate
NO
uglL
0.050
1
12120116 16:16
12/28/16 17:28
1031-07-8
Endrin
NO
ug/L
0-050
1
12/2011616:16
12128/1617:28
72-20-8
Endrin aldehyde
NO
ug/L
0.050
1
12/20/16 16:16
12/28/16 17:28
7421-93-4
Heptachlor
NO
ug/L
0.050
1
1212011616:16
12128/1617:28
76-44-8
Heptachlor epoxide
ND
ug/L
0,050
1
12/20/16 16:16
12128/16 17:28
1024-57-3
PCB-1016 (Arocfor 1016)
ND
ug/L
0.50
1
12/20/16 16:16
12128M6 17:28
12674-11-2
PCB-1221 (Arocfor 1221)
NO
ug/1-
0.50
1
12/20/16 16:16
12128/16 17:28
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
1
12/20/16 16:16
12/28/16 17:28
11141-16-5
PCB-1242 (Aroclor 1242)
NO
ug/L
0.50
1
12/20/16 16:16
12/28/16 17:28
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ugh-
0.50
1
12/20/16 16:16
12/28/16 17:28
12672-29-6
PCB-1254 (Aroclor 1254)
NO
ug/L
0.50
1
12/20/16 16:16
12/28/16 17:28
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
1
12/20/16 16:16
12/26/16 17:28
11096-82-5
Toxaphene
NO
ug/L
0.50
1
12120/1616:16
12/2811617:28
8001-35-2
Surrogates
Tetrachloro-m-xylene (5)
102
%
20-110
1
12120/16 16:16
12/28/16 17:28
877-09-8
Decachlorobiphenyl (S)
53
%
20-138
1
12/20/16 16:16
12/28/16 17:28
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA
200.7
Copper
NO
ug/L
5.0
1
12121/16 00-30
12/27/16 23:46
7440-50-8
Lead
ND
ug/L
5.0
1
12/21/16 00-30
12127/16 23:46
7439-92-1
Zinc
NO
ug/L
10-0
1
12121/16 00:30
12/27116 23:46
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
NO
ug/L
5.0
1
12/2IM616.07
1212311619:47
83-32-9
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
Date: 12/30/2016 04:24 PM
without the written consent of Pace Analytical Services, LLC.
Page 5 of 33

5ac
(
e Analytical
www.patalebsown
ANALYTICAL RESULTS
Project: 5tormwater 12-2015
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HuntersWie, NC 28078
[phone]
Pace Project No.: 92323876
Sample: Outfall #1 Lab ID: 92323876001 Collected: 12/18/16 14:00 Received: 12/19/16 10:46 Matrix: Water
Parameters Results Units Report Limit DF Prepared
625 MSSV
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
4-Bromophenylphenyl ether
Butyl benzylphthalate
4-Chloro-3-methylphenol
bis(2-Chloroethoxy )methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
3,3'-❑ich lorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1, 3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
lsophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenyla mine
2,2'-Oxybis(1-chloropropa ne)
Pentachlorophenol
Phenanthrene
Analytical Method: EPA 625 Preparation Method: EPA 625
Analyzed CAS No.
ND
ug1L
5.0
1
12/21/1616:07
12/23/1619:47
208-96-8
ND
ug1L
5.0
1
12/21/1616:07
12123/1619:47
120-12-7
N❑
ug1L
5.0
1
12/21/1616:07
12123/1619A7
56-55-3
ND
ug1L
5.0
1
12/2111616:07
i2I2311619:47
50-32-8
ND
ug1L
5.0
1
12/21/1616:07
12/23/1619:47
205-99-2
ND
ug1L
5.0
1
12/21/1616:07
1212311619:47
191-24.2
ND
ug/L
5.0
1
12121/1616:07
1212311619:47
207-08-9
ND
ug/L
5.0
1
12/21/1616:07
12123/1619:47
101-55-3
ND
ug1L
5.0
1
1212111616:07
1212311619:47
85-68-7
ND
ug/L
5.0
1
12/2111616:07
1212311619:47
59-50-7
NO
ug/L
10.0
1
1212111616:07
12/2311619:47
111.91-1
ND
ug/L
5.0
1
12/21/1616:07
12123/1619:47
111-44-4
ND
ug1L
5.0
1
1212111616:07
12I2311619:47
91-58-7
ND
ug1L
5.0
1
12/21/1616:07
12/23/1619:47
95-57-8
ND
ug/L
5.0
1
12/21/16 116:07
12123/16 19:47
7005-72-3
ND
ug/L
5.0
1
12/2111616:07
1212341619:47
218-01-9
ND
ug1L
5.0
1
12/2111616:07
1212311619:47
53-70-3
ND
ug1L
25.0
1
12/2111616:07
12/2311619:47
91-94-1
ND
ug1L
5.0
1
12/2111616:07
1212311619:47
120-83-2
ND
ug/L
5.0
1
1212111616:07
12/2311619:47
84-66-2
ND
ug1L
10.0
1
12/2111616:07
1212311619:47
105-67-9
ND
ug/L
5.0
1
12/21/1616:07
12123/1619:47
131-11-3
ND
ug1L
5.0
1
12/2111616:07
1212311619:47
84-74-2
ND
ug1L
20.0
1
12121/1616:07
1212311619:47
534-52-1
ND
ug1L
50.0
1
12/2111616:07
1212311619:47
51-28-5
ND
ug1L
5.0
1
12/2111616:07
12/2311619:47
121-14-2
ND
ug1L
5.0
1
1212111616:07
12123li619:47
606-20-2
ND
ug1L
5.0
1
12/2111616:07
12/2311619:47
117-84-0
ND
ug1L
5.0
1
12/21/1616707
12/2311619:47
117-81-7
ND
ug/L
5.0
1
1212111616:07
12/2311619:47
206-44-0
ND
ug1L
5.0
1
1212111616:07
1212311619:47
86-73-7
ND
ug1L
5.0
1
12/2111616:07
12/230619747
87-68-3
ND
ug1L
5.0
1
1212111616:07
12/2311619:47
118-74-1
ND
ug1L
10.0
1
1212111616:07
12/2311619:47
77-47-4
ND
ug/L
5.0
1
1212111616:07
12/23/1619:47
67-72-1
ND
ug1L
5.0
1
12/2111616:07
12/23/1619A7
193-39-5
ND
ugIL
10.0
1
1212111616:07
12/23/1619:47
78-59-1
ND
uglL
5.0
1
1212111616:07
12/23/1619:47
91-20-3
ND
ug/L
5.0
1
1212111616:07
12/23/1619:47
98-95-3
ND
uglL
5.0
1
1212111616:07
12/23/1619:47
88-75-5
ND
ug/L
50.0
1
1212111616:07
12/23/1619:47
100-02-7
ND
ug1L
5.0
1
12/2111616:07
12123/1619:47
62-75-9
ND
ug1L
5.0
1
1212111616:07
12/23/1619:47
621-64.7
NO
ug/L
10.0
1
12121/1616:07
12/2311619:47
86-30-6
ND
uq&
5.0
1
1212111616:07
12/2311619:47
108-60-1
ND
ug/L
10.0
1
12121/1616:07
12123/1619:47
87-86-5
ND
uglL
5.0
1
1212111616:07
12/23/1619:47
85-01-8
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 33

Pace Analytical Services, LLC
aeeAnalytrcal• 9800 K inceyAve. Suite 100
Huntersville, NC 2807878
Wwr.pacobbxmm
[phone]
ANALYTICAL RESULTS
Project: Stormwater 12-2016
Pace Project No.: 92323876
Sample: Outfall 41 Lab ID: 92323876001 Collected: 12/18/16 14:00 Received: 112141116 10:46 Matrix: Water
Parameters Results Units Report Limit DF
625 MSSV
Phenol
Pyrene
1,2,4-Trichiorobenzene
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
624 Volatile Organics
Benzene
Bromodichloromelhane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
11-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1, 2-Dichloroethene
trans-1, 2-Dichloroethene
1,2-Dichloropropane
cis- 1.3-Dichloropropene
tra ns-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1.1,1-Trichl0roethane
1,1,2-Trichloroethane
Trchloroethene
Trichloroguoromethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Analytical Method: EPA 625 Preparation Method: EPA625
Prepared Analyzed CAS No. Qua]
ND
ug/L
5.0
1
12/21/1616:0T
12/23/1619:47
ND
ug/L
5.0
1
1212111616:07
1212311019A7
129-00.0
ND
ug/L
5.0
1
1212111616:07
12/2311619:47
120-82-1
ND
ug/L
10.0
1
1212111616:07
12123/1619:47
88-06-2
79
%
10-120
1
12/2111616:07
12/2311619:47
4165-60-0
78
%
15-120
1
1212111616:07
1212311619:47
321-60-8
102
%
11-131
1
1212111616:07
1212311619747
1718-51-0
27
%
10-120
1
12/21/1616:07
1212311619,47
13127-88-3
39
%
10-120
1
1212111616:07
12123/1619:47
367-12-4
75
%
10-137
1
12/21/1616:07
1212311619:47
118-79-6
Analytical Method: EPA 624
ND
ug1L
2.0
1
12122/1613:44
71-43-2
ND
uglL
2.0
1
12122/161144
75-27-4
ND
uglL
2.0
1
12/22/1613:44
75-25-2
ND
ug1L
2.0
1
12/22/161144
74-83-9
ND
ug/L
2A
1
12/22/1613:44
56-23-5
ND
ug/L
2.0
1
12/22/1013:44
108-90-7
ND
ug/L
2.0
1
12/22/1613;44
75-00-3
ND
ug/L
2.0
1
12/22/1613:44
67.66-3
ND
ug/L
2.0
1
12/22/1613:44
74-87-3
ND
ug/L
2.0
1
12/22/1613:44
124-48-1
ND
ug/L
2-0
1
12/22/1613:44
95-50-1
ND
ug/L
2-0
1
12122/1613:44
541-73-1
ND
ug/L
2.0
1
12/22/1613:44
106-46-7
ND
ug/L
2.0
1
12/2211613:44
75-34-3
ND
ug/L
2.0
1
12/2211613:44
107-06-2
ND
u91L
2.0
1
1212211613:44
75-35-4
ND
ug/L
2.0
1
12122/1613:44
156-59-2
ND
ug/L
2.0
1
12/22/1613:44
156-60-5
ND
ug/L
2.0
1
12122/1613:44
78-87-5
ND
ug/L
2.0
1
12122/1613:44
10061-01-5
ND
u911-
2.0
1
12/2211613:44
10061-02-6
ND
ug/L
2.0
1
1212211613:44
100-41-4
ND
ug/L
2.0
1
1212211613:44
75-09-2
ND
ug/L
2.0
1
12/22/1613:44
79-34-5
ND
ug1L
2.0
1
12122/1613:44
127-18-4
ND
ug/L
2.0
1
12122/1613:44
108-88-3
ND
ug1L
2.0
1
1212211613:44
71-55-6
ND
ug/L
2-0
1
1212211613:44
79-00-5
ND
ug/L
2.0
1
1212211613:44
79-01-6
ND
ug/L
2.0
1
1212211613:44
75-69-4
ND
ug/L
2.0
1
12(27J1613:44
75-01-4
98
%
70-130
1
1212211613:44
460-00-4
106
%
70-130
1
1212211613:44
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 33

Pace Analytical Services, LLC
Cr<��/ 111Rljl✓U! ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wrw•pv*absmm [phone]
ANALYTICAL RESULTS
Project: Slormwater 12-2046
Pace Project No.: 92323876
Sample: Outfall #1 Lab ID: 92323876001 Collected: 12118116 14:00 Received: 12/19/16 10:46 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624
Surrogates
1,2-Dichloroethane-d4 (S)
85 %
70.130
1
12/22/16 13:44
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
20.6 mg1L
3.1
1
12/20/16 18:49
420.4 Phenolics, Total
Analytical Method: EPA 420A
Phenol
ND mg1L
0 010
1
12/29/16 12:10
450OCNE Cyanide, Total
Analytical Method: SM 4500-CN-E
Cyanide
ND mg/L
0.0080
1
1212711615:14
57-12-5
Sample: Outfalf #2
Lab ID: 92323876002 Collected: 12/18/16 14:00
Received: 12/19/16 10:46 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
Field Data
Analytical Method:
Collected By
Gerald
1
12/18/16 14:00
Runkles
Collected Date
12/18/16
1
12/18/16 14:00
Collected Time
14:00
1
12/18/16 14:00
Field pH
7.2 Std. Units
0,10
1
12118/16 14:00
HEM, Oil and Grease
Analytical Method: EPA 16648
Oil and Grease
ND mg/L
5.0
1
12/30/16 06:53
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
ND ug/L
0.050
1
1212011516:16
12/28/16 17:46
309-O -2
alpha-BHC
ND ug/L
0.050
1
12120/1616:16
12/2811617:46
319-84-6
beta-BHC
ND ug&
0.050
1
1212011616:16
12/28/16 17:46
319-85-7
delta-BHC
ND ug/L
0.050
1
12/20/16 16:16
12/28/16 17:46
319-86-8
gamma-BHC (Lfndane)
ND ug/L
0.050
1
12/20/16 16:16
12/28/16 17:46
58-89-9
Chlordane (Technical)
ND ug/L
0.50
1
12/20/16 16:16
12/28/16 17A6
57-74-9
4,4'-DD❑
ND ug/L
0.050
1
12120/1616:16
12128/1617:46
72-54-8
4,4'-DDE
ND ug/L
0.050
1
12/2011616:16
1212811617:46
72-55-9
4,4'-DDT
ND ug/L
0.050
1
1212011616:16
12/28/1817:46
50-29-3
Dieldrin
ND ug/L
0.050
1
12/20/16 16:16
12128/1617:46
60-57-1
Endosulfan I
ND ug/L
0,050
1
12/20/16 16:16
12/28/16 17A6
959-98-8
Endosulfan Il
ND ug/L
0.050
1
12/20/16 16:16
12/28/16 17:46
33213-65-9
Endosulfan sulfate
ND ug/L
0.050
1
12120/16 16:16
12128/16 17:46
1031-07-8
Endrin
ND ug/L
0,050
1
12/2011616:16
1212811617:46
72-20-8
Endrin aldehyde
ND u9/L
0.050
1
12120/16 16:16
12/28/16 17:46
7421-93-4
Heptachlor
ND ug/L
0.050
1
12120/t616:16
12128/1617,46
76-44-8
Heptachlor epoxide
ND ug/L
0-050
1
12120/16 16:16
12128/16 17:46
1024-57-3
PCB-1016 (Aroclor 1016)
ND ug/L
0.50
1
12120/16 16:16
12/28/16 17:46
12674-11-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 12130/2D16 04:24 PM
without the written consent of Pace Analytical Services, LLC.
Page 8 of 33

1
aceAnalytical
Mww.yso@fab&=n
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater 12-2016
Pace Project No.: 92323876
Sample: Outfali #2 Lab lD: 92323876002 Collected: 12/18/16 14:00 Received: 12119/16 10:46 Matrix: Water
Parameters Results Units Report Limit DP Prepared Analyzed CAS No. Qual
608 GCS Pesticides and PCBs Analytical Method: EPA606 Preparation Method: EPA3510
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
1
12/20/16 16716
12/28/16 17:46
11104-28-2
PCB-1232 (Aroclor 1232)
NO
uglL
0.50
1
12/20/16 16:16
12128/16 17:46
11141-16-5
PCB-1242 (Aroclor 1242)
NO
uglL
0.50
1
12/20/16 16:16
12128/16 17:46
53459-21-9
PCB-1248 (Aroclor 1248)
NO
uglL
0.50
1
12/20/16 16716
12/28/16 17:46
12672-29-6
PCB-1254 (Aroclor 1254)
NO
ug/L
0.50
1
12/20/16 16:16
12/28/16 17:46
11097-69-1
PCB-1260 (Aroclor 1260)
NO
uglL
0,50
1
12/20/16 16:16
12/28/16 17:46
11096-82-5
Toxaphene
ND
uglL
0.50
1
12/20/1616A6
12128/1617:46
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
75
%
20-110
1
12120116 16:16
12128/16 17:46
877-09-8
Decachlorobiphenyl (S)
48
%
20-138
1
12/20/16 16:16
12/28/16 17:46
2051-24-3
200.7 MET ICP
Analytical Method: EPA200.7
Preparation Method: EPA200.7
Copper
NO
ug/L
5.0
1
12/21/16 00:30
12J27116 23:49
7440-50-8
Lead
NO
ug/L
5.0
1
12/21/16 00:30
12/27/16 23:49
7439-92-1
Zinc
NO
ug/L
10.0
1
12/21/16 00:30
12/27/16 2149
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
83-32-9
Acenaphthylene
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
208-96-8
Anthracene
ND
uglL
5.0
1
12/21/16 16:07
12/23/16 20A4
120-12-7
Benzo(a)anthracene
ND
uglL
5.0
1
12/21/16 16:07
12/23/16 20:44
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
12/21/16 16:07
12/23116 20:44
50-32-8
Benzo(b)fluoranthene
ND
uglL
5.0
1
12/21116 16:07
12/23/16 20:44
205-99-2
Benzo(g,h,i)perylene
NO
ug/L
5.0
1
12121/16 16:07
12/23/16 20A4
191-24-2
Benzo(k)fluoranthene
NO
ug/L
5.0
1
12/21/16 16.07
12/23/16 20:44
207-OS-9
4-Bromophenylphenyl ether
NO
uglL
5.0
1
12/21/16 16:07
12/23/16 20:44
101-55-3
Butylbenzytphthalate
ND
uglL
5.0
1
12/21116 16:07
12123116 20A4
85-68-7
4-Chloro-3-methylphenol
ND
uglL
5.0
1
12121/16 16:07
12123116 20:44
59-50-7
bis(2-Chloroethoxy)methane
ND
uglL
10.0
1
12/21/16 16:07
12/23/16 20:44
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
111-44-4
2-Chloronaphthalene
NO
ugk
5.0
1
12/21/16 16:07
12/23116 20:44
91-58-7
2-Chlorophenol
NO
ug1L
5.0
1
12/21/16 16:07
12/23/16 20:44
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
12121/16 16:07
12/23/16 20:44
7005-72-3
Chrysene
ND
uglL
5.0
1
12/21116 16:07
12/23/16 20:44
218-01-9
Dibenz(a,h)anthracene
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
53-70-3
3,3'-DicNiorobenzidine
NO
ug/L
25.0
1
12J21116 16:07
12/23/16 20A4
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
12121/16 16:07
12/23/16 20:44
120-83-2
Diethylphtha late
NO
uglL
5.0
1
12/21/16 16:07
12/23/16 20:44
64-66-2
2,4-Dimethylphenol
NO
uglL
10.0
1
12121/16 16:07
12/23/16 20A4
105-67-9
Dimethylphthalate
NO
ug/L
5.0
1
12/21116 16:07
12/23/16 20:44
131-11-3
Di-n-butylphthalate
ND
ug/L
5-0
1
12121/16 16:07
12/23116 20A4
84-74-2
4,6-Dinitro-2-methylphenol
ND
Uq&
20.0
1
12121116 16:07
12/23116 20:44
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
12/21116 16:07
12/23/16 20:44
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5-0
1
12i21/16 16:07
12/23116 20A4
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
12/21/16 16:07
1PJ23/16 20:44
606-20-2
Di-n-octylphthelate
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
117-84-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/3012016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 33

Pace Analytical Services, LLC
aceAnalytical0 9800 Kincey Ave. Suite 78
Huntersville, NC 2807
wwwpacmbftcom [phone]
ANALYTICAL RESULTS
Project: Stormwater 12-2016
Pace Project No.: 92323876
Sample: Outfall #2 Lab ID: 92323876002 Collected: 12/18/16 14:00 Received: 12/19/16 10:46 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual
625 MSSV Analytical Method: EPA625 Preparation Method: EPA625
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
117-81-7
Fluoranthene
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
206-44-0
Fluorene
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
86-73-7
Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
87-68-3
Hexach loro benzene
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
118-74-1
Hexachlorocyclopentadiene
NO
ug1L
10.0
1
12/21/16 16:07
12/23/16 20:44
77-47-4
Hexachloroethane
NO
ug1L
5.0
1
12/21/16 16:07
12/23/16 20:44
67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug1L
5.0
1
12/21/16 16:07
12/23/16 20:44
193-39-5
Isophorone
NO
ug1L
10.0
1
12/21/16 16:07
12/23/16 20:44
78-59-1
Naphthalene
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
91-20-3
Nitrobenzene
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
98-95-3
2-Nitrophenol
NO
uglL
5.0
1
12/21/16 16:07
12/23/16 20:44
88-75-5
4-Nitrophenol
NO
ug/L
50.0
1
12/21/16 16:07
12/23/16 20:44
100-02-7
N- Nitrosodim ethyla mine
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
62-75-9
N-Nitroso-di-n-propylamine
NO
ug1L
5.0
1
12/21/16 16:07
12/23M6 20:44
621-64-7
N-Nitrosodiphenylamine
NO
ug1L
10.0
1
12/21/16 16:07
12/23/16 20:44
86-30-6
2,2'-Oxybis(1-chloropropane)
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20744
108-60-1
Pentachlorophenol
NO
ug/L
10.0
1
1212V16 16:07
12/23/16 20:44
87-86-5
Phenanthrene
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
85-01-8
Phenol
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
Pyrene
NO
uglL
5.0
1
12/21/16 16:07
12/23/16 20:44
129-00-0
1,2,4-Trichlorobenzene
NO
ug/L
5.0
1
12/21/16 16:07
12/23/16 20:44
120-82-1
2,4,6-Trichlorophenol
NO
ug/L
10.0
1
12/21/16 16:07
12/23/16 20:44
88-06-2
Surrogates
Nitrobenzene-d5 (S)
67
%
10-120
1
12/21/16 16:07
12/23/16 20:44
4165-60-0
2-Fluorobiphenyl (S)
63
%
15-120
1
12/21/16 16:07
12/23/16 20A4
321-60-8
Terphenyl-d14 (S)
93
%
11-131
1
12/21/16 16:07
12/23/16 20:44
1718-51-0
Phenol-d6 (S)
21
%
10-120
1
12121/16 16:07
12/23/16 20A4
13127-88-3
2-Fluorophenol (S)
30
%
10-120
1
12/21/16 16:07
12/23/16 20:44
367-12-4
2,4,6-Tribromophenol (S)
61
%
10-137
1
12121/16 16:07
12/23/16 20:44
118-79-6
624 Volatile Organics
Analytical Method:
EPA 624
Benzene
NO
uglL
2.0
1
12/22/1614:01
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1
12/22/1614:01
75-27-4
Bromoform
NO
ug/L
2.0
1
12122/1614:01
75-25-2
Bromomethane
NO
ug/L
2.0
1
12122/1614:01
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
12/22/16 14:01
56-23-5
Chlorobenzene
NO
ug/L
2.0
1
1212211614:01
108-90-7
Chloroethane
NO
ug/L
2.0
1
12122/1614:01
75-00-3
Chloroform
NO
ug/L
2.0
1
1212211614:01
67-66-3
Chloromethane
NO
ug/L
2.0
1
12/22/1614:01
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1
12/2211614:01
124-48-1
1,2-Dichlorobenzene
NO
ug/L
2.0
1
12/2211614:01
95-50-1
1,3-Dichlorobenzene
NO
ug/L
2.0
1
1212211614:01
541-73-1
1,4-Dichlorobenzene
NO
ug/L
2.0
1
12122/1614:01
106-46-7
1,1-Dichloroethane
NO
ug/L
2.0
1
12/2211614:01
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
12/22/1614:01
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 33

(�55'neAnalytical*
%"pacMa6s=n
ANALYTICAL RESULTS
Project: Stormwaler 12-2016
Pace Project No.: 92323876
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall #2
Lab ID: 92323876002
Collected: 12118116 14:00
Received: 12J19/16 10:46 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qua]
624 Volatile Organics
Analytical Method: EPA624
1,1-Dichloroethene
ND
uglL
2.0
1
12122/1614:01
75-35-4
cis-1,2-Dichloroethene
ND
ug1L
2.0
1
12122/1614:01
156-59-2
trans-1,2-Dichloroethene
ND
uglL
2.0
1
1212211614:01
156-60-5
1,2-Dichloropropane
ND
uglL
2.0
1
12122/1614:01
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
12/22/1614:01
10061-01-5
trans-1,3-Dichloropropene
ND
ug1L
2.0
1
12/2211614:01
10061-02-6
Ethylbenzene
ND
ug1L
2.0
1
12122/1614:01
100-41A
Methylene Chloride
ND
ug1L
2.0
1
12/22116 14:01
75-09-2
1.1,2,2-Tetrachloroethane
ND
ug1L
2.0
1
1212211614-01
79-34-5
Tetrachloroethene
ND
ug1L
2.0
1
12122A614:01
127-18-4
Toluene
N❑
ugfL
2.0
1
12J2211614:01
108-88-3
1,1,1-Trichloroethane
ND
uglL
2.0
1
12122/1614:01
71-55-6
1,1,2-Trichloroethane
ND
uglL
2.0
1
1212211614:01
79-00-5
Trichloroethene
ND
ugll-
2.0
1
12J2211614:01
79-01-6
Trichlorofluoromelhane
ND
ug1L
2.0
1
12J2211614:01
75-69-4
Vinyl chloride
ND
ug/L
2.0
1
121221i6 14:01
75-01-4
Surrogates
4-8romofluorobenzene (S)
98
%
70-130
1
12J22116 14:01
460-00-4
Toluene-d8 (S)
109
%
70-130
1
12/22/16 14:01
2037-26-5
1,2-Dichloroethane-d4 (S)
87
%
70-130
1
12/22/16 14:01
17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 5.0 1 12/20/16 18:49
420.4 Phenolics, Total Analytical Method: EPA420.4
Phenol ND mg1L 0.010 1 1 V29116 12:11
450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg1L 0.0080 1 12/27/1615:15 57-12-5
Date: 12/30/2016 04:24 PM
REPORT OF LABORATORY ANALYSIS
This report sholl not he reproduced. except in full,
without the written consent of Pace Analytical Services. LLC.
Page 11 of 33

o
aceAnalytical
*Wpacebbs.cem
QUALITY CONTROL DATA
Project: Stormwater 12-2016
Pace Project No.: 92323876
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
QC Batch: 342987
Analysis Method:
EPA 16648
QC Balch Method: EPA 1664E
Analysis Description:
1664 HEM, Oil and Grease
Associated Lab Samples: 92323876001, 92323876002
METHOD BLANK: 1902460
Matrix: Water
Associated Lab Samples: 92323876001, 92323876002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Oil and Grease
mglL
ND 5.0 12/30/16 06:48
LABORATORY CONTROL SAMPLE:
1902461
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Gil and Grease
mglL
40 36.2
90 78-114
MATRIX SPIKE SAMPLE:
1902462
92324900001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Oil and Grease
mglL
ND 40
36.5 91 78-114
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in cull,
Date: 12130/2016 04:24 PM without the written consent of Pace Analytical Services, I.I.C. Page 12 of 33

aceAnalytical
'
www.pacelabscom
Project: Stormwater 12-2016
Pace Project No.: 92323876
QC Batch: 341624
QC Batch Method: EPA 200.7
Associated Lab Samples: 92323876001, 92323876002
METHOD BLANK: 1895479
Associated Lab Samples: 92323876001, 92323870002
Parameter Units
Copper ug1L
Lead ug1L
Zinc uglL
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 5.0 12/27/16 23:02
ND 5.0 12/27/16 23:02
N❑ 10.0 12/27/16 23:02
Qualifiers
Paco Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1895480
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Copper
ug1L
500
459 92 85-115
Lead
ug/L
500
456 91 85-115
Zinc
ug1L
500
476 95 85-115
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
1895481
1895482
MS
MSD
92323766001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc,
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper ug/L
ND
500
500
543
506
109
101
70-130
7
Lead ug/L
ND
500
500
535
502
107
100
70-130
6
Zinc uglL
ND
500
500
564
526
113
105
70-130
7
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1895483
1895484
MS
MSD
92323876002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper ug1L
ND
500
500
520
519
104
104
70-130
0
Lead ug/L
ND
500
500
516
519
103
104
70-130
1
Zinc ug/L
ND
500
500
541
545
107
108
70-130
1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 33

.aceAnalytical
*W patxlab$.mm
QUALITY CONTROL DATA
Project: Stormwater 12-2016
Pace Project No.: 92323876
QC Batch: 342037 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92323876001, 92323876002
Pate Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilte, NC 28078
[phone]
METHOD BLANK: 1897514
Matrix: Water
Associated Lab Samples: 92323876001, 92323876002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1. 1. 1 -Trichloroethane
ug1L
NO
2.0
12/2211612:33
1,1.2,2-Tetrachloroethane
ug/L
NO
2.0
12/22/1612:33
1. 1, 2-Trichloroethane
ug/L
NO
2.0
12/22/1612:33
1.1-Dichloroethane
ug1L
ND
2.0
12/22/1612:33
1,1-Dichloroethene
ug1L
NO
2.0
12122J1612:33
1,2-Dichlorobenzene
ug/L
NO
2.0
12/22/1612:33
1,2-Dichloroethane
ug1L
NO
2.0
1212211612:33
1,2-Dichloropropane
ug/L
NO
2.0
1212211612:33
1,3-Dichlorobenzene
ug/L
NO
2.0
12/22J1612:33
1,4-Dichlorobenzene
ug1L
NO
2.0
12/22/1612:33
Benzene
ug/L
NO
2.0
12/22/1612:33
Bromodichloromethane
ug/L
ND
2.0
12/2211612:33
Bromoform
ug/L
ND
2.0
12/22/1612:33
Bromomethane
ug/L
ND
2.0
1212211612:33
Carbon tetrachloride
ug/L
ND
2.0
12/22/16 12:33
Chlorobenzene
ug/L
ND
2.0
12/2211612:33
Chloroethane
ug/L
ND
2.0
1212211612:33
Chloroform
ug/L
ND
2.0
1212211612:33
Chloromethane
ug/L
ND
2.0
12/22/1612:33
cis-1,2-Dichloroethene
ug/L
ND
2.0
12/22/1612:33
cis-1,3-Dichloropropene
ug1L
ND
2.0
12122/1612:33
D ibromoch lorom ethane
ug/L
ND
2.0
1212211612:33
Ethylbenzene
ug/L
ND
2.0
12/2211612:33
Methylene Chloride
ug/L
ND
2.0
12/22/16 12:33
Tetrachloroethene
ug/L
ND
2.0
1212211612:33
Toluene
ug1L
ND
2.0
1212211612:33
trans- 1, 2-Dichloroethene
ug/L
ND
2.0
1212211612:33
trans-1,3-Dichloropropene
uglL
ND
2.0
1212211612:33
Trchloroethene
ug/L
ND
2.0
12/2211612:33
Tdchlorofluoromethane
ug1L
ND
2.0
12/2211612:33
Vinyl chloride
ug/L
ND
2.0
12122/16 12:33
1,2-Dichloroethane-d4 (S)
%
87
70-130
12/22/16 12:33
4-Bromofluorobenzene (S)
%
99
70-130
12/22116 12:33
Toluene-d8 (S)
%
104
70-130
12/22116 12:33
LABORATORY CONTROL SAMPLE:
1897515
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
1,1,1-Trichloroethane
ug/L
20
18.0
90 52-162
1,1,2,2-Tetrachloroethane
ug/L
20
18.1
90 46-157
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not Ite reproduced, except in Full,
Dale: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 33

Pace Analytical Services, LLC
e 9800 Kincey Ave. Suite 100
ac6Malytkal Huntersville, NC 28078
WWwPacPW&WM
[phone]
QUALITY CONTROL DATA
Project: Stormwater 12-2016
Pace Project No.: 92323876
LABORATORY CONTROL SAMPLE: 1897515
Spike
LCS
LCS
% Rec
Parameter
Units
Colic.
Result
% Rec
Limits
Qualifiers
1,1,2-Tdchloroethane
ug/L
20
19.5
98
52-150
1,1-Dichloroethane
ug/L
20
19.1
96
59-155
1,1-Dichloroethene
ug1L
20
19.8
99
1-234
1,2-Dichlorobenzene
ug/L
20
19.3
96
18-190
1,2-Dichloroethane
ug/L
20
16.6
83
49-155
1,2-Dichloropropane
ug/L
20
20.1
100
1-210
1,3-Dichlorobenzene
ug/L
20
19.6
98
59-156
1,4-Dichlorobenzene
uglL
20
19.6
98
18-190
Benzene
ug/L
20
19-6
98
37-151
Bromodichloromethane
ug/L
20
18.9
95
35-155
Bromoform
ug/L
20
17.6
88
45-169
Bromomethane
ug/L
20
19.6
98
1-242
Carbon tetrachloride
ug/L
20
18.9
95
70-140
Chlorobenzene
ug/L
20
19.0
95
37-160
Chloroethane
ug/L
20
19.9
99
14-230
Chloroform
ug/L
20
17.7
88
51-138
Chloromethane
ug/L
20
23.0
115
1-273
cis- 1,2-Dichloroethene
ug/L
20
18.3
91
68-146
cis- 1,3-Dich loropropene
ug/L
20
20.5
103
1-227
Dibromochloromethane
ug/L
20
19.0
95
53-149
Ethylbenzene
ug/L
20
18.8
94
37-162
Methylene Chloride
ug/L
20
18.7
93
1-221
Tetrachloroethene
ug/L
20
18.9
95
64-148
Toluene
ug/L
20
19.1
96
47-15D
trans-1,2-Dichloroethene
ug/L
20
19.3
96
54-156
trans-1,3-Dichloropropene
ug/L
20
18.6
93
17-183
Trichloroethene
ug/L
20
19.6
98
71-157
Trichlorofluoromethane
ugfL
20
20.1
100
17-181
Vinyl chloride
ug/L
20
17.6
88
1.251
1,2-Dichloroethane-d4 (S)
%
88
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
1897517
92323196006
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1-Tdchloroethane
ug/L
ND
80
83.6
105
46-171
1,1,2,2-Tetrachloroethane
ug1L
ND
80
74.3
93
73-159
1,12-Trichloroethane
ug/L
ND
80
76.7
96
64-152
1,1-Dichloroethane
ug/L
NO
80
83.4
104
43-172
1,1-Dichloroethene
UWL
ND
80
81.5
102
48-189
1,2-Dichlorobenzene
ug/L
ND
80
82.9
103
54-154
1,2-Dichloroethane
ug/L
ND
80
76.3
93
42-171
1,2-Dichloropropane
uglL
ND
80
85A
106
55-157
1,3-Dichlorobenzene
ug/L
ND
80
84.4
105
57-148
Results presented on this page are in the units Indicated by the -Units' column except where an alternate unit is presented to the right at the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 1213012016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 33

aceAnalytical
www ptrtarabswm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: Slormwater 12-2016
Pace Project No.: 92323876
MATRIX SPIKE SAMPLE: 1897517
92323196006
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
NO
80
84.3
105
58-149
Benzene
ug/L
586
80
648
78
54-163
Bromodichloromethane
ug/L
ND
80
79.5
99
56-152
Bromeform
uglL
NO
80
70.2
88
53-151
Bromomethane
ug/L
ND
80
58.8
73
10-200
Carbon tetrachloride
ug/L
NO
80
83.5
104
41-175
Chlorobenzene
ug/L
14.3
80
98.0
105
67-152
Chioroethane
ug/L
NO
80
71.8
90
23-200
Chloroform
ug/L
ND
80
82.3
101
51-156
Chioromethane
ug/L
NO
80
44.5
51
40-175
cis-1,2-Dichloroethene
ug/L
ND
80
81.8
102
45-174
cis-1,3-Dichloropropene
ug/L
NO
80
84.6
106
38-146
❑ibromochioromethane
ug/L
NO
80
78.4
98
65-144
Ethylbenzene
ug/L
ND
80
86.5
103
57-152
Methylene Chloride
ug/L
11.9
80
82.0
88
40-167
Tetrachloroethene
uglL
NO
80
85.7
107
59-155
Toluene
ug/L
19.1
80
100
102
47-162
trans-1,2-Dichloroethene
ug1L
NO
80
85.6
107
47-178
trans- 1,3-Dichloropropene
ug/L
NO
80
77.3
97
39-148
Trichloroethene
ug1L
NO
80
83.9
105
W153
TdchloroAuoromethane
ug1L
NO
60
78.3
98
42-199
Vinyl chloride
uglL
NO
80
42.4
52
46-176
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-BromoHuorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 1897516
Parameter
Units
92323196002
Result
Dup
Result RPD Qualifiers
1.1,1-Trichloroethane
ug/L
NO
NO
1,1,2,2-Tetrachloroethane
ug/L
NO
NO
1,1,2-Trichloroethane
ug1L
NO
NO
1,1-Dichloroethane
ug/L
NO
NO
1,1-Dichloroethane
ug1L
NO
NO
1,2-Dichlorobenzene
ug/L
ND
NO
1,2-Dichloroethane
ug1L
NO
NO
1,2-Dichlaropropane
ug/L
ND
ND
1,3-Dichlorobenzene
ug1L
ND
ND
1,4-Dichlorobenzene
ug1L
NO
NO
Benzene
ug/L
616
66T 8
Bromodichloromethane
ug/L
NO
NO
Sromoform
ug/L
NO
NO
Bromomethane
uglL
NO
ND
Carbon tetrachloride
uglL
ND
NO
Chlorobenzene
ugll-
ND
ND
Results presented on this page are In the units Indicated by the 'Units- column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 33

aceAnalytical.
W, pacildi crnn
QUALITY CONTROL DATA
Project: Slarmwater 12-2016
Pace Project No.: 92323876
SAMPLE DUPLICATE: 1897516
Parameter
Units
92323196002
Result
Dup
Result
Chloroethane
uglL
ND
NO
Chloroform
uglL
ND
ND
Chloromethane
uglL
ND
NO
cis-1,2-Dichloroethene
uglL
NO
ND
cis-1,3-Dichloropropene
uglL
ND
ND
Di bromochlorom ethane
uglL
ND
NO
Ethylbenzene
uglL
10.9
11.0
Methylene Chloride
ug1L
16.6
16.9
Tetrachloraethene
ug1L
ND
NO
Toluene
ug1L
39.6
41.1
trans-12-Dichtoroethene
ug1L
ND
ND
trans-1,3-Dichloropropene
ug1L
ND
ND
Trichloroethene
uglL
ND
NO
Trich lorofluorom ethane
uglL
NO
ND
Vinyl chloride
uglL
NO
ND
1,2-Dichtoroethane-d4 (S)
%
87
92
4-Bromofluorobenzene (S)
%
98
101
Toluene-d8 (S)
%
104
110
RPD Qualifiers
2
2
4
5
3
6
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit la presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 33

aceAnalytical e
W w.Pac"&com
QUALITY CONTROL DATA
Project: Stormwater 12-2016
Pace Project No.: 92323876
QC Batch: 341800 Analysis Method: EPA 608
QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB
Associated Lab Samples: 92323876001, 92323876002
METHOD BLANK: 1896371
Matrix: Water
Associated Lab Samples:
92323876001, 92323876002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
4,4'-DDD
ug/L
ND
0.050
12128/1618:38
4,4'-DDE
ug/L
NO
0.050
12128/1618:38
4,4'-DOT
ug/L
NO
0.050
12f28/1618:38
Aldrin
ug/L
NO
0.050
12128/1618:38
alpha-BHC
ug/L
ND
0.050
12f28/1618:38
beta-BHC
uglL
ND
0.050
1212811618:38
Chlordane (Technical)
ug/L
NO
0.50
12/28116 18:38
delta-BHC
ug/L
NO
0.050
12128/1618:38
Dieldrin
ug/L
NO
0.050
12128/161&38
Endosulfan I
ug/L
NO
0.050
12/28/16 18:38
Endosulfan II
ug/L
NO
0.050
12/28/16 18:38
Endosulfan sulfate
ug/L
NO
0.050
12/28/16 18:38
Endrin
ug/L
NO
0.050
1212811618:38
Endrin aldehyde
ug/L
ND
0.050
12/28/16 18:38
gamma-BHC (Lindane)
ug/L
NO
0.050
12/28/16 18:38
Heptachlor
ug/L
NO
0.050
1212811618:38
Heptachlor epoxide
ug/L
NO
0.050
12/28/16 18:38
PCB-1016 (Aroclor 1016)
ug/L
ND
0.50
12128)16 18:38
PCB-1221 (Aroclor 1221)
ug/L
NO
0.50
12128116 18:38
PCB-1232 (Aroclor 1232)
ug/L
NO
0.50
12/28116 18:38
PCB-1242 (Aroclor 1242)
ug/L
ND
0.50
12/28/16 18:38
PCB-1248 (Aroclor 1248)
ug/L
ND
0.50
12f28/16 18:38
PCB-1254 (Aroclor 1254)
ug/L
ND
0.50
12/28116 18:38
PCB-1260 (Aroclor 1260)
ug/L
ND
0.50
12/28/16 18:38
Toxaphene
ug/L
ND
0.50
12/28/1618:38
Decachlorobiphenyl (S)
%
81
20-138
12/28/16 18:38
Tetrachlora-m-xylene (S)
%
76
20-110
12/28/16 18:38
Pace Analytical Services, I -LC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1896372
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4,4'-DDD
ug1L
.25
0.25
99
31-141
4,4'-DDE
ug1L
.25
0.25
100
30-145
4,4'-DDT
uglL
.25
0.25
100
25-160
Aldrin
ug/L
.25
0.20
81
42-122
alpha-BHC
ug/L
.25
0.23
91
37-134
beta-BHC
ug/L
.25
0.25
99
17-147
delta-BHC
ug/L
.25
0.33
133
19-140
Dieldrin
ug/L
25
0.23
94
36-146
Endosulfan I
ugfl-
.25
0.25
100
45-153
Results presented on this page are In the units indicated by the "Units- column except where an alternate unit Is presented to the eight of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 33

aeeAnalytical`
WWW..pacelahs.com
QUALITY CONTROL DATA
Project: Stormwaler 12-2016
Pace Project No.: 92323876
LABORATORY CONTROL SAMPLE:
Parameter
1896372
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Endosulfan II
ug1L
.25
0.26
105
1-202
Endosulfan sulfate
ug/L
.25
0.27
108
26-144
Endrin
ug/L
.25
0,25
103
30-147
Endrin aldehyde
uglL
.25
0.22
89
50-150
gamma-BHC (Lindane)
ug1L
.25
0.23
95
32-127
Heptachlor
uglL
.25
0.22
87
34-111
Heptachlor epoxide
ug/L
.25
0.25
100
41-126
Decachlorobiphenyl (S)
%
79
20-138
Tetrachloro-m-xylene (S)
%
86
20-110
Pace Analytical Services, LLC
98M Kincey Ave- Suite 100
Hunlersville, NC 28078
[phone]
Qualifiers
Results presented on this page are In the units indicated by the unit' column except where an alto, to unll Is presented to the right of She result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12130/2016 04:24 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 33

aceAnalytical"
winr.bs Dorn
QUALITY CONTROL DATA
Project: Slormwater 12-2016
Pace Project No.: 92323876
QC Batch: 342056
QC Batch Method: EPA625
Associated Lab Samples: 92323876001, 92323876002
Analysis Method:
Analysis Description:
EPA 625
625 MSS
METHOD BLANK: 1897681
Matrix: Water
Associated Lab Samples: 92323876001, 92323876002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
12122/1614:59
2,2'-Oxybis(1-chloropropane)
ug/L
NO
5.0
1212211614:59
2,4,6-Trichlorophenol
ug/L
ND
10.0
12122/1614.59
2,4-Dichforophenol
ug/L
ND
5-0
12/2211614:59
2,4-Dimethylphenol
ug/L
NO
10.0
12122116 14:59
2,4-Dinitrophenol
ug1L
NO
50.0
1212211614.59
2,4-Dinitrotoluene
ug/L
NO
5.0
12/2211614:59
2,6-Dinitrotoluene
ug/L
NO
5.0
1212211614:59
2-Chloronaphthalene
ug/L
NO
5.0
12/2211614:59
2-Chlorophenol
ug/L
NO
5.0
1212211614:59
2-Nitrophenol
ug/L
NO
5.0
1212211614:59
3,3'-Dichlorobenzidine
ug/L
NO
25.0
1212211614:59
4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
12/22/1614:59
4-Bromophenylphenyl ether
ug/L
ND
5.0
12/22/16 14:59
4-Chloro-3-methylphenol
ug/L
NO
5.0
1212211614:59
4-Chlorophenylphenyl ether
ug/L
NO
5.0
12/22/16 14:59
4-Nitrophenol
ug/L
NO
50.0
1212211614:59
Acenaphthene
ug/L
ND
5.0
1212211614:59
Acenaphthylene
ug/L
ND
5.0
12122/1614:59
Anthracene
ug/L
NO
5.0
1212211614:59
Benzo(a)anthracene
ug/L
ND
5.0
12122f1614:59
Benzo(a)pyrene
ug/L
ND
5-0
12/22/1614:59
Benzo(b)Ouoranthene
ug/L
ND
5.0
12/22/1614:59
Benzo(g,h,i)perylene
ug/L
ND
5-0
12/2211614:59
Benzo(k)fluoranthene
ug1L
ND
5.0
1212211614:59
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
12/22/16 14:59
bis(2-Chloroethyl) ether
ug/L
NO
5.0
12/22/16 14:59
bis(2-Ethylhexyl)phthalate
uglL
ND
5.0
12/22/1614:59
Butylbenzylphthalate
ug/L
ND
5.0
12/22/1614:59
Chrysene
ug1L
NO
5.0
12/22/1614:59
Di-n-bulylphthalate
ug/L
ND
5.0
12/22/1614:59
Di-n-octylphthalate
ug/L
NO
5.0
12122/1614:59
Dibenz(a,h)anthracene
ug/L
ND
5.0
12/22/1614:59
Diethylphtha late
ug/L
ND
5.0
1212211614:69
Dimethylphthalate
ug/L
ND
5.0
12/22/1614:59
Fluoranthene
ug1L
ND
5.0
12/22/1614:59
Fluorene
ug/L
ND
5.0
12122/1614:59
Hexachloro-1,3-butadiene
1191L
ND
5.0
1212211614:59
Hexachlorobenzene
ug/L
ND
5-0
12122/1614:59
Hexachlorocyclopentadiene
ug1L
Nil
10.0
12122116 14:59
Hexachtoroethane
ugJL
NO
5.0
12122/1614:59
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Results presented on thts page are In the units indicated by the "Unit$- column except where an alternate unit is presented to the right of the reudt,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 33

Pace Analytical Services, LLC
aC4i1!li7llisQ�® 9800 KinceyAve. Suite 100
1i r J Nuntersville, NC 28078
"Wpaowabs.ccrn [phone]
QUALITY CONTROL DATA
Project: Stormwater 12-2016
Pace Project No.: 92323876
METHOD BLANK: 1897681
Associated Lab Samples: 92323876001, 92323876002
Parameter Units
Matrix
Blank
Result
Water
Reporting
Limit
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
NO
5.0
12/2211614:59
Isophorone
ug/L
NO
10.0
12122/1614:59
N-Nitroso-di-n-propylamine
ug/L
NO
5.0
1212211614:59
N-Nitrosodimethylamine
ug/L
NO
5.0
12/22/1514:59
N-Nitrosodiphenylamine
ug/L
ND
10.0
12/22/1614:59
Naphthalene
ug/L
ND
5.0
1212211614:59
Nitrobenzene
u911-
NO
5,0
12/2211614:59
Pentachlorophenoi
ug/L
ND
10.0
12/2211614:59
Phenanthrene
ug/L
ND
5.0
12/22/1614:59
Phenol
ug/L
ND
5.0
12f2211614-.59
Pyrene
ug1L
NO
5.0
12/2211614:59
2,4,6-Tribromophenol (S)
%
80
10-137
12/22/16 14:59
2-Fluarobiphenyl (S)
%
73
15-120
12/22/16 14:59
2-Ftuorophenol (S)
%
43
10-120
12/22/16 14:59
Nitrobenzene-d5 (5)
%
67
10-120
12/22/16 14:59
Phenol-dB(S)
%
30
10-120
12/22/16 14:59
Terphenyl-d14 (S)
%
88
11-131
12/22/16 14:59
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1897682
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
32.3
65
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
37.1
74
36-166
2,4,6-Trichlorophenol
ug/L
50
42.1
84
37-144
2,4-Dichlorophenol
ugiL
50
42.5
85
1-191
2,4-Dimethylphenol
ug/L
50
41.0
82
32-119
2,4-Dinitrophenol
ug/L
250
145
58
1-181
2,4-Dinitrotoluene
ug/L
50
39.1
78
39-139
2,6-Dinitrotoluene
ug/L
50
40.5
81
50-168
2-Chloronaphthatene
ug/L
50
37.5
75
60-118
2-Chlorophenol
ug/L
50
38.7
77
23-134
2-Nitrophenol
ug/L
5o
39.3
79
29-182
3,3'-Dichlorobenzidlne
ug/L
100
77.6
78
1-262
4,6-Dinitro-2-methyl phenol
ug/L
100
88.1
88
1-181
4-Bromophenylphenyl ether
ug1L
50
39.4
79
53-127
4-Chloro-3-methylphenol
ug/L
100
78.0
76
22-147
4-Chlorophenylphenyl ether
ug/L
50
37.8
76
25-158
4-Nitrophenol
ug/L
250
74.4
30
1-132
Acenaphthene
ug/L
50
40.0
80
47-145
Acenaphthylene
ug/L
50
40.8
82
33-145
Anthracene
ug/L
50
42.0
84
1-166
Benzo(a)anthrecene
ug/L
50
39.7
79
33-143
Benzo(a)pyrene
ug/L
50
42.7
85
17-163
Benzo(b)Suoranthene
ug/L
50
38.5
77
24-159
Qualifiers
Results presented on this page are In the units indicated by the 'units' column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall mat be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent or Pace Analytical Services, LLC. Page 21 of 33

aceAnalytical
www.pacefabscom
QUALITY CONTROL DATA
Project: Stormwater 12-2016
Pace Project No.: 92323876
LABORATORY CONTROL SAMPLE:
Parameter
1897682
Units
Spike
Cone.
LCS
Result
Benzo(g,h,i)perylene
uglL
50
44.9
Benzo(k)Ruoranthene
uglL
50
43.8
bis(2-Chloroethoxy)methane
uglL
50
37.4
bis(2-Chloroethyl) ether
uglL
50
38.5
bis(2-Ethylhexyl)phthalate
uglL
50
44.4
Butylbenzylphthalate
uglL
50
43.2
Chrysene
uglL
50
40.9
Di-n-butylphthalate
uglL
50
44.8
Di-n-octylphthatate
ug1L
50
44.1
Dibenz(a,h)anthracene
ug1L
50
43.2
Diethyfphthalate
ug1L
50
42A
Dimethylphthalate
ug1L
50
40.5
Fluoranthene
ug1L
50
42.8
Fluorene
ug1L
50
40.7
Hexachloro-1,3-butadiene
ug1L
50
28.0
Hexachlorobenzene
ug1L
50
40.5
Hexachlorocyclopentadiene
ug1L
50
30.6
Hexachloroethane
ug1L
50
28.6
Indeno(1,2,3-cd)pyrene
ug1L
50
44.9
Isophorone
uglL
50
38.2
N-Nitroso-di-n-propylamine
ug1L
50
40A
N-Nitrosodirnethylamine
U91L
50
28.9
N-Nitrosodiphenylamine
uglL
50
43.5
Naphthalene
uglL
50
36.6
Nitrobenzene
uglL
50
35.5
Pentachlorophenol
uglL
100
87.7
Phenanthrene
ugfL
50
41.5
Phenol
uglL
50
20.4
Pyrene
ug/L
50
38.8
2,4,6-Thbromophenol (S)
%
2-Fluorobiphenyl (3)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
MATRIX SPIKE SAMPLE: 1897683
Parameter Units
1,2,4-Trichlorobenzene
ug1L
2,2'-Oxybis(1-chloropropane)
uglL
2,4,6-Trichiorophenol
ug1L
2,4-Dichlorophenol
ug1L
2,4-Dimelhylphenol
ug(L
2,4-Dinitrophenol
uglL
LCS
% Rec
% Rec
Limits
90 1-219
88 11-162
75 33-184
77 12-158
89 B-158
86 1-152
82 17-168
90 1-118
88 4-146
86 1-227
85 1-114
81 1.112
86 26-137
81 59-121
56 24-116
81 1-152
61 25-150
57 40-113
90 1-171
76 21-196
81 1-230
58 25-150
87 25-150
73 21-133
71 35-180
88 14-176
83 54-120
41 5-112
78 52-115
90 10-137
73 15-120
44 10-120
70 10-120
33 10.120
76 11-131
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
92323876001 Spike MS MS % Rec
Result Cone. Result % Rec Limits Qualifiers
ND
50
40A
80
44-142
ND
50
36.4
73
36-166
ND
50
49.7
99
37-144
NO
50
46.5
93
1-191
ND
50
44A
89
32-119
ND
250
188
75
1-181
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12/30/2010 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 33

aCeAnalytical.
WNW.pecefabs, oom
QUALITY CONTROL DATA
Project: Stormwater 12-2016
Pace Project No.: 92323876
Pace Analytical Services, LLC
9800 Kincey Aye. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
1897683
Units
92323876001
Result
Spike
Conc.
MS
Result
Ms
% Rec
% Rec
Limits Qualifiers
2,4-Dinitrotoluens
uglL
ND
50
50.7
101
39-139
2,6-Dinitrotoluene
uglL
NO
50
50.9
102
50-158
2-Chloronaphthalene
uglL
NO
50
44.1
88
60-118
2-Chlorophenol
ugfL
ND
50
40.6
81
23-134
2-Nitrophenol
uglL
NO
50
47.2
94
29-162
3,3'-Dichlorobenzidine
ugfL
NO
100
86.6
87
1-262
4,6-Dinitro-2-methylphenol
ugfL
NO
too
97.8
98
1-181
4-Bromophenylphenyl ether
uglL
ND
50
43.6
87
53-127
4-Chloro-3-methylphenol
uglL
NO
100
95.8
96
22-147
4-Chtorophenylphenyl ether
ug/L
NO
50
43.0
86
25-158
4-Nitrophenol
ugfL
ND
250
126
51
1-132
Acenaphthene
ug1L
ND
50
45-9
92
47-145
Acenaphthylene
ug/L
ND
50
45.4
91
33-145
Anthracene
ug1L
NO
50
47.3
95
1-166
Benzo(a)anthracene
ug1L
ND
50
45.4
91
33-143
Benzo(a)pyrene
ug/L
ND
50
46.0
92
17-163
Benzo(b)fluoranthene
uglL
NO
50
48.9
98
24-159
Benzo(g,h,i)perylene
ug1L
NO
50
41.5
83
1-219
Benzo(k)fluoranthene
ug1L
ND
50
49.4
99
11-162
bis(2-Chloroethoxy)methane
ug1L
ND
50
41.9
84
33-184
bis(2-Chloroethyl)ether
ug1L
ND
50
40.1
80
12-158
bis(2-Ethylhexyl)phthala1e
uglL
ND
50
48.7
97
8-158
Butylbenzylphthalate
ug/L
ND
50
48.7
97
1-152
Chrysene
uglL
ND
50
45A
90
17-168
Di-n-bulylphthatate
ug1L
ND
50
51.0
102
1-118
Di-n-octylphthalate
ugfL
ND
50
51.6
103
4-146
Dibenz(a,h)anthracene
ugfL
ND
50
45.6
91
1-227
Diethylphthalate
ugfL
NO
50
50.4
101
1-114
Dimethylphthalate
ugfL
ND
50
49.6
99
1-112
Fluoranthene
ugfL
ND
50
50.4
101
26-137
Fluorene
uglL
ND
50
45.6
91
59-121
Hexachloro-11,3-butadiene
uglL
ND
5o
36.5
73
24-116
Hexachlorobenzene
ugfL
ND
50
45.0
92
1-152
Hexachlorocyclopentadiene
uglL
ND
50
38.0
76
25-150
Hexachloroethene
uglL
ND
50
31.7
63
40-113
Indeno(1,2,3-cd)pyrene
uglL
ND
50
44.0
88
1-171
Isophorone
uglL
ND
50
42.7
85
21-196
N-Nitroso-di-n-propylamine
uglL
ND
50
40.8
82
1-230
N-Nitrosodimethylamine
uglL
ND
50
28.1
56
25-150
N-Nitrosodiphenylamine
uglL
ND
50
47.5
95
25-150
Naphthalene
uglL
ND
5o
40.5
81
21-133
Nitrobenzene
uglL
ND
50
45.2
90
35-180
Pentachlorophenol
ugfL
ND
100
122
122
14-176
Phenanthrene
ugfL
ND
50
46-9
94
54-120
Phenol
ugfL
NO
50
17.9
36
5-112
Pyrene
uglL
ND
50
46.2
92
52-115
2,4,6-Tribromaphenol (S)
%
104
10-137
Results presented on this page are In the units Indicated
by the "Units' column
except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 33

aoAnalytical
www.paceisftoom
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater 12.2016
Pace Project No.: 92323876
MATRIX SPIKE SAMPLE: 4897683
92323876001 Spike MS MS
% Rec
Parameter Units
Result Conc. Result % Rec
Limits Qualifiers
2-Fluorobiphenyl (S) %,
87
15-120
2-Fluorophenol (S) %,
49
10-120
Nitrobenzene-d5 (S) %
91
10-120
Phenol-d6 (S) %
33
10-120
Terphenyl-d14 (S) %
97
11-131
SAMPLE DUPLICATE: 1897684
Parameter
Units
92323876002
Result
Dup
Result
1,2,4-THchlorobenzene
uglL
NO
NO
2,2'-Oxybis(1-chloropropane)
uglL
ND
NO
2,4,6-Trichlorophenol
ug1L
NO
NO
2,4-Dichlorophenol
ug1L
NO
ND
2,4-Dimethylphenol
uglL
ND
NO
2,4-Dinitrophenol
uglL
ND
NO
2,4-Dinitrotoluene
ug1L
ND
NO
2,6-Dinitrotoluene
ug1L
ND
NO
2-Chloronaphthalene
ug1L
NO
NO
2-Chlorophenol
Ug1L
NO
ND
2-Nitrophenol
uglL
NO
NO
3,3'-Dichlorobenzidine
ug/L
NO
ND
4,6-Dinitro-2-methylphenol
ug1L
NO
ND
4-Bromophenylphenyl ether
uglL
NO
NO
4-Chloro-3-methylphenol
ug1L
NO
NO
4-Chlorophenylphenyl ether
ug1L
NO
ND
4-Nitrophenol
ug1L
NO
NO
Acenaphthene
uglL
NO
ND
Acenaphthylene
ug1L
NO
NO
Anthracene
ug1L
NO
NO
Benzo(a)anthracene
ug1L
NO
ND
Benzo(a)pyrene
ug1L
NO
NO
Benzo(b)fluoranthene
ug1L
NO
ND
Benzo(g,h,i)perylene
ug1L
NO
ND
Benzo(k)fluoranthene
ug1L
NO
ND
bis(2-Chloroethoxy)methane
uglL
NO
NO
bis(2-Chloroethyl) ether
ug/L
NO
NO
bis(2-Ethylhexyl)phthalate
uglL
NO
ND
Butylbenzylphthalate
ug/L
NO
ND
Chrysene
ug/L
NO
NO
Di-n-butylphthalate
ug/L
NO
ND
Di-n-octylphthalate
ug1L
NO
NO
Dibenz(a,h)anthracene
ug1L
NO
ND
Diethylphthalate
ug1L
NO
ND
Dimethylphthalate
ug1L
NO
ND
Fluoranthene
ug1L
NO
ND
RPD Qualifiers
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, L-C. Page 24 of 33

IeAnalytical
www.pacebbs.cam
QUALITY CONTROL DATA
Project: Stormwater 12-2016
Pace Project No.: 92323876
SAMPLE DUPLICATE: 1897684
Parameter
Units
92323876002
Result
Dup
Result
Fluorene
uglL
ND
ND
Hexachloro-1,3-butadiene
uglL
ND
ND
Hexachlorobenzene
uglL
N❑
ND
Hexachlorocyclopentadiene
ug/L
ND
ND
Hexachloroethane
uglL
ND
ND
Indeno(1,2,3-cd)pyrene
uglL
ND
ND
Isophorone
uglL
ND
ND
N-Nitroso-di-n-propylamine
uglL
ND
ND
N-Nitrosodimethylamine
uglL
ND
ND
N-Nitrosodiphenylamine
uglL
ND
ND
Naphthalene
uglL
ND
ND
Nitrobenzene
uglL
ND
ND
Pentachlorophenol
ug1L
ND
ND
Phenanthrene
uglL
ND
ND
Phenol
uglL
ND
ND
Pyrene
uglL
ND
ND
2,4,6-Tribromophenol (S)
%
61
91
2-Fluorobiphenyl (S)
%
63
87
2-Fluorophenol (S)
%
30
45
Nitrobenzene-d5 (S)
%
67
83
Phenol-d6 (S)
%
21
28
Terphenyl-d14 (S)
%
93
97
RPD Qualifiers
40
31
38
22
28
4
Pace Analytical Services, I -LC
9800 Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the -Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 33

(�laceAnalytical
* tnrwpw "stmr
QUALITY CONTROL DATA
Project: Stormwater 12-2016
Pace Project No.: 92323876
QC Batch: 341807 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92323876001, 92323876002
METHOD BLANK: 1896433 Matrix: Water
Associated Lab Samples: 92323876001, 92323876002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 12120/16 18:46
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1896434
Spike LCS LCS % Ree
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 244 98 90-110
SAMPLE DUPLICATE: 1896435
92323837025 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L ND ND
SAMPLE DUPLICATE: 1896436
92323876002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mgJL NO ND
Results presented on this page are in the units indicated by the 'Units" column except where an alternate unit Is presented to the rfght of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 33

y
aceAnalytical
WW,,paultift o=
Project: Stormwater 12-2016
Pace Project No.: 92323876
QC Batch: 342739
QC Batch Method: EPA420.4
Associated Lab Samples: 92323876001, 92323876002
METHOD BLANK: 1901094
Associated Lab Samples: 92323876001, 92323876002
Parameter Units
Phenol mg1L
LABORATORY CONTROL SAMPLE: 1901095
Parameter Units
Phenol mglL
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huniersville, NC 28078
(704)875.9D92
QUALITY CONTROL DATA
Analysis Method: EPA 420.4
Analysis Description: 420.4 Phenolics
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.010 12129/1611:49
Spike LCS LCS % Rec
Conc. Result % Rec Limits Ouatifiers
.05 0,047 95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1901096 1901097
MS MSD
92322797002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Phenol mg/L 0.085 .05 .05 0.13 0.13 93 100 90-110 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1901098 1901099
MS MSD
92322819001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phenol mg1L ND .05 .05 0.053 0.053 88 89 90-110 1 M1
Results presented on this page are In the units Indicated by the -Units' column except where an alternate unit Is presented to the right of the restitt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the wrllten consent of Pace Analytical Services, LLC.
Page 27 of 33

aceAnalytical
wxw.pactakb:=n
Project: Stormwater 12-2016
Pace Project No,: 92323876
QC Batch: 342534
QC Batch Method: SM 4500-CN-E
Associated Lab Samples: 92323876001, 92323876002
METHOD BLANK: 1900216
Associated Lab Samples: 92323876001, 92323876002
Parameter Units
Cyanide mg/L
LABORATORY CONTROL SAMPLE: 1900217
Parameter Units
Cyanide mg1L
QUALITY CONTROL DATA
Analysis Method:
Analysis Description
Matrix: Water
SM 4500-CN-E
450OCNE Cyanide, Total
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Blank Reporting
Result Limit Analyzed Qualifiers
NO O.D080 1212711614:48
Spike LCS LCS % Rec
Conc, Result % Rec Limits Qualifiers
.1 0.10 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1900218 1900219
MS MSD
92323615002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual
Cyanide mg1L NO A .1 0.10 0.095 98 94 75-125 5
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1900220 1900221
MS MSD
92323758005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Cont. Result Result % Rec % Rec Limits RPD Qual
Cyanide mg/L ND A .1 0,11 0.094 104 92 75-125 11 R1
Results presented on this page are in the units indicated by the 'Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 33

aceAnalytical
www.pw&'abs.cora
QUALIFIERS
Project: Stormwater 12-2016
Pace Project No.: 92323876
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MD -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 33

I
e
5aceftlyfical
(�www.PF0086s oar
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stormwater 12-2016
Pace Project No.: 92323876
Lab ID
92323876001
92323876002
92323876001
92323876002
92323876001
92323876002
92323876001
92323876002
92323876001
92323876OD2
92323876001
92323876002
92323876001
92323876002
92323876001
92323816002
92323876001
92323876002
Sample ID
Outfall #1
Outfall #2
Outfall #1
Outfall #2
Outfall #1
Outfall #2
Outfall #1
Outfall #2
Outfall #1
Outfall #2
Outfall #1
Outfall #2
Outfall #1
Outfall #2
Outfall #1
Outfall #2
Outfall #1
Outfall #2
Date: 12130/2016 0424 PM
QC Batch Method
EPA 16648
EPA 1664E
EPA 3510
EPA 3510
EPA 200.7
EPA 200.7
EPA 625
€PA 625
EPA 624
EPA 624
SM 2540D
SM 2540D
EPA 420A
EPA 420A
SM 4500-CN-E
SM 4500•CN-E
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huniersville. NC 28078
(704 )8759092
QC Batch Analytical Method
342987
342987
341800
341800
341624
341624
342056
342056
342037
342037
341807
341807
342739
342739
342534
342534
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
E PA 608
EPA 60B
EPA 20D.7
EPA 200 7
EPA 625
EPA 625
Analytical
Batch
342227
342227
342091
342091
342216
342216
Page 30 of 33

I
t
Analytical 15
Document Name:
Condition Upon Receli
Document No,:
F-CAR-CS-033-Revr01
'icument Revised: Sept. 21, 2016
_ Page 1 of.2
Issuing Authority:
Pace Quality Office
Laboratory receiving Sa ples:
Asheville Eden❑ • . Greenwood ❑ Huntersvilie ❑ Raleigh❑ Mechanicsville❑
client Name: Wv# : 92323876
Pra du:
-Courier: ❑Fed Ex ❑UPS ❑USPS fiffClient
❑ Commercial ❑Pace ❑Other: 92323876
Custody Seal Present? ❑Yes] f� O seals Intact? ❑Yes ❑No
Date/Initkals Person Examining Contents: �df •i2 �Y if+
Packing Material: ❑Bubble Wrap ❑Bubble Bags one ❑Other:
Thermometer
yJ IRGun ID: Type of Ice
et [:]Blue []None _—]Samples an ice, cooling process has b gC
Correction Factor: (' Co le Temp Corrected ('C): �; Biological Tissue Frozen? ❑Yes ONO
NIA
Temp should be above freez to 6-C
USDA Regulated Soil ( r /A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Inte�rnat�ally,
F lYes MNo inrtudinv Hawaii aHr.
and Puartn ni7 I IV4-t IYINn
.11
Comments/Discrepancy:
Chain of Custody Present?
dYek
❑No
❑N/A
1.
Samples Arrived within Hold Time?
GfYes
nNo,
❑N/A
2.
Short Hold Time Analysis (02 hr,)?
❑Yes
N
QN/A
3.
Rush Turn Around Time Requested?
❑ye
No
❑N/A
4.
Sufficient Volume?
Y
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
ZE3�,
❑No
❑No
❑N/A
❑N/A
6.
Containers Intact?
Yes
❑No
❑
7.
Samples Field Filtered?
❑Y
❑No
N A
8. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
-Includes Date/fime/10/Analysis Matrix.
Yes
❑No
❑ia/A
9.
Heads ace in VOA Vials (>5-6mm)?
❑yes
N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Oyes
❑Yes
No
❑N/A
❑N/A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Date/Time:
Field Data Required? ❑Yes [:]NO
Project Manager SCURF Review: Z Date:
Project Manager SRF Review: Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers)
Page 31 of 33

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BP4U-125 mL Plastic Unpreserved (N/A) (CI-)
MU-250 mL Plastic Unpreserved (N/A)
BP2U-500 mL Plastic Unpreserved (N/A)
—'
BP1U-1 liter Plastic Unpreserved (N/A)
BP35-250 mL Plastic H2SO4 (pH < 2) (CI-)
BP3N-250 mL plastic HNO3 (pH < 2)
BP3Z-250 mL Plastic ZN Acetate & NaOH (>9)
zz_
ZZZZZZ--7-1"
C-250 mL Plastic NaOH (pH > 12) (Cl-)
WGFU-Wide-mouthed Glass jar Unpreserved
r. l
AGiU-1 liter Amber Unpreserved (N/A) (CI-]
7
AG1H-1 liter Amber HCI (pH < 2)
AG3U-250 mL Amber Unpreserved (N/A) (CI-)
AGiS-1 liter Amber H2504 (pH < 2)
AG3S-250 mLAmber H2SO4 (pH <2)
AG3A(DG3A)-250 mL Amber NH4Cl (N/A)(Ci-)
i ti
DG91­140 mL VOA HO (N/A)
VG9T-40 mL VOA NoZ5203 (N/A)
VG9U-40 mL VOA Unp (N/A)
DG9P-40 mL VOA H3PO4 (N/A)
VOAK (6 vials per kit)-5035 kit (N/A)
V/GK (3 vials per kit)-VPH/Gas kit (N/A)
SPST-125 mL Sterile Plastic (N/A —lab)
SPZT-250 ml.Sterile Plastic (N/A —lab)
ZA7ZZZZZxZZZBP3A-250
mL Plastic (NH2)2SQ4 (9.3-9.7)
Cubitainer
VSGU-20 mL Scintillation vials (N/A)
GN
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S
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CHAIN -OF -CUSTODY I Analytical Request Document. th
The Chain af-Custody is a LEGAL DOCUMENT- All relevant fields must be completed accurately.
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Section A Section B Section C
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Required ChenntJInformatiioon., Required Project Inhxmation: Invoice Information:
CReW To: Attention:
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2070132
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Addn:is; S 3
Copy To:
Company Namo:
REGULATORY AGENCY
Addross:
i- NPDES f- GROUNDWATER j- DRINKING WATER
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Email To:
Purchase Omer Na.:
Paw Ouole
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Fax:
ProjeCi Name: -� A
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Paul Prgw
NLtlVeer.
Site Location
STATE.
Requested Due Date/iAT:
ProjKl Number:
Pate Pfe
Requested'Analysis
Filtored'IYINj
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ADDITIONAL COMMENTS
RELINQUISHED BY I AFFN.JATt0H
BATE
TIME
ACCEPTED BY f AFitLkAT.ON
DATE
TIME
SAMPLE CONDITM5
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SAMPLER NAME AND SIGNATURE
ORIGINAL
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PRINT Name of SAMPLER: CZ.er( 4 41wili28
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DATE Signed
SIGNATURE of SAMPLER: '
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IMM ONYI:
•Impod—i notu: By bkjn-q Ut+ roan you mu arnepmg Rai NET 30 day pAyiino i fauns We agooing tc LOW UW[l s 01 1.5% per ewnth Ia any in—� not P+U within 30 pays. F-ALL-0-020rev.07. 1 SMay-2007

r_
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls_
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Pace Analytical Lab Cert. #40
Comments on sample collection or analysis: See page 4
Date submitted _August 11, 2015
SAMPLE COLLECTION YEAR _2015
SAMPLE PERIOD ® Jan -June ❑ July -Dec
Q or ❑ Monthly'_ (month)
DJS
Fes_ ._ .
-CHARGING TO CLASS ❑ORW []HCiW ❑Trout ❑PNA
AUG 14 2015 _=;:
❑Zero -flow -]Water Supply ❑SA
®Other: Class C, Swannanoa River_
Land PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
. IIl1 A�AW@
Part A: Stormwater Benchmarks and Monitoring Results
❑ No discharge this period?'
.
Date Sample
24-hour rainfall
pH,
Non -Polar O&G/Total
Toxic
Outfali No.
Collected'
amount,
Total Suspended Solids
Standard units
Copper
Lead
Zinc
Total Petroleum
Organics5
(mo/dd/yr)
Inches3
Hydrocarbons
Benchmarks =__>
-
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
i mg/L
1
06/30/15
0.42
5.00 mg/L
7.4
<0.005 mg/L
0.0050
0.005mg/L
<5.0 mg/L
BRL
2
06/30/15
0.42
10.0 mg/L
7.2
<0.005 mg/L
0.0050
0.005mg/L
<5.0 mg/L
BRL
}}
fk
M1
i.,
1;Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
'See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.1.2; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 1 of 4

"ifte yjlfwq hand
9rllvWfeA

Faciiiiies that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
'Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Jason Stone
Name (Print name)
Plant Manager
II_ Title (Print title)
f
w c_ cr�� _ 8/11/2015
)nature)g(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg1V where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Mote: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier x, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No dischorge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 5U
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
+ A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑
REGIONAL OFFICE CONTACT NAME: _ Laura Herbert, P.E.
Mail an oriainal and one coov of this DMR, including all "No Discharge" reports. within 30 dovs of receipt of the lab results for at end of monitorina period
in the case o "No Discharge" reports) to:
tiftDivision of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
re of
8/11/2015
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-24S, last revised 10/25/2012
Page 3 of 4

accAnalytical
mvwpac+fa"Wrn
July 23, 2015
Gerald Runkles
Pentair Valves & Controls
953 Old US Hwy 70
Black Mountain, NC 28711
RE: Project: Outflow 6130
Pace Project No.: 92256776
Dear Gerald Runkles:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on July 01, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted_
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 9 of 26

aceAnalytical
WWWP x="
Project Outflow 6/30
Pace Project No. 92256776
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone] '
Charlotte Certification iDs
9800 Kinsey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NFLAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
UrrginiafVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
MrginiaNi=LAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, inc.. Page 2 of 26

Pace Analytical Services, Inc.
aceMalXkal o 980o Kincey Ave. Suite 100
Huntersville, NC 28078
r►w+�Ps [phone]' 1
SAMPLE ANALYTE COUNT
Project: Outflow 6130
Pace Project No.: 92256776
Lab ID Sample ID
Method
Analysts
Analysts
Reported
Laboratory
92256776001 Outflow #1
EPA 1664B
JMS
1
PASI-C
EPA608
SWB
27
PASI-C
EPA 200.7
JMW
3
PASI-A
EPAfi25
Bpi
58
PASI-C
EPA 624
GAW
34
PAS I-C
SM 2540D
MDW
1
PASI-A
92256776002 Outflow #2
EPA 1664B
JMS
1
PASI-C
EPA608
SWB
27
PASI-C
EPA200.7
JMW
3
PASI-A
EPA625
BPJ
58
PASI-C
EPA624
GAW
34
PASI-C
SM 2540D
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 26

r� -
Pace Analytical Services, Inc.
(�Ia'G)eMaljftal
9800Kincey Ave. Suite 78 Huntersvilie, NC 28D78
wwwpsodebs-mm
[phone] '
SUMMARY OF DETECTION
Project: Outflow 6130
Pace Project No.: 92256776
Lab Sample ID Client Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
92256776002 Outflow #2
SM 2540D Total Suspended Solids 10.0 mg/L 2.5 07/06/15 17:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc.. Page 4 of 26

it ,
aceAnalidical
w�w.peoefatracem
ANALYTICAL RESULTS
Pace Analytical Services, Irtc.
9800 Kincey Ave. Suite too
Hun,.ersville, NC 28078
(704 )8759092
Project: Outflow 6130
Pace Project No.: 92256776
Sample: Outflow 01 Lab ID: 92256776001 Collected: 06130115 19:25 Received: 07/01115 10:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 16648
Oil and Grease
NO
mg&
5.0
1
07/14/15 09:38
608 GCS Pesticides and PCBs
Analyticai Method: EPA608 Preparation Method: EPA 3510
Aldrin
ND
ug/L
0,050
1
07/07/15 18:40 07110/1517:06
309-00-2
alpha-8HC
NO
ug/L
0.050
1
07/0711518:40 07/10/16IT06
319-84-6
beta-BHC
NO
ug/L
0.050
1
0710711518:40 0711011517:06
319-85-7
delta-BHC
NO
ug1L
0.050
1
07/07/15 18:40 07110/1517:06
319416-8
gamma-BHC (Lindane)
ND
ug/L
0.050
1
07/07/15 18:40 07/10/15 17:06
58-89-9
Chlordane (Technical)
NO
ug/L
0.50
1
07/07115 18:40 07/10115 17:06
57-74-9
4,4'-DDD
NO
ug/L
0.050
1
07/0711518:40 07110/1517:06
72-54-8
4,4'-DDE
NO
ug/L
0.050
1
07107/15 18:40 07110/1517:06
72-55-9
4,4'-DDT
NO
ug1L
0.050
1
07107/15 18:40 07/1011517:06
50-29-3
Dieldrin
NO
ug/L
0.050
1
07107/15 18:40 07/10/15 17:06
60-57-1
Endosulfan I
NO
ug/L
0.050
1
07/07/15 18:40 07/10/15 17:06
959-98-8
Endosulfan II
NO
ug/L
0.050
1
07/07/15 18:40 07/10/15 17:06
33213-05-9
Endosulfan sulfate
NO
ug/L
0.050
1
07/07/15 18:40 07/10/15 17:06
1031-07-8
Endrin
ND
ug/L
0.050
1
07/07/15 18:40 0711011517:06
72-20-8
Endrin aldehyde
ND
ug/L
0.050
1
07/07/15 18:40 07/10/15 17:06
7421-93-4
Heptachlor
NO
ug/L
0.050
1
07107/1518A0 07/10/1517:06
76-44-8
Heptachlor epoxide
NO
ug/L
0.050
1
07/07/15 18:40 07/10/15 17:06
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
1
07/07/15 18:40 07/10/15 17:06
12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
1
07/0711518:40 07/10/15 17:06
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
1
07/07/15 18:40 07/10/15 17:06
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0-50
1
07107/15 18:40 07/1011517:06
53469-21-9
PCB-1248 (Aroclor 1248)
ND
uglL
0.50
1
07/07115 18:40 01110/1517:06
12672-29-6
PCB-1254 (Arodor 1254)
ND
uglL
0.50
1
07/07/15 18:40 07/10/15 17:06
11097-69-1
PCB-1260 (Arodor 1260)
ND
ug/L
0.50
1
07107/15 18740 07/10/15 17:06
11096-82-5
Toxaphene
ND
ug/L
0.50
1
07/0711518:40 0711011517:06
800f-35-2
Surrogates
Tetrachloro-m-xylene (S)
41
20-110
1
07/07/15 18:40 07110/15 17:06
877-09-8
Decachlorobiphenyl (S)
49
%
20-138
1
07/07/15 18A0 07/10/15 17:06
2051-24-3
200.7 MET ICP
Analytical Method: EPA200.7 Preparation Method: EPA200.7
Copper
NO
ug/L
5.0
1
07102/1517:30 07/06/1518:31
7440-50-8
Lead
ND
ug/L
5.0
1
07102/1517:30 07/06/1518:31
7439-92-1
Zinc
ND
ug/L
10.0
1
07102/1517:30 0710611518:31
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
83-32-9
Acenaphthylene
NO
uglL
5.0
1
07/07/15 10:15 07/09/15 09:54
208-96-8
Anthracene
NO
ug1L
5-0
1
07/07/15 10:15 07/09/15 09:54
120-12-7
Benzo(a)anthracene
ND
ug1L
5.0
1
07107/15 10:15 07/09/15 09:54
56-55-3
Benzo(a)pyrene
NO
uglL
5.0
1
07/07/15 10:15 07/09115 09.54
50-32-8
Benzo(b)fluorantherte
ND
ug/L
5.0
1
07/07115 10:15 07/09/15 09:54
205-99-2
Benzo(g,h,i)perylene
NO
ug1L
5-0
1
07/07/15 10:15 07109/15 09:54
191-24-2
Benzo(k)fluoranthene
NO
ug/L
5.0
1
07/07/15 10:15 07109/15 09:54
207-08-9
REPORT OF LABORATORY ANALYSIS
This report shall riot be reproduced. except in full,
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc- Page 5 of 26

aceAnalWical
wwwpacab tom
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Outflow 6130
Pace Project No.: 92256776
Sample: Outflow tf t Lab ID: 92256776001 Collected: 06/30/15 19:25 Received: 07/01/15 10:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
625 MSSV Analytical Method: EPA625 Preparation Method: EPA625
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
07/07/15 10:15 07/09115 09:54
59-50-7
bis(2-Chloroethoxy)methane
NO
ug/L
10.0
1
07/07/15 10:15 07/09/15 09:54
111-91-1
bis(2-Chloroethyl) ether
NO
ug/L
.5.0
1
07/07/15 10:15 07/09/15 09:54
111-44A
bis(2-Chloroisopropyl) ether
ND
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
108-60-1
2-Chloronaphthalene
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
91-58-7
2-Chlorophenol
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
95-57-8
4-Chlorophenyiphenyl ether
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
7005-72-3
Chrysene
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
218-01-9
Dibenz(a,h)anthracene
NO
ug/L
5.0
1
07107/15 10:15 07/09/15 09:54
53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
25.0
1
07107/1510:15 07/09115 09:54
91-94-1
2,4-Dichlorophenol
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
120-83-2
Diethylphthalate
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
84-66-2
2,4-Dimethylphenol
NO
ug/L
10.0
1
07/07/15 10:15 07/09115 09:54
105-67-9
Dimethylphthalate
NO
ug/L
5.0
1
07/07/15 10:15 07109/1509:54
131-11-3
Di-n-butylphthalate
ND
ug1L
5.0
1
07/07/15 10:15 07/09/15 09:54
84-74-2
4,6-Dinitro-2-methylphenol
NO
ug1L
20.0
1
07/07/15 10:15 07/09/15 09:54
534-52-1
2,4-Dinitrophenol
NO
ug/L
50.0
1
07/07/15 10:15 07/09115 09:54
51-28-5
2,4-Dinitrotoluene
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
121-14-2
2,6-Dinitrotoluene
NO
ug/L
5.0
1
07/07/16 10A 5 07/09/15 09:54
606-20-2
Di-n-octylphthalate
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
117-84-0
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
0710711510:15 07/09/15 09:54
117-81-7
Fluoranthene
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
206-44-0
Fluorene
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
86-73-7
Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
07/07/15 10:15 0710911509:54
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
119-74-1
Hexachlorocyclopentadiene
ND
uglL
10.0
1
07/07/15 10:15 07/09/15 09:54
77-47-4
Hexachloroethane
NO
uglL
5.0
1
07/07/15 10:15 07/09/15 09:54
67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug/L
5.0
1
07/07/15 10:15 07109/1509:54
193-39.5
Isophorone
NO
ug/L
10.0
1
07/0711510A5 07109/1509:54
78-59-1
Naphthalene
NO
uglL
5.0
1
07/07/15 10:15 07/09/15 09:54
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
07/0711510A5 07/09/15 09:54
98-95-3
2-Nitrophenoi
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
88-75-5
4-Nitrophenol
NO
ug/L
50.0
1
07/07/15 10:15 07/09/15 09:54
100-02-7
N-Nitrosodimethylamine
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
62-75-9
N-Nitroso-di-n-propytamine
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
07/07/15 10:15 07/09/15 09:54
86-30-6
Pentachlorophenol
NO
ug1L
10.0
1
07/07/15 10:15 07/09/15 09:54
87-86-5
Phenanthrene
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
85-01-8
Phenol
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
108-95-2
Pyrene
NO
ug/L
5.0
1
07/07/15 10:15 07/09/15 09:54
129-00-0
1,2,4-Trichlorobenzene
ND
uglL
5.0
1
07/07/15 10:15 07/09/15 09:54
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
07/07/15 10:15 07/09/15 09:54
88-06-2
Surrogates
Nitrobenzene-d5 (S)
72
%
10-120
1
07/07/15 1015 07/09/15 09:54
4165-60-0
2-Fluorobiphenyl(S)
77
%
15.120
1
07/07/15 10:15 07109/1509:54
321-60-8
REPORT OF LABORATORY ANALYSIS
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aceAnalj cal
wwwprscelabsoom
Project: Outflow 6130
Pace Project No.: 92256776
Sample: Outflow #1
Pace Analytical Services, Inc.
9800 Kincey Aye. Suite 100
Huntersyille, NC 280790
(704 )875-W92
ANALYTICAL RESULTS
Lab ID: 92256776001 Collected: 06/30/15 19:25 Received' 07101/15 10:30 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA625 Preparation Method: EPA625
Surrogates
Terphenyl-d14 (S)
89
%
11-131 1
07/07/15 10:15
07/09/15 09:54
1718-51-0
Phenol-d6 (S)
34
%
10-120 1
07/07/15 10:15
07/09/15 09:54
13127-88-3
2-Fluorophenol (S)
46
%
10-120 1
07/07/15 10:15
07/09/15 09:54
367-12-4
2,4,6-Tribromophenol (S)
84
%
10-137 1
07/07/15 10:15
0710/15 09:54
118-79-6
624 Volatile Organics Analytical Method: EPA 624
Benzene
NO
ug/L
2.0
1
07/08/15 08:27
71-43-2
Bromodichloromethane
NO
uglL
2.0
1
07/08/15 08:27
75-27-4
Bromoform
NO
ugll-
2.0
1
07/08115 08:27
75-25-2
Bromomethane
NO
ug/L
2.0
1
07/08/15 08:27
74-83-9
Carbon tetrachloride
NO
uglL
2.0
1
07/08/15 08:27
56-23-5
Chlorobenzene
NO
ug/L
2.0
1
07/08/15 08:27
108-90-7
Chloroethane
NO
ug/L
2.0
1
07/08/15 08:27
75-00-3
Chloroform
NO
ug/L
2.0
1
07/08/15 08:27
67-66-3
Chloromethane
NO
ug/L
2.0
1
07/08/15 08:27
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
07/08/15 08:27
124-48-1
1,2-Dichlorobenzene
NO
ug/L
2.0
1
07/08/15 08:27
95-50-1
1,3-Dichlorobenzene
NO
ug/L
2.0
1
07108/15 08:27
541-73-1
1,4-Dichlorobenzene
NO
ug/L
2.0
1
07108/15 08:27
10646-7
1,1-Dichloroethane
NO
ug/L
2.0
1
07/08/15 08:27
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
07/08/15 08:27
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
1
07/0811508:27
75-35-4
cis- 1,2-Dichloroethene
NO
ug/L
2.0
1
07/08/15 08:27
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
07/08/15 08:27
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1
07/08/15 08:27
78-87-5
cis-1,3-Dichloropropene
NO
ug/L
2.0
1
07/08/15 08:27
10061-01.5
trans-1,3-Dichloropropene
NO
ug/L
2.0
1
07/08/15 08:27
10061-02-6
Ethylbenzene
NO
ug/L
2.0
1
07/08/15 08:27
100-41-4
Methylene Chloride
NO
ug/L
2.0
1
07/08/15 08:27
75-09-2
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
0710811508:27
79-34-5
Tetrachloroethene
NO
ug/L
2.0
1
07/08/15 08:27
127-16-4
Toluene
NO
ug/L
2.0
1
07/08/15 08:27
108-88-3
1,1,1-Trichforoethane
ND
ug/L
2.0
1
07/08/15 08:27
71-55-6
1,1,2-Trichloroethane
NO
ug/L
2.0
1
07108/1508:27
79-00-5
Trichloroethene
ND
ug/L
2.0
1
07/08/15 08:27
79-01-6
Trichlorofluoromethane
ND
ug/L
2.0
1
07/08/15 08:27
75-69-4
Vinyl chloride
NO
ug/L
2.0
1
07/08/15 08:27
75-01-4
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
07/08/15 08:27
46"0-4
Toluene-d8 (S)
98
%
70-130
1
07/08/15 08:27
2037-26-5
1,2-Dichloroethane-d4 (S)
105
%
70-130
1
07/08/15 08:27
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND
mg/L
2.5
1
07/06/15 17:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 26

Pace Analytical Services, Inc.
acemalytical • 9800 KineyAve. Suite 100
Huntersvi[le, NC 28070
wwgr7etwaftcom [phone] ,
ANALYTICAL RESULTS
Project: Outflow 6130
Pace Project No.: 92256776
Sample: Outflow #2 Lab ID: 92256776002 Collected: 06/30/15 19:30 Received: 07101115 10:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO
mg/L
5.0
1
07/14/15 09:39
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
ND
uglL
0.050
1
0710711518:40 07/10/15 17:24
309-00-2
a1pha-8HC
NO
ug/L
0.050
1
0710711518:40 0711011517:24
319-84-6
beta-BHC
NO
ug/L
D.050
1
07107/1518:40 07110/1517:24
319.85-7
delta-BHC
NO
ug/L
0.050
1
07107/1518:40 07/10115 17:24
319-86-8
gamma-BHC (Lindane)
NO
ug/L
0-050
1
07/07/15 18:40 07110/15 17:24
58-89-9
Chlordane (Technical)
ND
ug/L
0.50
1
07/07/15 18:40 07/10/15 17:24
57-74-9
4,4'-DDD
NO
u91L
0,050
1
D7/0711518:40 07110/1517:24
72-54-8
4,4'-DDE
NO
ug1L
0.050
1
07/0711518:40 07110/1517:24
72-55-9
4,4'-DDT
NO
uglL
0.050
1
07107/1518:40 07/10/15 17:24
50-29-3
Dieldrin
ND
ug/L
0,050
1
07107/1518:40 07/10115 17:24
60-57-1
Endosulfan I
NO
ug/L
0.050
1
07/07/15 18:40 07/10/15 17:24
959-98-8
Endosultan it
NO
ug/L
0.050
1
07/07/15 18:40 07/10/15 17:24
33213-65-9
Endosulfan sulfate
NO
ug/L
0.050
1
07/07/15 18A0 07110115 17:24
1031-07-8
Endrin
NO
ug/L
0.050
1
07107/1518:40 0711011517:24
72-20-8
Endrin aldehyde
NO
ug/L
0.050
1
07/07/15 18:40 07/10/15 17:24
7421-93A
Heptachlor
NO
ug/L
0.050
1
07/07/15 18:40 07/10115 17:24
76-44-8
Heptachlor epoxide
ND
ug/L
0,050
1
07/07/15 18:40 07/10115 17:24
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
1
07/07/15 18:40 07/10/15 1714
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
1
07/07/15 18A0 07/10/15 17:24
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
1
07/07/15 18:40 07/10/15 17:24
11141-16-5
PCB-1242 (Aroclor 1242)
NO
ug/L
0,50
1
07107/15 18:40 0711011517;24
53469-21-9
PCB-1248 (Aroclor 1248)
NO
ug1L
0.50
1
07107/15 18:40 07/10/15 17:24
12672-29-6
PCB-1254 (Aroclor 1254)
NO
ug/L
0.50
1
07/07115 18:40 07/10/15 17:24
11097-69-1
PC8-1260 (Aroclor 1260)
ND
ug/L
0.50
1
07/07/15 18:40 07/10115 17:24
11096-82-5
Toxaphene
NO
ug/L
0-50
1
07/07/15 18:40 07/10115 17:24
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
52
%
20-110
1
07/07/15 18:40 07/10/15 17:24
877-M8
Decachlorobiphenyl (8)
69
%
20-138
1
07/07/15 18:40 07/10115 17:24
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200,7 Preparation Method: EPA 200.7
Copper
NO
ug/L
5.0
1
0710211517:30 07106/1518:34
7440-50-8
Lead
NO
ug/L
5.0
1
07/0211517:30 07/0611518:34
7439-92-1
Zinc
NO
ug/L
10.0
1
07/0211517:30 07/06/1518:34
7440-6"
625 MSSV
Analytical Method: EPA625 Preparation Method: EPA625
Acenaphthene
NO
ug/L
5.0
1
0710711510:15 D7109/1510:22
83-32-9
Acenaphthylene
NO
ug/L
5.0
1
07107/1510:15 07109/1510:22
208-96-8
Anthracene
NO
ug1L
5.0
1
07/0711510:15 07/0911510:22
120-12-7
Senzo(a)anthracene
ND
uglL
5.0
1
07/0711510:15 07109/1510:22
56-55-3
Benzo(a)pyrene
NO
ug1L
5.0
1
0710711510:15 07/09/1510:22
50-32-8
Benzo(b)Ruoranthene
NO
uglL
5.0
1
07/0711510:15 07/0911510:22
205-99-2
Benzo(g,h,i)perylene
NO
u911-
5.0
1
07/07/1510:15 07109/1510:22
191-24-2
Benzo(k)fluoranthene
NO
ug/L
5-0
1
07/07/1510:15 0710911510:22
207-08-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 26

aceAnapical
arskft.wnr
ANALYTICAL RESULTS
Project: Outflow 6130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hurtersville, NC 28076t
[phone]
Pace Project No,: 92256776
Sample: Outflow #2 Lab ID: 92256776002 Collected: 06130/15 19:30 Received: 07/01/15 10:30 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 MSSV
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
bis(2-Chloroethoxy)metha ne
bis(2-Chloroethyl) ether
W2-Chtoroisopropyt) ether
2-Chioronaphftlene
2-CMoropheW
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h )anthracene
IT -Dish lorobenz€dine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1, 3-butadiene
Hexachlorobenzene
Hexachtorocyclopentad iene
Hexachloroethane
I ndeno(1, 2, 3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodim ethyla mine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2, 4-Trichlorobenzene
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-45 (S)
2-Fluorobiphenyl (S)
Analytical Method: EPA 625 Preparation Method: EPA 625
NO
u9/1-
5.0
1
07/07/1510:15 07/0911510:22
NO
ug/L
5.0
1
07/0711510:15 07/09/1510:22
ND
ug/L
5.0
1
07107/1510A5 07/09/1510:22
ND
ug/L
10.0
1
0710711510:15 07/0911510:22
ND
ug/L
5.0
1
07/0711510:15 07109/1510:22
ND
ug/L .
5.0
1
07/07/15 10:15 07/09/15 10:22
ND
ug/L
5.0
1
0710711510:15 07109/1510:22
ND
ug/L
5.0
1
0710711510:15 07109/1510:22
ND
ug/L
5.0
1
07107/1510:15 0710911510:22
ND
ug/L
5.0
1
071DWIS 10:15 07109/15 10:22
ND
ug/L
5.0
11
07/07/1510:15 07/09/1510;22
NO
ug/L'
25.0
1
07/07/1510:15 07/09/1510:22
ND
ug/L
5.0
1
07/07/1510:15 07/09/1510:22
NO
ug/L
5.0
1
0710711510:15 0710911510:22
NO
ug1L
10.0
1
07/0711510:15 07109/1510:22
ND
ug/L
5.0
1
0710711510:15 0710911510:22
NO
ug/L
5.0
1
07/0711510:15 07109/1510:22
NO
ug/L
20.0
1
07107/1510:15 0710911510:22
ND
ug/L
50.0
1
0710711510:15 0710911510:22
NO
ug/L
5.0
1
07107/1510:15 07/0911510:22
ND
ug/L
5.0
1
07107/1510:15 07/09/1510:22
NO
ug/L
5.0
1
0710711510:15 0710911510:22
NO
ug&
5.0
1
071071151015 07/0911510:22
ND
ug/L
5.0
1
0710711510:15 07/0911510:22
ND
ug/L
5.0
1
0710711510:15 07109/1510:22
ND
ug/L
5-0
1
0710711510.15 07109/1510:22
NO
uglL
5.0
1
07107/1510:15 07109/1510:22
ND
ug/L
10.0
1
07107/1510:15 07109/1510:22
ND
ug/L
5.0
1
0710711510:15 0710911510:22
NO
ug/L
5.0
1
07107/1510:15 0710911510:22
NO
ug/L
10.0
1
0710711510:15 0710911510:22
ND
ug)L
5.0
1
07/07/1510:15 07109/1510:22
NO
uglL
5.0
1
0710711510:15 07/09/1510,22
NO
ugll-
5.0
1
07/07/1510:15 07/09/1510:22
NO
ug/L
50.0
1
07/07/1510:15 07109/1510:22
NO
ug/L
5.0
1
07/07/1510:15 07109/1510:22
ND
ug/L
5.0
1
0710711510:15 07109/1510:22
NO
ug/L
10.0
1
0710711510:15 07/09/1510:22
NO
ug/L
10.0
1
0710711510:15 07109/1510:22
NO
ug/L
5.0
1
07/0711510:15 07/09/1510:22
NO
ug/L
5.0
1
07/0711510:15 07109/1510:22
NO
ug/L
5.0
1
07/0711510:15 0710911510:22
ND
ug/L
5.0
1
0710711510-15 07109/1510:22
NO
ug/L
10.0
1
07107/1510:15 0710911510:22
101-55-3
85-68-7
59-50-7
111-91-1
111-44-4
108-60-1
91-5&7
95-57-8
7005-72-3
218-01-9
53-70-3
91-94-1
12M3-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
8&75-5
100-02-7
62-75-9
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
120-82-1
W06-2
68 % 10-120 1 07/07/1510:15 07/0911510:22 4165-60-0
71 % 15-120 1 0710711510:15 07109/1510:22 321-6"
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2016 01:05 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 26

I
Pace Analytical Services, Inc.
�^� 9800 Kincey Ave. Suite 100
V �f r fY[ UR Huntersville, NC 2807d ,
wWW.P CDM [phone]
ANALYTICAL RESULTS
Project: Outflow 6/30
Pace Project No.: 92256776
Sample: Outflow #2 lab ID: 92256776002 Collected: 06/30/15 19:30 Received: 07/01/15 10:30 Matrix: Water
Parameters
625 MSSV
Surrogates
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol (S)
624 Volatile Organics
Benzene
Bromodichloromethane
Bromoform
Bromornethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Surrogates
4-BromoRuorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
2540D Total Suspended Solids
Total Suspended Solids
Date: 07/23/2015 01:05 PM
Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 625 Preparation Method: EPA 625
81
%
32
%
43
%
85
%
Analytical Method: EPA 624
NO
ug/L
NO
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
NO
ug1L
ND
ug1L
NO
uglL
NO
ug/L
NO
uglL
NO
uglL
NO
ug/L
NO
ug/L
NO
uglL
NO
ug/L
NO
ug1L
NO
ug/L
NO
ug/L
NO
ug1L
NO
ug/L
NO
uglL
NO
ug/L
NO
ug/L
NO
uglL
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug1L
NO
ug1L
NO
ug1L
ND
ug/L
108 %
100 %
100 %
Analytical Method: SM 2540D
10.0 mg1L
11-131
1
07107/1510:15
0710911510:22
1718-51-0
1D-120
1
07/07/1510:15
0710911510:22
13127-88-3
10-120
1
07107/1510:15
07109/1510:22
367-12-4
10-137
1
07/0711510A5
07/0911510:22
118-79-6
2.0
1
07/08/15 09:01
71-43-2
2.0
1
07/08/15 09:01
75-27-4
2.0
1
07/08/15 09:01
75-25-2
2.0
1
07/08/15 09:01
74-83-9
2.0
1
07/08/15 09:01
56-23-5
2.0
1
07108/15 09:01
108-90-7
2.0
1
07/08/15 09:01
75-00-3
2.0
1
07/08/15 09:01
67-66-3
2.0
1
07/08115 09:01
74-87-3
2.0
1
07/08/15 09:01
12448-1
2.0
1
07/08/15 09:01
95-50-1
2.0
1
07/08/15 09:01
541-73-1
2.0
1
07108/15 09:01
106-46-7
2.0
1
07/08/15 09:01
75-34-3
2.0
1
07/08/15 09:01
107-06-2
2.0
1
07/08/15 09:01
75-35-4
2.0
1
07/08/15 09:01
156-59-2
2.0
1
07/08/15 09:01
156-60-5
2.0
1
07/08/15 09:01
78-87-5
2.0
1
07/08/15 09:01
10061-01-5
2.0
1
07/08/15 09:01
10061-02-6
2.0
1
07/08115 09:01
100-41-4
2.0
1
07/08/15 09:01
75-09-2
2.0
1
07/08/15 09:01
79-34-5
2.0
1
07/08/15 09:01
127-18-4
2.0
1
07/08/15 09:01
108-88-3
2.0
1
07/08/15 09:01
71-55-6
2.0
1
07/08/15 09:01
79-00-5
2.0
1
07/08/15 09:01
79-01-6
2.0
1
07/08/15 09:01
75-69-4
2.0
1
07/08/15 09:01
75-014
70-130 1
70-130 1
70-130 1
2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consenl of Pace Analytical Services, Inc..
07/08/16 09:01 460-00-4
07/08/15 09:01 2037-26-5
07/08115 09:01 17060-07-0
07106/15 17:28
Page 10 of 26

aceAnalytical
W&W4eaitt &COM
QUALITY CONTROL DATA
Project: Outflow 6130
Pace Project No.: 92256776
QC Batch: GCSV121938 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92256776001, 92256776002
METHOD BLANK: 1508469 Matrix: Water
Associated Lab Samples: 92256776001, 92256776002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mgJL NO 5.0 07/14/15 09:29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 2807fi1 ,
[phone]
LABORATORY CONTROL SAMPLE_ 1501 470
Spike LCS LCS % Rec
Parameter Units Cont. Result % Rec Limits Qualifiers
Oil and Grease mg)L 40 34.3 86 78-114
MATRIX SPIKE SAMPLE: 1508471
92256845005 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg1L ND 40 40.0 100 78-114
Results presented on this page are In the units Indicated by the 'Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 26

aceAnapical
rvww.paGsWMaxn
Project: Outflow 6/30
Pace Project No.: 92256776
QC Batch: MPRP118906
QC Batch Method: EPA 200.7
Associated Lab Samples: 92256776001, 92256776002
METHOD BLANK: 1501009
Associated Lab Samples: 92256776001, 92256776002
Parameter
Units
Copper
ug/L
Lead
ug/L
Zinc
ug/L
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Sunk Reporting
Result Limit Analyzed
ND 5.0 07/0611514:30
ND 5.0 07/06/1514:30
NO 10.0 07/06/1514:30
Qualifiers
Pace Analytical Services, Inc.
9800 Kinsey Ave_ Su" 100
Huntersviile. NC 2BD7*
[phone]
LABORATORY CONTROL SAMPLE:
1501010
Spike
LCS LCS % Rec
Parameter
Units
Cone_
Result % Rec Limits Qualifiers
Copper
ug/L
500
471 94 85-115
Lead
ug/L
500
456 91 W115
Zinc
ug/L
500
449 90 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1501011
1501012
MS
MSD
92256814001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Conc.
Result
Result
% Rec
% Rec
Limits
RPO Qual
Capper ug/L
10.9
500
500
519
474
102
93
70-130
9
Lead ug/L
NO
500
500
491
451
97
89
70-130
8
Zinc ug/L
204
500
500
684
645
96
88
70-130
6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1501013
1501014
MS
MSD
92256770013
Spike
Spike
MS
DASD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPO Qual
Copper ug/L
ND
500
500
537
469
107
93
70-130
14
Lead ug/L
NO
500
500
505
441
101
88
70-130
14
Zinc ug/L
50.7
500
500
563
497
102
89
70-130
12
Resutts presented on this page ate in the ul t indicated by the "Unhs" column eximpi v*mv an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in furl,
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 26

5
acoAnalytical
'
www.paaelabsoant
QUALITY CONTROL DATA
Project: Outflow 6/30
Pace Project No.: 92256776
QC Batch: MSV132470 Analysis Method: EPA 624
OC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92256776001, 92256776002
METHOD BLANK: 1503660
Associated Lab Samples: 92256776001, 92256776002
Parameter units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1, 1. 1 -Trichloroethane
ug/L
ND
2.0
07/07/15 21:42
1,1,2,2-Tetrachloraethane
ug/L
ND
2.0
07/07/15 21:42
1,1,2-Trichloroethane
ug/L
ND
2.0
07/07/15 21:42
1,1-Dichloroethane
ug/L
ND
2.0
07/0711521A2
1,1-Dichloroethene
ug/L
ND
2.0
07/07/15 21:42
1,2-Dichlorobenzene
ug/L
ND
2.0
07/07/15 21:42
1,2-Dichloroethane
ug/L
ND
2.0
07107/15 21:42
1,2-Dichloropropane
ug/L
ND
2.0
0710711521:42
1,3-Dichlorobenzene
ug/L
ND
2.0
07107/1521:42
1,4-Dichlorobenzene
ug/L
ND
2.0
07/07/15 21:42
Benzene
ug/L ,
ND
2.0
07/07/15 21:42
Bromodichloromethane
ug/L
ND
2.0
07/07/15 21:42
Bromoform
ug/L
ND
2.0
07/07/15 21:42
Bromomethane
ug/L
ND
2.0
07/07/15 21:42
Carbon tetrachloride
ug/L
ND
2.0
07/07/15 21:42
Chlorobenzene
ug/L
ND
2.0
07/07/15 21:42
Chloroethane
UgIL
ND
2.0
07/07/15 21:42
Chloroform
ug/L
ND
2.0
07/07/15 21:42
Chloromethane
ug/L
ND
2.0
07/07/15 21:42
cis-1,2-Dichloroethene
ug/L
ND
2.0
07/07/15 21:42
cis- 1,3-Dichloropropene
ug/L
ND
2.0
07/07/15 21:42
Dibromochloromethane
ug1L
ND
2.0
07/07/15 21:42
Ethylbenzene
ug/L
ND
2.0
07/07/15 21:42
Methylene Chloride
ug/L
ND
2.0
07/07/15 21:42
Tetrachloroethene
ug/L
ND
2.0
07/07/15 21:42
Toluene
ug/L
ND
2.0
07/07115 21:42
trans-1,2-Dichloroethene
ug1L
ND
2.0
07/07/15 21:42
trans-1,3-Dichloropfopene
ug/L
ND
2.0
07/07/15 21:42
Tdchloroethene
ug/L
ND
2.0
07/07/15 21:42
Trichlorofluoromethane
ug/L
ND
2,0
07/07/15 21:42
Vinyl chloride
ug/L
ND
2.0
07/07/15 21:42
1,2-Dichloroethane-d4 (S)
%
96
70-130
07/07/15 21:42
4-Bromofluorobenzene (S)
%
99
70-130
07/07/15 21 A2
Toluene-d8 (S)
%
99
70-130
07/07/15 21:42
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HuntersAle, NC 28076
(704)8759092 y'
LABORATORY CONTROL SAMPLE: 1503661
Spike LC5 LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 50 54.5 109 52-162
1,1,2,2-Tetrachloroethane ug/L 50 47.9 96 46-157
Results presented on this page are In the units Indicated by the -Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 26

541ceAnalj6cal
(�t►ww.peodwmc m
QUALITY CONTROL DATA
Project: Outflow 6/30
Pace Project No.: 92256776
LABORATORY CONTROL SAMPLE: 1503661
Parameter
Units
Spike
Conc.
LCS
Result
1,1,2-Trichloroelhane T
uglL
50
52.3
1,1-Dichioroethane
ug/L
50
47.3
1,1-Dichloroethene
ug/L
50
51.4
1,2-Dichlorobenzene
ug/L
50
51.6
1,2-Dichloroethane
ug/L
50
49.2
1,2-Dichloropropane
ug/L
50
50.4
1,3-Dichlorobenzene
ug/L
50
50.5
1,4-Dichlorobenzene
uglL
50
47.5
Benzene
ug1L
50
50.1
Bromodichloromethane
ug/L
50
55-2
Bromoh)rm
ug/L
50
49.1
Bromomethane
uglL
50
50.3
Carbon tetrachloride
ug/L
50
54.8
Chlorobenzene
ug/L
50
47.6
Chloroethane
ug/L
50
41.4
Chloroform
ug/L
50
51.3
Chloromethane
ug/L
50
43.1
cis-1,2-Dichloroethene
uglL
50
49.9
cis-1,3-Dichloropropene
ug/L
50
58.6
Dibromochloromethane
ug/L
50
49.8
Ethylbenzene
ug/L
50
48.3
Methylene Chloride
ug/L
50
53.8
Tetrachloroethene
ug/L
50
47.3
Toluene
ug/L
50
49.3
trans-1,2-Dichloroethene
ug/L
50
47.5
trans-1,3-Dichloropropene
ug/L
50
50.1
Trichiomethene
ug/L
50
47.9
Trichlorafluoromethane
ug/L
50
46.7
Vinyl chloride
ug/L
50
45.3
1,2-Dichioroethane-d4 (S)
%
4-Bromotluorobanzene (S)
%
Toluene-d8 (S)
%
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 2807io ,
[phone]
LCS % Rec
% Rec Limits Qualifiers
105 52-150
95 59-155
103 1-234
103 18-190
98 49-155
101 1-210
101 59-156
95 18-190
100 37-151
110 35-155
98 45-169
101 1-242
110 70-140
95 37-160
83 14-230
103 51-138
86 1-273
100 68-146
117 1-227
100 53-149
97 37-162
108 1-221
95 64-148
99 47-150
95 54-156
100 17-183
96 71-157
93 17-181
91 1-251
97 70-130
98 70-130
101 70-130
Results presented on this page are In the units Indicated by the 'Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 26

(�5ace
A talk{ •
xrw.yeraleba.com
QUALITY CONTROL DATA
Project: Outflow 6130
Pace Project No.: 92256776
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
�
Hunlersville, NC 280-h
[phone]
OC Batch; OEXT136240
Analysis Method:
EPA 608
QC Batch Method: EPA 3510
Analysis Description: 608 GCS Pest PCB
Associated Lab Samples: 92256776001, 92256776002
METHOD BLANK: 1503602
Matrix: Water
Associated Lab Samples: 92256776001, 92256776002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
4,4'-DDD
ug/L
NO
0.050
07110115 18:01
4,4'-DDE
ug/L
NO
0.050
07110115 18:01
.
4,4'-DDT
ug/L
NO
0.050
07/10/15 18:01
Aldrin
ug1L
NO
0.050
07/10/15 18:01
alpha-BHC
ug1L
ND
0.050
07/10/15 18:01
beta-BHC
uglL
NO
0.050
07/10/15 18:01
Chlordane (Technical)
uglL
NO
0.50
07110/15 18:01
delta-BHC
ug/L
NO
0.050
07/1011518:01
Dieldrin
ug1L
ND
0.050
07/1011518:01
Endosulfan I
ug/L
NO
0.050
07/10/15 18:01
Endosulfan II
ug/L
NO
0.050
07/10/15 18:01
Endosulfan sulfate
ug/L
NO
0.050
07/10/15 18:01
Endrin
ug/L
NO
0.050
07110115 18:01
Endrin aldehyde
ug1L
NO
0.050
07/10/15 18:01
gamma-BHC (Lindane)
ug/L
NO
0.050
07/10/15 18:01
Heptachlor
ug1L
NO
0.050
07/1011518:01
Heptachlor epoxide
ug/L
NO
0.050
07/10/15 18:01
PCB-1016 (Aroclor 1016)
ug/L
NO
0.50
07110115 18:01
PCB-1221 (Aroclor 1221)
uglL
NO
0.50
07/10/15 18:01
PCB-1232 (Aroclor 1232)
ug/L
NO
0.50
07/10/15 18:01
PCB-1242 (Aroclor 1242)
ug/L
NO
0.50
07/10/15 18:01
PCB-1248 (Aroclor 1248)
ug/L
NO
0.50
07/10/15 18:01
PCB-1254 (Aroclor 1254)
ug/L
NO
0.50
07/10/15 18:01
PCB-1260 (Aroclor 1260)
ug/i_
NO
0,50
07/10/15 18:01
Toxaphene
ug1L
NO
0.50
07/10/15 18:01
Decachlorobiphenyl (S)
%
75
20-138
07/10/15 18:01
Tetrachloro-m-xylene (S)
%
50
20-110
07110115 18:01
LABORATORY CONTROL SAMPLE & LCSD:
1503603
1503604
Spike
LCS
LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD RPD
4,4'-DDD
ug1L
.25
0.22
0.23
87 92
31-141 5 30
4,4'-DDE
ug1L
25
0.21
0.21
83 85
30-145 3 30
4,4'-DDT
ug/L
.25
0.22
0.23
90 94
25-160 4 30
Aldrin
ug1L
.25
0.19
0.20
76 79
42-122 5 30
alpha-BHC
uglL
.25
0.20
0.23
80 92
37-134 13 30
beta-BHC
ugIL
.25
0.22
0.24
91 97
17-147 7 30
delta-BHC
ug/L
.25
0.23
0.25
94 102
19-140 8 30
Dieldrin
ug/L
25
0,22
0.24
90 97
36-146 7 30
Endosulfan I
ug/L
25
0.23
0.24
91 96
45-153 5 30
Results preaented on this page are
in the unto lodlcated by the'unit - column except whore an alternate unit is presented lathe right of the rasult.
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced. except in full,
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc- Page 15 of 26

ceAnaocal
r►ttw.psra�bs.tzrrt
QUALITY CONTROL DATA
Project: Outflow 6/30
Pace Project No_: 92256776
i
Pace Analytical Services, Inc.
g800 Kincey Ave. Sulte 100
ifuntersvine, NC 2801S
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
1503603
1503604
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc,
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Endosulfan II
ug1L
.25
0.23
0.24
92
98
1-202
7
30 R1
Endosulfan sulfate
ug/L
.25
0.23
0.24
91
98
26-144
7
30 R1
Fndrin
ug/L
.25
0.23
0.25
95
102
30-147
7
30
Endrin aldehyde
ug1L
.25
0.18
0.20
71
80
W150
11
30
gamma-BHC (Lindane)
ug/L
.25
0.21
0.24
87
95
32-127
9
30
Heptachlor
WL
.25
0.23
0.22
92
91
34-111
1
30
Heptachlor epoxide
ug/L
.25
0.22
0.24
89
95
41-126
7
30
Decachlorobiphenyl (S)
%
84
89
20-138
Tetrachloro-m-xylene (S)
%
76
80
20-110
Result$ presented an this page are In fire units indicated by the -Units' cdurnn except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2015 01:05 PM without the written consent of Parse Analytical Services, Inc..
Page 16 of 26

IceAnai�yt�cal
wrwpaoat &MM
Project: Outflow 6/30
Pace Project No.: 92256776
QC Balch: OEXT/36226
OC Batch Method: EPA625
Associated Lab Samples: 92256776001, 92256776002
QUALITY CONTROL DATA
Analysis Method: EPA 625
Analysis Description: 625 MSS
METHOD BLANK: 1502801
Associated Lab Samples: 92256776001, 92256776002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
07/08/15 09:36
2,4,6-Trichlorophenot
ug/L
ND
10.0
07/08/15 09:36
2,4-Dichlorophenol
ug/L
ND
5.0
07/08/15 09:36
2,4-Dimethylphenol
ugiL
ND
10.0
07108/15 09:36
2,4-Dinitrophenol
ug/L
ND
50.0
07/08/15 09:36
2,4-Dinitrotoluene
ug/L
ND
5.0
07/08/15 09:36
2,6-Dinitrotoluene
ug/L
ND
5.0
07/08/15 09:36
2-Chloronaphthalene
ug/L
ND
5.0
07/08/15 09:36
2-Chlorophenol
ug/L
NO
5.0
07108/15 09:36
2-Nitrophenol
ug/L
NO
5.0
07108M509:36
3,T-Dichlorobenzidine
ug1L
ND
25.0
07/08/15 09:36
4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
07/08/15 09:36
4-Bromophenylphenyl ether
ug/L
ND
5,0
07/08/15 09:36
4-Chloro-3-methylphenol
ug1L
ND
5.0
07/08/15 09:36
4-Chlorophenylphenyl ether
ug/L
NO
5.0
07/08/15 09:36
4-Nitrophenol
ug1L
ND
50.0
071OW15 09:36
Acenaphthene
ug1L
ND
5.0
07/08/15 09:36
Acenaphthylene
ug1L
ND
5.0
07/08/15 09:36
Anthracene
ugiL
NO
5.0
07/08/15 09:36
Benzo(a)anthracene
ug/L
ND
5.0
07/08/15 09:36
Benzo(a)pyrene
ug/L
ND
5.0
07/08/15 09:36
Senzo(b)fluoranthene
ug/L
ND
5.0
07108115 09:36
Benzo(g,h,i)perylene
ug/L
NO
5.0
07/08115 09:36
Benzo(k)f>uoranthene
ug/L
ND
5.0
07/08/15 09:36
bis(2-Chloroethoxy)methane
ug1L
ND
10.0
07/08/15 09:36
bis(2-Chloroethyl) ether
ug/L
NO
5.0
07/08/15 09:36
bis(2-Chloroisopropyl) ether
ug/L
NO
5.0
07108/15 09:36
bis(2-Ethylhexyi)phthalate
ug/L
ND
5.0
07108/15 09:36
Butylbenzylphtha late
U91L
ND
5.0
07/08/15 09:36
Chrysene
ug/L
ND
5.0
07/08/15 09:36
Di-n-butylphthalate
ug/L
ND
5.0
07/08/15 09:36
Di-n-octylphthalate
ug/L
NO
5.0
07/08/15 09:36
Dibenz(a,h)anthracene
ug/L
NO
6.0
07108/15 09:36
Diethylphthalale
ug/L
ND
5.0
07108/15 09:36
Dimethylphthalate
ug/L
ND
5.0
07/08/15 09:36
Fluoranthene
ug/L
NO
5.0
07/08/15 09:35
Fluorene
ug/L
ND
5.0
07/08/15 09:36
Hexachloro-1,3-butadiene
ug/L
ND
5.0
07/08/15 09:36
Hexachlorobenzene
ug1L
NO
5.0
07108/15 09:36
Hexachlorocyclopentadiene
ugiL
ND
10.0
071MI5 09:36
Hexachloroethane
ug1L
ND
5.0
07/08115 09:36
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Surge 100
Huntersville, NC 28Wi
[phone]
Results presented on this page are in the units Indlcated by the -Units" column except where an altemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not tre reproduced, except in full,
Date: 07/23/2015 01:05 PM without the written consent of face Analytical Services, Inc.. Page 17 of 26

acMnalytical
www.pacefabs.com
QUALITY CONTROL DATA
Project: Outflow 6130
Pace Project No.: 92256776
METHOD BLANK: 1502801 Matrix: Water
Associated Lab Samples: 92256776001. 92256776002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Indeno(1,2,3-cd)pyrene
ug1L
ND
5.0
07/08/15 09:36
Isophorone
ug/L
ND
10.0
07/08/15 09:36
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
07/08/15 09:36
N-Nitrosodimethylamine
ug/L
ND
5.0
07/08/15 09:36
N-Nitrosodiphenylamine
ug1L
NO
10.0
07/08/15 09:36
Naphthalene
ug1L
ND
5.0
07/08/15 09:36
Nitrobenzene
ug/L
ND
5.0
07/08/15 09:36
Pentachlorophenol
ug1L
ND
10.0
07/08115 09:36
Phenanthrene
ug/L
ND
5.0
07/08/15 09:36
Phenol
ug/L
ND
5.0
07/08/15 09:36
Pyrene
ug/L
ND
5.0
07/08/15 09:36
2,4,6-Tribromophenol (S)
%
88
10-137
07/08/15 09:36
2-Fluorobiphenyl (S)
%
92
15-120
07/08/15 09:36
2-Fluorophenol (S)
%
47
10-120
07/08/15 09:36
Nitrobenzene-d5 (S)
%
84
10-120
07/08/15 09:36
Phenol-d6 (S)
%
32
10-120
07/08/15 09:36
Terphenyl-d14 (S)
%
107
11-13l
07/08/15 09:36
Pace Analytical Services. Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 2807f1
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1502802
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
34.0
68
44-142
2,4,6-Trichlorophenol
ug/L
50
44.9
90
37A44
2,4-Dichlorophenol
ug1L
50
39.6
79
1-191
2,4-Dimethylphenol
ug1L
50
37.9
76
32-119
2,4-Dinitrophenol
ug1L
250
216
87
1-181
2,4-Dinitrotoluene
ug/L
50
47.6
95
39-139
2,6-Dinitrotoluene
ug/L
50
44.9
90
50-158
2-Chloronaphthalene
ug/L
50
43.9
88
60-118
2-Chlorophenol
ug/L
50
37.1
74
23-134
2-Nitrophenol
ug/L
50
38.3
77
29-182
3,3'-Dichlorobenzidine
ug/L
100
67.8
fib
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
95.7
96
1-181
4-Bromophenylphenyl ether
ug1L
50
46.6
93
53-127
4-Chloro-3-methylphenol
ug1L
100
75.8
76
22-147
4-Chlorophenylphenyl ether
ug1L
50
49.0
98
25-15B
4-Nitrophenol
ug1L
250
102
41
1-132
Acenaphthene
ug/L
50
45.7
91
47-145
Acenaphthylene
ug/L
50
45.1
90
33-145
Anthracene
ug/L
50
49.5
99
1-166
Benzo(a)anthracene
ug/L
50
44.9
90
33-143
Senzo(a)pyrene
ug/L
50
48.9
98
17-163
Benzo(b)fluoranthene
ug/L
50
49A
99
24-159
Benzo(g,h,i)perylene
ug1L
50
52.2
104
1-219
Results presented on this page are In the units Indicated by the -Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 26

aceAnalytical
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QUALITY CONTROL DATA
Project: Outflow 6130
Pace Project No.: 92256776
LABORATORY CONTROL SAMPLE:
Parameter
1502802
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
Benzo(k)fluoranthene
ug/L
50
49.6
99
11-162
bis(2-Chloroethoxy)methane
ug/L
50
36.8
78
33-184
bis(2-Chloroethyl) ether
ug/L
50
41.1
82
12-158
bis(2-Chioroisopropyl) ether
ug1L
50
36.0
72
36-166
bis(2-Ethylhexyl)phthalate
ug/L
50
43.2
86
8-158
Butylbenzylphthalate
ug/L
50
42.3
85
1-152
Chrysene
ug/L
50
46.1
92
17-168
Di-n-butylphthalate
ug/L
50
46.4
93
1-118
Di-n-octylphthalate
ug/L
50
35.5
71
4-146
Dibenz(a,h)anthracene
ug/L
50
51.4
103
1-227
Diethylphthalate
uq/L
50
46.0
92
1-114
Dimethyiphthalate
ug/L
50
45.6
91
1-112
Fluoranthene
ug/L
50
48.4
97
26-137
Fiuorene
ug/L
50
47.4
95
59-121
Hexachloro-1,3-butadiene
ug/L
50
35.9
72
24-116
Hexachlorobenzene
ug/L
50
46.9
94
1-152
Hexachlorocyclopentadiene
ug/L
50
39.2
78
25-150
Hexachloroethane
ug/L
50
33.6
67
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
50.4
101
1-171
Isophorone
ug/L
50
36.2
72
21-196
N-Nitroso-di-n-propylamine
ug/L
50
42.6
85
1-230
N-Nitrosodimethylamine
ug/L
50
27.7
55
25-150
N-Nitrosodiphenyla mine
ug/L
50
50.1
100
25-150
Naphthalene
ug/L
50
37.0
74
21-133
Nitrobenzene
ug/L
50
38.7
77
35-180
Pentachlorophenol
ug/L
100
94.2
94
14.176
Phenanthrene
ug/L
50
48.4
97
54-120
Phenol
ug/L
50
17.3 _
35
5-112
Pyrene
ug/L
50
48.0
96
52-115
2,4,6-Tribromophenol (S)
%
103
10-137
2-Fluorobiphenyl (S)
%
89
15-120
2-Fluorophenoi (S)
%
45
10-120
Nitrobenzene-d5(S)
%
80
10-120
Phenol-d6 (S)
%
32
10-120
Terphenyl-d14 (S)
%
103
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1502803
MS
Parameter
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
92257174007
Spike
Units
Result
Cone.
ug/L
ND
100
ug/L
ND
100
ug/L
ND
100
ug/L
ND
100
ug/L
ND
500
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 10{0
Huntersville, NC 28078 `
[phone]
Qualifiers
1502804
MSD
Spike
MS
MSD
MS
MSD
% Rec
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
100
73.1
74.2
73
74
44-142
1
100
101
101
101
101
37-144
1
100
85.6
91.3
86
91
1-191
6
100
81.7
85.9
82
86
32-119
5
500
211
378
42
76
1-181
57 R1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 26

�ce �j Anal�`� f0 f
"'""=A00M
Project: Outflow 6130
Pace Project No_: 92256776
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28071b►
[phone] . r
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
15021503
1502804
MS
MSD
92257174007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units Result
Conc
Conc.
Result
Result
% Rec
°% Rec
Limits
RPD Qual
2,4-Dinitrotoluene
uglL
ND
100
100
88.8
97.9
89
98
39-139
10
2,6-Dinitrotoluene
ug/L
ND
100
100
90.2
94.4
90
94
50-15B
5
2-Chloronaphlhalene
ug/L
ND
100
100
92.3
89A
92
89
60-118
4
2-Chlorophenol
ug/L
ND
100
100
88.3
103
88
103
23-134
16
2-Nitrophenol
ug/L
ND
100
100
85.1
79.0
85
79
29-182
8
3,3'-Dichlorobenzidine
ug/L
ND
200
200
143
145
72
73
1-262
1
4,6-Dinitro-2-methylphenol
ug/L
ND
20D
200
106
151
53
76
1-181
35 R1
4-Bromophenylphenyl ether
ug1L
ND
100
100
93.8
93.0
94
93
53-127
1
4-Chloro-3-methylphencl
ug1L
NO
200
top
153
185
76
92
22-147
19
4-Chlorophenylphenyl ether
ug/L
ND
100
lot)
94.9
102
95
102
25-158
7
4-Nilrophenot
ugfL
ND
500
500
295
333
59
67
1-132
12
Acenaphthene
ug/L
ND
100
100
90.6
91.4
91
91
47-145
1
Acenaphthylene
ug/L
ND
100
100
91.7
92.6
92
93
33-145
1
Anthracene
ug/L
ND
100
100
95.1
94.8
95
95
1-166
0
Benzo(a)anthracene
ug/L
ND
100
100
89.0
91.9
89
92
33-143
3
Benzo(a)pyrene
ug/L
ND
100
100
87.6
92.1
88
92
17.163
5
Benzo(b)1luoranthene
ugIL
ND
100
100
90.4
94.2
90
94
24-159
4
Benzo(g,h,i)perylene
ug/L
ND
100
100
84.7
92.5
85
93
1-219
9
Benzo(k)Fluoranthene
ug/L
ND
100
100
83.8
88.4
84
88
11-162
5
bis(2-Chloroelhoxy)methane
ug/L
ND
100
100
77.6
71.4
78
71
33-184
8
bis(2-Chloroethyl) ether
ug/L
ND
100
100
86.2
88.1
86
88
12-158
2
bis(2-Chloroisopropyl) ether
ug/L
ND
100
100
68.3
73.3
68
73
36-166
7
bis(2-Ethylhexyl)phthalate
ug/L
ND
100
100
87.2
99.6
87
90
8-158
3
Butytbenzylphtha late
ug/L
ND
100
100
850
87.8
85
88
1-152
3
Chrysene
ug/L
NC
100
100
90,0
92.4
90
92
17-168
3
Di-n-butylphthaiate
ug/L
ND
100
100
89.5
91.0
90
91
1-118
2
Di-n-octylphthalate
ug/L
ND
100
100
83.3
84.6
83
85
4.146
2
Dibenz(a,h)anth racene
uglL
ND
1()0
100
86 -5
95.8
86
96
1-227
10
Diethylphthatate
ug/L
NO
100
100
86.6
94.6
87
95
1-114
9
Dimethylphthalate
ug/L
ND
100
100
89.2
92.4
89
92
1-112
3
Fluoranthene
ug/L
ND
100
100
97.0
95.7
97
96
26-137
1
Fluorene
ug1L
ND
100
100
91.6
97.2
92
97
59-121
6
Hexachloro- 1, 3-butad iene
ug/L
ND
100
100
76.0
78.3
76
78
24-116
3
Hexachlorobenzene
ug/L
ND
100
100
92.3
91.2
92
91
1-152
1
Hexachlorocyclopentadiene
ug/L.
ND
100
100
47A
53.5
47
53
25-150
13
Hexachloroclhanc
ug/L
ND
100
100
62.1
76.0
62
76
40-113
20
Indeno(1,2,3-cd)pyrene
uglL
ND
100
100
84.9
92A
85
92
1-171
8
Isophorone
ug/L
ND
100
100
70.1
65.7
70
66
21-196
6
N-Nitroso-di-n-propylamine
ug/L
ND
100
100
76.6
90.5
77
90
1-230
17
N-Nitrosodimethylamine
ug/L
ND
100
100
67.9
62.4
68
62
25-150
8
N-Nitrosodiphenylamine
ug1L
ND
100
100
95.9
96.3
96
96
25-150
0
Naphthalene
ug/L
ND
100
100
75.5
76.8
75
77
21-133
2
Nitrobenzene
ug/L
ND
100
100
80.8
73.6
81
74
35.180
9
Pentachlorophenol
ug/L
ND
200
200
185
192
93
96
14.176
4
Phenanthrene
ug/L
ND
100
100
92,0
92.6
92
93
54-120
1
Phenol
uglL
NO
100
100
5.2J
70.1
5
70
5-112
Results presented on this page are in the
units Indicated
by the -Units- column
except where an altemate unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 07/2312015 01 05 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 26

Iac
(
eAnalWcal
www.peordebs.txlm
QUALITY CONTROL DATA
Project: Outflow 6130
Pace Project No.: 92256776
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
kuntersville. NC 28071P:
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1502803
1502804
MS
MSD
92257174007 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
Pyrene
ug/L ND 100
100
88.3
92.5 88
92
52-115 5
2,4,6-Tribromophenol (S)
%
107
104
10-137
2-Fluorobiphenyl (S)
%
93
85
15-120
2-Fluorophenol(S)
%
68
73
10-120
Nitrobenzene-d5 (S)
%
84
76
10-120
Phenol-d6 (S)
%
53
fib
10-120
Terphenyl-d14 (S)
%
93
97
11-131
Results presented on this page are in the units Indicated by the "Units" cdumn except where an alternate unit IS presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc..
Page 21 of 26

aceAna4 tr'cal
www ombbs now
QUALITY CONTROL DATA
Project: Outflow 6130
Pace Project No.: 92256776
QC Batch: WET138615 Analysls Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92256776001, 92256776002
METHOD BLANK: 1502380
Associated Lab Samples: 92256776001, 92256776002
Parameter Units
Total Suspended Solids mgJL
LABORATORY CONTROL SAMPLE: 1502381
Parameter Units
Total Suspended Solids mgfL
Pace Analytical Servicesa Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078 r,a
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 07/0611517:23
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 242 97 90-110
SAMPLE DUPLICATE: 1502382
92256765006 Dup
Parameter Units Result Result
Total Suspended Solids mglL _ 6.8 7.0
SAMPLE DUPLICATE: 1502383
92256795001 Dup
Parameter Units Result Resull
Total Suspended Solids m94- 67.0 70.0
RPD Qualifiers
3
RPD Qualifiers
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 26

Pace Analytical Services, Inc.
�acie
,Malj4ical*
98o0 KinceyAve. Suit&100
Huntersvitle, NC 28071 .
""" [phone]
QUALIFIERS
Project: Outflow 6130
Pace Project No.: 92256776
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
POL - Practical Quanlitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anatyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Ouplicatej
OUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each anatyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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Date: 07/23/2015 01:05 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 26

5Lqc
(
eAnalj4kal
www.pxaedab cam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Paco Analytical Services, Inc.
9800 Kincey Ave. Suit 10n.,�
Huntersville. NG 28078V
[phone]
Project.
Outflow 6130
Pace Project No.:
92256776
Analytical
Lah ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92256776001
Outflow 01
EPA 1664B
GCSV121938
92256776002
Outflow #2
EPA 1664E
GCSV121938
92256776001
Outflow #1
EPA 3510
OEX71-136240
EPA 608
GCSV121919
92256776002
Outflow #2
EPA 3510
OEXT/36240
EPA 608
GCSV/21919
92256776001
Outflow #1
EPA 200.7
MPRP118906
EPA 200.7
ICP116967
92256776002
Outflow #2
EPA 200.7
MPRP118906
EPA 200.7
ICP116967
92256776001
Outflow #1
EPA 625
OEXT/36226
EPA 625
MSSV110911
92256776002
Outflow #2
EPA 625
0EXT/35226
EPA 625
MSSV110911
92256776001
Outflow #1
EPA 624
MSV/32470
92256776002
Outflow #2
EPA 624
MSV/32470
92256776001
Outflow #1
SM 2540D
WET138615
92256776002
Outflow #2
SM 2540D
WET/38615
Date: 07/23/2015 01:05 PM
REPORT Of LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written conSenl of Pace Analytical Services, Inc..
Page 24 of 26

CHAIN -OF -CUSTODY 1 Analytical Request Document to
acEArralytiial The Chain•uf•Custwy is a LEGAL DOCUMENT. Ail relevant fields must be completed accurately.LO
7p
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Papa. ca
Seon A Section a Section C
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Required CNent Information: Requlred Project Irdonnation: Invoice Information:
Company: Report To/ `I tpn
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Copy To:
Company Name:
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REfat3LA70-f2Y AGENCY
AAvj� � 19: 4-
dress:
r NPOES F GROUNDWATER j— DRINKING WATER
j UST f RCRA r OTHER
Emad To: r ,� a
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1Requested'AnakysisFittaredl(YIN)'7-
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DATE
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SAMPLEiZ NAME AND'StGNATUitE. - •'
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PRINT Name of SMAPLER: IC.=� �`
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SIGNATURE Of SAMPLER: DATE Signed
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'Impotent Note: 6y signing this form you are aacapling Pero•s NET 30 day payment %M4 and agreainp to late ehatges of 1.5% por nwnlh for any krAk as not pad %wiWm 30 days- F-ALL-0-020rev.07, 15-May-2007

Document Name: Sample-Condition'Upon
* d6l'Gm
Recei:'tySOUR
F-ASV-CS-bOtrev.14" , ti;_".='3, Pace
wised: May 16, 20
ie 1 of 2*
Office
Client Name: +}ur' f` �* page 2 of 2 is for Internal Use Only
k ,
r
Courier (Circle): Fed Ex UPS t1SPS , Client ' Commercial Pace Other
Custody Seal on CoolerlBox Present: ❑ yes 'no- Se Is int_act:. (] yes no
Packing Material: Bu .1�fjR-E3. Bubble Bags Non ' , Other
Thermometer Use � IR Gun#3 • Type of ice: Wet 1 Blue None mples on Ice, cooling process has begun
IR Gun #4 SN.140290365 Other. ! i
Temp Correction 'Factor: Add 1 Subtract 0,0 C'
Corrected Cooler Temp.: a• l C
Btolcgical Tlssue'Is Froieri: Yea Nn NIA` "teend Initials of per on xamining
contents: 15
Temp should be above freezing to 6•C
; Comments: 1
Chain of Custody Present: ,
ea` .ON.
❑hllq
1: i r 1
Chain of Custod FINed Out:
es ONo
' OMIA
2 ;
Chain of Custoti ReA ulshed:
es ' No
❑HIA
31
Sampler Narrie & Si nature on COC: ,
� ea No
E]NIA
4
Sam..les'Arrlved with In Hold Time:
es ❑No
-- MIA
5r • i
Short Hoid.Time Analysis <72hr :
Oyes'. K No.
41A
6:
Rush Turn Around Time Re uested:
❑Yea`, o.. Ohm
7'
Sufficient Volurhe.
' ei: No
❑NIA
8.
Correct Containers Used:
;.
ee El
❑NIA
9.
-Pace Containers Used:
es C]No
❑NIA
l
Containers Intact:
cal 0N6
❑t
1b.
Filtered volume received for Dissolved tests
Oyes' No
NIA
I.J.
Sample Labels match COO:
es ©No
❑NIA
12. -
-Includes date/tlmeNDlAnal sis Matrix:
W
All containers needing preservation have been checked.
13'es ONO
❑NIA
13,
All containers, needing preservation are found to be In
Yes ONo
❑N!A
compliance with EPA recommendation.
excepllans: VOA, cot orm, TOC, O&G, V"RQ ie
❑Yea jBNo .
Samples checked for.dechlorination:
es ON.
ONr
14.
Headspaee in VOA Vials ( >6mm :
Dyes ONO
61NI:l
15,
Trip Blank Present:
Ores ON.
Nr 1,16.
Trip Blank Custody Seals Present
Oyes ONO
QN`IA
Pace Trip Blank Lot # if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
Datemme:
Field Data Required? Y I N
SCURF Review: Date: r dry. Place label here
SRF Review: Date:L. WD# : 92256776
Note: Whenever there Is discrepancy affecting o h Carolina
compliance samples, a copy of this form will be sent to the North I ��
Carolina DEHNR Certification Office (i.e out of hold, Incorrect
preservative, out of temp, Incorrect containers) 92266776
It
Page 26 of 26

Semi-annual Stormwater Discharge Monitoring Report
r for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted August 25, 2014
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls_
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Pace Analytical Lab Cert. #40
Comments on sample collection or analysis: See page 4
'art A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR �2014
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ® Monthly' August month
DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
®Other: Class C, Swannanoa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inche53
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organics
Benchmarks =__>
-
-
100 mg/L ar 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
08/08/14
1.09
21.1 mg/L
7.1
0.026 mg/L
0.006
0.064mg/L
<5.0 mg/L
BRL
2
08/08/14
1.09
11.9 mg/L
7.2
0.029 mg/L
0.0050
0.222 mg/L
<5.0 mg/L
BRL
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfatl.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31),
Permit Date: 11/1/2012-10/31/2017
Received
AUG 2 12014
Land Quality Section
Asheville
SWU-245, last revised 10/25/2012
Page 1 of 4

r-
noifso-2 Y-qi!ruP bnaJ
'..., A

FScilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Jason Stone
Name (Print name)
Plant Manager
Title (Print title)
J(.,, 8/26/2014
Olature) (Date)
Note: Results must be reported in numerical format. Do not re art Below Detection Limit, 8DL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<U ng/l", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period72
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inche53
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
-
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 -- 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

r
Abte: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text.
�R_,/
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑
REGIONAL OFFICE CONTACT NAME: _ Laura Herbert, P.E.
Mail an_original and one copy of this DMR including all "No Discharge" reports, within 30 day, of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of water Quality
ttn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
ature of Permittee)
8/26/2014
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 4

ly Zinc reporting value exceeds permit limit 0.067 for outfall #1 and #2
�- a) Finding;
i) Roofing material is galvanized metal could be a contributing factor for outfall #1 and #2.
b) Corrective actions;
i) Reviewed BMP, ensured good management practices are being followed.
2) Copper reporting value exceeds permit limit 0.007 for outfall #2
a) Finding;
i) Roofing material is metal could be a contributing factor for outfall 42.
ii) We do not find potential sources of copper exposure in outfall #2.
b) Corrective actions;
i) Review of BMP's
ii) Have increased housekeeping, Lugger Pad Area and Center Pad are being inspected and cleaned after each use.
iii) Dump bins are cleaned off prior to being taken outside for dumping into luggers
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 4 of 4

aceAnalytical
wwwpacelab&mrn
August 19, 2014
Gerald Runkles
Pentair Valves & Controls
953 Old US Hwy 70
Black Mountain, NC 28711
RE: Project: August 2014 8f8
Pace Project No.: 92212683
Dear Gerald Runkles:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on August 06, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
2 �O
r Agp �,Cp�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
hout the written Consent of Pace Analytical Services, Inc..
Page 1 of 27

ace Analytical
wwW4mN arabs.awn
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: August 2014 818
Pace Project No.: 92212683
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Urglnia/VELAP Certification #: 460221
North Carolina Wastewater Certification #. 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
UrginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, li
f ,f
Page 2 elf 27
R

aceAnalytical
www.pacerabs cam
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
August 2014 818
92212683
Analyses
Lab ID
Sample 10
Method
Analysts
Reported
Laboratory
92212683001
OUTFALL # 1
EPA 1664B
CLW
1
PASI-C
EPA 608
RES
27
PAS!-C
EPA 200.7
JMW
3
PASI-A
EPA 625
Bpi
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MAB
1
PASI-A
92212683002
OUTFALL # 2
EPA 1664B
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA200.7
JMW
3
PASI-A
EPA 625
BPJ
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MAB
1
PASI-A
.. REPORT OF LABORATORY ANALYSIS
V.
•
This report shall not be reproduced, except in full,
hout the written consent of Pace Analytical Services, Inc.. Page 3 of 27
r
a

�acmnalj#ical`
W".pecelabs.w n
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project: August 2014 818
Pace Project No.: 92212683
Lab Sample ID
Client Sample ID
Method
Parameters
Result Units
Report Limit
Analyzed Qualifiers
92212683001
OUTFALL # 1
EPA 200.7
Copper
25.5 ug/L
5.0
08/11/14 18:59
EPA 200.7
Lead
6.0 ug/L
5.0
08/11/14 18:59
EPA 200.7
Zinc
63.8 ug/L
10.0
08/11/14 18:59
SM 2540D
Total Suspended Solids
21.1 mg1L
2,5
08/13/14 12:15
92212683002
OUTFALL # 2
EPA 200.7
Copper
29.0 ug/L
5.0
08/11/14 19:02
EPA 200.7
Zinc
222 uglL
10.0
08111114 19:02
SM 2540D
Total Suspended Solids
11.9 mg1L
5.2
08/13/14 12:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ir
J w
Page 4 of 27
h

aceAnalytical
www.pacelab&=
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: August 2014 818
Pace Project No,: 92212683
Sample: OUTFALL # 1 Lab ID: 92212683001 Collected: 08/08/14 10:00 Received: 08/08/14 14:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 16648
Oil and Grease
NO mg/L
5.0
1
08111l14 10:35
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 0319
309-00-2
alpha-BHC
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:19
319-84-6
beta-BHC
NO ug/L
0,050
1
08/11/14 16:05
08/14/14 03:19
319-85-7
delta-BHC
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:19
319-86-8
gamma-BHC (Lindane)
NO ug/L
0.050
1
08/11/14 16:05
08/14114 03:19
58-89-9
Chlordane (Technical)
NO ug/L
0.50
1
08111114 16:05
08/14/14 03:19
57-74-9
4,4'-DDD
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:19
72-54-8
4,4'-DDE
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:19
72-55-9
4,4'-DDT
ND ug/L
0.050
1
08/11/14 16:05
08/14/14 03:19
50-29-3
Dieldrin
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:19
60-57-1
Endosulfan I
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03,19
959-98-8
Endosulfan II
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:19
33213-65-9
Endosulfan sulfate
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:19
1031-07-8
Endrin
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:19
72-20-8
Endrin aldehyde
NO ugiL
0.050
1
08/11/14 16:05
08/14/14 03:19
7421-93-4
Heptachlor
NO ugiL
0.050
1
08/11/14 16:05
08/14/14 03:19
76-44-8
Heptachlor epoxide
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:19
1024-57-3
PCB-1016 (Aroclor 1016)
NO ug/L
0.50
1
08/11/14 16:05
08/14/14 03:19
12674-11-2
PC13-1221 (Aroclor 1221)
NO ug/L
0.50
1
08/11/14 16:05
08/14/14 03:19
11104-28-2
PCB-1232 (Arodor 1232)
NO ugiL
0.50
1
08/11114 16:05
08/14/14 03:19
11141-16-5
PCB-1242 (Arodor 1242)
NO ug/L
0.50
1
08/11/14 16:05
W14114 03:19
53469-21-9
PCB-1248 (Arodor 1248)
ND ug/L
0.50
1
08111114 16.05
W14114 03:19
12672-29-6
PCB-1264 (Arodor 1254)
ND ug/L
0.50
1
08/11/14 16.05
08/14114 03:19
11097-69-1
PCB-1260 (Arodor 1260)
NO ug/L
0.50
1
08/11/14 16:05
08/14/14 03:19
11096-82-5
Toxaphene
NO ug/L
0,50
1
08/11/14 16:05
08/14/14 03:19
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
26 %
20-110
1
08/11/14 16:05
08/14/14 03:19
877-09-8
Decachlorobiphenyl (S)
27 %
20-138
1
08/11/14 16:05
08/14/14 03:19
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA
200.7
Copper
25.5 ug/L
5.0
1
08/0811419:30
08/11/1418:59
7440-50-8
Lead
6.0 ug/L
5.0
1
08/08/14 19:30
08/1111418:59
7439-92-1
Zinc
63.8 ug/L
10.0
1
08/08/14 19:30
08/11M418:59
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
NO ug/L
6.2
1
08111/14 08:27
08/12/14 23:37
83-32-9
Acenaphthylene
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
208-96-8
Anthracene
NO ug/L
6.2
1
08M1114 08:27
08/12/14 23:37
120-12-7
Benzo(a)anthracene
NO ugiL
6.2
1
08/11/14 08.27
08/12114 23:37
56-55-3
Benzo(a)pyrene
NO ug/L
6.2
1
08/it/14 08:27
08112114 23:37
50-32-8
Benzo(b)fluoranthene
NO ug1L
6.2
1
08/11/14 08:27
08/12114 23:37
205-99-2
8enzo(g,h,i)perylene
NO ugiL
6.2
1
08/11/14 08:27
08/12/14 23:37
191-24-2
Benzo(k)fluoranthen e
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
207-08-9
REPORT OF LABORATORY ANALYSIS
t ,` This report shall not be reproduced, except in full,
Gatei 08/19/2014 06:14 PM hout the written consent of Pace Analytical Services, Inc..
r
Page 5 of 27

aceAnalytical"
www.pecatebs.etun
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: August 2014 818
Pace Project No.: 92212683
Sample: OUTFALL # 1 Lab ID: 92212683001 Collected: 08108/14 10:00 Received. 08108/14 14:50 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
4-Bromophenylphenyl ether
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
101-55-3
Butylbenzylphthalate
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
85.68-7
4-Chloro-3-methylphenot
NO ug/L
6.2
1
08/11/14 08:27
Call2114 23:37
59-50-7
bi8(2-Chloroethoxy)methane
NO ug/L
12.5
1
08/11/14 08.27
08/12/14 23:37
111-91-1
bis(2-Chloroethyi) ether
NO ug/L
6.2
1
08/11/14 08:27
08/12114 23:37
111-44-4
bis(2-Chloroisopropyl) ether
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
108-60-1
2-Chloronaphthalene
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
91-58-7
2-Chlorophenol
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
95-57-8
4-Chlorophenylphenyl ether
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
7005-72-3
Chrysene
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
218-01-9
Dibenz(a,h)anthracene
ND ug/L
6.2
1
08/11/14 08:27
08li2/14 23:37
53-70-3
3,T-Dichlorobenzidine
ND uglL
31.2
1
08/11/14 08:27
08112114 23:37
91-94-1
2,4-Dichlorophenol
ND ug/L
6.2
1
08111/14 08:27
08112114 23:37
120-83-2
Diethyl phthalate
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
84-66-2
2,4-Dimethylphenol
NO ug/L
12.5
1
08/11/14 08:27
08/12/14 23:37
105-67-9
Di methyl phtha late
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
131-1i-3
Di-n-butylphthalate
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
84-74-2
4,6-Din1tro-2-methyiphenol
NO ug/L
25.0
1
08/11/14 08:27
08/12/14 23:37
534-52-1
2,4-Dinitrophenol
ND ug/L
62.5
1
08/11/14 08:27
08/12/14 23:37
51-28-5
2,4-Dinitrotoluene
ND ug/L
6.2
1
08/11/14 08:27
08/12114 23:37
121-14-2
2,6-Dinitrotoluene
ND ug/L
6.2
1
08111/14 08.27
08/12/14 23.37
606-20-2
Di-n-octylphthalate
NO ug/L
6.2
1
08/11/14 08*27
08112/14 23:37
117-84-0
bis(2- Ethylhexyl)phtha late
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
117-81-7
Fluoranthene
NO ugfL
6.2
1
08/11/14 08:27
08/12/14 23:37
206-44-0
Fluorene
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
87-68-3
Hexachlorobenzene
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
116-74-1
Hexachlorocyclopentadiene
ND ug/L
12.5
1
08/11/14 08:27
08/12/14 23:37
77-47-4
Hexachloroethane
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
6.2
1
08/11/14 08:27
08/12114 23:37
193-39-5
Isophorone
NO ugfL
12.5
1
08/11/14 08:27
08/12/14 23:37
78-59-1
Naphthalene
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
91-20-3
Nitrobenzene
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
98-95-3
2-Nitrophenol
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
88-75-5
4-Nitrophenol
NO ug/L
62.5
1
08/11/14 08:27
08/12/14 23:37
100-02-7
N-Nitrosodimethylamine
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
6.2
1
08111/14 08:27
08/12/14 23:37
621-64-7
N-Nitrosodiphenyiamine
ND ug/L
12.5
1
08/11/14 08:27
08/12/14 23:37
86-30-6
Pentachtorophenol
ND ugfL
12.5
1
08111114 08:27
08/12/14 23:37
87-86-5
Phenanthrene
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
85-01-8
Phenol
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
108-95-2
Pyrene
ND ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
129-00-0
1,2,4-Trichlorobenzene
NO ug/L
6.2
1
08/11/14 08:27
08/12/14 23:37
120-82-1
2,4,6-Trichlorophenol
ND ug/L
12.5
1
08/11/14 08:27
08/12/14 23:37
88-06-2
Surrogates
Nitrobenzene-d5 (5)
29 %
10-120
1
08111114 08:27
08/12/14 23:37
4165-60-0
2-Fluorobiphenyl (S)
30 %
15.120
1
08/11/14 08:27
08/12/14 23:37
321-60-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, ,
Date: 08/19/2014 06:14 PM without the written consent of Pace Analytical Services, 1• Page 6 Of 41

Pace Analytical Services, Inc.
aeeAnalytical 8800 I<incey Ave. Suite 100
Huntersville, NC 28078
www.pecftbs.00m [phone]
ANALYTICAL RESULTS
Project: August 2014 818
Pace Project No.: 92212683
Sample: OUTFALL # 1 Lab ID: 92212683001 Collected: 08/08/14 10:00 Received: 08/08/14 14:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Surrogates
Terphenyl-d14 (S)
68 %
11-131
1
08/11/14 08:27
08/12/14 23:37
1718-51-0
Phenol-d6 (S)
12 %
10-120
1
08/11/14 08:27
08/12/14 23:37
13127-88-3
2-Fluorophonol (S)
16 %
10-120
1
08/11/14 08:27
08/12/14 23:37
367-12-4
2,4,6-Tribromophenol (S)
57 %
10-137
1
08/11/14 08:27
08/12/14 23:37
118-79-6
624 Volatile Organics Analytical Method: EPA624
Benzene
Bromodichioromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
ds-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1, 3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethene
1,1,2-Trichloroethene
Trichloroethene
Trichlorotiuoromethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
2540D Total Suspended Solids
Total Suspended Solids
ND ug/L
2.0
1
08/18/14 23:28
71-43-2
ND ug/L
2.0
1
08/18/14 2128
75-27-4
ND ug/L
2.0
1
08/18/14 2128
75-25-2
ND ug/L
2.0
1
08/18/14 23:28
74-83-9
ND ug/L
2.0
1
08/18/14 23:28
56-23-5
NO ug/L
2.0
1
08/18/14 23:28
108-90-7
NO ug/L
2.0
1
08/18/14 2128
75-00-3
NO ug/L
2.0
1
08/18/14 23:28
67-66-3
NO ug/L
2.0
1
08/18/14 23:28
74-87-3
NO ug/L
2.0
1
08/18/14 23:28
124-48-1
ND ug/L
2.0
1
08/18/14 23:28
95-50-1
ND ug/L
2.0
1
08/18/14 23:28
541-73-1
NO ug/L
2.0
1
08/18/14 23:28
106-46-7
NO ug/L
2.0
1
08/18/14 23:28
75-34-3
NO ug/L
2.0
1
08/18/14 23:28
107-06-2
ND ug/L
2.0
1
08118114 23.28
75-35-4
NO ug/L
2.0
1
08/18/14 23:28
156-59-2
ND ug/L
2.0
1
08118114 23:28
156-60-5
ND ug/L
2.0
1
08/18114 23:28
78-87-5
NO ug/L
2.0
1
08/16114 23:28
10061-01-5
NO ug/L
2.0
1
08/18/14 23:28
10061-02-6
NO ug/L
2.0
1
08/18/14 23:28
100-41-4
NO ug/L
2.0
1
08/18/14 23:28
75-09-2
NO ug/L
2.0
1
08/18/14 23:28
79-34-5
NO ug/L
2.0
1
08/18/14 2128
127-18-4
NO ug/L
2.0
1
08/18/14 23:28
108-88-3
ND ug/L
2.0
1
08/18/14 23:28
71-55-6
NO ug/L
2.0
1
08/18/14 23:28
79-00-5
NO ug/L
2.0
1
08/18/14 23:28
79-01-6
ND ug/L
2.0
1
08/18/14 23:28
75-69-4
ND ug/L
2,O
1
08/18/14 23:28
75-01-4
100 %
70-130
1
08/18/14 23:28
460-00-4
101 %
70-130
1
08/18/14 23:28
2037-26-5
106 %
70-130
1
08/18/14 23:28
17060-07-0
Analytical Method: SM 2540D
21.1 mg/L
2.5 1
REPORT OF LABORATORY ANALYSIS
08/13/14 12:15
date,08119/2014 06:14 PM
This report shall not be reproduced, except in full,
)out the written consent of Pace Analytical Services, Inc..
Page 7 of 27

Pace Analytical Services, Inc.
aceAnalytieal0 9800 KineyAve. Suite 100
Huntersvil2e, NC 28078
www.peoelebs.mm [phone]
ANALYTICAL RESULTS
Project: August 2014 8/8
Pace Project No.: 92212683
Sample: OUTFALL # 2 Lab ID: 92212683002 Collected: 08/08/14 10:05 Received: 08/08/14 14:50 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg1L
5.0
1
08/11/14 10:35
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
NO ug/L
0.050
1
08/11/14 16:05
081104 03:37
309-00-2
alpha-BHC
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:37
319-84-6
beta-BHC
NO ug/L
0.050
1
08/11/14 16:05
06/14/14 03.37
319-85-7
delta-BHC
NO ug/L
0.050
1
08111/14 16:05
08/14114 03:37
319-86-8
gamma-BHC (Lindane)
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:37
58-89-9
Chlordane (Technical)
ND ug/L
0.50
1
08/11/14 16:05
08/14114 03.37
57-74-9
4,4'-DDD
NO ug/L
0-050
1
08/11/14 16:05
08114/14 03:37
72-54-B
4,4'-DDE
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:37
72-55-9
4,4'-DDT
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:37
50-29-3
Dieldrin
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:37
60-57-1
Endosulfan I
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03,37
959-98-8
Endosulfan II
NO ug/L
0.050
1
08/11/14 16:05
08/14/14 03:37
33213-65-9
Endosulfan sulfate
ND ug/L
0.050
1
08/11/14 16:05
08/14/14 03:37
1031-07-8
Endrin
ND ug/L
0.050
1
08/11/14 16:05
08/14/14 03:37
72-20-8
Endrin aldehyde
ND ug/L
0.050
1
08/11/14 16:05
08/14/14 03:37
7421-93-4
Heptachlor
ND ug/L
0,050
1
08/11/14 16:05
08/14/14 03:37
76-44-8
Heptachlor epoxide
ND ug/L
0,050
1
08/11/14 16:05
08/14/14 03:37
1024-57-3
PC6-1016 (Aroclor 1016)
ND ug/L
0.50
1
08/11/14 16:05
08/14/14 03:37
12674-11-2
PCB-1221 (Aroclor 1221)
NO ug1L
0.50
1
08/11/14 16:05
08/14/14 0137
11104-28-2
PCB-1232 (Aroelor 1232)
ND ug/L
0.50
1
08/11/14 16:05
08/14/14 03:37
11141-16-5
PCB-1242 (Aroclor 1242)
ND ug/L
0.50
1
08/11/14 16:05
08/14/14 03:37
53469-21-9
PCB-1248 (Aroolor 1248)
ND ug/L
0-50
1
08/11/14 16:05
08/14/14 03:37
12672-29-6
PCB-1254 (Aroclor 1254)
ND ug/L
0-50
1
08/11/14 16:05
08/14/14 03:37
11097-69-1
PCB-1260 (Aroclor 1260)
ND ug/L
0.50
1
08/11/14 16:05
08/14/14 03:37
11096-82-5
Toxaphene
ND ug/L
0.50
1
08/11/14 16:05
08/14/14 03:37
8001-35-2
Surrogates
Tetra chloro-m-xylene (S)
73 %
20-110
1
08/11/14 16:05
08/14/14 03:37
877-09-8
Decachlorobiphenyl (S)
64 %
20-138
1
08/11/14 16:05
08/14/14 03:37
2051-24-3
200.7 MET ICP
Analytical Method: EPA200.7 Preparation Method: EPA200.7
Copper
29.0 ug/L
5.0
1
08/08/14 19:30
08/11/14 19:02
7440-50-8
Lead
NO ug/L
5.0
1
0810811419:30
08/11/14 19:02
7439-92-1
Zinc
222 ug/L
10.0
1
0810811419:30
08/11/14 19:02
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
NO uglL
6.2
1
08/11/14 08:27
08/13/14 00:05
83-32-9
Acenaphthytene
ND ug/L
6.2
1
06/11/14 08:27
08/13/14 00:05
208-96-8
Anthracene
ND ug/L
6.2
1
08/11/14 08727
08/13/14 00:05
120-12-7
Benzo(a)anthracene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
56-55-3
Benzo(a)pyrene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
50-32-8
Benzo(b)fluoranthene
NO ug/L
6.2
1
08/11114 08:27
08/13/14 00:05
205-99-2
Benzo(g,h,i)perylene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
191-24-2
Benzo(k)fluoranthene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
207-08-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/19/2014 06:14 PM without the written consent of Pace Analytical Services, I
Page 8 of 27
ti

Pace Analytical Services, Inc.
aeeAnalytieal 0 9800 Kincey Ave. 2 100
Huntersville, NCC 213078
www.peoefebscam [phone]
ANALYTICAL RESULTS
Project: August 2014 618
Pace Project No.: 92212683
Sample: OUTFALL # 2 Lab ID: 92212683002 Collected: 08/08/14 10:05 Received: 08/08/14 14:50 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared
Analyzed
CAS No. Quaff
625 MSSV
Analytical Method: EPA 625
Preparation Method: EPA 625
4-Bromophenylphenyl ether
NO ug1L
6.2
1
08111/14 08:27
08/13/14 00:05
101-55-3
Butylbenzylphthalate
ND ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
85-68-7
4-Chloro-3-methylphenol
NO ug1L
6.2
1
08/11/14 08:27
08/13/14 00:05
59-50-7
bis(2-Chloroethoxy)methane
NO ug/L
12.5
1
08/11/14 08:27
08/13/14 00:05
111-91-1
bis(2-Chloroethyl) ether
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
111-44A
bis(2-Chtoroisopropyl) ether
ND ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
108-60-1
2-Chioronaphthalene
NO ug/L
&2
1
08111114 08:27
08/13114 00:05
91-58-7
2-Chlorophenol
ND ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
95-57-8
4-Chlorophenylphenyl ether
NO ug/L
6.2
1
08/11114 08:27
08/13/14 00:05
7005-72-3
Chrysene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
218-01-9
Dibenz(a,h)anthracene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
53-70-3
3,3'-Dichlorobenzidine
NO ug/L
31.2
1
08/11/14 08:27
08/13/14 00:05
91-94-1
2,4-Dichlorophenol
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
120-83-2
Diethyl phthalate
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
84-66-2
2,4-Dimethylphenol
NO ug/L
12.5
1
08/11/14 08:27
08/13/14 00:05
105-67-9
Dimethylphthalate
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
131-11-3
Di-n-butylphthalate
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
84-74-2
4,6-Dinitro-2-methylphenol
NO uglL
25.0
1
08/11/14 08:27
08/13114 00:05
534-52-1
2,4-Dinitrophenol
NO ug/L
62.5
1
08/11/14 08:27
08/13/14 00:05
51-28-5
2,4-Dinitrotoluene
NO ug1L
6.2
1
08/11/14 08:27
08/13/14 00:05
121-14-2
2,6-Dinitrotoluene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
606-20-2
Di-n-octylphthalate
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
117-84-0
bis(2-Ethylhexyl)phthalate
NO ugll-
6.2
1
08/11/14 08:27
08/13/14 00:05
117-81-7
Ftuoranthene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
206-44-0
Fluorene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
86-73-7
Hexachloro-1,3-butadiene
NO ug1L
6.2
1
08/11114 08:27
08/13/14 00:05
87-68-3
Hexachlorobenzene
NO ug/L
6.2
1
08/11/14 0&27
08/13114 00:05
118-74-1
Hexachlorocydopentadiene
NO ug/L
12.5
1
08/11/14 08:27
06113/14 00:05
77-47-4
Hexachloroethane
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
67-72-1
Indeno(1,2,3-cd)pyrene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
193-39-5
Isophorone
NO ug/L
12.5
1
08/11/14 08:27
08/13/14 00:05
7&59-1
Naphthalene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
91-20-3
Nitrobenzene
NO ug/L
6.2
1
08/11/14 08:27
08113/14 00:05
98-95-3
2-Nitrophenol
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
88-75-5
4-Nitrophenol
NO ug/L
62.5
1
08/11/14 08:27
08/13/14 00:05
100-02-7
N-Nitrosodimethylamine
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
62-75-9
N-Nitroso-di-n-propylamine
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
621-64-7
N-Nitrosodiphenylamine
NO ug/L
12.5
1
08/11/14 08:27
08/13/14 00:05
86-30-6
Pentachlorophenol
NO ug/L
12.5
1
08/11/14 08:27
08/13/14 00:05
87-86-5
Phenanthrene
NO ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
85-01-8
Phenol
ND ug/L
6.2
1
08/11/14 08:27
08113114 00:05
108-95-2
Pyrene
ND ug/L
6.2
1
08/11/14 08:27
08/13/14 00:05
129-00-0
1,2,4-Trichlorobenzene
NO ug/L
6.2
1
08111/14 08!27
08/13/14 00:05
120-82-1
2,4,6-Trfchlorophenol
NO uglL
12.5
1
08111114 08:27
08/13/14 00:05
88-06.2
Surrogates
Nitrobenzene-d5 (S)
72 %
10-120
1
08/11/14 08:27
08/13/14 00:05
4165-60-0
2-Fluorobiphenyt (S)
70 %
15-120
1
08/11/14 08:27
08/13/14 00:05
321-60-8
REPORT OF LABORATORY ANALYSIS
lf'1
"N. This report shall not be reproduced, except in full,
Date; 08/19/2014 06:14 PM hout the written consent of Pace Analytical Services, Inc.. Page 9 of 27
11

aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
ANALYTICAL RESULTS
Project: August 2014 8/8
Pace Project No.: 92212683
Sample: OUTPALL # 2 Lab ID: 92212683002 Collected: 08/08/14 10:05 Received: 08/08/14 14:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Surrogates
Terphenyl-d14 (S)
83 %
11-131
1 08/11/14 08:27
08/13/14 00:05
1718-51-0
Phenol-d6 (S)
30 %
10-120
1 08/11/14 08:27
08/13/14 00:05
13127-88-3
2-Fluorophenol (S)
40 %
10-120
1 08/11/14 08:27
08/13/14 00:05
367-12-4
2,4,6-Tribromophenol (S)
75 %
10-137
1 08/11/14 08:27
08/13/14 00:05
118-79-6
624 Volatile Organics Analytical Method: EPA624
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochiorom etha ne
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1.1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1, 3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Tri chloroetha ne
1,1,2-Tri chloroetha n e
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
2540D Total Suspended Solids
Total Suspended Solids
ND ug/L
20
1
08/18/14 23.45
71-43-2
ND ug1L
2.0
1
08118/14 23:45
75-27-4
ND uglL
2.0
1
08/18/14 23:45
75-25-2
ND ug/L
2.0
1
08/18/14 23:45
74-83-9
ND ug/L
2.0
1
08/18/14 23:45
56-23-5
ND ug/L
2.0
1
08/18/14 23:45
108-90-7
ND ug1L
2.0
1
08/18/14 23:45
75-00-3
ND ug/L
2.0
1
08/18/14 23:45
67-66-3
ND ug/L
2.0
1
08/18/14 23;45
74-87-3
ND ug/L
2.0
1
08/18/14 23:45
124-48-1
ND ug/L
2.0
1
08/18/14 23:45
95-50-1
ND ug/L
2.0
1
08/18/14 2145
541-73-1
ND ug1L
2.0
1
08/18/14 23:45
106-46-7
ND ug1L
2.0
1
08/18/14 23:45
75-34-3
ND ug/L
2.0
1
08/18/14 23:45
107-06-2
ND ug/L
2.0
1
08/18/14 23:45
75-35-4
ND ug/L
2-0
1
08/18/14 23:45
156-59-2
ND ug/L
2-0
1
08/18/14 23:45
156-60-5
ND ug/L
2.0
1
08/18/14 23:45
78-87-5
ND ug1L
2.0
1
08118114 23:45
10061-01-5
ND ug/L
2.0
1
08/18/14 23:45
10061-02-6
ND ug/L
2.0
1
08/18/14 23:45
100-41-4
ND ug/L
2.0
1
08/18/14 23:45
75-09-2
ND ug/L
2.0
1
08/18/14 23:45
79-34-5
ND ug/L
2.0
1
08/18/14 23:45
127-18-4
ND ug/L
2.0
1
08/18/14 23;45
108-88-3
ND ug/L
2.0
1
06/18/14 23:45
71-55-6
ND ug/L
2.0
1
08/16/14 23;45
79-00-5
ND ug1L
2.0
1
08/18/14 23:45
79-01-6
ND ug1L
2.0
1
08/18/14 23:45
75-69-4
ND ug/L
2.0
1
08/18/14 23:45
75-01-4
100 %
70.130
1
08/18/14 23;45
460-00-4
100 %
70.130
1
08/18114 23:45
2037-26-5
103 %
70-130
1
08/18/14 23:45
17060-07-0
Analytical Method: 5M 2540D
11.9 mg/L
5.2 1
REPORT OF LABORATORY ANALYSIS
08/13/14 12:16
Date: 08/19/2014 06:14 PM
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ir
N1�
Page 10 of 2`/

aoAnalytical
www.p&oeJab&=n
QUALITY CONTROL DATA
Project: August 2014 818
Pace Project No.: 92212683
QC Batch: GCSV118517 Analysis Method: EPA 1664B
OC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92212683001, 92212683002
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1261007 Matrix: Water
Associated Lab Samples: 92212683001, 92212683002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L ND 5.0 08/11/14 10:33
LABORATORY CONTROL SAMPLE: 1261008
Spike LCS LCS % Rec
Parameter Units Cone, Result % Rec Limits Qualifiers
Oil and Grease mg/L 40 38.0 95 78-114
MATRIX SPIKE SAMPLE: 1261009
92212701002 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Oil and Grease mg1L ND 40 39.7 99 78-114
Results presented on this page are in the units indicated by the 'units" column except where an alternate unit is presented to the right of the result.
.` REPORT OF LABORATORY ANALYSIS
3
This report shall not be reproduced, except in full,
Date 08/19/2014 06:14 PM hour the written consent of Pace Analytical Services, Inc.. Page 11 of 27

aceAnalytical
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Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: August 2014 818
Pace Project No.: 92212683
QC Batch: MPRP116639
QC Batch Method: EPA200.7
Associated Lab Samples: 92212683001, 92212683002
METHOD BLANK: 1260763
Associated Lab Samples: 92212683001, 92212683002
Parameter Units
Copper ug1L
Lead uglL
Zinc ug1L
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 08/11/1418:35
ND 5-0 08/11/1418:35
ND 10-0 08/1111418:35
LABORATORY CONTROL SAMPLE:
1260764
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Copper
uglL
500
488 98 85-115
Lead
uglL
500
496 99 85-115
Zinc
uglL
S00
486 97 85-115
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
1260765
1260766
MS
MSD
92212055014
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Capper
ugfL
30.9
500
500
514
530
97
100
70.130
3
Lead
ug1L
ND
500
500
466
479
93
95
70-130
3
Zinc
ug1L
52.7
500
500
527
539
95
97
70-130
2
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
1260767
1260768
MS
MSD
92212701002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper
uglL
ND
500
500
488
478
98
96
70-130
2
Lead
uglL
ND
500
S00
492
493
98
99
70-130
0
Zinc
uglL
206
500
500
682
701
95
99
70-130
3
1
Results presented on this page are in the units indicated by the 'Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
A
This report shall not be reproduced, except in full,
n;
Date: 08/19/2014 06:14 PM without the written consent of Pace Analytical Services, II Page 12 of 27

aceAnalXical
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Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: August 2014 8/8
Pace Project No.: 92212683
QC Batch: MSV127985
QC Batch Method: EPA 624
Associated Lab Samples: 92212683001, 92212683002
Analysis Method: EPA624
Analysis Description: 624 MSV
METHOD BLANK: 1265998
Matrix: Water
Associated Lab Samples: 92212683001, 92212683002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,1,1-Trichlofoethane
ug/L
ND
2.0
08118/1411:15
1.1,2,2-Tetrachloroethane
ug/L
ND
2.0
0811811411:15
1.1,2-Trichloroethane
ug/L
ND
2.0
0811811411:15
1,1-Dichloroethane
uglL
ND
2.0
08/18/1411:15
1,1-Dichloroethene
ug/L
NO
2.0
08J18/1411:15
1,2-Dichlorobenzene
ug/L
NO
2.0
08/18/14 11:15
1,2-Dichloroethane
ug/L
NO
2.0
08/1811411:15
1,2-Dichloropropane
ug/L
NO
2.0
08/1811411:15
1,3-Dichlorobenzene
ug/L
ND
2.0
08/1811411:15
1,4-Dichlorobenzene
ug/L
ND
2.0
08/18/1411:15
Benzene
ug1L
ND
2.0
08/18M411:15
Bromod ichlorometha n e
ug/L
NO
2.0
08/18/14 11:15
Bromoform
ug/L
ND
2.0
08/18/14 11:15
Bromomethane
ug1L
ND
2.0
0811811411:15
Carbon tetrachloride
ug/L
NO
2.0
08/18/14 11:15
Chlorobenzene
ug/L
NO
2.0
08/1811411:15
Chloroethane
ug/L
NO
2.0
0811811411:15
Chloroform
uglL
NO
2.0
0811811411:15
Chloromethane
ug/L
NO
2.0
0811811411:15
cis-1,2-Dichloroethene
ug/L
NO
2.0
08/1811411:15
cis-1,3-Dichloropropene
ugfL
NO
2.0
08118I1411:15
Dibromochforomethane
ug/L
ND
2.0
0811811411:15
Ethylbenzene
ug/L
ND
2.0
08118/1411:15
Methylene Chloride
ug/L
ND
2.0
08/18/14 11:15
Tetra ch loroeth ene
ug/L
ND
2.0
08/18/14 11:15
Toluene
ug/L
ND
2.0
08/18/14 11:15
trans-1,2-Dichloroethene
ug/L
ND
2.0
08/18/14 11:15
trans- 1, 3-Dichloropropene
ug/L
ND
2.0
08/18/14 11:15
Trichloroethene
ug/L
ND
2.0
08/18/14 11:15
Trichlorofluoromethane
ug/L
ND
2.0
08/1811411:15
Vinyl chloride
ug/L
ND
2.0
08/18/14 11:15
1,2-Dichloroethane-d4 (S)
%
103
70-130
08/18/14 11:15
4-Bromofluorobenzene (S)
%
105
70-130
08/18/14 11:15
Toluene-d8 (S)
%
99
70-130
08/18/14 11:15
Qualifiers
LABORATORY CONTROL SAMPLE: 1265999
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 16.7 83 52-162
1,1,2,2-Tetrachloroethene ug/L 20 19.6 98 46-157
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
1 REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Da a 08/1912014 06:14 PM bout the written consent of Pace Analytical Services, Inc.
Page 13 of 27

aceAnalytical
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Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: August 2014 8/8
Pace Project No., 92212683
LABORATORY CONTROL SAMPLE:
Parameter
1265999
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,12-Trichloroethane
ug/L
20
18.5
93
52-150
1,1-Dichloroethane
ug/L
20
17.0
85
59-155
1,1-Dichloroethene
ug/L
20
17.4
87
1-234
1,2-Dichlorobenzene
ug/L
20
20.3
101
18-190
1,2-Dichloroethane
ug/L
20
17.8
89
49-155
1,2-Dichloropropane
ug/L
20
19.3
96
1-210
1,3-Dichlorobenzene
ug/L
20
20.2
101
59-156
1,4-Dichlorobenzene
ugtL
20
19.9
100
18-190
Benzene
ug/L
20
19.2
96
37-151
Bromodiohloromethane
ug/L
20
19.9
100
35-155
Bromoform
ug/L
20
20.2
101
45-169
Bromomethane
ug/L
20
13.6
58
1.242
Carbon tetrachloride
ug/L
20
16.8
84
70-140
Chlorobenzene
ug/L
20
19.8
99
37-160
Chloroethane
ug/L
20
14.4
72
14-230
Chloroform
ug/L
20
20.2
101
51-138
Chloromethane
ug/L
20
14.7
74
1-273
cis-1,2-Dichloroathene
ug/L
20
19.7
98
68-146
cis-1,3-Dichloropropene
ug/L
20
19.0
95
1-227
Dibromochloromethane
ug/L
20
21.2
106
53-149
Ethylbenzene
ug/L
20
20.3
102
37-162
Methylene Chloride
ug/L
20
16.7
83
1-221
Telrachloroethene
ug/L
20
19.8
99
64-148
Toluene
ugiL
20
19.0
95
47-150
trans-1,2-Dichloroethene
ug/L
20
19.8
99
54-156
trans-1,3-Dichloropropene
ug/L
20
19.4
97
17-183
Trichioroethene
uglL
20
18.7
94
71-157
TrichloroHuoromethane
ug/L
20
14.7
73
17-181
Vinyl chloride
ug/L
20
14.1
70
1-251
1,2-Dichloroethane-d4 (S)
%
103
70-130
4-Bromofluorobenzene (S)
%
107
70-130
Toluene -dB (S)
%
98
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1266000
1266001
MS
MSD
92212869001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
50
50
52.5
50.3
105
101
46-171
4
1,1,2,2-Tetrachloroethane
ug/L
ND
50
50
53.9
50.9
108
102
73-159
6
1,12-Trichloroethane
ug/L
ND
50
50
56.0
52.4
112
105
64-152
7
1,1-Dichloroethane
ug/L
ND
50
50
52.2
48.7
104
97
43-172
7
1,1-Dichloroethene
ug/L -
ND
50
50
58.4
55.8
117
112
48-189
4
1,2-Dichlorobenzene
ug/L
ND
50
50
54.8
52.2
110
104
54-154
5
1,2-Dichloroethane
ug/L
ND
50
50
52.3
48.0
105
96
42-171
9
1,2-Dichioropropane
uglL
ND
50
50
57.6
54.0
115
108
55-157
6
Results presented on this page are in the units indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
A
This report shall not be reproduced, except in full, [
n.
Date: 08/19/2014 06:14 PM without the written consent of Pace Analytical Services, Ir Page 14 of 27
r

acmnalytical
mww.patMlabs.00m
QUALITY CONTROL DATA
Project: August 2014 8/8
Pace Project No.: 92212683
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1266000
1266001
MS
MSD
92212869001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,3-Dichlorobenzene
ug/L
ND
50
50
53.7
51.7
107
103
57-148
4
1,4-Dichlorobenzene
ug/L
ND
50
50
55.0
52.0
110
104
58-149
6
Benzene
ug/L
ND
50
50
56.7
54.5
113
109
54-163
4
Bromodichioromethane
ug/L
ND
50
50
61.1
55.9
122
112
56-152
9
Bromoform
ug/L
ND
50
50
56.7
53.8
113
108
53-151
5
Bromomethane
ug/L
ND
50
50
67.5
44.7
135
89
10-200
41 MO,R1
Carbon tetrachloride
ug/L
ND
50
50
55.2
51.9
110
104
41-175
6
Chlorobenzene
ug/L
ND
50
50
54.4
51.8
109
104
67-152
5
Chloroethane
ug/L
ND
50
5o
51.4
37.9
103
.76
23-200
30
Chloroform
ug/L
ND
50
50
61.6
57.1
123
114
51-166
8
Chloromethane
ug/L
ND
50
50
55.8
52.5
112
105
40-175
6
cis-1,2-Dichioroethene
ug/L
ND
50
50
59.7
56.0
119
112
45-174
6
cis-1,3-Dichloropropene
ug/L
ND
50
50
60.5
57.2
121
114
38-146
6
Dibromochloromethene
ug/L
ND
50
50
62.2
58.9
124
118
65-144
6
Ethylbenzene
ug/L
ND
50
50
57.7
55.0
115
110
57-152
5
Methylene Chloride
ug/L
ND
50
50
48.8
45.4
97
90
40-167
7
Tetrachloroethene
ug/L
ND
50
50
56.9
56.1
114
112
59-155
1
Toluene
ug/L
ND
50
50
56.5
53.1
113
106
47-162
6
trans-1,2-Dichloroethene
ug/L
ND
50
50
60.6
56.7
121
113
47-178
7
trans-1,3-Dichloropropene
ug/L
ND
50
50
59.4
55.6
119
111
39-148
7
Trichloroethene
uglL
ND
50
50
55.7
52.4
111
105
60-153
6
Trichlorofluoromethene
ug/L
ND
50
50
53.3
52.3
107
105
42-199
2
Vinyl chloride
ug/L
ND
50
50
55.9
52.0
112
104
46-176
7
1,2-Dichloroethane-d4 (S)
%
102
98
70-130
4-Bromofluorobenzene (S)
%
102
103
70-130
Toluene-d8 (S)
%e
102
102
70-130
Results presented on this page are in the units indicated 4y the "Units" column except where an alternate unit is presented to the right or the result.
�.� REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Datteej,08/19/2014 06:14 PM hour the written consent of Pace Analytical Services, Inc.
Page 15 of 27

aceAnalytical
www.pecelahs.am
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: August 2014 818
Pace Project No.: 92212683
QC Batch: OEXT129347 Analysis Method: EPA608
QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB
Associated Lab Samples: 92212683001, 92212683002
METHOD BLANK: 1261407 Matrix: Water
Associated Lab Samples: 92212683001, 92212683002
Parameter
Units
Blank
Result
4.4'-DDD
ug/L
NO
4,4'-DDE
ug/L
NO
4,4'-DDT
ug/L
NO
Aldrin
ug/L
NO
alpha-BHC
U91L
NO
beta-BHC
ug/L
NO
Chlordane (Technical)
ug/L
NO
delta-BHC
ug/L
ND
Dieldrin
ug/L
ND
Endosulfan i
ug/L
ND
Endosulfan II
ug/L
ND
Endosulfan sulfate
ug/L
ND
Endrin
ug/L
NO
Endrin aldehyde
ug/L
ND
gamma-BHC (Lindane)
ug/L
ND
Heptachlor
ug/L
ND
Heptachlor epoxide
ug/L
NO
PCB-1016 (Aroclor 1016)
ug/L
NO
PCB-1221 (Aroclor 1221)
ugiL
NO
PCB-1232 (Aroclor 1232)
ugiL
ND
PCB-1242 (Aroclor 1242)
ug/L
ND
PCB-1248 (Aroclor 1248)
ug/L
NO
PCB-1254 (Aroclor 1254)
ug/L
NO
PCB-1260 (Aroclor 1260)
ug/L
ND
Toxaphene
ug/L
ND
Decachlorobiphenyl (S)
%
85
Tetrachloro-m-xylene (S)
%
67
Reporting
Limit
Analyzed Qualifiers
0.050
08/13/1418:49
0.050
08t1311418:49
0.050
08/1311418:49
0,050
08/13/1418:49
0.050
08113/1418:49
0.050
08113/1418:49
0.50
08113/1418:49
0.050
08113/1418:49
0.050
08113/1418:49
0.050
08/13/1418:49
0.050
08/13/1418:49
0.050
08/13/1418:49
0.050
08/13/14.18:49
0.050
08/13/1418:49
0.050
08/13/1418:49
0.050
08/1311418:49
0.050
08/13/14 18:49
0.50
08113/1418:49
0.50
08/13/14 18:49
0.50
08113/1418:49
0.50
08/1311418.49
0,50
08/1311418:49
0.50
08/13114 18:49
0.50
08/13/1418:49
0.50
08/1311418:49
20-138
08/13/1418:49
20-110
08/13/1418:49
LABORATORY CONTROL SAMPLE:
1261408
Spike
LCS
LCS
% Ree
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
4,4'-ODD
ug/L
.25
0.21
84
31-141
4,4'-DDE
ug/L
.25
0.20
80
30-145
4,4'-DOT
ug/L
.25
0.21
86
25-160
Aldrin
ug/L
.25
0.14
55
42-122
alpha-BHC
ug/L
.25
0.20
82
37-134
beta-BHC
ug/L
.25
0.21
86
17-147
delta-BHC
ug/L
.25
0.23
94
19-140
Dieldrin
ug/L
.25
0.20
83
36-146
Endosulfan I
ugiL
'25
0.20
83
45-153
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 08/19/2014 06:14 PM without the written consent of Pace Analytical Services, I
Page 16 r4 27

aceAnalytical
tnvw.pacetabs.com
i(
QUALITY CONTROL DATA
Project: August 2014 8/8
Pace Project No.: 92212683
LABORATORY CONTROL SAMPLE:
Parameter
1261408
Units
Spike
Conc.
LCS LCS
Result % Rec
Endosulfan 11
ug/L
.25
0.23
Endosulfan sulfate
ug/L
.25
0.24
Endrin
ug/L
.25
0.22
Endrin aldehyde
ug/L
.25
0.19
gamma-BHC (Lindane)
ug/L
.25
0.20
Heptachlor
ug/L
.25
0.16
Heptachlor epoxide
ug/L
.25
0.19
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1261409
MS
Parameter
4,4'-DDD
4,4'-DDE
4,4'-DDT
Aldrin
alpha-BHC
beta-BHC
delta-BHC
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
92211859001 Spike
Units
Result Conc.
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
NO
ug1L
NO
ug1L
NO
ug1L
NO
ug/L
ND
ug1L
ND
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
% Rec
Limits
92 1-202
96 26-144
87 30-147
75 50-150
82 32-127
65 34-111
79 41-126
94 20-138
78 20-110
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
1261410
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
.5 .5
0.54
0.54
109
109
31-141
0
.5 .5
0.53
0.51
107
103
30-145
3
.5 .5
0.51
0.51
103
102
25-160
1
.5 .5
0.42
0.39
84
79
42-122
5
.5 .5
0.41
0A0
83
80
37-134
3
.5 .5
0.62
0.59
124
119
17-147
5
.5 .5
0.48
0.46
97
92
19-140
5
.5 .5
0,48
0.45
96
91
36-146
5
.5 .5
0.51
0.48
103
97
45-153
6
.5 .5
0.57
0.55
115
111
1-202
3
.5 .5
0.52
0.50
104
100
26-144
4
.5 .5
0.54
0.51
109
103
30-147
6
.5 .5
0.45
0.45
91
90
50-150
1
.5 .5
0.48
0.48
98
97
32-127
1
.5 .5
0.43
0.40
87
82
34-111
6
.5 .5
0.48
0.46
98
93
41-126
5
94
87
20-138
236
222
20-110
S5
Resutts presented on this page are in the units indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
� This report shall not be reproduced, except in full,
Date3 08/1912014 06:14 PM hout the written consent of Pace Analytical Services, Inc..
4
Qual
Page 17 of 27

ace Analytical
www.pscelabxcom
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: August 2014 8/8
Pace Project No.: 92212683
QC Batch: OEXT/29328 Analysis Method: EPA625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92212683001, 92212683002
METHOD BLANK: 1260959
Associated Lab Samples: 92212683001, 92212683002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
08/12/14 08:33
2,4,6-Trichlorophenol
ug/L
ND
10.0
08/12/14 08:33
2,4-Dichlorophenol
ug/L
ND
5.0
08/12/14 08:33
2,4-Di methyl phenol
ug/L
ND
10.0
08/12/14 08:33
2,4-Dinitrophenol
ug/L
ND
50.0
08/12/14 08:33
2,4-Dinitrotoluene
ug/L
ND
5.0
08/12/14 08:33
2,6-Dinitrotoluene
ug1L
ND
5.0
08/12/14 08:33
2-Chloronaphthalene
ug/L
ND
5.0
08/12/14 08:33
2-Chlorophenol
ug/L
NO
5.0
08/12/14 08:33
2-Nitrophenol
ug/L
NO
5.0
08/12/14 08:33
3,3'-Dichiorobenzidine
ug/L
NO
25.0
08/12/14 08:33
4,6- Din itro-2-methylphenol
ug1L
NO
20.0
08/12/14 08:33
4-Bromophenylphenyl ether
ug1L
NO
5.0
08/12/14 08:33
4-Chloro-3-methylphenol
uglL
NO
5.0
08/12/14 08:33
4-Chlorophenylphenyl ether
ug1L
NO
5.0
08/12/14 08:33
4-Nitrophenol
ug/L
NO
50.0
08/12/14 08:33
Acenaphthene
ug/L
NO
5.0
08/12/14 08:33
Acenaphthylene
uglL
NO
5.0
08/12/14 08:33
Anthracene
uglL
NO
5.0
08/12/14 08:33
Benzo(a)anthrecene
uglL
ND
5.0
08/12/14 08:33
Benzo(a)pyrene
ug/L
NO
5.0
08/12/14 08:33
Benzo(b)fluoranthen e
uglL
NO
5.0
08/12/14 08:33
Benzo(g,h,i)perylene
ug/L
NO
5.0
08/12/14 08:33
Benzo(k)fluoranthene
ug/L
ND
5.0
08/12/14 08:33
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
08/12/14 08:33
bis(2-Chloroethyl) ether
ug/L
ND
5.0
08/12/14 08:33
bis(2-Chloroisopropyl) ether
ug/L
ND
5.0
08/12/14 08:33
bis(2- Ethyl hexyl)phthalate
ug/L
ND
5.0
08/12/14 08:33
Butyibenzylphthalate
ug/L
NO
5.0
08/12/14 08:33
Chrysene
ug/L
NO
5.0
08/12/14 08:33
Di-n-butylphthalate
ug1L
NO
5.0
08/12/14 08:33
Di-n-octylp htha late
ug/L
NO
5.0
08/12/14 08:33
Dibenz(a,h)anthracene
ug/L
ND
5.0
08/12/14 08:33
Diethylphtha late
ug/L
NO
5.0
08/12/14 08:33
Dim ethylphtha late
ug/L
NO
5.0
08/12/14 08:33
Fluoranthene
ug/L
NO
5.0
08/12/14 08:33
Fluorene
ug/L
NO
5.0
08/12/14 08:33
Hexachloro-1,3-butadiene
ug/L
NO
5.0
08/12/14 08:33
Hexachlorobenzene
ug/L
NO
5.0
08/12/14 08:33
Hexachlorocyclopentadiene
ug/L
ND
10.0
08/12/14 08:33
Hexachloroethane
ug/L
NO
5.0
08/12/14 08:33
Qualifiers
Results presented on this page are in the units Indicated by the -Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Date: 08/19/2014 06:14 PM
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ii
Page 18 V27

aceAnalytrcal
Ww.Paceiabs.cW
QUALITY CONTROL DATA
Project: August 2014 818
Pace Project No.: 92212683
METHOD BLANK: 1260959
Associated Lab Samples: 92212683001, 92212683002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed Qualifiers
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
08/12/14 08:33
Isophorone
ug/L
ND
10.0
08/12/14 08:33
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
08/12/14 08:33
N-Nitrosodimethylamine
ug/L
ND
5.0
08/12/14 08:33
N-Nitrosodiphenylamine
ug/L
ND
10.0
08/12/14 08:33
Naphthalene
ug/L
ND
5.0
08112/14 08:33
Nitrobenzene
ug/L
ND
5.0
08112/14 08:33
Pentachlorophenol
ug/L
ND
10.0
08112/14 08:33
Phenanthrene
ug1L
ND
5.0
08/12/14 08:33
Phenol
ug/L
ND
5.0
08/12114 08:33
Pyrene
ug/L
ND
5.0
08/12/14 0&33
2,4, 6-Tribromo phenol (S)
%
49
10-137
08/12/14 08:33
2-Fluorobiphenyl (S)
%
49
15-120
08/12/14 08.33
2-Fluorophenol (S)
%
25
10-120
08/12/14 08:33
Nitrobenzene-d5 (S)
%
48
10-120
08/12/14 08:33
Phenol-d6 (S)
%
18
10-120
08/12/14 08:33
Terphenyl-d14 (S)
%
69
11-131
08/12/14 08:33
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1260960
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
24.1
48
44-142
2.4,6-Trichlorophenol
ug/L
50
26.0
52
37-144
2,4-Dichlorophenol
ug/L
50
26.2
52
1-191
2,4-Dimethylphenol
ug/L
50
28.8
58
32-119
2,4-Dinitrophenol
ug/L
250
153
61
1-181
2,4-Dinitrotoluene
ug/L
50
34.0
68
39-139
2,6-Dinitrotoluene
ug1L
50
31.2
62
50-158
2-Chloronaphthalene
ug/L
50
26.0
52
60-118 L2
2-Chlorophenol
ug/L
50
24.3
49
23-134
2-Nitrophenol
ug/L
50
27.3
55
29-182
3,3'-Dichlorobenzidine
ug/L
100
62.6
63
1-262
4,6-Dinitro-2-methylphanol
ug/L
100
69.4
69
1-181
4-Bromophenylphenyl ether
ug/L
50
30.5
61
53-127
4-Chloro-3-methylphenol
ug/L
100
57.2
57
22-147
4-Chlorophenylphenyl ether
ug/L
50
30.9
fit
25-158
4-Nitrophenol
ug/L
250
77.2
31
1-132
Acenaphthene
ug/L
50
28.5
57
47-145
Acenaphihylene
ug/L
50
28-3
57
33-145
Anthracene
ug/L
50
31-3
63
1-166
Benzo(a)anthracene
ug/L
50
30-4
61
33-143
Benzo(a)pyrene
ug/L
50
29.0
58
17-163
Benzo(b)fluoranthene
ug/L
50
28.9
58
24-159
Benzo(g,h,i)perylene
ug/L
50
27.3
55
1-219
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date{ 05/19/2014 06:14 PM hout the written consent of Pace Analytical Services, Inc. Page 19 of 27

aceAnalytical
»ww.pacttleb&=n
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: August 2014 8/8
Pace Project No.: 92212683
LABORATORY CONTROL SAMPLE:
Parameter
1260960
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
Benzo(k)fluoranthene
ug/L
50
28.8
58
11-162
bis(2-Chloroethoxy)methane
ug/L
50
26.5
53
33-184
bis(2-Chloroethyl) ether
ug1L
50
25.6
51
12-158
bis(2-Chloroisopropyl) ether
ug/L
50
25.4
51
36-166
bis(2-Ethylhexyl)phthelate
ug/L
50
32.5
65
&158
Butylbenzylphthalate
ugIL
50
33.2
66
1-152
Chrysene
ug/L
50
30.5
fit
17-168
Dl-n-butylphthaiate
ug/L
50
322
64
1-118
Di-n-octylphthalale
ug/L
50
29.6
59
4-146
Dibenz(a,h)anthracene
ug/L
50
28.0
56
1-227
Diethylphthatate
ug/L
50
32.8
66
1-114
Dimethylphthalate
ug/L
50
32.3
65
1-112
Fluoranthene
ug/L
50
31.5
63
26-137
Fluorene
ug/L
50
31.1
62
59-121
Hexachloro-1,3-butadiene
ug/L
50
23.9
48
24-116
Hexachlorobenzene
ug/L
50
29.0
58
1-152
Hexachlorocydopentadiene
ug/L
50
24.5
49
25-150
Hexachloroethane
ug/L
50
21.5
43
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
22.0
44
1-171
Isophorone
ug/L
50
27.6
55
21-196
N-Nitroso-di-n-propylamine
ug/L
50
27.5
55
1-230
N-Nitrosodim ethyla mine
ug/L
50
16.9
34
25-150
N-Nitrosodiphenylamine
ug/L
50
30.6
61
25-150
Naphthalene
ug/L
50
25.8
52
21-133
Nitrobenzene
ug/L
50
28.1
56
35-180
Pentachlorophenol
ug/L
100
59.5
59
14-176
Phenanthrene
ug/L
50
30.1
60
54-120
Phenol
ug/L
50
124
25
5-112
Pyrene
ug/L
50
32.9
66
52-115
2,4,6-Tribromophenol (S)
%
65
1D-137
2-Fluorobiphenyl (S)
%
54
15-120
2-Fluorophenol(S)
%
28
10-120
Nitrobenzene-d5(S)
%
55
10-120
Phenol-d6 (S)
%
21
10-120
Terphenyl-d14 (S)
%
68
11-131
(qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1260961
1260962
MS
MSD
92212724001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone,
Conc,
Result
Result
% Rec
% Rec
Limits
RP❑ Qual
1,2,4-Trichlorobenzene
ug/L
ND
100
100
66.9
67.3
67
67
44-142
1
2,4,6-Trichlorophenol
ug/L
ND
100
100
70.4
75.2
70
75
37-144
7
2,4-Dichlorophenol
uglL
ND
100
100
76.3
75.7
76
76
1-191
1
2,4-Dimethylphenol
uglL
ND
100
100
75.6
77.0
76
77
32-119
2
2,4-Dinitrophenol
ug/L
ND
500
500
382
396
76
79
1-181
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Date: 08/19/2014 06:14 PM
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, h
Page 20 if 27

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville. NC 28078
[phone]
QUALITY CONTROL DATA
Project: August 2014 818
Pace Project No.: 92212683
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1260961
1260962
MS
MSD
92212724001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
2,4-Dinitrotoluene
ug1L
ND
100
100
83.4
96.2
83
96
39-139
14
2,6-Dinitrotoluene
ug/L
ND
100
100
79.6
88.0
80
88
50-158
10
2-Chloronaphthalene
ug1L
ND
100
100
68.9
71.0
69
71
60-118
3
2-Chlorophenoi
ug1L
ND
100
100
70.9
70.3
71
70
23-134
1
2-Nitrophenol
ug/L
ND
100
100
73.6
76.3
74
76
29-182
4
3,3'-Dichlorobenzidine
ug/L
ND
200
200
151
173
75
87
1-262
14
4,6-Dinitro-2-methyl phenol
ug/L
ND
200
200
159
178
80
89
1-181
11
4-Bromophenylphenyl ether
ug/L
ND
100
100
74.3
82.4
74
82
53-127
10
4-Chloro-3-methylphenoi
ug/L
ND
200
200
170
173
85
86
22-147
2
4-Chlorophenylphenyl ether
ug/L
ND
100
100
80.0
85.1
80
85
25-158
6
4-Nitrophenol
ug/L
ND
500
500
291
318
58
64
1-132
9
Acenaphthene
ug/L
ND
100
100
74.9
76.9
75
77
47-145
3
Acenaphthylene
ug/L
ND
100
100
74.5
77.1
75
77
33-145
3
Anthracene
ug/L
ND
100
100
73.8
84.6
74
85
1-166
14
Benzo(a)anthracene
ug/L
ND
100
100
69.4
79.7
69
80
33-143
14
Benzo(a)pyrene
ug/L
ND
100
100
67.7
77.5
fib
78
17-163
13
Benzo(b)fluoranthene
ug/L
ND
100
100
65.5
80.4
65
80
24-159
21
Benzo(g,h,i)perylene
ug/L
ND
100
100
64.4
73.2
64
73
1-219
13
Benzo(k)fluoran then e
ug/L
ND
100
100
66.7
71.2
67
71
11-162
6
bis(2-Chloroethoxy)methane
ug/L
ND
100
100
71.9
73.5
72
73
33-184
2
bis(2-Chloroethyl) ether
ug/L
ND
100
100
74.2
75.6
74
76
12-158
2
bis(2-Chloroisopropyl) ether
ug/L
ND
100
100
71.0
70.0
71
70
36-166
1
bis(2-Ethylhexyl)phthalate
ug/L
ND
100
100
79.0
91.6
79
92
8-158
15
Butylbenzylphthalate
ug/L
ND
100
100
78.3
93.2
78
93
1-152
17
Chrysene
ug/L
ND
100
100
69.4
79.4
69
79
17-168
13
Di-n-butylphthalate
ug1L
ND
100
100
82.2
95.5'
82
96
1-118
15
Di-n-octylphthalate
ug/L
ND
100
100
77.5
89.6
78
90
4-146
15
Dibenz(a,h)anthracene
ug1L
ND
100
100
67.3
75.0
67
75
1-227
11
Diethylphtha late
ug/L
ND
100
100
83.9
95.5
84
95
1-114
13
Dimethylphthalate
ug/L
ND
100
100
80.7
90.5
81
90
1-112
11
Fluoranthene
ugIL
ND
100
100
81.5
91.3
81
91
26-137
11
Fluorene
ug/L
ND
100
100
80.2
86.7
80
87
59-121
8
Hexachloro-1,3-butadiene
ug/L
ND
100
100
68.5
69.4
68
69
24-116
1
Hexachlorobenzene
ug/L
ND
100
100
69.3
76.9
69
77
1-152
10
Hexachlorocyclopenladiene
ug/L
ND
100
100
60.4
60.0
60
60
25-150
1
Hexachloroethane
ug/L
ND
100
100
63.0
63.6
63
64
40-113
1
Indeno(1,2,3-cd)pyrene
ug/L
ND
100
100
53.3
60.5
53
60
1-171
13
Isophorone
ug/L
ND
100
100
75.6
75.0
76
75
21-196
1
N-Nitroso-di-n-propylamine
ug/L
ND
100
100
80.0
78.9
80
79
1-230
1
N-Nitrosodimethylamine
ug/L
ND
'100
100
51.4
52.9
51
53
25-150
3
N-Nitrosodiphenylamine
ug/L
ND
100
100
72.5
81.2
73
81
25-150
11
Naphthalene
ug/L
ND
100
100
71.4
70.4
71
70
21-133
1
Nitrobenzene
ug/L
ND
100
100
71.8
71.5
72
72
35-180
0
Pentachlorophenol
ug/L
ND
200
200
143
151
72
75
14-176
5
Phenanthrene
ug/L
ND
100
100
72.0
81.9
72
82
54-120
13
Phenol
ug/L
ND
100
100
50.9
50.8
51
51
5-112
0
Results presented on this page are in
the units indicated
by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This
report shall
not be reproduced, except in full,
Datee08119/2014 06:14 PM
bout the written consent of Pace Analytical Services, Inc..
Page 21 of 27

aceAnalytical
*W,P4celaha,=n
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: August 2014 818
Pace Project No.; 92212683
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1260961
1260962
MS
MSD
92212724001 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
Pyrene
ug1L ND 100
100
70.5
84.7 70
85
52-115 18
2,4,6-Tribromophenol (S)
%
78
85
10-137
2-Fluorabiphenyl (S)
%
70
71
15-120
2-Fluoraphenal(S)
%
49
50
10-120
Nitrobenzene-d5(S)
%
71
70
10-120
Phenol-d6 (S)
%
42
43
10-120
Terphenyl-d14 (S)
%
73
86
11-131
Results presented on this page are in the units Indicated by the *Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
r
This report shall not be reproduced, except in full, l
Date: 08/19/2014 06:14 PM without the written consent of Pace Analytical Services, Ir Page 22 -f 27

aceAnalytical
w",,pacdab&WM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
ltuntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: August 2014 8/8
Pace Project No.: 92212683
QC Batch: WET132619 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92212683001, 92212683002
METHOD BLANK: 1262641 Matrix: Water
Associated Lab Samples: 92212683001, 92212683002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL NO 2.5 08/13114 12:11
LABORATORY CONTROL SAMPLE: 1262642
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 260 104 90-110
SAMPLE DUPLICATE: 1262781
92212673003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 7.6 7.6 0
SAMPLE DUPLICATE: 1262782
92212683002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 11.9 13.1 10
Results Presented an this page are in the units Indicated by the "Unite" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
A This report shall not be reproduced, except in full,
Date; 08/19/2014 06A4 PM hout the written consent of Pace Analytical Services, Inc. Page 23 of 27
i

,�acmnalyticalo
ksw pecambs.=
QUALIFIERS
Project: August 2014 818
Pace Project No., 92212683
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kirtcey Ave. Suite 100
Huntersvilte, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-0pheny1hydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values_
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration. '
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MD Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
REPORT OF LABORATORY ANALYSIS
(704 )875-9092
Date: 08/19/2014 06-14 PM
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ir
1'
.a
Page 24 Gf 27

aceAnalytical
www.pacefebs.wn
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: August 2014 818
Pace Project No., 92212683
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92212683001
OUTFALL # i
EPA 16648
GCSV/18517
92212683002
OUTFALL # 2
EPA 1664B
GCSV/18517
92212683001
OUTFALL # 1
EPA 3510
OEXT/29347
EPA 608
92212683002
OUTFALL # 2
EPA 3510
0EXT129347
EPA 608
92212683001
OUTFALL # 1
EPA 200.7
MPRP/16639
EPA 200.7
92212683002
OUTFALL # 2
EPA 200.7
MPRP/16639
EPA 200.7
92212683001
OUTFALL # 1
EPA 625
OEXT/29328
EPA 625
92212683002
OUTFALL # 2
EPA 625
OEXT129328
EPA 625
92212683001
OUTFALL # 1
EPA 624
MSV/27985
92212683002
OUTFALL # 2
EPA 624
MSV/27985
92212683001
OUTFALL # 1
SM 2540D
WET/32619
92212683002
OUTFALL # 2
SM 2540D
WET/32619
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Datei .; 08/19/2014 06:14 PM :hout the written consent of Pace Analytical Services, Inc.
Analytical
Batch
GCSV/18547
GCSW18547
ICP/15021
ICP/15021
MSSV/9515
MSSW19515
Page 25 of 27

p., CHAIN -OF -CUSTODY 1 Analytical Request Document V4 1
�� FU Ia>� 1�a1 • The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
,., I ca
• - -
ar
Page: of m
Section A Section B Section C
Required Client Informattors- Requtred Project Information: Invoice Intormafion:
Company: Report To: Attention:
1787918
•� �� ��
Address:
Co To:
Copy
Cam Nam,
c '
REGULATURYAGEIVCY`:
yNPDES
Address:
r r GROUNDWATER r DRINKING WATER
r tJ$T j" RGRA r OTHER
Email To:
Purchase Order No.:
Pace Quote
>zetare�a:
Phone:
Fax:
Project Name:
Pace Proles
2
Manager
STATE.
Requested Due DatMTAT:
Project Number.
Paw Pmf➢e M
=.Re
-quested
Analysis
Fll_tered
(Y1N):.
::
-
-
'
Section D Matrix Codes
IiequUedGfarct inf9rmadOn MAC 1 CODE
' 9
¢
COLLECTED
Preservatives
~
'2'•
Drinking water DW
zz
Water WT
P:
-T
Waste Water WW
ProOMct P
COMPOSITE
ai'ART
COMPOSITE
EHOMaRAe
W.
_
Z
SOIVSalid SL
t7
SAMPLE ID oil WID
H
c
pe
(A-Z o-e a ;1 Air AR
a
x
a
Set le IDS MUST 3E UNIQUE Tissue TS
O
w
a
m
=:r�
\
U
Other OT
U
w
O
Z
m
n
o
'.ut
p
V
a
g
a
a
iL
tz
Y
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S
m
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`N
,_
4
ni
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DATE
TIME
DATE
TIME
z"
z
z
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2
!r Pace Project NoJab I.Ci.
J
`.p, —% 1
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--'- ADDETiONAL COMMENTS
4
. REvLINQlIl5tFE0 BY 1 AFFILIAiiON _' . `i••_;
;;. _,- DATE `-_,�
TIME -
- -,-ACCEVII ED BY f AFFILIATION
- A E
-TSH^IE-�-'
SAMPLE CONDITIONS
r
I(jr-g-liv
SAMPLER NAME'AND SIGNATURE
DORIGINALPRlNT
a
> �
n �
c
Z
ue _
m
Name otSAMPLER. /
c0a V
—
a
3 m
U
p �
DATE Signed
9
SIGNATURE of SAMPLER:
- .
iM"DlYYI:
ID
-Irr PW-L NOW By alrft this form yoe are araapb% Pace's NET 30 day payer terms and appredng to late cfierges of 1.5% per nwnth rot arty invoices not paid vdrun 3a days. / F-ALL."20rev.07. 15-Mav-2007

Document Name: Sample Condition Upon
Document Revised: June 10, 2014
aceAnaoical.
Receipt (SCUR)...
Page .1 of 2
Document No.:
Issuing Authorities:
F-ASV-CS-003-rev.14
Pace Asheville Quality Office
Client Nalme: ��.�
Courier (Clrcfe): Fed Ex UPS USP Commercial Pace
Custody Seal on Cooler/Box Present: 0 yes no Seals intact: ❑ yes
Packing Material: ❑ Bubble Wrap ubble Bags ❑ :None ❑ Other
Thar ometer Used: IR Gun*3-130265263 Type of Ice: limit Blue None
IR n SN-140290365 Other: �lfJ
Te Correction Factor: Add / Subtract ~` C
Other
no
Samples on- Ice, cooling process has begun
Corrected (Cooler Temp.: C
Biologi
issue is Frozen: Yes No Aj
Date and Ini a o on ining
Temp should be above freezing to we
Comments:
contents:
Chain of Custody Present:
No
❑NIA
1.
Chain of Custody Filled Out:
DIVO.N.
❑NIA
2.
Chain of Custody Relinquished:
Y o
❑N/A
3.
Sampler Name $ S" nature on COG:
y ❑No
(-)NIA
4.
Samples Arrived within Hold Time:,
2fYW ❑NO
NIA
5.
Short Hold Time Analysis -�72hr :
Dyes VNI,16NIA
6. .
Rush Turn Around Time Requested:
❑Ye No
❑NIA
7.
Sufficient Volume:
dyewdNo, ❑NIA
8.
Correct Containers Used`
No
ny
❑NIA
9.
-Pace Containers Used:
ON.
❑NIA
Containers Intact:
VIYes ONO
ON/
10.
Filtered volume received for Dissolved tests
❑Y ❑No
EAM
11.
Sample Labels match COC:
VfYes ❑No
❑NIA
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
No
❑NIA
13.
AEI containers needing preservation are found to be in
7.'sNo
NIA
compliance with EPA recommendation.
exceptions: VOA, conform, TOC, O&G, WI-DRO (water)
❑Y o
Samples checked for dechlorination:
Yes ONO
DwL
14.
Headspace in VOA Vials ( >6mm):
Dyes ONa
/
5.
Trip Blank Present:
❑Yes ONO
N.
16.
Trip Blank Custody Seals Present
[Dyes ONo
NrA
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution: Field Data Required? Y . / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF
SRF Review: c� _ JDate: I �M-r
Note: Whenever there is a discrepancy affecting N rth Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( Le out of hold, incorrect
preservative, out of temp, incorrect containers)
Page 27 of 27

Semi-annual Stormwater Discharge Monitoring; Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _August 15, 2014
CERTIFICATE OF COVERAGE No. NCG030529
FACILITY NAME: Pentair Valves And Controls
COUNTY: Buncombe
PERSON COLLECTING- SAMPLES: Gerald Runkles
LABORATORY: Pace Analytical Lab Cert. #40
Comments on sample collection or analysis: See page 4,
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR �2014
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ® MonthW July (montht
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow []Water Supply ❑SA
®Other: Class C, 5wannanoa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -->
No discharge this period?2
Dutfall No.
Date Sample
Collected'
(mo/dd/yr)
24-Dour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks ==->
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
07-31-2014
0.18
33.1 mg/L
7.1
0.069 mg/L
0.0072
0.148 mg/L
<5.0 mg/L
BRL
2
07-31-2014
0.18
47.8 mg/L
7.2
0.0576 mg/L
0.0051
0.610 mg/L
<5.0 mg/L
BRL
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469,31).
Permit Date: 11/1/2012-10/31/2017 SWIJ-24S, last revised 10/25/2012
Page 1 of 4

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(170),1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Jason Stone
Name (Print name)
Plant Manager
Title (Print title)
r* �---- 8/15/2014
6Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX ma/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall Na.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks ===>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTIONS.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑
REGIONAL OFFICE CONTACT NAME: _ Laura Herbert, P.E.
Mail an original and one copy of this DMft, Including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
In the case of "No Discharge"_reports to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
" 1 Certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
of Permittee}
8/15/20
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 4

1) Zinc reporting value exceeds permit limit 0.067 for outfall #2
a) Finding;
i) Roofing material is galvanized metal could be a contributing factor for outfall # 1 and 42.
b) Corrective actions;
i) Reviewed BMP, ensured good management practices are being followed.
2) Copper reporting value exceeds permit limit 0.007 for outfall # l and #2
a) Finding;
i) Roofing material is metal could he a contributing factor for outfall #land #2.
ii) Scrap Lugger pad could be a contributing factor for outfall # l . We do not find potential sources of copper exposure in outfall #2.
b) Corrective actions;
i) Review of BMP's
ii) Have increased housekeeping, Lugger Pad Area and Center Pad are being inspected and cleaned after each use.
iii) Dump bins are cleaned off prior to being taken outside for dumping into luggers
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 4 of 4

e
aceAnalytical
www.pacelabs,c m
August 08, 2014
Gerald Runkles
Pentair Valves & Controls
953 Old US Hwy 70
Black Mountain, NC 28711
RE: Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )B75-9092
Dear Gerald Runkles:
Enclosed are the analytical results for sample(s) received by the laboratory on July 31, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNi standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
F
Enclosures
REPORT OF LABORATORY ANALYSIS
r
`9eORA�,
This report shall not be reproduced, except in full,
wit ie written consent of Pace Analytical Services, Inc..
Page 1 of 26

aceAnalytrcal
wwwPeceiabs.00m
Pace Analytical Services, Inc.
11
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
CERTIFICATIONS
Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification M 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification M 37712 VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Serv' 3c..
Page 2 of 26

0
aceAnalyti{cal
www.pacelabs.awn
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersvilfe, NC 28078
[phone]
Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
Lab Sample ID
Client Sample ID
Method
Parameters
92211506001
OUTFALL # 1
EPA 200.7
Copper
EPA 2001
Lead
EPA 200.7
Zinc
SM 2540D
Total Suspended Solids
92211506002
OUTFALL # 2
EPA 200.7
Copper
EPA 200.7
Lead
EPA 200.7
Zinc
SM 2540D
Total Suspended Solids
SUMMARY OF DETECTION
Result Units Report Limit Analyzed
69.6 ug1L
5.0
08/06/14 00:40
7.2 ug1L
5.0
08/06/14 00:40
148 ug1L
10.0
08/06/14 00:40
33.1 mg1L
3.6
0810511410:40
57.6 uglL
5.0
08/06/14 00:44
5.1 ug1L
5.0
08/06/14 00:44
610 ug/L
10.0
08/06/14 00:44
47.8 mg1L
2.5
08/05/14 10:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wi' he written consent of Pace Analytical Services, Inc..
Qualifiers
Page 4 of 26

aceAnalytical
www.pscelabsoan
Pace Analytical Services,,lnc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: JULY 2014 Samples 7131
Pace Project No.: 922115DB
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92211506001 OUTFALL # 1
92211506002 OUTFALL # 2
EPA 1664B
CLW
1
PASI-C
EPA608
RES
27
PASI-C
EPA200.7
SH1
3
PASI-A
EPA 625
Bpi
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MAB
1
PASI-A
EPA 1664E
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA200.7
SH1
3
PASI-A
EPA625
Bpi
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MAB
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Servi 1c.,
Page 3 of 26

0
aceAnalytical
wrrw.pacelab&=n
ANALYTICAL RESULTS
Project: JULY 2014 Samples 7/31
Pace Project No.: 92211506
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OUTFALL # 1 Lab ID: 92211506001 Collected: 07/31/14 00:00 Received: 07/31/14 15:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
608 GCS Pesticides and PCBs
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosultan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
200.7 MET ICP
Copper
Lead
Zinc
625 MSSV
Analytical Method: EPA 1664B
NO mg1L 5.0 1 08/0111417:23
Analytical Method: EPA 608 Preparation Method: EPA 3510
ND ug/L
0.050
1
08/01/14 16:35
08/07/14 00:15
309-00-2
ND ug/L
0.050
1
08/01/14 16:35
08/07/14 00:15
319-84-6
ND ug/L
0.050
1
08/01/14 16:35
08/07/14 00:15
319-85-7
ND ug/L
0.050
1
08/01/14 16:35
08/07/14 00:15
319-86-8
NO ug/L
0,050
1
08/01/14 16:35
08/07/14 0015
58-89-9
ND ug/L
0.50
1
08/01/14 16:35
08/07/14 0015
57-74-9
ND ug/L
0.050
1
08/01/14 16:35
08/07/14 00!15
72-54-8
ND ug/L
0.050
1
08/01/14 16:35
08/07/14 00!15
72-55-9
NO ug/L
0.050
1
08/01/14 16:35
08/07/14 00:15
50-29-3
ND ug/L
0.050
1
08/01/14 16:35
08/07/14 00:15
60-57-1
ND ug/L
0.050
1
08/01/14 16:35
08/07/14 00:15
959-98-8
ND ug1L
0.050
1
08/01/14 16:35
08/07/14 00:15
33213-65-9
ND ug/L
0.050
1
08/01/14 16:35
08/07/14 0015
1031-07-8
ND ug1L
0.050
1
08/01/14 16:35
08/07/14 00:15
72-20-8
ND ug1L
0.050
1
08/01/14 16:35
08/07/14 00:15
7421-93-4
NO ug1L
0.050
1
08/01/14 16:35
08/07/14 00:15
76-44-8
NO ug1L
0.050
1
08/01/14 16:35
08/07/14 00:15
1024-57-3
NO uglL
0.50
1
08/01/14 16:35
08/07/14 00:15
12674-11-2
NO ug/L
0.50
1
08/01/14 16:35
08/07/14 00:15
11104-28-2
ND ug/L
0,50
1
08/01/14 16:35
08/07/14 00:15
11141-16-5
ND ug/L
0,50
1
08/01/14 16:35
08/07/14 00:15
53469-21-9
ND ug/L
0.50
1
08/01/14 16:35
08/07/14 00:15
12672-29-6
NO ug/L
0.50
1
08/01/14 16:35
08/07/14 00:15
11097-69-1
NO ug/L
0.50
1
08/01/14 16:35
08/07/14 00:15
11096-82-5
NO ug/L
0.50
1
08/01/14 16:35
08/07/14 00:15
8001-35-2
68 %
20-110
1
08/01/1A 16:35
08/07/14 00,15
877-09-8
47 %
20-138
1
08/01/14 16:35
08/07/14 0015
2051-24-3
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
69.6 ug/L 5.0 1 07/31/14 21:25 08/06/14 00:40 7440-50-8
7.2 ug/L 5.0 1 07/31/14 21:25 08/06/14 00:40 7439-92-1
148 ug/L 10.0 1 07/31/14 21:25 08/06/14 00:40 7440-66-6
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
NO ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
83-32-9
Acenaphthylene
NO ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
208-96-8
Anthracene
NO uglL
5.0
1
08/06/14 11:53
08/08/14 04:03
120-12-7
Benzo(a)anthracene
NO ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
56-55-3
Senzo(a)pyrene
NO ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
50-32-8
Benzo(b)fluoranthene
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
205-99-2
Benzo(g,h,i)perylene
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
191-24-2
Benzo(k)fluoranthene
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
207-08-9
REPORT OF LABORATORY
ANALYSIS
This report shall
not be reproduced, except in
full,
Date: 08/08/2014 05:39 PM
without the written consent of Pace Analytical Services, Inc..
Page 5 of 26

aceAnalytical
wwh:pstdabs.own
Pace Analytical Services,.lnc.
9800 Kincey Ave. Suite 100
Huniersville. NC 28078
[phone]
ANALYTICAL RESULTS
Project: JULY 2014 Samples 7/31
Pace Project No.: 92211506
Sample: OUTFALL# 1
Parameters
Lab ID: 92211506001
Results Units
Collected: 07/31/14 00:00
Report Limit DF
Received: 07131/14 15:00 Matrix: Water
Prepared Analyzed GAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
4-Bromophenylphenyl ether
ND ug/L
5.0
1
08/06M4 11:53
08/08/14 04:03
101-55-3
Butylbenzylphlhalate
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
85-66-7
4-Chloro-3-methylphenol
ND ug/L
5.0
1
08/06114 11:53
08108M4 04:03
59-50-7
bis(2-Chloroethoxy)methane
ND ug1L
10.0
1
08/06f14 11-53
08/08114 04:03
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
108-60-1
2-Chloronaphthalene
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
91-58-7
2-Chlorophenol
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
7005-72-3
Chrysene
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
218-01-9
Dibenz(a,h)anthracene
ND ug/L
5.0
1
08106/14 11:53
08108/14 04:03
53-70-3
3,3'-Dichlorobenzidine
ND ugtL
25.0
1
08/06/14 11:53
08/08114 04:03
91-94-1
2,4-Dichlorophenot
ND ug/L
5.0
1
08/06114 11:53
08108114 04:03
120-83-2
Diethylphthalate
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
84-66-2
2,4-Di methyl phenol
ND ug/L
10.0
1
08/06114 11:53
08/08/14 04:03
105-67-9
Dimethylphthalate
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
131-11-3
Di-n-butylphthalate
ND ug1L
5.0
1
08/06/14 11:53
08/08/14 04:03
84-74-2
4,6-Dinitro-2-methylphenol
ND ug1L
20.0
1
08/06/14 11:53
08/08/14 04:03
534-52-1
2,4-Dinitrophenot
ND ug/L
50.0
1
08/06/14 11;53
08/08/14 04:03
51-28-5
2.4-Dinifrotoluene
ND ug1L
5.0
1
08106/14 11:53
OW08/14 04:03
121-14.2
2,6-Dinitrotoluene
ND ug/L
5.0
1
08f06114 11:53
08/08/14 04:03
606-20-2
Di-n-octylphthalate
N❑ ug/L
5.0
1
08/06/14 11:53
08/08f14 04:03
117-84-0
bis(2-Elhylhexyl)phthalate
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
117-81-7
Fluorenthene
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
206-44-0
Fluorene
ND ug/L
5.0
1
08/06114 11:53
08/08/14 04:03
86-73-7
Hexachloro-1,3-butadiene
ND ug1L
5.0
1
08/06/14 11:53
08/08/14 04:03
87-68-3
Hexachlorobenzene
ND ug1L
5.0
1
08/06/14 11:53
08/08/14 04:03
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.0
1
08/06/14 11:53
08/08/14 04:03
77-47-4
Hexachloroethane
ND ug/L
5.0
1
08/06/14 11:53
08/08114 04.03
67-72-1
lndeno(1,2,3-cd)pyrene
ND ug/L
5.0
1
08106f 14 11.53
0810811404:03
193-39-5
Isophorone
ND ug/L
10.0
1
08/06114 11!53
08/08/14 04:03
78-59-1
Naphthalene
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
91-20-3
Nitrobenzene
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
98-95-3
2-Nilrophenol
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
08/06/14 11:53
08/08/14 04:03
100-02-7
N-Nitrosodimethylamine
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
5.0
1
08/06/14 W53
08/08/14 04:03
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1
08/06/14 11:53
08/08114 04:03
86-30-6
Pentachlorophenol
ND ug/L
10.0
1
08/06114 11:53
08/08/14 04:03
87-86-5
Phenanthrene
ND ug/L
5.D
1
08/06114 11:53
08/08/14 04:03
85-01-8
Phenol
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
108-95-2
Pyrene
ND ug/L
5.0
1
08/06/14 11:53
08/08/14 04:03
129-00-0
1,2,4-Trichlorobenzene
ND ug1L
5.0
1
08/06/14 11:53
08/08/14 04:03
120-82-1
2,4,6-Trichlorophenol
ND ug1L
10.0
1
08/06/14 11:53
08/08/14 04:03
88-06-2
Surrogates
Nitrobenzene-d5 (S)
29 %
10-120
1
08/06/14 W53
08/08114 04:03
4165-60-0
2-Fluorobiphenyl (S)
31 %
15-120
1
OS/06/14 11:53
08/08/14 04:03
321-60-8
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in
full,
Date: 08/08/2014 05:39 PM
without the written
consent of Face Analytical
Services, Inc..
Page 6 of 26

Pace Analytical Services, Inc.
ac�{ n9800 Kinsey Ave. Suite 100
G rnayfical• kuntersville, NC 2807878
www.pecelabs=m [phone]
ANALYTICAL RESULTS
Project: JULY 2014 Samples 7/31
Pace Project No.: 92211506
Sample: OUTFALL # 1 Lab ID: 92211506001 Collected: 07/31/14 00:00 Received: 07/31/14 15!00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Surrogates
Terphenyl-d14 (S)
47 %
11-131
1
08/06/14 11:53
08/08/14 04:03
1718-51-0
Phenol-d6 (8)
11 %
10-120
1
08/06/14 11:53
08/08/14 04:03
13127-88-3
2-Fluorophenol (S)
15 %
10-120
1
08/06/14 11:53
08/08/14 04:03
367-12-4
2,4,6-Tribromophenol (S)
48 %
10-137
1
08/06/14 11:53
08/08/14 04:03
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND ug/L
2.0
1
08104/1418:25
71-43-2
Bromodichloromethane
NO ug/L
2.0
1
08/04/14 18:25
75-27-4
Bromoform
NO ug/L
2.0
1
08/04/14 18:25
75-25-2
Bromomethane
ND ug/L
2.0
1
08/04/14 18:25
74-83-9
Carbon tetrachloride
ND ug/L
2.0
1
08/04/14 18:25
56-23-5
Chlorobenzene
ND ug/L
2.0
1
08/04/14 18:25
108-90-7
Chloroethane
ND ug/L
2.0
1
08/04/14 18:25
75-00-3
Chloroform
ND ug/L
2.0
1
08/04/14 18:25
67-66-3
Chloromethane
NO ug/L
2.0
1
08104/1418:25
74-87-3
Dibromochloromethane
ND ug/L
2.0
1
08/04/14 18:25
124-48-1
1,2-Dichlorobenzene
ND ug/L
2.0
1
08/04/14 18:25
95-50-1
1,3-Dichlorobenzene
NO ug/L
2.0
1
08/04/14 18:25
541-73-1
1,4-Dichlorobenzene
ND ug/L
2.0
1
08/04/14 18:25
106-46-7
1,1-Dichloroethane
ND ug/L
2.0
1
08/04/14 18:25
75-34-3
1,2-Dichloroethane
ND ug1L
2.0
1
08/04/14 18:25
107-06-2
1,1-Dichloroethene
ND ug/L
2,0
1
08/04/14 18:25
75-35-4
cis-1,2-Dichloroethene
ND ug/L
2.0
1
08104/1418:25
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
2.0
1
08/04/14 18:25
156-60-5
1,2-Dichloropropane
ND ug1L
2.0
1
08/04/14 18:25
78-87-5
cis-1,3-Dichloropropene
ND ug1L
2.0
1
08/0411418:25
10061-01-5
trans- 1,3-Dichloropropene
ND ug1L
2.0
1
08/0411418:25
10061-02-6
Ethylbenzene
ND ug/L
2.0
1
08/0411418:25
100-41-4
Methylene Chloride
ND ug1L
2.0
1
08/04/14 18:25
75-09-2
1,1,2,2-Tetrachloroethane
NO ug/L
2.0
1
08/0411418:25
79-34-5
Tetrachloroethene
NO ug1L
2.0
1
08/0411418:25
127-18-4
Toluene
NO uglL
2.0
1
08/04/14 18:25
108-88-3
1,1,1-Trichloroethane
ND ug/L
2.0
1
08/0411418:25
71-55-6
1,1,2-Trichloroethane
NO uglL
2.0
1
08/04/14 18:25
79-00-5
Trichloroethene
NO uglL
2.0
1
08/04/14 18:25
79-01-6
Trichlorofluoromethane
NO uglL
2.0
1
08/04/14 18:25
75-69-4
Vinyl chloride
ND ug/L
2.0
1
08/04/14 18:25
75-01-4
Surrogates
4-Bromofluorobenzene (S)
92 %
70-130
1
08/04/14 18:25
460-00-4
Toluene-d8 (S)
99 %
70-130
1
08/04/14 18:25
2037-26-5
1,2-Dichloroethane-d4 (S)
109 %
70-130
1
08/04/14 18:25
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
33.1 mg/L
3.6
1
08/05/14 10:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 26

Pace Analytical Services, Inc.
Q �7 r • 9800 Fincey Ave. Suite 100
aCeA alXica`rHuntersvilte, NC 28078
www.pecetaba•svm [phone]
ANALYTICAL RESULTS
Project: JULY 2014 Samples 7/31
Pace Project No.: 92211506
Sample: OUTFALL # 2 Lab ID: 92211506002 Collected: 07/31/14 00:00 Received: 07/31/14 15:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/01/14 17:24
608 GCS Pesticides and PCBs Analyboal Method: EPA 608 Preparation Method: EPA3510
Aldrin
ND ug/L
0.071
1
08/01114 16:35
08/07/14 00:32
309.00-2
alpha-BHC
ND ug/L
0,071
1
08/01/14 16:35
08/07/14 00:32
319-84-6
beta-BHC
ND ug/L
0.071
1
08/01/14 16:35
08/07/14 00:32
319-85-7
delta-BHC
ND ug/L
0.071
1
08/01/14 16:35
08/07/14 00:32
319416-8
gamma-BHC (Lindane)
ND ug/L
0.071
1
08/01/14 16:35
08/07/14 00:32
58-89-9
Chlordane (Technical)
ND ug/L
0.71
1
08/01/14 16:35
08/07/14 00:32
57-74.9
4,4'-DDD
ND ug/L
0.071
1
08/01/14 16:35
08/07/14 00:32
72-54.8
4,4'-DDE
ND ug/L
0.071
1
08/01/14 16:35
08107/14 00:32
72-55.9
4,4'-DDT
ND ug/L
0.071
1
06/01114 16:35
08/07/14 00:32
50-29-3
Dieldrin
ND ug/L
0.071
1
08/01/14 16:35
08107114 00:32
60-57-1
Endosulfan I
ND ug/L
0.071
1
08/01/14 16,35
08/07/14 00:32
959-98-8
Endosulfan II
ND ug/L
0.071
1
08/01/14 16:35
08/07/14 00:32
33213-65-9
Endosulfan sulfate
ND ug/L
0.071
1
08/01/14 16:35
08/07/14 00:32
1031-07-8
Endrin
ND ug/L
0.071
1
08/01/14 16:35
08/07/14 00:32
72-20.8
Endrin aldehyde
ND ug/L
0.071
1
08/01/14 16:35
08/07/14 00:32
7421-93-4
Heptachlor
ND ug/L
0.071
1
08/01/14 16:35
08/07/14 00:32
76-44-8
Heptachlor epoxide
ND ug/L
0.071
1
08/01/14 16:35
08/07/14 00:32
1024-57-3
PCB-1016 (Arodor 1016)
ND ug/L
0.71
1
0810111416:35
08/07/14 00:32
12674-11-2
PCB-1221 (Aroclor 1221)
ND ug/L
0,71
1
08101/14 16:35
08/07/14 00:32
11104-28-2
PCB-1232 (Arodor 1232)
ND ug/L
0.71
1
08/01/14 16:35
08/07/14 00:32
11141.16-5
PCB-1242 (Arodor 1242)
ND ug/L
0,71
1
08/01/14 16:35
08/07/14 00:32
53469-21-9
PCB-1248 (Aroclor 1248)
ND ug/L
0.71
1
08/01/14 16:35
08/07/14 00:32
12672-29-6
PCB-1254 (Aroclor 1254)
ND ug/L
0.71
1
08/01/14 16:35
08/07/14 00:32
11097-69-1
PCB-1260 (Arodor 1260)
ND ug/L
0.71
1
08/01/14 16:35
08/07/14 00:32
11096-82-5
Toxaphene
ND ug/L
0.71
1
08/01/14 16:35
08/07/14 00:32
8001-35-2
Surrogates
Telrachloro-m-xylene (S)
83 %
20-110
1
08/01/14 16:35
08/07114 00:32
877-09-8
❑ecachtorobiphenyl (S)
136 %
20-138
1
08101/14 16:35
08/07/14 00:32
2051-24-3
200.7 MET ICP
Analytical Method: EPA200.7 Preparation Method: EPA200.7
Copper
57.6 ug/1-
5.0
1
07/31/14 21:25
08/06/14 00:44
7440-50-8
Lead
5.1 ug/L
6.0
1
07/31/14 21:25
08/06/14 00:44
7439-92-1
Zinc
610 ug/L
t0.0
1
07/31/14 21:25
08/06/14 00:44
7440-66-6
625 MSSV
Analydeal Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND ug/L
6.2
1
08106/14 11:53
08/08/14 04:34
83-32-9
Acenaphthylene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
208-96-8
Anthracene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
120-12-7
Benzo(a)anthracene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
56-55-3
Benzo(a)pyrene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
50-32-8
Benzo(b)fluoranthene
ND ugll-
6.2
1
08/06/14 11:53
08/08/14 04:34
205-99-2
Benzo(g.h,i)perytene
ND ug/L
6.2
1
08/06114 11:53
08/08/14 04:34
191-24-2
Senzo(k)fluoranthene
ND ug/L
6.2
1
08/06114 11:53
08/08/14 04:34
207-08-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 26

Pace Analytical Services, Inc.
aceAnalytrcal 980D Kincey Ave. Suite 100
Huntersville, NC 28078
"ww.pub&com [phone]
ANALYTICAL RESULTS
Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
Sample: OUTFALL # 2 Lab lD: 92211506002 Collected: 07/31/14 00:00 Received: 07131/14 15:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
4-Bromophenylphenyl ether
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
101-55-3
Butylbenzylphlhalate
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
85-68-7
4-Chloro-3-methylphenol
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
59-50-7
bis(2-Chloroethoxy)methane
ND ug/L
12.5
1
08/06/14 11:53
08/08/14 04:34
111-91-1
bis(2-Chloroethyl) ether
ND ug/t_
6.2
1
08/06/14 11:53
08/08/14 04:34
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
108-60-1
2-Chloronaphthalene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
91-58-7
2-Chlorophenol
ND uglL
6.2
1
08/06/14 11:53
08/08/14 04:34
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
7005-72-3
Chrysene
ND uglL
6.2
1
08/06/14 11:53
08/08/14 04:34
218-01-9
Dibenz(a,h)anthracene
ND uglL
6.2
1
08/06/14 11:53
08/08/14 04:34
53-70-3
3,3'-Dichlorobenzidine
ND ug/L
31.2
1
08/06/14 11:53
08/08/14 04:34
91-94-1
2,4-Dichlorophenol
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
120-83-2
Diethylphtha late
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
84-66-2
2,4-Dimethylphenol
ND ug/L
12.5
1
08/06/14 11:53
08/08/14 04:34
105-67-9
Dimethylphthalate
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
131-11-3
Di-n-butylphthalate
ND ug/L
6.2
1
08/06/14 W53
08/08/14 04:34
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/L
25.0
1
08/06/14 11:53
08/08/14 04:34
534-52-1
2,4-Dinitrophenol
ND ug/L
62.5
1
08/06/14 11:53
08/08/14 04:34
51-28-5
2,4-Dinitrotoluene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
121-14-2
2,6-Dinitrotoluene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
606-20-2
Di-n-octylphthalate
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
117-81-7
Fluoranthene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
206-44-0
Fluorene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
87-68-3
Hexachlorobenzene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
118-74-1
Hexachlorocyclopentadiene
ND ug/L
12.5
1
08/06/14 11:53
08/08/14 04:34
77-47-4
Hexachloroethane
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
193-39-5
Isophorone
ND ug/L
12.5
1
08/06/14 11:53
08/08/14 04:34
78-59-1
Naphthalene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
91-20-3
Nitrobenzene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
98-95-3
2-Nitrophenol
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
88-75-5
4-Nitrophenol
ND ug/L
62.5
1
08/06/14 11:53
08/08/14 04:34
100-02-7
N-Nitrosodimethylamine
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
621-64-7
N-Nitrosodiphenylamine
ND ug/L
12.5
1
08/06/14 11:53
08/08/14 04:34
86-30-6
Pentachlorophenol
ND ug/L
12.5
1
08/06/14 11:53
08/08/14 04:34
87-86-5
Phenanthrene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
85-01-8
Phenol
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
108-95-2
Pyrene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
6.2
1
08/06/14 11:53
08/08/14 04:34
120-82-1
2,4,6-Trichlorophenol
ND ug/L
12.5
1
08/06/14 11:53
08/08/14 04:34
88-06-2
Surrogates
Nitrobenzene-d5 (S)
82 %
10-120
1
08/06/14 11:53
08/08/14 04:34
4165-60-0
2-Fluorobiphenyl (S)
83 %
15-120
1
08/06/14 11:53
08/08/14 04:34
321-60-8
REPORT OF
LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
Date: 08/08/2014 05:39 PM
without the written consent of Pace Analytical Services, Inc..
Page 9 of 26

aceAnalytical
WWWWve10113.00n
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Hunlersville. NC 28078
[phone]
ANALYTICAL RESULTS
Project: JULY 2014 Samples 7/31
Pace Project No.: 92211506
Sample: OUTFALL # 2 Lab 10- 92211506002 Collected: 07/31114 00.00 Received: 07/31/14 15:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quai
625 MSSV Analytical Method; EPA 625 Preparation Method: EPA 625
Surrogates
Terphenyl-d14 (S)
97 %
11-131
1
08/06/14 11:53
08/0811404:34
1718-51-0
Phenol-d6 (S)
33 %
10-120
1
08/06/14 11:53
08t08114 04:34
13127418-3
2-Fluorophenol (S)
45 %
10-120
1
08/06/14 11:53
08108/14 04:34
367-12-4
2.4.6-Tribromophenol (S)
91 %
10-137
1
08/06/14 11:53
08/08114 04:34
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND ug/L
2.0
1
08/04/14 18:42
7143.2
Bromodichloromethane
ND ug/L
2.0
1
08104/1418:42
75-27-4
Bromoform
ND ug/L
2.0
1
08/04/14 W42
75-25-2
Bromomethane
ND ug/L
2.0
1
0810411418:42
74-83-9
Carbon tetrachloride
ND ug/L
2.0
1
08104114 18:42
56.23-5
Chlorobenzene
ND ug/L
2.0
1
08104/1418:42
108.90-7
Chioroethane
ND ug/L
2.0
1
06/04/14 18:42
75-00-3
Chloroform
ND ug/L
2.0
1
08104/1418:42
67-66-3
Chloromethane
ND ug/L
2.0
1
08/04/14 18:42
74-87-3
Dibromochloromethane
ND ug/L
2.0
1
0810411418:42
124.48-1
1,2-Dichlarobenzene
ND ug/L
2,0
1
08/04/14 18:42
95-50-1
1,3-Dichlarobenzene
ND ug/L
2.0
1
08104/1418:42
541.73-1
1,4-Dichiorobenzene
ND ug/L
2.0
1
08/04/14 18.42
106-46-7
1,1-Dichloroethane
ND ug/L
2.0
1
08104/1418:42
75-34-3
1,2-Dichloroethane
ND ug/L
2.0
1
08/04114 18:42
107-06-2
1,1-Dichloroethene
ND ug/L
2.0
1
08/04/14 18:42
75-35-4
cis-1,2-Dichloroethene
ND ug/L
2.0
1
08/04/14 18:42
156-59-2
trans•1,2-Dichloroethene
ND ug/L
2.0
1
08/04/14 18:42
156-60-5
1,2-Dichloropropane
ND ug/L
2.0
1
08104/1418:42
78-87-5
cis-1,3-Dichloropropene
ND ug/L
2,0
1
08/04/14 18:42
10061.01-5
trans-1,3-Dichloropropene
ND ug/L
2.0
1
08/0411418:42
10061.02-6
Ethylbenzene
ND ug/L
2.0
1
0810411418:42
100-41-4
Methylene Chloride
ND ug/L
2.0
1
08104/14 18.42
75-09-2
1,12.2-Tetrachloroethane
ND ug/L
2.0
1
08/04/14 18:42
79-34-5
Tetrachloroethene
ND ug/L
2.0
1
08/04/14 18:42
127-18-4
Toluene
ND ug/L
2.0
1
08/04/14 18:42
108-88-3
1,1,1-Trichloroethane
ND ug/L
2.0
1
0810411418:42
71-55-6
1,1,2-Trichloroethane
ND ug/L
2.0
1
08104/1418:42
79-00-5
Trichloroethene
ND ug/L
2.0
1
08/0411418:42
79-01-6
Trichlorofluoromethane
ND ug/L
2.0
1
0810411418:42
75-694
Vinyl chloride
ND ug/L
2.0
1
08/04114 18:42
75-01-4
Surrogates
4-Bromofluorobenzene (S)
91 %
70-130
1
08/04/14 18:42
460-00-4
Toluene-c18 (S)
98 %
70-130
1
08/04/14 18:42
2037-26-5
1,2-Diohloroethane-d4 (S)
110 %
70-130
1
08/04/14 18:42
17060-07-0
25400 Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
47.8 mg/L
2.5
1
08/05/14 10:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 26

aceAnalytical
wwwpecarabimn
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7/31
Pace Project No.: 92211506
QC Batch: GCSV/18421 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Descripfion: 1664 HEM, Oil and Grease
Associated Lab Samples: 92211506001, 92211506002
METHOD BLANK: 1255306 Matrix: Water
Associated Lab Samples: 92211506001, 92211506002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 08/01/14 17:17
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1255307
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg[L
40 36.2
90
78-114
MATRIX SPIKE SAMPLE:
1255308
35148214001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
1.8J 40
36.8
88
78-114
Results presented on this page are in the units indicated by the "Units` eolumn except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 26

aceAnalXical
www.pecelahs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7/31
Pace Project No.: 92211506
QC Batch: MPRP/16576 Analysis Method: EPA 200.7
QC Batch Method: EPA200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92211506001, 92211506002
METHOD BLANK: 1254502 Matrix: Water
Associated Lab Samples: 92211506001, 92211506002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper uglL ND 5.0 08/05/14 23:05
Lead uglL ND 5.0 08105/14 23:05
Zinc ug L ND 10.0 08105114 23:05
LABORATORY CONTROL SAMPLE:
1254503
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Copper
ug1L
500
525 105 85-115
Lead
ug/L
500
523 105 85-115
Zinc
ug/L
500
505 101 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1254504
1254505
MS
MSD
92211325001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper ug/L
10.7
500
500
547
545
107
107
70-130
0
Lead ug/L
ND
500
500
490
491
98
98
70-130
0
Zinc ug/L
0.80
500
500
1300
1310
101
102
70-130
0
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1254506
1254507
MS
MSD
92211505001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper ug/L
ND
500
500
523
530
105
106
70-130
1
Lead ug/L
ND
500
500
512
519
102
104
70-130
1
Zinc ug/L
ND
500
500
498
500
99
99
70-130
0
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analyticat Services, Inc.. Page 12 of 26

aceAnalytical.
wwwpacelahs.=n
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
QC Batch: MSV127818 Analysis Method: EPA624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92211506001, 92211506002
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1256160
Matrix:
Water
Associated Lab Samples: 92211506001, 92211506002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1,1-Trichloroethane
ug/L
ND
2.0
08104/1416:12
1,1,2,2-Tetrachloroethane
ug/L
ND
2.0
0810411416:12
1,1,2-Trichloroethane
ug/L
ND
2.0
08104/1416:12
1,1-Dichloroethane
ug/L
ND
2.0
08104/1416:12
1.1-Dichloroelhene
ug/L
ND
2.0
08104/1416:12
1,2-Dichlorobenzene
ug/L
ND
2.0
08/04/1416A2
1,2-Dichloroethane
ug/L
ND
2.0
0810411416:12
1,2-Dichloropropane
ug/L
ND
2.0
08104/1416:12
1,3-Dichlorobenzene
ug/L
NO
2.0
08104/1416:12
1,4-Dichlorobenzene
ug/L
ND
2.0
08104/1416:12
Benzene
ug1L
ND
2.0
08104/1416:12
Bromod ich lorom ethane
ug/L
ND
2.0
08/04/1416:12
Bromoform
ug/L
ND
2.0
08/04/1416:12
Bromomethane
ug/L
ND
2.0
08/04/1416:12
Carbon tetrachloride
ug/L
ND
2.0
08/04/14 16:12
Chlorobenzene
ug/L
ND
2.0
08/0411416:12
Chloroethane
ug1L
ND
2.0
08/0411416:12
Chloroform
ug1L
ND
2.A
08/0411416:12
Chloromethane
ug1L
ND
2.0
0810411416:12
cis- 1, 2-Dich loroethene
ug1L
ND
2.0
08/0411416:12
cis- 1, 3-Dich loropropene
ug1L
ND
2.0
08/0411416:12
Dibromochloromelhane
ug1L
ND
2.0
08/0411416:12
Ethylbenzene
ug/L
ND
2.0
08/04/1416:12
Methylene Chloride
ug1L
ND
2.0
08/04/14 16:12
Tetrachloroethene
ug1L
ND
2.0
08/04/1416:12
Toluene
ug/L
ND
2.0
08/04/1416:12
trans-1,2-Dichloroethene
ug/L
ND
2.0
08104/1416:12
trans-1,3-Dichloropropene
ug/L
ND
2.0
08104/1416:12
Trichloroethene
ug/L
ND
2.0
08/04/1416:12
Trichlorofluoromethane
ug/L
ND
2.0
08104/1416:12
Vinyl chloride
ug/L
ND
2.0
08/04/14 16:12
1,2-Dichloroethane-d4 (S)
%
105
70-130
08/04/14 16:12
4-Bromofluorobenzene (S)
%
98
70-130
08/04/14 16A2
Toluene-d8 (S)
%
99
70-130
08/04/14 16:12
LABORATORY CONTROL SAMPLE:
1256161
Spike
LCS
LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane
ug1L
20
19.1
96 52-162
1,1,2,2-Tetrachloroethane
ug1L
20
19.4
97 46-157
Results presented on this page are in the units indicated by the "Units" column except where an attemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 26

aceAnalytrcal
wwwpacelahscom
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
LABORATORY CONTROL SAMPLE:
Parameter
1256161
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,2-Trichloroethane
ug/L
20
19.9
100
52-150
1,1-Dichloroethane
ug/L
20
18A
92
59-155
1,1-Dichloroethene
ug/L
20
19A
97
1-234
1,2-Dichlorobenzene
ug/L
20
18.6
93
18-190
1,2-Dichloroethane
ug/L
20
18.1
91
49-155
1,2-Dichloropropane
ug/L
20
18.7
93
1-210
1,3-Dichlorobenzene
ug/L
20
18.6
93
59-156
1,4-Dichlorobenzene
ug/L
20
18.2
91
18-190
Benzene
ug/L
20
19.4
97
37-161
Bromodichloromethane
ug/L
20
22.2
111
35-155
Bromoform
ug/L
20
24.9
125
45-169
Bromomethane
ug/L
20
12.0
60
1-242
Carbon tetrachloride
ug/L
20
21.0
105
70-140
Chlorobenzene
ug/L
20
19.6
98
37-160
Chloroethane
ug/L
20
17.5
87
14-230
Chloroform
ug/L
20
22.4
112
51-138
Chloromethane
ug/L
20
15.0
75
1-273
cis-1,2-Dichioroethene
ug/L
20
20.6
103
68-146
cis-1,3-Dichloropropenc
ug/L
20
20.5
102
1-227
Dibromochloromethane
ug/L
20
25.1
125
53-149
Ethylbenzene
ug/L
20
19.5
97
37-162
Methylene Chloride
ug/L
20
18.0
90
1.221
Tetrachloroethene
ug/L
20
20.1
101
64-148
Toluene
ug/L
20
19.4
97
47-150
trans-1,2-Dichloroethene
uglL
20
20.6
103
54-156
trans-1,3-Dichloropropene
ug/L
20
20.4
102
17-183
Trichloroethene
ug1L
20
19.3
97
71-157
Trichlorolluoromethane
ug/L
20
18.7
94
17-181
Vinyl chloride
ug/L
20
17.4
87
1-251
1,2-Dichloroethane-d4 (S)
%
105
70-130
4-Bromoftuorobenzene (S)
%
97
70-130
Toluene-d8 (5)
%
98
70-130
Qualifiers
Results presented on this page are in the units Indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, inc..
Page 14 of 26

0
acmnalytical
www.pecelabs.wm
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
QC Batch: OEXT/29164 Analysis Method: EPA 608
OC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB
Assocated Lab Samples: 92211506001, 92211506002
METHOD BLANK: 1255276
Associated Lab Samples: 92211506001, 92211506002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
4,4'-DDD
ug/L
ND
0.050
08/06/14 23:22
4,4'-DDE
ug/L
ND
0.050
08/06/14 23:22
4,4'-DDT
ug/L
ND
0.050
08/06/14 23:22
Aldrin
uglL
ND
0.050
08/06/14 23:22
alpha-BHC
ug/L
ND
0.050
08/06/14 23:22
beta-BHC
ug/L
ND
0.050
08/06/14 23:22
Chlordane (Technical)
ug/L
ND
0,50
08/06/14 23:22
delta-BHC
ug/L
ND
0.050
08/06/14 23:22
Dieldrin
ug/L
ND
0.050
08/06/14 23:22
Endosulfan I
ug/L
ND
0.050
08/06/14 23:22
Endosulfan II
ug/L
ND
0.050
08/06/14 23:22
Endosulfan sulfate
ug/L
ND
0.050
08/06/14 23:22
Endrin
ug/L
ND
0.050
08/06/14 23:22
Endrin aldehyde
ug/L
ND
0.050
08/06/14 23:22
gamma-BHC (Lindane)
ug/L
ND
0.050
08/06/14 23:22
Heptachlor
ug/L
ND
0.050
08/06/14 23:22
Heptachlor epoxide
ug/L
ND
0.050
08/06/14 23:22
PCB-1016 (Arodor 1016)
ug/L
ND
0.50
08/06/14 23:22
PCB-1221 (Arodor 1221)
ug/L
ND
0.50
08/06/14 23:22
PCB-1232 (Arodor 1232)
ug/L
ND
0.50
08/06/14 23:22
PCB-1242 (Arodor 1242)
ug/L
ND
0.50
08/06/14 23:22
PCB-1248 (Arodor 1248)
ug/L
ND
• 0.50
08/06/14 23:22
PCB-1254 (Arodor 1254)
ug/L
ND
0.50
08/06/14 23:22
PCB-1260 (Arodor 1260)
ug1L
ND
0.50
08/06/14 23:22
Toxaphene
ug1L
ND
0.50
08/06/14 23:22
Decachlorobiphenyl (S)
%
91
20-138
08/06/14 23:22
Tetrachloro-m-xylene IS)
%
75
20-110
08/06/14 23:22
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1255277
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
.25
0.20
82
31-141
4,4'-DDE
ug1L
.25
0,21
84
30-145
4,4'-DDT
ug/L
.25
0,22
89
25-160
Aldrin
ug/L
.25
0,16
66
42-122
alpha-BHC
ug/L
.25
0,22
90
37-134
beta-BHC
ug/L
.25
0.22
90
17-147
delta-BHC
ug/L
.25
0.26
103
19-140
Dieldrin
ug/L
.25
0.20
81
36-146
Endosulfan I
ug/L
.25
0.20
82
45-153
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 26

aceArlalytical
w+vWvpaceiabxccM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7131
Pace Project No_: 92211506
LABORATORY CONTROL SAMPLE:
Parameter
1255277
Units
Spike
Cone.
LCS
Result
LCS
% Rec.
% Rec
Limits
Endosulfan It
ug/L
.25
0.22
89
1-202
Endosulfan sulfate
ug/L
.25
0.23
94
26-144
Endrin
ug/L
.25
0.22
87
30-147
Endrin aldehyde
ug/L
.25
0.20
81
50-150
gamma-BHC (Lindane)
ug/L
25
0.22
88
32-127
Heptaciiior
ug/L
.25
0.19
76
34-111
Heptachlor epoxide
ug/L
.25
0.19
77
41-126
Deoachlorobiphenyl (S)
%
87
20-138
Tetra oh loro-m-xylene (S)
%
84
20-110
Qualifiers
Results presented on this page are in the unite indicated by 0*'Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 26

0
aceAnalytical
www.pacdabs.com
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
QC Batch: OEXT/29237 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92211506001, 92211506002
METHOD BLANK: 1257691
Associated Lab Samples: 92211506001, 92211506002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
08/08/14 09:32
2,4,6-Trichlorophenol
ug/L
ND
10.0
08/08/14 09:32
2,4-Dichlorophenol
ug/L
ND
5.0
08/08/14 09:32
2,4-D imethyl phenol
ug/L
ND
10.0
08/08/14 09:32
2,4-Dinitrophenol
ug/L
ND
50.0
08/08/14 09:32
2,4-Dinitrotoluene
ug/L
ND
5.0
08/08/14 09:32
2,6-Dinitrotoluene
ug/L
ND
5.0
08/08/14 09:32
2-Chloronaphthalene
ug/L
NO
5.0
08/08/14 09:32
2-Chlorophenol
ug/L
ND
5.0
08/08/14 09:32
2-Nitrophenol
ug/L
ND
5.0
08/08/14 09:32
3,3'-Dichlorobenzidine
ug/L
NO
25.0
. 08/08/14 09:32
4,6-Dinitro-2-methyiphenoi
ug/L
NO
20.0
08/08/14 09:32
4-Bromophenylphenyl ether
ug/L
NO
5.0
08/08/14 09:32
4-Chloro-3-methylphenol
ug/L
NO
5.0
08/08/14 09:32
4-Chlorophenylphenyl ether
ug1L
ND
5.0
08/08/14 09:32
4-Nitrophenol
ug/L
ND
50.0
08/08/14 09:32
Acenaphthene
ug/L
NO
5.0
08/08/14 09:32
Acenaphthyiene
ug1L
NO
5.0
08/08/14 09:32
Anthracene
ug/L
ND
5.0
08/08/14 09:32
Benzo(a)anthracene
ug1L
NO
5.0
08/08/14 09:32
Benzo(a)pyrene
ug/L
ND
5.0
08/08/14 09:32
Benzo(b)fluoranthene
ug1L
ND
5.0
08/08/14 09:32
Benzo(g,hJ)perylene
ug1L
ND
5.0
08/08/14 09:32
Benzo(k)fluoranthene
uglL
NO
5.0
08/08/14 09:32
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
08/08/14 09:32
bis(2-Chloroethyl) ether
ug/L
ND
5.0
08/08/14 09:32
bis(2-Chloroisopropyl) ether
ug1L
ND
5.0
08/08/14 09:32
bis(2-Ethylhexyl)phthalate
ug1L
ND
5.0
08/08/14 09:32
Butylbenzylphthalate
ug/L
ND
5.0
08/08/14 09:32
Chrysene
ug/L
ND
5.0
08/48/14 09:32
Di-n-butylphthalate
ug/L
ND
5.0
08/08/14 09:32
Di-n-octylphthalate
ug/L
ND
5.0
08/08/14 09:32
Dibenz(a,h)anthracene
ug/L
ND
5.0
08/08/14 09:32
Diethylphtha late
ug/L
NO
5.0
08/08/14 09:32
Di methyl phthalate
ug/L
ND
5.0
08/08/14 09:32
Fluoranthene
ug/L
ND
5.0
08/08/14 09:32
Fluorene
ug/L
ND
5.0
08/08/14 09:32
Hexachloro-1,3-butadiene
ug/L
ND
5.0
08/08/14 09:32
Hexachlorobenzene
ug/L
ND
5.0
08/08/14 09:32
Hexachlorocyclopentadiene
ug/L
ND
10.0
08/08/14 09:32
Hexachloroethane
ug/L
ND
5.0
08/08/14 09:32
Qualifiers
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 26

to
aceAnalytical
www.pecelsbxocm
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville. NC 28078
[phone]
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7131
Pace Project No_: 92211506
METHOD BLANK: 1257691 Matrix: Water
Associated Lab Samples: 92211506001, 92211506002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Indeno(1,2,3-od)pyrene
ug/L
ND
5.0
08108/1409:32
Isophorone
ug/L
ND
10.0
08108/14 09:32
N-Nitroso-di-n-propylamine
uglL
ND
5.0
08f08/14 09:32
N-Nitrosodimethylamine
ug/L
ND
5.0
08/08/14 09:32
N-Nitrosodiph enyla mine
ug/L
ND
10.0
08/08/14 09:32
Naphthalene
ug/L
ND
5.0
08/08/14 09:32
Nitrobenzene
ug/L
ND
5.0
08/08/14 09:32
Pentachlorophenol
ug/L
ND
10.0
08/08/14 09:32
Phenanthrene
ug/L
ND
5.0
08/08/14 09:32
Phenol
ug/L
ND
5.0
08/08/14 09:32
Pyrene
ug/L
ND
5.0
08108/14 09:32
2,4,6-Tribromophenol (S)
eta
107
10-137
08108/14 09:32
2-Fluorobiphenyl (S)
%
85
15-120
08108/14 09:32
2-Fluorophenol (S)
%
41
10-120
08/08/14 09:32
Nitrobenzene-d5 (S)
%
81
10-120
08/08/14 09:32
Phenol-d6 (S)
%
29
10-120
08/08/14 09:32
Terphenyl-d14 (S)
%
92
11-131
08/08/14 09:32
LABORATORY CONTROL SAMPLE.
Parameter
1257692
Units
Spike
Conc.
LC5
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
36.7
73
44-142
2,4,6-Trichlorophenol
ug/L
50
47.4
95
37-144
2,4-Dichlorophenol
ug/L
50
46A
93
1-191
2,4-Dimethylphenol
ug/L
50
46.8
94
32-119
2,4-Dinitrophenol
ug/L
250
366
146
1-181
2,4-Dinitrotoluene
ug/L
50
48.8
98
39-139
2,6-Dinitrotoluene
ug/L
50
51.1
102
50-158
2-Chloronaphthatene
ug/L
50
411.3
83
60-118
2-Chlorophenol
ug/L
50
39.8
80
23-134
2-Nitrophenol
ug/L
50
53.4
107
29-182
3,3'-Diohlorobenzidine
ug/L
100
88.1
88
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
162
162
1-181
4-Bromophenylphenyl ether
ug/L
50
49.0
98
53-127
4-Chloro-3-methylphenol
ug/L
100
94A
94
22-147
4-Chiorophenylphenyl ether
ug/L
50
44.9
90
25-158
4-Nitrophenol
ug/L
250
100
40
1-132
Acenaphthene
ug/L
50
44A
89
47-145
Acenaphthylene
ug/L
50
45.2
90
33-145
Anthracene
ug/L
50
46.9
94
1-166
Benzo(a)anthracene
ug/L
50
43.0
86
33-143
Benzo(a)pyrene
ug/L
50
43.7
87
17-163
Senzo(b)fiuoranthene
ug/L
50
39.0
78
24-159
Benzo(g.h,i)perylene
ug/L
50
41.9
84
1-219
Results preseMed on this page are In the units indicated by the'0niW coiunut except where an aiternale unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 26

aceAnalytical
www.peaerabxaom
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7/31
Pace Project No.: 92211506
LABORATORY CONTROL SAMPLE
1257692
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Benzo(k)fluoranthene
ug/L
50
44.7
89
11-162
bis(2-Chloroethoxy)methane
ug/L
50
42.5
85
33-184
bis(2-Chloroethyl) ether
ug/L
50
41.9
84
12-158
bis(2-Chloroisopropyl) ether
ug/L
50
37.4
75
36-166
bis(2-Elhylhexyl)phthalate
ug/L
50
52.1
104
8-158
Butylbenzylphthalate
ug/L
50
53.5
107
1-152
Chrysene
ug/L
50
46.7
93
17-168
Di-n-butylphthalate
ug/L
50
48.2
96
1-118
Di-n-octylphthe late
ug/L
50
54.6
109
4-146
Dibenz(a,h)anthracene
ug/L
50
42.3
85
1-227
Di ethyl phtha late
ug/L
50
44.5
89
1-114
Dimethylphthalate
ug/L
50
45.6
91
1-112
Fiuoranthene
ug/L
50
45.4
91
26-137
Fiuorene
ug/L
50
47.2
94
59-121
Hexachloro-1,3-butadiene
ug/L
50
35.8
72
24-116
Hexachlorobenzene
ug/L
50
42.8
86
1-152
Hexachlorocyclopentadiene
ug/L
50
51.4
103
25-150
Hexachloroethane
ug/L
50
38.3
77
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
33.6
67
1-171
Isophorone
ug/L
50
45.1
90
21-196
N-Nitroso-di-n-propylamine
ug/L
50
43.7
87
1-230
N-Nitrosodimethylamine
ug/L
50
24.7
49
25-150
N-Nitrosodiphenylamine
ug/L
50
48.7
97
25-150
Naphthalene
ug/L
50
40.4
81
21-133
Nitrobenzene
ug/L
50
45.4
91
35-180
Pentachlorophenol
ug/L
100
96.3
96
14-176
Phenanthrene
ug/L
50
44.8
90
54-120
Phenol
ug/L
50
20.7
41
5-112
Pyrene
ug/L
50
47.3
95
52-115
2,4,6-Tribromophenol (S)
%
111
10-137
2-Fluorobiphenyl (S)
%
91
15-120
2-Fluorophenol(S)
%
46
10-120
Nitrobenzene-d5(S)
%
88
10-120
Phenol-d6 (S)
%
35
10-120
Terphenyl-d14 (S)
%
96
ii-131
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Oualifiers
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
1257693
1257694
MS
MSD
92212023001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Oual
1,2,4-Trichlorobenzene
ug/L
ND
100
100
74.2
79.4
74
79
44-142
7
2,4,6-Trichlorophenol
ug/L
ND
100
100
87.2
92.7
87
93
37-144
6
2,4-Dichlorophenol
ug/L
ND
100
100
84.0
90.6
84
91
1-191
7
2,4-Dimethylphenol
ug/L
ND
100
100
87.4
92.5
87
92
32-119
6
2,4-Dinitrophenol
ug/L
ND
500
500
712
825
142
165
1-181
15
Results presented on this page are in the units indicated by the -Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc..
Page 19 of 26

e
aceAnalyfical
*WWPmefabstmm
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7131
Pace Project No_: 92211506
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1257693 1257694
MS
MSD
92212023001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc,
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Oual
2,4-Dinitrotoluene
ug/L
ND
100
100
98.0
98.4
98
98
39-139
0
2,6-Dinitrotoluene
ug1L
ND
100
100
100
103
100
103
50-158
3
2-Chloronaphthatene
ug/L
ND
100
100
80.7
85.0
81
85
60-118
5
2-Chtorophenol
ug/L
ND
100
100
74.0
78.1
74
78
23-134
5
2-Nitrophenol
ug/L
ND
100
100
94.2
108
94
108
29-182
13
3,3'-Dichlorobenzidine
ug/L
ND
200
200
145
160
73
80
1-262
10
4,6-Dinitro-2-methylphenol
ug/L
ND
200
200
300
341
150
170
1-181
13
4-Bromophenylphenyl ether
ug/L
ND
100
100
95.1
99.6
95
100
53-127
5
4-Chloro-3-m ethyl phenol
ug1L
ND
200
200
176
186
88
93
22-147
5
4-Chlorophenylphenyl ether
ug1L
ND
100
100
88.7
90.9
89
91
25-158
2
4-Nitrophenol
ug/L
ND
500
500
263
268
53
54
1-132
2
Acenaphthene
ug/L
ND
100
100
86.7
88.8
87
89
47-145
2
Acenaphthylene
ug/L
ND
100
100
86.9
90.8
87
91
33-145
4
Anthracene
ug/L
ND
100
100
90.2
92.9
90
93
1-166
3
Benzo(a)anthracene
ug/L
ND
100
101)
82.8
86.3
83
86
33-143
4
Benzo(a)pyrene
ug/L
ND
100
100
83.3
87.5
83
88
17-163
5
Benzo(b)fluoranthene
ug/L
ND
100
100
77.1
81.1
77
81
24-159
5
Benzo(g,h,i)perylene
ug/L
ND
100
100
76.9
82.2
77
82
1-219
7
Benzo(k)fluoranthene
ug/L
ND
100
100
82.7
86.6
83
87
11-162
5
bis(2-Chloroethoxy)methane
ugiL
ND
100
100
82.5
87.1
83
87
33-184
5
bis(2-Chloroethyl) ether
ug/L
ND
100
100
79.5
83.3
79
83
12-158
5
bis(2-Chloroisopropyl) ether
ug1L
ND
100
100
72.0
74.0
72
74
36-166
3
bis(2- Ethyl hexyl)phthalate
ug/L
ND
100
100
97.2
103
97
103
8-158
6
Butyibenzylphthalate
ug/L
ND
100
100
103
107
103
107
1-152
4
Chrysene
ug/L
ND
100
100
89.1
92.0
89
92
17-168
3
Di-n-butyl phthalate
ug/L
NO
100
100
96.4
99.0
96
99
1-118
3
Dl-n-ocryiphthalate
ug/L
ND
100
100
101
109
101
109
4-146
7
Dibenz(a,h)anthracene
ug/L
ND
100
100
79.0
84.3
79
84
1-227
6
Diethylphthalate
ug/L
ND
100
100
90.1
90.2
90
90
1-114
0
Dirrtethyiphthalate
ugiL
ND
100
100
89.0
91.2
89
91
1-112
2
Fluoranthene
ug/L
ND
100
100
92.1
92.6
92
93
26-137
1
Fluorene
ug/L
ND
100
100
92.2
94.8
92
95
59-121
3
Hexachloro-1,3-buladiene
ug/L
ND
100
100
73.9
78.9
74
79
24-116
6
Hexachlorobenzene
ug/L
ND
100
100
82.7
86.8
83
87
1-152
5
Hexachlorocyclopentadiene
ug1L
NO
100
100
101
116
101
116
25-150
14
Hexachloroethane
ug/L
ND
100
100
80.4
82.7
80
83
40-113
3
Ind eno(1,2,3-cd)pyrene
ug/L
ND
100
100
60.8
66.2
61
66
1-171
8
Isophorone
ug1L
ND
100
100
85.0
90.1
85
90
21-196
6
N-Nitroso-di-n-propylamine
ug/L
ND
100
100
79.7
85.0
80
85
1-230
7
N-Nitrosodimethylamine
ug/L
ND
100
100
59.8
61.9
60
62
25-150
3
N-NitrosodiphenylamIne
ug/L
ND
100
100
92.6
97.5
93
97
25-150
5
Naphthalene
ug/L
ND
100
100
79.9
85.1
80
85
21-133
6
Nitrobenzene
ug/L
ND
100
100
87.0
92.8
87
93
35-180
6
Pentachlorophenol
ug/L
ND
200
200
175
201
87
101
14-176
14
Phenanthrene
ug/L
ND
100
100
87.7
90.2
88
90
54-120
3
Phenol
ug/L
ND
100
100
48.0
50.8
48
51
5-112
6
Rowtts presented on this papa are in the units indicated by the
"Units' column except wherean aitemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc.- Page 20 of 26

acmnalytical
mm.pacelabs.com
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1257693
1257694
MS
MSD
92212023001 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
Pyrene
ug1L ND 100
100
90.5
91.6 90
92
52-115 1
2,4,6-Tribromophenol (S)
%
101
108
10-137
2-Fluorobiphenyl (S)
%
86
90
15-120
2-Fluorophenol (S)
%
51
53
10-120
Nitrobenzene-d5 (S)
%
83
89
10-120
Phenol-d6 (S)
%
41
43
10-120
Terphenyl-d14 (S)
%
89
92
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc..
Page 21 of 26

acsArralytical
www.pwebb&wm
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
p04j875-9092
QUALITY CONTROL DATA
Project: JULY 2014 Samples 7131
Pace Project No.: 92211606
QC Balch: WET/32455 Analysis Method: SM 2540D
QC Balch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92211506001, 92211506002
METHOD BLANK: 1256382 Matrix: Water
Associated Lab Samples: 92211506001, 92211506002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg[L ND 2.5 08/05/14 10:25
LABORATORY CONTROL SAMPLE: 1256383
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 270 108 W110
SAMPLE DUPLICATE: 1256364
92211826001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 129 132 2
SAMPLE DUPLICATE: 1256385
92211484001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL ND ND
Results presented on this page are in the units indicated by the "Units' column except where an attemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc..
Page 22 of 26

aceAnalytical
www,paceiabs.com
QUALIFIERS
Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anaiytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAS!-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 26

aceAnalytical
www.pxcarn
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: JULY 2014 Samples 7131
Pace Project No.: 92211506
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92211506001
OUTFALL # 1
EPA 1664B
GCSV/18421
92211506002
OUTFALL # 2
EPA 1664E
GCSV/18421
92211506001
OUTFALL # 1
EPA 3510
OEXT/29164
EPA 608
GCSWI8435
92211506002
OUTFALL # 2
EPA 3510
OEXT129164
EPA 608
GCSV118435
92211506001
OUTFALL # 1
EPA 200.7
MPRP/16576
EPA 200.7
ICP/14966
92211606002
OUTFALL # 2
EPA 200.7
MPRP/16576
EPA 200.7
ICP114966
92211506001
OUTFALL # 1
EPA 625
OEXT/29237
EPA 625
MSSV/9501
92211506002
OUTFALL # 2
EPA 625
OEXT/29237
EPA 625
MSSV/95011
92211506001
OUTFALL # 1
EPA 624
MSV/27818
92211506002
OUTFALL # 2
EPA 624
MSV/27818
92211506001
OUTFALL # 1
SM 2540D
WET/32455
92211506002
OUTFALL # 2
SM 2540D
WET/32455
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 08/08/2014 05:39 PM without the written consent of Pace Analytical Services, Inc..
Page 24 of 26

aceAnalytical `
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chakn-of-Cvslody is a LEGAL DOCUMEW. All relevant fields must be completed accurately.
--- . -
to
Page: of
Section A Section 8 Section C
Required Client Information: Required Project Information: Invoice lnformaWn:
Company: ' Report To: Attention:
`
8 8363
Address:
7p
copy To:
Company Name:
- ,. -
RE6 LATDR_YAGENCY-"- s
3in/ w
j
, s _
4/
Address:
NPOES f GROUND WATER r ,DRINKING WATER
� UST r- RCRA (" OTHER
EmoYTo: f/
Purchase Order No.:
puce CPAAe
�+ra%+�, •+t 4H n�r.i,
Rehxvnce:
Phone:
Fox:
Project Name:
' sA
Pace Project
naarrager.
- -
Skte Location
r.t
Repuesled Due DateITAT:
Project Number. f++j�� r
Pace Profile
,; Requeste,.
Anaiysis
Filtered
(YIN),.-,
-
Section D Matrix Codes
==
RequiradCiientInformaWn - MATRIX 1 CODE
COLLECTED
Preservatives
Drlr*ingWater DW
,�
zz
_
Water VJT
aler WW
,
coM rte
eaoa+ue
C.)
Z
Product
SoIVSolld SL
p
}
SAMPLE ID
Wipe WP
w'
(A-2, 0-9! .-) Air AR
O
a
Lu
z
Sampie iDs MUST BE UNIQUE Tissue TS-
O
L)
w
IL
tu-
zz
L
U
x
Other OT
X
w
w
U
-6
oca
_u
�
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,
ILVC
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CV
16
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DATE
TIME
DATE
TIME
x
2=
Z
Z
i
O
e PIA t o.! La I.D,
Pacz j b hT
:"
•':
2
?
9
-4.
r.,._
72
ADDITIONAL COMMENTS :
PLELINQUISNED ISY f AFFILIATION '
DATE
;.311YFE' ;
�ACCEPT_ED BY 1 AFFILIATION
DATE'
TIME
SAMPLE CONDITIONS
SAMPLER NAME AND SIG-
ORIGINAL
a
PRINT Nome of SAMPLER,r�;�rr
.
U
$
SIGNATURE of SAMPLER: ��� DATE ned 1-1
r
(7
tr
O m
N
(MMiDDg"
.1
'Important Note: By signing this form you are accepting Paces NET 30 day payment terms and agreeing to Late d'iargea of 1.5% per month for any Invoices not paid withEn 30 days. F-ALI.-(3-(9Amv n7 t 1-U—)nn7

Docur Name:
`gym Document. No.:
F-ASV-CS-003-reV.14
Client Name. f 1M-+&; ",
on Upon ac ant Revised: June 10, 2014
Page 1 of 2
Issuing Authorities:,
Pace Asheville Quality Office
Courier (Circle): Fed Ex UPS LISPS Client Commercial Pace Other
Custody Seal on Cooler/Box Present: ❑ yes no Seals intact: yes 7 no
Packing Material:, Bubble Wrap 2,1tubble Bags . ' ❑ No
Other
Thermometer used: IR Gun#3 -IN265953 Type of Ice: et Blue None (D.Zamples on ice, cooling process has begun
Gun #4 SNA40290365 Other,.
Temp Correction Factor: Add Afulbltr-a-a C
Corrected Cooler Temp.: a r V f C
Biological Tissue Is Frozen: Yes No
Date and Initials f person examining
contents:
Temp should be above freezing to VC
Comments:
Chain. of Custody Present:
E11r., Cl No
❑NIA
1.
Chain of Custody Filled Out:
QYs Duo
❑NIA
2.
Chain of Custody Relinquished:
B{res ONo
0NIA
3.
Sampler Name & Signature on COC:
XRf. ❑No
❑NIA
4.
Samples Arrived within Hold Time:
0<ea ON.
❑N1A
5.
Short Hold Time Analysis <72hr :
Dyes 11KO
El N/A
6.
Rush Turn Around Time Requested:
❑Yea
❑NIA
7.
Sufficient Volume:
9K.1 ON.
❑NIA
8.
Correct Containers Used
Dries ❑No
❑WA
9.
-Pace Containers Used:
13�res [)No
ONIA
Containers Intact:
lrreu ❑No
❑NIA
10.
Filtered volume received for Dissolved tests
es ON.
❑NIA
11.
Sample Labels match COC:
es ❑ND
❑N1A
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
.
des ❑ No
❑ N!A
13.
Ail containers needing preservation are found to be in
2�es ❑No
❑NIA
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, W!-DRO (water)
I3fes ON.
Sarno les checked for dechlorination:
Vas ❑No
❑NIA
14.
Headspaoe in VOA Vials. >6mm :
[5es ❑No
❑NIA
15,
Trip Blank Present:
Oyes &No
❑NIA
16.
Trip Blank Custody Seals Present
❑Yes 04
❑NIA
Papa Trip Blank Lot # Pf purchasAkd
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: (>� (,fin Date/Time. 1 hG ? cy
Comments/Resolution: ,;Z ez l' e'',;,_-L ,.. _ F.,pt= L'��_.�' Lrv� �' . -2s
SCURF Revfew:
SRF Review:l Cam' ]Date: 1 11/1'1
Note: Whenever there is a discrepancy affecting Korth Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
Page 26 of 26

7-22-2014
Division Water Resources
Asheville Regional
2090 US Hwy 70
Swannanoa, NC 28778
Subject; Regulatory Relief Review Request
Pentair Valves and Controls.
ODES No. NCG030529
To Whom It May Concern:
Please find enclosed our June 2014 DMR and additional sampling results from our downspouts and the
unnamed stream behind our facility.
We are requesting a review for regulatory relief from the Tier 11 additional sampling requirements. These
Tier I I responses are necessitated by exceedances of the zinc and copper benchmarks for two consecutive
semiannual sampling episodes. Since entering into the Tier It requirements, we have completed a review of
our process.
In summary of the BMP's that were reviewed and changed. We have developed,a process that prevents
chip hoppers from being overfilled to reduce process material and chips from being spilled. All hopper
frames are cleaned of process material prior to being taken outside to the Luggers. We also clean and sweep
the area around the Luggers after each use. There is no storage of process material outside our facility. We,
have -implemented •a wet mopping procedure inside -the plant.to help.eliminate process material from being
tracked outside. The.tires on our industrial,fork.trucks,have been inspected to insure they were not high
zinc material; also our process lubricants and coolants have been audited to ensure they are low zinc
formulas.
I have attached some additional background Storm Water results from the unnamed stream behind our
facif i and from our roof rain gutters and downspou� is far ytr review .The additional sampl gin points are
t e constituents of our estgnated Outfalls. Also included are samples of upstream from our facility and one
from downstream of our property.
After reviewing and revising our BMP's as well as reviewing these additional sampling results we are
unsure of a way to be in compliance with our zinc and copper benchmarks.
Pentair is committed to being compliant with all regulatory requirements but, moreover we are committed
to being good stewards of our environment and community. We are currently investigating a way to harvest
the rain water from our roof to be used in our Steam generators this will reduce the runoff from our
property. ,We welcome your review and input on our process.
If you have any questions regarding this letter, please feel free to contact me at 828.669.3753
Sincerely,
Sal Vaccaro
General Manager
Black Mountain
Received
JUi 2 9 2014
Land Quality Section
Asheville
RECEIVED
ilM ision of wwar F an"roa*
JUL 2 8 2014
Water Ouali y Regional Op. ►dens
Asheville ttegio.pat OfPEcnr €

1 .14
►;:3� U,�t ��,h Zama')
!'C i AG
L

Parameter
Maximum Daily Limit cant.
Outfall #1 2014 DMR Tracking
Ave ra a
Permit Limit
Units
January February March May June July August September October November Decembe
Flaw (Sample Period)*
0.556
inches 1
24hour
nod
0.520
0.210
0.310
1.740
Temperature
#DIVl0!
0
Deg, F
H min & max
7.18
9
Std. units
7.20
7.20
7.20
7.20
7.10
21-,
TSS
58
100
m 1L
34
28
29
11.100
iA871000
Oil & Grease
5
15
m IL
5.0
5.0
5.0
5.000
5.000
Copper
0.142
0.007
m 1L
5' 100
W010 '
O'490
! 0!046
0 063V.?
Lead
0.018
0.03
m 1L
0.0200
0.0200
0.0200
0.0200
0.010
Zinc
0.103
0.067
m 1L
LA0!;160R
M0;120-Q
0.064
0.060
^ZA0;1r13E�
Total Toxic Or anic9
#DlVIO!
1
ng/L
na
na
na
na
na
Parameter
Maximum Daily Limit Cont.
Outfall #2 2014 DMR Tracking
Average
Permit Limit
Units
January February March May June July August September October November December
Flow (Sample Period)*
1
inches !
24hour
eriod
0.520
0.210
0.310
1.740
Temperature
#DIVIO!
140
Deg. F
H(min & max
7.12
9
Std. units
6.90
7.20
7.50
6.90
7.10
TSS
6
100
m 1L
8.2
5.0
5.0
6.6
3.4
Oil & Grease
5
15
m 1L
5.0
5.0
5.0
5.0
5.0
Copper
0.044
0.007
m 1L
0.005
0.005
},'0":030i;
i 0 08,1!i�
0:,%100.X
Lead
0.016
0.03
m 1L
0.0200
0.0200
0.0200
0.0100
0.0115
Zinc
0.274
0.07
m 1L
30'160;e
U. .05120"
9�%'0"850.'2
i-E,'0°1;1-3
OM28W."
Total Toxic Organics
4DIV10!
1
mg[L
na
na
na
na
na

Semi-annual Stormwater Discharge Monitorin Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _July 22, 2014
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls_
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Pace Analytical Lab Cert. #40
Comments on sample collection or analysis: See page 4
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR �2014
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ® Monthly' June (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flaw []water Supply . ❑SA
®Other: Class C, Swannanoa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this Feriod?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches35
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
06-18-2014
0.63
187 mg/L
7.1
0.063 mg/L
<0.030
0.113 mg/L
<5.0 mg/L
BRL
2
06-18-2014
0.63
<3.4 mg/L
7.1
0.100 mg/L
0.011
0.128 mg/L
<5.0 mg/L
BRL
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same out#all.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from anon -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 4

Facilities that incorporate a solvent management plan into the 5tormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Sal Vaccaro
Name (Print name)
General Mana er
Title (Print title)
2�2LL,,�dL_A�p 7/22%2014
(Signature (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX me/0, where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note. if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period ?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches;
Nora -polar O&G/TPH by
EPA 166i4 (SGT-HEM)
Total suspended solids
pH
Benchmarks
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART 11 SECTION B.
• 2 EXCLEDANCES IN A ROW FORTH E SAME PARAMETER AT THE SAME OUTFALL TRiGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
+ TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE QUTFALL? YES Z NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO
REGIONAL OFFICE CONTACT NAME: _ Laura Herbert, P.E.
Mail an original and one copy of this DMR including all "No Discharge" reports, within 3a days of receipt of the lob results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
{Signature of
7/22/2014
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 4

1) Zinc reporting value exceeds permit limit 0.067 for outfall #2
a) Finding;
i) Roofing material is galvanized metal could be a contributing factor for outfall #1 and 42.
b) Corrective actions;
i) Reviewed BMP, ensured good management practices are being followed.
2) Copper reporting value exceeds permit limit 0.007 for outfall #1 and #2
a) Finding;
i) Roofing material is metal could be a contributing factor for outfall # 1 and #2.
ii) Scrap Lugger pad could be a contributing factor for outfall #l. We do not find potential sources of copper exposure in outfall #2.
b) Corrective actions;
i) Review of BMP's
ii) Have increased housekeeping, Lugger Pad Area and Center Pad are being inspected and cleaned after each use.
iii) Dump bins are cleaned off prior to being taken outside for dumping into luggers
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 4 of 4

aceAnalyfical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
July 07, 2014
Gerald Runkles
Pentair Valves & Controls
953 Old US Hwy 70
Black Mountain, NC 28711
RE: Project: Outfall6/18
Pace Project No.: 92205886
Dear Gerald Runkles:
Enclosed are the analytical results for sample(s) received by the laboratory on June 18, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's {duality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
,out the written consent of Pace Analytical Services, Inc..
Page 1 of 24

Pace Analytical Services, Inc.
8"'Malyfical " 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
w•pacews'com (704 )875-9092
CERTIFICATIONS
Project: Outfall 6118
Pace Project No.: 92205886
Charlotte Certification Ids
9800 KinceyAve. Ste 100, Huntersville, NC 28078
FloridalNELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ir Page 2 of 24

aceAnalj cal
www,pacoaft=
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Outfall 6118
Pace Project No., 92205886
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92205886001 OUTFALL # 1
92205866002 OUTFALL # 2
r
EPA 1664E
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA200.7
JMW
3
PASI-A
EPA 625
RES
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
JTJ
1
PASI-A
EPA 1664E
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA 200.7
JMW
3
PASI-A
EPA 625
RES
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
JTJ
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not 5e reproduced, except in full,
out the written consent of Pace Analytical Services, Inc..
Page 3 of 24

aceAnalyticaio
~,pacskbs. rn
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project: Outfall 6/18
Pace Project No.: 92205886
Lab Sample ID Client Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
92205986001
OUTFALL # 1
EPA 200.7
Copper 63.2 uglL
5.0
06/20/14 19:48
EPA 200.7
Lead 10.0 uglL
5.0
06/20/14 19:48
EPA 200.7
Zinc 113 ug/L
10.0
06/20/14 19:48
SM 2540D
Total Suspended Solids 187 mg/L
16.7
06/24/14 15:54
92205886002
OUTFALL # 2
EPA200-7
Copper 100 ug/L
5-0
06/20/1420M
EPA 200.7
Lead 11.5 ug/L
5.0
06/20114 20:00
EPA 200.7
Zinc 128 ug/L
10.0
06/20/14 20:00
SM 2540D
Total Suspended Solids 3.4 mg/L
2.5
06/24/14 15:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ir
Page 4 of 24

aceAnalytical
wwwpacela6Room
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Ouffall 6/18
Pace Project No.: 92205686
Sample: OUTFALL # 1 Lab ID: 92205886001 Collected: 06/18/14 16:00 Received: 06/18/14 16:55 Matrix; Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg/L
5.0
1
06/19/14 12:02
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:20
309-00-2
alpha-BHC
ND ug/L
0.050
1
06/25/14 11:12
06/29/14 21:20
319-84-6
beta-13HC
ND ug/L
0.050
1
06/25114 11:12
06129/14 21:20
319-85-7
delta-BHC
ND ug/L
0.050
1
06/25/14 11:12
06129/14 21:20
319-86-8
gamma-BHC (Lindane)
ND ug/L
0,050
1
06125/14 11:12
06129/14 21:20
58-89-9
Chlordane (Technical)
ND ug/L
0.50
1
06125114 11:12
06129114 21:20
57-74-9
4,4'-DDO
ND ug/L
0.050
1
06125/14 11:12
06129114 21:20
72-54-8
4,4'-DDE
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:20
72-55-9
4,4'-DDT
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:20
50-29-3
Dieldrin
ND ug/L
0.050
1
06/25/14 11:12
06/29/14 21:20
60-57-1
Endosulfan I
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:20
959-98-8
Endosulfan 11
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:20
33213-65-9
Endosulfan sulfate
ND ug/L
0.050
1
06/25/14 11:12
06/29/14 21:20
1031-07-8
Endrin
NO ug1L
0.050
1
06/25/14 11:12
06/29/14 21:20
72-20-8
Endrin aldehyde
NO ug1L
0.050
1
06/25/14 11:12
06/29/14 21:20
7421-93-4
Heptachlor
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:20
76-44-8
Heptachlor epoxide
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:20
1024-57-3
PCB-1016 (Aroclor 1016)
ND ug1L
0.50
1
06/25/14 11:12
06/29/14 21:20
12674-11-2
PCB-1221 (Aroclor 1221)
NO ug/L
0.50
1
06/25/14 11A2
06/29/14 21:20
11104-28-2
PCB-1232 (Aroclor 1232)
ND ug/L
0.50
1
06125/14 1112
06129/14 21:20
11141-16-5
PCB-1242 (Aroolor 1242)
NO ug/L
0.50
1
06/25/14 11:12
06/29/14 21:20
53469-21-9
PCB-1248 (Aroclor 1248)
ND ug/L
0.50
1
06/25/14 11.12
06/29114 21:20
12672-29-6
PCB-1254 (Aroclor 1254)
NO ug/L
0.50
1
OS/25114 11:12
06/29114 21:20
11097-69-1
PCB-1260 (Aroclor 1260)
ND ug1L
0.50
1
06/25114 11:12
06129/14 21:20
11096-82-5
Toxaphene
ND ug/L
0.50
1
06/25/14 11:12
06/29/14 21:20
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
50 %
20-110
1
06/25/14 11:12
06/29/14 21:20
877-09-8
Decachlorobiphenyl (S)
39 %
20-138
1
06/25/14 11:12
06/29/14 21:20
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA
200.7
Copper
63.2 ug/L
5.0
1
06/19/14 12:40
06/20/14 19:48
7440-50-8
Lead
10.0 ug/L
5.0
1
06/19/1412:40
06/20/14 19:48
7439-92-1
Zinc
113 ug/L
10.0
1
06/19/14 12:40
06120Y14 19:48
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND ug/L
5.0
1
06/25/14 12:30
G6127114 21:05
83-32-9
Acenaphthylene
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
208-96-8
Anthracene
ND ug/L
5.0
1
06/25114 12:30
06/27/14 21:05
120-12-7
Benzo(a)anthracene
ND ug/L
5.0
1
06125/14 12:30
06127/14 21:05
56-55-3
Benzo(a)pyrene
ND ug/L
5.0
1
06/25114 12:30
06127/14 21:05
50-32-8
Benzo(b)fluoranthene
ND ug/L
5.0
1
06/25114 12:30
06/27/14 21:05
205-99-2
Benzo(g,h,i)perylene
NO ug/L
5.0
1
06/25/14 12:30
06127/14 21:05
191-24-2
Benzo(k)fluoranth ene
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21;05
207-08-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2014 03:57 PM out the written consent of Pace Analytical Services, Inc.. Page 5 of 24

Pace Analytical Services, Inc.
® 9800 KinceyAve. Suite 100
alceAnalytrlca!
Hunters�iile, NC 28078
xwwpecaubs.com [phone]
ANALYTICAL RESULTS
Project: Oulfall 6/18
Pace Project No.: 92205886
Sample: OUTFALL # 1 Lab ID: 92205886001 Collected: 06/18/14 16:00 Received: 06/18/14 16:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
4-Bromophenyiphenyl ether
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
101-55-3
Butylbenzylphthalate
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
85-68-7
4-Chloro-3-methylphenoi
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
59-50-7
bis(2-Chloroethoxy)methane
NO ug/L
10.0
1
06/25/14 12:30
06/27/14 21:05
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
111-44-4
bis(2-Chloroisopropyl) ether
NO ug/L
5.0
1
06/25/14 12:30
06127/14 21:05
108-60-1
2-Chloronaphthalene
NO ug/L
5.0
1
06/25/14 12:30
06/27114 21:05
91-58-7
2-Chlorophenol
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
95-57-8
4-Chlorophenylphenyl ether
NO ug/L
5.0
1
06/25114 12:30
06127/14 21:05
7005-72-3
Chrysene
ND ug/L
5.0
1
06125/14 12:30
06127/14 21:05
218-01-9
Dibenz(a,h)anthracene
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
53-70-3
3,3'-Dichlorobenzidine
ND ug/L
25.0
1
06/25/14 12:30
06/27/14 21:05
91-94-1
2,4-Dichlorophenol
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
120-83-2
Di ethyl phthalate
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
84-66-2
2,4-Dimeth ylphenol
ND ug/L
10.0
1
06/25/14 12:30
06/27/14 21:05
105-67-9
Dimethylphthalate
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
131-11-3
Di-n-butylphthalate
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/L
20.0
1
06/25/14 12:30
06/27/14 21:05
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
1
06/25/14 12:30
06/27/14 21:05
51-28-5
2,4-Dinitrotoluene
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
121-14-2
2,6-Dinitrotoluene
NO uglL
5.0
1
06/25/14 12:30
06/27/14 21:05
606-20-2
Di-n-octylphthalate
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
117-84-0
bis(2-Ethylhexyl)phthalate
NO ug/L
5.0
1
06125/14 12:30
06127/14 21:05
117-81-7
Fluoranthene
NO ug/L
5.0
1
06/25/14 12:30
06127/14 21.05
206-44-0
Fluorene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
5.0
1
06125/14 12:30
06/27114 21:05
87-68-3
Hexachlorobenzene
NO ug/L
5.0
1
06125114 12:30
06/27/14 21:05
118-74-1
Hexachlorocyciopentadiene
ND ug/L
10.0
1
06125/14 12:30
06/27/14 21:05
77-47-4
Hexachloroethane
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
67-72-1
Indeno(1,2,3-od)pyrene
NO ug1L
5.0
1
06/25/14 12:30
06/27/14 21:05
193-39-5
Isophorone
ND ug/L
10.0
1
06/25/14 12:30
06/27/14 21:05
78-59-1
Naphthalene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
91-20-3
Nitrobenzene
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
98-95-3
2-Nitrophenol
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
06/25/14 12:30
06/27/14 21:05
100-02-7
N-Nitrosodimethylamine
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1
06//25114 12:30
06/27/14 21:05
86-30-6
Pentachiorophenol
ND ug/L
10.0
1
06/25/14 12:30
06/27/14 21:05
87-86-5
Phenanthrene
NO ug/L
5.0
1
06/25114 12:30
06127114 21,05
85-01-8
Phenol
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:05
108-95-2
Pyrene
NO ug/L
5.0
1"
06/25/14 12:30
06/27/14 21:05
129-00-0
1,2,4-Trichlorobenzene
NO ug/L
5.0
1
06/25114 12:30
06/27/14 21:05
120-82-1
2,4,6-Trichlorophenol
ND ug/L
10.0
1
06125114 12:30
06/27/14 21:05
88-06-2
Surrogates
Nitrobenzene-d5 (S)
32 %
10-120
1
06/25/14 12:30
06/27114 21:05
4165-60-0
2-Fluorobiphenyl (S)
31 %
15-120
1
06/25/14 12:30
06/27/14 21:05
321-60-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
+ Date: 07/07/2014 03:57 PM without the written consent of Pace Analytical Services, In,
Page 6 of 24

1��alce Analytical�
~..pecelabs.com
f
ANALYTICAL RESULTS
Project: Out#all 6/18
Pace Project No.: 92205886
Pace Analylical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Sample: OUTFALL # 1
Parameters
Lab 1D: 92205886001
Results Units
Collected: 06/18/14 16:00
Report Limit OF
Received: 06/18/14 16:55 Matrix: Water
Prepared Analyzed CAS No, Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Surrogates
Terphenyl-d14 (S)
64 %
11-131
1
06/25/14 12:30
06/27/14 21:05
1718-51-0
Phenol-d6 (S)
11 %
10-120
1
06/25/14 12:30
06/27/14 21:05
13127-88-3
2-Fluorophenol (S)
17 %
10-120
1
06/25/14 12:30
06/27/14 21:05
367-12-4
2,4,6-Tribromophenol (S)
48 %
10-137
1
06/25/14 12:30
06127/14 21:05
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND ug/L
2.0
1
06/28114 17:28
71-43-2
Bromodichloromethane
ND ug1L
2.0
1
06/28/14 17:28
75-274
Bromoform
NO ug1L
2.0
1
06/28114 17:28
75-25-2
Bromomethane
ND ug/L
2.0
1
06/2811417:28
74-83-9
Carbon tetrachloride
ND ug/L
2.0
1
06/28/14 17:28
56-23-5
Chlorobenzene
ND ug/L
2.0
1
0612811417:28
108-90-7
Chloroethane
ND ug1L
2.0
1
06/28/14 17:28
75-00-3
Chloroform
ND ug/L
2.0
1
06/28/1417;28
67-66-3
Chloromethane
ND ug/L
2.0
1
06/28/14 17:28
74-87-3
Dibromochloromethane
ND ug/L
2.0
1
06128/1417t28
124-48-1
1,2-Dichlorobenzene
ND ug/L
2.0
1
06/28/14 17:28
95-50-1
1,3-Dichlorobenzene
ND ug/L
2.0
1
06/28114 17:28
541-73-1
1,4-Dichlorobenzene
ND ug/L
2.0
1
06/28/14 17:28
106-46-7
11-Dichloroethane
ND ug/L
2.0
1
06128/14 17:28
75-34-3
1,2-Dichloroethane
ND ug/L
2.0
1
06128/14 17:28
107-06-2
1,1-Dichloroethene
NO ug/L
2.0
1
06/28/14 17:28
75-35-4
cis-1,2-Dichloroethene
ND ugIL
2.0
1
06/28114 17:28
156-59-2
trans-1.2-Dichloroethene
ND ug/L
2.0
1
06/28/14 17:28
156-60-5
1,2-Dichloropropane
ND ug/L
2.0
1
06128/14 17:28
78-87-5
cis-1,3-Dichloropropene
NO ug/L
2.0
1
06/28/14 17:28
10061-01-5
trans-1.3-Dichloropropene
ND ug/L
2.0
1
06/28/14 17:28
10061-02-6
Ethylbenzene
ND ug/L
2.0
1
06/28/14 17:28
100-41-4
Methylene Chloride
ND ug/L
2.0
1
06/28/14 17:28
75-09-2
1,1,2,2-Tetrachloroethane
ND ug/L
2.0
1
06128/14 17:28
79-34-5
Tetrachloroethene
ND ug/L
2.0
1
06/28/14 17:28
127-18-4
Toluene
ND ug1L
2.0
1
06/28/14 17:28
108-88-3
1,1,1-Trichloroethane
ND ug/L
2.0
1
06/28/14 17:28
71-55-6
1,1,2-Trichloroethane
NO ug/L
2.0
1
06/28114 17:28
79-00-5
Trichloroethene
ND u911-
2.0
1
06/28/14 17:28
79-01-6
Trichlorofluoromethane
ND ug1L
2.0
1
06128/14 17:28
75-69-4
Vinyl chloride
ND ug/L
2.0
1
06/28/14 17:28
75-01-4
Surrogates
4-Bromofluorobenzene (S)
90 %
70-130
1
06/28114 17:28
460-00-4
Toluene-d8 (S)
99 %
70-130
1
06/28114 17:28
2037-26-5
12-Dichloroethane-d4 (S)
98 %
70-130
1
06/28/14 17:28
17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 187 mg/L 16.7 1 06124/14 15,54
REPORT OF LABORATORY ANALYSIS
This report $hall not be reproduced, except in full, : c
Date: 07/07/2014 03:57 PM out the written consent of Pace Analytical Services, Inc.. Page 7 of 24

Pace Analytical Services, Inc.
e
aiCeArralytiiCal 980D Kincey Ave. Suite 100
Huntersville, NC 28078
wwwpacalabs.00m
[phone]
ANALYTICAL RESULTS
Project: Oulfalt 6118
Pace Project No,: 92205886
Sample: OUTFALL # 2 Lab ID: 92205886002 Collected: 06/18/14 16:00 Received: 06/18/14 16:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg/L
5.0
1
06/19/14 12:03
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:38
309-00-2
alpha-BHC
NO ug/L
0.050
1
06/25/14 11:12
06/29114 21:38
319-84-6
beta-611C
ND ug/L
0.050
1
06125114 11.12
06/29114 21:38
319-85-7
delta-BHC
ND ug/L
0-050
1
06/25/14 11:12
06/29/14 21:38
319-86-8
gamma-BHC (Lindane)
ND ug/L
0.050
1
06/25/14 11:12
06129/14 21:38
58-89-9
Chlordane (Technical)
ND ugiL
0.50
1
06/25/14 11:12
06/29114 21:38
57-74-9
4,4'-DOD
NO ug/L
0-050
1
06/25114 11:12
06/29/14 21:38
72-54-8
4,4'-DDE
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:38
72-55-9
4,4'-DDT
NO ug/L
0.050
1
06/25/14 1112
06/29/14 21:38
50-29-3
Dieldrin
NO ug/L
0,050
1
06/25/14 11:12
05/29/14 21:38
60-57-1
Endosulfan I
NO ug/L
0,050
1
06/25/14 11:12
06/29/14 21:38
959-98-8
Endosulfan II
NO ug/L
0,050
1
06/25/14 11:12
06129/14 21:38
33213-65-9
Endosulfan sulfate
NO ug/L
0.050
1
06/26/14 11:12
06/29/14 21:38
1031-07-8
Endrin
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:38
72-20-8
Endrin aldehyde
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:38
7421-93-4
Heptachlor
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:38
76-44-8
Heptachlor epoxide
NO ug/L
0.050
1
06/25/14 11:12
06/29/14 21:38
1024-57-3
PCB-1016 (Aroclor 1016)
NO ug/L
0.50
1
06/25/14 11:12
06/29/14 21:38
12674-11-2
PCB-1221 (Aroclor 1221)
NO ug/L
0.50
1
06/25114 11:12
06/29/14 21:38
11104.28-2
PCB-1232 (Aroclor 1232)
ND ug/L
0-50
1
06/25114 11.12
06129114 21:38
11141-16-5
PCB-1242 (Aroclor 1242)
NO ug/L
0.50
1
06125/14 11:12
06/29/14 21:38
53469-21-9
PCB-1248 (Aroclor 1248)
NO ug/L
0.50
1
06/25/14 11:12
06/29/14 21:38
12672-29-6
PCB-1254 (Aroclor 1254)
NO ug/L
0-50
1
06125/1411A2
06/29/14 21:38
11097-69-1
PCB-1260 (Aroclor 1260)
NO ug/L
0.50
1
06/25/14 1112
06/29/14 21:38
11096-82-5
Toxaphene
NO ug/L
0.50
1
06/25/14 11:12
06/29/14 21:38
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
52 %
20-110
1
06/25/14 11:12
06/29/14 21:38
877-09-8
Decachlorobiphenyl (S)
59 %
20-138
1
06/25/14 11:12
06/29/14 21:38
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA
200.7
Copper
100 ug/L
5.0
1
06/19/14 12:40
06/20/14 20:00
7440-50-8
Lead
11.5 ug/L
5.0
1
06/19/14 12:40
06/20/14 20:00
7439-92-1
Zinc
128 ug/L
10.0
1
06/19/14 12:40
06/20/14 20:00
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method:
EPA 625
Acenaphthene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
83-32-9
Acenaphthylene
NO ug/L
5.0
1
06125/14 12:30
0&27/14 21:33
208-96-8
Anthracene
NO ug/L
5.0
1
06/25114 12:30
06/27/14 21:33
120-12-7
Benzo(a)anthracene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
56-55-3
Benzo(a)pyrene
NO ug/L
5.0
1
06/25/14 12:30
06/27114 21:33
50-32-8
Benzo(b)fluoranthene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
205-99-2
Benzo(g,h,i)perylene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
191-24-2
Benzo(k)fluoranthene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
207-08-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 07/07/2014 03:57 PM without the written consent of Pace Analytical Services, Ir Page 8 of 24

,�aceAnalj&al"
www.paceleb&=n
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Outfall 6/18
Pace Project No.: 92205886
Sample: OUTFALL # 2 Lab ID: 92205886002 Collected: 06/18/14 16!00 Received: 06/18/14 16:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
4-Bromophenylphenyl ether
ND uglL
5.0
1
06/25/14 12:30
06/27/14 21:33
101-55-3
Butylbenzylphthalate
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
85-68-7
4-Chloro-3-methylphenol
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
59-50-7
bis(2-Chloroethoxy)methane
NO ug/L
10.0
1
06/25/14 12:30
06/27/14 21:33
111-91-1
bis(2-Chloroethyl) ether
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
111-44-4
bis(2-Chloroisopropyl) ether
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
108-60-1
2-Chloronaphthalene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
91-58-7
2-Chlorophenol
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
7005-72-3
Chrysene
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
218-01-9
Dibenz(a,h)anthracene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
53-70-3
3,3'-Dichlorobenzidine
NO uglL
25.0
1
06/25/14 12:30
06/27/14 21:33
91-94-1
2,4-Dichlorophenol
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
120-83-2
0iethyl phthalate
ND uglL
5.0
1
06/25/14 12:30
06/27/14 21:33
84-66-2
2,4-Dimethyl phenol
NO ug1L
10.0
1
06/25/14 12:30
06/27/14 21:33
105-67-9
Dimethylphthaiate
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
131-11-3
Di-n-butyiphthalate
NO ug1L
5.0
1
06/25/14 12:30
06/27/14 21:33
84-74-2
4,6-Dinitro-2-methylphenol
NO ug1L
20.0
1
06/25/14 12:30
06/27/14 21:33
534-52-1
2,4-Dinitrophenol
NO ug/L
50.0
1
06/25/14 12:30
06/27/14 21:33
51-28-5
2,4-Dinitrotoluene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
121-14-2
2,6-Dinitrotoluene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
606-20-2
Di-n-octylphthalate
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
117-84-0
bis(2- Ethyl hexyl)phthalale
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
1W-81-7
Fluoranthene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
206-44-0
Fluorene
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
87-68-3
Hexachlorobenzene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
118-74-1
Hexachlorocyclopentadiene
NO ug/L
10.0
1
06/25/14 12:30
06/27/14 21:33
77-47-4
Hexachloroethane
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
67-72-1
Indeno(1,2,3-cd)pyrene
NO ug/L
5.0
1
06/25/14 12:30
06127/14 21:33
193-39-5
Isophorone
NO ug/L
10.0
1
06/25/14 12:30
06/27/14 21:33
78-59-1
Naphthalene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
91-20-3
Nitrobenzene
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
98-95-3
2-Nitrophenol
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
88-75-5
4-Nitrophenol
NO ug/L
50.0
1
06/25/14 12:30
06/27/14 21:33
100-02-7
N-Nilrosodimethylamine
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
62-75-9
N-Nitroso-di-n-propylamine
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
621-64-7
N-Nitrosodiphenylamine
NO ug/L
10.0
1
06/25/14 12:30
06/27/14 21:33
86-30-6
Pentachlorophernol
NO ug/L
10.0
1
06/25/14 12:30
06/27/14 21:33
87-86-5
Phenanthrene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
85-01-8
Phenol
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
108-95-2
Pyrene
NO ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
5.0
1
06/25/14 12:30
06/27/14 21:33
120-82-1
2,4,6-Trichlorophenol
NO ug/L
10.0
1
06/25/14 12:30
06/27/14 21:33
88-06-2
Surrogates
Nitrobenzene-d5 (S)
36 %
10-120
1
06/25/14 12:30
06/27/14 21:33
4165-60-0
2-Fluorobiphenyl (S)
38 %
15-120
1
06/25/14 12:30
06/27/14 21:33
321-60-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2014 03:57 PM ',out the written consent of Pace Analytical Services, Inc..
Page 9 of 24 `'

I
eAliali+cal
waw.paC3debs.own
ANALYTICAL RESULTS .
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Outfal 16/18
Pace Project No.: 92205886
Sample: OUTFALL f# 2 Lab ID: 92205886002 Collected: 06/18/14 16:00 Received: 06/18/14 16:55 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Surrogates
Terphenyl-d14 (S)
61 %
11-131
1
06/25/14 1210
06/27114 21:33
1718-51-0
Phenol-d6 (S)
13 %
10-120
1
06/25/14 12:30
06/27/14 21.33
13127-88-3
2-Fluorophenol (S)
20 %
10-120
1
06/25/14 12:30
06127/14 21.33
367-12-4
2,4,6•Tribromophenol (S).
43 %
10-137
1
06125/14 12:30
06/27114 21:33
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND ug/L
2,0
1
06/28/14 17:44
71-43-2
Bromodichloromethane
ND ug)L
2.0
1
06/28/14 17:44
75-27-4
Bromoform
NO ug1L
2.0
1
06/28/14 17:44
75.25.2
Bromomethane
ND ug/L
2.0
1
06/28114 17:44
74-83-9
Carbon tetrachloride
NO ug/L
2.0
1
06/28/14 17:44
W23-5
Chlorobenzene
NO ug/L
2.0
1
06/28/14 17.44
108-90.7
Chloroethane
ND ug/L
2,0
1
06/28/14 17A4
75-00-3
Chloroform
NO ug/L
2.0
1
06/28/14 17:44
67.66-3
Chloromethane
ND ug/L
2.0
1
06/28/14 17:44
74-87-3
Dibromochlorom ethane
ND ug/L
2.0
1
06/28/14 17:44
124-48-1
1,2-Dichlorobenzene
ND ug/L
2.0
1
06/28/14 17:44
95-50-1
1,3-Dichlorobenzene
NO ug/L
2.0
1
06/28/14 17:44
541-73-1
1,4-Dichlorobenzene
ND ug1L
2.0
1
06/28114 17:44
106-46-7
1,1-Dichloroethane
ND ug/L
2.0
1
0612811417.44
75-34-3
1,2-Dichloroethane
NO uglL
2.0
1
0612811417:44
107-06-2
1.1-Dichloroethene
NO ug/L
2.0
1
06/28/14 17:44
75-35-4
cis-1,2-Dichioroethene
NO ug/L
2,0
1
06/28114 17:44
156-59-2
trans-1,2-Dichloroethene
NO ug/L
2.0
1
0612811417:44
156-60-5
1,2-Dichloropropane
NO ug/L
2.0
1
06/28/14 17:44
78-87-5
cis- 1,3-Dichloro propene
NO ug/L
2.0
1
06/28/14 17:44
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
2.0
1
06128/1417:44
10061-02-6
Ethylbenzene
ND ug/L
2.0
1
06128/1417:44
100-41-4
Methylene Chloride
NO ug/L
2.0
1
06/28114 W7 44
75.09-2
1,1,2,2-Tetrachloroethane
NO ug/L
2.0
1
06/28/14 17:44
79-34-5
Tetra chloroethene
NO ug/L
2,0
1
06/28114 17:44
127-18-4
Toluene
NO ug/L
2.0
1
06/28114 17:44
108-88-3
1,1,1-Trichloroethane
ND ug/L
2.a
1
06/28114 17:44
71-55-6
1,1,2-Trichloroethane
ND ug/L
2.0
1
06/28114 17:44
79-00-5
Trichloroethene
NO ug/L
2.0
1
06/28114 17:44
79-01-6
Trichlorofluoromethane
NO ug/L
2.0
1
06128/14 17:44
75-69-4
Vinyl chloride
NO ug/L
2.0
1
06/28/14 17:44
75.01-4
Surrogates
4-Bromofluorobenzene (S)
92 %
70-130
1
06/28/14 17:44
460-00-4
Toluene-d8 (S)
98 %
70-130
1
06)28114 17:44
2037-26-5
1,2-Dlchloroethane-d4 (S)
100 %
70-130
1
06/28/14 17:44
17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 3A mglL 2.5 1 06124/1415:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in furl,
Date: 07107/2014 03:57 PM without the written consent or Pace Analytical Services, In- Page 10 of 24

aceAnaIXical
www.pacefed&WM
Pace Analytical Services, Inc.
9800 KinCey Ave. Suite 100
Hu ntersville, NC 29078
[phone]
QUALITY CONTROL DATA
Project: Oudall 6118
Pace Project No.: 92205886
QC Batch: GCSV117960 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92205886001, 92205886002
METHOD BLANK: 1224612 Matrix: Water
Associated Lab Samples: 92205886001, 92205886002
Blank deporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 0&19114 11:55
LABORATORY CONTROL SAMPLE: 1224613
Parameter Units
Oil and Grease mg/L
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 38.6 96 78-114
MATRIX SPIKE SAMPLE: 1224614
92205865004 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L ND 40 37.5 93 78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2014 03:57 PM out the written consent of Pace Analytical Services, Inc..
Page 11 of 24

Pace Analytical Services, Inc.
aceAnalytr'ea1 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pmtabs.com (704 )875-9092
Project: Outfa 116/18
Pace Project No.: 92205886
QC Batch: MPRP116256
QC Batch Method: EPA 200.7
Associated Lab Samples: 92205886001, 92205886002
METHOD BLANK: 1224807
Associated Lab Samples: 92205886001, 92205886002
Parameter Units
Copper
Lead
Zinc
ug/L
Lg/L
LgIL
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 5.0 06/2011418:47
ND 5.0 06/2011418.47
ND 10.0 06I20/1418:47
Qualifiers
LABORATORY CONTROL SAMPLE:
1224808
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Copper
ug/L
500
490 98 85-115
Lead
ug/L
500
487 97 85-115
Zinc
ug/L
500
470 94 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1224809
1224810
MS
MSD
92205590001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc,
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper ug/L
0.030
500
500
525
528
99
100
70-130
1
mg/L
Lead ug/L
ND
500
500
477
488
95
97
70-130
2
Zinc ug/L
0.11
500
500
570
578
93
94
70-130
1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1224811
MS
92205886001 Spike
Parameter Units Result Conc.
Copper ug/L 63.2 500
Lead ug/L 10.0 500
Zinc ug/L 113 500
1224812
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits RPD
500
551
552
98
98
70-130 0
500
500
505
98
99
70-130 1
500
581
584
94
94
70-130 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
' Date: 07/07/2014 03:57 PM without the written consent of Pace Analytical Services, it
r
Qual
Page 12 of 24

aceAnalytical
ww.pacelab&c=
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Outfall 6118
Pace Project No.: 92205886
QC Batch: MSV127386 Analysis Method: EPA624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92205886001, 92205886002
METHOD BLANK: 1231927
Associated Lab Samples: 92205886001, 92205886002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichloroethane
uglL
NO
2.0
06128/1414:46
1,1,2,2-Telrachloroethane
uglL
NO
2.0
06128/1414:46
1,1,2-Trichloroethane
uglL
NO
2.0
06128/1414:46
M-Dichloroethane
ug/L
NO
2.0
06128/1414:46
1,1-Dichloroethene
uglL
NO
2.0
0612811414:46
1,2-Dichlorobenzene
uglL
NO
2.0
06128/1414:46
1,2-Dichloroethane
uglL
NO
2.0
06128/1414:46
1,2-Dichloropropane
uglL
NO
2.0
06128/1414:46
1,3-Dichlorobenzene
uglL
NO
2.0
06128/1414:46
1,4-Dichlorobenzene
uglL
NO
2.0
06128/1414:46
Benzene
` uglL
NO
2.0
06/28/14 14:46
Bromod ichlorom ethane
ug/L
ND
2.0
06/28/1414:46
Bromoform
uglL
NO
2.0
06/28/1414:46
Bromomethane
uglL
NO
2.0
06128/1414:46
Carbon tetrachloride
uglL
NO
2.0
06/28/14 14:46
Chlorobenzene
uglL
NO
2.0
06128/1414:46
Chloroethane
uglL
NO
2.0
06/28/1414:46
Chloroform
uglL
NO
2.0
06/28/1414:46
Chloromethane
uglL
NO
2.0
06/28/1414:46
cis-1,2-Dichloroethene
uglL
NO
2.0
06/2811414:46
cis-1,3-Dichloropropene
ug1L
NO
2.0
06/28/1414:46
Dibromochloromethane
ug1L
NO
2.0
06/2811414:46
Ethylbenzene
ug1L
NO
2.0
06/28/1414:46
Methylene Chloride
ug1L
NO
2.0
06/28114 14:46
Tetrachloroethene
uglL
NO
2.0
06/2811414:46
Toluene
uglL
NO
2.0
06/2811414:46
trans- 1,2-Dichloroethene
ug/L
NO
2.0
06/2811414:46
trans- 1,3-Dichloropropene
ug1L
ND
2.0
06/2811414:46
Trichloroethene
ug1L
NO
2.0
06/2811414:46
Trichlorofluoromethane
ug1L
NO
2.0
06/2811414:46
Vinyl chloride
ug1L
NO
2.0
06/28/14 14:46
1,2-Dichloroethane-d4 (S)
%
97
70-130
06/28/14 14:46
4-Bromofluorobenzene (S)
%
99
70-130
06/28/14 14:46
Toluene-d8 (S)
%
99
70-130
06/28/14 14746
Qualifiers
LABORATORY CONTROL SAMPLE: 1231928
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,11-Trichloroethane ug1L 20 19.5 98 52-162
1,1,2,2-Tetrachloroethane uglL 20 19.6 98 46-157
Results presented on this page are In the units indicated by the 'Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2014 03:57 PM iut the written consent of Pace Analytical Services, Inc.. Page 1� of 24

acmnalyl#lcal
mrtepaOfs &COO
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Outfall 6/18
Pace Project No.: 92205886
LABORATORY CONTROL SAMPLE:
Parameter
1231928
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,2-Trichloroethane
ug/L
20
19.7
99
52-150
1,1-Dichloroethane
ug/L
20
18.8
94
59-155
1,1-Dichloroethene
ug/L
20
22.3
i11
1-234
1,2-Dichlorobenzene
ug/L
20
21.3
106
18-190
1,2-Dichloroethane
ug/L
20
19.2
96
49-155
1,2-Dichloropropane
ug/L
20
20.1
100
1-210
1,3-Dichlorobenzene
ug/L
20
21.3
106
59-156
1,4-Dichlorobenzene
ug/L
20
20.8
104
18-190
Benzene
ug/L
20
20.8
104
37-151
Bromodichloromethane
ug/L
20
21.2
106
35-155
Bromoform
ug/L
20
20.5
102
45-169
Bromomethane
ug/L
20
18,0
90
1-242
Carbon tetrachloride
ug/L
20
21.6
108
70-140
Chlorobenzene
ug/L
20
21.1
105
37-160
Chloroethane
ug/L
20
21,5
108
14-230
Chloroform
ug/L
20
21.1
106
51-138
Chloromethane
ug/L
20
20.3
101
1-273
cis-1,2-Dichloroethene
ug/L
20
21.3
107
68-146
cis-1,3-Dichloropropene
ug/L
20
20.5
102
1-227
Dibromochlorom ethane
ug/L
20
21.9
110
53-149
Ethylbenzene
ug/L
20
20.3
101
37-162
Methylene Chloride
ug/L
20
21.5
107
1-221
Tetrachloroethene
ug1L
20
20.3
102
64-148
Toluene
ug/L
20
20,0
100
47-150
trans- 1,2-Dich loroethene
ug/L
20
22,1
110
54-156
trans- 1, 3-Dich loropropene
ug/L
20
20.8
104
17-183
Trichloroethene
ug/L
20
20.4
102
71-157
Trichlorofluoromethane
ug/L
20
25.2
126
17-181
Vinyl chloride
ug/L
20
21.4
107
1-251
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
98
70-130
Qualifiers
Results presented on this page are In the units indicated by the -Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2014 03:57 PM without the written consent of Pace Analytical Services, P
Page 14 of 24

aceAnalytical
www.pacWabs.corn
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Outfall 6/18
Pace Project No.: 92205886
QC Batch: OEXT128496 Analysis Method: EPA 608
OC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB
Associated Lab Samples: 92205886001, 92205886002
METHOD BLANK: 1228772
Matrix:
Water
Associated Lab Samples: 92205886001, 92205886002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
4,4'-DDD
ug1L
ND
0.050
06/29/14 19:17
4,4'-DDE
ug1L
ND
0.050
0612911419:17
4,4'-DDT
ug/L
ND
0.050
06129/1419:17
Aldrin
ug/L
ND
0.050
06129/1419:17
alpha-SHC
ug/L
ND
0,050
06/29/14 19:17
beta-BHC
ug/L
ND
0.050
06129/1419:17
Chlordane (Technical)
ug/L
ND
0.50
06/29/14 19:17
delta-BHC
ug/L
ND
0.050
06129/1419:17
Dieldrin
ug/L
ND
0.050
06/29/14 19:17
Endosulfan 1
ug/L
ND
0,050
06/29/14 19:17
Endosulfan II
ug/L
ND
0.050
06/29/14 19:17
Endosulfan sulfate
ug/L
ND
0.050
06/29/14 19:17
Endrin
ug/L
ND
0,050
06/29/14 19:17
Endrin aldehyde
ug/L
ND
0.050
06/29/14 19:17
gamma-BHC (Lindane)
ug/L
ND
0,050
06/29/14 19:17
Heptachlor
ug1L
ND
0.050
06129/1419:17
Heptachlor epoxide
ug/L
ND
0,050
06/29/14 19:17
PCB- 1016 (Aroclor 1016)
ug/L
ND
0.50
06/29/14 19:17
PCB-1221 (Aroclor 1221)
ug/L
ND
0.50
06/29/14 19:17
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
06/29/14 19:17
PCB-1242 (Aroclor 1242)
ug/L
ND
0.50
06/29/14 19:17
PCB-1248 (Aroclor 1248)
ug/L
ND
0.50
06/29/14 19:17
PCB-1254 (Aroclor 1254)
ug/L
ND
0.50
06/29/14 19:17
PCB-1260 (Aroclor 1260)
ug1L
ND
0.50
06/29/14 19:17
Toxaphene
ug1L
ND
0.50
06/2911419:17
Decachlorobiphenyl (S)
%
87
20-138
06/29/14 19:17
Tetrachloro-m-xylene (S)
%
64
20-110
06/29/14 19:17
LABORATORY CONTROL SAMPLE:
1228773
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
4,4'-DDD
ug1L
.25
0.17
68
31-141
4,4'-DDE
ug/L
.25
0.15
62
30-145
4,4'-DDT
ug/L
.25
0.18
72
25-160
Aldrin
ug1L
.25
0,089
36
42-122 LO
alpha-BHC
ug1L
.25
0.17
69
37-134
beta-BHC
ug1L
.25
0.18
74
17-147
delta-BHC
ug/L
.25
0.18
74
19-140
Dieldrin
ug/L
.25
0.16
66
36-146
Endosulfan I
ug/L
.25
0.17
69
45-153
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2014 03:57 PM lout the written consent of Pace Analytical Services, Inc.. Page 15 of 24 .,

Pace Analytical Services, Inc.
aceARalytitcat • 9800 Ki1 lanceyAve. Suite 100
ntersville, NC 20078
W+:pt 3'VV r [phone]
QUALITY CONTROL DATA
Project: Outfall 6118
Pace Project No_: 92205886
LABORATORY CONTROL SAMPLE: 1228773
Parameter
Units
Spike
Conc.
Endosulfan it
ug/L
.25
Endosulfan sulfate
ug/L
.25
End rin
ug/L
.25
Endrin aldehyde
uglL
25
gamma-BHC (Lindane)
ug1L
.25
Heptachlor
ug/L
.25
Heptachlor epoxide
ug/L
.25
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
0.19
77
1-202
0.20
82
26-144
0.18
74
30-147
0.17
69
50-150
0.17
69
32-127
0.11
43
34-111
0.16
64
41-126
86
20-138
68
20-110
Results presented on this page ere In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
x Date: 07/07/2014 03:57 PM without the written consent of Pace Analytical Services, Ins
4 -
Page 16 of 24

aceAnalytical
www.pacelabs o=
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)B75-9092
QUALITY CONTROL DATA
Project: Outfall 6/18
Pace Project No.: 92205886
QC Batch: OEXT128478 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92205886001, 92205886002
METHOD BLANK: 1228135
Associated Lab Samples: 92205886001, 92205886002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,2,4-Trichicrobenzene
ug1L
NO
5.0
06126/14 08:59
2,4,6-Trichlorophenol
ug/L
NO
10.0
06/26114 08:59
2,4-Dichlorophenol
ug/L
NO
5.0
06126114 08:59
2.4-Dimelhylphenol
ug/L
ND
10.0
06/26/14 08:59
2,4-Dinitrophenol
ug/L
NO
50.0
06126/14 08:59
2,4-Dinitrotoluene
ug/L
NO
5.0
06/26/14 08:59
2,6-Dinitrololuene
ug/L
NO
5.0
06/26/14 08:59
2-Chloronaphthalene
ug/L
NO
5.0
06/26/14 08:59
2-Chlorophenol
ug/L
NO
5.0
06/26/14 08:59
2-Nitrophenol
ug/L
NO
5.0
06/26/14 0&59
3,3'-Dichiorobenzidine
ug/L
NO
25.0
06/26/14 08:59
4,6-Dinitro-2-methylphenol
ug/L
ND
20.0
06/26/14 08:59
4-Bromophenylphenyl ether
ug/L
ND
5.0
06/26/14 08:59
4-Chloro-3-methylphenol
ug/L
NO
5.0
06/26/14 08:59
4-Chlorophenylphenyl ether
ug/L
NO
5.0
06/26/14 08:59
4-Nitrophenol
ug/L
NO
50.0
06/26/14 08:59
Acenaphthene
ug/L
NO
5.0
06/26/14 08:59
Acenaphthylene
ug/L
ND
5.0
06/26/14 08:59
Anthracene
ug/L
ND
5.0
06126/14 08-59
Benzo(a)anthracene
ug/L
ND
5.0
06/26114 08:59
Benzo(a)pyrene
ug/L
ND
5.0
06/26/14 08.59
Benzo(b)tluoranlhene
ug/L
NO
5.0
06/26/14 08:59
Benzo(g,h,i)pefylene
ug/L
NO
5.0
06/26/14 08:59
Benzo(k)fluoranthene
ug/L
NO
5.0
06/26/14 06:59
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
06/26/14 08:59
bis(2-Chloroethyl) ether
ug/L
NO
5.0
06/26/14 08:59
bis(2-Chloroisopropyl) ether
ug/L
NO .
5.0
06/26/14 08:59
bis(2- Ethyl hexyl)phthalate
ug/L
NO
5.0
06/26/14 08:59
Bu tyl benzylphtha late
ug/L
NO
5.0
06/26/14 08:59
Chrysene
ug/L
NO
5.0
06/26/14 08:59
Di-n-butylphthalate
ug/L
NO
5.0
06/26/14 08:59
Di-n-octylphthalate
ug/L
NO
5.0
06/26/14 08:59
Dibenz(a,h)anthracene
ug/L
NO
5.0
06/26/14 08:59
Diethylphtha late
ug/L
NO
5.0
06/26/14 08:59
Dimethylphthalate
ug/L
ND
5.0
06/26/14 08.59
Fluoranthene
ug1L
NO
5.0
06126114 08:59
Fluorene
ug/L
NO
5.0
06126114 08:59
Hexachloro-1,3-butadiene
ug/L
ND
5.0
06126/14 08:59
Hexacftlorobenzene
ug/L
NO
5.0
06/26/14 08:59
Hexachlorocyclopentadiene
ug/L
NO
10.0
06/26/14 08:59
Hexachloroethane
ug/L
NO
5.0
06/26/14 08:59
Qualifiers
Results presented on this page are In the units indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2014 03:57 PM out the written consent of Pace Analytical Services, Inc.. Page 17 of 24

aceAnalytrcal.
www.pamiabs.com
QUALITY CONTROL DATA
Project: Outfall 6118
Pace Project No.: 92205886
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1228135
Associated Lab Samples: 92205886001, 92205886002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed Qualifiers
Indeno(1,2,3-od)pyrene
ug/L -
ND
5.0
06/26/14 08:59
Isophorone
ug/L
ND
10.0
06/26/14 08:59
N-Nitroso-di-n-propylamine
ug1L
ND
5.0
06/26/14 08:59
N-Nitrosodimethylamine
ug1L
ND
5.0
06/26/14 08:59
N-Nitrosodiphenylamine
ug1L
ND
10.0
06/26/14 08:59
Naphthalene
ug1L
ND
5.0
06/26/14 08:59
Nitrobenzene
ug1L
ND
5.0
06/26/14 08:59
Pentachlorophenol
ugIL
ND
10.0
06/26/14 08:59
Phenanthrene
ug/L
ND
5.0
06/26/14 08:59
Phenol
ug/L
ND
5.0
06/26/14 08:59
Pyrene
ug1L
ND
5.0
06/26114 08:59
2,4,6-Tribromophenol (S)
%
75
10-137
06/26/14 08:59
2-Fluorobiphenyl (S)
%
61
15-120
06/26/14 08:59
2-Fluorophenol (S)
%
43
10-120
06/26/14 08:59
Nitrobenzene-d5 (S)
%
68
10-120
06/26/14 08:59
Phenol-d6 (S)
%
32
10-120
06/26/14 08:59
Terphenyl-d14 (S)
%
76
11-131
06/26/14 08:59
LABORATORY CONTROL SAMPLE & LCSD: 1228136
Parameter Units
Spike
Cone.
1228137
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
28.5
27.6
57
55
44-142
3
30
2,4,6-Trichlorophenol
ug/L
50
36.2
36.0
72
72
37-144
1
30
2,4-Dichlorophenol
ug1L
50
34.1
33.2
68
66
1-191
3
30
2,4-Dimethyl phenol
ug1L
50
34.3
33.7
69
67
32-119
2
30
2,4-Dinitrophenol
ug1L
250
320
319
i28
128
1-181
0
30
2,4-Dinitrotoluene
ug/L
50
49.2
47,6
98
95
39-139
3
30
2,6-Dinitrotoluene
ug1L
50
45.1
45.7
90
91
50-158
1
30
2-Chloronaphthalene
ug1L
50
32.6
30.7
65
61
60-118
6
30
2-Chlorophenol
ug/L
50
35.5
35.4
71
71
23-134
0
30
2-Nitrophenol
ug/L
50
40.7
41.4
81
83
29-182
2
30
3,3'-Dichlorobenzidine
ug/L
100
83.0
78.0
83
78
1-262
6
30
4,6-Dinitro-2-methylphenol
ug/L
100
120
122
120
122
1-181
1
30
4-Bromophenyiphenyl ether
ug/L
50
31.4
30.9
63
62
53-127
2
30
4-Chloro-3-methylphenol
ug/L
100
66.2
66.6
66
67
22-147
1
30
4-Chlorophenylphenyl ether
ug/L
50
35.0
34.0
70
68
25-158
3
30
4-Nitrophenol
ug/L
250
89.2
84.9
36
34
1-132
5
30
Acenaphthene
ug/L
50
32.6
31.0
65
62
47-145
5
30
Acenaphthylene
ug/L
50
34.2
32.8
68
66
33-145
4
30
Anthracene
ug/L
50
34.1
31.8
68
64
1-166
7
30
Benzo(a)anthracene
ug1L
50
35.4
33.8
71
68
33-143
5
30
Benzo(a)pyrene
ug/L
50
37.4
35.7
75
71
17-163
5
30
Benzo(b)fluoranthene
ug1L
50
36.3
32.3
73
65
24-159
12
30
Benzo(g,h,i)perylene
ug1L
50
35.4
33A
71
67
1-219
6
30
Results presented on this page are In the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
' Date: 07/07/2014 03:57 PM without the written consent of Pace Analytical Services, Ir Page 18 of 24

aceAnalytical
www,pacelebs cam
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Outfall 6118
Pace Project No.: 92205886
LABORATORY CONTROL SAMPLE & LCSD: 1228136
1228137
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD
Benzo(k)fluoranthene
ug/L
50
34.3
33A
69
67
11-162
3
30
bis(2-Chloroethoxy)methane
ug/L
50
35.4
33.8
71
68
33-184
4
30
bis(2-Chloroethyl) ether
ug/L
50
37.8
37.0
76
74
12-158
2
30
bis(2-Chloroisopropyl) ether
ug/L
50
36.8
34.8
74
70
36-166
5
30
bis(2-Ethylhexyl)phthalate
ug/L
50
41.7
42.0
83
84
8-168
1
30
Butylbenzylphthalate
ug/L
50
39.5
40.5
79
81
1-152
3
30
Chrysene
ug/L
50
35.0
32.8
70
66
17-168
6
30
Di-n-butytphthalate
ug/L
50
40.2
38.4
80
77
1-118
5
30
Di-n-octylphthalate
ug/L
50
45.3
45.1
91
90
4-146
0
30
Dibenz(a.h)anthracene
ug/L
SO
37.5
35.3
75
71
1-227
6
30
Diethylphthalate
ug/L
50
37.0
36.0
74
72
1-114
3
30
Dimethylphthalate
ug/L
50
35.4
34.5
71
69
1-112
2
30
Fluoranthene
ug/L
50
38.9
34.8
78
70
26-137
11
30
Fluorene
ug/L
50
34.7
33.3
69
67
59-121
4
30
Hexachloro-1,3-butadiene
ug/L
50
26.7
24.8
53
50
24-116
7
30
Hexachlorobenzene
ug/L
50
30.6
29.2
61
58
1-152
5
30
Hexachlorocyclopentad iene
ug/L
50
34.8
33.5
70
67
25-150
4
30
Hexachloroethane
ug/L
50
29.3
29.2
59
58
40-113
0
30
Indeno(1,2,3-cd)pyrene
ug/L
50
29.6
28.0
59
56
1-171
6
30
Isophorone
ug/L
50
40.0
39.1
80
78
21-196
2
30
N-Nitroso-di-n-propylamine
ug/L
50
41.8
40.2
84
80
1-230
4
30
N-Nitrosodimethylamine
ug/L
50
24.4
24.8
49
50
25-150
1
30
N-Nitrosodiphenylamine
ug/L
50
32.5
31.2
65
62
25-150
4
30
Naphthalene
ug/L
50
30.9
29.2
62
58
21-133
5
30
Nitrobenzene
ug/L
50
42.0
40.6
84
81
35-180
3
30
Pentachtorophenol
ug/L
100
86.1
85.8
86
86
14-176
0
30
Phenanthrene
ug/L
50
32-3
30.2
65
60
54-120
7
30
Phenol
uglL
50
16A
16.4
33
33
5-112
0
30
Pyrene
ug/L
50
31.8
32.8
64
66
52-115
3
30
2,4,6-Tribromophenol (S)
%
85
83
10-137
2-Fluorobiphenyl(S)
%
64
62
15-120
2-Fluorophenol(S)
%
44
44
10-120
Nitrobenzene-d5(S)
%
71
69
10-120
Phenol-d6(S)
%
32
32
10-120
Terphenyl-d14 (S)
%
66
67
11-131
Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit Is presented to tho right of the result.
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 07/07/2014 03:57 PM out the written consent of Pace Analytical Services, Inc.. Page 19 of 24 ''

aceAnalytical
wwwpecelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Outfal 16118
Pace project No.: 92205886
QC Batch: WET131761 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92205886001, 92205886002
METHOD BLANK: 1228192 Matrix: Water
Associated Lab Samples: 92205886001, 92205886002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 06/24/14 15:50
LABORATORY CONTROL SAMPLE: 1228193
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 204 82 80-12D
SAMPLE DUPLICATE: 1228234
92205876001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 108 98.0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of Who rosult.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
•Date: 07/07/2014 03:57 PM without the written consent of Pace Analytical Services, In- Page 20 of 24

lacieAnalyticalo
www.pecefabs.wm
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Outfall 6118
Pace Project No.: 92205886
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LOD - Limit of Detection.
LOQ - Limit of Quantitation.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
L0 Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2014 03:57 PM out the written consent of Pace Analytical Services, Inc.. Page 21 of 24

Pace Analytical Services, Inc.
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville, NC 28078
WWW'bs.com {704}875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Outfall 6118
Pace Project No.:
92205886
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92205886001
OUTFALL # 1
EPA 1664E
GCSV117960
92205886002
OUTFALL # 2
EPA 1664E
GCSV117960
92205886001
OUTFALL # 1
EPA 3510
OEXT128496
EPA 608
GCSV118050
92205886002
OUTFALL # 2
EPA 3510
OEXT128496
EPA 608
GCSV118050
92205886001
OUTFALL # 1
EPA 200.7
MPRP116256
EPA 200.7
ICP114691
92205886002
OUTFALL # 2
EPA 200.7
MPRP116256
EPA 200.7
ICP114691
92205886001
OUTFALL # 1
EPA 625
0EXT128478
EPA 625
MSSV19305
92205886002
OUTFALL # 2
EPA 625
0EXTI28478
EPA 625
MSSV19305
92205886001
OUTFALL # 1
EPA 624
IVISV127386
92205886002
OUTFALL # 2
EPA 624
MSV127386
92205886001
OUTFALL # 1
SM 2540D
WET131761
92205886002
OUTFALL # 2
SM 2540D
WET131761
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
'Date: 07/07/2014 03:57 PM without the written consent of Pace Analytical Services, Ir
Page 22 of 24

1�2ceAnalytical'
CHAIN -OF -CUSTODY / Analytical Request Document
The Chairs-of-Custady is a LEGAL DOCUMENT- AD relevant fiekis mast t)e completed awuratelly.
rn 4
(D
Page: Of Cb
Section A Section B Section C
fO
17 87773
Required Client Information: Required Project Information: Invoice Information:
Cornpawt Report Attention:
P
Address:
CopyTo:
Company Name;
R LATORY
z.
Address:
F NPDES f- GROUND WATER r DRINKING WATER
r UST f- RCRA OTHER
Emesl To:
Order No.;
pow Cluoto
Ralarence:
Fax;
Project Name:
Pace "ea
?Site , Location
Manager;
Requested Due dateMAT:
Project Number
Pace Profile 4:
e--,
d6�ted'Ariaiysis
Flit
(YIN)
Section D Matrix Codes
I
R*quUW Client information MATRIX I CODE
COLLECTED
Preservatives
. 5.
2:C
a
Drinking Water DW
z
0
Water wr
waste Walar VVw
COMPOSME
COMPOWIF
Product P
SofifSofid SL
to
SAMPLE ID oil OL
Wipe M
(A-Z, 0-9 /,-) M AR
w
¢
LL?
z
Sample lDs MUST BE UNIQUE Tissue TS
0
0
Lu
dL
OT
0
X
Lu
ul
0
0
r-
(J
U-
0
cc
V
-t2
0
CL
Z
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DATE
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Ewe
TIME
Z
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2
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Pace Project NoJ Lab I.D.
oc) i
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2 is 0 dbrir el
acid-T
L'a
-7
I ei 2 2,42
—
—
—
—
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—
10
,11
-- I . 2 .-
RELINQUISHED BY I AFFILIATION
DATE
-14ME
N EPTEDBYIAFFILIATIO
DATE
SAMPLE CONDITIONS
-if.rti- Phi- zr 7,
11 W:L
SAMPLER. NAME AND SIGNATURE
V
c
ORIGINAL PRINT Name of SAMPLER:
a
z
E
SIGNATURE of SAMPLER: DATE Signed I
m
�Mmmoryy):
—J
mtPOnm wb: 11Y BWKL9 ft' bFM YOV are AccepUng PaoWs NET 30 day payment terms and pgreeft to late OftGEW 011.5% per n3onth for any invoices nqR paid withiri 3D days. F-ALL-0-020rev.07.15-MaV-2007

Document Name: Sample Condition Upon
Document Revised: June 10, 2014
?ac�Analytical*Rece€
t SCUR
Pa e 1 of 2
Document No.:
Issuing Authorities:
acaoAe-com
I
F-ASV-CS-003-rev.14
Pace Asheville Quality Office
Client Name;
Courier (Circle): Fed Ex UPS LISPS Client Commercial Paoe Other
Custody Seal on Cooler/Box Present: yes no Seals intact: ❑ yes R no
Packing Material: ElBu Bubble Bags E None Other
Thermometer Used: Gun#3 -i302 9 Type of Ice: Wet Blue None Samples on ice, cooling process has begun
IR Gun #4 SN:140290365 Other:
Temp Correction Factor: Add 1 Subtract 4 .0 C
Corrected Cooler Temp.: 12 ,1 _ C
Temp should be above freezing to 6"C
Biological Tissue Is Frozen: Yes No N/A
Comments:
Date and Ins: als of po o
content
exa [Wing
�
Chain of Custody Present:
0<x
Ono
Ell
1.
Chain of Custod Filled Out:
(WKSW
ENO
❑NIA
2.
Chain of Custody Relinquished:
Ye
❑No
❑NIA
3.
Sampler Name & Signature on COC:
2o
❑No
El NIA
4.
Samples Arrived within Hold Time:
Yes
0NV
❑NIA
5.
Short Hold Time Analysis (<72hr):
Oyes
l
❑NIA
6.
Rush Turn Around Time Re uested:
Oyes
No
❑NIA
7.
Sufficient Volume:
❑No
❑NIA
8.
Correct Containers Used:
-Pace Containers Used:
Z��
Ono
Ono
El NIA
0N1A
9.
Containers Intact:
C4.
❑No
ON/
10.
Filtered volume received for Dissolved tests
❑Ye
ONO
❑ /A
11.
Sample Labels match COC:
-Includes dateltlme/ID/Anal sis Matrix:
es
W
Ono
❑il
12,
All containers needing preservation have been cher-ked.
All containers needing preservatlon are found to be in
compliance with EPA recommendation.
exceptions VOA, coliform, T , O&G, -1 (water)
was
yes
❑No ❑NIA
❑No ❑NIA
13.
Samples checked for dechlorination:
La<es
©No
NIA
14.
Meads ace in VOA Vials >6mm2:
❑Yes
91ro
W !A
15.
Trip Blank Present:
Blank Custody Seals Present
Pace Trip Blank Lot # if purchased):
Oyes
❑Yes
14
�#No
fVIATrip
Client Notification/ Resolution:
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review:
SRF Review: z/_,_ Date: I C rs i-4
Note: Whenever there is a discrepancy affecting Nol Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y 1 N
Page 24 of 24

•
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
July 15, 2014
Gerald Runkles
Pentair Valves & Controls
953 Old US Hwy 70
Black Mountain, NC 28711
RE: Project: SW non comp 7/10/2014
Pace Project No.: 92208805
Dear Gerald Runkles:
Enclosed are the analytical results for sample(s) received by the laboratory on July 10, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical, Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
% without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnalytical
WWW..pecefebs.cvm
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW non comp 7/1012014
Pace Project No,: 92208805
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
FloddalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 10

4ceAnalytical"
www.paceablown
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: SW non comp 7/1012014
Pace Project No.: 92208805
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92208805001
Lugger
EPA 200.7
JMW
3
PASI-A
92208805002
Upstream
EPA 200.7
JMW
3
PASI-A
92208805003
Downstream
EPA 200.7
JMW
3
PASI-A
92208805004
Rain Gutter Front
EPA 200.7
JMW
3
PASI-A
92208805005
Rain Gutter Back
EPA 200.7
JMW
3
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 10

Pace Analytical Services, Inc.
aceAnalytical 9800 Kincey Ave. Suit 100
Huntersville, NC 28078
WWW.000wabtaom (704 )875-9092
Project:
Pace Project No.:
SW non comp 7/10/2014
92208805
Lab Sample ID
Client Sample ID
Method
Parameters
92208805001
Lugger
EPA 200.7
Copper
EPA 200.7
Lead
EPA 200.7
Zinc
92208805002
Upstream
EPA 200.7
Copper
EPA 200.7
Lead
EPA 200.7
Zinc
92208805003
Downstream
EPA 200.7
Copper
EPA 200.7
Lead
EPA 200.7
Zinc
92208805004
Rain Gutter Front
EPA 200.7
Zinc
92208805005
Rain Gutter Back
EPA 200.7
Zinc
SUMMARY OF DETECTION
Result Units
Report Limit
Analyzed
26.1 ug/L
5.0
07/14/14 16:56
29.2 ug/L
5.0
07/14/14 16:56
71.0 ug/L
10.0
07/14/14 16:56
30.8 ug/L
5.0
07/14114 17:00
10.0 ug/L
5.0
07/14114 17:00
34.9 ug/L
10.0
07/14/14 17:00
25.7 ug/L
5.0
07/14/14 17:13
5.4 ug/L
5.0
07/14/14 17:13
30.8 ug/L
10,0
07/14/14 17:13
25.8 ug/L
10.0
07/14/14 17:16
82.7 ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
10.0 07/14/14 17:19
Qualifiers
Page 4 of 10

' v
aceAnalyfical
WW.paW8b&c=
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
ANALYTICAL RESULTS
Project: SW non comp 7/10/2014
Pace Project No.: 92208805
Sample: Lugger Lab ID: 92208805001 Collected: 07/10/14 00:00 Received: 07/10/14 15:51 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper 26.1 ug/L 5.0 1 07/11/1419:45 07/14/1416:56 7440-50-8
Lead 29.2 ug/L 5.0 1 07/11/14 19:45 07/14/14 16:56 7439-92-1
Zinc 71.0 ug/L 10.0 1 07/11/14 19:45 07/14/14 16:56 7440-66-6
Sample: Upstream
Lab ID: 92208805002
Collected: 07/10/14 00:00
Received: 07/10114 15:51 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared
Analyzed
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
30.8 uglL
5.0 1
07/11/14 19:45
0711411417:00
7440-50-8
Lead
10.0 uglL
5.0 1
07111/1419:45
07/1411417:00
7439-92-1
Zinc
34.9 uglL
10.0 1
07/11/14 19:45
07/1411417:00
7440-66-6
Sample: Downstream Lab ID: 92208805003 Collected: 07/10/14 00:00 Received: 07/10/14 15:51 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper 25.7 ug1L 5.0 1 07/11/14 19:45 07/14/14 17:13 7440-50-8
Lead 5.4 ug/L 5.0 1 07/11/14 19:45 07/14/14 17:13 7439-92-1
Zinc 30.8 ug/L 10.0 1 07/11/14 19:45 07/14/14 17:13 7440-66-6
Sample: Rain Gutter Front Lab ID: 92208805004 Collected: 07/10/14 00:00 Received: 07/10/14 15:51 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA200.7
Copper NO ug/L 5.0 1 07/11/1419:45 07114/1417:16 7440-50-8
Lead NO ug/L 5.0 1 07/11/1419:45 07/14/1417:16 7439-92-1
Zinc 25.8 ug/L 10.0 1 07/11/1419:45 07/14/1417:16 7440-66-6
Sample: Rain Gutter Back Lab ID: 92208805005 Collected: 07/10/14 00:00 Received: 07110114 15:51 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper NO ug1L 5.0 1 07/11/14 19:45 07/14/14 17:19 7440-50-8
Lead NO ug1L 5.0 1 07111/1419:45 07/1411417:19 7439-92-1
Zinc 82.7 ug1L 10.0 1 07111/1419:45 07/1411417:19 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/15/2014 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

aceAnailytitcal
wwwPecelabs=M
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078 `
[phone]
QUALITY CONTROL DATA
Project: SW non comp 7/1012014
Pace Project No.: 92208806
QC Batch: MPRPl16439 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92208805001, 92208805D02, 92208805003, 92208805004, 92208805005
METHOD BLANK: 1240835 Matrix: Water
Associated Lab Samples: 92208805001, 92208805002, 92208805003, 92208805004, 92208805005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper uglL ND 5.0 07/14/1414:22
Lead uglL ND 5.0 07114/1414:22
Zinc uglL ND 10.0 07114/1414:22
LABORATORY CONTROL SAMPLE:
1240836
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Copper
uglL
500
498 100 85-115
Lead
uglL
500
497 99 85-115
Zinc
uglL
500
487 97 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1240837
1240838
MS
MSD
92208623001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RI Qual
Copper ug1L
3.3J
500
500
495
494
98
98
70-130 0
Lead ug1L
ND
500
500
480
477
96
95
70-130 1
Zinc uglL
68.1
500
500
544
541
95
95
70-130 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1240839
1240840
MS
MSD
92208667001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper uglL
0.094
500
500
646
641
110
109
70-130
1
mglL
Lead ug1L
ND
500
500
433
420
87
84
70-130
3
Zinc uglL
ND
500
500
561
545
112
109
70-130
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of "result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/15/2014 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 10

4
aceAnalytical
WW..pacerabawm
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hvntersville, NC 28078
[phone]
QUALIFIERS
Project: SW non comp 7/10/2014
Pace Project No.: 92208805
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
POL - Practical Qua ntitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/15/2014 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

Face Analytical Services, Inc.
ltqc"nalXical ®
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wrwpawlabs.com
[phone]
QUALITY CONTROL
DATA CROSS REFERENCE TABLE
Project: SW non comp 7/1W2014
Pace Project No.: 92208805
Analytical
Lab ID Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92208805001 Lugger
EPA200.7
MPRP116439
EPA200.7
ICP114848
92208805002 Upstream
EPA200.7
MPRPI16439
EPA200.7
ICP114848
92208805003 Downstream
EPA200.7
MPRPI16439
EPA200.7
ICP/14848
92208805004 Rain Gutter Front
EPA200.7
MPRP/16439
EPA200.7
ICP114848
92208805005 Rain Gutter Back
EPA 2007
MPRP116439
EPA 200.7
ICP114848
Date: 07/15/2014 05:12 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 10

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _June 11, 2014
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Environmental Testing Solutions Lab Cert. #600mg/L
Comments on sample collection or analysis: See page 4
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2014
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ® Monthly' May jmonth)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
[]Zero -flow ❑Water Supply ❑SA
®Other: Class C, Swannanoa River
PLEASE REMEMBER TO SIGN ON PAGES Z AND/OR 3 4
No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks ==_>
-
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
05-15-2014
1.74
11 mg/L
7.2
0.046 m
<0.010
0.060 mg/L
<5.0 mg/L
BRL
2
05-15-2014
1.74
<5.0 mg/L
6.9
0.081 mg/L
<0.020
0.113 mg/L
<5.0 mg/L
BRL
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge, Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Received
JUN 13 2M4 `.
d Qua
Permit Date: 11/1/2012-30/31/2017 SWU-2�naast % ed 2
Page 1 of 4 ,,r

i
.9
puq Gf IsIgA 2GCOM
tkl 13
�iJcMiit..£

A
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following -certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoriring.r`uirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the ail the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Sal Vaccaro
Name (Print name)
General Manager
Title (Prin title)
6-l1-t
(Signal re) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera! Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?2
Outfall Na
Date Sample
Collected
(mo/dd/yr)
24-hour rainfall
amount,
inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks ==_>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 2 of 4

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all. "No Discharge." reparts, within 30 days of receipt of the lab results (or at end of monitoring period
in the case af "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
.617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 4

1) Zinc reporting value exceeds permit limit 0.067 for outfall 42
a) Finding;
i) Roofing material is galvanized metal could be a contributing factor for outfall #2.
b) Corrective actions;
i) Review BMP, ensured good management practices are being followed.
2) Copper reporting value exceeds permit limit 0.007 for outfall #1 and #2
a) Finding;
i) Roofing material is metal could be a contributing factor for outfall #land #2.
ii) Scrap Lugger pad could be a contributing factor for outfall #1 . We do not find potential sources of copper exposure in outfall #2.
b) Corrective actions;
i) Review of BMP's
ii) Have increased housekeeping, Lugger Pad Area and Center Pad are being inspected and cleaned weekly.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 4 of 4

aceAnaVica!
wwwpecetabs.com
i
May 28, 2014
Gerald Runkles
Pentair Valves & Controls
953 Old US Hwy 70
Black Mountain, NC 28711
RE: Project: Outfall5/15
Pace Project No.: 92201618
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
t704�875-9092
Dear Gerald Runkles:
Enclosed are the analytical results for sample(s) received by the laboratory on May 15, 2014, The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 26

aceAnalyticaf
",mparefabi.cam
.i -
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: Outfall 5115
Pace Project No.: 92201616
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 2BO78
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr„ Asheville, NC 28804 North Carolina Wastewater Certification #: 40
FloridalNELAP Certification #: E87648 South Carolina Certification 4: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 26

aceAnalXical
wwwpecelahs coin
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HuntersWle, 128078
(704 )875-9092
Project:
Pace Project No.:
Outfall 5115
92201618
Analytes
Lair ID
Sample ID
Method
Analysts
Reported
Laboratory
92201618001
OUTFALL #1
EPA 1664B
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA 200.7
JMW
3
PASI-A
EPA 625
Bpi
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
WRC
1
PASI-A
92201618002
OUTFALL 92
EPA 1664E
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA200.7
JMW
3
PASI-A
EPA 625
BPJ
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
WRC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 26

aceAnalytical
wwX.p8refa8�.mm
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviiie, NC 28078
[phone]
Project: Outfall 5115
Pace Project No.: 92201618
Sample: OUTFALL #1 Lab ID: 92201618001 Collected: 05/15/14 09:30 Received: 05115/14 15:45 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, oil and Grease
Analytical Method: EPA 16648
Oil and Grease
ND mg/L
5.0
1
05/19/14 13:14
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
NO ug/L
0.050
1
05/21/14 17:55
05/27194 23:50
309-00-2
alpha-BHC
NO ugiL
0.050
1
05/21114 17:55
05/27/14 23:50
319-84-6
beta-BHC
NO ug/L
0.050
1
05121/14 17:55
05/27114 23:50
319-85-7
delta-BHC
NO ug/L
0.050
1
05/21/14 17:55
05/27/14 23:50
319-86-8
gamma-BHC (Lindane)
NO ug/L
0.050
1
05/21/14 1Z55
05127/14 23:50
58-89-9
Chlordane (Technical)
ND ugiL
0.50
1
05121114 17:55
05/27114 23:50
57-74-9
4,4'-DDD
ND ug/L
0.050
1
05/21114 17:55
05127/14 23:50
72-54-8
4,4'-DDE
ND ugiL
0.050
1
05/21/14 17:55
05/27/14 23:50
72-55-9
4,4'-DDT
NO ug/L
0.050
1
05/21/14 17:55
05/27/14 23:50
50-29-3
Dieldrin
NO ug/L
0.050
1
05/21/14 17:55
05/27/14 23:50
60-57-1
Endosulfan I
NO ugiL
0.050
1
05/21/14 17:55
05/27/14 23:50
959-98-8
Endosulfan II
NO ug/L
0.050
1
05/21/14 17:55
05/27/14 23:50
33213-65-9
Endosulfan sulfate
ND ug/L
0.050
1
05/21/14 17:55
05/27/14 23:50
1031-07-8
Endrin
NO ug/L
0.050
1
05/21/14 17:55
05/27/14 23:50
72-20-8
Endrin aldehyde
NO ug/L
0.050
1
05/21/14 17:55
05/27/14 23:50
7421-93-4
Heptachlor
NO ug/L
0.050
1
05/21/14 17:55
05/27114 23:50
76-44-6
Heptachlor epoxide
ND ug/L
0.050
1
05/21/14 17:55
05/27114 23:50
1024-57-3
PCB-1016 (Aroclor 1016)
NO ug/L
0.50
1
05/21/14 17:55
123:50
12674-11-2
PCB-1221 (Aroclor 1221)
NO uglL
0.50
1
05/21/14 17:55
05/27114 23:50
11104-28-2
PCB-1232 11232)
NO ugiL
0.50
1
05/21114 17:55
05127114 23:50
11141-16-5
PCB-1242 (Aroclor 1242)
ND ug/L
0.50
1
05121/14 17:55
05/27/14 23.50
53469.21-9
PCB-1248 (Aroclor 1248)
ND ug/L
0.50
1
05121/14 17:55
05/27/14 23:50
12672-29-6
PCB-1254 (Aroclor 1254)
ND ug/L
0.50
1
05121/14 17:55
05/27/14 23:50
11097-69-1
PCB-1260 (Aroclor 1260)
ND ugiL
1
1
05121114 17:55
05/27/14 2150
11096-82-5
Toxaphene
ND ug/L
0.50
1
05/21/14 17:55
05/27/14 23:50
8001-35-2
Surrogates
Tetrachiloro-m-xylene (S)
43 %
20-110
1
05/21/14 17:55
05/27/14 23:50
877-09-8
Decachlorobiphenyt 1
46 %
20-138
1
05/21/14 17:55
05/27/14 23:50
2051-24-3
200.7 MET ICP
Analytical Method: EPA200.7 Preparation Method: EPA200.7
Copper
45.5 ug/L
5.0
1
05/20/14 15:45
05/21/14 21:29
7440-50-8
Lead
NO ugiL
5.0
1
05120/14 15:45
05/21/14 21:29
7439-92-1
Zinc
59.7 ug/L
10.0
1
05120/14 15A5
05/21114 21:29
7441
625 MSSV
Analytical Method: EPA625 Preparation Method: EPA625
Acenaphthene
NO ug/L
5.0
1
05122/14 13:00
05127/14 22:30
83-32-9
Acenaphthylene
NO ugiL
5.0
1
05122/14 13:00
05/27114 22:30
208-96-8
Anthracene
ND ugiL
5.0
1
05122114 13:00
05/27/14 22:30
120-12-7
Benzo(a)anthracene
ND ug/L
5.0
1
05122114 13:00
05/27/14 22:30
56-55-3
Benzo(a)pyrene
ND ug/L
5.0
1
05/22/14 13:00
05/27/14 22:30
50-32-8
Benzo(b)fluoranthene
ND ug/L
5.0
1
05/22114 13:00
05/27/14 22:30
205-99-2
Benzo(g,h,i)perylene
ND ug/L
5.0
1
05122/14 13:00
05/27114 22:30
191-24-2
Benzo(k)fluoranthene
ND ugiL
5.0
1
05/22/14 13:00
05/27114 22:30
207-08-9
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 05/28/2014 1 PM
without the written consent
of Pace Analytical
Services,
Inc..
Page 4 of 26

aceAnalytical
- wrvwpare;aflscom
i
i
ANALYTICAL RESULTS
Pro)ect. Outfall 5115
Pace Project No.: 92201618
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OUTFALL #1 Lab I❑: 92201618001 Collected: 05/15/14 09:30 Received: 05/15/14 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV
4-Bromaphenylphenyl ether
Butylbenzylphthalate
4-Ch lord-3- methylpheno I
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalens
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h )anthracene
3,3'-Dichlorohenzid ine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthelate
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-❑initrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyt)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
2-Nitrophenot
4-Nitrophenol
N-Nitrosodimelhylamine
N-Nitroso-di-n-propylemine
N-Nitrosodiphenylamine
Pentaehlorophenot
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Analytical Method: EPA 625 Preparation Method: EPA 625
NO ug/L
5.0
1
05/22/14 13:00 05127/14 22:30
101-55-3
NO ug/L
5.0
1
05/22/14 13:00 05l27114 22:30
85-68-7
NO ug/L
5.0
1
05/22114 13:00 05/27114 22M
59-50-7
NO ug/L
10.0
1
05t2211413:00 05/27/14 22:30
ill-91-1
NO ug/L
5.0
1
05122114 13:00 05127/14 22:30
11144-4
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
108-60-1
NO ug/L
5.0
1
05/22114 13:00 05/27/14 22:30
91-58-7
NO ugil
5.0
1
05/22114 13:00 05127/14 22:30
95-57-8
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
7005-72-3
NO ug/L
5.0
1
05122114 13:00 05/27/14 22:30
218-01-9
NO uglL
5.0
1
05122114 13:00 05127/14 22:30
53-70-3
NO ug/L
25.0
1
05/22114 13:00 05127/14 22:30
91-94-1
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
120-83-2
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
84-66-2
NO ug/L
10.0
1
06/22/14 13:00 05/27/14 22:30
105-67-9
NO ug/L
5.0
1
05/22114 13:00 05/27/14 22:30
131-11-3
ND ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
84-74-2
ND uglL
20.0
1
05/22/14 13:00 05/27114 22:30
534-52-1
NO ug/L
50.0
1
05/22/14 13:00 05/27/14 22:30
51-28-5
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
121-14-2
NO ug/L
5.0
1
05122114 13:00 05127/14 22:30
606-20-2
ND ug/L
5.0
1
05122M4 13:00 05/27/14 22:30
117-84-0
NO ug/L
5.0
1
05122/14 13:00 05127/14 22:30
117-81-7
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
206-44-0
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
86-73-7
NO ug/L
5.0
1
05/22/14 13:00 05127/14 22:30
87-68-3
NO ug/L
5.0
1
05/22114 13:00 M27114 22:30
118-74-1
NO ug/L
10.0
1
05IM14 13:00 05/27/14 22:30
77-47-4
NO ug/L
5.0
1
05122/14 13:00 M27/14 22:30
67-72-1
NO ug1L
5.0
1
05/22/14 13:00 05/27/14 22:30
193-39-5
NO ug/L
10.0
1
05/22/14 13:00 05127/14 22:30
78-59-1
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
91-20-3
ND ug/L
5.0
1
05/22114 13:00 05127/14 22:30
98-95-3
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
88.75-5
ND ug/L
50.0
1
05/22/14 13:00 05127/14 22:30
100-02-7
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
62.75-9
NO ug/L
5.0
1
05/22/14 13:00 05/27/14 22:30
621-64-7
NO ug/L
10.0
1
05/22/14 1100 05/27/14 22:30
86-30-6
NO ug/L
10.0
1
051221i4 13:00 05/27A4 22:30
87-86-5
NO ugll-
5.0
1
05/22/14 1100 05/27114 22:30
85-01-8
NO ug1L
5.0
1
05/22114 13:00 05/27/14 22:30
108-95-2
NO ug/L
5.0
1
05/22114 13:00 05/27/14 22:30
129-00-0
NO uglL
5.0
1
05/22/14 13:00 05127114 22:30
120-82-1
NO ug/L
10.0
1
05122/14 13:00 05/27/14 22:30
88-06-2
39 %
10-120
1
05122114 13:00 05/27114 22:30
4165-60-0
28 %
15-120
1
05122/14 13:00 05127/14 22:30
321-60-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 05:37 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 26

?CeAnapical
r www.pemiaba.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvllie, NC 28078
[phone]
Project: Outfall 5115
Pace Project No.: 92201618
Sample: OUTFALL #1 Lab ID: 92201618001 Collected: 05/15/14 09:30 Received: 05115/14 15:45 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quaff
625 MSSV Analytical Method EPA625 Preparation Method: EPA625
Surroga tes
Terphenyl-d14 (S)
71 %
11-131
1
05/22/14 13:00 05/27/14 22:30
1718-51-0
Phenol-d6 (S)
10 %
10-120
1
05/22/14 13:00 05/27/14 22:30
13127-88-3
24%orophenol (S)
15 %
10-120
1
05/22/14 13:00 05/27/14 2130
367-12-4
2,4,6-Tribrornophenal (S)
62 %
10-137
1
05/22/14 13:00 05127/14 22:30
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND uglL
2.0
1
05/20114 06A3
71-43-2
Bromodichloromethane
ND ug1L
2.0
1
05120114 06A3
75-27-4
Bromoform
ND ug1L
2.0
1
05120114 06A3
75-25-2
Bromomethane
ND ug1L
2.0
1
05/20114 06:43
74-83-9
Carbon tetrachloride
ND uglL
2.0
1
05/20114 06:43
56-23-5
Chlorobenzene
ND uglL
2.0
1
05/20114 06:43
108-90-7
Chloroethane
ND uglL
2.0
1
05/20114 06:43
75-00-3
Chloroform
ND uglL
2.0
1
05/20/14 06:43
67-66-3
Chloramethene
ND uglL
2.0
1
05/20/14 06:43
74-87-3
Dibromochloromethene
ND ug1L
2.0
1
05/20/14 06:43
124-48-1
1,2-Dichlorobenzene
ND uglL
2.0
1
05/20/14 06:43
95-50-1
1,3-Dichlorobenzene
ND uglL
2.0
1
05/20114 06:43
541-73-1
1,4-Dichlorobenzene
ND ug1L
2.0
1
05/20/14 06:43
106-46-7
1,1-Dichloroethane
ND uglL
20
1
05/20/14 06:43
75.34-3
1,2-Dichtoroethane
ND ug1L
2.0
1
05/20/14 06A3
107-06-2
1,1-Dichloreethene
NO ug1L
2.0
t
05/20114 06:43
75-35-4
cis-1,2-Dichloroethene
ND ug1L
2.0
1
05/20114 06A3
156-59-2
trans-1,2-Dichloroethene
NO ug1L
2.0
1
05/20/14 06:43
156-60-5
1,2-Dichloropropane
NO ug1L
2.0
1
05/20114 06:43
78-87-5
cis- 1, 3-Dichloropropene
ND ug1L
2.0
1
05120/14 06A3
10061-01-5
trans-1,3-Dichloropropene -
ND ug1L
2.0
1
05/20114 06:43
10061-02-6
Fthylbenzene
ND uglL
2.0
1
05/20114 06:43
100-41-4
Methylene Chloride
ND uglL
2.0
1
05/20114 06:43
75-09-2
1,122-Tetrachloroethane
ND ug1L
2.0
1
05120114 06:43
79-34-5
Tetra chloroethene
ND uglL
2.0
1
05/20/14 06:43
127-18-4
Toluene
ND ug1L
2.0
1
05/20/14 06:43
108-88-3
1,1,1-Trichloroethane
ND ug1L
2.0
1
05/20/14 06:43
71-55-6
1,1,2-Trichloroethane
ND ug1L
2.0
1
05/20/14 06:43
79-00-5
Trichloroethene
ND ug1L
2.0
1
05/20/14 06:43
79-01-6
Trichlorofluoromethane
ND ug1L
2.0
1
05/20/14 06:43
75-69-4
Vinyl chloride
ND ug1L
2.0
1
05/20/14 06:43
75-01-4
Surrogates
4-Bmmofluorobenzene (S)
87 %
70-130
1
05/20/14 06:43
460-00.4
Toluene -dB (S)
98 %
70-130
1
05120/14 06:43
2037.26-5
1,2-Dichloroethane-d4 (S)
103 %
70-130
1
05/20/14 06:43
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
11.1 mg1L
2.5
1
05/22114 16:17
Date: 05/2812014 05:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 26

2eAnalytili
.!
"W'Pgcelabs. com
ANALYTICAL RESULTS
Project: Outfak 5/15
Pace Project No.: 92201618
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, 128078
[phone]
Sample: OUTFALL #2 Lab ID: 92201618002 Collected: 05/15/14 09:40 Received: 05/15/14 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua!
HEM, Oil and Grease Analytical Method: EPA 16646
Oil and Grease
608 GC5 Pesticides and PCBs
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-li (Lindane)
Chlordane (Technical)
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan i i
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Toxaphene
Surrogates
Tetrachloro-n iene (S)
Decachlorobiphenyl (S)
200.7 MET ICP
N❑ mg1L
5.0 1
Analytical Method: EPA608 Preparation Method: EPA3510
05/19/14 13:14
NO ug1L
0.050 '
1
05/21/14 17:55
05/28114 00:08
309-00-2
ND uglL
0-050
1
05/21114 17:55
05128f14 00:08
319-84-6
NO ug1L
0.050
1
05121114 17:55
05128/14 00:08
319.85-7
NO ui
0-050
1
117:55
05/28114 00:08
319-8"
ND ug1L
0.050
1
05/21/14 17:55
05/28/14 00:08
58-89-9
NO ui
0.50
1
05121/14 17:55
05128/14 00:08
57-74-9
ND ug1L
1
1
05121/14 17:55
05128/14 1
72-54-8
ND uglL
0.050
1
05/21/14 17:55
05128/14 00:08
72-55-9
ND uglL
0.050
1
05/21/14 17:55
05/28/14 00:08
51
ND ug1L
0.050
1
05/21/14 17:55
05/28/14 00:08
60-57-1
ND ug1L
0.050
1
05121/14 17:55
05/28/14 00708
959-98-8
NO ugl1-
0.050
1
1 17:55
05/28/14 00:08
33213-65-9
ND uglL
0,050
1
05/21/14 17:55
05/28/14 00:08
1031-07-8
ND ugl1-
0.050
1
05/21/14 17:55
05/28/14 00:08
72-20-8
ND u911-
0.050
1
05/21/14 1T55
05/28114 00:08
7421.93-4
ND uglL
0.050
1
05/21/14 17:55
05/28114 00:08
76-44-8
NO uglL
0.050
1
05/21/14 17:55
05/28/14 00:08
1024-57-3
NO ug/L
0.50
1
05/21/14 1T55
05/26/14 00:08
12674-11-2
NO uglL
0.50
1
05/21/14 17:55
05/28/14 00:08
11104-28-2
ND uglL
0.50
1
05I21f14 17:55
05/28114 1
11141-16-5
ND ug/L
0.50
1
05/21114 17:55
05/28/14 00:08
53469-21-9
ND ug1L
0.50
1
05/21/14 17:55
06/28/14 00:08
12672-29-6
ND ug1L
0.50
1
05121/14 17:55
05/28/14 00:08
11097-69-1
ND ug1L
0-50
1
05/21/14 17:55
05128/14 X08
11096-82-5
NO uglL
0.50
1
05/21114 17:55
05/28114 00:08
8001-35-2
46 %
20-110
1
05/21/14 17:55
05/28114 00:08
877-09-B
60 %
20-138
1
05/21/14 1T55
05/28114 00:08
2051-24-3
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
80.5 uglL
5.0
1
05/20/14 15:45
05/21/14 21:32
7440-50-8
Lead
10.0 ug1L
5.0
1
05/20/14 15:45
05/21/14 21:32
7439-92-1
Zinc
113 ug1L
10.0
1
05/20/14 15:45
05/21/14 21:32
7440-66-6
625 MSSV
Analytical Method: EPA625
Preparation Method: EPA625
Acenaphthene
NO ug11-
5.0
1
05/22/14 13:00
05127/14 22 58
83-32-9
Acenaphthylene
NO uglL
5.0
1
05122114 13:00
05/27/14 22:58
208-96-8
Anthracene
ND uglL
5.0
1
05/22114 13:00
05127/14 22:58
120-12-7
Benzo(a)anthrecene
ND ug1L
5.0
1
05/22/14 13:00
05127/14 22:58
56.55-3
Benzo(a)pyrene
NO ui
5.0
1
05IW14 13:00
05/27/14 22:58
50.32-8
Benzo(b)fluoranthene
NO ug1L
5.0
1
05122114 1100
122:58
205-99-2
Benzo(g,h,i)perylene
NO ug1L
5.0
1
05/27114 13:00
05/27114 22:58
191-24-2
Benzo(k)fluoranthene
ND uglL
5.0
1
05/22/14 13:00
05127/14 22:58
21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0512B12014 05:37 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 26

aceAnalytical
wmvperelabs,sam
ANALYTICAL RESULTS
Project: O utfal l 505
Pace Project No.: 92201618
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Sample: OUTFALL #2 Lab ID: 92201618002 Collected: 06/15/14 09:40 Received: 05/15/14 15:45 Matrix: Water
Parameters Results Units Report Limit OF Prepared Anatyzed CAS No. Qual
625 MSSV Analytical Method EPA 625 Preparation Method: EPA 625
4-Bromophenylphenyl ether
NO uglL
5.0
1
05122/14 13:00
05/27/14 22:58
101-55-3
Butylbenzylphlhalate
NO uglL
5.0
1
05/22/14 13:00
05/27/14 22:58
85-68-7
4-Chloro-3-methylphenol
ND ug1L
5.0
1
05/22/14 13:00
05/27/14 22:58
59-50-7
bis(2-Chloroethoxy)methane
NO uglL
10.0
1
05/22/14 13:00
05/27114 22:58
111-91-1
bis(2-Chloroethyl) ether
NO ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
111-44-4
bis(2-Chloroisopropyl) ether
NO uglL
5.0
1
05/22/14 13:00
05/27/14 22:58
108-60-1
2-Chloronaphlhalene
NO ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
91-58-7
2-Chlorophenol
NO ug/L
5.0
1
05/22/14 13:00
05/27114 22:58
95-57-8
4-Chlorophenylphenyl ether
ND ug/l.
5.0
1
05/22/14 13 00
05/27/14 22:58
7005-72-3
Chrysene
ND ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
218-01-9
❑ibenz(a,h)anthracene
NO ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
53-70-3
3,3'-Dichlorobenzidine
NO ug/L
25.0
1
05/22/14 13:00
05/27/14 22:58
91-94-1
2,4-Dichlorophenol
NO uglL
5.0
1
05/22/14 13:00
05127/14 22:58
120-83-2
Diethyl phthalate
NO uglL
5.0
1
05/22/14 13:00
05127/14 22:58
84-66-2
2,4-Dimethyiphenol
NO uglL
10.0
1
05122/14 13:00
05127/14 22:58
105-67-9
Dimethylphthalate
ND uglL
5.0
1
05/22/14 13:00
05/27/14 22:58
131-11.3
Di-n-butylphthalate
NO uglL
5.0
1
05/22/14 13:00
05/27/14 22:58
84-74-2
4,6-Dinitro-2-methylphenol
NO uglL
20.0
1
05/22/14 13:00
05/27114 22:58
534.52.1
2,4-Dinitrophenol
ND ug1L
50.0
1
05/22/14 13:00
05/27/14 22:58
51-28-5
2,4-Dinitrotoluene
ND ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
121-14-2
2,6-Dinitrotoluene
NO ug/L
5,0
1
05/22/14 13:00
05/27/14 22:58
606-20-2
Di-n-octylphthalate
NO ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
117-84-0
bis(2- Ethyl hexyl)phthalate
NO ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
117-81-7
Fluoranthene
NO ug/L
5,0
1
05/22/14 13:00
05/27/14 22:58
206-44-0
Fluorene
NO ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
86-73-7
Hexachloro-1,3-butadiene
NO uglL
5.0
1
05/22/14 13:00
05/27/14 22:58
87-68-3
Hexachlorobenzene
NO uglL
5.0
1
05/22/14 13:00
05/27/14 22:58
118-74-1
Hexachlorocyclopenladiene
NO uglL
10.0
1
05122/14 13:00
05/27/14 22:58
77-47-4
Hexachloroethane
NO ug1L
5.0
1
05/22/14 13:00
05127/14 22:58
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug1L
5.0
1
05122/14 13:00
05/27/14 22:58
193-39.5
Isophorone
NO ug/L
10.0
1
05122/14 13:00
05/27/14 22:58
78-59-1
Naphthalene
ND ug/L
5.0
1
05/22114 13:00
05/27114 22:58
91-20-3
Nitrobenzene
ND ug/L
5.0
1
05/22114 13:00
05/27/14 22:58
98-95-3
2-Nitrophenol
NO ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
05/22/14 13:00
05/27/14 22:58
100-02-7
N-Nitrosodimethylamine
ND ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
62-75-9
N-Nitroso-di-n-propylamine
NO ug/L
5.0
1
05/22/14 13:00
05/27/14 22:58
621-64-7
N-Nitrosodiphenylamine
NO ug1L
10.0
1
05/22/14 13:00
05/27/14 22:58
86-30-6
Pentachlorophenol
NO uglL
10.0
1
05/22/14 13:00
05127/14 22:58
87-86-5
Phenanthrene
NO uglL
5.0
1
05/22/14 13:00
05/27/14 22:58
85-01-8
Phenol
ND uglL
5.0
1
05/22/14 13:00
05/27/14 22:58
108-95-2
Pyrene
NO uglL
5.0
1
05122/14 13:00
05/27/14 22:58
129-00-0
1,2,4-Trichlorobenzene
ND ug1L
5.0
1
05/22114 13:00
05/27/14 22:58
120-82-1
2,4,6-Trichlorophenol
NO ug1L
10.0
1
05/22/14 13:00
05/27/14 22:58
88-06-2
Surrogates
Nitrobenzene-d5 (S)
77 %
1 D-120
1
05/22/14 13:00
05/27/14 22:58
4165-60-0
2-Fluorobiphenyl (S)
64 %
15-120
1
05/22/14 13:00
05/27/14 22:58
321-60-8
REPORT OF LABORATORY ANALYSIS
This report shah not be reproduced, except in full,
Date: 05/28/2014 05:37 PM without thewritten consent of pace Analytical Services, Inc.. Page 8 of 26

aceAnalytical®
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r
E
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Outfall 6/15
Pace Project No.: 92201618
Sample: OUTFALL #2 Lab ID: 92201618002 Collected: 05/15/14 09:40 Received: 05/15/14 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Surrogates
Terphenyl-dl4 (S)
86 %
11-131
1
05/22/14 13700 05/27114 22:58
1718-51-0
Phenol-d6 (S)
21 %
10-120
1
05/22/14 13:00 05/27/14 22:58
13127-88-3
2-Ftuorophenol (S)
31 %
10-120
1
05122/14 13:00 05/27/14 22:58
367-12-4
2,4,6-Tribromophenol (S)
88 %
10-137
1
05/22/14 13:00 05/27/14 22:58
118-79.6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND ug1L
2.0
1
05/20/14 11:00
71-43-2
Bromodichioromethane
ND ug/L
2.0
1
05/20/14 11:00
75-27-4
Bromoform
ND ug/L
2.0
1
05/20/14 11:00
75.25-2
Bromomethane
ND ug1L
2.0
1
05120/14 11:00
74-83-9
Carbon tetrachloride
ND ug/L
2.0
1
05/20/14 11:00
56.23-5
Chlorobenzene
ND ug1L
2.0
1
05/20/14 11:00
108-90-7
Chloroethane
ND ug/L
2.0
1
05/20/14 11:00
75-00-3
Chloroform
ND ug/L
2.0
1
05/20/14 11:00
67-66-3
Chloromethane
ND ug/L
2.0
1
05/20/14 11:00
74-87-3
Dibromochloromethane
ND ug/L
2.0
1
05/20/14 11:00
124-48-1
1,2-Dichlorobenzene
ND ug/L
2.0
1
05/20/14 11:00
95-50-1
1,3-Dichlorobenzene
ND ug/L
2.0
1
05/20/14 11:00
541-73-1
1,4-Dichlorobenzene
ND ug/L
2.0
1
05/20/14 11:00
106-46-7
1,1-Dichloroethane
ND ug/L
2.0
1
05/20/14 11:00
75-34-3
1,2-Dichloroethane
ND uglL
2.0
1
05/20/14 11 :00
107-06-2
1,1-Dichloroethene
ND ug/L
2.0
1
05/20/14 11:00
75-35-4
cis-1,2-Dichloroethene
ND ug1L
2.0
1
05/20/14 11:00
156-59-2
trans-1,2-Dichloroethene
ND ug1L
2.0
1
05/20/14 11:00
156-60-5
1,2-Dichloropropane
ND ug1L
2.0
1
05120/14 11:00
78-87-5
cis-1,3-Dichloropropene
ND ug1L
2.0
1
05/20/14 11:00
10061-01-5
trans- 1, 3- Dichloropropene
ND ug/L
2.0
1
05/20/14 11:00
10061-02-6
Ethylbenzene
ND ug1L
2.0
1
05/20/14 11:00
100-41-4
Methylene Chloride
ND ug/L
2.0
1
05/20/14 11:00
75-09-2
1,1,2,2-Tetrachloroethane
ND ug/L
2.0
1
05/20114 11:00
79-34-5
Tetrachloroethene
ND ug/L
2.0
1
05/20114 11:00
127-18-4
Toluene
ND ug/L
2.0
1
05/20/14 11:00
108-88-3
1,1,1-Trichloroethane
ND ugll-
2.0
1
05/20114 11:00
71-55-6
1,1,2-Trichloroethane
ND ug/L
2.0
1
05/2011411:00
79-00-5
Trichloroethene
ND uglL
2.0
1
05/20/14 11:00
79-01-6
Trichlorofluoromethane
ND ug/L
2.0
1
05/20/14 11:00
75-69-4
Vinyl chloride
ND ug/L
2.0
1
05/20/14 11:00
75-01-4
Surrogates
4-Bromofluorobenzene (S)
88 %
70-130
1
05/20/14 11:00
460-00-4
Toluene-d8 (S)
97 %
70-130
1
05/20/14 11:00
2037-26-5
1,2-Dichloroethane-d4 (S)
103 %
70-130
1
05/20/14 11:00
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.6 mg/L
5.0
1
05/22114 22:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/2812014 05:37 PM without the written consent of Pace Analytical Services, Inc,. Page 9 of 26

aceAnapical
IswwpaceW(u.com
k
QUALITY CONTROL DATA
Project: Outfall 5115
Pace Project No.: 92201616
QC Batch: GCSV117643 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92201618001, 92201618002
METHOD BLANK: 1202010 Matrix: Water
Associated Lab Samples: 92201618001, 92201618002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ott and Grease mglL NO 5.0 05/19114 13:04
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1202011
Spike LCS
LCS
% Rec
Parameter
Units
Gone. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg1L
40 37.4
94
78-114
MATRIX SPIKE SAMPLE:
1202012
92201505001 Spike
MS
Ms
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg1L
N❑ 40
37.2
93 78-114
Results presented on this page are in the units indicated by the "Unite" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
Date: 05/28/2014 05:37 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 26

1�?ceAnalytical"
www.pacelabs.com
i f.
Project: Outfall 5115
Pace Project No.: 92201618
QC Batch: MPRP/15999
QC Batch Method: EPA 200.7
Associated Lab Samples: 92201618001, 92201618002
METHOD BLANK: 1202860
Associated Lab Samples: 92201618001, 92201618002
Parameter Units
Copper
Lead
Zinc
ug/L
ug/L
ug/L
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 5.0 05/21/14 20:38
ND 5.0 05/21114 20:38
ND 10.0 05/21114 20:38
LABORATORY CONTROL SAMPLE: 1202861
Spike
Parameter Units Conc.
Copper ug/L 500
Lead ug/L 500
Zinc ug/L 500
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
LCS LCS % Rec
Result % Rec Limits Qualifiers
452 90 85-115
462 92 85-115
462 92 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1202862
1202863
MS
MSD
92201088001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
Copper ug/L
5.0
500
500
471
468 93
93
70-130 1
Lead uglL
ND
500
500
462
459 92
92
70-130 1
Zinc ug/L
37.6
500
500
506
506 94
94
70-130 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1202873
1202874
MS
MSD
92201642001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper u911-
ND
500
500
466
464
92
92
70-130
0
Lead ug1L
ND
500
500
471
465
94
93
70-130
1
Zinc ug/L
19A
500
500
487
478
94
92
70-130
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shaii not be reproduced, except in full,
Date: 05/2812014 05:37 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 26

aceAnalj&al
wwwpocelaba cam
i
QUALITY CONTROL DATA
Project: Out fall 5115
Pace Project No.: 92201618
QC Batch: MSV126872 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92201618001, 92201618002
METHOD BLANK: 1202236
Associated Lab Samples: 92201618001, 92201618002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1, 1 -Trichloroethane
ugiL
NO
2.0
05/2011400:43
1,1,2,2-Tetrachloroethane
ug1L
ND
2-0
05120114 00:43
1,1,2-Trichloroethane
ugiL
NO
2.0
05/20/14 00:43
1,1-Dichloroethane
ugiL
NO
2.0
05/20/14 00:43
1,1-Dichloroethene
ugiL
ND
2.0
05120/14 00:43
1,2-Dichlorobenzene
ug1L
ND
2.0
05/20114 00:43
1,2-Dichloroethane
uglL
ND
2.0
05/20/14 00:43
1,2-Dichloropropane
uglL
NO
2.0
05120/14 00:43
1,3-Dichlorobenzene
uglL
NO
2.0
05/20/14 00:43
1,4-Dichtorobenzene
uglL
NO
2.0
05/20/14 00:43
Benzene
ug1L
ND
2.0
05/20/14 00:43
Bromodichloromethene
uglL
NO
2.0
05/20/14 00:43
Bromoform
ug1L
ND
2.0
05/20/14 00:43
Bromomethane
ug1L
NO
2.0
05/20/14 00:43
Carbon tetrachloride
ugiL
NO
2.0
05/20/14 00:43
Chlorobenzene
ug1L
NO
2.0
05/20/14 00:43
Chloroethane
ug1L
NO
2.0
05/20/14 00;43
Chloroform
uglL
NO
2.0
05/20/14 00:43
Chioromelhane
ugiL
NO
2.0
05120/14 00:43
cis-1,2-Dichloroethene
uglL
NO
2.0
05120/14 00:43
cis-1,3-Dichloropropene
uglL
NO
2.0
05/20/14 00:43
Dibromochloromelhane
uglL
ND
2.0
05120/14 00:43
Ethyfbenzene
ug1L
NO
2.0
05i2004 00:43
Methylene Chloride
uglL
NO
2.0
05/20/14 00:43
Tetrachloroethene
ug1L
NO
2.0
05/20/14 00:43
Toluene
uglL
NO
2.0
05/20/14 00:43
trans- 1,2-Dichloroethene
ug11-
ND
2.0
05/20/14 00A3
trans- 1,3•Oichloropropene
ug1L
ND
2.0
05/20/14 00A3
Trichlorciethene
uglL
NO
2.0
05/20/14 00:43
Trichloroflucromethane
uglL
NO
2.0
05/20/14 00A3
Vinyl chloride
uglL
NO
2.0
05/20/14 00:43
1,2-Dichloroethane-d4 (S)
%
101
70-130
05/20/14 00:43
4-Bromofluorobenzene (S)
%
98
70-130
05/20114 00:43
Toluene -dB (S)
%
97
70-130
05/20114 00:43
Qualiriers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviiie, NC 28078
[phone]
LA130RATORY CONTROL SAMPLE: 1202237
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichlaroethane Ug1L 20 20.9 104 52-162
1,1,2,2-Tetrachloroethane ugiL 20 21.7 109 46-157
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
• Date: 05/28/2014 05:37 PM without the written eensent of Pace Analytical Services, Inc.. Page 12 of 26

;aceAnalytical"
wwwpar iobs.corn
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 1CO
Huntersviile, NC 28078
(704 )875-9092
Project: Outfall 5115
Pace Project No.: 92201616
LABORATORY CONTROL SAMPLE:
1202237
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits
Qualifiers
1,12-Trichloroethane
uglL
20
22.0
110
52-150
1,1-Dichloroethane
uglL
20
21.1
105
59-155
1,1-Dichloroethene
ug1L
20
21.4
107
1-234
1,2-Dichlorobenzene
uglL
20
22.2
ill
18-190
1,2-Dichloroethane
uglL
20
21.9
110
49-155
1,2-Dichloropropane
uglL
20
21A
107
1-210
1,3-Dichlorobenzene
uglL
20
21.2
106
59-156
1,4-Dichlorobenzene
uglL
20
21.8
109
18-190
Benzene
uglL
20
23.2
116
37-151
Bromodichtoromethane
UgA-
20
20.8
104
35-155
Bromoform
uglL
20
19.6
98
45-169
Bromomethane
ug/L
20
14.1
70
1-242
Carbon tetrachloride
uglL
20
19.9
100
70-140
Chlorobenzene
uglL
20
20.6
103
37-160
Chlorcethane
uglL
20
23.6
118
14-230
Chloroform
uglL
20
21.9
109
51-138
Chloromethane
uglL
20
16.7
84
1-273
cis-1,2-Dichloroethene
ug1L
20
21.3
106
68-146
cis-1,3-Dichloropropene
uglL
20
21.4
107
1-227
❑ibromochloromethane
uglL
20
19.8
99
53-149
Ethylbenzene
uglL
20
21.0
105
37-162
Methylene Chloride
uglL
20
22.4
112
1-221
Tetrachloroethene
uglL
20
21.1
105
64-148
Toluene
ug1L
20
21.0
105
47-150
trans- l,2-Dichloroethene
uglL
20
22.0
110
54-156
trans-1,3-Dichloropropene
ug/L
20
21.0
105
17-183
Trichloroethene
uglL
20
23.0
115
71-157
Trichlorofluoromethane
uglL
20
20.2
101
17-181
Vinyl chloride
uglL
20
22.5
112
1-251
1,2-Dichloroethane-d4 (S)
%
107
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE SAMPLE:
1202424
92201352002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,11-Trichloroethane
uglL
ND
50
55.3
ill
46-171
1,1,2,2-Tetrachloroethane
uglL
ND
50
51.9
104
73-159
1,12-Trichloroethane
uglL
ND
50
51.8
104
64-152
1,1-Dichloroethane
uglL
ND
50
52.3
105
43-172
1,1-Dichloroethene
uglL
ND
50
56.8
114
48-189
1,2-Dichlorobenzene
uglL
ND
50
51.9
104
54-154
1,2-1)ichloroethane
uglL
ND
50
53.3
107
42-171
1,2-Dichloropropane
uglL
ND
50
52.5
105
55-157
1,3-Dichlorobenzene
uglL
ND
5o
50.8
102
57-148
Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 05:37 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 26

aceAnapical
www.pecelab,mm
1
QUALITY CONTROL DATA
Project: OutWl 5115
Pace Project No.: 92201618
Pace Analytical Services, Inc.
9800 Kincay Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
MATRIX SPIKE SAMPLE:
Parameter
1202424
Units
92201352002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
uglL
NO
50
51.9
104
58-149
Benzene
ug1L
NO
50
57.1
114
54-163
Bromodichloromethane
uglL
NO
50
51.4
103
56-152
Bromoform
uglL
NO
50
50.6
101
53-151
Bromomethane
uglL
NO
50
58.7
117
10-200
Carbon tetrachloride
uglL
NO
50
54.5
109
41-175
Chlorobenzene
uglL
NO
50
50.0
100
67-152
Chloroethane
uglL
NO
50
45.5
91
23-200
Chloroform
uglL
NO
50
53.5
107
51-166
Chloromethane
uglL
ND
50
47.1
94
40-175
cis- 1, 2- Dichforoethene
uglL
ND
50
52.8
106
45-174
cis-1,3-Dichloropropene
ug1L
NO
50
53.5
107
38-146
Dibromochloromethane
ug1L
NO
50
50.2
100
65-144
Ethylbenzene
ug1L
NO
50
49.7
99
57-152
Methylene Chloride
ug1L
NO
50
47.4
94
40-167
Tetrachloroethene
uglL
NO
50
54.9
110
59-155
Toluene
uglL
NO
50
51.6
103
47-162
trans-1,2-Dichloroethene
uglL
NO
50
54.9
110
47-178
trans-1,3-Dichloropropene
uglL
NO
50
51.7
103
39-148
Trichloroethene
ug1L
NO
50
56.9
114
60-153
Trichlorofluoromethane
uglL
NO
50
55.4
111
42-199
Vinyl chloride
uglL
ND
50
64.2
128
46-176
1,2-Dichloroethane-d4 (S)
%
102
70-130
4-Bromofluorobenzene (S)
%
93
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE: 1202425
Parameter
1,1,1-Trich loroethane
1,1,2, 2-Teirach loroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-❑ichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
B romodi chloro methane
Bromoform
Bromomethane
Carbon tetrachloride
Chlarobenzene
Units
92201354002
Result
Dup
Result
uglL
NO
NO
uglL
NO
NO
uglL
NO
NO
uglL
NO
NO
uglL
NO
ND
uglL
ND
NO
uglL
ND
NO
ug1L
ND
NO
uglL
NO
NO
uglL
NO
ND
uglL
NO
NO
uglL
NO
ND
uglL
NO
NO
uglL
ND
NO
uglL
NO
NO
uglL
NO
NO
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the reSult.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/2812014 05:37 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 26

-01
aceAnalocal
f wwwpact)abs-com
f
QUALITY CONTROL DATA
Project: Outfall 5115
Pace Project No.: 92201618
SAMPLE DUPLICATE: 1202425
92201354002
Dup
Parameter
Units
Result
Result
Chloroethane
uglL
NO
NO
Chloroform
uglL
NO
ND
Chloromethane
ug1L
NO
NO
cis- 1,2-Dichloroethene
ug1L
ND
NO
cis-1,3-Dichloropropene
uglL
NO
ND
Dibromochlorom ethane
i
ND
NO
Ethylbenzene
ug1L
NO
NO
Methylene Chloride
ug1L
ND
NO
Tetrachloroethene
uglt-
NO
NO
Toluene
ug1L
NO
NO
trans-1,2-Dichloroethene
uglL
NO
NO
trans- 1,3-Dichloropropen e
uglL
NO
NO
Trichloroethene
uglL
NO
ND
Trichlorofluoromethane
ug1L
NO
ND
Vinyl chloride
ug1L
NO
ND
1,2-Dichloroethane-d4 (S)
%
104
102
4-Bromofluorobenzene (S)
%
88
88
Toluene -dB (S)
%
98
97
RPD Qualifiers
2
0
0
Pace Analytical Services, Inc.
9800 KinceyAve, Suite 100
Huntersville, NC 28078
(704 )875-9092
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 05128/2014 05:37 PM without the written consent of Pace Analytical Services, Inc.,
Page 15 of 26

aceAnalytical
wtywpecelabs,Com
i�
I
QUALITY CONTROL DATA
Project: Outfali 5/15
Pace Project No.: 92201618
QC Batch: OEXT127835 Analysis Method: EPA 608
QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB
Associated Lab Samples: 92201618001, 92201618002
METHOD BLANK: 1204226
Associated Lab Samples: 92201618001, 92201618002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
4,4'-DDD
ug1L
ND
0.050
05127/1416A7
4,4'-DDE
ug1L
ND
0.050
05127/1416:47
4,4'-DDT
ug1L
ND
0.050
05/27/14 16:47
Aldrin
ug1L
ND
0.050
05/27/14 16:47
alpha-BHC
ug1L
ND
0.050
05/27/141647
beta-BHC
ug/L
ND
0.050
05/27/14 16:47
Chlordane (Technical)
ug/L
ND
0.50
05/27/14 16:47
delta-BHC
uglL
ND
0.050
05/27/14 16:47
Dieldrin
ug1L
ND
0.050
0512711416:47
Endosulfan I
ug1L
ND
0.050
05/27/14 16:47
Endosulfan 11
ug/L
ND
0.050
05/27/14 16:47
Endosulfan sulfate
ug/L
ND
0.050
05/27/14 16:47
Endrin
ug/L
ND
0.050
05/27/14 16:47
Endrin aldehyde
ug/L
ND'
0.050
05/27/14 16:47
gamma-BHC (Lindane)
ug/L
ND
0.050
05/27/14 16:47
Heptachlor
ug/4
ND
0,050
05/27/14 16:47
Heptachlor epoxide
ug/L
ND
0.050
05/27/14 16:47
PCB-1016 (Aroclor 1016)
ug/L
ND
0.50
05/27/14 16:47
PCB-1221 (Aroclor 1221)
ug/L
ND
0.50
05/27/14 16:47
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
05/27/14 16A7
PCB- 1242 (Aroclor 1242)
ug1L
ND
0.50
05127/14 16:47
PCB- 1248 (Aroclor 1248)
ug1L
ND
0.50
05/27/14 16:47
PCB-1254 (Aroclor 1254)
ug1L
ND
0.50
05/27/14 16:47
PCB-1260 (Aroclor 1260)
ug/L
ND
0.50
05/27/14 16:47
Toxaphene
ug/L
ND
0.50
05/2711416:47
Decachlorobiphenyl (S)
%
75
20-138
05/27/14 16:47
Tetrachloro-m-xylene (S)
%
50
20-110
05/27/14 16:47
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1204227
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
.25
0,18
75
31-141
4,4'-DDE
ug/L
.25
0.17
69
30-145
4,4'-DDT
ug/L
.25
0.18
74
25-160
Aldrin
ug/L
.25
0.11
43
42-122
alpha-BHC
ug/L
.25
0.18
73
37-134
beta-BHC
ug/L
.25
0.18
72
17-147
delta-BHC
ug/L
25
0.19
75
19-140
Dieldrin
ug1L
.25
0.18
72
36-146
Endosulfan I
ug1L
25
0.18
74
45-153
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 05:37 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 26

�;aqeAnalyfical
wwwperelabs.com
i
i
QUALITY CONTROL DATA
Project: Oulfall 5115
Pace Project No.: 92201618
LABORATORY CONTROL SAMPLE:
Parameter
1204227
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Endosulfan It
uglL
.25
0.19
77
1-202
Endosulfan sulfate
uglL
.25
0.20
81
26-144
Endrin
uglL
.25
0.19
75
30-147
Endrin aldehyde
uglL
.25
0.17
67
50-150
gamma-BHC (Lindane)
uglL
.25
0.18
72
32-127
Heptachlor
uglL
.25
0.12
49
34-111
Heptachlor epoxide
uglL
.25
0.17
68
41-126
Decachlorobiphenyl (S)
%
76
20-138
Tetrachloro-m-xylene (S)
%
71
20-110
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 05:37 PM without the written consent of Pace Analytical Services, Inc..
Page 17 of 26

aceAnalytical
! � :vwwpa:rlai:sccm
QUALITY CONTROL DATA
Project: Ou tfail 5115
Pace Project No.; 9220161 B
QC Batch; OEXT127846 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92201618001, 92201618002
METHOD BLANK: 1204687
Associated Lab Samples: 92201618001, 92201618002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
05127/14 20:33
2,4,6-Trichlorophenol
ug1L
NO
10.0
05/27114 20:33
2,4-Dichlorophenol
ug/L
ND
5.0
05/27/14 20:33
2,4-Dimethylphenol
ug1L
ND
10.0
05/27/14 20:33
2,4-Dinitrophenol
ug/L
NO
50.0
05127/14 20:33
2,4-Dinitrotoluene
ug1L
ND
5.0
05127/14 20:33
2,6-Dinitrotoluene
ug/L
NO
5.0
05/27114 20:33
2-Chloronaphthalene
ug1L
ND
5.0
05/27/14 20:33
2-Chlorophenol
ug1L
NO
5.0
05/27/14 20:33
2-Nitrophenol
uglL
NO
5.0
05/27/14 20:33
3,3'-Dichlorobenzidine
ug1L
NO
25.0
05/27/14 20:33
4,6- Din itro-2-methylphenol
ug1L
ND
20.0
05/27/14 20:33
4-Bromophenylphenyl ether
ug1L
ND
5.0
05127/14 20:33
4-Chloro•3-methylphenol
ug1L
NO
5.0
05/27/14 20:33
4-Chlorophenylphenyl ether
ug1L
Nln
5.0
05/27/14 20:33
4-Nitrophenol
ug1L
NO
50.0
05/27/14 20:33
Acenaphthene
ug1L
NO
5.0
05/27/14 20:33
Acenaphthylene
ugiL
ND
5.0
05127/14 20:33
Rnthracene
ug?L
NO
5.0
05127/14 20:33
Benzo(a)anlhracene
ug!L
N3
5-0
05/27/14 20:33
Benzo(a)pyrene
uglL
NO
5.0
05/27/14 20:33
Benzo(b)fluoranlhene
ug1L
ND
5.0
05/27/14 20.33
Benzo(g,h,i)perylene
ug1L
NO
5.0
05/27/14 20.33
Benzo(k)fluoranthene
ug/L
ND
5.0
05127/14 20:33
bis(2-Chtoroelhoxy)methane
uglL
ND
10.0
05127/14 20:33
bis(2-Chloroethyl) ether
ug1L
ND
5.0
05/27/14 20:33
bis(2-Chloroisopropyl) ether
uglL
NO
5.0
05/27/14 20:33
bis(2- Ethyl hexyl)phthalate
uglL
ND
5.0
05/27/14 20:33
Butylbenzylphthalate
uglL
ND
5.0
05/27114 20:33
Chrysene
ug/L
NO
5.0
05127I14 20:33
Di -n-butylphtha late
ug11-
No
5.0
05/27114 20:33
Di-n-octylphthe late
ug/L
ND
5.0
05/27/14 20:33
Dibenz(a,h)anthrecane
uglL
NO
5.0
05/27/14 20:33
Diethylphthalate
uglL
NO
5.0
05/27/14 20:33
D imethylphth a late
uglL
ND
5.0
05/27/14 20:33
Fluoranthene
ug/L
ND
5.0
05/27/14 20:33
Fluorene
i lL
ND
5.0
05127/14 20:33
Hexachloro-1,3-butadiene
uglL
ND
5.0
05/27/14 20:33
Hexachlorobenzene
ug1L
ND
5-0
05/27/14 20:33
Hexachlorocyclopentadiene '
ug1L
NO
10.0
05/27/14 20:33
Hexachloroethane
uglL
ND
5.0
05i27/14 20:33
Qualifiers
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the rigM of the resulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date; 05/2812014 05:37 PM wltheut the written consent of Face Analytical Services, Inc . Page 18 of 26

aceAnalyfical
mw..;wcelabs Coin
QUALITY CONTROL DATA
Project: Outfalt 5115
Pace Project No.: 9220161 B
METHOD BLANK? 1204687
Associated Lab Samples: 92201618001, 92201618002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
lndeno(1,2,3-cd)pyrene
uglL
ND
5.0
05/27/14 20:33
lsophorone
uglL
ND
10.0
05/27/14 20:33
N-Nitroso-di-n-propylamine
uglL
ND
5.0
05/27/14 20733
N-Nitrosodimethylamine
ug1L
ND
5.0
05/27/14 20:33
N-Nitrosodiphenylamine
ug1L
ND
10.0
05/27/14 20:33
Naphthalene
ug1L
ND
5.0
05/27/14 20:33
Nitrobenzene
ug1L
ND
5.0
05/27/14 20:33
Pentachlorophenol
uglL
ND
10.0
05/27/14 20:33
Phenanthrene
uglL
ND
5.0
05/27/14 20:33
Phenol
ug1L
ND
5.0
05/27/14 20:33
Pyrene
uglL
ND
5.0
05/27/14 20:33
2,4,6-Tribromophenol (S)
%
60
10-137
05/27/14 20:33
2-Fluorobiphenyl (S)
%
44
15-120
05/27114 20:33
2-Fluorophenol (S)
%
24
10-120
05/27/14 20:33
Nitrobenzene-d5 (S)
%
51
10-120
05/27/14 20:33
Phenol-d6 (S)
%
15
10-120
05/27/14 20:33
Terphenyl-d14 (S)
%
84
11-131
05/27/14 20:33
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1204688
Units
Spike
Conc.
LCS
Result
LGS
% Rec
% Rec
Limits
1,2,4-Trichlorobe nzene
ug/L
50
35.7
71
44-142
2,4,6-Trichlorophenol
ug1L
50
39.4
79
37-144
2,4-Dichlorophenol
ug1L
50
38.5
77
1-191
2,4-Dimethyl phenol
ug/L
50
34.4
69
32-119
2,4-Dinitrophenol
uglL
250
233
93
1-181
2,4-Dinitrotoluene
uglL
50
52.9
106
39-139
2,6-Dinitrotoluene
uglL
50
50.5
101
50-158
2-Chloronaphthalene
uglL
50
35.2
70
60-118
2-Chlorophenol
uglL
50
31.0
62
23-134
2-Nitrophenol
uglL
50
44.3
89
29-182
3,3'-Dichlorobenzidine
uglL
100
77.1
77
1-262
4,6-Dinitro-2- methyl phenol
ug1L
100
967
97
1-181
4-Bromophenylphenyl ether
ug1L
50
40.0
80
53-127
4-Chloro-3-methylphenol
ug1t.
100
82.7
83
22-147
4-Chlorophenylphenyl ether
ug1L
50
40.2
80
25-158
4-Nitrophenol
U91L
250
121
49
1-132
Acenaphthene
ug1L
50
35.5
71
47-145
Acenaphthylene
uglL
50
34.7
69
33-145
Anthracene
uglL
50
41.9
84
1-166
Benzo(a)anthfacene
uglL
50
39.8
80
33-143
Benzo(a)pyrene
ug/L
50
40.8
82
17-163
Benzo(b)iluoranthene
uglL
50
40.9
82
24-159
Benzo(g,h,i)perylene
ug/L
50
30.9
62
1-219
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NO 28078
(704 )875-9092
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 05/28/2014 05:37 PM
IN4li]a91daWTI -.'I*] 01111to] :Y/_V61
This report shali not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 26

_- I
"nalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: 0utfall 5115
Pace Project No.: 92201618
LABORATORY CONTROL SAMPLE:
Parameter
1204688
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Benzo(k)fluoranthene
ug/L
50
38.4
77
11-162
bis(2-Chloroelhoxy)methane
ug/L
50
38.2
76
33-184
bis(2-Chloroethyl) ether
ug1L
50
35.4
71
12-158
bis(2-Chloroisopropyl) ether
ug1L
50
36.0
72
- 36-166
bis(2-Ethylhexyl)phthalate
ugIL
50
41.2
82
8-158
Butyl benzylphthalate
uglL
50
42.5
85
1-152
Chrysene
uglL
50
39.7
79
17-168
Di-n-butylphthalate
uglL
50
38.3
77
1-118
Di-n-octylphthalate
ug1L
50
40A
81
4-146
Dibenz(a,h)anthracene
ug1L
50
32.2
64
1-227
Diethylphthaiate
ug11-
50
31
76
1-114
Dimethylphthalate
ugIL
50
40.8
82
1-112
Fluaranthene
ugIL
50
45.1
90
26-137
Fluorene
ug/L
50
40.6
81
59-121
Hexachloro-1,3-butadiene
ug1L
50
36.8
74
24-116
Hexachlorobenzene
ug/L
50
40.3
81
1-152
Hexachlorocyclopentadiene
ug1L
50
31.7
63
25-150
Hexachloroethane
ug/L
50
35.4
71
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
25.8
52
1-171
Isophorone
ug/L
50
49A
99
21-196
N-Nitroso-d i-n-propyla mine
ugIL
50
34.2
68
1-230
N-Nitrosodimethylamine
uglL
50
21.6
43
25-150
N-Nitrosodiphenylamine
uglL
50
32.6
65
25-150
Naphthalene
ug1L
50
32.2
64
21-133
Nitrobenzene
ug1L
50
50.6
101
35-180
Pentachlorophenol
ug1L
100
77.2
77
14-176
Phenanthrene
ugIL
50
41.0
82
54-120
Phenol
ug/L
50
16.0
32
5-112
Pyrene
ug1L
50
41.4
83
52-115
2,4,6-Tribromophenol (5)
%
100
10-137
2-Fluorobiphenyt (S)
%
74
15-120
2-Fluorophenol (S)
%
41
10-120
Nitrobenzene-d5 (S)
%
93
10-120
Phenol-d6 (S)
%
28
10-120
Terphenyl-d14 (S)
%
90
11-131
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, 128078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 05:37 PM without the written consent of Pace Analytical Services, Inc..
Page 20 of 26

aceAnalyfical
taww.paceiabs.tdm
I
QUALITY CONTROL DATA
Pace Analytical Services, Inc,
9800 Kincey Ave. Suite 100
Huntersville, 128078
[phone]
Project: Outfall 5115
Pace Project No.: 92201618
QC Batch: WET131158
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92201618001
METHOD BLANK; 1205108
Matrix:
Water
Associated Lab Samples: 92201616001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND
2.5 05/22/14 16:10
LABORATORY CONTROL SAMPLE:
1205109
Spike
LCS
LCS % Rec
Parameter
Units
Cone.
Result
% Rae Limits Qualifiers
Total Suspended Solids
mg/L
250
272
109 80-120
SAMPLE DUPLICATE: 1205110
92201582002
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
rri
&2
10.8 27 D6
SAMPLE DUPLICATE: 1205111
92201584007
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
26.4
27.8 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 05:37 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 26

aceAnalytical
wwwpacela8scom
I
I
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve, Suite 100
Huntersville, NC 28C78
[phone]
Project: Outfall 5115
Pace Project No.: 92201618
QC Batch: WET131162
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92201618002
METHOD BLANK: 1205422
Matrix: Water
Associated Lab Samples: 92201618002
Blank Reporting
'
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 05/22/14 22:42
LABORATORY CONTROL SAMPLE:
1205423
Spike LCS
LCS. % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 272
109 80-120
SAMPLE DUPLICATE: 1205424
92201618002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
6.6
ND
SAMPLE DUPLICATE: 1206425
92201690002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an anernate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 05:37 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 26

7aceAnaVical 2
wwwpecelabs.com
r
I
QUALIFIERS
Project: Outfah 5115
Pace Project No.: 92201618
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method B270. The result reported for
each analyte is a combined concentration
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full,
Date: 05/28/2014 05:37 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 26

aceAnalytical
I wwwpacelabs.corn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Outfall 5115
Pace Project No.: 92201618
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
92201618001
OUTFALL #1
EPA 1664B
GCSVI17643
92201618002
OUTFALL #2
EPA 1664B
GCSV117643
92201618001
OUTFALL #1
EPA3510
OEXT127835
EPA 608
92201618002
OUTFALL #2
EPA3510
OEXTl27835
EPA 608
92201618001
OUTFALL #1
EPA200.7
MPRP115999
EPA 200.7
92201618002
OUTFALL #2
EPA 200.7
MPRP115999
EPA 200.7
92201618001
OUTFALL #1
EPA625
OEXTI27846
EPA 625
92201618002
OUTFALL #2
EPA 625
0EXT127846
EPA 625
92201618001
OUTFALL #1
EPA 624
MSV126872
92201618002
OUTFALL #2
EPA 624
MSV126872
92201618001
OUTFALL #1
SM 2540D
W ET131158
92201618002
OUTFALL #2
SM 2540D
WETl31162
& Date: 05/2812014 05:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except it full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
GCSV117718
GCSV117718
ICP114473
ICP114473
MSSV19169
MSSVI9169
Page 24 of 26

CHAIN -OF -CUSTODY i Analytical Request. Document
72eAmlyi ! Tthe Chain -of -Custody is a LEGAL DOCUMENT. Alt relevant fields must be completed accurately.
rD
4
• _wivw.pacenhrs.nam -
-
Paps: of rn
Sectjon A ' Section B Section C
m„
Required Client Information: Required Project Information: - invoice Information;
Wr: _
Gumpany: -yf Report To: j Atten72
jj
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Address:, � - f..! 1 ..
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Copy
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REGI LATOf2Y'AGENGY. � _•_ .. - - - _ __
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Address: St :;Y
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NP[)ESw �: .• GRQUND WATER r- (" . DRINKING WATER
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Email To: ` Purchase
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Order No.: - ..
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Fax: Project
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RetlussSedDue DafelTAT: Project
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Section D Matrix Codes
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Wavle Water WW
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Samplo IDs MUST BE LIM61JE Tissue TS
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RELINQUISHES BYIAFFIL1ATiON#,,; ;=i
DATE;
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DATE `:
TIME'.'
SAMPL@ C{7NDIT10N5 '
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SAMPLER NAME AND SIGNATURER o- I
PRINT Name Of SAMPLE�
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SIGNATURE of SAMPLER: � II /
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DATE Signed _ _
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(MMIODNY):
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'Important Note'. BY signing ihr lam you are accepting Pace's NET 30 lay payment terms and agmairg tc Iats charges 0f 1.5% per month for any tnvOICes net W within 30 days. - r - F-ALL-Q-020rev,07; 15-May-2007

Document Name: Sample Condition Upon
Document Revised: April 9, 2014
aceAnalytical�
I a
Receipt SCUR
Page I of 2
Document No.:
Issuing Authorities:
""'"�'
>"-ASV-CS-003-rev.1
Pace Asheville Quality Office
Courier (Circle): Fed Ex UPS LISPS Glienf Commercial Pace Other
Custody Seal on Cooler/Box Present: yes o Seals intact: yes no
Packing Material: 0 Bubble Wrap Bubble Sags lone Other
Thermometer Used: I<Gun#3 -13026 6 Type of Ica: Wet Blue None amples on ice, cooling process nos begun
Othe,
Temn Correction Factor: Add ! Subtract C
r�c o
Corrected Cooler Temp.: r'b C Biological Tissue is Frozen: Yes No NIA
Temp should be above freezing to 6°C Comments:
Date and initials o arson a amin' g
contents: r 1 'f
Chain of Custody Present: es No ❑wA
1.
Chain of Custody Filled Out: Ules No ❑NIA
2.
Chain of Custody Relinquished; 1241ao No ❑NIA
3.
Sampler Name & Signature on COC: es No ❑NIA
4.
Samples Arrived within Hold Time: es ONo NIA
5.
Short Hold Time Analysis <72hr): ❑Yea o NIA
6.
Rush Turn Around Time Requested: 0Yes o OwA
7.
Sufficient Volume: aVIL❑No ❑NIA
8.
Correct Containers Used: Zl,% ❑No ❑NIA
-Pace Containers Used: es too ❑NIA
9.
Containers intact: es ©No ONA
Filtered volume received for Dissolved tests ❑Yes o IA
11.
Sample Labels match COC: ea ❑ o ❑NIA
-includes date/time/ID/Analysis Matrix: W.
12.
All containers needing preservation have been checked.
❑ s Na El NIA
All containers needing preservation are found to be in es No ❑NIA
compliance with EPA recommendation -
exceptions: VOA, cdiform, TO O&G, I-DRO (water)
13.
Samples checked for dechlorination: 5Z<es ❑No 2NiA
14.
Headspace in VOA Vials (>6mm): ❑Yes Elo WA
15.
Trip Blank Present: Dyes No NIA
Trip Blank Custody Seals Present [Yes o ❑wA
Pace Trip Blank Lot # ifpurchased):
16.
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review:
Date:
SRF Review: e — JDate: ' Y
Note: Whenever there is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i,e out of hold, incorrect
preservative, out of temp, incorrect containers)
WOi{ : 92201618
92201618
a
Page 26 of 26

4
Semi-annual St_ormwater Discharge Monitoring_ Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _May 21, 2014,
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Environmental Testing Solutions Lab Cert. #600mg/L
Comments on sample collection or analysis: See
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2014
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ® Monthly' April (month)
DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
®Other: Class C, Swannanaa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
® No discharge this period?2
Outfall No.
Date Sample
,
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
s
Organics
Benchmarks =__>
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
' Monthly sampling (instead'of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Received
J U N 13 2014
Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012
Land Quality Section Page 1 of 4
Asheville

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Sal Vaccaro
Name (Print name)
General_ Manager
Title [Print it J
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera! Permit text.
Part I3: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
® No discharge this period?Z
Outfali No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part iB
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

r:.
r
f
' Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER I REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME:
Mail an on final and one copy of this DMR includin all "No Discharge' re oMs within 30 days of receipt of the lab results for at end of monitorin eriod
in the case of "No Discharge" reports) to:
Division of Water Quality
4ttn: DWQ Central Files
-617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
of Permitteej
d-l"? I i y
(Date]
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 4

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted April 21, 2014
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls_
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkies
LABORATORY: Environmental Testing Solutions Lab Cert. #i600mg/L
Comments on sample collection or analysis: See page 4
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2014
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ® Monthly' March (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
®Other: Class C, Swannanoa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
No discharge this period:2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
inches,
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Nan -Polar O&G/Total
Total petroleum
Hydrocarbons
Toxic
Organicss
Benchmarks ===>
-
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
03-17-2014
0.31
29 mg/L
7.2
0.049 mg/L
<0.020
0.064 mg/L
<5.0 mg/L
BRL
2
03-17-2014
0.31
<5.0 mg/L
7.5
0.030 mg/L
<0.020
.085 mg/L
<5.0 mg/L
BRL
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
" See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic Crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
WAY -1 2014 '..
MAY -1 2W
Permit Date: 11/1/2012-10/31/2017 tand QUafty Sectim W&W
Asheville I AsheWls Aeeional nfrim
SWU-245, last revised 10/25/2012
Page 1 of 4

OBVII-203FI
=.-I t; mxvQ
UM I — Y.4141
yum
tracep

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
May be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit, For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since fling the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Sal Vaccaro
Name (Print name)
General Manager
Title (print 'tle)
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera! Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks ===>
-
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text
FOR PART A AND PART B MONITORING RESULTS:
s A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
s 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
s TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days_of receipt of the lab results (or at end at monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
{Signatu
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 4

1) Zinc,reporting value exceeds permit limit 0.067 for outfall #2
a) Finding;
i) Roofing material is galvanized metal could be a contributing factor for outfall #2.
b) Corrective actions;
i) Review BMP, ensured good management practices are being followed.
2) Copper reporting value exceeds permit limit 0.007 for outfall # 1 and 42
a) Finding;
i) Roofing material is metal could be a contributing factor for outfall #land Q.
ii) Scrap Lugger pad could be a contributing factor for outfall #1. We do not find potential sources of copper exposure in outfall 92.
b) Corrective actions;
i) Review of BMP's
ii) Have increased housekeeping, Lugger Pad Area and Center Pad are being inspected and cleaned weekly.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 4 of 4

0
O
0
0
0
V) Environmental Testing Solutions, Inc.
Project name:
Pentair
Collection date:
17-Mar-14
Date received:
17-Mar-14
Sample identification: Outfall #1
Certificate of Analysis
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 140317.509
Sample number: 114361
Parameter
Method
Result RL
Units
Date
Analyst Footnotes
Analyzed
624
624 - 8260 B
See Attached sheet
µg/L
20-Mar-14
LBW 1
625
625 - 8270 D
See Attached Sheet
µg/L
29-Mar-14
RJM 1
608
608
See Attached sheet
µg/L
26-Mm44
RKH 1
Solids, Total Suspended
SM 9222-D
29 5.0
mg/L
19-Mar-14
KW
Oil & Grease, Total HEM
1664 A
<5.0 5.0
mg/L
21.Mar-14
CTS
Copper
200.8
0.049 0.001
mg/L
19-Mw44
DER I
Lead
200.7
<0.020 0.020
mg/L
20-Mar44
MEC I
Zinc
200.7
0.064 0.010
mgfL
20-Mar.14
MEC
Sample identification: Outfall #2
Sample number:
114362
Parameter
Method
Result RL
Units
Date
Analyst Footnotes
Analyzed
624
624 - 8260 B
See Attached Sheet
µg/L
20-Mar-14
LBW
625
625 - 8270 D
See Attached Sheet
µg/L
28-Mar-14
RJM 1
608
608
See Attached Sheet
µg/L
26-Mar-14
RKH
Solids, Total Suspended
SM 9222-D
<5.0 5.0
mg/L
19-Mar-14
KW
Oil & Grease
1664 A
<5.0 5.0
mg/L
21-Mar-14
CTS I
Copper
200.7
0.030 0.001
mg/L
19-Mar-14
DER I
Lead
200.7
<0.020 0.020
mg/L
20-Mar-14
MEC I
Zinc
200.7
0.085 0.010
mg/L
20-Mar-14
MEC I
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
Date reviewed:
Data reviewed by: Kelley E. Keenan
Signature:
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirely, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

a Rogers & Callcott
ENVIRONMENTAL
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 28801-4310
Dear Client:
Laboratory Report
Project:
Work Order:
Received:
Laboratory Services
Pentair
4030600
03/18/2014 10:30
Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of
custody for samples that were received on March 18, 2014. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all
analyses performed under NELAP certification have complied with all the requirements for the NELAC standard. The analyses met the QA/QC
confidence interval for each test method unless otherwise qualified, Estimated uncertainty is available upon request.
Privileged 1 Confidential information may be contained in this report and is intended only for the use of the addressee. if you are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by
mistake, please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients. Please contact Amy Ashley, your Project Manager, at anty.ashley a rogersandeallcott.com or
(864)-335-4962 if you have any questions about this report,
Report Approved By:
ozlln ',
Amy Ashley
Project Manager
This mporl muv not he mprodaced, evicepa in fill. %whouu wriiren permissionirwa Rogers & (ullcon, Inc.
PO Box 5655 1 Greenville, SC 29606 1 426 Fair -forest Way I Greenville, SC 29607 1 main 864,232.1556 1 fax [phone] rogersandcallcott.com
an employee -owned company
Page 1 of 31

�rl� Rogers & Callcott
t ENVIRONMENTAL
South Carolina Greenville Laboratory Identification 23105
Certificate
of Analysis
South Carolina Columbia LaboraforyIdentification 40572
North Carolina Laboratory Certification Nunther 27
North Carolina Drinking Water Lah Number 45710
NELAP Laboratory Identification E87822
Client
Environmental Testing Solutions
Project: Pentair
Kelley E. Keenan
Work Order: 4030600
351 Depot St.
Received: 03/18/2014 10:30
Asheville, NC 288014310
Sample Number
Sample Description
Matrix Sampled
Type
4030600-01
Pentair Outfal1 91 - Grab
Other 03/17/14 09:05
Grab
4030600-02
Pentair Outfal I #1 -Grab
Other 03/17/14 09:05
Grab
4030600-03
Pentair Outfall #2 - Grab
Other 03/17/14 09:10
Grab
4030600-04
Pentair Outfall #2 - Grab
Other 03/17/14 09:10
Grab
PO Box 5655 1 Greenville, SC 296% ! 426 Fait -forest Way I Greenville, SC 29607 1 main 864.232.1556 9 fax [phone] rogersandealleott.eom
an employee -owned company
04,0412014 08:09 Thi.v report Wray not be reproduced, except inridl, xvithout written pennission jroni Rai;ery & Callcou, Inc.
Page 2 of 31

a Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot SL Work Order: 4030600
Asheville, NC 28801-4310 Reported: 04/04/14 09:09
Sample Data
Sample Number 4030600-01
Sample Description Pentair OutfalI I - Grab collected on 03/17/14 09:05
Reporting
Parameter Result Limit Units
DF
Analyzed
Method
Flag Analyst
Batch
General Chemistry Parameters
Oil and Grease, Total, HEM
ND
5.0
m8/L
1.00
03/21/14 08:00
EPA 1664A
CTS
134C0664
Total Metals
Copper
0.049
0.001
mg/l.
1.00
03/19/14 15:53
EPA 200.8
DER
134C0590
Lead
ND
0.020
mg/L
1.00
03/20/14 12:47
EPA 200.7
MEC
134C0600
Zinc
0,064
0.010
mg/L
1.00
03/20/14 12:47
EPA 200.7
MEC
B4C0600
Volatile Organics
Benzene
ND
2.0
UO,
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
Bromoform
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
Carbon tetrachloride
ND
2.0
ug/l,
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
Chlorobenzene
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
Dibromochloromethane
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
Chloroethane
ND
2.0
uglL
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
2-Chloroethylvinyl ether
ND
5.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
Chloroform
ND
2.0
ugfL
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
Bromodichloromethane
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
1,1-Dichloroethene
ND
2,0
uglL
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
1,2-Dichloroethene
ND
2,0
ugfL
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
trans-1,2-Dichloroethene
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
1. 1 -Dichloroethene
ND
2.0
a81L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
1,2-Dichloropropane
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
114C0837
Ethylbenzene
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
64CO837
Bromomethane (Methyl Bromide)
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
Chloromethane (Methyl Chloride)
ND
2.0
ugll,
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
1,1,2.2-Tetrachloroethane
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
Tetrachloroethene
ND
2.0
ug/L
1,00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
Toluene
ND
2.0
Ug/t,
1.00
03/20/14 10:50
EPA 624-8260B
LAW
B4C0837
1,1,l-Trichloroethane
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
1,1,2-Trichloroethane
ND
2.0
ugfL
1,00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
Trichloroethenc
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
Vinyl chloride
ND
2.0
ug/L
L00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
Dichlorodifluoromethane
ND
2.0
ug1l,
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
Methylene Chloride
ND
2,0
ug/L
1,00
03120/14 10:50
EPA 624-8260B
LBW
134C0837
Trichlorofluoromethane
ND
2.0
ugli.
1.00
03120,114 10:50
EPA 624-8260B
LBW
B4C0837
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.com
an employee -owned company
04 04QO14 0:09 Tbi.% report may not be repr`xluced, except in,frdl, without urillen permission from Rogers & Colima. Inc.
Page 3 of 31

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported- 04/04/14 08:09
Sample Number 4030600-01
Sample Description Pentair Outfall # 1 - Grab collected on 03/17/14 09:05
Parameter
Result
Reporting
Limit
Units
DF
Analyzed
Method
Flag Analyst
Batch
Volatile Organics
1,2-Dichlorobenzene
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
13-Dichlorobenzene
ND
2.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
1,4-Dichlorobenzene
ND
2.0
ug1L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
1,2,4-1'richlorobenzene
ND
2.0
og/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
cis-1,3-Dichloropropene
ND
1.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
134C0837
trans- l,3-Dichloropropene
ND
1.0
ug/L
1.00
03/20/14 10:50
EPA 624-8260B
LBW
B4C0837
Surrogates
% REC
% REC Limits
Flag
1,1-Dichlarocthane-IN
78
70-130
!-Ntanrofluaruhrn_enc
102
70-130
Toluene-IM
99
70-130
Semi-Volatiles Organics
2-Chlorophenol
ND
5.00
ug/L
1,00
03/28/14 15:43
EPA 62518270D
RJM
B4C0739
2,4-Dichlorophcnnl
ND
5.00
ubA.
1,00
03/28/14 15:43
EPA 625/8270D
RJM
B4C0739
2,4-Dimethylphenol
ND
5.00
uglL
1.00
03/28/14 15:43
EPA 625/8270D
RIM
B4C0739
2-Methyl4,6-dinitrophenol
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 625/8270D
RJM
B4C0739
2,4-Dinitrophenol
ND
5.00
ug/L
1,00
03/28/14 15:43
EPA 625/8270D
RJM
134C0739
2-Nitrophenol
ND
5.00
ug/1.
1.00
03/28/14 15:43
EPA 625/8270D
RJM
B4C0739
4-Nitrophenol
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 62518270D
RJM
B4C0739
p-Chloro-m-cresol
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 625/9270D
RJM
144C0739
Pentachlorophenol
ND
5.00
ugn.
1.00
03/28/14 15:43
EPA 62518270D
RJM
B4C0739
Phenol
ND
5,00
ug/L
1.00
03/28/14 15:43
EPA 62518270D
RJM
134C0739
2,4,6-Trichlorophenol
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 62518270D
RJM
B4C0739
Acenaphthene
ND
5.00
ug/L
1.00
03/28/14 15A3
EPA 625/8270D
RJM
B4C0739
Acenaphlhylene
ND
5.00
ug/L
1.00
03128/14 15:43
EPA 62518270D
RJM
B4C0739
Anthracene
ND
5.00
ug11.
1.00
03/28/14 15:43
EPA 625/9270D
RJM
B4C0739
Benzidine
ND
80,0
ug/L
1.00
03/28/14 15;43
EPA 625/8270D
RJM
B4C0739
Benzo(a)anthracene
ND
5.00
uWL,
1.00
03/28/14 15:43
EPA 625192701)
RJM
134C0739
Benzo(a)pyrene
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 625/8270D
RJM
134C0739
Benzo(b)fluoranthene
ND
5,00
ug/L
1.00
03/28/14 15:43
EPA 625/8270/)
RJM
134C0739
Bcnzo(g,h,i)perylene
ND
5.00
ug/L.
1.00
03/28/14 15:43
EPA 625/9270D
RJM
B4C0739
13enzo(k)fluoranthene
N❑
5.00
ug/L
1.00
03/28/14 15:43
EPA 62518270D
RJM
B4C0739
Ais(2-chloroethoxy)Methane
ND
5.00
ug/L
1.00
03/28/14 15:43
EiPA 62518270[)
RJM
134C0739
Bis(2-chloroethyl)Ether
ND
5.00
ug/L
1,00
03/28/14 15:43
lIPA 6251827013
RJM
B4C0739
bis(2-Chloroisopropyl)cther
ND
5.00
ug/L
L00
03/28/14 15:43
EPA 62518270D
RJM
B4C0739
Bis(2-ethylhexyl)Phthalatc
ND
5.00
ug/L
1.00
03/28/14 15:43
FPA 62$/8270D
RJM
B4C0739
PO Box 5655 1 Greenville, 5C 29606 1 426 Fairdorest Way I Greenville, 5C 29607 1 main 864,232.1556 1 tax 864.232.6140 rogersandeallcott.eom
an employee owned company
04,0412014 118:09 This report may not he reproduced, excepl in frill, withow xriteen permission from Rogers & Calleon, Inc.
Page 4 0( 31

b Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville, NC 298014310 Reported: 04/04/14 08:09
Sample Number 4030600-01
Sample Description Pentair Outfall 41 -
Grab collected on 03/17/14
09:05
Reporting
Parameter
Result
Limit
Units
DF
Analyzed
Method
Flag Analyst
Batch
Semi-Volatiles Organics
4-Bromophenylphenyl ether
ND
5.00
w /l-
1.00
03/28/14 15:43
EPA 62518210D
RJM
134C0739
Butylbenzylphthalale
ND
5.00
ub1L
1.00
03/28/14 15:43
EPA 6251827013
RJM
134C0739
2-Chioronaphthalene
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 62518270D
RIM
134C0739
4-Chlorophenylphenyl ether
ND
5,00
WiL
1.00
03/28i14 15:43
EPA 62518270D
R1M
84CO739
Chrysene
ND
5.00
ugil.
1.00
03/28/14 15:43
EPA 62518270D
RJM
134C0739
Dibenzo(a,h)anlhracene
ND
5-00
ug/L
1.W
03/28/14 15:43
EPA 625/82701)
RIM
114C0739
3,3'-Dichlorobcnzidine
ND
5.00
ugA.
1.00
03/28/14 15:43
EPA 62518270D
RIM
134C0739
Diethylphthalate
ND
5.00
Ug/L
1.00
03/28/14 15:43
EPA 625/8270D
RIM
134C0739
Diniethylphthalate
ND
5.00
u8J1.
1.00
03/28/14 15:43
EPA 625/8270D
RIM
134C0739
Di-n-butylphthalate
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 625/8270D
RIM
134C0739
2,4-Dinitrotoluene
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 625/82701)
RIM
B4C0739
2.6-Dinitrotoluene
ND
5,00
ug/L
1.00
03/28/14 15:43
EPA 625182701)
RJM
134C0739
Di-n-octylphthalate
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 625/8270D
RJM
134C0739
1,2-Diphenylhydrazene(Azobenzene)
ND
5.00
ugll.
1.00
03/28/14 15A3
EPA 625/8270D
RIM
134C0739
Fluoranthene
ND
5,00
ug/L
1.00
03/28/14 15:43
EPA 625/8270D
RJM
B4C0739
Fluorene
ND
5.00
u0.
1.00
03/29/14 15:43
EPA 625/8270D
RJM
B4C0739
Hcxachlorebenzene
ND
5,00
1164,
1.00
03128/14 15-43
EPA 625/8270D
RJM
B4C0739
Hexachlorobuladiene
ND
5.00
ugll.
1.00
03MI14 15:43
EPA 62518270D
RJM
B4C0739
1-lexachlorecyclopenladicne
ND
5.00
u91L
1.00
03/28/14 15:43
EPA 62519270D
RIM
134C0739
Hexachloroethane
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 625/8270D
RJM
B4C0739
lndeno(1,2,3-cd)pyrene
ND
5.00
ug1L
1.00
03/28/14 15:43
EPA 62518270D
RIM
B4C0739
Isophorone
ND
5.00
ug/l.
1.00
03/28/14 15:43
EPA 625/82701)
RIM
B4C0739
Naphthalene
ND
5,00
ug/L
LD0
03/28/14 15:43
EPA 62518270D
RIM
134C0739
Nitrobenzene
ND
5.00
ugfL
I.00
03/28/14 15:43
EPA 62518270D
RJM
134C0739
N-Nitroso-di-methylatnine
ND
5.00
ugll,
I.00
03/28/14 15:43
EPA 625/8270D
RJM
134C0739
N-Nitroso-di-n-propylamine
ND
5.00
ug1L
1.00
03/28/14 15:43
EPA 625/8270D
RJM
114C0739
N-Nilrosodiphenylamine (Diphenylamine)
ND
5.00
ug1L
1.00
03/28/14 15:43
EPA 625/8270D
RIM
134C0739
Phenanthrene
ND
5.00
ugJL
1,00
03/28/14 15:43
EPA 62518270D
RJM
134C0739
Pyrene
ND
5.00
ug/L
1.00
03/28/14 15:43
EPA 625W70D
RJM
W0739
Surrogates
%REC
% REC Limits
Flag
Numhemene-W
70
35-114
2-1--hwrohtplieMl
90
43-116
Terphenyl-1)14
86
33-141
2-Flnomphewd
46
21-110
Pheuol-1)5
30
10-I 10
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.com
an employee -awned company
04,0412014 08: u9 This reporl muy na1 he reprrdiuced, ercepl in,fiill. xilleoiu x-riven permission from Rogers & Collcon, 1ne.
Page 5 of 31

�bRogers & Callcott
,m ENVIRONMENTAL_
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville, NC 28801-4310 Reported: 04/04/14 08:09
Sample Number 4030600-01
Sample Description Pentair Oulfall # 1 - Grab collected on 03/17/14 09:05
Reporting
Parameter Result Limit Units D>H Annlyred Method Flag Analyst Batch
Semi-Volatiles Organics
Surrogates %REC %REC Limits Flag
2, a, 6-Tribromophenot 97 10-123
PCBs
PCB-1016
ND
0.50
ugiL
1.00
03/26/14 23:15
EPA 608
RKH
B4C0673
PCB-1221
ND
0.50
ug1L
1.00
03/26/14 23:15
EPA 608
RKH
134C0673
PCB-1232
ND
0.50
uglL
1.00
03/26/14 23:15
EPA 608
RKH
134C0673
PCB-1242
ND
0.50
ugiL
1.00
03/26/14 23:15
EPA 608
RKH
134C0673
PCB-1248
ND
0,50
ug1l-
1.00
03/26/14 23:15
EPA 608
RKH
114C0673
PCB-1254
ND
0.50
uglL
1.00
03/26/14 23:15
EPA 609
RKH
134C0673
PCB-1260
ND
0.50
ug1L
1.00
03/26/14 23:15
EPA 608
RKH
B4C0673
Surrogates
%REC
%REC Limits
Flag
2,4,5,6-Tcrrachl(,ro-m-.rylenc
100
60-130
Decuchlowhiphenli-I
77
30-150
Sample Number
4030600-02
Sample Description
Pentair OutfalI #1 - Grab collected on 03/17/14
09:05
Reporting
Parameter
Result
Limit
Units
DF
Analyzed
Method
Flag
Analyst
Batch
Volatile Organics
Acrolein
ND
5.0
uglL
1.00
03/24/14 14:24
EPA624-8260B
LBW
B4C0865
Acrylonilrile
ND
5.0
ugiL
1.00
03/24/14 14:24
EPA 624-8260B
LBW
B4C0865
Surrogate
%REC
%REC Limits
Flag
1,2-Dchloroethane-D4
85
70-130
'1'uhrene-1)8
101
70-130
4-Rromofltrorohen=ene
106
70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fair -forest Way 1 Greenville, SC 29607 1 main 664.232.1556 1 fax [phone] rogersandeallcott.com
an employee -owned company
04 0412014 OR:09 This reporl uruy not he reprachiced, except in find!, wilhoat written pernrission.1rom Roger.¢ & Callcou, Inc.
Page 6 of 31

Rogers & Callcott
ENVfRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Sample Number 4030600-03
Sample Description Pentair Outfall 42 - Grab collected on 03/17/14 09:10
Reporting
Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch
General Chemistry Parameters
Oil and Grease,'rotal, ITEM
ND
5.0
mg/L
1.00
03/21/14 08:00
EPA 1664A
CTS
B4C0664
Total Metals
Copper
0.030
0,001
mt;n-
1.00
03/19/14 15:58
EPA 200.8
DER
B4C0590
Lead
ND
0.020
nigh,
1.00
03/20/14 12:50
EPA 200.7
MEC
B4C0600
Zinc
0.085
0.010
mall.
1.00
03/20/14 12:50
EPA 200.7
MEC
B4C0600
Volatile Organics
Benzene
ND
2.0
ugfL
1.00
03/20/14 11:19
EPA 624-8260B
LBW
134CO837
Bromoform
ND
2.0
ug/L
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Carbon tetrachloride
ND
2.0
ugl1.
1.00
03/20/14 11:19
EPA 624-826013
LBW
B4C0837
Chlorohenzene
NI)
2.0
uglL
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Dibrornochloromcthane
ND
2.0
uglL
1.00
03/20/14 11:19
EPA 624-8260B
L13W
134C0837
Chloroethane
ND
2.0
ug/L
1.00
03/20/14 1119
EPA 624-8260B
LBW
B4C0837
2-Chloroethylvinyl ether
ND
5.0
uWL
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Chloroform
ND
2.0
ug/L
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Bromodichloromethane
ND
2.0
ug/l•
1.00
03/20/14 11:19
EPA 624-8260B
LBW
134C0837
I,1-Dichloroethane
ND
2.0
uglL
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
1,2-Dichloroethane
ND
2.0
ug/L
1,00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
trans-1,2-Dichtoroethene
ND
2.0
ug/L
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
],1-Dichloroethene
ND
2.0
ug/L
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
1,2-Dichloropropane
ND
2.0
ug1L
1.00
03/20/14 11:19
EPA 624-9260B
LBW
B4C0837
lithylbenzene
ND
2.0
ug/L
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Bromomethane (Melhyl Bromide)
ND
2.0
ug/L
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Chloromethane (Methyl Chloride)
ND
2.0
ug/l,
1.00
03/20/14 11:19
EPA 624-9260B
LBW
B4C0837
1,1,2,2-Tetrachlotoethane
ND
2.0
ug/L
1.00
03/20/14 11:19
EPA 624-8260B
I,BW
B4C0837
Tetrachloroethene
ND
2.0
ug/l.
I
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Toluene
ND
2.0
ug1l,
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
1,1,1-Trichloroethane
ND
2.0
ug/L
1.00
03/20/14 11:19
EPA 624-8260B
LBW
134C0837
1.1,2-Trichloroethane
ND
2.0
ug1L
1,00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Trichloroethene
ND
2.0
ugll-
I
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Vinyl chloride
ND
2.0
ug/L
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Dichloroditluoromethane
ND
2.0
ugll,
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Methylene Chloride
ND
2.0
ugfi,
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Trichlorofluoromethane
ND
2.0
ugiL
1,00
03120M4 11:19
EPA 624-8260B
LBW
B4C0837
1,2-Dichlarobenzene
ND
2.0
00,
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
1,3-Dichlorobenzene
ND
2.0
ug/l,
1.00
03/20/14 11:19
EPA 624-8260B
LBW
114C0837
PO Box 5655 1 Greenville, SC 29606 1426 Fairforest Way 1
Greenville,
SC 29607 main 864.232.1556 1 tax 864.232.6140 rogersandcallcott,com
an employee -owned company
04d14/2014 08:09 This nPnrl tatty not he reproduced, except in Iidl, wilhout wrilten permiatvion front Rogers & ('ullcolf. Inc. page 7 of 31

�b Rogers & Callcott
1r ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Sample Number
4030600-03
Sample Description
Pentair Oullall #2 - Grab collected on 03/17/14 09:10
Reporting
Parameter
Result
Limit
Units
DF
Analyzed
Method
Flag Analyst
Batch
Volatile Organics
1,4-Dichlorobenzene
ND
2.0
ug/L
1,00
03/20/14 11:19
EPA 624-8260B
LBW
B40837
1,2,4-Trichlorobenzene
ND
2.0
ug1L
1,00
03/20/14 11:19
EPA 624-826013
LBW
B4C0837
cis-1,3-Dichloropropene
ND
1.0
uglL
1.00
03/20/14 11:19
EPA 624-826013
LBW
B4C0837
trans-1,3-Dichloropropene
ND
1.0
ug/L
1.00
03/20/14 11:19
EPA 624-8260B
LBW
B4C0837
Surrogates
% REC
% REC Limits
Flag
1,2-Diehl oroelhane-D4
81
70-130
4-Broma heorahenrene
106
70-130
7oluene-D8
99
70-130
Semi-Volatiles Organics
2-Chlorophenol
ND
5,00
ug/L
1.00
03/28/14 16:13
EPA 62518270D
RJM
B4C0739
2,4-Dichlorophenol
ND
5,00
uglL
1.00
03/28/14 16:13
EPA 625I8270D
RJM
B4C0739
2,4-13imethylphenol
ND
5.00
utJL
1.00
03/28/14 16:13
EPA 625I8270D
RJM
134C0739
2-Methyl-4,6-dinitrophenol
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
2,4-Dinitrophenol
ND
5.00
ug/L
1,00
03/28/14 16:13
EPA 62518270D
RJM
B4C0739
2-Nitrophenol
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 62518270D
RJM
B4C0739
4-Nitrophenol
ND
5.00
ugJ1.
1.00
03P28/14 16:13
EPA 625/8270D
RJM
134C0739
p-Chloro-m-cresol
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
B4C0739
Pentachlorophenol
ND
5,00
ug11.
1,00
03/28/14 16:13
EPA 625I8270D
RJM
B4C0739
Phenol
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625I8270D
RJM
134C0739
2,4,6-Trichlorophenol
ND
5.00
ugli,
1.00
03/28/14 16:13
EPA 625/8270D
RJM
B4C0739
Acenaphthene
ND
5.00
UO,
1.00
03/28/14 16:13
EPA 625/8270D
RJM
B4C0739
Acenaphthylene
ND
5.00
ug/L
1,00
03/29/14 16:13
EPA 62518270D
RJM
B4C0739
Anthracene
ND
5.00
oy/L
1.00
03/28/14 16:13
EPA 625I8270D
RJM
B4C0739
Benzidine
ND
80.0
ugll-
1.00
03/28/14 16:13
EPA 625I8270D
RJM
B4C0739
Benzo(a)anthracene
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/9270D
RJM
B4C0739
Benzo(a)pyrene
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 62518270D
RJM
134C0739
Benzo(b)fluoranthene
ND
5.00
ugll.
1.00
03/28/14 16:13
EPA 62519270D
RJM
B4C0739
Benzo(g,h,i)perylene
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 62518270D
RJM
134C0739
Benzo(k)lluoranthcne
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 62518270D
RJM
134C0739
Bis(2-chloroethoxy)Methane
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
Bis(2-chlorocthyl)Ether
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
bis(2-Chloroisopropyl)ether
ND
5-00
uglL
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
Bis(2-ethylhexyl)Phthalate
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
B4C0739
4-Bromophenylphenyl ether
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
B4C0739
Butylbenzylphihalate
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
PO Box 5655 1 Greenville, SC 29606 1 426 hirforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.COm
an employee -owned company
04,0V2014 08:09 This report may not he reproduced, ercepi inTdl, without wriilen permission frwit Rogers & Cullcott. Inc.
Page 8 of 31

7
Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville, NC 28801-4310 Reported: 04/04/14 08:09
Sample Number 4030600-03
Sample Description Pentair Oulfall #2 - Grab collected on 03/17/14 09:10
Reporting
Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch
Semi-Volatiles Organics
2-Chloronaphthalene
4-Chlorophenylphenyl ether
Chryscne
Dibenzo(a,h)anihracene
3,Y-Dichlorobenzid ine
Diethylphihalate
Dimethylphthalate
Di-n-butylphthalate
2,4-Dinitrotoluerie
2,6-Dinilrotoluene
Di-n-octylphihalate
12-Dipheny1hydrazene(Azobenzene)
Fluoranthene
Fluorene
Ilexachlorobenzene
tlexachlorobutadiene
Ilexachlorocyclopentadiene
Ilexachloroethane
lndeno(1,2,3-ed)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-N i lroso-di-methylam ine
N-N ilroso-di-n-propyl amine
N-Nitrosodiphenylamine (Diphenylamine)
Phenanthrene
Pyrene
ND
5.00
ng/1'
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
ND
5.00
uWL
1.00
03/28/14 16:13
EPA 625/8270D
RJM
114C0739
ND
5.00
ug/L
1,00
03/28/14 16:13
EPA 62518270D
RJM
134C0739
ND
5,00
ug/L
1.00
03/28/t4 16:13
EPA 625/8270D
RJM
R4C0739
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
B4C0739
ND
5,00
ugA,
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
ND
5,00
ug/L
1,00
03/28/14 16:13
EPA 625/8270D
RIM
134C0739
NI)
5.00
ugfL
1.00
03/28/14 16:13
EPA 6251827DD
RJM
134C0739
ND
5.00
ug/l.
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
ND
5.00
UWL
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 62518270D
RJM
134CO739
ND
5.00
ug/L
1,00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
ND
5.00
ugfL
1,00
03/28/14 16:13
EPA 625/8270D
RJM
B4C0739
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RUM
B4C0739
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
ND
5.00
uglL
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 62518270D
RJM
134C0739
ND
5.00
ug/L
1.00
03/29/14 16:13
EPA 625/827013
RJM
134C0739
ND
5.00
ugfL
1.00
03/28/14 16:13
EPA 625/8270D
RJM
134C0739
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 625/9270D
RJM
B4C0739
ND
5.00
ug11.
1.00
03/28/14 1& 13
EPA 62518270D
RJM
134C0739
ND
5.00
ug/L
1.00
03/28/14 1613
EPA 62518270D
RJM
134C0739
ND
5.00
ug/L
1.00
03/28/14 16:13
EPA 62518270D
RJM
134C0739
ND
5.00
ugfL
1.00
03/28/14 16:13
EPA 62518270D
RJM
134C0739
ND
5.00
ug/L
1.00
03/28/14 W13
EPA 62518270D
RJM
134C0739
Surrogates
%REC
%REC Limits Flag
Nitrobenzene-D5
78
35-114
2-Fluorohiphent'l
88
43-116
Terphenyl-014
118
33-141
2-Fluurophenul
52
21-110
Phenol-05
33
10-1 10
2,4,04'rihramophenol
85
10-123
PCBs
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville, 5C 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.conl
an employee -owned company
04,0412014 08:09 This report may not he reproduced, except ur fell, without wrinen permis.siat from Rogers & Callrott, Inc. L. Page 9 of 31

Rogers &Callcott
b ENVIRONMENTAL
Environmental Testing Soiulions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville, NC 28801-4310 Reported: 04/04/14 08:09
Sample Number 4030600-03
Sample Description Pentair Outfall 02 - Grab collected on 03/17/14 09:10
Reporting
Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch
PCBs
PCB-1016
ND
0.50
ug1L
I A0
03/26/14 23:46
EPA 608
RKE I
B4C0673
PC13-1221
ND
0.50
ugll.
I
03/26/14 23:46
EPA609
RKH
W0673
PCB-1232
ND
0.50
ug/L
1,00
03/26/14 23:46
EPA608
RKH
B4C0673
PCB-1242
ND
0.50
ug/L
1-00
03/26/14 23:46
EPA608
RKH
B4C0673
PCB-1248
ND
0.50
ng/L
1.00
03/26114 23:46
EPA 609
RICH
B4C0673
PCB-1254
ND
0.50
ug/L
1.00
03/26/14 23:46
EPA 608
RKH
B4C0673
PCB-1260
ND
0,50
ug1L
1.00
03/26/14 23:46
EPA 608
RKH
64C0673
Surrogates
%REC
%REC Limits
Flag
2,a.5,6-7i7ruchluru-m•sylcne
101
60-130
Decuchlorohiphen)l
91
30-150
Sample Number 4030600-04
Sample Description Pentair Outfall #2 - Grab collected on 03/17/14 09:10
Reporting
Parameter Result Limit Units DF An2I)zed Method Flag Analyst Batch
Volatile Organics
Acrolein ND 5.0 U91L 1.00 03/24/14 14:53 EPA 624-82608 LBW WOW
Acrylonitrile ND 5.0 ugfL 1.00 03/24114 14:53 EPA 624-8260B LBW WOW
Surrogates %REC %REC Limits Flag
1,2-1)ichloroefhane•1)4 83 70-130
!'oluene-UR 100 70-130
4-Rrumojluoruhen:ene 107 70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232,6140 rogersandeallcott.eom
an employee owned company
04,041201 d 08: n) ThLr reporl rnuy nor he reproduced, ercepr in ffdl. w•ithani wrilren permisvion from Rogers & C allculf, fne-
Page 10 of 31

Mil
�6Rogers & Callcott
�1'_Iln ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28901-4310 Reported: 04/04/14 08:09
General Chemistry Parameters
Quality Control Summary
Reporting Spike Source % REC RPD
Parameter Result Limit Units Level Result `/.REC Limits RPD Limit Flags
Batch B4C0664 - General Prep - Wet Chem
Blank (B4C0664-BLKI)
Oil and Grease, Total, HEM NU 5.0 mg1L
LCS (B4Co664-BSI)
Oil and Grease, Total, HEM 36.7 5-0 nigiL 40.0 92 78-114
LCS Dup (B4C0664-BSD1)
Oil and Grease, Total. I{EM 37.7 5.0 mgiL 40.0 94 78-I l4 3 35
PO Box 5655 1 Greenville, 5C 29606 1 426 Fairforest Way I Greenville, 5C 29607 1 main 864.232.1556 1 fax 864.232,6140 rogersandcallcott.com
an employee -owned company
04,4a42014 08 t19 This report may not he reprexlaceel. except in fill, a idrow u-niten permission from Raters & C'alleatf, Inc.
Page 11 of 31

Rogers & Callcott
b
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RpD Limit Elaga
Batch B4C0590 - EPA 200.8
Blank (B4C0590-BLKI)
Copper ND 0.001 mglL
Duplicate (NC0590-DUPI) Source. 4030612-01
Copper
0.001
0.001
mg/L
ND
8 20
Matrix Spike(B4C0590-MSl)
Source:4030612-01
Copper
0.196
0.001
mg/L
0.200
ND
97
70.130
Post Spike (B4C0590-PSI)
Source: 4030612-01
Copper
0.243
mg/L
0.250
ND
97
75.125
Batch B4C0600 - EPA 200.7
Blank (B4C0600-BLKI)
Lead
ND
0,020
mg/L
Zinc
ND
0.010
mg/L
LCS (B4C0600-BSI)
Lead
0.99
0.020
mg/L
1.00
99
95-115
Zinc
0.97
0.010
mg/L
1.00
97
85-115
Duplicate (B4C0600-DIfPI)
Source: 4030662-01
Lead
ND
0,050
mglL
ND
20
Zinc
0.02
0.010
mglL
0.02
0.2 20
Duplicate (B4C0600-DUP2)
Source: 4030675-01
Lead
ND
0.050
mg/L
ND 20
Zinc
0.01
0.010
mg/L
0.01 3 20
Matrix Spike (B4C0600-I11S1)
Source: 4030662-01
Lead
1.00
0.050
mg/L
1.00 ND 100 70-130
Zinc
0,99
0,010
mg/L
1,00 0.02 96 70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.eom
an employee -owned company
04-04201 a 08:09 This report muy nol be reproduced. except in fill, wilhow woffen permiseion from Rogers r& Callcou, Inc.
Page 12 of 31

�b Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville, NC 28801-4310 Reported: 04/04/14 08:09
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit knits Level Result %REC Limits RPU Limit Flags
Batch B4C0600 - EPA 200.7
Matrix Spike (B4C0600-I11S2) Source: 4030675-01
Lead 1,01 0.050 mg/L 1.00 ND 101 70-130
Zinc 1.01 0.010 mgA, 1,00 0.01 100 70-130
Post Spike (R4C0600-PSI) Source: 4030662-01
Lead 0.97 mglL 1.00 ND 97 85-115
Zinc 0.98 mg1L 1.00 0,02 95 85-115
Post Spike (B4C0600-PS2) Source: 4030675-01
Lead 0.99
Zinc 0,98
mglL 1.00 ND 98 85-115
mglL 1.00 0.01 97 85-I15
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesc Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.com
an employee -awned company
04-04?2014 08:09 This reparf may nol he reproduced except in, jdl, without wriffen permission franc Rogers & C allcon, Inc.
Pogo 13 of 31

b Rogers & Callcott
{ ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Volatile Organics
Quality Control Summary
Reporting Spike Source %.REC RPD
Parameter Result Limit Units bevel Result % REC Limits RPD Limit Flags
Batch B4C0837 - EPA 624-5030
Blank (B4C0837-RLKI )
Benzene
Bromoform
Carbon tetrachloride
Chlorobenzene
D i bro m u c h to r o me I ha ne
Chloroethane
2-Chloroethylvinyl ether
Chloroform
B rom o d i c h l o rom e t h au e
1,1-Dichlowethane
1,2-Dichloroethane
trans-1,2-Dichloroethene
l,l-Dichloroethene
l ,2-Dichim opropane
Fthylbenzene
Bromomethane (Methyl Bromide)
Chloromethane (Methyl Chloride)
1,1,2,2-Teirachloroethane
Toruchloroethene
Toluene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroohane
Trichloroethene
Vinyl chloride
Dichlorodifluoromethane
Methylene Chloride
Tr i c h 1 o ro f l u o ro m e t h a n e
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
I ,2,4-Trichlorobenzene
cis-1,3-Dichloropmpene
trans-1,3-Dichloropropene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Arrogate. 1,2-Diehl oroerhatre-D4
Surmgule: 4-Bromr flunrohenrene
2.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2, 0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2,0
2.0
2.0
2.0
2.0
2.0
1.0
1.0
ug/L
ug/L
ug/L
ug/l.
ug/L
ugfL
ug/L
ugf],
ugA,
ug/L
ug/L
uglL
ug/L
ug/l.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L.
ug/L
ug/l,
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L,
ug/L
uglL
ug/L
ug/L
ug/L
88 70-130
104 70-131)
PO Box 5655 1 Greenville, SC 29606 1 426 Faitforest Way I Greenville, SC 29607 1 main 864.232.1556 1 Fax [phone] rogersandcallcott.com
an employee -owned company
04.0412014 08:09 This report may uol he reprrkluced. except in jell. without written permierion frorn Rogers & callcuu, Inc.
Page 14 of 31

�
Rogers & Callcott
__art ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville, NC 28801-4310 Reported: 04/04/14 08:09
Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RFD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4C0837 - EPA 624-5030
Rion (R4C0837-RLKI)
Surrogale: Toluene -UN 97 70-130
LCS (MC0837-RSI)
Benzene
20,8
2.0
ug/L
20.0
104
70-130
Bromoform
19,5
2.0
ug/L
20.0
98
71-129
Carbon tetrachloride
19,9
2.0
ug/L
20.0
99
73-127
Chlorobenzene
19,8
2.0
ug/L
20.0
99
70-130
Dibromochloromethane
18.9
2.0
ug/L
20.0
95
70-130
Chloroethane
19.8
2.0
ugl1,
20.0
94
60-140
2-Chloroe1hylvinyl ether
19.8
5.0
ug/L
20.0
94
50-150
Chloroform
19.9
2,0
ug/L
20.0
too
70-130
Bromodichloromelhane
19.6
2.0
UO,
20.0
98
70-130
I,1-Dichloroethane
20.9
2.0
uglh
20.0
105
73-127
1,2-Dichloroethaue
20.2
2.0
uglL.
20.0
101
70-130
trans-1,2-Dichloroethene
20.6
2.0
ug/L
20.0
103
70-130
1,1-Dichloroethene
20.9
2.0
ug/1'
20.0
105
70-130
1,2-Dichloropropane
21,4
2,0
ugfL
20.0
107
70.130
Ethylbenzene
21.8
2.0
ug1L
20.0
109
70-130
Bromomethune (Me(hyl Bromide)
15.6
2.0
ug/L
20.0
78
60-140
Chloromethane (Methyl Chloride)
12.1
2.0
ug/L
20.0
61
60.140
1,1,2,2-Teirachloroetharre
22.2
2.0
ugll-
20.0
111
70-130
Tetrachloroethene
19.6
2.0
ug1L
2&0
98
74-126
Toluene
20.7
2.0
uglL
20.0
103
75-125
I,1,1-Trichloroetharre
19.6
2.0
ug/L
20.0
98
75-125
1,1,2-Trichloroethaue
20,6
2.0
ug/L
20,0
103
71-129
Ttichlomethene
17.5
2.0
uglL
20,0
88
71-130
Vinyl chloride
17.5
2.0
ug/L
20.0
88
W140
Dichlorodifluoromethane
17.0
2.0
ug/L
20.0
85
60-140
Methylene Chloride
20,5
2.0
ug/L
20.0
103
70-130
Ti ichl0r0flu0r0mctbarre
20,8
2,0
ug/L
20.0
104
60-140
l,2-Dichlorobenzene
20,6
2.0
ug/L
20.0
103
70-130
1,3-Diclrlorobenzene
20,4
2.0
ug/L
20.0
102
73-127
IA-Dichlorobenzenc
19,8
2.0
ug/1-
20.0
99
70-130
1,2,4-Trichlorobemcne
21.7
2.0
ug/L
20.0
108
60-140
cis-1,3-Dichloroptopene
193
1.0
ugR,
20.0
96
70-130
trans-1,3-Dichloropropene
20.8
1.0
ugL
20.0
104
70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way
I Greenville,
SC 29607 1 main 864.232.1556
1 fax [phone]
rogersandealleott.eom
an employee -owned company
04,04/2014 UN; 09 This report may nol he reproduced, except in fill, n'Ithoul mitten permission front Rogers & (allcoa, Inc.
Page 15 of 31

, Rogers & Callcott
Al ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville, NC 28801-4310 Reported: 04/04/14 08:09
Volatile Organics
Quality Control Summary
Reporting Spike Source % REC RPD
Parameter Result Limit Units Level Result Y.RFC Limits RPD Limit Flags
Batch B4C0837 - EPA 624-5030
LCS (84C0837-BS I)
Snrnrgure:l.2-1)ichloruelhunr-U4 104 70-130
Surrogate:4-Browylnorobenzvne 105 70-130
Surrogate: Toluene-D8 111 70-130
Nlatrix Spike (R4C0837-NfS1) Source: 4030609-05
Benzene
21.2
2.0
ug/L
20.0
ND
106
37-151
Brornoform
18,2
2.0
ug/L
20.0
ND
91
45-169
Carbon tetrachloride
MO
2.0
ugl1.
20.0
ND
100
70.140
Chlorobenzene
19.9
2.0
u8l1.
20.0
ND
99
37-160
❑ibromochloromethane
19.1
2.0
ug/L
20.0
ND
91
53-149
Chloroethane
19.4
2.0
ug/L
20.0
ND
97
14-200
2-Chloroethy]vinyl ether
17.4
5.0
uglL
20.0
ND
87
3-200
Chloroform
19.7
2.0
ug1L
20.0
ND
98
51-138
Bromodichloromethane
18.7
2.0
ug/L
20.0
ND
93
35-155
1,1-Dichloroethane
20.8
2.0
ugll,
20.0
ND
104
59-155
1,2-Dichloroethane
19.5
2.0
uglL
20.0
ND
92
49-155
trans-1,2-Dichloroethene
20.7
2.0
uglL
20.0
ND
104
54-156
1,1-Dichlowethene
21.7
2.0
ug/l
20.0
ND
108
3.200
1,2-Dichloropropane
20.7
2.0
ug/L
20.0
ND
104
3-200
Ethylbenzene
22.7
2.0
ug(L
20,0
ND
114
37-162
Bromomethane (Methyl Bromide)
16.1
2.0
ug1L
20.0
ND
80
3-200
Chloromethane (Methyl Chlonde)
13.3
2,0
ugfL
20.0
N❑
66
3-200
1,1,2,2-Teiracidoroethane
21.2
2.0
ug/L
20.0
ND
106
46-157
Teirschloroethene
20.5
2,0
ug/L
20,0
N❑
102
64-148
Toluene
21.7
2.0
ug/L
20.0
ND
109
47-150
],I,l-Trichlowethane
19.7
2.0
ug/L
20.0
ND
99
52-162
1,1,2-Trichloroethane
19.6
2.0
ug/L
20.0
ND
98
52-150
Trichloroethene
18.1
2.0
uglL,
20.0
ND
90
71-157
Vinyl chloride
18.1
2.0
ug/L
20.0
ND
90
3-200
Dichtorodifluoromelhane
16.7
2.0
ug/L
20.0
ND
83
60-140
Methylene Chloride
19.6
2.0
ug/L
20,0
ND
98
3-200
Trichlorofluoromethane
21.3
2.0
ug/L
20.0
ND
106
17-181
1,2-Dich]orobenzem
20.4
2.0
ug/L
20.0
ND
102
18-190
1.3-Dichlorobenzene
20.9
2,0
ug/L
20,0
ND
104
59.156
1,4-Dichlorobenzene
20.0
2.0
ug/L
20.0
ND
100
18-190
1,2,4-Triehlorobenzene
21.3
2.0
ug1L
20.0
ND
106
60-140
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232,1556 1 tax 864.232.6140 rogersandcallcott.Com
an employee -owned company
04,04f2014 0R:09 This report pray not be reprexluced, weep( in frdl, wilhoul written permission from Rogers & C ullcolt, Inc.
Page 16 of 31

Rogers &Callcott
ENVIRONMENTAL
Environmenlal Tesling Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4C0837 - EPA 624-5030
lltafrix Spike (134CO837-NISI) Source: 4030609-05
cis-1,3-Dichlatoproperte
trans-1, 3-DichWopropene
18.8 IA u6,L 200 ND 94 3-200
20,2 1.0 OWL 20.0 ND 101 17-183
Surregure. i,1-13irlrlamrrlurrre-W 46 70.130
Surrugule: a-Bromq/luoruhrn_ene 107 70-130
Surrogute: Toluene-D8 115 70.130
Matrix Spike Dup (B4C0837-NISDI) Source: 4030609-05
Benzene
20.0
2.0
ug/L
20.0
ND
100
37-151
6
20
Bromofornt
17.6
2.0
uglL
20,0
ND
88
45-169
4
20
Carbon tetrachloride
19.1
2,0
ug/L
20.0
ND
96
70-140
4
20
Chlorobenzene
18.5
2.0
ug/L
20.0
ND
93
37-160
7
20
Dibromochloromethanc
17.8
2,0
ug/L
20.0
ND
89
53.149
2
20
Chloroethane
19.7
2,0
ugft-
20.0
ND
98
14-200
2
20
2-Chlormhylvirr}'1 ether
19.1
5.0
ugll.
20.0
ND
91
3-200
4
26
ChluT0f0rrtr
18.8
20
ug/L
20.0
ND
94
51-138
4
20
13mmodichlorornethane
ISO
2.0
ugfl.
20.0
ND
90
35-155
4
20
1,1-Dichloroethane
21.0
2.0
u8/L
20.0
ND
105
50-155
0.8
20
1,2-Dichlowethane
19.1
2.0
u911-
20.0
ND
96
49.155
3
20
trans-1,2-Dichlowethene
20,8
2.0
uglL
20.0
ND
104
54-156
0,5
20
LI-DlchlOToethene
20.2
2.0
uoA
20.0
ND
101
3-200
7
20
1,2-Dichloropropane
21.0
2.0
uglL
20,0
ND
105
3.200
1
20
Ethylbenzene
20.9
2.0
ug/I-
20.0
ND
104
37.162
8
20
Brvmomcthanc (Methyl Bromide)
15.5
2.0
ug/1.
MO
ND
77
3.200
4
20
C1110Tonlelhane (Methyl Chloridc)
13.6
2.0
ug/L
20.0
ND
68
3.200
3
20
1.1,2,2-Tetrachloroethwit
20.6
2.0
ug1L
20.0
ND
103
46.157
3
20
Tetrachloroethene
199
2.0
ug/L
20,0
ND
95
M-148
8
20
Toluene
20,1
2.0
ug/L
20.0
ND
101
47.150
8
20
1,1,1-Trichloroethane
t8,5
2.0
ugiL
20.0
ND
93
52.162
6
20
1,1,2-Trichloroethane
19.1
2.0
ug/L
20.0
ND
%
52-150
2
20
Trichloroethene
17.4
2,0
ug/L
20.0
ND
87
71.157
4
20
Vinyl chloride
18.0
2.0
uyL
20.0
ND
90
3-200
0.4
20
Dichlotodifluoromelhane
15.6
2.0
UA
20.0
ND
78
60.140
7
20
Methylent Chloride
18.7
2.0
u91L
20.0
ND
93
3-200
5
20
Trichloroiluoromethane
20.4
2.0
ug/l.
20.0
ND
t02
17-181
4
20
1,2-Dichlorobenzene
18.6
2.0
ug/L
20.0
ND
93
18-190
10
20
1,3-Dichlorobenmric
19.0
2.0
ugtL
20.0
ND
95
59-156
9
20
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville,
SC 29607 1 main 864,232.1556
1 fax [phone]
rogersandcallcott.com
an ernployee•owned
company
04,0412014 08:09 This report nruy not he reproduced. eTcept in full, w1houl %when permisaioar,from Rogers & Callcotf, Inc.
Page 17 of 31

a Rogers & Callcott
1.2rr _ ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville, NC 28801-4310 Reported: 04/04/14 08:09
Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result •/ REC Limits RPD Limit Flags
Batch B4C0837 - EPA 624-5030
Matrix Spike Dup (B4C0837-AISDI) Source: 4030609-05
14-Dichlorohenzene
18.4
2.0
ug/L
20.0
ND
92
18-190 9
20
1,2,4-Trichlorobe zene
19.6
2.0
ug/L
20.0
ND
98
60-140 8
20
cis-1,3-Dichloropropene
18.6
1,0
uglL
20,0
ND
93
3-200 1
20
trans-1,3-Dichloropropenc
10.7
LO
ugll.
20.0
ND
98
17-183 2
20
Surrogate: 1,1-Dch1aroe7hanc-1J4
99
70.130
Srtrrogare:4-Bromofluorohenzene
98
70-130
Surrugare: Talrmne-D8
JU6
70-130
Batch B4C0865 - EPA 624-5030
Blank (B4C0865-BLKI)
Acrolein ND 5.0 uglL
Acrylonitrile ND 5.0 UO,
Surrogate: 1,2-Achloroethane-W
78
70-130
Surrogate: Toluene-1)8
98
70-130
Surrogate: 4-Bromofluarohen_ene
101
70-130
LCS (B4C0865-BSI)
Acrolein
Acrylonitrile
93.6
17.8
5.0
5,0
ug1L
ug1L
100
20.0
94
89
91.8-108
82.4-118
Surrogate:l,2-Dichloroethane-1)4
88
70-130
Surrogate: "Toluene-1)8
110
70-130
Surrogate: 4-BronroJluarohenzene
104
70-130
LCS (B4C0865-BS2)
Acrolein
104
5.0
ug/1.
100
104
91.8-109
Acrylonitrile
19.4
5.0
ug/L
20,0
97
82.4-118
Surrogate: 1,1-Dichlurnerlrare-U4
98
70-130
Surrogare:7'olucne-1)8
114
70.130
Surrogate: 4-BromoJluorohencene
1N1
70-130
;Matrix Spike (B4C0865-NISI)
Source: 4030490-02
Acrolein
98:1 5.0
"PA, 100 ND 98
88.119
Acrylonitrile
18,0 5.0
uglL 20.0 ND 90
71-135
Srrrrogate:l,1-Dichluroerhane-W
92
70-130
Surrugare: Toluene-DS
114
70-130
Surrogate: 4-Bromr fluoruhemeue
102
70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville,
SC 29607 1 main 864.232.ISS6 I fax [phone]
rogersandealleott.com
an employee -owned company
04,0412014 08:09
This report may prat he reprarluced, except
in ft11, without whiten permission frarn Rogers & Callcoll, Inc.
Page 18 of 31

1b Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4C0865 - EPA 624-5030
Matrix Spike [Sup (B4C0865-IN1SD1) Source: 4030490-02
Acrolein 107 5,0 ug/L 100 ND 107 88-118 9 20
Acrylonitiilc 18.8 5.0 ug/L 20.0 ND 94 71-135 4 20
Surrogate: 1, 2-Dichloroerhane-IN
SurrohWe: Toluene-b8
Surrogate: a-BrnmoJhrorohenzene
93 70-130
106 70-130
97 70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864,232,1556 1 fax [phone] rogersandealleott.com
a i employee -owned company
04,0412014 08:119 This report may not he reproduced, eccepi in dl, without written permi.%xion Pram Rogers & Callcolt, Inc.
Page 19 of 31

Rogers & Callcott
d ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville, NC 28801-4310 Reported: 04/04/14 08:09
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source % R£C RP I)
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B4CO739 - EPA 625
Blank (B4CO739-BLKI )
2-Chlorophenol
ND
5.00
ug/L
2,4-Dichlowphenol
ND
5.00
ug/L
2,4-Dimethylphenol
ND
5.00
ug/L
2-Me1hyl-4,6-dinitrophenol
ND
5.00
ug/L
2,4-Dinitrophenol
ND
5.00
uglL
2-Nitrophenol
ND
5.00
ug/L
4-Nitrophcnol
ND
5,00
ug/L
p-Chloro-m-cresol
ND
5.00
ug/l,
Pentachlorophenol
ND
5.00
ug)L
Phenol
ND
5.00
ug/L
2,4,6-Triclilorophenol
ND
5.00
ug/L
Acenaphthene
ND
5.00
ug/L
Accnaphthylenc
ND
5.00
ug/L
Anthracene
ND
5.00
ugil.
Benzidine
ND
80.0
ug/L
Benzo(a)anthracene
ND
5.00
ug/L
Benzo(a)pymne
ND
5.00
ug/l,
Benzo(b)tluoranthene
ND
5.00
ug/L
Benzo(g,h,i)per)4ene
ND
5.00
ug/L
Betizo(k)fluoran the ne
ND
5.00
ug/L
Bis(2-chloroethoxy)Methane
ND
5.00
uglL
Bis(2-chloroeth),1)E1her
ND
5.00
ug/L
bis(2-Chlowisopropyl)cther
ND
5.00
ug/L
Bis(2-ethylhexy1)Phtha1ate
ND
5.00
ug/L
4-Bromopheny1phenylether
ND
5.00
ug/L
But lbenzylphthalate
ND
5.00
ug/L
2-Cliloronaphihalene
ND
5.00
ug/L
4-Chlorophenylphenylether
ND
5.00
uglL
Chrysenc
ND
5.00
ug/L
Dibenzo(a,h)anthracene
ND
5.00
ug/L
3,Y-Dichlorobenzidine
ND
5.00
ug/L
Diethylphthalate
ND
5.00
ug/l.
Dimelhylphihalate
ND
5.00
ugfL
Di-n-butylphthalate
ND
5.00
ug/L
2,4-Dininutoluenc
ND
5.00
ug/L
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 I main 864.232.1556 1 fax [phone] rogersafldcallcott.eom
an employee -owned company
w,0412014 08: d9 This repnrr rnuv nur he reprrxluced, ercepi in rrdl, wilhous wrNren permission {roar Rogers h (ullcvlt, Inc.
Page 20 of 31

a Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St, Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Sourte % RF;C RPD
Parameter Result Limit Units level Result '/.REC Limits RPb Limit Slags
Batch B4C0739 - EPA 625
Blank (B4C0739-BLKI)
2,6-Dinitrotoluene
ND
5.00
uglL
Di-n-octylphthalate
ND
5.00
ugll.
1,2-Diphenylhydrazene(Azohenzene)
ND
5.00
ug/L
Fluoranthene
ND
5,00
ug/L
Fluorene
ND
5.00
ug/t.
Hexachlorobenzene
ND
5.00
uglL
liexachlorobutadiene
ND
5.00
ug/L
Ilexachlorocyclopentadiene
ND
5.00
ug/L
Hexachloroetham
ND
5.00
ug/L
1ndeno(1,2,3-cd)pyrene
ND
5.00
ug/L
Isophorone
ND
5.00
ug/L
Naphthalene
ND
5.00
ugll,
Nitrobenzene
ND
5.00
ug/L
N-Nitroso-di-methylamine
ND
5,00
ugA.
N-Nitroso-di-n-propylamine
ND
5.00
ug4,
N-Nitrosodiphenytamine (Diphenylamine)
ND
5,00
ug/L
Phenanthrcne
ND
5,00
00,
Pyrene
ND
5.00
ugil,
Surrogute: Nilrahen;ene-h5
77
33-114
Surrogate: 2-1-harrohiphenvl
91
43-116
Surrogate: Terphenvl-D14
74
33-141
Surrogate:2-Fluorophenol
50
21-110
Surrogate: Phenol-D5
33
10-110
Surrogate: 2, 4, 64 rihromophenol
78
10-123
LCS (B4C0739-BSI)
2-Chiorophenol
73.9
5.00
ug/L
]00
74
23-134
2,4-Dichlorophenol
90.6
5.00
ug/L
100
91
39-135
2,4-Dimethylphenol
77.4
5.00
ug/L
100
77
32-119
2-Methy]-4 6-dinitrophenol
87.1
5.00
ug/L
100
87
1-181
2,4-Dinitrophenol
85.9
5.00
ug/L
100
86
1-191
2-Nitrophenol
91.9
5.00
ug11,
100
92
29-182
4-Nitrophenol
36.8
5.00
ug1l,
100
37
1-132
p-Chloro-m-cresol
88.1
5.00
ug/L
100
88
22-147
Pentachlorophe1101
76.8
5.00
ug/L
100
77
14.176
Phenol
33.9
5.00
U91L
100
34
5-112
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232,6140 rogel'SandcallCOtt.CORI
an employee -owned company
04-0412014 o w This report may not he reprekluc'ed. exeepl in rrdl. w•iihora w'raten permasion from Ragers h Callcotl, Inc.
Page 21 of 31

a Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St, Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source % REC RPD
Parameter Result Limit Units bevel Result % RF,C Limits RPD Limit Flags
Batch B4C0739 - EPA 625
LCS (64C0739-11SI)
2,4 6-Trichlorophenol
91.6
5.00
ug/L
100
92
37-144
Acenaphthene
90.3
5.00
ugfL
100
90
47-145
Acenaphthylene
91.2
5.00
ug/L
100
91
33-145
Anthracene
93.$
5,00
ugfL
100
93
27-133
Benzidine
214
80.0
ugfL
500
43
1-139
Benzo(a)aalhracene
95.4
5.00
ugfl.
100
95
33-143
Benzo(a)pyrene
94.2
5.00
ugft.
100
94
17-163
Benzo(b)Iluoranthene
97.3
5,00
ug1L
IN
97
24-159
Benzo(g,h,i)perylene
97.5
5.00
ugi[.
100
97
1-200
Benzo(k)f]umanthene
99.5
5.00
ug/L
IN
t00
11-162
Bis(2-chloroethoxy)Methane
86,5
5.00
ug/1-
100
86
33-184
Bis(2-ch1oroe1hyl)Ether
79.9
5,00
aglL
I00
80
12-159
bis(2-Chloroisopropyl)ether
81.7
5.00
ugfL
l00
82
36-166
Bis(2-ethylhexyl)Phthalate
t04
5,00
ugli,
100
104
8-158
4-Bromophenylphenyl ether
93.2
5,00
ug 1,
100
93
53-127
ButVIk11zylph1haJa1e
114
5,00
ug/L
100
114
1-152
2-Chloranaph1halene
92A
5.00
uglL
100
92
60-118
4-Chlorophenylphenylether
92,4
5.00
ug/L
100
92
25.158
Chrysene
96.5
5.00
ug/1,
l00
96
17-168
Dibenzo(a,h)anihracene
103
5.00
ugA-
100
103
1-200
3,Y-Dichlorobenzidine
65.3
5.00
ug/L
100
65
1-200
Diethylphthalate
95.9
5.00
ug/L
100
96
1414
Dimethylphthalate
96.9
5,00
ug/L
IN
97
1-112
Di-n-butylphthalate
103
5.00
ug/L
100
103
1-118
2,4-Dinivotoluene
102
5.00
ugll.
100
102
39-139
2,6-Dinitrotoluene
99.7
5,00
ug/L
100
100
50-158
Di-n-ocrylphthalate
105
5.00
ug/L
100
105
4-146
1,2-Dipheny1hydrazene(Azobenzene)
90.3
5.00
u0.
100
90
65-130
Fluoranthcnc
98.6
5.00
ug/I.
100
99
26-137
Fluorene
90.5
5,00
ugg.
100
90
59-121
Hexachlarobenzene
97.6
5.00
ug)L
100
98
1-152
Hexachlorobutadiene
79.8
5.00
ug/L
100
80
24-I16
Hcxachloracyclopentadiene
86,5
5,00
ugll,
100
86
37-130
Hexachloroethane
73.2
5.00
ugA,
100
73
40-113
lndeno(1,2,3-cd)pyrene
101
5.00
ug/i,
100
101
1-171
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way # Greenville, SC 29607 1 main 864.232,1556 1 fax [phone] rogersandeallcott.eom
an employee -owned company
04a141201a o8:09 This report may nut he reproduced. evicepr in fill!, wilhout wrirlen permission from Rogers h Callcolt, Inc.
Page 22 of 31

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B4C0739 - EPA 625
LCS (B4C0739-BSI )
Isophorone
92.6
5.00
ug/L
100
93
21-196
Naphthalene
W7
5.00
ug/L
too
81
21-133
Nitrobenzene
90.6
5.00
uglL
100
91
35-180
N-Nitroso-di-melhylamine
49.0
5,00
ug1L
IN
48
30-100
N-Nitroso-di-n-propylamine
93.0
5,00
ug[L
100
93
1-200
N-Nitrosodiphenylamine(Diphenylamine)
94.9
5.00
ug1L
100
95
60-130
Phenanthrene
91.7
5.00
u9JL
IN
92
54-120
Pyrene
99.1
5.00
UFA,
100
99
52-115
1'urrogule: Nitrobenzene-D5
86
35-114
Surmgufe:2-Flonrohiphemd
98
43-116
tinrrogute., Terphen14-D14
66
33-141
Surrogate: 2-Fluorophenol
49
21-111)
Surrogate: 1'lienal-D5
32
10-11 f)
Surrogate: 2, 4, 6-7 rihrumophenol
101
10-123
Matrix Spike (B4C0739-NISI)
Source: 4030788-01
2-Chlorophenol
75.7
5M
ugA,
IN
ND
76
23-134
2,4-Dichlorophenol
92.6
5.00
ug/L
100
ND
93
39-135
2,4-Dime1hylphenol
77.7
5,00
ug/L
too
ND
78
32-119
2-Me1hyl-4,6-dinitrophenol
92.0
5.00
ug/L
100
ND
92
1-191
2,4-Dinitrophenol
99.3
5.00
ugl1.
100
ND
99
1-191
2-Nilrophenol
95.3
5.00
ug1L
100
ND
95
29-182
4-Nitrophenol
38,0
5.00
ug/L
100
ND
38
1-132
p-Chloro-m-cresol
90,2
5.00
ug/L
100
ND
90
22-147
Penlachlorophenol
83,5
5.00
ug/L
100
ND
83
14-176
Phenol
33.3
5.00
u9n,
100
ND
33
5-112
2,4,6-Trichlorophenol
99.5
5.00
ugA,
100
ND
100
37.144
Acenaphthene
90.1
5.00
ug/l.
too
ND
90
47-145
Acenaphlhylenc
91,8
5.00
ug/L
100
ND
92
33-145
Anthracene
93.5
5.00
ug/L
100
ND
93
27-133
Benzidine
ND
80.0
ug/L
500
ND
1-139
Q6,S1
Benzo(a)anthracene
101
5,00
ugll,
100
ND
101
33-143
13enz0(3)pyre11e
97.5
5.00
ug1L
100
ND
98
17-163
Sertzo(h)fluoraothene
101
5.00
ug/L
100
ND
101
24-159
Benzo(g,h,i)perylene
102
5.00
ug/L
100
ND
102
1-200
Benzo(k)fluoranthene
106
5.00
ug/L
too
ND
106
11-162
PO Sox 5655 [ Greenville, SC 29606 1 426 Fairforest Way
I Greenville,
SC 29607
1 main 864.232.1556 1
fax 864.232,6140
rogersandcalleott.eom
an employee -owned company
0440412014 08:09 This relxut nuq not be reproduced, except in frd1, withmu x'ritien permi.vtoor from Rogers & Cullcott, Inc.
Page 23 of 31

Rogers & Callcott
6
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville- NC 28801-4310 Reported: 04/04M 08:09
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source % REC RPD
Parameter Result Limit [Units Level Result %REC limits RPD Limit Flags
Batch B4CO739 - EPA 625
Matrix Spike (B4C0739-MSI)
Source: 4030788-01
Bis(2-chloroerhuxy)Methane
99.4
5.00
u91L
100
ND
89
33-184
Bis(2-ch1oroe1hyl)E1her
83.9
5.00
u9fL
100
Nt3
84
12-158
bis(2-Chloroisopropyl)ether
82.2
5.00
ug/I.
too
ND
82
36-166
13is(2-cIhylhexyl)PhtIialaIc
104
5.00
ug/L
100
ND
109
8-158
4-Bromophenylphenyl ether
91.3
5,00
uglL
too
ND
91
53-127
Butylbeuzylphthalate
118
5.00
ug/L
1o0
ND
I18
1-152
2-Chloronaphthalene
94.5
5.00
ug/L
too
ND
95
60.118
4-Chlorophenylphenyl ether
94.9
5.00
ug/L
100
ND
95
25-158
Chrysene
101
5,00
ug/L
Ioo
ND
101
17.169
Dibenzo(a,h)anthracene
108
5,00
ug/L
100
ND
108
1-200
3,3'-Dichlorobenzidine
78.1
5.00
ug/L
100
ND
78
1-200
Diethylphthalate
49.9
5.00
ugn,
too
N)
loo
1414
Dintethylphihalaie
06
5.00
ug1L
100
ND
100
1-112
Di-u-butylphthalate
108
5.00
ug/L
100
ND
108
1-119
2,4-Dinitrotoluene
107
5.00
ug/L
too
ND
107
39-139
2,6-Dinitrotoluene
104
5.00
uglL
too
ND
104
50-158
Di-n-octytphthalate
111
5.00
ug/L
Hl0
ND
111
4-146
1,2-Dipheny1hydrazene(Azobenzene)
88.4
5.00
ug/L
too
ND
88
65-130
Fluoranthene
104
5.00
ug/L
100
ND
104
26-137
Fluorene
91.6
5.00
ug/L
100
ND
92
59-121
Hexachlorobenzeue
93.4
5,00
ug/L
100
ND
93
1.152
Hexachlowbutadiene
79.8
5.00
ug/L
Mo
ND
80
24-116
Hexachlorocyclopentadiene
91.3
5.00
uglL
100
ND
91
37-130
Hexachloroethane
78.0
5.00
ug1L
too
ND
78
40-113
1 ndeno( 1,2,3-cd)pyrene
123
5.00
ug/L
too
ND
123
1-171
Isophorone
95.9
5.00
ug/L
100
ND
96
21-196
Naphthalene
82.8
5.00
ug/L
too
ND
83
21-133
Nitrobenzene
96.0
5.00
ug/L
100
ND
96
35480
N-Nitw50-di-mohylaniine
50.3
5,00
ug/L
100
ND
49
30-100
N-Nitroso-di-n-propylamine
97.2
5.00
uglL
100
ND
97
1-200
N-Nitrosodiphenylamine (Diphenylamine)
91.2
5.00
ugR,
too
ND
91
60-130
pheuantireue
92.8
5,00
ug/L
100
ND
93
54.120
Pyrene
105
5.00
ug/L
100
ND
105
52.115
Srtrrugare: Nl1r(hcn_ene-1)5 88 35-11.1
Surrugule.2-11vorohrpheorvl 97 43-116
Surrugwe: "1'erphenyl-1)1d 61 33-141
PO Box 5655 I Greenville, 5C 29606 1 426 Fait -forest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandealleott.eom
an employee -owned company
04,0412014 08; 09 This re port may oral he reprexlreced, eacepr rn, fidl, x•ilhoxr wrruen permismon from Rogers & Callcon, Inc.
Page 24 of 31

6 ' L Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28901-4310 Reported: 04/04/14 08:09
Semi-VolatileS Organics
Quality Control Summary
Reporting Spike Source %REC RPD
arameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4C0739 - EPA 625
Matrix Spike {84C0739-NISI) Source: 4030788-01
3urrogufe: 1-Flaorophenul
47
11-110
Surrogate: Phenol-D5
31
10-110
Surrogate: 2,4.6-Trihromoplrenol
96
10-123
Matrix Spike Dup (134120739-N1SD1) Source: 4030788-01
2-Chlorophenol
76,2
5.00
ug/L
too
ND
76
23-134
0.7
30
2,4-Diddorophenol
91,6
5,00
ug/L
100
ND
92
39-135
1
30
2,4-Dimethylphenol
85.1
5.00
ugA,
too
ND
85
32.119
9
30
2-Mohy14,6-diuitrophenol
89.8
5.00
ug/L
i00
ND
90
1-191
2
30
2,4-Dininophenol
98.6
5.00
ugA,
too
ND
99
I-191
0.7
30
2-Nitrophenol
96.2
$.00
ug/L
100
ND
96
29-182
1
30
4-Nitrophenol
38.0
5.00
ugA-
too
ND
38
1-132
0,05
30
p-Chloro-m-cresol
89.5
5.00
ug/L
too
ND
90
22-147
0.8
30
Pentachlorophenol
83.2
5.00
ug/L
100
ND
83
14-176
0.4
30
Phenol
36.4
5.00
ug/L
100
ND
36
5-112
9
30
2,4,6-Trichlorophenol
100
5.00
ugA,
100
ND
100
37-144
0.5
30
Acenaphihene
89.5
5.00
ug/L
too
ND
89
47-145
0.6
30
Acenaphthylene
89.9
5.00
ugA.
100
ND
90
33-145
2
30
Anihmeene
93.1
5.00
ug/L
too
ND
93
27-133
0.4
30
Benzidine
ND
80.0
ug/L
500
ND
1$
1-139
5o
Benzo(a)anthraceue
100
5.00
ug/L
100
ND
100
33-143
0.3
30
Beuzo(a)pyrene
97.0
5.00
UO,
too
ND
97
17463
0.5
30
Benzo(b)fluoranihene
99.6
5,00
u84,
100
ND
100
24-159
1
30
Benzo(g,h,i)perylene
103
5.00
U&I
too
ND
103
1-200
1
30
Beuzo(k)fluoranihene
104
5.00
ug11,
IN
ND
104
II-162
1
30
Bis(2-chloroethoxy)Methane
93,7
5.00
ugA,
100
ND
94
33-184
5
30
Bis(2-chloroethyl0her
88,7
5,00
ug/L
100
ND
89
12-158
6
30
bis(2-Ch1oroisopropy1)e1her
85.9
5.00
ugA.
100
ND
86
36-166
4
30
Bis(2-cthy1hexy1)Ph1hata1e
109
5.00
ug/L
too
ND
109
8-158
0.09
30
4-Bromopheny1pheny1 o6cr
90,2
5.00
ug/L
100
ND
90
53-127
1
30
Bug9benzylphthalate
118
5.00
ugA.
100
ND
118
I-152
0,2
30
2-Chlomnaphihalene
93.5
5.00
ug/L
too
ND
94
60-118
1
30
4-Chlorophenylphenyle1her
93.6
5.00
ug/L
100
ND
94
25-158
l
30
Cbryscne
99.6
5.00
ug/L
100
ND
100
17-168
l
30
Dibenzo(a,h)anthracene
109
5.00
ugA,
100
ND
Io9
1.200
0.6
30
3,3'-Dichloroberrzidine
83.5
5.0o
ugA,
too
ND
84
1-200
7
40
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232,1556 1 fax [phone] rogersandeallcott.eom
an employee -owned company
0-s,041211 a 08: i19 This reporf may not he reproduced, except in 01, %whow xrinen permi.vaimr Jrom Rogers h Callcolt, Inc.
Page 25 of 31

b Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08;09
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source % REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4CO739 - EPA 625
Matrix Spike Dup (B4C0739-NISD1) Source: 4030788-01
Diethylphthalate
98A
5.00
ugfL
100
ND
98
1-114
2
30
Dimethylphihalate
98,9
5.00
ugfL
100
ND
99
1-112
0,7
30
Di-n-butylphthalate
106
5.00
ug/L.
100
ND
106
1-118
2
30
2,4-Dinitrololuene
106
5.00
ugfL
100
ND
106
39-139
1
30
2,6-Dinitrotolueue
104
5.00
ug/L,
100
ND
104
50-159
0A
30
Di-n-octylphihalaie
109
5,00
1191L
]00
ND
109
4-146
2
30
1,2-Diphenylhydrazene(Azobcnzene) 88.7
5.00
ug/L
100
ND
89
65-130
0.3
30
Fluoranthene
104
5.00
ug/L
100
ND
104
26-137
0.6
30
Fluorene
90.9
5.00
ug/l.
100
ND
91
59-121
0.8
30
Hexachlorobenzene
93.3
5.00
ug/L
100
ND
93
1-152
0.03
30
11cxachi0robutadiene
79.7
5.00
ug1L.
100
ND
80
24-116
0.09
45
Hexachlorocyclopentadiene
90.3
5.00
ugfL
IN
ND
90
37-130
1
45
Hexachlowelhane
80.1
5.00
ug/L
100
ND
80
40-113
3
45
Indeno(1,2,3-cd)pyrene
123
5.00
ugfL
IN
ND
123
1-171
0
30
Isophorone
98.5
5.00
ugli.
100
NO
98
21-196
3
30
Naphthalene
94.2
5.00
ugfL
100
ND
84
21-133
2
45
Nitrobenzene
IN
5.00
ug/L
100
ND
100
35-180
4
30
N-Nitmso-di-methylamine
53.1
5.00
ugll.
100
ND
52
30-100
5
30
N-Nilroso-di-n-propylamine
99.8
5.00
ug/L
100
ND
100
1-200
3
30
N-Nitrosodiphenylamine (Diphenylamine)
92.1
5.00
ugfL
100
ND
92
60-130
0.9
30
Phenanthrene
93,4
5.00
ug/L
100
ND
93
54-120
0,6
30
Pyrene
104
5,00
ug1L
l00
ND
104
52-115
l
30
S'nrrugute: Nitrahelr-ene-D5
9U
35-114
S'nrrogule: 2-1-hrurohiphenyl
97
43-116
Nnrruguie:7erphen-W-1)!4
52
33-141
S'urrogale: 2.1-7rmrophenol
51
21-110
Nnrrogule: Phen,914)5
34
10-110
Nurrogale: 2, a, &Tribrornophenn!
95
10-123
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.com
an employee -owned company
04,0412014 08:09 This report nruv nal he reproduced. except in fall. Rogers h C allcort, Inc,
Page 26 of 31

7
Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
PC BS
Quality Control Summary
Reporting Spike Source %REC RFD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
f
Batch B4C0673 - EPA 608
Blank (B4C0673-BLKI )
PCB-1016
ND
0.50
ug/L
PCB-1221
ND
0.50
ug/L
PCB-1232
ND
0.50
ug/L
PCB-1242
ND
0.50
ug/L
PCB-1248
ND
0.50
ug/L
PCB-1254
ND
0.50
ug/L
PCB-1260
ND
0.50
ug/L
Surrogate:2,4,5,h-7etrachloro-no-,Tylene
96
60.130
Surrogate: Decachlorohipheml
77
30-150
LCS (B4C0673-BSI)
PCB-1016
2.59
0.50
ug/L
2.50
104
50-114
PCB-1260
2.56
0.50
ug/L
2.50
102
8-127
Surrogate:2,a,5,6-Telrachloro-nr-xylene
94
60-130
Surrogate: DecachloreAphem-1
87
30-150
LCS Dup (B4C0673-BSD1)
PCB-1016
2.62
0.50
ug/L
2.50
105
50-114 l 20
PCB-1260
157
0.50
ug/L
2.50
103
8-127 0.6 20
Surrogate: 2,4,5,6-Teirachloro-nr-Tylene
96
h0-130
Surrogate: Deeachlorohiphen-vi
77
30-150
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 I main 864.232.1556 1 fax [phone] rogersandealleott.eom
an employee -owned company
040412014 08: 09 This reporl uray not he reproduced, e,veept in full, wilhoul wrulen permixvion from Rogers & Callcorl, Inc.
Page 27 of 31

r
a- Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Sample Preparation Data
Parameter
Batch
Sample 11)
Prepared
Analyst
EPA 200.7 Metal Digestion
EPA 200.7
B4C0600
4030600-01
03/19/2014 16:16
MEC
EPA 200.7
B4C0600
4030600-03
03/19/2014 16:16
MEC
EPA 200.8 Metal Digestion
EPA 200.8
B4C0590
4030600-01
03/18/2014 16:58
DER
EPA 200.8
B4C0590
4030600-03
03/18/2014 16:58
DER
EPA 608 Extraction
EPA 608
134CO673
4030600-01
03/21/2014 09:30
DBB
EPA 608
B4C0673
4030600-03
03/21/2014 09:30
DBB
EPA 625 Extraction
EPA 625
B4C0739
4030600-01
03/24/2014 10:00
DBB
EPA 625
B4C0739
4030600-03
03/24/2014 10:00
DBB
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandealleott.eom
an employee -owned company
04,0412014 08:09 This reporl mov not be reproilnced, ercepi in,jdl, x'ilholrr stiffen permission from Rogers & Collcou, Inc..
Page 28 of 31

r
Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. _ Work Order: 4030600
Asheville. NC 28801-4310 Reported: 04/04/14 08:09
Data Qualifiers and Definitions
ND Analyze NOT DETECTED at or above the reporting limit
NR Not reported
RPD Relative Percent Difference
Q6 Benzidine is an unstable compound which is subject to oxidative loss and variable recovery during solvent concentration.
S l The matrix spike and I or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. The
Laboratory Control Sample (LCS) was within control limits.
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.eom
an employee -owned company
04,0412014 rix: U9 Thi.v reporl way uol he repr(hluced, excepl in fill, uwhoml Cullcoll, Inc.
Page 29 0# 31

ROGERS & C,r
. LABORATORY SERANCFS
P.O. Sm 585b, GnmftvM% SC 29"
Ph" MK 232.16W Fax M84) =4140
e
Shlpp N Addren: 426 Fskformt Way
QV6144. SC 29W
Client Name
Address
Report To:
Telephone No.
FAX No.
i 1'0 No.
Project No.
Rogers be
Yr.,,.,.
Cailcott
Time
Sample Descriytkxl
Lob No.
Dote
t-�_A D
SAMPLER
Relinquued by�Slq.}
Relinquished by (Sig.)
© FLi _u4
Relinquished by (Sly.)
Seal / ot'chd
crate/Time Received by (Sig.)
Shipper ,
Dote/Time R ved y )
Dote/Time ®e� Oy t
ipper Name
Recvd. Intact b Seal III
� M Wo
GiAIN OF CUSTODY RECORD PACE 1 OF �
a
9 lg 11,91,
Date/Tine
Date/Time
t'Chd byC) Recvd• Intact
Filtered (Yes
Cooled as a)
Container Type
Container VolumgQv_uy>
Sample Type ob omposile)
Sample Source (WW, GW, DW, tier
Sample Source chlorin (Yes/do)
Lab Receipt " Che
Lob Receipt pH Check
Preserved (Code)
A• -furls D-NOCH C-Boric Acid
H--HN0, E-HU H-Awarwc AM
C-N=Sa, F-Ne,S,O, 1-
COMMEM
4_
r tftA I �0 ff �40
Temperature of blank or representative sample
At time of eolleetia
At time of lob receipt V .0 ■
d
Form Revised July 2008
1

r
Rogers & Callcott
ENVIRONMENTAL
Sample Receipt Verification
Date � � � � Work
Client: Received: Order:— Z-6 —
Carrier Name: Client /-1FedExZ UPS US Mail %couriel Field Services Other:
Tracking umber:
Receipt Criteria
Y
e
s
o
A
Comments
Shipping container # cooler intact?
Yj
Damaged Leaking Other:
Custody seals intact?
COC included with samples?
COC signed when relinquished and received?
Sample bottles intact?
Damaged Leaking Other:
Sample ID on COC agree with label on bottle(s)?
Date 1 time on COC agree with label on bottle(s)?
Number of bottles on COC agrees with number of bottles received?
Samples received within holding time?
Sample volume sufficient for analysis?
VOA vials free of headspace (Timm bubble)?
Samples cooled? Temp at receipt recorded on COC
Temp measured with LR thermometer - $N: 97450067
Ice Cold Packs Dry Ice None
Samples requiring pH preservation at proper pH?
Note: Samples for metals analysis may be preserved upon receipt in the lab.
If in-house preservation used -- record Lot #
HCL
H,PO,
H,SO,
NaOH
HNO3
Other
Comments:
Were non-conformance issues noted at sample receipt? Yes or No
Non -Conformance issue other than noted above:
Revised January 2014
IN
Y
Completed b :
p
Page 31 of 31

r
4
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _April 2, 2014
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Environmental Testing Solutions Lab Cert. #600mg/L
Comments on sample collection or analysis: See page 4
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2014
SAMPLE PERIOD ® Jan -June ❑ July -Dec
or DKMonthlyl February lmonth)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow []water Supply ❑SA
®Other: Class C, Swannanoa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -->
❑ No discharge this period:
Outfall No.
•Date Sample
Collected;
(mo/dd/yr)
24-hour rainfall
amount,
lnches3
Total Suspended Solids
pH,
standard units
Copper
Lead
Zinc
Non -Paler O&G/
Total Petroleum
Hydrocarbons
Total Toxic
OrganicsS
Benchmarks
-
100 mg/L or 50 mgJL
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
0Z-19-2014
0.21
28 mg/L
7.2
0.01 mgJL
<0.020 y
.12 mgJL
<5.0 mg/L
BRL
2
02-19-2014
0.21
<5.0 mg/L
7.2
<.005 mg/L
<0.020
0.12 mg/L
<5.0 mg/L
BRL
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31),
APR -42014
Permit Date: 11/1/2012-10/31/2017 t.",r, ," !atlty SeClJOA swu z4s, last revised 10/25/2012
Page 1 of 4

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART li SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART It SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME:
Mall an original and one copy of this DMR�ncluding all "No Discharge" reports, within 317 day of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
�ttn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
L
(pate)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 4

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Sal Vaccaro
Name (Print name)
General Manager
Title (Print title) /
�/� I
(Signature (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Mote. If you report a sample value in excess of the benchmark, you must implement Fier I, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
No discharge this period?'
Outfall No.
Date Sample
collected"
(mo/dd/yr)
24-hour rainfall
amount,
lnches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
PH
Benchmarks ===y
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012-
Page 2 of 4 '

1) Zinc reporting value exceeds permit limit 0.067 for outfall 41 and 92
a) Finding;
i) Roofing material is galvanized metal could be a contributing factor for outfall #1 and 92.
ii) Scrap Lugger pad could be a contributing factor for outfall 41.
b) Corrective actions;
i) Review BMP
ii) Increase housekeeping. Lugger Pad Area and Center Pad to be inspected weekly.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 4 of 4

•
0 .R
o F
6 Environmental Testing Solutions, Inc.
Project name: Pentair
Collection date: _
Date received:
Sample identification
19-Feb-14
19-Feb-14
Outfall #1
Certificate of Analysis
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number:
140219.510
Sample number: 113789
Parameter
Method
Result RL
Units
Date
Analyst Footnotes
Analyzed
624
624 - 8260 B
See Attached Sheet
µg/L
26-Feb-14
LBW 1
625
625 - 8270 D
See Attached Sheet
}tg/L
5-Mar-14
RJM 1
608
608
See Attached Sheet
µg/L
27-Fetr14
RKH 1
Solids, Total Suspended
SM 9222-D
28 5.0
mg/L-
20-Fela14
KW
Oil & Grease, Total HEM
1664 A
<5.0 5.0
mg/L
24-Feb-14
CTS i
Copper
200.7
0.01 0.005
mg/L
25-Feb-14
MEC I
Zinc
200.7
0.12 0.010
mg/L
25-Feb-14
MEC I
Lead
200.7
<0.020 0,020
mg/L
25-Feb-14
MEC l
Sample identification: Outfall #2
Sample number; 113790
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
624
624 - 8260 B
See Attached Sheet
ug/L
26-Fet>-14
LBW 1
625
625 - $270 D
See Attached Sheet
gg/L
6-Mar-14
RJM 1
609
608
See Attached Sheet
µg/L
27-Feb-14
RKH I
Solids, Total Suspended
SM 9222-D
<5.0 5.0
mg/L
20-Feb-14
KW
Oil & Grease
1664 A
_<5.0 5.0
mg/L
24-Feb-14
CTS
Copper
200.7
<0.005 0.005
mg/L
25-Fc1r14
MEC
Zinc
200.7
0.012 0.010
mg1L
25-Feb-14
MEC I
Lead
200.7
<0.020 0.020
mg/L
25-Fetr14
MEC 1
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
Date reviewed: 05-011 14 NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
Signature; NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

Rogers & Callcott
ENVIRONMENTAL
Client Environmental Testing Solutions
Kelley E, Keenan
351 Depot St.
Asheville, NC 28801-4310
Dear Clicnl:
Laboratory Report
Project:
Work Order:
Received:
Laboratory Services
Pentair Valves
4020675
02/21/2014 10:30
Rogers and Callcott appreciates the opportunity to be of service to you.- The attached laboratory services report includes analytical results and chain of
custody for samples that were received on February 21, 2014, Rogers and Callcott maintains a formal QAIQC program. Unless otherwise noted, all
analyses performed under NELAP certification have complied with all the requirements for the NELAC standard. The analyses met the QAIQC
confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request.
Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else, I fyou receive this message by
mistake, please notify Rogers and Cailcott immediately.
We strive to provide excellent service to our clients. Please contact Amy Ashley, your Project Manager, at [e-mail] rogersandeallcott.com or
(864)-335-4962 if you have any questions about this report.
Report Approved By:
Amy Ashley
Project Manager
This mporr may not he teprodhmcd, awepr in frdl, H iilmut wrrnen pcnnmvinx from Ro eerr R- C allenu, Inc,
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 tax B64.232.6140 rogersandeallcott.eom
an employee -owned company
Page 1 at 30

Rogers & Callcott
ENVIRONMENTAL
Certificate Anal
South Carolina LaboratorvIdentificarion23105
of Y S1S
South Carolina Mobile Lab Identification 40572
North Carolina Laboratory Certification Number 27
NELQP Laboratory Identrfrcation E87822
Client
Environmental Testing Solutions
Project: Pentair Valves
Kelley E. Keenan
Rork Order: 4020675
351 Depot St.
Received: 02121/2014 10:30
Asheville, NC 29901-4310
Sample Number
Sample Description
matrix Sampled
Type
4020675-01
Pentair Valves Outfall 91
Stormwaler 02/19/14 09:30
Grab
4020675-02
Pentair Valves Outfall 91
Stormwater 02/19/14 09:30
Grab
4020675-03
Pentair Valves Owfall #2
Stormwater 02/19/14 09:30
Grab
4020675-04
Pentair Valves Gutfall #2
Stormwater 02/19/14 09:30
Grab
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandealleott.eom
an employee -owned company
03,0712014 O& H This rrpnrr m�ry nnr he reprr+dated, except in full, Page 2 0 30

'LfRogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St, Work Order: 4020675
Asheville, NC 29901-4310 Reported: 03/07/14 08711
Sample Data
Sample Number 4020675-01
Sample Description Pentair Valves Outfall #I collected on 02/19/14 09:30
Reporting
Parameter Result Limit Units DF Aoalwed Method Flag Analyst Batch
General Chemistry Parameters
Oil and Grease, Total, HEM ND 5-0 mM- 1.00 02124/14 08:00 EPA 1664A CTS B4B0675
Total Metals
Copper
0.099
0.005
mg/L
1,00
02/25/14 11:41
EPA 200.7
MEC
B4B0705
Lead
ND
0020
mg/L
1.00
02/25114 1 ] A I
EPA 200.7
MEC
B4B0705
Zinc
0.12
0,010
mpJL
1.00
02/25/14 11:41
EPA 200.7
MEC
B4B0705
Volatile Organics
Benzene
ND
2.0
ug/L
1.00
02/26/14 10:46
EPA624-8260B
LBW
134B0820
Bromoform
ND
2.0
ug/L
1.00
02/26/14 10:46
EPA 624-8260B
LBW
134B0920
Carbon tetrachloride
ND
2.0
ug/L
1.00
02/26/14 10:46
EPA 624-9260B
LBW
B4B0820
Chlorobenzene
ND
2.0
ug/L
1.00
02/26/14 10:46
EPA 624-9260B
LBW
134B0820
Dibromochloromethane
ND
2,0
ug/L
1,00
02/26/14 10:46
EPA 624.8260B
LBW
B4B6820
Chloroethane
ND
2.0
ug/L
1,00
02/26/14 10:46
EPA 624-9260B
LBW
B4B0820
2-Chlorotthylviny) ether
ND
5.0
ugll.
1.00
02/26/14 10:46
EPA 624.82608
LBW
B4B0820
Chloroform
ND
2.0
atr/L
1.00
02126/14 10:46
EPA624-8260B
LBW
B4B0820
Bromodichloromethane
ND
2.0
urlL
1.00
02/26/14 10.46
EPA 624-8260B
LBW
B4B0820
1.1-Dichloroethene
ND
2.0
ug/L
1.00
02/26114 10:46
EPA 624-9260B
LBW
B4B0820
1,2-Dichloroethane
ND
2.0
ug/L
1.00
02/26114 10:46
EPA 624-8260B
LBW
B4B0820
trans-1,2-Dichloroethene
ND
2.0
u81L
1.00
02/26/14 10:46
EPA 624.8260B
LBW
B4B0820
1,1-Dichloroethene
ND
2,0
ugrL
1.00
02126/14 10:46
EPA624-8260B
LBW
B4B0820
1,2-Dichloropropane
ND
2.0
ug/L
1.00
02/26/14 ]0:46
EPA 624-82608
LBW
BQ0820
Ethylbenzene
ND
2.0
up/L
1.00
02/26/14 IQ46
EPA 624.8260E
LBW
B4B0820
Bromomethane (Methyl Bromide)
ND
2.0
uglL
1.00
02/26/14 10:46
EPA 624-9260B
LBW
B4B0820
Chloromethane (Methyl Chloride)
ND
2,0
ug/L
1.00
02/26/14 10A6
EPA 624-8260B
LBW
134130820
1,1,2,2-Tetrachloroethane
ND
2.0
ug/L
L00
02/26/l4 ]0:46
EPA 624.8260B
LBW
B4130820
Tetrachloroethene
ND
20
ug/L
1.00
02/26/14 10:46
EPA 624-826DB
LBW
B4B0820
Toluene
ND
2.0
ug/L
1.00
02/26/14 10:46
EPA 624-826DB
LBW
B4130820
1. 1. 1 -Trichloroethane
ND
2.0
ug/L
1.00
02/26/14 10:46
EPA624426DB
LBW
B4B0820
1,1,2-Trichloroethanc
ND
2.0
u81L
I
02/26114 10:46
EPA624-8260B
LAW
B4B0820
Trichloroelhene
ND
2.0
ug/L
1.00
02126/14 10:46
EPA 624.8260E
LBW
MGM
Vinyl chloride
ND
2.0
ug/L
1-00
02/26/14 10:46
EPA 624-9260B
LBW
B4B0820
Dichlorodifluoromethane
ND
2.0
ug/l-
1.00
02/26114 10:46
EPA624-9260B
LBW
B4B0820
Methylene Chloride
ND
2,0
us/L
1.00
02/26/14 10:46
EPA 624-8260B
LBW
B4B0820
TrlchlOrt)flUOremethane
ND
2.0
ug/L
1.00
02/26114 10:46
EPA 624.9260B
LBW
B4B0820
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesc Way I Greenville, SC 29607 1 main 664.232.1556 1 fax [phone] rogersandealleott.com
an employee -owned company
03,0711014 011 This repan rngv not he repru+luced. txrepr in {r�fl, u hhm+r xrirlen penni.rrinn frv+m kugers rK r.'alfcnrl, Inc.
Page 3 a 30

Rogers & Callcott
ENVIRONMENTAL
Environmental 'Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville, NC 28801-4310 Reported: 03/07/14 08:11
Sample Number
Sample Description
Parameter
4020675-01
Pentair Valves Outfal1 81 collected on 02/19/14 09:30
Reporting
Result Limit Units
DF
Analyzed
Method
Flag Analyst
Batch
Volatile Organics
1,2-Dichlorobenzene
ND
2.0
u811.
1.00
021204 10:46
EPA 624-8260B
LBW
B4B0820
1,3-Dichlorobenzene
ND
2.0
u811-
1.00
02126/14 10:46
EPA 624.8260E
LBW
B4B0820
1.4-Dichlorobenzene
ND
2.0
ug1L
1.00
02/26114 10:46
EPA 624-8260B
LBW
B4B0820
1,2,4-Trichlorobenzcne
ND
20
oglL
1.00
02/26/14 10:46
EPA 624-8260B
LBW
B4B0820
cis-1.3-Dichloropropene
ND
1.0
og/L
1.00
0226114 10:46
EPA 624-9260D
LBW
B4B0820
trans-1,3-Dichloropropene
ND
1.0
ug1L
1,00
0226114 10:46
EPA624.82600
LBW
B4130820
Surrotatts
%REC
%REC Limits
Flag
1,2-1Jich1oroe1hane-1)4
74
70-130
4-Brnmrjdnomhemene
98
70.130
Tnhrene-08
99
70-130
Semi-Vulatiles Organics
2-ChlorophenDl
ND
5,00
og1L
1.00
03/05/14 23:37
EPA 62518270D
RJM
134130693
2,4-Dichlorophenol
ND
5.00
ug1L
1 00
03/05/14 23:37
EPA6251827oD
RJM
134B0693
2,4-Dimeshylphenol
ND
5.00
utrlL
1,00
03/05/14 23:37
£PA625/9270D
RJM
B4B0693
2-Methyl-4,6-dinitrophenol
ND
5.00
ug1L
1.00
03105114 23:37
EPA 625t82701)
RJM
BQ0693
2,4-Diniirophenol
ND
5.00
14/L
1.00
03/05114 23:37
EPA 62518270D
RJM
B4B0693
2-Nitrophenol
ND
5.00
UWL
1.00
03/05/14 23:37
EPA 625/8270D
RJM
B4B0693
4-Nitrophenol
ND
5.00
ug1L
L00
03/05/14 23:37
EPA 62516270D
RJM
64B0693
p-Chloro-m-cresol
ND
5.00
utS4-
1.00
03/05114 23:37
EPA 62518270D
RJM
B4130693
Pentachlorophenol
ND
5.00
uBVL
1.00
03/05/14 23:37
EPA 62519270D
R.IM
B4B0693
Phenol
ND
5.00
ug1L
1.00
03/05/14 23:37
EPA 62518270D
RJM
B4B0693
2,4,6-Trichlorophenol
ND
5.00
ug1L
1.00
03/05/14 23:37
EPA 625182701)
RJM
B4B0693
Acenaphthene
ND
5.00
ug/L
1.00
.03/05/14 23:37
EPA 625/32701)
RJM
B4130693
Acenaphthylene
ND
5.00
vgll-
1,00
03/05/14 23:37
EPA 6298270D
RJM
B4110693
Anthracenc
ND
500
u81L
1.00
03/05/14 23:37
EPA 625/8270D
RJM
134B0693
Benzidine
ND
90.0
u81L
1.00
03/05/14 23:37
EPA 625/8270D
RJM
B4B0693
Benzo(a)anthracenc
ND
5.00
ug1L
1.00
03/05/14 23:37
EPA 62518210D
RJM
134B0693
Benzo(a)pyrene
ND
5.00
ug1L
1.00
03/05/14 23:37
EPA 625/8270D
RJM
B4B0693
Benzo(b)fluoranthene
ND
5.00
WIL
1.00
03105114 23:37
EPA 6251927DD
RJM
B4130693
Benzo(g,h,i)perylene '
ND
5.00
uSIL
1.00
03/05/14 23:37
EPA 625/8270D
RPub
B4B0693
Benzo(k)iluoranthene
ND
5.00
usf]-
1.00
03/05/14 23:37
EPA625/9270D
RJM
134BO693
Bis(2-chloreethoxy)Methane
ND
5,00
ug/L
].00
03105/14 23:37
EPA625r8270D
RJM
B4130693
Bis(2-chloroethyl)Ether
ND
5,00
ug/L
L00
03105/14 23:37
EPA 62518270D
RJM
134130693
bis(2-Chloroisopropyl)ether
ND
5.00
u81L
1.00
03/05/14 23:37
EPA 62519270D
RJM
B4110693
Bis(2-ethy1hcxyl)Phtha1ate
ND
5.00
uglL
1,00
03/05/14 23:37
EPA 625/8270D
RJM
134B0693
PO Box 5655 1 Greenville, SC 29606 1
426 Fairforest Way I
Greenville,
SC 29607
1 main 864.232.1556 1 fax [phone] rogersandcallcott.eom
an employee -awned company
03,0712014 08:11 Thi,c repnrr mqv nnr he reprrHlrecerl, eruept in full. N'irhniri wrirtrn perrni.vinn.frnnr kagerr & {'ajlcart, lnr.
Page 4 0 30

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot Si, Work 0rder. 4020675
Ashcville, NC 28801-43 10 Reported: 03/07/14 WII
Sample Number 4020675-01
Sample Description Pentair Valves Outfall #1 collected on 02/19/14 09:30
Reporting
Parameter Result Limit Units DF Analyzed Method l4ag Analyst Batch
Semi-Volatiles Organics
4-Bromophenylphenylcihcr
Batylbenzylphthalate
2-Chloronaphilutlene
4-Chlorophenylphenylether
Chrvsene
13ibenzo(a-h)anlhracene
3,T-Dichlarobenzidine
Diethylphthaltate
Dimethylphthalate
Di-n-butylphthalate
2,4-Dinitrotoluene
2.6-Dinitrotoluene
Di-n-octylphthalate
1,2-Diphenylhydrazene(Azobenzene)
Fluoranthene
FluOrene
Ilexachlorobenzenc
llexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pYrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitroso-di-mathylamine
N-N itroso-di-n-propyl amine
N-Nilrosodiphenylamine (Diphenylamine)
Phenanthrene
Pyrene
Surrogates
ND
5.00
ug/L
1.00
03/05/14 23:37
EPA 625/9270D
RJM
B4B0693
ND
5.00
ug/L
1,00
03/05/14 23:37
EPA 62519270D
RJM
134130693
ND
5.00
Usti.
I
03/05/14 23:37
EPA 625/8270D
RJM
B4B0693
ND
5.00
ug/L
1.00
03/05/14 23:37
EPA 62SJ8270D
RJM
B4130693
ND
5.00
U£n-
1.00
03/05/34 23:37
EPA 62519270D
RJM
B4B0693
ND
5,00
ug/L
1.00
03/05114 23:37
EPA 625/9270D
RJM
B4B0693
ND
5.00
ug/L
1.00
03/05/14 23:37
EPA 625/8270D
RJM
B4B0693
ND
5,00
ug/L
1.00
03/05/14 23:37
EPA 62518270D
RJM
B4B0693
ND
5,00
ug/L
1.00
03/05/14 23:37
EPA 62519270D
RIM
1300693
ND
Soo
ug/L
1.00
03/05/14 23:37
EPA 625182701)
RJM
B4B0693
ND
5.00
ug/L
1.00
03/05/14 23:37
EPA 625/8270D
RJh1
B4130693
ND
5.00
uglL
1.00
03/05/14 23:37
EPA 625/82701)
RJM
B4B0693
ND
5.00
u911,
1.00
03/05/14 23:37
EPA 625/9270D
RJM
B4B0693
ND
5,00
ug/L
1.00
03/05/14 2337
EPA62518270D
RJM
134130693
ND
5.00
u81L
1.00
03/05/14 23 37
EPA 625/9270D
RJM
B4B0693
ND
5.00
uglL
1.00
03/05/14 23:37
EPA 625/8270D
RJM
B4130693
ND
5.00
uWL
1.00
03/05/14 23:37
EPA62518270D
RJM
B4B0693
ND
5.00
Ugn-
1.00
03/05/14 23:37
EPA62518270D
RJM
134130693
ND
5.00
ug/L
1.00
03/05114 2337
EPA 625/8270D
RJM
B4S0693
ND
5.00
ug/L
1.00
03/05/14 23:37
EPA 625/92701)
RJM
B4B0693
ND
5.00
uB/L
1.00
03/05/14 23:37
EPA 62518270D
RJM
B4B0693
ND
5.00
UBA,
1.00
03/05/14 23:37
EPA 62519270D
RJM
B4B0693
ND
5.00
ug/L
1.00
03/05/14 23:37
EPA625/92701)
RJM
B4B0693
ND
5.00
UWL
1.00
03105/14 23:37
EPA 62518270D
RJM
B4130693
ND
5.00
ug/L
L00
03/05/14 23:37
EPA 625/8270D
RJM
134B0693
ND
5.00
ug/L
1,00
03/05/14 23:37
EPA 625/8270D
RJM
B4B0693
ND
5.00
ug/L
1,00
03/05114 23:37
EPA 625/8270D
RJM
H4B0693
ND
5.00
ug1L
1.00
03/05/14 23:37
EPA 62518270D
RJM
B4130693
ND
500
ug1L
1.00
03/05/14 23:37
EPA 62519270D
RJM
B4B0693
%REC
%REC Limits
Flag
Afarn,hemene-US
82
35-114
2-Hlrmrnhipheteyl
86
43-116
1'erphenyl-W4
94
33-141
2-Flunmphenol
49
21-110
Phenol-W
34
10-110
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 E main 664.232.1556 1 fax 864.232,6140 rogersandcallcott-COm
an employee -owned company
03,0712014 O l ! This report m ry rea he rrpmduced, ercapr 1n fu1d, x iahmra wrlllrn pervnis,rinn,{mn7 Hogec n (.'u!lcnrr, !n
Page 5 of 30

Rogers & Cal[cott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville, NC 28801-4310 Repurted: 03/07/14 08:1 1
Sample Number 4020675-01
Sample Description Pentair Valves Outfall #1 collected on 02/19/14 09:30
Reporting
Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch
Semi-Volatiles Organics
Surrogates %REC %REC Limits Flag
1,4,6-Y' hromophenal
99
10-123
PCBS
PCB-1016
ND
0.50
ug/l,
1.00
02/27/14 01:14
EPA609
RKH
B4130740
PC13-1221
ND
0-50
ugl1.
1,00
02/27/14 01:14
EPA609
RKH
B4130740
PCB-1232
ND
0-50
ug/L
1,00
02/27/14 01:14
EPA 609
RKH
BU0740
PCB-1242
ND
0.50
ug/L
1.00
02/27/14 01:14
EPA608
RKH
B4B0740
PCB-1248
ND
0,50
ug1L
1 00
02127/14 01:14
EPA609
RKH
B4B0740
PCB-1254
ND
0.50
ug1L
1.00
02/27/14 01:14
EPA608
RKH
B4B0740
PCB-1260
ND
0.50
ugrL
1.00
02/27/14 01:14
EPA606
RKH
B4B0740
Surrogates
%REC
%REC Limits
Flag
2,4,5,6-Telrachlnro-m-xylene
87
60-130
berorhlorohephenvl
69
30-150
Sample Number
4020675-02
Sample Description
Penlair Valves Outfall 41 collected on 02/19/14 09:30
Reporting
Parameter
Rrsult Limit Units DF
Analyzed Method Flag Analyst Batch
Volatile Organics
Acrolein
gib 5.0 uglL 1.00
03/03/14 16:46 EPA 6244260B LBW B4CG096
Acrylonitr'tle
ND 5.0 uglL 1.00
03M3/14 16:46 EPA 624.8260B I.BW 134C0096
Surrogates
%REC
°/ REC Limits Flog
1,2-Dwhlnroelhane-D4
96
70-130
Y'nlreene-nK
95
70-130
1-drnnrnflraur+hen_ene
102
70.130
PO Box 5655 I Greenville, SC 29606 1426 Fairforest Why I Greenville, SC 29607 1 main 664.232.1556 I fax 864.232,6140 rogersandcallcott.com
an employee -owned company
03,0712014 08:11 This reporl mu}, nnr he reprrrdncerl except in f dl, r+'uirc+trt wrirlen prrmis,rdonJrruu Bogen A- C.'alluolt, Inv,
Page fi o 34

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville, NC 28801-4310 Reported: 03/07/14 08:11
Samplt Number 4020675-03
Sample Description Pentair Valves Outfall 92 collected on 02/19/14 09:30
Reporting
Parameter Result Limit Ilnitl DF Analyzed 'slethod Flag Analyst Batch
General Chemistry Pararneters
Oil and Grease, Total, HEM
ND
5.0
mg/L
1.00
02/24/14 08:00
EPA 1664A
CTS
B4130675
'r01ai metals
Capper
ND
0.005
mgfl-
1.00
02125/14 11:43
EPA 200.7
MEC
B4B0705
Lead
ND
0.020
MA
1,00
02/25/14 11:43
EPA2W7
MEC
B4B0705
"Zinc
0.012
0.010
mg/L
1.00
02/25/14 11:43
EPA 2003
MEC
134130705
Volatile Organics
Benzene
ND
2,0
ug1L
1.00
02/26/14 11:14
EPA 624-826013
LBW
134B0920
Bromoromi
ND
2.0
u911-
1.00
0226114 11:14
EPA 624-8260B
LBW
B4130920
Carbon tetrachloride
ND
2.0
ug/L
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B4B0820
Chlorobcnzene
ND
2.0
ugfl-
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B4B0920
Dibromochloromcthane
ND
2,0
ug1L
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B4B0820
Chloroethane
ND
2.0
uUIL
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B480820
2-Chloroethylvinyl ether
ND
5.0
u8I-
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B4B0820
Chloroform
ND
2,0
ug/L
1.00
02/26/14 11:14
EPA 624-8260A
1.3W
1300820
Bromodichloromethane
NI)
2.0
nglL
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B4B0820
1,1-Dichioroethane
NI)
2.0
ug1L
1.00
02/26/14 11:14
EPA 624-8260R
LBW
B4B0820
1.2-Dichloroethane
ND
2.0
401-
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B4B0820
trans-1 2-Dichloroeihene
ND
2.0
uglL
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B4130820
l,l-Dichloroethene
ND
2.0
ug/L
1.00
02/26/14 1IT14
EPA 624-82608
LBW
B4B0820
1.2-Dichloropropane
ND
2.0
ug/L
1.00
02126/14 11:14
EPA 624-82603
LBW
B4B0820
Ethvlbenzene
ND
2.0
ugll-
I.00
02/261M I1:14
EPA 624-8260B
LRW
B4B0820
Bromomethane (Methyl Bromide)
ND
2.0
ug/L
1.00
0226/14 11:14
EPA 624-9260B
LBW
B4130820
Chloromethane (Methyl Chloride)
ND
2.0
uglL
1.00
02/26/14 l I A4
EPA 624-8260E
LBW
134B0820
1,1,2,2-Tetrachloroethane
ND
2.0
ug/L
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B00820
Tetrachloroethene
ND
2.0
uglL
1.00
02/26/14 11:14
EPA 624-8260B
LBW
134B0820
Toluene
ND
2.0
ug/L
1.00
02/26/14 11:14
EPA 624-826OR
LBW
B4B0820
1, 1, 1 -Trichloroethane
NI)
2.0
ug/L
1.00
0226/14 11:14
EPA 624-8260B
LBW
BQ0820
1,12-Trichloroethane
ND
2.0
uglL
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B4130820
Trichlornethene
ND
2.0
ug/L
1.00
02/26/14 11:14
EPA 624-8260B
LBW
134130820
Vinyl chloride
ND
2.0
ug/L
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B4B0820
Dichloroditluoromethane
ND
2.0
u91L
1,00
02/26/14 11:14
EPA 624-8260B
LBW
B4B0820
Methylene Chloride
ND
2.0
ug/L
1.00
02/26/14 11:14
EPA 624-8260B
LBW
B400820
Trichlorofluoromethane
ND
2.0
ug/L
1,00
02/26/14 11:14
EPA 624.8260E
LBW
B4130820
1,2-Dichlorobenzene
ND
2.0
ug/L
1.00
02/26/14 11:14
EPA 624-826013
LBW
B4130820
1.3-Dichlorobenzene
ND
2.0
u91L
1.00
02/26/14 11:14
EPA 624-82608
LBW
B4B0820
PO Box 5655 1 Greenville, SC 29606 1 426 fairforest VVay I Greenville,
5C 29607 I main 864•232.1556 I fax [phone]
rogersandcallcott.eom
an employee -owned company
03,0712014 UN; I1
lhia rennrt mqv nnr hr n prnrGrcrrl, crcrpr in,fi+/f, x ilhmil
wrinen �7erinissinr Jrnnr kngrne
K Culfcnrt, 1r c.
Page 7 0! 30

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville, NC 28801-4310 Reported: 03/07/14 08.11
Sample Number
4020675-03
Sample Description
Pentair Valves Outfal€ 42 collected on 02/19/14
09:30
Reporting
Paramtter
Result
Limit
Units
DF
Analyzed
Wthod
Flag Analyst
Batch
Volatile Organics
1,4-Uichlorobenzene
ND
2.0
u911-
1,00
02/26/14 11:14
EPA 624-3260H
LBW
B4B0820
1.2.4-Trichlorobenzene
ND
2.0
uglL
1.00
02/26/14 11:14
EPA 624-9260H
LBW
B4R0820
cis-1,3-Dichloropropene
ND
1.0
ug/L
1.00
02/26/14 11:14
EPA 624-B260B
LBW
B4B0820
trans-1„3-Dichloropr0pcnc
ND
1.0
ug/L
1.00
02/26/14 11:14
EPA 624.8260E
LBW
B4B0820
Surrogates
%REC
'% REC limits
Flag
1.2-D1ch1orveihune-D4
76
70-130
4-Bromofhenrnhercene
9!
70-130
Toluene -DM
97
70-130
Scmi-Volatiles Organics
2-Chlorophenol
ND
5.00
uglL
1,00
03/06/14 00:07
EPA 625/8270D
RIM
B4130693
2,4-Dichlorophenol
ND
5.00
ug/L
1 00
D3/06/14 00:67
EPA 62PB270D
RIM
B4B0693
2.4-Dimethylphenol
ND
5.00
ug/L
1,00
03/06/14 00:07
EPA 62518270D
RJM
B4130693
2-Methyl-4,6-dinitrophenoi
ND
5.00
U9fL
1.00
03/06/14 00:07
EPA 62518270D
RJM
134BO693
2,4-Dinitrophenol
ND
5.00
UWL
1 M
03AW14 00:07
EPA 625/9270D
RJM
84BO693
2-Nitrophenol
ND
5.00
US&
1,00
03106/14 00:07
EPA625/827UD
RJM
B4B0693
4-Nitrophenol
ND
5.00
ug/L
1.00
03/06/14 00:07
EPA 625/8270D
RIM
B4B0693
p-Chloro-m-cresol
ND
5.00
UWL
1.00
03/06/14 00:07
EPA 62518270D
RJM
B4B0693
Pentachlorophenol
ND
5.00
uglL
1,00
03/06/14 00:07
EPA 62518270D
RIM
R4B0693
Phenol
ND
5.00
U91L
1.00
03/06/14 00:07
EPA 625/8270D
RIM
B4B0693
2,4,6-Trichlorophenol
ND
5.00
U91L
1.00
03/06/14 00:07
EPA 62518270D
RJM
BQ0693
Accnaphthene
ND
5.00
ug/L
1.00
03/06/14 00:07
EPA 62519270D
RIM
B4B0693
Aeenaphthylene
ND
5,00
ug/1•
1.00
03106/14 00:07
EPA 625/9270D _
RJM
B4130693
Anthraeene
ND
5,00
,ig/L
1.00
03/06/14 00:07
EPA 62518270D
RJM
B4B0693
Benzidine
ND
80.0
ug1L
1.00
03/06/14 00:07
EPA 62518270D
kJM
134B0693
Benzo(a)anthracene
ND
5,00
ug/L
1.00
03/06/14 00:07
EPA 625A2701)
RJM
B4B0693
Benzo(a)pyrene
ND
5.00
ug/L
1.00
03/06/14 00:07
EPA 62518270D
RJM
B4B0693
Benzo(b)fluoranthene
ND
5.W
uglL
1,00
03/06/14 00:07
EPA 625/9270D
RJM
B4B0693
Benzo(g.b,i)perylene
ND
5.00
ug/L
1.00
03/06/14 00:07
EPA 62318270D
RJM
B4B0693
Benzo(k)fluoranthene
ND
5.00
ug/L
I.00
03/06/14 00:07
EPA625/8270D
RJM
R4B0693
Bis(2-chlotoethoxv)Methane
ND
5.00
us<L
1.00
03/06/14 00:07
EPA 625/8270D
RJM
B4R0693
Bis(2-chloroethyl)ELher
ND
5,00
u81L
1,00
03/06/14 00:07
EPA 625/8270D
RJM
B4130693
bis(2-Chloroisopropyl)ether
ND
5.00
uSIL
1,00
03/06/14 00:07
EPA 625/8270D
RIM
B4130693
Bis(2-ethylhexyl)Phtha1ate
ND
5.00
ug/L
1,00
03/06/14 00:07
EPA 6298270D
R.iM
B4B0693
4-Bromophenylphenyl ether
ND
5.00
ug/L
1.00
03/06/14 00:07
EPA 625/9270D
RJM
B4B0693
Butylbenzylphthalate
NE)
5.00
ug1L
1,00
03/06/14 00:07
EPA 625/9270D
RJM
B4110693
PO Box 5655 t Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 I fax [phone] rogersandcallcott.COm
an employee -owned company
03,0712W4 06:11 This repnrr mg, nor he rrpmduced, rscepi in frill, u ithoiu x Nfran prrrnicrirrn.frvrert Rogers K. (Adhnrr, Inc.
Page 8 of 30

Rogers & Callcott
ENVIRONMENTAL
Environnientai Testing Solutions Project: Pentair Valves
351 Depot St, Work Order: 4020675
Asheville, NC 28801-4310 Reported: 03/07/14 08:11
Sample Number 4020675-03
Sample Description Pentair Valves Outfal1 #2 collected on 02119/14 09:30
Reporting
Parameter Result Limit Units DF Analyzed Method Flag Analyst Ratch
Semi-Volatiles Organics
2-Chloronaphthalene
4-Chlorophenylphenylether
Chrysene
Dibervo(a,h)anthracene
3,T-Dichlorobenzidine
Diethylphthalate
Dimethylphthalate
Di-n-butyl phthalate
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalale
1,2-Dipheny1hydrazene(Azobenzene)
Fluoranthene
Fluorene
Hexachlorobenzene
1Jexachlorobutadiene
Hexachlorocyclopentadiene
llexachloroethane
1ndeno(1,2,3-ed)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitroso-di-methylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine (Diphenylamine)
Phenanthrene
l'ytene
Surrogates
ND
5.00
ug1L
I.00
03/06/14 00:07
EPA 62518270D
RJM
134B0693
ND
5.00
ug/L
1.00
03/06/14 00:07
EPA 62518270D
RJM
B4B0693
ND
5.00
ug1L
1.00
031061]4 00:07
EPA 625/8270D
RJM
B4B0693
ND
5.00
ug1L
1,00
03/06/14 00:07
EPA 62519270D
RJM
B4H0693
ND
5.00
ug/L
1.00
03/06/14 00:07
EPA 62518270D
RJM
134130693
ND
5.00
ug1L
1.00
03/06/14 00:07
EPA 625/8270D
LIM
B4B0693
ND
5.00
ug1L
I.00
03/06/14 00:07
EPA 625/8270D
RJM
B4B0693
ND
5.00
ug1L
1.00
03/06/14 00:07
EPA 625/8270D
RJM
B4B0693
ND
5.00
ng1L
1.00
03/06/14 00:07
EPA 625/8270D
RJM
B4B0693
ND
5.00
ug1L
1.00
03/06/14 00:07
EPA 62519270D
RJM
B4B0693
ND
5.00
ug1L
1.00
03/06/14 00:07
EPA 625/8270D
RJM
B4B0693
ND
5.00
ug1L
I.00
03/06/14 00:07
EPA 625/8270D
RJM
B4B0693
ND
5.00
ug/L
1.00
03/06/14 00:07
EPA 625/8270D
RJM
B4B0693
ND
5.00
ugIL
I.00
03/06/14 00:07
EPA 625/8270D
RJM
B4B0693
ND
5.00
Ug/L
1.00
03/06/14 00:07
EPA 62518270D
RIM
B4B0693
ND
5.00
u81L
1.00
03/06/14 00:07
EPA 62518270D
RJM
B4B0693
ND
5.00
uglL
1.00
03/06/14 00:07
EPA625JR270D
RJM
B4130693
ND
5.00
u81L
1.00
03/06/14 00:07
EPA 6251827DD
RJM
B4130693
ND
5.00
uglL
1.00
03/06/14 00:07
EPA 625/827DD
RJM
B4B0693
ND
5.00
11g1L
1.00
03/06/14 00:07
EPA 62518270D
RJM
B4130693
ND
5,00
uglL
1.00
03/06/14 00',07
EPA 625/8270D
RJM
B4B0693
ND
5,00
u8/l.
1.00
03/06/14 00:07
EPA 62518270D
RJM
B4130693
ND
5.00
ug1L
1.00
03/06/14 00:07
EPA 625/8270D
RJM
B4130693
ND
5,00
ugll.
1.00
03/06/14 00:07
EPA 625/8270D
RJM
B4B0693
ND
5.00
ug/L
1.00
03/06/14 00:07
EPA 625/8270D
RJM
B4B0693
ND
5.00
ug/L
1.00
03/06/14 00:07
EPA 62518270D
RJM
B00693
ND
5.00
u81L
1.00
03106A4 00:07
EPA 62518270D
RJM
B4B0693
%REC
% REC Limih
Flag
Nitrobenzene-D5
77
35-114
24-71hmrabiphenvl
80
43-116
Yerphenyl-D14
89
33-141
2-Flnoraphenol
47
21-] 10
Phenol-D5
33
10-110
1,4,F4'nbramopherm1
72
10-123
PCBs
PO Box 5655 I Greenville, SC 29606 1426 Fairforest Way I Greenville, SC 29607 I main 864.232.1556 I fax [phone] rogersarldcallcott.corrl
an employee -owned company
03,0712014 08 11 Ah reporr may n01 he reproduced, except in,full, N irhoul wrinen pernni.ceion fronr 1{ngerr & Callcotl Inc.
Page 9 0 30

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville, NC 29801-4310 Reported: 03/07/14 08:11
Sample Number
4020675-03
Sample Description
Pentair Valves Outfall #2 collected on 02/19/14
09:30
Reporting
Parameter
Result
limit
Units
DF
Analyzed
Method
Flag
Analyst
Batch
PCBs
PCB-1016
ND
0.50
ug1L
1.00
0212M4 00:42
EPA 608
RKH
B4BO740
PCB-1221
ND
0.50
ug1L
1.00
02/27/14 00:42
EPA 608
RKH
B4BO740
PCB-1232
ND
0.50
vg[L
1.00
02/27/14 00:42
EPA 608
RKH
B4130740
PCB-1242
ND
0,50
og/L
1.00
02/27/14 00:42
EPA 608
RKH
MR0740
PCB-1249
NT)
0.50
ugn-
1.00
02/27/14 00:42
EPA 608
RKH
B4BO740
PCB-1254
ND
0.50
u91L
1.00
02/27/14 00:42
EPA608
RKH
B4BO740
IICB-1260
ND
0.50
ug/L
1.00
02/27/14 ODA2
EPA 608
RKH
134B0740
Surrogates
%REC
%REC limits
Flag
1.4.S.C,-'1'etraehlnro-m:vrlene
86
60-130
Ihcachlnrr�hiphrttvl
85
30-I50
Sample Number
4020675-04
Sample Description
Pentair Valves Oulfall #2 collected
on 02/19/14
09:30
Reporting
Parameter
Result
Limit
Units
DF
Analyzed
Method
Flag
Analyst
Batch
Volatile Organics
Acrolein
ND
5.0
uglL
1.00
03/03/14 17:15
EPA 624-8260B
LBW
134C0096
Acrylonitrile
ND
5.0
ugfL
1.00
03/03/14 17:15
EPA 624-8260A
LBW
134C0096
Surrogates
%RF,C
%REC Limits
Flag
1,2-Uich1aroethane-D4
84
70-130
7'uluene-1)8
96
70-130
4-Hromgjleorobencene
103
70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 ta. 864.232.6i4o rogerSandcallcott.COm
an employee -owned company
03,0712014 08,11 This reporr mar not he reproduced, except m fidl, withnar writren permission from Rngrrr rK Callcon, Inc.
Page 10 of 30

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville, NC 28801-4310 Reported: 03/07/14 08:11
General Chemistry Parameters
Quality Control Summary
Reporting Spike Source % REC RFD
Parameter Result Limit Units level Result %REC Limits RPD Limit Flags
Batch 84BO675 - General Prep - Wet Chem
Blank (64130675-8LI(I )
Oil and Grease, Total, HEM ND 5.0
mg/L
LCS (84B0675-BSI)
Oil and Grease. Total, HEM 39.0 5.0
mg1L 40.0 98 78-214
LCS (64130675-BS2)
Oil and Grease, Total. HEM 35.9 5.0
mgil- 40.0 90 78-f 14
LCS Dup (B4B0675-BSDI)
Oil and Grease, Total, HEM 33.8 5.0
mglL 40.0 84 78-114 14 35
PO Box 5655 1 Greenville, SC Z9606 1 426 Fairforest Way 4 Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcalieott.eom
an employee -awned company
b3,0712014 08:11 This report corm not he reprodneed, except in fadl, m W ow written perinission frrrrn Hogerr n- (,'allcon, Inc. I Page 11 Of $O

Rogers & CaUcott
,ly ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot Si. Work Order: 4020675
Asheville, NC 28801-4310 Keportvd: 03/07/14 08.11
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Paramrtcr Result Limit Units Lr.tl Result %REC Limits RPD Limit Flags
Batch B4B0705 - EPA 200.7
Blank (M0705-BLKI)
Copper
ND
0.005
mglL
Lead
ND
0.020
mglL
Zinc
ND
0.010
mglL
LCS (B00705-11SI )
Copper
1.02
0.D05
m91L,
1.00 102 85-115
Lead
0.99
0.020
mgfL
1.00 99 85-115
Zinc
0.96
0,010
mg/L
1.00 96 85-115
Duplicate (B4B0705-D11P1)
Source: 4020586-03
Copper
ND
0.005
mglL
ND 20
Lend
ND
0.050
Dig/I.
ND 20
Zinc
0.02
0.010
my'1.
0.02 5 20
Duplicate (114B0705-DUP2)
Source: 4020630-07
Copper
ND
0,005
mglL
ND 20
Lead
ND
0,050
mgl1,
ND 20
Zinc
0.16
0,610
mglL
0.16 0.3 20
Matrix Spike (114130705-41S1)
Source: 4020586-03
Copper
0.99
0.005
mg1L
I
ND
99
70-130
Lead
0.96
0 050
mgll.
1.00
ND
95
70.130
Zinc
0.96
0.010
mglL
1,00
0.02
93
70.130
Matrix Spike (B4B070.5-R1S2)
Source: 4020630-07
Copper
I.06
0.005
m8lL
LOD
ND
106
70-130
Lead
1.03
0.050
mglL
1,00
ND
103
70.130
Zinc
1,18
0.010
mg/L
1.00
0-16
103
70.13D
Post Spike (PAB0705-PSI)
Source: 4020586-03
Copper
100
mg/L
1.00
ND
99
85-115
Lead
0.97
mglL
1.00
ND
96
85-115
Zinc
0.97
mglL
1.00
0.02
95
85-115
PO Box 5655 1 Greenville, SC 29606 1426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.COm
an employer. -owned company
03,0712014 08r 11 Thrs rrpnrr rrary nr+r he ►epxxl++ced, excrpl in.Jidl, n irhuu+ x rtrren Jfcr+nivainn frnn+ Rngcnv x• Cedler+u, Inv.
Page 12 0 30

Rogers & Callcott
ENVIRONMENTAL
fAvironmental Testing Solutions Project: 1 enlair Valves
351 Depot St. Work Order: 4020675
Asheville. NC 2990143 10 Kepurtt:d: 03/07/14 08:11
Total Metals
Quality Control Summary
Reporting Spike Source '%REC RFD
Parameter Result Limit Units Level Result % KF-C Limits RPD Limit Flags
Batch B4B0705 - EPA 200.7
POst Spike (113490705-PS2) Source: 402063047
Capper 1.02 tngll- 1.00 ND 101 85-115
Lead 0,99 mglL 1.00 ND 99 95-115
Zinc 1.14 mg1L 1 00 0.16 99 95-115
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesr Way I Greenville, SC 29607 1 main $64.232.1556 1 tax 864.232.614o rogersandcallcott.COm
an employee -owned company
03�07/:014 08:11 This report nuq not he reproducrd, except infill, a irhour wraren permission front Rogem & C:olkon, Inc.
Page 13 of 30

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
35I Depot St. Work Order: 4020675
Asheville, NC 28801-4310 Reported: 03/07/14 08:11
Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B4B0820 - EPA 5030
Blank (B4B0820-BLX11)
Benzene
ND
2,0
ug/L
Bromolurm
ND
2.0
ug/L
Carbon tetrachloride
ND
2.0
ug/L
Chlorobenzene
ND
2.0
ag/L
Dibramoehloromethane
ND
2.0
ug/L
Chloroethane
ND
2.0
ug/L
2-Chloroethylviny) ether
ND
5.0
ug/L,
Chloroform
ND
2.0
ug/L
Bmmodichiorometbanc
ND
2.0
ug/L
I.l-Dichlorocibane
ND
2.0
ug/L
1,2-Dichtmaeshane
ND
2.0
ug1L
Irans-1,2-Dichloroethene
ND
2.0
u811.
1,1-Dich1nroethene
ND
2.0
ug1L
1,2-Dichloropropane
ND
2.0
ug11.
Ethylbenzene
ND
2.0
uglL
Bromomethane(MethylBromide )
ND
2.0
ug/L
Chloromethane (Methyl Chloride)
ND
2.0
ug/L
1,3.2,2-Temechloroeihane
ND
2.0
ug/L
Tetrechlornethene
ND
2.0
ug/L
Toluene
ND
2.0
ug/L
1,1,1-Trichlorocthane
ND
2.0
ug/L
1,1,2-Trichloroethane
N❑
2.0
ug/L
Trichloroethene
ND
2.0
ug/L
Vinyl chloride
ND
2.0
ug/L
Dichlorodifluoromethanc
ND
2.0
ug1L
Methylene Chloride
ND
2.0
ug/L
Trichlorofluoromcihane
ND
2,D
ug/L
I2-Dichlorobcnzcnc
ND
2.0
ug/L
1,3-Dichloroben7zne
ND
2.0
uWL
1.4-Dichlurobciwene
ND
2,0
ug1L
UA-Trichlorobenzene
ND
2.0
ug/L
cis-1,3-Dichloropeopena
ND
1.0
ugll.
trans-1,3-Dichloropropene
ND
1.0
ug/L
Surrogarer 1,2-Dichlornerhanp-D4
80 70-13U
Surrugare: 441romglluorobenzene
103 70-130
PO Box 5655 1 Greenville, 5C 29606 1 426 Fairforest Way I Greenville, 5C 29607 1 main 864.232.1556 1 fax [phone] rogerSandcallcott.eom
an employee -owned company
03,07/2014 0831 Thi,r repori miry not he reprodirced, a cep1 irr fill, %Lnhorrr wnuen permission from Rogers at Cadlcan, Inc:,
Page 14 a 30

Rogers & Cailcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville. NC 28801-4310 KeTwrled: 03/07114 08:1 1
Volatile Organics
Quality Control Summary
Reporting Spike Source % RE KIT
Parameter Result Limit Units Lrvel Result %REC limits KPO Limit Flags
Batch B4B0820 - EPA 5030
Blank (8480820-BLKI)
.Snrrngote: 'Toluene-U8 98 70-130
LCS (B4BO820-BSI)
senune
20.2
2.D
ug/L
20.0
IN
70-130
Bromoform
19.4
2.0
ug/L
20.0
97
71-129
Carbon tetrachloride
195
2.0
1191L
20.0
93
73-127
Chlorobanzeoc
19.4
2.0
08fl-
20.0
97
70.130
Dibromochloromeihane
18.9
2.0
ug/L
20.0
94
70-130
Chloroethane
19.2
2.0
ug/L
20.0
96
60-140
2-Chloroethylvinyl ether
IC6
5.0
ug/L
20 n
73
5D-150
Chloroform
20.0
2.0
ug/L
20,9
100
70-130
Brtmoodtchloromethane
1S.9
2.0
uglL
2D.0
95
70-130
1,1-Dichloroobanr
16.7
2.0
ug/L
20.0
84
73-127
1.2-Dichlotocthsne
17.1
2.0
ug/L
20.0
86
7D-130
trans-1,2-Dichloroethene
17.4
2.0
uo.
20,0
87
70-130
I,l-Dichloroethene
18.7
2.0
ug/L
20.0
94
70-130
1,2-Dichloropropane
16.0
2.0
ug/L
20.0
SO
70.130
Eth0benzene
22.7
2.0
uglL
20.0
113
70-130
Bromninethane (Methyl Bromide)
21.7
2.0
ug/L
20.0
l08
60-140
Chloromethane (Methyl Chloride)
27.7
2.0
ug/L
20.0
138
60-140
1,1.2,2-Tetrachloroethane
20.4
2.0
ug/L
20.0
102
70.130
Te"chlorocthenc
21.4
2.0
ug/L
20.0
107
74-126
Toluene
22.1
2.0
ag1L
20.0
110
75-125
1,1.1-Trichloroethane
19.2
2.0
uglL
20.0
96
75.125
1,1.2-Trichl0rnethane
20.0
2,0
ug/L
20.0
100
71-129
Trichlorocthene
17.9
2.D
ug/L
20.0
89
71-130
Vinylohloridc
2L5
2.0
UWL
20.0
108
60-140
Dichlorodi0uoromed mu
27.8
2-0
ug/L
2oA
t35
60-140
Methylene Chloride
19.1
2.0
ng/l.
20.0
96
70-130
Trichlorofluoromohane
22.3
2.D
ug1L
20.0
112
60-140
1,2-Dichlorobenzene
19.7
2.0
ug/L
20,0
98
70-130
1.3-Dichlorobenzcne
19.8
2.0
ug/L
20 0
99
73-127
1,4-Dichlorobenzene
19.2
2.0
ug/L
M0
96
70-130
1.2.4-Trichlorobenzene
20.6
2.0
ug/L
2D.D
l03
6D•140
cis.1.3-Diehlorupropene
20.0
1.0
ttg1L
20.0
100
70-130
trans-l.3-DicMaropropene
20.8
1.0
u81L
20-0
104
70-130
PO Box 5655 1 Greenville, 5C 29606 1 426 Fairforesc way I Greenville,
5C 29607 1 main 864.232.1556
1 fax [phone]
rogersandcalleott.com
an employee -owned company
03,0712014 08:11 This report muv not he reproducrrf errept m fidl, a Oboist w'rirren permission from Rogers d• (AdItotr, Inc.
Page 15 of 30

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville. NC28801-4310 Keporled 03/07/14 08.11
Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result limit Units Level Result % REC Limits RPD Limit Flags
Batch B4130820 - EPA 5030
LCS (R430820-BSI )
Surmgure:1,2-Dichloraerhune-1N
93
70-130
Surrogate: d-BromgJluoroheuzene
100
70.130
Surrogate: Toluene-UR
111
10-130
Matrix Spike (64130820-ti1Sl)
Source: 4020511-02
semxhe
2!,6
2.0
us/L
20.0
ND
108
37-151
eromofom
20 0
2.0
usll
20.0
ND
100
45-169
Carbon tetrachloride
20.3
2.D
U91L
20.0
ND
102
70.140
Chlorobenzene
20.8
2,D
ug/L
20.0
ND
104
37-160
Dihromochloromethane
20.3
2.0
ug/L
20.0
ND
102
53.149
Chloroethanc
20.4
2.0
ug)L
20.0
ND
102
14-200
2-Chloroethylvinyl ether
149
5.0
ugll
20.0
ND
75
3-200
Cblorofnrm
21.7
2.0
Usti-
20.0
ND
108
51-118
Hrornodichioromeibane
20.4
2.0
U91L
20.0
ND
102
35-155
1.1-DIChl0TDethane
19.3
2.0
ug/L
20.0
ND
90
59-155
1,2-Diehlotocthane
19.4
2.0
ug/L
20,0
ND
92
49.155
trans-1,2-Dichloroethene
19.6
2.0
ug/L
20.0
ND
98
54-156
1,1-Dichlorocthcnc
21,6
2,D
ug/L
2D D
ND
104
3.200
1,2-Dichloropropane
17,6
2.0
ug/L
20,0
ND
88
3-200
Ethylbenzene
24.2
2.0
ug/L
20.0
ND
121
37-162
Bromomethane (Methyl Bromide)
7 L4
2 0
ugfl-
20.0
ND
107
1-200
Chlerromerhane (Methyl Chloride)
27.7
2.0
ug/L
2D.0
ND
138
7-2110
1.1,2,2-Tetrachloroethnne
21.9
2.0
ug/L
20,0
ND
ID9
46-157
Tetraehlororthene
23,5
2.0
ugtl,
20,0
ND
117
64-148
Toluene
24.0
2.0
uglL
20.0
ND
120
47-150
1,1,1-Trichlarowhane
21,9
2.0
ug/L
20.0
ND
105
52-162
1.1,2-Trichlomethane
212
2,o
ng/L
20.0
ND
106
52-150
Trichloroethcne
19.9
2.0
ug/L.
20.0
ND
100
71-157
Vinyl chloride
23.8
2.0
ug/L
20.0
ND
119
3-1D0
Dichlorodifluoromethane
28,2
2.0
ug/L
20.0
ND
141
60-140 sl
Methylene Chloride
20.1
2.0
ugll.
20.0
ND
100
3-200
TrichlorDFluoromethanc
24.6
2.D
uglL
20.0
ND
123
17-191
1,2-Dieh1ombcnzcne
19.9
2.0
ugiL
20,0
ND
99
18-190
1,3-Diehlorobcnzcne
20,6
2.0
ug/L
20.0
ND
103
59-156
1.4-Dialdorobenzene
203
2,0
UW1
20.0
ND
101
18.190
1,2,4-Trichlorobcnzcnc
20.5
2.0
qil-
20.0
ND
102
60.140
PO Box 5655 I Greenville, SC 29606 1426 Fairforest Way I Greenville, 5C 29607 1 main 664.232.1556 1 fax [phone] rogersandcalICOtt.CO1T1
an employee -owned company
03 07/2014 08:11 This reporl rnam hnl he reprnriocrd, e.rcepl infill, withmrr wrirren perrni.%sirrn frrnn Hogerts et- Collcon, Inc.
Pagel 0 30

Rogers &Cakott
ENVIRONMENTAL
Environmental Testing Solutions I'roject: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville, NC 288014310 Reported: 03/07/14 08.11
Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD limit Flags
Batch 84BO820 - EPA 5030
Matrix Spike(R00820-MSI) Source:4020511-02
cis-1,3-lliehloropropene
21.0
1.0
ugfL
20.0
ND
105
3-200
tws- 1,3 -Dichlompropene
21.2
1.0
uglL
20,0
ND
106
17-183
Surragd1e:1,2•Dichloroefhane-D4
102
70-130
Setrragatc:4-Nrnnm/henrahenzene
10
70-130
Surmg(fler TnhwRe-D8
Il o
7f1-130
Matrix Spike Dup (B41B0820-11SD1) Source: 4020511-02
Benzene
20-7
2.0
ug/l,
20.0
ND
104 _
37-151
4
20
Bromcfotm
19,5
2.0
uglL
20,0
ND
97
45.169
2
20
Carbon tetrachloride
19,9
2.0
ug/L
20,D
ND
100
70-140
3
20
Chlorobcnzcne
19.7
2,D
ug/L
20.0
ND
99
37.160
5
20
Dibromachloromcthanc
20,0
2A
ug/L
20.0
ND
)00
53-149
2
20
Chlornethene
20.9
2,0
UO-
20,0
N❑
105
14-200
3
20
2-Chloroethylvinyl ether
15.4
5.0
ngiL
20.0
ND
77
3-200
3
20
Chloroform
20.4
2.0
nWL
2D.D
ND
102
51-138
6
20
8ramodiehloromethane
19.4
2.0
uglL
200
ND
97
35-155
5
20
I,1-Dichlorocihene
19-7
2.0
ug/L
20.0
ND
92
59-155
2
20
1,2-Dichloroethanc
18.8
2.0
uSIL
20.0
ND
94
49.155
2
20
Iran®-1.2-Diehloroethene
19,8
2.0
11gfL
20.0
ND
99
54.156
1
20
1,1-Dichloroethcnc
20.4
2.0
ugiL
20.0
ND
99
3-200
5
20
1,2-lliehloropropene
17.6
2-0
ug/L
20.0
ND
88
3-200
0.1
20
Ethylbenzene
22.8
2.0
ug/L
20.0
ND
114
37-162
6
20
Bromomohnne (Methyl Bromide)
21.4
2.0
ug/L
20.0
ND
107
3-200
0.3
20
Chloromethane (Methyl Chloridel
29.6
2.0
ug/L
20.0
ND
143
3-200
3
2D
1.1,2,2-Tetrachlomcihanc
22.0
2.0
ug/L
20.0
ND
110
46.157
0.7
20
Tetraehlowefhcne
21.4
2.0
ugiL
20.0
ND
107 '
64.148
9
20
Toluene
22.1
2.0
ug/L
20.0
ND
110
47-150
8
20
1,1.I-Trichlorocthene
20.7
2.0
ugiL
20.0
ND
99
52-162
6
20
1,1,2-Triehloroethanc
20.6
2.0
ug/L
20.0
ND
103
52-150
3
20
Trichloroethene
19.0
2.0
ug/L
20.0
ND
95
71-157
5
20
Vinyl chloride
23.0
2.0
ug[L
20.0
ND
115
3.200
3
20
Dichlorodifluoromethane
26.1
2.0
ug/L
20.0
ND
130
60-14D
8
20
Methylene Chloride
19.2
2.0
uglL
20.0
ND
96
3-200
5
20
Trichiorofluoromethime
23.8
2.0
uglL
20.0
ND
119
17-181
4
20
1.2-Dichiorabenzene
19.8
2.9
ugiL
20.0
ND
99
78-190
0.2
20
1,3-Dichlorobenzene
20.1
2.0
ug/L
20.0
ND
101
59.156
_
20
PO Box 5655 I Greenville,
SC 29606 l 426 fairforest Way
I Greenville,
SC 29607 1 main 864.232.1556
l
fA- 864.232.6140
rogersandcallcoct.eom
an employee• -awned company
0,0712014 08:11 This report mqv not he rrproduced, except in full, n ifhaut w'riRen permis.rinn fmrn kagere d• Cullcoff, Inc.
rPage 17 of 30

Rogers & Cakott
ENVIRONMENTAL
Environmental 'Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asbcville, NC 28801-4310 Reported: 03/07/14 08:11
Volatile Organics
Quality Control Summary
Reporting Spike Source %AEC RPD
Parameter Result Limit Units Level Result %AEC Limits RPD Limit Flags
Batch B4B0820 - EPA 5030
diatrix Spike Dup (B460820-MISPI) Source: 4020511-02
1,4-Dichlorobenzene 19.5
2.0
uglL
20.0
ND
97
19-190
4
20
1,2,4-Trichlorobenmric 20,5
2.0
uglL
20.0
ND
102
60-140
0.1
20
cis.1,3-Dichlornpropene 20,2
1.0
uglL
MO
ND
101
3-200
4
20
trans-1,3-Dichloropropene 2.0.8
1,0
uglL
20.0
ND
104
17-IV
2
20
Surrogate: 1,2-Dicchlornethune-DJ
103
70-130
Surrogate: a-Bronrr+fluornhenzene
105
70-130
Surrognie: Toluene -DM
113
70-130
Batch B4C0096 - EPA 5030
Blank (134C0096-BLKI)
Acrolcin ND
5.0
ug1L
Acrylanilrile ND
5.0
ugll.
.Surmgare: 1,2-Dichloroerherne-D4
1Y3
70-130
Surrogate: Toluene-D8
95
70-130
Nurrogate: 4-Rrumafluurohenzene
1 f11
70-130
LCS (64C0096-BSI)
Acrolcin 92,6
5.0
uglL
100
93
91.8-108
Acrylonitrile 19.3
5.0
uglL
20,0
97
814-119
Surrogare:1,2-Dwhloroerhune-Da
94
70-130
,Surrogate: Toluene -DR
106
70-130
Surrogate:4-Rrumnfluurnhenzene
102
70-130
LCS (MC.0096-BS2)
Acrolcin 98.4
5.0
ug/L
100
98
9I.9-I08
Acrylonilrile 19.2
5.0
nglL
20.0
96
82.4-118
.Surrogate: 1.2-Drehlor'aerherne-De
97
71)-13f1
Surrogate: Tohiene-D8
104
70-130
Surrat•rrte: -0-RrnnurJlnaruheruene
101
70-130
Matrix Spike (B40096-MS1) Source: 4020675-04
Acrolcin 102 5.0 uglL 100 ND 102 88-I18
Acrylonitrile 19,0 5.0 aglL 20.0 ND 95 71-135
Surrogate; 1, 2-Dirhh+roethane-Da 104 70-130
Surrogate:7niteene-D8 112 70-130
Surrugair: 4-8romofharroherizene 108 70-130
PO Box 5655 l Greenville, SC 29606 1 426 Fairforest Way I Greenville, 5C 29607 1 main 864.232.1556 1 fax [phone] rogersandcall cott.eom
an employee -owned company
03+0712014 08:11 7hia reporl miry not he reprodmed,, _excepr in,full, a irhnat u riftcn perrnir,rian front knfirrr rC t:allcorr, Inc.
Page 18 0 30

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville, NC 29801-4310 Reported: 03/07/14 08:11
Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4C0096 - EPA 5030
Matrix Spike I)up (B400096-NISDI) Source: 4020675-04
Acrolein 109 5.0 u&fL too ND 104 89.118 7 20
Acrvlonitrile 20.8 5.0 ug/L 20.0 ND 104 71-135 9 20
,1'rrrrogure; 1,?-1)rchl0r0elhunr-1)4
Rurrngalc: Toluene -UK
Surrogole; 4-Bronug1luorobenzene
104 70-130
104 70-130
102 70-130
PO Box 5655 1 Greenville, SC 29606 i 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandeallcott.COm
an employee -owned company
03,0712014 08:11 !'his report may nor he repreuluced except in hull, %irhnut written pennixrion from kngerr & Callcon, Inc.
Page 19 of 30

Rogers & Callcott
ENVIRONMENTAL
Environmentai Testing Solutions Project: Pentair Valves
351 Depot St, Work Order: 4020675
Asheville. NC 288014310 Reported: 03/07/14 09:11
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source %REC RYD
Parameter Result Limit Units Level Result % REC Limits RPD Lirnit Flags
Batch 04BO693 - EPA 625
Blank (B4B(1693-BLK1)
2-Chlorophenal
NO
5.00
ug1L
2,4-Dichlorophenol
NO
5.00
ug/L
2,4-Dimethylphenol
ND
5.00
ug/L
2 ;MtLhvW,6-dinitrophcnol
ND
5.00
ug/L
2 4-Dinitrophenol
ND
5.00
ug/L
2-Nitrophenol
ND
5.00
ug1L
4-Nitrophenol
ND
5.00
ug1L
p-Chloro-m-cresol
ND
5A0
ngfL
Pentachlnrophenol
ND
5.00
ug/L
Pbenol
NO
5.00
ug/L
2,A,6-Triohlor0phenul
NO
5.00
ug/L
Acensphthene
ND
5.00
ug/L
Acenaphthylene
ND
5.00
ug/l-
Anthracenc
ND
5.00
ug/L
Beiivdine
ND
50.0
ug/L
Benzo(alanthracene
ND
5.00
ug/L
Benzo(alpyrene
NO
5.00
ug/L
Henzo(b)iluoranthene
NO
5,00
ug/L
Sanzo(g.hJ)PCrylene
NO
5.00
uglL
Benzo(kllluoranthene
NO
5.00
ug/L
Ais(2-chlorocthoxy)Mcthanc
NO
5.00
ugil.
l3is(2-ehlaroethyl)Ether
ND
5.00
ugll-
bis(2-Chlaroisopropyl)ether
ND
5,00
ug/L
Bis(2-ethylhexyl)Ph1halatc
NO
5.00
ug/L
4-13rmnophenylphenyl ether
NO
5.00
ug/L
Butylben2VIphthalate
NO
5.00
ug/L
2-Chloronaphthalene
ND
5.00
ug/L
4-Chlorophenylpheny) ether
NO
5.00
ug/L
Chrysene
NO
5 00
ug/L
Dibvnzo(a,h)anthracene
NO
5.00
ug/L
3Y-Dichlurobenzidine
NO
5.00
ug/L
Diethylphthalate
NO
5.00
uglL
Dimethylphihalate
ND
5.00
uglL
Di-a-buhdphihalate
NO
5.00
ug/L
2,4-Dinitrotoluene
ND
5.00
u91L
PO Box 5655 1 Greenville. SC 29606 1 426 Fairforest May I Greenville, 5C 29607 I main 864.232.1556 I fax 864,232.6140 rogerSandcallcott.com
-- ---- an employee-Dwned company
03,0711014 08:11 Thii rrport rnuv nor he reproduced, ercepi in fill, N ithour wrinen permusion from Rogem A CaRvoir, Inc.
Page 20 of 30

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Girder: 4020675
Asheville, NC 28901-4310 Reported: 03107/14 08:11
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source %REC RFD
Yarameter Result Limit Units Level Result % REC Limit$ RPD Limit Flags
Batch B4B0693 - EPA 625
Blank (B4B0693.BI,k 1)
2,6-Dlmlrotolmrtc ND
5.00
ug/L
Di-n-ocNlphthalale ND
5.00
agll-
1.2-DiphenvlhydrazeneIAzobenzene) ND
5.00
ug/L
Fluoranthene ND
5.00
uglL
Fluamne ND
5.00
ug/L
Ifexachlorobenzene ND
5,00
ug/L
Hexachlombwadiene ND
5A0
ug/L
Hexachlorocyclopentadiene ND
5.00
ug/L
llcxachlorocthanc ND
5.00
uga,
lndcno(1,2,3-cd)p5,nrne ND
5.00
ng/l.
Isophorone ND
5_on
ug1L
Naphthalene ND
5.00
ug/L
Niuobenzcne ND
5.00
ug/L
N-Nilmso-di-methylamine ND
S."
ug/L
N-Nitroso-di-n-propylamine ND
5.00
ayll.
N-Nitrosudiphenvlamine(Diphenylmnine) ND
5.00
ug/L
Phenanthrene ND
5.00
ug/L
PyTcnc Nil
5.00
ug/L
Surrogate: Sirrohen_rne-D5
Q
35-114
Surmgarr:2-Nvornhiphenvl
83
33-116
574rruxafe: Tcrphen0.1)14
62
33.141
Surrogate: 2-Fhrorophenal
54
21-110
.Surrogate: Phenol -US
38
10410
.Surrogate: 2,4,5-Trrhrmnnphenn1
83
1f1-123
LCS (B4Bp693-BSI)
2-Chlnrophcnol
763
5.00
ug1L
100
76
23-134
2,4-Dichlorophenol
80.8
5.00
us&
100
81
39.135
2.4-Dimethylphenol
82,6
5.00
ug/L
100
81
32-119
2-Mcthvl-4.6-dinitrophenoi
102
500
ug/L
too
IV
1-181
2,4-Dinitmphcnol
93.0
5.00
ug/L
100
93
1-191
2-Nitrophenol
85.0
5.00
ug1L
100
85
29-182
4-Nitrophenol
41A
5.00
ug/L
100
41
1-132
p-Chlorn-m-crc3ol
93.1
5.00
ug/L
100
93
22-147
Peniachlorophenol
93,2
500
ugfL
100
93
14-176
Phenol
39.6
5.00
ug/L
100
39
5.112
Po Box 5655 1 Greenville, SG 29606 1 426 Fairforest Way I Greenville,
SC 29607
1 main 864.232.1556
1 fax [phone] rogersandcallcott.eom
an employee -owned company
03,07/2014 09:11 This repan miry unr he reproduced,, ervepi in fall, %ithour wriuert penni monfmm Rngem d Callcnrr. Inc.
Page 21 of 30

Rogers & Cakott
ENVIRONMENTAL
Environtnenlal Testing Solutions Project: Pentair Valves
351 Depot St, Work Order: 4020675
Asheville, NC 28901-4310 Reported: 03/07/14 08:1 1
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source '/ k E C RFD
Parameter Result Limit Units Level Result %REC Limits kl'D Limit Flags
Batch B41B0693 - EPA 625
LCS (MB0693-BSI)
24,6-Trichlorophenol
97.4
5.00
uglL
too
97
37.144
Acenaphthene
89,4
5,00
u84-
100
89
47-145
Acennphthylene
82.5
5,00
ug/L
100
82
33-145
Anthmcene
99.1
5,00
ug/L
100
88
27-133
Benzidine
176
1.00
ugA-
5D0
35
1-139
Renzo(a)anthracene
89.7
5.00
ug/L
100
90
33-143
Benzo(a)pyrene
93.3
5.00
ug/L
Wo
93
17-163
Henzo(h)Fluotanihone
92.4
5,00
ug/L
100
92
24-159
Benzo(0.0mylene
90.5
5,00
ug/L
too
90
1-200
Bcnzn(k)1111oramhcnc
48.8
5.00
ug/L
100
99
11-162
Bis(2-chlorocthanyl4kthanc
99.0
5.00
ug/L
100
99
33-I84
Bis(2-610roothyl}Ether
84,2
5.00
ug/L
100
84
12-158
bis(2-Chlaroisopropyl)ethei
89,6
5,00
ug/L
100
90
36-166
Bis(2-e1hy1hcxy1)Ph1ha1ste
84.1
5.00
ng/L
too
89
8-158
4-Bromoplwnylphony)ether
99.0
5.00
u8/L
too
99
53-)27
Butylbenzylphthalaie
92.3
3.00
ugfL
wo
92
I-152
2-Chloranaphthalene
811.5
5.00
ug/L
100
89
60-118
4-Chlorophenylphenylether
103
5.00
uglt,
100
103
15-158
Chrysene
92.2
5.00
ug/L
too
92
17-168
Dibenra(a,h)anthracene
88.3
5.00
uglL
too
88
1-200
3,3'-Diehlorobenzidine
73,4
5.00
ug/L
100
73
1-200
Diethylphthalate
91.6
5.00
uglL
100
92
1-114
Dimethylphthalate
92.5
5.00
ug/L
100
92
1-112
Di-n-burylphihalate
85.2
5.00
ug/L
100
85
1-11$
2,4-Dlnitra101vene
91.4
5.00
ug/L
100
91
39-139
2,6-Dirdtrotoluene
88.8
5.00
ug/L
100
89
50-158
Di-n-octydphthalate
85.1
5.00
uBIL
100
85
4-146
1,2-Diphenylhydrazene(Aznbenzenc)
89.3
5.00
ug/L
100
89
65-130
Fluoranthenc
99.2
5.00
ug/L
Wo
98
26.137
Fluorcnc
92.1
5.00
ug/L
100
92
59.121
Hexachlorobenzene
89.3
5.00
ug/L
Wo
89
1-152
Hexachlowbutadicne
77.0
5.00
ug/L,
too
77
24-116
Hexachlaracyclopentadiene
91.5
5.00
ug/L
100
82
37-130
Hexachloroethane
75.3
5.00
ug/L
100
75
40-113
Indenn(1,2,3-cd)pyrene
91.1
5.00
ug/L
100
91
1-171
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.614o rogersandcallcott.com
an employee -owned company
03,0712014 ONt I This report mrry not he reproduced, errepr in full, wilbaw wriaten pennission -rim Hogcrr X Calkorl, Inc.
Page 22 a 30
0

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Ashevilie, NC 28901-4310 Reported: 03/07/14 0& 11
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B4B0693 - EPA 625
LCS (B460693-11SI )
lsophorone
83.2
5,00
og/L
100
83
21-196
Naphihalcnc
74.2
5.00
uglL
too
74
21-133
Nitrobenzene
77.4
5,00
ug/L
100
77
35-180
N-Nitroso-di-methylamine
51.4
5A0
ug/L
100
51
30-100
N-Nitroso-di-n-propylamine
85.7
5,00
LVL
too
86
I.200
N-Nitrnsodiphenylamine(Diphenvlamine)
85.2
5.00
ug/L
100
85
60-130
Phenanduene
88.0
5.00
ug/L
100
88
54-120
1')'rene
83.9
5.00
ug/L
l00
84
52-115
Surrogrrrer Mlrohen_ene-D5
87
35-114
Surragme:2-Fluorohiphenyl
94
43-116
Sarrogwe: Terph®nrl-D14
55
33-141
Srrrraprne: 2-1--hiurophcnd
51
21-110
Surrogate: Phenol-D5
38
10.110
Su,rmgaie: 2, 4, 6-Trihromophenol
91
1 f1-123
Matrix Spikt (134110693-i9St) Source: 4020503-04
2-Chlorophenol
139
Mo
ug/L
200
ND
69
23.134
2,4-Dichlorophcnol
140
10.0
uglL
200
ND
70
39-135
2,4-Dimethylpheno]
155
10.0
ugfL
200
ND
78
32-119
2-Methyl-4,6-diniirophenol
186
Wo
ag1L
200
ND
93
I-181
2,4-Dinitrophenol
172
10.0
u8/L
200
ND
86
1-191
2-Nitrophenol
150
10,0
ug/L
200
ND
75
29-182
4-Nitrophenol
76.4
Mo
ug/L-
200
ND
38
1-132
p-Chloro-m-cresol
L64
10.0
ug/L
200
ND
82
22-147
PentaChlorophennl
179
10.0
ug/L
200
N❑
89
14-176
Phenol
66.8
10.0
ug/L
200
ND
33
5-112
2,4,6-Trichlarophenol
173
10.0
1181L
200
ND
87
37-144
Acenaphthene
162
10.0
Ug/L
200
ND
81
47-145
Acenaphthylene
151
10.0
ug/L
200
ND
76
33-145
Anihracene
158
10.0
ug/L
200
ND
79
27-133
13enzidine
109
2.00
ug/L
1D00
ND
11
1-139
Benzo(a)anthracene
160
10.0
ug/L
200
ND
80
33.143
Benzo(a)pyrene
164
10.0
ug/L
200
ND
82
17-163
Rcnzo(b)fluoranthene
167
10.0
ul;IL
200
ND
83
24-159
Bcnzo(g,hj)perylene
161
10.0
ug/L
200
ND
81
1-200
Benzo(k)0uoranihene
171
10,0
vg/L
200
ND
86
II-162
PO Box 5655 I Greenville, SC 29606 1 426 Fair -forest Way
I Greenville,
SC 29607
I main 864.232.1556
1
fax [phone]
rogersandealleott.eom
an employee -owned company
03,0712014 08:11 This report niay nnr he reprodwed,, excapr in fudl, u ilhaur »riven pennia.rinn from Rugera & Cancan, Inc,
Page 23 of 30

I
Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville, NC 28801-4310 Reported: 03/07/14 08:1 1
Semi-Volatiles Organics
Quality Control Summary.
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD limit Flags
Batch B4BO693 - EPA 625
Matrix Spike (134130693-1151) Source: 4020503-04
•
Sis(2-chloroethaxy)Me1hane
167
10.0
uglL
200
ND
83
33-184
Ris(2-chlornethyl)Fther
150
10.0
ug/L
200
ND
75
12-158
bis(2-Chiumisopropy))cthcr
165
10.0
ug/L
200
ND
82
36-166
Ris(2-ethylhexyl)Phthalate
170
10.0
ug/L
200
ND
85
8-158
4-13rontophenylphenylether
182
10.0
ug/L
200
ND
91
53-127
Rutylbenzylphthalate
170
10.0
ug/L
200
ND
85
1-152
2-Chloronaphthalene
159
10 0
ug/L
200
ND
80
60-118
4-Chlorophenylphenyle1her
182
10,0
uglL
200
ND
91
25-158
Chrysene
166
10,0
oo,
200
ND
83
17.168
Dihenzn(a,h)anthr=ne
161
10.0
ug1L
200
Ni)
80
1-200
3,3'-Diehlorobenzidine
140
10.0
ug/L
200
ND
70
1-200
Diethylphthalatc
164
10.0
ug/l.
200
ND
82
1-114
Dimethylphthalate
164
10.0
ug/L
200
ND
82
1-112
Di-n-butylphthalate
160
10.0
ug/L
200
ND
so
1-119
2,4-Dinitrotoluene
160
10.0
uglL
2D0
ND
80
39-139
2,6-Dinitrotoluene
156
10.0
uglL
200
N➢
78
50-158
Di-n-octylphthalatc
156
10.0
ug/L
200
ND
78
4-146
1,2-Dipheny1hydrazene(Azobenzene)
160
10.0
ugll.
200
ND
80
65-130
Pluoranthene
175
10.0
ug/L
200
ND
88
26-137
Fluorene
163
10.0
ug/L
200
ND
81
59-121
Hexachlorubenzene
162
10.0
u8/L
200
ND
81
1-152
Hexaehlorobutadiene
137
10,0
ugll,
200
ND
69
24-116
Hexachlorocyclopentadiene
143
I0,0
ug/L
200
ND
72
37-130
Hcxaphloroethane
140
10,0
ug/L
200
ND
70
40-113
]ndcno(1,2,3-cd)pyrcne
164
10.0
ug/L
200
ND
82
I-171
Isophorone
142
10.0
uglL
200
ND
71
21-196
Naphthalene
139
10.0
ug/L
200
ND
69
21.133
Nitrobenzene
135
Mo
ug/L
200
ND
67
35-la0
N-Nitroso-di-methylamine
93.9
10.0
ug/L
200
ND
47
30-100
N-NitrosD-di-n-limpylaminc
153
10.0
ug/L
200
ND
77
1.200
N-Nitrosodiphenylamine(Diphenyltunine) 150
10.0
ug/L
200
N➢
75
60-130
Phenanthrene
162
10.0
ug/L
200
ND
81
54-120
Pyrene
149
10.0
- ugfL
200
ND
75
52-115
Surragare: Nnrnherr_ene-D5
80
35-114
Surrugure, 2-F7noruhiphenyl
82
43.116
.S'lvrogure, Terphenl!-1114
46
33-141
PO Box 5655 1 Greenville,
SC 29606 j 426 Fairforest Way Greenville,
SC 29607 main 864.232.1556
1 fax 864.232.614U
rogersandeallcott.com
an employee -owned company
03,0712014 08:1) Ihis rcpnrr rnuy nn1 he reprndwed, except in,liill, N ithmrr written perrnissinn Jrnnr Rngem & Cullcnrr, Inc.
Page 24 0 30

Rogers & Callcott
ENVIRONMENTAL
Environnienial Testing Solutions Project: Pentair Valves
351 Depot Si, Work Order: 4020675
Asheville, NC 288014310 Reported: 03/07/14 09:11
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units level Result %REC Limits RPD Limit Flags
Batch B4BQ693 - EPA 625
Matriz Spike (B4130693-NISI)
%uree: 4020503-04
Surrngure:2-Fhmrophenol
47
21-110
,Surrogate: Phenol-1)5
33
10.110
,Surm ate: 2,4,6-Tribrumophenol
83
10.123
'
hlalrix Spike Dup (B4B0693-A1SD1) Souree: 4020503-04 .
2-Chlorophenol
130
10,0
ugIL
200
ND
65
23-134
6
30
2,4-Dichlorophewl
132
10.0
ug1L
200
ND
66
39-135
6
30
2,4-Dimethylphenol
154
10.0
ug/L
200
ND
77
32-119
1
30
2-Methyl-4,6-dinitrophenol
195
10.0
ug/L
200
ND
97
1-I81
5
30
2,4-Dinitrophenol
179
10.0
ug/L
200
ND
89
1.191
4
30
2-Nitrophenol
137
10.0
ug/L
200
ND
69
29.182
9
30
4-Nitrophenol
79.1
10,0
ug1L
200
ND
40
1432
4
30
p-Chloro-m-cresol
164
ip 0
ug/L
200
ND
82
22-147
0.3
30
Penrachlorophenul
182
]cc
ug/L
200
ND
41
14-176
2
30
Phenol
60.7
10.0
uglL
200
ND
30
5.112
10
30
2,4.6-Trichlorophenol
174
10,0
ug/L
200
ND
87
37-144
0.4
30
Acenaphihene
163
W o
ug/L
200
ND
82
47-145
0.7
30
Acenaphihylene
152
10.0
ug/l,
200
ND
76
33-145
0,6
30
Anthracene
161
10.0
uglL
200
ND
s0
27-133
1
30
Bruzidine
20)
2.00
ug/L
1000
ND
20
1-139
59
50 P2, Q6
Rcnzo(manthrecene
162
10.0
ug/L
200
ND
81
33-143
1
30
Renzo(alpyrene
167
10,0
ug/L
2D0
ND
84
17-163
2
30
ScnzoWfluoranihene
167
10.0
ug/L
200
ND
83
24-159
U
30
Benzo(g,h,i)perylcne
163
10.0
ug/L
200
ND
82
1-200
1
30
Benzo(k)fluoranthene
175
10.0
uglL
200
ND
88
I1.162
3
30
3is(2-ch t"1hoay)Methnne
155
10.0
uglL
200
ND
77
33-184
7
30
Bis(2-chloroethyl)F-ther
121
10.0
-9fL
200
ND
61
12-158
21
30
bis(2-Chloroisopropyl)dhcr
;39
100
ug/L
200
ND
69
36-166
17
30
Bi5(2-c1hylhexy1)Phthalate
171
10.0
ug/L
200
ND
85
8-159
0.6
M
4-Bromophenylphenyle1her
194
10.0
ug/L
200
ND
92
53-127
1
30
Butylbenzylphthalatc
173
10.0
ug/L
200
ND
86
I-152
1
30
2-Chloronaphrhalcnc
154
10.0
ug/L
200
ND
77
60-118
4
30
4-Chlarophenylphenyleher
197
10.0
ugfL
200
ND
94
25.158
3
30
Chrysene
169
10.0
U91L
200
ND
84
17-168
1
30
Dibenzo(a.h)anthracene
)65
10.0
ug/L
200
ND
83
1-200
3
30
3,Y-Dichlombenzidine
140
10.o
ug/L
200
ND
74
1.2110
6
40
PO Box 5655 1 Greenville, 5C 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 i fax [phone] rogersandCallcott.COm
an employee -owned company
03,OW014 08: 11 This report rmryy not he reproduced, e:aepi infill, ill, u ithold written Imernisriun -orn Rogers .& (.' dIcorf, Inc.
Page 25 of 30

Rogers & CaLlcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot Si. Work [Order: 4020675
Asheville, NC 28801.4310 Reported: 03/07/14 08:11
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source °/ RkC RPD
Parameter Result Limit Units Level Result %REC Limits 101 Limit Flags
Batch B4BO693 - EPA 625
Matrix Spike bap (B460693-NISD1) Source: 4026503-04
Dicthylphthalate 169
10.0
ug/L
200
ND
84
1-114
2
30
Dimethylphthalate 166
10.0
ug/L
200
ND
93
1-112
1
30
Di-a-butylphthalate 156
10.0
ug/L
201)
ND
78
1-119
3
30
2.4-Dinilrololuene 166
10,0
ug/L
200
ND
83
39-I39
4
30
2,6•Dinitrotolucne 158
10,0
ug/L
200
ND
79
50.158
1
30
Di-rrnctylphiholate 155
10.0
ug/L
200
ND
77
4-146
0.6
30
1,2-Dipheny1hydrazene(Azobcnzcnc) 162
10.0
ug/L
200
ND
81
65.130
1
30
Fluoranthene 175
10.0
ug/L.
200
ND
89
26-137
0.07
30
Flumenc 166
10.0
ugll-
200
ND
83
59-121
2
30
Hexachlorobenuna 164
10,0
uga,
200
ND
82
1.152
0.8
30
Hexachloroboadiene 124
10.0
uglL
200
ND
62
24-116
10
45
Hexachiarocyclopenteditne 135
10.0
ug1l.
200
ND
68
37-130
6
45
Hexachlaroethane 132
10.0
ug1L
200
ND
66
40-113
6
45
Indeno11.23-ed)pyrcne 165
10.0
ul/L-
200
ND
82
1.171
0.3
30
Isaphoronc 135
10.0
uglL
200
ND
68
21-1%
5
30
Naphthalene 132
10.0
ug/L
200
ND
66
21-133
5
45
Nitrobenzene 121
10.0
og1L
200
ND
60
35-180
11
30
N Nitroso-di-mcthylamine 86.6
10.0
ug/L
200
ND
43
30-100
8
30
N-Nitrnso-dim-prupylamine 142
10.0
ug/L
200
ND
71
1-200
8
30
N-Nitrosodiphenylamine (Diphenylamine) 151
10.0
ug/L
200
ND
75
60-130
03
30
Phenanthrene 161
10.0
USI
200
ND
81
54-120
0.3
30
pwene - 150
10.0
ug/L
200
ND
75
52.115
07
30
.Surmgure: Niirohenzene-1)5
71
35-114
.Surmgare:2-Fluombiphenyl
79
43-I16
,Surrogate: Terphem0-1)14
43
33.141
Surrogate: 2-Fluamphenol
43
11.110
.Surrogate: Phenol-D5
30
10-1111
,Surrogate: 2.4.6-7'rihrwnr phenol
H5
I0-113
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesc Way I Greenville, 5C 29607 1 main 864,232.1556 1 fay 864.232,6140 rogersandcalleott.eom
an employee -owned company
03,0712014 08JI Yhfr report may nor he repmdnceel, awepr in,0tll, viiihmu wnngnpermfrsion from Retgem ctCallco0, Inc, Page 26 of 30

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depot St. Work Order: 4020675
Asheville, NC 28801-4310 Reported: 03/07/14 09:11
PCBs
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units level Result `/.REC Limits RPD Limit Flags
Batch 8480740 - EPA 608
Blank (B4B0740-BLKI)
PCB-1016
ND
0.50
ug/L
PCB-1221
ND
0.50
ug/L
PCB-1232
NO
0.50
ug/L
PCB-1242
ND
0,50
ugfL
PCB-1248
NO
0.50
ugfL
PCB-1254
ND
0.50
ugfL
PCB-1260
NO
0,50
ugfL
Snrxl;vre: 2,4,S.h-Terrachlnrn-nf rr4rm
90
60-130
SnrrnFure: Drcuchlnrnhiphenf 1
53
30-150
LCS (B4B0740-BSI)
PCB-1016
L92
0.50
ugfL
2.50
77
50-114
PCB-1260
2,12
0,50
ugfL
2.50
85
9-127
Surrergare.• 2,-i,5,6-Terruchlarrr-nr-ndene
55
60-130 R
Snrrogaw Uerachirwobiphem4
74
SO-150
LCS Dup (B4B0740-BSDI)
PCB-1016
2.12
0,50
uglL
2150
85
50-114 10 20 ,
PCB-1260
2.29
0.50
ugfL
2.50
91
8-127 7 20
Sumgait; $4,5.6-Trrrachlora-m-.n4one
74
60430
Surrrxarr: Drcac1lnrnhrphrn0
72
30450
Sample Preparation Data
Parameter 8ate6 Sample ID Prepared Analyst
EPA 200.7 Metal Digestion
EPA 200.7
B4B0705
4020675-01
02/24/2014 16:29
MEC
EPA 200.7
134RO705
4020675-03
02/24/2014 16:29
MEC
EPA 608 Extraction
EPA 608
BQ0740
4020675-01
02/25/2014 10:00
DBB
EPA 608
B4130740
4020675-03
02/25/2014 10:00
DBB
EPA 625 Extraction
EPA 625
B4130693
4020675-01
02/24/2014 09:00
DBB
EPA 625
R4130693
4020675-03
02/24/2014 09:00
DBB
PO Box 5655 1 Greenville, SC 29606 1426 Fairforest Way I Greenville, SC 29607 1 maln 864.232.1556 I fax [phone] rogersandealleott.eom
a i employee -owned company
03,07/2014 08:11 This rep wi wqv prat he reproduced. excepr in fr+ll, m irhow wriffen perrpri.%sion franc Rogers & Callcmr, 1nc.
Page 27 of 30
a

'[&7
Rogers & CaRcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair Valves
351 Depol St, Work Order: 4020675
Asheville, NC 28801-4310 Rcportcd: 03/0V14 08:11
Data Qualifiers and Definitions
ND Analyte NOT DETECTED at or above the reporting limit
NR Not reported
RPD Relative Percent Difference
P2 The RPI) result exceeded the control limits; however, both matrix spike recoveries were within control limits.
Q6 Benzidine is an unstable compound which is subject to oxidative loss and variable recovery, daring solvent concentration.
R The surrogate was not -Aithin quality control limits.
S 1 The matrix spike and 1 or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. The
Laboratory Control Sample (LCS) was within control limits.
PO Box 5655 1 Greenville, 5C 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.614U rogersandcallcott.eom
an employee -owned company
03,0712011 08:11 This reporr may not he mpmduced, eraepf in hdl, wthow a raren perrnissinn fmm Roger., & Caillcon, Inc.
.Page 28 of 30

r
ROGERS & 4LDCUrT
JABORATORY SERVICES
P.O. Box 56SS, G7eetM'ie, SC 296M
Phc,n (H64( 232-1556 Fax [phone](40
®
Shipping Address: 426 Fakforest Way
Greewile, SC 29607
Gient Name
Address
�t
Report To:
Telephone No,
tom% t0 No.
Rogers do yr`
Callcatt Time
Lob No. Dote
ff �'
in, �a
SAMPLER
©lirvqu+' shed by (Sig.)
Y_ E
Relin b
fl C..
Relinquished by (Sig.)
5eo! #� at'ehd
Form Revised July 2008
FAX No.
Project No.
Sample Description
Date/rime
Received by (Sig.)
Shipper
ante%lime
® Sig.
Shipper a �!
Date/Time
Received (Sig.
C
hipper Nam dt
Recvd. Intoct b
Seal # at'
CHAIN OF CUSTODY RECORD PAGE or -
Date/Time
0270H P
q e,,ime
I 4� 1 A 0
Date/Time
Recvd. Intact by
Filtered (Yes
Calved es a} ,
Container Type �
Container Volume vWIA,Uj)
Sample Type rob omposite)
Sample Source WW, GW, DW, Other)
Sample Source Chlorinote (Yes/No)
Lab Receipt CI, Chec 341 i
Lab Receipt pH Check
Preserved (Code)
A -Neva 0-1400H G-Bork Acid
B-HNQ, E-HCL H-Ascorbic Add
C-Hr50, F-.Na,5,0, S-
COMMENM-
PenfO-4.4. VOA V e
w
KNM HAZARDS ASSIMA7® WTH SAWPLE5
Temperature of blank or representative sample
At time of collection G
At time of lab receipt "C
i
R C COC FORA

Rogers & Callcott
ENVIRONMENTAL
Sample Receipt Verification
Date /. Work
Client: Received: L/ !/ I Order:
Carrier Name: Client Fed UPS US Mail Courier Field Services Other:
Tracking Number: ZZ —1 0
14
Receipt Criteria I
Y
e
s
o
A
Comment%
Shipping container/ cooler intact?
Damaged Leaking Other:
Custody seals intact'?
COC included with samples?
COC signed when relinquished and received?
Sample bottles intact?
Damaged Leaking Other:
Sample ID on COC agree with label on bottle(s)?
Date I time on COC agree with label on bottle(s)?
Number of bottles on COC agrees with number of bottles received?
Samples received within holding time?
Sample volume sufficient for analysis?
VOA vials free of headspace (<&mm bubble)?
Satrapies cooled? lc'np at receipt recorded on COC
'romp measured with IR thermometer - SN- 97050067
Ice Cold Packs Dry Ice None
Samples requiring pH preservation at proper pl-I?
Note: Samples ror metals analysis may be preserved upon receipt in the lab.
E t
If in-house preservation used — record Lot #
HCL
H,PO4
H,SOa
NaOH
HNO,
Other
Comments:
Were non-conformance issues noted at sample receipt? Yes or No %
Non -Conformance issue:
Revisad November 2012 Completed by:

C.
Y
0 �.
o
0
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Proiect Name.- 'C-g-!A rC f TM t✓r�y✓ _ _
CHAIN -OF -CUSTODY 1 Analytical Request
Client Name: rzf J-4ziz. V VE!5
Address: 9<--3 old ue, ,�% ,� 70
Report to: �� (� 14L, e-r-.5
Phone: Fax:
PO Humber:
Re„urcteri Anahses
Project Number:
pH Checked Upon Receipt
CIt < 0.2 nio Upon Receipt
Preservatives
Sample Identification
`'
L
F:
s
_
L
�
O G
e
f
S
o
c
O
O
rZj
U
Field
n
n-
c S
"=
s'
z
I=
Iz
Iz
Temp. ("C) Comments
O
�'
Jet ,
��`r �:� t
I # 3
3°
}`
2-
v�
C,
id 7.
.Swinple Condition
Upon ,B
Temperature (C)
S . 3
FfMI }
b31
Omko
Received on Ice:
Y / N
Sealed Cooler:
Y /
Samples Intact:
Y / N
Additional Comments:
Printed Name of Sampler:
�+�y
Signature of Sampler:

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted ,February 18, 2014
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls_
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Environmental Testing Solutions Lab Cert. #600rng/L
Comments on sample collection or analysis: See page 4
part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2014
SAMPLE PERIOD ® Jan June ❑ July -Dec
or ❑ Monthly' January (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply []SA
®Other: Class C, Swannanoa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?2
Outfall No.
Date Sample
Collected4
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics3
Benchmarks =-_>
-
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
` 1
01-10-2014
0.52
34 mg/L
7.2
0.10 mg/L
<0.020
.16 mg/L _
<5.0 mg/L
BRL
2
01-10-2014
0.52
8.2 mg/L
6.9
0 mg
<0.020
0.16 mg/L
<5.0 mg/L
BRL
----------------------
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4Aee General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals; or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.1.1; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
z/V7 /ZO/Lf
Permit Date:11/1/2012-10/31/2017
F E 8 2 4 2014 Y:
! _n,; i, j f _►ality Sec lon swu=245, last revised 10/25/2012—,
Page 1 of

-'.Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the stormwater Pollution Prevention Plan."
Sal Vaccaro
Name (Print name)
General Manager
Title (Print title)
(Signature) (bate)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period:
Outfall Na.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit -Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
I}
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART li SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAd 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO 0
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within_30 days of receipt -of -the lob results (or at end of monitoringyeriod
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penafty'of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are `sign'ificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permitteey
( Date)
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 4

;1) Copper reporting value exceeds permit limit 0.007 for Outfall #1
a). Finding;
i) Roofing material is 10 years old in the sample area and could be a contributing factor for both outfall sampling points.
ii) Scrap Lugger pad could be a contributing factor for outfall 41
b) Corrective actions;
i) Review BMP's,
ii) • Increase housekeeping, Lugger Pad Area to be inspected weekly.
2) Zinc reporting value exceeds permit limit 0.067 for outfall #1
a) Finding;
i) Scrap Lugger pad could be a contributing factor for outfall 41 and #2.
b) Corrective actions;
i) Review BMP
ii) Increase housekeeping, Lugger Pad Area and Center Pad to be inspected weekly.
Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012
Page 4 of 4

Mrs PO Box 7565
O Asheville, NC 28802
Phone: [phone]
Q :y} Fax: [phone]
Q
Environmental Testing Solutions, Inc. Certificate of Analysis
Project name: Pentair Project number: 140110.500
Collection date: 10-Jan-14
Date received: 10-Jan-I4
Sample identification: Outfall #1 Sample number: 112733
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
624
624 - 8260 B
See Attached Sheet
µglL
15-Jan-14
LBW 1
625
625 - 8270 D
See Attached Sheet
ug/L
21-Jan-14
RJM 1
608
608
See Attached Sheet
pg/L
i7-Jan-14
RKH 1
Solids, Total Suspended
SM 9222-D
34 5.0
mg/L
15-Jan-14
KW
Oil & Grease, Totai HEM
1664 A
<5.0 5.0
mg/L
i5-Jan-14
CTS 1
Copper
200.7
0.10 0,005
mg/L
15-Jan-14
MER 1
Zinc
200.7
0.16 0.010
mg/L
15-Jan-14
MER 1
Lead
200.7
<0.020 0.020
mg/L,
15-Jan-14
MER 1
Sample identification: Outfall #2
Sample number: 112734
Parameter
Method
Result RL
Units
Date
Analyst Footnotes
Analyzed
624
624 - 8260 B
See Attached Sheet
pg/L
15-Jan-14
LBW I
625
625 - 8270 D
See Attached Sheet
}tg/L
21-Jan-14
RJM 1
608
608
See Attached Sheet
pg/L
17-Jan-14
RKH 1
Solids, Total Suspended
SM 9222-D
8.2 5.0
mg/L
15-Jan-14
KW
Oil & Grease
1664 A
<5.0 5.0
mg/L
15-Jan-14
CTS 1
Copper
200.7
<0.005 0.005
mg/L
15-Jan-14
MER 1
Zinc
200.7
0.016 0.010
mg/L
15,1an-14
MER 1
Lead
200.7
<0.020 0.020
mg/L
15-Jan-14
MER 1
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only,
1. Sample analyzed by Rogers & Callcott Environmental.
Date reviewed: -Z, .1 NC Certification Number: 600
Data reviewed by: _ Kelley E. Keenan SC Certification Number: 99053
Signature: NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc
The results in this report relate only to the samples submitted for analysis,

Rogers &Callcott
ENVIRONMENTAL
Client Environmental Testing Solutions
Kellev E. Keenan
351 Depot St,
Asheville, NC 28801-4310
Dear Client:
Laboratory Report
Project:
Work Order:
Received:
Laboratory Services
Pentair
40)0496
01/14/2014 09:20
Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of
custody for samples that were received on January 14, 2014. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all
analyses performed under NELAP certification have complied with all the requirements for the NELAC standard. The analyses met the QAIQC
confidence interval for each test method unless otherwise qualified. Fstimated uncertainty is available upon request.
Privileged 1 Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. Ifyou receive this message by
mistake, please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients. Please contact Amy Ashley, your Project Manager, at amy.ashley 041 rogersandcailcott.com or
(864)-335-4962 ifyou have any questions about this report.
Report Approved By:
Amy Ashley
Project Manager
This repnrr may nni he reproduced. awepl infill. wuhour wrnten permission rum Rngcrs & Callonrr. Me.
PO Box 5655 1 Greenville, SC 29606 1426 iairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone]
rogersandcal Icott.com
an employee -owned company
Page 1 of 27

Rogers & Callcott
ENVIRONMENTAL
Certificate of Analysis
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville- NC 28801-4310
South Carolina Laboratwy Identification 23105
South Carolina Mobile Lab Identification 40572
North Carolina Laboratory Certification Number 27
NELAP Laboratory Identification E87822
Project: Pentair
Work Order: 4010496
Received: 01/14/2014 09:20
Sample Number
Sample Description
Matrix
Sampled
Type
4010496-01
Pentair Outfall 41 - Grab
Other
01/10/ 14 09:30
Grab
4010496-02
Pentair Outfall#1-Grab
Other
01/10/14 09:30
Grab
4010496-03
Pentair Outfall 42 - Grab
Othcr
01/10/14 09:40
Grab
4010496-04
Pentair Outfall #2 - Grab
Other
01/10/14 09:40
Grab
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest V�ty I Greenville, SC 29607 I main 864.232,1556 1 fax 864.232,6140 rogersandcallcott.COm
an employee -owned company
0112NI2014 11:04 This report inirt nor.he reproduced, e.rcepi in,firtt, Nithoet writlen pernnissir,n,frnni knger.r & Cullcmi Inc.
Page 2 of 27

Rogers & Cakott
ENVIRONMENTAL
Environmental 'resting Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville. NC 28801 4310 Reported: 01128/14 11:04
Sample Data
Sample Number 4010496-01
Sample Description Pentair Outfall 41 - Grab collected on 01/10/14 09:30
Parameter
Result
Reporting
Limit
Units
DF
Analyzed
Method
Flag Analyst
Batch
General Chemistry Parameters
Oil and Crease, Total, HEM
ND
5.0
mg/L
i.00
01115/14 08:00
EPA 1664A
CT5
B4A0433
Total Metals
Copper
0.10
0,003
mg/L
1.00
01/15/14 12:24
EPA 200.7
MER
H4A0400
Lead
ND
0.020
ms1L
1.00
01/15/14 12:24
EPA 200.7
MER
B4AO400
Zinc
0.16
0,010
mg/l.
1.00
01115/14 12:24
EPA 200.7
MER
134AO400
Volatile Organics
Benzene
ND
2.0
ug/L
1.00
Ol/15114 16:32
EPA 624-8260B
LBW
B4AO763
Bromoform
ND
2.0
ug/L
1.00
01/15/14 16:32
EPA 624-B260B
LBW
B4AO763
Carbon tetrachloride
ND
2.0
ug/L
1.00
01/15/14 16:32
EPA 624-8260B
LBW
134A0763
Chlorobenzene
ND
2.0
ug/L
1.00
O1/15114 16:32
EPA 624-8260B
1.BW
B4AO763 `
Dibromochloromethane
ND
2 0
ug/L
1.00
01/15/14 16:32
EPA 624-6260B
LBW
134A0763
Chloroethane
ND
2.0
ug/L
1.00
Q1f15/14 16:32
EPA 624.8260B
LBW
B4AO763
2-Chloroethylviny) ether
ND
5.0
uglL
1.00
Oi/15114 16:32
EPA 624.8260E
LBW
114A0763
Chloroform
ND
2.0
ug/L
1,00
01/15/14 16:32
EPA 624-82608
LBW
B4AO763
Bromodichloromelhane
ND
2.0
u611.
1.00
01/15/14 16:32
EPA 624-9260B
LBW
B4A0763
1.1-Dichloroethane
ND
2.0
ug/L
1.00
01/15/14 16:32
EPA 624-92608
LBW
B4AO763
1,2-Dichloroathane
ND
2,0
U9fL
1,00
01/15/14 16:32
EPA 624.8260E
LBW
134AG763
trans-1,2-Dichloroe:thene
ND
2.0
ug1L
1.00
01/15/14 16:32
EPA 624.8260E
LBW
B4AO763
l,l-Dichloroethene
ND
2.0
uWL
1.00
01/15/14 16:32
EPA 624-8260B
LBW
B4AO763
1,2-Dichloropropane
ND
2.0
ug1L
1.00
01/15/14 16:32
EPA 624.8260B
LBW
B4A0763
Ethylbenzene
ND
2.0
o61L
1,00
01/15/14 16:32
EPA 624.8260E
LBW
B4A0763
Bromomelhane (Methyl Bromide)
ND
2.0
ugfL
1.00
01/15/14 16:32
EPA 624.8260E
LBW
134AO763
Chloromethane (Methyl Chloride)
ND
2.0
up/I.
1.00
01/15/14 16:32
EPA 624.8260E
LBW
134AO763
L1,2,2-Tetrachloroethane
ND
2.0
uWL
1.00
01/15/14 16:32
EPA 624.8260E
LBW
B4AO763
Tetrachloroethene
N❑
2.0
ug/L
1,00
01/15/14 16:32
EPA624.8260B
L13W
134A0763
Toluene
ND
2.0
ug/L
1.00
01/15114 16:32
EPA 624.8260E
LBW
B4A0763
LLt-Trichloroethane
ND
2.0
ur/L
1.00
01/15/14 16:32
EPA 624-8260B
LBW
B4A0763
L1,2-Trichloroethane
ND
2.0
ug/L
1.00
01/15/14 16:32
EPA 624-8260B
LBW
B4A0763
Triehloroethene
ND
2.0
ug/L
1.00
01/15/14 16:32
EPA 624.8260E
LBW
B4AO763
Vinvl chloride
ND
2.0
ug/L
1.00
01/15/14 16:32
EPA 624-8260B
LBW
B4A0763
Dichlorodifluoromethane
ND
2.0
uWL
1.00
01/15114 16:32
EPA624.8260B
LBW
B4AO763
Methylene Chloride
ND
2.0
utJL
1,00
01/15114 16:32
EPA 624.8260E
LBW
B4AO763
Trichlorofluoromethane
ND
2.0
utJL
1.00
01/15/14 16:32
EPA 624.8260E
LBW
B4AO763
PD Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main, 864,232,1556 1 fax [phone] rogersandcallcott.com
an employee -owned company
01/28/1014 11:04 1hra report may nor he reproducers, ereepr in,Fell, M hhneu Written permission from Rogers rt C'alholl, Inc.
Page 3 of 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 2880143 10 Reported: 01/28/14 11:04
Sample Number
Sample Description
Parameter
4010496-01
Penlair Oolfail III - Grab collected on 01/10/14 09:30
Reporting
Result Limit Units
DF
Analyzed
Method
Flag Analyst
Batch
%'olatile Orranies
1.2-Dichlorobenzene
ND
2.0
ug/L
1,00
01/15/14 16-32
EPA 624-9260B
LBW
B4AO763
13-Dichlotobenzxne
ND
2.0
ug/L
1.00
01/15114 16:32
EPA 624-6260B
LBW
134A0763
1.4-Dichlorobenzene
ND
ID
ug/L
1.00
01/15/14 16:32
EPA 624-9260B
LBW
134AO763
1,2,4-Trichlorobenzene
ND
2.0
ug/L
1.00
01/15/14 16:32
EPA 624-8260B
LRW
B4AO763
cis-1,3-Dichloropropene
ND
1.0
ug/L
1.00
01/15/14 16:32
EPA 624-8260B
LBW
B4AO763
Iran%-1,3-nichloropropene
ND
I.0
ug11.
1.00
01/15114 16:32
EPA 624-8260B
LBW
134A0763
Surrogates
%,REC
%REC Limits
FIWZ
1.2-1lrrhlnrncrh..4)4
77
70-130
J•Rrnnrnjlunrnhen-roe
91
70-130
7'niticne-U8
92
70-130
Semi-ls'olatiles Organics
2-Chlorophenol
ND
5.00
uglL
1.00
0112l/14 15:03
EVA62519270D
RJM
134A0394
2A-Dichlorophenol
ND
5.00
u91L
1.00
01/21/14 15:03
EPA 62518270D
RJM
134AO394
2A-Dimethylphenol
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/82701)
RJM
B4A0394
2-Meihyl-4,6-dinitrophenol
ND
5.00
utJL
1.00
01/21/14 15.03
EPA 6251927DD
P)M
B4AO394
2,4-Dinitrophenol
ND
5.00
ugJL
1.00
01/21/14 15:03
EPA 625/8270D
RJM
B4AO394
2-Nitrophenol
ND
5.00
ugll.
1.00
0312l/14 15:03
EPA 625/8270D
RJM
B4AO394
4-Nitrophenol
ND
5.00
ug/L
1.00
01/21/14 15 03
EPA 625/82701)
RJM
B4AO394
p-Chloro-m-cresol
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 62518270D
RJM
B4AO394
Pentachiomphenol
ND
5.00
ug/L
1.00
0121/14 15:03
EPA 62519270D
RJM
B4A0394
Phenol
ND
5.00
ug/L
1,00
01/21/14 15:03
EPA 625/8270D
RJM
B4A0394
2.4,6-Trichlorophenol
ND
5.00
ug/l.
1.00
01/21114 15:03
EPA 62518270D
RJM
B4AO394
Acenaphthene
ND
5,00
ugft.
1.00
01/21/14 15:03
EPA 625/9270D
RJM
134A0394
Acenaphthy)ene
ND
5.00
ug/l.
1.00
01/21/14 15:03
EPA 625/8270D
RJM
134A0394
Anthracene
ND
5,00
uglL
1.00
01/21/14 15:03
EPA 62518270D
RJM
134A0394
Benzidine
ND
90.0
ug/L
1.00
01/21114 15:03
EPA 62518270D
- RJM
B4A0394
Benzo(a)anthracene
ND
5.00
ug/L
1.00
0121/14 15:03
EPA 625/92701)
RJM
B4A0394
Benzo(a)pyrenc
ND
5.00
n91L
LOO
0121/14 15:03
EPA 625182701)
RJM
B4A0394
Benzo(blfluomnlhene
ND
5.00
ug/1-
1.00
01/21114 15:03
EPA 625)8270D
RJM
B4AO394
Benzo(g.h,i)perylene
ND
5.00
ug/L,
1.00
01/21/14 15:03
EPA 625/8270D
RJM
B4AO394
Benzo(Ofluoranthene
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 62518270D
RJM
B4AO394
Bis(2-chloroethoxq)Methane
ND
5.00
up)L
1.00
01/21/14 15:03
EPA 62518270D
RJM
B4AO394
Bis(2-chloroethyl)Elhei
ND
5.00
ug/L
1,00
0121/14 15:03
EPA625I8270D
RJM
B4A0394
bis(2-Chloroisopropyl)ether
ND
S.W
OWL
1.00
0121/14 15:03
EPA 625/9270D
RJM
B4A0394
Bis(2-ethylhexyl)Phthalate
ND
5.00
uNL
1.00
0121/14 15.03
EPA 62518270D
RJM
B4AO394
PO Box 5655 1 Greenville, SC 29606 1426
Fairforest Way
I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersarldeallcott.eom
an employee -owned company
01128,201 a 11: 0a T his repnrr rnrry nor he reprodmed, e,xcepr in fidl, W irlrnar wrirvan prnni.rsrra+.Ji ran Rugetw A, Calkorr, Inc.
Page 4 of 27

Rogers & Callcott
ENVIRONMENTAL
Fnvironmental. Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 28801-4310 Reported: 01/28/14 11:04
Sample Number 4010496-01
Sample Description Pentair outfall kl - Grab collected on 01/10/14 09:30
Reporting
Parameter Result Limit Units
DF
Analyzed
Method
Flag Analyst
Batch
Semi-Volatiles Organics
4-Bromophenylphenyl ether
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/8270D
RJM
B4A0394
Butylbenzylphthalate
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/8270D
RIM
B4A0394
2-Chlorenaphthalene
ND
5.00
USA,
1.00
01/21/14 15:03
EPA 625/8270D
RJM
134A0394
4-Chlorophenylphenyl ether
ND
5.00
ug/L
1-00
01/21/14 15:03
EPA 625/8270D
RJM
134A0394
Chrysene
ND
5.00
ugll,
1.00
01/21/14 15:03
EPA 62518270D
RJM
B4A0394
Dibenzo(a,h)anthracene
ND
5,00
ug/L
1,00
01/21/14 15:03
EPA 62518270D
RJM
B4A0394 "
3-3'-Dichlorobenzidine
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 62518270D
RJM
B4A0394
Diethylphthalate
ND
5,00
ug/L
1,00
01/21/14 15:03
EPA 625/8270D
RJM
B4A0394
Dimethylphthalate
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 62SJ8270D
RJM
B4AD394
Di-n-butylphthalate
ND
5.00
ug/L
I.00
01/21/14 15:03
EPA 62518270D
RJM
B4A0394
2,4-Dinitrotoluene
ND
5.00
ug/L
1,00 `01/21114 15:03
EPA 62518270D
RJM
B4A0394
2,6-Dinitrotoluene
ND
5.00
ug/L
100
01/21/14 15:03
FPA62518270D
RJM
134A0394
Di-n-octylphihalate
ND
5.00
ug/L
1,00
01/21/14 -15:03
EPA 62518270D
RJM
B4A0394
1,2-Diphenylhydrazene(Azobenzene)
ND
5.00
uglL
1,00
01/21/14 15:03
EPA 62518270D
RJM
B4A0394
Fluoranthene
ND
5.00
uglL
I.00
01/21/14 15:03
EPA 625/8270D
RJM
B4A0394
Fluorene
ND
5.00
ug/L
I.00
01/21/14 15:03
EPA 62518270D
RJM
134A0394
Hexachlorobenzene
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 62518270D
RJM
B4A0394
Hexachlorobutadiene
ND
5.00
uglL
1.00
01/21/14 15:03
EPA 62518270D
RJM
134A0394
Hexachlorocyclopeniadiene
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 62518270D
RJM
134A0394
Hexachl0r0ethane
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/9270D
RJM
134A0394
lndeno(1,2,3-cd)pyrcnc
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/9270D
RJM
134A0394
Isophorone
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/9270D
RJM
134A0394
Naphthalene
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/8270D
RJM
B4A0394
Nitrobenzene
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/8270D
RJM
134A0394
N-Nitroso-di-methylamine
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/8270D
RJM
B4A0394
N-Nitroso-di-n-propyiamine
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/8270D
RJM
B4A0394
N-Nitrosodiphenylamine (Diphenylamine)
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/9270D
RJM
B4A0394
Phenanthrene
ND
5.00
ug/L
1.00
01/21/14 15:03
EPA 625/8270D
RJM
B4A0394
Pyrene
ND
5.00
ug1L
1.00
01/21/14 15:03
EPA 62518270D
RJM
B4A0394
Surrogates
%REC
%REC Limits
Flag -
Nitrohenzene-D5
97
35-114
2-Fluornhiphen)'l
95
43-116
Terphenyl-W4
103
33-141
2-Fhmrophenol
57
21-110
Phenol-D5
40
10-1I0
PO Box 5655 I Greenvilte, SC 29606 1 426 hirforesr Way I Greenville, SC 29607 1 main 864.232,1556 1 fax W.232,6140 rogersandealleott.eom
an employee -owned company
01128e2014 11:04 This report mrry not he reprodnced, ercepi rn,fiell, a ithoeer wrilten pernnixsrnn from Rogues A. Collcou, Ine.
Page 5 of 27

Rogers & Calleott
ENVIRONMENTAL
Environmenlal Testing Solutions Project: Pentair
351 Depot St, Work Order: 4010496
Asheville- NC 28801-4310 Reported: 01/28/14 1 1:04
Sample Number 4010496-01
Sample Description Pentair Outfall 01 - Grab collected on 01/10/14 09:30
Reporting
Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch
Semi-Voiatiles Organics
Surrogates %REC' %REC Limits Flag
2, 4, 6-Trihromrrplrenol 119 10-123
PCBs
PCB-1016
ND
0.50
13R1L
1.00
01/17/14 16:12
EPA 608
RKH
B4A0454
PCB-1221
ND
0.50
ugiL
1.00
01/17/14 16:12
EPA 608
RKH
B4A0454
PCB-1232
ND
0.50
uglL
1.00
01/17/14 16:12
EPA 608
RKH
134A0454
PCB-1242
ND
0.50
ugiL
1.00
01/17/14 16:12
EPA 608
RKH
B4A0454
PCB-1248
ND
0,50
ug1L
1.00
01/17/14 16:12
EPA 608
RKH
B4AO454
PCB-1254
ND
0.50
ublL
1.00
01/17/14 W 12
EPA 608
RKH
B4AO454
PCB-1260
ND
0.50
ug1l,
1.00
01/17/14 16,12
EPA 608
RKH
B4AO454
Surrogates
%.REC
%.REC Limits
Flag
2,4,5,6.1eo-aclrloro-m-x),lrne
93
60-130
Uecnrhluruhiphrnv!
68
30-150
Sample Number
4010496-02
Sample Description
Pcnlair Oulfall 41 - Grab collected on 01/10/14 09:30
Reporting
Parameter
Result
Limit
Units
DF
Analyzed
Method
Flag
Analyst
Batch
Volatile Organics
Acrolein
ND
5.0
ugiL
1.00
01/23/14 11:27
EPA624-826DB
LBW
64A0864
Acrvlonitrile
ND
5.0
ug/L
1.00
OIY23114 11:27
EPA624-8260B
LBW
134A0864
Surrogates
%REC
%REC limits
Flag
!.l-Uirhlorncrhrrnc-Ua
72
70-130
Talucnc-!7N
87
70-130
a-Bronrr,Jlrrorohen= ere
96
70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.com
an employee -awned company
6112812011 11:04 This report mr?v na1 he repmdnceei, except m idl, irilhnnr Hvirren permission.trnnr Rnger.s t CuAcmi, Inc.
Page 6 of 27

Rogers & Cattcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 28801-4310 Reported: 01/28/14 11:04
Sample Number 4010496-03
Sample Dcsrriptiou Pentair Outfall 42 - Grab collected on 01/I0/14 09 40
Reporting
Parameter Result Limil Units DF, Analyzed Method Flag Analyst Batch
General Chemistry Parameters
Oil and Grease, Total, HEM ND 5.0 mg/L 1.00 01115/14 WOO EPA 1664A CTS B41A0433
Total Metals
Copper
ND
0.005
ms4-
1.00
01/15/14 12:26
EPA 200.7
MER
B4A0400
Lead
ND
0.020
mg/L
1.00
01/15/14 12:26
EPA 200.7
MFR
144AO400
Zinc
0.016
0.010
mg/L.
1.00
Ol/15/14 12:26
EPA 200,7
MER
B4AO400
Volatile Organics
Benzene
ND
2.0
og/L
1.00
OV15114 17:01
EPA624.8260B
1-BW
B4AO763
Bromororm
ND
2.0
og/L
1.00
01/15/14 17:01
EPA624-8260B
LBW
B4A0763
Carbon tetrachloride
ND
2.0
uiVL
1.00
01/15/14 17:01
EPA 624.8260E
LBW
B4AO763
ChWobenzenc
ND
2.0
ug/L
1.00
01/15/14 17:01
EPA 624.8260E
LBW
B4AO763
Dibromochloromethane
ND
2.0
uglL
1.00
O1115/14 17:01
EPA624.8260B
1,BW
B4A0763
Chlomethane
ND
2.0
ug/L
1.00
01/15/14 17:01
EPA 624-8260B
LBW
B4AO763
2-Chloroethylvinyl ether
ND
5.0
uWL
1.00
01115114 17:01
EPA 624.8260B
LBW
B4AO763
Chloroform
ND
2.0
n0L
1,00
Ol/I5114 IT01
EPA624-8260B
LBW
B4AO763
Bromodichlorometham
ND
2.0
Ug/L
1.00
01/15/14 17:01
EPA 62-1-9260B
LBW
B4AO763
1.1-Dichloroethane
ND
2.0
ug/L
1.00
01/15/14 17:01
EPA 624-8260H
LBW
114A0763
2-Dichloroethane
ND
2.0
ug&
1.00
01/15/14 17:01
EPA 624.8260B
LBW
134A0763
trans-1,2-Dichlomethene
ND
2.0
ug/L
1.00
01/15/14 IT01
EPA624-9260B
LBW
B4AO763
1.1-Dichloroetherte
ND
2.0
ugtL.
1.00
01/15114 17:01
EPA 624-8260B
LBW
B4AO763
11-Dichloropropane
NO
2.0
uKIL
1.00
01115/14 17:01
EPA624-8260B
LBW
B4A0763
Ethvlhenzene
ND
2.0
ug/L
1.00
01/15/14 17:01
EPA 624-826011
LBW
B4AO763
Bromomethane (Methyl Bromide)
ND
2.0
ug/l,
1.00
01/15/14 17:01
EPA 624.8260B
LBW
B4AO763
Chloromethane (Methyl Chloride)
ND
2.0
ug/L
1.00
01/15/14 17:01
EPA 624.8260B
LBW
B4AO763
I,1,2,2-Tctrachloroethane
ND
2.0
ug/L
1.00
01/15/14 17:01
EPA624-8260B
LBW
B4AO763
Tetrachloroethene
ND
2,0
ug/L
1.00
01/15/14 17:01
EPA 624.8260E
LBW
B4AO763
Toluene
ND
2.0
iteJL
1.00
01/15/14 17:01
EPA 624.8260E
LBW
B4AO763
1,1,1-Trichloroethane
ND
2,0
ug/L
1.00
01/15/14 17:01
EPA624.8260B
LBW
B4AO763
1,1,2-Trichloroethane
ND
2.0
ug/L
1.00
01/15/14 17:01
EPA 624.8260E
LBW
B4AO763
Trichloroethene
ND
2.0
u!/L
1.00
01/15/14 17:01
EPA624-8260B
LBW
B4AO763
Vinvl chloride
ND
2.0
ug/L
1.00
01/15/14 17:01
EPA 624-82603
1-B W
B4AO763
Dichlorodilluoromethane
ND
2.0
ug/L
1.00
01/15/14 17:01
EPA 624-8260B
L$W
B4AO763
Methylene Chloride
ND
2.0
u91L
1.00
01/15/14 17:01
EPA 624-92605
LBW
114A0763
Trichlorofluoromethane
ND
2.0
ug/L
1.00
01/15/14 17:01
EPA 624-9260B
LBW
134A0763
1,2-Dichlorobenzene
ND
2,0
W91
1.00
01/15/14 17:01
EPA624-8260B
LBW
B4AO763
13-Dichlorobenzene
ND
2.0
ug/L
100
D1/15114 17:01
EPA624-8260E
LBW
B4AO763
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville, 5C 29607 1 main 864,232,1556 1 tax 864,232.6140 rogersandcallcott,Com
an employee -owned company
0112812014 Il: (la Thin relx r1 muv nur he reprodutrd e.�c'ep+ in fief!, H ithruu wriflen pernri.csinn Jrr ie Hn�erc X Cullcnrr. lnc.
Page 7 of 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 28801-4310 Reported: DI/28/14 11:04
Sample Number 4010496-03
Sample Drwription Pentair Outlull #2 - Grab collected on 01/10/14 09:40
Parameter
Result
Reporting;
Limit
Units
DF
Analyzed
Method
Flag Analyst
Batch
Volatile Organics
,
[,4-Diehlorobenzene
ND
2.0
u81L
1.00
01/15/14 17:01
EPA 624-8260B
LBW
B4A0763
11A-Trichlorubenzene
ND
2.0
ug/L
1.00
01115114 17:01
EPA 624-8260B
LBW
B4A0763
cis-1,3-Dichioropropene
ND
1.0
ug1L
1.00
01/15/14 17:01
EPA 624-92608
LBW
B4A0763
trans- l,3-DichlorDpropene
ND
1.0
ug/L
1.00
01/]5/14 17:01
EPA 624-92608
I-BW
F14AO763
Surrogates
%REC
1 REC Limiq
Mae
1,2•Divh1nme1hanr-D4
76
70-130
4-8romg1trorobrimme
87
70-130
T(luene-08
82
70-130
Semi-Volatiles Organics
2-Chlorophenol
ND
5.00
ug/L
1.00
01121/14 15:33
EPA 625182701)
RIM
B4A0394
2,4-Dichlorophenol
ND
5.00
ug/L
1.00
01/21/14 15:33
EPA625r8270I)
RJM
134A0394
2,4-Dimcthylphenol
ND
5.00
uglL
1.00
01/21/14 15:33
EPA 625/82701)
RJM
B4A0394
2-Methyl-4,6-dinitrophenol
ND
5.00
ag/L
1.00
01/21/14 15:33
EPA62519270D
RJM
134A0394
2,4-Dinitrophenol
ND
3.00
ug1L
1.00
01/21114 15:33
EPA 62518270D
RJM
B4AD394
2-Nitrnphenol
ND
5.00
agfL
1.00
01/21/14 15:33
EPA 62518270D
RJM
B4A0394
4-Nitrophenol
ND
5.00
U91L
1.00
01/21/14 15:33
EPA 62518270D
RJM
B4A0394
p-Chloro-m-cresol
ND
5.00
U81L
1.00
01/21/14 15:33
EPA 62518270D
KJM
B4A0394
Pentachlorophenol
ND
5.00
u8/L
1.00
01/21/14 15:33
EPA 62518270D
RJM
R4A0394
Phenol
ND
5.00
ug/L
1,00
01/2l/14 15:33
EPA 625/8270D
RJM
B4A0394
2,4,6-TricNorophenol
ND
5.00
ugn-
1.00
01121J14 15:33
EPA 62518270D
RIM
B4A0394
Acenaphthene
ND
5,00
ug1L
1.00
0112U14 15:33
EPA625/82701)
RJM
B4A0394
Acenaphthylene
ND
5.00
ug/L
1,00
01/21/14 15:33
EPA 625/8270D
RJM
B4A0394
Anthracene
ND
5.00
ug/L
1.00
01/21/14 15:33
EPA 625/8270D
RJM
B4A0394
Benzidine
ND
80.0
ug/L
1.00
01/21/14 15:33
EPA WA270D
RJM
B4A0394
Benzo(a)anthracene
ND
5.00
ug/L
1.00
01/21/14 15:33
EPA 625/9270D
RIM
B4A0394
Benzo(a)pyrene
ND
5.00
ug/L
1.00
01/21114 15:33
EPA 625/8270D
RIM
B4A0394
Benzo(b)Fluorunthene
ND
5.00
uP1L
I,OQ
01/21/14 15:33
EPA625/927DD
RJM
B4A0394
Benzo(g.h.i)perylene
ND
5.00
ug/L
1,00
Ol/21114 15:33
EPA 6298270D
RJM
B4A0394
Benzo(k)tluoranlhene
ND
5.00
ug/L
1.00
01/21/14 15:33
EPA 62519210D
RJM
B4A0394
Bis(2-chloroethoxy)Methhne
ND
5.00
09AL
1.00
01/21/14 15:33
EPA 62519270D
RJM
B4A0394
Bis(2-chloroethyl)Ether
ND
5.00
u911,
1.00
01/21/14 15:33
EPA 62513270D
RIM
R4A0394
bis(2-Chloroisopropyl)ether
ND
5.DO
og/L
1.00
01/21/14 15:33
EPA62518270D
KJM
B4A0394
Bis(2-ethylhexyl)Phtha1ate
ND
5.00
ug/L
1.00
01/21/14 15:33
EPA 62518270D
RJM
B4A0394
4-Bromophenylphenyl ether
ND
5.DO
uglL
1.00
01/21/14 15:33
EPA 62518270D
RJM
B4A0394
Butylbenzylphthalate
ND
5.00
ug/L
1.00
01/21/14 15:33
EPA 625/8270D
RIM
B4A0394
PO Box 5655 1 Greenville, 5C 29606 1 426 Fairforest Way I Greenville, 5G 29607 1 main 864.232,1556 1 tax 864.232,6140 rogersandcall cott.COm
an employee -awned company
01/2812014 11 aN I hi.+ ri pnri nnry nor her rrproduced, rxcepi hr Jiell, wilhnul wriorn perrni.e. on Irony Rogers Y ('u!lcr.rr, im
Page 8 of 27

,1h
Rogers & Calkott
ENVIRONMENTAL
Environmental Tesling Solutions Project: Pentair
351 Depot St. Work Order. 4010496
Asheville, NC 288014310 Reported: 01128/14 11:04
Sample Number 4010496-03
Sample Drsrriplion Pentair Outfall #2 - Grab collected on 01/10/14 09:40
Reporting
Parameter Result Limit Units OF Analyzed Nlethod Flag Analyst Batch
Scmi-Volatiles Organics
2-Chloronaphthalene
4-Chlorophenylphtnyiether
Chrysene
Dibenzo(a.h)anthracene
3,3'-Diehlnrobenzidine
Diethylphthalate
Dimethylphthalate
Di-n-butyiphthalatc
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
1,2-Diphenylhydraxene (Azobenzene)
Fluotanthene
Fluorene
Nexachlorobenzene
I lexachlombutadiene
Iiexachlorocyclopentadiene
liexachloroethane
lndeno(1,2,3-cd)pyrene
Isophotone
Naphthalene
Nitrobenzene
N-Nitroso-di-methylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine(Diphenylamine)
Phenanthrene
f'yrene
ND
5.00
ug/L
1.00
0121114 15:33
EPA 625A270D
RJM
B4A0394
ND
5.00
091L
1.00
0121/14 15:33
EPA 625/8270D
RJM
B4A0394
ND
5.00
u8/L
1,00
0121114 15:33
EPA 62518270D
RJM
B4A0394
ND
5.00
uy1L
1.00
0121/14 15:33
EPA 62518270D
RIM
B4A0394
ND
5.00
ug/L
1.00
0121/14 15:33
EPA 625/8270D
RJM
B4A0394
ND
5.00
ug/L
1.00
01/21/14 15:33
EPA62S18270D
RJM
B4A0394
ND
5.00
nwl-
1.00
01/21/14 15:33
EPA 62518270D
KIM
B4A0394
ND
5,00
ug/L
1.00
01/21/14 1533
EPA 62518270D
RJM
134A0394
ND
5.00
uwL
1,00
01/21/14 1533
EPA 62518270D
RJM
B4A0394
ND
500
uh1l.
1.00
01/21/14 15:33
EPA625/82701)
RJM
B4A0394
ND
5.00
ug1L
1.00
01/21/14 1533
EPA 625/8270D
RJM
B4A0394
ND
5.00
ug11.
1.00
01/21/14 15:33
EPA 625/82701)
RJM
B4A0394
ND
5.00
ug/L
1.00
01/21/14 15:33
EPA6251827DD
RJM
B4A0394
ND
5.00
uiVL
1.00
01/21/14 15:33
EPA625/8270D
RJM
B4A0394
ND
3.00
ug7L
1.00
(11/21114 15.33
EPA6251827DD
RJM
B4A0394
ND
5.00
ug/L
1.00
01121114 15:33
EPA 62518270D
RJM
B4A0394
N❑
5.00
ug/L
1.00
0121/14 15:33
EPA 62519270D
RJM
B4A0394
ND
5,00
ug/L
1.00
0121/14 1533
EPA 62519270D
RJM
B4A0394
ND
5.00
ugrL
I"00
0121/14 15:33
EPA62$18270D
RJM
B4A0394
ND
5.00
ug)L
I PO
0121/14 15:33
EPA 62518270D
RJM
B4A0394
ND
5,00
ng11,
1.00
0112)114 15:33
EPA 62519270D
RJM
B4A0394
ND
5.00
ug/L
I.00
01/21/14 15:33
EPA 625/8270D
RJM
B4A0394
ND
5,00
ug/L
1,00
0121114 15:33
EPA625/9270D
RJM
B4A0394
ND
5,00
ag/L
1.00
01/21/14 15:33
EPA 625/9270D
RJM
134A0394
ND
5.00
ug/L
1.00
01/21/14 15:33
EPA 625YB270D
RJM
134A0394
ND
5,00
uSIL
1.00
01/21/14 15:33
EPA 62$/8270D
RJM
B4A0394
ND
5.00
a814
1.00
01/21/14 15:33
EPA 625/8270D
RJM
B4A0394
Surrogates
%REC
'% REC Limits Flag
Narohen_em-D5
96
35-114
2-F'lrrorobtplr<•rn!
95
43-116
Terphenyl-1)14
1 1 1
33-141
2-Fluorop4n•ttot
56
21-110
I'hcnal-D5
37
10-110
2,4,6.TrlbraW)p renol
101
10-123
PC:BS
PO Box 5655 1 Greenville, SC 296D6 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.556 1 fax [phone] rogersandcallcott.COm
an employee -owned company
0112NI2014 11.,04 This rrparl rout' nor he reproduced, except infill. wiihaur N rwen perrnis.won /rust Hngrra & Cullcon, Inc.
Page 9 of 27

Rogers &Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St, Work Order: 4010496
Asheville, NC 28801-4310 Reported: 01/29/14 11:04
Sample Number
Sample Description
Parameter
4010496-03
Pentair Outfall 92 - Grab collected on 01/10/14 09:40
Reporting
Result Limit Units
DF
Analyzed
Method
Flag Analyst
Batch
PCBs
PCB-10i6
ND
0,50
US/L
1.00
01117/14 16:43
F.PA60B
RKH
B4A0454
PCB-1221
ND
0.50
uglL
1.00
01/17/14 16:43
EPA 6D8
RKH
B4A0454
PCB-1232
NB
0.50
idyl.
1,00
01/17/14 16.43
EPA 609
RKH
B4A0454
PCB-1242
ND
0.30
uglL
1.00
01/17/14 16:43
EPA 609
RKH
B4A0454 ,
PCB-1248
ND
0.50
uwl.
1.00
01/17/14 16:43
EPA 609
RKIi
B4A0454
PCB-1254
ND
0.50
ug/L
1.00
01/17/14 16:43
EPA 609
RKH
B4A0454
PCB-1260
ND
0.50
uglL
1.00
01/17/14 16:43
EPA 609
RKH
B4A0454
Surrngatts
% R E C
% REC Limits
Flag
2,l,5,6.7bmrc'hlnrr+•n1•xvlrnc
N4
60-130
!)ecuchlnmh+fherry!
68
30-150
Sample Number
4030496-04
Sample Description
Pentair Outfall P2 - Grab collected on 01/10/14 09:40
Reporting
Parameter
Result Limit Units DF
Analyzed Method Flag Analyst Batch
Volatile Organics
Acrolein
ND 5.0 ugn. I.00
01/23/14 11:56 EPA 624•92608 LBW B4A0864
AMionitrile
ND 5.0 uWL 1.00
01/23/14 11:56 EPA 624.9260H LAW B4A0864
Surrngatn
%REC
% REC Limits Flat
1,2-Drehlurue Ilwpe•1.14 73 70-131)
!'nlucnr•1)✓ 88 70-130
-Hromglhrnrohrnoknr 96 70-130
PO Box 5655 1 Greenville, SC 29606 f 426 FairforestWhy I Greenville, SC 29607 1 main 864.232.1556 i fax [phone] rogersandcalICOEE.CO11.1
an employee -owned company
W12,w2U1 d 11, 04 7&ia report mare nn1 he reprndrrc'er1, except 1n,f dT, wirheno written pennissinre'Irurn Roger, & ('nllcntt. lnu.
Page 10 of 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville. NC 28801-4310 Reported: 01/28/14 11:04
General Chemistry Parameters
Quality Control Summary
Reporting Spike Source % RE RP❑
Yararneter Result Limit Units level Result %REC Limits RPD Limit Flags
Batch B4A0433 - General Prep - Wet Chem
Blank (134A0433-BLKI)
Oil and Grease, Total, HEM ND 5,0 mg/L
U.S (B4A0433-BSI)
Oil and Grease, Total, HEM 'MA 5.0 mg/L 40,0 96 79.1 l4
LCS Dup (B4A0433-BSDI)
Oil and Crease, Total, HEM
390 5.0 mglL 40,0 98 78-114 2 35
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 I main 864.232.1556 1 fax 864.232.614o rogersandcalleott.eom
an employee -awned company
0112,4r2014 11: 04 This report miry nni he repmducrd, ercept in dill, N ithow x raven pertn6siun fmni Rogers K Cedfurar. Inc,
Page 11 of 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project; Pentair
351 1)epot St. Work Order: 4010496
Asheville, NC 28801-4310 Reported: 01/28/14 11:04
Total Metals
Quality Control Summary
Reporting Spike Source °/REC RFD
Parameter Result Limit Units level Result % REC Limits RPD Limit Flags
Batch B4A0400 - EPA 200.7
Blank (R4A0404-BLKI)
Copper
ND
0.005
n1wl-
Lead
ND
0,020
mg/L
Zinc
ND
0.010
rngll.
LCS (MA0400-BSI)
Capper
1.04
0.005
mgq. 1,00 104 85-115
Lead
1.08
0,020
mgll. 1.00 108 95.115
Zinc
1.10
0.0I0
mg/l, 1.00 110 95.115
Duplicate (B4A0400-DUP1)
Source: 4010327-02
Copper
0.04
0.005
mg/L 0.04 2 20
Lead
ND
0,050
mg/L ND 20
Zinc
0.17
0.010
mglL 0.17 2 20
Duplicate (B4A0400-DtJP2)
Source: 4010329-04
Copper
0.01
0.005
mg/L
0.01
4 20
Lead
ND
0.050
mg/L
ND
20
Zinc
006
0.010
mgrL
C_G6
0.6 20
Matrix Spike (B4A0400-,]Sl)
Source: 4010327-02
Copper
1.09
0.005
mg1L
1,00
0.04
103
70.130
Lead
L05
0,050
mg1L
1.00
ND
104
70.130
Zinc
1.27
0.010
mgJL
1.00
0.17
110
70.130
Matrix Spike (B4A0400-NtS2)
Source: 4010329-04
Copper
1.06
0.005
mgrL
1.00
0.01
105
70-130
Lead
L07
0.050
mgrL
1.00
ND
107
70.130
Zinc
1.16
0.010
rng/l.
1.00
0.06
110
70-130
Post Spike (B4A0400-PSI)
Source: 4010327-02
Capper 1.04
Lead 1.02
Zinc 1,22
mg1L 1.00 0.04 100 95-115
mg/L I.00 ND 100 95-1 is
my'L 100 0.il 105 93-115
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandCallcott.Com
an employee -owned company
01123Q014 11:04 Thin mporr finny nor he reprodui ed, are'rpt infill, without u'rirren perinis.rion fironr Rogerr X Cal/e oir. Inc.
Page 12 of 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville. NC 28901-4310 Reported: 01/28/14 11:04
Total Metals
Quality Control Summary
Reporting Spike Source % RE RPD
Parameter Result Limit Units level Result % REC Limits RPD' Limit Flags
Batch B4A0400 - EPA 200.7
Post Spike (MA0400-PS2) Source: M0329-04
Copper 1.01
Lead 1.02
Zinc I .I 1
mglL 1.00 0,01 100 85-115
mglL I.00 ND 102 85-115
mglL 1.00 0.06 105 95-115
PO Box 5655 1 Greenville, SC 29606 1426 FairforestVVay 1 Greenville, SC 29607 I main 864.232.1556 I fax [phone] rogersandcalleott.eom
an employee -owned company
01128,2014 11, 04 This report muv nol he reproduced• e.xcepi in fidl• "j1hoer wrirren permission from krrgem 4- Callcotl, Inc.
Page 13 of 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 28801-4310 Reported: 01/28/14 11:04
Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %RFC Limits RPD Limit Flags
Batch B4A0763 - EPA 5030
Blank (B4A0763-BLI;I) -
Benzene
ND
2,0
uglL
Hromnform
ND
2.0
ug1L
Carbon tetrachloride
ND
2.0
ug/L
Chlorobenzme
ND
2.0
ug/L
DibrmmUehl0r0me1htme
ND
2.0
uglL
Chloroethane
ND
2.0
ug/L
2-Chlornethylvinyl ether
ND
5.0
ug1L
Chloroform
ND
2.0
ug1L
Rromodichloromohnne
ND
2.0
uglL
1. 1 -Dichloroethane
ND
2.0
uglL
1,2-Dichloroethane
ND
2.0
uSfL
trans-1,2-Dichlnrocthenc
ND
2.0
uglL
IJ-Dichloroelhene
ND
2.0
uglL
1,2-Dichloroprnpanc
ND
2.0
ug/L
Ethylbetzzene
ND
2.0
uglL
Bromomethane (Methyl Bromide)
ND
2.0
uglL
Chloromcthanc (Methyl Chloride)
ND
2.0
ug/L
1,1,2,2-Tetrachloroethane
NA
2.0
uglL
Telrachlornethene
ND
2.0
ug/L
Toluene
ND
2.0 _
uglL
I,I,I-Trichlnroethene
ND
2.0
ug/L
1,1,2-Trichloroethane
ND
2.0
ugtL
Trichlorocihene
ND
2.0
nglL
Vinyl chloride
ND
2.0
uglL
Dichioradifluoromethane
ND
2.0
uglL
Methylene Chloride
ND
2.0
ug1L
Trichlorofluoromethane
ND
2.0
uglL
1,2-Dichlurobenzene
ND
2.0
uglL
1.3-Dichlorobenzene
ND
2.0
uglL
[A-Dichlnrobenzene
ND
20
ug1L
1,2,4-Trichtorobenzene
ND
2.0
ug/L
cis-1,3-Dichloropropene
ND
1.0
ug1L
trans-1,3-Dichloropropene
ND
1.0
t=gtL
Surrogate: 1,2-Dwh1ornelhune-D4 79 70-130
Surrugate: 4-BrontuJ1uurohe=ene 89 70-130
PO Box 5655 1 Greenville, 5C 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.eom
an employee -owned company
0112SIPd 14 1 hita This report otoy not he reproduced excepr in, idl, uvrhutrr written permi,.,rinn Jrr nr Ifn} rn & Crtllenrr, Inc.
Page 14 Of 27

Rogers & CaUcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 28801-4310 Reported: 01/28/14 11:04
Volatile Organics
Quality Control Summary
Reporting Spike Source 'Y-REC RI'D
Yararntirr Result Limit Units Level Result % REC Limits RI'D Limit Flags
Batch B4A0763 - EPA 5030
Blank (114A0763-BLKI)
Srrrragarer Aluenr-DR
LCS (94A0763-BSI )
x2 7n-13n
Benwae
19.1
2.0
uglL
200
96
70.130
Branrnform
18.3
2.0
ug/L
20.0
92
71-129
Carbon tetrachloride
18.4
20
ugh-
20.0
92
73.127
Chlorabenzene
19.4
2.0
u8/i.
20.0
97
70-130
Dibromochloromethane
18.1
2.0
ugd,
200
90
70.130
Chloroethane
21.2
2.0
ug/L
20.0
]06
60.140
2-Chloroethylvinyl ether
19.1
5.0
ug/L
20.0
96
50.150
Chloroform
18.6
2.0
ug1L
20.0
93
70.130
Bromodichloramethaae
20.9
2.0
uglL
20.0
105
70.1.10
l,l-Dichloroethane
20.0
2.0
ug11.
20.0
100
73.127
1,2-Dichloroethane
20,5
1.0
ug11-
20.0
102
70-130
trans-1?-Dichloroethene
19.2
2.0
ug/L
20.0
%
70-130
1.1-Dichloroethene
19.2
2.0
ug/L
20.0
96
70-130
1,2-Dichloropropane
21.7
2.0
ug/L
20.0
109
70-110
Ethv@enzene
21.9
2.0
ug/L
20.0
109
70-130
Bmmamctlwc(Methyl Bromide)
214
2.0
u91L
20.0
107
60-140
Chlornmethane (Methyl Chloride)
20.1
2.0
u81L
20.0
lei
60.140
1,1,2,2-Terrachloroethane
18.5
2.0
ug/L
20.0
92
70-130
Tetrachlornethene
19.1
2.0
ugll.
20.0
96
74.126
Toluene
20.1
2.0
ug/L
20.0
I00
7$-W
L1,l-Trichloroethane
18.6
2.0
ug/L
20.0
93
75.125
I,1,2-Trichloroethane
19.7
2.0
ug/L
20.0
99
71.129
Trichloroethene
19.7
2,0
ug/L
20.0
98
71-130
Vinyl chloride
21.3
2.0
ug/L
20.0
106
60.140
Dichlorodilluoromethane
17.0
2.0
ug/L
20.0
85
60-140
Methylene Chloride
18.o
2,0
ug11,
20.0
90
70-130
Trichlorotluoromethatte
21.5
2.0
u91L
20.0
108
60-140
1,2-Dichlorobenzene
18.7
.2.0
ug1L
20.0
93
70-110
13-Dichlorobenzene
183
2.0
ug/L
20.0
92
73-127
1.4-Dichlorohcnzcnc
19.4
2.0
mg1L
20.0
92
70-130
L2,4-Trichlorobenzene
19.9
2,0
ug/L
20.0
99
60-140
cis-1,3-Dichloropropene
21.2
1.0
ugn,
20,0
106
70.130
trans-1,3-Dichloropropene
22.9
1.0
ug/L
20.D
115
70.130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville,
SC 29607 1 main 864.232,1556
1 lax 861.232,6140
rogersandealleott.eom
an ernployee-owned company
01128'2011 1104 This rrpnrr rn<ry not he reprorinceel, e.rcepi in fill, wllhnnr wrilten permusion frnnr Rogers & Cullcnrr. Im.
Page 15 of 27

J Rogers & Callcott
ENVIRONMENTAL.
Environmental Testing Solutions Project: Pentair
351 Depot St. work Order: 4010496
Asheville, NC 28801-4310 Reported: 01f28114 t 1:041
Volatile Organics
Quality Control Summary
Reporting Spike Source % RE RPD
Parameter Result Limit Vnits Level Result % R E C Limits RPD Limit Flags
Batch B4At1763 - EPA 5030
LCS (1134A0763-8SI)
Snrmgme:l,2-Dwhlarrerhane-nl
95
70-130
Nurmgare,- 4-8romgouoroheniene
89
70-130
Surmgale: Toluene-IM
95
10-130
Matrix Spike (WA0763-NISI)
Source: 40103304M
Benzene
39.6
4,0
ug/L
40.0
ND
96
37-JSI
Rromoforns
33.8
4.0
nglL
40,0
ND
84
45.169
Carbon tetrachloride
36,8
4,D
uglL
40.0
ND
92
70-14D
Chlorobenzene
39.2
4,0
ug/L
40,0
ND
98
37.160
Dibromochloramethane
34.4
4,0
ug/L
40.0
ND
86
53-149
Chlorocthme
41.0
4,D
ug/L
40,0
ND
102
14-20D
2-Chlaroethylvinylelher
31.9
10.0
ug/L
4O.D
ND
80
3.200
Chloroform
38.1
4.0
ug/L
40,0
ND
93
51.IU
Hromodichloromethane
41.6
4.0
ug ]-
40.0
ND
104
35-155
1,1-Dichloroethane
36.7
4.0
ug/L
40.0
ND
92
59-155
1,2-Dichloroethant
35.5
4.0
og1L
400
ND
89
49-155
trans-1,2-Diehloroethene
36.5
4.0
ng/L
40.0
ND
91
54-156
I,1-Dichloroethene
40.7
4.0
uglL
40.0
ND
102
3-200
1,2-Dichloropropano
39.8
4.0
nglL
40.0
ND
100
3-200
Eihplbcnaent
46.8
4.0
ug/L
40.0
ND
1.17
37-162
Brwnomethane (Methyl Bromide)
41.2
4.0
ug/L
40.0
ND
103
3-200
Chloromethane (Methyl Chloride)
37.5
4.0
ug/L.
40.0
ND
94
3-200
1,1,2,2-•Tetrachlorocthane
34.0
4.0
uglL
40.0
ND
85
46-157
Teirachloroethene
41.5
4.0
ug(L
40.0
N❑
104
64.148
Toluene
42.6
4.0
isgil-
40.0
ND
106
47.150
1.1,1-Trichloraethant
38,8
4,0
ug/L
40.0
ND
97
52-162
1,1,2-Trichloroelhane
3T5
4.0
ugiL
40.0
ND
94
52.150
Trichloroelhene
40.0
4.0
ug1L
40.0
ND
100
7)-157
Vinyl chloride
44.2
4.0
ug,L
40A
ND
110
3-200
Dichlorodilhtototnethane
35.9
4.0
ug/L
40.0
ND
90
60-140
Methylene Chloride
36,2
4.0
1Igi1,
40,0
ND
90
3-200
Trichloro[luoromethant
45.3
4,0
uglL
40.0
ND
113
17-191
1,2-Dichlurobenzene
37.3
4.0
ug/L
40.0
ND
93
18-190
0-Dichlorobenzene
3T 1
4.0
uglL
400
ND
93
59-156
14-Dichloruhenzene
373
4.0
ug/L
40,8
ND
93
16-190
1,2,4-Trichlorobenzane
40.1
4.0
nBR.
40,0
ND
100
60-140
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesc Way
I Greenville,
SC 29607 I main 864.232.1556
1 fax 864,232,6140
rogersandcallcott.com
an employee -owned company
011281014 11,04 This report inuv not he reproehtced, excepl in full, r+irhnur> riuen penniasir n /turn 1{ugera K Calleoll, Inc.
Page 1fi of 27

Rogers & Caklcott
4-t�..l�_ ENVIRONMENTAL
Environmenlal Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Ashcvillc, NC 28801-4310 Reported: 01/29/14 11:04
VDlatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Yaramcter Result Limit Units Level Result %REC Limits RFD Limit Flags
Batch B4A0763 - EPA 5030
Matrix Spike (134A0763-NISI) Source: 4010330-04
cis-1,3-Dichlotopropene 40.6 2.0 ug1L 40.0 ND 102 3-200
trons-1,3-Dichloropropene 43.4 2.0 u}11L 40.0 ND log 17.183
Surmgufe. 1.2-Dichlarnefhanr-14 N4 :0_13f1
Stmrogurc: 4-Rro n'Jim, rrhenzene N9 70-130
Surrngure: 7nLrene-1J8 48 SU-130
Matrix Spike 0up (B4A0763-NSbI) Source: 4010330-114
Benzene
36.3
4.0
uglL
40.0
ND
91
37.151
6
20
RTPn5af0rm
33.5
4.0
ogli,
40.0
ND
84
45-160
03
20
Carbon tetrachloride
36.1
4.0
ug1L
40.0
ND
90
70-140
2
20
Chlombenzene
36.2
4.0
uivi,
40.0
ND
90
37-160
8
20
Dibromochlor0mothane
33.6
4.0
uglL
40.0
ND
84
53.149
2
20
Chloroc[hane
41.4
4.0
ug/L
40.0
ND
103
14-200
0.9
20
2-Chlorocthylvinyl ether
35.9
t0.0
ng1L
400
ND
90
3-200
12
20
Chloroform
35.6
4.0
ug1L
40.0
ND
86
51-138
7
20
Brnmadichloromethant
39.2
4.0
nglt,
40.0
ND
98
35-155
6
20
1,1-Dichlotoethone
39.6
4.0
nglL
40.0
ND
96
39.155
5
20
1,2-Dichloroothane
39.3
4.0
U VL
40.0
ND
98
49-155
10
20
trans-1,2-Dichlormthena
37.3
4,0
nglL
40 0
ND
93
54.156
2
20
l,l-Dichloroe[hmc
3T5
4.0
ug/h
40,0
ND
94
3-200
8
20
1,2-Dichloraptapane
41.1
4.0
i%1L
40,0
ND
103
3-200
3
20
Eth}'lbenzene
41.4
40
uglL
40,0
ND
104
37.162
12
20
Bromomethane (Methyl Bromide)
40.7
4,0
uglL
40,0
ND
t02
3-200
1
20
Chloromelhane (Mcthyl Chloride)
39.0
4.0
ug1L
40,0
ND
98
3-200
4
20
1,1,2,2-Tetrachlorocthane
33.9
4.0
ug1L
40,0
ND
85
46-157
0.06
20
Tetracl[loroelhunc
36.5
4.0
ug/L
40,0
ND
91
64.148
13
20
Toluene
39.2
4.0
uglL
40,0
ND
96
47-150
11
20
1.1,1-Trichlorocthane
36.1
4.0
ug11.
40)
ND
90
52-162
7
20
1.1,2-Trichloreelhane
36.7
4,0
ug1L
400
ND
92
52-150
2
20
Trichloroethene
39.4
4.0
ugiL
40.0
ND
96
71-157
4
20
Vinyl chloride
42.0
40
ug1L
40.0
11.11)
105
3.200
5
20
DichlorodiFluorometham
32.6
4.0
ug/L
4011
ND
82
60-140
10
20
Methylene Chloride
33.9
4.0
ug/L
40.0
ND
85
3.200
7
20
Trichlnrofluororne[hane
43.2
4,0
i4fL
40.0
ND
108
17-191
5
20
1.2-Dichlorobcnzene
34.5
4,0
ug11-
40.0
ND
86
18-190
8
20
1,3-Dichlorohenzene
34.4
4.0
q/1,
40.0
ND
86
59-156
8
20
PO Box S655 I Greenville; SC 29606 1 426 Fairforest Way I
Greenville,
SC 29607 I main 864,232,1556
1
fax [phone]
rogersandealicott.eom
an employee
-owned company
01/23t2014 I PO4
This report rngv not he reproduced
ereepf in,/id1, µ ahont
written permisaion.1ronr Rogers K Cnllcnrr,
/ns.
Page 17 of 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
AshevilIt;, NC 28801-4310 Reported: 01/29/14 11;04
Volatile Organics
Quality Control Summary
Reporting Spike source % RE RPD
Parameter Result Limit Units level Result %REC Limits RPD Limit Flags
Batch B4A0763 - EPA 5030
Matrix Spike Dup (NA07634 0SDi) Source: 4010330-04
I.4-Dichlorobenttne 34.2
4.0
ug/L
40.0
ND
86
18-190
9
20
1,2,4-Trieblorobenxene 36.9
4.0
ug/L
40-0
ND
92
60-140
8
20
cis-1.3-Dichloropropenc 394
2.0
ug/L
40.0
ND
98
3-200
3
20
smuts-1,3-Dichloropropene 41.3
2.0
uSIL
40.0
ND
103
17-193
5
20
• Surrogate: 1.2-Dirhlomerhone-D4
Y0
79-13o
Surragetle:4-Bmnrnfluornhen-ene
84
79-130
Surrogure: Tnhrene-D8
s8
70-130
Batch B4A0864 - EPA 5030
Blank (B4A0864-BLK1)
Acrolein ND
5,11
ug/L
AcrOonitr le ND
5.0
ug/l,
Surrogene: 1.1-Dich1oroerhane-D4
74
70-130
.SurrnlNile: Tohre•ne-1h4
88
70-130
Surrngme: 4-HrmmqJlrrorohc)zxr;e
Yb
70-130
LCS (84Ai1864-BS 1)
Acrolein 111
5.0
ug/L
100
111
60440
Aerylonittile 20.7
5.0
ug/L
20.0
104
82.4-119
Surrogate: L2-Dreh1omerhune-D4
93
70-130
Surrogate: lbluene-DS
IY7
70.131i
Surrogate: 4-Hromolluornhexzene
104
70-130
LCS (B4A0864-BS2)
Acrolein
98,2 3.0 ug/L
]00 98
91.8-108
Acrylonirrile
19,2 5.0 ug/L
20.0 96
92.4-119
Surrogate:l,2-Drrhlorrrefhune-D4
90
70430
Surmgafe: Toluene-1h4
102
70-130
Surrogate:4-Bromnlhrnmbew-ene
104
70.130
Matrix Spike (840864-MS1)
Source: 4010379-05
Acrolein
115 5.0 u5%L
100 ND 115
88-119
Acrylonitrile
22.0 5.0 ug/L
20.0 ND 110
71-115
55irmgene: 1, 2-Dreh1oroethune-D4
96
I0-130
1'nrrogure: Toluene-P8
1(14
70-130
t7irrogore; 4-Hromo.flooruhc1wene
102
70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesc Way I Greenville, 5C 29607 1 main 864.232,1556 1 fax [phone]
rogersandcall cott.eom
an employee -owned company
f1)124/1014 11:04
This report miry not he reproduced, "vepr in fill. trrrhow wrfnen perrra.ccton frone Rogers rr- C.'4111coH, Inc.
page 18 of 27

Rogers & Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 28801-4310 Reported: 01/28/14 11:04
Volatile Organics
Quality Control Summary
Reporting Spike Source % REC RPD
Parameter Result Limit Units Level Result %REC limits RPD Limit Flags
Batch B4A0864 - EPA 5030
Matrix Spike Dup (MA0864-NISD1) Source: 4010379-05
Acrolein 128 5.0 ug/L too ND 128 88-118 10 20 SI
Acn9onitrile 23.1 5.0 ugfL 20,0 ND 116 71-135 5 20
Surmgwe:I,_^-l7rcirinmcrhonr-13a 97 70-130
Surrogate: Toluene -DR 103 70-130
Surrogate: 4-llromolluoroherr_ene 99 70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest VVay I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.614o rogersandcallcott.corn
an employee -awned company
0112812014 11: 04 7hly report ttnry nor he reproduced eecepr rn f:dl. N ahmu ti. rirtrn pennrcrinn.frnrn Rogers K {',tllcntr, Inc.
Page 19 of 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville. NC 28801-4310 Reporled: 01/28/14 11:04
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source '% REC RI'D
Parameter Result Limit Units Level Result %RF,C Limits RPD Limit Flags
Batch B4A0394 - EPA 625
Blank (B4A0394-BLK1)
2-Chlorophenol
ND
5.00
ug/L
2,4-Dichlorophcnol
ND
5.00
ug/L
2,4-Dimethylphenol
ND
5.00
ug/L
2-Methy1-4,6-dinitrophenol
ND
5.00
uglL
2,4-Dinitrophenol
ND
5.00
ug/L
2-Nitrophcnol
ND
5,00
ug/L
4-Nirrophenol
ND
5.00
ug/L
p-Chloro-nt-cresol
ND
5.00
ugil.
Pentachlorophenol
ND
5.00
ugfL
Phenol
ND
5.00
ug/L
2,4,6-Tnch10rophcnol
ND
5.00
ugfi.
Acenaphthene
ND
5.00
ug/L
Aeenaphthylene
ND
5.OD
ug/L
Anihracene
ND
5.00
ugfL
Renzidine
ND
8D.0
uglL
Benzo(ayanthracene
ND
5.00
ugfL
Benzo(a)pyrene
ND
5.00
ug/L
Renzo(blfluoranthene
ND
5.00
ug/L
Benzo(g,h,i)perylene
ND
5.00
ug/L
Benzo(klfluoranthene
ND
5A0
ug/L
Bis(2-chloroethoxy)Mahane
ND
5.00
ug/L
Bis(2-chloroethyl)Fther
ND
5,00
ug/L
bis(2-Chlomisopropy1)cthcr
ND
5.00
ug/L
Bis(2-e1hylhexy1)Phthalate
ND
5.00
ug/L
4-Br0rrr0pheny)phenyl ether
ND
5.00
ug/L
Butylbenzylphthalate
ND
5.00
ug/L
2-Chloronaphthalene
ND
5.00
ug/L
4-Ch1nrophenylphenyl ether
ND
5.00
ug/L
Chrysenc
ND
5.00
ug/L
Dibenzo(a,h)anthracene -
ND
5,00
ug/L
3.3'-Dichlorchenzidine
ND
5.00
ug/L
Diethviphthalaic
ND
5.00
ug/L
Dimethylphthalate
ND
5.00
ug/L
Di-n-butylphihalate
ND
5.00
uglL
2,4-DiniErotoluene
ND
5.00
ugfL
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, 5C 29607 1 main 864,232,IS56 I fax [phone] rogersandealleou.eom
an employee -owned company
0112812014 11:04 This repr.ri miry nor he reprndnced, excepr m fdl, n above oralm permis ir+n from Rogers d Cullcon, Inc.
Page 20 of 27

Rogers & Callcott '
ENVIRONMENTAL
Environmental Testing Solutions Project- Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 28801-4310 Reported: 01/28l14 11,04
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source % NEC RPD
Parameter Result Limit Units Level Result % REC Limits RFD Limit Flags
Batch B4AO394 - EPA 625
Blank (B4 A0394-R L K 1)
2,6-13initrololuenc
ND
5,00
ug/L
bi-n-octylphthalate
ND
5.00
ug/L
1.2-Diphenv1hydrazene(AzAenzene)
Tall
5,00
ug/L
Fluoranthcne
N➢
5.oa
ug1L
Fhiorene
ND
5.00
ug/L
Hexaebinrubenzene
ND
5.00
ug/L
Hexachlorobutadiene
ND
5.00
uglL
Ilexachlorocyelopentediene
N➢
5.00
ug/L
Hexachloroethane
ND
5.00
ug/L
Indenn( I,2,.3•cd)pyrene
ND
5,00
❑g1I,
lsophorone
ND
5.00
uglL
Naphthalene
ND
5,00
ug/L
Nitrobenzenc
ND
5,00
uWl.
N-Nitraso-di-me thy lamine
ND
5.00
ng/L
N-Nitroso-di-n-propylanime
ND
5.00
ug/L
N-Nitrosodiphenylaminc(Dipheny omine) ND
5.00
ug/L
Phet=lhrene
N❑
5.00
UA
PyMme
ND
5.00
ug/L
,Surrogare: Nurohen_ene-D5
89
35-114
Nurrngure: 2-Pluorohiphenyl
90
43-116
Nurragme:7irphet(id-W4
9d
33-141
,Surrogate:2-Fluorophenul
55
21-110
Surrogare: PhcmnLDS
39
10-110
Surrogate, 2 a, 6-Trihrome phenol
96
10.123
LCS (84A0394-HSl)
2-Chlorophenol
83.5
5.00
tig/L
I00
83
23-134
2,4-Dichlorophenol
93.5
5,00
ug/L
100
94
39.135
2,4-Dimethylphenal
76.5
5.00
ug/L
10o
77
32-119
2-Me W-4,6-dinitrophenol
117
5.00
ug/L
100
117
1-191
2.4-Dinitrophenol
109
5.00
ug/L
106
108
1-191
2-Nitrophenol
102
5.00
ugiL
3O0
102
29-182
4-Nitmphtnol
45.2
5.00
uglL
100
45
1-132
p-Chloro-m-cre3ol
98.3
500
ug/L
I Ot)
98
22-147
Pentachlorophenol
969
5,00
ug/L
100
97
14-176
Phenol
37.2
5,00
ug/L
100
37
5-112
PO Box 5655 I Greenville, SC 29606 1426
Fair -forest Way
I Greenville, SC 29607
I main 864.232.1556
I fax 864,232.614b rogersandcallcott.eom
an employee -owned company
0112,V2014 11:04 This repnr tnrq, nnr he reprnr$rcetf eecepr on fill, withntu written permission frntu Rngecv n- Callcear, Inv. Page 21 of 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 288014310 Reported: 01/28/14 11:04
Semi-Volatiles Organics
Quality Control Summary
Reporting Spike Source %RF,C RPD
Parameter Result Limit Units Level Result %REC Limits I411) Limit Flags
Batch B4AO394 - EPA 625
U-9 (B4A0394-111SI)
2.4.6-rrichlorophenol
99.1
5.00
DglL
100
98
37-144
Acennphthene
91.5
5,00
ug/L
]00
92
47-145
Acenaphthylenc
94.5
5.00
ug1L
too
95
33-145
Anihrnccne
99.0
5,00
ug1L
]00
98
27-133
Henzidine
293
80.0
ug/L
500
59
1-139
Rcnzo(a)amhrecene
109
5,00
ug1L
100
109
33.)43
Henza(a)pyrene
117
5 D0
ug/L
100
117
17.163
Benzo(h)Iluoranihme
122
5.00
uglL
100
122
24.159
Benzo(g,h,i)peryIene
122
5.00
USA,
100
122
1-200
Hen7.a(k)fl10ran1hene
107
5.00
ug/L
]00
107
11-162
His(2-chlorocthoxy)Mathane
96.0
5.00
uglL
100
96
33.184
Bis(2-ch1aroethy1)Ether
89A
5.00
uglL
100
89
12.158
bis(2-Ch1Dr0is0pr0pyl)ethcr
88.0
5.00
uglL
too
88
36.166
Ris(2-ethylhexyl)ph1ha1nte
116
5.00
ng1[-
100
116
8-159
4-Hromophenylphenyl ether
104
5.00
ug/L
100
. 104
53-)27
Butylbc",lphthalale
114
5.00
ng/L
100
114
1-152
2-Chlononaphlhakne
91.3
5.00
ug/L
l00
91
60-119
4-Chiorophenylphenylether
106
5.00
1181L
100
106
25.158
Chryscne
104
5.00
ug1L
Inc
104
17-169
DibcnzD(a,h)anthracene
117
5.00
ug/L
t00
117
1.200
3,3'-Dichlurubcnzidinc
106
5.00
uglL
100
106
1-200
Diethylphihslate
105
5.00
ug/L
100
105
1.114
Dimelh}lphthalste
104
5.00
ug/L
too
104
1.112
Di-n-butylphthalate
108
5.00
ug/l.
100
109
1.119
2,4-Dinilrotuluene
113
5.00
ug1L
]00
H3
39-139
2,6-Dinitrotoluene
106
5.00
u01L
No
106
50-15a
Di-n-ooylphthalate
121
5.00
ug/L.
100
121
4.146
1,2-Diphcny)hydrazene(Azobenzcne)
97.6
5.00
ustL
100
99
65-130
Flutrranthene
110
5.00
WL.
100
I10
26-137
Fluorcne
102
5.00
ug/L
100
102
59-121
Hexacblorobcnzene
103
5,00
ug/L
100
103
1-152
Hexachlorobutadiene
"A
590
ug/L
too
83
24-116
Hexachlorecyelopentadiene
91.6
5.00
ug/L
100
92
37-130
Hexachlornethanc
71.5
5,00
ug1L
100
71
40-113
Indent)(],2,3-cd)pyrene
122
5.06
ug1L
too
122
1-171
rt
PO Box 5655 1 Greenville, SC 29606 1 426 Nirforest Way I Greenville, SC 27607 I main 864.232.1556 1 fax [phone] r-OgerSandCallGOtt.Com
an employee -owned company
0112V201 a 11:04 1'hie rrpnrr rr+en not he reprnduued, asecp7 br, full, edfhuu7 n'riucn perrnis.rinn f •nrrr Ifagcre K (, olholl, Inez
Page 22 0 27

Rogers & Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 288014310 Reported: 03/28/14 11:04
Semi-Volatiles Organics
Quality Control Summary
Reporting Spikt Source °1 kEC RPD
Parameter Result Limit Writs Level Result % REC Limits RYA limit Flags
Batch B4A0394 - EPA 625
LCS (B4AO394-RS 1)
Isophownc
101
5.00
110,
100
101
21-196
Naphthalene
89.2
5,00
ug1L
100
89
21-133
Niunbenzene
86.0
5.00
uglL
100
$6
35-190
N-Nitroso-di-mertrylamine
58.0
5.00
ug/L
100
58
10.100
N-Nirrnso-di-n-pmpyiantine
91.9
5.00
ug/L
Wo
92
I-200
N-Nirrosodiphenylarnine(Diphenylamine)
98.3
5.00
uglL
100
98
60.1.10
Phennnthrene
101
- 5.00
uglL
100
101
54.120
Pyrene
105
5.00
ug/L
100
105
52.115
Surmgare: Nurohen_ene-W
90
35-114
Surrogate: 1-Flnorohrphenyl
91
43-11 b
Surrog0te:lrrphei+t1-1)14
Jy
33.141
Surrogate: 2-Fhtorophenol
54
21-110
Surrogate: Phrnol-D5
16
10-110
Surrogate: 2,4,6-T rrhromuhhenol
119
10-123
PO Box 5655 I Greenville, 5C 29606 1 426 Fairforest Way I Greenville, SC 29607 I main 864.232,1556 I fax [phone] rOgersandcallcott.Com
an employee -owned company
ol/2,Y12o1-r 11:04 ThL, report moy not he rrproduceel, except in jiff, wirhow written prrtnisrron Irom Rogerx A, Callcotr, 1ne,
Page 23 of 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Ashev'illc.. NC 28801-4310 Reported: 01/28114 1 1:04
PCBs
Quality Control Summary
Reporting Spike Source % REC RFD
Parameter Result Limit Units Level Result %RFC Limits RPD Limit Flags
Batch B4A0454 - EPA 608
Blank (B4A0454-BLKIj
PCB_ 1016
ND
0.50
ug1L
PCB-1221
ND
0.50
ug/L
PCB-1232
ND
0.50
ug1L
PCB-1242
ND
0.50
uglL
PCB-1249
ND
0.50
ug1L
PCB-1254
ND
0.50
ug1L
PCB-1260
ND
0.50
USA.
Snrrr 1;ase: 2, 4,5, 6-Terrachlnm-nrrt 1 erre
81
60.130
Sarrogale: DererchlomhiphenYl
75
30-150
LCS (B4A0454-BSI)
PCB-1016
4.62
0.50
ug1L
5.00
92
50-114
PCB-1260
4.49
0.50
uglL
5.00
90
8-127
Si+rrngaie:
90
60.130
Surrnl,wfr Derachlnrnhiphenrl
tf5
30-150
IX''S (94A0454-BS2)
PCB-1016
2.43
0.50
og/L
2.50
97
50-114
PCB-1260
2.31
0.50
USIL.
2.50
92
5-127
Surrngore:2.�,5,6-Tcrruchlnm-nr-rr•lcru
85
610-130
Surrugure: Dciuchlorahiphcm•I
39
30.1511
Sample Preparation Data
Parameter Batch Sample ID Prepared AnAIVSI
EPA 200.7 Aletal Digestion
EPA 200.7
134A0400
4010496-01
01/14/2014 15 52
MER
EPA 200.7
B4AD400
40t0496-03
01/14/2014 15:52
MER
EPA 608 Extraction
EPA 608
B4A0454
4010496-01
01/15/2014 11:00
DBB
EPA 608
B4A0454
4010496-03
01115f2014 11:00
DBB
EPA 625 Extraction
EPA 625
B4A0394
4010496-01
01114f2014 09:00
DBB
EPA 625
B4A0394
4010496-03
01/14/2014 09:00
DBB
PO Sox 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, 5C 29607 1 main 864.232,1556 1 fax [phone] rogersandealleoet.eom
an employee -owned company
0112P2014 11: 04 This report may not he repmdreced, except in, fill, N idunU x rirrrn pernrisrinn /rr rn Hugrrr & Crrllrnrr, Inc.
Page 24 a 27

Rogers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Pentair
351 Depot St. Work Order: 4010496
Asheville, NC 28801-4310 Reported: 01128/14 11:04
Data Qualifiers and Definitions
ND Analyte NOT DETECTED at or above the reporting limit
NR Not reported
RPD Relative Percent Difference
5 I The matrix spike and l or the matrix spike duplicate sample recovery was not within control limits due to matriX interference. The
Lahoratory Control Sample (LCS) was within control limits.
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogerSandcallcott.Com
an employee -owned company
111128,2014 11:04 lhu report cony not he reproduced, except to f:dl, H irhnru ivrmen permrr.kwn fn,m Rogert ,C (.'nllcort, Inc.
Page 25 of 27

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Rotes & "ter
LABORATORY SERVICES
P.O. Box 5856, Oraerwga, SC 2WO
Phme JW4) 232-15M Fax (884) M-6140
SNppf0 Addmw 4S ftWre Way
Gmanv$e, SC 2DO07
Client Nome
Address
I
Rann.t Tr,•
CHAIN OF CUSTODY RECORD
PAGE OF f
f lltered (Yes o)
Cooled es o)
Container Type /w)
Container Volume V Qf11t_:tuj
Somple T, posite)
Sample Source (WW, GW, DW, thee)
Scmpfe Source Chlof naAo (Yes/bio)
Telephone No. FAX No.
PO No. PrnJext No.! -
3
a
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Lob Receipt C1; Cite
K� �IMt lob Receipt pH Check
(}
Preserved (Code)
A-Nwo D-�NC0w 0-Doric Actd
8-HRO, E--HU H-Ascorbic Acid
C-H,M, r-mNs.u, i-
n
Rogers �C
Callcott
l.ob No,
Yr._
Dote
Time
Sample Description
IL
1�
9
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9fvr�
COMMENTS:
�4wj
050
O emu '-f - cab
SAMPLER
Relin wished b Sig.)
(D , -
Dote/Time!
I E31y
Received by (Siq.)
r .
ShiWar NuMs
Date/Time
KNOWN}S ASSOCIATED WM SAMPLES
Reltnquished by (Sig.)
Dote/lime
Alec ' by 1
Strip N m do
ate/1- ne
✓j! j W
Relinquished by (Slq-)
Q
Dote/Time
Received W (Sig
per Nome dot
Date/Time
Temperature of blank or representative sompie
At time of cdlectia
At time of fah receipt
Seal at'ehd b Recvd. lntoct Seal at'chd b
Recvd. Intact b
Fo77n Revised .3uN zoGa `-I

Rogers & Callcott
ENVIRONMENTAL
Sample Receipt Verification
Date j
Client: Received: I
Carrier Name: Client FedEx UPS US Mail Courier
Tracking Number: i7 117 �51 7, U
Work
Order:
Field Services Other:
Receipt Criteria
Y
e
s
o
A
Comments
Shipping container / cooler intact?
Damaged Leaking Other:
Custody seals intact?
COC included with samples?
COC signed when relinquished and received?
Sample bottles intact?
Damaged Leaking Other:
Sample ID on COC agree with label on bottle(s)?
Date 1 time on COC agree with label on bottles)?
Number of bottles on COC agrees with number of bottles received?
Samples received within holding tinge?
Sample volume sufficient for analysis?
VOA vials free ofheadspace (<6mm bubble)?
Samples cooled? Temp at receipt recorded on COC
Tcmp measured with IR thennometer - SN: 97050067
Ice Cold Packs Dry Ice None
Samples requiring pH preservation at proper pil?
Note: Samples for metals analysis may be preserved upon receipt in the tab.
�
G
If in-house preservation used -- record Lot #i!
HCL
Ham,
H2SO4
NaOH
HNO3
Other
Comments:
I Were non-conformance issues noted at sample receipt? Yes . or ( No / y -�-
1 Non -Conformance issue:
Revised November2012 Completed by:
Page 27 of 27

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PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Project Name:
CHAIN -OF -CUSTODY / Analytical Request
Client Name:
Address: plc/ u.s o
Report to:
Phone: 628 462 - 3 7 5'3 Fax:
PO Number: Yf 000 le ��&
Reauested Analvses
Project Number:
11 Checked Upon Receipt
Preservatives
C1, < 0.2.0 Upon Receipt
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Identification
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Samples Intact:
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Additional Comments:!
Printed Name of Sampler:
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�r

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _February 18, 2014
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls_
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Environmental Testing Solutions Lab Cert. #600mg/L
Comments on sample collection or analysis: See page 4
Part A: Stormwater Benchmarks and Monitoring Results
MaR 4 ZO)q .
;OENR.
SAND H
SAMPLE COLLECTION YEAR _2014
SAMPLE PERIOD ® Jan -June ❑ July -Dec
or ❑ Monthly'_ January (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
®Other: Class C, Swannanoa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -->
❑ No discharge this period?z
Outfall No.
Date Sample
Collected }
(mo/dd/yr)
24-hour rainfall
amount,
Inches -'Hydrocarbons
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Total Toxic
s
Organics
Benchmarks ===>
-
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
01-10-2014
0.52
34 mg/L
7.2
40.10 mg/L ,.
<0.020
.16 mg/L _
;' <5.0 mg/L
BRL
2
01-10-2014
0.52
8.2 mg/L
6.9
mg
<0.020
0.16 mg/L
` <5.0 mg/L
BRL
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
FFB 2 4 2014 r
Permit Date: 11/1/2012-10/31/2017 (._':;i' '��saiity Section SWU-245, last revised 10/25/2012
��tfill� Page 1 of 4

r
Facilities=that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
ay be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
ermit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the stormwater Pollution Prevention Plan."
Sal Vaccaro
Name (Print name)
General Manaee_ r
Title (Print title)
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX mg1V where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > SS gal of new oil per month.
❑ No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =_=?
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

4
Note: ifyou report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal and one copy of this DM& including all "No Discharge" reports, within 30 days of receipt of the lab results or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly respOsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are'sign'ihtant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 4

A
1) Copper reporting value exceeds permit limit 0.007 for Out -fall # 1
a). Finding;
i% Roofing material is 10 years old in the sample area and could be a contributing factor for both outfall sampling points.
ii) Scrap Lugger pad could be a contributing factor for outfall #1
b) Corrective actions;
i) Review BMP's,
ii) Increase housekeeping, Lugger Pad Area to be inspected weekly.
2) Zinc reporting value exceeds permit limit 0.067 for outfall 41
a) Finding;
i) Scrap Lugger pad could be a contributing factor for outfall 41 and #2.
b) Corrective actions;
i) Review BMP
ii) Increase housekeeping, Lugger Pad Area and Center Pad to be inspected weekly.
I
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 4 of 4

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _December 17, 2013
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Environmental Testing Solutions Lab Cert. #600mg/L
Comments can sample collection or analysis: See page 4
® Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2013
SAMPLE PERIOD ❑ Jan -June Z July -Dec
or ❑ Monthly'_ (monch)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
®Other: Class C, Swannanoa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period ?2
Outfall No.
Date Sample
Collected;
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks
-
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
09-25-2013
1.11
<5.0 mg/L
7.2
-0:078'mg&V
<0.020
10:12-mg/L
<5.0 mg/L
BRL
2
09-25-2013
1.11
6.4 mg/L
7.2
:900-29-mg/L
<0.020
0.042 mg/L
5.5 mg/L
BRL
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
DEC 2 3 2013
Permit Date: 11/1/2012-10/31/2017 I.B11LI Quality Section SWU-245, last revised 10/25/2012
,r-.Slheville Page 1 of 4

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Sal Vaccaro
Name (Print name)
General Manager
Title (Print title)
- :::�& I -dA, d,:r-'2 i,;2 -12 3
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?2
C1
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
+ A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER. AT ANYONE OUTFAft? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Dischaar a"_reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports] to:
Division of Water Quality
1ttn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
l y -/-13
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 4

1) Copper reporting value exceeds permit limit 0.007 for Outfall #1 and #2
a) Finding;
i) Roofing material is 10 years old in the sample area and could be a contributing factor for both outfall sampling points.
ii) Scrap Lugger pad could be a contributing factor for outfall #In
b) Corrective actions;
i) Review BMP's,
ii) Increase housekeeping, Lugger Pad Area to be inspected weekly.
2) Zinc reporting value exceeds permit limit 0.067 for outfall #1
a) Finding;
i) Scrap Lugger pad could be a contributing factor for outfall #1.
b) Corrective actions;
i) Review BMP
ii) Increase housekeeping, Lugger Pad Area to be Inspected weekly.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 4 of 4

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _December 17, 2013
CERTIFICATE OF COVERAGE NO. NCG030529
FACILITY NAME: Pentair Valves And Controls
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Gerald Runkles
LABORATORY: Environmental Testing Solutions Lab Cert. #600mg/L
Comments on sample collection or analysis: See page 4
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2013
SAMPLE PERIOD ❑ Jan -June ® July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
®other: Class C, Swannanoa River_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/Yr)
24-hour rainfall
amount,
lnches3
Total Suspended Solids
pH,
Standard units
' Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks =__>
-
-
100 mg/L or 5o mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
09-25-2013
1.11
<5.0 mg/L
7.2
0.078 mg/L
<0.020
0.12 mg/L
<5.0 mg/L
BRL
2
09-25-2013
1.11
6.4 mg/L
7.2
0.029 mg/L
<0.020
0.042 mg/L
5.5 mg/L
BRL
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 4

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Sal Vaccaro
Name (Print name)
General Manager
Title (Print title)
.- :::&i / /,0,6,dzL:12i--;2 -IR3
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
Imo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (5GT-HEM)
Total Suspended Solids
pH
Benchmarks
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 4

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab resultslor at end of monitoring period
in the case of "No Discharge" reports? to:
Division of Water Quality
ttn: DWQ Central Files
.617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
/�-�-1�
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 4

1) Copper reporting value exceeds permit limit 0.007 for Outfall #1 and #2
a) Finding;
i) Roofing material is 10 years old in the sample area and could be a contributing factor for both outfall sampling points.
ii) Scrap Lugger pad could be a contributing factor for outfall #In
b) Corrective actions;
i) Review BMP's,
ii) Increase housekeeping, Lugger Pad Area to be inspected weekly.
2) Zinc reporting value exceeds permit limit 0.067 for outfall #1
a) Finding;
i) Scrap Lugger pad could be a contributing factor for outfall #1,
b) Corrective actions;
i) Review BMP
ii) Increase housekeeping, Lugger Pad Area to be Inspected weekly.
0
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 4 of 4

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STORM WATER POLLUTION PREVENTION PLAN (SWP3)
Pentair Valves and Controls (PVC)
(Formerly Tyco Valves and Controls)
953 Old US Highway 70
Black Mountain, North Carolina 28711
APPLICABLE REGULATORY STATUTES & LAWS
• CLEAN WATER ACT (CWA) - 33 USC 1251, 40 CFR PARTS 122, 124.
• NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM - 33 USC 1342.
• NORTH CAROLINA GENERAL STATUTE 143-215.1.
• NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL
RESOURCES - DIVISION OF WATER QUALITY - GENERAL PERMIT NO. NCG030000
These provisions satisfy the regulatory requirements of a Storm Water Pollution Prevention
Plan, and will hereafter be referred to as the "SWP3".
RESPONSIBLE PERSONNEL
Sal Vaccaro
General Manager
Gerald Runkles
EHS Manager
Also serves as, Environmental (Emergency) Coordinator
IMPLEMENTATION DATE: April 1, 2006
Revision: March 17, 2009
Revision: Updated December 2011
Latest Revision: June 18 2013
Original Plan written 412312004 by: James W. Brown, CSP and CHMM— EHS Associate
Tyco Engineered Products & Services
COPY OF

Pentair Valves & Controls — Black Mountain, NC SWP3
STORM WATER POLLUTION PREVENTION PLAN (SWP3)
TABLE OF CONTENTS
Page
Management Approval and Implementation
4
Emergency Coordination Acknowledgment
4
Preamble Statement
5
Facility Contact Information
6
1.0 Site Plan
1.1 General Location and Map
7
1.2 Description of Critical Practices and Activities
7
1.3 Site Map
7
1.3.1 Drainage System
8
1.3.2 Predicted Drainage Flow
8
1.4 Description of Potential Pollution Sources
9
1.4.1 Significant Exposed Materials
9
1.4.2 Water Priority Chemicals
9
1.4.3 Risk Identification and Assessment
9
1.5 Significant Spills or Leaks of Pollutants
11
1.6 Certification of Non -Storm Water Discharges
11
1.6.1 Potential Significant Sources
11
1.6.2 Certification Format
11
2.0 Storm Water Management Plan
2.1 Feasibility Study 12
2.2 Secondary Containment Schedule 12
2.3 Best Management Practice (BMP) Summary 12
2.4 Inspection Schedule 13
3.0 Spill Prevention and Response Plan
3.1
General Spill Prevention and Response Procedures
13
3.1.1 Prevention and Controls
13
3.1.2 Bypassing of Storm Water Control Facilities
14
3.1.3 Response Requirements
11
3.2
Storm Water Pollution Prevention Team (SWPPT)
16
3.3
SWPPT Methodology
16
3.4
Additional response and reporting
16
3.5
Duties of the SWPPT Leader
16
4.0 Preventive
Maintenance and Good Housekeeping Program
4.1
Good Housekeeping
17
4.2
Preventive Maintenance
17
4.3
Sediment and Erosion Control
18
Page 2

Pentair Valves & Controls — Black Mountain, NC SWP3
5.0 Employee Training
5.1 Training for SWPPT and Others 19
5.2 Training Program Responsibility 19
5.3 Training topics 19
6.0 Responsible Party 19
7.0 Plan Amendment and Review 20
8.0 Facility Inspections
8.1 Ongoing Inspection Program 20
8.1.1 Weekly 20
8.1.2 Monthly 20
9.0 Storm Water Discharge Characteristics Monitoring
9.1 Storm Water Discharge Monitoring
21
9.1.1 Representative Sampling and Storm Event
21
9.1.2 Representative Outfall
22
9.2 Analytical Monitoring Requirements
22
9.2.1 Laboratory Certification
22
9.2.2 Discharge Monitoring Report (DMR)
22
9.3 Qualitative Monitoring Requirements
23
9.3.1 First Monitoring Event
23
9.3.2 Semi -Annual Monitoring Requirements
23
9.3.3 Documentation
23
10.0 Implementation
23
Appendixes
Appendix I
SWP3 Review and Revisions Record
Appendix II
Site Map - Aerial View[Topographic Features
Appendix III
Site Map - Storm Water Drainage
Appendix IV
Inventory of Exposed Significant Materials
Appendix V
Storm Water Pollution Event Record Sheet
Appendix VI
Certification of Testing for Non -Storm Water Discharge
Appendix VI
Equipment Preventive Maintenance Inspection Checklist
Appendix Vlll
SWPPT Training Record
Appendix IX
Storm Water Point Source and Outfall Inspection Record
Appendix X
Storm Water Discharge Outfall (SDO) Monitoring Report
Appendix XI
Qualitative (Visual) SDO Monitoring Record
Page 3

Pentair Valves & Controls — Black Mountain, HC SWP3
MANAGEMENT APPROVAL AND IMPLEMENTATION
This Storm Water Pollution Prevention Plan (SWP3) and the associated Best Management
Practices are approved by the management team of Pentair Valves & Controls, Black Mountain,
NC and will be implemented as described herein. It is understood that in the event of an
emergency event as described herein, the plan may be implemented at the discretion of the
EHSIMaintenance Supervisor & Environmental Coordinator or his designated alternate.
Signature:
Name: Sal Vaccaro
Date:
Title: General Manager
ENVIRONMENTAL COORDINATOR ACKNOWLEDGEMENT
I hereby acknowledge my role and responsibilities for implementing and monitoring all aspects
of this Storm Water Pollution Prevention Plan (SWP3) and the associated Best Management
Practices (BMP) described herein.
Signature: Date:
Name: Gerald Runkles Title: EHS Manager
Environmental Coordinator
Page 4

Aentair Valves & Controls — Black Mountain, NC SWP3
STORM WATER POLLUTION PREVENTION PLAN
Preamble Statement
DATE: April 1, 2006
SUBJECT: SWP3 for Pentair Valves and Controls, Black Mountain, NC
STATE REGULATORY STANDARD: North Carolina General Statute 143-215.1.
BASIS
The federal Clean Water Act (CWA) prohibits any person from discharging pollutants into a
waterway from a point source unless a permit issued either by EPA or an authorized state
agency authorizes the discharge. The National Pollutant Discharge Elimination System
(NPDES) permit program forms the cornerstone of the federal program.
DEFINITIONS
Storm water, defined in 40 CFR 122.26(b) (3) as "storm water runoff, snow melt, and surface
runoff and drainage" which is associated with industrial activity must discharge through a oint
source.
Point source discharge of storm water; as defined in Part VI (Definitions) of the North
Carolina Department of Environment and Natural Resources (NCDENR) Division of Water
Quality General Permit No NCG030000, is "any discernible, confined and discrete conveyance
including, but not specifically limited to, any pipe, ditch, channel, tunnel, conduit, well, or
discrete fissure from which storm water is or may be discharged to waters of the state." Point
source discharge may include storm water that flows off facility property, funnels into a naturally
occurring ditch, and issues into a water body.
Storm water discharge, associated with industrial activity is defined by EPA, discharge from
any conveyance that is used for collecting and conveying storm water and that is directly related
to manufacturing, processing, or raw materials storage areas at an industrial plant.
Storm Water Pollution Prevention Plan (SWP3), as defined in NCDENR's General Permit No
NCG030000, is a comprehensive site -specific plan, which details measures and practices to
reduce storm water pollution, and is based on an evaluation of the pollution potential of the site.
PURPOSE AND PLAN MAINTENANCE
The primary purpose of the SWP3 is to provide a step-by-step process for ensuring that
pollutants do not enter storm water discharges originating from the Pentair Valves and Controls
facility site in Black Mountain, NC. The SWP3 includes the use of Best Management Practices
(BMPs) — both non-structural and structural. As required under the NPDES General Permit,
BMPs are designed to prevent or minimize storm water exposure to pollutants, and provide
required degrees of sediment and erosion control. The Emergency Coordinator is the sole
person authorized to amend the plan. SWP3 reviews and amendments shall be documented
using Appendix I. The Emergency Coordinator shall maintain the master copy of the SWP3 at
the Pentair Valves and Controls - Black Mountain facility.
Page 5

Pentair Valves & Controls — Black !Mountain, NC SWP3
REGULATORY COMPLIANCE
The requirement that Pentair Valves and Controls - Black Mountain develop and implement a
SWP3 is the most significant condition of compliance under the NCDENR Division of Water
Quality General Permit for storm water point source discharges associated with Metal
Fabrication activities (General Permit No. NCG030000). The Pentair Valves and Controls,
Black Mountain certification number under NCDENR's General Permit is NCG030529
ADMINISTRATION AND ENFORCEMENT
As authorized by EPA under the NPDES program, NCDENR's Division of Water Quality
administers and enforces the state's storm water discharge permit rules. Violations of NPDES
General Permit provisions under the Clean Water Act (CWA) can bring administrative, civil, and
criminal penalties punishable by fines up to $50,000 per day of violation and/or imprisonment
for not more than 3 years. Under North Carolina law (NC General Statutes 143-215.6A), a daily
civil penalty of not more than $10,000 per violation may be assessed against any person who
violates or fails to act in accordance with the terms, conditions, or requirements of a permit.
Pentair Valves and Controls, Black Mountain, NC shall comply with all applicable conditions of
General Permit No. NCG030000.
FACILITY CONTACT INFORMATION
OWNER/OPERATOR INFORMATION
Pentair Valves & Controls (formerly Tyco Valves and Controls)
953 Old US Highway 70
Black Mountain, North Carolina 28711
[phone]
OWNER OR PARENT COMPANY
Pentair Valves & Controls LP
10707 Clay Rd Ste 200
Houston, Texas 77041,
[phone].
OPERATOR OR PERSON IN CHARGE OF FACILITY
Sal Vaccaro - General Manager
[phone] work hours
[phone] cell / non -work hours
EMERGENCY COORDINATOR
Gerald Runkles — EHS Manager and Environmental Coordinator
[phone] work hours
[phone] cell / non -work hours
BACK-UP EMERGENCY COORDINATOR
Dan McPeters - Maintenance Lead
[phone] work hours
[phone] cell / non -work hours
Page 6

Pentair Valves & Controls — Black Mountain, NC 5WP3
1.0 SITE PLAN.
1.1 General Location and Map. Pentair Valves and Controls (PVC) (formerly Tyco Valves
and Controls) is located at 953 Old U.S. Highway 70 in the city of Black Mountain, North
Carolina 28711 (Buncombe County). The surrounding area consists of residential property (for
example, private homes along the east properly line of the manufacturing building) integrated
with light manufacturing facilities, municipal, and other commercial or public property to the
west. The nearest significant body of water or navigable waterway is a creek tributary, which
runs along the east and south property lines of the manufacturing building and the south
property line of the Drexel warehouse building. The Swannanoa River is a navigable waterway
of Western North Carolina regulated under the authority of NCDENR's Division of Water
Quality, Appendix II depicts an aerial view of the facility in relation to transportation routes,
surface waters, and other topographic features required by Part II Section A.1 of the General
Permit No. NCG030000.
1.2 Description of Critical Practices and Activities. The facility is engaged in the
manufacture of safety relief valves, pressure regulators and Penberthy products for commercial
industrial clients. Industrial operations and processes conducted at the facility include receiving
raw materials and parts, material handling, storage, machining, sub -assembly, assembly,
testing, painting, packaging and shipment of finished products. Other functions housed at the
facility include product design, engineering, plant administration, payroll, order processing and
customer service. The facility normally operates 1" and 2nd shift five days a week with overtime
on weekend, when needed. PVC work force includes approximately 150 employees. The United
States Department of the Interior has verified that "no federally endangered or threatened
species or their habitats occur on or in close proximity of the facility". The local Black Mountain-
Swannanoa Chamber of Commerce has verified that "there are no historic sites or known
animal species or plants that are affected by the facility storm water run-off'.
The facility is comprised of two buildings:
• The primary building located at 953 Old Highway 70 sits on a 7.5 acre parcel of land and
is approximately 45,000 square feet of covered manufacturing, product testing,
engineering and maintenance support, and administrative spaces.
• A support building, known as the Drexel Warehouse/Building #200 and part of a closed
furniture manufacturing operation, is located on about 2 acres of land approximately 100
yards to the southwest . of the main facility. Functions contained in the approximately
23,000 square foot Building #200 are marketing, sales, customer service, lapping
operations, material receiving, warehouse storage of parts, subassemblies and finished
goods.
1.3 Site Maps. Maps contained in Appendix III, Storm Water Drainage, depict the storm
water drain systems for the Pentair Valves & Controls - Black Mountain facility. The maps
identify buildings and grounds, material loading and unloading areas, exterior material storage,
and waste management areas. The maps show the location of all existing storm water
collection structures, flow channels and directions, and discharge points to the environment
(Outfalls 001 — 003).
Page 7

Pentair vaives & Controls — Black Mountain, AFC swP3
1.3.1 Drainage System. Both the main manufacturing/administration building and separate
warehouse building are built on concrete slabs. Facility drainage systems include interior floor
and plumbing drains connected to a permitted sanitary sewer and industrial (processing)
wastewater system for discharge into the local publicly operated treatment works (POTW), and
exterior storm water collection systems that discharges to the environment. The natural
topography of the grounds and engineered gradient of gravel and/or paved areas channel storm
water and non -storm water runoff into one or more water drainage collection structures (e.g.,
storm drain gratings, piping, sluice, gully, etc.) located outside the buildings.
1.3.2 Predicted Drainage Flow. As depicted in Appendix ill, there are several natural and
man-made features at the facility for storm water collection and discharge. The property is
graded and planted with grass, trees, and other landscaping to channel drainage into the storm
water collection systems. Roofs of both buildings are sloped and fitted with drains, gutters and
downspouts for collecting and channeling rainwater. In addition, asphalt and gravel roads and
employee parking and truck maneuvering areas are sloped to channel storm water and non -
storm water discharge into one of the 8 Outfalls serving the property. Arrows indicate predicted
drainage flow. Three storm water systems for the Manufacturing Building and five storm water
systems for the Drexel Warehouse provide water collection, drainage and discharge as
described below:
Outfall 001: Storm water runoff is collected from the manufacturing building's east and
northeast lawns, loading dock ramp, outside scrap storage pad, and lower parking lot and is
channeled into a 2 ft. wide concrete sluice for discharge through Outfall 001 located in the
southeast quadrant of the property. Outfall 001 discharges into the creek tributary that runs
along Pentair`s east and south property lines. The creek flows west to the Swannanoa
River.
• Outfall 002: Storm water runoff from roof downspouts serving the plant roof east of the open
concrete material storage slab (located south side of the manufacturing building) is collected
in a buried pipe and channeled for discharge to the creek tributary through Outfall 002, a 6
inch drain pipe located approximately midway between Outfalls 001 and 003, and situated
down slope from a gravel road that runs behind the south side of the plant and empties onto
the sloping bank with a run of approximately 20 feet to reach the creek. Riprap stone is
installed around the drain exit to minimize erosion of the grass -covered slope. The creek
flows west to the Swannanoa River.
• Outfall 008: Features on the west side of the Drexel warehouse include a covered elevated
loading dock and gravel approach, a gravel -covered truck maneuvering and parking area
and a grassy lawn sloping to the creek a short distance to the south. Due to natural
topography, storm water from this area is channeled south from the loading dock south
through a swale down to the creek, where riprap stone minimizes erosion where it empties
into the creek bank. The creek flows west to the Swannanoa River. Outfall 008 is located a
short distance downstream from Outfalls 004 through 007.
Two rectangular drainage grates located along the north side of the Drexel warehouse
building collect storm water runoff from roof downspouts and asphalt parking/driving areas
immediately surrounding the building. Due to pavement slope, some storm water would be
Page 8

Pentair Valves & Controls — Black Mountain, NC 5WP3
diverted away from the warehouse and collected into drainage grates located in loading
dock wells belonging to an adjacent building of the former Drexel furniture factory. It is
believed that storm water collected by these grates flows into a larger storm water drain
system that served industrial buildings of the old Drexel Furniture factory complex. Due to
this area being used as a vehicle travel lane, there is no Pentair Valves and Controls
material storage or production activity; it is unlikely that pollutants will contaminate storm
water drainage through these grates.
1.4 Description of Potential Pollution Sources. Potential sources that may reasonably be
expected to add pollutants to storm water discharges have been identified. With the possible
exception of used oil spilled from storage drums, the discharge of pollutants into storm sewers
from listed potential sources during dry weather is unlikely.
1.4.1 Significant Exposed Materials. An inventory by type of materials handled and stored at
Pentair Valves and Controls - Black Mountain that has potential to be exposed to
precipitation is provided in Appendix IV, Inventory of Exposed Significant Materials.
1.4.2 Water Priority Chemicals. Pentair Valves and Controls - Black Mountain stores and
uses materials that contain water priority chemicals as defined by Federal EPA and listed
under SARA (EPCRA) Title III, Section 313. Process and spent material on site in
significant quantities include: brass bar stock and processed scrap (turnings) containing
Copper (CAS 7440-50-8) and Lead (CAS 7439-92-1); respectively; stainless steel bar
stock and processed scrap (turnings) containing Chromium (CAS 7440-47-3), copper,
Nickel (CAS7440-02-0), and Yellow Phosphorous (CAS 7723-14-0); gray iron parts
containing chromium and nickel; bronze castings and processed scrap (turnings)
containing copper and lead; boiler water test kits containing Sulfuric acid (CAS 7664-
93-9); forklift truck batteries containing lead and sulfuric acid; solvent spray paint booth
production material and hazardous waste containing Ethylbenzene (CAS 100-41-4),
Toluene (CAS 108-88-3), Xylene (CAS 1330-20-7) and wooden crates for incoming
China parts treated with Methyl bromide (alias Methyl methacrylate, CAS 80-62-6).
Practices taken to minimize exposure of materials to water priority chemicals are
delineated in Section 2.3, Best Management Practice (BMP) and Appendix IV.
1.4.3 Risk Identification and Assessment. A risk identification and assessment has been
made of potential pollutant sources existing at facility areas. Potential storm water exposure is
judged to be High (material often is delivered, handled, and/or stored outside and uncovered),
Medium (material is stored outside but is covered), or Low (material is used and/or stored
inside).
• Category 1 - Load inglunloading operations
• Category 2 - Outdoor storage activities
• Category 3 - Outdoor manufacturing or processing activities
• Category 4 - Significant dust or particulate generating processing
• Category 5 - On -site waste disposal practices.
CAT
Significant
Location
Pollutant /
Potential
Past
Potential Pollution
(Mfg = Manuf. Bldg;
Parameter of
SW
Significant
Source
WH = Warehouse)
Concern
Exposure
Spill or Leak
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Pentair Valves & Controls - Black Mountain, NC 5WP3
1
Brass bar stock
Mfg: Inside storage
Copper, Lead
High *
None
racks
1
Stainless steel tsar
Mfg: Inside storage
Chromium,
High *
Nome
stock
racks
Copper, Nickel,
Phosphorous
1,2
Processed brass,
Mfg: Covered steel
Copper, Lead
Med
None
turnings scrap
lugger on drip pan
outside pant
1,2
Processed bronze,
Mfg: Covered steel
Copper, Lead
Med
None
turnings scrap
lugger on drip pan
outside plant
1,2
Processed
Mfg: Covered steel
Chromium,
Med
None
stainless steel,
lugger on drip pan
Copper, Nickel,
turnings scrap
outside plant
Phosphorous
1, 2, 5
Metal floor
Mfg: Covered steel
(Potentially)
Med
None
sweepings and
lugger on drip pan
Copper, Lead,
mixed turnings
outside plant
Chromium,
Copper, Nickel,
Phosphor us
1, 2, 5
Waste paint
Mfg: Waste matl
Ethylbenzene,
Med
None
related material,
drummed and stored
Toluene, Oil,
used water/oil,
outside in
Xylene
used lapping
containment shed
compound
1, 2, 5
Treated wooden
Mfg: Stored inside
Methyl bromide
Med
None
crates for
semi -trailer East side
incoming parts
parking lot
from China
WH: Stored inside
semi -trailer at West
side roll -up door
2
Transformer Oil
Mfg: PIE room and
Oil
Med
None
See Note 1
transformer bank
1,5
Washer Liquid
Bowden parts washer
BB-1818
Med
None
1, 2, 5
Used wooden
Mfg: Stored inside
Oil and grease
Med
None
pallets (not
semi -trailer East side
exposed to
parking lot
production
WH: Stored inside
processes)
semi -trailer at West
side roll -up door
1, 2, 5
Cardboard waste
Mfg: East outside in
Oil, grease
Med
None
covered dum ster
1, 2, 5
Plant trash
Mfg: Trash
Oil, grease
Med
None
compactor located in
East parking lot
1
Grey iron parts
Mfg: Inside storage in
Chromium, Nickel
Low
None
boxes
1
Bronze castings
WH: Inside storage in
Copper, Lead
Low
None
crates
1
Brass scrap solids
Mfg: Matl Review
Copper, Lead
Low
None
Area inside facility
1
Stainless steel
Mfg: Matl Review
Chromium,
Low I
None
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Pentair Valves & Controls - Black Mountain, NC SWP3
scrap solids
Area inside facility
Copper, Nickel,
Phosphorous
1
Paint related
Paint booth area,
Toluene, Xylene
Low
None
materials
Paint storage
cabinets
1
Oils, lubricants
Mfg: Machine shop
Oil, grease
Low
None
and tool crib
* = Bar stock is delivered to the facility by open -bed truck and is often not crated or otherwise
packaged to avoid contact by rainwater during transit.
Note: 1. Transformers are maintained by electric power provider (Progress Energy) who is
solely responsible for spill clean-up, if needed,
1.5 Significant Spills or Leaks of Pollutants. There have been no significant events
involving spills or leaks of any toxic, hazardous, or non -hazardous materials at Pentair Valves
and Controls - Black Mountain in the past three years that have exposed pollutants to storm
water or to other precipitation. If a significant spill or leak event occurs that results in storm
water pollution during the term of the permit certification, the incident will be recorded in
Appendix V, Storm Water Pollution Event Record Sheet. The SWP3 will be updated as required
once methods to prevent or control future spills or leaks have been identified.
1.6 Certification of Non -Storm Water Discharges.
1.6.1 Potential Significant Sources. The following non -storm water discharges may
occur periodically at the Pentair Valves and Controls - Black Mountain facility:
• Flows from fire fighting activities
Fire hydrant and potable water line flushing; no detergents, other chemical
compounds, or chlorine concentrations above detectable limits (average at the
outfall) or exceeding 0.5 mg/L (occasional peak) are allowed
• Lawn watering
• Routine external building wash -down that does not use detergents or other
compounds
• Pavement wash waters where minor spills or leaks of toxic or hazardous
materials (e.g., motor oil) have not occurred; unless all spilled material has
been removed and detergents not used
• Air conditioning condensate
• Permitted non -contacted machinery cooling water evaporator condensate.
1.6.2 Certification Format. In compliance with Part II Section A.1 (e); of General
Permit No NCG030000, a certification that outfall discharge has been evaluated
for the presence of non -storm water discharges shall include the following:
• Identification of potential significant sources of non -storm water at the site
• Description of test and/or evaluation results for the presence of non -storm
water discharges
• Evaluation criteria or testing method used
• Date of test and/or evaluation
• On -site drainage points that were directly observed during the test and/or
evaluation.
"I certify, under penalty of law, that this document and all attachments were prepared under my
direction or supervision in accordance with a system designed to assure that qualified personnel
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Pentair Valves & Controls - Black Mountain, NC SWP3
properly gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
The Certification that storm water outfalls have been evaluated for the presence of non -storm
water discharges is contained in Appendix VI, Certification of Testing for Non -Storm Water
Discharge,
2.0 STORM WATER MANAGEMENT PLAN
2.1 Feasibility Study. The Risk Identification and Assessment delineated in Section 1.4.3
of the SWP3 points out that the way to reduce the potential for storm water exposure of
materials listed in the "High" category is to package and/or cover bar stock during
transport. Requiring and accomplishing this action for 100% of stock purchases and
every delivery has been considered, but is not economically feasible as of the SWP3
implementation date. The BMP to reduce the exposure (the expeditious moving of
delivered material inside the plant, and enforcing the policy of storing all bar stock inside)
will be implemented.
2.2 Secondary Containment Schedule. The plant's schedule for secondary containment
protection of storm water pollution events from the release of bulk liquid materials, SARA
Title III Section 313 water priority chemicals, and hazardous substance storage includes
(1) a RCRA-compliant satellite storage area is provided for solvent spray paint booth
liquid materials, and (2) drummed used oil, other non -hazardous material, and hazardous
waste is stored on a RCRA-compliant outside storage pad that is covered and protected
by secondary containment.
2.3 Best Management Practice (BMP) Summary. A combination of nonstructural and
structural BMP's have been implemented to minimize the potential for pollutants to enter
into the storm water draining from the Pentair Valves & Controls - Black Mountain facility.
BMP's are presented in detail as a column in Appendix VI. In general, non-structural
BMP's are procedural in nature, and include the following:
• Unless it is absolutely necessary, no material handling activity is to take place
outdoors during a rainstorm.
• Whenever possible, delivery vehicles are properly backed and material is loaded
or unloaded under cover of shipping dock overhangs.
• Metal bar stock, parts, and castings will be stored or processed inside the
manufacturing building or warehouse; material stored outside will be covered and
not exposed directly to rain.
• Processed metal scrap is stored in covered Lugers awaiting disposal. Secondary
containment consists of drip pans under each Luger. There is a curb around the
slab with an emergency drain plug. There is also a barrel of absorbent material
and socks stored on the concrete slab.
• Empty insecticide -treated wooden crates will be stored inside semi -trailers
awaiting disposal.
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Pentair Vales & Controls — Black Mountain, MC SWP3
• Cardboard and paper trash is collected in a covered trash compactor or bins.
Structural BMPs for storm water pollution prevention include the following:
• Drummed used oil, other non -hazardous material, and hazardous waste are
stored on a RCRA-compliant outside storage pad that is covered and protected by
secondary containment.
2.4 Inspection Schedule. The Emergency Coordinator will schedule, monitor, and
document inspections of storm water conveyances, controls, and measures to be taken
to limit or prevent erosion associated with storm water systems as required in Part II
Section A.2. NCDENR General Permit No NCG030000. A detailed description of
site inspection criteria, methodology, and periodicity is presented in Part 8 of this Plan.
3.0 SPILL PREVENTION AND RESPONSE PLAN.
3.1 General Spill Response Procedures.
• Response procedures during an on -site environmental emergency (including spill
detection and control for the release of oil, oil -based material, hazardous and non-
hazardous substance, or other potential pollutants) at the Pentair Valves &
Controls - Black Mountain facility are managed by the Emergency Coordinator.
• Any spills of potential pollutants occurring at the facility shall be responded to, and
the incident shall be recorded in Appendix V.
• Procedures, including what cleanup equipment to use, are contained in
substance -specific response actions (e.g., metal cutting machines coolants/oils,
solvent paint booth materials, used lapping compound, etc.) found in the facility's
Spill Response Plan source document.
• For all intents and purposes, spill response team personnel described in the
facility's Spill Response Plan source document and SW PPT members are one
and the same. Team members receive training on applicable spill prevention and
response procedures.
• Emergency response equipment necessary to contain spills, to prevent pollutants
from entering the storm water drainage system, and to clean up the spill area is
kept available for use at all times.
3.1.1 Spill Prevention and Controls. Procedures and controls that help minimize the
chance of pollutants entering the storm water drainage system include:
• Care in loading/unloading containers or drums of bulk oil, lubricants, or solvents,
or other liquids at shipping/receiving loading docks.
• Availability and close proximity of spill stations and absorbent material to the
loading docks and other areas where spills of exposed material could occur.
• Enforcing BMP work procedures to include (1) not allowing outside storage of
spillable materials, and (2) training employees to take extra care in loading trash
or debris into the metal scrap luggers, dumpsters and trash compactor so as to
prevent spillage.
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Pentair Valves & Controls - Black Mountain, NC SWP3
• Training of SWPPT personnel to identify spilled material, and hazards to human
health and the environment posed by spills, to make prudent decisions, and to
initiate correct response actions (e.g., emergency notifications, block spills from
entering storm water drains and other point sources, etc.)
3.1.2 Bypassing of Storm Water Control Facilities. A bypass is the known diversion
of storm water from any portion of a storm water control facility, including the
collection system (e.g., sluice, drain grates, roof downspout piping, etc.), which is
not a designated or established operating mode for the Pentair Valves & Controls
- Black Mountain facility. In accordance with Part III Section C.3 of the General
Permit, bypass is prohibited unless:
• It is unavoidable to prevent loss of life, personal injury, or severe property
damage; and
• There is no feasible alternative to the bypass.
Notices to NCDENR and other agencies must always be submitted as delineated in
Section 3.1.3 of the SWP3.
3.1.3 Response Requirements. All Pentair Valves and Controls - Black Mountain
personnel shall take all reasonable steps to minimize or prevent noncompliance
(e.g., process bypass, system changes, or other actions that could result in
discharges of pollutants in violation of General Permit No. NCG030000
requirements, etc.), that may endanger health or the environment. In general,
actions upon discovering a noncompliance situation shall include:
• Initial Notification. During 1st Shift work hours, immediately notify the
Emergency Coordinator by overhead page or V dialing "3753" or the Back -Up
Emergency Coordinator by dialing "3718". 4n 2n Shift, notify the Shift Supervisor
by overhead page or by dialing "3709". At a minimum, be prepared to tell the
Emergency Coordinator, Back -Up Emergency Coordinator or Shift Maintenance
Lead Man the following:
o Your name,
o Location and time of the spill or other noncompliance event,
o Material discharged to the environment (Give process, Container label,
Substance, Color, Smell, etc.), and
o Approximate amount of the discharge (judge by container size - 1 gal. can,
55 gal. drum, etc.) or by floor space covered (3 ft. diameter spill, an area of
about one parking space, etc.).
• Spill Control Actions. To prevent migration, the discharge source shall be
determined, leakage contained and/or stopped, and additional discharge
controlled. In no instance should any person, including SWPPT members,
attempt to stop or contain discharged material without proper training, equipment,
or backup personnel. Specific discharge. control actions include:
Response personnel shall initially use granular floor absorbent, mats, pads, socks,
and equipment from the nearest spill control station or kits to contain the spill and,
Page 14

Pentair Valves & Controls — Black Mountain, NC SWP3
if necessary, channel any liquid flow away from drains, from beneath doors, or
other external routes to soil or surface water.
For any discharge occurring inside or outside the plant in the vicinity of loading
docks or truck wells, response personnel shall take extraordinary- measures to
block discharged material from reaching storm water drains.
Additional equipment and absorbent material shall be brought to the area and
shall be used as needed for discharge containment and clean up.
• Emergency Coordinator Action. The Emergency Coordinator (or, in his
absence, a designated alternate) will determine if reporting a spill to outside
agencies is required. Where, in a 24 hour period, a release occurs containing a
hazardous substance (e.g., oil, hazardous materials, copper and/or storm water
runoff tainted with SARA Title III Section 313 water priority chemicals such as
copper, chromium, lead, nickel, sulfuric acid, etc.) in the amount equal to or in
excess of the reportable quantity (RQ) established under 40 CFR 117 or 40 CFR
302 for that hazardous substance, the following compliance action steps must
take place. In addition, NCDENR defines in Section E.8 of the General Permit No.
NCG030000 that a spill "...or any noncompliance which may endanger health or
the environment" must be reported within 24 hours" from the time of knowledge of
the incident.
Step 1: Report the potential water pollution incident to the 24-hour NCDENR
Emergency Spill Response Hotline at 1-800-858-0368 and the EPA 24-hour
National Response Center at 1-800-424-8802. The Storm Water Pollution Event
Record Form (Appendix V) shall be used to collect and report as much information
as possible. However, do not delay making the initial report waiting on information
to fill in the form. Make the initial report and provide more information in follow-up
calls if necessary.
Step_2: A written submission must be provided to the North Carolina Division of
Water Quality, Storm Water and General Permits Unit, 1617 Mail Service Center,
Raleigh, NC 27699-1617 (Phone: [phone], Fax: [phone]) within 5
days of knowledge of the potential pollution discharge event. In accordance with
Section E.8 of the General Permit, the written submission shall contain the
following information:
o A description of the noncompliance incident and its causes,
o The period of noncompliance, including exact dates and times,
o If the noncompliance has not been corrected, the anticipated time when
compliance is expected, and
a Steps taken or planned to reduce, eliminate, and prevent reoccurrence of
the noncompliance event.
Step 3: Within 14 calendar days of knowledge of the release, a written report of
the incident must be submitted to EPA Region 4, 61 Forsyth Street, S.W., Atlanta,
GA 30303-3104. The report must describe the following elements:
Page 15

Pentair Valves & Controls — Black Mountain. NC SW133
o The release (type and amount of material released),
o Date release occurred,
o Circumstances leading to the release, and
o Steps and measures taken to prevent the reoccurrence of the release and
to improve response if appropriate.
Step 4: Within 14 calendar days of knowledge of the release, the SWP3 shall be
reviewed to identify measures to prevent reoccurrence and to improve response to
such releases. The SWP3 is to be modified where appropriate. Section 4.4
(Spills and Leaks) of the SWP3 will be updated to include listing of the release
event. Post -release reviews and revisions are to be recorded in Appendix I.
3.2 Storm Water Pollution Prevention Team (SWPPT). The SWPPT is headed by the
EHS Manager and Environmental Coordinator, who is the facility's designated Emergency
Coordinator. Administrative responsibilities of the SWPPT are to assist the Emergency
Coordinator to develop, implement, and maintain proficiency in the Spill Prevention and
Response Plan (SPRP) segment of the overall SWP3. Operational responsibilities of the
SWPPT include taking action to ensure (through a program of training, process research, and
periodic facility inspections) that methods are being taken to minimize the risk of storm water
pollution and responding to incidental spills or leaks that could infiltrate the facilities storm water
system. The members of the team and their primary responsibilities are tabulated below:
Name
Contact Information
Responsibilities
Gerald Runkles
828 669-3753 work
• Emergency Coordinator
EHS Manager
828 301-4053 cell
. SWPPT Leader
Environmental Coordinator
828 505-5572
Dan McPeters
828 669- 3718 work
• Back -Up Emerg Coord
Maintenance Lead Man
828 545-9767 cell
. Alternate SWPPT Leader
828 669-5515
• SWPPT Member
2nd Shift Supervisor
828 cell
3.3 SWPPT Methodology. The SWPPT will train, prepare and, during a spill incident, work
to prevent and eliminate all forms of pollution, especially the kind that could infiltrate the facility's
storm water collection system. Shift Supervisors shall render assistance when needed and as
directed by the SWPPT Leader or Alternate.
3.4 Additional Response and Reporting. Spills or leaks involving oil or oily substances
defined and regulated by 40 CFR Part 112.2 may require additional emergency response,
contact/notification, and spill reporting (e.g., local, state and federal agencies, etc.)
3.5 Duties of the SWPPT Leader. With respect to the SWP3, specific duties of the.SWPPT
Leader include, but are not necessarily limited to, the following:
• On behalf of management, maintain overall responsibility for the SWP3.
Page 16

Pentair Valves & Controls — Black Mountain, NC SWP3
• Coordinate program requirements with management, team leaders, and
employees to develop, implement and enforce appropriate storm water pollution
prevention procedures and Best Management Practices (BMPs).
Assist team leaders to develop practices, precautions, and procedures to minimize
risk of release of polluting substances into storm water point sources, channels
and ditches, and/or outfalls.
• Conduct a comprehensive inspection of the facility physical site, operations, and
SWP3 every 12 months, at a minimum, to ensure that BMPs and controls are still
effective and that the SWP3 is up to date. Record accomplishment of periodic
reviews and copies of annual inspection memos in Appendix 1.
• Perform or supervise periodic (at least monthly) and post -heavy rainfall
inspections in and around the facility, including visual inspections of all storm
water point sources and outfalls on Pentair Valves and Controls' - Black Mountain
property. Take or supervise action to clear debris that clog or have the potential to
clog point sources, channels and ditches, and/or outfalls. Ensure all inspections
and field actions are documented using the format in Appendix IV.
• Train members of the SWPPT to conduct visual inspections and monthly
preventive maintenance inspections, as required, to ensure policies and BMPs
remain valid as designated in the SWP3.
• Ensure that appropriate training has been provided to all employees involved in
SWP3 procedures and responsibilities as designated in the SWP3.
M Maintain current knowledge concerning the regulatory compliance and legal
requirements governing this SWP3.
• Ensure that a signed copy of the SWP3 is available at the facility for review by the
U.S. Environmental Protection Agency (EPA), NCDENR Division of Water Quality,
or other regulatory officials if requested.
4.0 PREVENTIVE MAINTENANCE AND GOOD HOUSEKEEPING PROGRAM.
4.1 Good Housekeeping. Good housekeeping practices will be the prima rt' method used at
the Pentair Valves and Controls - Black Mountain facility to minimize the potential for
pollutants to enter storm water discharge from the site. The areas assessed to be most
at risk for pollution of storm water as identified in Section 1.4.3 will be monitored on an at
least weekly basis. Corrective action will be promptly taken for any problems identified.
Shift lead persons have the responsibility to keep the areas clean and report any spills or
discharges that may occur. Frequent area walk-through inspections (at least weekly) will
be performed to ensure the facility is in compliance with housekeeping directives.
4.2 Preventive Maintenance. Pentair Valves and Controls - Black Mountain's management
team is required under Part 111 Section C of the NCDENR General Permit No.
NCG030000 to "...at all times properly operate and maintain all facilities and systems of
treatment and control... which are installed or used... to achieve compliance with the
conditions of this general permit". Maintenance employees will complete monthly
inspections to identify those areas that may require maintenance, repairs or,
modifications in order to eliminate or minimize the contribution of pollutants to storm
water discharge from the site. On a monthly basis, all equipment whose operation may
affect the quality of storm water discharged from the site will be inspected using the
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Pentair Valves R Controls — Black Mountain, NC SwP3
format provided in Appendix VII, Equipment Preventive Maintenance Inspection
Checklist. Inspection items which may require that corrective action be taken may
include, but not limited to, the following:
• Parking lots >> clear of motor oil puddles; storm drains free of debris
• Shipping/receiving areas >> free of wood/other debris; rain canopy in place;
• Storm water piping, drain connections, sluices, weirs, gullies/ditches, and storm
grates >> properly connected and in good repair; adequate flow gradient; free of
debris/flow not blocked; rip -rap stone or other erosion control material properly
positioned.
• Metal lugers >> rain covers in place and in good conditions; seals/seams intact; no
standing water/liquids other than in drip pans; drip pans no more than 50% full; no
scrap on ground.
• Hazardous/non-hazardous waste and used oil storage areas >> material in
designated area; containers properly labeled; drums closed and covered/no standing
water; no evidence of spills or leaks; secondary containment intact; area free of trash
and other debris.
• Storage semi -trailers >> material inside is dry/no liquid leaks from stored material
inside trailers; surrounding area free of trash and other debris.
• Trash compactor >> intact hydraulic hoses and hose connections; no standing liquids;
no debris on ground.
• Cardboard dumpsters >> covered; no standing liquids; no debris on ground.
Employees identifying equipment or areas requiring corrective action will notify the
Environmental & Maintenance Team Leader and, as feasible, will take immediate action to
safeguard the environment. All corrective action, whether preventive or emergent in nature, will
be documented,
4.3 Sediment and Erosion Control. Structural or vegetation stabilization measures used to
limit erosion and control sediment loss from storm water runoff includes the following:
Typical building surfaces (asphalt, concrete, or gravel) or natural groundcover (grass,
trees, shrubs, etc.) surround both buildings of the Pentair Valves and Controls - Black
Mountain facility. The grounds are maintained by a contract landscape service.
The grounds are graded to provide adequate channeling of storm water runoff into
the drainage system.
Like many manufacturing operations, some outside areas have significant potential for, and
show the effects of, soil erosion from storm water runoff. Soil erosion shall be monitored, and
countermeasures shall be implemented, at the following areas:
• Soil is eroded from around the 3.5 ft. cinder block retainer wall extending out from the
Loading Dock on the west side of the Drexel Warehouse building. Fill dirt, grass
and/or gravel should be added and properly maintained so as to limit further erosion
in this area.
• Soil is eroded, and ground depressions have been carved, along building foundations
roof gutter downspout troughs, especially along the west side of the Manufacturing
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Pentair Valves & Controls - Black Mountain, NC SWP3
Building. Backfill, gravel, and/or splash pebbles should be added to better retain soil
and to channel storm water runoff away from the building foundations in these areas.
• The drain system on the East side of the main facility is in need of repair and/or
replacement due to deterioration and blockage. This will be corrected during 2007.
• The drain system on the West side of the main facility has one damaged downspout
that will be replaced during 2006. The soil will be sloped and graded to maintain flow
away from the foundation and exit the property via the creek that flows around the
East and South perimeter of the Manufacturing Building.
5.0 EMPLOYEE TRAINING.
5.1 Training for SWPPT and Others. Once every 12 months, all members of the SWPPT
shall receive initial or refresher training regarding the components, goals, and procedures of the
SWP3 for Pentair Valves and Controls - Black Mountain. The training will augment instruction
SWPPT members may receive specific to oil or oily substance spill response. Other recipients
of this training may include additional employees from maintenance, shipping/receiving, and
production departments, and other employees who, in the course of their duties, are involved in
any of the facility's operations that have the potential to contaminate storm water runoff from the
plant site.
5.2 Training Program Responsibility. The Emergency Coordinator is responsible for
developing, scheduling, implementing and coordinating the SWP3 training program. The
Emergency Coordinator will determine the appropriate level of training required for SWPPT
members and other personnel as applicable.
5.3 Training Topics. Classroom training will be augmented by hands-on drills (drills will be
scheduled and conducted twice a year), and shall include critiques of team performance.
Training will be documented and records kept using the format in Appendix VIII. Training will
address, but will not be limited to, the following topics.
• SWP3 goals and objectives
• Good housekeeping procedures
• Equipment preventive maintenance activities and erosion control aspects
• Spill prevention, response, and cleanup procedures
• Material handling and storage procedures
• Site inspection requirements
• Record keeping and reporting requirements
• Other topics pertaining to storm water management and pollution prevention.
6.0 RESPONSIBLE PARTY. As the facility's Emergency Coordinator, the EHS Manager &
Environmental Coordinator is designated the primary "Responsible Person" by the General
Manager and tasked with having overall responsibility for the SWP3 program at the Pentair
Valves and Controls - Black Mountain facility. As the Back-up Emergency Coordinator, the
Maintenance Lead Man also is designated a "Responsible Person" by the General Manager.
As required in Part II Section A.3. General Permit No NCG030000, a Responsible Person shall
be on site at all times during facility operations that have the potential to contaminate storm
water runoff through spills or exposure of materials associated with the facility operations. The
Page 19

Pentair Valves & Controls - Black Mountain, NC SWP3
EHS Manager & Environmental Coordinator has full authority to make necessary decisions to
ensure success of the program, and is authorized to halt any operation of the company where
there is danger of pollutants entering storm water discharges and/or actions which are in direct
violation of the facility's permit.
7.0 PLAN AMENDMENT AND REVIEW. The SWP3 shall be amended as necessary to
improve BMPs already in place, and whenever there is a change in facility design, construction,
operation, or maintenance that has a significant effect on the potential for the discharge of
pollutants to surface waters. In accordance with Part II, Section A.7 of General Permit No
NCG030000, the SWP3 shall be reviewed and updated by the Emergency Coordinator
annually. The Emergency Coordinator is the sole person authorized to amend the plan. SWP3
reviews and amendments shall be documented using Appendix I.
8.0 FACILITY INSPECTIONS
8.1 Ongoing Inspection Program. A robust facility inspection program of storm water
pollution control structures and practices forms a critical line of defense between compliance
and noncompliance with the NCDENR General Permit No. NCG030000. Although Part Il
Section A.8 of the General Permit requires formal documented facility inspections on a
semiannual schedule only, Pentair Valves and Controls - Black Mountain's management team
will conduct and record facility inspections on a weekly and monthly basis, as delineated below.
8.1.1 .Weekly. The Emergency Coordinator/SWPPT Leader shall be responsible for assigning
and training designated employees to perform weekly (daily if feasible) housekeeping
inspections of the areas listed in Section 1.4.3 of the SWP3 (Risk Identification and
Assessment) where materials bearing water priority chemicals, oil and grease, and other
environmentally harmful materials are handled and/or stored. If scrap metal, water or other
liquids, trash, and/or other debris are found in any of these areas, the employee shall take
prompt and appropriate action to avoid a noncompliance or potential pollution incident by
cleaning up the area(s).
• Load inglunloading dock areas
• Inside bar stock storage locations
• Metal luggers and surrounding concrete pad area
• China wooden crates/used pallets storage semi -trailers and surrounding area
• Trash compactor and cardboard dumpsters
• Hazardous waste and used oil storage shed
• Metal parts, castings, and scrap (turnings) inside storage/collection areas
• Paint and oils/lubricants inside storage areas.
8.1.2 Monthly. The Emergency Coordinator/SWPPT Leader shall be responsible for
assigning and training SWPPT members to conduct monthly visual inspections. Monthly visual
inspections of the facility, including a survey of preventive maintenance equipment and outfali
and all storm water point sources and outfalls, will be scheduled, conducted and recorded. The
purpose of the inspection is to identify key equipment and areas that have the potential for
contributing to the pollution of storm water runoff. Inspections will use the formats contained in
Appendix VII - Equipment Preventive Maintenance Inspection Checklist, and Appendix IX -
Storm Water Point Source and Outfall Inspection Record, and will:
Page 20

0
Pentair Valves & Controls — Black Mountain, NC SWP3
• Verify that adequate supplies of spill control materials and equipment are maintained
and readily available for use.
• Verify that measures and controls (BMPs) listed in Appendix IV are being followed
and are effective.
• Make provisions for flagging identified deficiencies to ensure that corrective actions
can be tracked.
• Be recorded and retained for a minimum of 2 years.
If during the monthly survey the inspector identifies a need or deficiency in any area of the
facility that has the potential for increasing the risk of pollutants being released to storm water
runoff, the employee will take immediate and appropriate action and/or notify the Emergency
Coordinator.
9.0 STORM WATER DISCHARGE CHARACTERISTIC MONITORING
9.1 Storm Water Discharge Monitoring, By virtue of the possibility of runoff coming in
contact with oil and other lubricants, grease, and SARA Title III Section 313 water toxic
chemicals present at Pentair Valves and Controls - Black Mountain, the facility is required under
Part II Section B and C of the NCDENR General Permit No. NCG030000: to monitor storm
water discharge annually for analytical discharge parameters; and semi-annually for qualitative
(visual) discharge characteristics.
9.1.1 Measurable Storm Event. As required by NCDENR in Part III Section D of the General
Permit No. NCG030000, samples collected and measurements taken "...shall be characteristic
of the volume and nature of the permitted (storm water) discharge". In addition, NCDENR
requires that analytical sampling "...shall be performed during a measurable storm event",
defined as a storm event that has "actual discharge" from the outfall and preceded by at least
72 hours in which no storm event measuring greater that 0.1 inches has occurred. A single
storm event may contain up to 10 consecutive hours of no precipitation. For example, if it rains
for 2 hours without producing any collectable discharge at an outfall and then stops raining, a
sample may be collected if rain producing a discharge begins again within the next 10 hours.
In addition, the following representative sampling requirements shall be followed:
• All samples shall be taken before the discharge joins or is diluted by any other waste
stream, water body, or substance.
• Monitoring points once implemented (outfalls, as delineated in Section 1.3.2 of the
SWP3), shall not be changed without notifying NCDENR Division of Water Quality.
• At a minimum, the following information shall be recorded for each measurement,
sample, or observation ("sampling activities") performed:
o Date, location, and time of sampling
o Name/title of individuals conducting sampling activities
o Date sampling performed
o Name/title of individuals performing analysis/results of sampling
o Analytical techniques or methods used
o Results of each analysis.
9.1.2 Representative Outfall. NCDENR's General Permit No. NCG030000 allows for
sampling to be performed at a reduced number of outfalls given that the discharge locations
produce substantially identical storm water discharges.
Page 21

I Pentair Valves & Controls - Black Mountain, NC SWP3 I
9.2 Analytical Monitoring Requirements. As specified in Part II Section B of the general
permit, analytical monitoring of storm water discharges shall be performed as specified in the
following table:
Discharge Characteristics and
Analytical
Units
Limits
Measurement
Frequency
Sample
T e
Sample
Location
Total Lead Pb
mg/1
0.033 m ll
Semi-annual
Grab*
SDO#
Total Copper
mg/1
0,007 mg/1
Semi-annual
Grab*
SDO#
Total Zinc
m 11
0,067 m II
Semi-annual
Grab*
SDO#
H
H scale
6.0 — 9.0
Semi-annual
Grab*
SDO#
Oil and Grease
mg/1
15 m li
Semi-annual
Grab*
SDO#
Total Suspended Solids TSS
m 11
100 mg/1
Semi-annual
Grab`
SDO#
Total Toxic Organics (TTO)
m ll
1 m 11
Semi-annual
Grab*
SDO#
Total Rainfall @
inches
NA
Semiannual I
Rain gauge
Notes
Grab Sample is an individual sample collected instantaneously. Grab samples must be taken within
the first 30 minutes of discharge.
# SDO = storm water discharge outfall (outfalls 001-008 per Section 1.3.2 of the SWP3).
+ TTO monitoring shall only be performed during the first year that the permit is obtained and the last
year before the permit is renewed.
@ For each measurable storm event the total rainfall, storm duration, and total flow must be recorded. Total flow
shall be either. (1) measured continuously, (2) calculated based on the amount of area draining to the outfall, the
amount of built -upon -(impervious) area, and the total amount of rainfall, or (3) estimated by the measurement of
flow at 20 minute intervals during the storm event.
Analytical, or quantitative, monitoring records, including laboratory reports and analytical
instrument calibration data, shall be maintained at the facility for a period of 5 years from the
date of the sample. All analytical monitoring shall be performed during a representative storm
event as defined in Section 9.1.1 of the SWP3, and recorded in the format provided in Appendix
X, SDO Monitoring Report.
9.2.1 Laboratory Certification. A North Carolina certified lab must be used to perform
analytical monitoring. The only exception to this rule is when measuring pH value of a sample.
Because sample pH may change considerably between from when the sample is pulled and
when it is analyzed at a lab, pH values shall be measured and recorded in the field. Laboratory
test procedures for the analysis of pollutants shall conform to the North Carolina Environmental
Management Commission regulations published pursuant to NCGS 143-215.63 ET. seq, the
Water and Air Quality Reporting Acts, and to regulations published pursuant to Section 304(g),
33 USC 1314 of the Federal Water Pollution Control Act, as Amended, and 40 CFR 136.
9.2.2 Discharge Monitoring Reports (DMR). As required in Part III Section E of the
NCDENR General Permit No. NCG030000, results of annual analytical monitoring (including
reporting total toxic organics for the first and last year of the permit) shall be submitted on SDO
Monitoring Report forms (see Appendix X) to be received by NCDENR no later than 30 days
from the date sampling results were received from the laboratory. Duplicate signed copies of
Appendix X shall be submitted to: Central Files
NCDENR Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Documentation of the qualitative (visual) monitoring associated with the initial analytical
monitoring event shall be included with the analytical monitoring submittal for the first year of
coverage under the permit. Analytical results from sampling during the final year of coverage
Page 22

Pentair Valves & Controls — Black Mountain, NC SWP3
under the permit shall be submitted using Appendix X as part of the facility's permit renewal
application. Analytical data submitted by the Pentair Valves and Controls - Black Mountain
facility shall not be considered confidential (on the contrary, the data is free for public inspection
at NCDENR Division of Water Quality offices) as required by Section 308 of the Federal Act, 33
USC 1318.
9.3 Qualitative Monitoring Requirements. The purpose of qualitative monitoring is to
evaluate the effectiveness of the SWP3 and to assess new sources of storm water pollution.
No analytical tests are required. As specified in Part II Section C of the general permit,
qualitative monitoring "
-.requires a visual inspection of each storm water outfall regardless of
representative outfall status".
9.3.1 First Monitoring Event. Although the first qualitative monitoring event under the permit
must coincide with the initial analytical monitoring event (regardless of the season), qualitative
monitoring does not need to be performed during a representative storm event as defined in
Section 9.1.1 of the SWP3. All other qualitative monitoring shall be conducted twice per year,
once from (January - June) and (July— December).
9.3.2 Semi -Annual Monitoring Requirements. Qualitative (visual) monitoring storm water
discharaes shall be performed as specified in the followina table:
Discharge Characteristics
Monitoring Frequency
Monitoring Location
Color
Semi -Annual
SDO#
Odor
Semi -Annual
SDO#
Clarity
Semi -Annual
SDO#
Floating Solids
Semi -Annual
SDO#
Suspended Solids
Semi -Annual
SDO#
Foam
Semi -Annual
SDO#
Oil Sheen
Semi -Annual
SDO#
Other obvious indicators of storm water pollution
Semi -Annual
SDO#
Notes
# SDO = storm water discharge outfall (outfalls 001-008 per Section 1.3.2 of the SWP3)
9.3.3 Documentation. Qualitative monitoring results shall be documented using Appendix XI,
Qualitative (Visual) SDO Monitoring Record, with records maintained at the facility for a period
of 5 years from the date of observations. As stated in Section 9.2.2 of the SWP3,
documentation of the qualitative monitoring associated with the initial analytical monitoring
event shall be included with the analytical monitoring submittal for the first year of coverage
under the permit.
10.0 IMPLEMENTATION. The implementation date of this SWP3 is April 23, 2004. As
required by Part II, Section A of the NCDENR General Permit No. NCG030000, implementation
of this SWP3 shall include documentation of all monitoring, analytical measurements and
sampling data, inspections, management and maintenance activities to implement BMPs, and
training provided to SWPPT members and other employees. Such documentation shall be kept
on site on file in the custody of the designated Emergency Coordinator (EHS Manager and
Environmental Coordinator) for a period of 5 years, and shall be made available to NCDENR
Division of Water Quality officials immediately when requested.
Page 23

CHAIN -OF -CUSTODY I Analytical Request Document a
aceArralytical The Ghalnrof-Custody Is a LEGAL DOCUMENT. All relevant flelds must be completed accurately. o
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Section A Section B Section C
Page: of (L
Required Client Information: Required Project Informetl'on: Invoice Information:
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Document Name: Sample Condition Upbn
_ Document Revised: June 10, 2014 '61
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Receipt SCUR
Page 1 of 2
Document No.:
Issuing Authorities:
F-ASV-CS-003=rev.14
Pace Asheville Quality Office
Client Name: p e nfa; a ..
Courier (Circle): Fed Ex UPS, LISPS . Client Commercial Pace Other
Custody Seal on CoolerlBox Present: [] yes no Seals intact: yes no
Packing Material: ❑ Bubble Wrap ❑ Bubble Bags None n Other
Thermometer Used: IR Gun#3-130265963 Type of Ice: Wet Blue 1h o� Samples on ice, cooling process has begun
—4R1ru-nnjk4 SN:140290365 Other:
p Correction Factor: Add Subtrac ©-_ C
Corrected Cooler Temp.: 6 C
Biological Tissue Is. Frozen: Yes N�l Date and Initia of person examining
Temp should be above freezing to 6°C
contents:
Comments:
Chain of Custody Present:
Yes ONO
❑NIA
1,
Chain of Custody Filled Out:
es No
❑NIA
2. Al,,.
Chain of Custody Relinquished:
Yes ONO
0NIA
3.
Sampler Name & Signature on COC:
es ONO
❑NIA
4.
Samples Arrived within Hold Time:
es ❑No
❑NIA
5.
Short Hold Time Analysis (<72hr :
Dyes
❑NIA
6.
Rush Turn Around Time Requested:
❑Yes No'
❑NIA
7.
Sufficient Volume:
Yes ONO
❑NIA
8.
Correct Containers Used:
4Yes ONO
❑NIA
9.
-Pace Containers Used:
4es ONO
❑NIA
Containers Intact:
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❑NIA
10,
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yes ONO
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compliance with EPA recommendation.
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Comments/ Resolution:
SCURF Reviewa IDate:
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Note: Whenever there is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( Le out of hold, incorrect
preservative, out of temp, incorrect containers)
Page 10 of 10

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TYCO VALVES & CONTROLS
MANUFACTURING BUILDING
FACILITY DIAGRAM- ➢RA WAGE
953 OLD US 70,
BLACK MOUNTAIN, NC 28711
TEL, [phone]
FAX- [phone]
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JTF ALL 400l ® DRAWING SCALE I' = 55'-0"
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CERT. NUMBER
CLASS
NPDES PERMIT NUMBER NC G D3O�A_ OTHER PERMIT NO.
STATE P FEDERAL DATE ISSUED
DATE ISSUED
EXPIRATION DATE S. Gene Logan
ENS/Maintenance Supervisor'
Tyco Valves & Controls
STREAM: NAME 953 Old US Highway 70
Vice Slack Mountain, NC28771
CLASS Flow Control Phone: [phone]
Fax: [phone]
gloganatycovalves.com
7 Q 10 www. tycovalves. com
SUB -BASIN
OPERATOR

W ATF Michael F. Easley, Governor
`OHO 9WG William G. Ross Jr., Secretary
North Carolina Depa. rit of Environment and Natural Resources
U) Alan W_ Klimek, P.E.
Director
Division of Water Quality
lid`i,�
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June 4, 2004 JUN _ 8 2004
Mr. R.W. Batchelder
Tyco Valves and Controls WATER QUALITY SECTION
953 Old U.S. Highway 70 ASHEVILI_E REGIONAL OFFICE
Black Mountain, NC 28711
Subject: General Permit No. NCG030000
Tyco Valves and Controls
COC NCG030529
Buncombe County
Dear Mr. Batchelder:
In accordance with your application for a discharge permit received on April 28, 2004 we are
forwarding herewith the subject certificate of coverage to discharge under the subject state -- NPDES general
permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated May
9, 1994 (or as subsequently amended).
Please take notice that this certificate of coverage is not transferable except after notice to the Division
of Water Quality. The Division of Water Quality may require modification or revocation and reissuance of the
certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management
Act or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Jonathan Dings at telephone number
[phone] ext. 537.
OR IGINAL'SIGNED BY
WILLIAM G. MILLS
Alan W. Klimek. P.E.
CC' Asheville Regional Office
Central Files
Stormwater and General Permits Unit Files
N. C. Division o1 Water Quality 1647 Mail Service Center Raleigh, NC 27699-1617 [phone]
�A
NCDENR
Customer Service
1 800 623-7748

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030529
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission. and the
Federal Water Pollution Control Act, as amended,
Tyco Valves and Controls
is hereby authorized to discharge stormwater from a facility located at
Tyco Valves and Controls
953 Old US Highway 70
Black Mountain, North Carolina
Buncombe County
to receiving waters designated as UT to the Swannanoa River, a class C river in the French Broad River Basin in
accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, II, III, IV,
V, VI and Vll of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective June 4, 2004.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day June 4, 2004.
ORIGINAL SIGNED BY
WILLIAM C. MILLS
Alan W. Klimek. Director
Division of Water Quality
By Authority of the Environmental Management Commission

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Name: Tyco Valves and Controls NCG030529
Short Name: TycVly
Coordinates: 0350 36' 30.6" N, 0820 21' 26.2" W
Comment: Tyco Valves and Controls NCG030529, subbasin 04-03-02, French Broad River
Basin, Buncombe County, UT to Swannanoa River, Class C, USGS quad E09SE