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HomeMy WebLinkAboutNCG030529_COMPLETE FILE - HISTORICAL_20180419STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. IV Cc, Q.3D 5a DOC TYPE HISTORICAL FILE ❑ MONITORING REPORTS DOC DATE ❑ � �� D �� � YYYYMMDD A� Division of Water Quality / Surface Water Protection National Pollutant Discharge Elimination System NCDENR "WMMW`AND U" Ft`"'°' PERMIT NAME/OWNERSHIP CHANGE FORM Fx.+w�warr Iwo NaiwK RealwC�s I. Please enter the permit number for which the change is requested. FOR AGENCY USE ONLY Date Received Year Month Da rnad p ie,r�f Acove— q `I a.j ! 8 _ Ptk e.- I 1aow"j NPDES Permit (or) Certificate of Coverage a� 0 13 10 1 5 2 9 Il. Permit status prior to requested change. a. Permit issued to (company name): Pentair Valves & Controls b. Person legally responsible for permit: Jason Stone First MI Last C n Plant manager C C�.�v R G 1 G1•d Title RECEIVED A� PR 19 2 953 old US Hwy 70 FEB 13 2918 Permit Holder Mailing Address CFNTRP►L FILES Black Mountain NC 27711 DWR SEcnoN DENR-LAND QUALITY City State Zip gTQFWATERPERMIITING (828) 669-5515 { } Phone Fax c. Facility name (discharge): Pentair Valves & Controls d. Facility address: 953 old US Hwy 70 Address Black Mountain NC 28711 City State Zip e. Facility contact person: Gerald Runkles (828) 669-3753 First / MI / Last Phone III. Please provide the following for the requested change (revised permit). a. Request for change is a result of: ❑ Name change of the facility or owner If ocher please explain: Name change for Responsible Person b. Permit issued to (company name): Emerson Automation Solutions c. Person legally responsible for permit: Jason Stone First M l Last Plant Manager Title 953 Old US Hwy 70 _ permit Holder Mailing Address Black Mountain NC 28711 City State Zip 828 669-5515 Jason. stone emerson.com Phone E-mail Address d. Facility name (discharge): Pentair Valves & Controls e. Facility address: 953 Old US Hwy 70 Address Black Mountain NC 28711 City State Zip f Facility contact person: Gerald Runlcles First Ml Last (828) 669-3753 gerald.runkles@emerson.com Phone E-mail Address Revised 2412Apf23 NPDES PERMIT NAME/OWNERSHIP CHANGE FORM Page 2 of 2 IV. Permit contact information (if different from the person legally responsible for the permit) Permit contact: Gerald Runkles First M I Last EHS Manager Title 953 old US Hwy 74 Mailing Address Black Mountain NC 28711 City State Zip (828) 669-3753 Gerald.runkles emerson.com Phone �E-mail Address V. Will the permitted facility continue to conduct the same industrial activities conducted prior to this ownership or name change? ® Yes No (please explain) vl Required Items: THIS APPLICATION WELL BE RETURNED UNPROCESSED IF ITEMS ARE INCOMPLETE OR MISSING: ® This completed application is required for both name change and/or ownership change requests. ® Legal documentation of the transfer of ownership (such as relevant pages of a contract deed, or a bill of sale) is required for an ownership change request. Articles of incorporation are not sufficient for an ownership change. ..................................................................................................................... The certifications below must be completed and signed by both the permit holder prior to the change, and the new applicant in the case of an ownership change request. For a name change request, the signed Applicant's Certification is sufficient. PERMITTEE CERTIFICATION (Permit holder prior to ownership change): 1, Jason Stone, attest that this application for a name/ownership change has been reviewed and is accurate and complete to the best of my knowledge. I understand that if all required parts of this application are not completed and that if all required supporting information is not included, this application package will be returned as incomplete. wa °_^" t /% t /Tot 9 UAPPLSignature Date * ICANT CERTIFICATION 1, Jason Stone, attest that this application for a name/ownership change has been reviewed and is accurate and complete to the best of my knowledge. 1 understand that if all required parts of this application are not completed and that if all required supporting information is not included, this application package will be returned as incomplete. Signature I I Date PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO: Division of Water Quality Surface Water Protection Section 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Revised 7/2008 Delaware Page 1 The First State I, JEFFREY W. BULLOCK, SECRETARY OF STATE OF THE STATE OF DELAWARE, DO HEREBY CERTIFY THE ATTACHED IS A TRUE AND CORRECT COPY OF THE CERTIFICATE OF AMENDMENT OF "PENTAIR VALVES & CONTROLS US LP", CHANGING ITS NAME FROM "PENTAIR VALVES & CONTROLS US LP" TO "EMERSON AUTOMATION SOLUTIONS FINAL CONTROL US LP", FILED IN THIS OFFICE ON THE THIRTEENTH DAY OF OCTOBER, A.D. 2017, AT 1.44 O'CLOCK P.M. 3100932 8100 z\� 5R# 20176612274 You may verify this certificate online at corp.delaware.gov/authver.shtml - 'J.ttr.rw4Buaoc., f�snaNy cf iu�. _ . Authentication: 203396584 Date;10-13-17 STATE OF DELAWARE AMENDMENT TO THE CERTIFICATE OF LIMITED PARTNERSHIP The undersigned, desiring to amend the Certificate of Limited Partnership pursuant to the provisions of Section 17-202 of the Revised Uniform Limited Partnership Act of the State of Delaware, does hereby certify as follows: FIRST: The name of the Limited Partnership is Fq=. Valves & Controls, US LP. SECOND: Article'I and III of the Certificate of Limited Partnership shall be amended to read as follows: I. The name of the limited partnership is Emerson Automation Solutions Final Control US LP III. The name and mailing address of the general partner is as follows: Name Address TV&C GP Holding, LLC 8100 W. Florissant Ave., St. Louis, MO 63136 IN WITNESS WHEREOF, the u esFsi ned tht. eeuted dment tp the Certificate of Limited Partn&ship on this day of A.D 20.1'. TV&C GP HOLDING, LLC By: General Partner(s) Name: Steven A. Cl}elesnik Print or Type State of Delaware Secretary of State Divhlon of Corporations Delh•ered 01:44 PI11011312017 FILED 01:44 PAl 1011312017 SR 20176612274 - Fite\umber 3100932 aceAnaWal' May 11, 2017 Gerald Runkles Pentair Valves & Controls 953 Old US Hwy 70 Black Mountain, NC 28711 RE: Project: Outfalls 511 Pace Project No.: 92338864 Dear Gerald Runkles: Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)8759092 Enclosed are the analytical results for sample(s) received by the laboratory on May 01, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, �-- Chris Derouen christopher.derouen@pacelabs.com (704)875-9092 Project Manager Enclosures 6 REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 32 Pace Analytical Services, LLC ac00 6Am1j Gal r Flu9800 neY Ave. Suite 78 ntersvilEe. NC 2ti4378 wwwpacebb&oom (704)875-9092 CERTIFICATIONS Project: Outfalls 511 Pace Project No.: 92338864 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification #: 37706 FloridalNELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 Vrginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NCO30 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 32 lace Arr IYAC81 www.Pacefsbaoam SAMPLE ANALYTE COUNT Project: Outfatis 511 Pace Project No_: 92338864 Pace Analytical Services, LLC 9SW Kincey Ave, Suite IOD Huniemville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92338864001 Outfall #1 EPA 1664B JMS 1 PASI-C EPA608 RES 27 PASI-C EPA200.7 SH1 3 PASi-A EPA 625 RES 58 PASI-C EPA 624 GAW 34 PASI-C SM 2540D MDW 1 PASI-A EPA 420.4 DMN 1 PASI-A SM 4500-CN-E AES2 1 PASI-A 92338864002 Outfall #2 EPA 1664B JMS 1 PASI-C EPA 608 RES 27 PAS1-C EPA200.7 SH1 3 PASI-A EPA 625 RES 56 PASI-C EPA 624 GAW 34 PASI-C SM 2540D MDW 1 PASI-A EPA 420.4 DMN 1 PASI-A SM 4500-CN-E AES2 1 PASI-A - Received JUN 2 0 2017 L>lnd Quality section Asheville REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 32 IaXftlyfical- wwwPacaftba.com SUMMARY OF DETECTION Project: Outfalls 511 Pace Project No.: 92338864 Lab Sample ID Method Client Sample ID Parameters Result 92338864001 Outfall #1 EPA 200.7 Copper 13.6 EPA 200.7 Zinc 31.2 SM 2540D Total Suspended Solids 4.8 92338864002 Outfall #2 EPA 200.7 Copper 11.5 EPA 200.7 Zinc 18.8 SM 2540D Total Suspended Solids 19.5 Received lity Section Land RASYteville Pace Analytical Services, LLC 9800 Kincey Ave. SuOs 100 HuntersviVe, NG 28078 (704)875-9092 Units Report Limit Analyzed Qualifiers ug1L 5.0 05/0411715:01 ug1L 10.0 05/0411715:01 mglt 2.5 05/02/17 20:04 ug/L 5.0 0510411715:06 ug/L 10.0 05104/1715:06 mglL 4.2 05102J17 20:05 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 32 aceAnalytical aOM paCWMLI Com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Outfalls 5/1 Pace Project No,: 92338864 Sample: Outfall #1 Lab ID: 92338864001 Collected: 05/01/17 08:00 Received: 05101/17 09:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 05/09/17 06:36 608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510 Aldrin ND ug/L 0.050 1 05102/17 10:00 05/02/17 21:25 309-00-2 alpha-BHC ND ug1L 0.050 1 05/02/17 10:00 05/02/17 21:25 319-84-6 beta-BHC ND ug1L 0.050 1 05/02/17 10:00 05102/17 21:25 319-85-7 delta-BHC ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:25 319-86-8 gamma-BHC (Lindane) ND ug1L 0.050 1 05/02/17 10:00 05102/17 21:25 58-89-9 Chlordane (Technical) ND ug/L 0,50 1 05/02117 10:00 05102/17 21:25 57-74-9 4,4'-DDD ND ug/L 0.050 1 05/02/17 10:00 05/02/17 2125 72-54-8 4,4'-DDE ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:25 72-55-9 4,4'-DDT ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:25 50-29-3 Dieldrin ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:25 6G-57-1 Endosulfan I ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:25 959-98-8 Endosulfan II ' ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:25 33213-65-9 Endosulfan sulfate ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:25 1031-07-8 Endrin ND ug/L 0.050 1 05/02117 10:00 05/02/17 21:25 72-20-8 Endrin aldehyde ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:25 7421-93-4 Heptachlor ND ug1L 0.050 1 05/02117 10:00 05/02/17 21:25 76-44-8 Heptachlor epoxide ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21,25 1024-57-3 PCB-1016 (Aroclor 1016) ND ug/L 0.50 1 05/02/17 10:00 05/02/17 21:25 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.50 1 05/02/17 10:00 05/02/17 21:25 11104-28-2 PCB-1232 (Aroclor 1232) ND ug1L 0-50 1 05/02/17 10:00 05102117 21:25 11141-15-5 PC13-1242 (Aroclor 1242) ND uglL 0-50 1 05102/17 10:00 05/02/17 21:25 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 1 05102/17 10:00 05102/17 21:25 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 1 05102/17 10:00 05102117 21725 11097-69-1 PC8-1260 (Aroclor 1260) ND ug/L 0.50 1 05102/17 10:00 05/02M 7 21725 11096-82-5 Toxaphene ND ug/L 0.50 1 05/02/17 10:00 05102117 21:25 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 49 % 20-110 1 05/02/17 10:00 05102117 21:25 877-09-8 Decachlorobiphenyl (S) 40 % 20-138 1 05/02/17 10:00 05/02/17 21:25 2051-24-3 200.7 MET ICP Analytical Method: EPA200.7 Preparation Method: EPA200.7 Copper 13.6 ug/L 5.0 1 05/0311712:15 05/04/1715:01 7440-50-8 Lead ND ug/L 5.0 1 0510311712:15 05/0411715:D1 7439-92-1 Zinc 31.2 ug/L 10.0 1 0510311712:15 05/04/1715:01 7440-66-6 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Acenaphthene ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 83-32-9 Acenaphthylene ND ug/L 5.0 1 05/02/17 16:15 05104/17 06:00 208-96-8 Anthracene ND ug/L 5.0 1 05102J1716:15 05/04/1706:00 120-12-7 Benzo(a)anthracene ND ug/L 5-0 1 05/02117 16:15 05/04117 06:00 56-55-3 Benzo(a)pyrene ND ug/L 5-0 1 05102/17 16A5 05104117 06:00 50-32-8 Benzo(b)fluoranthene ND ug/L 5.0 1 05102/17 16:15 05/04/17 06:00 205-99-2 Benzo(g,h,i)peryfene ND ug/L 5.0 1 05/02/17 16:15 05104117 06:00 191-24-2 Benzo(k)fluoranthene ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 207-08-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05111 /2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 32 aceAnalytical wxw.paoer§ &G= Project: Outfalls 5/1 Pace Project No.: 92338864 Sample: Outfall #1 Parameters 625 MSSV 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a, h )anthracene 3, 3'-Dichlorobenzidine 2,4-Dichlorophenol Diethylphtha late 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentad iene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nilrosodimethylamine N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine 2,2'-Oxybis(1-chloropropane) Pentachlorophenol Phenanthrene Phenol Pyrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab ID: 92338864001 Collected: 05/01/17 08:00 Received: 05/01/17 09:50 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA625 Preparation Method: EPA625 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 101-55-3 ND ug1L 5.0 1 05/02/17 16:15 05/04/17 06:00 85-68-7 ND ug/L 5.0 1 05/02/17 16:15 05104117 06:00 59-50-7 ND ug/L 10.0 1 05/02/17 16:15 05/04/17 06:00 111-91-1 ND ug1L 5.0 1 05/02/17 16:15 05/04/17 06:00 111-444 ND ug1L 5.0 1 05/02/17 16:15 05/04/17 06:00 91-58-7 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 95-57-8 ND uglL 5.0 1 05/02/17 16:15 05/04/17 05:00 7005-72-3 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 218-01-9 NO ug1L 5.0 1 05/02/17 16:15 05/04/17 06:00 53-70-3 NO ug1L 25.0 1 05/02/17 16:15 05/04/17 06:00 91-94-1 NO uglL 5.0 1 05/02/17 16:15 05/04/17 06:00 120-83-2 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 84-66-2 ND ug1L 10.0 1 05/02/17 16:15 05/04/17 06:00 105-67-9 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 131-11-3 NO uglL 5.0 1 05/02/17 16:15 05/04/17 06:00 84-74-2 NO uglL 20.0 1 05/02/17 16:15 05/04/17 06:00 534-52-1 ND uglL 50.0 1 05/02/17 16:15 05/04/17 06:00 51-28-5 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 121-14-2 NO ug1L 5.0 1 05/02/17 16:15 05/04/17 06:00 606-20-2 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 117-84-0 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 117-81-7 ND uglL 5.0 1 05/02/17 16:15 05/04/17 06:00 206-44-D ND uglL 5.0 1 05/02/17 16:15 05/04/17 06:00 86-73-7 ND uglL 5.0 1 05/02/17 16:15 05/04/17 06:00 87-68-3 NO ug1L 5.0 1 05/02/17 16:15 05/04/17 06:00 118-74-1 NO uglL 10.0 1 05/02/17 16:15 05/04/17 06:00 77-47-4 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 67-72-1 NO ug1L 5.0 1 05/02/17 16:15 05/04/17 06:00 193-39-5 NO uglL 10.0 1 05/02/17 16:15 05/04/17 06:00 78-59-1 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 91-20-3 NO uglL 5.0 1 05/02/17 16:15 05/04/17 06:00 98-95-3 ND ug1L 5.0 1 05/02/17 16:15 05/04/17 06:00 88-75-5 NO ug/L 50.0 1 05/02/17 16:15 05/04/17 06:00 100-02-7 ND uglL 5.0 1 05/02/17 16:15 05/041W 06:00 62-75-9 ND ug/L 5.0 1 05/02/17 16:15 05/04/47 06:00 621-64-7 ND ug/L 10.0 1 05/02/17 16:15 05/04/17 06:00 86-30-6 NO ug1L 5.0 1 05/02/17 16:15 05/04/17 06:00 10M0-1 NO ug/L 10.0 1 05/02/17 1615 05/04/17 06:00 87-86-5 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 85-01-8 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 108-95-2 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 129-MD ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:00 120-82-1 ND ug/L 10.0 1 05/02/17 16:15 05/04/17 06:00 88-06-2 32 % 10-120 1 05/02/17 16:15 05/04/17 06:00 4165-60-0 30 % 15-120 1 05/02/17 16:15 05/04/17 06:00 321-60-B REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 32 aeeAnalytkal wwwpacelaimmm ANALYTICAL RESULTS Project_ Outfalls 511 Pace Project No.: 92338864 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvflfe, NC 28078 (704)8759092 Sample: Outfall #1 Lab ID: 92338864001 Collected; 05101117 08:00 Received: 05/01/17 09:50 Matrix; Water Parameters Results units Report Limit OF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Surrogates Terphenyl-d14 (S) 48 % 11-131 1 05/0211716:15 0510411706.00 1718-51-0 Phenol-& (S) 16 % 10-120 1 05102M 7 16:15 05104117 06:00 13127-88-3 2-Fluorophenol (S) 17 % 110.120 1 05102/1716:15 05/0411706:00 367-12-4 2,4,6-Tribromophenol (S) 44 % 10-137 1 05/02/17 16:15 05/04/17 06:00 118-79-6 624 Volatile Organics Analytical Method: EPA624 Benzene NO ug1L 2.0 1 05/0211718:38 71-43-2 Bromodichloromethane NO ug1L 2.0 1 05/02/1718:38 75-27-4 Bromoform NO ug1L 2.0 1 051=1718:38 75-25.2 Bromomelhane NO uglL 2.0 1 0510211718-.38 74-83-9 Carbon tetrachloride NO ug/L 2.0 1 05/02117 18:38 56-23-5 Chlorobenzene NO ug/L 2.0 1 05102/1718:38 108.90-7 Chloroethane NO ug/L 2.0 1 05/0211718:38 75-00-3 Chloroform NO ug/L 2.0 1 05/02/1718:38 67-66-3 Chloromethane NO uglL 2.0 1 05/0211718:38 74-87-3 Dibromoch lorom ethane NO ug/L 2.0 1 05102/1718:38 124-48-1 1,2-Dichiorobenzene ND uglL 2.0 1 0510211718:38 95-50-1 1,3-Dichlorobenzene NO ug/L 2.0 1 05/0211718:38 541-73-1 1,4-Dichlorobenzene NO ug/L 2.0 1 05102/1718:38 106.46-7 1,1-Dichloroethane NO ug/L 2.0 1 05102I718:38 75.34-3 1,2-Dichloroethene NO ug/L 2.0 1 0510711718:38 107-06-2 1,1-Dichloroethene NO ug/L 2.0 1 05102/1718:38 75.35-4 cis-1,2-Dichloroethene NO ug/L 2.0 1 05/02/1718:38 156.59-2 trans-1,2-Dichloroethene NO ug1L 2.0 1 05102/1718:38 156.60-5 1,2-Dichloropropane ND ug/L 2.0 1 05/02/1718:38 78.87-5 cis-1,3-Dichloropropene ND ug/L 2.0 1 0510211718:38 10061-01-5 trans-1,3-Dichloropropene ND uglL 2.0 1 05102/1718:38 10061-02-6 Ethyibenzene ND ug1L 2.0 1 0510211718:38 10041-4 Methylene Chloride NO ug1L 2.0 1 05/02117 18:38 75-09-2 1,1,2,2-Tetrachloroethane NO ug1L 2.0 1 05/02/1718:38 79.34-5 Tetrachloroethene NO ug1L 2.0 1 05/02/1718:38 127-18-4 Toluene ND ug1L 2.0 1 05/02/1718:38 108-88-3 1,1,1-Trichloroethane NO ug1L 2.0 1 05/02/1718:38 71-55-6 1,1,2-Trichloroethane NO uglL 2.0 1 05/02/1718:38 79-00-5 Trichloroethene NO ug1L 2.0 1 0510211718:38 79.01-6 Trichlorofluoromethane ND ug1L 2.0 1 0510211718:38 75-69-4 Vinyl chloride ND ug/L 2.0 1 05102/17 18:38 75-014 Surrogates 4-Bromaftuorobenzene (S) 95 % 70430 1 05/02/17 18:38 460-00-4 Toluene-d8 (S) 103 % 70-130 1 05102117 18:38 2037-26-5 1,2-Dichloroethane-d4 (S) 88 % 70-130 1 05/02/17 18:38 17060-07-0 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 4.8 mg1L 2.5 1 05/02117 20:04 Date; 05/11/2017 04:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be repmduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 32 aceAnalytical e W0VW.Pscsk6s0arn Project: Outfalls 5/1 Pace Project No.: 92338864 Sample: Outfail #1 Parameters 420.4 Phenolics, Total Phenol 450OCNE Cyanide, Total Cyanide Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab ID: 92336864001 Collected: 05/01/17 08:00 Received: 05/01/17 09:50 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 420A ND mg/L 0.010 1 05/11/1712:30 108-95.2 Analytical Method: 5M 4500-CN-E NO mg/L 0.0080 1 05/06/1715:09 57-12-5 Sample: Outfall 02 Lab iD: 92338864002 Collected: 05101/17 08:15 Received: 05/01117 09:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 05/09/17 06:36 608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510 Aldrin ND ug/L 0.050 1 05/02/17 10:00 05102/1721A3 309-00-2 alpha-BHC ND ug/L 0.050 1 05/02/17 10:00 05/02117 21:43 319-84-6 beta-BHC ND ug/L 0.050 1 05102/17 10= 05/02/17 21:43 319-85-7 delta-BHC ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:43 319-86-8 gamma-BHC (Lindane) ND uglL 0,050 1 05/02/17 10:00 05/02/17 21:43 58-89-9 Chlordane (Technical) ND ug/L 0.50 1 05/02/17 10:00 05/02/17 21:43 57-74-9 4,4'-DDD ND ug/L 0.050 1 05/02/17 10:00 05/02JI7 21:43 72-54-8 4,4'-DDE ND ug/L 0.050 1 05/02/17 10:00 05102/17 21:43 72-55-9 4,4'-DDT ND ug/L 0.050 1 05/02117 10:00 05102/17 21:43 50.29-3 Dieldrin ND ug/L 0.050 1 OW02117 10:00 05/02/17 21:43 60-57-1 Endosulfan I ND ug/L 0,050 1 05/02/17 10:00 05/02/17 21:43 959-98-8 Endosulfan II ND ug1L 0.050 1 05/02/17 10.00 05/02/17 21:43 33213-65-9 Endosulfan sulfate ND uglL 0.050 1 05/02/17 10:00 05/02/17 21:43 1031-07-8 Endrin ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:43 72-20-8 Endrin aldehyde ND uglL 0.050 1 05/02/17 10:00 05/02/17 21:43 7421-93-4 Heptachlor ND ug/L 0,050 1 05/02/17 10:00 05/02/17 21:43 76-44-8 Heptachlor epoxide ND ug/L 0.050 1 05/02/17 10:00 05/02/17 21:43 1024-57-3 PCB-1016 (Aroclor 1016) ND ug/L 0.50 1 05/02/17 10:00 05/02/17 21:43 12674-11-2 PCB-1221 (Arocfor 1221) ND ug1L 0,50 1 05/02/17 10:00 05/02/17 21:43 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.50 1 05/02/17 10:00 05/02/17 21:43 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.50 1 05/02/17 10:00 05/02/17 21:43 53469-21-9 PCB-1248 (Arodor 1248) ND ug/L 0,50 1 05/02/17 10:00 05/02/17 21:43 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 1 05/02/17 10:00 05/02/17 21:43 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 1 05/02/17 10:00 05102J17 21 A3 11096-82-5 Toxaphene ND ug/L 0.50 1 05/02/17 10:00 05102M721:43 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 60 % 20-110 1 05102 I7 10.00 05/02/17 21 A3 877-09-8 Decachtorobiphenyl (S) 54 % 20-138 1 05/02/17 10:00 05/02/17 21:43 2051-24-3 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 11.5 ug1L 5.0 1 0510311712:15 05104/1715:06 744D`50-8 Lead ND ug/L 5.0 1 0510311712:15 05104/1715:06 7439-92-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 32 aceAnalytical www.parslabs.mm Project: Outfalls 511 Pace Project No.: 92338864 Sample: Outfall #2 Parameters 200.7 MET ICP Zinc 625 MSSV Acenaphthene Acenaphthylene Anthracene Ben70(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol bis(2-Chloroethoxy)methane bis(2-Chtoroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Di benz(a, h )anthracene 3,3'-Dich lorobenzidine 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl )phthalate Fluoranthene Fluorene Hexachloro-1, 3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitrosodimethylamine N-Nitroso-di-n-propylamine Date: 05/11/2017 04:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hurtersville, NC 28078 (704)8759092 ANALYTICAL RESULTS Lab ID: 92338864002 Collected: 05/01/17 08:15 Received: 05/01/17 09:50 Matrix: Water Results Units Report Limit OF Prepared Analyzed CAS No Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 18.8 ug1L 10.0 1 05/03/1712:15 05104/1715:06 7440-66-6 Analytical Method: EPA 625 Preparation Method: EPA 625 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 83-32-9 NO uglL 5.0 1 05/02/17 16:15 05/04/17 06:27 208-96-8 NO ug1L 5.0 1 05/02/17 16:15 05/04/17 06:27 120-12-7 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 56-55-3 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 50-32-8 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 205-99-2 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 191-24-2 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 207-08-9 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 101-55-3 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 85-68-7 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 59-50-7 NO uglL 10.0 1 05/02/17 16:15 05/04/17 06:27 111-91-1 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 111-44-4 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 91-58-7 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 95-57-8 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 7005-72-3 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 218-01-9 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 53-70-3 NO ug/L 25.0 1 05/02/17 16:15 05/04/17 06:27 91-94-1 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 120-83-2 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 84-66-2 NO ug/L 10.0 1 05/02/17 16:15 05/04/17 06:27 105-67-9 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 131-11-3 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 84-74-2 NO ug/L 20.0 1 05/02/17 16:15 05/04/17 06:27 534-52-1 NO ug1L 50.0 1 05/02/17 16:15 05/04/17 06:27 51-28-5 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 121-14-2 NO uglL 5.0 1 05/02/17 16:15 05/04/17 06:27 606-20-2 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 117-84-0 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 117-81-7 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 206-44-0 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 86-73-7 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 87-68-3 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 118-74-1 ND ug/L 10.0 1 05/02/17 16:15 05/04/17 06:27 77-47-4 ND ug/L 5.0 1 05/02/17 16:15 05104/17 06:27 67-72-1 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 193-39-5 ND ug/L 10.0 1 05/02/17 16:15 05104/17 06:27 78-59-1 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 91-20-3 ND ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 98-95-3 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 O6s27�i8&+%5=5 NO ug/L 50.0 1 05/02/17 16:15 05/04/17 06:27 100-02-7 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06:27 62-75-9 NO ug/L 5.0 1 05/02/17 16:15 05/04/17 06 ` 7 17 �621-64U7JON REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Land Quality Section Asheville Qua[ Page 9 of 32 aceAnalyfibal www.pacelabs mn ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: Outfalls 511 Pace Project No.: 92338864 Sample: Outfall #2 Lab ID: 92338864002 Collected: 05/01/17 08:15 Received: 05/01/17 09:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 N-Nitrosodiphenylamine ND ug/L 10.0 1 05/02/17 16:15 05/04/17 06:27 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 5.0 1 05/02/17 16:15 05104/17 06:27 108-60-1 Pentachlorophenol ND ug/L 10.0 1 05/02/17 16:15 05104/17 06:27 87-86-5 Phenanthrene ND ug/L 5-0 1 05/02117 16:15 05/04/17 06:27 85-01-8 Phenol ND ug/L 5.0 1 05IM17 16:15 05104117 06:27 108-95-2 Pyrene ND ug/L 5.0 1 05102/17 16:15 05/04117 06:27 129-OM 1,2,4-Trichlorobenzene ND ug/L 5.0 1 05/0211716:15 05104/1706:27 120-82-1 2,4,6-Trichlorophenol ND ug/L 10.0 1 05/02/17 16:15 05/04/17 06:27 88-06-2 Surrogates Nitrobenzene-d5 (S) 53 % 10-120 1 05/02/17 16:15 05/04/17 06:27 4165-60-0 2-Fluorobiphenyl (S) 52 % 15-120 1 05/02/17 16:15 05/04/17 06:27 321-60-8 Terphenyl-d14 (S) 71 % 11-131 1 05/02/17 16:15 05104/17 06:27 1718-51-0 Phenol-d6 (S) 23 % 10-120 1 05/02/17 16:15 05/04/17 06:27 13127-88.3 2-Fluorophenol (5) 33 % 10-120 1 05/02/17 16:15 05/04/17 06:27 367-12-4 2,4,6-Tdbromophenol (S) 69 % 10-137 1 05/02/17 16:15 05/04/17 06:27 118-79-6 624 Volatile Organics Analytical Method: EPA624 Benzene ND ug/L 2.0 1 05/0211718:20 71-43-2 Bromodichloromethane ND ug/L 2.0 1 0510211718:20 75-27-4 Bromoform ND ug/L 2.0 1 05/0211718:20 75-25-2 Bromomethane ND ug/L 2.0 1 0510211718:20 74-83-9 Carbon tetrachloride ND ug/L 2.0 1 05/02/17 18:20 56-23-5 Chlorobenzene ND ug/L 2.0 1 0510211718,20 108-90-7 Chloroethane ND uglL 2.0 1 0510211718:20 75-00-3 Chloroform ND ug/L 2.0 1 05/0211718:20 67-66-3 Chloromethane ND ug/L 2.0 1 05/020718:20 74-87-3 Dibromochloromethane ND ug/L 2.0 1 05102M718:20 124-46-1 1,2-Dichlorobenzene ND ugh- 2.0 1 05102/1718:20 95-50-1 1,3-Dichlorobenzene ND ug1L 2.0 1 05/02/17 18:20 541-73-1 1,4-Dichlorobenzene ND uglL 2.0 1 05/0211718:20 106-46-7 1,1-Dichloroethane ND ug1L 2.0 1 0510211718:20 75-34-3 1,2-Dichloroelhane ND ug/L 2.0 1 0510211718:20 107-06-2 1,1-Dichloroethene ND uglL 2.0 1 05/0211718:20 75-35-4 cis-1,2-Dichloroethene ND ug/L 2.0 1 0510211718:20 156-59-2 trans- 1,2-Dichloroethene ND ug/L 2.0 1 05102/1718:20 156-60-5 1,2-Dichloropropane ND ug/L 2.0 1 05102/1718:20 78-87-5 cis-1,3-Dichloropropene ND ug/L 2.0 1 05/0211718:20 10061-01-5 trans-1,3-Dichloropropene ND ug/L 2.0 1 05/02/1718:20 10061-02-6 Ethylbenzene ND ug/L 2.0 1 05/02/1718720 100414 Methylene Chloride ND ug/L 2.0 1 05/02/17 18:20 75-09-2 1,1,2,2-Tetrachloroethane ND ug/L 2-0 1 05102/1718:20 79-34-5 Tetrachloroethene ND ug/L 2-0 1 05102/1718.20 127-18-4 Toluene ND ug/L 2.0 1 05/0211718:20 108-88-3 1,1,1-Tdchloroethane ND ug/L 2-0 1 0510211718:20 71-55-6 1,1,2-Trichloroethane ND ug/L 2-0 1 05102/1718:20 79-00-5 Trichloroethene ND ug/L 2.0 1 05/02/17 18:20 79-01-6 Tdchlomfluoromethane ND ug1L 2.0 1 0510211718:20 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC, Page 10 of 32 © 0 ('-�55'ne Analytical ~pftV1b:cam ANALYTICAL RESULTS Project: Outfalls 511 Pace Project No,: 92338864 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Sample: Outfall #2 Lab ID: 92338864002 Collected: 05101/17 08:15 Received: 05/01117 09:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 624 Volatile Organics Analytical Method: EPA624 Vinyl chloride ND uglL 2.0 1 05/02/17 18:20 75-01-4 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 05/02/17 18:20 460-00-4 Toiuene-d8 (S) 103 % 70-130 1 05/02/17 18:20 2037-26-5 1,2-Dichloroethane-i4 (S) 84 % 70-130 1 05/02117 18:20 17060-07-0 2S40D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 19.5 mg1L 4.2 1 05/02/17 20.05 420.4 Phenolics, Total Analytical Method: EPA 420.4 Phenol ND mg1L 0.010 1 0511111712:32 108-95-2 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND mg1L 0.0080 1 05/06/1715:10 57-12-5 Date: 05111/201704:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 32 aceAnalytical utvw.ps wm Project: Outtalls 511 Pace Project No.: 92338864 QC Balch: 359654 QC Batch Method: EPA 1664B Associated Lab Samples: 92338864001, 92338864002 METHOD BLANK: 1994539 Associated Lab Samples: 92338864001. 92338864002 Parameter Units Oil and Grease mglL QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 05/09/17 06:22 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1994539 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mglL 40 38.6 97 78-114 MATRIX SPIKE SAMPLE: 1994540 92338864002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 36.2 89 78-114 Results presented on this page are In the units indicated by the "units- column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 32 aceAnalylical' www.p3ata0acpm DUALITY CONTROL DATA Project Outfalls 511 Pace Project No.: 92338W QC Batch: 358814 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92338864001, 92338864002 METHOD BLANK: 1989844 Associated Lab Samples: 92338864001, 92338864002 Parameter Units Copper uglL Lead uglL Zinc ug1L Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 05/0411713:24 ND 5.0 05/0411713:24 ND 10.0 05/04/171127 Qualifiers Pace Analytical Services, LLC 98W Kinrey Ave. Suite 100 HuntersviKe, NC 28078 (704)875.9092 LABORATORY CONTROL SAMPLE: 1989845 Spike LCS LCS % Rec Parameter Units Conc_ Result %Rec Limits Qualifiers Copper ug1L 500 526 105 85-115 Lead ug1L 500 497 99 85-115 Zinc uglL 500 602 100 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1989846 1989847 NIS MSD 92338369001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug1L ND 500 500 551 493 109 98 70-130 11 Lead ug1L ND 500 500 453 416 91 83 70-130 8 Zinc uglL 30.2 500 500 509 474 96 89 70-130 7 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1989848 1989849 MS MSD 92338866001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug1L ND 500 500 524 508 104 101 70-130 3 Lead ug1L ND 500 500 473 461 95 92 70-130 3 Zinc ug1L 18.2 500 500 473 464 91 89 70-130 2 Received w_ JUN 2 Q 2017 ; Lslnd Quality lS��ection R.'KWA19an this page are in the units indicated by the "units' column excep t where an atternats unit is presented to the rVA or the rmsutt- REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 32 eeAnalytical' wwwPnWb&cam QUALITY CONTROL DATA Project: Outfalls 511 Pace Project No.: 92338864 OC Batch: 358837 Analysis Method: EPA 624 OC Batch Method: EPA 624 Analysis Description: 624 MSV Associated Lab Samples: 92338864001, 92338884002 METHOD BLANK: 1990007 Matrix: Water Associated Lab Samples: 92338864001, 92338864002 Parameter Units 1, 1. 1 -Trichloroethane ug1L 1,1,2,2-Tetrachloroethane ug1L 1,1,2-Trichloroethane ug1L 1,1-Dichloroethane ug1L 1,1-Dichloroethene ug1L 1.2-Dichlorobenzene ugfL 1,2-Dichloroethane ug1L 1.2-Dichloropropane ugfL 1,3-Dichlorobenzene ug/L 1,4-Dichlorobenzene ug/L Benzene uglL Bromodichloromethane uglL Bromoform ug/L Bromomethane ug/L Carbon tetrachloride ug/L Chiorobenzene ugfL Chloroethane ug1L Chloroform ug1L Chloromethane ug1L cis-1,2-Dichloroethene ug1L cis-1,3-Dichloropropene ug1L Dibromochloromethane ugfL Ethylbenzene ug1L Methylene Chloride ug1L Tetrachloroethene ugfL Toluene ugfL trans-1,2-Dichloroethene ug/L tra n5-1, 3-Dichloropropene ug/L Trichloroethene ug/L Trichlorofluoromethane ug/L Vinyl chloride ug/L 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzens (S) % Toluene-d8 (S) % Blank Result Reporting Limit Analyzed ND 2.0 0510211713:20 ND 2.0 0510211713:20 ND 2.0 0510211713:20 ND 2.0 0510211713:20 ND 2.0 05/0211713:20 ND 2.0 0510211713:20 NO 2.0 0510211713:20 ND 2.0 0510211713:20 NO 2.0 05/0211713:20 ND 2.0 05/0211713:20 ND 2.0 05/02/1713:20 ND 2.0 05/02/1713:20 ND 2.0 05/0211713:20 ND 2.0 05/02/1713:20 ND 2.0 05102/1713:20 ND 2.0 OW0211713:20 NO 2.0 05/0211713:20 ND 2.0 05102/1713:20 ND 2.0 05/0211713:20 ND 2.0 05/0211713:20 ND 2.0 05/02/1713:20 ND 2.0 0510211713:20 NO 2.0 05/02/1713:20 ND 2.0 05/0211713:20 NO 2.0 0510211713:20 ND 2.0 0510211713:20 NO 2.0 05/0211713:20 NO 2.0 05102/1713:20 NO 2.0 0510211713:20 NO 2.0 05102J1713:20 ND 2.0 05/02/1713:20 84 70-130 05102/171120 98 70-130 05/02/1713:20 102 70-130 05/0211713:20 Qualifiers Pace Anstylical Services, LLC 9t100 Kinsey Ave_ Suite 100 Huntersvitie, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1990008 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1-Trichloroethane ug1L 20 20.2 101 52-162 1,1,2,2-Tetrachloroethane ug1L 20 18.3 91 46-157 Results presented on this paw we in the units indlcated by Me -Unks- column except where an attamate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 32 r aceAnalj6cal` www.parcom QUALITY CONTROL DATA Project: Outfails 511 Pace Project No.: 92338864 Pace Analytical Services, LLC 98W Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 LABORATORY CONTROL SAMPLE: Parameter 1990008 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,2-Trichloroethane ug1L 20 18.8 94 52-150 1,1-Dichloroethane ug/L 20 19.4 97 59-155 1,1-Dichloroethene ug1L 20 20.5 103 1.234 1,2-Dichlorobenzene ug/L 20 19.7 98 18-190 1,2-Dichloroethane ug/L 20 18.7 94 49-155 1,2-Dichloropropane ug1L 20 19.1 96 1-210 1,3-Dichlorobenzene ug1L 20 19.5 97 59-156 1,4-Dichlorobenzene ug1L 20 20.0 100 18-190 Benzene uglL 20 20.2 101 37-151 Bromodichloromethane ug/L 20 19.9 100 35-155 Bromoform ug/L 20 19.0 95 45-169 Bromomethane ug/L 20 24.3 121 1-242 Carbon tetrachloride ug1L 20 20.6 103 70-140 Chlorobenzene ug/L 20 19.4 97 37-160 Chloroethane ug/L 20 18.3 91 14-230 Chloroform ug1L 20 19.6 98 51-138 Chloromethane ug1L 20 24.4 122 1-273 cis- 1,2-Dich loroethene ug/L 20 19.2 96 68-146 cis- 1,3-Dichloropropene ug/L 20 21.9 110 1-227 Dibromochloromethane ug/L 20 20.5 103 53-149 Ethylbenzene ug/L 20 19.5 97 37-162 Methylene Chloride ug/L 20 18.6 93 1-221 Tetrachloroethene ug/L 20 19.2 96 64-148 Toluene ug/L 20 20.0 100 47-150 trans- 1,2-Dichloroethene ug/L 20 18.8 94 54-156 trans-1,3-Dichloropropene ug/L 20 20,9 105 17-183 Trichloroethene ug/L 20 20.0 100 71-157 Trichlorofluoromethane ug/L 20 21.9 110 17-181 Vinyl chloride ug/L 20 20.3 101 1-251 1,2-Dichloroethane-d4 (S) % 103 70-130 4-Bromoguorobenzene (S) % 103 70-130 Toluene-d8 (S) % 101 70-130 MATRIX SPIKE SAMPLE: Parameter 1990010 Units 92338724001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1-Trichloroethane ug1L ND 20 21-6 108 46-171 1,1,2,2-Tetrachlomethane ug/L ND 20 20.3 102 73-159 1,1,2-Trichloroethane ug/L ND 20 21.7 108 64-152 1,1-Dichloroethane ug/L ND 20 22.2 111 43-172 1,1-Dichloroethene ug/L ND 20 23.6 118 48-189 1,2-Dichlorobenzene ug/L ND 20 22A 112 54-154 1,2-Dichloroethane ug/L ND 20 20.7 104 42-171 1,2-Dichloropropane ug/L ND 20 22.9 114 55-157 1,3-Dichlorobenzene ug/L ND 20 23.3 116 57-148 Results presented on this page are in the units Ind"ted by the -Units- column except where an altercate unit IS presented to the right of the reutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11 /2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 32 aceAnalytical e wew{vaetabs.carn QUALITY CONTROL DATA Project: Outfalls 5/1 Pace Project No,: 92338864 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE SAMPLE: Parameter 1990010 Units 92338724001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,4-Dichlorobenzene ugIL ND 20 23.0 115 58-149 Benzene ug1L NO 20 23.5 118 54-163 Bromodichloromethane ug/L ND 20 22.0 110 56-152 Bromoform ug/L NO 20 20.5 102 53-151 Bromomethane ug/L ND 20 23.1 115 10-200 Carbon tetrachloride ug/L ND 20 23.7 119 41-175 Chlorobenzene u9/L ND 20 21.7 108 67-152 Chloroethane ug/L ND 20 22.6 113 23-200 Chloroform ug/L NO 20 21.4 107 51-166 Chloromethane ug/L NO 20 26.3 132 40-175 cis-1,2-Dichloroethene ug/L NO 20 22.9 114 45-174 cis-1,3-Dichloropropene ug/L NO 20 22.9 114 38-146 Dibromochloromethane ug/L NO 20 23.7 118 65-144 Ethylbenzene ug/L NO 20 22.4 112 57-152 Methylene Chloride uglL NO 20 20.2 101 40-167 Tetrachloroethene ug/L NO 20 22.0 110 59-155 Toluene ug/L ND 20 22.1 111 47-162 trans-1,2-Dichloroethene ug/L ND 20 23.5 117 47-178 trans-1,3-Dichloropropene ug/L ND 20 21.5 107 39-148 Trichloroethene ug/L ND 20 23.9 120 60-153 Trichlorofluoromethane ug/L ND 20 24.0 120 42-199 Vinyl chloride ug/L ND 20 23.2 116 46-176 1,2-Didvoroethan"4 (S) % 98 70-130 4-Bromotluorobenzene (S) % 102 70-130 Toluene-d8 (5) % 101 70-130 SAMPLE DUPLICATE: 1990009 Parameter Units 92338724002 Result Dup Result RPD Qualifiers 1,1,1-Trichloroethane ug/L NO NO 1,1,2,2-Tetrachloroethane ug/L NO ND 1,1,2-Trichloroethane uglL NO ND 1,1-Dichloroethane uglL ND ND 1,1-Dichloroethene uglL NO ND 1,2-Dichlorobenzene uglL NO NO 1,2-Dichloroethane ug1L NO ND 1,2-Dichloropropene uglL ND ND 1,3-Dichlorobenzene ug/L ND NO 1,4-Dichlorobenzene uglL ND NO Benzene ug/L ND ND Bromodichloromethane ug/L ND NO Bromoform ug/L ND NO Bromomethane ug/L ND NO Carbon tetrachloride Ug/L NO NO Chlarobenzene ug/L ND NO Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 32 aclQArralytrcal www.perefa &00M QUALITY CONTROL DATA Project: Outfalis 511 Pace Project No.: 92338864 SAMPLE DUPLICATE: 1990009 Parameter Units 92338724002 Result Dup Result Chloroethane ug1L NO NO Chloroform ug/L NO NO Chloromethane ug1L NO NO cis-1,2-Dichloroethene ug/L NO NO cis- 1,3-Dichloropropene ug1L ND NO Dibromochloromethane ug/L ND NO Ethylbenzene ug1L NO NO Methylene Chloride ug1L NO ND Tetrachloroethene ug/L NO ND Toluene ugifL ND ND trans-12-Dichloroethene ug/L NO ND trans- 1,3-Dichloropropene ug/L NO NO Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl chloride ug/L NO ND 1,2-Dichloroethane-d4 (S) % 81 93 4-8romofluorobenzene (S) % 101 101 Toluene-d8 (S) % 102 104 RPD Qualifiers 14 0 3 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Results presented on this page are In the units Indicated by the'Units- column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/1112017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 32 s aceAnalytrcal • OWNPI QUALITY CONTROL DATA Project: Outfalls 511 Pace Project No.: 92338864 QC Batch: 358641 Analysis Method: EPA 608 QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB Associated Lab Samples: 92338864001, 92338864002 METHOD BLANK: 1989142 Matrix: Water Associated Lab Samples: 92338864001, 92338864002 Parameter Units 4,4'-DDD ug/L 4,4'-DD£ ug/L 4,4'-DDT ug/L Aldrin ug1L alpha-BHC ug1L beta-BHC ug/L Chlordane (Technical) ug1L delta-BHC uglL Dieldrin ug1L Endosulfan I ug1L Endosulfan II ug/L Endosulfan sulfate ug/L Endrin uglL Endrin aldehyde ug/L gamma-BHC (Lindane) ug/L Heptachlor ug/L Heptachlor epoxide ug/L PCB-1016 (Aroclor 1016) ug/L PCB-1221 (Aroclor 1221) ug/L PCB-1232 (Aroclor 1232) ug/L PCB-1242 (Aroclor 1242) ug/L PCB-1248 (Aroclor 1248) ug1L PCB-1254 (Aroclor 1254) ug/L PCB-1260 (Aroclor 1260) ug/L Toxaphene ug1L Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % LABORATORY CONTROL SAMPLE: 1989143 Blank Result Reporting Limit Analyzed NO 0.050 05102/1718:27 ND 0.050 0510211718:27 ND 0.050 05MV1718:27 ND 0.050 05102/1718:27 ND 0.050 OSM2/1718:27 NO 0.050 0510211718:27 ND 0.50 05/02/1718:27 NO 0.050 05102/1718:27 NO 0.050 0510211718:27 NO 0.050 05/02/1718:27 NO 0.050 05/0211718:27 ND 0.050 05102/1718:27 ND 0,050 05102/1718:27 ND 0.050 05/0211718:27 ND 0.050 051D211718:27 ND 0,050 05/02/1716:27 NO 0.050 05102J1718:27 ND 0.50 05/0211718:27 NO 0.50 0510211718:27 NO 0.50 05/0211718:27 NO 0.50 05/0211718:27 ND 0.50 05102/1718:27 ND 0.50 05/0211718:27 NO 0.50 0510211718:27 NO 0.50 05/0211718:27 98 20-138 0510211718:27 97 20-110 0510211718:27 Qualifiers Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Received JUN 2 0 2017 :-: Land Quality Section A5heville Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 4,4'-DDD ug1L .25 0.24 99 31-141 4,4'-DDE ug/L .25 0.23 93 30-145 4,4'-DDT ug1L .25 0.24 96 25-160 Aldrin ug/L .25 0.20 79 42-122 alpha-ISHC ug/L .25 0.25 99 37-134 beta-BHC ug1L 25 0.20 82 17-147 delta-BHC ug/L .25 0.24 98 19-140 Diekfrin UA .25 0.24 97 36-146 Endosulfan I ug1L .25 0.25 99 45-153 Results presented on this page are In the units Indicated by the 'Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 32 aceAnalj cal Ir+vw.pxohbs ccm QUALITY CONTROL DATA Project: Outfalls 511 Pace Project No.: 92338864 LABORATORY CONTROL SAMPLE: 1989143 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Endosulfan II ug1L .25 0.25 100 1-202 Endosulfan sulfate ug1L .25 0.25 100 26-144 Endrin uglL .26 0.25 102 30-147 Endrin aldehyde uglL .25 0.23 93 50-150 gamma-BHC (Lindane) ug1L .25 0.25 102 32-127 Heptachlor uglL .25 0.21 87 34-111 Heptachlor epoxide ug1L .25 0.24 99 41-126 Decachlorobiphenyt (S) % 93 20-138 Tetrachloro-m-xylene (5) % 97 20-110 Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LA130RATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 06/11/2017 04 A4 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 32 aceAnaly cal' wuw.pacsA tmn QUALITY CONTROL DATA Project: Outfatls 511 Pace Project No.: 92338864 QC Batch: 358866 Analysis Method; EPA625 QC Batch Method: EPA 625 Analysis Description: 625 MSS Associated Lab Samples: 92338864001, 92338864002 METHOD BLANK: 1990326 Matrix: Water Associated Lab Samples: 92338864001, 92338864002 Parameter Units Blank Result Reporting Limit Analyzed Qualifiers 1,44-Trichlorobenzene ug/L NO 5.0 05/04/17 00:38 2,2'-Oxybis(1-chloropropane) ug/L NO 5.0 05/0411700:38 2,4,6-Thchlorophenol ug/L NO 10.0 05/04/17 00:38 2,4-Dichlorophenol ug/L NO 5.0 05104/17 00:38 2,4-Dimethylphenol ug/L NO 10.0 05/04/17 00:38 2,4-Dinitrophenol ug/L NO 50.0 05104/17 00:38 2,4-Dinitrotoluene ug/L NO 5.0 W04/17 00:38 2,6-Dinitrotoluene ug/l. ND 5.0 05104117 00:38 2-Chloronaphthalene uglL ND 5.0 05/04/17 00:38 2-Chlorophenol uglL NO 5.0 05/04/17 00:38 2-Nitrophenol uglL NO 5.0 05/04/17 00:38 3,3'-Dichlorobenzidine uglL ND 25.0 05/04/17 00:38 4,6-Dinitro-2-methylphenol uglL ND 20.0 05/04/17 00:38 4-Bromophenylphenyl ether uglL ND 5.0 05/04/17 00:38 4-Chloro-3-methylphenol uglL NO 5.0 05/04/17 00:38 4-Chlorophenylphenyl ether uglL NO 5.0 05104/17 00:38 4-Nitrophenol uglL ND 50.0 05/G4/17 00:38 Acenaphthene uglL NO 5.0 05/04/17 00:38 Acenaphthylene ug1L NO 5.0 05/04/17 00:38 Anthracene ug/L NO 5.0 05/04/17 00:38 Benzo(a)anthracene ug/L ND 5.0 05/04/17 00:38 Benzo(a)pyrene ug/L NO 5.0 05/04/17 00:38 Benzo(b)fluoranthene ug/L NO 5.0 05/04/17 00:38 Benzo(g,h,i)perylene ug/L NO 5.0 05/04/17 00:38 Benzo(k)fluoranthene ug/L ND 5.0 05104/17 00:38 bis(2-Chloraethoxy)methane ug/L ND 10.0 05/04117 00:38 bis(2-Chloroethyl) ether ug/L NO 5.0 05/04/17 00:38 bis(2-Ethylhexyl)phthalate ug/L NO 5.0 05/04/17 00:38 Butylbenzylphthalate ug/L NO 5.0 05/04/17 00:38 Chrysene ug/L NO 5.0 05/04/17 00:38 Di-n-butylphthalate ug/L NO 5.0 05/04/17 00:38 Di-n-octylph tha late ug1L NO 5.0 05/04/17 00:38 Dibenz(a,h)anthracene ug1L ND 5.0 05/04/17 OD:38 Diethylphthalate ugtL ND 5.0 05104/17 00:38 Oimethylphthalate ug/L ND 5.0 05/04/17 00:38 Fluoranthene ug/L NO 5.0 05/04117 00:38 Fluorene ug/L NO 5.0 05/04/17 00:38 Hexachloro-1,3-butadiene ug/L NO 5.0 0510411700:38 Hexachlorobenzene ug/L ND 5.0 05/04/17 00:38 Hexachiorocyclopentadiene ug/L NO 10.0 05/04/17 00:38 Hexachloroethane uglL NO 5.0 05/04/17 00:38 Pace Analytical services, LLC 9800 KinceyAve. Suite 100 Ftuntersville, NC 28078 (704)875-9092 Results presented on Mis page are En the units Indicated by the -ur8ta- column except vobare an alternate unit is pts"nted to the FlgW of the resutL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC, Page 20 of 32 aceAnalyti►ca!' nww.pacslabimm QUALITY CONTROL DATA Project: Outfalls 511 Pace Project No.: 92338864 METHOD BLANK: 1990326 Associated Lab Samples: 92338864001, 92338864002 Parameter Units Matrix: Water Blank Reporting Result Limit Analyzed Indeno(1,2,3-ed)pyrene ug/L ND 5.0 05/04/17 00:38 isophorone ug1L NO 10-0 05104/17 00:38 N-Nitroso-di-n-propylamine ugfL NO 5.0 05/04/17 00:38 N-Nitrosodimethyfamine ugfL NO 5.0 05104/17 00:38 N-Nitrosodiphenylamine ugfL NO 10.0 05/04/17 00:38 Naphthalene ugfL ND 5.0 05/04/17 00:38 Nitrobenzene ug/L ND 5.0 05/04/17 00:38 Pentachlorophenol ugfL NO 10.0 05/04/17 00:38 Phenanthrene ugfL ND 5.0 05/04/17 00:38 Phenol ugfL ND 5.0 05/04/17 00:38 Pyrene ugfL NO 5.0 05/04/17 00:38 2,4,6-Tribromophenol (S) % 85 10-137 05104/17 00:38 2-Fluorobiphenyt (S) % 71 15-120 G5104117 00:38 2-Fluorophenol (S) % 37 10-120 05/04/17 00:38 Nitrobenzene-d5 (S) % 67 10-120 05/04/17 00:38 Phenol-d6 (S) % 25 10-120 05/04/17 00:38 Terphenyl-d14 (S) % 93 11-131 05/04/17 00:38 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1990327 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4-Trichlorobenzene ugfL 50 29.7 59 44-142 2.2'-Oxybis(1-chloroprepane) ugfL 50 26.9 54 36-166 2,4,6-Trich lorophen ol ugfL 50 37.8 76 37-144 2,4-Dichlorophenol ugfL 50 35.8 72 1-191 2,4-Dimethylphenol ugfL 50 35.3 71 32.119 2,4-Dinitrophenol ugfL 250 162 65 1-181 2.4-Dinitrotoluene ug/L 50 45.2 90 39-139 2.6-Dinitrotoluene ug/L 50 45.2 90 50-158 2-Chloronaphthalene ugfL 50 33.8 68 60-118 2-Chlorophenol ugfL 50 28.1 56 23-134 2-Nitrophenol ugfL 50 33.0 66 29-182 3,3'-Dichlorobenzidine ugfL 100 73.9 74 1-262 4,6-Dinitro-2-methylphenol ugfL 100 76.8 77 1-181 4-Bromophenylphenyl ether ugfL 50 38.3 77 53-127 4-Chloro-3-methylphenol ug/L 100 73.2 73 22-147 4-Chlorophenylphenyl ether ug/L 50 35.6 71 25-158 4-Nitrophenof ug/L 250 73.0 29 1-132 Acenaphthene ug/L 50 35.1 70 47-145 Acenaphthylene ug/L 50 34.5 69 33-145 Anthracene ug/L 50 38.7 77 1-166 Benzo(a)anthracene ug/L 50 36.8 74 33-143 Benzo(a)pyrene ugfL 50 36.0 72 17-163 Benzo(b)fiuoranthene ugfL 50 36.3 73 24-159 Pace Analytical Services, LLC 98M Kincey Ave. State 100 Huntersville, HC 28078 (704)875-9092 Qualifiers Results presented on this page are in the units Indicated By the -Units" column except where an alternate unit Is presented to the right of the ratan. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 32 aceAnalytical rwwor tett* mn QUALITY CONTROL DATA Project: Outfalls 511 Pace Project No.: 92338864 LABORATORY CONTROL SAMPLE: 1990327 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Benzo(g,h,l)perylene ugiL 50 37.2 74 1.219 Benzo(k)fiuoranthene ugiL 50 35.7 71 11-162 bis(2-Chloroethoxy)methane ugiL 50 31.6 63 33-184 bis(2-Chloroethyl) ether ugiL 50 28.5 57 12-158 bis(2-Ethylhexyl)phthalate ugiL 50 41.7 83 8-158 Butylbenzyiphthalate ugiL 50 40.6 81 1-152 Chrysene ug1L 50 35.4 71 17-168 Di-n-butylphthalate ug1L 50 41-3 83 1-118 Di-n-ocrylphthalate ug/L 50 46.9 94 4-146 Dibenz(a,h)anthracene ugiL 50 38.5 77 1-227 Diethylphthalate ugiL 50 37.5 75 1-114 Dimethylphthatate ug1L 50 36.6 73 1-112 Fluoranthene ugiL 50 41.7 83 26-137 Fluorene ug1L 50 36.6 73 59.121 Hexachloro-1,3-butadiene ugiL 50 27.7 55 24-116 Hexachlorobenzene ug1L 50 38.1 76 1-152 Hexachlorocyclopentadiene ugiL 50 17.5 35 25-150 Hexachloroethane ugiL 50 21.8 44 40-113 Indeno(1,2,3-cd)pyrene ug1L 50 38.1 76 1-171 Isophorone ugiL 50 40.0 80 21-196 N-Nitroso-di-n-propylamine ugiL 50 31.7 63 1-230 N-Nitrosodimethylamine ugiL 50 19.0 38 25-150 N-Nitrosod iphenyta mine ugiL 50 37.1 74 25-150 Naphthalene ugiL 50 29.7 59 21-133 Nitrobenzene ugiL 50 34.1 68 35-180 Pentachlorophenol ug1L 100 84-7 85 14-176 Phenanthrene ugiL 50 37.3 75 54-120 Phenol ug1L 50 14.1 28 5-112 Pyrene ugiL 50 35.4 71 52-115 2,4,6-Tribromophenol (S) % 82 10-137 2-Fluorobiphenyl (S) % 67 15-120 2-Fluorophenol (S) % 34 10-120 Nitrobenzene-d5 (S) % 63 10-120 Phenol-d6 (S) % 24 10-120 Terphenyl-d14 (S) % 78 11-131 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1990328 1990329 MS MSD 92338916001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD (Dual 1,2,4-Trichlorobenzene ug1L 0.98U 100 100 71,3 48.7 71 49 44-142 38 R1 2,2'-Oxybis(1-chloropropane) ugiL 0.95U 100 100 64.4 44-0 64 44 36-166 38 R1 2,4,6-Trichlorophenol ug1L 1.3U 100 100 81.6 60.9 82 61 37-144 29 2,4-Dichlorophenol U911- 1.7U 100 100 82.4 54.1 82 54 1-191 42 R1 2,4-Dimethylphenol ugiL 1.2U 100 100 61 6.8J 6 7 32-119 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shrill not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 32 Pace Analytical Services, LLC ace,afytrcal • 9800 Kincey Ave. Suite 100 Nuntersville, NC 28078 wwwplll wmcom (704)875-9092 QUALITY CONTROL DATA Project: OkMalls 5/1 Pace Project No.: 92338864 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1990328 1990329 Parameter 92338916001 Units Result MS Spike Conc. MSD Spike Conc. MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual 2,4-Dinitrophenol ug/L 9.OU 500 500 410 327 82 65 1-181 23 2,4-Dinitrotoluene ug/L 0.90U 100 100 95.7 78.5 96 78 39-139 20 2,6-Dinitrotoluene ug1L 0.98U 100 100 99.6 78.7 100 79 50-158 23 2-Chloronaphthalene ug/L 0.98U 100 100 75.0 51.2 75 51 60-118 38 M1,R1 2-Chlorophenol ug/L 1.3U 100 100 70.1 45.6 70 46 23-134 42 Ri 2-Nitrophenol ug/L 0.91U 100 100 81.0 54.9 81 55 29-182 38 R1 3,3'-Dichlorobenzidine ug1L 2.1U 200 200 NO ND 0 0 1-262 M1 4,6-Oinitro-2-methylphenol ug1L 21U 200 200 161 133 50 66 1-181 19 4-Bromophenylphenyl ether ug/L 0.82U 100 100 78.8 62.5 79 63 53-i27 23 4-Chloro-3-methylphenol ug/L 3.7U 200 200 155 121 77 60 22-147 24 4-Chlorophenylphenyl ether ug1L 0.87U 100 100 77.0 58.7 77 59 25-158 27 4-Nitrophenol ug1L 4.1U 500 500 256 226 51 45 1-132 12 Acenaphthene ug/L 0.25U 100 100 75.7 54.9 77 55 47-146 33 R1 Acenaphthylene ug/L 0.21U 100 100 70.5 50.7 71 51 33-145 33 R1 Anthracene ug/L 0.14U 100 100 52.6 45.4 53 45 1-166 15 Benzo(a)anthracene ug/L 0.33U 100 100 72.0 53.6 72 64 33-143 12 Benzo(a)pyrene ug/L 0.30U 100 100 43.4 39.8 43 40 17-163 9 Benzo(b)fluoranthene ug1L 0.28U 100 100 80.2 69.6 80 70 24-159 14 Benzo(g,h,i)perylene ug/L 0.38U 100 100 80.1 58.9 80 69 1-219 15 Senzo(k)fluoranthene ug/L 0.43U 100 100 78.7 67.9 79 68 11-162 15 bis(2-Chioroethoxy)methane ug/L 0.92U 100 100 72.8 47.2 73 47 33-184 43 R1 bls(2-Chloroethyl) ether ug/L i.OU 100 100 66.6 45.5 67 46 12-158 38 R1 bis(2-Ethylhexyl)phthalale ug/L 0.79U 100 100 88.3 77.2 88 77 8-458 13 Butylbenzylphthalate ug/L 0.79U 100 100 86.5 76.9 85 77 1-152 12 Chrysene ug/L 0,21 U 100 100 76.1 65.8 76 66 17-168 15 Di-n-burylphthalate ug1L 0,75U 100 100 85.4 72.0 85 72 1-118 17 Di-n-octylphthalate ug/L 0,66U 100 100 104 88.6 104 89 4-146 16 Dibenz(a,h)anthracene ug/L 0.55U 100 100 85.4 72.0 85 72 1-227 17 Diethylphthalate ug/L 0.58U 100 100 81.5 64.0 82 64 1-114 24 Dimethylphthalate uglL 0.76U 100 100 80.2 61.6 80 62 1-112 26 Fluoranthene uglL 0.21 U 100 100 88.6 76.4 89 76 26-137 15 Fluorene uglL 0.21 U 100 100 78.8 61.0 79 61 59.121 25 Hexachloro-1,3-butadiene ug1L 0,94U 100 100 69.4 47,9 69 48 24-116 37 R1 Hexachlorobenzene ug/L 0,72U 100 100 77.2 61.4 77 61 1-152 23 Hexachlorocyclopentadiene ug/L 0.88U 100 100 50.4 33.2 50 33 25-150 41 R1 Hexachloroethane uglL 1AU 100 100 61.8 43.9 62 44 40-113 34 R1 Indeno(1,2,3-cd)pyrene ug/L 029U 100 100 85.1 72.5 85 72 1-171 16 Isophorone ug/L 0.89U 100 100 84.2 58.2 84 58 21-196 37 RI N-Nitros"i-n-propylamine ug/L 0.99U 100 100 75.3 48.7 75 49 1-230 43 R1 N-Nitrosodimethylamine ug/L 0.91U 100 100 53.4 39.1 53 39 25-150 31 R1 N-Nitrosodiphenyiamine ug/L 1,OU 100 100 67A 50.4 67 50 25-150 29 Naphthalene ug/L 0.34U 100 100 72.2 48.7 72 49 21-133 39 RI Nitrobenzene ug/L 1.1 U 100 100 132 81.9 132 82 35-180 47 R1 Pentachlorophenol ug/L 4.6U 200 200 177 150 88 75 14-176 16 Phenanthrene ug/L 0,22U 100 100 76.5 63.8 76 64 54-120 18 Phenol ug/L 2.81 100 100 47.6 31.8 45 29 5.112 40 R1 Results Presented on this Pate are in the units indlcated by the -Units" column except where in alternate unit is presented to the right of the rezuX REPORT OF LABORATORY ANALYSIS This report shall not t>e reproduced, except in full. Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 32 (� laneAnalyfical" tnnrpaaetatrxoom QUALITY CONTROL DATA Project: Outfalls 5/1 Pace Project No,: 92338864 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875.9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1990328 1990329 MS MSD 92338916001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Pyrene ug/L 0.19U 100 100 70.3 613 70 62 52-115 13 2,4,6-Tribromophenol (S) % 81 67 10-137 2-Fluorobiphenyl (S) % 69 46 15-120 2-Fluorophenol (S) % 43 31 10-120 Nitrobenzene-d5 (S) % 70 47 10-120 Phenol-d6 (S) % 35 24 10.120 Terpttenyl-d14 (S) % 75 60 11-131 Results presented on this pass are in the units Indicated by the "Units" column except where an alternate unit ie presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/1112017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 32 lace Analytical" www.pat:afabsoorn QUALITY CONTROL DATA Project: Outfalls 5/1 Pace Project No_: 92338864 QC Batch: 358895 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 02338864001, 92338864002 METHOD BLANK: 1990420 Associated Lab Samples: 92338864001, 92338864002 Parameter Units Total Suspended Solids mgtL LABORATORY CONTROL SAMPLE: 1990421 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, LLC 9800 Kinsey Ave- Suile 100 Huntersvitie, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result limit Analyzed Qualifiers ND 2.5 0510211719:48 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 244 98 90-110 SAMPLE DUPLICATE: 1990422 92338739003 Dup Parameter Units Result Result Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1990423 92338939004 Oup Parameter Units Result Result Total Suspended Solids mgJL 4.3 4.5 RPD Qualifiers RPD Qualifiers 3 Results prowted on M pao are in the units indicated by the -Units' column except where sn altemate unit is presented to am right of the resu it. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull. Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 32 aceAnalytical • ..pacafabacxn Project: Outfalls 511 Pace Project No.: 92338864 QC Batch: 359857 QC Balch Method: EPA 420.4 Associated Lab Samples: 92338864001, 92338864002 METHOD BLANK: 1995617 Associated Lab Samples: 92338864001, 92338864002 Parameter Units Phenol mg/L QUALITY CONTROL DATA Analysis Method: EPA420.4 Analysis Description: 420.4 Phenolics Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.010 05111/1712:05 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1995618 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phenol mg/L .05 0.049 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1995619 1995620 MS MSD 92338369006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phenol mg/L 0.012 .05 .05 0.064 0.062 104 99 90-110 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1995621 1995622 MS MSD 92339059001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phenol mg/L 0.083 �.05 .05 0.12 0.11 64 62 90-110 1 M7 Received JUN 2 0 2017 Land Quality Section Asheville Results presented on thle page are In bre unite Indicated by the'Units' column except where an altemate unit is presentee to Ne right of the rewit. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, L-C. Page 26 of 32 I aCeAna1y[ a1 wwwpacpra6:com QUALITY CONTROL DATA Project: Outfalls fill Pace Project No_: 92338864 QC Hatch: 359331 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92338864001, 92338864002 Pace Analyticar Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 1992843 Matrix: water Associated Lab Samples: 92338864001. 92338864002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide mg1L ND 0.0080 05I0611714:49 LABORATORY CONTROL SAMPLE: 1992844 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide mg1L A 0.10 105 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1992845 1992846 MS MSD 92339029002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Cyanide mg1L 0.013 _i .1 0.024 0.023 11 11 80-120 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1992847 1992848 MS MSD 92339049002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide mglL ND ,1 .1 0.11 0.10 103 98 80-120 5 Reeutts presented on this page are in the units indicated by Ow "UnW column except where an atternste unit ie presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 32 CBAnalyt►Ca1. wwwpsowfiftom QUALIFIERS Project: Clutfalls 5/1 Pace Project No_: 92338864 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave_ Suite 100 Hurnersvige, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. POL - Practical Quandtation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenytamine decomposes and cannot be separated from Diphenylamine using Method 8270. The resutt reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analyzes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded 40 limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 32 a aceAnaly�rcal xww.pacsumaum QUALITY CONTROL DATA CROSS REFERENCE TABLE Project, Outfalls 511 Pace Project No.'. 92338864 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 10C Huntersvilie, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92338864001 Outfall #1 EPA 16645 359654 92338864002 Outfall #2 EPA 1664E 359654 92338864001 Outfall 01 EPA 3510 358641 EPA 508 92338864002 Outfall #2 EPA 3510 358641 EPA 608 92338864001 Outfall #1 EPA 200.7 358814 EPA 200.7 92338864002 Outfall #2 EPA 200.7 358814 EPA 200.7 92338864001 Outfall #1 EPA 625 358866 EPA 625 92338864002 Outfall #2 EPA625 358866 EPA 625 92338864001 Outfall #1 EPA 624 358837 92338864002 Outfall #2 EPA624 358837 92338864001 Outfall #1 SM 2540D 358895 92338864002 Outfall #2 SM 2540D 358895 92338864001 Outfall #1 EPA 420.4 359857 92338864002 Outfall #2 EPA 420A 359857 92338864001 Outfall #1 SM 4500-CN-E 359331 92338864002 Outfall #2 SM 4500-CN-E 359331 Date: 05/11/2017 04;44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 358823 358823 359058 359058 359027 359027 Page 29 of 32 9 r 0 Document Name: Document Revised: Sept. 21, 2016 �aceAnalj6cal' Sample Condition Upon Recei tjSCUR) Aage 1 of 2 Document No,: Issuing Authority: / F-CAR-CS-033-Rev.01 Pace Quality Office Laboratory receiving sam . • .... , _ _Asheville -- ___ EdanE •.. _- .-Greenwood Q - Huntersville ❑ - RaielghQ .. ,.., Vechanicsville0... Client Name: W®# ' 92338864 INctA � Pr__ ' Courier; ❑Fed Ex ❑UPS OUSPS Client ❑ Commercial ❑Pace ❑Other, 92336864 Custody Seal Present? ❑Yes o Seals intact? Dyes - ONO Dale/Initials Person Examining Contents: '��G j Packing Material: ❑Bubble Wrap ❑Bubble Bags one ❑Other: Thermometer; et ❑❑ Slue None ❑. Samples on ice, cooling process has be un ❑GunID: Type of Ic � Correction Factor. Q Cooler Temp Corrected ('C): Li , Biological Tissue Frozen? ❑Yes ❑No N/A Temp should be above freezin VC USDA Regulated Sail (Q A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source Vnternati y, ❑Yes [—]No including Hawaii and Puerto Rico)? []Yes {A o Chain of Custody Present? Qfe'5 No N/A 1. Samples Arrived within Hord Time? Yes ©No (:31,J/A 2. Short Hold Time Analysis (02 hr.)? Dyes o N/A I Rush Turn Around Time Requested? ❑Yes o N/A 4. Sufficient Volume? IJxes ©No ❑N/A S. Correct Containers Used? -Pace Containers Used? ae's ONo ,�.., I f;._ _r­lNo ❑N/A I-lN/A 6. Containers Intact? L:4es LJNo N/A 7. Samples Field Filtered? ❑Yes No A 8, Note if sediment is visible in the dissolved container Sample labels Match COC? es [:]No ❑N/A 9, Incivoesuareiiirneliii/i4naiysis Matrix: -• - - . -•_- . .,-. __._ . ,-. _ . ­­.. . , .. _ Headspace in VOA Vials (>S-Timm)? Oyes a ❑N/A 10. Trip Blank Present? ❑Yes Ne [NfA il. Trip Blank Custody Seals Present? ❑Yes (]No ❑N/A CLIENT NOTIFICATION/RESOWTION Field Data Required? ❑Yes ❑No Person Contacted: Comments/Sampie Discrepancy: Date/Time: Project Manager SCURF Review: 1! Date: Project Manager SRF Review: 1_� Date: Note; Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, Incorrect containers) Page 30 of 32 VS 3 m 8 K M 'n n d m S a A � m. S 9 n C v a P, m A 0 nF g G � o A a ro M m m � CL n vy N R � n ° a a ro Ln D O d � a CL a m M CL m S m as hJ Y p 'n 00 ., cn W a w ^' '" Item# ZZZZ -7 Z BP4U-125 mt Plastic Unpreserved (NIA) (CI-) BP3U-ZS0 mt Plastic Unpreserved (N/A) BP2U-500 mL Plastic Unpreserved (N/A) BPiU-1 liter Plastic Unpreserved (N/A) BM-250 mL Plastic H2SO4 (pH < 2) (0.1 SP3N-250 mL plastic HNO3 (pH <2) mL Plastic ZN Acetate & NaOH (>9) z7zBP3Z-250 Z z V MC-250 mL Plastic NaOH (pH > 12) (CI-) WGFU-Wide-mouthed Glass jar Unpreserved AG]U-1 liter Amber Unpreserved (N/Al (CI-) ZZ47-Z ZZZ2�41, AG1H-1 liter Amber HCI (pH < 2) AG3U-ZS0 mL Amber Unpreserved (NIA) (CI-) AG1S-1 liter Amber H2SO4 (pli < 21 AG35-250 mL Amber H2SO4 (pH < 2) zzz z `AG3A(DG3A)-250 mL Amber NH4Cl (N/A)(CI-) DG9H-4O m L VOA HCI (N/A) VG9T-40 mL VOA Na2S203 (N/A) • VG9U-40 mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 (NIA) VOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SPST-JZ5 mt Sterne Plastic (NIA —Fab) SP2T-250 mL Sterile Plastic (N/A —lab) BP3A-250 mL Plastic (NHZ)2SQ4 (9.3-9.7) Cubitainer VSGU-20 mL Scintillation vials (N/A) GN n 0 M O � • CL 3 w pr CL IU Q 0 3 o Cr -0 = tat q tD is sat n x `S LA 3 rr fG t9 it y o � Cr � m m _ w t9 In O a m °* n 3 v C a 3 M 0 C w to C 5 ' c w t0 C m rn � � ro �o a n M C n z � 2L Q 7-0 o c r0 • ■ 3 ro 7 { (A) nro_. Ot Q C a N Q @ ()0 C� Q�1 rr'a N f- N C v N r U1 v ®I� l PkeAnalytical' CHAIN -OF -CUSTODY 1 Analytical Request Document N The Chairt-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accuratety. 0 CV Patio: of Section A Section B Section C Required Client information: Required Project Inlormatiorl: Invoice Information: Company: 't RCpon To: Allenlion: 2210988 r Address: y ' / G/ —7 ( ! Copy To: Company Nama; REGULATORY AGENCY t Address: F- NPDES r GROUND WATER 1— DRINKING WATER E— LISTRCRA OTHER Email To; Purchase Order No.: P•rcu Or+r+ur RO—: Phone; Fax: Protect Name: Paeu P1pI"cl 9-- Site Location STATE: Requoated Duo DWdTAT: Project Number: Pass Protilo R: Requested Analysis Filtered (YIN) Section D Matrix Cedes RequlmdClienl Information MATRIX r cDDE s COLLECTED Preservatives, Drinking Water DW Water WT WasloWater WW $ Z Lj � COMPOSITE .1 V Product P J �.i V - Z SoillSolid SL m p l SAMPLE ID oil OL 4 T F tr w H t v fA•2.091;j Are' AR w a ? H T Sample IDs MUST BE UNIOUE Tissue TS 00 L) a ,wItz Z •T f •b U Other OT r QZ —p r aow R N DATE TIME DATE TIME _ _ _ Z O y '. !r Pace Project No.1 Lab I.D. 4 5 6 7 B 9 !0 11 12 ADDITIONAL COMMENTS RELINQUISHED BY t AFFILIATION DATE ACCEPTED BY t AFFILIATION DATE TIME SAMPLE CONDITIONS fp ",��G _fir 7 p�.TIME i ti5�i 1I l, 7v 5A SAMPLER NAME AND SIGNATURE V u w m ORIGINAL PRINT Name of SAMPLER: -Lr1�, r %! Z (GC c = y o a z it v, 5. DATE Signed SIGNATURE of SAMPLER: ,..��rtMN1DDlYYI: r C) ra E -.. 'I.gotam Now By sWmg Utz W. you are erapiirrg Paoli s NET 30 day payrnenl tutu and a9r00wV 0 Late cR rges kI 1.5% Per mends for any inveica%not paid within 30 drys. r F-ALL."20rev.07. 15•May-2007 ALI NCDENR NZn C 0� �o+llTl4lMT O, Ewli ..ew.Ho NmyR Rzl0 .CE9 •1 �sion of Water Quality / Surface Wa Protection National Pollutant Discharge Elimination System PERMIT NAME/OWNERSHIP CHANGE FORM FOR AGENCY USE ONLY Date Received Year Nfonth oay 1. Please enter the permit number for which the change is requested. NPDES Permit (or) Certificate of Coverage N G. S© N G G. 0 1 3_1 0 0 0 0 I1. Permit status prior to requested change. a. Permit issued to (company name): Pentair Valves & Controls b. Person legally responsible for permit: Salvatore First RECEP amaian of water AUG 1 8 2014 Water Oual ty RegWal apentlans Asheville Re ional Office c. Facility name (discharge): d. Facility address: e. Facility contact person: Vacarro MI Last General Manager Title 953 old US Hwy 70 Permit Holder Mailing Address R �� Black Mountain _NC 27711 City State Zip (828) 669-5515 ) Phone Fax Pentair Valves & Controls 953 old US Hwy 70 Address Black Mountain NC 28711 City State Zip Gerald Runkles (828) 669-3753 First / MI / Gast Phone 111. Please provide the following for the requested change (revised permit). a. Request for change is a result of: ❑ Change in ownership of the facility ❑ Name change of the facility or owner If other please explain: Name change for Responsible Person b. Permit issued to (company name): c. Person legally responsible for permit: Jason Stone First Ml Las1 Received AUG 19 2014 Land Quality Section Ashevilie d. Facility name (discharge): e. Facility address: f. Facility contact person: Plant Manacer Title 953 Old US Hwy 70 _ Permit Holder Mailing Address Black Mountain NC 28711 City State Zip (828) 669-5515 Jason.stone@pentair.com Phone E-mail Address Pentair Valves & Controls 953 Old US Hwy 70 Address Black Mountain NC 28711 City State Zip Gerald Runkles First MI Last (828) 669-3753 gerald.runldes@pentair.com Phone E-mail Address Revised 2012Ap23 IN"luk IXAEMfW LI 14 -n (4 UCCOAED I` 4 PNP`D—ES PERMIT N 'OWNERSHIP CHANGE FARM ^ N. Peru eo..nhtxwu�.t inlor_ ion (differatt fi om theperson le�a11Y respsble far the permit) r' , •f Pamlit contact: , a ° - ., aY.. _-- Gaa1d Runkles .e ,s� a n, u, 01 _ •.i u`a•.1� tali S old `953 US � 4f�n ,� err, aA. 0S.11uCwj}�egatCfb B +���0f { „ p' w ���. ,Dye ..-�....•v /y1,.. - n QLrO I hwk ' ' �` -r ° .• " - 'Osr�/i�t��i��rWYlai�l. _ ° 'Nip .ai. a - ZIP1/�� '/ `- . • `'. < - S ' + �'•'�•Y'.4^ '' " , .. 4., , �f"Cit!'� '. �.•. r'1 Y' J•' 14 h'•O,`h0 D� 9.. .p6{59*3753 '' __['11dOEti -"r Jr •'�TrA®i� [1SWiA? r S �•s • u-'�' oilVitl.tbe permitted •facility► coatinue to coipdgct the ta&e indi trial activ es wmductcd�pri r to this own ersWp,or gkkue cha . ,.�. �® `Yes IVb (*ase axplain)a Req iirM'i#er .'MIS APPL,iCA'I'tON'Witt E RETURNED ITIVPRUG'E;;.SED:YF a1TEM5,:. Q� a 4°".,"ay ARE 'INCOWLETi OR IVllSSING:. a - ❑ i'his completed applicati is reg�iired foi liotls name cliangC�and/or own_erstiip r.FgG - -- - T -- Y4.1„ rA. u requests: U •� 0 > `l egal'docuzne.Aiation of the tisnsf a of owiiershlp (guoh as; ielevai t'pages,of ati contradt doer!;` or a bill.of sale).is jeaa�ro•for an ownership ciiaage request .Article$ ofi�acoaporatio� a w 'not s ifficierit for an ownership change r +, ` ;; w ,m :: s�4 J '_ ,w • . .The:ee�rtificationsrbelow must beY ompleted and signed by both the permit solder pnar #o tlte:cliattpe, and° , Y' the new aliplicarit'in the'case bf an ownersh ip o ge request: For a name change r+eq ,iSu .FS ` y�` ' w hail Vest,+the s o3 Applicant's Certification is'§efficient. t d • '; PERMI'ITLE CERTIFICATIUNr(Perr�eit holder prior"ta ownership. change): I; Salvatore Yacitrro, attest diet this.applicatio'n for ai ols leiownership+changehas b6en r�eviewedabil,is accurate'and complete to tlie'liest of my iCnuwledge-"`{I understand that ifall re�yined'pasts oftliis •:` applicationrare not completed and that if all required supporhrig inf'ormat�on is,notitne uded;:itti�s application R Be'will be returner! asJncomplete._., - - J C:� ••f a •]/7l/1���A�`•/1/��rY L.• 3� `5 •`+��9. •r�'Q °'•C O- .. 3- . S1�1Atllfe ', a _ I .* • 4A . LDnti .. _ _^ ' 1- 7 •,��1 , . 1 APPLICANT' CER'IICATION aW ' _J_Nq i Stahe, attest that this`application`for a nanieiowneirshipchange 1ias,treen nvieti o 4nd`is+ acc rate;- 't'. 0 and complete to the best.of my knowledge. 'l-understand that if all required putsaafthis applicahr14 completed' aadEthat'if all t+ege�ir�ed supporting igforr�tion is not included, this,a'pplrcation+pkage ca a. .in-cioinpkta. nrA Vw 5}` ,; •F' n '` �tl �.. ,�'a'`�" .. � r,' b y A .. •1. s, •Y. tl, r'+m . 8 rn ' .,l - A ..c, , o �»c�e,; ' °,+,o•+_ - • " ` I _ I Y - Sign$ti reL1Ate'i.0 • f. . 7 I . � "t + •t . " ` • aA r_ :S . � ,� - t r +�►�rh �'n •� �¢ Yap • aLs� 9. 'F. 1i - ;- SEND{ CKAG PLEASE THEJC4MPLETE ARPLIeAT1-UN PAS, r E Tp R r s a _ Division � Mater Quality t ••1' �,- ar"<.�l,,��a,�=��{�/fhC-Qc�,�,�f�LP�' i_ _ `� :3r '4 .'F- R �� ,�. '' � 'b ✓t,:`-F „� ' 47�' fiIrl G{�W_ �tM+•a7R�li� �J ;•!4 9 Pa , y , jam, `a a r - „, - i-.. A J t* ?] �}•i e' s'-'c� �..,. -/0.w� '�A��ay., . - v- a ... � �z,-•�•1.611:'�RF�n�r�'tWLV�1\vi-[ S"3- ��`•••'�•g�.'. 'L`� ry;' q r i .• •-.. Raleigh Camlfiia:276 -161.7 ��s"yy":e����b ��fyy�� .+ •Jp'= yc- r a1 - e _ ;�r.+� i.�� '-' Jr 4 -' a• - , y ••' F y .4a • ,r s�fYtPW 7TSVIq a - o{� .y J' rJ t}-Y "�.� r°�.`4_- �', �~ 'e ?'a,.. •y�p��y �� Zb�'...'V•.*. ••'.''`�"+ Pat McCrory Governor iNCDE IR North Carolina Department of Environment and Natural Resources August 27, 2014 Pentair Valves and Controls ATTN: Salvatore Vacarro, General Manager 953 Old US Hwy 70 Black Mountain, North Carolina 27711 John E. Skvarla, III Secretary SUBJECT: NPDES Stormwater Permit: Request for Regulatory Relief Pentair Valves and Controls General Permit No: NCG030000; COC No: NCG030529 Buncombe County Dear Mr. Vacarro: In response to your request for regulatory relief received by this office on July 29, 2014, NCDENR-Land Quality Section staff conducted a site inspection on August 12, 2014. The primary goal of this inspection was to evaluate compliance with the conditions of the NCG030000 General Permit, and to discuss any actions that have been or could be taken to identify and limit potential sources of zinc and copper related to process operations. At the time of this inspection the facility was found to be in compliance with permit NCG030529 and no illicit discharges were discovered. Monthly monitoring has been triggered by two consecutive exceedances of the zinc and copper benchmarks in Storm Drain Outfall Nos. 01 and/or 02 at your facility. Please keep in mind that benchmark exceedances are NOT limit violations or violations of permit conditions; however, you are obligated to follow the tiered response actions outlined in your permit. Pentair Valves and Controls (Pentair) has been following the tiered response actions and therefore is in compliance with the permit. As part of tiered response, Pentair initiated housekeeping actions that appear to have addressed potential process exposures (reference July 22, 2014 letter from you). These include: developing a process that prevents chip hoppers from being overfilled; cleaning of hopper frames prior to being taken outside to the Luggers; cleaning and sweeping the area around the Luggers; wet mopping procedures inside the plant; and assessing on -site forklift tires, lubricants and coolants to assure they are not sources of zinc. Based on the aforementioned items, we are granting regulatory relief from Tier II sampling for zinc and copper only. Upon receipt of this letter, Pentair may resume the Division of Energy, Mineral, and Land Resources -- Land Quality Section Asheville Regional Office, 2090 US Highway 70, Swannanoa, North Carolina, 28778-8211 Telephone 828-296-4500 Fax 828-299-7043 One http://Dortal.ncdenr.org/web/ir/iand-guality NorthCaralina An Equal Opportunity 1 Affirmative Action Employer NatimMly Mr. Salvatore Vacarro, Ge. jI Manager August 27, 2014 Page 2 of 2 permit specified semi-annual analytical monitoring for the remainder of the current permit term, Your current permit is set to expire on October 31, 2017. This decision only applies to the zinc and copper benchmarks. A benchmark exceedance of any other parameter listed in your permit will trigger tiered response actions as described in the general permit. You must notify this office in writing, within five business days, if you become aware of any significant source of zinc or copper at your facility that has the potential to be exposed to stormwater. The relief granted in this letter is contingent upon the current industrial practices at Pentair. If industrial practices change and zinc or copper does become a significant stormwater exposure risk then this office reserves the right to withdraw this decision and reinstate the permit specified tiered response or other actions that may be warranted by the new set of circumstances. Please refer to the enclosed Compliance Inspection Report for additional comments, observations, and recommendations made during the inspection. Please retain and append this letter to your Stormwater Pollution Prevention Plan (SPPP) or permit_ If you have any questions or comments concerning this letter, please contact Darlene Kucken or me at (828) 296-4500. Sincerely, XLaurakHerbert, PE Regional Engineer Enclosures: Inspection Report ec: Bethany Georgoulias, RCO w•• 1 Compliance Inspection Report Permit: NCG030529 Effective: 11/01/12 Expiration: 10/31117 Owner: Pentair Valves B Controls SOC: Effective: Expiration: Facility: Pentair Valves $ Controls County: Buncombe 953 Old US Highway 70 Region: Asheville Black Mountain NC 2$711 Contact Person: Gerald Runkles Title: Phone: 828.669-3753 Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Representative(s]: Related Permits: Inspection pate: 08/12/2014 Primary Inspector: Carlene J Kucken Secondary Inspector(s): Certification: Phone: EntryTime: 10:OOAM Exit Time: 12:OOPM Phone: Laura C Herbert Phone: Fred Walker Reason for Inspection: Routine inspection Type: Compliance Evaluation Permit inspection Type: Metal Fabrication Stortowater Discharge COC Facility Status: Compliant ❑ Not Compliant Question Areas: 0 Storm Water (See attachment summary) Page: 1 Permit: NCG030529 Owner - Facility: Pentair Valves & Controls Inspection Date: 08112/2014 Inspection Type : Compliance Evaluation Reason for Visit: Routine Inspection Summary: The facility is clean and well -maintained. A number of housecleaning activities were initiated to source and reduce the copper and zinc levels that initiated the Tier 11 requirements of the permit. Please remove outfall #8 from the site map and provide a reference history in the SPPP. Please continue with plans for painting areas for wet mopping on a regular basis to reduce potential sources of zinc and copper. The facility has plans to install a water reclamation system from the roof; if this system is installed you may apply for a no exposure permit. Based on this site inspection, you are relieved from the Tier II requirments for copper and zinc only. Page: 2 Permit: NCG030529 Owner • Facility: Pentair Valves 8& Controls Inspection Date: 08/1212014 Inspection Type : Compliance Evaluation Reason for Visit: Routine Stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwater Pollution Prevention Plan? e ❑ ❑ ❑ # Does the Plan include a General Location (USGS) map? ® ❑ ❑ ❑ # Does the Plan include a "Narrative Description of Practices"? E ❑ ❑ ❑ # Does the Plan include a detailed site map including outfall locations and drainage areas? ® ❑ ❑ ❑ # Does the Plan include a list of significant spills occurring during the past 3 years? N ❑ ❑ ❑ # Has the facility evaluated feasible alternatives to current practices? ■ ❑ ❑ ❑ # Does the facility provide all necessary secondary containment? 0 ❑ ❑ ❑ # Does the Plan include a BMP summary? 0 ❑ ❑ ❑ # Does the Plan include a Spill Prevention and Response Plan (SPRP)? ® ❑ ❑ Cl # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? 0 ❑ ❑ ❑ # Does the facility provide and document Employee Training? E ❑ ❑ ❑ # Does the Plan include a list of Responsible Party(s)? 0 ❑ ❑ ❑ # Is the Plan reviewed and updated annually? N ❑ ❑ ❑ # Does the Plan include a Stormwater Facility Inspection Program? ® ❑ ❑ ❑ Has the Stormwater Pollution Prevention Plan been implemented? N ❑ ❑ ❑ Comment: Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring semi-annually? ■ ❑ ❑ ❑ Comment: Analytical Monitoring Yes No NA NE Has the facility conducted its Analytical monitoring? 0 ❑ ❑ ❑ # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ ® ❑ Comment: Permit and Outfalls Yes No NA NE # Is a copy of the Permit and the Certificate of Coverage available at the site? E ❑ ❑ ❑ # Were all outfalls observed during the inspection? ■ ❑ ❑ ❑ # If the facility has representative outfall status, is it properly documented by the Division? ❑ ❑ 0 ❑ # Has the facility evaluated all illicit (non stormwater) discharges? ❑ ❑ 0 ❑ Comment: Page: 3 Il. NCDENR Kq C..XL 00%m w. a 9_vw Yam{ A N.%. L wsou iC , Division of Water Quality / Surface Water Protection National Pollutant Discharge Elimination System PERMIT NAME/OWNERSHIP CHANGE FORM N��r63 I. Please enter the permit number for which the change is requested. 05D-cl NPDES Permit (or) Certificate of Coverage N 1 C I S 0 N 1 C G 0 13 10.0 1 0 0 Permit status prior to requested change. a. Permit issued to (company name): Pentair Valves & Controls b. Person legally responsible for permit: Salvatore Vacarro . First MI Lest 'JEIVED General Manager water Resourca - - Title FOR AGENCY U SE ONLY Date Reaet;A Year Month i 953 old US Hwy 70 q U G 1 S 2014 Permit Holder Mailing Address Black Mountain NC 27711 Waist OUaMy Fleglonal 013eraftns City state Zip Asheville Regional Office (828) 669-5515 ( ) Phone Fax +2 c. Facility name (discharge): Pentair Valves & Controls _ d. Facility address: 953 old US Hwy 70^ T - Address Black Mountain NC 28711 City State Zip c. Facility contact person: Gerald Runkles (828) 669-3753 First / MI / Last Phone III. Please provide the following for the requested change (revised permit). a. Request for change is a result of: ❑ Change in ownership of the facility ❑ Name change of the facility or owner If other please explain:. Name change fot: Responsible Person . b. Permit issued to (company name): c. Person legally responsible for permit: Jason Stone First Ml Last Plant Manager - Title 953 Old US j!M 70 Permit Holder Mailing Address Black Mountain NC 28711 d. Facility name (discharge): e. Facility address: f Facility contact person: City State Zip (8281669-5515 Jason.stone@pentair.com Phone E-mail Address Pentair Valves & Controls 953 Old US Hwy 70 Address Black Mountain NC 28711 City State Zip Gerald Runkles First Ml Last (828) 669-3753 gerald.ntnUesAp_entaincom Phone &mail Address Revised 2012ApO Facility: Date: gd Location Address: COC#: C O�OS Contact Name: (2, if Phone #: Contact Mailing Address: County: `�Ll- Directions: Routine Compliance Inspection Rescission Request Complaint Investigation Other - Explain: A Storm Water Pollution Prevention Plan Yes No N/A Comments 1 Is a copy of the permit and the Certificate of Coverage available at the site? dQ O reNrouc D� »o exs��Se a 'ate. S 2 Ps a copy of the signed and certified SWPPP at the facility? 2.7 3 Does the Plan include a "Narrative Description of Practices"? 4 Does the plan include a general location (USGS) map? S Does the plan include a detailed site map including outfall locations and drainage areas? 6 Does the plan include a Spill Prevention and Response Plan? SPRP ✓ 7 Does the plan include a Preventative Maintenance and Good Housekeeping Plan? 8 Does the plan include a Stormwater Facility Inspection Program? 9 Does the Plan include a BMP Summary? 10 Does the plan include a list of Responsible Party(s)? 11 Has the SWPPP been implemented? B Monitoring and Records Yes No N/A 1 Does the plan include a list of significant spills occurring during the past 3 ears? 2 Does the facility provide and document employee training? 3 Has the facility conducted its Qualitative Monitoring? (semi- annual) 4 Has the facility conducted its Analytical Monitoring? (s-a) S Is the facility meeting all permit specified benchmark goals? 6 Is the facility following the tiered response? 7 Has the facility conducted its Analytical Monitoring from vehicle Maintenance areas? C iWaste Management Yes No N/A 1 Does the facility provide all necessary secondary containment? 2 Are current BM Ps in material storage areas adequate? 3 Are appropriate spill containment and cleanup materials kept on - site and in convenient locations? D Outfalls Yes,No N/A 1 Were all outfalls observed during the inspection? 2 If the facility has representative outfall status, is it properly documented by the Division? 3 Has the facility evaluated all illicit (non stormwater) discharges? VT E Sector specific questions Yes I No N/A 1 Have zinc or copper benchmarks been exceeded in the past 3 sampling periods? 2 Have potential sources for copper and zinc been evaluated at your facility? 3 4 5 `s Comments Ln C,, ') C) ter s.ti, o c �-�-- .7�4 104r,24, . Facility: P.r /- / Ca r (lay o -5 Date: 8 12 Za/ Location Address: 51 Rd, Ln��� fAIK COC#: 4 Contact Name: d &r y _ E Phone 4: Contact Mailing Address: j1gr47jt-, eo ?8 // County: Directions: ( 0 ttK/ Routine Compliance Inspection Rescission Request Complaint Investigation Other. Explain: &"Afte"e— A Storm Water Pollution Prevention Plan Yes No N/A Comments is a copy of the permit and the Certificate of Coverage available ,Ka/� fYu/ydcr�c It�iv� 1 at the site? ► 2-1WS / �✓wr�/ , „�, 61 2 1 Is a copy of the signed and certified SWPPP at the facility? 3 Does the Plan include a "Narrative Description of Practices"? Sru-lam .yrlHro . 4 Does the plan include a general location (USGS) map? S Does the plan include a detailed site map including outfall locations and drainage areas?��"� �L�U / 6 Does the plan include a Spill Prevention and Response Plan? I(SPRP) ✓ 7 Does the plan include a Preventative Maintenance and Good Housekeeping Plan? 8 Does the plan include a Stormwater Facility Inspection Program? �1.sScraa� 9 IDoes the Plan include a BMP Summary? ✓ J ✓ 10 Does the plan include a list of Responsible Party(s)? 5�{,�,��t�al� 11 Has the SWPPP been implemented? ✓ B Monitoring and Records Yes No N/A Does the plan include a list of significant spills occurring during 1 the past 3 ears? Sf.,,�c,l,� cow/ fV l" 2 Does the facility provide and document employee training? ✓ �rnns, , 3 Has the facility conducted its Qualitative Monitoring? (semi- ✓ annual) 4 Has the facility conducted its Analytical Monitoring? (s-a) S Is the facility meeting all permit specified benchmark goals? 6 Is the facility following the tiered response? 7 Has the facility conducted its Analytical Monitoring from vehicle Maintenance areas? C Waste Management Yes No N/A 1 Does the facility provide all necessary secondary containment? / 2 Are current BMPs in material storage areas adequate? 3 Are appropriate spill containment and cleanup materials kept on - site and in convenient locations? D Outfalls Yes No N/A 1 Were all outfalls observed during the inspection? 2 if the facility has representative outfall status, is it properly documented by the Division? 3 Has the facility evaluated all illicit (non stormwater) discharges? E Sector specific questions Yes No N/A 1 Have zinc or copper benchmarks been exceeded in the past 3 ✓ sampling periods? 2 Have potential sources for copper and zinc been evaluated at your facility? 3 4 5 Comments 9 krof- 6,-ese • Alp p.M ,t <<- Iy,AntAcf4� G 1 - 5, 2�'- , I c"4r Ae r fr �c l•-`4. c�tscr.�-xsr� ,,� � os�..sc/ .dos .�.- ac 3,. 0 513 b A-Y-d R1 4AWls44� 1,1,1 A4e- hrlo�) , S"G, Goo /hs !'o/,f, /a /27to —� Fm r irf - ry Ah.cr �7nrs. SrytYrQ. G 14 r fs Md OW $2�- Pickle, Ken From: Herbert, Laura C Sent: Tuesday, June 17, 2014 11:24 AM To: gerald.runkles@pentair.com Cc: Kucken, Darlene; Georgoulias, Bethany; Pickle, Ken Subject: Pentair Valves and Controls Buncombe County NCG030529 Gerald, Thank you for your time during our telephone call today. As we discussed we have been receiving your monthly sampling results of your outfalls as required by the Tier II requirements of your permit. This Tier II response was necessitated by exceedances of the zinc and copper benchmarks for two consecutive semiannual sampling episodes. Thank you for the monitoring reports. To initiate a review for regulatory relief from the Tiered response, we will need a request from you that summarizes the results, what actions you have taken in the tiered response, and an inventory/process review for zinc and copper exposures generated as part of the process. Any information concerning background levels of zinc, copper or non -process sources will also be helpful. Once we receive this, we will schedule an inspection as part of our review of the request. Let me know if you have any questions or need more information. We look forward to working with Pentair and appreciate all efforts that you all have made to address these process exposures. Thanks, Laura Laura Herbert, P.E. Regional Engineer Division of Energy, Mineral, and Land Resources - Land Quality Section. NCDENR-Asheville Regional Office 2090 US Highway 70 Swannanoa, NC 28778 Tel:828-296-4500 Fax:828-299-7043 http://Portal.ncdenr.org/web/Ir Notice: E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and therefore may be disclosed to third parties unless the content is exempt by statute or other regulation. Herbert, Laura C From: Herbert, Laura C Sent: Tuesday, June 17, 2014 1114 AM To: 'gerald.runkles@pentair.com` Cc: Kucken, Darlene; Georgoulias, Bethany; Pickle, Ken Subject: Pentair Valves and Controls Buncombe County NCG030529 Gerald, Thank you for your time during our telephone call today. As we discussed we have been receiving your monthly sampling results of your outfalls as required by the Tier II requirements of your permit. This Tier 11 response was necessitated by exceedances of the zinc and copper benchmarks for two consecutive semiannual sampling episodes. Thank you for the monitoring reports. To initiate a review for regulatory relief from the Tiered response, we will need a request from you that summarizes the results, what actions you have taken in the tiered response, and an inventory/process review for zinc and copper exposures generated as part of the process. Any information concerning background levels of zinc, copper or non -process sources will also be helpful. Once we receive this, we will schedule an inspection as part of our review of the request. Let me know if you have any questions or need more information. We look forward to working with Pentair and appreciate all efforts that you all have made to address these process exposures. Thanks, La ura Laura Herbert, P.E. Regional Engineer Division of Energy, Mineral, and Land Resources - Land Quality Section NCDENR-Asheville Regional Office 2090 US Highway 70 5wannanoa, NC 28778 Tel:828-296-4500 Fax:828-299-7043 http://porta 1. ncden r.org/web/Ir Notice: E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and therefore may be disclosed to third parties unless the content is exempt by statute or other regulation. NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Pat McCrory Thomas A. Reeder John E. Skvarla, III Governor Acting director Secretary July 16, 2013 Pentair Valves & Controls Attn: Gene Logan 953 Old U.S. Hwy 70 Black Mountain, NC 28711 SUBJECT: NPDES Stormwater Permit Compliance Inspection Pentair Permit No: NCG030529 Buncombe County Dear Mr. Logan: This letter is in follow-up to the NPDES Stormwater Permit Compliance Inspection conducted on June 12, 2013. The facility was found not to be in compliance with permit NCG030529 due to analytical benchmark limits. Enclosed is a copy of the Compliance Inspection Report, which contains additional observations and comments for your reference. Please contact me at (828) 296-4664 or Tilxl.Fax�am nedenr.gov, if I can be of any further assistance. Sincerely, Tim Fox Environmental Specialist Surface Water Protection Enclosure cc: Central Files Asheville Files S:1SWP15-NonpointSourceXStormwaterllndustriailCompiiance\CEl_Tim 5 2012_doc Location: 2090 U.S. Highway 70, Swannanoa. North Carolina 28778 Phone: 828.296.45001 FAX: 828-299.7043 tntemet: www.Acwaterquality.org An Equal Opportunity l Affirmative Action Employer Nne orthCarolina Natuidll_� 1 Compliance Inspection Report Permit: NCG030529 Effective: 11/01/12 Expiration: 10/31/17 Owner: Tyco Valves $ Controls SOC: Effective: Expiration: Facility: Tyco Valves and Controls County: Buncombe 953 Old US Highway 70 Region: Asheville Black Mountain INC. 28711 Contact Person: Gene Logan Title: Phone: 828-669-3753 Directions to Facility: System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): On -Site Representative(s): Related Permits: Inspection Date: 06/12/2013 Entry Time: 10:00 AM Exit Time: 11:30 AM Primary Inspector: Timothy R Fox Phone: 828-296-4500 Secondary Inspector(s): Jonathan Stepp Phone: Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Metal Fabrication Stormwater Discharge COC Facility Status: Ll Compliant N Not Compliant Question Areas: N Storm Water (See attachment summary) Page: 1 Permit: NCG030529 Owner - facility: Tyco Valves & Controls Inspection Date: 06112/2013 Inspection Type: Compliance Evaluation Reason for Visit: Routine Inspection Summary: Tim Fox and Jonathan Stepp with The Division of Water Quality, Asheville Regional Office, met with Gene Logan (EHS Supervisor) and Gerald Runkles (EHS Manager) with Pentair Valves & Controls_ Record Keeping was in order and provided during the inspection. Outfall #3 has been eliminated due to no exposure. There are two remaining outfalls at the facility. Analytical data benchmarks have been exceeded. The facility has intiated a Tier One response and evaluated possible causes of the benchmark exceedance. We suggested to continue efforts to identify and implement improvements at the facility. Conditions and analytical data will need to be re-evaluated after the next sampling period results. Page: 2 Permit: NCGO30529 Owner - Facility: Tyco Valves R Controls Inspection Date: 06/12/2013 Inspection Type: Compliance Evaluation Reason for Visit: Routine Stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwater Pollution Prevention Plan? ■ n n n # Does the Plan include a General Location (USGS) map? ■ 0 0 0 # Does the Plan include a "Narrative Description of Practices"? ■ 0 0 n # Does the Plan include a detailed site map including outfall locations and drainage areas? ■ 0 0 0 # Does the Plan include a list of significant spills occurring during the past 3 years? ■ Q n ❑ # Has the facility evaluated feasible alternatives to current practices? ■ Q 0 U # Does the facility provide all necessary secondary containment? ■ D D 0 # Does the Plan include a BMP summary? ■ ❑ 0 0 # Does the Plan include a Spill Prevention and Response Plan (SPRP)? ■ ❑ 0 n # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? ■ Q 0 0 # Does the facility provide and document Employee Training? ■ ❑ D 0 # Does the Plan include a list of Responsible Party(s)? ■ ❑ 0 ❑ # Is the Plan reviewed and updated annually? ■ D Q n W Does the Plan include a Stormwater Facility Inspection Program? ■ 0 n n Has the Stormwater Pollution Prevention Plan been implemented? ■ 11 11 0 Comment: Record Keeping was in good order during the inspecion process. Qualitative Monitoring Has the facility conducted its Qualitative Monitoring semi-annually? Comment: Analytical Monitoring Has the facility conducted its Analytical monitoring? # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? Comment: Analytical benchmark valves were exceeded. Permit and Outfalls # Is a copy of the Permit and the Certificate of Coverage available at the site? # Were all outfalls observed during the inspection? # If the facility has representative outfall status, is it properly documented by the Division? # Has the facility evaluated all illicit (non Stormwater) discharges? Comment: Outfall #3 has been eliminated. There are two olltfalls at the facility. Yes No NA NE ■ p 0 0 Yes No NA NE ■Q❑Q U Q 0 0 Yes No NA NE Page: 3 0 4- 0 O O d 7-7 Environmental Testing Solutions, Inc. Certificate of Analysis Project name: Tyco Valves & Controls Collection date: 17-Apr_ 13 Date received: 17-Apr-13 Sample identification: Outfall #1 e PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 130417.521 Sample number: 104985 Parameter Method Result RL Units Date Analyst Footnotes Analyzed 624 624 See Attached Sheet pg/L 29-Apr-13 VHL 1,2 625 625 See Attached Sheet Pg/L 23-Apr-13 KC I Solids, Total Suspended SM 9222-D <5.0 5.0 mg/L 18-ApU-13 1 MHF Oil & Grease 1664 A t5.0 5.0 mg/L 30-Ap�13 JAB I Copper 200.7 <0.010 0,010 mg/L 2&Apr43 BGM I Zinc 200.7 ' 0.15 0.030 mglL 26-Apr-13 BGM 1 Lead 200.7 <0.0050 0.0050 mg/L 23-Apr-13 BGM 1 Sample identification. Outfall #2 Sample number: 104986 Parameter Method Result RL Units Date Analyst Footnotes Analyzed 624 624 See Attached Sheet µg/L 29-Apr.-13 VHL 1,2 625 625 See Attached sheet µg/L 23-Apr-13 KC 1 Solids, Total Suspended SM 9222-D 6.0 5.0 mg/L I8-Apr-13 MHF Oil & Grease 1664 A <5.0 5.0 mg/L 30-Apr-13 JAB Copper 200.7 0.18 0.010 mg/L 26-Apr-13 BGM Zinc 2003 0.18. 0.030 mg1L 26-Apr-13 BGM I Lead 200.7 0.025 0.0050 m 23-Apr43 BGM I ik7 U L'1 T MAY 10 2013 Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. 1. Sample analyzed by Prism Laboratories, Inc, 2. Samples received with headspace. Date reviewed: NC Certification Number: 600 Data reviewed by: Kelley E. Keenan SC Certification Number. 99053 Signature: NC Drinking Water Certification Number: 37786 This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing 501utions, Inc The results in this report relate only to the samples submitted for analysis. IPRyISM �/ tWC Full -Service Analytical $ Environmental Solutions Environmental Testing Solutions Kelley Keenan PO Box 7565 Asheville, NC 28802 e NC Certification No. 402 Sr_ Certification No. 99012 NC Drinking Water Cert No. 37735 VA Certification No. 460211 DoD FLAP Certification No_ L2307 Project: (Tyco) Pentair Valves & Controls Lab Submittal Date: 04/19/2013 Prism Work Order: 3040546 Case Narrative 05/10/2013 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this Case narrative. Narrative Notes: This is a Revised Report and supercedes the original laboratory report dated 5/1113. Additional metals added to both samples at the client's request. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Peggy F. Kendall Project Manager Data Qualifiers Key Reference: �N � Reviewed By Terri W. Cole For Peggy F- Kendall Project Manager 1 Samples for volatiles analysis received with headspaee A ICV % recovery outside of QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MOIL and reporting limit indicated with a J. This report should not be reproduced, except In its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0643 Phone: 7041529.6364 - Toll Free Number. 1-8001529-6364 - Fax: 704162h-0409 Qbhf l2jp931 P,R i S M I EnvF.11-Service Analytical 8 Environmental Solutions �f�ggp{ArgpE51NC *Sample Receipt Summary 05/10/2013 Prism Work Order: 3040546 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received Outfall #1 3040546-01 Water 04/17/13 04/19/13 Outfall #2 3040546-02 Water 04/17/13 04/19/13 Samples received in good condition at 3.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.OS43 Phone: 7041529-6364 - Toll Free Number. 1-0001529-6364 - Fax: 70416264409 Obhf �3lp�31 ,n R I S A � I Full -Santee Analytical r � V' Environmeatat Solutions �ueon�Towr k'w Environmental Testing Solutions Attn: Kelley Keenan PO Box 7565 Asheville, NC 28802 Project: (Tyco) Pentair Valves & Controls Sample Matrix: Water Laboratory Report 05/1012013 Client Sample ID: Outfall #1 Prism Sample ID: 3040546-01 Prism Work Order: 3040546 Time Collected: 04/17/13 14:15 Time Submitted: 04/19/13 11:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters Oil & Grease (HEM) BRL mg1L 6.0 1.4 1 '1864A 4130113 9:05 JAB P3D0626 Senlivolatile Organic Compounds by GCIMS 1,2,4-Trichkxobenzene BRL ug/L 10 1,6 1 '625 4123113 13-26 KC P3D0448 1,2-0ichlonAxnzene BRL ug/L 10 1.8 1 1625 4123113 13:26 KC P300448 1,3-Dichlorobenzene BRL ug1L 10 1.8 1 '625 4/23113 13:26 KC P3Do448 1,4-Dichlorobenzene BRL ug/L 10 1.8 1 '625 4/23/13 13:26 KC P3DD448 I-Methyinaphthalene BRL ug/L 10 1.7 1 '625 4/23113 13:20 KC P3D0448 2,4,6-Trichlorophenol BRL ug/L 10 2.0 1 'fi25 4123113 13:26 KC P3130448 2,4-Dichlorophenol BRL ug1L 10 1.8 1 '625 4123/13 13:26 KC P3D0448 2.4-Dimethylphenol BRL ug/L 10 1.6 1 '625 4/23/13 13:26 KC P3D0448 2.4-Dinitrophenol BRLA ug1L 10 5.8 1 '625 4123113 13:26 KC P31004413 2,4-Dinitrotoluene BRL ug/L 10 2.8 1 '625 4123113 13:26 KC P3130448 2,6-Dinitrotoluene BRL ug/L 10 2.2 1 '625 4123113 13:26 KC P3DD448 2-Chloronaphthalene BRL ug/L 10 2.0 1 '625 4123113 13:26 KC P3D()448 2-Chlorophenol BRL ug/L 10 1.8 1 '625 4123113 13:26 KC P300448 2-Methyinaphthalene BRL ug/L 10 2.0 1 '625 4123113 13:26 KC P3DD448 2-Nitrophenol BRL u91L 10 1.5 1 '625 4/23113 13:26 KC P3100448 31-0010robenzidine BRL ug/L 10 2.9 1 '625 4/23113 13:26 KC P3D0448 4,6-Dinitro-2-methytphenol BRL ug1L 10 5.4 1 '625 4/23113 13:26 KC P3D0448 4-Bromophenyl phenyl ether BRL ug/L 10 1.9 1 '625 4123113 13:26 KC P3DD448 4-Chloro-3-methylphenol BRL ug/L 10 1.7 1 '625 4/23/13 13:26 KC P300448 4-Chlorophenyl phenyl ether BRL ug/L 10 1.6 1 '625 4123113 13:26 KC P3D0448 4.Nitrophenol BRL ug/L 50 1.1 1 '625 4123113 13:26 KC P300445 Acenaphthene BRL ug1L 10 1.8 1 *625 4123113 13:26 KC P3DD448 Acenephthylene BRL u91L 10 1.8 1 '625 4123113 13:26 KC P3130448 Anthracene BRL ug1L to 2.6 1 '625 4/23113 13:26 KC P3D0448 Benzidine BRLA ugll- 100 11 1 '625 4123/13 13:26 KC P3DD448 Benzo(a)anthracene BRL ug/L 10 2.0 1 *625 4123/13 13:26 KC P3D0448 Benzo(a)pyrene BRL ug/L 10 2.2 1 '625 4/23113 13:26 KC P3D0448 Benzo(b)fluoranthene BRL ug/L 10 1.7 1 '625 4/23113 13:26 KC P3D0446 Benzo(g,h,i)perylene BRL ug1L 10 3.2 t '625 4123113 13:26 KC P3DD446 Benzo(k)fluoranthene BRL ug/L 10 2.3 1 '625 4123113 13:26 KC P3DD448 bis(2-Chloroethoxy)methane BRL ug/L 10 2.0 1 *625 4123113 13:26 KC P3D044B Sis(2-Chloroethyl)ether BRL ugA- 10 1.7 1 '825 4123113 13:26 KC P3DD448 Bis(2-chloroisopropyl)ether BRL ug/L 10 1.6 1 '625 4123/13 13:26 KC P300448 Bi9(2-Ethylhexyl)phthalate BRL ug/L 10 3.2 1 '625 4/23113 13:26 KC P3D0448 Butyl benzyl phthalate BRL ug/L 10 2_D 1 '625 4/23/13 13:26 KC P3Do448 Chrysene BRL uglL t0 2.2 1 '625 4123l13 13:26 KC P300448 Dibenzo(a,h)anthmcene BRL ug1L 10 3.2 1 '625 4123113 13:26 KC P3Da448 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240843 - Charlotte, NC 28224-0643 Phone: 704162"364 - Toll Free Number. 1.8001529-6364 - Fax: 7041526.0409 Cbhf !4!p 31 0 0 Laboratory Report QP R I S Ni Full-SBlVIO9 Analytical d Environmental Solutions 175/1012013 Environmental Testing Solutions Project: (Tyco) Pentair Valves 8 Client Sample ID: Outfall #1 Attn. Kelley Keenan Controls Prism Sample ID: 3040546-01 PO Box 7565 Prism Work Order: 3040546 Asheville, NC 28802 Sample Matrix- Water Time Collected: 04117/13 14:15 Time Submitted: 04/19/13 11:45 Parameter Result units Report MDL Dilution Method Analysis Analyst Batch limit Factor DatelDmer ID Diethyl phthalate BRL ug/L 10 2.1 1 '625 4123113 13:26 KC P3D0448 Dimethyl phthalate BRL ug1L 10 2.9 1 •625 4123113 13:26 KC P300448 Di-n-butyl phthalate BRL u91L 10 2.5 1 '625 4/23113 13:26 KC P3D0448 Di-n-octyl phthalate BRL ug1L 10 3.2 1 '625 4123113 13:26 KC P3DD448 Fluoranthene BRL ug/L 10 2.5 1 '625 4/23113 13:26 KC P300448 Fluorene BRL ug1L 10 1.7 1 '625 4123M3 13:26 KC P3D0448 Hexachforobenzene BRL ug/L 10 2.4 1 1625 4/23113 13:26 KC P3D0448 Hexachlorobutadiene BRL ug/L 10 1.8 1 '625 4123/13 13:26 KC P31310448 Hexachlorocyclopentadiene BRLA ug/L 10 2.0 1 '625 4/23/13 13:26 KC P3D0448 Hexachloroethane BRL ug/L 10 1.8 1 '625 4123113 13:26 KC P3DQ448 Indeno(1,2,3-cd)pyrene BRL ug/L 10 2.8 1 1625 4123113 13:26 KC P3D0448 Isophorone BRL ug/L 10 2.0 1 "625 4123113 13:26 KC P3D0448 Naphthalene BRL ug/L 10 1.7 1 '625 4/23113 13:26 KC P3D0446 Nitrobenzene BRL ug/L 1D 1.9 1 `625 4123113 13:26 KC PBD0448 N-Nitrosodimethylamine BRL ug/L 10 1.1 1 "625 4123113 13:26 KC P31DD448 N-Nitros"l-n-propylamine BRL ug/L 10 2.8 1 '625 4123/13 13:26 KC P3DD448 N-Nitrosodiphenyiamine BRL ug/L 10 1.9 1 '625 4123113 13:26 KC P3130448 Pentachlorophetioi BRL ug/L 10 2.7 1 '625 4123113 13:26 KC P3130448 Phenanthrene BRL ug/L 10 2.0 1 '625 4/23113 13:26 KC P3DD448 Phenol BRL ug1L 10 0.48 1 `625 4/23113 13:26 KC P3D0446 Pyrene BRL ugfL 10 1.4 1 '625 4123013 13:26 KC P3D0446 Surrogate Recovery Control Limits 2,4,&Tribromaphenol 92 % 31.144 2-Fluarobiphenyl 96 % 49-118 2-Fluorophenol 53 % 22-64 Nitrobenzene-d5 64 % 43-123 Phenol-d5 36 % 10-63 Terphenyl-d14 104 % 49-151 Total Metals Copper BRL mglL 0,010 0.00060 1 '200.7 4123113 20:02 BGM P3D0475 Lead BRL mg/L 0.0050 0.00068 1 '200.7 4123113 20:02 BGM P3D0475 Zinc 0.16 mgfL 0.030 D.0050 1 '200.7 4123113 20:02 BGM P31010476 Volatile organic Compounds by GCIMS 1 1,11-Trichloroethane BRL ug/L 5.0 0.12 1 '624 4/20/13 14:04 VHL P3D0555 1,1,2,2-Tetrachloroethane BRL ug/L 5-0 0.10 1 '624 4/29113 14:04 VHL P3D0555 1,1,2•Tdchloroethane BRL ug/L 5.0 0.085 1 "624 4129/13 14:04 VHL P3D0555 1,1-Dichloroethane BRL ug/L 5-0 0A1 1 '624 4129113 14:04 VHL P3D0555 1,1-Dichloroethylene BRL ug/L 5-0 0.094 1 '624 4129113 14:04 VHL P3D0555 1,2-Dichlorobenzene SRL ug/L 5.0 0,099 1 '624 4129113 14:04 VHL P3D0555 1,2-Dichloroethane BRL ug/L 5.0 0,063 1 '624 4129/13 14:04 VHL P3D0555 1,2-Dicmaropropane BRL ug/L 5.0 0.12 1 '624 4/29113 14:04 VHL P300555 This report should not be reproduced, except in its entirety, without the written consent at Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number. 1-800/529-6364 - Fax: 7041526-0409 abhf NP931 P R! S M Fun -Service al Solutions s Environmental SoEutions Laboratory Report 05/10/2013 Environmental Testing Solutions Attn: Kelley Keenan PO Box 7565 Asheville, NC 28802 Project: (Tyco) Pentair Valves & Controls Sample Matrix: Water Client Sample ID: Outfall #1 Prism Sample ID: 3040546-01 Prism Work Order: 3040546 Time Collected: 04/17/13 14:15 Time Submitted: 04/19/13 11:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,3-Dichlorobenzene BRL uglL 5.0 0.11 1 *624 4129113 14:04 VHL P3D0555 1,4-Dichlorobenzene BRL uglL 5.0 0.11 1 *624 4/29113 14:04 VHL P3005$5 2-Chloroethyl Vinyl Ether BRL ug1L 10 0,44 1 *624 4/29113 14:04 VHL P3D0555 Acrolein BRL ug1L 100 0.86 1 *624 4129113 14:04 VHL P3D0555 Acrylonitrile BRL ug1L 100 0,73 1 *624 4129/13 14:04 VHL P3D0555 Benzene BRL ug1L 5.0 0.066 1 *624 4/29/13 14:04 VHL P300555 Bromodichloromethane BRL ug1L 5.0 0.082 1 1624 4129/13 14:04 VHL P3D0555 Bromoform BRL uglL 5.0 0.15 1 `624 4129113 14:04 VHL P3130555 Bromomethane BRL uglL 10 0.19 1 *624 4/29/13 14:04 VHL P3130555 Carbon Tetrachloride BRL ug1L 5,0 0.086 1 *624 4/29113 14:D4 VHL P3D0555 Chlorobenzene BRL ug1L 5.0 0.098 1 *624 4129/13 14:04 VHL P3130555 Chloroethane BRL ug1L 10 0.26 1 *624 4129/13 14:04 VHL P3D0555 Chloroform BRL ugll- 5.0 0.059 1 *624 4/29113 14:04 VHL P3D0555 Chloromethane BRL ug1L 10 0.18 1 *624 4129113 14:04 VHL P300556 cis-1,3-Dichloropropylene BRL ug1L 5.0 0.20 1 '624 412g113 14:04 VHL P3D0555 Dibromochloromethane BRL uglL 5.0 0.087 1 *624 4129113 14:04 VHL P3130555 Ethylbenzene BRL ug1L 5.0 0.12 1 '624 4/29113 14:04 VHL P3Do555 Methylene Chloride BRL ug1L 5.0 0.069 1 "624 4/29113 14704 VHL P3D0555 Tetrachloroethylene BRL ug1L 5.0 0.14 1 *624 4/29/13 14:04 VHL P3130555 Toluene BRL ug1L 5.0 0.088 1 *624 4/29/13 14:D4 VHL P3130555 Vans-1,2-Dichloroethylene BRL uglL 5.0 0.093 1 *624 4129/13 14:04 VHL P3D4555 trans- 1, 3-Dichloropropylene BRL ug/L 5.0 0.065 • 1 *624 4129113 14:04 VHL P3D0555 Trichloroethylene BRL ug1L 5.0 0.15 1 *624 4129113 14:04 VHL P3D0555 Trichlorofluoromethane BRL uglL 10 0.018 1 *624 4/29113 14:04 VHL P3D0555 Vinyl chloride BRL ug1L 10 0.51 1 *624 4/29113 14:04 VHL P3130555 Surrogate Recovery Control Limits 4-Bromofluorobenzene 100 % 74-126 Dibromofluoromethane 122 % 75-127 Toluene -dB 107 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Sox 240643 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number. 1-800/629-6364 - Fax: 704I626-0409 Qbhf !61pd31 PRISM I Full -ea Analytical & EnNro-onmnmontel Solutions ✓�n8o,1wS0(aEy IMC Environmental Testing Solutions Attn: Kelley Keenan PO Box 7565 Asheville, NC 28802 e Laboratory Report 0511012013 Project: (Tyco) Pentair Valves & Client Sample ID: Outfall #2 Controls Prism Sample ID: 3040546-02 Prism Work Order: 3040546 Sample Matrix: Water Time Collected: 04/17/13 14:30 Time Submitted: 04/19/13 11:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datelrime ID General Chemistry Parameters Oil & Grease (HEM) BRL mg1L 5.0 1.4 1 '1664A 4130/13 9:50 JAB P3D0626 Semivolatile Organic Compounds by GUMS 1,2,4-Trichlorobenzene BRL uglL 10 1.8 1 '625 4/23113 14:05 KC P300448 1,2-Dictlorobenzene BRL uglL 10 1.8 1 '625 4123113 14:05 KC P3D0448 1,3-Dichiorobenzene BRL uglL 10 1.8 1 `625 4/23113 14:05 KC P3D0448 1,4-Dichlorobenzene BRL uglL 10 1.8 1 '625 4/23113 14:05 KC P3DD448 1-lethylnaphthalene BRL ug1L 10 1.7 1 '625 4123l13 14:05 KC P31310448 2,4,6-Trichlorophenol BRL ug1L 10 2.0 1 '625 4/23113 14:05 KC P3D0448 2,4-Dichlorophenol BRL uglL 10 1.8 1 '625 4123/13 14:05 KC P3D0448 2,4-Dimethylphenol BRL ug1L 10 1.6 1 '625 4123113 14:05 KC P3D0448 2,4-Dinitrophenol BRLA uglL 10 5.8 1 '625 4/23113 14:05 KC P3D0448 2,4-Dinitrotoluene BRL ug/L 10 2.6 1 '625 4/23113 14:05 KC P3D0448 2,6-Dinitrotoluene BRL ug1L 10 2.2 1 '625 4/23/13 14:05 KC P3D0448 2-Chloronaphthalene BRL ug1L 10 2.0 1 '625 4123113 14:05 KC P3130448 2-Chlorophenol BRL uglL 10 1.8 1 '625 4123/13 14:05 KC P3D0448 2-Methylnaphthalene BRL uglL 10 2.0 1 `825 4/23113 14:05 KC P300448 2-Nitrophenol BRL ug1L 10 1.$ 1 1625 4123113 14:05 KC P3130448 3,3'-Dichlorobenzidine BRL uglL 10 2.9 1 '625 4/23/13 14:05 KC P3DD446 4,6-Dinitro-2-methylphenol BRL uglL 10 5.4 1 '625 4123113 14:05 KC P300448 4-Bromophenyl phenyl ether BRL ug/L 10 1.9 1 'fi25 4123/13 14:05 KC P3D0446 4-Chloro-3-methylphenol BRL ug/L 10 1.7 1 '625 4123/13 14:05 KC P31)0448 4-Chlarophenyl phenyl, ether BRL uglL 10 1.6 1 '625 4123113 14:05 KC P300448 4-Nitrophenol BRL uglL 50 1.1 1 "625 4123113 14:05 KC P3D0448 Acenaphthene BRL uglL 10 1.8 1 '625 4/23113 14:05 KC P31DD448 Acenaphthylene BRL ug1L 10 1.8 1 `625 4/23/13 14:05 KC P3DD448 Anthracene BRL ug1L 10 2.6 1 '625 4123/13 14:05 KC P3DD448 Benzidine BRLA ug1L 100 11 1 '625 4123/13 14:05 KC P3D0448 Benzo(a)anthracene BRL uglL 10 2.0 1 '625 4/23/13 14:05 KC P3DD448 Benzo(a)pyrene BRL uglL 10 2.2 1 '625 4123/13 14:05 KC P3DD448 Benzo(b)fluoranthene BRL ug1L 10 1.7 1 '625 4/23113 14:05 KC P3D044B Benzo(g,h,i)perylene BRL uglL 10 3.2 1 '625 4/23/13 14:05 KC P3DD448 Benzo(k)fluoranthene BRL ug1L 10 2.3 1 '625 4123113 14:05 KC P3D0448 bis(2-Chloroethoxy)methane BRL ug1L 10 2.0 1 '625 4123/13 14:05 KC P300448 Bis(2-Chloroethyl)ether BRL ug1L 10 1.7 1 '625 4123113 14:05 KC P3D0448 Bis(2-chloroisopropyl)ether BRL uglL 10 1.6 1 '625. 4/23113 14:05 KC P3D0448 Bis(2-Ethylhexyl)phthalate BRL ug1L 10 3.2 1 '625 4/23113 14:05 KC P3DD448 Butyl benzyl phthalate BRL ug1L 10 2.0 t '625 4/23113 14:05 KC P3D0448 Chrysene BRL ug1L 10 2.2 1 '625 4123/13 14:05 KC P3DD448 Dibenzo(a,h)anthracene BRL ug1L 10 3.2 1 '625 4123/13 14105 KC P3DD448 Diethyl phthalate BRL ug1L 10 2.1 1 '625 4123113 14:05 KC P3130448 This report should not be reproduced, except in its entirety, without the written consent or Prism Laboratories, Inc. 449 5pringbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 -Top Free Number. 1-8001629-6364 - Fax: 70V62"409 Cbhf 17!p�31 0 Laboratory Report 0511012013 0 �P.R I S M .-'r/y..Apnwrpa Analytical 8 I Environmental Environmontpl Solutions Environmental Testing Solutions Attn: Kelley Keenan PO Box 7565 Asheville, NC 28802 Project: (Tyco) Pentair Valves & Controls Sample Matrix: Water Client Sample ID: Outfall #2 Prism Sample ID: 304OW-02 Prism Work Order: 3040546 Time Collected: 04/17/13 14:30 Time Submitted: 04/19/13 11:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datelrime ID Dimethyl phthalate BRL ug/L 10 2.9 1 '625 4123113 14:05 KC P3D0448 Di-n-butyl phthalate BRL ug/L 10 2.5 1 '625 4123143 14:05 KC P3D044B Di-n-octyl phthalate BRL ug/L t0 3.2 1 `625 4123/13 14:05 KC P3D0448 Fiuoranthene BRL ug1L 11) 2.5 1 "625 4/23113 14:05 KC P3DG448 Fluorene BRL ug1L 10 1.7 1 "625 4/23113 14:05 KC P3DD448 Hexachloroberszene BRL ug/L 10 2.4 1 '625 4123113 14:05 KC P31)0448 Hexachlarobutadiene BRL ug/L 10 1.8 1 '625 4123113 14:05 KC P3D0446 Hexachlorocydopentadiene BRLp ug/L 10 2.0 1 '625 4123113 14:05 KC P3DD448 Hexachloroethene BRL ug/L 10 1.6 1 '625 4/23A3 14:05 KC P3130448 Indeno(1,2,3-cd)pyrene BRL ug& 10 2.8 1 '625 4123113 14:05 KC P3D0448 Isophorone BRL ug1L 10 2.0 1 '625 4123113 14:05 KC P3DD448 Naphthalene BRL u911. 10 1.7 1 '625 4/23113 14:05 KC P3DG448 Nitrobenzene BRL uglL 10 1.9 1 '625 4123113 14:05 KC P3D0448 N-Nitrosodimethylamine BRL uglL 10 1.1 1 '625 4123113 14:05 KC P3D0448 N-Nitroso-di-n-propylamine BRL ug/L 10 2.8 1 "625 4/23113 14:05 KC P3DD448 N-Nitrosodiphenytamine BRL ug1L 10 1.9 1 `625 4123/13 14:05 KC P3DG44B Pentachlorophenoi BRL ug/L 10 2.7 1 '625 4123113 14:05 KC P3DG448 Phenanthrene BRL ug1L 10 2.0 1 '625 4123113 14:05 KC P3D0448 Phenol BRL ug/L 10 0.48 1 '625 4123113 14:05 KC P3D0448 Pyrene BRL ug/L 10 1.4 1 '625 4123113 14:05 KC P31010448 Surrogate Recovery Control Limits 2,4,6-Tribromophend 101 % 31-144 2-Fluorobiphenyl 90 % 49.116 2-FWrophenol 44 % 22-84 Nitrobenzene-d5 72 % 43-123 Phenol-tJ5 35 % 1"3 Terphenyl-d14 106 % 49-151 Total Metals Copper 0.18 mg/L 0.010 0.00060 1 '200.7 4123113 19:42 BGM P3D0475 Lead 0.026 mg1L 0.0050 0.00068 1 '200.7 4423113 19:42 BGM P3D0476 Zinc 0.18 MA 0.030 0.0060 1 '200.7 4123M3 19:42 BGM P3D0476 Volatile Organic Compounds by GCIMS 1 1,1,1-Trichlomethane BRL ug/L 5.0 0.12 1 '624 4/29/13 14:29 VHL P3DD555 1,1,2,2-Tetrachlaroethane BRL ug/L 5.0 0.10 1 '624 4/29113 14:29 VHL P3D0555 1,1,2-Trichloroethane BRL ug/L 5.0 0.085 1 '624 4129113 14:29 VHL P3D0555 1,1-DiUtbroethane BRL ug/L 5.0 0.11 1 '624 4/29113 14.29 VHL P3D0555 1,1-Dichloroethylene BRL u91L 5.0 0.094 1 '624 4129/13 14:29 VHL P3D0555 1,2-Diehlorobenzene BRL u91t. 5.0 0.099 1 '624 4129113 14:29 VHL P3D0555 1,2-Dichloroethane BRL ug1L 5.0 D.G63 1 '624 4129113 14:29 VHL P3D0555 1,2-Dichloropropane BRL ug/L 5.0 0.12 1 '624 4129/13 14:29 VHL P3D0555 1,3-Dichlorobenzene BRL ug1L 5.0 oAl 1 1624 4129/13 14:29 VHL P3DG555 This report should not be reproduced, except In its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road • P.O, Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number. 1.8001629-6364 - fax: 7041626-0409 Obhf !8!p�31 ® Full -Service Analytical & 0 Laboratory Report r Environmental R I S NI I Solutions 05l1012013 �Aa �i/ueonnrniea ono Environmental Testing Solutions Project: (Tyco) Pentair Valves 8 Client Sample ID: Outfall #2 Attn: Kelley Keenan Controls Prism Sample ID: 3040546-02 PO Box 7565 Prism Work Order: 3040546 Asheville, NC 28802 Sample Matrix: Water Time Collected: 04/17/13 14:30 Time Submitted: 04/19/13 11:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datelrme ID 1,4-Dichlorobenzene BRL ugIL 5.0 0,11 1 "624 4f29113 14:29 VHL P3DO555 2-Chloroethyl Vinyl Ether BRL ug1L 10 0.44 1 '624 4129113 14:29 VHL P3D0555 Acrolein BRL ug1L 100 0.86 1 '624 4/29113 14:29 VHL P31)0555 Acrylonithle BRL ug/L 100 0.73 1 '624 4/29113 14:29 VHL P3D0555 Benzene BRL ug1L 5.0 0.066 1 '624 4129113 14:29 VHL P31)0555 Bromodichlommethane BRL ug1L 5.0 0.082 1 '624 4/29/13 14:29 VHL P3D0555 Bromofarm BRL ugIL 5.0 0.15 1 '624 4129113 14:29 VHL P3D0555 Bromomethane BRL ug1L 10 0.19 1 '624 4/29113 14:29 VHL P3D0555 Carbon Tetrachloride BRL ug1L 5.0 0.088 1 `624 4/29113 14:29 VHL P3DD555 Chlorobenzene BRL ugIL 5.0 0,098 1 '624 4129113 14:29 VHL PX0555 Chloroethane BRL ug1L 10 0.26 1 'B24 4129113 14:29 VHL P3D0555 Chloroform BRL ug/L 5.0 0,059 1 'fi24 4129/13 14:29 VHL P3D0555 Chloromethane BRL ugIL 10 D.18 1 `624 4/29113 14:29 VHL P3D0555 cis-1,3-Dichloropropylene BRL ug1L 5.0 0.20 1 '624 4129/13 14:29 VHL P360555 Dibmmochloromethane BRL ug1L 5.0 0.087 1 '624 4129113 14:29 VHL P3130555 Ethylbenzene BRL ug1L 5.0 0,12 1 '624 4129113 14:29 VHL P3D0555 Methylene Chloride BRL ug/L 5.0 0.069 1 '624 4/29/13 14:29 VHL P31)0555 Tetrachloroethylene SRL ug1L 5.0 0.14 1 "624 4/29/13 1429 VHL P3D0555 Toluene BRL ug1L 5.0 0,088 1 `624 4I29113 14:29 VHL P3D0555 trans-1,2-Dichloroethylene BRL ug1L 5.0 0.093 1 '624 4/29/13 14:29 VHL P3D0555 trans- 1, 3-Dichloropropylene BRL ugfL 5.0 0.065 1 '624 4129113 14:29 VHL P3130555 Trichloroethylene BRL ug/L 5.0 0.15 1 '624 4129I13 14:29 VHL P31)0555 Thrliloratluoromethane BRL ug/L 10 0.018 1 '624 4129/13 14:29 VHL P31)0555 Vinyl chloride BRL ug1L 10 0.51 1 "624 4129/13 14:29 VHL P3D0555 Surrogate Recovery Control Limits 4-Bramofluorobenzene 98 % 74-126 Dibromofluoromethane 114 % 75-127 Toluene -dB 109 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number 1-8001629-6364 - Fox., 7041525-W9 Cbhf !9!pg3l Level II QC Report 5/10/13 IS M j Envi onm1enial Solu ons Environmental Testing Solutions Attn: Kelley Keenan PO Box 7565 Asheville, NC 28802 Project: (Tyco) Pentair Valves & Controls Volatile Organic Compounds by GC1MS - Quality Control Prism Work Order: 3040546 Time Submitted: 4/19/2013 11:45:00AM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P3D0555 - 624 Blank (PM0555-BLK1) Prepared & Analyzed: 04/29/13 1,1,1-TOchloroethane BRL 5.0 ugfL 1,1,22-Tetrachloroethane BRL 5.0 ugfL 1,1,2-Trichloroethane BRL 5.0 ugfL 1,1-Dichloroethane BRL 5.0 ugfL 1,1-Dichloroethylene BRL 5.0 ug1L 1,2-Dichlorobenzene BRL 5.0 ugfL 1,2-Dichioroethane BRL 5.0 ugfL 1,2-Dichloropropane BRL 5.0 ugfL 1,3-Dichlorobenzene BRL 5.0 ugfL 1,4-Dichlorobenzene BRL 5.0 ugfL 2-Chloroethyl Vinyl Ether BRL 10 ugfL Acrolein BRL 100 ugfL Acrylonitrile BRL 100 ugfL Benzene BRL 5.0 ugfL Bramodichloromethane BRL 5.0 ugfL Bromoform BRL 5.0 ugfL Bromomethane BRL 10 ug/L Carbon Tetrachloride BRL 5.0 ugfL Chlorobenzene BRL 5.0 ugfL Chloroethane BRL 10 ugfL Chloroform BRL 5.0 ugfL Chloromethane BRL 10 ugfL cis-1,3-Dichloropropytene BRL 5.0 ugfL Dibromochloromethane BRL 5.0 ugfL Ethylbenzene BRL 5.0 ugfL Methylene Chloride BRL 5.0 ugfL Tetrachloroethylene BRL 5.0 ugfL Toluene BRL 5"0 ugfL trans-1,2-Dichloroethylene BRL 5.0 ugfL trans-1,3-Dichloropropylene BRL 5.0 ugfL Trichloroethylene BRL 5.0 ugfL Trichloroftuoromethane BRL 10 ugfL Vinyl chloride BRL 10 ugfL Surrogate.,4-Bromolluorobenzene 49,6pp1 ug/L 50.00 99 74-126 Surrogate: Dibromoiluoromefhane 57.9 ug/L 50.00 116 M127 Surrogate: Toluene-dS 55.2 ug/L 50.00 110 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, tnc. 449 3pringhrook Road - P.O. Box 240643 - charlotte, NC 28224-0643 Phone: 704/629-6364 -Toll Free Number. 1-8001529-6364 - Fax: 7041526-0409 OW IF 11-Service Analytical 8 P R I S M Environmental Solutions Level it QC Report 5110/13 Environmental Testing Solutions Project: (Tyco) Pentair Valves & Controls Prism Work Order: 3040546 Attn: Kelley Keenan Time Submitted: 4/19/2013 11:45:OOAM PO Box 7565 Asheville, NC 28802 Volatile Organic Compounds by OCIMS - Quality Control Reporting Spike Source %REC ' RPD Analyte Result limit Units Level Result %REC Limits RPO Limit Notes Batch P3D0555 - 624 LCS (P3D0666-BSI) Prepared 8 Anatyzed: 04/29/13 1,1,1-Trichloroethane 18.7 5.0 ug/L 20,00 94 52.162 1,1,2,2-Tetrachloroethane 17.2 5.0 ug1L 20.00 86 46-157 1,1,2-Trichloroethane 19.8 5.0 ug/L 20,00 99 52-150 1,1-Dichloroethane 18.4 5.0 ug/L 20.00 92 59-155 1, 1 -Dichloroethylene 18.4 5.0 ug/L 20,00 92 10-234 1,2-Dichlorobenzene 19.1 5.0 ug/L 20.00 95 18-190 1,2-Dichioroethane 16.8 &0 ug/L 2001). 84 49-155 1,2-Dichtoropropane 16.4 5.0 uglL 20.00 92 10-210 1,3-Dichlorobenzene 19.8 5.0 ug1L 20.00 99 59-156 1,4-Dichlorobenzene 19.5 5.0 uglL 20,00 97 16-190 2-Chioroethyl Vinyl Ether 24.8 10 ug/L 20.00 124 10-305 Acrolein 50.3 100 uglL 40.00 126 10-196 Acrylonitrile 36.8 100 ug/L 40.00 92 60-134 Benzene 20.0 5,0 ug/L 20.00 100 37-151 Bromodichloromethane 19.2 5.0 uglL 20.00 96 35-155 Bromoform 21.2 5.0 uglL 20,00 106 45-169 Bromomethane 23.1 10 ug/L 20.00 116 10-242 Carbon Tetrachloride 19.9 5.0 ug/L 20,00 99 70-140 Chlorobenzene 20.8 5.0 ug/L 20.00 104 37-160 Chloroethane 20.0 10 ug/L 20.00 100 14-230 Chloroform 19.2 5.0 ug/L 20.00 96 51-138 Chloromethane 20.9 10 uglL 20.00 104 10-273 cis-1,3-Dichloropropylene 21.6 5.0 uglL . 20.00 108 10-227 Dibromochloromethane 19.9 5.0 ug1L 20.00 99 53-149 Ethylbenzene 21.0 5.0 ug/L 20.00 105 37-162 Methylene Chloride 16.5 5.0 ug/L 20.00 83 10-221 Tetrachloroethylene 23.7 5.0 ug/L 20.00 119 64-148 Toluene 20.8 5.0 ug/L 20.00 104 47-150 trans-1,2-Dichloroethylene 19.9 5.0 ug/L 20.00 100 54-156 trans-1,3-Dichloropropylene 19.2 5.0 uglL 20,00 96 17-183 Trichloroethylene 21.3 5.0 ug/L 20.00 107 71-157 Tdchlorofluoromethane 18.1 10 ug/L 20,00 91 17-181 Vinyl chloride 24.9 to ug/L 20.00 125 10-251 Sur7ogate:4-Bromofluorobenzene 44.3 ug/L 50.00 89 74-126 Surrogate: Dibromofluoromethane ST2 ug/L $0,00 114 75-127 Surrogate: Toluene-d8 54.1 ug/L 50.00 108 74-122 This report should not be reproduced, except in its entirety, without the written consent of prism Laboratories, Inc. 449 Spring brook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number. 1.8001629.6364 - Fax: 7041626-0409 Cbhf !21 !p931 'C7 Level II QC Report PRISM Service Analytical 8 5110113 Envi Environmental Solutions �" �,\Tusoa�rannEs we Environmental Testing Solutions Attn: Kelley Keenan PO Box 7565 Asheville. NC 28802 Project: (Tyco) Pentair Valves & Controls Prism Work Order: 3040546 Time Submitted: 4/19/2013 11:45:00AM Volatile Organic Compounds by GClMS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch MOMS - 624 LCS Dup (P3D0555-BSD1) Prepared & Analyzed: 04/29/13 1,1,1-Trichloroethane 17.8 5.0 ug/L 20,00 89 52-162 5 200 1,1,2,2-Tetrachloroethane 17.5 5.0 ug/L 20.00 88 46-157 2 200 1,1,2-Thchloroethane 18.8 5.0 ug/L 20.00 94 52-150 5 200 1,1-Dichloroethane 17.5 5.0 ug/L 20.00 87 59.155 5 200 1,1-Dichloroethylene 16.8 5.0 ug1L 20.00 84 10-234 9 200 1,2-Dichlorobenzene 19.5 5.0 ug/L 20.00 98 18A90 3 200 1,2-Dichloroethane 16.7. 5.0 ug/L 20.00 84 49-155 0.9 200 1,2-Dichloropropane 17.8 5.0 ug/L 20,00 89 10.210 3 200 1,3-Dirhlorobenzene 19.7 5.0 ug/L 20.00 98 59-156 0.5 200 1,4-Dichlorobenzene 19,6 5,0 ug/L 20.00 98 18-190 0.7 200 2-Chloroethyl Vinyl Ether 23.5 10 uglL 20.00 118 10-305 5 200 Acrolein 44.9 100 ug/L 40.00 112 10-196 11 200 . Acrylonitrile 35.8 100 ug1L 40.00 90 60-134 3 200 Benzene 19.1 5.0 ug/L 20.00 96 37-151 5 200 Bromodichloromethane 18.9 5.0 ug/L 20.00 94 35-155 2 200 Bromofonn 20.9 5.0 ug1L 20.00 104 45-169 2 200 Bromomethane 19.7 10 ug/L 20.00 98 10-242 16 200 Carbon Tetrachloride 18.9 5.0 ug/L 20.00 94 70-140 5 200 Chlorobenzene 20.4 5.0 ug/L 20.00 102 37-160 2 200 Chloroethane 19.0 10 ug/L 20.00 95 14-230 5 200 Chloroform 18.2 5.0 ug1L 20.00 91 51-138 5 200 Chloromethane 1 B.6 10 ug/L 20.00 93 10-273 12 200 cis-1,3-Dichloropropylene 20.5 5.0 ug/L 20.00 102 10-227 5 200 Dibromochloromethane 19.6 5.0 ug/L 20.00 98 53-149 2 200 Ethylbenzene 20A 5.0 ug/L 20.00 102 37-162 3 200 Methylene Chloride 15.8 5.0 ug/L 20,00 79 10-221 5 200 Tetrachloroethylene 22.7 5.0 ug/L 20,00 114 64-148 4 20D Toluene 19.9 5.0 ug/L 20,00 99 47-160 4 200 trans-1,2-Dichioroethylene 19.4 5.0 uglL 20.00 97 54-156 3 200 trans-1,3-Dichloropropylene 18.8 5.0 ug/L 20.00 94 17-183 2 200 Trichloroethylene 20.8 5.a ug/L 20.00 iO4 71-157 3 20D Trichlorofluoromethane 17.1 10 ug1L 20.00 85 17-181 6 200 Vonyl chloride 22.5 10 ug/L 20.00 113 10-251 10 200 Surrogate:4-Sromofluorobenzene 45.2 ugiL 50.00 90 74-126 Surrogate: Dibmmofluorometharre 56.9 ug/L 50.D0 114 75-127 Surrogate: Toluene -dill 54.6 ug/L 50.00 109 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240W - Charlotte, NC 28224-0643 Phone: 7041629.6364 - Toll Free Number. 1-6001629-6364 - Fax: 7041626-0409 Cbhf 122!= Enicai s f �PRISM =✓Tp_s. Environmental Solutions Environmental Testing Solutions Attn: Kelley Keenan PO Box 7565 Asheville, NC 28802 Project: (Tyco) Pentair Valves & Controls 5ernivolatile Organic Compounds by GC/MS - Quality Control eLevel II QC Report 5110113 Prism Work Order: 3040546 Time Submitted: 4/19/2013 11:45MAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits - RPD Limit Notes Batch P3D0448 - 626 Blank (P3D9448-BLK1) 1,2,4-Trichloro4enzene BRL 10 ug/L 1,2-Dichtorobenzene BRL 10 uglL 1,3-Dichlorobenzene BRL 10 ug1L 1,4-Dichlorobenzene BRL 10 ug1L 1-Methyinaphthalene BRL 10 ug/L 2,4,6-Trichlorophenol BRL 113 ug1L 2,4-Dichlorophenol BRL 10 ug1L 2,4-Dimethylphenoi BRL 10 ug1L 2,4-Dinitrophenol BRL 10 ug1L 2,4-Dinitrotoluene BRL 10 ug1L 2,6-Dinitrotoluene BRL 10 ug1L 2-Chloronaphthalene BRL 10 ug1L 2-Chlorophenol 8RL 10 ug1L 2-Methyinaphthaiene BRL 10 ug1L 2-Nitrophenol BRL 10 ug1L 3,T-Dichlorobenzidine BRL 10 ug1L 4,6-Dinitro-2-methylphenol BRL 10 ug1L 4-Bromophenyl phenyl ether BRL 10 ug1L 4-Chloro-3-methylphenol BRL 10 uglL 4-Chlorophenyl phenyl ether BRL 10 ug1L 4-Nitrophenol BRL 50 ug1L Aoenaphthene BRL 10 ug/L Acenaphthylene BRL 10 ug1L Anthracene BRL 10 ug1L Benzidine BRL 100 ug1L Benzo(a)anthracene BRL 10 uglL Benzo(a)pyrene BRL 10 ug1L Senzo(b)fjuoranthene BRL 10 ug1L Benzo(g,hJ)perylene BRL 10 ug/L Benzo(k)tiuoranthene SRL 10 ug1L bis(2-Chloroethoxy)methane BRL 10 ug1L Bis(2-Chloroethyl)ether BRL 10 ug1L Bis(2-chloroisopropyi)ether BRL 10 ug1L Bis(2-Ethythexy0phthalate BRL 10 uglL Butyl benzyl phthalate BRL 10 ug1L Chrysene BRL 10 uglL Dibenzo(a,h)anthracene BRL 10 ug1L Diethyl phthalate BRL 10 ug1L Dimethyl phthaiale SRL 10 ug1L Din -butyl phthalate BRL 10 ug1L Di-n-octyl phthalate BRL 10 uglL Fluoranthene BRL 10 uglL Fluorene BRL 10 uglL Hexachlorobenzene BRL 10 ug1L Hexachlorobutadiene BRL 10 uglL Hexachlorocyctopentadiene BRL 10 ug1L red & Analvzed: 04122/13 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240S43 - Charlotte, NC 28224-0643 Phone: 704/629-6364 - Toll Free Number. 1-8001629.6364 - Fax: 7041626.0409 Cbhf !2_7p 31 r� P I S n A I Full -Service alSolutiol 3 ' V � Environmemal Solutions �` � uearvTan�s iMc Environmental Testing Solutions Attw Kelley Keenan PO Box 7565 Asheville, NC 28802 Project: (Tyco) Pentair Valves & Controls Semivolatile Organic Compounds by GCIMS - Quality Control Analyte Batch P300448 - 625 e Level 11 QC Report 5110113 Prism Work Order: 3040546 Time Submitted: 4/19/2013 11:45:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result °%REC Limits RPD Limit Notes Blank (P3D0448-BLKij Prepared 8 Analyzed: 04/22/13 Hexachloroethane BRL 10 ug1L Indeno(1,2,3-od)pyrene BRL 10 ug1L Isophorone BRL 10 ug1L Naphthalene BRL 10 uglL Nitrobenzene BRL 10 uglL N-Nitrosodimethylamine BRL 10 ug1L N-Nitroso-di-n-propylamine BRL 10 ug1L N-Nitrosodiphenylamine BRL 10 ug1L Pentachlorophenof BRL 10 ug1L Phenenthrene BRL 10 ug1L Phenol BRL 10 ugtL Pyrene BRL 10 ug1L unknown (1) 10,9 uglL Surrogate: 2,4,6-Tribromophenol 86.6 U91L 100.0 89 31-144 Surrogate:2-Fluorobiphenyl 49.3 U91L 50.00 99 49-118 Surrogate:2-Fluorophenol 54.9 ug/L 100.0 55 22-84 Surrogate: Nitrobenzene-d5 4T3 U91L 50.00 95 43-123 Surrogate: Phenol-d5 40.6 U91L 100.0 41 10-63 Surrogate: Terpheny6414 42.7 u91L 50.00 65 49-151 LCS (P3D0448-BSI) Prepared 8 Analyzed: 04/22/13 1,2,4-Trichtorobenzene 84.4 10 ug1L 100.0 84 44-142 1,2-Dichlorobenzene 76.4 10 uglL 100.0 76 32-120 1,3-Dichlorobenzene 73.8 10 ug1L 100.0 74 20-124 1,4-Dichlorobenzene 73.5 10 ug1L 100.0 73 20-124 1-Methylnaphthalene 75,2 10 ug/L 100.0 75 40-135 2,4,6-Tdchiorophenol 87.6 10 ug1L 100.0 88 37-144 2,4-Dichlorophenol 86.5 10 ug1L 100.0 86 39-135 2,4-Dimethylphenoi 81.7 10 ug1L 100.0 82 32-119 2,4-Dinitrophenol 133 10 ug1L 100.0 133 10-191 2,4-Dinitrotoluene 106 10 uglL 100.0 106 39-139 2,6-Dinitrotoluene 99.2 10 uglL 100.0 99 50-158 2-Chloronaphthalene 110 10 ug/L 100.0 110 60-118 2-Chlorophenol 82.9 10 ug1L 100.0 83 23-134 2-Methylnaphthalene 74.2 10 ug1L 100.0 74 18-121 2-Nitrophenol 89.7 10 ug1L 100.0 90 29-182 3,T-Dichlorobenzidine 132 10 ug1L 100.0 132 10-262 4,6-Dinitro-2-methylphenol 122 10 ug1L 100.0 122 10-181 4-Bromophenyl phenyl ether 86.1 10 uglL 100.0 86 53-127 4-Chloro-3-methylphenol 81.6 10 ug1L 100,0 82 22-147 4-Chlorophe%l phenyl ether 88.4 t0 ug1L 100.0 88 26-168 4-Nitrophenol 49.5 50 ug1L 100.0 50 10-132 Acenaphthene 80.5 10 ug1L 100.0 81 47-145 Acenaphthylene 85.6 10 ug1L 100.0 86 33-145 Anthracene 91.6 10 ug1L 100.0 92 27-133 Senzidine 101 100 ug1L 100.0 101 15-150 Benzo(a)anthracene 101 10 ug1L 100.0 101 33-143 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Sox 240643 - Charlotte, NC 28224-0643 Phone: 704162M364 - Toil Free Number. 1-8001629-6364 - Fax: 704/526-0409 Obhf !24!pg31 APRISM '�j- �. ueaauoAEs'r Full -Service Analytical 8 Environmental Solutions e Level Ii QC Report 5110/13 Environmental Testing Solutions Project: (Tyco) Pentair Valves & Controls Prism Work Order. 3040546 Attn: Kelley Keenan Time Submitted: 4/19/2013 11:45:OOAM PO Box 7565 Asheville, NC 28802 Semivolatile Organic Compounds by GCIMS - Quality Control Reporting Spike Source %REC RPD Anafyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P3D0448 - 625 LCS (P3D0448-BSI) Prepared 8 Analyzed: 04/22/13 Benzo(a)pyrene 105 10 ug1L 100.0 106 17-163 Benzo(b)fluoranthene 103 10 ug1L 100.0 103 24-159 Benzo(g,h,i)perylene 106 10 ug1L 100.0 106 10-219 Benzo(k)fluaranthene 107 10 ug& 100.0 107 11-162 bis(2-Chloroethoxy)methane 78.1 10 ug1L 100.0 78 33-184 E is(2-Chloroethy0ether 79,5 10 ugR 100.0 79 12-158 Bis(2-chioroisopropyl)ether 72-7 10 ug/L 100.0 73 36-166 Sis(2-Ethylhexyf)phthalate 92.9 10 ug1L 100.0 93 10-158 Butyl benzyl phthalate 96.4 10 ug1L 100.9 96 10-152 Chrysene 95.2 10 ug1L 100.0 95 17-168 Dibenzo(a,h)anthracene 105 10 ug1L 100.0 105 10.227 Diethyl phthalate 83.5 10 ug1L 100.0 83 10-114 Dimethyl phthalate 60.7 10 uglL 1 D0.0 61 10-112 Di rl-butyl phthalate 79.8 10 uglL 100.0 80 10-118 Di-n-octyl phthaiate 104 10 ug/L 100.0 104 10-146 Fluoranthene 90.4 10 ug1L 100.0 90 28-137 Fluorene 90.5 10 ug1L 100.0 90 59-121 Hexachlorobenzene 88.5 10 ug1L 100.0 Be 10-152 Hexachlorobutadiene 8D.5 10 ug1L 100.0 81 24.116 Hexachlorocyclopentadiene 94.9 10 ug1L 100.0 95 32-117 Hexachloroethane 73.4 10 uVL 100.11 73 4D-113 Indeno(1,2,3-cd)pyrene 106 10 ug1L 100.0 106 10-171 lsophorone a0.1 10 ug1L 100.0 80 21-196 Naphthalene 71-9 10 ug1L 10D.0 72 21-133 Nitrobertzene 64-4 10 uA 100.0 04 35-180 N-Nitrosodimethyiamine 72.3 10 ug/L 100.0 72 10-119 N-Nitroso-di-n-propylamine 86.1 10 ug/L 100.0 86 10.230 N-Nitrosodiphenylamine 81.5 10 ug1L 100.0 82 69.162 Pentathlorophenol 104 10 ug/L 100.0 104 14-176 Phenanthrene 87.3 10 ug1L 100.0 87 54-120 Phenol 41.2 10 ug1L 100.0 41 10-112 Pyrene 108 10 ug1L 100.0 108 52-115 Surrogate:2,4,6-Tdbmmophenol 99.1 u91L 100.0 99 31-144 Surrogate:2-Fluorobiphenyl 53.6 ag/L 50.00 107 49-118 Surrogate:2-Fluorophenol 65.9 u91L 100.0 66 22-84 Surrogate: Nifrobenzene-d5 45.2 ug/L 50.00 90 43-123 Sunrogate: PhenoFdS 37.3 ug/L 100.0 37 i0.63 Surrogate: Terphenyt-d 14 MA ugA 50.00 112 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P,o, Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toil Free Number. 1-600162"364 - Fax: 7041826-04o9 Page 14 & 20 A�- Environmental Senrivolatile Organic Compounds by GCfMS - Quality Control Reporting Spike Source %REC RPD Anslyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P3D0446 - 625 LCS Dup (P3DOA48-13SDII) Prepared: D4122/13 Analyzed: 04/23/13 1.2,4-Trichicrobenzene BS_2 10 ug/L 100.0 85 44-142 0.9 200 1,2-Dichlorobenzene 73.5 10 uglL 100.0 74 32-129 4 200 1,3-Dichlorobenzene 88.8 10 ug/L 100.0 69 20-124 7 200 1,4-Dichlorobenzene 71.6 10 uglL 100.0 72 2D-124 3 200 1-Methyinaphthalene 77.4 10 uglL 100.0 77 40-135 3 200 2,4,6-Trichlorophenol 85.1 10 uglL 100.0 85 37-144 3 200 2,4-Dichloraphenot 90.5 10 ug/L 100.0 90 39-135 5 200 2,4-Dimethylphenol 82.5 10 uglL 100.0 82 32-119 0.9 200 2,4-Dinitrophenol 98.4 10 uglL 100.0 98 10.191 30 200 2,4-Dinitrotoluene 106 10 uglL 100.0 106 39-139 0.09 20D 2,6-Dinitrotoluene 101 10 ugtL 1D0.0 101 50-158 2 200 2-Chlomnaphthaiene 103 10 uWL 100.0 103 SO.118 6 200 2-Chlorephenot 80.0 10 uglL 100.0 80 23-134 4 200 2-Nethy1naphthalene 77.0 10 uglL 100.0 77 1 &121 4 200 2-Nitrophenol 66,7 10 uglL 100.0 87 2D-182 3 200 3,T-Dichlvrabenzidine 136 10 uglL 10D,0 136 10-262 3 20D 4,6-Dinitro-2-methylphenol 104 10 ug/L 10D.0 104 10-181 16 20D 4-Bromophenyl phenyl ether 05.4 10 ug1L 100.0 85 53-127 0.8 200 4-Chloro-3-methylphenot 79.4 10 uglL 100.0 79 22147 3 200 4-Chiorophenyl phenyl ether 88.1 10 ug(L 100.0 88 25-156 o,3 200 4-Nitrophenol 41.7 50 uglL 100.0 42 10-132 17 200 Acenaphthene 8D.7 10 uglL 100.0 81 47-145 0.2 200 Acenephthylene 85.8 10 ug/L 1 DDA 86 33-145 0.2 200 Anthracene 89.7 10 uglL 100.0 90 27-133 2 200 Senzidine 92.1 100 ug1L 100.0 92 15-150 9 200 Benzo(a)anthracene 99.1 10 ug(L 100.0 99 33-143 2 200 Benzo(a)pyrene MIS 10 uglL 100.0 100 17-163 6 200 Benzo(b)fluoranthene 98.6 10 uglL 100.0 99 24-159 4 20D 6enzo(g,h,i)peryiene 109 10 uglL 100.0 109 M219 2 200 Benzo(k)ftuoranthene 97.3 10 ug1L 100'0 97 11-162 9 200 bis(2-Chloroethoxy)methane 81.2 10 ug/L 100.0 81 33-184 4 200 8is(2-Chloroethyl)ether 76.2 10 ug/L 100.0 76 12-158 4 200 Bis(2-chloroisopropyl)ether 68.7 10 ug/L 100.0 69 36-166 6 200 Bis(2-EthylheW)phtha1ate 94.1 10 uglL 100.0 94 10-158 1 200 Butyl benzyi phthalate 92.2 10 uglL 100.0 92 M152 4 200 Chrysene 93.4 10 uglL 100.0 93 17-168 2 20D Dibenzo(a,h)anthracene 106 10 uglL 100.0 106 10-227 1 200 Diethyl phthalate 8111 10 ug/L 10010 81 10-114 3 200 Dimethyl phthalate 59.1 10 ug/L 100,0 59 10-112 3 200 Di-n-butyl phthalate 79.2 10 ug/L 100.0 79 10-118 0.7 200 Di-n-octyl phthalate 95.0 10 ug(L 100.0 95 10-146 9 200 Fluoranthene 86.2 10 uglL 100.0 86 26-137 5 200 Fluorene 90.6 10 uglL 100.0 81 59-121 0.2 200 Hexachlorobenzene 88.0 10 uglL 100.0 88 10-152 0.6 20C Hexachlvrobutadiene 81.9 10 uglL 100.0 82 24-116 2 200 Hexachlorocyclopentadiene 93.5 10 ug/L 100.0 94 32-117 1 200 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 2822"S43 Phone: 7041629-6364 - Toll Free Number. 1-8001529- i364 - Fex: 7041626.0409 Page 15 of 20 Level II QC Report �] n r n`Icavamwull-SemiceAnalytical 5110I13 .n.ronmen7al Solutions M I Environmental Testing Solutions Project: (Tyco) Pentair Valves & Controls Prism Work Order: 3040546 Attn: Kelley Keenan Time Submitted: 4/19/2013 11:45.00AM PO Box 7565 Asheville, NC 28602 Semivolatile Organic Compounds by GC1MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limas RPD Limit Notes Batch P3D0448 - 626 LCS Dup (M0448-13SD1) Prepared_ 04/22/13 Analyzed. 04123/13 Hexachtoroethane 69.3 10 uglL 100,0 69 40-113 6 200 Indeno(1,2,3-cd)pyrene 109 10 ug1L 100.0 109 10-171 3 200 Isophorone 80.0 10 ug1L i00.0 so 21-196 0.1 200 Naphthalene 73.9 10 ugtL 100.0 74 21-133 3 200 Nitrobenzene 66,2 10 uglL 100.0 66 35-180 3 200 N-Nitrwodimethylamine 62.8 10 uglL 1oD,D 63 10-119 14 200 N-Nitroso-di-n-propylamine 83.4 10 ug1L 100.0 83 10-230 3 200 N-Nitrosodiphenylamine 80.5 10 ug1L 100.0 80 69-152 1 200 Pentachlorophenol 96.6 10 ug1L 100.0 97 14-176 7 200 Phenanthrene 86.1 10 ug1L 100.0 86 54-120 1 200 Phenol 39.9 10 ug1L 100.0 40 1D-112 3 200 Pyrene 96.0 10 ug& 100.0 96 52-116 12 200 Sumogate:2,4,6-Tribromophenol 94.9 ug/L 10D.0 95 31-144 Sur►ogate:2-Fluorobiphenyl 53.5 ug/L 50.00 107 49-118 Surrogate:2-Fluorophenol 63.8 u91L 100.0 64 22-84 Surrogate: Nihabenzene-o[5 47.4 ug's 50.00 95 43-123 Surrogate: phenotd5 36.4 ug/L 100.0 36 10-63 Surrogate: Terphenyl-dM 51.9 Mt. 50.00 104 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-8364 - Toll Free Number: 1-8001629-6364 - Fax: 7041626-0409 Page 16 Of 20 A-115" I S M F°Il.Sgmice Analytical a Environmental Solutions �e0navomea n1e Environmental Testing Solutions Attm Kelley Keenan PO Box 7565 Asheville, NC 28802 Total Metals - Quatlty Control Analyte Project: (Tyco) Pentair Valves & Controls 19 Level li QC Report 5110113 Prism Work Order: 3040546 Time Submitted: 4/1812013 11:45:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Satch MOM - 200.7 Blank (P3DD475-BLK1) Prepared & Analyzed: 04/23/13 Copper BRL 0.010 rng& Lead BRL 0.0050 mgiL Zinc BRL 0.030 mg1L LCS (P3D0475-BSI) Prepared & Analy2ed: 04/23/13 Copper 0.253 0.010 mg1L 0.2500 101 85-115 Lead 0.262 0.0050 mglL 0.2500 105 85-115 Zinc 0,270 0.030 mglL 0.2500 108 85-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc- 449 Springbrook Road - P.O. Box 240543 • Charlotte, NC 28224-0643 Phone: 7041629-6364 -Toll Free Number. 1-8001529-63fi4 -Fax: 7041626-Mg Page 17 of 20 LJ10-1 10 0Level II QC Report R S M Full-ServiceEavinarin Analytical a A alyticsolutions 5/10113 7�arir+.+or�a nc Environmental Testing Solutions Project: (Tyco) Pentair Valves & Controls Prism Work Order: 3040546 Attn: Kelley Keenan Time Submitted: 4/19/2013 11:45:OOAM PO Box 7565 Asheville, NC 28802 General Chemistry Parameters - Quality Control Reporting Spike Source %REC RPD Anatyte Result Limit units Level Result %REC Limits RPD Limit Notes Batch MOM - NO PREP Blank (P3D0526-BLK1) Prepared & Analyzed: 04130M 3 Oil & Grease (HEM) BRL 5.0 mg1L LCS (P300626-BS1) Prepared & Anatyzed: 04/30/13 Oil & Grease (HEM) 35.0 5.0 m9/L 40.00 Be 76-114 Sample Extraction Data Prep Method: 626 Lab Number Batch Initial Final DateMme 3040545-01 P3D0448 1000 mL 1 mL 04/23/13 8;05 3040546-02 P3D0448 1000 mL 1 mL 04123/13 8:05 Prep Method: 200.7 Lab Number Batch Initial Final Daterrime 304054rr01 P300475 50 mL 50 mL 04123113 8:15 3040546-02 P3130475 50 mL 50 mL 04123/13 8:15 Prep Method: 624 Lab Number Batch Inttlal Final Daterrlme 3040546-01 P3D0555 10 mL 10 mL 04/29/13 8:43 304054"2 P3D0555 10 mL 10 mL 04/29/13 8:43 This report should not be reproduced, except in its entirety, without the written consent of Pnsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704l629.6364 - Toll Free Number. 1-8001529-6364 - Fax: 7041626.0409 Page 18 of 20 v Q Full -Service Analytical & �I - ISM S Environmental Sclutions is Tfm O LA80l INC 449 Springbrook Road • P.O. Box 240W • Charlotte, NO 28224-0543 Phone:7041529-6364 - ll 704/525-0409 Client Company Name: Report To/Contact Name: Reporting Address: Phc Em EDI Sit( Sitc I\s 143D WASTEWATER CHAIN OF CUSTODY PAGE —I— OF J— GUOTE 4 TO ENSURE PROPER BiLLINO: �e'JAlrLValdu� Project Name: T— .. —ry Short Hold Analysis: (Yes) V-ific UST Project: (Yes) No 'Please ATTACH any project reporting (QC LEVEL I) I IV) provisions and/or QC Requirements Invoice To. - Address: no: Fax (Yes) (No): Purchase Order No,/Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Iil (Yes) (No) Email Address FIegU85t8d Duo Oa10 ra t tray a z Days Cl 3 Rays ❑ 4 Days ❑ 5 Days Certification: NELAC iJSACE FL NC �/ I Type: PDF—Exce gr, Must Be yp Un ,7 �� -Working Days" U 6-9 Days r lendsrd 10 days 0 Rush WorPre-Approved F� Ps roved Location Name: T Ci�i I 11—VO t SC OTHER - _NIA Samples received altar 15:00 will he processed next business day. day. Location Physical Address: Turnaround time Is based on business days, excluding weekends and hoildoys. Water Chlorinated: YES NO_ (SEE REVERSE FOR TERMS & CONOmONS REaARDING SERVICES Sample Iced Upon Collection: YES "VNO RENDERIED BY PRISM LABORATORIES, INC. TO CLIENT) — SAMPLE TYPE CONTAINER TYPE AND SIZE (ML) PRESERVATIVES USED ANALYSES TO BE PERFORMED ON THE SAMPLES PRISM CLIENT SAMPLE LAB Comp Crab Plastic Glass Other None Iced HCI NaOH HNO3 H,SO4 pH SOD TSS Cd Cr Cu Pt) Ni Ag Zn 0&G ll as N rA x x x < Ixaz F r " Sampler's Slgnatur,: Sampled By (Print Name) Affiliation _ Upon rallnqu s ng, this Chain of ustody, s your authorization for Prism to proceedwith e analyses as roqueste a ova. Any changes must be submftted In wrltir to the Prism Project Manager. There will be charges for an chap es after ana! sea ha+ae been Initialized. ' NLY � ,.,.;.:•;_:;,,�, ,. SitsARlval`;Tme, r't'":` slinpyis gnature 'f Y�-� e gnarl re Iz:s `� I :I;a y; ou s Addillanal Comments: Relinquished ay: Signature) RecsWad By: (Signature) CJaso SlielpapgftUre Tlrna Relinquished By. {Signature) Re ce For P i y: Dnt r FlBldf'Techi'Fde Method or Shipment: NOTE: ALL SAMPLE COOLF3i3 SHOULD BE TAPEO UT 3 DY S F RTA710N 70 THE LABORATORY. UNTIL REC 70RY. oup SMII�@g9 SAMPLES ARE NOT A.CCEP7Eb AND VERIFIED A A7 E LA 7if•`?t;.-r"��iiri.<.rpr%=%r:cl�c : Led Ex ❑ uPS Li Hand-delvered Ul Posm raid SHrfoa CI Qtller _ C,(� o;: :�vs•:'; •�v:::.. ;., .: ' F.:':::.... Composite Type: FLOW TIME HAND (circle one) Start Date & Time for Composite Sampler: > > Stop Date & Time for Composite Sample: / Date & Time Composite Sample Collected: Total Hours Composite Collected Over. Hours. End Flow: Start Flow: Total: Hrs Date & Time Grab(s) Taken: 04 Hrs Field pH Meter Calibrated: Yes No T Hrs Field pH Result: Analyst's Initials: Gal / Cu Feet Field Temp. Result: Analyst's Initials: (circle one) Sampler Interrupted: Yl No If Yes, Why? SEE REVERSE FOR TERMS & CONDITIONS l CHAIN -OF -CUSTODY./ Analytical Request Client Name: Address: Report to: Phone: Y4 .. 5 Fax:�2ff PO Number: 1 J tnfto"11V, {b. Environmental Testing Solutions, Inc. P4 Box 7565, Asheville, NC 28802 Phone: (828) 350-9364, Fax: (828) 350-9368 Project Name: Project Number: rr i NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Charles Wakild, P. E. Governor Director December 4, 2012 Salvatore Vaccaro Tyco Valves & Controls 953 Old US Hwy 70 Black Mtn, NC 28711 Dee Freeman Secretary Subject: NPDES Stormwater Permit Coverage Renewal Tyco Valves and Controls COC Number NCG030529 Buncombe County Dear Permittee: In response to your renewal application for continued coverage under stormwater General Permit NCG030000 the Division of Water Quality (DWQ) is forwarding herewith the reissued General Permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October 15, 2007 (or as subsequently amended). The following information is included with your permit package: • A new Certificate of Coverage (COC) • A copy of General Permit NCG030000 • A copy of the Technical Bulletin for the General Permit • Two copies of the Discharge Monitoring Report (DMR) Form • Two copies of the Qualitative Monitoring Report Form The General Permit authorizes discharges of Stormwater, and it specifies your obligations for discharge controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself with all the changes in the reissued permit- Your facility has six (6) months from the time of receipt of the permit to update your current SPPP to reflect all new permit requirements. The first sample period of your permit begins January 1, 2013. Your facility must sample a "measureable storm event" beginning during the periods beginning January 1 and July 1 of every year (or, if applicable, report "No Flow," as outlined in Part III, Section E). Also, please note that Tier 3 Actions in Part II of your permit are triggered by benchmark exceedances on four occasions beginning on the effective date of this permit and do not count prior exceedances. The more significant changes in the General Permit since your last COC was issued are noted either in the Draft Permit Fact Sheet that accompanied the public notice (http://portal.ncdenr.org/web/wq/ws/suYcurrent- notices), or in the Response to Comments / Summory of Changes and Technical Bulletin documents that are posted on the 5tormwater Permitting Unit's website with the new General Permit. Please visit http://portal-ncdenr.org/web/wq/ws/su/nodessw (click on 'General Permits' tab) to review that information for your specific General Permit carefully. 1617 Mail Service Center, Ralegh, North Carolina 27699-1617 Location! 612 N. Salisbury 5t. Raleigh, North Carolina 27604 Phone: 91 M07-63001 FAX: S : 9-807-6492 Internet; www.ncwaterguality.org One NorthCarolina An -:quaff Opp iunity\Afrmatije.yaicl Emp!cyer r Salvatore Vaccaro December 4, 2012 Page 2 of 2 Some of the changes include: Part II: • Section A. The Stormwater Pollution Prevention Plan (SPPP) section, if applicable, has been updated to the most current language of our permits. Additional conditions for specific industry sectors have been added to the SPPP requirements in some cases. • Sections B, C: Failure to perform analytical stormwater monitoring may result in the Division requiring that the permittee begin a monthly sampling scheme. • Sections B, C: A lower TSS benchmark of 50 mg/I for HQW, ORW, PNA and Tr Waters applies to these more sensitive waters. • Sections B, C: The monitoring parameter Oil & Grease (O&G) has been replaced by the parameter Total Petroleum Hydrocarbons (TPH) for vehicle maintenance areas, and in some cases, other analytical monitoring requirements. • Sections B, C, D: Inability to sample due to adverse weather must be recorded in the SPPP, or in separate on -site records if your General Permit does not require an SPPP. Adverse weather is defined in the "Definitions' section of the permit. • Sections B, C. The term "Representative Storm Event" has been replaced by "Measurable Storm Event." A measurable storm event is defined in the permit. • Section D: if the permittee fails to respond effectively to problems identified by qualitative monitoring, DWQ may require the permittee to perform corrective action. Please review Parts III and IV to understand the Standard Conditions of your new NPDES General Permit, including Compliance and Liability, Reporting, Monitoring and Records requirements; Operation and Maintenance obligations; and Definitions. Please note that all samples analyzed in accordance with the terms of this permit must be submitted to the Division on Discharge Monitoring Report (DMR) forms available on the Stormwater Permitting Unit's website above. DMR forms must be delivered to the Division no later than 30 days from the date the facility receives the sampling results from the laboratory. Also note that existing permittees do not need to submit a renewal request prior to expiration unless directed by the Division. Your coverage under the General Permit is transferable only through the specific action of DWQ. This permit does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit package, please contact the Division's Stormwater Permitting Unit at (919) 807-6300. Sincerely,/ for Charles Wakild, P.E. cc: DWQ Central Files Stormwater Permitting Unit Files Asheville Regional Office STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030529 STORMWATER NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Tyco Valves & Controls is hereby authorized to discharge stormwater from a facility located at: Tyco Valves and Controls 953 Old US Highway 70 Black Mountain Buncombe County to receiving waters designated as Swannanoa River, a class C waterbody in the French Broad River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III, and IV of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective December 4, 2012. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this 4th day of December, 2012. for Charles Wakild, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission Michael F. Easley, Governor William G- Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.E. Director Division of Water Quality March 29, 2007 Mr. Gene Logan Tyco Valves and Controls 953 Old US Highway 70 Black Mountain, NC 28711 Subject: General Permit No. NCG030000 Tyco Valves and Controls COC NCG030529 Buncombe County Dear Mr. Logan: The Division of Water Quality's Stormwater Permitting Unit received your request for Representative Outfall Status on March 29, 2007. Your request to sample outfalls 001, 002, and 008 as representative of Your eight outfalls (001, 002, 003, 004, 005, 006, 007, and 008) has been granted. If you have any questions concerning this issue, please contact me at telephone number (919) 733-5083 ext. 376. cc: DWQ Asheville Regional Office, Laurie Moorhead Central Files Stormwater Permitting Unit Files . Sincerely, Ke11y Jo son Environmental Engineer NamN` Carolin #uralk North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone (919) 733-5083 Customer Service Internet: www,ncwaterouality.org Location: 512 N. Salisbury St. Raleigh, NC 27604 Fax (919) 733-9612 1-877- 623-6748 An Equal Opportunity/Affirmative Action Employer — 50% Recyeled110% Post Consumer Paper Mar•24. 2007 9:23AM Tyco Valves .and Controls EF:.r-�lU=NCG030-529Owner - Faclllty. Tyco Valves and Ci inspection Date: 03t2V2007 Inspection Type: Stormwater Inspection Summary: Post -it' Fax Note 7671 I- V • . V J I- ' Vale car s� To L c— A`��� Frain CojGept co Phase 8 Phons *S 2 _ y 92 Fax a 9 c9 73 - Fax a dJ! Gene Logan of Tyco Valves and Controls provided a site tour and all documents for review. The stormwater pollution prevention plan and the spill respo se Ian were up to date as were all monitoring and training records. No vehicle maintenance is conducted on site Upon review a e o ells and their analytical monitoring data, it is recommen I a e cl I c or requesting representative outfall status from the Division of Water Quality so that only the 3 outfalls which might ever reflect contamination are monitored analytically (#001, #002, and *008), Representative outfall status must be approved of the Division Director, Mr Alan Klimek. who may be contacted at the following address: Alan Klimek % %� d S , Division of Water Quality D `� � `" ,�f 1617 Mail Service Center Raleigh, NC 27699-1617 '^�/"*� While the site is in compliance with at( permit requirements, it is recommended that the curbing at the scrap metal concrete pad be fully connected with a manual valve installed to allow purposeful draining of uncontaminated rainwater The inspector acknowledges that there are drip pans located under each lugger, but the potential for spills during the emptying of the drip pans exists and the open curbing allows spills and contamniated stormwater to leave the pad. Monitoring of this area already is occurring but the addition of this best management practice would require keeping an eye on the quality of rainwater exiting the area. The stormwater management plan would also need to be updated to reflect this modification Site conditions and all paperwork reflect close attention to the intent and requirements of this permit Mr -Logan is to be commended for such a conscientious effort ce-,lua L�M\ I*C) \401\re5 °\ 5 3 0�A k<, N u N Km' niC a3-711 c hc.c-)" E I �'tltS l �1X ti�J It� �ZCS E 6J7A-7t \FE- C"fPkA- �7���5. Ct�ssEfl ?p ue*knS1 , 3�aa1 �7 4 Page° 2 y, �.. �+'.. P, 't � • �•• 'i. r i � ,� a • � � ,; � +� � A, � 1 k i . r • � �E �. .t .. � . - i f . � S • "r ,� � + i r +( \NATF Michael F. Easley, Governor \OHO RQG William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources 0) 7 Alan W. Klimek, P.E. Director Division of Water Quality June 4, 2004 Mr. R.W. Batchelder Tyco Valves and Controls 953 Old U.S. Highway 70 Black Mountain, NC 28711 Subject: General Permit No. NCG030000 Tyco Valves and Controls COC NCG030529 Buncombe County Dear Mr. Batchelder: In accordance with your application for a discharge permit received on April 28; 2004 we are forwarding herewith the subject certificate of coverage to discharge under the subject state — NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .l and the Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated May 9, 1994 (or as subsequently amended). Please take notice that this certificate of coverage is not transferable except after notice to the Division of Water Quality. The Division of Water Quality may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit that may be required. If you have any questions concerning this permit, please contact Jonathan Diggs at telephone number (919) 733-5083 ext. 537. Sincerely, ORIGINAL SIGNED BY WILLIAM C. MILLS Alan W. Klimek, P.E. cc: Asheville Regional Office Central Files Stormwater and General Permits Unit Files N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-7015 NCOENR Customer Service 1 800 623-7748 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030529 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Tyco Valves and Controls is hereby authorized to discharge stormwater from a facility located at Tyco Valves and Controls 953 Old US Highway 70 Black M011ntaln, North Carolina Buncombe County to receiving waters designated as UTto the Swannanoa River, a class C river in the French Broad River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set firth in Parts L II. III, IV, V, VI and VII of Gencral Permit No. NCG030000 as attached. This certificate of coverage shall become effective June 4, 2004. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day June 4, 2004. ORIGINAL SIGNED BY WILLIAM C. MILLS Alan W. Klimek, Director Division of Water Quality By Authority of the Environmental Management Commission Ax. A 1 1 "I rj A)J, "IS III — OP. W N lip � \� C� �F F0 tc .j_\' t i}l.� 1� cr�3Q �r t' � \Ll��,, ���a a. :a r \. . 11A I Wo, 11. m log I 0.1 zy on 0 A, e Mv �SRZ` 2 0 — fi f9m%� lt�l yFCO-Va.jp�p 4 0529 'Xi TES T,-f� U, b SO RAOIG 9 I ToWERS A I PAI Ali ne "C 646 V, C it j w "qu ffl ij Copyright (C) 1997, Maptech, Inc. Markers Name: Tyco Valves and Controls NCG030529 Short Name: TycVly Coordinates: 035' 36' 30.6" N, 082° 21' 26.2" W Comment: Tyco Valves and Controls NCG030529, subbasin 04-03-02, French Broad River Basin, Buncombe County, UT to Swannanoa River, Class C, USGS quad E09SE Compliance Inspection Report Permit: NCG030529 Effective: 11/01/12 Expiration: 10131/17 owner: Pentair Valves 6 Controls SOC: Effective: Expiration: Facility: Pentair Valves & Controls County: Buncombe 953 Old US Highway 70 Region: Asheville Black Mountain NC 28711 Contact Person: Gerald Runkles Title: Phone: 828-669-3753 Directions to Facility: System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): On -Site Representative(s): Related Permits: Inspection Date: 08/12/2014 EntryTime: 10:OOAM Exit Time: 12:00PM Primary Inspector: Qartene J Kucken Phone: Secondary Inspector(s): Laura C Herbert Phone Fred Walker Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Metal Fabrication Stonnwater Discharge CO . Facility Status: Compliant ❑ Not Compliant Question Areas: Storm Water (See attachment summary) Page: 1 Permit: NCG030529 Owner - Facility: Pentair Valves & Controls Inspection Date: 08/12/2014 Inspection Type : Compliance Evaluation Reason for Visit: Routine Inspection Summary: The facility is clean and well -maintained. A number of housecleaning activities were initiated to source and reduce the copper and zinc levels that initiated the Tier II requirements of the permit. Please remove outfall #8 from the site map and provide a reference history in the SPPP. Please continue with plans for painting areas for wet mopping on a regular basis to reduce potential sources of zinc and copper. The facility has plans to install a water reclamation system from the roof; if this system is installed you may apply for a no exposure permit. Based on this site inspection, you are relieved from the Tier ll requirments for copper and zinc only. Page: 2 permit: NCG030$29 Owner - Facility: Pentair Valves & Controls Inspection Date: 08/1212014 Inspection Type: Compliance Evaluation Reason for Vlstt: Routine Stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwaler Pollution Prevention Plan? 0 ❑ ❑ ❑ # Does the Plan include a General Location (USGS) map? 0 ❑ ❑ ❑ # Does the Plan include a'Narrative Description of Practices"? 0 ❑ ❑ ❑ # Does the Plan include a detailed site map including outfall locations and drainage areas? 0 ❑ ❑ ❑ # Does the Plan include a list of significant spills occurring during the past 3 years? E ❑ ❑ ❑ # Has the facility evaluated feasible alternatives to current practices? ® ❑ ❑ ❑ # Does the facility provide all necessary secondary containment? E ❑ ❑ ❑ # Does the Plan include a BMP summary? N ❑ ❑ ❑ # Does the Plan include a Spill Prevention and Response Plan (SPRP)? 0 ❑ ❑ ❑ # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? 0 ❑ ❑ ❑ # Does the facility provide and document Employee Training? 0 ❑ ❑ ❑ # Does the Plan include a list of Responsible Party(s)? 0 ❑ ❑ ❑ # Is the Plan reviewed and updated annually? Q ❑ ❑ ❑ # Does the Plan include a Stormwater Facility Inspection Program? 0 ❑ ❑ ❑ Has the Stormwater Pollution Prevention Plan been implemented? 0 ❑ ❑ ❑ Comment: Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring semi-annually? 0 ❑ ❑ ❑ Comment: Analytical Monitoring Yes No NA NE Has the facility conducted its Analytical monitoring? E ❑ ❑ ❑ # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ 0 ❑ Comment: Permit and Outfalls Yes No NA NE # Is a copy of the Permit and the Certificate of Coverage available at the site? N ❑ ❑ ❑ # Were all outfalls observed during the inspection? 0 ❑ ❑ ❑ # If the facility has representative outfall status, is it properly documented by the Division? ❑ ❑N ❑ # Has the facility evaluated all illicit (non stormwater) discharges? ❑ ❑ ❑ Comment: Page: 3 Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P. E. Director Division of Water Quality- Coleen H. Sullins, Deputy Director Division of Water Quality Asheville Regional Office WATER QUALITY SECTIQDL..:, _,. , June 4, 2004 Mr, Bill Batchelder, Environmental Coordinator Tyco Valves and Controls 953 Old U.S. 70 Black Mountain, North Carolina 28711 Subject: Investigation of'li�fcirma�on "`"""" '�--` �~ Tyco Valves and Controls Black Mountain Stormwater Permit Number NCG030529 Buncombe County Dear Mr. Batchelder: The purpose of this letter is to confirm our meeting yesterday, June 3, 2004, regarding your stormwater permit application NCG030529. The reason for the meeting was confusion on your application regarding the definition of a "lugger". During our meeting you showed me the "loggers", which are covered bins for metal recycling with secondary containment. You also informed me that the secondary containment is inspected, pumped regularly and documented. I was very satisfied with what I saw and have communicated my findings to Mr. Jonathan Diggers in the NPDES Stormwater Permitting Unit. would like to thank you for your cooperation and time. If you should have any questions regarding this matter please call me at (828) 296-4500. Sincerely, arry Frost Environmental Chemist xc: Jonathan Diggers, Stormwater and General Permitting Unit *F. r :iNICDE' 2090 U.S_ 70 Hiehvvav Svvannanoa, North Carolina 28778 Telephone (928) 296-4500 fax (828) 299-7043 Customcr Service 1-877-623-6798 E7 NCDFNR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Coleen H. Sullins Dee Freeman Governor Director Secretary March 1, 2011 Gene Logan Tyco Valves & Controls 953 Old US Highway 70 Black Mountain NC 28711 SUBJECT: NPDES Stormwater Permit Compliance Inspection Tyco Valves and Controls Permit No: NCG030529 . Buncombe County Dear Mr. Logan: This letter is in follow-up to the NPDES Stormwater Permit Compliance Inspection conducted on February 15, 2011. The facility was found to be in compliance with permit NCG030529. Enclosed is a copy of the Compliance Inspection Report, which contains additional observations and comments for your reference. Please contact me at (828) 296-4664 or chuck. cranford.cr,ncdenr.g_o_v , if I can be of any further assistance. Sincerely, / r Chuck Cranford Environmental Specialist Surface Water Protection Enclosure cc: Central Files Asheville Files S:IS WP14-NonpointSource\StomtwaterllndustriallCompliancckCEI_Chuck.2. doc Location: 2090 U.S. Highway 70, Swannanoa, North Carolina 28778 Phone: 828-296-450M FAX: 828-299-70431 Customer Service: 1-877-623-6748 Internet: www.ncwaterquality.org NorthCarolina Aaturdlj(y An Equal Opportunity 1 Affirmative Action Employer Compliance Inspection Report Permit: NCGO30529 Effective: 11/01/07 Expiration: 10/31/12 Owner: Tyco Valves & Controls SOC: Effective: Expiration: Facility: Tyco Valves and Controls County: Buncombe 953 Old US Highway 70 Region: Asheville Black Mountain NC 28711 Contact Person: Gene Logan Title: Phone: 828-669-3753 Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Representative(s): Related Permits: Certification: Phone: Inspection Date: 021151201 i Entry Time: 02:30 PM Exit Time: 03:45 PM Primary Inspector: Susan A Wilson Phone: 828-294-4500 Secondary lnspector(s): Reason for Inspection: Complaint Inspection Type: Stormwatef Permit Inspection Type: Metal Fabrication Stormwater Discharge COC Facility Status: ■ Compliant ❑ Not Compliant Question Areas: Storm Water (See attachment summary) Page: 1 Permit: NCO030529 Owner - Facility: Tyco Valves & Ccntrois Inspection Date: 02/15/2011 Inspection Type: Stormwater Reason for Visit: Complaint Inspection Summary: DWQ staff was met on site by Gene Logan. A tour was conducted of the interior and exterior of the facility, observing the stormwater conveyances and outfalls and site conditions. During the visit, the SPPP manual was reviewed, operational activities and existing stormwater exposures were discussed_ Permit requirements were also reviewed. At the time of the inspection the site was found to be in compliance with the permit. The inspector noted that the facility appeared to maintain good housekeeping practices and records were found to be in good order. According to Mr. Logan, the permittee conducts stormwater sampling at the primary facility located at 953 Old US Highway 70 as well as 905 Old US Highway 70. According to DWQ records the permittee requested a No Exposure Certification for the facility. A_No_ Exposure —Certification is not -appropriate. The site must maintain coverage under a NPDES NCG030000 stormwater permit. However, the warehouse at 905 does not require a stormwater permit. All monitoring at 905 Old US Highway 70 may be discontinued. The facility might consider implementing a Solvent Management Plan to reduce analytical requirements, if appropriate. Page: 2 Permit: NCG030529 Owner - Facility: Tyco Valves & Controls Inspection fate: 02/15/2011 Inspection Type: Stormwater Reason for Visit: Complaint Stormwater Pollution Prevention Plan Yes No NA HE Does the site have a Storrwater Pollution Prevention Flan? ■ ❑ ❑ ❑ # Does the Plan include a General Location (USGS) map? ■ ❑ n n # Does the Plan include a "Narrative Description of Practices"? s ❑ ❑ ❑ # Does the Plan include a detailed site map including outfali locations and drainage areas? O it ❑ ❑ # Does the Plan include a list of significant spills occurring during the past 3 years? ■ ❑ ❑ ❑ # Has the facility evaluated feasible alternatives to current practices? ■ ❑ ❑ ❑ # Does the facility provide all necessary secondary containment? ■ n Cl n # Does the Plan include a BMP summary? ■ ❑ ❑ ❑ # Does the Plan include a Spill Prevention and Response Plan (SPRP)? ■ fl in ❑ # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? ■ ❑ ❑ ❑ # Does the facility provide and document Employee Training? e n n n # Does the Plan include a list of Responsible Party(s)? ■ ❑ ❑ ❑ # is the Plan reviewed and updated annually? ■ ❑ ❑ ❑ # Does the Plan include a Stormwater Facility Inspection Program? ■ n n n Has the Stormwater Pollution Prevention Plan been implemented? ■ ❑ ❑ ❑ Comment: Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring semi-annually? ■ ❑ ❑ ❑ Comment: Analytical Monitoring Yes No NA NE Has the facility conducted its Analytical monitoring? ■ ❑ Cl ❑ # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ ■ ❑ Comment: Permit and outfalls Yes No NA NE # Is a copy of the Permit and the Certificate of Coverage available at the site? ■ ❑ ❑ ❑ # Were all outfalls observed during the inspection? ■ ❑ Q ❑ # if the facility has representative outfall status, is it properly documented by the Division? 0000 # Has the facility evaluated all illicit (non stormwater) discharges? ■ ❑ Q ❑ Comment: Page: 3 tyco oeA �� � c Flow Control t A]C&--1) W; Z r April 7, 2009 Stormwater Permitting Unit Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 K() ✓sy „ Valves &Controls 953 1JCCTNf,96� 953 Old US Highway 70 Black Mountain, NC 2871 Phone 828-669-5515 Fax. 828-669-4017 Subject: NO EXPOSURE CERTIFICATION for Exclusion NCGNE0000; application Ref: NPDES Permit Number: NCG030529 Dear Sir/Madame, Subject document and associated support documentation is enclosed for your review. Please be advised, the application applies to the facility located at 905 Old US Highway 70 West in Black Mountain, North Carolina, (Outfalls 4 thru 8). That facility is used for receiving material, warehouse storage, production, customer service and sales. The receiving dock is covered and no outside material handling operations are performed during precipitation. No equipment or material is exposed to the elements. The facility located at 953 Old US Highway 70 West will remain covered under the referenced permit. Please contact me if 1 can be of further assistance or if you need any other S E (Gene ogan EHS/Maintenance Supervisor Telephone: 828 669-3753 Tyco Valves and Controls 953 Old US Highway 70 West Black Mountain, NC 28711 k ,/Sy A� ApffaftsNOMMOL NCDENR Fn�rts.Mr.n .Nn h4Vt.+. Rrw..Kre Division of Water Quality / Surface Water Protection National Pollutant Discharge Elimination System NO EXPOSURE CERTIFICATION for Exclusion NO EXPOSURE CERTIFICATION NCGNEOOD4 FOR AGENCY USE ONLY Date Received Year Month Day . p O Certificate ot covcrapc D Please check here if this is a renewal: n RENEWAL National Pollutant Discharge Elimination System application for exclusion from a Stormwater Permit based on NO EXPOSURE: Submission of this No Exposure Certification constitutes notification that your facility does not require a permit for stormwater discharges associated with industrial activity in the State of North Carolina because it qualifies for a no exposure exclusion. A condition of no exposure at an industrial facility means all industrial materials and activities are protected by a storm resistant shelter (with some exceptions) to prevent exposure to rain, snow, snowmelt, and/or runoff. For permitted facilities in North Carolina, DWO must approve your application for No Exposure Certification before this exclusion is effective. Until you are issued a No Exposure Certification and your NPDES permit is rescinded, your facility must continue to abide by the terms and conditions of the current permit. Industrial materials or activities include, but are not limited to: material handling equipment or activities, industrial machinery, rare materials, intermediate products, by-products, final products, or waste products. Material handling activities include the storage, loading and unloading, transportation, or conveyance of any raw material, intermediate product, final product or waste product. A storm resistant shelter is not required for the following industrial materials and activities: drums, barrels, tanks, and similar containers that are tightly sealed, provided those containers are not deteriorated and do not leak. "Sealed" means banded or otherwise secured and with locked or non -operational taps or valves; adequately maintained vehicles used in material handling; and final products, other than products that would be mobilized in stormwater discharges (e.g., rack salt). A No Exposure Certification must be provided for each facility qualifying for the no exposure exclusion. In addition, the exclusion from NPDES permitting is available on a facility -wide basis only —not for individual outfalls. If any industrial activities or materials are, or will be, exposed to precipitation, the facility is not eligible for the no exposure exclusion. By signing and submitting this No Exposure Certification form, you certify that a condition of no exposure exists at this facility or site and are obligated to comply with the terms and conditions of 40 CFR 122.26(g). You are required to reapply for the No Exposure Exclusion once eve[five years. For questions, please contact the DWQ Regional Office for your area. (See page 6) (Please print or type) 1) Mailing address of owner/operator address to which all certification correspondence will be mailed Name r5) *4b e-ci—Ad LS Contact I % ' L..0 t_ _ Street Address 4f 5-S 0 l ( I) LO s 1 City AA 00-'rAr �1J State kJ(-- ZIP Code 7 Telephone No. �`{ _ iD i, - — � .'L_S -- Fax: _ r 4 Page t of 7 5WU-NE-021309 Last revised 2/13/2009 NCGNE0000 No Exposure Certification 2). Location of facility producing discharge: 3) Facility Name Facility Contact Street Address City County Telephone No. fn62 ,f 5f _ Fax: Physical location information: Please provide a narrative description of how to get to the facili (use street names, stateroad numbers, and distance and direction from a roadway intersection). �-- D C d TQ t (A copy of a map with the facility clearly located on it should be included with the certification application.) -rp IrVfc 4) Is the facility located on Native American Lands? ❑ Yes VNo 5) Is this a Federal facility? ❑ Yes &No 6) Latitude 0 Longitude —�602. (deg., min., seconds) 7) This NPDES No Exposure Exclusion application applies to which of the following: ❑ New or Proposed Facility Date operation is to begin 0 Existing Date operation began ❑ Renewal of existing No Exposure Certification Certification No.: NCGNE 8) Was this facility or site ever covered under an NPDES Stormwater Permit? ip Yes ❑ No If yes, what is the NPDES Permit Number? 10 Q ?, Q S raj 9) Standard Industrial Classification: Provide the 4 digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial activity at this facility SIC Code: Al 10) Provide a brief description of the types of industrial activities and products produced at this facility: 11) Does this facility have any Non -Discharge permits (ex: recycle permits)? A No ❑ Yes If yes, list the permit numbers for all current Non -Discharge permits for this facility: Page 2of7 5W U-NE-021309 Last revised 2/13/2009 NCGNEOOOO No Exposure Certification Exposure Checklists (12. - 14.) 12) Are any of the following materials or activities exposed to precipitation, now or in the foreseeable future? (Please check either "Yes" or "No.") If you answer "Yes" to any of these items, you are not eligible for the no exposure exclusion. a. Eking, storing, or cleaning industrial machinery or equipment, and areas where ❑ Yes a No ❑ NIA residuals from using, storing or cleaning industrial machinery or equipment remain and are exposed to stormwater b. Materials or residuals on the ground or in stormwater inlets from spills/leaks ❑ Yes 0 No ❑ NIA c. Materials or products from past industrial activity ❑ Yes 0 No ❑ NIA d. Material handling equipment (except adequately maintained vehicles) ❑ Yes ® No ❑ NIA e. Materials or products during loading/unloading or transporting activities ❑ Yes . a No ❑ NIA f. Materials or products stored outdoors (except final products intended for outside ❑ Yes IF No 0 NIA use [e.g., new cars] where exposure to stormwater does not result in the discharge of pollutants) g. Materials contained in open, deteriorated or leaking storage drums, barrels, tanks, ❑ Yes R No ❑ NIA and similar containers h. Materials or products handled/stored on roads or railways owned or maintained by ❑ Yes 91 No ❑ NIA the discharger i. Waste material (except waste in covered, non -leaking containers [e.g., dumpsters]) []Yes ® No ❑ NIA j. Application or disposal of process wastewater (unless otherwise permitted) ❑ Yes ® No Cl NIA k. Particulate matter or visible deposits of residuals from roof stacks and/or vents not 0 Yes ® No ❑ NIA otherwise regulated (i.e., under an air quality control permit) and evident in the stormwater outflow I. Empty containers that previously contained materials that are not properly stored ❑ Yes iv No ❑ N/A (i.e., not closed and stored upside down to prevent precipitation accumulation) m. For any exterior ASTs, as well as drums, barrels, tanks, and similar containers ❑ Yes 0 No ❑ NIA stored outside, has the facility had any releases in the past three (3) years? 13) Above Ground Storage Tanks (ASTs): If you answer "No" to any of the following items, you are not eligible for the no exposure exclusion. a. Are exterior ASTs or piping free of rust, damaged or weathered coating, pits, or ❑ Yes ❑ No 10 N/A deterioration, or evidence of leaks? b. Is secondary containment provided for all exterior ASTO If so, is it free of any ❑ Yes ❑ No a N/A cracks, holes, or evidence of leaks, and are drain valves maintained locked shut? Page3of7 SWU-NE-021309 Last revised 7J13/2oo9 NCGNE0000 No Exposure Certification 14) Secondary Containment: If you answer "No" to any of the following items, you are not eligible for the no exposure exclusion. . a. is secondary containment provided for single above ground storage containers (including drums, barrels, etc.) with a capacity of more than 660-gallons? b. Is secondary containment provided for above ground storage containers stored in close proximity to each other with a combined capacity of more than 1,320- gallons? c. 1s secondary containment provided for Title III Section 313 Superfund Amendments and Reauthorization Act (SARA) water priority chemicals"? d. Is secondary containment provided for hazardous substances" designated in 40 CFR §116? e. Are release valves on all secondary containment structures locked? 15) Hazardous Waste: a. is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility? b. Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste generated per month) of hazardous waste? c. is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste generated per month) of hazardous waste? If you answered yes to questions b. or c., please provide the following information: Type(s) of waste: How is material stored: Where is material stored: How many disposal shipments per year: Name of transport / disposal vendor: Vendor address: Footnotes to questions 14) c. & d. ❑ Yes ❑ No I@ NIA ❑ Yes ❑ No ® NIA ❑ Yes ❑ No ® NIA ❑ Yes ❑ No M NIA ❑ Yes ❑ No Up NIA ❑ Yes ® No ❑ N/A 17't tr�i;• +� a'I Cl Yes ® No ❑ NIA "Note that amounts below the 660-gallon (single) and 1,320-gallon (combined) bulk storage minimums require secondary containment. However, some exceptions may be made for de minimis amounts of certain substances, and/or other qualifiers, as described in the exemptions from reporting requirements of Title III SARA 313 in 40 CFR §372.38, "Note that amounts below the 660-gallon (single) and 1,320-gallon (combined) bulk storage minimums require secondary containment. However, some exceptions may be made for amounts less than the Reportable Quantities of the hazardous substances listed in 40 CFR §117.3. Page 4 of 7 5WU-NE-021309 Last revised 2113t2oo9 NCGNE0000 No Exposure Certification. 16) Other information: If you answer "Yes" to any of the following items, you might not be eligible for the no exposure exclusion. A more In-depth evaluation of the site circumstances may be required. a. Does your facility store used, recycled, or otherwise reclaimed pallets outside? ❑ Yes 9 No ❑ N/A b. Does your facility have coal piles on site? ❑ Yes V No ❑ NIA c. Does your facility store other fuel sources outside in piles, such as wood chips, ❑ Yes ® No ❑ NIA sawdust, etc.? d. Does your facility have air emissions associated with its industrial activity (e.g., ❑ Yes &No ❑ NIA degreasing operations, plating, painting and metal finishing)? If so, describe the industrial activity: e. If you answered yes to d., are those emissions permitted by an Air Quality Permit? ❑ Yes ❑ No 10 N/A Please specify: f. Please list any other environmental program permits (federal, state, etc.) not specified earlier in this application (such as Hazardous Waste Permits, etc.): Permit: Program: Permit: Program: Permit: Program: Permit: Program: Permit: Program: Permit: Program: Permit: Program: Page 5 of 7 SWU-NE-021309 Last revised 2/13/2009 NCGNE0000 No Exposure Certification 17) Certification: I certify under penalty of law that I have read and understand the eligibility requirements for claiming a condition of "no exposure" and'obtaining an exclusion from NPDES stormwater permitting. certify under penalty of law that there are no discharges of stormwater contaminated by exposure to industrial activities or materials from the industrial facility or site identified in this document (except as allowed under 40 CFR 122.26(g)(2)). I understand that I am obligated to submit a no exposure certification form once every five QLyears to the North Carolina Division of Water Ouality and, if requested, to the operator of the local municipal separate storm sewer system (MS4) into which the facility discharges (where applicable). I understand that I must allow the North Carolina Division of Water Quality, or MS4 operator where the discharge is into the local MS4, to perform inspections to confirm the condition of no exposure and to make such inspection reports publicly available upon request. In the event that the site no longer qualifies for a No Exposure Exclusion, I understand that I must obtain coverage under an NPDES permit prior to any point source discharge of stormwater from the facility, Additionally, I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is to the best of my knowledge and belief true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations - I certify that 1 am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete, and accurate. Printed a of Person Signing_ �--V�n �_7 Title: Na2- (Signature of Applicant) (Date Signed) Please note: This application for the No Exposure Exclusion is subject to approval by the NCDENR Regional Office prior to issuance. The Regional Office may inspect your facility for compliance with no exposure conditions prior to that approval. The Regional Office may also inspect your facility at any time in the future for compliance with the No Exposure Exclusion. North Carolina General Statute 143-215.6 B(I) provides that: Any person who knowingly makes any false statement, representation, or certification in any application, record, report, plan, or other document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the [Environmental Management] Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000). There is currently no fee for a No Exposure Exclusion. Page 6 of 7 SWtl-NE-021309 Last revised 211312009 NCGNE0000 No Exposure Certification Final Checklist This application should include the following items: ig This completed application and all supporting documentation. W A map with the location of the facility clearly marked. If this is a renewal, indicated current NCGNE number in Question 7. It the site currently has an NPDES Stormwater Permit, be sure to indicate the perrnit number in Question 8. Mail the entire package to: Stormwater Permitting Unit Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Note The submission of this document does not guarantee the issuance of a No Exposure Exclusion. For questions, please contact the DWO Regional Office for your area. DWQ Regional Office Contact Information_ Asheville Office ...... (828) 296-4500 Fayetteville Office ... (910) 433-3300 Mooresville Office ... (704) 663-1699 Raleigh Office ........ (919) 791-4200 Washington Office ...(252) 946-6481 Wilmington Office ... (910) 796-7215 Winston-Salem ...... (336) 771-5000 Central Office .........(919) 807-6300 Page 7 of 7 .... . .• . SWU-NE-021309 last revised 211W009 TerraServer Image Courtesy of the S S Page 1 of 1 Is Send To Printer Back To TerraServer Change to 11x17 Print Size Show Grid Lines Change to Landscape MUSGS 4 km SW of Black Mountain North Carolina United States 05 Apr 1999 sf 00 -� w rti ►,`+ t R +k LIL 4-1 41 rift 4. �. _ - � • +w• � COY Yam...--' � y'"'..i�--� a� � (/r�_I/�{\� r..���yyyJJh� � 'w t] ., a .. � • �� a i ` i`j e J 'lam .. .Yd o` -- `loom v. 'looyd Image courtesy of the U.S. Geological Survey © 2004 Microsoft Corporation. Terms of Use Privacy Statement http://terraserver-usa.com/Printlmage.aspx?T=I&S=l O&Z=1 7&X=l 884&Y=19705&W=1 &qs=905+Old... 3/16/2009 I,atilhide and Longitude of a Point Page 1 of 2 IiTouchMap.com Al Mobile and Donktop Maps Home » Latitude and Longitude of a Point Maps I Country - State I Places I Google Earth I Cities i Earthgt To find the latitude and longitude of a point Click on the map, Drag the marker, or enter the... a Address: 905 Old.US=Highway 70 West Black Mountain NC Go Map Center: Land Plat Size - Street View - Google Earth 3D - Area Photographs Try out the Google Earth Plug-in. Google Earth gives you a 3D look of the area around the center of the mal which is usually your last click point, and includes latitude, longitude and elevation information. Ads by Google GPS World World Map Coordinates GPS Map Prices GPS Updates Latitude and Longitude of a Point �> `PC " 4a c Qa fi a� 2474 y1ol Rd �k Rd a 2472 11 ca`ateC5 \S5 1'Z'yo Note: Right click on a blue marker to remove it Clear/Reset All Markers Center Red Marker Get the Latitude and Longitude of a Point Show Point from Latitude and Longitude Use this if you know the latitude and longitude coordina- a point and want to see where on the map the point is. Use: + for N Lat or E Long - for S Lat or W Long. Example: +40.689060-74.044636 Note: Your entry should not have any embedded space http://itouchmap.com/latlong.htmi 3/16/2009 Latitude and Longitude of a Point Page 2 of 2 When you click on the map, move the marker or enter an address the latitude and longitude coordinates of the point are inserted in the boxes below. Latitude: 35.60677180923596 Longitude: 82.36033916473388 Degrees Minutes Seconds Latitude: ; 35 .36 24.3786 Longitude: -82 .21 37.2198 Decimal Deg. Latitude: Decimal Deg. Longitude: Show Point Example: +34 40 50.12 for 34N 40' 50.12" Degrees Minutes Seconds Latitude: Longitude: Show Point Q TouchMap.t.om 2008 http:l/itouchmap.com/latlong.html 3/16/2009 Compliance Inspection Report Permit: NCG030529 Effective: 11/01/07 Expiration: 10/31/12 Owner: Tyco Valves & Controls SOC: Effective: Expiration: Facility: Tyco Valves and Controls County: Buncombe 953 Old US Highway 70 Region: Asheville Black Mountain NC 28711 Contact Person: Gene Logan Title: Phone: 828-669-3753 Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Representative(s): Related Permits: Certification: Phone: Inspection Date: 04116/2009 Entry Time: 03:15 PM Exit Time: 04:00 PM Primary Inspector: Susan A Wilson Phone: 828-294-4500 Secondary Inspector(s): Reason for Inspection: Other Inspection Type: Stormwater Permit Inspection Type: Metal Fabrication Stormwater Discharge COC Facility Status: ❑ Compliant Q Not Compliant Question Areas: ■ Other (See attachment summary) Page: 1 or Permit: NCG030529 Owner - Facility: Tyco Valves & Controls Inspection Date: 04/16/2009 Inspection Type: Stormwater Reason for Visit: Other Inspection Summary: See comments under questions as to why site visit was conducted (site visit 4/16/2009), Told Mr. Logan they could manually clear out the debris that was fallen and some of the overhanging trees that may fall into the creek. Also told him to call MSD regarding plugging the manhole to prevent any flood waters going into it. Also told him he could call DOT to see if they would clear out culvert. Called him back 4/23/2009 - he had called MSD and they came to plug nearby manhole. Told him any debris removal must be manual only - no heavy equipment in creek, etc. Other Yes No NA NE Comment: Gene Logan with Tyco wanted assistance with debris in creek adjacent to property (that runs from culvert at old Hwy. 70 and stormwater outfall on their site). Also an MSD manhole on -site - Tyco was worried their creek was so clogged up that manhole would flood with heavy rains. Wanted to clean out debris from creek. Page: 2 ti' .?7(1 611b' -r! J"O s [err c�'�I V c? M=TrrI� oo,+r La CA r r.. i a t, tt 40 ((ram. V• � / fi /.� tom, Si v �f 61 l el p ♦JF €€.. �r # t Calm . 0 Subject: Call From: Chuck Cranford <Chuck.Cranford@ncmail. net> Date: Wed, 08 Apr 2009 12:30:01 -0400 To: Susan A Wilson <Susan.A.WIIson@ncmai1.net> Susan -- � Mr. Gene Logan 828-669-3753 Tyco Corp. (Black Mountain) needs some advice about a stream and culvert on their property with accumulated sediment. He wishes to remove it because of flooding concerns. Could you please discuss that with him. 1 told him not to do anything at this point. Chuck Cranford - Chuck-Cranfordencmail.net North Carolina Dept`.• of Environment and Wa-tural Resources Asheville Regional Office Division of Water Quality - Surface Water Protection Section 2090 U.S. 70 Highway swannanoa, NC 2877E Tel: 828-296-4500 Fax: 828-299--7043 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. Chuck Cranford <ChLick, Cranford a,nctrtail.net> `'C DE\R - Asheville Regional Office a+ Div. of Water Quality - Surface Water Protection 0 If %•� /�Gr'lJ� i1 -� T�I N C� / rrt' Ors �t� RAPPA�` �� �re•'tc_- Cu�� � G+� �Y Crt�X auk I of] 4/9/2009 8:35 AM W 47 4. M-r� . PrrAO C LR �� r n ,, W` o F tp �r D Q"D. - PLIS Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.B. Dircctor Division of Water Quality March 29, 2007 Mr. Gene Logan Tyco Valves and Controls 953 Old US Highway 70 Black Mountain, NC 28711 Subject: General Permit No. NCG030000 Tyco Valves and Controls COC NCG030529 Buncombe County Dear Mr. Logan. The Division of Water Quality's Stormwater Permitting Unit received your request for Representative Outfall Status on March 29, 2007. Your request to sample outfalls 001, 002, and 008 as representative of your eight outfalls (001, 002, 003, 004, 005, 006, 007, and 008) has been granted. If you have any questions concerning this issue, please contact me at telephone number (919) 733-5083 ext. 376. Sincerely, elly Jo on Environmental Engineer cc: DWQ Asheville Regional Office, Laurie Moorhead 1 Central Files Stormwater Permitting Unit Files 7 D L-- / APR - 2 2007 WATER OUALIT`,' SECTION ASHEVII_LE REGIONAL OFFICE —, N"oy�`ItCatch d dZr Alrrlly North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone (919) 733-5083 Customer Service Internet: www.newaterguality-or¢ Location: 512 N. Salisbury St. Raleigh, NC 27604 Fax (919) 733-9612 1-877- 623-6748 An Equal Opportun4/Af3irmative Action Employer — 50% Recycled/10% Post Consumer Paper pF'ATF,q Michael F. Easley, Governor O� QG William G. Ross Jr., Secretary %g North Carolina Department of Environment and Natural Resources � r Alan W. Klimek, P.E. Director Division of Water Quality Asheville Reglonal-Off, ice SURFACE WATER PROTECTION { March 22, 2007 Mr. Gene Logan Tyco Valves & Controls 953 Old US Highway 70 Black Mountain, NC 28711 SUBJECT: Compliance Evaluation Inspection Tyco Valves & Controls Permit Number NCG030529 Buncombe County Dear Mr. Logan: Enclosed please find a copy of the Compliance Evaluation Inspection report from the inspection conducted on March 21, 2007. The facility at 953 Old US Highway 70 is Compliant with all terms and conditions of its general stormwater permit NCG030529. In following up on our discussion of seeking representative outfalf status from our Division Director, Mr. Alan Klimek, please see the summary for contact information. Also please refer to the summary for other recommendations for improved operations. appreciate your time and assistance during the site inspection and file review. Your close attention to the intent and requirements of this permit are reflected in the condition of the facility and its documentation of your efforts. If you should have any questions regarding your permit or compliance with its requirements, please feel free to contact me at 828/296-4664. Enclosure cc: Danny Smith — NPS ACO Unit ARO Files Central Files Sincerely, Laurie L. Moorhead Environmental Specialist NorthCaroli.na NaturallJ 2090 US Hwy 70, Swannanoa, NC 28778 828-296-4500 Fax 828-299-7043 Customer Service 877-623-6748 Permit: NCG030529 SOC: County: Buncombe Region: Asheville Compliance Inspection Report Effective:06104/04 Expiration: 08/31/07 Effective: Expiration: Contact Person: R W Batchelder Directions to Facility: Primary ORC: Certification: Secondary ORC(s): On -Site Representative(s): Owner: Tyco Valves and Controls Facility: Tyco Valves and Controls 953 Old US Highway 70 Black Mountain NC 28711 Phone: 828-669-5515 Phone: On -site representative Gene Logan Phone: 828-669-3753 Related Permits: Inspection Date: 03/21/2007 Entry Time: 10:30 AM Exit Time: 1 1:52 AM Primary Inspector: Laurie L Moorhead IV _�- �� M0C 3r��p-7 . Phone: 828-296-4500 cN,Ext.4664 Secondary Inspector(s): Reason for Inspection: Routine Inspection Type: Stormwater Permit Inspection Type: Metal Fabrication Stormwater [Discharge COG Facility Status: IN Compliant Q Not Compliant Question Areas: ® Storm Water (See attachment summary) Page: 1 W Permit: NGG030529 Owner - Facility: Tyco Valves and Controls Inspection Date: 0312112007 Inspection Type: stormwater Reason for Visit: Routine Inspection Summary: Gene Logan of Tyco Valves and Controls provided a site tour and all documents for review. The stormwater pollution prevention plan and the spill response plan were up to date as were all monitoring and training records. No vehicle maintenance is conducted on site. Upon review of the 8 outfalls and their analytical monitoring data, it is recommended that the facility consider requesting representative outfall status from the Division of Water Quality so that only the 3 outfalls which might ever reflect contamination are monitored analytically (#001. #002, and #008). Representative outfall status must be approved of the Division Director, Mr. Alan Klimek, who may be contacted at the following address, - Alan Klimek Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 While the site is in compliance with all permit requirements, it is recommended that the curbing at the scrap metal concrete pad be fully connected with a manual valve installed to allow purposeful draining of uncontaminated rainwater. The inspector acknowledges that there are drip pans located under each lugger, but the potential for spills during the emptying of the drip pans exists and the open curbing allows spills 'and contamniated stormwater to leave the pad_ Monitoring of this area already is occurring but the addition of this best management practice would require keeping an eye on the quality of rainwater exiting the area. The stormwater management plan would also need to be updated to reflect this modification. Site conditions and all paperwork reflect close attention to the intent and requirements of this permit. Mr.Logan is to be commended for such a conscientious effort. Page: 2 Permit: NCGO30529 Owner - Facility: Tyco Valves and Controls Inspection Date: 03/2112007 Inspection Type: Stormwater Reason for Visit: Routine Stormwater Pollution Prevention Plan Yes No NA NE Does the site have a Stormwater Pollution Prevention Plan? d ❑ ❑ ❑ # Does the Plan include a General Location (USGS) map? ■ ❑ ❑ ❑ # Does the Plan include a `Narrative Description of Practices"? 13 ❑ ❑ ❑ # Does the Plan include a detailed site map including outfall locations and drainage areas? ® ❑ ❑ ❑ # Does the Plan include a list of significant spills occurring during the past 3 years? ■ ❑ Q ❑ # Has the facility evaluated feasible alternatives to current practices? ❑ ❑ ❑ ■ # Does the facility provide all necessary secondary containment? ■ ❑ ❑ ❑ # Does the Plan include a BMP summary? ®❑ ❑ Cl # Does the Plan include a Spill Prevention and Response Plan (SPRP)? ® ❑ ❑ Cl # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? ®❑ Cl ❑ # Does the facility provide and document Employee Training? is ❑ ❑ # Does the Plan include a list of Responsible Party(s)? 0 ❑ ❑ # Is the Plan reviewed and updated annually? ❑ ❑ ❑ # Does the Plan include a Stormwater Facility Inspection Program? ■ Cl Cl ❑ Has the Stormwater Pollution Prevention Plan been implemented? ® ❑ ❑ ❑ Comment: Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring semi-annually? ® ❑ ❑ ❑ Comment: Anal ttcal Mor1ltOCln -_..__.Y._.._........_.._._.....__�...__ ...._.. - Yes No NA NE Has the facility conducted its Analytical monitoring? ■ ❑ ❑ Cl # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ ® Q Comment: No vehicle maintenance is conducted at this site. Permit and Outfalls Yes No NA NE # Is a copy of the Permit and the Certificate of Coverage available at the site? ®❑ ❑ 0 # Were all outfalls observed during the inspection? 93000 # If the facility has representative outfall status, is it properly documented by the Division? Q ❑ ■ ❑ # Has the facility evaluated all illicit (non stormwateo discharges? ® ❑ ❑ ❑ Comment: The inspector recommends that the facility seek representative outfall status and monitor only outfalls 001, 002, and 008. Page: 3 Michael F. Easley, Govcmor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.E. Director Division of Water Quality March 31, 2006 Tyco Valves and Controls 953 Old U.S Highway 70 Black Montain, NC 28711 Subject: General Stormwater Permit Inspections Tyco Valves and Controls Permit No. NCG030529 Buncombe County Dear Sir or Madam: Your facility holds a general permit from the North Carolina Division of Water Quality to discharge stormwater associated with industrial activities performed at your facility. Please be advised that the Asheville Regional Office will be performing NPDES stormwater inspections sometime in the near future. If this office has not previously inspected your facility, you should be prepared to demonstrate compliance with all terms and conditions included in the permit. Specifically, we will be evaluating the following: your stormwater pollution prevention plan, stormwater outfall locations, qualitative and analytical monitoring data and any other activities required by your permit. Please note that any data reported to the State must be analyzed by a facility that has a North Carolina laboratory certification, either as a full laboratory or as a facility certified to perform on -site Field testing. If you have any questions regarding the generation of your facility's data, please feel free to call Gary 1=rancies at (828) 296-4677. Copies of the general permits and accompanying documents can be accessed from the following webpage: http:/hvt-t,tv.nciv(ttergtiality.org/.Su/Forn2,s_Docun?ents.ht)i?#storinu1aterGP. If you have any questions, please contact me in the Asheville Regional Office at (828) 296-4500. Sincerely, Qxy_� 0.All-4-11 Roy Davis Environmental Engineer cc: NPS Compliance & Assistance Oversight Unit SWP-Central Files ARO Files NorthCarolina Aaturall� North Carolina Division of Water Quality 2090 US, Hwy 70 Swannanoa, NC 28778 Phone (828) 296-4500 Fax (829) 299-7043 Internet: htip:/hgm.nrwalerquality.org1 An Equai Opportunity/Affirmative Action Employer Aole. elke � 14Af to OLD! US H W T 10 FIREPLUG I %I I 7AIAL- GRASS J jr FLAW I FIREMAN %pq�r:'' SIJRMLORAIN RISER �" (ASPHALT <BENEAI SCpRM DRAIN OFFICES LLJ G A� 1 ❑Lll US HWY 70 SEVER MANHOLE GRASS t 1 F'LOw Y W L" GRASS N. of N D T E i Un-named creek +' Flows into the , f � � CJML ��j Swannanoa Rive which Flows intos'�',`� I the French Bro d River Basin, NC 303(d) lists the Swannanoa River �of,Aj Sod„I�s as Imfired biological integrity. CONCRE',- BRUSH ldi� CONCRETE SLAB� HAZVA,iTe r SLAB (CURRE� GRASS +F ;PAS; � - STORAGE y lA U; CQNTAINMEfJt x 1 ` o ANCRE Tr SLAB C ? wr rs w war GRASS Tyca VALVES 6 CONTROLS CRASH ' MANUFACTURING BUILDING l \ "7MPACCOR 5 FACILITY DIAGRAM -DRAINAGE 953 OLD US 70, BLACK MOUNTAIN, NC 28711 A TEL, (828) 669-5515 SEWER FAX, (828) 669-4117 OUTFALL _ MANHOLE �4 GRAS GRAVEL0c- _0 ® DRAWING SCALE V = 55'-0' "NCRECE RIP -RAP, S}p SEWER CD KHEAQ �� FLOW STONE -� 0000. MANWOLE CIREEK CREEK IV MAIN SITE 7 5 ACRES 49 PERCENT I (PERVIOUS AREA REVISIONS REV DESCRIPTION A ADDED NOTE & DRAWING SCALE