Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
NCG030516_MONITORING INFO_20190102
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V to DOC TYPE ❑ HISTORICAL FILE C�, MONITORING REPORTS DOC DATE ❑ „ apicl YYYYM M DD SURTRONICS, INC. 4001 Beryl Rd. Raleigh, NC 27606 (919)834-8027 12/21/18 N e c, o 30,5-1,6 Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh NC 27699-1617 Subject: Permittee-Stormwater Data Fall 2018 Sample— 10/11/18 To Whom It May Concern: P_O. Box 33459 Raleigh, NC 27636-3459 Fax (919)828-9972 Two copies of one set of data accompany this letter based on sampling of a Fall 2018 event. The events occurred on 10/11/18. The data includes: Two (2) copies of one set of qualitative data for each of three sampling points are enclosed. If you have any questions please call me at (919)834-8027 Ext 235. CC: Surtronics File Enclosures: Storm Data 4*2412VTT t6 I it V Sincerely yours Lee Br haw General Manager R&CPI vE1) JqQ 2 N 2019 CeN7S D>NR L E FfL� C-r/o S �i�-� NCDENR storm' water Discharge Dutfall (SDQ) Qualitative Monitoring Report For guidance on filling out this form, please visit. http://Vortal,ncdenr.org/web/wq/ws/su/npdessw#tab__-4 Permit No.: N/C/_/ /�/�%_/�_/ or Certificate of Coverage No.: 1V Facility Name: nTiz,4 1n County: _� L. Phone No. `11 If c/ - I'd Z. Inspector: J4"y R.U& Date of Inspection: A —1 r l ' Time of Inspection: I Total Event Precipitation (inches): 6 r Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred- A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours i prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee { obtains approval from the local DWQ Regional Office. C By this signature, I certify tl}pt this report is accurate and complete to the best"of my knowledge: of Perhiltee or Designee) A2 -2r-T Z6It Pagel of 2 SWU-242, Last modified i0/2512012 1. Outfall Description: Outfall No, i-- 2- 3- - � Receiving Stream: e� Describe the industrial activi cture (pipe, ditch, etc.) Ao,�Q ! /or Q ran h that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 196 *A 3. Odor: Describe any distinct odors that the discharge may have (i.e.; smells strongly of oil, weak chlorine odor, etc.): AAA,- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: b2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 6) 3 4 S 7. Is there any foam in the stormwater discharge? Yes S. Is there an oil sheen in the stormwater discharge? Yes Flo 9. Is there evidence of erosion or deposition at the outfall? Yes Na 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG03.6_ 6 O_ FACILITY NAME rbf1LC COUNTY U)Ok.G PERSON COLLE TING SAM A CS LABORATORY A LES Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR alge SAMPLE PERIOD ❑ Jan -June July -Dec or 0 Monthly'. month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA []Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No dischorge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks ===> _ 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L Ojvif `] R6f0.6 b •Oo2. „d /o 1)-it a .3 6 D . oo'a- p - bolt AJ /D-lif Q.3i /1b,w L .od"L b.oa� a� of r 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall, 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1h012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TrO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) 614 sr2y Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, B.DL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. iri mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part g: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' OutfaN No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, lnches3 Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ No ❑ REGIONAL OFFICE CONTACT NAMI -. Mail an original and one copy of this DMA' including all "No Discharge" reports, within 30 days of receipt of the lab results or at end of monitorina Period in the case of "No Discharge" reports) to: Division of Water Quality Attm DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete, I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) IZ--Z� (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 National Oceanic & Atmospheric Administration National Environmental Satellite, Data, and Information Service Current Location: Elev: 428 Pt. Lat: 35.8116' N Lon:-78.7140' W Station: RALEIGH 3.2 WSW, NC US USINCWK0181 Rta:UIU Ul %A111tdLV1UY1k;d1 %JUbt:1VdUV11b These data are quality controlled and may not be Identical to the original observations. Generated on 12121/2018 151 Patton Avenue Asheville, North Carolina 28801 Observation Time Temperature: Unknown Observation Time Precipitation: Unknown Temperature F Precipitation Eva oration Soil Tent rature F y e a r M ° n t h D a y 24 Hrs. Ending at Observation Time At 0 b Is e r v tSnow, i a n 24 Hour Amounts Ending at Observation Time At Obs. Time 24 Hour Wind Movement (mil Amount of Eva in p I 4 in. Depth 8 in. Depth Max. Min. Rain, Melted Eta, (in) F I a 9 Snow, Ice Pellets, Hail (in) F I a g Snow, Ice Pellets, Hail, Ice on Ground (in) Ground Cover (see') Max. Min, Ground Cover (see'j Max. Min. 2018 10 01 2018 10 02 2018 10 03 2018 10 04 2018 10 05 2018 10 06 2018 10 07 2018 10 08 2018 10 09 — I 2018 10 10 0.18 2018 10 11 0.13 2018 10 12 3.06 2018 10 13 2018 10 14 2018 10 15 2018 10 16 2018 10 17 2018 10 18 2018 10 19 2018 10 20 2018 10 21 — 2018 10 22 2018 10 23 2018 10 24 2018 10 25 2018 10 26 2018 10 27 2018 10 28 2018 10 29 2018 10 30 2018 10 31 Summary3.37 D.0 Empty, or blank, cells indicate that a data observation was not reported. 'Ground Cover: 1=.Grass; 2=Fallow; 3=Bare Ground; 4=Brome grass; 5=Sod; 6=Straw mulch; 7=Grass muck; 8=Bare muck; O=Unknown "s" This data value failed one of NCDC's quality control tests. "T" values in the Precipitation or Snow category above indicate a "trace" value was recorded. "A" values in the Precipitation Flag or the Snow Flag column indicate a multiday total, accumulated since last measurement, is being used. acmnalytical www.pacefabs.00m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )875-9092 ANALYTICAL RESULTS Project: Wastewater 10111 Pace Project No.: 92403250 Sample: 10/11/2018 Lab ID: 92403250001 Collected: 10111/18 13:00 Received: 10/12/18 11:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mglL 4.8 1 10/26/18 04:31 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Aldrin ND uglL 0.045 1 10/1611811:30 10/18/18 10:59 309-00-2 alpha-BHC ND uglL 0.045 1 10/16/18 11:30 10/18/18 10:59 319-84-6 beta-BHC ND ug/L 0.045 1 10/16/18 11:30 10118/1810:59 319-85-7 delta-BHC ND ug1L 0.045 1 10/16/18 11:30 10118/1810:59 319-86-8 gamma-BHC (Lindane) ND ug/L 0.045 1 10/16/18 11:30 10/18/18 10:59 58-89-9 Chlordane (Technical) ND ug/L 0.18 1 10/16/18 11:30 10/18/18 10:59 57-74-9 4,4'-DDD ND ug/L 0.045 1 1011611811:30 10/1811810:59 72-54-8 4,4'-DDE ND ug/L 0.045 1 10116/1811:30 10/1811810:59 72-55-9 4,4'-DDT ND ug/L 0.045 1 10116/1811:30 10/1811810:59 50-29-3 Dieldrin ND ug& 0.045 1 10116/1811:30 10/18/1810:59 60-57-1 Endosulfan I ND ug/L 0.045 1 10/16/18 11:30 10/18/18 10!59 959-98-8 Endosulfan II ND ug1L 0.045 1 10/16/18 11:30 10/18/18 10:59 33213-65-9 Endosulfan sulfate ND ug/L 0.045 1 10/16/18 11:30 10/18/18 10:59 1031-07-8 Endrin ND ug/L 0.045 1 10/16/18 11:30 10118/1810:59 72-20-8 Endrin aldehyde ND uglL 0,045 1 10/16/18 11:30 10/18/18 10:59 7421-93-4 Endrin ketone ND ug1L 0,045 1 10/16/18 11:30 10/18/18 10:59 53494-70-5 Heptachlor ND ug/L 0.045 1 10/1611811:30 10118/1810:59 76-44-8 Heptachlor epoxide ND ug1L 0.045 1 10/16/18 11:30 10/18/18 10:59 1024-57-3 Hexachlorobenzene ND ug/L 0.045 1 10/16/18 11:30 10/18/18 10:59 118-74-1 Methoxychlor ND uglL 0.14 1 10/1611811:30 10/18/18 10:59 72-43-5 Mirex ND ug1L 0.14 1 10/1611811:30 10/18/18 10:59 2385-85-5 Toxaphene ND uglL 0,18 1 10/1611811:30 10/18/18 10:59 8001-35-2 Surrogates Tetra ch loro-m-xylene (S) 83 % 20-130 1 10/16/18 11:30 10/18/18 10:59 877-09-8 Decachlorobiphenyl (S) 48 % 20-130 1 10/16/18 11:30 10/18/18 10:59 2051-24-3 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C PC13-1016 (Aroclor 1016) ND ug1L 0.42 1 10/16/18 11:30 10/18/18 14:30 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.42 1 10/16/18 11:30 10/18/18 1430 11104-28-2 PCB-1232 (Aroclor 4232) ND ug/L 0.42 1 10/16/18 11:30 10/18/18 14:30 11141-16-5 PCB-1242 (Aroclor 1242) ND uglL 0.42 1 10/16/18 11:30 10/18/18 14730 53469-21-9 PCB-1248 (Aroclor 1248) ND ug1L 0,42 1 10/16/18 11:30 10118/18 14:30 12672-29-6 PC6-1254 (Aroclor 1254) ND uglL 0,42 1 10/16/18 11:30 10/18/18 14:30 11097-69-1 PCB-1260 (Aroclor 1260) ND uglL 0.42 1 10/16/18 11:30 10/18/18 14:30 11096-82-5 Surrogates Decachlorobiphenyl (S) 44 % 10-132 1 10/16/18 11:30 10/18/18 14:30 2051-24-3 8270 RVE Analytical Method: EPA 8270D Preparation Method: EPA 3510C Acenaphthene ND uglL 10.0 1 10/1811814:56 10/20/1811:12 83-32-9 Acenaphthylene ND ug/L 10.0 1 10118/1814:56 10120/1811:12 208-96-8 Aniline ND ug/L 10.0 1 10118/1814:56 10/2011811:12 62-53-3 L2 Anthracene ND ug1L 10.0 1 10118/1814:56 10/2011811:12 120-12-7 Benzo(a)anthracene ND ug/L 10.0 1 10M8/1814:56 10/2011811:12 56-55-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/2018 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 29 aceaAnalytical www.pacetah3.mr+� Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wastewater 10111 Pace Project No.: 92403250 Sample: 10/11/2018 Parameters Lab ID: 92403250001 Collected: 10/11/18 13:00 Results Units Report Limit DF Received: 10/12/18 11:20 Matrix: Water Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 82606 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 10/18/18 16:15 460-00-4 1,2-Dichloroethene-d4 (S) 103 % 70-130 1 10/18/18 16:15 17060-07-0 Toluene-d8 (S) 104 % 70-130 1 10/18/18 16:15 2037-26-5 2540D Total Suspended Solids Analytical Method: SM. 2540D-2011 Total Suspended Solids 40.0 mg1L 5.0 1 10/15/18 19:41 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/2018 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 29 r,�Arialytical CHAIN -OF -CUSTODY ! Analytical Request Document The Crl�uamdy Is a LEGAL ODCL)WENT, All ra%vard fieida m&LO be onlzpl Aod otFffb!iy Soudan A Soction la suction C P�ye: W Requiffld MW irdrrtvlion_ Rsgtrtred Pmjoa trEmrrpti M: tmoico Ir4armoderr compaw sLutrontus f r- Repon Ta: ,BRIE$ Blue AMM7"T Natalie Dion dmns 4001 Beryl Raid Copy To. CaT"MNemo:. Surbunics REGULATORY AGENCY - Raleigh. NC 276W Addr9s& 4001 Biry1 Rd. Ralefgh, NC 27606 F NPDES T F UST r- GROUND RCM WATER l` DRINKiNG WATER r- OTHER Eme1 To: ]blue®su. bU.iL carat Puralme Oruff No.: nr was Phn—: 919711%422 F— D198289972 pmjoa uer ro: vq=ew-adsr rlc;ea R: Sitri LocaUon STATE." e Requu!W Duo D*WrAT: Rape Number- Pon PooNrC ROgtwl'ted AradysEs fii3tered (YRN " on D VaBd hlabtl Codes x RWmk.d Ckffl "k—d- MAMW QQM s COLLECTED Prowrmf/1Bs `s aarMCWAaa Orr S L� z PRODUCT P q 9TMr ET16R7NB V to � 0. in 6! SAMPLE ID �, m (A-Z, 0.9l,a Sn" IDS MUST BE UNIQUE AR 07HER W- 0r T9 O ul O W (� a a f- O 00 � C� t3 F � ft 25 IL w O �%� '4' L� .� -�7 L.• a O C,) Q N H [n V! <D DATE 11ME t�rE rLl�[}: x r x sO0 z z "r U CL Paco Pr '9C! Na1 L8b Lb. 1 10111/2D18 WI" iownins too 12 7 1 5 1 1 9 2 2 2 1 1 2 1 1 2 3 4 r10 i ADDITIONALCOUII'EIM REUMOUtstwo IYY I "nuATMN T.:A1F TWE DATE TIRE AM SPLE James Rua 16112l1B l �BYIAFFLATIDN 'x..[ �- Zv n -Z � ACtlf'aDfTit7115 'v ` SAMKFER NAME AND SLGNAT URE u 6 1 •� S PFVTNamaofSWFLPR:.1Smes $ � SANFLER: DA '..IHraed r- Q • SIGNATURE of 1pl12118 a) N O CN N m CL -Unparlam we: By s1pL49 Nla ram Tau am wxcpd'y PoDes NET 30 day ptimeot mane rd av"M m Il- drpes of I-S96 per m.a ror Oar tffw a nnr pap Nleir 30 mye F-ALL-4-020ray.CS. 12-00- 007 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE No. NCG03 0 5 { (p FACILITY NAME S —1 ion C i n— COUNTY %.Jo..L C PERSON COLLf�TING SAMPLES _JPr1- - S BLW LABORATORY_ ace. Lab Cert. # Comments on sample collect on.or analysis: JUN 2 2 2018 DWR SECTic : Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR Zb l6' SAMPLE PERIOD Q Jan -June ❑ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow []Watersupply []SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. Date Sample. Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organlcss Benchmarks 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L i q. S L a •063 D• o Z /00 tjD ,A�rJeorG.3Q 4-zy-�r .11 I nti !� cs ova 0 �� sAP D a,,e d f `-k►.�.i - 6 - j �,C.2 . 7 It 0 a - b 6:) o � z, 4� (J a Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012 maiia5vIIICI 11 I„rari 11110 Me 3iormwaier eonutlon Nrevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan_" Name (Print name) 6 Evrafz Title (Print title) zI1z ZD/.q (Signature) (Dot ) Note: Results roust be reported in numerical format. Do not report. Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they' must be reported in the format, "<XX mg/L', where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B. Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall Na. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ==> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/2S/2012 Page 2 of 3 HCDEHR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: � w a - Permit No.: �l/S;/�/�/_/ _/�/_/_/ or Certificate of Coverage No.: bJ-C/-Q/,j/ Facility Name: S —4 rc c S Comity: UVa-k-e- Phone No. Inspector: ) ",5 LLu c Date cif Inspection: I— Zq I r Tune of Inspection: 4 — zq- i r-- Total Event Precipitation (inches): /. I I Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) �es ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event." or "measureuble storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify th4t this report is accurate and complete to the best of my knowledge: (Signature of Perintt*e or Designee) Page 1 of 2 SWO-242, last modified 10/'L i/2012 17 a6ed 1. Outfall Description: j� Outfall No. l Structure (pipe, ditch, etc.) P` vi+/t bc,� Receiving Stream: �a _u & �X Describe the industrial activities that occur within the outfall drainage area:.6" roan J( c�.k 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 'LJ a nk 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is dear and S is very cloudy: 61- Z 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids; 1 2) 3 4 5 6. Suspended Solids. Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 7. U. 9. 1 D 3 Is there any foam in the stormwater discharge? 4 5 Yes Is there an oil sheen in the stormwater discharge? Yes Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: taw clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWII-242, Last modified 10/25/2012 �� RMENR Stormwateir Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out thus form, please visit: httU://ourtal.ncdenr.urg/web��wsl5u/il.pdessw#tad -4 Permit No.: LV//�/_/_/_/_/_/_/ or Certificate of Coverage No.: Facility Name: S ,ar r61 L S County: WO-Lt. Phone No. 9 tom-- t; q' 3-5 --- ---- Inspector:-,JA�rA t Date ol' Inspection: Time oflnspection: 2-q- I C' 4- 2,4- 1 r / 6 qfA -- Total Event Precipitation (inches): I Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) 19 Yes ❑ No Please verify whether Quulitutive Monitoring must be performed during u "representative storm event" or "measureuble storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureabie storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "treasurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that Ois report is accurate and complete to the best of my knowledge: (Signattt4ofPern�tjee or Designee) Pagel of 2 SWII-242, Last modified io/ZS/2012 b 85ed 'I. Outfall Description: k t Ouffall No. 2- Structure (pipe, ditch, etc.) 1 � Qa'' Fj Receiving Stream: 1? n c 1�.ge," E t' Describe the industrial activities that occur within the outfali drainage area: _Gra, ,jd f 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: mil s�urc_n f 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): !1 n,Az 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5_ Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1. is no solids and 5 is the surface covered with floating solids: 1 62 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: � /2) 3 4 5 7, is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: list and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/depositions may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWI1-242, Last mndiRed 10/25/2012 WJDBTR Storrnwater Discharge Outfall (SDO) Qualitative Monitoring Report Fnrguidonce on filling out this form, please visit: http://portal�ncdenr.org/webf w{{/jwsjsu./n pdgsj yw#[ab-4 Vermit No.: Facility Name: S 4.xAr6n %L.S T=C,C. County: Wak-t.. Inspector: _,Pry" S]�LL-C Late of inspection: 4" 2 LL - f l* Time of Inspection: 4 — z i-i r / 'I`otal h.'vent Precipitation (inches)_ or Certificate of Coverage No.: ,/_./ Phone No. 9 h - 8; 41' � bZ1 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (Set: information below.) E Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storin event" or "measureahle storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureahle storm event." However, s0111e permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prier. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee ohtains approval from the local DWQ Regional Office. Hy this signature, I oNtify thatAhis report is accurate and complete to the best of my knowledge: (signature of PerniAtie or Designee) Page k of 2 WWII-242, UNL modified 10/25/2012 t, a6ed 1.. Outfall Description: �r�} Outfall No. Structure (pipe, ditch, etc. F-tvt) Dt I,I- `j Receiving Stream: d Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the�harge using basic colors (red, brown, blue, etc.)and tint. (;light, medium, dark) as descriptors: f /`G-ns pa.tN a 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _ Na -p- 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: V `2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: t D 3 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspendt:d solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 D 3 4 5 7. Is there any foam in the stormwater discharge? Yes V� R. Is there an oil sheen in the stormwater discharge? Yes /Rlp 9. Is there evidence of erosion or deposition at the outfall? Yews No 10. Other Obvious Indicators of Stormwater pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may he indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWIE-242, last modified 10/25/2012 e acmnalytical wwwpKelabs=M ANALYTICAL RESULTS Project: Stormwater 4/24 Pace Project No.: 92382184 Pace Anatytical Services, LLC 9800 KinceyAve. Suite too Huntersvilte, NC 28078 (704)875-9o92 Sample: Stormwater Parameters Lab ID: 92382184001 Results Units Collected: 04/24/18 10:45 Report Limit OF Received: 04/25/18 10:00 Matrix: Water Prepared Analyzed CAS No, Qual 8270 MSSV RVE Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene NO ug/L 10.0 1 04129/18 23:02 04/30/18 13:57 83-32-9 Acenaphthylene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 208-96-8 Aniline NO ug/L 10.0 1 04/213/18 23:02 04/30/18 13:57 62-53-3 Anthracene NO ug/L 10.0 1 04129/18 23:02 04/30/18 13:57 120-12-7 Senzo(a)anthracene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 56-55-3 Benzo(a)pyrene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 50-32-8 Benzo(b)fluoranthene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 205-99-2 Benzo(g,h,i)perylene NO uglL 10.0 1 04/29/18 23:02 04/30/18 13:57 191-24-2 Benzo(k)fluoranthene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 207-08-9 Benzoic Acid NO ug/L 50.0 1 04/29/18 23:02 04130/18 13:57 65-85-0 L2 Benzyl alcohol NO ug/L 20.0 1 04/29/18 23:02 04/30/18 13:57 100-51-6 4-Bromophenylphenyl ether NO ug/L 10.0 1 04/29/18 23:02 04130/18 13:57 101-55-3 Butylbenzylphtha late NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 85-68-7 4-Chloro-3-methylphenoi NO ug/L 20.0 1 04/29118 23:02 04/30/18 13:57 59-50-7 4-Chloroanitine NO ug/L 20.0 1 04/29/18 23:02 04/30/18 13:57 106-47-8 bis(2-Chloroethoxy)methane NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 111-91-1 bis(2-Chloroethyl) ether NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 111-44-4 2-Chloronaphthalene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 91-58-7 2-Chlorophenol NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 95-57-8 4-Chlorophenylphenyl ether NO ug1L 10.0 1 04/29/18 23:02 04/30/18 13:57 7005-72-3 Chrysene NO uglL 10.0 1 04/29/18 23:02 04/30/18 13:57 218-01-9 Dibenz(a,h)anthracene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 53-70-3 Dibenzofuran NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 132-64-9 1,2-Dichlorobenzene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 95-50-1 1,3-Dichlorobenzene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 541-73-1 1,4-Dichlorobenzene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 106-46-7 3,3'-Dichlorobenzidine NO ug/L 20.0 1 04/29/18 23:02 04/30/18 13:57 91-94-1 2,4-Dichlorophenol NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 120-83-2 Diethylphthalate NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 84-66-2 2,4-Dimethylphenol NO ug/L 10.0 1 04129/18 23:02 04/30/18 13:57 105-67-9 Dimethylphtha late NO ug/L 10.0 1 04129/18 23:02 04/30/18 13:57 131-11-3 Di-n-butylphthalate NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 84-74-2 4,6-Dinitro-2-methyl phenol NO ug/L 20.0 1 04/29/18 23:02 04/30/18 13:57 534-52-1 2,4-Dinitrophenol NO ug/L 50.0 1 04/29/18 23:02 04/30/18 13:57 51-28-5 2,4-Dinitrotoluene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 121-14-2 2,6-Dinitrotoluene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 605-20-2 Di-n-octylphthalate NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 117-84-0 bi5(2-Ethylhexyl)phthalate NO ug/L 6.0 1 04/29/18 23:02 04/30/18 13:57 117-81-7 Fluoranthene NO ug/L 10.0 1 04/29/18 23:02 04/30/16 13:57 206-44-0 Fluorene NO ug/L 10.0 1 04/29/18 23:02 04130/18 13:57 86-73-7 Hexachloro-1,3-butadiene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 87-68-3 Hexachloro benzene NO uglL 10.0 1 04/29/18 23:02 04/30/18 13:57 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 77-47-4 Hexachloroethane NO uglL 10.0 1 04/29/18 23:02 04/30/18 13:57 67-72-1 Indeno(1,2,3-cd)pyrene NO ug1L 10.0 1 04/29/18 23:02 04/30/18 13:57 193-39-5 Isophorone NO ug1L 10.0 1 04/29/18 23:02 04/30/18 13:57 78-59-1 1-Methyinaphthalene NO ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 90-12-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/08/2018 05:32 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 30 aoAnalytical www.pacelabsoom Project: Stormwater 4/24 Pace Project No.: 92382184 Sample: Storrnwater Parameters Pace Analytical Services, LLC 9800 Kincey Ave, Suite100 HuMersvd:e, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab ID: 92382184001 Collected: 04/24/18 10:45 Received: 04/25/18 10:00 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No, Qual 8270 MSSV RVE Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 2-Methylnaphthalene ND ug11- 10.0 1 04/29/18 23:02 04/30118 13:57 91-57-6 2-Methyl phenol(o-Cresol) ND ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 9548-7 3&4-Methylphenol(m&p Cresol) ND ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 15831-104 Naphthalene ND ug/L 10.0 1 04129/18 23:02 04/30/18 13:57 91-20-3 2-Nitroaniline ND ug/L 50.0 1 04129/18 23:02 04130/18 13757 88-74-4 3-Nitroaniline ND ug/L 50.0 1 04/29/18 23:02 04130/18 13:57 99-09-2 4-Nitroaniline ND ug/L 20.0 1 04/29/18 23:02 04/30/18 13:57 100-01-6 Nitrobenzene ND ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 98-95-3 2-Nitrophenol ND ug/L 10.0 1 04/29/18 23:02 04130/18 13757 88-75-5 4-Nitrophenol ND ug/t- 50.0 1 04/29/18 23:02 04130/18 13:57 100-02-7 N-Nitrosodimethylamine ND ug1L 10.0 1 04129/18 23:02 04/30/18 13:57 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 10.0 1 04129/18 23:02 04130/18 13:57 621-64-7 N-Nitrosodiphenylamine ND ug1L 10.0 1 04129/18 23:02 04/30/18 13:57 86-30-6 2,2'-Oxybis(1-chlorapropane) ND ug1L 10.0 1 04/29/18 23:02 04/30/18 13:57 108-60-1 Pentachlorophenol ND ug1L 25.0 1 04/29/18 23:02 04/30/18 13:57 87-86-5 Phenanthrene ND ug1L 10.0 1 04/29/18 23:02 04/30/18 13:57 85-01-8 Phenol ND ug1L 10.0 1 04/29/18 23:02 04/30/18 13:57 108-95-2 Pyrene ND ug1L 10.0 1 04/29/18 23:02 04/30/18 13:57 129-00-0 1,2,4-Trichiorobenzene ND ug/L 10.0 1 04129/18 23:02 04/3011813:57 120-82-1 2,4,5-Trichlorophenol ND ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 95-95-4 2,4,6-Trichlorophenol ND ug/L 10.0 1 04/29/18 23:02 04/30/18 13:57 88-06-2 Surrogates Nitrobenzene-d5 (S) 37 % 40-121 1 04/29/18 23:02 04/30/18 13:57 4165-60-0 1g,S2 2-Fluorobiphenyl (S) 38 % 45-139 1 04/29/18 23:02 04/30/18 13:57 321-60-8 S2 Terphenyl-d14 (S) 43 % 48-146 1 04/29/18 23:02 04/30/18 13:57 1718-51-0 S2 Phenol-d6 (S) 8 % 18-105 1 04/29/18 23:02 04/30/18 13:57 13127-88-3 S2 2-Fluorophenol (S) 1 % 13-118 1 04/29/18 23:02 04/30/18 13:57 367-12-4 S2 2,4,6-Tribromophenol (S) 5 % 31-170 1 04/29/18 23:02 04/30118 13:57 118-79-6 S2 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 0510711815:09 67-64-1 Benzene ND ug/L 5.0 1 0510711815:09 71-43-2 Bromobenzene ND ug/L 5.0 1 0510711815:09 108-86-1 Bromochloromethane ND ug/L 5.0 1 0510711815:09 74-97-5 Bromodichloromethane ND ug/L 5.0 1 0510711815:09 75-27-4 Bromoform ND ug/L 5.0 1 05/07/1815:09 75-25-2 Bromomethane ND ug/L 10.0 1 05107/1815:09 74-83-9 2-Butanone (MEK) ND ug/L 10.0 1 05/07/18 15:09 78-93-3 tent -Butyl Alcohol ND ug/L 100 1 05/07/18 15:09 75-65-0 n-Butylbenzene ND ug/L 5.0 1 05/07/1815:09 104-51-8 sec-Butylbenzene ND ug1L 5.0 1 05107/1815:09 135-98-8 tert-Butylbenzene ND ug/L 5.0 1 0510711815:09 98-06-6 Carbon tetrachloride ND ug1L 5.0 1 05/07/18 15:09 56-23-5 Chlorobenzene ND uglL 5.0 1 05107/1815:09 108-90-7 Chloroethane ND ug1L 10.0 1 05/0711815:09 75-00-3 Chloroform ND ug1L 5.0 1 05/0711815:09 67-66-3 Chloromethane ND ug1L 5.0 1 05/07/1815:09 74-87-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/08/2018 05:32 PM without the written consent of Pace Analytical Services, LLC, Page 6 of 30 ace Analytical www.pacelabs.com ANALYTICAL RESULTS Project: Stormwater 4124 Pace Project No.: 92382184 Pace Analytical Services, LLC 9800 Kinoey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Sample: Stormwater Parameters Lab ID: 92382184001 Collected: 04/24/18 10:45 Results Units Report Limit OF Received: 04/25/18 10:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 2-Chlorotoluene NO uglL 5.0 1 05/07/18 15:09 95-49-8 4-Chlorotoluene NO ug1L 5.0 1 05/0711815:09 106-43-4 1,2-Dibromo-3-chloropropane NO uglL 2.0 1 05/0711815:09 96-12-8 Dibromochloromethane NO uglL 5.0 1 05/07/18 15:09 124-48-1 1,2-Dibromoethane (EDB) NO uglL 5.0 1 05107118 15:09 106-93-4 Dibromomethane NO uglL 5.0 1 05/0711815:09 74-95-3 1,2-Dichlorobenzene NO ug1L 5.0 1 05/0711815:09 95-50-1 1,3-Dichlorobenzene NO ug1L 5.0 1 05/0711815:09 541-73-1 1,4-Dichlorobenzene NO ug1L 5.0 1 05/0711815:09 106-46-7 Dichlorodifluoromethane NO uglL 5.0 1 05/0711815:09 75-71-8 1,1-Dichloroethane NO uglL 5.0 1 0510711815:09 75-34-3 1,2-Dichloroethane NO uglL 5.0 1 0510711815:09 107-06-2 1,2-Dichloroethene (Total) NO uglL 5.0 1 05/07/18 15:09 540-59-0 1,1-Dichloroethene NO uglL 5.0 1 05107/1815:09 75-35-4 cis-1,2-Dichloroethene NO uglL 5.0 1 05107/1815:09 156-59-2 trans-1,2-Dichloroethene NO uglL 5.0 1 05/07/18 15:09 156-60-5 1,2-Dichloropropane NO uglL 5.0 1 05/07/18 15:09 78-87-5 1,3-Dichloropropane NO uglL 5.0 1 05107/1815:09 142-28-9 2,2-Dichloropropane NO uglL 5.0 1 05/07/18 15:09 594-20-7 1, 1 -Dichloropropene NO ugiL 5.0 1 05/07/18 15:09 563-58-6 cis- 1,3-Dichloropropene NO ug1L 5.0 1 05107/1815:09 10061-01-5 trans- l,3-Dichloropropene NO ug1L 5.0 1 0510711815:09 10061-02-6 Diisopropyl ether NO ug1L 5.0 1 05/07/18 15:09 108-20-3 Ethylbenzene NO ug1L 5.0 1 0510711815:09 100-41-4 Hexachloro-1,3-butadiene NO ug1L 5.0 1 05/07/18 15:09 87-68-3 2-Hexanone NO ug1L 10.0 1 0510711815:09 591-78-6 Isopropyl benzene (Cumene) NO ug1L 5.0 1 05/07/18 15:09 98-82-8 p-Isopropyltoluene NO ug1L 5.0 1 0510711815:09 99-87-6 Methylene Chloride NO ug1L 5.0 1 05/07/18 15:09 75-09-2 4-Methyl-2-pentanone (MIRK) NO ug1L 10.0 1 05/07/18 15:09 108-10-1 Methyl-terl-butyl ether NO ug1L 5.0 1 05/07/18 15:09 1634-04-4 Naphthalene NO ug1L 5.0 1 05107/1815:09 91-20-3 n-Propylbenzene NO ug1L 5.0 1 05107/1815:09 103-65-1 Styrene NO ug1L 5.0 1 05107/1815:09 100-42-5 1,1,1,2-Tetrachloroethane NO ug1L 5.0 1 0510711815:09 630-20-5 1,1,2,2-Tetrachloroethane NO ug1L 5.0 1 05/07/18 15:09 79-34-5 Tetrachloroethene NO ug1L 5.0 1 05/07/18 15:09 127-18-4 Toluene NO ug1L 5.0 1 05/07/18 15:09 108-88-3 1,2,3-Trichlorobenzene NO ug1L 5.0 1 05/0711815:09 87-61-6 1,2,4-Trichlorobenzene NO ugiL 5.0 1 05/0711815:09 120-82-1 1,1,1-Trichloroethane NO ug1L 5.0 1 05/0711815:09 71-55-6 1,1,2-Trichloroethane NO ug1L 5.0 1 05/0711815:09 79-00-5 Trchloroethene NO uglL 5.0 1 05/0711815:09 79-01-6 Trichlorofluoromethane NO uglL 10.0 1 05/0711815:09 75-694 1,2,3-Tdchloropropane NO ugiL 5.0 1 05/0711815:09 96-18-4 1,2,4-Trimethylbenzene NO uglL 5.0 1 05/0711815:09 95-63-6 1,3,5-Trimethylbenzene NO uglL 5.0 1 05/0711815:09 108-67-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/08/2018 05:32 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 30 acmnalytical wwwpawlaba mm ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater 4124 Pace Project No.: 92382184 Sample: Stormwater Lab ID: 92382184001 Collected: 04/24/18 10:45 Received: 04/25/18 10:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Vinyl acetate ND ug1L 10.0 1 05107/18 15:09 108-05-4 Vinyl chloride NO ug1L 5.0 1 05107/18 15:09 75-01-4 m&p-Xytene ND ug1L 10.0 1 0510711815:09 179601-23-1 o-Xylene NO ug1L 5.0 1 0510711815:09 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/07/18 15:09 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 05/07/18 15:09 17060-07-0 Toluene-d8 (S) 104 % 70-130 1 05/07/18 15:09 2037-26-5 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 19.5 mg/L 4.2 1 04/30/18 18:53 Date: 05/08/2018 05:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuH, without the written consent of Pace Analytical services, L.LC. Page 8 of 30 CeAnalyAm •....+ asca..c. eex CHAIN -OF -CUSTODY ! Analytical Request Document The Chain-d-Cu510dY 13 a LEGAL ODCUMEN I. All rokrvBM GM3 rrwst be completed 00mrately. MEMO Addmgr 4001 Sc' rr -i t • ! .En%a Txr • .. • - - ,pa,�Zmg aw WATER V" JR r e ■r■■�■�■r■■©■■■■■■■ ■■■e■■■■■■■■■■■ e ■r■■■r■■■■■e��■■■■■ ■■■■e■■■■■■■■� e ■r■■��■■■■■e■■■■ EMOMMMIMMI r e sir ■�i■!i■■�i■�rriii■rii■ iiiriiirri Is e ■■■■r■�■■r■■■■■■.■■■■ r ■.■■.■...■ e ■.■...■........■.C. ■■■■■■■■.r■■. IMN4 r+ Nole: BY fi(Xlhyl tYs 1am1 Iw ar• arsap4np Psc1Y NET 30011p,rl lean 6 aplaalnp low, lu", d 1.5% per mardh tar any lwww M paw W Nn 30 day.. F-ALL-0-020rev. D8, 12-0d-2DO7 Semi-annual Sto_rmwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 1- C - 6 CERTIFICATE OF COVERAGE NO. NCG03 b 6 U 0 O�� 0 S/b FACILITYNAME S+•.l4rbA,cs J,11 COUNTY �vA K C PERSON COLLECTING SAMPLES �uE LABORATORY A/uLI ��1,J Lab Cert. # Comments on sample collection or analysis: SAMPLE COLLECTION YEAR Z6 0 SAMPLE PERIOD ❑ Jan -June July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water supply [:]SA ty,rr-�'',�jyi�.� — ❑Other AN 3 0 2q,, Part A: Stormwater Benchmarks and Monitoring Results DWR SECTION INFORWTION PRddkd§JN@ yuu PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period:2 Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids PH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss i Benchmarks ===s _ - 200 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 12-�-Ii D MQ IL- 6. 1VL 0.061 D A -K rJ UC 1.-Us t- 3 A ().001 0 •q-)S N � <l .3 I2-Q -ti1 I,ZS 1 M L (o • 3 It"I , v6-1- 0.141 S �-- 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 1!/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 .0— 1 ..;,2 f Q�IIILIC., LlIdl IHLva purdLt d saivent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Resuits roust be reported in numerical format. Do not report Below Detection limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note; if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera! Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Qutfali No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Semi-annual Stormwater Discharge „Monitoring Report for North Carolina Division of Water Quality General Permit No, NCG030000, Date submitted r- rg- le CERTIFICATE OF COVERAGE NO. N0003_U b Ca 6 FACILITY NAME _S",4rjb.11CS :Z7e%r_ COUNTY fnrA K C PERSON COLLECTING SAMPLES Lu G LABORATORY - Atw L Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR Z6 )7 SAMPLE PERIOD ❑ Jan -June July -Dec or []Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply []SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks =_=> _ - 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 IZ-�'li1 5b L o• 1.11- bL D "Os to �- ►18 n .t5 iSb ota IL 3 p•A 6.601 o•q-)� 1 3 l2-7 -Il f<, s t µ L.. (o.3 DIts �01- 0 �+� j- � 1 it 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 7 ... I F ] QS & I I LiV.] t.„QL II IW, 1JuI dLe d suivent management plan into the stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) G O'4 Title (Print title) / / (5 nature) 0 (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection limit, reporting limit, etc, in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement tier I, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' outfall N°" Rate sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches) Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> SS mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 2 of 3 e aceAnalytical www.pacclabs.com { SAMPLE ANALYTE COUNT Project: Stormwater 1218 Pace Project No.: 92367253 Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92367263001 STORMWATER EPA 1664E JMS 1 PAS I-C EPA 8081 PKS 24 PASI-C EPA 8082 PKS 8 PASI-C EPA 6010 SER 3 PASI-A EPA 8270 RES 74 PASI-C EPA 8260 GAW 71 PASI-C SM 2540D SLB 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 33 I19 eAnalytical wwwpacetabscom Project: Stormwater 1218 Pace Project No.: 92367253 Sample: STORMWATLR Parameters HEM, Oil and Grease Oil and Grease 8081 Organochlorine Pesticides Aldrin - alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4.4'-DDD 4.4'-DDE 4,4%13DT Dieldrin Endosulfan i Endosulfan it Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Arocar 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 6010 MET ICP Copper Lead Zinc Date: 01/03/2018 12:47 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab ID: 92367253001 Collected: 12/08/17 13:30 Received: 12/15117 12:40 Matrix: Water Results Units Report Limit DP Prepared Analyzed CAS No. Qua] Analytical Method: EPA 1664E NO mg1L 5.0 1 12129117 04:44 Analytical Method: EPA 8081 Preparation Method: EPA 3510 NO ug1L 0.050 1 12/19/17 09:00 12/19/17 22:01 309.00-2 H2 NO uglL 0,050 1 12/19/17 09:00 12/19/17 22:01 319-84-6 H2 NO uglL 0.050 1 12/19/17 09:00 12/19/17 22:01 319-85-7 H2 NO uglL 0.050 1 12/19/17 09:00 12/19/17 22:01 319-86.8 H2 NO uglL 0.050 1 12/19/17 09:00 12/19/17 22:01 58-89-9 H2 NO uglL 0.20 1 12/19/17 09:00 12/19/17 22:01 57-74-9 H2 NO uglL 0.050 1 12/19/17 09:00 12/19/17 22:01 72-54-8 H2 NO ug1L 0.050 1 12/19117 09:00 12/19/17 22-01 72-55-9 H2 ND ug1L 0.050 1 12/19/17 09:00 12/19117 22.01 50-29-3 H2 ND uglL 0.050 1 12119/17 09:00 12/19117 22:01 60.57.1 H2 NO uglL 0.D50 1 12119/17 09:00 12/19/17 22:01 959-98-8 H2 NO ug1L 0.050 1 12/19/17 09:00 12/19/17 22:01 33213-65-9 H2 NO ug1L 0.050 1 12/19/17 09:00 12/19/17 22:01 1031-07-8 H2 NO uglL 0.050 1 12/19/17 09:00 12/19/17 22:01 72-20-8 H2 NO ug1L 0.050 1 12/19/17 09:00 12/19/17 22:01 742143-4 H2 NO ug1L 0,050 1 12/19117 09:00 12/19117 22:01 53494-70-5 H2 NO ug1L 0.050 1 12/19/17 09:00 12119/17 22:01 76-44-8 H2 ND ug1L 0.050 1 12119117 09:00 12fl9117 22:01 1024-57-3 H2 NO ug t- 0.051) 1 12/19/17 09:00 12/19/17 22:01 11 B-74.1 H2 NO uglL 0.15 1 12/19/17 09:00 12/19/17 22:01 72.43-5 H2 NO uglL 0.15 1 12/19/11 09:00 12/19/17 22:01 2385-85-5 H2 NO uglL 0.20 1 12/19/17 09:00 12/19/17 22V 8001-35-2 H2 36 % 20-130 1 12/19/17 09:00 12/19/17 22:01 877-09-8 31 % 20-130 1 12119/17 09:00 12/19/17 22:01 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 NO ug1L 0.50 1 12/19/17 09:00 12/19/17 18:21 12874-11-2 NO ug1L 0.50 1 12/19/17 09:00 12/19/17 18:21 11104-28-2 ND ug/L 0.50 1 12/19/17 09:00 12/19/17 18:21 11141-16-5 NO ug1L 0.50 1 12/19/17 09:00 12/19/17 18:21 53469-21-9 ND ug1L 0.50 1 12/19/17 09:00 12/19/17 18:21 12672-29-6 NO ug1L 0.50 1 12 I9117 09:00 12/19/17 18:21 11097-69-1 NO ug1L 0.50 1 12 I9117 09:00 12/19117 18:21 11096-82-5 43 % 10-132 1 12119/17 09:00 12 I9117 18:21 2051-24-3 Analytical Method: EPA 6010 Preparation Method: EPA 3010A 112 ug/L 5.0 1 01/02/18 11:30 01/02/18 22:54 7440-50-8 21.9 ug1L 5.0 1 01/02/18 11:30 01/02/18 22:54 7439-92-1 475 uglL 10.0 1 01/02/18 11:30 01/02/18 22:54 7440-86-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Ana]ytical Services, LLC. Page 4 of 33 aceAnalytical wwwpecelabs com r ANALYTICAL RESULTS Project: Stormwater 12/8 Pace Project No.: 92367253 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: STORMWATER Parameters Lab ID: 92367253001 Results Units Collected: 12/08/17 13:30 Report Limit OF Received: 12/15/17 12:40 Matrix: Water Prepared Analyzed CAS No. Qual 8270 MSSV RVE Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA3510 Acenaphthene ND uglL 10.0 1 12/19/17 08:00 12/20/17 12:55 83-32-9 H2 Acenaphthylene NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 208-96.8 H2 Aniline ND uglL 10.0 1 12/19/17 08:00 12/20/17 12:55 62-53-3 H2 Anthracene NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 120-12-7 H2 Benzo(a)anthracene NO ug/L 10.0 1 12/19/17 08!00 12/20/17 12:55 56-55-3 H2 Benzo(a)pyrene NO ug/L 10,0 1 12/19/17 08:00 12/20/17 12:55 50-32-6 H2 Benzo(b)fluoranthene NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 205-99-2 H2 Benzo(g,h,i)perylene NO ug/L 10.0 1 12/19117 08:00 12/20/17 12:55 191-24.2 H2 Benzo(k)fluoranthene NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 207-08-9 H2 Benzoic Acid NO uglL 50.0 1 12/19/17 08:00 12/20/17 12:55 65-85-C H2 Benzyl alcohol NO ug/L 20.0 1 12/19/17 0&00 12/20/17 12:55 100-51-6 H2 4-8romophenylphenyl ether NO uglL 10.0 1 12/19/17 08:00 12/20/17 12:55 101-55-3 H2 Butylbenzylphthalate NO uglL 10.0 1 12/19/17 08:00 12/20/17 12:55 85-68-7 H2 4-Chloro-3-methylphenol NO ug/L 20.0 1 12/19/17 08:00 12/20/17 12:55 59-50-7 H2 4-Chlaroaniline NO ug/L 20.0 1 12/19117 08:00 12/20/17 12:55 106-47-8 H2 bis(2-Chloroethoxy)methane NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 111-91-1 H2 bis(2-Chloroethyl) ether NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 111-44-4 H2 2-Chloronaphthalene NO ug/L 10.0 1 12/19117 08:00 12/20/17 12:55 91-58-7 H2 2-Chlorophenol ND ug/L 10.0 1 12/19117 08:00 12/20/17 12:55 95-57-8 H2 4-Chlorophenylphenyl ether ND ug/L 10.0 1 12/19117 08:00 12/20/17 12:55 7005-72-3 H2 Chrysene ND ug/L 10.0 1 12/19117 08:00 12/20117 12:55 218-01.9 H2 Dibenz(a,h)anthracene ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 53-70-3 H2 Oibenzofuran ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 132-64-9 H2 1,2-Dichlorobenzene ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 95-50-1 H2 1,3-Dichlorobenzene ND ug/L 10.0 1 12/1911708:00 1212011712:55 541-73-1 H2 1,4-Dichlorobenzene NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 106-46-7 H2 3,3'-Dichlorobenzidine NO ug/L 20.0 1 12/19117 08:00 12/20/17 12:55 91-94-1 H2 2,4-Dichlorophenol NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 120-83.2 H2 Diethylphthalate NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 84-66-2 H2 2,4-Dimethylphenol ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 105-67.9 H2 Dimethylphtha late NO uglL 10.0 1 12/19/17 08:00 12/20/17 12:55 131-11-3 H2 Di-n-butyiphthalate NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 84-74.2 H2 4,6-Dinitro-2-methylphenol NO ug/L 20.0 1 12/19/17 08:00 12/20/17 12:55 534-52-1 H2 2,4-Dinitrophenol NO ugIL 50.0 1 12/19/17 08:00 12/20/17 12:55 51-28-5 H2 2,4-Dinitrotoluene NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 121-14-2 H2 2.6-Dinitrotoluene NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 606-20-2 H2 Di-n-octylphthalate NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 117-84-0 H2 bis(2-Ethylhexyl)phthalate NO ug/L 6.0 1 12/19/17 08:00 12/20/17 12:55 117-81-7 H2 Fluoranthene NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 206-44-0 H2 Fluorene ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 86-73-7 H2 Hexachloro-1,3-butadiene NO ug/L 10.0 1 1211911708:00 12/2011712:55 87-68-3 H2 Hexachlorobenzene NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 11 B-74-1 H2 Hexachlorocyclopentadiene ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 77-474 H2 Hexachloroethane NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 67-72-1 H2 Indeno(1,2,3-cd)pyrene NO uglL 10.0 1 12/19/17 08:00 12/20/17 12:55 193-39-5 H2 lsophorone NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 78-59-1 H2 1-Methyinaphthalene ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 90-12-C H2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/03/2018 12:47 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 33 aceAnalytrcal' _pacelabs.com ANALYTICAL RESULTS Project: Stormwater 12/8 Pace Project No.: 92367253 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hurltersville. NC 28078 (704)875-9092 Sample: STORMWATER Parameters Lab ID: 92367253001 Collected: 12108/17 13:30 Results Units Report Limit OF Received: 12/15/17 12:40 Matrix: Water Prepared Analyzed CAS No. Qual 8270 MSSV RVE Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 2-Methyl naphthalene NO ug/L 10.0 1 12/19/17 0&00 12/20/17 12:55 91-57-6 H2 2-Methylphenol(o-Cresol) ND ug/L 10.0 1 12/19/17 0&00 12/20/17 12:55 95-48-7 H2 3&4-Methylphenol(m&p Cresol) ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 15831-10-4 H2 Naphthalene ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 91-20-3 H2 2-Nitroaniline ND ug/L 50.0 1 12/19/17 08:00 12/20/17 12:55 88-74-4 H2 3-Nitroaniline NO ug/L 50.0 1 12/19/17 08:00 12/20/17 12:55 99-09-2 H2 4-Nitroaniline NO ug/L 20.0 1 12/19/17 08:00 12/20/17 12:55 100-01-6 H2 Nitrobenzene NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 98-95-3 H2 2-Nitrophenol NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 88-75-5 H2 4-Nitrophenol NO ug/L 50.0 1 12/19/17 08:00 12/20/17 12:55 100-02-7 H2 N-Nitrosodimethylamine NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 62-75-9 H2 N-Nitroso-di-n-propylamine NO ug/L 10.0 1 12/19/17 08!00 12/20/17 12:55 621-64-7 H2 N-Nitrosodiphenylamine NO ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 86-30-6 H2 2,2'-Oxybis(1-chloropropane) NO ug/L 10.0 1 12119/17 08:00 12/20/17 12:55 108-60-1 H2 Pentachlorophonol NO ug/L 25.0 1 12/19/17 08:00 12/20/17 12:55 87-66-5 H2 Phenanthrene NO ug1L 10.0 1 12/19/17 08:00 12/20/17 12:55 85-01-8 H2 Phenol ND ug1L 10.0 1 12/19/17 08:00 12/20/17 12:55 108-95-2 H2 Pyrene ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 129-00-0 H2 1,2,4-Trichlorobenzene ND uglL 10.0 1 1211911708:00 12/20/1712755 120-82-1 H2 2,4,5-Trichlorophenol ND uglL 10.0 1 12/19/17 08:00 12/20/17 12:55 95-95-4 H2 2,4,6-Trichlorophenol ND ug/L 10.0 1 12/19/17 08:00 12/20/17 12:55 88-06-2 H2 Surrogates Nitrobenzene-d5 (S) 48 % 40-121 1 12/19/17 08:00 12/20/17 12:55 4165-60-0 2-Fluorobiphenyl (S) 48 % 45-139 1 12/19/17 08:00 12/20/17 12:55 321-60-8 Terphenyl-d14 (S) 52 % 48-146 1 12/19/17 08:00 12/20/17 12:55 1718-51-0 Phenol-d6 (S) 34 % 18-105 1 12/19/17 08:00 12/20/17 12:55 13127-88-3 2-Fluorophenol (S) 39 % 13-118 1 12/19/17 08:00 12/20/17 12:55 367-12.4 2,4,6-Tribromophenoi (S) 49 % 31-170 1 12/19/17 08:00 12/20/17 12:55 118-79-6 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 1212111716:23 67-64.1 Benzene ND ugtL 5.0 1 12/2111716:23 71-43-2 L2 Bromobenzene ND uglL 5.0 1 1212111716:23 108-86-1 Bromochloromethane NO ug/L 5.0 1 1212111716:23 74-97-5 Bromodichloromethane ND ug/L 5.0 1 12/21/1716:23 75-27-4 Bromoform ND ug/L 5.0 1 12/2111716:23 75-25-2 Bromomethane NO ug/L 10.0 1 12/2111716:23 74-83-9 2-Butanone (MEK) NO ug/L 10.0 1 12121/17 16:23 78-93-3 tert-Butyl Alcohol ND ug/L 100 1 12/21/17 16:23 75-65-0 n-Butylbenzene NO ug1L 5.0 1 12/21/1716:23 104-51-8 sec-Butylbenzene NO ug/L 5.0 1 1212111716:23 135-98-8 tent -Butyl benzene NO ug/L 5.0 1 12121/1716:23 98-06-6 Carbon tetrachloride NO ug/L 5.0 1 1212l/17 16:23 56-23-5 Chlorobenzene NO ug/L 5.0 1 12121/1716:23 108-90-7 Chloroethane NO ug/L 10.0 1 1212111716:23 75-00.3 Chloroform NO ug/L 5.0 1 1212111716:23 67-66-3 Chloromethane ND ug/L 5.0 1 12121/1716:23 74-87-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/03/2018 12:47 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 33 aceAnalytical wwwpacefabs.com I ANALYTICAL RESULTS Project: Stormwater 1218 Paco Analytical Services, LLC 9800KinceyAve. Suite100 Huntersville, NG 2BO78 f704)875-9092 Pace Project No.: 92367253 Sample: STORMWATER Lab ID: 92367253001 Collected: 12/08117 13:30 Received: 12/15/17 12:40 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua] 8260 MSV Analytical Method: EPA 8260 2-Chlorotoluene NO uglL 5.0 1 12/21/1716:23 95-49-8 4-Chlorotoluene ND ug1L 5.0 1 12121/1716:23 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 12121/1716:23 96-12-8 Dibromochloromethane NO ug1L 5.0 1 12121/1716:23 124-48-1 1,2-Dibromoethane (EDB) NO ug1L 5.0 1 12/21/17 16:23 106-93-4 Dibromomethane NO ug1L 5.0 1 12121/1716:23 74-95-3 1.2-Dichlorobenzene NO ug/L 5.0 1 1212111716:23 95-50-1 1,3-Dichlorobenzene NO ug1L 5.0 1 12121/1716:23 541-73-1 1,4-Dichlorobenzene NO ug1L 5.0 1 12121/17 16:23 106-46-7 Dichlorodifluoromethane NO ug1L 5.0 1 12121/1716:23 75-71-8 1,1-Diehl oroethane NO ug1L 5.0 1 1212111716:23 75-34-3 1,2-Dichloroethane NO ug1L 5.0 1 1212111716:23 107-06-2 1,2-Dichloroethene (Total) NO uglL 5.0 1 12/21/17 16:23 540-59.0 1, 1 -Dichloroethene NO ug1L 5.0 1 1212111716:23 75-35-4 cis-1,2-Dichloroethene ND uglL 6.0 1 12/2111716:23 156-59-2 trans-1,2-Dichloroethene NO uglL 5.0 1 1212111716:23 156-60-5 1,2-Dichloropropane NO uglL 5.0 1 1212111716:23 78-87-5 1,3-Dichloropropane ND uglL 5.0 1 12/2111716:23 142-28-9 2,2-Dichloropropane NO uglL 5.0 1 1212111716:23 594-20-7 1,1-Dichloropropene NO uglL 5.0 1 12/2111715:23 563-58-6 cis- 1,3-Dichloropropene NO uglL 5.0 1 12/2111716:23 10061-01-5 trans- 1,3-Dichloropropene ND ug1L 5.0 1 12/2111716:23 10061-02-6 D]]sopropyl ether ND ug1L 5.0 1 12/21/17 16:23 108-20-3 Ethylbenzene NO uglL 5.0 1 12121/1716:23 100-41-4 Hexachloro-1,3-butadiene NO ug1L 5.0 1 1212111716:23 87-68.3 2-Hexanone NO ug1L 10.0 1 12/21/17 16:23 591-78-6 lsopropylbenzene (Cumene) NO ug1L 5.0 1 12/21/17 16:23 98-82-8 p-Isopropyltoluene NO ug1L 5.0 1 1212111716:23 99-87-6 Methyiene Chloride ND uglL 5.0 1 12/21/17 16:23 75-09-2 4-Methyl-2-pentanone (MIRK) ND ug1L 10.0 1 12/21/17 16:23 108-10-1 Methyl-tert-butyl ether NO ug1L 5.0 1 12/21/17 16:23 1634-04-4 Naphthalene NO ug1L 5.0 1 1212111716:23 91-20-3 n-Propylbenzene ND uglL 5.0 1 12/2111716:23 103-65-1 Styrene NO ug/L 5.0 1 12121/1716:23 100-42-5 1,1,1,2-Tetrachloroethane NO ug1L 5.0 1 12121/1716:23 630-20-6 1,1.2,2-Tetrachloroethane NO ug1L 5.0 1 12/21/1716:23 79-34-5 Tetrachloroethene ND ug1L 5.0 1 12/21/1716:23 127-18-4 Toluene NO ug1L 5.0 1 12121/1716:23 108-88-3 L2 1,2,3-Trichlorobenzene NO ug1L 5.0 1 12/21/17 16:23 87-61-6 1,2,4-Trichlorobenzene ND ug1L 5.0 1 12/21/1716:23 120-82-1 1,1,1-Trichloroethane NO ug1L 5.0 1 12/21/1716723 71-55-6 1,1,2-Trichloroethane NO ug1L 5.0 1 12/21/1716:23 79-00-5 Trichloroethene NO ug1L 5.0 1 12/21/1716:23 79-01-6 Trichlorofluoromethane NO ug1L 10.0 1 12/21/1716:23 75-69-4 1,2,3-Trichloropropane NO ug1L 5.0 1 12/21/1716:23 96-18-4 1,2,4-Trimethylbenzene ND ug1L 5.0 1 12/2111716:23 95-63-6 1,3,5-Trimethylbenzene NO ug1L 5.0 1 12121/1716:23 108-67-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01/03/2018 12:47 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 33 m aceAnalytical wwwpscetabs.com ANALYTICAL. RESULTS Project: Stormwater 1218 Pace Project No.: 92367253 Pace Analytical Services, LLC 9800 Kincey Ave, Suite SOD Huntersville, NC 28078 (704)875.9092 Sample: STORMWATER Lab ID: 92367253001 Collected: 12/08117 13:30 Received: 12115/17 12:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Vinyl acetate ND uglL 10.0 1 12/21117 16:23 108-05-4 Vinyl chloride ND uglL 5.0 1 12/21/17 16:23 75-01-4 m&p-Xylene ND ug1L 10.0 1 12/2111716:23 179601-23-1 o-Xylene ND ug1L 5.0 1 1212111716:23 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 12/21/17 16:23 460-00.4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 12/21/17 16:23 17060-07-0 Toluene-d8 (S) 123 % 70-130 1 12/21/17 16:23 2037-26-5 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 150 mglL 4.2 1 12/19/17 10:33 H1 Date: 01/03/2018 12:47 PM REPORT OF LABORATORY ANALYSIS This report shO not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 33 `0 CHAIN -OF -CUSTODY l Analytical Request Document E ' ns PaceAnalytica! The Chain -of -Custody is a LEGAL DOCUMENT. All rcMvanl kakis must Uc oor:pletcd aCc�ratery. D_ Section A Section B Section C i ' 3 Pape: M Requlretl Gle:tt Irttarma;nn Required Project Infom+atiar Etnrpoe Irrorma!ian Con9�7• SUrtrenjo$ Ins Rcpxt To- Jyr}i25 BfC[e Adeni3On. Natatte Oicn i Address: 4001 Beryl t load Copy To: Company Name: Surtionics REGULATORY AGENCY i Raleigh, NC 27606 Addnase, 4001 Beryl Rd, Raleigh, NC 27606 NPOES i' GROUND WATER ORMKING WATER — UST RCRA OTHER Emae Ttt jU1LeOSUrbtMiC.s WM Pkr"s£Order No, Psteemc ReYenu. I Pmw. 919795153422 IF= 9196289972 Pr*dcl Name. Wastewaler PUG Prq w Site Location / '01. wnaoer. STATE' Fall END rAl RequGtetl Die pattJTAT: Prolea Mmflcr. "cu P'0fi� ` Requested Analysis Filtered (YIN) Ems Section D VAId Ystdr Codes ? _ ' wutrca Crac Lnfoh �'= � g COLLECTED Pfeservatives i- E PRrAi wlSLll m U WIlSTESVATFR I., $ T ST�It =hpmTE EwXA4 U > J r C PRQT P PRODUCT exa ms a o . J E � t Q ¢ ¢ i OL OL .y O o O SAMPLE ID a W {A-Z D-9 r ,) 0 M O rssuE rs w 0 w ¢ ei '2 m - swoo IDS MUST BE UNIDUE o b co o V ;mm�" CM �; :�.. '•' Q .. :i• O CI p U m ce m s d N m !' n r/` DATErinsE DATE r rrtE > i i x 2 e1 a O .. Np m m Q tmi a rr a�S D a�i a W a: Paee Project NaJ Lab I.G. t 5torn1water OT 12MI17 1;w 12XM7 1',ao 13 1 1 3 3 � { 2 2 1 1 2 i , 3 2 2 6 2 x 6 i e 8 11 1 42 ! ADWTIONAL.COMMENTS REUNOWSHED BY I AFF1LasWN DATE TIME ACCEPTED BY I AMLIAT16N DATE IWE SAMPLE CDNDITIDN5 James Byre 12115117 { i , i 1 k 1 1 SAMPI-ER NAME AND 57GNATURE rs PFtINT Nama of SttMPUr7aw SIGNATURE 01 SAMPLER: NNlDOIYIfi: 12/15/17 'fPooa=Nate By s4 ukq ;. s mwm you an aceep'U'r9 Pears ?XT 30 day Gayle A to — ono a;ree:ri vo fav thwps eI S 5!t W mprah 13r"amcec net paid wJ-;!.T :7 days F-ALL-p-020r¢v.08, i2-d[i-2007 SURTRONICS, INC. 4001 Beryl Rd. P.O. Box 33459 Raleigh, NC 27606 Raleigh, NC 27636-3459 (919)834-8027 Fax (919)828-9972 May 30, 2017 N C 6_ 0.3 (D Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh NC 27699-1617 Subject: Permittee-Stormwater Data Spring 2017 Sample—4/24/17 To Whom It May Concern: Two copies of one set of data accompany this letter based on sampling of a Spring 2017 event. The events occurred on 'F�h49rtByfhe data includes: Two (2) copies of one set of qualitative data for each of three sampling points are enclosed. If you have any questions please call me at (919)834-8027 Ext 235. CC: Surtronics File Enclosures: Storm Data 4/24127 RECEIVED JUN 0 6 2017 CENTRAL FILES DWR SECTION Sincerely yours, Lee Br haw Genera Manager �',;-`A F4CDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance an filling out this form, please visit: htt : pia tal.n d a r. �r r web ws n e w# ab-4 Permit No.: IV/�/�/,/ _/�/�/�/�/ or Certificate of Coverage No.: FacilityName: Su 'tlle AjC County: " Phone No. qIQ - f34- AV Inspector: .)AMPS !hu, Date of Inspection: 5- Z4- l Time of Inspection: ^- 10'. qta._ Total Event Precipitation (inches): '41 - S Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ❑ Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureahle storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "treasurable storm event is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee ' obtains approval from the local DWQ Regional Office. By this signature, I certi th t this report is accurate and:. complete to the best of my knowledge: (Signature of P ittee or Designee) Page 1 of 2 SM-242, Last modified 10/25/2012 1. Outfall Description: , Outfall No. 1TI 3 Structure (pipe, ditch, etc.) ROJ Receiving Stream: Q Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Uggor 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _ None, 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 Q 3 4 5 5. Floating Solids: Choose the number which best describes the amount of Floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 1) 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1. is no solids and 5 is extremely muddy: 7. 8. 9. 1 3 Is there any foam in the stormwater discharge? 4 5 Yes Is there an oil sheen in the stormwater discharge? Yes Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may he indicative of pollutant exposure. These conditions warrant further investigation, Page 2 of 2 SWU-242, Last modified 10/25/2012 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted ,S 3a 1 7 CERTIFICATE OF COVERAGE No. NCG03n 0 b b FACILITY NAMf �)l>rr q%CS X COUNTY PERSON COLLECTING SAMPLES LABORATORY%CG &rVA L4TZ jS& Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR zo i r7 SAMPLE PERIOD [VJ Jan -June ❑ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout [_]RNA []Zero -flow ❑Water Supply []SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period?Z Outfall No. Date Sam le P Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids P H, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ==_> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L 1 A- ILA_11 4 -V -1 b, W(. a.000 it - �• % 1 4 "1 36.3 b-606 X$ p 6.00D ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be efigible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tunes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/2S/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." L €c" 1?4 Q s1.1,4 u1 Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit,.BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format ""<XX inA" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. IC Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results. only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample 24-hour rainfall Colilectedl amount, Non -polar 0&G/TPH by Total Suspended Solids pH (mo/dd/yr) lnches3 EPA 1664 (SGT-HEM) Benchmarks =__>_ . - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. . . A. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note, If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES EINOEJ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES []NO[] REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" re orts within 30 days of recei t of the lab results or at end of monitorin_q period in the case of "No Discharge" reports} to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and ccmplete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permi yl Z1?l1-7 (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2022 ace Analytical Knvw,pa>�eDs.cum a SAMPLE ANALYTE COUNT Project: Stormwater 4124 Pace Project No.: 92338806 9800Kin" Ave. Suite 100 Huntersville, NC 28078 (7D4)875-9092 Analytes Lab 10 Sample 10 Method Analysts Reported Laboratory 92338806001 STORMWATER EPA 1664B JMS 1 PASI-C EPA 8081 RES 24 PASI-C EPA 8082 HSK 8 PASI-C EPA 6010 SH1 3 PASI-A EPA 8270 RES 74 PASI-C EPA 8260 GAW 71 PASI-C SM 2540D CJH1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 28 aceAna lXicaI wwwpacsfabs.wm I ANALYTICAL RESULTS 9600 Kincey Ave. Suite 100 Muntersville. NC 28078 (704)875-9092 Project: Stormwater 4/24 Pace Project No.: 92338806 Sample: STORMWATER Lab ID: 92338806001 Collected: 04124/17 10:45 Received: 04/28117 11:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua! HEM, Oil and Grease Analytical Method: EPA 18648 Oil and Grease NO mg1L 5.0 1 05/09/17 06:26 8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510 Aldrin ND ug/L 0.050 1 0510211710:00 05/02/1718-.09 309-00-2 H2 alpha-BHC ND ug1L 0.050 1 05102A710:00 0510211718:09 319-84-6 H2 beta-BHC ND ug1L 0.050 1 0510211710:00 0510211718:09 319-85-7 H2 delta-BHC NO ug1L 0.050 1 0510211710:00 05/0211718:09 319-86-8 H2 gamma-BHC (Lindane) NO ug/L 0.050 1 05/02/17 10:00 05/02/17 18:09 58-89-9 H2 Chlordane (Technical) NO ug1L 0.20 1 05/02/17 10:00 05/02117 18:09 57-74-9 H2 4,4'-DDD NO ug1L 0.050 1 0510211710:00 05/0211718:09 72-54-8 H2 4,4'-DDE NO ug1L 0.050 1 05/02/17 10:00 05/02/17 18:09 72-55-9 H2 4,4'-DDT ND ug/L 0.050 1 05102/17 10:00 0510211718:09 50-29-3 H2 Dieldfin NO ug1L 0.050 1 05102/17 10:00 05102/1718:09 60-57-1 H2 Endosulfan I NO ug1L 0.050 1 05/02/17 10:00 05/02/17 1B:09 959-98-8 H2 Endosulfan ll NO ug/L 0.050 1 05J02/17 10:00 05/02/17 18:09 33213-65-9 H2 Endosulfan sulfate NO ug/L 0.050 1 05/02/17 10:00 05/02/17 18:09 1031-07-8 H2 Endrin NO ug/L 0.050 1 05/0211710:00 05102/1718:09 72-20-8 H2 Endrin aldehyde ND ug/L 0.050 1 05/02/17 10:00 05/02/17 18:09 7421-93-4 H2 Endrin ketone NO ug/L 0.050 1 05/02/17 10:00 05/02/17 18:09 53494-70-5 H2 Heptachlor ND uglL 0.050 1 05/0211710:00 05102/17 18:09 76-44-8 H2 Heptachlor epoxide NO ug/L 0.050 1 05/02/17 10:00 W02117 18:09 1024-57-3 H2 Hexachlorobenzene ND ug/L 0.050 1 05102/17 10:00 05102/1718:09 118-74-1 H2 Methoxychlor NO ug1L 0.15 1 05/0211710:00 05102/17 18:09 72-43-5 H2 Mirex NO ug1L 0.15 1 05/02/17 10:00 05102/1718:09 2385-85-5 H2 Toxaphene ND ug/L 0.20 1 05/02/1710:00 05/0211718:09 8001.35-2 H2 Surrogates Tetrachloro-m-xylene (S) 35 % 20-130 1 05102/17 10:00 05102/17 18:09 877-09-8 Decachlorobiphenyl (S) 28 % 20-130 1 05102/17 10:00 05/02/17 18.09 2051-24-3 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Aroclor 1016) NO ug/L 0,50 1 05/02/17 10:00 05/03/17 01:43 12674-11-2 PCB-1221 (Aroclor 1221) NO ug/L 0-50 1 05/02/17 10:00 05/03/17 01:43 11104-28-2 PC8-1232 (Aroclor 1232) NO ug1L 0.50 1 05/02/17 10:00 05103117 01:43 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.50 1 05/02/17 10:00 05fO3/17 01:43 53469-21-9 PCB-1248 (Aroclor 1248) NO ug/L 0.50 1 05/02/17 10:00 05/03/17 01:43 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0,50 1 05/02/17 10:00 05/03117 01:43 11097-69-1 PCB-1260 (Aroclor 1260) NO ug1L 0.50 1 05/02/17 10:00 05/03/17 01:43 11096-82-5 Surrogates Decachlorobiphenyl (S) 31 °10 10-132 1 05/02/17 10:00 05/03/17 01:43 2051-24-3 6010 MET ICP Anaytical Method: EPA 6010 Preparation Method: EPA 3010A Copper 8.3 ug/L 5.0 1 05102/17 20:10 05J03117 21:37 7440-50-8 Lead NO ug1L 5.0 1 05102/17 20:10 05/03/17 21:37 7439-92-1 Zinc 61.0 ug/L 10.0 1 05/02/17 20:10 05/03/17 21:37 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/11/2017 04:03 PM without the written consent of Pace Analytical Services. LLC. Page 4 of 28 ,�Iace Analytical www.pmwabs.com I ANALYTICAL RESULTS 9500 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater 4124 Pace Project No.: 92338806 Sample: STORMWATER Lab ID: 92338806001 Collected: 04/24/17 10:45 Received: 04/28/17 11:45 Matrix: Water Parameters Results Units report Limit DF Prepared Analyzed CAS No_ Oual $270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene NO ug/L 10.0 1 05/02/17 09A0 05/04/17 20:56 83-32-9 H2 Acenaphthylene NO ug/L 10.0 1 05/02/17 09A0 05/04/17 20:58 208-96-8 H2 Aniline NO ugll- 10.0 1 05102//17 09A0 05/04/17 20:58 62-53-3 H2 Anthracene NO ug/L 10.0 1 05/02/17 09:10 05/04117 20:58 120-12-7 H2 Benzo(a)anthrocene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 56-55-3 H2 Benzo(a)pyrene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 50-32-8 H2 Senzo(b)fluoranthene N❑ ug1L 10.0 1 05/02/17 09:10 05/04/17 20:58 205-99-2 H2 Benzo(g,h,i)perylene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 191-24-2 H2 Benzo(k)ftuoranthene ND ug/L 10.0 1 05/02/17 09:10 05/04/17 20,58 207-08-9 H2 Benzoic Acid NO uglL 50.0 1 05/02/17 09:10 05/04/17 20:58 65-85-0 H2 Benzyl alcohol NO ug/L 20.0 1 05/02/17 09:10 05/04/17 20:58 100-51-6 H2 4-Bromophenylphenyl ether NO ug/L 10.0 1 05J02117 09:10 05/04/17 20:58 101-55-3 H2 Butyibenzylphtha late ND ug/L 10,0 1 05/02/17 09:10 05/04/17 20:58 85-68-7 H2 4-Chloro-3-rnethylphenol ND vg1L 20.0 1 05/02/17 09:10 05104117 20:58 59-50-7 H2 4-Chtoroanitine NO ugA- 20.0 1 05/02/17 09:10 05/04/17 20:59 10647-8 H2 bis(2-Chloroethoxy)methane NO uglL 10.0 1 05/02/17 09:10 05/04/17 20:58 111-91-1 H2 bis(2-Chloroethyl) ether NO ug/L 10.0 1 05/02/17 09A0 05/04/17 20:58 111-44-4 H2 2-Chloronaphthalene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 91-58-7 H2 2-Chtorophenol NO uglL 10.0 1 05/02/17 09:10 05/04/17 20:58 95-57-8 H2 4-Chlorophenylphenyl ether NO ug/L 10.0 1 05/02/17 09:10 05104/17 20:58 7005-72-3 H2 Chrysene NO uglL 10.0 1 05/02/17 09:10 05/04117 20:58 218-01-9 H2 Dibenz(a,h)anthracene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 53-70-3 H2 Dibenzofuran NO ug/L 10,0 1 05/02/17 09:10 05/04/17 20:58 132-64-9 H2 1,2-Dichlorobenzene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 95-50-1 H2 1,3-Dichlorobenzene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 541-73-1 H2 1,4-Dichlorobenzene NO ug/L 10.0 1 05/02/17 09,10 05/04/17 20:58 106-46-7 H2 3,3'-Dichlorobe nzidine NO ug/L 20,0 1 05/02/17 09:10 05/04/17 20:58 91-94-1 H2 2,4-Dichlorophenol NO ug/L 10.0 1 05/02/17 09710 05/04/17 20:58 120-83-2 H2 Diethylphthalate NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 84-66-2 H2 2,4-Dimethylphenol NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 105-67-9 H2 Dimethylphthalate ND ug/L 10.0 1 05/02117 09:10 05/04/17 20:58 131-11-3 H2 Di-n-butylphihalate NO ug/L 10.0 1 05102/17 09:10 05/04117 20:58 84-74-2 H2 4,6-Dinitro-2-methylphenol NO ug/L 20.0 1 0902/17 09:10 05/04/17 20:58 534-52-1 H2 2,4-Dinitro phenol NO ug/L 50.0 1 05/02/17 09:10 05/04/17 20:58 51-28-5 H2 2,4-Dinitrotoluene ND ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 121-14-2 H2 2,6-Dinitrototuene NO uglL 10.0 1 05/02/17 09:10 05/04/17 20:58 606-20-2 H2 Di-n-octylphthalate NO ug/L 10.0 1 05/02/17 09:10 05104/17 20:58 117-84-0 H2 bis(2-Ethythexyl)phthalate NO ug/L 6.0 1 05/02/17 09:10 05/04117 20:58 117-81-7 H2 Fluoranthene NO ug/L 10.0 1 05/02/17 09:10 05104/17 20:58 206-44-0 H2 Fluorene NO uglL 10.0 1 05/02/17 09:10 05/04/17 20:58 86-73-7 H2 Hexachloro-1,3-butadiene NO uglL 10.0 1 05/02/17 09:10 05/04/17 20:58 87-68-3 H2 Hexachlorobenzene NO uglL 10.0 1 05/02/17 09:10 05/04/17 20:58 118-74-1 H2 Hexachlorocyclopentadiene NO ug/L 10.0 1 05102117 09:10 05/04/17 20.58 7747-4 H2 Hexachloroethane NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 67-72-1 H2 Indeno(1,2,3-cd)pyrene NO ug/L 10,0 1 05/02/17 09:10 05/04/17 20:58 193-39-5 H2 lsophorone NO uglL 10.0 1 05/02/17 09:10 05/04/17 20:58 78-59-1 H2 1-Methylnaphthalene NO ug1L 10.0 1 05/02/17 09:10 05/04117 20:58 90-12-0 H2 REPORT OF LABORATORY ANALYSIS This report shall not tre reproduced, except in full, Date: 05/11/2017 04:03 PM without the written consent of Pace Analytical Services. LLC. Page 5 of 28 ,�aceAnalytical* www.pacetens�m 9800 Kincey Ave. Suite 100 Hunten;ville, NC 2ao78 (704)875-9092 Project: Stormwater 4/24 Pace Project No.: 92338806 Sample: STORMWATER ANALYTICAL RESULTS Lab ID: 92338806001 Collected: 04/24/17 10:45 Received: 04/28/17 11:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8270 MSSV Sernivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 2-Methyinaphthalene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 91-57-6 H2 2-Methylphenol(o-Cresol) NO ug/L 10.0 1 05/02/17 09:10 05104/17 20:58 95-48-7 H2 3&4-Methylphenol(m&p Cresol) NO ug/L 10.0 1 05/02/17 09;10 05/04/17 20:58 15831-10-4 H2 Naphthalene NO ug/L 10-0 1 05102/17 09:10 05/04/17 20:58 91-20-3 H2 2-Nitroaniline NO ug/L 50.0 1 05/02/17 09:10 05104/17 20:58 88-74-4 H2 3-Nitroaniline NO ug1L 50.0 1 05/02/17 09:10 05104/17 20:58 99-09-2 H2 4-Nitroaniline NO ug/L 20.0 1 05/02/17 09:10 05/04/17 20:58 100-01-6 H2 Nitrobenzene ND ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 98-95-3 H2 2-Nitrophenol ND ug/L 10.0 1 05102/17 09:10 05/04/17 20:58 88-75-5 H2 4-Nitrophenol NO ug/L 50.0 1 05/02/17 09:10 05/04/17 20:58 100-02-7 H2 N-Nitrosodimethylamine ND ug1L 10.0 1 05/02/17 09:10 05/04117 20:58 62-75-9 H2 N-Nitroso-di-n-propylamine ND ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 621-64-7 H2 N-Nitrosodiphenylamine NO ug/L 10.0 1 05/02/17 09:10 05104/17 20:58 86-30-6 H2 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 1 05/02/17 09:10 05/04117 20:58 108-60-1 H2 Pentachlorophenol ND ug/L 25.0 1 05/02/17 09:10 05/04/17 20:58 87-86-5 H2 Phenanthrene ND ug/L 10.0 1 05/02/17 09:10 05J04/17 20:58 85-01-8 H2 Phenol NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 108-95-2 H2 Pyrene ND ug/L 10.0 1 05/02/17 09:10 05/04117 20:58 129-00-0 H2 1,2,4-Trichlorobenzene NO ug/L 10.0 1 05/02/17 09:10 05104117 20:58 120-82-1 H2 2,4,5-Trichlorophenol ND ug/L 10.0 1 05/02117 09:10 05/04/17 20:58 95-95-4 H2 2,4,6-Trichlorophenol ND ug/L 10.0 1 05102/17 09:10 05/04117 20:58 88-06-2 H2 Surrogates Nitrobenzene-d5 (S) 43 % 21-110 1 05/02/17 09:10 05/04/17 20:58 4165-60-0 2-Fluorobiphenyl (S) 49 % 27-110 1 05/02/17 09:10 05/04/17 20:58 321-60-8 Terphenyl-d14 (S) 61 % 31-107 1 05/02/17 09:10 05/04/17 20:58 1718-51-0 PhenoW6 (S) 15 % 10-110 1 05J02117 09:10 05/04/17 20:58 13127-88-3 2-Fluorophenol (S) 23 % 12-110 1 05/02/17 09:10 05J04117 20:58 367-12-4 2,4,6-Tribromophenol (S) 46 % 27-110 1 05/02/17 09:10 05/04/17 20:58 118-79-6 8260 MSV Analytical Method: EPA 8260 Acetone NO ug/L 25.0 1 05/02/1712:47 67-64-1 L1 Benzene NO ug/L 5.0 1 05102/1712:47 71-43-2 Bromobenzene ND ug/L 5.0 1 05102/1712A7 108-86-1 Bromochloromethane NO ug/L 5.0 1 0510211712:47 74-97-5 Bromodichloromethane ND ug/L 5.0 1 0510211712A7 75-27-4 Bromoform NO ug1L 5.0 1 05102/1712:47 75-25-2 Bromomethane NO ug/L 10.0 1 0510211712:47 74-83-9 2-Butanone (MEK) NO ug/L 10.0 1 05/02/17 12:47 78-93-3 tert-Butyl Alcohol ND ug/L 100 1 05/02/17 12:47 75-65-0 n-Butylbenzene NO ug/L 5.0 1 05/02/1712:47 104-51-8 sec-Butylbenzene NO uglL 5.0 t 05/02/1712:47 135-98-8 tert-Butyibenzene ND ug/L 5.0 1 0510211712:47 98-06-6 Carbon tetrachloride ND ug/L 5.0 1 05102/17 12:47 56-23-5 Chlorobenzene NO ug/L 5.0 1 05/0211712:47 108-90-7 Chloroethane NO uglL 10.0 1 05102/1712:47 75-00-3 Chloroform ND uglL 5.0 1 05/0211712:47 67-66-3 Chloromethane ND ug/L 5.0 1 05/0211712:47 74-87-3 REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in fun, Date: 05/11/2017 04-03 PM without the written consent of Pace Analytical Services. LLC. Page 6 of 28 aceAnalytieal www.paodlabs.coro t , ANALYTICAL RESULTS Project: Stormwater 4124 Pace Project No.: 92338806 9800 Kincey Ave. Suite 100 Huntergville, NC 28078 (704)875-9092 Sample: STDRMWATER Lab lD: 92338806001 Collected: 04/24/17 10:45 Received: 04/28/17 11:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 2-Chlorotoluene ND ug/L 5.0 1 05/0211712:47 95-49.8 4-Chlorotoluene NO ug/L 5.0 1 0510211712A7 106-43-4 1,2-Dibromo-3-chloropropane NO ug/L 2.0 1 05/0211712747 96-12-8 Dibromochloromethane NO ug/L 5.0 1 05/0211712:47 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 5.0 1 05102/17 12:47 106-03-4 Dibromomethane ND uglL 5.0 1 06/0211712:47 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 1 05102/1712:47 95-50-1 1,3-Dichlorobenzene NO ug/L 5.0 1 05/02J1712:47 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 1 0510211712:47 106-46-7 Dichtorodifluoromethane NO ug/L 5.0 1 05/02A712:47 75-71-8 1.1-Dichlaroelhane ND ug/L 5.0 1 0510211712:47 75-34-3 1,2-Dichloroethane NO ug/L 5,0 1 05102/1712:47 107-06-2 1,2-Dichloroethene(Total) ND ug/L 5.0 1 0510211712:47 540-59-0 1,1-Dichloroethene NO ug/L 5.0 1 05/02/1712:47 75-35-4 cis-1,2-Dichloroethene NO ug/L 5.0 1 05/0211712:47 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 1 05102/1712:47 156-60-5 1,2-Dichloropropane NO ug1L 5.0 1 05/0211712:47 78-87-5 1,3-Dichloropropane NO ug/L 5.0 1 0510211712:47 142-28-9 2,2-Dichloropropane NO ug1L 5.0 1 05102/1712:47 594-20-7 1.1-Dich[oropropene NO ug/L 5.0 1 05/0211712:47 563-58-6 cis- 1,3-Dich[oropropene ND ug/L 5.0 1 0510211712:47 10061-01-5 trans-1,3-Dichloropropene NO ug/L 5.0 1 05/02/1712:47 10061-02-6 Diisopropyl ether ND ug/L 5.0 1 05/0211712:47 108-20-3 Ethylbenzene NO ug/L 5.0 1 05/0211712A7 100-41-4 Hexachloro-1,3-butadiene NO ug/L 5.0 1 05/02/1712:47 87-68-3 2-Hexanone NO ug/L 10.0 1 05102/1712:47 591-78-6 isopropy lbenzene (Cumene) NO ug/L 5.0 1 05/02/17 12:47 98-82-8 p4sopropyltoluene NO ug/L 5.0 1 05102/1712,47 99-87-6 Methylene Chloride NO ug/L 5.0 1 05/02/17 12:47 75-09-2 4-Methyl-2-pentan©ne (Mi8K) ND ug/L 10.0 1 05/02/17 12A7 108.10-1 Methyl-tert-butyl ether NO ug/L 5.0 1 05102/17 12:47 1634.04-4 Naphthalene NO ug/L 5.0 1 05/0211712:47 91-20-3 n-Propylbenzene NO ug/L 5.0 1 05/02/1712:47 103-65-1 Styrene NO ug/L 5.0 t 05/02/1712.47 100-42-5 1,1,1,2-Tetrachloroethane ND ug1L 5.0 1 05/0211712A7 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 5.0 1 05102/1712;47 79-34.5 Tetra chtoroethene NO ug/L 5.0 1 05/0211712:47 127.18-4 Toluene NO ug/L 5.0 1 05/0211712:47 108-88-3 1,2,3-Trichlorobenzene NO ugtL 5.0 1 05102/171247 87-61-6 11,2,4-Trichlorobenzene NO ug/L 5.0 1 05/0211712-47 120-82-1 1,1,1-Trichloroethane NO ug/L 5.0 1 05102/1712:47 71-55-6 1,1,2-Trichloroethane ND ug/L 5.0 1 05/0211712:47 79-00-5 Trichloroethene ND ugll- 5,0 1 05102/1712:47 79-01-6 Trichlorofluoromethane ND ug/L 10.0 1 05102/1712:47 75-69-4 1,2,3-Trichloropropane NO ug/L 5.0 1 05/02/1712:47 96-18-4 1,2,4-Trimethylbenzene NO ug/L 5,0 1 05/02/1712:47 95-63-6 1,3,5-Trimethylbenzene ND ug/L 5.0 1 05/0211712A7 108-67-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:03 PM without the written oonsent of Pace Analytical Services, LLC. Page 7 of 28 IeAnafytical �'�Ag�bs.r�rn r ' ANALYTICAL RESULTS 9800 Kincey Ave. Suite 100 Nuntersvioe. NC 28078 (704)875-9092 Project: Stormwater 4124 Pace Project No.: 92338806 Sample: STORMWATER Labill): 92338806001 Coilected: 04124/17 10:45 Received: 04/28/17 11:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Vinyl acetate NO ug1L 10.0 1 05/02/17 12-47 109-05-4 Vinyl chloride NO ug/L 5.0 1 05/02/17 12:47 75-01-4 m&p-Xylene NO ug1L 10.0 1 05102/1712:47 179601-23-1 o-Xylene NO ug1L 5.0 1 05102/1712:47 95-47-6 Surrogates 4-Bfomoftuorobenzene (S) 96 % 70-130 1 05/02/17 12:47 460-00-4 1,2-Dlchtoroethane-d4 (S) 108 % 70-130 1 05/02/17 12:47 17060-07-0 Toluene-d8 (S) 112 % 70-130 1 05/02/17 12.47 2037-26-5 2WO Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 3.5 mg1L 2.5 1 05102/17 02:27 H1 Date: 05111 /2017 04:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Anafyticai Services, LLC, Page 8 of 28 Raleigh April Weather 2017 - AccuWeather Forecast for NC 27601 ENGLISH (US), T i Raleigh. NC -1 Follow us an lMl In pzrtnerslhlp with -----'--- .._I.-- -_._....- L'•uii,�d 5aates vVeatires I Raleigh, INC Local Weather 847 I ! Personalized Forecasts: Allergies — Now We&end Extended Month Radar I MllinuteCastz I II Watch Videos March 2017 View: April - 2017 May 2017 Dare HOW Preup Snow Forecast Avg, HI l LO Sat 411 75`149° 0 IN 0 IN 68'144' Sun 412 69'149' 0 IN 0 IN 69*144' Mon 413 76'150' 0.40 IN 0 IN 69't45' Tue 414 82'163' 0 IN 0 IN B9'145' Wed 415 78'/53' 0.32IN 0IN 70*145' Thu 416 70'150' 0.09 IN 0 IN 70'146' Fri 4n 59'143' 0 IN 0 IN 70'146` Sat 418 67'134' 0 IN 0 IN 70*146' Sun 419 77'138' 0 IN O IN 71'146' Mon 4110 78'149' 0 IN 0 IN 71'147' Tue 411 1 82'155' 0 IN 0 IN 71'147' Wed 4112 83'156' 0 IN 0 IN 72'147' Thu 4113 80'154' 0IN 0 IN 72'147" Fri 4114 81'153' 0 IN 0 IN 72'148° Sat 4115 85'!61' 0 IN 0 IN 72'148° Sun 4116 82*160' 0 IN 0 IN 73'148' Mon 4117 86'162' 0.05 IN 0 IN 73'148' Tue 4118 74°161' 0.03 IN 0IN 73'149' Wed 4119 69'155' 0 IN 0 IN 73'149' Thu 4120 851156' 0 IN 0 IN 74°149' Fri 4121 89'163' 0.21 IN 0 IN 74"149' Sat 4122 87'156' 0.09 IN 0 IN 74"150" Sun 4123 56'153' 0.77 IN 0 IN 74'150' Mon 4124 601153, 4.51 Ir+ 0 IN 75'150' Raleigh April Weather 2017 - AccuWeather Forecast for NC 27601 PI. HOLO PreCp "OW F"-"" Avg. HI I LO Tup 4125 70'158' 2.17 IN 0 IN 75"150' Wed 4126 81`156' 0IN 01N 75'151' Thu 4127 82'162° 0 IN 0 IN 77"151 Fri 4128 88'169° 0 IN 0 IN 76°151' Sat 4129 89'172' 0 IN 0 IN 76'152` Sun 4130 861170° 0.021N 01N 76*152° lc; - May 2017 Temperature Graph April 2017 100 90 80 70 so 50 40 30 20 1 2 3 4 5 6 7 6 9 10 11 12 13 14 15 16 17 to 19 20 21 22 23 24 25 25 27 26 29 30 Avg HI Avg. Lo Actual Hi Actual Lo Actual N-FM 7,1 DeparlLlre Record High 78' 72' 95° (1896) Low 55° 48° 23" (1923) Average 66° 60` +6° Prr-lp 8.66 in 2.92 in +5 74 In Snow 0 in CHAIN -OF -CUSTODY ! Analytical Request Document The Chain -of -Custody Is a LEGAL. DOCUMENT. An relevant fietds must be completed accurately. M: ®11�1111�I■11 SAMPLE ID C"T-ft SL lip III 1 11111 IS ■■■■ m■■o■l■■■■■ ■0■■■■■■■■0■ ® ■■��■■■►�■■■■■■■ ■■■►R110011i■ ■�■■�■■■�■■�■■�■ 0010001■■■ MINNOW ■■■m■m■■■■m7■■■■■ 1001110000■■ ■�■■■r■r�■■■�■r■■■■ ■■■■■■■■■■■■ ® ■■■m 111■■r■■r■1rr ■rrr■■■01■■■ EMISSION ii■�i ■ir�i iiiii r f m N n 00 N N CA a aeeAnalykal wwwpecQbs.=n 9800 Kincey Ave. Suite too Huntersvilte. NC 28078 (704 )875-9092 SAMPLE ANALYTE COUNT Project: Stormwater 4f24 Pace Project No.: 92338806 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92338806001 STORMWATER EPA 16648 JM5 1 PASI-C EPA 8081 RES 24 PASI-C EPA 8082 HSK 8 PASI-C EPA6010 Slit 3 PASI-A EPA 8270 RES 74 PASI-C EPA 8260 GAW 71 PASI-C SM 2540D CJH1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Lt.C. Page 3 of 28 ace AnaV cal rwrwpase+abs.com i ANALYTICAL RESULTS Project: Stormwater 4/24 Pace Project No.: 92338806 9800 Kincey Ave, Suite 100 Hurtersville, NC 28078 (704) 875-9092 Sample: STORMWATER Parameters Lab ID: 92338806001 Collected: 04/24/17 10:45 Results Units Report Limit DE Received: 04/28117 11:45 Matrix: Water Prepared Analyzed CAS No, Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mg1L 5.0 1 05/09/17 06:26 8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510 Aldrin NO ug/L 0.050 1 05/02/17 10:00 05102/1718:09 309-00-2 H2 alpha-BHC ND ug/L 0.050 1 05/0211710:00 06102/1718:09 319-84-6 H2 beta-BHC NO ug/L 0.050 1 0510211710:00 05/02117 18:09 319-85-7 H2 delta-BHC NO ug1L 0.050 1 05/02117 10:00 05102/1718:09 319-86-8 H2 gamma-BHC (Lindane) NO ug/L 0,050 1 05/02117 10:00 05/02117 18:09 58-89-9 H2 Chlordane (Technical) ND ug/L 0.20 1 05/02/17 10:00 05/02/17 18:09 57-74-9 H2 4,4'-DDD NO ug1L 0.050 1 05/0211710,00 05/02/17 18:09 72-54-8 H2 4,4'-DDE ND ug1L 0.050 1 05/02/17 10:00 0510211718:09 72-55-9 H2 4,4'-DDT NO ug1L 0.050 1 05/02117 10:00 05/02/17 18:09 50-29-3 H2 Dieldrin NO ug/L 0.050 1 05102M710:00 05f02/1718:09 60-57-1 H2 Endosulfan I NO ug1L 0.050 1 05/02/17 10:00 05/02/17 18:09 959-98-8 H2 Endosulfan II ND uglL 0.050 1 05/02/17 10:00 05/02/17 18:09 33213-65-9 H2 Endosulfan sulfate NO ug/L 0.050 1 05/02/17 10:00 05102/17 18:09 1031-07-8 H2 Endrin ND ug1L 0.050 1 05/02/17 10:00 0510211718:09 72-20-8 H2 Endrin aldehyde ND ug1L 0.050 1 05/02/17 10:00 05/02/17 18:09 7421-93-4 H2 Endrin ketone ND ug1L 0.050 1 05/02/17 10:00 05/02/17 18:09 53494-70-5 H2 Heptachlor ND ug/L 0,050 1 0510211710:00 0510211718:09 76-44-8 H2 Heptachlor epoxide NO ug1L 0.050 1 0510211710700 051021171&09 1024-57-3 H2 Hexachlorobenzene NO ug/L 0.050 1 0510211710:00 05/02/17 18:09 118-74-1 H2 Methoxychlor ND ug/L 0.15 1 05/02/1710:00 05102/1718:09 7243-5 H2 Mirex NO ug/L 0.15 1 05/02/17 10:00 05102/1718:09 2385-85-5 H2 Toxaphene ND uglL 0.20 1 05102/1710:00 05102/1718:09 8001-35-2 H2 Surrogates Tetrachloro-m-xylene (S) 35 % 20-130 1 05/02/17 10:00 05t02/17 18:09 877.09-8 Decachlorobiphenyl (S) 28 % 20-130 1 05/02/17 10:00 05/02/17 18:09 2051-24-3 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Arodor 1016) ND ug/L 0.50 1 05/02/17 10:00 05/03/17 01:43 12674-11-2 PCB-1221 (Aroclor 1221) ND ug1L 0.60 1 0510207 10:00 05/03/17 01:43 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.50 1 05/02/17 10:00 05/03/17 01:43 11141-16-5 PCB-1242 (Aroclor 1242) NO ug1L 0.50 1 05/02/17 10:00 05/03/17 01:43 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 1 05/02/17 10:00 05/03/17 01 43 12672-29-6 PCB-1254 (Aroclor 1254) NO ug1L 0.50 1 05/02/17 10:00 05/03117 01:43 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 1 05/02/17 10:00 05iO3/17 01:43 11096-82-5 Surrogates Decachlorobiphenyl (S) 31 % 10-132 1 05/02/17 10:00 05/03/17 01:43 2051-24-3 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Copper 8.3 ug/L 5.0 1 05/02/17 20:10 05/03/17 21:37 7440-50-8 Lead NO ug/L 5.0 1 05/02/17 20:10 05/03/17 21:37 7439-92-1 Zinc 61.0 ug1L 10.0 1 05102/17 20:10 05/03/17 21:37 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05111 /2017 04:03 PM without the whiten consent of Pace Analytical Services, LLC. Page 4 of 28 ,�IaceAnalytical* www.pacwabs.com I ANALYTICAL RESULTS 9B00 Kinney Ave. Suite 100 Huntersviue, NC 2807E (704)875.9092 Project: Stormwater 4/24 Pace Project No.: 92338806 Sample: STORMWATER Lab ID: 92338806001 Collected: 04/24/17 10:45 Received: 04/28/17 11:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Cual 8270 MSSV Semivolatite Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 83-32-9 H2 Acenaphthylene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 208-96-8 H2 Aniline NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 62-53-3 H2 Anlhracene ND uglL 10.0 1 05/02117 09:10 05/04117 20:58 120-12-7 H2 Senzo(a)anthracene NO ug/L 10.0 1 05102/17 09:10 05/04/17 20:58 56-55-3 H2 Benzo(a)pyrene NO ug/L 10.0 1 05102A7 09:10 05/04/17 20:58 50-32-8 H2 Benzo(b)fluoranthene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 205-99-2 H2 Benzo(g,h,i)perylene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 191-24-2 H2 BenzoNfluoranthene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 207-08-9 H2 BenzoicAcid NO ug/L 50.0 1 05/02/17 09:10 05/04/17 20:58 65-85-0 H2 Benzyl alcohol NO ug/L 20.0 1 05/02/17 09:10 05/04/17 20:58 100-51-6 H2 4-Bromophenylphenyl ether NO ugil- 10.0 1 05/02/17 09:10 05104/17 20:58 101-55-3 H2 Butylbenzylphthalate NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 85-68-7 H2 4-Chloro-3-methytphenol NO ug/L 20.0 1 05/02/17 09:10 05104/17 20:58 59-50-7 H2 4-Chloroaniline NO ug/L 20.0 1 05/02/17 09:10 05/04/17 20:58 10647-8 H2 bis(2-Chloroethoxy)methane NO ug/L 10.0 1 05/02/17 09:10 06/04117 20:58 111-91-1 H2 bis(2-Chloroethyl) ether NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 111-44-4 H2 2-Chloronaphthalene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 91-58-7 H2 2-Chlorophenol NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 95-57-8 H2 4-Chlorophenylphenyl ether NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 7005-72-3 H2 Chrysene ND ug/L 10.0 1 05/02/17 09:10 05104117 20:58 218-01-9 H2 Dibenz(a.h)anthracene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 53-70-3 H2 Dibenzofuran NO ug/L 10.0 1 05/02/17 09,10 05/04/17 20:58 132-64-9 H2 1,2-Dichlorobenzene NO uglL 10.0 1 05102/17 09:10 05/04/17 20:58 95-50-1 H2 1,3-Dichlorobenzene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 541-73-1 H2 1,4-Dichlorobenzene NO ug/L 10.0 1 05/02/17 09:10 05/04117 20:58 106-46-7 H2 3,3'-Dichlorobenzidine NO ug/L 20.0 1 05/02/17 09:10 05/04/17 20:58 91-94-1 H2 2,4-Dichlorophenol ND ug/L 10-0 1 05/02/17 09:10 05/04/17 20:58 120-83-2 H2 Diethylphtha late NO ugtL 10.0 1 05/02/17 09:10 05/04/17 20:58 84-66-2 H2 2,4-Dirnethylphenol NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 106-67-9 H2 Dimethyfphthatate ND ug/L 10D 1 05/02/17 09:10 05/04/17 20:58 131-11-3 H2 Di•n-butylphthalate NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 84-74-2 H2 4,6-Dinitro-2-methylphenol NO ug/L 20.0 1 05/02/17 09:10 05/04/17 20:58 534-52-1 H2 2,4-Dinitrophenol ND ug/L 50.0 1 05/02/17 09:10 05/04/17 20:58 51-28-5 H2 2,4-Dinitrotoluene NO ug/L 100 1 05/02/17 09:10 05/04/17 20-58 121-14-2 H2 2,6-Dinitrotoluene ND ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 606-20-2 H2 Di-n-octylphthalate NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 117-84-0 H2 bis(2-Ethylhexyl)phthalate NO ug/L 6.0 1 05/02/17 09:10 05104117 20:58 117-81-7 H2 Fluoranthene NO ug/L 10.0 1 05/02117 09:10 05104/17 20:58 206-44-0 H2 Fluorene ND ug/L 10.0 1 05Y02117 09:10 05/04/17 20i58 86-73-7 H2 Hexachloro-1,3-butadiene ND ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 87.68-3 H2 Hexachlorobenzene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 118-74-1 H2 Hexachlorocyclopentadiene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 7747-4 H2 Hexachioroethane NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 67-72-1 H2 lndeno(1,2,3-cd)pyrene NO ug/L 1&0 1 05/02/17 09:10 05/04/17 20:58 193.39-5 H2 Isophorone NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 78.59-1 H2 1-Methylnaphthatene NO ug/L 10.0 1 05102/17 09:10 05104/17 20:58 90-12-0 H2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/11/2017 04:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 28 aceAnalytical4 ~pacMbs = 9800 K ncey Ave. Suite 100 Hunter9ville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Stormwaler 4/24 Pace Project No.: 92338806 Sample: STORMWATER . Parameters Lab ID: 92338806001 Collected: 04/24/17 10:45 Results Units Report Limit DF Received: 04/28/17 11:45 Matrix: Water Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 2-Methyinaphthalene ND ug/L 10.0 1 05102/17 09:10 05/04/17 20:58 91-57-6 H2 2-Methylphenol(o-Cresol) NO ug/L 10.0 1 05/02/17 09:10 05/04117 20i58 95-48-7 H2 3&4-Methylphenot(m&p Cresol) NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 15831-10-4 H2 Naphthalene ND ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 91-20-3 H2 2-Nitroaniline NO ug/L 50.0 1 05/02/17 09:10 05IG4117 20:58 88-74-4 H2 3-Nitroanifine ND ug1L 50.0 1 06/02/17 09:10 05/04/17 20:58 99-09-2 H2 4-Nitroaniline NO ug/L 20.0 1 05/02/17 09:10 05/04/17 20:58 100-01-6 H2 Nitrobenzene NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 98-95-3 H2 2-Nitrophenol ND ug/L 10.0 1 05/02117 09:10 05/04/17 20:58 88-75-5 H2 4-Nitrophenol NO uglL 50.0 1 05/02/17 09:10 05/04/17 20:58 100-02-7 H2 N-Nitrosod imethyla mine NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 62-75-9 H2 N-Nitroso-di-n-propylamine ND ug/L 10.0 1 05102/17 09:10 05/04/17 20:58 621-64-7 H2 N-Nitrosodiphenylamine NO ug& 10.0 1 05/02/17 09:10 05104/17 20:58 86-30-6 H2 2,2'-Oxybis(1-chloropropane) NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 108-60-1 H2 Pentachlorophenol NO ug/L 25.0 1 05/02117 09:10 05/04/17 20i58 87-86-5 H2 Phenanthrene NO ug/L 10.0 1 05/02117 09:10 05/04/17 20:58 85-01-8 H2 Phenol NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 108-95-2 H2 Pyrene ND ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 129-00-0 H2 1,2,4-Trichlorobenzene ND ug/L 10.0 1 05102117 09:10 05/04/17 20:58 120-82-1 H2 2,4,5-Trichlorophenol NO ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 95-95-4 H2 2,4,6-Trichlorophenol ND ug/L 10.0 1 05/02/17 09:10 05/04/17 20:58 88-06-2 H2 Surrogates Nitrobenzene-d5 (S) 43 % 21-110 1 05/02/17 09:10 05/04/17 20:58 4165-60-0 2-Fluorobiphenyl (S) 49 % 27-110 1 05/02/17 09:10 05/04/17 20:58 321-60-8 Terphenyl-d14(S) 61 % 31-107 1 05102/1709:10 05/04/17 20:58 1718-51-0 Phenol-dB(S) 15 % 10-110 1 05/02117 09:10 05/04/17 20:58 13127-88-3 2-Fluorophenol (S) 23 % 12-110 1 05/02/17 09:10 05/04/17 20:58 367-12-4 2,4,6-Tribromophenol (S) 46 % 27-110 1 05/02/17 09:10 05/04117 20:58 118-79-6 8260 MSV Analytical Method: EPA 8260 Acetone NO ug/L 25.0 1 05102M712:47 67-64-1 L1 Benzene ND ug/L 5.0 1 05/02117 12:47 71-43-2 Bromobenzene ND ug/L 5.0 1 05/02/17 12:47 108-86-1 Bromochloromethane NO ug/L 5.0 1 05102/1712:47 74-97-5 Bromodichloromethane ND ug1L 5.0 1 05/02117 12:47 75-27-4 Bromoform NO ug/L 5.0 1 05102/1712A7 75-25-2 Bromomethane ND ug/L 10.0 1 05102/1712:47 74-83-9 2-Butanone (MEK) NO ug/L 10.0 1 05/02/17 12:47 78-93-3 terl-Butyl Alcohol ND ug/L 100 1 05/0211712A7 75-65-0 n-Butylbenzene ND ug/L 5.0 1 0510211712:47 104-51-8 sec-Butylbenzene N❑ ug/L 5.0 1 05102/1712:47 135-98-8 terl-Butylbenzene NO ug/L 5.0 1 05102/1712:47 98-06-6 Carbon tetrachloride ND ug/L 5.0 1 05/02/17 12:47 W23-5 Chlorobenzene ND ug/L 5.0 1 05102/1712:47 108-90-7 Chloroethane NO ug/L 10.0 1 05/02117 12:47 75-00-3 Chloroform NO ug/L 5.0 1 05/02/17 12:47 67-66-3 Chloromethane ND ug/L 5.0 1 05102/1712:47 74-87-3 REPORT OF LABORATORY ANALYSIS This report $hail not be reproduced, except in full. Date: 0511112017 04:03 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 28 aceAnalytical wwwpacllbbs cam j ANALYTICAL RESULTS 9800 Kinsey Ave. Suite 100 Kuntersville, NC 28078 (704)875-9092 Project: Stormwater 4/24 Pace Project No.: 92338806 Sample: STORMWATER Lap ID: 92338806001 Collected: 04124/17 10.45 Received: 04128/17 11:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 2-Chlorotofuene ND ug/L 5.0 1 05/0211712:47 95-49-8 4-Chlorototuene ND ug/L 5.0 1 05/0211712:47 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 20 1 05/02/1712A7 96-12-8 Dibromochloromethane ND ug/L 5.0 1 05/02/1712:47 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 5-0 1 05/02/17 12:47 106-93-4 Dibromomethane ND ug/L 5.0 1 05/0211712:47 74-95-3 1,2-Dichlorobenzene ND ugfL 5.0 1 05/0211712747 95-50-1 1,3-Dichlorobenzene ND uglL ' 5.0 1 05/02/17 12:47 541-73-1 1,4-Dichlorobenzene NO ugfL 5.0 1 05/02/1712:47 10646-7 Dichlorodifluoromethane ND ug/L 5.0 1 0510211712:47 75-71-8 1,1-Dichloroethane ND ug/L 5.0 1 05/02/1712:47 75-34-3 1,2-Dichlomethane ND ug/L 5.0 1 05/0211712:47 107-06-2 1,2-Dichloroethene (Total) ND ug/L 5.0 1 05/02117 12:47 540-59-0 1,1-Dichloroethene ND ug/L 5.0 1 0510211712:47 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 1 0510211712:47 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 1 05102/1712:47 156-60-5 1,2-Dichloropropane ND ug/L 5.0 1 0510211712:47 78-87-5 1,3-Dichloropropane NO ug/L 5-0 1 0510211712:47 142-28-9 2,2-Dichloropropane ND ug/L 5.0 1 05/0211712:47 594-20-7 1,1-Dichloropropene ND ug/L 5.0 1 05102/1712:47 563-58-6 cis- 1,3-Dich lorop rope ne NO ug/L 5.0 1 05102/1712:47 10061-01-5 trans-1,3-Dichloropropene ND ug& 5.0 1 05102/1712:47 10061-02-6 Diisopropyl ether NO ug/L 5.0 1 05/02117 12:47 108-20-3 Ethylbenzene ND ug/L 5.0 1 05102/1712:47 100-41-4 Hexachloro-1,3-butadiene ND uglL 5.0 1 05/0211712:47 87-68-3 2-Hexanone ND ug/L 10.0 1 05/0211712:47 591-78-6 Isopropylbenzene (Cumene) ND ug/L 5.0 1 05/02/17 12:47 98-82-8 p-lsopropyltoluene ND ug/L 5.0 1 05102/1712:47 99-87-6 Methylene Chloride ND uglL 5.0 1 05/02/17 12:47 75-09-2 4-Methyl-2-pentanone (MIRK) ND ug/L 10.0 1 05/02/17 12A7 108-10-1 Methyl-tert-butyl ether ND ug/L 5.0 1 05/02/17 12:47 1634-04-4 Naphthalene ND ug/L 5.0 1 05/0211712:47 91-20-3 n-Propylbenzene ND ug/L 5.0 1 05/0211712A7 103-65-1 Styrene ND ug/L 5.0 1 05/0211712:47 100-42-5 1, 1, 1,2-Tetrachloroethane ND ug/L 5.0 1 0510211712:47 630-20-6 1,1,42-Tatrachloroethane ND ug/L 5.0 1 05102/1712:47 79-34-5 Tetrachtoroethene ND ug/L 5.0 1 05102/1712:47 127-134 Toluene ND uglL 5.0 1 05102/1712:47 108-88-3 1,2,3-Trichforobenzene ND ug/L 5.0 1 0510211712:47 87-61-6 1,2,4-Trichlorobenzene ND ug/L 5.0 1 05/0211712:47 120-82-1 1,1,1-Trichforoethane ND ug/L 5.0 1 05102/17 t2:47 71-55.6 1,1,2-Trichloroethane ND ug/L 5.0 1 05/0211712:47 79-00-5 Trichloroethene ND ug/L 5.0 1 05/02/1712:47 79-01-6 Triehlorofluoromethane ND ug/L 10.0 1 05/02/1712:47 75-69-4 1,2,3-Trichlofopropane ND ugil- 5.0 1 05/0211712:47 96-18-4 1,2,4-Trimethylbenzene ND ug/L 5.0 1 05/0211712A7 95-63-6 1,3,5-Trimethylbenzene ND uglL 5.0 1 05/0211712:47 108-87-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/1112017 04:03 PM without the written consent of Pace AnalytioW Services, LLC. Page 7 of 28 aceAnalytical www.psoelahs.= 9800 Klncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Stormwater 4124 Pace Project No.: 92338806 Sample: STORMWATER Lab ID: 92338806001 Collected: 04/24/17 10:45 Received: 04/28117 11:45 Matrix: Water Parameters Results Units Report limit DP Prepared Analyzed CAS No. Qual 8260 MSV Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2540D Total Suspended Solids Total Suspended Solids Date: 05/11/2017 04:03 PM Analytical Method: EPA 8260 ND ug/L 10.0 1 05102/1712:47 108-05-4 ND ug/L 5.0 1 0510211712:47 75-01-4 ND ug/L 10.0 1 05/02/17 12:47 179601-23-1 ND ug/L 5.0 1 0510211712:47 95-47-6 96 % 70-130 1 05/0211712:47 460-00-4 108 % 70-130 1 05/0211712:47 17060-07-0 112 % 70-130 1 0510211712:47 2037-26-5 Analytical Method: SM 2540D 3.5 mg/L 2.5 1 05/02/17 02:27 REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, without the written consent of Pace Analytical Services, t.t.C. H1 Page 8 of 28 Raleigh April Weather 2017 - AccuWeather Forecast for NC 27601 .. ,. , . ENGLISH (NS), T -i Follow us an }arias Raleigh. NC '0 11 in partncm,hIp with III;Iad States'a11L Ih::I I Raleigh, NC Local Weather 84T I r I PersonalizeI d Forecasts: Allergies I Now Weakend Extended I Month I Radar I I MinutecasM Watch Videos March 2017 View; April - 2017 May 2017 Dale HULo Preap Snow Forecast Avg_ HI f LO Sat 411 75'149' 0 IN 0 1N 58'144' Sun 412 69'149' 0 IN 0 IN 69*144' Mon 413 76'150' 0.40 IN 0 w 69'145' Tue 414 82`163' 0 IN 0 w 69'145' Wed 415 78`153' 0.32 IN 01N 70'145' Thu 416 70*150' 0.09 IN 0 IN 70'146' Fri 417 59'143' 0 IN 0 IN 70'146' Sat 418 67`134' 0 iN 0 w 70'146' Sun 419 77138' 01N 01N 71*146' Mon 4110 78'149' 0 IN 0 IN 71'147' Tue 4111 82'155' 0 IN 0 IN 71'147' Wed 4112 83'156' 0 IN 0 IN 72*147' Thu 4113 80'154' 0 IN 0 IN 72*141' Fri 4114 81*153' 0 IN 0 IN 72`148' Sat 4115 85'161` 0 m 0 IN 72'148' Sun 4116 82'160' 0 IN 0 IN 73*148' Mon 4117 86'162' 0.051N 0 IN 73*148' Tue 4118 74*161' 0.03 1N 01N 73'149' Wed 4119 69755' 0 IN 0 IN 73'149' Thu 4120 85'156' 0 IN 0 IN 74"149' Fri 4121 89763" 0.21 IN 0 IN 74'149' Sat 4122 87'156` 0,09 IN 0 IN 74*150' Sun 4123 56'153' 0.77 IN 0 IN 74*150' Mon 4124 60'153' 4.51 IN 0 IN 75°150' Raleigh April Weather 2017 - AccuWeather Forecast for NC 27601 HiRa Preup Snow F, Avg HI I LO To- 4125 70°158' 2.171N 0 IN 75-150' Wed 4128 81'156' 0 IN O iN 75°151' l hu 4127 82*162' 0 !N 0 IN 7''151 ° Fri 4128 88°169° 0 IN 0 IN 76"!51 ° Sat 4129 89'172' O IN 0 IN 76°152' Sun 4/30 86'170° 0 02 IN 0 IN 76°152° March 2017 Temperature Graph April 2017 100 90 80 70 60 50 40 30 20 1 2 3 4 5 6 7 6 9 10 11 12 13 14 15 16 17 1S 19 20 21 22 23 24 25 26 27 2a 29 30 Avg. Hi Avg. L0 Actual Hi Actual L0 Actual N ;rni', Departure Record High 78° 72' 95° (1896) Law 55° 48- 23° (1923) Average 66' 60, +6" Prr+-,.3 8.66 in 2.92 in +5.74 in Snow 0 in OZAW*ia4 CHAIN -OF -CUSTODY ! Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. Ali relevant fields must be completed acwratety. section A sealon B Section C Raqukwd Clk4V InlorrwAioa: R,•qu d Prom s Worinaderr k"Ice Lrrlarw&a : Pt e I QT , r-cr vanif. &xVo NrA AIP Sf'roP Chonl Rouon To Jwrw* Slue 'left nr: AddMZS 4" Bay Road Copy Ta' caffv" dance meaGn, MC 278DG ibis' mail. nuvon;cs com Yutmasc oaks s F%=Qunm Phone 9t 7954!k4T7 jFu Ptujen Name. Slrlirnwalcr Pao@ Prcpa Mtanagec emwnw,ei. aoa cam. sbas f loaeelon Roqueowd DUP OM: Pr 4cd r Poi„ Prdi4 a An FM rrad 1R WTROS CnUL 9 COLLECTED Pre&ervatives ?' Grant Y/mow OW � V Q 710•e YJS [I Y6tl� WMn wfV v T SAMPLE ID � ot ; 1 �_ START cmD � m � Or* ChAr=ttr per bent. WW Ga Z *� yy IA-2-"1. -j o w � s Ssnwk Wa twM br mlqut C '� Q M o �XXQ� �< � w F = kZ33sr� DALE TIME DATC TIME, � z z z z z � o � 2 a � o � er c t : 414-d� 4till gAEGb Y fl a �r } -10 11 '. 12 ADOfTt[}W_G rr9 RELlIE LOW4Pn BY fAMILATIOM DATr- TWE BY fArf LATn9W{ DIETS TNC wwPL.E wxVI9oeO_ �. .. .. SAK➢LER KM WE MUD 9GMATURE S, c PRWTUmm of SAMPLER: n SIG,mATtNtE 01 SAMPLER: DATE 11 R Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 C � �� cs{boate submitted , o 11.1617 CERTIFICATE OF COVERAGE NO. NCG03 0 d 0 0 FACILITYNAME 9-_,4<01\ iCS I'N . COUNTY LX�ALe PERSON COLLECTING SAMPLES LABORATORY;Ia o, 4,0.�� tall Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 161(0 SAMPLE PERIOD ❑ Jan -June 'July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW^❑HQW []Trout ❑PNA []Zero -flow ❑Water Supply []SA [—]Other RECEIVED PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 JAN 17 2017 CENTRAL FILES D1n. R Si=rr1nK1 ❑ No discharge this period?z nnl Outfall No. Rate Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inchess Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L L (D•z`I �-� b•00y (aD 12 +Q- I[o 33 [o •'Z D � cb3 Feu 1L, 1 3 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali. 2 For sampling periods with no discharge at any single outfali, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date.11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 racinues tnat incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TfO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TfO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not resort Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L". where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier2, or Tier 3 responses. See General Permit text. Part iB: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month, n No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies, Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES 1N A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART it SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Moil an oriainal and one _copy.of this_DMR includinu a!1 "No Discharge" reports. within 3i7 days of receipt the lab results (or at endof monitorin eriod in the case of "No Discharge" reportsi to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date; 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 DapP 3 of 4 1 RECEIVED NC�E1�R Stormwater Discharge Outfall (SDO) JAN 17 Z017 Qualitative Monitoring Report CENTRAL FILES For aAneeonrTllgoutthisform, lease visit: htt //aortal.ncdenr.ore/web n gIws u n dessw#tab 4 Permit No.: N///_/_/_/w/_J_/ or Certificate of Coverage No.: N/-C Facility Name: County: Inspector: Phone No. Date of Inspection: 17--l-l- I(n F=r,FmIN mil_ Time of Inspection: _. �, Dom_ L-� Total Event Precipitation (inches): CENTRAL FILES DWR SECTION Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ['Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureablestorm even t"(requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter E interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, 1 certify that th♦s Wort is accurate and complete to the best of my knowledge: (Signature o'rPermitte� + Designee) Pagel of 2 SWU-242, last modified 10/2S/2012 1. Outfall Description: Outfall No. � Structure (pipe, ditch, etc.) Zaj n ur-Linj Utoi-kAd Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: C tp_ct r 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): WDA 1, 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: (�l l 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 {t2 } 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3� 4 5 7. is there any foam in the stormwater discharge? Yes 00 8. is there an oil sheen in the stormwater discharge? Yes DN 9. Is there evidence of erosion or deposition at the outfall? Yes LoNo 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 ��ace Analytical' wwwpacelabs.com Project: Stormwater 12119 Pace Project No.: 92324326 Lab ID Sampte ID 92324326001 12/19/2016 Pace Analytical Services, tLC 9800 Kinoey Ave. Suite tan Huntersville, NC 28078 (704)875-9?92 SAMPLE ANALYTE COUNT Method Analysts Analyses Reported Laboratory EPA 1664B JMS 1 PASI-C EPA 8081 SWB 24 PASI-C EPA 8082 SWB 8 PASI-C EPA 8270 RES 74 PASI-C EPA 8260 GAW 71 PASI-C SM 2540D MLS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC- Page 3 of 32 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 �aceAnai3dicale Huntersville. NC 28078 wwwpacetabs.com (704)875-9092 ANALYTICAL RESULTS Project: Stormwater 12119 Pace Project No.: 92324326 Sampie: 12/19/2016 Parameters Lab ID: 92324326001 Collected: 12/19/16 08:00 Results Units Report Limit OF Received: 12/21/16 13:00 Matrix: Water Prepared Analyzed CAS No. Oual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg1L 5.0 1 12/30/16 06:57 8081 Organochlorine Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510 Aldrin NO ug/L 0.050 1 1212311611:43 12/28/1613:40 309-00-2 alpha-BHC NO ug/L 0.050 1 12/23/16 11:43 1212811613:40 319-84-6 beta-BHC NO ug/L 0.050 1 12/2311611:43 12128/1613:40 319-85-7 delta-BHC NO ug/L 0.050 1 12123/1611:43 12126/1613:40 319-86-8 gamma-BHC (Lindane) NO ug/L 0.050 1 12/23/16 11:43 12/28116 13:40 58-89-9 Chlordane (Technical) ND ug/L 0,20 1 12/23/16 11:43 12/28/16 13:40 57-74-9 4,4'-DDD NO ug/L 0.050 1 12/23/16 11:43 12/28/1613:40 72-54-8 4,4'-DDE NO ug/L 0.050 1 12123/1611:43 12/2811613:40 72-55-9 4,4'-DDT NO ug/L 0.050 1 12123/1611:43 12/28l1613:40 50-29-3 Oieldrin NO ug/L 0,050 1 12123/1611:43 121281161140 60-57-1 Endosulfan I NO ug/L 0.050 1 12/23/16 11.43 12128/16 13.40 959-98-8 Endosulfan Il NO ug/L 0.050 1 12/23116 11:43 12/28/16 13:40 33213-65-9 Endosulfan sulfate NO ug/L 0.050 1 12/23/16 11:43 12/28/16 13:40 1031-07-8 Endrin NO ug/L 0.050 1 1212311611:43 1212811613:40 72-20-8 Endrin aldehyde NO ug/L 0.050 1 12/23/16 11:43 12/28/16 1140 7421-93-4 Endrin ketone NO ug/L 0.050 1 12/23/16 11:43 12/28/16 13.40 53494-70-5 Heptachlor NO ug/L 0.050 1 1212311611:43 1212811613:40 76-44-8 Heptachlor epoxide NO ug/L 0.050 1 12/23/16 11:43 12/28/16 13:40 1024-57-3 Hexachlorobenzene ND ug/L 0.050 1 12/2311611:43 1212811613:40 118-74-1 Methoxychlor ND ug/L 0,15 1 12/2311611:43 1212811613:40 72-43-5 Mirex NO ug1L 0.15 1 12/23/16 11:43 1212811613:40 2385-85-5 Toxaphene NO uglL 0.20 1 12123/1611:43 12/2811613:40 8001-35-2 Surrogates Teirachloro-m-xylene (S) 134 % 20.130 1 12/23/16 11 A3 12/28/16 13:40 877-09-8 S3 Decachlorobiphenyl(S) 27 % 20-130 1 12123116 11 A3 1212811613:40 2051-24-3 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Aroclor 1016) NO ug/L 0.50 1 12/23/16 11:43 12/27/16 13:44 12674-11-2 PCB-1221 (Aroclor 1221) NO ug/L 0.50 1 12123/16 11:43 12/27/16 13:44 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.50 1 12/23/16 11:43 12/27/16 13:44 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.50 1 12/23/16 11:43 12/27/16 13:44 53469-21-9 PCB-1248 (Aroclor 1248) NO uglL 0.50 1 12/23/16 11 A3 12/27/16 13:44 12672-29-6 PCB-1254 (Aroclor 1254) NO ug/L 0.50 1 12/23116 11:43 12127/16 13:44 11097-69-1 PCB-1260 (Aroclor 1260) NO uglL 0.50 1 12/23/16 11:43 12/27/16 13:44 11096-82-5 Surrogates Decachlorobiphenyl (S) 34 % 10-132 1 12/23/16 11:43 12/27/16 1144 2051-24-3 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene NO ug/L 10.0 1 12123/t611:00 12/23/1618:22 83-32-9 Acenaphthylene NO ug/L 10.0 1 12123/1611:00 12/23/1618:22 208-96-8 Aniline NO ug/L 10.0 1 12/23/1611:00 12/2311618:22 62-53-3 Anthracene NO ug1L 10.0 1 12123/1611:00 12/2311618:22 120-12-7 Benzo(a)anthracene NO ug/L 10.0 1 1212311611:00 1212311618:22 56-55-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/05/2017 10:06 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 32 Pace Analytical Services, �LC 9804 Kinoey Ave. Suite too aceanalytical Huntersville, NC 28078 www.pacetehs.cm (704)875-9092 ANALYTICAL RESULTS Project: Stormwater 12119 Pace Project No.: 92324326 Sample: 12/19/2016 Labi0: 92324326001 Collected: 12/19/16 08:00 Received: 12/21/16 13:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quat 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzo(a)pyrene NO ug1L 10.0 1 12/2311611:00 12123/1618:22 50-32-8 Benzo(b)fluoranthene ND ug/L 10.0 1 12/23/1611:00 1212311618:22 205-99-2 Senzo(g,h,i)perylene ND ug/L 10.0 1 12/23/1611:00 12/23/1618:22 191-24-2 Benzo(b)fluoranthene NO ug/L 10.0 1 12123/1611:00 12/23/1618:22 207-08-9 Benzoic Acid NO ug/L 50.0 1 12/2311611:00 12123/1618:22 65-85-0 Benzyl alcohol NO ug/L 20.0 1 12/23116 11:00 12)23116 1822 10D-51-6 4-Bromophenytphenyl ether ND ug/L 10.0 1 12/23/16 11:00 12/23/16 18:22 101-55-3 Butylbenzylphtha late ND ug/L 10.0 1 12123/1611:00 12123/1618:22 85-68-7 4-Chloro-3-methylphenol NO ug/L 20.0 1 12/23/1611:00 12123/1618:22 59-50-7 4-Chloroaniline NO ug1L 20.0 1 12123/1611:00 12123/1618:22 106-47-8 bis(2-Chloroethoxy)methane ND ug/L 10.0 1 1212311611:00 12/2311618:22 111-91-1 bis(2-Chloroethyl) ether NO ug/L 10,0 1 12/23/16 11:00 12/23/16 18:22 111-44-4 2-Chloronaphthalene NO ug1L 10.0 1 12/2311611:00 12/2311618:22 91-58-7 2-Chlorophenol NO ug/L 10.0 1 12/2311611:00 12/23/1618:22 95-57-8 4-Chlorophenylphenyt ether NO uglL 10.0 1 12/23/16 11:00 12/23116 18:22 7005-72-3 Chrysene ND ug/L 10.0 1 12/23/1611:00 1212311618:22 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 12/23/1611:00 12123/1618:22 53-70-3 Dibenzofuran ND uglL 10.0 1 12123/1611:00 12/23/1618:22 132464-9 1.2-Dichlorobenzene NO ug/L 10.0 1 12/23/1611:00 12/23/1618:22 95-50-1 1,3-Dichlorobenzene ND ug/L 10.0 1 12/2311611:00 1212311618:22 541.73-1 1,4-Dichlorobenzene ND ug/L 10.0 1 12/23/1611:00 12/2311618:22 106-46-7 3,3'-Dichlorobenzidine ND ug/L 20.0 1 12/23/1611:00 12/23/1618:22 91-94-1 2,4-Dichlorophenol ND uglL 10.0 1 12i23/1611:00 1212311618:22 120-83-2 Diethylphthalate ND ug/L 10.0 1 12123/1611:00 12/2311618:22 84-66-2 2,4-Dimethylphenol NO ug/L 10.0 1 12/23/1611:00 12/2311618:22 105-67-9 Dimethylphtha late NO ug/L 10.0 1 12123/1611:00 12/2311618:22 131-11-3 Di-n-butylphthalate ND uglL 10.0 1 12123/1611:00 12/2311618:22 84-74-2 4,6-Dinitro-2-methylphenol ND ug1L 20.0 1 1212311611:00 1212311618:22 534-52-1 2,4-Dinitrophenot ND ug/L 50.0 1 12123/1611:00 12/2311618:22 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1 12/2311611:00 12/2311618:22 121-14-2 2,6-Dinitrotoluene ND ug1L 10.0 1 12/23/1611:00 1212311618:22 606-20-2 Di-n-octylphthalate NO ug/L 10.0 1 12123/1611:00 1212311618:22 117-84-0 bis(2- Ethyl hexyi)phthalate ND ug/L 6.0 1 12/2311611:00 1212311618:22 117-81-7 Fluoranthene NO uglL 10.0 1 12123/1611:00 12123/1618'22 206-44-0 Fluorene ND uglL 10.0 1 1212311611:00 12123/1618:22 86-73-7 Hexachloro-1,3-butadiene ND ug/L 10.0 1 12/2311611:00 12//23/1618:22 87-68-3 Hexachlorobenzene NO ug/L 10.D 1 12/2311611:00 12/23/1618:22 118-74-1 Hexachlorocyclopentadiene NO ug/L 10.0 1 12/23/16 11 ;00 12)23/1618:22 77-47-4 Hexachloroethane NO uglL 10.0 1 12/2311611:00 12/23/1618:22 67-72-1 lndeno(1,2,3-cd)pyrene NO ug1L 10.0 1 1212311611:00 12/2311618:22 193-39-5 lsophorone ND uglL 10.0 1 12/2311611:00 12123/1618i22 78-59-1 1-Methylnaphthalene ND ug/L 10.0 1 12/23/1611:00 12)23/1618:22 90-12-0 2-Methylnaphthalene NO ug/L 10.0 1 12/2311611:00 12123/1618:22 91-57-6 2-Methylphenot(o-Cresol) NO ug/L 10.0 1 12/2311611:00 12/2311618:22 95-48-7 384-Methylphenol(m8,p Cresol) ND uglL 10.0 1 12/23/16 11:00 12123116 18:22 Naphthalene ND ug/L 10.0 1 12/2311611:00 12/23/1618:22 91-20-3 2-Nitroaniline ND ug/L 50.0 1 12/23/1611:00 12/2311618:22 88-74-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 01/05/2017 10:06 AM without the written consent of Pace Analytical Services. LLC- Page 5 of 32 eAnalXical. www.pwdabs,cm r8C0 Analyttca! Services, b,LC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875.902 ANALYTICAL RESULTS Project: Stormwater 12/19 Pace Project No.: 92324326 Sample: 17JI912016 Lab ID: 92324326001 Collected: 12/19116 08:00 Received: 12/21116 13:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 3-Nitroaniline NO ug/L 50.0 1 12/2311611:00 12123/1618:22 99-09-2 4-Nitroaniline NO ug/L 20.0 1 12/2311611:00 12123/1618:22 100-01-6 Nitrobenzene ND uglL 10.0 1 12/23/16 11:00 12/2311618:22 98.95-3 2-Nitrophenoi ND ug1L 10.0 1 12/23/16 11:00 121231161812 88-75-5 4-Nitrophenol NO ug1L 50,0 1 1212311611:00 121231161822 100-02-7 N-Nitrosodimethylamine NO ug/L 10.0 1 12123/16111)0 12/23/161822 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 10.0 1 12/23116 11 :00 12/23/16 18:22 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1 12/23/16 11:00 12/231161822 86-30-6 2,2'-Oxybis(1-chloropropane) NO ug1L 10.0 1 12/23/16 11:00 12/2311618:22 108-60-1 Pentachlorophenol NO ug/L 25.0 1 12/23/16 11:00 1212311618:22 87-86-5 Phenanthrene ND ug/L 10.0 1 12123/1611:00 12/23/16 18:22 85-01-8 Phenol ND ug/L 100 1 12123/16 11:00 12123116 18:22 Pyrene ND uglL 10.0 1 1212311611:00 1212311618:22 129-00-0 1,2,4-Trichlorobenzene ND ug/L 10.0 1 12123/1611;00 12/23/16 18:22 120-82-1 2,4,5-Trichlorophenoi NO ug1L 10.0 1 12123/1611:00 12/23/16 18:22 95-95-4 2,4,6-Trichlorophenol NO ug/L 10.0 1 12123/1611:00 12/23/16 18:22 88-06-2 Surrogates Nitrobenzene-d5 (S) 34 % 21-110 1 12/23/16 11:00 12/23/16 18:22 4165-60-0 2-Fluorobiphenyl (S) 33 % 27.110 1 12/23/16 11:00 12/23/16 18:22 321-60-8 Terphenyl-d14 (S) 50 % 31.107 1 12123/1611:00 12123/16 18:22 1718-51-0 Phenol-d6 (S) 13 % 10-110 1 12123/16 11:00 12/23/16 18:22 13127-88-3 2-Fluorophenoi (S) 19 % 12-110 1 12123/16 11:00 12/23/16 18:22 367-12-4 2,4.6-Tribromophenol (S) 48 % 27-110 1 12/23/16 11:00 12/23/16 18:22 118-79-6 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 12130/1613:52 67-64-1 Benzene NO ug/L 5.0 1 12/30/1613:52 7143-2 Bromobenzene ND ug/L 5,0 1 12/30/1613:52 108-86-1 Bromochloromethane ND ug/L 5.0 1 12t3011613:52 74-97-5 Bromodichloromethane ND ug/L 5 0 1 12130/16 13:52 75-27-4 Bromoform ND uglL 5.0 1 12/3011613:52 75-25-2 Bromomethane ND uglL 10.0 1 1213011613:52 74-83-9 2-Butanone (MEK) ND ug/L 10.0 1 12/30/16 13:52 78-93-3 tert-Butyl Alcohol ND ug/L 100 1 12/30/16 13:52 75-65-0 n-Butylbenzene ND ug/L 5.0 1 12/3011613:52 104-51-8 sec-Butylbenzene NO ug/L 5.0 1 12/30/1613:52 135-98-8 tert-Butylbenzene NO ug/L 5.0 1 12/30/1613:52 98-06-6 Carbon tetrachloride NO ug/L 5.0 1 12130116 13:52 56-23-5 Chlorobenzene ND ug1L 5,0 1 12I30/1613:52 108-90-7 Chloroethane NO ug/L 10.0 1 1213011613:52 75-00-3 Chloroform NO ug/L 5.0 1 12/30/1613:52 67-66-3 Chloromethane NO ug/L 5.0 1 12130/1613:52 74-87-3 2-Chiorotoluene NO ug1L 5.0 1 1213011613:52 95-49-8 4-Chlorotoluene NO ug/L 5.0 1 12/3011613:52 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 12/30/1613752 96-12-8 Dibromochloromethane NO ug/L 5.0 1 12/3011613:52 12448-1 1.2-Dibromoethane (EDB) ND uglL 5.0 1 12/30116 13:52 106-934 REPORT OF LABORATORY ANALYSIS M1 This report shall not be reproduced, except in full. Date: 01/05/2017 10:06 AM without the written consent of Pace Analytical Services, LLC- Page 6 of 32 �acceAnalyftca( www.pac&Ubs.=n race ,analytical services, I&C 9800 Kincey Ave. Suite 100 Huntersville, NC 2807E (704)875.9092 ANALYTICAL RESULTS Project: Stormwater 12119 Pace Project No.: 92324326 Sample: 12119/2016 Lab ID: 92324326001 Collected: 12119116 08:00 Received: 12/21/16 13:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Dibromomethane ND ug/L 5.0 1 12/3011613:52 74-95-3 1,2-Dichlorobenzene ND ugll- 5.0 1 12/30/1613-52 95-50-1 1,3-Dichlorobenzene NO ugiL 5.0 1 12/30/1613:52 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 1 12/30/1613:52 106-46-7 Dichlorodifluoromethane NO ug/L 5.0 1 12/3011613:52 75-71-8 1,1-Dichloroethane NO ug/L 5.0 1 1213011613:52 75.34-3 1.2-Dichloroethane NO ug/L 5.0 1 12/30/1613:52 107-06-2 1,2-Dichloroethene (Total) NO ug/L 5.0 1 12/30/16 13:52 540-59-0 1,1-Dichloroethene NO ug/L 5.0 1 12130/1613:52 75-35-4 cis- 1,2-Dichloroethene NO ug/L 5.0 1 12130/1613:52 156-59-2 trans- 1. 2-Dichloroethene NO ug1L 5.0 1 12/3011613:52 156-60-5 1,2-Dichloropropane ND uglL 5.0 1 12/30/1613:52 78-87-5 1,3-Dichloropropane NO ug/L 5.0 1 12/3011613:52 142-28-9 2,2-Dichloropropane NO ug/L 5.0 1 1213014613:52 594-20-7 1,1-Dichloropropene NO ugiL 5.0 1 12/3011613:52 563-58-6 cis- 1,3-Dichloropropene NO ug/L 50 1 12/30/16 13:52 10061-01-5 trans-1,3-Dichloropropene ND ug/L 5.0 1 12/3011613:52 10061-02-6 Diisopropyl ether ND ug/L 5.0 1 12/30/16 13:52 108-20.3 Ethylbenzene NO ug/L so 1 12/30116 13:52 100-41-4 Hexachloro-1,3-butadiene ND ug/L 5.0 1 12130/1613:52 87-68-3 2-Hexanone NO ug/L 10.0 1 12130/1613:52 591-78-6 Isopropylbenzene (Cumene) ND ug/L 5.0 1 12/30/16 13:52 98-82-8 p-Isopropyltoluene ND ug/L 5.0 1 1213011613:52 99-87-6 Methylene Chloride NO ugiL 5.0 1 12130/16 13:52 75-09-2 4-Methyl-2-pentanone (MIBK) NO ugiL 10.0 1 12/30/16 13:52 108-10-1 Methyl-tert-butyl ether NO ug/L 5.0 1 12/30/16 13:52 1634-04-4 Naphthalene NO ug/L 5.0 1 1213011613:52 91-20-3 n-Propylbenzene NO ug1L 5.0 1 12130/1613:52 103-65-1 Styrene ND ug/L 5.0 1 12/30/1613:52 100-42-5 1,1,1,2-Tetrachloroethane NO ug/L 5.0 1 12/30/1613-52 630-20-6 1,1,2,2-Tetrachloroethane NO ug1L 5.0 1 1213011613:52 79-34-5 Tetrachloroethene NO ugiL 5.0 1 12/30/1613:52 127-18-4 Toluene ND ug/L 5.0 1 12/30/1613:52 108-88-3 1,2,3-Trichlorobenzene NO ugk 5.0 1 12/30/1613:52 87-61-6 1, 2,4-Trich lo ro benzene NO ug/L 5.0 1 1213011613:52 120-82-1 1,1,1-Trichloroethane NO ug/L 5.0 1 1213011613:52 71-55-6 1,1,2-Trichloroethane ND ugiL 5.0 1 12/30116 13:52 79-00-5 Trichloroethene ND ug1L 5.0 1 12/30/4613:52 79-01-6 Trichlorofluoromethane ND ug/L 10.0 1 12/30/1613:52 75-69-4 M1 1,2,3-Trichioropropane ND ug1L 5.0 1 12/3011613:52 96-18-4 1,2,4-Trimethylbenzene NO ug/L 5.0 1 1213011613:52 95-63-8 1,3,5-Trimethylbenzene ND ug/L 5.0 1 12/30/161152 108-67-8 Vinyl acetate NO ug/L 10.0 1 12/30/16 13:52 108-05.4 Vinyl chloride ND ug1L 5.0 1 12/30/16 13:52 75-01-4 m&p-Xyiene NO ug/L 10.0 1 12/30/1613:52 179601-23-1 o-Xylene NO ug/L 5.0 1 12/3011613:52 95-47-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01/05/2017 10:06 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 32 ,�aceAnaljdicai" wwwpacelabs.mrn ANALYTICAL RESULTS Project: Stormwater 12/19 Pace Project No.: 92324326 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-£-092 Sample: 12/19/2016 Lab lD: 92324326001 Collected: 12119/16 08:00 Received: 12/21/16 13:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Surrogates 4-Bromoftuorobenzene (S) 103 % 70-130 1 12/30/16 13:52 460-00-4 1,2-Dichloroethane-d4 (S) 104 % 70-130 1 12/30/16 13:52 17060-07-0 Toluene-d8 (S) 109 % 70-130 1 12/30/16 13:52 2037-26-5 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 23.0 mg1L 8.3 1 12/23/16 10:58 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01 /05/2017 10:06 AM without the written consent of Pace Analytical Services, Ll-C, Page 8 of 32 Semi-annual Stormwater Discharge Monitoring Report North Carolina Division of Water Quality General Permit No. NCG030000 e submitted CERTIFICATE OF COVERAGE 0. NCG03 a L L FACILITY NAME L>R rC J-n G COUNTY PERSON COLLECTING SAMPLES 3rb1AC-_S 9 (_LX ry LABORATORY CQ M P L,- &%v nn Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2()I SAMPLE PERIOD ❑ Jan -June July -Dec or ❑ Monthly'_ _ (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA p []zero -flaw ❑Water Supply []SA �T&Cile1V ❑Other DEC. 2 ® I CF $ ZQ15 PLEASE REMEMBER TO SIGN ON PAS .2 AND/OR 3 3 DWR SELF/Les �/ Tbiv No discharge this period?' Clutfall No. Date Sample Collected' (mo/dd/yr) 24rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non-Polar O&G/hour Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L Z C -60 t G- 6003 A 6 12 b b3b .2pf M WD3 L Z ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of T tal Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the d6 1 �n s found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use thldeIF ftio has f rind in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Py Permit Date; 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Pmao 1 of i Facilities that i ncorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the 5tormwater Pollution Prevention Plan." Name (Print name) Title (Print title} {Signature) (bate) (Vote: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, NO, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mgL where XX is the numerical value of the detection limit, reporting limit, etc, in mg/L. Note: If you report o sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera! Permit text. Part B. Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outial! No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 -- 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 AAA NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this farm, please visit. http: //portal.ncdenr.org/web/wgjws jsu/npdessw#tab-4 Permit No.: N/C/_/_/�/T/ _/_/Y/ or Certificate of Coverage No.: Facility Name+ eS U�nc, County: RAV-6 Phone No. Li- 271 Inspector Date of Inspection: Time of Inspection: I� Total Event Precipitation (inches): d . IC4 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) [0 Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 01 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfail. The previous measurable storm event must have been at least 72 hours 1 prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Perri ttee or Designee) 12-17-I,�— Page 1 of 2 SWU-242, Last modified 10/25/2012 U 1. Outfall Description: Outfall No. 1 , Z - 3 Stru ure (pipe, ditch, etc.) Receiving Stream: Zca Describe the industrial activities that �f 4 V Ek211u - q� rc)J Lzyi� e� % A a within the outfall drainage arpea:-- L-. LW OO-J I w v, � 1L , ACL V L..1 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: C [ e zr- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): N 0 A f1 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and S is the surface covered with floating solids: 1 G 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 � 3 4 5 7. Is there any foam in the stormwater discharge? YesN S. Is there an oil sheen in the stormwater discharge? Yes a� 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution, List and describe l Vela, Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 ANALYSIS DATA SHEET STORMWATER Client: SURTRONICS Lab ID' 1508031-01 SDG: 1508031 Project: STORM WAFER %Solid; Matrix; Water Sampled: 08/11/15 Received: 08/12/15 CAS NO. Analvte Canc. (mg1L) MD1, RL D.F. Q Method Sequence Anak•zed A GREASE Oil & Grease (SG'r-HE:%t) 1.98 0.832 5.00 1 J EPA 1664A 5H 19013 8118I15 9J 5 TSS Total Suspended Solids 13,1 0.416 5A0 1 SNt 2540D 5H 14001 8/13/15 BAR w Llt��rty Ar�elytical "�v �N ACCOg0A o '�' Page 14 of 18 Client: SURTRONICS Matrix: Water Initial/Final: 500mL / 2500ul- Dilution: I pH: % Moisture: NA Batch: 5081308 ANALYSIS DATA SHEET 8082A SDG: 1509031 Extraction: EPA 3510C GC Sul Fur Cleanup: N Florisil Cleanup: N GPC Cleanup: N Sequence: 5H 17010 Project: STORM WATER File ID: 020c1508031-0t.d Lab ID: 1509031-01 GPC Cleanup Factor; N Calibration: 5082006 STORMWATER Sampled: 08/ l 1115 13:15 Received: 08112,15 10:50 Prepared: 081171'15 10:25 Analyzed; 081181'15 01:29 Instrument: traceac86 CAS NO, COMPOUND CONC. (ug/L) MDL RL Q 12674-11-2 Aroclor-1016 0.073 0.50 U 11104-28-2 Aroclor-1221 0,064 0.50 U 11141-16-5 Aroclor-1232 0.065 0.50 U 53469-21-9 Aroclor-1242 0.14 0.50 U 12672-29-6 Aroclor-1248 0.044 0.50 U 11097-69-1 Aroclor-1254 0.072 0.50 U 11096-82-5 Aroclor-1260 0.050 0.50 U SYSTEM MONITORING COMPOUND ADDED (ug/L) CONC (ug/L) % REC QC LIMITS Q DCB (A) 0.6000 0.4724 79 43 - 144 DCB (A) l2Cl 0.6000 0.6039 101 43- 144 TCX {A) 0.3000 0.2648 88 43 - 135 TCX (A) f2Cl 0.3000 0.3356 1 l2 43 - 135 * Values outside of QC limits ��O N A C C O qD-4 F Llbc r•ty Ar�al�ytlCai Page 17 of 21 Client: SURTRONICS Matrix: Water Initial/Final: 500mL 1 500uL Dilution: I PH: % Moisture: NA Batch: 5081306 ANALYSIS DATA SHEET SW8270D SDG 1508031 Project: STORM WA,rFR Extraction: FPA 3510C SVOA Pile ID: 1508031-0162.d Sulfur Cleanup: Ill Lab ID: 1508031-01 Florisil Cleanup: N GPC Cleanup: N GPC Cleanup Factor: N Sequence: 5H17005 Calibration: 5072408 STORMWATER Sampled: 08/1 1115 13:15 Received: 08/12/15 10:50 Prepared: 08/ 17/15 10:25 Analyzed: 08/ 17/ 15 19:01 Instrument: 5972hp62 CAS NO. COMPOUND CONC. (ug/L) MDL RL Q 84-74-2 Di-n-butylphthalarc 0.74 5.0 U 206-44-0 Fluoranthene 0.58 5.0 U 92-87-5 Benzidine 2.0 5.0 U 129-00-0 Pvrcne 0.73 5.0 U 85-69-7 9utylbenzy1phthalate 0.55 5.0 U 91-94-1 3,3'-Dichlorobenzidine 1.4 5.0 U 117-91-7 bis(2-ethylhexy1)Phthala1e 057 5.0 U 56-55-3 Benzo (a) ambracene 0,57 5.0 U 218-01-9 Chrysene 2,2 5.0 U 117-84-0 Di-n-octylphthalate 0,71 5.0 U 205-99-2 Benzo (b) fluoranthene 0.68 5.0 U 207-08-9 Benzo(k)fluoranthene 1.5 5.0 U 50-32-8 Benzo (a) pyrene 0.70 5.0 U 193-39-5 1ndeno(1,2,3-cd)pyrene 0.64 5.0 U 53-70-3 Dibenzo(a,h)anthracene 0.74 5.0 U 191-24-2 Benzo(g,h,i) perylene 0.61 5.0 U 122-66-7 1,2-Diphenyl Hydrazine 0.79 5.0 U SURROGATE RECOVERY RESULTS ADDED (ug/L) CONC (ug/L) % RLC QC LIMITS Q 2-Fluorophenol 100.0 52.07 52 33 - 110 Phenol-d5 100.0 39.84 40 20 - 110 Nitrobenzene-d5 50.00 33.53 67 45 - 110 2-Fluorobiphcnvl 50.00 31.20 62 46 - 110 2,4,6-Tribromophenol 100.0 84.14 84 42 - 119 Terphenvl-dl4 50.00 38.25 76 59 - 110 CAS NO. TICS CONC. (ug/L) Response R.T. % Match Q 55335-06-3 Acetic acid, [(3,5,6-trich loro-2-pyrid in 4.9 405444 16,925 96 JN 143-22-6 Ethanol, 6.0 508922 13.161 86 JN NA Unkno«n 6.068 14 940987 6.068 0 J (1) - N-nitrosodiphenylain ine cannot be separated from diphenylamine. It is acceptable to report the combined result. (2) - 112-Dipheny1hydrazine is unstable and converts to azobenzene, (3) - 3 & 4-Methylphenol cannot be separated for quantization. l..lbc�rty A�alytical P c� Page 17 of 21 Client: SURTRONICS Lab ID: 51-I19008-SRDI Sequence: 5H19008 SERIAL DILUTION EPA 6020A Matrix: Water SDG: 1508031 Project: STORM WATER Lab Source ID: 1508031-01 Dilution: 5 STORN1WATERL Source Sample: STORMWATER Report to MDL: YES Initial Sample Analyte Result (1) Serial Dilution Result (S) RL % Difference Q Method QC Limits % Difference Copper 19.30 20.43 2.00 5.98 EPA 6020A 10 Lead 3.72 168 J I 1.11 EPA 6020A 10 Zinc 121.23 128.08 2,00 5.65 EPA 6020A 10 w ��[aPrry .o,r-tietUr���t 1AAC C C 0 9dq �C+ Page 12 of 15 Client: SURTRONICS Matrix: Water Initial/Final: 500ml, / 2500ul- Dilution: 1 pH: % Moisture: NA Batch: 5081307 ANALYSIS DATA SHEET 8081B SDG: 1508031 Extraction: EPA 3510C GC Sulfur Cleanup: N Florisil Cleanup: N GPC Cleanup: N Sequence: 5 H 18003 Project: STORM WATER File ID: 0170508031-01A LablD: 1508031-01 GPC Cleanup Factor: N Calibration: 5082004 STORMWATER Sampled: 08/ 1 1/ l 5 l 3:15 Received: 09/ 12/ 15 10:50 Prepared: 08/17/15 10:25 Analyzed: 08/18/15 l 8:49 lnstrument: tracegc80 CAS NO. COMPOUND CONC. (uglL) MDL RL Q 319-84-6 alpha-BHC 0.016 0.0019 0.025 JP 58-89-9 gamma-BHC (Undane) 0.033 0.0019 0.025 B 76-44-8 Heptachlor 0.016 0.0024 0.025 JBP 309-00-2 A]drin 0.0027 0.025 U 319-85-7 beta-BHC 0.031 0.0095 0.025 319-86-8 delta-1311C 0.015 0.0032 0.025 J 1024-57-3 Heptachlor epoxide 0.0029 0.025 U 939-98-8 Endosulfan1 0.041 0.0043 0.025 72-55-9 4,4'-DDE 0.0039 0.050 U 60-57-1 Dieldrin 0.0051 0.050 U 72-20-8 Endrin 0.0069 0.050 U 72-54-8 4,4'-D[)D 0,013 0.0055 0.050 JP 33213-65-9 Endosuifan II 0.0065 0.0055 0.050 J 50-29-3 4,4'-DDT 0.011 0.0051 0.050 JP 7421-93-4 Endrin aldehyde 0.012 0.050 U 1031-07-8 Endosulfan sulfate 0.0068 0.050 U 8001-35-2 Toxaphene 0.48 2.5 1J 57-74-9 Technical Chlordane 0.24 0.80 U SYSTEM MONITORING COMPOUND ADDED (ug/L) CONC (uglL) % REC QC LIMITS Q DCB (A) 0.6000 0.4586 76 44 - 141 DCB (A) 12C1 0.6000 0A396 73 44 - 141 TCX (A) 0.3000 0.2290 76 42 - 115 TCX (A) 12C1 0.3000 0.2990 100 42 - 115 * Values outside of QC limits w L It7C rty .4r-�alytical Page 18 of 22 CHAIN OF CUSTODY 29079 Page — of — A Division 501 Madison Ave. %NLiberty Analytical Corp. Cary. NC 27513 Phoilc:919-379-4100 Fax9l9-379-4040 Courier Airbill No. Sam pling Completc. Y or N ic�nrting Infournation:;'...: formatitid CompnNam ) Project Nac llir1L-M1,C5 <36 (3 C,� GW - Ground water WW - Waste water SW - Surface water SO - Soil/Sediment TB - Trip Blank Rl - Rinsatc Wr - Wipe 0 - Other Address Sampling Location City Stale Zip Turnaround time i C,3 Project ContactBatch m Vue, QC or Project Specific'? I(Specific, which Sample ID? Pho,tle# Are aqueous samples field Filtered I , or Lndak? Y or N saalpler's Name Are high concentrations expected? Y or N? If yes, which I D(s)? E., C06AOChe'nvNo'� Field ID Collection Matrix #or bottles Number of Preserved Boltics Date Time 0 0 0 V) 0 150`3V -01 S-11ftVA-IFUL 9-111 )25 17 ;y 1 1 Lab Use U4317113 Sam le Unpacked By: ICyanide samples checked for sulfide & chlorine? Y o NA 1625 & Phenol samplei checked for chlorine'? Y oAA Sample Order Entry By: Samples Received in Good C do r N 1608 samples checked for pH between 5.0-9.0? Y o nNA If no. explain: yy Relingwished h Date/Time:-1 6Y9 J,Y1/S Received b4 Daterrime: Relinquished b Date/Time: Received b Date/Time: ,Subcontact-? Y o4N If yes, where? Custody Seals ) intact? Y 0�0 On Icef Y),, N Cooler TeTR: -C Samples stored 60 dalyq4fter date report mailed at no extra charge. Z364— APLThits & Yellow copy to lab - Pink copy forWsl(PR�,Obj <, A _. 1A J 44 0 01 rd 124 Weather History for RDU, North Carolina I Weather Underground Page 1 of 4 report this ad Raleigh -Durham International, NC A Raleigh -Durham International Weather History for KRDU - August, 2015 August i 2015 Tuesl�ay August 11, 2015 Daily i Weekly � Monthly Custom Actual Temperature Mean Temperature Max Temperature Min Temperature Degree Days Heating Degree Days Month to date heating degree days Since 11une heating degree days Since 1 July heating degree days Cooling Degree Days Month to date cooling degree days Year to date cooling degree days Since 1 June cooling degree days Growing Degree Days Moisture Dew Point Average Humidity Maximum Humidity Minimum Humidity Precipitation Precip;tation Month to date precipitation 78 IF 87IF 69 IF 0 0 0 0 13 158 1337 1067 28 (Base 501 69 IF 79 97 60 0.29 in 1.99 Average [KRDUI 79 IF 89 °F 69'F 0 D 4 0 14 159 1181 972 0.12 in 1.52 D 2:17 PM EST on December 17, 2015 [GMT -05001 Record [KRDUI 101 °F (19991 59 *F 119721 2.11 In [20011 hap;//www.wunderground.com/history/airport/RDU/2015/8/1 l /Dai]yH istory.html?req_city=&req_state=&req... 12/ 17/2015 Weather History for RDU, North Carolina I Weather Underground Page 2 of 4 Actual Average [KRDU] Year to date precipitation 31.19 26.130 Sea Level Pressure Sea Level Pressure 29.90 in Wind Wind Speed 7 mph [SW I Max Wind Speed 21 mph Max Gust Speed 32 mph Visibility 9 miles Events Rain, Thunderstorm T = Trace of Precipitation. MM = Missing Value Source: NWS Daily Summary Daily Weather History Graph Temper=e Dew Pont Normai FEig111Lota 90 800 _ �o 65 55 midnight 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 In Hg Barometric Pressure 30.0 299 29.8 midrottl 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 3 10 11 mph .....s r 28.0 8 midnightt 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 360.0 270.0 180.0 90.0 00 midnigh 1 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 report this ad I why ads? Search for Another Location Airport or City: KRD[i Submit hpa 1016 1013 1008 Record [KRDU] Trip Planner Search our weather history database for the weather conditions in past years. The results will help you decide how hot, cold. wet, or windy it might be! Date: http://www.wunderground.comAiistory/airporuRDU/2015/8/1 I /DailyHistory.htm l?req_city=&req_state=&req... 12/ 17/2015 Weather History for RDU, North Carolina f Weather Underground Page 3 of 4 August ' 11 Submit Astronomy Aug. 11, 2015 Actual Time Civil Twilight '............... Nautical Twilight Astrnnomicai Twilight _..._--•--------------•---- Moon Len [h of Visible Li ht Length of DaY report this ad I why ads? Rise Set 6:30 AM EDT 8:09 PM EDT 6:02 AM EDT 8:37 PM EDT 5:29 AM EOT 9:10 PM EDT 4:54 AM EDT 9:45 PM EDT 3:47 AM EDT 18/111 f p01 PM EDT (8/11) 14h 34m 13h 39m Waning Crescent, 9% of the Moon is Illuminated Aug 11 Aug 14 I Waning Crescent New Hourly Weather History & Observations Aug 22 Aug 29 First Quarter Full report this ad I why ads? I T�Y Sep 5 I Last Quarter Time [EDT[ Temp. Heat Index Dew Humidity Pressure Visibility Wind Wind Gust Precip Events Conditions Paint Dir Speed Speed 12:51 AM 77.0 IF - 66.0 IF 69% 29.91 in 10.0 mi South 8.1 mph - N/A Mostly Cloudy 3:51 AM 77.0 IF - 63.0 ° F 62 % 29.91 in 10.0 mi SSW 8.1 mph - N/A Overcast 2:51 AM 75.9 ° F 64.0 ° F 67% 29.90 in 10.0 mi SSW 10.4 mph N/A Overcast 3:51 75.0 °F - 64.9 °F 711/6 29.88 in 10.0 mi SSW 8.1 mph - N/A Overcast AM 4:51 AM 75.0 °F - 66.9 °F 76% 29.8a in 10.0 mi SSW 9.2 mph - N/A Overcast 5:51 75.0 IF - 68.0 IF 79% 29.88 in 10.0 mi SSW 9.2 mph - NIA Overcast AM 6:51 AM 75.9 IF - 69.1 IF 79% 29.89 in 10.0 mi SW 12.7 mph - NIA Overcast 7�5AM AM 77.0 °F - 70.0 IF 79% 29.90 in 10.0 mi SW 12.7 mph - N/A Mostly Cloudy 8:51 AM 75.9 IF - 70.0 IF 82 % 29.92 in 10.0 mi WSW 10.4 mph 18.4 mph N/A Overcast 77.0 IF - 70.0 °F 79% 29.93 in 10.0 mi WSW 10.4 mph - N/A Overcast AM AM 10-51 AM 73.9 °F - 71.1 °F 91% 29.93 in 6.0 mi SW 8.1 mph - 0.01 in Rain Light Rain http://www.wunderground.com/history/airporURDU/2015/8/1 1/DailyHistory.html?req_city=&req_state=&req... 12/17/2015 Weather History for RDU, North Carolina I Weather Underground Page 4 of 4 Time Temp. Heat new Humidity Pressure Visibility Wind Wind Gust precip Events Conditions [E011 Index Point 0ir speed Speed 11:51 73.9 IF - 72.0 IF 93% 29.92 in 8.0 mi sw 6.9 mph - 0.09 in Rain Light Rain AM 12:51 75.0 IF - 72.01F 90% 29.92 in 10.0 mi WSW 8.1 mph - 0.00 in Rain Light Rain PM 1:16 PM 75.2 IF - 73.4IF 94% 29.93 in 10.0 mi SW 9.2 mph - 0.00 in Overcast 1:51 PM 77.0 °F - 73.0 IF 88% 29.90 in 10.0 mi SW 6.9 mph - 0.00 in Mostly Cloudy 2:5F 81.0 °F 86.2 IF 73.9 °F 79% 29.88 in 10.0 mi SSW 6.9 mph - N/A Mostly Cloudy PM 3:51 82.9 IF 88.8 °F 73.0 °F 72% 29.85 in 10.0 mi South 5.8 mph N/A Mostly Cloudy PM 4:51 86.0 IF 93.0 IF 73.0 IF 65% 29.84 in 10.0 mi WSW 92 mph - N/A Scattered Clouds PM 5.51 84.9 ° F 91.4' F 73.0 e F 671/. 29.83 in 10.0 mi South 4.6 mph - N/A Mostly Cloudy PM 6:39 Rain, Heavy PM 71.6 °F - 64.4 IF 78 % 29.91 in 2.0 mi WNW 12.7 mph 32.2 mph 0.05 in Thunderstorm Thunderstorms and Rain 6:45 Rain, Heavy 69.8 IF - 66.2 °F 88% 29.91 in 1.0 mi NW 4.6 mph 28.8 mph 0.13 in Thunderstorms and PM Thunderstorm Rain 6:49 69.81F - 66.2 IF 88% 29.90 in 2.0 mi Variable 3.5 mph 16.1 mph 0.16 in Rain. Thunderstorms and PM Thunderstorm Rain 6:51 Rain, Thunderstorms and PM 700 IF - 66.0 °F 87% 29.89 in 3.0 mi Variable a.$ mph 16.1 mph 0.17 in Thunderstorm Rain Light PM 71.6 ° F 68.0 IF 88% 29.90 in 6.0 mi SSW 4.6 mph 0.00 in Thunderstorm Thunderstorms and Rain 7:53 Rain, Light PM 72.0IF - 69.1 °F 91% 29.88 in 7.0 mi South 5.8 mph - 0.01 in Thunderstorm thunderstorms and Rain 8:31 71.6 °F - 68.0 IF 88% 29.89 in 10.0 mi SW 5.8 mph - 0.01 in Mostly Cloudy PM 8.51 70.0 °F 68.0 IF 93% 29.88 in 10.0 mi WSW 8.1 mph 0.01 in Mostly Cloudy PM 9:51 70.0 IF 68.0 IF 93% 29.90 in 10.0 mi WSW 4.6 mph N/A Mostly Cloudy PM 10:23 698 IF - 66.2 °F 881/6 29.92 in 10.0 mi WSW 3.5 mph - N/A Scattered Clouds PM 10: 69.1 IF - 68.0 IF 96% 29.90 in I0.0 mi WSW 5.8 mph - N/A Scattered Clouds PPM M 11:51 69.1' F - 68.0 IF 96% 29.90 in 10.0 mi West 3.5 mph - N/A Scattered Clouds PM report this ad hup:l/www.wunderground.com/history/airportJRDU/2015/8/11/DailyHistory.him I?req_city=&req_state=&req... 12/17/2015 -�- Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 ate submitted NCCr6,3 CERTIFICATE OF COVERAGE NO. NCG03-c 0 Qb��D FACILITYNAME rbAti;A 1Ac COUNTY_ inED.k� _ PERSON COLLECTING SAMPLES „�Rre►EiSL. _ LABORATORYresmaLx iR cM. lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2-rJ IS SAMPLE PERIOD [�f 'Jan -June ❑ July -Dec or [] Monthly' (month) DISCHARGING TO CLASS ❑ORW [JHQW []Trout ❑PNA RErPIVED []Zero -flow ❑Water Supply []SA []Other .1s 0: 6 S 2015 Uft o__GT10N PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -� III FIZA1TON PROCESSING UNIT ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks =_-> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L D-on -5&o% L 0oW Y ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° 5ee General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 racniiies tnat incorporate a solvent management plan into the Storrnwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. i further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) CM Title (Print title) ,/, (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format, When results are below the applicable Hmits,,'theY must be reported in the format, "<XX mg/L"' where XX is the numerical value of the detection Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. [] No discharge this period?z Qutfal! No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L , 100 mg/L or 50 mg/L' 6.0 — 9.0 SU Footnotes from Part A also apply to this Part 8 rt See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 *- Page 2 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 11-31-iU L� CERTIFICATE OF COVERAGE NO. NC OP6O Z? nC�4/ SAMPLE COLLECTION YEAR 201 `- FACILITY NAME CORs r SAMPLE PERIOD ❑ Jan -June July Dec COUNTY er or monthly' (month) PERSON COLLECTING SAMPLES p:mcS uu`e DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout [JPNA LABORATORY Cr M41t t �Ncft Lab Cert. t# RECEIVED ❑Zero -flow ❑Water Supply ❑SA Comments on same ee cl ollection or analysis: ❑ Other Part A: Stormwater Benchmarks and Monitoring Results JAN 0 2 2915 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL FILES DWR SECTION ❑ No discharge this period?z Clutfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids PH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks =__> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L I L t� • a• oab o -L- o - 2 7. u Z -0 Z-1 m (,.t p 0-owl, 2.2 1 2Z • L} 3 ci -Z-li4 2Z.. 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceed'ance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sitesfrnay be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (70), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the storrnwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. 1 further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be,reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non detect, ND, or other similar -non -numerical format. When results are below the applicable limits, they must be retorted in the format, "<XX m L", where XX is the numerical value of the detection limit,•reporting limit,•etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gat of new oil per month. ` n No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24•hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA. 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 su Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving watercl"assifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 2 of 3 Semi-annual Stormwater Discharge Monitoring Report for North arolina Division of Water Quality General Permit No, NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. FACILITY NAME S t9ACbA 6 COUNTY PERSON COLLECTING SAMPLES JRrINES jjt" LABORATORY Cbr''4 aM Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2J2� 14 SAMPLE PERIOD [✓Jan -June ❑ July -Dec or ❑ Monthly' (month) ����RGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA C ❑Zero -flow []Water Supply ❑SA J U L 21 2014 ❑Other CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 OWQIBOG No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L - ►1—� 0 . 11. i0 (0.13 G - (?L3 0.0 0 - I l -A • `1 4 Wb k 19 • to L0.33 -c5 -6c4 -It "I re l% o. t .3 1% 0-W . 4, 0 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requitement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement; "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) ,!!�M Title (Print title) 711 Vey (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or.other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX m L", where XX is the numerical value of the detection limit, reporting limit, etc. in-mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfail No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA, 1664 (5GT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 r AjA NCDENR Stormwater Discharge 4utfall (SOO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://portal.ncdenr.org/web/wg/ws/su/npdessw#tab-4 Permit No.: Facility Name: 5ur+r-ot'.0 County: Inspector: .F E.hE: Date of Inspection: `LI Time of Inspection: 10 or Certificate;of Coverage No.: Total Event Precipitation (inches): 6 • 3 9 Phone No. Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) 1YYes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. c A "representative storm,event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, l certify that this report is accurate and complete to the best of my knowledge: (Signature of Permit(ej or Designee) Pagel of 2 SWU•242, Last modified 10/25/2012 :. 1. Outfal,Descri Outfall No. `[� Receiving Stream: Describe t e industrial ption: r Structure (pipe, ditch, etc.) RAe- hite, that occur within the outttfal drainage area: XJS Qrb.y��t �5Ql1 2. Color: Describe the color of %Ir scharge sing basic colors (red, brown, blue, etc.) and tint iight,,medium, dark) as descriptors:r; Pracent_- 3. Odor: Describe any distinct odors that the discharge may have (i.e_, smells strongly of oil, weak chlorine odor, etc.): _ t rJllQ _ 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 n 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 V 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 & 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. is there evidence of erosion or deposition at the outfall? Yes V' 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, Last modified 10/25/2012 ..AIX4 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://portal.ncdennorg/web/wq/wsIsu/npdessw#tab-4 Permit No.: N/C/_/ Facility Name:� County: -u-)Ac- Inspector: �S Date of Inspection: -1 I Time of Inspection: lOe-nn, or Certificate of Coverage No.: N/C/G/Q/,�/_b/.U41 C Total Event Precipitation (inches): b - 3 e1 Phone No. Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) dyes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. I A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I ceAtifyAhat this report is accurate and complete to the best of my knowledge: (Signature of Permit+�r Designee) Pagel of 2 SWU-242, Last modified 10/25/2012 I. Outfal! Description: `�.� '� outfall No. I Structure (pipe, ditch, etc.) t�y El ! Jf �� �,t,J 0 Receiving Stream: escribe the industria activities that occur within the outfall drainage area: �ftJe � 2. Color: Describe the color of the di (light, medium, dark) as descriptors: harge usipg basic colors (red, brown, blue, etc.) and tint -%$ PDX 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 6L &A P— _ 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy- 1 © 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with. floating solids: 1 2 3 1:V 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 4 5 7. Is there any foam in the stormwater discharge? Yes 9 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes Na 10. Other Obvious Indicators of Stormwater Pollution: List and describe 0 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 V - NCDENR Stormwater Discharge Outfall (SDO) Qualitative Moni.toring Report For guidance on filling out this form, please visit: http:/Jporta1.ncdenr.org/web/wqf ws/su/npde55w#tab-4 Permit No.: IV/�/_/_/ _/^/_/_ /�--/ or Certificate of Coverage No.:/C/G/�/,�]Q Facility Name: County: wCL4 nspector:,%nes Date of Inspection: _ Time of Inspection: _ .IL,-t to 0% Total Event Precipitation (inches): Phone No. QlQ — 934- eOZ-) Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. I A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge From the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee Obtains aDoroval from the local DWO Regional Office. By this signature, I certify th�fjhis report is accurate and complete to the best of my knowledge: (Signaturevof Permittee(or�Designee) SWU-242, Last modified 10/2S/2012 Pagel of 2 1. Outfall Description: Outfall No. Receiving Stream�pt Describe the ind re (pi e, ditch, etc.) AVCA INVtu)0�6 gQpC Club that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium;•'dark) as descriptors: C kegr 3. Odor: Describe any distinct odors that the discharge may have (i.e., sriiells.strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the -clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 & 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 03 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yeso 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, last modified 10/25/2012 ' 1 SURTRONiCS, INC. 4001 Beryl Rd. P.O. Box 33459 Raleigh, NC 27606 Raleigh, NC 27636-3459 (919)834-8027 Fax (919)828-9972 July 18, 2014 Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh NC 27699-1617 Subject: Perm ittee-Stormwater Data Spring 2014 Sample — 6/12/2014 To Whom It May Concern: Two copies of one set of data accompany this letter based on sampling of a Spring 2014 event. The events occurred on 6/1212014. The data includes: Two (2) copies of one set of qualitative data for each of three sampling points are enclosed. If you have any questions please call me at (919)834-8027 Ext 235. Sincerely yours, DZI-- Lee Bradsh General Manager CC: Surtronics File Enclosures: Storm Data 6/12/2014 aceAnalytr"cal" irrarpBcaraba.can July 08, 2014 Ms. Adrianna Rosati Special Metals Welding Products 1401 Burris Road Newton, NC 28658 RE: Project: SW SUMMER 2014-R 6129 Pace Project No.: 92207395 Dear Ms, Rosati: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on June 30, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted, If you have any questions concerning this report, please feel free to contact me. Sincerely, Lord Patton lorri.patton(.cDpacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report $hall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 aceMaIximi"' Uri1ryiCOM Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Project: SW SUMMER 2014-R 6129 Pace Project No.: 92207395 Charlotte Certification IDs 9800 Kincey Ave. Ste 100. Nuntersville, NG 28078 FloridalNELAP Certification#: EB7627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDS 2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc„ Page 2 of 14 ceAnalytical warw.p W6W&cam Project: SW SUMMER 2014-R 6129 Pace Project No.: 92207395 Lab ID Sample 10 92207395001 W1-4 92207395002 S1-4 Pace Analytical Services, Inc. 2225 Riverside or. Asheville, NC 28804 - (828)254-7176 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 166413 CLW 1 PASI-C EPA200.7 JMW 1 PASI-A SM 2540D TEP 1 PASI-A SM 4500-H+B MOW 1 PASI-A EPA 1664E CLW 1 PASI-C EPA 200.7 JMW 1 PASI-A SM 2540D WRC 1 PASI-A SM 4500-1-1+13 MOW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 14 acemalxical s wwwPoom ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: SW SUMMER 2014-R 6/29 Pace Project No.: 92207395 Sample: W1-4 Lab ID: 92207395001 Collected: 06/29/14 13:34 Received: 06/30/14 16:22 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 07/03114 09:26 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Lead NO ug1L 5.0 1 07/03/14 18:00 07/03114 2021 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 3.9 mg1L 3.1 1 07102/14 04:53 4500H+ pH, Efectrometric Analytical Method: SM 4500-1-1+13 pH at 25 Degrees C 6.5 Sid. Units 1.0 1 07/02/14 17.44 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/08/2014 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 14 aceAna1j&al' antrorPW6W aC= ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Ashev$le, NC 28864 (828)254-7176 Project: SW SUMMER 2014-R 6129 Pace Project No.: 92207395 Sample: S1-4 Lab ID: 92207395002 Collected: 06/29/14 13:42 Received: 06/30/14 16:22 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] HEM, Oil and Grease Analytical Method: EPA 16649 Oil and Grease ND mg/L 5.0 1 07/03/14 09:25 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Lead NO ug/L 5.0 1 07/03/14 18:00 07103114 20:24 7439-92-1 25400 Total Suspended Sollds Analytical Method: SM 25401) Total Suspended Solids ND mg1L 5.3 1 07/02114 15A4 4500H+ pH, Electrometric Analytical Method: SM 4500-H+B pH at 25 Degrees C 5.8 Std, Units 1.0 1 07/02/14 17:44 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/08/2014 02:46 PM without she written consent of Pace Analytical Services, inc.. Page 5 of 14 aceAnalyiical nww.pacemmcom QUALITY CONTROL DATA Project: SW SUMMER 2014-R 6129 Pace Project No.: 92207395 QC Batch: GCSV118112 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92207395001, 92207395002 METHOD BLANK: 1235039 Matrix: Water Associated Lab Samples: 92207395001, 92207395002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mglL ND 5.0 07/03/14 09:10 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 1235040 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mglL 40 38.2 96 78-114 MATRIX SPIKE SAMPLE: 1235041 35143334002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 1AU 40 37.7 93 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/08/2014 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 14 aceAnalytical' wwwpacwacom Project: SW SUMMER 2014-R 6129 Pace Project No.: 92207395 QC Batch: MPRP116369 QC Batch Method: EPA 200.7 Associated Lab Samples: 92207395001, 92207395002 METHOD BLANK: 1234755 Associated Lab Samples: 92207395001, 92207395002 Parameter Units Lead ug1L QUALITY CONTROL DATA Analysis Method: EPA200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 07107/1416:30 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, MC 288b4 (828)254-7176 LABORATORY CONTROL SAMPLE: 1234756 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead ug1L 500 504 101 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1234757 1234758 MS MSD 92207584002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cana Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L NO 500 500 494 490 99 98 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1234759 1234760 MS MSD 92207654001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Lead ug/L NO 500 500 507 485 101 97 70-130 4 Results presented on this page are In the units Indicated by the "Lints" column except where an altemate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS Ibis report shall not be reproduced, except in full, Date: 07/08/2014 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 14 aceAnalXical' wwwpaC�bStom Project: SW SUMMER 2014-R 6129 Pace Project No.: 92207395 QC Batch: WET131902 QC Batch Method: SM 2540D Associated Lab Samples: 92207395001 METHOD BLANK: 1233832 Associated Lab Samples: 92207395001 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 1233833 Parameter Units Total Suspended Solids mglL SAMPLE DUPLICATE: 1233834 Parameter Units Total Suspended Solids mglL SAMPLE DUPLICATE: 1233835 Parameter Units Total Suspended Solids mg1L QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 07/02/14 04:38 Spike LCS Conc, Result 250 234 92207552001 Dup Result Result 2100 1820 92207555001 Dup Result Result 2180 2180 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LCS % Rec % Rec Limits Qualifiers 94 80-120 RPD Qualifiers 14 D6 RPD Qualifiers 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/08/2014 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 14 aceAnalylical' WWWP&Vhft=n QUALITY CONTROL DATA Project: SW SUMMER 2014-R 6129 Pace Project No.: 92207395 QC Batch: WET131918 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92207395002 METHOD BLANK: 1234477 Associated Lab Samples: 92207395002 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 1234478 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1234479 Parameter Total Suspended Solids SAMPLE DUPLICATE: 1234480 Parameter Total Suspended Solids Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 07102/1415:43 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 238 95 80-120 92207396002 Dup Units Result Result mg1L ND ND 92207496001 Dup Units Result Result rng1L 10.0 10.6 RPD Qualifiers RPD Qualifiers 6 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS . This report shall not be reproduced, except in full, Date: 07/08/2014 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 14 aceAnalytical' ww w'Pwghft0= QUALITY CONTROL DATA Project: SW SLIMMER 2014-R 6/29 Pace Project No__ 92207395 QC Batch: VVET131911 Analysis Method: SM 4500-H+B QC Batch Method: SM 4500-H+B Analysis Description: 4500H+B pH Associated Lab Samples: 92207395001, 92207395002 SAMPLE DUPLICATE: 1234363 Parameter Units pH at 25 Degrees C Std_ Units 92207395001 Result 6.5 Dup Result 6.6 RPD Qualifiers 1 H6 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Results presented On this page are in the units indicated by the'Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/08/2014 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 14 aceAnalytical" www.peralatzioam QUALIFIERS Project: SW SUMMER 2014-R 6/29 Pace Project No.: 92207395 DEFINITIONS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the Sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit, RL- Reporting Limit. S - Surrogate 1,2-Diphenythydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicales the compound was analyzed for, but not detected. N-N itrosod iphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. LOD - Limit of Detection. LOO - Limit of Quantitation. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyses. TNI - The NEIAC Institute - LABORATORIES PAST -A Pace Analytical Services - Asheville PAST-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA recommended holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07108/2014 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14 axAnalytical www.yaearabsrzrn QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: SW SUMMER 2014-R &29 92207395 Analytical Lab l❑ Sample ID QC Batch Method QC Batch Analytical Method Batch 92207395001 W1-4 EPA16648 GCSV118112 92207395002 S1-4 EPA1664B GCSV118112 92207395001 W1.4 EPA 200.7 MPRPI16369 EPA 200,7 ICPl14789 92207395002 S1-4 EPA200.7 MPRP116369 EPA200.7 ICP114789 92207395001 W1-4 SM 2540D WETI31902 92207395002 S1-4 SM 25400 WET131918 92207395001 W1.4 SM 4500-H+B WET131911 92207395002 S1-4 SM 4500-H+B WETM911 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/0812014 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 14 V ;�' .-paceAnalytical' ww etcelaS�s_uue SIR SPEEDY PRINTING CENTER - MINNEAPOLIS, MN 55414 • 012-378.7778 CHAIN -OF -CUSTODY 1 Analytical Request Document The Chainof-Custody is a LEGAL DOCUMENT. All relevant fields must be completed acatrately, a Cl) CD 0. Page: e1 Section A Section B Section C Required CUenl Information: Required Project Informatlam invalps information: Camoan ReportTo! Attenfon:m . W P L ait O *,,»1Z`S�s s Address: ^ _t �� J f A Copy To: Company Name: SmYfPG REGULATORY AGENCY ^ OA G Z6 5 Addj ie�' b., r' NPDES f- GROUND WATER '- DRINKING WATER LIST �- RCRA `.- OT'riER Emell To'. 04- smw GC.e�iA PurGR85e Order Na.: � b'[rsEda ll Pau QuetA Rpe enter Project Nama. _ ��yl� PaoeP�oJed .. Site Location g 6 V M"�a`rV a STATE: n Requested Duo Date1TAT: ProJacl Number: :j-Z0t4j)jC09 1 Requested Analysis Filtered (YIN) Section D Matrix Codes 2 6 z Required Client lntarmation Mp MIX f CODE 9 COLLECTED b` PIL56N8iIV85 F Drinking Water OW Vlr3ter WT 9 r o WoWater WW . m tempos" se tmroR w z Product Scil1S01id St. $ p to } SAMPLE ID CJ QL Wipe WP (A-Z09fA Air AR W ra Sample 103, MUST BE UNIQUE Tissue TS D a w ru N J U # f Olhcr OT X N a W � Q ur n O p � to � iu � ro � • � yy II� �% xx G — C w DATE TIME CSATE llAA12 N O # = x z z S ,.� it. Pace Project Nod Lab I.D. at - 1 u !�!'s 1 6 z N'rI X . -, tif7 ey" . x-01-11ua!J WW C Z9 Ys'1 6127 1T;f 17, J I XI I I I ' a - A our t G 6 7 2$ 1'i'S3 ; t Y, r� 4 Q - W to J f,I Z /q:i Li qS X 3- A F7wrildeG UZ# lei r i lil',sx 4Y i , 6 3- 04 4 1 VA c 61AZ9 .r jr ch� rq• sc i x 7 1 q -A tov r Mtr [ 6 Z 11:d'z 00 It; Y e D Y' ►'►I!� o 1� G Z9 l'�t 3o X k 9 —IS —.1n 1D 11 42 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY ! AFFILIATION DATE TIME SAMPLE CONDITIONS WIT -4r. } , / , .2 11 aceRn:�fXIMI" Sample Condition U on Receipt SCUR VyV Pa e 1'of 2 if - Document Number: Issuing Authority: F-CHR-CS-003-rev.14 Pace Huntersville Quality Office Client Name: b,) L Courier. ❑ Fed Ex ❑ UPS❑ tJSPVClient❑ Commercia❑ Pace Other Custody Seal on Cooler/Box Present: ❑ yes �Z( no Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble WrapBubble Bags ❑ None ❑ Other Thermometer Used. iR Gun T1102 14 Type of Ice: & Blue None Samples on ice, coding process has begun Temo Correction Factor T1102: No Correction T1301: No Correction Corrected Cooler Temp.:_ C Temp should be above freezing to 6'C Biological Tissue is Frozen: Yes No wA Comments: Date and Ent s of personexamining contents. C� Chain of Custody Present: Y ONo ❑N)A 1, Chain of Custody Filled Out: A4 ❑No ❑NIA 2. Chain of Custody Relinquished: s ONO ❑NIA 3, Sampler Name & Signature on COC: 6ps ONO ❑N/A 4. Samples Arrived within Hold Time: 6Yes GNo CNlA 5 Short Hold Time Analysis (a72hr : Dyes P4110 ONrA 6, Rush Turn Around Time Requested: ❑Yes o ❑WA 7. Sufficient Volume: ldyes ❑;vo ON/A t3. Correct Containers Used: -Pace Containers Used: ONO ;19sCiNo OWA ❑NIA g, Containers intact: Yes ❑No ©NIA 10. Filtered volume received for Dissolved tests ❑Yes ❑No IA 11. Sample Labels match COC: -Includes dateltlme/ID/Anal sis Matrix: f �[!Yes UNo ❑NIA 12. All container8 needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation, exceptions: VOA, colIform, TOC, O&G, WI-DRO (water) Yes ONO es CJNo ❑Yes VNo ❑N/A CNIA 13, Samples checked for dechlorination: ❑Yes UNo VN± 14. Headspace in VOA Vials >Bmm): DYes CNo A 15, Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): OYes ONO7N/A [ayes ©No A 16. Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: DatelTlme: Comments/ Resolution: SCURF Review:[Date: � SRF Review: Date: 30 Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina QEHNR Cert-sftcatton Office ( L6 out of hold, incorrect preservative, out of temp, Incorrect containers) Page 14 of 14 27952 CHAIN OF CUSTODY Page of 501 Madison Ave. WILiberty, Analytical Corp. Cary, NC 27513 Phone: 919-379-4100 Fax 919-379-4W Courier Airbill No. Samp ling Complete. Y or N aenV tri n ormstron' ,'., jeer nluma¢twn t -Area sas inn ude m an a Company Natrae plGs Project Name C7 ~� Q<b !a- `�` `D {� Z f GW - Ground water WW - Waste water SW - Surface water SO - SoiltScdiment TB - Trip Blank RI - Rinsatc WP - Wipe O -Other Address , j h [ trij 1 Sampling Location � Q,TII City State 2ip�� �� Tumaround time Project Cuntac _ Batch QC' or Projcel Specific? 11'Spceific, which Sample Its? Phone q r /�. J � ^ Are aqueous sumplea field filtered for metals? Y or N Sampicr s Nam t A m Are high cntaccntr]iions expected? Y or N? It yes, which ID{s):' pFI1.5prto�le inM y vdc se t t/l^T._•n s 7 Clrrnpu,Cheoi to : Field ID CuEEeetiun Matrix # of bottles Numher oFPreserved Bottles� Date 'Time x o o p Ia �2 17 49 n b Use IF Sam le Unpacked $ Cyanide samples checked for sulfide &. chlorine'? Y o i A 625 & Pbenol checked for chlorine? Y o A samples Sample Order Ent B Samples Received in Good Con tti ' orN-- 1608samples checked for pH between 5,0.9.0? Y o A If no, explain: Resin uished b L DarrlTime: Received b : Date/Time: 61Z' Relinquished b : Date/Time: I Received by- DalePi'itne: Subcontact? Y o N Fes, where? Custod Seal(s) intact? Y or N 10, lee 'Y r N Cooler Tem : St 2. °C Samples slorcd 60 daYllcr date report mailed at nu aura charge. C%nt- mar & Yellow copy to lab • Pink copy , r mstorn r WO`Q �1 v f f`o ANALYSIS DATA SHEET 6-12-14 Client: SURTRONICS Lab ID: 140 1-01 SDG: 1406091 Project: STORM WATER %Solid: Matrix: Water Sampled: 06/12/14 Received: 06/13/14 CAS NO. Analyte Cone. (mg1L) NIDL R1, R.F. Q A'temhod Segvcncv Analyzed ILGREASE Dil & Grease (SGT-HEM) 4.67 0,778 5.00 1 3 EPA 1664A 41`21004 6/20/14 11:45 TSS Total Suspended Solids 17.6 0.620 5.00 1 SM 2540D 4F19011 6117/14 16:15 y\'t ti Sfjff F CP hem v A Diri;iaoi Of `X-o� Lib ertvAii-d 7I Corp, Page 14 of 18 27952 CHAIN OF CUSTODY Page of 501 Madison Ave. Liberty Analytical Corp. Cary, NC 27513 Phone: 919-379-4100 Fax 919-379-4040 Courier Airbill No. Sampling Com lete? Y or N teo to n ormation "._ rolect tomtatton '. :: :: :: ..:: .: t Ana sts me u tt1ethod an a ,",:,. ..k trttxs- Company Name A 1 A s b Project Name 4 13:;.pFi o r (-,::;L- ( GW - Ground water WW - Waste water SW • Surface water SO - SoillSediment TB - Trip Blank RI - Rinsatc IMP - Wipe 0 -Other l Sai13p1a Info u' ,.,z. a Address Gr Sampling Location S �! ` r, Q, City State G Zip�� n� UU4— Turnaround time Project CVntac _ Batch QCor Projcct Specific? If Specific, which Sample Ill? Phone 4 ct r l}_ J il� Arc aqueous samples Field filtered for metals'? Y or N Sampie0%, Name Mocss ' • r Are high tonLrmratiom expceted? Y or N? If yes, which ID(s)" ;'�?•:' Catn(2uC m Nu:. Field 1D Collection Matrix 9 of bottles Number ofPnserved Bottles Date Time z o z z z N z a 0 1.- 16 :. . ah se —777 Sample Un acked B Cyanide samples checked for sulfide & chlorine'? Y o A 625 St Phenol samples checked for chlorinc7 Y o A Sample Order Ent S 11± Samples Received in Good Con iti ' or 608 samples checked for RH between 5,0-9.0? Y o If no, explain: A -17 Re1in uished b . DatrlTitne: (a Received b : Date/Time:67 1311Y Relinquished by.' Date]Time: Received by- DatcfFime: Subcontact? Y o N f yes, where? Custod Seal(s) intact? Y or N On Ice 'Y r N Cooler Temp: 5, 2— °C Samples steed 60 da�Tafler date report trailed at no extra charge. �i tip mar ���uN, & Yellow copy to tab • Pink copy r W010 Client: SURTRONICS Matrix: Water Initial/Final: 500mL / 2500uL Dilution: 1 pH: % Moisture: NA Batch: 4061614 ANALYSIS DATA SHEET 8082A SDG: 1406091 Extraction: EPA 351 OC GC Sulfur Cleanup: N Florisil Cleanup: N GPC Cleanup: N Sequence: 4F18016 Project: STORM WATER File ID: 293wl406 91-Ol.d Lab ID: 1406091-01 GPC Cleanup Factor: N Calibration: 4060603 6-12-14 Sampled: 06/ 12114 10:15 Received: 06/13114 13:25 Prepared: 06/ 18114 10: I I Analyzed: 06/ 18/ 14 19:23 Instrument: trace c8b CAS NO. COMPOUND CONC. (ug/L) MDL RL Q 12674-11-2 Aroclor-1016 0.0730 0,500 U 11104-28-2 Aroclor-1221 0.0640 0.500 U 1114E-16-5 Aroclor-1232 0.0650 0.500 U 53469-21-9 Aroclor-1242 0.140 0 500 U 12672-29-6 Aroclor-1248 0.044D 0.500 t1 11097-69-1 Aroclor-1254 0.0720 U00 U 11096-82-5 Aroclor-1260 10.0500 0500 U SYSTEM MONITORING COMPOUND ADDED (ug/L) CONC (ug/L) °/a REC QC LIMITS Q DCB (A) 0.6000 0.4064 68 43 - 144 DCH (A) [2C] 0.6000 0.3692 62 43 - 144 TCX (A) 0.3000 0.1773 59 43- 135 TCX (A) f2Cl 0.3000 0.2130 71 43 - 135 " Values outside of QC limits Ctp�hem d c A Dili imt Of Liberty Analytical Corp_ Page 18 of 24 r 27952 CHAIN OF CUSTODY Page of_ �t)y�tstae qr 50E Madison Ave;, Liberty Analytical Corp. Cary, NC 27513 I W- Phone: 919-379-4100 Fax 919-379-4W Courier Airbill No. --40 gampling Com letY or N --, let rt[n nnm9lrOn'% Information roJelL t:naSlytnmethod an e' Company Name t� Project Name Q � ♦ dc ` (�] v = { � ' Groundwater WW- Writ water SW - Surface water SO - Soil/Sediment TB - Trip Blank RI - Rinsatc WP • Wipe 0, Other Address ! At i h k Sampling Location T (� City State G zip�� Turnaround time Project Contac Batch QC or Projcct Specific? if Specific, which Sample ID? Phone # r] r Are aqueous snmplcs field filtered for metals? Y or N Sampler's Name Are high concentrations expected? Y or N? If yes, which I13{s)? pH / $aiip&s laf0;:'.'. z� +" Cp1+i0;; :. 6 Us'c) ;'..... Field Ip C'allixtion Matrix ltof bottles Nuinberof Preserved Bottles Date Time 1- l b 11 iq 16 42 L Use OJI] y Sam le Un acked By- Cyanide samples checked for sulfide & chlorine? Y o FA) 625 & Phenol samples checked for chlorine? Y o A Sample Order Ent By: Samples Received in Good Co. ttt or 608 sanVies checked for pH between S.0.9.©? Y OM If no, explain: ... Relinquished b . DdtelTime: (a Received b : Date/Time: I 13< 2 Relinquished b: 19=11 IDatcaime: lReceivedby: Date/IEMU; Subcontact? Y o [� f es, where? Custod Seal(s intact? Y or N On Ice 'Y r N Cooler Temp: 5+ 2—°C Samples stored 60 dweller date reptm mailed at no extra aitargc. C��n1r ,J� t}ljiiJff(e & Yellow copy to lab • Pink copy r�customer5 W010 Client: SURTRONICS Lab ID: 1406091-01 ANALYSIS DATA SHEET SDG: 1406091 Project: STORM WATTFR % Solid: Matrix: Water Sampled: 06/12/14 Received: 06/13/14 CAS NO. Analyte Cone. (ug/L) MDL RL D.F. Q L11ett►od Sequence Almlyzed 7440-50-8 Copper 23.8 0.910 5.00 1 EPA6010C 4F20008 6/19114 19:17 7439.92-1 Lead 8.65 3.58 10.0 1 J EPA 6010C 4F20008 6/19114 19:17 7440.66-6 Zinc 119 10.2 30.0 1 EPA 6010C 4F2 M 6/19/14 19:17 �esrj��r COMP hem tT : A DisisiMA Of Liberty AneJvti,-al Corp. Page 15 of 16 ?2 1:......11111104mrVa CHAIN OF CUSTODY 27952 Page — of A Division or 501 Madison Ave. Liberty Analytical Corp. Cary, NC 27513 Phone- 919-3794100 fax9)9-379-4040 Courier Airbill No. V 'Ram tingCompfete? Y or N (inn ludcmethod and. ttlel type),..,, Company Na Vw-6ntGj Project Name )t-- 0C r, Z 1�4 CJ C- GW - Ground water WW - Waste water SW -Surf= Water SO - Soil/Sedimcni TB -Trip Blank I RI - Ri"Sate WP - Wipe 0 - Other Address 4W Btm 1-,�) Sampling Location 3 f-6 rmii oky- I CityState C/ Zip iw� n( Turnaround time ProjcctConiacil BaLCII QC or Projccl Specific! 11-Specific. which Sample 11)? Phone # Ci Am aqueous qiimplcs field filtered for metals'! Y or N Sampler's Name RILE Are high concentrations expected'? Y or N? If yes. which ID(s)? 7777 1: Field 10 Collection Matrix 4 of bottles Number of Pri:scrvcd Bottles Date Time 0 C 0 q00q1-01 17 ...... kX U= .1.'CDUU%1PW Sample Unpacked By: hl-� 1171tk.-11\1 Y 0 A JCya-ide samples checked for sulfide & chlorine'.) P 1625 & Phenol samples checked for chlorine? Y oy;W - Sample bider Entry By:�-� '4 ZZ& Samples Received in Good Co iti 8F N 1608 samples checked for pH between 5.0-9.01 Y If no, explain: Sample Rclinqui hf.,d by, Dalcmrm: 1. 1 fil 14 13 &5 Received by: Date/Time: 1 132<- Relinquished by: IDateaime: --Tcus(ody I Received by: Daterrime: o .) N f yes LSubcontact? Y 1 , where? Seal (s) intact? Yor nN On Ice `Y N ooler Ternp, a� 2- -c Samples stored 60 da)Tfficr date report mailed at no extra charge. &rfe & Yellow copy to lab - Pink copy for customer ►F\Lyjfv. V 8—W IV Client: SURTRONIICS Matrix: Water InitiallFinal: 500ntL / 2500ul, Dilution: I PH: % Moisture: NA Batch: A061 Ul ANALYSIS DATA SHEET 8081E SDG: 1406091 Extraction: EPA 3510C GC Sulfur Cleanup: N Florisil Cleanup: N GPC Cleanup: N Sequence: 4F18014 Project: STORM WATER File 1 D: 0520406091-01 A Lab ID: 1406091-01 GPC Cleanup Factor: N Calibration: 4061305 6-12-14 Sampled: 06112114 10:15 Received: 061133/ 4 13:25 Prepared: 06/ 18114 10: I I Analyzed: 06/1.8,1114 19751 Instrument: traceu84 CAS NO. COMPOUND CONC. (ug/L) MDL RL Q 319-84-6 alpha-BHC 0.0304 0,00190 0.0250 P 58-89-9 gamma-BHC (Lindane) 0.0167 0.00190 0.0250 ! 76-44-8 Heptachlor 0.00725 0.00240 0.0250 J 309-00-2 Aldrin 0.00600 0,00270 0.0250 JP 319-85-7 beta-BHC 0.0302 0,00950 0.0250 319-96-8 delta-BHC 0.00479 0.00320 0.0250 1P 1024-57-3 }leptachlor epoxide 0.00915 0.00290 0.0250 JP 959-98-8 Endosulfan 1 0.00515 0.00430 0.0250 JP 72-55-9 4,4'-DDE 0.00390 0.0500 U 60-57-1 Dieldrin 0.W510 0.0500 U 72-20-8 Endrin 0.00690 0.0500 U 72-54-8 4,4'-DDD 0.00550 0.0500 U 33213-65-9 Endosulfan lI 0.00550 0.0500 U 50-29-3 4,4'-DDT 0.00510 0.0500 U 7421-93-4 Endrin aldehyde OM 20 0 05M U 103 1 -07-8 F.ndosulfan sulfate 0.00680 0.0500 U 8001-35-2 Toxaphene 0.480 2.50 U 57-74-9 Technical Chlordane 0.240 0,800 U SYSTEM MONITORING COMPOUNDS ADDED (ug/L) CONC (ug/L) %REC QC LIMITS Q DCB (A) 0.6000 0.1299 22 43 - 144 DCB (A) 12C1 0.6000 0.1263 21 43 - 144 TCX (A) 0.3000 0.1809 60 43 - 135 TCX (A) F2Ci 0.3000 0,4186 140 43 - 135 * Values outside of QC limits \�Caljrr' -'' CP hear Z? A Di zicni Of ''rri-1 ,;,�� �.ibertyr".nal-rticttl Corp. Page 20 of 26 27952 CHAIN OF CUSTODY Page — of — 00 r �36::;rAAA % ZVisifin 501 Madison Avc- Liberty Analytical Corp. Cary, NC 27513 Phone: 919-379-4100 Fax 919-379-4040 Courier Airbill No. Sam pting Complete? Y or N lien rttnr Information';... TrU*tlJ3fbn11a1i00 K eftqrLj=cst6d.'AnaJys Malys (include method tt a Company Na —Jjbp 6lb� Project Name <3 dc 14 V 44- t C/- < GW - Ground water WW - Waste water SW - Surface water SO - Soil[Sediment TH - Trip Blank Rl - Ritmite WP - Wilic 0 - Other pFl fSampie Inf6:;; Address t ru Sampling Location 5 f rmw a-kf City',) Slaw, Tumaround time Project Cu:nlacl )PfAAE,� Batch Q('or Project Spiecific'? If Specific. which Sample 11)? Phone ft Art: aqueous samples field filtered ror metals'? Y or N--7- Sampler's Namc Are high roncciwatiom expected? Y or N? Ifycs, which 11)(s)? Nb- Field ID Collection Matrix # of bottles Number of Preserved Bottles Date Time z 0 i C-4 0 W O ---4— Sample Unpacked B --------------- Cyanide samples checked for sulfide & chlorine? Y oA6z ) 1625 & Phenol samples checked for chlorine? Y oAY Sample Order Entry By: Samples Received in Good Con'6' —'r-v- 1608 samples checked for pH between 5.0-9.0? Y a If no, explain: 'A-T" -'i . V:" : 6 "' , . I " L .% .: -: I - tQ � - Relimuished by DaicfFime: 1131 It) 13 &5 Rcceied tX: 4 Datefrime: Relinquish d b IlDaiefTimei %Z N� lReceived bX: ISubcontact? Y 01 N )fycs, where? .--Iq ustody Seal(s) intact? Y or Ice 'y N -K Cooler Temp: 52- -c - - Samples stored 60 daWlaftcr date report mailed at no extra charge. & Yellow copy to lab - Pink copy for customer 5 J P, GUN.- WO 10 Client: SURTRONICS Matrix: Water Initial/Final: 500rnL 1 500uL Dilution_ 1 PH % Moisture: NA Batch: 4061616 ANALYSIS DATA SHEET SM270D SDG 1406091 Extraction: I- PA 35510C SVGA Sulfur Cleanup: U Florisil Cleanup: N GPC Cleanup: N Sequence: 4F18011 Project: STORM WATER File ID: 1406091-0166,0 I.ah 11). 1406091-01 GPC Cleanup Factor: N Calihratiom 4061501 6-12-14 Sampled: 06/ 12114 10:15 Received: 06/ 13114 13:25 Prepared: 06118/ 14 10:0i Analyred: 0 /1Kl6 14 21:20 Instrument: 99 2h 66 CAS NO, COMPOUND CONC. (ug/L) MIX- Kl- Q 62-75-9 N-Nitrosodimethylamine 0.98 5.0 U 108-95-2 Phenol 0.62 to U 111444 Bis(2-ehloroethyl)eEher 1.3 5,0 U 95-57-8 2-Chlomphenol 1.4 10 li I 108-60-1 2,2'-owbis(1-Chloropropane) 1.6 5.0 (i 621-64-7 N-Nitroso-di-N-pmpylamine 1.8 5,0 U 67-72-1 Hexachloroethane 1.1 5.0 U 98.9$-3 Nitrobenzene 1.3 5.0 U 78-59-1 Isophomne 0,94 88-75-5 2-Nitrophenol 0.99 10 U 105-67-9 2.4-Uimethylphenol 4.8 10 U 111-91-1 Bis(2-chloroethoxy)methane 0.99 5B (I 120-83-2 2.4-Dichlorophenol 1.6 10 U 91.20-3 Naphthalene 1.3 5.0 (J 59-50-7 4-Chloro-3-methylphenol 0,82 10 U 77.474 licxachlorocvelopentadiene 0.91 5.0 U 88-06.2 2.4,6-Trichlorophenol 0.89 10 U 91-58-7 2-Chlomnaphthalene 10 5.0 Ii 131-11-3 Dimethylplttha)ate 0.64 5.0 U 606-20-2 2.6-Dinitrotoluene 0.75 5.0 U 208-96-8 Acenaphthylme 0.96 5.0 U 83-32-9 Acenaphthene 0.80 5.0 U 51-28-5 2.4-Diaitrophenal 2.1 10 (i 100-02-7 4-Nitrophenol 23 10 U j 121-14-2 2.4-Dinitrotoluene 0.84 5.0 U R4-66-2 Diethylphthalate 0,52 5 0 U 7005-72-3 4-Ch)orophenyl-phenylether 0.66 5.0 U 86-73.7 Fluorene 0.71 5.0 U 534-52-1 4,6-Din itro-2-methyl phenol 1.1 10 7! 86-30-6 N-Nitrosodiphenylamine (1) 0.97 5.0 U j 101-55-3 1-13romophenyE-phe nylether 080 U 118-74-1 Hexachlorobemew R57 t s fjrf , CPOM�c hem A Divi:iou Of ✓�frr�J�.�, LibertyAnalytieal Corp. Page 19 of 28 Client: SURTRONICS Matrix: Watcr Initial/Final: 5 0(0MML_/ 500ul- Dilution: I pH: %Moisture: NA Batch: 406116 ANALYSIS DATA SHEET SW8270D S DG 1406091 Extraction: EPA 3510C SVOA Sulfur Cleanup: N Florisil Cleanup: N GPCCleanup: N Sequence: 4F18011 Project: STORM WATER File ID: 1406091-0166.d Lab ID: 1406091-01 GPC Cleanup Factor: N Calibration: 4061501 6-12-14 Sampled: 06112/ 14 10:15 Received: 06/13/14 13:2513:25 Prepared: 06/1 /1410:05 Analyzed: 06118/14 21:20 Instrument: 5972hV66 CAS NO. COMPOUND CONC. (ug/L) MDL RL Q 87-86-5 Pentachlorophenol 2.6 10 U 85-01-8 Phenanthrene 0.70 5.0 U 120-12-7 Anthracene 0.77 5,0 U 84-74-2 Di-n-butylphthalate 0.74 5.0 U 206-44-0 Fluoranthene 0.58 5.0 U 129-00-0 Pyrene 0.73 5.0 U 85-68-7 Butylbenzyiphthalate 0.55 5.0 U 91-94-1 3,Y-Dichlorobenzidine 1.4 5.0 U 117-81-7 bis(2-ethy1hexyl)Phthaiate 0.97 0.57 5.0 J 56-55-3 Benzo (a)anthracene 0.57 5.0 U 218-01-9 Chrysene 2.2 5.0 U 117-84-0 Di-n-octylphthalate (0 1 5.0 U 205-99-2 Benzo (b) Ouoranthene 0.68 5.0 U 207-08-9 Benzo(k)Ouoranthene 1.5 5.0 U 50-32-8 Benzo (a) pyrene 0.70 5.0 U 193-39-5 Indeno(1.2,3-cd)pyrene 0.64 5.0 U 53-70-3 Dibenzo(a,h)anthracene 0.74 5.0 U 191-24-2 Benzo (g,h,i) perylene 0,61 5.0 U 122-66-7 1,2-Diphenyl Hydrazine 0.79 5.0 U SURROGATE RECOVERY RESULTS ADDED (ug/L) CONC (ug/L) % REC QC LIMITS Q 2-Fluoronheno) 100.0 41.46 41 33 - 110 Phenol-d5 100.0 28.44 28 20 - 110 Nitrobenzene-d5 50.00 23.68 47 45 - 110 2-Fluorobiphenvl 50.00 27.06 54 46 - 110 2,4,6-Tribrontophenal 100.0 90.64 91 42 - 119 Temhenvl-dl4 50,00 38. l 1 76 59 - 110 CAS NO. TICS CONC. (ug/L) Response R.T. % Match Q 0001 12-37-8 Undecanoic acid 4.2 131209 19.521 80 J NA Unk. Alkane 8.3 174844 11.313 0 J NA Unk. Atkane(t) 3.3 83942 23.375 0 J NA Unknown 10.985 10 211612 10,985 0 J NA Unknown 12.478 25 676037 12.478 0 J CtP�hem a Diri: ice. Of LibertyAtialytical Corp. Page 20 of 28 Client: SURTRONICS Matrix: Water Initial/Final: 500ml- / 500uL Dilation: I PH: % Moisture: NA Batch: 4061616 ANALYSIS DATA SHEET' SW8270D SDG 1406091 Extraction: 1-,,PA 35IOC SVQA Sulfur Cleanup: N F lorisil Cleanup: N GPC Cleanup: h Sequence: 4E 18011 Project: STORM WATER File ID: 1406091-0166A Lab 10: 1406091-01 GPC Cleanup Factor N Calibration: 4061501 6-12-1 4 Sampled: W1211410:15 Received: 06/1'/� 1413.2 t'rcparcd: 06/ 18/14 10:0S Analyzed: 06/IR114 21:24 Instrument: 5972hp 6 CAS NO. TICS CONC. (ugll-) Response R.T- % Match Q NA Unknown 13.521 14 394208 13.521 0 J NA Unkno�tin 15.964 3.0 85518 15,964 0 J NA Unknotirn 16.577 4.3 124770 W577 0 1 NA Unknown 17,620 2.2 64471 17.62 0 J NA Unknown 18,233 4.3 1 122326 18.233 1 0 J NA Unknown 19.041 2.9 L086 j 19.041 j 0 1 NA Unknavm 9,043 13 274118 1 9.043 1 n J (1) - N-nitrosodiphenylamine cannot be separated from diphenylarninc. It is acceptable to repon the combined resuk. (2) - 1,2-Diphenylhydrazine is unstable and converts to azobenzene, (31- 3 & 4-Methylphenol cannot be separated for quantitation. cPuChem 4n COM A Division Of j1 .3\ LibertyAnalytical Corp. Page 21 of 28 27952 CHAIN OF CUSTODY Page of � A plvtstoe pr 501 Madison Ave. Liberty Analytical Corp. Cary, NC 27513 - WI Phone: 919-379.4100 Fax 919-379-4044 Courier Airbill No. —E gam Sin Com fete? Y or N roject. oforntauon ' " R t °Ana su ine udt. m ttn ' e k Company Name t <j S Project Nance Q (_,:;I-Qb I Z �I GW - Ground water W W - Waste water SW - Surface water SG -Soil/Sediment TOB-RTrip Blank WP - Wipe O - Other Address /� t �"' bb ! r i Sampling Location a, City Slate Zip„ L TllMWOUnd time Project Conrac Batch Q(' or Project Specific' If Specific, which Sample 11)? Phone # r} r r t- Are aqueous sumplct field Iiltered Ibr metals? Y or N Sampler's Name A m& RILL Are high enncentntions expected'? Y or N? If yes, which 11)(s)" pH h59rnpla ltifn' - r }•. CorripuClrr�n Nv; k .rq "bUse)>:'°,.• Field ID (o11�ti11an Matrix # of bottles Number of Preserved Bottles Date -rime z Q z O Y z p -01 16 �Z Lob U= Sample Unpacked By: Cyanide samples checked for sulfide & chlorine? Y o , A 625 & Pbcnol samples checked for chlorine? Y a A Sample Order EntryB Samples Received in Good Con rti or 6N sau ples checked for pH between 5.0-9.0? Y o A If no, explain: uull Relin uishedb , DateiTime:(m 113114 137,5 Receivedb Date/Time:" Relinquished by, Daterrime: Received by: Datefrime: Subcontacl? Y o N f es, where?]Custody Seal(s) intact? Y or N Ott lee 'Y r N Cooter Temp: 5, Z °C Samples stored 60 daygUcr dale report mailed at no extra dhagc. C�iG J., i lyq)fyfe 8 Yellow copy to lab • Pink copy or customer 1 0 10 Client: SUR-FRONICS Matrix: Water Initial/Final: 5ML / 5ML Dilution: I pH: 1 % Moisture: NA Batch: 4061902 ANALYSIS DATA ,SHEET SW 8260B SDG 11400091 Preparation: EPA 5035A Sequence; 4Fi9002 Project: STORM WA'LTR File 1D: 1406091-0159A I_ab ID: W06091-01 Calibration; 4062101 Sampled: 06/ 12/ 14 10:1510:15 Received: 06/ t 3/14 13:25 Prepared: 06/19/14 19:05 Anal} zed: 06/ 19/ 14 20:38 Instrument: 975i..72hp3 ci CAS NO. COMPOUND CONIC. (ug/L) MDL Rl, Q 74-87-3 Chloromethane 0.39 5.0 U 75-01-4 Vinyl chloride 0.48 5.0 U 74-83-9 Brornomethanc 0.76 5.0 U 75-00-3 Chloroethane 0.55 5,0 U 107-02-8 Acrelein 7.3 50 U 75-35-4 1.1-Dichloroethene 0.53 5,0 U 75-09-2 Methylene chloride 0.49 5.0 U 107-13-1 Acrylonitrile 5.1 50 U 156-60-5 trans-1,2-Dichloroethene 0.44 S.0 U 75-34-3 1,1-Dichloroethane 0.27 5.0 U 67.66-3 Chlorofonn 0.27 5.0 U 71-55-6 1,1,1-Trichloraethane 0.32 5.0 (! 56-23-5 Carbon tetrachloride 0.31 5.0 U 107-06-2 1,2-Dichloroethane 0.23 5.0 U 7143-2 Benzene 0.28 5.() U 79-01-6 Trichlornethene 0.28 5.0 U 78-87-5 1,2-Dichlaropropane 0.86 5.0 U 75-274 Bromodichloromethane 0.36 5.0 U I10-75-8 2-Chloroethylvinyi ether 0.97 5.0 U 108-88-3 Toluene 0.31 3.0 U 79-00-5 1.1,2-Trichloroethane 0.51 5 0 U 127-18-4 Tetrachloroethene 0.42 5.0 U t24-48-1 Dihromochloromethane U32 5.0 U 108-90-7 ChlorobLnzrne 0,27 5.0 U 100-41-4 Ethylbenzene 0.42 5,0 U 75.25-2 Bromoform 0.95 50 U 79-345 1,1.2,2-leitachloroeihane 0,64 5.0 U 541.73-1 1.3-Dichlorobenzene 0.36 5.0 U 106-46-7 [A-Dichlorobcnzene 0.30 5.0 U 95-50-1 1,2-Dichlorobanzene 0,35 5.0 U 120-82-1 1.2.4-Trichlorobenzene 0.48 5.0 U 87-68-3 U machlorobutadiene 0.51 5 0 U ` =�- COMPhem Cr v A Divi:i = Of LibertyAnaiytical Corp. Page 18 of 25 Client: SURTPONICS Matrix; Initial/Fiaal: 5mL 15rnL Dilution: 1 PH: i % Moisture: NA Batch: 4061902 ANALYSIS DATA SHEET SW 8260E SDG 1406091 Preparation: EPA 5035A Sequence: 4FI9002 Project: STORM WATER File ID: 1406091-0159.d I.ah ID: 1406091-01 Calibration: 4062101 6-12-I Sampled: 06/ 12/ 14 10:15 Received: 06/13/l4 13:25 Prepared: 00/19/14 19;05 Anahzcd: 06/19I14 20:38 Instrument: 597, 72hp59. SURROGATE RECOVERY RESULTS ADDED (ttgJL) CONC (up/L) % REC QC LIMITS Q Dihromoijuoromethane 50.00 52.22 104 66 - 128 1.2-Dichlorocthanc-d4 50.00 50.73 101 55 - 147 Toluene-M 50.00 50.45 101 50 - 150 Bronto(luorobenzene 50.00 54.39 109 70 - 132 CAS NO, I TICS CONC. (uWL) Response R.T. % Match (� Cprc hem c ti A DiriL;ca, Or G I� 'rel.q Liberty Analytical Corp Page 19 of 25