NCG030459_MONITORING INFO_20171204

A.
STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO. ` Iv, 03�q'�R
DOGTYPE O HISTORICAL FILE
MONITORING REPORTS
DOC DATE ❑ aDl r? is D4"
YYYYMMDD
0

-- 'y Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 12/04/2017
CERTIFICATE OF COVERAGE NO. N00030459
FACILITY NAME The Council Tool Company
COUNTY Columbus
PERSON COLLECTING SAMPLES Kyle Greene
LABORATORY TBL Lab Cert. # 27965
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2017
SAMPLE PERIOD ❑ Jan -June ® July -Dec
or ❑ Monthly' (month)
RECEDrSCEARRGING TO CLASS ❑ORW ❑HQW [:]Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
DEC 12 2017 ®Other Drainage Ditch
CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
DWR SECTION
❑ No discharge this period?'
Outfall No.
Date Sample
Collected ,
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics s
Benchmarks =_=>
-
-
100 mg/L or 50 mg/L"
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
Outfall #1
10/25/17
0.0
21.5 mg/L
6.3
ND
NO
0.0824
ND
ND
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
e_ &
Nam rint name)
1
�2v
Title (Print title)
�P).c4L
la
(Signatu ) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If y`ou report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including_all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
re of Permittee)
(Date)
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 3

TBL
Shipping: Mailing:
2401 W. 5"' St. PO Box 589
Lumberton NC 28358 Lumberton, NC 28359
COUNCIL TOOL COMPANY
345 PECAN LANE
LAKE WACCAMAW, NC 28450
ATTN: VELTON JACOBS
SAMPLE NUMBER - 3842
DATE SAMPLED - 10/25/17
DATE RECEIVED-10/26/17
TIME RECEIVED - 0730
PAGE 1 OF 1
ANALYSIS
BIOCHEMICAL OXYGEN DEMAND
TOTAL SUSPENDED SOLIDS
AMMONIA NITROGEN
FECAL COLIFORM
CONDUCTIVITY
CHEMICAL OXYGEN DEMAND
PH
VOLATILE SUSPENDED SOLIDS
N/R = ANALYSIS NOT REQUESTED
FINAL REPORT OF ANALYSES
Phone: [phone]
Fax: [phone]
Email:pam.hester-
tblf& otmail.com
PROJECT NAME:TBL-27965
REPORT DATE:10-26-17
SAMPLE ID - OUTFALL # 1 SAMPLE MATRIX - WW
SAMPLER - KYLE GREENE TIME SAMPLED - 0530
DELIVERED BY - CLIENT RECEIVED BY - THK
QUAL
DIET.
METHOD DATE
RESULT
UNITS CODE
LIMIT
SM5210-B
N/R
MG/L
2.0
SM2540D 10/26/2017
21.5
MG/L
6.3
SM4500NH3D
N/R
MG/L
0.1
SM9222D
N/R
COL/100ML
1
SM2510B
N/R
UMHOS/CM
10
SM5220D
N/R
MG/L
30.0
SM4500 H+B 10/26/2017
6.3
STD UNITS
0.1
SM2540E
N/R
MG/L
500
LABORATORY DIRECT
NCDENR DWQ # 37, NCDENR DW # 37781

Billinglnformatiow._ Ana lysis/ContainerlPreservalive
TBL Environmental — —'
Laboratory , Inc.
2401 VV. 5th St
Lumberton, NC 28358 eportlo'
[phone] mail to. TBL VERIFIED O/G
ShMPLE VOLUME TO BE
P roject � f? �ity/Sate S? ?laao MLS AS COMPARED
Description: C©uvtc. 170 Ca ..ouzcmd TO GAL 1 BR A T EO sar r
Phone: Client Project #: ESC Key: �k .1 a `f-1 66
0
FAX: —1195-
Colleceed by: Site/Facility ID#: P.O.#: lip— I (0 O
Collected by (signa e): Rush? ( Lab MUST Be Notified) Tate Resin^T�'ceded*. � CoCode (lab use only)
�j Same Day.......200% _ ` No 1
0*-CTJ'l�t:►AA—A— Next Day........ 100% Email? _No_Yes d Q TemplatelPrelogin
Two Day .........50%
Immediately Packed on ice NI Y ° FAX? —No—Yes d r1� 1 Shipped Via:
Cntrs
Sample if] Comp/Grab IJIa1rlx' Depth Dale Time ly Remarks/Contaminant Sample tk (lab only)
4 c-
PH NH3 EN CL2 Y N
_ n
COO METb S INT
'Matrloc SS-Soil/Solid GW _ Groundwater WW - Wastewater DEN- Drinking Water OT - Other pH Temp
Remarks:
T��� /0"b(ilil Flow Other
' d by: lgnature)
[Rreli.nquihed b V(seat re)
Date:
Time:
Received b1y 4a+gnat r)
Received by: (Signature)
SamAles returned via: ©UP5
❑ FedEx ❑ Courier ❑
Condit)on: (lab use only)
Date:
Time:
Temp:
Boffies Received:
CoC Seats Intact: _ Y _ N NA
Relnquished by: (Signature)
Date:
Time:
Received for lab by: (Sicdna lure)
Date:
Time:
pH Checked:
NCF:

rp

*ESC ANALYTICAL REPORT myESC
November 07, 2017
TBL Laboratory
Sample Delivery Group
Samples Received:
Project Number:
Description:
L946946
10/27/2017
TBL-27965
Council Tool Co.
Entire Report Reviewed By:
Darren Reeder
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This lest report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is
performed per guidance provided in laboratory standard operating procedures, 060302. 060303, and 060304.
:r'

TABLE OF CONTENTS ONE LAB. NATIONWIDE.
Cp: Cover Page
1
Tc: Table of Contents
2
p
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
rss
OUTFALL #1 L946946-01
5
,
Oc: Duality Control Summary
8
Cn
Wet Chemistry by Method 16648
8
�Sr
Metals (ICP) by Method 200.7
9
Volatile Organic Compounds (GCIMS) by Method 624
10
GQc
Pesticides (GC) by Method EPA 608
12
Gi
Polychlorinated Siphenyls (GC) by Method EPA-608
14
Semi Volatile Organic Compounds (GC/MS) by Method 625
35
AI
GI: Glossary of Terms
19
Al: Accreditations & Locations
20
CSC
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG: DATEITI ME: PAGE:
TBL Laboratory TBL-27965 L946946 11107/17 07AS 2 of 22

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected dateltime Received dateltime
OUTFALL #1 L946946-01 WW Kyle Greene 10/2511717:30 10127/1708:45
Cp
Method
Batch
Dilution Preparation
dateltime
Analysis
dateltime
Analyst
'T�
Wet Chemistry by Method 1664B
WG1038659
1 1110311Y 07:53
11/03015:56
STM
Metals {ICP) by Method 200.7
WC1036916
1 1110111717:49
1110211712:05
CCE
Volatile Organic Compounds (GUMS) by Method 624
WGIO36628
1 1012811717:28
10/28117 IT28
DWR
Volatile Organic Compounds (GUMS) by Method 624
WGIO36628
1 11101/17 05:52
11/01/17 05:52
ACG
Pesfrtides (GC) by Method EPA 608
WG1036867
1 11/01/17 09:17
102A714:46
VKS
Fln
Polychlorinated Biphenyls (GC) by Method EPA-608
WG1036857
1 11/01/17 09:17
1110211716:26
JNS
Semi Volatile Organic Compounds (GUMS( by Method 625
WG1038708
1 11/01/17 07:15
11104/1713:30
JF
S I"
FC1
Gi
JAI
Sc
ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
TBL Laboratory TBL-27965 L946946 11/07/17 07:48 3 of 22

CASE NARRATIVE
ONE LAB. NATIONWIDE. J#
Elp
Ail MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the
dilution factor used in the analysis. All radiochemical sample results for solids are reported on a dry
weight basis with the exception of tritium, carbon-14 and radon, unless wet weight was requested by
fc
the client. All Method and Batch Quality Control are within established criteria except where
addressed in this case narrative, a non-conformance form or properly qualified within the sample
results. By my digital signature below, I affirm to the best of my knowledge, all problemslanomalies
5S
r]
observed by the laboratory as having the potential to affect the quality of the data have been identified
by the laboratory, and no information or data have been knowingly withheld that would affect the
quality of the data.
Fri
'Qc
Gi
Darren Reeder
Technical Service Representative
Al
FS
Sample Handling and Receiving
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
ESC Sample ID Project Sample ID Method
L946946-01 OUTFALL #1 1664B
The analysis for 2-Chloroethyl Vinyl Ether was conducted from a chemically preserved container.
ESC Sample ID Project Sample ID Method
L946946-01 OUTFALL#1 624
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
TBL Laboratory TBL-27965 L946946 11/07/17 07AB 4 of 22

OUTFALL,41 SAMPLE RESULTS - 01 ONE LAB.NATtONWIDE.
Collected date/time: 10/25117 17:30 L946946
Wet Chemistry by Method 1664B
Result Qualifier RDL Dilution Analysis Batch
Analyte mgll mgfl date 1 time
Oil & Grease (Hexane Extr) ND
4.90
1 11103/201715:56
WG103B659
Metals (ICP) by Method 200.7
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte mgll
mgll
date 1 time
Copper NO
0.0100
1 11102/201712:05
WG1036916
Lead NO
0.00500
1 11/021201712:05
WGID36916
Zinc 0.0824
0.0500
1 111021201712:05
WG1036915
Volatile Organic Compounds (GC/MS) by Method 624
Result
Oualifer RDL
Dilution Analysis
Batch
Analyte mgfl
mgll
date 1 time
Acrolein
NO
Acrylonitrile
NO
Benzene
NO
Bromodichloromethane
ND
8romoform
ND
Bromomethane
ND
Carbon tetrachloride
NO
Chiatobenzene
ND
Chlcrodibromomethane
NO
Chlorcethane
ND
2-Chloroethyl vinyl ether
ND
Chloroform
NO
Chloromethane
NO
1,2-Dichtorobenzene
ND
1,3-Dichlofobenzene
NO
1,4-Dichlorobenzene
NO
Dichlorodlfluoromethane
NO
1,1-Dichloroethane
ND
1,2-1)lLhloroethane
ND
1,1-DiLhlaroethene
ND
trans-1,2-Dichloroethene
ND
1,2-Dichloropropane
NO
cis-1.3-Dichloropropene
NO
trans-1.3-Dichloropropene
NO
Ethylbenzene
ND
Methylene Chloride
ND
1,1,2.2-Tetrachloroethane
ND
Teirachloroethene
ND
Toluene
ND
1,1,1-Trichloroeihane
NO
1,1,2-Trichloroeihane
ND
Trichloroethene
NO
Trichloro0uoromethane
ND
Vinyl chloride
ND
(S) Toluene d8
110
(S) Toluene-d8
112
(S) Dibromofluoromelhone
91.8
R Dibromofluoromethone
101
(S)a,0,0-Trifluorotoluene
III
(S)a.o,o-TriRuorotoluene
105
(5) 4-8romofluorobenzene
107
(5) 4-8romofluorobenzene
104
ACCOUNT:
TBL Laboratory
0.0500 1
1110112017 05:52
0.0100 1
101281201] 17:28
0.00100 1
101281201717:28
0.00100 1
101281201717:28
0.00100 1
1012 B1201717:2 B
0. 00500 1
1012 81201717: 2 8
U0100 1
101281201717:28
D.00100 1
10128/2017 17:28
MOM 1
10128/201717:28
0.00500 1
10128r 2 01717:28
0.0500 1
10I2812 01717:28
0.00500 1
101281201717:28
0.00250 1
10/281201717:28
0.00100 1
101281201717:28
0.00100 1
101281201717:28
0.00100 1
10/281201717:28
0.00500 1
10/281201717:28
0.00100 1
10128/201717:28
0.00100 1
101281201717:28
0.00100 1
10/28120171728
0.00100 1
101281201717:28
MGM 1
101281201717:28
0.00100 1
101281201717:26
0.00100 1
101261201717:28
0.00100 1
10128/201717:28
0.00500 1
10128120171728
0.00100 1
10128/201717:28
0-00100 1
101281201717:28
0.00100 1
101281201717:28
0.00100 1
101281201717:28
0.00100 1
10/281201717:28
0-00100 1
10/281201717:28
0.00500 1
10128/201717:28
0.00100 1
101281201717:28
80.0-120
F012WO1717:28
80.0-120
711011201105:52
76.0-123
1110112017 05:52
76. 0-113
1012WO1717:28
80.0-120
1110112017 05:52
30. 0-110
1012812 01717; 28
80.0720
1110112017 05:52
80. 0-120
1012W201717:18
PROJECT:
SDG:
TBL-27965
L945946
WG1036628
WG1036628
WGIO36628
WG1036628
WG1036628
WGIO36628
WG1036628
WGIO36628
WG1036628
WG1036628
WG1036628
WGID36628
WG1036626
WG1036628
WG1036626
WG1036628
WG1036628
WG1036628
WG1036628
WGIO36628
WGIO36628
WG1036629
WG1036628
WGi036628
WG1036628
WG1036628
WG1036628
WGIO36623
WGIO36628
WGIO36628
WG1036628
WG1036528
WG1036628
NIG1036628
WGIO36628
WG1036628
WG1036628
WG1036628
DATEM ME:
11/07/17 07:48
PAGE:
5of22

OUTFAL� #1 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected daiehime: 10/25117 17:30 L946946
Pesticides (GC) by Method EPA 608
Result
mg11
Oualifier RDL
mgA
Dilution
Analysis
date 1 time
Batch
LPAnalyte
Aldrin
NO
0.0000500
1
11/02/201714:46
WG1036667
TC
Alpha BHC
NO
0.0000500
1
lV021201714:46
WG1036867
Beta BHC
NO
0.0000500
1
111021201714:46
WG1036867
Delta BHC
NO
0.0000500
1
111021201714746
WGIO36867
r qS
Gamma BHC
ND
0.0000500
1
11/02/201714:46
WG1036867
Chlordane
NO
0.000500
1
11102/201714:46
WG1036867
FCn]
4,4-DDD
ND
0.0000500
1
11/02/201714:46
WG1036867
4,4-DDE
ND
0.0000500
1
11102/201714:46
WG1036867
4,4-DDT
NO
0.0000500
1
11/021201714:46
WG1036867
Dieldrin
NO
0.0000500
1
1110212017 1446
WG1036867
Endosulfan I
NO
0.0000500
1
17102/201714:46
WG1036867
G
QC
Endosulfan 11
ND
0.0000500
t
t1I021201114A6
WGIO36867
Endosulfan sulfate
NO
O.O000500
1
11/02/2017 14:46
WG1036867
Endrin
NO
CL0000500
1
11/02/201714:46
WG1036867
GI
Endrin aldehyde
NO
0.0000500
1
111021201714:46
WG1036867
Endrin ketone
NO
0.00005DO
1
11/02/2017 14:46
WG1036867
`AI
Heptachlor
ND
0.0000500
1
11102/201714:46
WG1036867
Heptachlor epoxide
ND
0.0000500
1
11102/2017 14:46
WG1036867
Hexachlorobenzene
ND
0.0000500
1
11102/201714:46
WG1036857
FSU
Methoxychlor
ND
0.0000500
1
111021201714:46
WG1036867
Toxaphene
NO
0.000500
1
1V021201714:46
WG1036867
(S) Deco chlorobiphenyl
58.6
10.0-144
11102120171446
WG103f867
(S) Tetrochloro-m xylene
578
70.0-135
IV021201714.46
WG1036667
Polychlorinated Biphenyls (GC) by Method EPA-608
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte
mgll
mg/I
date 1 time
PCB 1016
NO
0.000500
1
111021201716:26
VIG1036867
PCB 1221.
NO
0.000500
1
111021201716:26
WG1036867
PCB 1232
ND
0.000500
1
11102/20171626
WG1036867
PCB 1242
NO
0.000500
1
111021201716:26
WGID36867
PCB 1248
ND
0.000500
1
111021201716:26
WG1035867
PCB 1254
NO
0,000500
1
11102120171626
WGIO36867
PCB 1260
NO
0,000500
1
11/02/201716:26
VJG1036867
(S) Dexchlorobrphenyl
67,7
10.0-744
1 V02120171626
%VG1036867
(S) Tetrochloro-m-xylene
66.7
10.0-135
111021201716:26
WGIO36867
Semi Volatile Organic Compounds
(GUMS) by Method 625
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
mg1l
mg11
date 1 time
Acenaphthene
NO
0.00100
1 W041201713:30
WG1038708
Acenaphthylene
ND
0,D0100
1 ll/D4/201713730
4VG1038708
Anthracene
NO
0,00100
1 111041201713:30
WG1038708
Benzidine
ND
0.0100
1 1110412017 1130
1NG1038708
Benzo(a)amhracene
NO
0.00100
1 11104/201713:30
WGID38708
Benzo(b(fluoranthene
ND
0.00100
1 1V041201713:30
1"IG1038708
Senzo(k)Iluoranthene
ND
0.00100
1 11/041201713:30
WG1038708
Benzo(g,hJ)perylene
NO
0.00100
1 111041201113:30
WC1038708
Benzo(a)pyrene
NO
0.00100
1 111041201713:30
WGIO38709
Bis(2-chlorethoxy)methane
NO
0.0100
1 111041201713:30
WGIC38708
Bis(2-chloraethyl)ether
ND
0.0100
1 11104/201713:30
WG1038708
Bis(2-chloroisopropyllether
ND
0.0100
1 111041201713:30
WGIO38708
4-Biomophenyl-phenyfether
ND
0.0100
1 11104/201713:30
WG1038708
2-Chloronaphthalene
ND
0.00100
1 IIJ041201713:30
WG1038708
4-Chlorophenyl-phenylether
ND
0.0100
1 111041201713:30
WG1038708
ACCOUNT: PROJECT; SDG: DATE/TIME: PAGE:
TEL Laboratory TBL-27965 L946946 11/07/17 07:46 6 of 22

OUT -FALL, #1 SAMPLE RESULTS - 01 ONE LAB.NATIONW10C.
Collected daleltime: 10125/17 17:30 L946946
Semi Volatile Organic Compounds (GC/MS) by Method 625
Analyte
Result
mgll
Ouatifier RDL
mgll
Dilution
Analysis
date 1 time
Batch
C p
Chrysene
ND
U0100
1
111041201713:30
WG1038708
TC
Dibenz(a,h(anthracene
ND
0,00100
1
11104/201713:30
WG1038708
33-Dichlorobenzidine
NO
0.0100
1
111041201713:30
WG1038708
,
2,4-Dlnitrotoiuene
ND
0,0100
1
1V041201713:30
WG1038708
S5
2,6-Dinitrotoluene
NO
0,0100
1
11/04/201713:30
WG1038108
1,2-0tphenylhydrazine
ND
0.0100
1
111041201713:30
WG1038708
FC
Fluorarthene
ND
0.00100
1
111041201713:30
WG1039708
Fluorene
ND
0.00100
1
111041201713:30
WG1038708
Hexachlorobenzere
ND
0.00100
1
11/041201713:30
WGi038708
Hexachloro-1,3-butadiere
NO
0.0100
1
111041201713:30
WG1038708
Hexachlorocyclopentadiene
ND
0,0100
1
111041201713730
WG1038708
QC
Hexachloroethane
ND
0.0100
1
111041201713:30
WG1038708
Indeno(1,2,3-cd)pyrene
ND
0.00100
1
11104/201713:30
WG1038708
Isophorone
NO
0.0100
1
11104/201713:30
WG1038708
Gi
Naphthalene
ND
0.00100
1
111041201713:30
WG1038708
Nitrobenzene
ND
0.0100
1
11/041201713:30
WGID38708
�AI
n-Nitrosodimethylamine
NO
0.0100
1
111041201713:30
WG1038708
n-Nitrosodiphenylamine
NO
0-0100
1
111041201713:30
WG1038708
y
n-Nitrosodi-n-propylamine
ND
0.0100
1
111041201713:30
WG1038708
SC
Phenanthrene
NO
0.00100
1
111041201713:30
WG1038708
Benrylburyl phthalate
NO
0.00300
1
111041201713:30
WG1038708
Bis(2-ethylhexy1)phthalate
ND
0.00300
1
111041201713:30
WG1038708
Di-r-butyl, phthalate
ND
0.00300
1
111041201713:30
WG1038708
Diethyl phthalate
ND
0.00300
1
1VO4/201713:30
WG1038708
Dimethyl phthalate
ND
0.00300
1
111041201713:30
WG1038708
Di-n-octyl phthalate
ND
0.00300
1
11/04/201713:30
WG7038708
Pyrene
ND
0.00100
1
111041201713:30
WG7038708
1.44-Trichlorobenzene
ND
0.0100
1
111041201713:30
WG1038708
4-Chloro-3-methylphenol
ND
0.0100
1
11/041201713:30
WG1038708
2-CWorophenot
N0
0.0100
1
111041201713:30
WG1038708
2,4-Dichlorophenol
ND
0.0100
1
111041201713:30
WG1038708
2,4-Dimethylphenol
NO
0,0100
1
11104/201713:30
WG1038708
4,6-Dinitro-2-methylphenol
ND
0.0100
1
111041201713:30
WG1038708
2,4-Dinitrophenai
ND
0.0100
1
11/041201713:30
WG1038708
2-Nitrophenol
ND
0.0100
1
111041201713:30
WG1038708
4-Nitrophenol
NO
0.0100
1
11/04/201713:30
WG1038708
Pentaehlorophenol
ND
0.0100
1
W041201713:30
WG1038708
Phenol
ND
0.0100
1
11/041201713:30
WG1038708
2,4,6-Trichlorophenol
ND
0.0100
1
111041201713:30
WGID38708
f5J2-F1uorophenol
49.8
10.0-120
W041201713:30
WG1038708
(, J PhenoPd5
32.5
10.0-120
111041201713:30
WG103870B
(5}NTtrobenrene-d5
68.6
10.0-126
111041201713:30
WG1038708
(5)2-Fluorobiphenyl
61.7
22.0-121
11104120T113:30
WG1038708
(S)1,4,6-Tribrowophenol
113
10.0-153
171041201713.30
WG1038708
Q p-Terphenyl-dN
51.6
29.0-141
1110412Gil T3:30
WC1038708
ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
TBL Laboratory TBL-27965 L946946 11/07117 07:48 7 of 22

WG1038659 QUALITY CONTROL SUMMARY ONE LAB NATIONWIDE,
Wet Chemistry by Method 16648 L946946-01
Method Blank (MB)
(MS) R3262989-1 1110311715'S2 w
MB Result M8 Oualiriet MBMDL MB RDL
A"yte m9A mgll mgll _ �TC
Oil Grease (Hexane ExlO U 1.16 5.00
Laboratory Control Sample (LCS( • Laboratory Control Sample DLlpl)cate (LCSD)
(LCS) R3262989-2 1V03/17 15.53 • (LCSD) R3262989.3 11,03)17 15 53
Spke Amount LCS Result LCSD Result LCS Rec. LCSt7 Re[. Rec. Limits LCS OUaliSer LCSD 6uali4er RPD RPD Limits
Anetyte mgA mi)A mgA % % % % %
Oil & Grease IHexane Extr) 40.0 40.0 49.1 100 100 78.0-114 U50 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
TESL Laboratory TBL27965 L946945 11107A7 07.48 6 ar 22

WG1036916 QUALITY CONTROL SUMMARY
ONE NATIONWIDE.
!�
Metals tICP) by Method 200.7 L946946-0t
Method Blank (MB)
�Q
(MB) R3262577-1 W02W 10.33
Me Result Me Oualifier Me MOL MB i
�TC
Analyze mg71 mg11 mgA
Capper U 0 007 0.010
Lead U_ 01 0.00500
'�
SS
Zinc U 0.0034 0.0500
4Cn
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (Li
(LCS) R3262577-2 1V02117 10:36 • (LCSD) R3262577-3 1V02A7 10:39
`$r
Spike Amount LCS Result LCSO Result LCS Rec. LCSD Rec- Rec. Limits LCS Qualifier LCSO Qualifier RED
RED Limits
Analyze mgll my mgA % % % %
%
Copper 1.00 1.0p 0.980 100 98 85-I15 2 LL
20
Lead 1.00 1.01 0981 101 98 85-115 3
21nc Li 1 0.975 TOO 97 H1115 2
20
20
FG1
L946823-04 Original Sample (i • Matrix Spike (MS) • Matrix Spike Di (MSD)
F1
(OS) L9a6823-04 1V02117 10:43 • (MS) R3262577-5 1V021171i
Spike Amount Original Result MS Result MSD Result MS Rec, MSD Rec. nilution Rec. Limits MS Qualifier
MSD Qualifier
RED
RPD Limits
SC
Analyze mgll mgli my my % % %
%
%
Copper I.00 ND 1.06 1.03 106 103 1 70-130
2
20
Lead 1.00 ND 1.06 1.03 106 103 1 70-130
3
20
Zinc 1.00 0,229 1.23 1.20 101 97 1 70-130
3
20
L946993-01 Original Sp.i (OS) • Mainx Spike (MS} • Matrix Spike Duplicate (MSD)
(OS) 1.946993,01 11102A7 10.57• (1 R3262577-7 1V02117 11.00 • (MSD) R3262577•8 11/02M711:04
Spike Amount original Result MS Result MSD Result MS Rec. MSD Rec, 011u0on Rat. Limits MS thraliRer MSD Oualifier RED RPD limits
Analyze Inv r1911 M94 my % % % % %
Capper 1.00 0.161 1.20 1.18 104 *2 1 70-130 2 20
Lead 100 0.D0988 1.06 1.05 105 104 1 70-130 1 20
Zinc 1,00 0.157 Ire 1.17 102 102 1 70.130 1 20
ACCOUNT: PROJECT: s0m' DATEITIME PAGE:
TBL Laboratory TBL-27065 L946948 11/07l17 07 48 9 o1 22

WG1036628
Volatile Organic Compounds
(GC/MS)
by Method 624
Method Blank (MB)
(MH) R3261354-2 10128/17 12:30
M9 Result
MB Qualifier MB MDL
Anal
mgA
mgR
AcrNeir1
U
000887
Aclybnilnle
U
0.00187
Benzene
U
0,000331
Bw Ddichlommelhane
U
0,000380
Bromoform
U
0,000469
Bromomethanc
U
0.000866
Caron tetrachloride
U
0.000379
Chlorobenzene
u
C.000348
CRlowdibromomethane
U
C.000327
Chicuoethane _
U
0 X0453
2-Chlcroethyl vinyl ether
U
C.00301
Chloroform
U
0.000324
Cnldrometnane
U
0000276
1,2-Dichlorebenzene
U
C.000349
1,3-Dichlorobenzene
U
COOD220
1,4-McNorobenzene
U
C.000274
Dichlorodinucromethane
U
0000551
1,1-Dichlorcemane
U
C,00,0259
1,2-Dichloroethane
U
C,000361
11-Dichl0roelhene
U
C,000398
trans-1.2-Dicriwoethene
U
0000396
1,2-Dichloropropane
U
C,000306
cis-1,3-Dichlompropene
U
C,000418
Van0.3 Dic loropropene
U
o.000419
Ethylbenzene
U
C_000384
Metnyleae Chloride
U
0.00100
1,1,42-Telrachloroethane
0
0.000130
Tetrachloroethene
U
C.000372
Toluene
U
C.000412
1.1.1-Tr0loroethane
U
0.000319
1,1,2-Trichlowethane
U
0.000383
Tnchlo oethene
U
0.000398
Irkinloro0tgmmethane
_
U
0,00120
Vinyl Cl _
U _
0.000259
(Sj Tbluene48
109
(SJ 03wnpAlror0me1bdne
103
`Sjo.a.a-T0wrolaluene
704
(Sj 4-Brompfl arobenzene
A21
QUALITY CONTROL SUMMARY
t 946946.01
MB ROL
mgA
0.0500
0.0100
0.00100
0.00100
0.00100
0.DO500
0.00100
0.00100
0-00100
0.00500
00500
0-005DO
0,00250
0-OD100
O.00W
0.00100
0.00500
0.00100
0.00100
0 001GO
O.00i00
0,00100
0,00100
0,00100
0.00100
0,00500
0 00)00
000100
000100
0.00100
0.00100
0.00100
0.00500
0 00100
80 0-120
76 0-T23
80.0-120
80.000
ONE LAB- NATIONWIDE.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
TBL Laboratory TBL-27965 L946946 1V07/17 07 48 10 of 22
Cp
�Ss
ACn
SSr
IN
�GI
CAI
Sc

WG1036628
QUALITY CONTROL SUMMARY
CN@ LAC. NATICNWIDE.
Volatile Organic Compounds
(GCIM5)
by Method 624
1946946-01
Laboratory Control
Sample (LCS)
(LCS) R3261354-1 1072871711:33
F
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
_
�7C
Analyte
MqA
mgA
%
%
Acrolein
0.125
00137
109
10.0-160
AtrylonAnle
0.125
0.126
101
60.0-142
3c
Benzene
0.0250
0.0240
96.0
690-123
Bromodichraromethan_e
01)250
0.0220
8?9
76.0-120
_
aCN
Bromolorm
0.0250
0.0231
92.5
67.0-032
Biomomethene
0.0250
0.0270
108
18.0.160
Carbon tetrachloride
C.0250
0.0202
80.7
63.0-122
_
'Sr
Chlorobenzene
C.0250
0.0236
94.6
794121
Chlorodibramomelhane
0.0250
0.0232
92.9
75.0-125
IIMII
Chloroethare
0.0250
0.0251
100
47-0-152
2-Chloroethyl vinyl ether
0.125
0.129
103
100-160
Chloroform
00250
0.0224
89.7
72.0121
GI
Chloromethaae
0.0250
0.0293
117
49.0-139
1,2-Dichlorobenzere
0G250
00238
95,2
80.0.120
1,3-Dichlarobenzene
0,0250
00235
93,9
72.0-123
AI
1.4 Dichlorabenzene
0.0250
0.0234
93.7
77.0-170
0iWorodittioromethane
0-0250
0.0251
100
49.D-155
5�
I,1-Oichlor0etnane
0.0250
0.0249
99.6
10.0126
1,2-Dichlaroethane
0.0250
0.0254
102
67,0-126
1,1-Akhlaroethene
D-0750
0-0209
83.5
64.0-129
trans-7.2.0icnloroelnene
0.0250
0.0224
89.8
770-121
1.2-Dichloropropane
00250
00248
99A
75.D-125
cis-i3-Dichloroptopene
0.0250
0.C229
91.5
79.0-123
trans-l.3-Dichl'oropropene
0.0250
0.0237
94.7
74,0.127
Elhyfbenzene
0-0250
0-0238
95.2
77.0.120
Methylene Chlande
0.0250
0.0247
98.3
560l121
1,1,2,2. letrachioroelhane
0,0250
0,0262
105
710.122
Tetrachlorcelhene
0.0250
00229
91.7
70.0-127
Toluene
0,0250
0.0237
95.0
77.0.120
11,1-Trichioroethane
0.0250 _
0.021B
87.1
680a22
I U-Trichkxuelhane
0.0250
0.0241
964
78 0-120
Tdchloroelhene
0,0250
0.0243
97.0
78.0420
Tdchloronuoromethane
00250
0,0243
97.1
56.0137
Vinyl chloride _
0.0250
0,0275
110
64.0.133
(SrToluene-d8
107
80.0-120
(SJOlbromaAuoromethane
102
760-123
(SJa,o.o-TrOuorororuene
f05
800.120
(S) 4-Broma,4lmradenzene
708
80 0-120
ACCOUNT: PROJECT: SUG: OATEITiME: PAGE:
TEL Laboratory TBL-27965 L946946 1V07A7 07.46 110 22

WG1036867 QUALITY CONTROL SUMMARY
Pesticides (GC) by Merhea EPA 608 L946946.01
Method Blank (MB)
tM8) R3263447-3 11(02117 11�10
MB Result MB Ouatifler M8 MOL MB RDL
Aldrin
U
0.0000081[3
0.0000500
Alpha BHC
U
0.0000166
0.0000500
Beta BHC
U
0.0000184
0.0000500
Delta BHC _
_ U
0000007
0,0000500
Gamma BHC
U
0.0000176
0,0000500
44-DDD
U
00000170
0,0000500
4 4-DDE
U
0.0000164
0,0000500
4.4-DDT
U
0.0000177
00000500
0leldnn
U
00000179
0.0000500
Endosulfan I
U
C.0000179
0.0000500
Endosulfan it
U
0.0000176
0.00005DO
Endosulfan sulfate
U
0.0000196
0.0000500
Endrin
U
0.0000189
0.0000500
Endrin aldehyde.
U
0-0000142
0.0000500
Endrin kelone
U
0.0000170
0.0000500
Heptachlor
U
a0000108
0.0000500
Heptachlor epoxide
U
D.0000175
0.00005DO
Hexachloiobenzene
U
0.000024
a 0000500
MelhoKyChldr
U
0.0000193
0.0000500
Mordane -
U
0.0000977
0.000500
_
Tosaphene
U
0-000158
0.000500
{S) DecacAlo obiphe ryl
81.1
10.0-144
(5) retrochloro-m-xyferre
82,5
100-135
Laboratory Convot Sample (LCS) • Laborr^,tery Control Sample Duplicate (LCSD)
ONE LAEf. NATIONAMDE. *
(LCS) R3263447-1 IV02117 10:42 - {LCSD) R3263447.2 11/02117 IC 56
Spike Amount
LC5 Result
tCSD Result
LCS Rec,
tCSD Roc
Rec. Limits
LCS Qualifier LCSO Qualifier RPD
RPD Lolls
Analyte
Mo
MWI
m911
%
%
%
%
�
%
-24 __...
Aldnn
0ON200
0.000182
0.000176
91.0
87.8
35,0-126
3.57
A!phaBHC
0.000200
0.000195
0.000190
97.5
94.3
550-133
2.77
10
BetaBFIC
(ION700
0OW211
0.000194
106
97.2
59.0-131
824
20
Delta BHC
0.000200
0.000215
0.000196
107
91.9
61.0-134
9,10
20
Gamma BHC
0.000200
0000203
0,000191
102
95.5
56.0-133
6.36
20
4.4-DDD
0.000200
0.000718
0,000197
109
98.6
59.0-138
10.2
20
44-DDE
0000200
0,000192
0.000170
95.8
85,0
58.0.131
11.9
20
4.4-0DT
00002CD
0,0002C1
0.000178
100
89.1
43.0-147
12.0
20
Dieldrin
0.000200
0,000219
0.000199
110
99.7
6210-136
9,55
20
Endosulfan1
0.000200
0000222
0.000202
ill
101
62,0.137
9,44
20
ACCOUNT:
PROJECT:
SOG:
DATEMmE:
TBL Laboratory
TBL-27965
L946946
11107117 07.48
PAGE'
12 of 22

WG1036867
QUALITY CONTROL SUMMARY
Pesticides (GC) by Method EPA 608
L946946,01
Laboratory Control
Sample (LCS) • Laboratory Control
Sample Duphcato (LCSD)
(LCS) R3263447-1 IV02/17 10:42 • (LC50( R3263447-2 1V02717 10:55
Spike Amount
LCS Result
LCSD ResuR
LCS Rm LCSD Rec.
Rec. Limits LCS Oualifier LCSD Ouaiiiier
RPD
Anatyte
mgA
mgA
mgA
%
%
%
%
Endasu!lan II
0.000200
0.000271
0000203
111
102
62,0-136
8,28
Endosulfan sullate
0.000200
0.000220
0.000210
110
105
60.0.139
4.88
Endrin
0-D00200
0000215
0.000195
107
97,6
58.0.135
9.49
Endrinaldehyde -
0.000200
0.000206
0000191
103
953
560-128
770
Endrin kelone
0.000200
0.000229
0.000214
114
107
54.0-142
6.69
Heptachlor
0.000700
0-000122
0.0001;1
91.2
85.6
37.0-134
6.34
HeplaOhlor ep0x1de
0,000200
0.000214
0.000195
107
97.5
60.0-132
9-21
Hexach!drobertzene
0.000200
0.D00144
0.000146
71.0
73.1
35.0-120
141
MelhoxyOlor
0.000200
0.000225
0.000209
112
105
440-160
7.28
(S AK0ch1Mbiphertyf
72.3
55.6
10.0-144
(S) Ietrocf;Wo-m,xylene
642
73 r
10.0-135
ACCOUNT: PROJECT: SDG:
T9L LaUoratory TBL-27g65 L946946
ONE LAB. NATiONWIOE.
Cp
RPD Limits
2a
20
Ss
20
20
20 e G rt
24
20 5r
25
22 ram
,GI
i15c
OATEJTIME: PAGE:
1p07n7 07-48 13 of 22

WG1036867 QUALITY CONTROL SUMMARY ONELAB.NA110NWIDG.
Polychlorinated Biphenyls 1GC1 by Method EPA-600 L946946.01
Method Blank (MB)
n
(MB( R3262611-1 11102117 15:36
L—J
MB ResuR M8 Oualifier MB MDL
Ma RDL
ETC
Analyte mgn my
mgn
PCB 1260 U 0,0000146
0.000500
PCCs1015 U 0-0000198
0.000500
3$5
PCB1221 U 0,0000244
0.000500
PCB 1232 U 0.0000213
0.000500
PCB 1242 U 0.0000242
0.000500
Crl
PCB 1249 Ll0,00DO135
0.000500
_
PCB 1254 U 0.0000181
0.000500
s
S r
N Decachlorobiphery! 83.9
100144
(5)retrachloro-mxyene 892
10.0-135
r
Laboratory Controt Sample (LCS) • Laboratory Control
Sample
Duplicate (LCSD)
FGI
(LCS) R3262611-2 11/0211715AB • �LCSD) R3262611-3 1V0211716:01
Spike Amount LCS Result LCSD Result
LCS Rec.
LCSD Ret
Rec. Limits
LCS OuakOer LCSD OualiBer RPO
RPD Limits
Analyte mgh mgll mgA
%
%
%
%
%
PC61260 0,000500 0,000418 0.000457
83.6
91.4
45,0-142
8.92
24
9
PC81016 0,000500 0,000418 0.000469
S3.6
93-9
41.0-134
11-6
23
$C
(SJ Decbchro+oorphenry4
86.8
90.4
* 044a
(SJ Tetruchwo- x)dene
69.3
870
10.0-135
ACCOUNT: PROJECT: SOG: DATEMME: PAGE:
TBL Laboratory TEL-27965 L946946 iVON17 C7.48 14 of 22

WG1038708
QUALITY CONTROL SUMMARY
ONE LAB. NATION4VIDE.
Semi Velntile Orgersic Compounds
(GCIMS1 by Method 625
L946946-01
-
Method Blank (MB)
CD
(MB) R3263321-3 11104/17 10',20
MB Result
MB Oualifier MB MDL
MB ROL
Anatyte mgA
mgA
mgAT,�C-.
Acenaphttrene U
0.000316
0,00100
Acenaphthylene U
0.000309
0,00100
s
Ss
Anthracene U
0.000791
000100
Azobenzene U
0.000164
0.0100
2
a
Benzidine U
0.00210
0,0100
Crl
Ben7o(a)an[Wcene U
0.000111
0,00100
Benzo(bl9uoramhene U
0.0000396
0,00100
7 S!
Benzo(kjfluorarthene U
0000265
0.00100
Benzo(g,h,i(perylene U
0.000161
0.00100
Benzo(a)pyrene tl
0,000269
0.00100
&s42-chlorethax�methane U
0.000214
0.0100
Bis(2-chloraethygether U� ..
0.000214
0.0100
GI
Bis(2-01010iwpropylMether U
0,000308
0.0100
4-Bwrn0pheny1-phenyle1aer U: V
0000180
00100
CAI
2-Chloronaphthalene U
0000204
0WOO
4{hwophe(ryl-phenyletner U
0000170
0.0100
Chrysene u
_
0000133
0-00100
'ts0
Dibenz(a.h)amhracene U',
0.000251
0.00100
3,3-Dichlorobenzidme U
0,D0169
00100
2,4.Dinitrotoluene U
0,000219
00100
2.6-Dinitrotoluene U
000143
0.0100
Fluoranthene U�
0000342
a.D0100
Fluorene U
0.000177
000100
Hexachlorobenaw U t
0.000227
0.00100
_
Hexachlaro-1,3-butadiene U
0.00264
0.0100
Hecachlorocydopentadiene U
0.00180
0.0100
Heochlaroetdane U
0.DOA13
0.0100
indeaop.2.3-ccilpyrene U
0000333
0.00100
Iwphorone U
0000238
00100
Naphthalene U
0.000413
0.00100
W(obenzene U
0.000200
0.0100
n-Nitrosodimelhytamine U
0.00255
00100
n-NitrasodEpherrylamine U
0,000137
0.0100
n-Karosodi-n-propylamine U
_ 0.000311
00100
Phenanthrene U
0000205
0.00100
Benrylbutyl pMalate U
0.000395
0.00300
902-ethylhexyllphlhalate U
0000496
0.00300
0i-n-butyl phthalate U
0000275
0-00300
Diethyl phthalate u
0.000356
0.00300
Dimethyl phthalate U
0.000338
0,00300
ACCOUNT:
PROJECT: SOG:
DATEMME: PAGE:
TSL Leborawy
TBL-27965 L945946
11107117 07:48 15 of 22

WG1038708
QUALITY CONTROL SUMMARY
ON=LAB NATIONWIDE. '
Semi Volntile Organic
Compounds
(GC1MS) by Method 625
1-946946,01
Method Blank (MB)
(MB) R3263321-3 11104/1710�20
p
•TC
MR Result MR Oeahfier M3 MDL MR RDL
Analyte
mgA
mgA
mgA
Di-n-"l phthalate
U
D.D00277
0,00300
Pyrene
U
0.000295
0.00100
Ss
1,24-Trlchlamhenzene
U
0.D00355
0,0100
4-Clnam-3-metnylphenol
U
0-D00229
0,0100
a
2-Chlorophenol
1)
0.000190
0,0100
G�
240chlorophenol
U
0.000972
0.0100
2 4-Dimethylphenol
U
0.00134
0.0100
Sf
4,6-Diniva-2-methylphenpl
U
000260
0.0100
2,4-DaUcphenol
U
0.00230
0,0100
2-Nlpophenol
U
0.000279
0,0100
Worm
4-Nnrbphen0l
U
0.00273
0.0100
Penta[hlorophenol
J,,
0.000407
0,0100
'GI
Phenol
U
0130113
0.0100
2.4,&Trlehlomphenol
U�'
0,DD0278
0.0100
f
(5)NiLabenrene-d5
56.3
10.0-726
0 2-Fluorobiphenyl
525
22.0-127
(5) p-Terpheny1414
48.9
29.0-141
� SC
(5) Pben045
25.8
V 0- r24
(5) 2-Fluorophendl
41.4
10 0720
(5)1,4.6-TribromophenO
79.3
10.0453
Laboratory Control 5antpie (LCS) • LaboratoIv Control Sample Duplicate (LCSD)
US) R3263321-1 11104117 09:33 - (LCSD) R3263321-2 1VO4117 09:57
Spike Amount
LCS Result
LCSD Result
LC5 Rec
LCSD Rec
Rec. Umits
LSS Qualifier LC50 Quatifer RPO
RPD Timis
Analyte
mgA
mg11
m9A
%
%
%
%
%
Acenaphlhene
0.0200
0,0114
0.0117
57.0
58.6
42.0-120
2.71
22
Acenaphlhylene
C.C200
00133
0.0134
66.7
66.8
43.0-12G
0.150
22
Anthracene
C.0200
0.0137
0.0148
68.7
73.9
44.0-120
7.39
20
AzoUenene
00200
0.0150
0,0156
75.1
78.2
37.0-125
415
2D
Benzidioe
0,0200
000898
0,0103
449
51.6
1.0W20
13.9
36
8enzo(a)an1hrace11e
00200
0.0132
0,0134
65.8
66.9
44.0.120
172
20
Senzo(binuoranlhene
00200
0.0130
0.0135
65.1
67.5
40.0-120
3.63
21
Benzo(>)Ouoronthene
0.0200
0.0139
C.0147
69.4
73.3
40-00
5.44
22
Benzalg,h,i)perylene
0 0200
0.0150
0.0157
741
7aA
45.0.12i
4.55
20
Benzo(a)pyrene
0,0200
0.0139
0 D144
69.5
71.8
41.0-120
3.2C
20
Bnl2-Chloreihory)methane
0,0200
0.0121
0.0115
60.5
57.7
36.0420
4.81
25
802-chloroezhyl)clher
00200
0.0132
0.0130
65.8
65.1
24.0-120
1,00
29
Bis(2�hloroiwpropy9elher
D.0200
0.0110
C,0114
55.1
We
32.0-120
3.02
29
ACCOUNT:
PROJLC7:
SDG:
pATFq[ME: PAGE:
TSL
Laboratory
TBL-27965
1-946346
wOV7 OZ48 16 01 22

WG1038708 QUALITY CONTROL SUMMARY
Semi Volatile Organic Comaounds 1GC1M61 t>y Method 625 L946946-01
Laboratory Control Sample (LCS) - Laboratory Control Sample Duplicate (LCSD)
(LCS) R3263321-1 11/04117 09:33 • (LCSD) R3263321-2 11/04/17 0957
Spike Amount LCS Result LCSD Result
Analyte n* mgll mg71
LCS Rec.
%
4-51CM03henyl-phenylether
0.0200
0.0140
0.0151
70.1
2-Dloronaphihalene
0.0200
0.0112
0.0111
55.8
4-Chloropne*pherrylether
00200
0-0133
0-0134
66-5
Chryseie
0.0200
0.0134
0.0140
66.8
Dibenz(a,h)anlhracene
0.0200
0.0157
0.0162
78.6
3.3-Dichlorobenzldine
0.020C
0.0157
0.0166
78,4
2,40rutrotoluene
0.0200
0.0153
0.0160
76.7
2.6-Dininiciluene
0.0200
0.0738
0.0144
69.9
Fluoranthene
0.0200
0.0149
0.0159
74,7
Fluorene
0.0200
0.C134
C C134
66.8
Hexachtorbbenzene
0.02r30
0.0158
0.0169
78.8
HerachloraL3-butadienp
0.0200
0.00911
0-00812
45.6
Hexachlorocytlopemabiene
0-0200
0.00768
0.00742
38A
HeNachloroethane
0.0200
0.00839
0,00774
42.0
Indeno(1,2,3-cdlC7rene
00200
0-0159
0-0163
79.5
ISOO=One
0.0200
0.0140
0.0139
70.2
Naphthalene
0-0200
000908
0,00363
45.4
N:uobenzene
0.0200
0.0121
0.0117
50.4
n-Nitrbsodimelhylamine
0.6200
OD108
0.00914
539
P-Nitr05odiphenylamine
0-0200
0,0129
0,0139
647
iAitr050d5-n-propylamine
0,0200
0,0136
0,0135
68,9
Pherlanituene
00200
0,0127
00137
53,7
Benaylbotyl phthalate
0D200
0,0127
0.0131
53.3
BisrDelhylheayljphlhalate
0,0200
0,0131
0,0130
656
Di-n-botyl phthalate
0,0200
0.0156
0,0162
77,8
Diethyl phthalate
0.0200
0,0147
00159
73.6
Oimelhylphthalale
010200
00140
00149
69.9
Di-n-aryl phthalate
0.0200
0.0135
0.0133
67.4
Pyrene
0,020C
00128
0.0133
638
1,2.4-frichlorabenzene
0.0200
0.00869
0.008C2
434
4-Chloro-3-meihophenal
0.0200
0.D133
0.0128
66.4
2-Chlorophenol
00200
00115
0.0109
57.8
2,4-Dichlorophenai
0.02C0
0.0123
0.0120
61.4
2,4-DimelNphenol
0.0200
0.0109
0.0103
544
-4,6-Dmitro-2-7ethylphenol
0.0200
0.0138
0.0149
69.0
24-0initrophenol
0.0200
0.0108
0.0101
540
2-14itrophenol
0.0200
0.0118
0.0108
59.1
4.Ndrophenol
0.0200
0.00494
0.00471
24.7
Pentachloropherol
0-0200
0.0108
0-0112
54.1
Pherwl
0.0200
0.00588
0.00532
29.4
ACCOUNT:
TBL
Laboratory
LCSD Rec.
Rec-Limits
LCSOualifer LCSD Qualifier APD
RPDLimits
75.5 T
42 0.121
7.35
21
555
37.(020
0460
74
56.8
44,0-120
0.380
21
69.8
45.0.120
4.49
20
80.9
44,0-171
2.73
21
82.9
29.0-153
5.55
23
80.0
47.0-127
4.27
21
72.1
42.0.120
4.44
12
79.4
46.0a21
6,10
20
65.9
45.0-120
0.260
21
84,4
410,124
686
21
40.6
26-0-120
115
31
37.1
10.0-120
345
31
3133
22.0-120
803
34
817
45.0-123
2.75
21
69.6
37,0-120
0.950
24
43.1
33.0-120
506
28
58.7
31.0-120
2,86
28
4S 7
10.C-120
16-3
34
69.3
44.0.120
6.77
21
67.9
MOAN
1.47
21
58 4
42-0-120
7,21
20
65.4
36.0-123
3.30
22
652
37.0.121
0580
21
81.1
43.0-122
4.15
21
793
48,0-123
7.49
20
74,6
47.0-120
6.43
20
66.4
38.0-120
1.52
22
56,6
430120
438
21
40,1
29.0-120
8.01
29
64.0
39 0-120
3.70
22
54,6
28.0.120
5,71
29
60.1
37.6-120
2.18
26
51.4
350.120
5-81
25
74.5
34.0.125
7.84
27
53.3
100.120
1.39
40
54.0
35.0.720
8,90
28
23.5
10.0.120
4.84
35
55.8
20.0-126
3,14
32
26.6
10.0.120
10.1
34
PROJECT:
SDG:
DATEMME:
TBL-27965
L946946
iV07/l7 07:49
ONE LAB. NATIONWOE.
PAGE:
17 of 22

WG1038708 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC7M5) by Method 62S 1946946-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
ONE LAB. NATiOPlVADE. �
CD
(LCS) R3263321-I 1v04n7 09:33 • (LCsoa R3263321-2 11r04n7 09:57
50ke Amount LCS Result LCSD Result
LCS Rec. LC50 Rec, Rec. Limits LCS Dua(ifier LCSD Qualifier RPD RFD Limits
Analyte nevi mgA mgA
%
% % % %
2,4,6-Tnchloraphenol 09200 0.0154 0.0153
77.0
76,6 40.0.122 0.530 24
(5) Nrfrobenrer+e-d5
636
610 10.0-126
3
SS
(Sj 2-FArorobtowyl
64.8
62.8 22.0-127
Pitt- reephenyfdr4
58.3
59.4 29.0.147
4
(SJ Phenol-d5
30.0
26.5 10.0420
C n
Q 2-Fluorophenol
49.5
42.5 10.0-120
(S) Z4,6-Tribromcphenol
117
122 10.0453
s f
�GI
Al
5c
ACCOUNT: PROJECT; SDG: DATE1TlME: PAGE:
T31- Laboratory TEIL-27965 L946946 - W0747074S 18 or 22

GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
Ed
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
`Tc
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
r
q
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Cn
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
El
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
QC
Analyle
The name of the parilcular compound or analysis performed, Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, or if concentrations of anafytes in the sample are higher than the
Dilution
highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value
different than 1 is used in this field. the result reported has already been corrected for this factor,
These are the target % recovery ranges or %difference value that the laboratory has historically determined as normal
AI
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analyses recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
SC
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result m this column may state "ND" (Not Detected) or "BDL"
Result '
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample lD and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
ACCOUNT: PROJECT: SSG: DATE/TIME: PAGE:
TBL Laboratory TBL-27965 L946946 11/07/17 07:46 19 of 22

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Tc
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Cn
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VT2006__
a
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C1915
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TNO0003_
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9980939910
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CERT0086
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A21LA
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Our Locations
ESC Lab Sciences has sixty-four client suppon centers that provide sample pickup andlor the delivery of sampling supplies. If you wouid like assistance from one of our support offices. please
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WA
0 ME
MT NO
OR r.1N
rD gp O V1rt NY
W y not 7p
IA a PA 0
NV NE OH i
MT P rL 1rr�
CA CO KS 410 WV VA
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AZKy
Nr.7 A AR � O
SC
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TX LA s
AK I? T \
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ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
TBL Laboratory TBL-27965 L946946 1110YI17 07:48 20 of 22

I
alTv Inrmmaton :, MaFjalsACaraalnsrlpresenati+a
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Laboratory , Inc.
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[phone] _ m_ ____
IRL VERIFIED o/s
SAMPLE VOLUME TO 9E
pmJees C -- j?
�faaa MLS As C014PARED
�ESC
TO CALIBRATED EOff Q'
►tea: cr�u, tiffs.: lsay:
FAY' aL
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(0 �p ca
CgOetued by (;agnate n)' (Lab MUST rid NLWIed) Aare lies, tip Nee�jd: �
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Temp: 13011tea Recehre
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Dale: Tlrnc; pltCheckGl: MCF:

EkIAB.�CIERCES
-.Cooler.Receiot Forni-
Glicni: -Tj3LL-A G SDGR C [ k
lA l
Cooler RvcdvcJJOpcneJ On: lOtIl 117 Temperawre:
1, J&-
Rco:ivcJ by. Kevin Turner
Receipt Check Ust NP
Yes
No
COC Seal Present / Intact?
COG Signed / Accurate?
Bottles arrive Intact?
Correct bottles used?
Sufficient volume sent?
If -Applicable..
VOA Zero headspace?
Preservation Correct / Checked?

e;
Semi-annual Stormwater Discharge Monitoring Report
for. North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted Ir f 3 - / 7_
ECEI v ED
JUN 2 p ?011
CERTIFICATE OF COVERAGE NO. NCG03 O 0 0 'b �C'� f 3b AMPLE COLLECTION YEAR _ o 17 BEN- RAL PIL,,,c
FACILITY NAME C-otit, �t Tdn L„ ,[� M .-„- �y V / SAMPLE PERIOD {�an-June ❑ July -Dec C7fOn.?
COUNTY l I/�I or El Monthly' monti�
PERSON COLLECTING SAMPLES DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY nL Lab Cert. tt GO 1 (a _ ❑Zero-fiow []Water Supply []SA
Comments on sample collection or analysis: tther 1R3.tnRa� ��k
Part A: Stormwater benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -)
❑ No discharge this period??
Outfall No,
-Date Sample
p
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
I
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics$
Benchmarks ===>
-
100 mg/L ar 5 mg/L
6.0 — 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
1 mg/L
`ram
0
•�5
.
o.
<
.1
cyth L
f
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance For the same parameter at the same outfall.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
" See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes, For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and far cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit pate: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TT'O monitoring waiver, the discharger shall sign the following certification statement:
" Liased upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility Is Implementing the all the provisions of the
solvent management plan included in the Stormwaater Pollution Prevention Plan."
Ve. slat '
Name (Print name)
Title (P int title)
/3-/7
{Signature) (Date)
Note: Results must be reported In numerical format. Do not rel2ort below Detection Limit, BDL, <PqL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they, must be repMed in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tierl, Tier1, or Tler3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
No discharge this period?2
Outfail No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
inches
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks ==_>
_
-
15 mg/L
100 mg/L or 50 mg/V
6.0 -- 9.0 SU
Footnotes from Part A also apply to this Part Q
See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date. 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note. If you report a sample value in excess of the benchmark, you must Implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text.
FOR PARTA AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART ti SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXC£EDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL7 YES ❑ NO Q�
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copv of this OMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitorina period
in the case of. "No Discharge" reports)to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION_ FOR ANY INFORMATION REPORTED_
"I certify, under penalty of law, that this document and -all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible forgathering the Information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
{Signature of
Permit Date: 11/1/2012-10/31/2017
-/-3- I %
(Date)
SWU-245, last revised 10/25/2012
Page 3 of 3

Shipping:
2401 W. 51" St.
Lumberton NC 28358
COUNCIL TOOL COMPANY
345 PECAN LANE
LAKE WACCAMAW, NC 28450
ATTN: VELTON JACOBS
SAMPLE NUMBER - 1290
DATE SAMPLED - 4-24-17
DATE RECEIVED-4-24-17
TIME RECEIVED - 1030
PAGE 1 OF 1
it
Mailing:
PO Box 589
Lumberton, NC 28359
FINAL REPORT OF ANALYSES
SAMPLE ID - OUTFALL # 1
SAMPLER - V. JACOBS
DELIVERED BY - CLIENT
Phone: [phone]
Fax: [phone]
Email: am.hester-
tbl(a�hotmaii.com
PROJECT NAME:TBL-27616
REPORT DATE:5-1-17
ANALYSIS
METHOD DATE
RESULT
BIOCHEMICAL OXYGEN DEMAND
SM5210-B
N/R
TOTAL SUSPENDED SOLIDS
SM2540D 4/25/2017
8.4
AMMONIA NITROGEN
SM4500NH3D
N/R
FECAL COLIFORM
SM9222D
N/R
CONDUCTIVITY
SM2510B
N/R
CHEMICAL OXYGEN DEMAND
SM5220D
N/R
PH
SM4500 H+B 4/25/2017
7.0
VOLATILE SUSPENDED SOLIDS
SM2540E
N/R
N/R = ANALYSIS NOT REQUESTED
LABORATORY DIRECTOR
SAMPLE MATRIX - WW
TIME SAMPLED - 0930
RECEIVED BY - THK
QUAIL
DET.
UNITS CODE
LIMIT
MG/L
2.0
MG/L
5.0
MG/L
0.1
COL/100M L
1
UMHOS/CM
10
MG/L
30.0
STD UNITS
0.1
MG/L
500
NCDENR DWQ # 37, NCDENR DW # 37781

T B L E nv i ro n m e n to l
Billing Information:..
Ana lysislContainerlPreservative
— _
Laboratory , Inc.
2401 W. 5th St
Lumberton, NC 28358
ePnrt,o:
[phone]
mail ,n.
P roject
Description: �61N v0`
C ity/sate
CollecL-d
N
Phone: Client Project #:
ESC Key:
FAX: -T6 L -
Collected by. ` Site/Facility lD#:
i'
P.O.#:
6
BOO
Collected by (s)gnature): Rush? ( Lab MUST Be Notified) Date Results Needed:
l
Cocode
(lab use only)
Same Day
Next Day........
....... 200%
100% Email? —No —Yes
No. t
� D
0TernplatelPrelogin
Two Day
Immediatei Packcd on ]ce N Y
.........50°/ FAX? No_Yes
° —
of
Cntrs i � 1
_
L O
Shipped Via:
Sample ID Comp/Grab Matrix`
Depth Date Time
Remarks/Contaminant
Sample # (lab only)
I 1-
1-21-11
9'.30
TRL VERIF
ED R/G
SAMPLE VO
DAME TO BE
TO CAL
- -
—
J
0 l 6 V�i
i
H 1 h R
EN MEN
LSI} IN1 -.
'Matrix SS-SciVSclid GW- Groundwater WW - WasteWater DW - Drinking Water OT- Qther
Remarks:
RZlt::A
pI ; Temp
Plow Other
RVuished by)n ure
Y: (
Relinquished b ture)
Date:
I —T
me:.
e eived b ig Lure)
Received by: (Signature)
Samples returned via: ❑UPS
❑ FedEx ❑ Courier ❑
Condition: lab use only)
Date:
Time:
Temp:
Bottles Received:
"Y
CoC Seals Intact: _ Y _ N NA
Petinquished by: (Signature)
Date:
Time:
Received for lab by: (Signature)
Date:
Time:
pH Checked: NCF:

elementOne
FINAL REPORT OF ANALYSES
Element One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Phone: [phone]
Fax: 9i 0 792-6853
[e-mail]
Pam Hester
May 4, 2017
TBL Laboratory
Client Project Name Council Tool
P.O. Box 589
Client Project Number TBL-27616
Lumberton, NC
28359
PO Number
E1 Project Number e29363
Sample #
Sample ID
Outfal[ # 1
Sample Matrix
WW
Sample Type
Date Received
04/26/2017
Date Sampled
04/24/2017
Time Sampled
0930 Time Received
1300
Delivered by
Picked Up
Sampler
V. Jacobs Received by
MFD
E1 Sample #
29363
Parameter
Result Unit Dilution DL Method
Date
Copper
0.009 mg/L
1 0.003 EPA 200.8
04/27/2017
Zinc
0.103 mg/L
1 0.005 EPA 200.8
04/27/2017
Lead
< 0.003 mg/L
1 0.003 EPA 200.8
04/27/2017
Katie Strickland, QA Coordinator
TBL-27616 Report Compiled by,
NC Certifications: DW 37788 and DWQ DENR 604

Collerle-d by (siynalure): Rusfr7 Late MUST Be Notified il
( ) ato Rcsul(s NcC�dc{l:
-- Same Day ....... 200% —_�- ' i I
ivnxtDay........ I00% Enrnil7--Nu—Yos
�• 1 ` CaCoJe (lab use orty)
Nc s
L 3 9 !J TClnplaielPCe.lOglrl
_ Two Day ......... a01/ FAX No _ —Yes
lrrru diztoly?�c'cd on Icc T �"•
of "�
5hippetl Via!
—•
i
Sample ID IComplC;rab iw^atrix* Depth Dale TimO
Gnhs
tiemarkcfCcnfomEaunl Sarnplc:t(lab oWy)
— -- — --- -- -- -- rrr
�T �fl �- -- --
►� w
J-a`(-l7
9 .3oA
Till. VER I
En 0/8
SAMPLE VO
RME TFBE
-- ----
— U-MtS
-S--" tP*R- U—
'
(—"
J
a/ 6
r r
FOR �1ETtL��y�)NT
-
Malrlr,. SS - SoillSohd GN- Groundwatel' M - WasteWatur DW - DrinkiaA UVater OT - le
Remarks:
Flaw
Temp
Other
P, li:.,ttished h^: {S n Lure
Rei'nquist ed h. 1q' '.trre)
Dale:
Date:
T , e:. -r
Time:
_
{eceived b ' g brre}
Row Ivedby: {Slgnalure}
5arm les returned via: 0 UPS
L FedFx O Courier
Condition: lab use onl
( Y)
GoCSaa:slniacf:NA
Temp:
�
Bo111es Received:
—
—Y—N
Rrllnquls}rCd w (510tkuture)
-- - — —�
Date:
Time:
E
Receiv d or I : {Slgna turn
4kOW',I
Dale:
Z -��
i ime:
pl i Checked:
L,
tvCF:

#ESC ANALYTICAL REPORT m ESC
L•A'6 5.5C.r•E.NIC'E-S May 02, 2017
TBL Laboratory
Sample Delivery Group:
L905120
Samples Received:
04/26/2017
Project Number:
TBL-27616
Description:
Council Tool
Report To: Pam Hester
P.O. Box 589
Lumberton, NC 28359
Entire Report Reviewed By
Darren Reeder
Technical Service Representative
Results re&ne only to the items rested Or Calibrated and are reported as rounded values. This lest report shall not be
reproduced, except in full, without written approval of the Idboratory, Where applicable. sampling conducted by ESC is
performed per guidance provided in laboratory standard operating procedures: 060302, 060303. and 060304.
'
�
t-
�

TABLE OF CONTENTS
ONE LAB. NATIONWIDE,
'Cp: Cover Page
1
2Tc: Table of Contents
2
3Ss: Sample Summary
3
0
4Cn: Case Narrative
4
5Sr: Sample Results
5
FSS
OUTFALL #1 L905120-01
5
r'Qc: Quality Control Summary
8
rCn]
Wet Chemistry by Method 1664B
8
rsrl
Volatile Organic Compounds (GC/MS) by Method 624
9
Pesticides (GC) by Method EPA 608
11
H
Polychlorinated Biphenyls (GC) by Method EPA-608
13
Fi
Semi Volatile Organic Compounds (GC/MS) by Method 625
14
7GI: Glossary of Terms
18
jAl
"Al: Accreditations & Locations
19
9Sc: Chain of Custody
20
9Sc
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
TBL Laboratory TBL-27616 L905120 0510211711:57 2 of 21

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected dateltime Received dateltime
OUTFALL #1 L905120-01 WW V Jacobs 041241170930 04126/1709:00 r
Cp
Method
Batch
Dilution Preparation
dateltime
Analysis
dateltime
Analyst
TC
Wet Chemistry by Method 16643
WG974724
1 04/28117 08:36
04128/1715:08
SHG
Volatile Organic Compounds (GCIMS) by Method 624
WG974433
1 04/27/1719:00
04127/1719:00
JHH
Pesticides (GC) by Method EPA 608
WG974316
1 04/28117 08A5
05/01117 12:41
VK5
Polychlorinated Biphenyls (GC) by Method EPA-60B
WG974316
1 04/28/17 08:45
0412911714:55
VKS
Semi Volatile Organic Compounds (GC/MS) by Method G25
WG974640
1 04/28117 08:43
05/02/17 08:56
JF
a
Cn
Fr
FC1
GI
VAI
9
SC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
TBL Laboratory TBL-27616 L905120 05/02/1711:57 3 of 21

CASE NARRATIVE ONE LAB, NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
-Ch
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
Tc
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problem s/anomahes observed by the
Ss
r]
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of
the data.
Qc
GI
Darren Reeder
Technical Service Representative
Al
r
ACCOUNT: PROJECT: SDG: DATEITIMiE: PAGE:
TEL Laboratory TBL-27616 L905120 05/02/17 ii:57 4 of 21

OUTFALL #1 SAMPLE RESULTS - 01
Collected dateltime: 04/24/17 09730 L905120
Wet Chemistry by Method 1664E
Result Oualifier ROL Dilution Analysis
Analyte mgA mgA date 1 time
ONE LAB, NATIONWIDE.
Batch
Oil & Grease (Hexane Extr) NO 5.00 1 04128/201715:08 WG974724
Volatile Organic Compounds (GC/MS) by Method 624
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
mgll
mgA
date/time
Acrolein
ND
J4 0.0500
1 041271201719:00
WG974433
Acrylonitrile
NO
0.0100
1 041271201719:00
WG974433
Benzene
NO
0.00100
1 04/271201719.00
WG974433
Bromodichloromethane
NO
0.00100
1 041271201719:00
WG974433
Bromoform
NO
0.00100
1 04127/201719:00
WG974433
Bromornelhane
NO
0.00500
1 04127120V 19:00
WG974433
Carbon tetrachloride
ND
0.00100
1 04127/2017 1900
WG974433
Chlorobenzene
NO
0.00100
1 04/271201719:00
WG974433
Chlorodibromomethane
NO
0.00100
1 04/27/201719:00
WG974433
Chloroelhane
NO
0.00500
1 041271201719:00
WG974433
2-Chlomethyl vinyl ether
NO
0.0500
1 04/27/201719:00
WG974433
Chloroform
NO
0.00500
1 04/271201719:00
WG974433
Chloromethane
ND
0.00250
1 04/27/201719:00
WG974433
1.2-Dichlorobenzene
NO
0.00100
1 04127/201719:00
WG974433
1,3-Dichlorobenzene
NO
0.00100
1 04/27/201719:00
WG974433
1,4-Dlchlorobenzene
NO
0,00100
1 04/27/201719:00
WG974433
Dichlorodiiluoromethane
ND
0.00500
1 041271201719:00
WG974433
1,1-Dichloroelhane
ND
0.00100
1 041271201719:00
WG974433
1,2-1chloraethane
NO
0-00100
1 04/27/201719:00
WG974433
1,1-Dichloraethene
NO
Moll)()
1 041271201719:00
WG914433
trans-1,2-Dichloraethene
ND
0,00100
1 041271201719:00
WG974433
1,2-Dichloropropane
ND
0.00100
1 04/27/201719:00
WG974433
cis-1,3-Dichloropropene
NO
0.00i00
1 04127/201719:00
WG974433
trans-1,3-Dichloropropene
NO
0.00100
1 041271201719:00
WG974433
Ethylbenzene
ND
0.00100
1 04/27/201719:00
WG974433
Methylene Chloride
NO
0-00500
1 04/27/2017 19:00
WG974433
1,1,2,2-Telrachloroethane
NO
0.00100
1 04127/201719:00
WG974433
Tetrachloroethene
ND
0,00100
1 04127/201719:00
WG974433
Toluene
NO
0,00100
1 04/271201 7 19:00
WG974433
1.1.1-Trlchloroethane
ND
0.00100
1 C41271201719:00
WG974433
1,1,2-Trichloroethane
ND
0.00100
1 041271201719:00
WG974433
Trichloroethene
NO
0.00100
1 04127/201719:00
WG974433
Trichlorofluoromethane
ND
0.00500
1 041271201719:00
WG974433
Vinyl chloride
ND
0.00100
1 041271201719,00
WG974433
(S) roluene-d8
105
80.0-120
041271201719:00
WG974433
(S) Dibromofluoromelhane
104
76.0-123
041271201119:00
WG974433
(S)a,a,o-Trifluorotoruene
103
80.0-120
041271201719:00
WG914433
(S) 4-Brornofluoroberrzene
93.7
80.0-120
041271201719:00
WG974433
Pesticides (GC) by Method EPA 608
Analyte
Result
mg/1
Qualifier RDL Dilution
mgll
Analysis
date 1 time
Aldrin
NO
0.0000500 1
05/01/201712:41
Alpha BHC
NO
0.0000500 1
051011201712:41
Beta BHC
NO
0.0000500 1
051011201712A1
Delta BHC
NO
0.0000500 1
05101/201712:41
Gamma BHC
NO
0000500 1
051011201712:41
Chlordane
NO
0.000500 1
05/011201712:41
4,4-DDD
NO
0,0000500 1
05101/201712:41
4,4-DDE
NO
0.0000500 1
05/011201712:41
ACCOUNT:
PROJECT:
SDG:
TBL Laboratory
TBL-27616
L905120
Batch
WG974316
WG974316
WG974316
WG974316
WG974316
WG974316
WG974316
WG974316
DATEMME:
05/02/17 11:57
PAGE:
5of21

OUTFALL #1
SAMPLE
RESULTS - 01
ONE LAB. NATIONWIDE.
Collected dateltime: 04124/17 09:30
L905120
Pesticides (GC} by Method EPA 608
Cp
Result Qualifier
ROL
Dilution
Analysis
Batch
Analyte mgA
mgll
date 1 time
4,4-DOT NO
0.0000500
1
0510i1201712:41
WG974316
TC
Dieldrin ND
0.0000500
1
05/01/201712:41
WG974316
Endosulfan I NO
0.0000500
1
05/011201712:41
WG974316
s
Endosulfan It NO
0.0000500
1
05/01/2017 12:41
WG974316
Ss
Endosulfan sulfate NO
0.0000500
1
05101/201712:41
WG974316
Endrin ND
0.0000500
1
051011201712:41
WG974316
rqn
Endrin aldehyde ND
0.0000500
1
05/01/201712:41
WG974316
Endrin ketone ND
0.0000500
1
05/01/2017 12:41
WG974316
Heptachlor NO
0.0000500
1
05/01/201712:41
WG974316
Heptachlor epoxide NO
0,0000500
1
051011201712A1
WG974316
Hexachlorobenzene NO
0.0000500
1
051011201712:41
WG974316
'QC
Melhoxychlor NO
0.0000500
1
051011201712:41
WG974316
Toxaphene ND
0.000500
1
051011201712:41
WG974316
(S)Oecachlorobrphenyl 53.7
10.0-744
051011201712:41
WG974316
GI
(5) Tetrochloro-m-xylene 60.9
10.0-135
05/01/201712:41
WG974316
yA!
Polychlorinated Biphenyls (GC) by Method
EPA-608
Result Qualifier
RDL
Dilution
Analysis
Batch
3
Sc
Analyte mg/1
mgA
date 1 time
PCB 1016 NO
PCB 1221 NO
PCB 1232 NO
PCB 1242 NO
PCB 1248 ND
PCB 1254 ND
PCB 1260 NO
(S) Decachlorobipheoyl 55.8
(S) Tetrachloro-m-xylene 6Z6
Semi Volatile Organic Compounds
0,000500 1
0.000500 1
0.000500 1
0.000500 1
0.000500 1
0.000500 1
0.000500 1
10.0-144
10.0-135
(GC/MS) by Method 625
04/29/201714:55
04/29/201714:55
041291201714:55
04129/201714:55
04/29/201714:55
041291201714:55
04/29/201714:55
04/29/201714:55
04/2W01714:55
WG974316
WG974316
WG974316
WG974316
WG974316
WG974316
WG974316
WGOY4316
WG974316
Result
Qualifier RDL Dilution
Analysis
Batch
Analyte
mgA
mg/1
date 1 time
Acenaphthene
NO
0.00100 1
05102/2017 08:56
WG97454D ^
Acenaphthylere
NO
0.00100 1
05/02/2017 08:56
WG974640
Anthracene
NO
0.00100 1
0510212017 08:56
WG974640
Benzidine
NO
0.0100 1
0510212017 08:56
W0974640
Benzo(a)anthracene
ND
0.00100 1
05/02/2017 08:56
WG974640
Benzo(b)Uoranthene
NO
0.00100 1
05/02/2017 08:56
WG974640
Benzo(k)fluorarthene
ND
0.00100 1
05/02/2017 08:56
WG974640
Benzo(g,h,i)perylere
NO
0.00100 1
05/021201708:56
WG974640
Berzo(a)pyrene
NO
0.00100 1
05/02/2017 08:56
WG974640
Bis(2-chlorethoxy)methane
NO
0.0100 1
051M2017 08:56
WG974640
Bis(2-chloroethyl)ether
NO
O.0)OG 1
05/021201708:56
WG974640
Bis(2-chloroiscpropyl)ether
NO
0.0100 1
05/02/2017 08:56
WG974640
4-Bromopheryl-pherylelher
NO
0.0100 1
05/021201708756
WG974640
2-Chloronaphihalene
NO
0.00100 1
05/02/201708:56
WG974640
4-Chloropheryl-phenylelher
NO
0.0100 1
05102/201708:56
WG974640
Chrysene
NO
0.00100 1
0510212017 OK56
WG974640
Dibenz(a.h)anthracene
NO,
0.00100 1
05102/201706:56
WG974640
3,3-Dichlorobenzidine
NO
0.0100 1
05102/2017 08:56
WG974640
2,4-Dinitrotoluene
ND
0.0100 1
05/02/2017 08:56
WG974640
2,6-1)initrotc}uene
ND
HIM 1
051021201708:56
WG974640
1,2-Dipheny[hydrazine
NO
0.0100 1
051021201708:56
WG974640
Flaaranthene
NO
0.00100 1
0510212017 08:56
kNG974640
Flucrene
ND
0.00100 1
05/02/2017 08:56
WG974640
ACCOUNT:
PROJECT:
SDG:
DATEITIME: PAGE:
TBL Laboratory
T13L-27616
L905120
05/02/17 11:57 6 of 21

OUTFALL #1 SAMPLE RESULTS - 01 ONE LAB.NATrONWiDE.
Collected dateltirne: 04124117 09:30 L905120
Semi V.olatOe organic Compounds (GC/MS) by Method 625
Analyte
Resuit
mgli
Qualifier RDL
Mgt!
Dilution Analysis
date 1 time
Batch
Hexachloroberzene
ND
0.06100
1 05/021201708:56
WG974640
Hexachloro-1,3-butadiene
ND
0.0100
1 05/0212017 08:56
WG974640
Hexachlorocydopentadiene
ND
0.0100
1 05/02/2017 08:56
WG974640
Hexachloroethane
NO
0.0100
1 0510212017 08:56
W6974640
Indeno(1,2,3-cdipyrene
ND
0.00100
1 05/02/201708:56
WG974640
Isophorone
ND
0.0100
1 0510212017 08:56
WG974640
Naphthalene
ND
0.00100
} 051D212017 08:56
WG974640
Nitrobenzene
ND
0.0100
1 05/021201708:56
WG914640
n-Nitrosodimethylamine
ND
0-0100
1 05/021201708:56
WG974640
n-Nitrosodiphenylamine
ND
0.0100
1 05102/2017 08:36
WG9)4640
n-Nitrosodi-n-propylamine
ND
0.0100
1 051021201708:55
WG974640
Phenanthrene
ND
0.00100
1 05/02/2017 08:56
WG974640
Benzylbutyl phthalate
ND
0,00300
1 0510212017 08:56
WG974640
Bis(2-ethylhexyl)phthal2te
ND
0.00300
1 05102/2017 08:56
WG974640
Di-n-butyl phthalate
ND
0.00300
1 05/02/2017 08:56
WG974640
Diethyl phthalate
ND
0.00300
1 05102/2017 08:56
WG974640
Dimethyl phthalate
ND
0.00300
1 05102/2017 08:56
WG974640
Di-n-octyl phthalate
ND
0.00300
1 05102/2017 08:56
WG974640
Pyrene
ND
0.DD100
1 05102/2017 09:56
WG974640
1,2,4-Tr'ichlorobenzene
ND
0-D100
1 051021201708:56
WG974640
4-Chloro-Intelhylphenol
NO
0.0100
1 05/02/2017 08:56
WG974640
2-Chlorophepol
ND
0.0100
1 05/02/2017 08:56
WG974640
2,4-Dichiorophenol
ND
0.0100
1 05/02/2017 08:56
WG974G40
2,4-Dimethylphenol
ND
0.0100
1 05102/2017 08:56
WG974640
4,6-Dinitro-2-methyiphenol
ND
0.0100
1 05102/2017 08.56
WG974640
2,4-Dinitro phenol
ND
0.0100
1 05/021201708:56
WG974640
2-Nitrophenol
ND
0.0100
1 05/02/201708-56
NIG974640
4-Nitrophenol
ND
0,0100
1 05/02/201708:56
WG974640
Pertachlorophenol
ND
0.0100
1 05/02/2017 08:56
WG974640
Phenol
NO
0.0100
1 05/02/2017 08:56
WG974640
2,4,6-Trichic rophenol ;
ND
0.0100
1 0510212017 08:56
WG974640
(S)2-Fltrorophenol
52..2
10.0-120
051021201708:56
WG974640
(S)Fhenol-d5
40,6
70.0-120
051021201708:56
WG974640
(S)Phtwbenzene-d5
83.5
Q.0-126
0510212017 08:56
WG974640
(S)2-Fluorobiphenyl
86,3
22.0-127
0510212017 08:56
WG974640
(S)2,4,6-Tr6ronrophenol
98.5
10.0-153
051021201708:56
WG974640
(5)p-Terphenyl-d14
92.1
29.0-741
051021201708.156
1dlG974640
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
TSL Laboratory . TBL-27616 L905120 05102/1711:57 7 of 21

WG974724 QUALITY CONTROL SUMMARY ONE LAB. NATIONW4C'.E
Wet Chemistry by Method 1664E L905120-01
Method Blank (MB)
)MB) R3214381-1 0408m 15:03 C?
Me Result ME Ouali6er MB MDL MB ROL
Analyte mgA mgA mgA
Oil & Grease )Flexane E=a) a 1.16 5.00
J5s
Laboratory Control Sample (LCS) . Laboratory Control Sample Duplicate (LCSD)
(LCS) R3214391-2 04128n715-.03 • (LCSD) R3214381-3 OW28W 15.04 a Cn
Spike Amount LCS Result LCSD Result LCS Rec, LCSD Rec. Rec. Limits LCS Oualifer LCSD Qualifier RPD RPD Limits
--
Anafyte mgA mg4 mgfl % % % % % $r
pi18Grease (Hexane Et[r) 40.0 � 37.3 38-6 93,3 96-5 J � 76.0-114 3.43 20
TGI
�5C
ACCOUNT: PROJECT: SDG', DATEfTXE: PAGE:
TEL 1-4bawory TBL-27616 L905120 051021T7 11,57 6 of 21

WG974433
QUALITY CONTROL SUMMARY
ONELaa �laT,oravleE.
Volatile Organic Compounds
(GC7MSl by Method 624
t9DS120-01
Method Sunk (MB)
(MB( R3214425-3 041270
17.36
�.I7
ME Respit
ME OLaliher M8 MDL
M8 RDL
ETC
Analyte
My
mgA
MqA
ACrolein
0
0,00887
0.0500
Acrylmntrile
u
0.00187
0.0100
;
SS
Benzene
U
0400331
0.00100
Bromcoichlorome:hane
U
0000380
0.00100
,
aromeorm
L
0000469
0.00100
CN
&omomeihane
U
0000866
0.00500
Carbon Iebachionde
U
0.000379
0.00100
asf
Chlorobenzene
U
0000348
0.00100
ChIcrodibwatomethane
u
0000327
0-00100
Chloroethane
U
0000453
0.00500
m9m
2-Chlaroethylwylether
U
000301
0.0500
Chloroform
U
0000324
0.00500
'GI
Chlnromethane
U
0000276
0.00250
1.2-Dichlorobenzene
U
0000349
0.00100
1,3-0lthlorotlenzene
L
000C220
0.00100
[A(
t4-Dichlorobemene
u
0.000274
0,00100
Dichlorodifluoromeinane
U
0,000551
0,00500
5c
1,1,Dichloroethane
U,
0,000259
0.00100
1,2-DICRloroethane
U
0.000361
000100
1,1-1ichloroethene
U
0000398
0.00100
bans-1.2-D¢hloroelhene
u
0.000396
0,00100
1,2-D+chlompropane
'U
0000306
0.00100
cis-1.3�0ichloropropene
U
0.000418
000100
tran5-1,10ichloroprWrie
U
�u
0.000419
0.00100
Ethylbenzenp
0000384
0.00100
Methylene Chloride
u
0.00100
0,00500
_
1,1,2,2-fehachlcroethane
U
0000130
0,00100
Teirachlaroethene
U
D,000372
000100
Toluene
U
a000412
000100
11,1-TuChloroeth,lno
U
0.000319
0.00100
1.1,2-Tnchiowelhane
U
0000383
000100
Trichloroethene
U
0.000398
000100
Tlichlorofluorame"ne
U
0.00120
0.00500
Vinyl chloride
U
0.000259
0.00100
jSJ Takwe-d8
101
80.0420
j5J Dra.,om00udome0we
700
16.0-123
15Jo.0.p-TraWralofuene
102
800-120
(5)4-Pzomo17uor0benzene
958
800-120
ACCOUNT: PROJECT: SDG: DATE/TIMB PAGE:
TEL Laboratory TSL-27b15 L905120 05102117 11.57 9 of 21

WG974433 QUALITY CONTROL SUMMARY ON,--- LAB PrAMNWDE.
volatile Organic Compounds (GC7M5) by Method 624 L905120-01
Laboratory Control Sample (LCS) • Labormory Control Sample Duplicate (LCSD)
(LCS) R3214425-1 04/27/1716�45 • ILC50) R3214425-2 04/27117 17:02
Spike Amount LCS Result LCSD Result
Analyze mgA mgA mi
LCS Rec.
%
LC$D Rec.
%
Rec. Limits
%
LCS Oualifier LCSD 17ualitfer RPD
%
RPD Limits
%
Acrolen
0.125
1,30
125
1040
998
10.0-I60
E v-1 E J° 4.02�
20
Acrylwitrile
0.125
0.112
0.112
89.8
69.6
60.0a42
0.160
20
Benzene
00250
1)A233
0,0231
934
92.3
69-0-123
IA
20
BromOCILCNoromethane
0.0250
0.0242
0.0240
96.7
95.8
76,0.120
0.920
20
Bromoform
0-0250
0.020$
0,0211
82.1
84,6
UAW
3,01
20
eromomelhane
0.0250
0.0149
0.0151
59.6
6D.2
18,0-160
0.960
20
Carbontetrachlorioe
0.0250
00212
0.0207
84.9
82.7
63.0-122
2.64
20
Chlorobenzene
0.0250
0.0222
0,023D
88.9
92.1
79.0-121
3,60
20
Chlorodibr"&Whane
0.0250
00209
0.0215
83.8
85.9
75-0-125
2.45
20
Chicroethane
00250
0.0212
0.0207
84.9
82-6
47,0.152
271
20
2-CUroethylwylether
0,125
0.0285
0-0275
22.2
22.0
10.0-160
3.50
22
Chloroform
0,0250
0.0249
0.0241
99,5
964
72.0-121
3.20
20
CnlnromeMane
00250
0.0307
00319
123
128
48.0-139
3.82
20
1.2-Dichloroberaene
0,0250
00234
0.0234
93-5
93.7
$00.120
0.210
i0
1,3-Dichloroben7ene
00250
0.0210
0.0218
84.0
872
72.0.123
3.73
70
14-D¢hloroberizene
0.0250
00228
0,0236
911
94.2
77.0.1,10
3.34
20
Dichlorotl:8uoromenane
0.0250
0.0271
0,0262
108
105
49.0.155
3.34
20
1,1-DicNcrochane
00250
0,0239
0,0237
95,4
94.8
70,0-126
0.640
20
1.2.Oichloroelhane
0.0250
0,0269
0.0262
108
lo5
67.0-126
2.61
20
1,1-Oichlomethene
0,0250
0.0242
0.0243
96.8
97.2
64,0-129
0.410
20
Trans-1.2.Orchloroethene
0.0250
00230
0,0227
971
90.9
71.0421
139
20
1,2-Dichloropropane
0,0250
0.0237
0,0241
94.9
96.4
75.0-125
157
20
05-13-Di[hloroproprme
00250
00224
0.0225
89 6
90.1
19 0-123
0.630
20
trans -l.3-Dichicroprapene
' 0.0250
0.0235
0.0225
94,0
89.9
74.0-127
4.39
20
Ethylbenrene
0.025o
0.0222
00225
88.9
B9.9
77.0-120
1.10
20
Methylene CRlwide -
0.0250
0.0229
0.0229
916
910
66.0-121
0.590
20
1,12,2-Tehachlpr0elhane
0.0250
C.C221
00217
884
86.9
71.0-122
1.73
20
Tetrachioroethene
00250
0.C234
0,0243
93.5
97.4
70.0.127
4.06
20
Toluene
00250
0.0239
D0238
95.6
95.4
77.0.120
0210
20
1.1,1-Trichloroethane -
0,0250
0.0250
D-0248
998
99.1
68,0-122
0,740
20
1.1,2-Trichloroethane
0.0250
0.0226
0.0224
91.0
89-5
780-120
1.63
20
Ttkhlornethene
0.0250
0.0243
00241
97.2
96.5
780-120
0.650
20
frichloronuoromethane
0,0250
00259
0.0254
103
102
550-137
1,74
20
Vinyl chloride
-0,0250
00239
0.0235
95.5
93.8
54.0-133
1,76
20 '
N 7p7ueem-d8
102
$02
900,120
r5/Dtbromofluorornernano
101
995
760,123
(s)G.a,o-Trrnuorololuene
702
of
80.0-120
(SJ4-8romu.?trwobenzene
94.2
96.6
80.0-00
ACCOUNT: PROJECT, $Or: OATEMME: PAGE:
TBL Laboratory TBL-27616 L905120 0510207 1157 ID of 21

WG974316
QUALITY CONTROL SUMMARY
ONE LAB NATIONWIDE
Pesticides (GC) by Method EPA 606
L905120-01 -
Method Blank (MB)
Cry
rMB) R3214757-3 05101117 1229
Me Result ME Qualifier
ME] MOL
M8 RDL
ETC
Analyte mgA
mgll
mg/1
Aldan U
0.90000813
0.0000500
Alpha BHC U
0.0000166
0.0000500
Sc
Beta BHC U
0.0000184
0.0000500
Delta SHC U
0.00%197
0.0000500
1
Gamma BHC U
0.0000176
0.0000500
Cr
a a-DDO U
0.0000170
0.00D0500
4,4-DDE U
0.0000154
0.0000500
`
4,4-DDT 9
C.0000177
D 0000500
Dielddn U
00000179
0.0000500
EndosulfanI U
00000179
00000500
EndoSulfan II U
0.0000176
0,0000500
Endosultan sulfate U
0,0000196
0,0000500
=
GI
Endnn U
0.0000189
0.0000500
Endnn aldenyde U
0,0000142
0.0000500
rAt
Endnn ketone U
0,0000110
0,0000500
Heptachlor U
0.0000108
O-G000500
Heptachldrepoxlde U
0-D000175
0.0000500
'SC
Hexachlumbenzene U
D.0000134
0-0000500
Melh0Kychlar U
0.0000193
0.0000500
Chlardane U
0.0000977
0.000500
Toxaphene U
0.000168
0.000500
(S) De(uGhlOrpbfpheny! 713
f0,0-44
is) Te[rv[lrloro m xy7ene 5-, 0
10.0435
Laboratory Control Sample (LCS) • L -,boratory Cantrot Sample Duplicate (LCSD
(LCS} R3214757-1 051007 1204 - (LCSD) R3214757-2 05101/17 12:16
Spike Amount
LCS Result
1.C50 Result
LCS Re[.
LCSA Rec.
Rec. Limits
LCS OuaBRet LCSD 001flef RPD
RPD Limits
Analyle
MV
mgfl
mgll
%
%
%
%
%
Aldrin
0.000200
0.000106
0.0001T2
53.2
560
35.0-126
5.12
24
Alpha BHC
0000200
0.000175
0.00001
87.7
853
55.0-133
2.69
20
Beta BHC
0.000200
0.000180
0.000177
90,2
88.5
59.0.131
1.87
20
00aBHC
DOW200
0.000167
0.000165
834
82.3
610.134
135
20
Gamma BHC
0.000200
0-000175
0.000172
87.6
86.1
$6,0-133
1-75
20
4,4LODD
0.000200
0.000209
0.000192
105
96,T
59-0-138
8.53
20
4,4.DDE
0.0p0200
0.000180
0.000167
89.9
83.7
58.0431
7.12
20
4.4-DDT
0.000200
00002CO
0.000191
100
953
13-0-147
4.38
20
Dieldrin
O.OW700
0.000203
0-000187
101
933
62.0.136
829
20
Endosulfa4l
C.000200
0.000197
0.000182
98,7
91.1
52,0-137
8.09
20
ACCOUNT: PROJECT: Soo DATEAIME: PAGE:
TEL Laboratory TOL-27616 LU05120 05/02/17 11..57 11 of 21

WG974316
QUALITY CONTROL SUMMARY
ONE LAS. NATIONWIDE
Pesticides 1GC) by Method EPA 609
L905120-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(1,CS) R3214757-1 057011171204 - (LCSD] R3214757-2
05/OV17 1216
Spike Amount
LCS Result
LCSD Result
LCS Rec. LCSD Rec.
Rec. Limits LCS Qualifier LCSD Ouakfier
RPD
RPD Limits
Analyle mgA
mgA
mgA
%
%
%
%
%
Endosullan II 0.000200
0.000204
0.000188
102
93.8
62.0-136
8.49
20
Enoflsullan sueate 0.000200
0.000205
0.000191
102
95,5
60.0-139
7.11
20
'
Ss
Endon 00002GO
0.000195
D_0001a8
97.4
94.1
58.0-135
3AI
10
.Endrinaldehyde 0.000200
0.000196
0.000186
97.9
93-0
56.0-126
519
20
Endnn ketone 0000200
0.000228
0000208
114
104
54.0-142
9.16
20
CN
Heptachlor 0,000200
0.000119
0.000130
594
652
37.0-134
918
24
Heptachlor epoxide 0,0002DO
0.000187
C.000176
93.4
Sol
60,0-132
5.83
20
FrHLxachlorobenzene
0.000200
0-000127
0.000131
63,6
65A
35-C-120
2.78
25
Methoxychlor 0.000200
0,000244
0.000222
122
ill
44.0-160
9.49
22
(5)DecGchi0rcbrphanyf 100 94.0 700445
(51 Teuochbro-m +ylene 50.3 $4 2 21.1-148
ACCOUNT: PROJECT: SDG: DATElTIMLt GAGE:
T6L Laboratory 7BL-27616 L905120 D5/02n71L57 11 of 21

WG974316
Polychlorinated Biphenyls
(GC) by
Method EPA-6C8
Method Blank (MB)
(MS) R3214768-1 041291714t17
M8 Result
ME Qualifier ME MUL
Analyle
mgA
mgA
PC81260
0.000125
1 0.0000146
PCB lots
U
0-0000198
PC81221
U
0.0000244
PC61232
U
0.0000213
PCB 1242
U
O.D000242
PC81248
U
0.0000135
PCB 1254
U
0.0000181
j$f VKQCh10r0b+phenyr
107
(5lletrachroram-ry4ene
6V
QUALITY CONTROL SUMMARY
ME ROL
mgp
0.000500
0.000500
0000500
0.000500
OQ%500
0000500
OM13500
10.a-114
10.0-135
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(1-CS) R3214768-2 04/29/17 14:30 • (LCSDj R3214768-3 04/2911714 a2
Spike Amount
LCS Result
LC5D Resull
LCS Rec.
LCSD Rec.
Rec. Limns
Analyte
mgll
mgq
mgR
%
% _
%
_
PCB1260
0.0005W
0000500
0-000495
100
98.9
45.0-142
PCB 1016
0.000500
0.000412
0.000443
82.4
68.7
41.0-134
(SJ OecochloroDlphenyl
106
100
10.0-1a5
(sJ red0chlor0-m-xyrene
566
62.6
211-148
iCSQualifier LCSD Qualifier RPD RPDUmits
1.11 _ 24
7,28 23
ONE LAB, NATIONWIDE. jo
ACCOUNT: PROJECT: SDG: OATUTIME: PAGE:
TEL Laboraay TBL-27616 L905120 D5f0211711.57 13 o121

WG974640
QUALITY CONTROL SUMMARY
ONELAB.NATiDNVJICIE.
Semi Volatile Organic Compoondy
(GCIMS) by Method 525
L905120.01
Method Blank JMB)
(MB) R3214878-3 05101M717.14
MB ReSult
MB Ouali6er MB MDL
MB ROL
Anayte m911
mgA
Y
MO
CC
Acenaphthene U
0000316
0.00100
Acenanhthylene u
0.000309
0,00100
'
Ss
Anthracene u
0.000291
0,00100
Azghenzehe u
0000164
0.0100
_
aCn
Benzidine u
0.00210
0.0100
Senzo(a)antnracene u
0.000111
0.00100
Benzo(b)iluoranthehe u
0.0000896
0100100
'5r
Benzo(klflucranthene U
0.000265
0.00100
Benxjg.N)perylene U
0,000161
000100
8enzo(aWene U
0.000269
0.00100
StW-chlorezhg"elhane U
0.000214
0.0100
Bis(2-Chlaroei1hyl)ewer u
0.000214
0,0100
'G{
Bis(2-chloroisopmpyllethpr u
0.000308
0,0100
4-13romophenyl-phenylether u
0.000180
00100
�7y1
2-Chloronaphthalene U
0000204
0.00100
4-Chloropheryl-phenyletner u
0.000170
0 MOO
Chrysene u
0.000t33
0.00100
�SC
Dibenz(ahlanthiacene u
0900251
0.00100
3,3 Oichlolobenzidine u
0.00169
0.0100
2,4-Oiniuotoluene 0 _
0.000219
0.0100
2 b-DiniUololvene u
0.00143
0.0100
Fluoranthene u
0.000342
0.00100
_
Fiuooene u
0000177
0.00100
Hexachlorobenzene u
0.000221
0-00100
Haxachloro-13-buladiene u
0.00264
0.0100
HexaChlorgryCloperladiene iJ
0,00180
0.0100
Hexacnlorumare 0
0,00313
0,0100
IndenopUA-cd)pyrene u
0,000333
0.00100
Isophorone a
0,000238
0.0100
Naphthalene a
0,000413
0,00100
Nitrobenzene 1
0,000200
0,0100
n-Nibosodlmethylamme 0
000255
0.0100
n Nilrosodiphenylamine a
0000137
0.0100
n4trosodi-n-prcpylarnme ll
0000311
0.0100
pheranthrene u
00002D5
0.00100
Benrylbutyl phthalate u
0000395
0.00300
9is(2-ethylhexAphthalate u
0000496
0.00300
DFn-0tityl phthalate u
0.000275
0.00300
Diethyl phthalate U
0.000356
0.00300
Dimethyl phthalate u
0.000338
0.00300
ACCOUNT:
PROJECT: SDG:
DATE(TIME: PAGE:
74 Laboratory
T9L27616 L905120
05/021171057 14 at 2l

WG974640
Semi Volatile Orghnic
Method Blark (MB)
Compounds
(GClMS) by Method 625
QUALITY CONTROL SUMMARY
1905120-01
ONE LAD. NATIONWIDE.
C
(MB) R3214878-3 05JOV1717:14
u
M8 Result
MB Oua4ner MB MOL
MB RDL
Anayte
mgA
mgA
mgll
Di-n-octylphthalate
U
0.060277
004300
Pyrene
D
0.000295
O.00IDO
J
Ss
1,2,4-Trichlorobpnzene
U
D_oOD355
0.0100
4-Chlora-3-metnyiphenol
U
0.000229
0.0100
c
2-Chlorophenol
U
0.000190
0.0100
Cn
2,4-DWhiorophenol
U
0.000972
0.0i00
2,4-Dimethylpherd
U
0,00134
0.0100
'S1
4.6-Dlnitro-2-melhylphenol
U
000260
0,0100
2,4-0init(ophenol
U
0.00230
00100
2-Nilropnenol
U
0,000279
0.0100
Mora
4,Nitrophen6
1t
0,00273
00100
PenLKNOTopnenol
U
0,000407
0.0100
'Gl
Phenol
U
0,00113
90100
24,6-Trichioroph0nal
U
0.000278
0.0100
-<;I
Pmrtrobenzene-d5
79.6
r0.0-126
(S) 2-Pluoroblpnenyl
80.1
22.0417
(SJp-Terpheny4-d14
95.8
29.0-141
FC
(51Phenol-05
29.0
10.0.7X
(5)2-R"Ophenal
56.0
10.0.120
p2.4,6-rnbromophenol
85.9
r0.0-153
Lobc,mtory Control Sample (€.CS) - Laboraicry Central Sample Duplicate (LCSD)
(LCS) R3214878-1 0510V17 16:27 • (LCSD7 93214878-2 05I0v17 16:51
Spike Amount
LC5 ReSDlt
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Anayte
mgA
mgn
mgA
%
%
%
Acenaphthpne
0,0200
0.0169
0.0174
84.4
87,1
42.0.120
Acenaph:hylene
0.0200
0.0187
00189
53.3
94.5
43.0-120
Anthracene
0.0200
0.0203
0.0196
101
98.1
4CO.120
Azobenzere
0.0200
0.0191
0,0190
95.3
95.2
37.0-125
Benzoine
0.0200
0.0214
0-0217
107
109
1,00-120
Benzo(a)anthracene
0.4200
0-C205
0.0198
103
48-8
44.0-12C
Benzo(b(Itucranthene
0.0200
0.0192
0.0188
96,0
93.9
40,0-120
Benzo(k)auotanthene
0.0200
00199
0.0189
99.3
94.6
410-120
9enz9(gh,1perylere
0.0200
0.0195
0.0189
9?4
94.4
45.0-121
Benzo(a)pyrene
0.0200
0,0196
0.0187
98.1
93.6
410-120
Bisr2-ch1orelhmrylmethane
00200
0.01"
a11151
77.5
75.4
360-120
Bisi2chloioeth*ther
0.0290
90174
0.0163
869
81.5
24,0-120
B5(2-chloroisopropyl)ether
0.0200
0.0168
0.0162
84.1
B1.0
32.0-120
ACCOUNT:
PROJECT:
78L Laborawy
1 BL-27616
tCS Qualifier JCSD Qualifier RPD
RPO Limits
3.06
22
133
22
3,15
20
0170
20
1.54
36
3.23
20
2,21
21
4,90
22
3.17
20
4.61
20
2.84
25
6.35
29
3.67
29
SDG: OATE7TIME:
L905120 051021171157
PAGE:
15 of 21

WG974640 QUALITY CONTROL SUMMARY oriELAB. NAIJONWIDE.
Semi Volatile Organic Compounds (GCIM5) by Method 625 005120-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3214878-1 05/01/17 1627 - (LCS01 R3214878-2 0510V17 16-51
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LC5D 0uahfier RPD
RPD Limits
Arialyte
my
mgA
mgll
%
%
%
%
4-Bromopherlyl-phenyVelher
00200
0.01841 ».�
0,0181T
92.2
90.6 --
42.4121
_ �T,.. 1.71W�
2-Chloronaphthalene
0.0200
00157
0,0160
78.3
79.9
37.0120
2.02
24
4-Chlorophenyl-phenylether
00200
0.0181
0.0186
90.6
93,0
44.0-12C
7.66
21
Chrysene
0.0200
0.0208
0.0200
104
]DO
45,0-120
3.84
20
0ibenz(a h(anthracene
00200
0,0193
0.0186
964
93,1
44.0-121
344
21
3.3-Olchlombenzidine
6D200
0-0304
0.0300
152
150
29.0-153
107
23
2.4-Dnirotoluene
0,0200
0.0221
0.0222
ll1
Ill
47,0127
0.340
21
2,6-0rmtroloiuene
0,0200
0.0212
0.0211
106
105
42.0-120
0.660
22
Fitioranthene
0-0200
0,0220
0.0210
110
105
46-0-171
4.96
20
Fludrene
0,0200
0.0188
0.0187
940
93.5
45.0-120
0.480
21
Hexachlorobeozene
0-0200
00190
0.0180
949
90.2
410-124
502
21
Hexachloro-1,3-butadiene
0.0200
0.00996
0.0705
49.8
52.6
26.0-120
5.49
31
Hexachlorocyclopentadlene
0.0200
0-0122
0.0126
60.8
63.0
100-120
3,63
31
Herachloroethane
0.0200
0,0113
0.0114
56.5
57,1
22,0-120
0.950
34
Indenap,2.3-cd)0yrene
0,0200
0-0200
0.0193
99-8
964
45-0-123
350
21
Isdpnorone
0.0200
0.0163
0.0160
81.7
80,2
37.0-120
1.86
24
Naphthalene
0.0200
00117
0.0118
$85
59.1
33.0-120
1,01
28
Nitrobenzene
0 D200
0.0147
0.0142
73,6
710
31.0-120
3.49
28
n-Mtrasolimethylamine
0.9200
0,00975
000909
48.B
45.4
10,0-120
7.05
34
mNurosodiphenylamine
00200
00197
0.0191
984
95,6
44.0-120
2.94
21
11-N410sodi-n-pro_pylamine
0.0200
0.0194
0.0124
96,9
92.0
29.0-120
5.23
27
Phenanthiene
0.0200
00199
0.0181
94.4
907
42.0-120
394
20
Benzylbulylphthalale
00200
0.0201
0.0193
101
96.5
36.0.121
4.19
22
Bis(2-ethylhexyllphthalate
0.0200
0,0198
0-GIBB
98.8
53.9
37.0-121
5.04
21
D.-n-hutylphthalate
00200
0,0222
0.0217
Ill
108
43-0-122
2.47
21
Diethyl phthalate
0.0200
0.0212
0.0211
106
106
48.D-123
0.360
20
DimemylPnthnlale
0,0200
0-0211
00206
105
103
47.0-120
2,15
20
Di-n-octyl phthalate
00200
0 C213
0.0205
107
102
38.0-120
4.30
22
Pyrene
0.0200
0.0185
00131
92.7
90,7
43.0-120
2,09
21
1,2.4-fricN0mbenzene
0,0200
0-0105
0.0111
53.1
55.3
29,0-120
4,15
29
4-Chloro-3-snelhylphenol
0,0200
00151
0,0155
80.4
77.3
39.0-120
4.04
22
2-Chlarophenol
0,0200
0.0170
0,0157
84.8
787
28.0-120
7.43
19
2,4-Oichlorophenol
0,0200
0.0155
0.0150
77,6
74.9
37.0.120
3.54
26
2,4-Difnethylphenol
0.0200
0.0156
l)_DW9
78,1
746
350-120
4.54
25
4,6-Dinitmo2�methylphenol
00200
0.0213
0.0210
107
105
34.0-125
1.51
27
2,4-0initrophenoi
0.0200
0.0152
0.0148
76.2
742
100120
2.59
40
2-Nmophenol
00200
0,0166
0.0161
83.2
80.3
350.120
3.57
28
4-Narophenel
0.0200
0.00936
000967
46.8
484
10.0-120
3.32
35
Penlacheraphenol
D.0200
0.0192
D.0190
96-1
95.1
20.0-125
0.930
32
Phenol
00200
0.009C8
0.00235
45.4
41,7
10.0-120
9.45
34
-
ACCOUNT:
PROJECT:
SDG-
DATEITIME:
TBL
Laboratory
T9L-27616
L905120
05102R7 11:57
PAGE,
16 nt 21

WG974640 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. �
Semi Volatile Orgaalc Compounds (GC/MS) by Merhad 625 r905120-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3214878-; 0570V57 16:27 • (LCSD) R321487B-2 05/01/17 16:51 Cp
Spike Amount LCS Result LCSD ResuA LCS Rec. LCSD Rec, Rec. Limits LCS Qualifier LCSD Oual&ier RAD RPD Limits
AnaMe mgll mg4 mgA % % % % %
2,4,6-Tnchlorophenol _ 0.0200 0.0199 00195 994 97.4 40.0-122 2.10 24
(SJNilropenrerkd5
69.8
679
TO OA26
l
SS
(5) 2-F1uoroWpneny4
87.5
871
11.0-T17
(5)p-TerphenyldW
99.5
94.4
190447
rCn
(5)PhenoT-d5
42.3
39.8
TO.0-110
(S)2-Fluorophend
59.8
55.8
100-110
6)2,4.5-TrRyomop onol
T00
971
TO0-153
I C,
ACCOUNT: PROJECT: SDG: DATETTIMS: PAGE:
TBL Laboratory TBL-27616 L905120 05/02/17 11:57 17 of 21

GLOSSARY OF TERMS
ONE LAB. NAPONWIDE.
Abbreviations and Definitions
SDG
Sample Delivery Group.
�p
MDL
Method Detection Limit.
El
RDL
Reported Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
3 SS
U
Not detected at the Reporting Limit (or MDL where applicable).
�Cn
RPD
Relative Percent Difference.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
SSr
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
`Qc
Rec.
Recovery,
Oualifier
Description
�Af
E
The analyte concentration exceeds the upper limit of the calibration range of the instrument
J
established by the initial calibration {ICAQ.
The identification is the is
rs Cl
of the analyte acceptable; reported value an estimate.
A
The associated batch QC was outside the established quality control range for accuracy.
ACCOUNT:
PROJECT: SDG: DATEITIME:
PAGE:
TBL Laboratory
TBL-27616 L905120 05102/1711:57
18 of 21

ACCREDITATIONS & LOCATIONS ONE LAB, NATIONWIDE.
ESC Lab Sciences Is the only environmental laboratory accredaedlcert lied to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other
lab Is as accessible or prepared to handle your needs Throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network' laboratories in our industry. The most significant
benefit to our 'one location"
design is the design of our laboratory campus. The model is conducive to accelerated productivity,
decreasing turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
' Not all certifications held by the laboratory are applicable to the results reported In the
attached report,
State Accreditations
Tc
Alabama
40660
Nevada
TN-03-2002-34
3
Alaska
UST-080
New Hampshire
2975
SS
Arizona
AZO612
New Jersey—NELAP
TN002
Arkansas
88-0469
New Mexico
TNO0003
FC
California
01157CA
New York
11742
Colorado
TNO0003
North Carolina
Env375
Conneticut—
PH-0197
North Carolina
DW21704
'SI.
Florida
E87487
North Carolina'
41
Georgia
NELAP
North Dakota
R-140
'
Georgia'
923
Ohio—VAP
CLC069
QC
Idaho
TNO0003
Oklahoma
9915
Illinois
200008
Oregon
TN200002
Indiana
C-TN-01
Pennsylvania
68-02979
Gi
Iowa
364
Rhode Island
221 —
Kansas
E-10277
South Carolina
84004
Kentucky'
90010
South Dakota
nla
Kentucky'
15
Tennessee"
2006
Louislana
A130792
Texas
T 1047042.45-01-TX _
q
Maine
TN0002
Texas s
LA80152
SC
Maryland
324
Utah
6157585858
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
109
Minnesota
047-999-395
Washington
C1915
Mississippi
TNO0003
West Virginia
233 -
Missouri
340
Wisconsin
99809399.10
Montana
CERT0086
Wyoming
A2LA
Nebraska
NE-OS-15-05
Third Party & Federal Accrecl�tations
A21LA-1SO17025 1461,01
AIHA-LAP,LLC 100789
A21LA — ISO 17025s 1461.02
DOD 1461.01
Canada 1461,01
USDA S-67674
EPA—Crypto TNO0003
Orinkiag Water : Underground Storage Tanks
' Aquatic Toxicity ' ChemicallMlcf0biological s. Mold " Accreditation not applicable
Our Locations
ESC Lab Silences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies- If you would like assislance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our Central laboratory.
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KS MO • VA?
LCl'
AR
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l
ACCOUNT:
TBL Laboratory
PROJECT:
SDG:
DATEITIME:
PAGE:
TBL-27616
L905120
05/02/17 11:57
19 of 21

T B L Environmental
Laboratory , Inc.
2401 W. 5th St
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LUmberton, NC 28358
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Date.
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—±:g, .. '€. ter..
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ficnt: T81LAd Sor. q /
Couler Received/Opened On: 4/26117 Te-wperature:
Received Eta•: jo:+ I?c}suarci
Signature:' l�i7.cr
Receipt Check 1.I51 NP
Yes
No
COC Seal Present / Intact?
COC Signed / accurate?
l
Bottles arrive intact?
Correct bottles used?
f
Sufficient volume sent?
If Applicable
VOA Zero headspace?
Preservation+Corretl / Checked? -

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03 0 0 0 0
FACILITY NAME Coo Go y
COUNTYC_.nLJyM1nJ-,
PERSON COLLECTING SAMPLES Ve.iTOn! T rA�S
LABORATORY 'T3 L Lab Cert. # a y23
Comments on sample collection or analysis: RECEIVED
LJEC 2 9 2016
��nIr
Part A: Stormwater Benchmarks and'Monitor��Jt &ILES
SECTION
MPLE COLLECTION YEAR
C (�t� `SCAMP PERIOD ❑ Jan -June ❑July -Dec
3 b 7 5" - or ❑ Monthly'
month
DIS HARGING TO CLASS ❑ORW ❑HQW []Trout❑PNA
RECEIVED ❑Zero -flow ❑Water Supply ❑SA
❑Other
DEC 2 9 2016 `
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
CENTRAL FILES
DWR SECTION
❑ No discharge this period?z
t' : •.:ta. E ;
Outfall No.
•,rit-• i �.. . .,
, , .,':.
17ate Sample"
1
Collected
b (mo/dd/,Yr)`�
24=h'our rainfall`
amount,
..SF 1rinChe53'-F�
+ •, •^� w':t°�-
,.
Total Suspended Solids-
,..,,4'SS..t. �,.,`� �.
pH,` - ' _
Standard units
:' ..
Capper
` .,
s�.ji�� . _•;
�,
Lead
5.� a 'I .3
' k,!'
Zinc
Non -Polar 0&G/
Total Petroleum
H drocarbons
t Ys. ,1a,
Total Toxic
Organics5
Benchmarks =__>
_
-
100 mg/ L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
1' mg/L
1 r
.aS
LL(al
.sr Su
o.o O
40.ao
,I 3y&5&
4.7 j,,a
fV6
1 Monthly. sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the.definition found in.40 CFR 469.31).
Permit Datd/1/2012-10/31/2017 SWU-245, last revised 5/2012
0 Page 1 of 3

Facilities �ncor orate a. solvent management Ian into the stormwater PoA..�on Prevention Plan may so certify, and the requirement forTTOQnitorin
� ... �tt.�' P g p Y Y, q .. g
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name ({-Print name)
14 TZ_%1-),o Ii
Title (Print title)
/a- go- 3a6
(Signature) (Date)
Note: Results must be reported in -numerical -format. -'Do not.report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, theymust be reported in the format "<XX m L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in -excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area•Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?Z
Outfall No.
ateSample•°' '24-hour
1
•Collected,
(mo/.dd/yr) _ ,..
rainfall
amount,
_ _Inches—_._
Non -polar O&G/TPH by,
EPA 1664 (SGT-HEM)
(Total Suspended. Solids.
br Y : ,pH, f. «
Benchmarks =_=>+
-
-
15 mg/L-
100 mg/L or 50 mg/L*
6.0 —.9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO [✓r
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Moil on_original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQCentral Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are sFant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
l/,)- aD ao/�
(Date)
Permit Date~•1/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
(�✓1 0 Page 3 of 3

m ritai �(,,:
TBL Ei—Mron a :r
AnalYslafConhl,�dPreia�vallva
,^
{. Laboratory ;..Inc.
2401 W. 5th St
' Lurnbeton; NC 28358
738-61
(910)
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C:odlcr.•Iteceived/OpcncJ On: t t/ ! h6 Tempermurc Uymn
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Receipt: 7
Reecivcd 13y: ju eph Roberts
Signature:
Receipt Check List
Yes No N/A
Were custody sea lson outside of cooler aid intact?
Were custody papers properlyflled:out?`
Ditl ail bottles arrive in good condition?
Were correct bottles used for the analyses.requested?
/
Was sufficient amount of sample sentin each bottle?
Were all apollcable sample containers coireetly preserved and
checked for preservation? {Any riot in_accepted,range noted on COC},
`
t/ .
if applicable,,was an observable VO.A headspace present?
'iVon Conformance Generated. {if yes see'attached NCF}

elementOne
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Sample #
Sample Matrix
Date Sampled 11/1412016
Delivered by Courier
Element One Inc.
6319-D Carolina Beach Rd.
Wilmington, INC 28412
Phone: [phone]
Fax: [phone]
[e-mail]
FINAL REPORT OF ANALYSES
November 28, 2016
Client Project Name Council Too]
Client Project Number TBL-27423
PO Number
E1 Project Number e28546
Sample ID
Outfall # 1
Sample Type
Grab
Time Sampled
1430
Sampler
V. Jacobs
E1 Sample #
28546
Date Received 11/1612016
Time Received 1355
Received by LLB
Parameter
Result
Unit
Dilution
DL
Method
Date
Copper
0.010
mg/L
1
0.003
EPA 200.8
11/17/2016
Zinc
0.138
mg/L
1
0.005.
EPA 200.8
11/17/2016
Lead
< 0.003
mg1L
1
0.003
EPA 200.8
11/17/2016
Total Suspended Solids
4.67
mg/L
1
2.5
SM2540D
11/16/2016
pH
6.51
SU
SM 4600 H B
11/16/2016
C
Ken Smi h, Laboratory Director
TBL-27423 Report Compiled by W�
NC Certifications: DW 37788 and DWQ DENR 604

TBL Environmental Billinginiormatlan;
Laboratory , Inc.
2401 W. 5th St
Lumberton, NC 28358 a,>4 U:
(91 {'�V) 138-6190 maHta.
AnalyalslConlaln©rlP reservalive
Urojecl \ ��' itylSala
Desorlptlon: .:1 p otZcotod
Phone: Cl lent Project M ESC Key;
FAX: 1-T G [. 2Da3 1 s
Called adby; `- SitelFac€ilty109: P.OA Ss�
-
Collactert by (aignhlure): Rush? ( Lab MUST Be NoUned) Me Results Not deli � � CoCode pab use only)
Same )ay ....... 20 q
Nexi Cey........ ioo°/a EM8117 Na Yes p' TemplololPrelogln
Two D ay .........So°/c of
inli:�cdln o u , FAX? —NO—Yea Skipped Via'.
C 1111a
Semple ID Compff3rab hatrlx` Oepih Date Time k RemarkalConlaminant Samplo 0(lab only)
tl��.11 1 G- j j-jq-1 r q3 o
Mw&Akr
"Matrix SS - SoIVSoild OW- Grotnidwater WW - We ateWater DW - Drfnldng Water OT - Othe
Time: {�OSOVd.lryr. iptuTo)
I a..30
'+
Tlmn:
°
Received : (Signal
12:4
�, ,..... .
r�
•coff Temp
)7 �
arnlr es ralrrrna v tt: CI UPS Condition: (lob use only)
❑FedFx 0Cduder d
Tamp; Miles R©oelved:
)e CoC Seals lntacl: ,____ Y _,_-N —NA
Dale: Tlrne
pH hacked: NCF:
�, ,(A+ -A

T B L Environmental Billing information:
Laboratory , Inc.
2401 W. 5th St
Lumberton, NC 28358 epo o:
[phone] mall to:
Project 1 ity/3ete
Description: CQ�.+.C.� 1 O 1 atlxted
Phone: Client Project #: ESC Key:
FAX: r l - 1'a3
Collected by: 5 Site/Facility ID#: P.0.#:
Collected by (slgnolure): Rush? ( Leb MIDST Be Notified Date Results Needed:
Same Q7ay....... 200% No.
Next Day........ 100% Emall7 —No Yes
�y TWO D;iy .........50% .." hi- V... °t
AnatysWContalner/Preservative
CoCode (leb'use only)
1
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if r@Ti.[Y7II1C!=!I� •a�d
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'Matrix. SS - SoIVSolid GW-Groundwater VVVV- WfiteWater DVV- DrinkingWater OT - Other PH Temp
Remarks; ^ llow Other
of I khed b . (S n a t u }
Jk
Relinquish Y. 51g aEut
ti p, rx,
Date:
Time:
Rem nature)
Received b SI nature �;5-41
Y' ( g �rf
Samples returns v w ❑ UPS
❑ FedEx ❑ Laurier ❑
Condition; (lab use only)
CoC Seals lalact: Y N NA
1 Date:
Time:
Temp:
Bottles Received:
`�{
_____
Relinquished by: {$ gnq(urd) ..�
4
Date:
i
Time:
Received for tab by: (Slgnaturp)'
I
Date:
Time:
pH Checked:
NCF: