NCG030459_COMPLETE FILE - HISTORICAL_20161229

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STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO. /v 7 9
DOC TYPE 0 HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE ❑ 301.ip J a � g
YYYYMMDD

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ANALYTICAL REPORT
EEC T yESC
L-A-B S-C-I-E.N•C•E-5 November 25, 2016
TBL Laboratory
b-3 c)et�j
CC,
Sample Delivery Group:
L.873129
Samples Received:
11/16/2016
Project Number:
TBL-27423
Description:
Council Tool
RECEIVED
Report To:
Pam Hester
DEC 2 8 2016
P.O. Box 589
Lumberton, NC 28359
CENTRAL FILES
DWR SECTION
Entire Report Reviewed By:
Jason Romer
Technical Service Representative
Results relate only to the Items Icsted or calibrated and are reported ,as rounded values. ThIS test report shall not be -
reproduced, except in full, without written approval of Me laboratory. Where applicable, sampling conducted by ESC is. ',
Performed per guidance provided in laboratory stgridard operating procedures- 060302, 060303, and 060304, t&'
r -

TABLE OF CONTENTS ONE LAB. NATIONWIDE.
'Cp: Cover Page 1 E
2Tc: Table of Contents
2
3Ss: Sample Summary
3
4Cn: Case Narrative
4
3S5
5Sr: Sample Results
5
,
Cn
OUTFALL #1 L873129-01
5
SQc: Quality Control Summary
8
'S
Wet Chemistry by Method 16648
8
Volatile Organic Compounds (GCIMS) by Method 624
9
FO cl
Pesticides (GC) by Method EPA 608
11
,
G1
Polychlorinated Biphenyls (GC) by Method EPA-608
13
SelTni Volatile Organic Compounds (GC/MS) by Method 625
14
Al
7G1: Glossary of Terms
18
Accreditations & Locations
19
RC8AL•
9Sc: Chain of Custody
20
ACCOUNT: PROJECT: SDG:
DATEMME:
PAGE:
TBL Laboratory TBL-27423 L873129
11/2511609,07
2 or21

SAMPLE
SUMMARY
ONE LAB. NATIONWIDE.
Collected by
Collected dateltirrae
Received dateltime
'OUTFALL #1 •L873129-01 WW
VJ
11/1411614:30
W16I1609:00
C p
Method
Batch
Dilution Preparation
Analysis
Analyst
dateltime
dale/time
FC
Pesticides (GC) by Method EPA 608
WG927375
1 11/21/16 07:23
11/2211612:52
LKD
Polychlorinaled Biphenyls (GC) by Method EPA-608
WG927375
1 11/21/16 07:23
1112211612:23
JNS
Semi Volatile Organic Compounds (GC1MS) by Method 625
WG927374
1 11121/16 06:34
11123/1615:22
JF
Volatile Organic Compounds (GUMS) by Method 624
WG926511
1 11117116 21:46
11/17/16 21:46
JHH
Wet Chemistry by Method 1664B
WG927851
1 11/18/16 07:54
11/1811613:16
SHG
Cn
Sr
FQ
�GI
EAI
9
SC
ACCOUNT: PROJECT: SDG:
TBL Laboratory TBL-27423 L873129
DATEITIME:
11/25/16 09:07
PAGE:
3ot21

CASE NARRATIVE ONE LAB. NATIONWIDE.
MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the
'
FP1All
dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria
except where addressed in this case narrative, a non-conformance form or properly qualified within the
F
sample results. By my digital signature below, I affirm to the best of my knowledge, ali
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
35s
❑
would affect the quality of the data.
Sr
ro
F
Jason Romer
V
Technical Service Representative
41
BSc
Sample Handling and Receiving
The analysis for 2-Chloroethyl Vinyl Ether was conducted from a chemically preserved container.
ESC Sample ID Project Sample ID Method
L873129-01 OUTFALL #1 624
ACCOUNT: PROJECT: - SSG: DATE/TIME:
PAGE:
TBL Laboralory TBL-27423 L873129 11/25/16 09:67
4 or 21

OUTFALL #1
SAMPLE
RESULTS - 01
ONE LAB.NATIONMDE. V
,Collecte4'dateltime:
11114116 14:30
1-873129
Wet Ch'emistry by Method 1664E
,
Result
Oualifier RDL
Dilution
Analysis
Batch
Cp
Analyte
mgll
mgll
date 1 time
Oil & Grease {Hexane Exirl
NO
4.76
1
111181201613:16
WG927851
TC
Volatile Organic
Compounds (GUMS)
by Method 624
3
Ss
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte
mgll
mgll
date 1 time
FC
Acrolein
NO
J4 0.0500
1
11/17/2016 21:46
WG926511
Acrylonitrile
NO
0.0100
1
11/1712016 21:46
WG926511
Benzene
NO
0.00100
1
11117/201621:46
WG926511
Biomodichloromethane
NO
0.00100
1
11/171k16 21:46
WG926511
Sromoform
NO
0.00100
1
11/17/2016 21:46
WG926511
s
Bromomethane
ND
0.00500
1
11/17/2016 21:46
WG926511
Carbon tetrachloride
ND
0.00100
1
11/17/2016 21:46
WG926511
7
Chlorobenzene
ND
0.00100
1
11/17/2016 21:46
WG926511
GI
Chlorodibromomethane
ND
0,00100
1
1111712 016 21:46
WG926511
Chloroethane ._
ND
0.00500
1
11117/2016 21:46
W0926511
FA I
2-Chloroethyl vinyl ether
ND
0.0500
1
1111712016 21:46
WG926511
Chloroform
ND
0.00500
1
11/17/2016 21:46
WG926511
9
Chtoromelhane
NO
0.00250
1
1111712016 21:46
WG926511
SC
.1,2-Dichlorobenzene
ND
0.00100
1
1111712016 21:46
WG926511
1,3.Oichicrcbenzene
ND
0.00100
1
1111712016 21:46
WG926511
1,4-Dichlorobenzene
NO
0.00100 1
11/17/2016 21A6
WG926511
DicWorodiiluoromethane
NO
0.00500 1
11/17/2016 21:46
WG925511
11-Dichloroethane
ND
0.00100 1
111t712016 21:46
WG926511
1,2•Dichloroethane
NO J4
0.00100 1
1111712016 21:46
WG926511
1,1-Dichloroethene
NO
0.00100 1
11/1712016 21:46
WG926511
trans-1,2-DiOloroethene
ND
0.00100 1
11/17/2016 21:46
WG926511
1,2-Dichloroprepane
NO
0.00100 1
11/17/2016 21:46
WG926511
cis-13-Dichloropropene
ND
0.00100 1
111171201521:46
WG926511
trans-1,3 Dichtoropropene
ND
0.00100 1
1111712016 21:46
WG926511 '
Ethylbenzene
NO
0.00100 1
11/17/2016 21:46
WG926511
Melhylene'Chloride
NO
0.00500 1
11/17/2016 21 A6
WG926511
1,1,2,2-Tetrachloroethane
ND
0.00100 1
111171201621:46
WG926511
Tetra chlor_oethene
NO
0.00100 1
11117/2016 21:46
WG926511
Toluene
NO
0.00500 1
1IM712016 21:46
WG926511
1,1,1-Trichloroethane
NO
0.00100 1
11/1712016 21:46
WG926511
1,1,2-Trichloroethane
ND
0.00100 1
11117/2016 21:46
WG926511
Trichloroothene
ND
0.00100 1
111171201621:46
WG926511
Trichloroflucrcmethane
NO
0.00500 1
11/17/2016 21A6
WG926511
Vinyl chloride
ND'
0.00100 1
11/17/2016 21:46
WG926511
(5) Toluene-d8
109
90.0-175
1111712016 21.46
WG926511
(S)Dibromofluoromethune
99.5
79LO.121
111171201621.46
WG926511
(5)o,o,o-TriRuorotofuene
104
90.4-If6
1111712016 21:46
WG92.6511
(S)4-BromoRuorobenzene
103
80.7-120
7111712G1621:46
WG926511
Pesticides (GC) by Method
EPA 608
Result Qualifier RDL Dilution Analysis Batch
Analyte mgll mgll date! time
Aldrin
NO
Alpha BHC
NO
Beta BHC
NO
Delta BHC
ND
Gamma BHC
ND
Chiordan_e
NO
T
4,4-DDD
NO
4,4-DDE
ND
ACCOUNT:
T13L Laboratory
0.0000500 1
11/22/201612:52
WG927375
0.0000500 1
11/221201612:52
WG927375
0.0000500 1
11122/201612:52
WG927375
0,0000500 1
111221201612:52
VIG927375 _
0,0000500 1
11/221201612:52
WG927375
0.000500 1
11122120161152
WG927375 ,
0,0000500 1
11/221201612:52
WG927375
0.0000500 1
11/221201512-52
WG927375
PROJECT:
SDG:
DATE7TIME:
TBL-27423
1-873129
11/25/16 09:07
PAGE:
5 of 21

OUTFALL #1
SAMPLE RESULTS - 01
ONE LAB. NATIONWIDE.
.- rollecte,a'tlate/time: 11/14/16 14:36
L873129
_
Pesticides (GC) by Method
EPA 608
Result
Qualifier RDL Dilution
Analysis
Batch
Cp
Analyte
mo
mgA
date 1 time
4,4-DDT
ND
0.0000500 1
111221201612:52
WG927375
FIC
Dieldrin
ND
0.0000500 1
111221201612:52
WG927375
Endosulfan I
ND
0.0000500 1
11/221201612:52
WG927375
3
Endosulfan II
ND
0,0000500 1
11/22/201612:52
WG927375
SS
Endosulfan sulfate
ND
0.0000500 1
11/22/201612:52
WG927375
Endrin
ND
0.0000500 1
11/22/201612:52
WG927375
Rn
Endrin aldehyde
ND
0.0000500 1
11/22/201612:52
WG927375
Endrin ketone
ND
0.0000500 1
11/22/20161152
WG927375
Heptachlor
ND
0.0000500 1
111221201612:52
WG927375
Heptachlor epoxide
ND
0.0000500 1
111221201612:52
W0927375
Hexachlorobenzene
ND
0.0000500 - 1
11122/201612:52
WG927375
QC
Methoxychlor
ND
0.0000500 1
111221201612:52
WG927375
_
Toxaphene
ND
0.000500 1
11/22/201612:52
WG927375
7G1
(S)Decachlorobiphenyl
91.8
10.0-145
111221201`612:52
WG927375
(S) retrachloro-m-xylene
88.6
20-148
111221201612:52
WG927375
Polychlorinated Biphenyls
by Method
EPA-608
[Al
(GC)
Result
Qualifier RDL Dilution
Analysis
Batch
-
9
Sc
Analyte
mgA
mg/1
date 1 time
PCB 1016
ND
0,000500 1
11122/201612'23
WG927375
PCB 1221
ND
-ND
- 0.000500 1
11/22/201612:23
WG927375
PCB 1232 -
0.000500 1
11122/201612:23
- WG927375
PC131242, .� -
ND_
0.000500 1
11/22/201612:23
WG927375
PCB 1248
ND
0.000500 1
11/22/201612:23
WG927375
r
PCB 1254
ND
0.000500 1
1112212016 12:23
WG927375
PCB 1260
ND
0.000500 1
11122/201612:23
WG927375
(5) DecacNorobiphenyl
90.7
10.0.145
111221201612:23
WG927375
(SJ Tetrachforo-m-xylene
88.7
21.1-148
1UZ21201612,23
WG927375
Semi Volatile Organic Compounds
(GUMS) by Method 625
Result
Dualifier, RDL Dilution
Analysis
Batch
-
Analyte
mgll
mg1l
date 1 time
Acenaphthene
ND
0.00100 1
111231201615:22
WG927374
Acenaphthylene
ND
0.00100 1
11123120161522
WG927374
Anthracene
ND
0.00100 1
11/23/201615:22
WG927374
Benzldlne
ND
0.0100 1
111231201615:22
WG927374
8enzo(a)anthracene
ND
0.00100 1
11123/201615:22
WG927374
Benzo(b)fluoranthene'
ND
0.00100 1 -
W231201615:22
WG927374
Benzo(k)fluoranthene
ND
0.00100 1
11123/201615:22
WG927374
Benzo(g,h,ijperylene
ND
0.00100 1
111231201615:22.
WG927374
Senzo(alpyrene
ND
0,00100 1
11123/201615:22
WG927374
Bis(2•chlorelhoxy)melhane-
ND
0.0100 1
11123120161522
WG927374
Bis(2-chloroelhyl)ether
ND
0.0100 1
11123/201615:22
WG927374
B1s(2-c4oroisopropygether
ND
0.0100 1
11123/201615 22
WG927374
4-Bromophenyl-phenylether
ND
0.0100 1
11/23/201615:22
WG927374
2-Chloronaphthalene
ND
0.00100 1
11123/201615:22
WG927374
4-Chlorophenyl-phenylether
ND
0.0100 1
11/23/201615:22
WG927374
Chrysene
ND
0,00100' 1
111231201615:22.
WG927374
Dibenz(a,h)anthracene
ND
0.00100 1
11/23/201615:22
WG927374
33-Dichlorobenzidine
ND
0.0100 1
11/231201615:22
WG927374
2,4-Dinitrotoluene
ND
0.0100 1
11/231201615:22
WG927374
2,6-Dinitrotoluene
NO
0.0100 1
11123120i615722
VVG927374
1,2-Diphenylhydrazine
ND
0.0100 1
11123/201615,22
WG927374
Fluoranthene
ND
0.00100 1
11/23120161522
WG927374
Fluorene
ND
0.00100 1
W231201615:22
WG927374
ACCOUNT:
PROJECT:
SDG:
DATEMME: PAGE:
TBL Laboratory
TBL-27423
L873129
W25116 09:07 6 of 21

OUTFALL #1 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected-dateltlm_e: 11/14116 14:30 L8731_29
Ser'ni Volatile Organic Compounds (GC/MS) by Method 625
Result OuaKer RDL Dilution Analysis Batch C
Analyte mg/1 mgh date 1 time
Hexachlorobenzene
ND
0.00100
Hexachloro-1,3-butadiene
ND
0.0100
Hexachlorocyclopeniadiene
_
ND
Hi00
Hexachloroethane
ND
0.0100
Indeno[1,2,3-cdlpyrene
ND
0.00100
lsophorone
ND
0.0100
Naphthalene
ND
0.00100
Nitrobenzene
ND
0.0100
r --%trosodimethylamine
ND
0.0100
n41rosodiphenylamine
NO
0.0100
n-Nilroso&n-propylamine
ND
0.0100
Phenanthrene
ND
0.00100
Benzytbutyl phthalate
ND
0.00300
Bis{2-ethylhexyl)phthalate
ND
0.00300
Di-n-butyl phthalate
ND
0.00300
Diethyl phthalate
ND
0.00300
Dimethyl phthalate
ND
0.00300
Di-n-octyl phthalate
ND
0.00300
Pyrene
ND
0.00100
1,2,4-Trichlorobenzene
ND
0.0100
4-Chloro-3-methyl phenol
ND
0,0100
2-Chlorophenol
ND
J3
0.0100
2,4-Dichlorophenol
ND
J3
0.0100
2,4•Dimelhylphenol
ND
0,0100
4,6-Dinitro-2-methylphenol_
ND
J3
0.0100
2,4-Dinitrophenol
ND
J3
0.0100
2-Nitrophenol
ND
J3
0.0100
4-Nitrophenol
ND
J4
0.0100
Pentachlorophenol
ND
J3
0.0100
Phenol
ND
J4
0.0100
2A,6-Trichlorophenol
ND
J3
0.0100
(SJ 2-Fluorophenol
11.5
10.0-74.1
(S)Phenol-d5
7.11
J2
-
10.0-63.2
(S) Nitrobenzene-d5
73.2
-
28.3-723
(S) 2-Flucrablpheny!
82.7
34.5.133
(S) Z4,6-Tribromophenol
66.7
21.6-154
(S) p-Terphenyl-dT4
106
30.4-148
1
11/23/20161522
WG927374
1
11123/201615:22
WG927374
1
11/23/201615:22
WG927374
1
11123/201615:22
W6927374-
1
11/23/201615:22
WG927374
1
W231201615:22
WG927374
1
11/23/201615:22
WG927374
1
11/231201615:22
WG927374
1
111231201615:22
WG927374
1
11/23/201615:22
WG927374
1
11/23/201615:22
WG927374
1
111231201615:22
WG927374
1
1112D201615:22
WG927374
1
11123/201615:22
WG927374
1 .._.
_ 11/23/201615:22
W0927374
1
111231201615:22
WG927374
1
11/23/201615:22
WG927374
1
11/231201615:22
WG927374
1
1V231201615:22.
WG927374
1
111231201615:22
WG927374
1
111231201615:22
WG927374
1
11l231201615:22
WG927374
1
lV231201615:22
WG927374
1
11/23/201615:22
WG927374
1
111231201615:22
WG927374
1
11123120151S:22
WG927374
1
111231201615:22
WG927374
1
111231201615:22
WG927374
1
111231201615:22
WG927374
1
11/23/20161522
WG927374
1
11123/201615:22
WG927374
IV231201615:22
WG927374
111231201615:22
WG927374
1112312M 1522
WG927374
111231201615:22
WG927374
111231201615.22
WG927374
111231201615.•22
WG927374
ACCOUNT: PROJECT: SD& DATEMME: PAGE:
TBL Laboratory TBL-27423 L873129 11/25/16 09:07 7 of 21

WG927851
QUALITY CONTROL SUMMARY
ONE: LAC. NATIONWIDE.
Wel.Chemistry_by Method 16646 _ -,. �. - _
.... _ - .._ _L. ..��. L873129-91
Method Blank (MB)
Cp
{M1Dl R3179162-1 117181161312
MB Result Me oualifier MB MDL
MB RDL
�TC
Analyte mgA mgR
mgR
Oil 6 Grease {Hexane Extrl U 1.16
5.00
aSS
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
c GD
(LCS) R3179162-2 IV16116 13:13 - (LC5D) R3179162-3 1V18116 13:12
Spike Amount LCS Result LCSD Result
LCS Rec. LCSD Rec. Ret Limits tCS Qualifier LCSD Ouallfer RPD RPD Umlts
Analyte mgll al l
% % % % %
—Sr
Oil & Grease (Hexane Eatri 400 39.5 38.7
96.3 96.8 78.0-114 0,518 20
�GI
LEI
)SC
ACCOUNT: PROJECT' 5w:
reL Laboratory TOL-27423 1-873129
DATEMME: PAGE:
tV25A6 09:07 8 o121

WG926511
QUALITY CONTROL SUMMARY
ONE LAB.NATIONW10C. !�
Volatile Or9anlc Compounds(GC7M$) by Melhoa 624
- _ L873129.01-
Method Blank (MB)
• Cp
(MB) R3179168-3 1V17716 12:35
Ma Result MB Dualifier
MB MDL
MB RDL
�TC
Anatyte mryA
11119A
mo
Acrolein U
0.00887
0-0500
AcMonnrile U
C.00187
0.0100
-
'
Ss
Benzene U
0.000331
0.00100
Bromod,01momethane U
0.000380
_0.00100_
Blomoform U
0,000469
0-00100
C�
Bi0momerlane U
0,000866
0.00500
Carbontetrachloade- U -
0.000379
0.00100
'Sr
Chlorohenzene U
- -
0.000348
:.-- __- ,. •Yi4. - - -
0.00100
.` _ -
-,
Chlorod,bmmomelhane U
Chloroethane U
0.000327
00453
0.00100
0.00500
--
2•Chloroelhylvinylether_ U _
_ _O.
0.00301
0.0500 _
Chlomtbrm U _
0.000174
0:00500
r
_ _
Colororremane _ - --u --
0.000275
0.00250-
1,2-bichloiobemene U
13-Dichlorobenrene u
0.000349
0.000220
0.00100 _
0,00100
1.4-Dlchlorobenzene U
0,000274
0,00100
_ _
D01orodinualomethane U
0,000551
0.005D0
1,1-Dichloroalhane„ - U ., - .
0,000259
000100 -, - _ _ _ _
- _,- _ ._ - _ _ _ _ -- _ - _ y _ ,
I,20chlomethane U
0,000361
0.00100
1.1-Dichlaroetheoe U _
0.000398
000100
trans-1,2-Dichloroeihene U
0.000396
0.00100
1.2-Dichloropropane - U _ -
0,000306
0.00100
cis-1,3 Dichloropropene U
0.000419
000100
Iran5-1,3-Dichloroprop_ene_. U _
0.000419
DAM
Ethylbenzene U
0.000384
000100
Methylene Chloddo U -
0.0010C
0,00500
1.1.2.2-Tetrachloroethane U
0.000130
0,00100
Tetmchloroethene �Uw
- - - _ - _ _-
000672
0,00700
T0,00500-
-
Toluene ll
0.000780
1,1,1-Trlchloroethane u
0000319
000i00
1,12-Trichloroelhane - - - U - - - -
0.0003B3
000100-
Trichloroethene U _
0.00039E
0.00100 _
Trichloro0uaramethane U
0,D0120
0.00500
Vinyl chloride U
- - -' - --
.. 0,000259
0.00100
(S) toluene-d8 107
90.0-115-
-
(s)O,oromanuaromezllone 99.3 ..-. _
-
79.6727
(s)D.a,odnnuorolofuene 10.7
90.4-116
(S)48romonuorobenrene 985 - -
801-170
ACCOUNT:
DATE[IlME: PAGE:
PROJECT', 5DG:
T9L Laboratory
TBL-27423 LE73129
11125l16 C9.07 9 o1 21

WG926511 QUALITY.CONTROL SUMMARY ONE LAB, NAITCNWiDl
Volatile,Organic,ComAounds,(GC1M5), by Method 624 T _ . - L373129-Dl
Laboratory Control Sample (LCS) . Laboratory Control Sample Dupllcwe (LCSD)
(LCS) R2179168-1 1111711611:32 • (LCSD) R3179168-2 11/17/16 11:53
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Red,
Rec. Limits LCS Qualifier
LCSD Qualifier RPD
RPD Limits
Analyle
mgA
ni
mg/1
%
%
A
%
%
Acrolein
0.125
1.38
1.77
1510
1410
88.0-ll F. ill
E. J4 6.51
28.1
Acryloniuile
0.125
0.135
0.126 _
108
-
_ 101 _
v102
71.0-135
•--
7-06
- _-- - �2.22
20
Benzene
0.0250
0.0249
C.C254
99.5
73.0-122
20
eromodichloromethane
0 .02 50
-0.0270
00272
108
199
75,5-121
_ 0-670
20
Bromoform
0.0250
0,0200
0.0209
8,01
83.6
71 5 131
4.31
20
Bromomethane
00250
0,0228
0,0229
911
918
22.4.127
-- -
- 6670
20 -'
Carbon tetrachloride
0.0250
0.0243
0,0247
97.0
98.8
709-129
1,84
20
Chlorohenzene
-
0,0250
' ^
00223
0.0225
89.3
89,8 _
� ...
797.122 _
_ _• - - _0,530.
� --
20
Chlored:bromomethane
0,0250
0.0227
0.0230
90-8
Sill
79.2-124�
1.11
20
Chloroetllane
0,0250 _
-_0.0245
DOL50
98,0_
99,9 _
-41,2-153
._ - - - 1.95
20
2-Chloroethyl vinyl ether
0.125
0.166
0.169
133
136
23.4-162
1.81
23.5 T
Cil loan -
0.0250
0.0266
0.0266 .
.107
107
73.2-125
OA100
20
C1llorometharie
0.0250
0.0275
C.C280
110
112
55,8134
206
20
1,2-Dich1orobenzene"
, 0.0250
0.0232
0.0245
92.9
98.1
84.7-118
5.3fi
,
20
1,3-pichlorabeozene
0025D
00211
0,0219
_
84.5
877
_
77,6-121
371
20
1,4-16ichlorobenzene
0.0250
0.0229
0.0233
91.7
93.1
32,2-114
1.53
20
DichlDrodiflijoromerilrane
00250
0.0252
0.0265
}fit
106
56.0-134
5,35
20
a,1-Dichloroelhane
0.0250
0.0263
0.0267
105
107
'^ 7r.7-127 - - _._
--_ I59
„^
1,2-9ichlorcethane
0.0250
00303
0.0317
_
121
127
T65.3-126
J4 455
-
_20-
20
1,1-Dichloroelhane _�
0.026
0.0219
C.C229 «
87.6 -
-91.9
91.5 _
-- 59.9-137
440 -
- 20 «
trans-1,2-Dichdroelhene
0-0250
0,0230
0,0235
94.1
72.6.125
2.42
20
1,2-Dichloropropane
0.0250
0.0270 -
0,0275
108
110 '
774.125
151
20.
cis-1,3-Dichloropropene
00250
00274
0,0278
110
ill
77.7-124
1,37
20
trans-1,3-Dichloropropene
0,0250 -
0.0272
0,0279
109
112,°
73.5.127 -
2.51
20
Ethylbeiri
0,0250
0.0220
00222
87.8
88.6
801
0.890
20
Methylene Chloride, v
00250
0.0226 . _
0.0245
- _
40.4
47,8
69 5120
_-W-123 A
7.87
_ 20 '
1A2.2-Telracnloroelh6ne
0.0250
0.0221
0.0229
884
9L6
3,47
20
Tetrachloroethene
00250
0.0220
-' 0.0227
98,0
90.9
735-130
315
20
Toluene
0.0250
00248
0.0250
99.0
-•
99.9
77,9-116
0.850
20
11,1-Trichlcroelhane
0.0250- -
0.0267
0.0271 -
_ 107 •-
109
- 711-129 -
1.76 _
- 20-
1,12-Tnchlorcelhane
0.0250
0,0230
00237
92.0
95.0
ltl.V20
3,17
20
Trichloroetlhene -
00250
0.0239
0,0242
95.5
96.7
79.5.121 _
- 1.20
.
-
Trirhlorolluolomethane
0,0250
0.0243
0,0252
T
97.1
101
491.157
_ 3.86
20
Vinyl chloride
0.0250
0.0258
0,0262
103
105
61.5.134-
1.59
20
(i Toluene-d8
w
f05
- -
90.0-Ir5
- (SJOibromoBuoronietnone
-
._
_ f00-
101
79- -721
(SJn,a,a-iriRuororoluene
102 _
10f
904-r76
(SJ-8romorluoro�enzene
-
-
995
97.0
'80.r-120
ACCOUNT: PROJECT: 50G: DATEfTIME: PAGE:
TAL Laboratory - TM-Z7423 � L873129 1V2511609:w 10W21

WG927375
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE �
Pesticides(GC1 by Method $PA 608
- .. _1.873129.01
Method Blank {MB)
RP
(MB) R3179925-3 11122f16 11:12
MB Result MB Guallfer
MB MDL
MB RDL
ETC
Analyte mgA
mgA
my
Alarm U
0.00000813
0,0000500
Alpha BHC U
D.0000166 _
_D.0000500
Beta BHC U
0.0000124
0,0000500
Delia BHC _ U
0,0000197
0.0000500
Gamma BHC U
0,000G176
0.0000500
Cn
4,4-DDD U
0,00OC170
00000500
4,4-DDE U
0.0000164
_
0.0000500
'$r
44-DDT _ U
0.0000177
D.D000500
Dieldfin U
0-0000179
0.0000500
Endosullan I ., _ U
0.0000179
0.0000500 _ -
_ _ I
_
EndoSuUanll U
0.0000176
a 00005DO
Endosullari Sulfate U
0.0000196
0.0000500
'
GI
Endrm U
0.0000189
0.0000500
_
Endnaaldehyde U
0.0000742
- _
0.0000500'
_ _
Er4da ketone U
00600170
0.0000500
Heptachlof '
0.0000108
0,0000500
_ _U _
Heplachlor epoxide U W
_
0,0000175
0,0000500
1
Hexachlorohe_nxenc ' U _
0,000C134
o.0ooD5d0 _ _
_ _ _
Methoxvchlof U
0,00DC193
0.000D500
ChlorUanc, U - -
0,6006977
-0,000500-
to,aphene U
0.006158
0.000500
(S)DecochloroblpAenyfr 100-- - - -
_
- -
- -
100-145
(S) Teirochloro rl7-Wene 77.7
2f FN8
Utolaton; Control Sample (LCS) • Lahoratory Control Sample Duplicate (LCSD)
(LCS) R3179925.2 11/22/16 10,59 • (LCSD) R3179925-1 11I22116 10P.47
Spike Amount LC5 Resull LC50 Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD OuallRer RPD RPD Limits
Analyte mgA mgA mgA % % % % %
Akhin
0,000200
0.000174
0,000174
87,1
Alpha BHC
0,000200
0.000210
0000206
105
Beta BHC
DD00200
0.000212
0 o06212
106
Delta BHC
0.000200
0.000201
0.000210
101
Gamma BHC
_
0000200
0.000211
0.000212
105
4,4-DDD
0.0002.06
0.000206
0.000209
103
4 4-DDE
0.00020G
0.000194
0.000197
96.9
4AMT
0.000200
0.000221
0.000225
111
Dieldrin
0.000200
0.000208
0.000211
104
Cndosulfanl
0.000200
0,000205
D�000208
103
ACCOUNT:
TBL Laboratory
86.9
100-124
103
66.6.106
106
641011
105
61.1-115
106
62.1.109
104
507429
98.5
_
37.1.131
713
43.9-131
-- 105
-- - 57,2419
104
_-57.2-48
PROJECT:
T13L-27423
0.250
315
1-96
20
0,130
20
434
20
0.670
20
1-25
20
1.70
20
1.76
20
US
20
1.16 V
20
SDG:
L873129
DATEITIME: PAGE:
11125A6 09.07 11 of 21

WG927375
QUALITY CONTROL SUMMARY
ONE LAB NATIONwfOE,
Pesticides (GC) by Method EPA 608
-
t873179.01
_
_
Laboratory Control Sample (LCS) • Laboratory Control Sample
Duplicate (LCSD)
(LCS) R3179925-2 11/22/16 10.59 • (LCSD)
R3179925-1
11122/16 10:47
r
Spike Amount
LCS Result
LC5D Resu't
LC5 Rec.
LCSD Rec.
Rec. Limits LCS Ouahfier LCSD Oualiner
RPD
RPD ❑mits
�TC
Analyte mgA
mgll
mgll
%
%
%
%
%
Endosullan It 0.000200
0.000203
0.000204
101
102
591-120
0.540
20
EntlosuRan sullate 0.000200
C.000202
0.000204
101
102
49,7.132
1,19
20
'
Endrin 0.000200
0.000214
0-000218
107
109
55.8-124
1.70
20
Endrir aldehyde 0.000206
0.600194 _ _
0.000190
96.8
94.9
_ -
46.7.122 -
L96
20
Endnn ketone 0.000200
0.000195
0-000198
97.6_
98.9
59.2-126
1.32
20
Cn
Heplachlor 0.000200
0.000174
0.000175
869
87.5
15.4-116
0,80.0
25,1
-
Heptachlor epoxide 0.000200
O.000194
0.000200
97.0
100
- -
573-117
3.15
20.'$!
Hexachlorbhenzene 0.000200
-
0.000174.
0,000172
87.0
85,9
28.7-100 q
1.31
20
_
Methmrychlor 0,000200�
0000215
0000218
-
IDS
109
55.7-121
1.26
20
(S)0ecochlorooiphen/
,,
982
V
r0.0a45
P retrdchloro-nt-Wene
79.5
71.3
741-148
7GI
�Af
'15c
ACC06N T: PROJECT: SOG OATWIME: PAGE:
TBL Laboratory TBL-27a23 L813129 11125116 0997 12 or 21

WG927375
QUALITY CONTROL SUMMARY
oNELAB.raATiGNwiDE.
Pnlychlorinnted Biphenyls (GC}.by Method EPA-608 -
_ ,_. ,,.,_ L877129-61__,
Method Blank (MBI
Cp
(MB) R3179943-1 11/2211611:45
MB ReSult MB Dualifier MB MOIL
MB RDL
AnaMe MO mgA
mgA
TC
PCB1260 U 0.0000146
D,0o0500
PCB 1616 _ v _ 0-0000198
0.000500 - - - _ ..
_ - - -
- - .. 3SS]
PCB 1221 L 0.101>00244
a 000500
_
PCB 1232 U - 00006213
C,000500-
K81242 U 0.0000242
0.000500
Cn
PCB 124e B 06000135
0.000500
PCB 1254� U 0,000C181
0.000560
f$J DP(O[hlOiQd�phPlryl 89.1
10.0-145
(5)Terrachloro-m-Xytne 74.2
21.1-148
.p
Laboratory Control Sample (I -CS) • Laboratory Control Sample Duplicate {LCSD)
'CI
(LCS) R3179943-2 1112211611:58 • (LC501 P3179943-3 1V22116 12:10
Spike Amount LCS Result LCSD Ri
LCS Rec. LCSD Re[. Rec. L1mlEs LIES Qualifier LCSD Dualifier RPD
RPD Limils
ail
Analyle mgI mgA mgll
% % % %
%
PCB 1260 0.000500 0.000422 D.OD0428
84,4 85.6 53.6-122 1.34
22
t
P_C6ID16 _ 0.600500 0.000401 0.000414
80.3 82.8 48-4.116 _ 3,06
20
SC
(5)5ecachi0roDlpheny1
,
84,8 88.1 10.0445
W
(SiTer
7t3 65.9 711-148
ACCOUNT: PROJECT: SDG:
TBL Laboratory THL-27423 L873129
DATEITIME:
IV25116 09.07
PAGE:
13 o1 21

WG927374
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE,
Semi Volaille_Organic
Compounds
lGClMS}.by Method 625
,• _ �_ LE73129-Ul
Method Blank (MB)
Cp
(MB) R3179979.3 1U217i61740
MB Result
MB Qualifier MB MOL
MB RDL
Anayle
mg4
mgll
mgA
TC
Acenaphthene
U
D.D00316
0.00100
ACenaphlhylene
U
0000309
000100
a
SS
Anthracene
U
0.OD0291
0.00100
Azcbenzene
11
0.000154
0.0100 _
a
Benndrne
U
0.D0210
0.0100
C11
Bcnzoldlanthractlne
U
0.000111
0 00100
BenzolbNOuoranthene
U
0.0000896
0.00100
s
SF
BenmlNpfiucranthene. .
U
0.000255
0,00100
BenMq,hAperylene
U
0.000161
0.00100
BennXalpyrene
U
0.000269
_0-00100 -
BcgkhlorethcMmethane
U
0.000214
0,0100
Bisl2.chloraethyllether _
U.
0.000214
•� �-
0,0100 _
91si2-chl0roi50pr0py1lelher`
U--�
0.000308
00100
4-Bramaphenyl-phMlylelher
U _
OL000180
00100
~A€
2-Chloronaphthalene
U
0.0013204
0.00100
4{hlaraphenybphenyletner
U
0-000170
0,0100
Chrysene
_
U
0,000133
- _
000100
• --
SC
Drbenr(a.h)anihracene- -
U
O.0D0251
0.00100
- - -
- - - - - -
3,30ichlorabenzidine
U
0.00169
0.0100
2 a-D1narotoluene - -`
U -
r ~
- 6.000219
0.0100 j
- _ -
2.6-Dinitrotaluene
U
0.00141
0-0100
Huoramhene •� •- _
7U'
_ 0.000342
0.00100-
Fluorene .�
.U__. -
0OD0177
0.00100
HLochlerabenz.Ln.
U't
0.000227
0.00100
HexacNaro-l.3-butadiene U
0.D0264
0.0100
Hexachlorocyclopen_ladiene U
6.00180
0.0100
Heaachl0roethane U
0,00313
0.0100
lndenop,2,3-colpy1ene V _
0,000333
000100
Isaphavone U
0.000238
0.0100
Naphthalene U - _
- -U - - -
~ 0000413.
0,00100
Nilrabenzene�
0.000200
0.0100--
n-Narasadimelhylamine U
000256
0.0100
_
n-Nibosodiphenylamine U
0.000137
0.0100
n-N;trosodi.n,propylamine _ U
- 0-000311
0.0100
Phenanthrene L
0.000205
0.00100
Ben_zylbutyl phthalate u _ _
_ 0:000395
0.00300-
_
Bis{2-ethylhexyl}phthalate U
O.00D496
0.00300
Dl-n-butyl phthalate 0.000276 _ J
0.00W75
0.00300 •' «
Diethyl phthalate U
0.000356
0-00300-
Dimelhyl phthalate _ U J
0,000338
0.00300
- •ACCOUNT'.
PROJECT: , SOG: OATEITIME: PAGE:
TBL Lebaratory
TBL-27473 t B73129 11125/16 09.07 14 or 21

WG927374
Semi Valntlle Orgnnic Compounds (rCIl by McLhod 625
Method Blank (MB)
QUALITY CONTROL SUMMARY ONCLAV NATIONWIDE.
(MB( R3179979.3 1V2111617.40
W Result
MB Ouallner MB l
Q RDL
Analyle
mgA
mg/1
ml
DI-n-octyl phthalate
a
D.Dpp2n
C.00300
U _-�
0.000295
0-50100 -
1,2,4-7ri0l0r0be0zene
U
0.000355
0.0100
4-Chloro3-methylph_en_oI
n
u _
_0.000229
_ -
0.0100
2-Chlo7ophenul
U
0.000190
C.0100
2 4:0i[hl0r0phenpl
U _
_ _ 0-000972
_ 0,010_0
2,4-Dimethylphenol
U
0100134
0,0100
4,6-Dimua2-methylphenol
U
0,00260
0,0100
2,4-Dinirr0phenol
U
C.0O230
0.0100
2-NilrophBnol _
U _
_ 0.000279
_ 0-0106 _
4-Nltrophenol
U
0,00273
00100
Pentachtorophen0l
u '
_ 0.0004D7
6.DI00
Phenol
Ll
0A0113
0.0100
24.6-Tiich4rophenol
U
0000278
0.0100
(S)Nitrabenrene-d5
652
2H}123
(5)2-Fluombpnenyf_
69.9
_ _
34.5-133 _
($1P-rerphenyl-d74
989
30.4448
(5J Phena145
33.5
10.0-632
(5) 2-Fluorophenol
483
*..0174.1
QZ4.6-7ribromophefml
78.0 v
-
21.6-154
Laboratory Control Sample {LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3179979.1 IV211161629 • (LCSDy R3779979-2 iV2V16 1652
Spilre Amount
LCS Re5ull
LC5D Result
LCS Rec,
LCSD Rec.
Rec. Limits
LCS Ouaoner ICSD Quallner RPD
RPD Limits
Anal
m9A
mgn
mgA
$
%
%
%
%
Acenaphlhene
0.0200
0.0171
0.0184
85.6
92.0
39.D-128
738
20
Acenaphthyleae
00200
6.0182
00195
91.2
97.5
41.D-135
_ - 6.63
20
Anthracenc -
- 0.0200
0,0195
0,0199
97.4
99.4
42.9-138
_
1,98
20-
'AzobOntene
OA200
0,0173
00183 _
86.6
91.5
372.129
5.46
20
Benzidine
00200
0.0146
0.0148
73.2
74,0
10.0.75.5
1.05
40
Benzo(alanihiacene
0.0200
0.0185
0.0190
923
94.9
42.3.137
2.75 _
20
13e1120(b)0uoranlhene
0.0200
0.0210
0.0211
105
105
40.5.137
0.310
20
BenzgklRueiamhene
_ 0.0200
0.0189
0.0202 --
- 94.6
_
101 -
-- 41,5-1a0
- _ ~- - - - 6,70
-20-
Oenzo(gh.ijperylene
_
00200
0.0201
0.0209
100
104
38.8-137
3.90
20 _
Benm(alpyrene
0.0200
0.0180
0.0186
90-2
93,2
417-138
_ _ _ 329
20
Bisl2-chlowl70xylmetiWe
_ _
0.0200
_
C.0165
0.0182
82.3
90.8
36.7,123
_ _
9,94
20
Bis(2thlar0eihynelher
0.0200
0.0130
0.0148
l
74.2 -
-_ 29.8-174
- -- a 13.5
25.3
-
BIsl2-chl or sopiupy8ethm
0.0200
_
0,0147
0,0168
73.5
84.0
33.1l
13.3
21,3
ACCOUNT:
PROJECT:
sl
IDATFJTIME: PAGE:
TRL Lalwra7ary
TBL-27423
L873t29
105AG 09 07 15 of 21

WG927374 QUALITY CONTROL SUMMARY ONE LAB NATIONWIDE. 0
Semi Volatile, Organic Compounds (GC7MS).by. Method 5Z5 - _ - - - L873129-01
Laboratory Control Sample (LCS) . Laboratory Control Sarnple Duplicate (LCSD)
(LCS) R3179979-1 11/2111616:29 - (LCSD) R3179IJ79-2 11/21/16 16:52
Spike Amount
LCS Result
LCSD Result
LCS Rec,
LCSD Rec.
Rec, limits
LCS Oualifier LCSD Dualifer RPD
RPD Limits
Analyte
mgA
mgA
mgA
%
%
%
%
%
4-eromophertyl-phenylether
00200
0,0181
0,0186
90.7
93 2
39 0-137
2.70'
20 W
2-Chloronaphthaiene
00200
0.0155
0,0168
77.7
84.0
35.1-123
7.71
20
4Chlaraphenyi-phenylether
0,0200
00172
0.0179
89,6
37.3-130
4.35 µ
20
Chrysene
0,0200
0.0201
0.0208
_85.8
100
104
40.5-140
3.36
_
20
Dibenz(a,hlanlhracene
0.0200
-
0.0185
0.6193
92.3
96.6
39,9-141
_
456
20 -
3.3-Dichlorobenbdine
00200
0.0197
0.0204
98.4
102
33.1-134
3,43
20
2,4-0iminoWuene
0.0200
0.0189
D.0197
94,3
98.7
42.3.143
4,64
20
2,6-Dlnitrotoluene
0.02D0
0-0180
C.0192
90.0
95.9
41.0.139
6.26
20
Fluaranlhene
0.0200
0.0199 _
0.0204
99.5
102
41.4A41
2.29
70
Flucrene
0.0200
0,0118
0-0189
89.1
94.3
39.9-132
5.64
20
He-achlorobenzene
0.020D
0,0183
0.0187
41.3
93.6
34.1-125
2.53
20
He,achloro-1,3-butadiene
_
00200
0,0122
00139
60,8
69.6
24.9-121
13.4
22
Hexachlorocglopenladiene
_-- 0.0200 r
0.0145 - -
0.0167
- 724
83.6
13,5-122
143
216
Hexachloroethane
0,0200
000988
00117
494
_
58,5
22.2-109
- _ _
16.8
25.8
Indena(1,2,3_•Cd)pyrene
0,0200 _
0.0186
_ 0.0195
92.8 _
_97.3
410-140
4-77
20_
15ophorone
00200
0.0118
00197
88.9
98.6
30.5.109
10,3
20
Naphlhatene
0.0200
_0.0145
0,0162
72A
91,2
33.0-117
_ _
11.5
20
Nitrobenzene
0.020D
0.0150
0,0170
7419
648
34A.121
_
L2.5
212
n-Nihosodlmelhylamine
002oo
0.00697
0,0OB69
34.8
434
12.3-7015
21.9
33
n-Nitmsodiphenylamine
0.0700
0.0194
0.0199
96.8
99.3
41.1-134
2.61
20
n-Niltosadl-n-pmpylamme
0-0200
0.0157_
0.0173
78.7
96.7
�35,6-125 -
- -
- _ 9.70
20 _ • - - -�
+
_
Phena51hrene
0.0200�
0.0185
00190
925
95,0
41.4-134
2.68
_ _ _� _- _ _ _ _�-
_
20
Renaylbutyl phthalate
00200
00188
0.0194
94.0 _
96.9 _
- 29.2.146 _
- _ . • _ _
- 3.04
207
Bis(2-ethylhcxygphlha1ale
0.0200
0.0190
0.020C
95.1
99.9
41,4150
4.90
20
D�•n-butyl phthalate
00200
0.0203
00208
102
104
33.0.151
-2.3B
20
Diethyl phthalate
0.0200
0.0191
00199
95.5
99.6
36.D-140
4.15
20
Mmethyt phthalate
00200
0-0182
0.0194
90-8
97.1
23.413E
6.69
20.2
Dbn-ociyl phthalate
0.0200
0.0180
0 C199
90.0
95.2
39.8-146
5.64
20
Pyrene
0.0200
0-0198
0-0202
99-2
101
40-2-135
1-89
20
1,244flChlorohenzene
0,0200
0,0126
0,0144
63.2
71.9
26.6-109
12.8
20
4{Moro-3-methylph_enal
0,0200
_0,0123
0,0139
51,5
69.6
34-6.130
12.3
20
7.Chlorophenol
0.0200
000711
0,00988
15.5
49.4
31.2-103
J3
32.6
20
2,4 Dichlorophenol
0.0100
0.0117
0.0153
58-3
79.2
- 396-121
J3
304
20
2,4-Dimethyl$enol
00200
a0131
0.0148
65,6
73.9
33.8.126
11.9
20
4,61initro 2-methylphenol
0.6200
0.00884
0.0159
44.2
793
28.2-134
J3
56.8
29.2
2A-Dinitrophenol
_ _
0,0200
0,00274
0,00441
137
22.1
1010.108
J3
_
45.9
40
2-Narophenol _
0,0200 _
0.0113_
00166
56.7
83.0
38,3-125
J3
37.6
_ 20
4 Ni-0_henol
0.0260
ND
ND
0.000
0.000
10.MS4
J4 J4
o.000
33.6
Pentachlorophenol
_ 0.0200_
0.00864
0.0165 -
43.2
82.3
- iL0.117
-
J3
- _
623
_ 34.3
Phenol
00200
a Kin
0.00224
8,84
11.2
10.0,77.3
J4
23.6
246
ACCOUNT: PROJECT: SDG: DATEJfIME: PAGE:
191. Laboratory TBL-27423 L973129 11125A6 09:07 IG or 21

WG927374 QUALITY CONTROL SUMMARY ONE LAS NATIONWIDE,
Semi VO14tile Organic -Compounds IGCJMS) by Method 625 L873129-01
Laboratory Control Sample (LCS) • Laboratory Control Sample DLIp)k lte (LCSD)
Cp
(LCS) R3179979-1 1112V1616:29 • (LCSO) R3179979-2 IV2111616:52
Splke Amount LCS Result LC5D Result LCS Rec. LC5D Rec. Rec. Llmlts LCS Oualifier LC5D Qualifier RPD RPD Limits
Analgte ml al mV
%
%
24,5-Trlchlomphenal 00200 0,0111 0.0188
55.5
94.0
35.9.129 J3 51.6 22.4
(SJN+rrobenrene-d5
74.9
85.4
283.123
3
Si
_ (5)2-6uoradrphe0yl •, _ _._
803
81.3 -,
345-733
j5)p-reroenyWM
96.5
100
- N r
30.4.146
- -
a
(S1Ahenol-d5
869
112
11.0-632 J2
Cn
_ -
(5%2-14uuropAenol .� _ -
11.1
_
179
_
100-141
(S) 2,4, 6-Tobfomopl+rnol - - - _
-- 63.5
97.0
21.6-I54 - _ - - - -
F,
ACCOLJNT; PROJECT: SDG: DATFJTIME: PAGE:
TDL Lab—[" T©L-27423 1873129 11125116 09,07 _ 17 01 21

GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Abbreviations
and Definitions
,
SDG
Sample Delivery Group.
Cp
-MDL
RDL
Method Detection Limit.
Reported Detection Limit.
Tc
ND
Not detected at the Reporting Limit (or MDL where. applicable).
U
Not detected at the Reporting Limit (or MDL where applicable).
FSS
RPD
Relative Percent Difference.
(S)
Surrogate (Surrogate Standard) - Analyses added to every blank, sample, Laboratory Control
;
SampVDuphcate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
Cn
recovery. Surrogates are not expected to be detected in all environmental media.
.Rec.
Recovery.
�Sr
Qualifier
Description
GQc
E
The analyte concentration exceeds the upper limit of the calibration range of the instrument
established by the initial calibration (ICAL).
J
The identification of the analyte is acceptable; the reported value is an estimate.
- - - - -_ .;
0
J2
Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3
The associated batch OC was outside the established quality control range for precision.
A!
J4
s
The associated batch QC was outside the established quality control range for accuracy.
r
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
TBL Laboratory
TBL-27423
L873129
11125/16 09.07
18 of 21

ACCREDITATIONS & LOCATIONS
ONE LAB. NATIONWIDE.
ESC Lab Sciences Is the only environmental laboratory accreditedlcenilied to Support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry. The most significant benefit to our "one location' design is the design of our laboratory campus. The model is conducive to accelerated productivity, Cla
decreasing turn -around time, and preventing cross contamination, thus protecting sample Integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
`Not all certifications held by the laboratory are applicable to the results reported In the attached report.
State AccreditaVons -Tc
Alabama 40660~-~ _- _Nevada _— -µ TN-03-2002-34 3
Alaska TUST-080 New Hampshire 2975 S5
Arizona -_. --_ _ AZO6_12 _ N_ew_Jersey--_NELAP_ TN_O02 _._..
Arkansas _ 88-0469 New Mexico TN00003
California 01157CA New York — - 11742 CD
Colorado TN00003 North Carolina Env375
Conneticut-PH-0197 North CarolinaDW21704
Florida �-_--_--_ __- _ E87487 � -�_ - North Carolina� .-..._.._- 41 - -. - LEI
Georgia ^� NELAP North Dakota R-140 -_
CLOO-
Georgia' --- _---- _-- 923 - - --_-_ Ohio-VAP -- 9915 FC
Idaho TN00003 -� Oklahoma 9915
Illinois 200008 Oregon TN200002
Indiana C-TN•O1 Pennsylvania 68-02979 G
Iowa _ 364 _ Rhode lsiand - - 221 _ - -
Kansas E-10277— South Carolina _ 840.04�
Kentucky' 90010 South Dakota nla
Kentucky _ — - 16 - _ _ _ Tennessee" ° 2006
Louisiana A130792 Texas T 104704245-07-TX
Maine - - - - - TN0002-- Texas' - — -- - - - - _ LABO152
Maryland —� --- 324 Utah 6157585858
Massachusetts M-TNO03 Vermont VT2006
Michigan 9958 Virginia 109
Minnesota 047-999-39.5 Washington C1915
_Mississippi _ TN00003 West Virginia 233
Missouri_ _ _ T 340 Wisconsin - 998093991D
Montana CERT0086 Wyoming v A21LA
Nebraska _ _ _ NE-OS-15-05
Third Party & Federal Accreditations
A2LA_- ISO 17025 1461.01 Al HA _ 100789_
A2LA - ISO 17025' 1461.02 — _-_ DOD 1461.01
Canada 146i,01 - USDA 5-67674
EPA-Crypto - --TN00003 _ � _._
Drinking Water ' Undefgfound Storage Tanks ' Aquatic Toxicity ' ChemlcallMicrobiological I Mold "° Accreditation not applicable
Our Locations
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices. please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
•
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• ♦ NV - � ♦ Ir ��♦{
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•A7 tJr,R r7T AS! SC
♦ o * t i AL cA
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47 F-L
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ACCOUNT: PROJECT: sUG: i'; OATEfTIME; PAGE:
TBL Labioratory TBL-27423 L873129 11125/16 09:07 19 of 21

.iVA
To whom it may concern;
COUNICILTOOL
Buiidinp Tools -Building Uust_SNxe 1 B86
j I'
N C &- o 3 6�/Sf
RECEIVED
JUL 2 2 2016 July 15, 2016
CENTRAL FILES
DWR SECTION
In regard to our General Permit No. NCG030000 effective November 1, 2012 expiring on midnight
October 31, 2017 because of some internal turnover and change of job responsibilities by responsible
employees, Council Tool Company submitted semiannual storm water samples to the Division of Water
Quality in December of 2012. Council Tool Company has however failed to submit samples to the
Division of Water Quality since that time until July 15, 2016 for year 4 period 1.
Council Tool Company has had no significant spills at our facility since the inception of our current
permit. Council Tool Company currently has in place a Storm Water Prevention Plan, Housekeeping and
Preventive Maintenance Procedures, Spill Prevention & Response Plan, a Pollution Prevention Team,
Best Management Practices, Qualitative Monitoring and ongoing Employee Training.
To prevent any future non compliance issues of our General Permit No. NCG030000 Council Tool
Company has partnered with TBL Laboratory of Lumberton NC who will notify us 30 days prior to the
next submittal of storm water samples which will be for year 4 Period 2 Sample 8 July 1, 2016 through
December 31, 2016. Council Tool Company also has in place an internal reminder set on our outlook
calendar for both Analytical and Qualitative Monitoring requirements.
Enclosed you will find signed copies of the results from the recently submitted storm water samples too
our independent laboratory TBL of Lumberton, N.C. I have also been in contact with Steve Pusey of the
Division of Water Quality in Wilmington NC who advised me in this matter and has been very helpful.
Please let me know if you are in need of anything else.
Regards,
Velton Jacobs /
HR / Compliance
Council Tool Company Inc.

8

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Dale submitted �— � — U/
CERTIFICATE OF COVERAGE NO. NCG03 O Q 40 SAMPLE COLLECTION YEAR RO/6
FACILITY NAME C�00#,JG► I, -L_Cr l __ [k REC E pv *,r LE PERIOD an -June ❑July -Dec
COUNTY ^� or ❑ Monthly' (month)
PERSON COLLECTING SAMPLES JUL 2 2 20116ISCHARGING TO CLASS ❑ORW ❑HQW (]Trout ❑PNA
LABORATORY :n2j _ Lab Cert. # _ 7/ 9s� ❑Zero -flow [:]Water Supply ❑SA
Comments on sample collection or analysis: CENTRAL FILES [vOtherDWR SECTION
:r
Part A: Stormwater Benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
`24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organlcss
�Benchmvrks
-
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
1 mg/L
.50
' .3
A. 3 sl Leuib40.003
.1(,m L
<1ma.1L
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date; 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTp), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the stormwater Pollution Prevention Plan."
V_eI TIO tq _ c� S
Name (Print name)
IJ � Corm
Title rint title)
715-I
(Signature) 1'1(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, the; must be reported in the format, "<XX melt.". where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
� o discharge this period??
outfall No.
Date Sample
Collected"
(ma/dd/yr)
24-hour rainfall
amount,
inches
Non -polar O&G/TPH by
EPA 1664'(SGT-HEM)
Total Suspended Solids
-
EpH
Benchmarks =_->
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an orlainal and one cony of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab -results for_ at endmonitoring t2eriod
in the case of.."No Dischar e" reports) -to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware tJiat there are sj"cant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
t '
I
3 '
3 Permit Date:11/112012-10/31/2017
7- /.5 - /6
{Date]
SWU-245, last revised 10/25/2012
Page 3 of 3

North Carolina
Beverly Eaves Perdue
Governor
MAR�......
NCDENR
Department of Environment and
Division of Water Quality
John Council
The Council Tool Company
PO Box 165
Lake Waccamaw, NC 29450-0165
Dear Permittee:
Charles Wakild, P. E.
Director
December 4, 2012
Natural Resources
Dee Freeman
Secretary
Subject: NPDES Stormwater Permit Coverage Renewal
Council Tool Company - Lake Waccamaw
COC Number NCG030459
Columbus County
In response to your renewal application for continued coverage under stormwater General Permit NCG030000
the Division of Water Quality (DWQ) is forwarding herewith the reissued General Permit. This permit is
reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of
Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October
15, 2007 (or as subsequently amended).
The following information is included with your permit package:
• A new Certificate of Coverage (COC)
• A copy of General Permit NCG030000
• A copy of the Technical Bulletin for the General Permit
• Two copies of the Discharge Monitoring Report (DMR) Form
• Two copies of the Qualitative Monitoring Report Form
The General Permit authorizes discharges of stormwater, and it specifies your obligations for discharge
controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself
with all the changes in the reissued permit. Your facility has six (6) months from the time of receipt of the
permit to update your current SPPP to reflect all new permit requirements.
The first sample period of your permit begins January 1, 2013. Your facility must sample a "measureable
storm event" beginning during the periods beginning January 1 and July 1 of every year (or, if applicable,
report "No Flow," as outlined in Part III, Section E}. Also, please note that Tier 3 Actions in Part II of your
permit are triggered by benchmark exceedances on four occasions beginning on the effective date of this
permit and do not count prior exceedances.
The more significant changes in the General Permit since your last COC was issued are noted either in the
Draft Permit Fact Sheet that accompanied the public notice (http://portal.ncdenr.org/web/wq/ws/su/current-
notices), or in the Response to Comments / Summary of Changes and Technical Bulletin documents that are
posted on the Stormwater Permitting Unit's well with the new General Permit. Please visit
http:IlQortal.ncdenr.org/web/wq/wsZsu/npdessw (click on 'General Permits' tab) to review that information
for your specific General Permit carefully.
1617 Mall Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Raleigh, North Carolina 27604
Phone: 919-81 \FAX: [phone]
Internet: www.nonaterquality.orq
1,n Equal Opportunity t Affirmabwe A=n Employer
One
NorthCarolina
,Xatura!!y

John Council
DecFmber 4, 2012
Page 2 of 2
Some of the changes include:
• Part II:
• Section A: The Stormwater Pollution Prevention Plan (SPPP) section, if applicable, has been updated
to the most current language of our permits. Additional conditions for specific industry sectors have
been added to the SPPP requirements in some cases.
• Sections B, C: Failure to perform analytical stormwater monitoring may result in the Division requiring
that the permittee begin a monthly sampling scheme.
• Sections B, C: A lower TSS benchmark of 50 mg/I for HQW, ORW, PNA and Tr Waters applies to these
more sensitive waters.
• Sections B, C: The monitoring parameter Oil & Grease (O&G) has been replaced by the parameter
Total Petroleum Hydrocarbons (TPH) for vehicle maintenance areas, and in some cases, other
analytical monitoring requirements.
• Sections B, C, D: Inability to sample due to adverse weather must be recorded in the SPPP, or in
separate on -site records if your General Permit does not require an SPPP. Adverse weather is defined
in the "Definitions" section of the permit.
• Sections B, C: The term "Representative Storm Event" has been replaced by "Measurable Storm
Event." A measurable storm event is defined in the permit.
• Section D: If the permittee fails to respond effectively to problems identified by qualitative
monitoring, DWQ may require the permittee to perform corrective action.
Please review Parts III and IV to understand the Standard Conditions of your new NPDES General Permit,
including Compliance and Liability, Reporting, Monitoring and Records requirements; Operation and
Maintenance obligations; and Definitions. Please note that all samples analyzed in accordance with the terms
of this permit must be submitted to the Division on Discharge Monitoring Report (DMR) forms available on
the Stormwater Permitting Unit's website above. DMR forms must be delivered to the Division no later than
30 days from the date the facility receives the sampling results from the laboratory. Also note that existing
permittees do not need to submit a renewal request prior to expiration unless directed by the Division.
Your coverage under the General Permit is transferable only through the specific action of DWQ. This permit
does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it
relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law,
rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit
package, please contact the Division's Stormwater Permitting Unit at [phone],
Sincerely,
for Charles Wakild, P.E.
cc: DWQ Central Files
Stormwater Permitting Unit Files
Wilmington Regional Office

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030459
STORM WATER
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
The Council Too] Company
is hereby authorized to discharge stormwater from a facility located at:
Council Tool Company - Lake Waccamaw
34S Pecan Ln
Lake Waccamaw
Columbus County
to receiving waters designated as Lake Waccamaw, a class B;Sw,ORW waterbody in the
Lumber River Basin in accordance with the effluent limitations, monitoring requirements, and
other conditions set forth in Parts I, II, III, and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective December 4, 2012.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this 41h day of December, 2012.
for Charles Wakild, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

o�0� w A
Vj 7
Michael P. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Mr. Velton Jacobs
Council Tool Company, Inc
345 Pecan Lane
Lake Waccamaw, NC 28450-0165
Dear Mr. Jacobs:
Coleen 11. Sullins Director
Division of Water Quality
February 1, 2008
Subject: NPDES Compliance Inspection Report
Council Tool Co., Inc.
NPDES Permit NCG030459
Columbus County
The North Carolina Division of Water Quality conducted an inspection of the Council Tool facility
on January 30, 2008. This inspection was conducted to verify that the facility is operating in
compliance with the conditions and limitations specified in NPDES Permit No. NCG030459.
The facility appeared to be clean, well maintained and properly operated. The stormwater
outfalls from the site appeared to be in good condition with no evidence of sediment from the site or
presence of any pollutants of concern. In the laboratory reports, analytical data did not display any
results that were above the "benchmark" values listed in the permit. The only issue noted was the lack
of employee training documentation. While employees are informed of stormwater impacts, there was
no record. In the future, please record dates of training, listing those present. All other aspects of the
Stormwater Pollution Prevention Plan appeared to be very thorough and compliant. Attached is a copy
of the compliance evaluation inspection.
Should you have any questions concerning the inspection, or if I can be of any further
assistance, please contact me at 910.796.7215.
Sincerely,
Wes Hare
Environmental Specialist
Surface Water Protection Section
Wilmington Regional Office
cc: DWQIRaleigh Central Files C o w m 6✓ 5
�NPDES-General-Permit Inspection Files-(Naw�—ver'County
NPS Assistance and Compliance Oversight/Raleigh
North Carolina Division of Water Quality 127 Cardinal Drkc Fxtension Wilmington, NC 28405 Phone [phone]
Internet: w)Aw,newateronaIity.ni Fax [phone]
No thCarolina
AratimallIf
Customer Service
1.877-623-6748
An Equal OpportunitylAffirmative Action Employer — 50% Recycled110% Post Consumer Paper

Compliance Inspection Report
Permit: NCG030459 Effective: 11/01/07 Expiration: 10/31/12 Owner: Council Tool Company
SOC: Effective: Expiration: Facility: Council Tool Company
County: Columbus 345 Pecan Ln
Region: Wilmington
Lake Waccamaw NC 28450
Contact Person: Velton Jacobs Title: Phone: [phone]
Directions to Facility:
System Classifications:
Primary ORC: Certification: Phone:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 01/30/2008 Entry Time: 02:00 PM Exit Time: 02:50 PM
Primary Inspector: Wes Hare Phone: [phone]
Secondary Inspector(s):
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Metal Fabrication Stormwater Discharge COC
Facility Status: ■ Compliant ❑ Not Compliant
Question Areas:
■ Storm Water
(See attachment summary)
Page: 1

Permit: NCG030459 Owner - Facility: Council Tool Company
Inspection Date: 01/30/2008 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
This facility is located on three corners, at the intersection of Pecan Lane and Oak Street. It consists of a small office
building, a small shipping warehouse and a manufacturing building on the three seperate corners. There were no
problems noted during the inspection of this facility. There was no stormwater discharge during the inspection. The only
issue noted was the lack of employee training documentation. While employees are informed of stormwater impacts, there
was no record. In the future, please record dates of training, listing those present.
Page: 2

Permit: NCG030459 Owner - Facility: Council Tool Company
Inspection Date: 01/30/2008 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Stormwater Pollution Prevention Plan Yes No NA NE
Does the site have a Stormwater Pollution Prevention Plan?
■
❑
❑ ❑
# Does the Plan include a General Location (USGS) map?
■
❑
❑
❑
# Does the Plan include a "Narrative Description of Practices"?
■
❑
Cl
❑
# Does the Plan include a detailed site map including outfall locations and drainage areas?
■
0
❑
❑
# Does the Plan include a list of significant spills occurring during the past 3 years?
■
❑
❑
❑
# Has the facility evaluated feasible alternatives to current practices?
■
❑
❑
❑
# Does the facility provide all necessary secondary containment?
■
❑
❑
❑
# Does the Plan include a BMP summary?
■
❑
❑
❑
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
■
❑
❑
❑
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
■
❑
❑
❑
# Does the facility provide and document Employee Training?
❑
■
❑
❑
# Does the Plan include a list of Responsible Party(s)?
■
❑
❑
❑
# Is the Plan reviewed and updated annually?
■
❑
❑
❑
# Does the Plan include a Stormwater Facility Inspection Program?
■
❑
❑
❑
Has the Stormwater Pollution Prevention Plan been implemented?
■
❑
❑
❑
Comment:
Qualitative Monitoring
Yes
No
NA
NE
Has the facility conducted its Qualitative Monitoring semi-annually?
■
❑
❑
❑
Comment:
Analytical Monitoring
Yes
No
NA
NE
Has the facility conducted its Analytical monitoring?
■
❑
❑
❑
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
■
❑
❑
❑
Comment:
Permit and Outfails
Yes
No
NA
NE
# Is a copy of the Permit and the Certificate of Coverage available at the site?
■
❑
❑
❑
# Were all outfalls observed during the inspection?
■
❑
❑
❑
# If the facility has representative outfall status, is it properly documented by the Division?
■
❑
❑
❑
# Has the facility evaluated all illicit (non stormwater) discharges?
■
❑
❑
❑
Comment:
Page: 3

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
August 23, 2002
VELTON JACOBS
COUNCIL TOOL COMPANY
POST OFFICE BOX 165
LAKE WACCAMAW, NC 28450
Subject: NPDES Stormwater Permit Renewal
COUNCIL TOOL COMPANY
COC Number NCG030459
Columbus County
Dear Permittee:
In response to your renewal application for continued coverage under general permit NCG030000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983.
The following information is included with your permit package:
* A new Certificate of Coverage
* A copy of General Stormwater Permit NCG030000
* A copy of the Analytical Monitoring Form (DMR)
* A copy of a Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or
decree -
If you have any questions regarding this permit package please contact Mack Wiggins of the Central Office
Stormwater and General Permits Unit at [phone], ext. 542
Sincerely,
Bradley Bennett. Supervisor
Stormwater and General Permits Unit
cc: Central Files
Stormwater & General Permits Unit Files
Wilmington Regional Office
TA
NCDENR
N. C. DiOsion of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030459
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
COUNCIL TOOL COMPANY
is hereby authorized to discharge stormwater from a facility located at
COUNCIL 'FOOL COMPANY
345 PECAN LN
LAKE WACCAMAW
COLUMBUS COUNTY
to receiving; waters designated as Lake Waccamaw, a class B SW stream, in the Lumber River Basin in accordance
with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II,1I1, IV, V, and VI
of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective September 1, 2002.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day August 23, 2002.
for Alan W. Klimek, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

State of North Carolina
Department of Environment [ITIt-1—,:- •
and Natural Resources L L_
Division of Water Quality #
71 JUN 2 5 2002
Michael F. Easley, Governor U
INCDENR
William G. Ross Jr., Secretary ---_______________________--
Alan W. Klimek, P.E. Director NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
06/06/2002
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
ATTN: ROY ROBINSON
THE COUNCIL TOOL CO.
POST OFFICE BOX 165
LAKE WACCAMAW, NC 28450
Subject: NOTICE OF VIOLATION
FAILURE TO SUBMIT RENEWAL APPLICATION
THE COUNCIL TOOL CO.
NCG030000
COC NUMBER NCG030459
COLUMBUS COUNTY
Dear Permittee:
This letter is to inform you that, as of the date of this letter, the Division of Water Quality has not received a
renewal request for the subject permit certificate of coverage. This is a violation of NCGS § 143.215.1 (c)(1) which
states "All applications shall be filed with the commission at least 180 days in advance of the date on which it is
desired to commence the discharge of wastes or the date on which an existing permit expires, as the case may be".
Any permittee that has not requested renewal at least 180 days prior to expiration or permittee that does not have a
permit after the expiration and has not requested renewal at least 180 days prior to expiration, will be subjected to
enforcement procedures as provided in NCGS § 143-215.6 and 33 USC 1251 et. seq.
In order to prevent continued, escalated action, including the assessment of civil penalties you must submit a
completed permit coverage renewal application to the attention of the "Stormwater and General Permits Unit" at
the letterhead address within ten (10) days of your receipt of this letter (renewal application enclosed). If the
subject discharge has been terminated, please complete the enclosed rescission request form. Mailing instructions
are listed on the bottom of the form. You will be notified when the rescission process has been completed.
Thank you for your prompt attention to this situation. If you have any questions regarding this matter, please
contact Mack Wiggins of the central office Stormwater and General Permits Unit at 919-733-5083, ext. 542.
Sincerely,
for Alan W. Klimek, P.E.
Director, Division of Water Quality
cc: Stormwater and General Permits Unit Files
Central Files
Wilmington Regional Office
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

ROY ROWNSON
COUNCIL TOOL COMPANY
POST OFFICE BOX 165
LAKE WACCAMAW, NC 28450
Dear Permittec:
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Gregory J. Thorpe, Ph.D.
Acting Director
� f Divisio of Water Quality
December 27, 2001 APR 10 2002
---------------------
Subject: NPDES Stormwater Permit Renewal
COUNCIL `POOL COMPANY
COC Number NCG030459
Columbus County
Your facility is currently covered for stormwater discharge under General Permit NCG030000, This permit expires
on August 31, 2002. The Division staff is currently in the process of rewriting this permit and is scheduled to have
the permit reissued by late summer of 2002. Once the permit is reissued, your facility would be eligible for
continued coverage under the reissued permit.
In order to assure your continued coverage under the general permit, you must apply to the Division of Water
Quality (DWQ) for renewal of your permit coverage. To make this renewal process easier, we are informing you in
advance that your permit will be expiring. Enclosed you will find a Ceneral Permit Coverage Renewal
Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued
coverage under the general permit.
Failure to request renewal within this time period may result in a civil assessment of at least $250.00. Larger
penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility
without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and
could result in assessments of civil penalties of up to $10,000 per day.
Please note that recent federal legislation has extended the "no exposure exclusion" to all operators of industrial
facilities in any of the l l categories of "storm water discharges associated with industrial activity," (except
construction activities). If you feel your facility can certify a condition of "no exposure", i.e. the facilty industrial
materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional
information contact the Central Office Stormwater Staff member listed below or check the Stormwater & General
Permits Unit Web Site at http://h2o.enr.state.ne.us/su/stormwater,11tniI
If the subject storm water discharge to waters of the state has been terminated, please complete the enclosed
Rescission Recluest Form. Mailing instructions are listed on the botlom of the form. You will be notified when the
rescission process has been completed.
If you have any questions regarding the permit renewal procedures please contact Ed Beck of the Wilmington
Regional Office at 910-395-3900 or Bill Mills of the Central Office Stormwater Unit at [phone], ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Wilmington Regional Office
A��
NCDENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Gregory J. Thorpe, Ph.D.
Acting Director
Division of Water Quality
December 27, 2001
ROY ROBINSON
COUNCIL TOOL COMPANY
POSTOFFICE. BOX 165
LAKE WACCAMAW, NC 29450
Subject: NPDES Stormwater Permit Renewal
COUNCIL TOOL COMPANY
COC Number NCG030459
Columbus County
Dear Permittce:
Your facility is currently covered for stormwater discharge under General Permit NCG030000. This permit expires
on August 31, 2002. The Division staff is currently in the process of rewriting this permit and is scheduled to have
the permit reissued by late summer of 2002. Once the permit is reissued, your facility would be eligible for
continued coverage under the reissued permit.
In order to assure your continued coverage under the general permit, you must apply to the Division of Water
Quality (DWQ) for renewal of your permit coverage. To make this renewal process easier, we are informing you in
advance that your permit will be expiring. Enclosed you will find a General Permit Coverage Renewal
Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued
coverage under the general permit.
Failure to reducst renewal within this time period may result in a civil assessment of at least $250.00. Larger
penalties may he assessed depending on the delinquency of the request. Discharge of stormwater from your facility
without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and
could result in assessments of civil penalties of up to $10,000 per day.
Please note that recent federal legislation has extended the "no exposure exclusion" to all operators of industrial
13tcilitics in any of the 1 1 categories of "storm water, discharges associated with industrial activity," (except
construction activities). If you feel your facility can certify a condition of "no exposure", i.e. the facilty industrial
materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional
information contact the Central Office Stormwater Staff member listed below or check the Stormwater & General
Permits Unit Web Site at htip:l/h2o.ertr.state.nc.us/su/stormwatei'.Iitntl
If the sul?ject stormwater discharge to waters of the state has been terminated, please complete the enclosed
Rescission Request Form. Mailing instructions are listed on the bottom of the form. You will be notified when the
rescission process has been completed.
If you have any questions regarding the permit renewal procedures please contact Ed Beck of the Wilmington
Regional Office at 910-395-3900 or Bill Mills of the Central Office Stormwater Unit at [phone], ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Filcs
Wilmington Regional Office
M NA,
NCDERR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

IN =
State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
Kerr T. Stevens, Director
Mr. Roy Robinson
The Council Tool Co.
Post Office Box 165
Lake Waccamaw, North Carolina 28450
Dear Mr. Robinson:
NCDENR
September 3, 1999
Subject: General Permit No. NCG030000
The Council Tool Co.
COC NCG030459
Columbus County
In accordance with your application for discharge permit received on June 30, 1999, we are forwarding
herewith the subject certificate of coverage to discharge under the subject state - NPDES general permit. This
permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .I and the Memorandum
of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division of
Water Quality. The Division of Water Quality may require modification or revocation and reissuance of the
certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act
or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Darren England at telephone number
919/733-5083 ext. 545.
Sincerely,
ORIGINAL SIGNED BY
WILLIAM C. MILLS
Kerr T. Stevens
cc: Wilmington Regional Office
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030459
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
THE COUNCIL TOOL CO.
is hereby authorized to discharge stormwater from a facility located at
THE COUNCIL TOOL CO.
345 PECAN LANE
LAKE WACCAMAW
COLUMBUS COUNTY
to receiving waters designated as Lake Waccamaw in the Lumber River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, 111,
IV, V, and VI of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective September 3, 1999.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day September 3, 1999.
ORIGINAL SIGNED BY
WILLIAM
for Kerr T. Stevens, Director
Division of Water Quality
By Authority of the Environmental Management Commission

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Facility:
Map ID
Latitude: 34G 1Q, d,g"
Longitude: '7,5° 3� j' 40••

I
FACILITY -z ",
COUNTY
NPDE5
.x
MAC' 2 5 C,J
OSN FLOW 1,11A
SUE BASIN
LAT'T TUOE
5
nt v2 WD E 7B
Ri vE VINE STREAM �_A„CA.r &JA eLAr- AL-3
STRWM CLASS /S 5
DISUCd' ARG,Ut' CtASS Z5 -vr-�